WQ0024508_Monitoring - 11-2021_20211213

Monitoring Report Submittal
Permit Number #*
Name of Facility:*
Month: * November
Report Information
Type *
GW-59
WQ00024508
Carolina Research Center
Confirmation Email Address: *
Name of Submitter: *
Signature:
Date of submittal:
Initial Review
Year:* 2021
Upload Document*
Carolina Research Center 3.11 MB
GW59.pdf
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
[e-mail]
[e-mail]
Reviewer: Zhong, Vivien
12/13/2021
This will be filled in automatically

Is the project number correct?* WQ00024508
Is the monitoring report accepted?* Yes No
Regional Office* Winston-Salem
Accepted Date: 12/20/2021

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NG 27699-1617
FACILITY INFORMATION
PleasePnntClearly orType
PERMIT Number: WQ0024508 Expiration Date: A rif 30, 2024
Facility Name: Carolina Research Cener
Non -Discharge UIC
NPDES Other
Permit Name (if different): Snlithers Viscient LLC
Facility Address: 2900 uakenbush Road
TYPE OF PERMITTED OPERATION BEING MONITORED
Snow Cam scr Ali NC
p
27349
Count Alamance
y
El Lagoon El Remediation: Infiltration Gallery
tC itf! (Stile)
(,-,PJ
❑ Spray Field El Remediation:
Contact Person: Gus Zieske
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled: 3
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-I
Date sample collected:
FIELD ANALYSES:
WAS
Well Depth: 35.00ft.
Well Diameter:
in.
pH 00400: units Temp. 00010: °C
DRY at
Depth to Water Level 82546: ft. below measuring point
Screened Interval:
ft, to
ft. Spec. Cond. 00094: µMhos
time ofsampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling:
gallons
Appearance
here:®
Samples for metals were collected unfiltered: ❑■ YES ❑
NO and field acidified: ❑■ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name:
Certification No.
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg1L
Nitrite (NOZ) as N 00615
mglL
Pb - Lead o1o51 uglL
Coliform: MF Fecal 31616
1100mL
Nitrate (NO3) as N 00620
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
M00mL Phosphorus:
Total as P 00665
mglL
(Note: use MPN method for highly turbid samples)
Orthophosphate 70507
mglL
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300
mglL
Al - Aiuminum 01105
mglL
pH (Lab) 00403
units
Ba - Barium 01007
uglL
TOC 00680
mg1L
Ca - Calcium oo916
mg1L
Chloride 00940
mglL
Cd - Cadmium 01027
ug1L
Arsenic 01002
ug1L
Chromium: Total o1o34
uglL
Grease and Oils 00552
mglL
Cu - Copper 01042
ri
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
uglL
Fe - Iron 01045
uglL
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mglL
Hg - Mercury 71900
uglL
Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 00095
pMhos
K - Potassium 00937
mglL
VOC 7873 method #
Total Ammonia 00610
mglL
Mg - Magnesium 00927
mglL
method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen. Total)
Mn - Manganese o1o55
ug/L
, method #
TKN as N 00625
mg1L
Ni - Nickel 01067
uglL
method #
For Remediation Systems Onfy (Attach Lab Reports): Influent Total VOCs: mg1L Effluent Total VOCs: mg1L VOC Removal%
1-?-1rvn IVG- ( GVL`-c
Permittee (cr Authorized Aqent) Name and Title - Please print or type
Signature of Permiltee (or
GW-59 Rev.06-07-2018

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENTAL QUALITY -DIV, OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: WQ0024508 Expiration Date: A 1ri[ 30, 2024
Faciiity Name: Caroliml Research Center
Non -Discharge UIC
NPDES Other
Permit Name (if different): Smilhers Viscient, LLC
Facility Address: 2900 Quakcnbush load
TYPE OF PERMITTED OPERATION BEING MONITORED
Snow Camp NC
27349 County Alanlance
❑ Lagoon ❑ Remediation: Infiltration Gallery
(rAv) fsvl,)
(G.rl)
❑ Spray Field ❑Remedlation:
Contact Person: Gus Zieske
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
3
❑ Water Source Heat Pump ❑ Other:
(from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-2
Date sample collected: 11/23/2021
FIELD ANALYSES:
WAS
Well Depth: 15.40t.
Well Diameter:
in.
pH 0040M -5.69 units Temp. 00010: 11.8 °C
DRY at
Depth to Water Level 82546: 14.46 ft. below measuring point
Screened Interval:
ft. to ---
ft. Spec. Cond. 00094: pMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling:
__ 0,5
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X YES
❑ NO and field acidified: ❑■. YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 1 1/23-12/07/2021
Laboratory Name: face Analytical Services Certification No. 12, 40 & 633
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mglL
Nitrite (NO2) as N 00615
mg1L
Pb - Lead o1o51 uglL
Coliform: MF Fecal 31616 <1.0
1100mL
Nitrate (NO3) as N 00620 0.55
mglL
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
1100mL
Phosphorus: Total as P 00665 1.6
mglL
(Note: use MPN method for highly turbid samples)
Orthophosphate 70507
mg1L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 82.0
mglL
At - Aluminum 01105
mglL
pH (Lab) 00403
units
Ba - Barium 01007
uglL
TOC 00680 <1.11
mglL
Ca - Calcium oog16
mglL
Chloride 00940 3.5
mg1L
Cd - Cadmium 01027
uglL
Arsenic 01002
uglL
Chromium: Total 01034
uglL
Grease and Oils 00552
mg1L
Cu - Copper 01042
mglL
ORGANICS: (by GC, GCIMS, HPLC)
Phenol 32730
ug1L
Fe - Iron 01045
uglL
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mglL
Hg - Mercury 71900
uglL
Lab Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance Doom
pMhos
K - Potassium 00937
mg1L
VOC 7873 method # 8260
Total Ammonia 00610 <0.10
mglL
Mg - Magnesium 00927
mglL
method #
(Ammonia Nitrogen, NH, as N: Ammonia Nitrogen, Tolal}
Mn - Manganese oims
uglL
, method #
TKN as N 00625
mglL
Ni - Nickel 01067
uglL
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs
_C
Name and Title - Please print or Lype
Totalmg/L Effluent
1plete, and that the laboratory analytical data
possibility of fines and Imprisonment for knt
.y s
mglL VOC Removal%
1-13-11
(Dale)
GW-59 Rev.06-07-2018

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
INK
DEPARTMENT OF ENVIRONMENTAL QUALITY - HIV. OF WATER RESOURCES
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number;WQ042455 Expiration Date: April 30, 2024
Facility Name: Carolina Rescarach Centcr
Non -Discharge UIC
NPDES Other
Permit Name (if different): Smithers Viscient, LLC
Facility Address: 2900 Quakenbush Road
TYPE OF PERMITTED OPERATION BEING MONITORED
STIow Cam " NC
27349
County Alanrulce
❑ Lagoon ❑ Remediation: Infiltration Gallery
I',Xi, (3I:l1H)
❑ Spray Field ❑Remediation:
Contact Person: Gus Zieske
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
3
❑ Water Source Heat Pump ❑ Other:
f From Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-3
Date sample collected: 1 7/23/2021
FIELD ANALYSES:
WAS
Well Depth: l ( Soft.
Well Diameter:
in.
pH 00400: 5.95 units Temp. coolo: 1 1.7 Cr
DRY at
Depth to Water Level B2546: 7.81 ft. below measuring point
Screened Interval:
ft. to
ft. Spec. Cond. 00094: umhos
time of
sampling,check
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor eooss:
Volume of water pumped/bailed before sampling:
2
gallons
Appearance
here:
❑
Samples for metals were collected unfiltered: K YES El
NO and field acidified: 0 YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 1 1/23-12/07/202 t
Laboratory Name: Pace Analytical Services Certification No. 12,40 & 633
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00336
rngtt-
Nitrite (NO2) as N ooe15
mg/L
Pb - Lead o1o51 ugJL
Coliform: MF Fecal 31616 <1 0
1100mL
Nitrate (NO.) as N 00620 <p 20
mg/L
Zn - Zinc 01092 mg1L
Coliform: MF Total 31504
MCOmL Phosphorus:
Total as P oc6a5 2.1
mg/L
(Note: use MPN method ror highly turbid samples)
Orthophosphate 70507
mg1L
Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 69.2
mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ugJL
TOC oeeeo 1 • I
mg/L
Ca - Calcium eog16
mglL
Chloride 0094o 4.0
mg/L
Cd - Cadmium 01027
ugJL
Arsenic 01002
ugJL
Chromium: Total 01034
ug1L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ugJL
Fe - Iron 01045
ugJL
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ugJL
Lab Report Attached? © Yes (1) ❑ No (0)
Specific Conductance Boom
ptMhos
K - Potassium o0e37
mg/L
VOC 7873 method # 5260
Total Ammonia co6lo <0.10
mg/L
Mg - Magnesium 00927
mglL
method #
(Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total)
Mn - Manganese Ot055
ug/L
, method #
TKN as N 00625
ni
Ni - Nickel 01067
ugJL
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg1 Effluent Total VOCs: mg/L VOC Rerri
I certify that,'. to the hest of my knowledgeandbelief, theInformation submitted in this report Is true; accurate; and complete, and that the laboratory analytical data: was produced using approved methods of analysis by a
l7WR-certlfied'labaratory..' f am aware that there are significant penalties for submitting false Information; Including the possibility ortines.and-lmprisonment for knowing violations.
L
Permittee (or Authorized Apent) Name and TItle - Please print or type Signature of Permiftee (or Authorized)=
GW-59 Rev.06-07-2018

aceAnalytical®
www.pacelahs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carolina Research MWIEff
Pace Project No.: 92574016
Sample: MW-2 Lab ID: 92574016001 Collected: 11/23/21 10:15 Received: 11/23/21 12:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed GAS No. Qual
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2015
Pace Analytical Services - Eden
Total Dissolved Solids
82.0 mg/L
25.0
1
11/30/21 13:42
350.1 Ammonia EDN
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, Ammonia
ND mg/L
0.10
1
11/23/21 14:56
7664-41-7
353.2 N021NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, Nitrate
0.55 mg1L
0.040
1
11/23/21 17:03
14797-55-8
MB10 9222D Fecal Coliform EDN
Analytical Method: SM 92221D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Eden
Fecal Coliforms
ND CFU1100 mL
1.0
1 11/23/21 14:18
11/24/21 12:35
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND ug/L
25.0
1
12103/2110:05
67-64-1
Benzene
ND ug/L
1.0
1
12103/2110:05
71-43-2
Bromobenzene
ND ug/L
1.0
1
1210312110:05
108-86-1
Bromochloromethane
ND ug/L
1.0
1
12103/2110:05
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
12103/2110:05
75-27-4
Bromoform
ND ug/L
1.0
1
12103/2110:05
75-25-2
Bromomethane
ND ug/L
2.0
1
12/03/2110:05
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
12/03/21 10:05
78-93-3
Carbon tetrachloride
ND ug/L
1.0
1
12/03/21 10:05
56-23-5
Chlorobenzene
ND ug/L
1.0
1
12103/2110:05
108-90-7
Chloroethane
ND ug/L
1.0
1
12103/2110:05
75-00-3
Chloroform
ND ug/L
1.0
1
12103/2110:05
67-66-3
Chloromethane
ND ug/L
1.0
1
12/03/2110:05
74-87-3
2-Chiorotoluene
ND ug/L
1.0
1
12/03/2110:05
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
12/03/2110:05
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
2.0
1
12/03/2110:05
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
12/03/2110:05
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
12/03/21 10:05
106-93-4
Dibromomethane
ND ug/L
1.0
1
12/0312110:05
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
1
12/03/2110:05
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
12/0312110:05
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
12/0312110:05
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
12/03/21 10:05
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
1
1210312110:05
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
12/0312110:05
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
12/0312110:05
75-35-4
cis- 1,2-D ichloroethen e
ND ug/L
1.0
1
12/031211Q05
156-59-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
12/0312110:05
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
12/0312110:05
78-87-5
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2021 04:33 PM
without the written consent of Pace Analytical Services, LLC.
Page 4 of 34

ace Analytical a,
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvide, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carolina Research MW/Eff
Pace Project No.: 92574016
Sample: MW-2 Lab ID: 92574016001 Collected: 11/23)21 10:15 Received: 11/23/21 12:40 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis- 1,3-Dichloropropene
trans- 1,3-Dichloropro pene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroetha ne
1,1,2,2-Tetrachloroethane
Tetra chloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Tri chlo roethane
1,1,2-Tri chlo roethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
300.0 IC Anions 28 Days
Chloride
365.1 Phosphorus, Total
Phosphorus
Date: 12/09/2021 04:33 PM
Analytical Method: EPA 8260D
Pace Analytical
Services -Charlotte
ND
ug1L
1.0
1
12/03/21 10:05
142-28-9
ND
ug1L
1.0
1
12/03/21 10:05
594-20-7
NO
ug1L
1.0
1
12/03/21 10:05
563-58-6
ND
ug1L
1.0
1
12/03/2110;05
10061-01-5
ND
ug/L
1.0
1
12/0312110:05
10061-02-6
ND
ug1L
1.0
1
12/03/21 10:05
108-20-3
ND
ug1L
1.0
1
12/0312110:05
100-41-4
ND
ug1L
2.0
1
12/03/21 10:05
87-68-3
ND
ug1L
5.0
1
12/03/2110:05
591-78-6
ND
ug/L
1.0
1
12/03/2110A5
99-87-6
ND
uglL
5.0
1
12/03/21 10:05
75-09-2
NO
ug/L
5.0
1
12/03/2110!05
108-10-1
NO
ug/L
1.0
1
12103/2110!05
1634-04-4
NO
ug/L
1.0
1
12/03/21 10:05
91-20-3
ND
ug/L
1.0
1
12/0312110:05
100-42-5
ND
ug/L
1.0
1
12/03/21 10:05
630-20-6
ND
ug/L
1.0
1
12/03/21 10:05
79-34-5
NO
ug/L
1.0
1
12/0312110:05
127-18-4
NO
ug/L
1.0
1
12/0312110:05
108-88-3
NO
ug/L
1.0
1
12/0312110:05
87-61-6
ND
ug/L
1.0
1
12/0312110:05
120-82-1
ND
ug/L
1.0
1
12/0312110:05
71-55-6
ND
ug/L
1.0
1
1210312110:05
79-00-5
ND
ug/L
1.0
1
12/0312110:05
79-01-6
ND
ug/L
1.0
1
12/0312110:05
75-69-4
ND
ug/L
1.0
1
1210312110:05
96-18-4
ND
ug/L
2.0
1
12/03/21 10:05
108-05-4
ND
ug/L
1.0
1
12/03/21 10:05
75-01-4
ND
ug/L
1.0
1
12/03/21 10:05
1330-20-7
ND
ug/L
2.0
1
12/03/21 10:05
179601-23-1
ND
ug/L
1.0
1
12103/2110:05
95-47-6
98
%
70-130
1
12/03/21 10:05
460-00-4
98
%
70-130
1
12103/2110:05
17060-07-0
100
%
70-130
1
12/03/21 10:05
2037-26-5
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
3.5 mg/L 1.0 1 11126/2117:43 16887-00-6
Analytical Method: EPA 365.1 Rev 2,0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
1.6 mg/L 0.050 1 12106/2122:17 12107/2117:27 7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 34

,�aceAnayical*
www.pacalabs.com
ANALYTICAL RESULTS
Project: Carolina Research MW1Eff
Pace Project No.: 92574016
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Nuntersville, NC 28078
[phone]
Sample: MW-2 Lab ID: 92574016001 Collected: 11/23/21 10:15 Received: 11/23/21 12:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5310B TOC Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon ND mg1L 1.0 1 12/05/21 16:14 7440-44-0
Date: 12/09/2021 04:33 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 34

c;
�aceAnalyticaI
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carolina Research MW/Eff
Pace Project No.: 92574016
Sample: MW 3 Lab ID: 92574016002 Collected: 11/23/21 09:35 Received: 11/23/21 12:40 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Qual
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2015
Pace Analytical Services - Eden
Total Dissolved Solids
69.2 mg1L
38.5
1
11/30/21 13:42
350.1 Ammonia EDN
Analytical Method: EPA 350.1 Rev 2.0
1993
Pace Analytical Services - Eden
Nitrogen, Ammonia
ND mg1L
0.10
1
11/23/21 14:58
7664-41-7
353.2 N021NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services - Eden
Nitrogen, Nitrate
ND mg/L
0.20
5
11/23/21 17:17
14797-55-8
MB10 9222D Fecal Coiiform EDN
Analytical Method: SM 9222D-2015 Preparation
Method: SM 9222D-2015
Pace Analytical Services - Eden
Fecal Coliforms
ND CFU1100 mL
1.0
1
11/23/21 14:18 11/24/21 12:35
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND ug/L
25.0
1
12/0312110:23
67-64-1
Benzene
ND ug/L
1.0
1
12/0312110:23
71-43-2
Bromobenzene
ND ug/L
1.0
1
12/0312110:23
108-86-1
Bromochloromethane
ND ug/L
1.0
1
12/0312110:23
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
12/0312110:23
75-27-4
Bromoform
ND ug/L
1.0
1
12/0312110:23
75-25-2
Bromomethane
ND ug/L
2.0
1
12/03/21 10:23
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
12/03/21 10:23
78-93-3
Carbon tetrachloride
NO ug/L
1.0
1
12/03/21 10:23
56-23-5
Chlorobenzene
N❑ ug/L
1.0
1
12/03/21 10:23
108-90-7
Chloroethane
ND ug/L
1.0
1
12/03/21 10:23
75-00-3
Chloroform
ND ug/L
1.0
1
12/03/21 10:23
67-66-3
Chioromethane
ND ug/L
1.0
1
12103/2110:23
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
12103/2110:23
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
12103/2110:23
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
2.0
1
12103/2110:23
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
12103/2110:23
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
12/03/21 10:23
106-93-4
Dibromomethane
ND ug/L
1.0
1
12/03/21 10:23
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
1
12/03/21 10:23
95-50-1
1,3-Dichlorobenzene
NO ug/L
1.0
1
12/03/21 10:23
541-73-1
1,4-Dichlorobenzene
NO ug/L
1.0
1
12/0312110:23
106-46-7
Dichlorodifluoromethane
NO ug/L
1.0
1
12/03/21 10:23
75-71-8
1,1-Dichloroethane
NO ug/L
1.0
1
12/0312110:23
75-34-3
1,2-Dichloroethane
NO ug/L
1.0
1
12/0312110:23
107-06-2
1,1-Dichloroethene
NO ug/L
1.0
1
12/0312110:23
75-35-4
cis- 1,2-Dich loroethene
NO ug/L
1.0
1
12/0312110!23
156-59-2
trans-1,2-Dichloroethene
NO ug1L
1.0
1
12/0312110:23
156-60-5
1,2-Dichioropropane
NO ug1L
1.0
1
12/0312110:23
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2021 04:33 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 34

,�aceAnalyfical'�!
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ANALYTICAL RESULTS
Project: Carolina Research MWIEff
Pace Project No.: 92574016
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-3 Lab ID: 92574016002 Collected: 11/23/21 09:35 Received: 11/23/21 12:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIRK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1, 2-Tetrachioroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1. 1. 1 -Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Tri chlorofluoromethan e
1,2,3-Tri chloropropa ne
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xyl ene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
300.0 IC Anions 28 Days
Chloride
365.1 Phosphorus, Total
Phosphorus
Date: 12/09/2021 04:33 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
1.0
1
12/0312110:23
142-28-9
ND
ug/L
1.0
1
12/0312110:23
594-20-7
ND
ug/L
1.0
1
12/0312110:23
563-58-6
ND
ug/L
1.0
1
12/0312110:23
10061-01-5
ND
ug/L
1.0
1
1210312110:23
10061-02-6
ND
ug/L
1.0
1
12/0312110:23
108-20-3
ND
ug/L
1.0
1
1210312110:23
100-41-4
ND
ug/L
2.0
1
1210312110:23
87-68-3
ND
ug/L
5.0
1
12/03/21 10:23
591-78-6
ND
ug/L
1.0
1
12/03/21 10:23
99-87-6
ND
ug/L
5.0
1
1210312110:23
75-09-2
ND
ug/L
5.0
1
1210312110:23
108-10-1
ND
ug/L
1.0
1
12/0312110:23
1634-04-4
ND
ug/L
1.0
1
12/0312110:23
91-20-3
ND
ug/L
1.0
1
12/0312110:23
100-42-5
N❑
ug/L
1.0
1
12/03/21 10:23
630-20-6
ND
ug/L
1.0
1
12/0312110:23
79-34-5
ND
ug/L
1.0
1
12/0312110:23
127-18-4
ND
ug/L
1.0
1
12103/2110:23
108-88-3
ND
ug/L
1.0
1
12/03/21 10!23
87-61-6
ND
ug/L
1.0
1
12/0312110:23
120-82-1
ND
ug/L
1.0
1
12/0312110!23
71-55-6
ND
ug/L
1.0
1
12/0312110:23
79-00-5
ND
ug/L
1.0
1
12/0312110:23
79-01-6
ND
ug/L
1.0
1
12/0312110:23
75-69-4
ND
ug/L
1.0
1
12/03/2110:23
96-18-4
ND
ug/L
2.0
1
12/03/2110:23
108-05-4
ND
ug/L
1.0
1
12/03/2110:23
75-01-4
ND
ug/L
1.0
1
12/03/2110:23
1330-20-7
ND
ug/L
2.0
1
12/03/2110:23
179601-23-1
ND
ug/L
1.0
1
12/03/2110:23
95-47-6
97
%
70-130
1
12/03/21 10:23
460-00-4
99
%
70-130
1
12/03/2110:23
17060-07-0
101
%
70-130
1
12/03/21 10:23
2037-26-5
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
4.0 mg1L 1.0 1 11/26/2117:59 16887-00-6
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
2.1 mg1L 0.050 1 12/06/21 22:17 12/07/2117:28 7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 34

laceAnaoical
www.pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Carolina Research MWIEff
Pace Project No.: 92574016
Sample: MW-3 Lab ID: 92574016002 Collected: 11/23/21 09:35 Received: 11/23/21 12:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
531013 TOG Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon 1.1 mg/L 1.0 1 12/05/21 16:29 7440-44-0
Date: 12/09/2021 04:33 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 34