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HomeMy WebLinkAboutWQ0004972_Monitoring - 10-2021_20211130Monitoring Report Submittal Permit Number #* Name of Facility:* Month: * October Report Information WQ0004972 Forest Lakes Preserve ELS Type * NDMR, NDAR-1, NDAR-2, NDMLR Confirmation Email Address:* Name of Submitter: * Signature: Date of submittal: Initial Review Year:* 2021 Upload Document* Forest Lakes_Nov.pdf 2.12MB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Jessica.Mize@pacelabs.com Jessica Mize jwd rA lip Reviewer: Zhong, Vivien 11 /30/2021 This will be filled in automatically Is the project number correct?* WQ0004972 Is the monitoring report accepted?* Yes No Regional Office* Winston-Salem Accepted Date: 12/10/2021 Page of 2 NON -DISCHARGE WAS'FE WATER MONITORING REPORT PERM11'NUMBER: WQ0004972 MONI'll, October YEAR: 2021 FACILITY NAME: Forest Lakes Preserve ELS COUNTY: Davie. Flow Monitoring Point:, Effluent: Influent: Parameter Monitoring Point Effluent: - LIV Surface Water SW: SW Code/Name: Was There Effluent Flow for this Month Generated At Thor Facky: Yes: No: flpuraYae 50050 00400 1 5OD60 00310 CC610 00530 31616 0066 25 00630 - 00600 - _�0620 _LUI Go 00940 Arnval Daily Ralo Fecal i 10W A Time operator ORC (Flow) into cofifi I Iwal T,mal Nitiaw D,,wlved 11, 24DO TlMo on LOR on Treatment R.idual BOD-5 TwM Kj6RA Mmg- NO2,1,03 Nimgo, NO3-N "Ad, Chl d, E e7 SAV S�mcrrl 1,11 - -.7 00 ir. ------ 20 V NH,3,N ISS McW) Pho, m NMT Niti'l %1GA, MUL --- �, �Tj 11, YN y N GvD - I- NF;T- NIG/L -Vo-,,tTTy- -3fy..r M,turawo,nos -7, -,A mk M,A mml,ly Nlmthly 1,1,0hly Wmady MoM 7"r rimtMy m"'1111 09,,54- 2 40 77 7= h", A 2 7, 7777q, 77777 77777777 4 5 4 753 0744 11,25 y 8,0110 --7- 000 6.9 777U7777, 77-- <10 W77, =77""'77,7" 77777 6 1317 015 B 8,000 66 <10 7 '140 0125 y/,,1,,,' A 4n/ 6 6. , o 0 'I���",�,""I"""",�,,I�f",;", 777777 77777 777 8 104M8 1048 IL25 y 8,000 1 6.5 <10 --7 - 77- 777777 8,00111 7 1536 1530, 1 71,077, 72, '77 77777 ""777"""', - i z 7- 320 (1,25 8,000 6.2 <11) 7- 73 �777177,,,�,7 7 7 14 1155 0.25 B 8,0011 6A <141, 77777777,77, '75 777- 7,777,777,777 -7,777,77 1 16 8,000 <10 Is 0920 0.25 y 8,000 63 I [20 77j5', 1120 0.25 y 8,0(10 C, <10 -7777777 7-7 7 777� it 75 11, 77,17" 7775i7 ­77 , , "77,77",=7 Z2 0955 7777711'', 0.25 B 8,000 6.5 ---va, <10 -77 77- -7- 77, --777/- 7 7=7-7/111-11/71-717111 7 11 24 75 8,000 777�7 IEEE 7 777 T77777= 7 26 1515 0.25 8,000 6.6 <10 77777777 777, 77 77 7`0-1 7 11 1 77,7777 7_7 �777!77,7,7,777' 7 2S 11 1340 015 B 8,000 6.4 <10 2.5 0.26 7,2 2420 3.0 12.0 15.0 12.7 000 "717777 777-77,777" '7 8,04)0 7 777777 77" 7, 7/77 ­726 7,7777, 7 Averattv 8,000 <10 7.2 2420 2.5 3.0 11.0 -T A Daily Maximum $,Ilff 0 6.9 <10 2•j 0,26 7.2 2420 10 3.0 Daily N1111111tuin 811.1041 6.2 <10 2.5 0.26 7.2 2420 2,0 3.0 1 12.0 ISM 12.7 Monthly I'latils (S) 24400 . Composlic v G rah (G) Flow Meter Estimated , Flow Meter inoperable Opvralor in Rcsponsible Charge (ORC): Cloon]"rick Grade: 11 Phone: 33k-996-2841 - Check Box if ORC Has Changed: 1-1 ORC Certification Number- 987911/20771 Certified Laboratories (1): Pace Analytical Serivces,- (2): . Person(s) Collecting Samples: Glenn Price Mail ORIGINAL and Two COPIES to, ........ . A'I,rN: Non -Discharge Compliance Unit 1) EN R (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) IANIslon of Water Quality I)y tbLs signature, I certify that this report Is accurate and 1617 Mail Service Center of) 1"plete to the best of illy knovvledgc. RALEIGH, NC 27699-1617 NON DISCHARGE WASTEWATER MONITORING REPORT FACILITY STATUS: Please answer the following question: 1. Does all monitoring data and sampling frequencies meet permit requirements? If the facility is non-complignt, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. * Flow Meter ingperable Flow Estimated Com liant Y,N) "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permitee)* Date Baron Neal McDuffie (Authorized Agent) (Permittee-Please print or type) 2N Riverside Plaza . Suite 800 Chicago, Il 60606 (Permittee Address) . 01002 Arsenic 01022 Boron - 00310 BOD5 01027 Cadmium 00916 Calcium 00940 Chloride 50060 Chlorine, Total Residual 01034 Chromium 00340 COD 31504 Coliform, Total 00094 Conductivity 01042 Copper 00300 Dissolved Oxygen 31616 Fecal Coliform 01051 Lead 00927 Magnesium 71900 Mercury_ 00610 NH3 as N 01067 Nickel Baron Neal McDuffie (Name of Signing Official -Please print or type) Field Services Director (Pace Analytical Services) (Position or Title) 3/31/21 (Permit Exp. Date) 00600 Nitrogen, Total 00630 NO2 & NO3 00620 NO3 00556 Oil & Grease W 09 PAN Plant Available 00400 pH 32730 Phenols 00665 Phosphorus, Total 00937 Potassium 00545 Settleable Matter 00929 Sodium 00931 SAR 00745 Sulfide 00515 TDS 00010 Temperature 00625 TKN 00680 TOC 00530 TSS/TSR 00076 Turbidity 01092 Zinc 7�j Parameter Code assistance may be obtained by calling the Water Quality Compliance/Enforcement Unit at (919) 733-5083, extension 529. The monthly average for Fecal Coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting facilijYs permit for reporting data. w if signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506 N (2) (D). Page 2_ Of 2 NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED PERNUT NUMBER. WQ004972 rv10NT14:_Q_ctobvr YEAR. 2021 FAcu.xrY NAME: Fo rest Lakes Prese i°ve ELS. COUNTY: Davie Formulas: Daily Loading (inclnasp = [Volume Applied (gallons) xO.1336 (mblcfeeVijalloi x 12 (Inches1fool))) [Area Sprayed (acres) x 43,560 (square feeVacca) or = lVolume Applied (gallons) /[Area Sprayed (acres) x 27,152 (gallonslacrci Maximum Hourly Loading (inches) = Daily Loading (inches)! [Time irrigated 150 (minulesihour)] Monthly Loading (inches) =Snm of Daily Loading Cinches) 12 Month Floating Total (inches) = Sum of this nivith's Monthly Loading (iricfiies) and previous I I month's Monillily Loadings inches) Average WeeMy Loading (inches) = [MantNy Loading Iinches)rriorith) ! Nurmier of days in the month idiyshnanth )] x 7 (aaysAveelk) *Uvaib,r Codtm; C-ckini VC -pa dy cloudy, 0-cloudy, R-rain, Sn-snow, Skslvvt Spray Irrigation Operator in RespoinsibleCharge(ORQ: Glenn Price_ Phorw 336-996-2841 01ZC Certification Nurnber: 987931/20771 Mail ORIGINAL and,rwo COPIES to: ATTN- Non -Discharge Cornolhowe Unit x DENR (SIGNATURE OF OPMA'FOR IN RESPONSIBIAL CIIARGE) Division of Water Quality By tills signature, I certify tilat tills report is accurate arld 1617 Mail Service Center cornplete to tile aest of illy knowledge. RAIXIGII, NC 27699-1617 Check Box if ORC Has Changed: i . 0 am I I NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) FACILITY STATUS: Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been compliant with the following permit requirements: (Note: If a requirement does not apply to your facility put (NA) in the compliant box.) Compliant (Y,N) L The application rate(s) did not exceed the limit(s) specified in the permit. Z Adequate measures were taken to prevent wastewater runoff from the site(s). 3. A suitable vegetative cover. was maintained on the site(s) in accordance with the permit. 4. All buffer zones as specified in the permit were maintained during each application. S. The freeboard in the treatment and/or storage lagoon(s) was not less than the ` limit(s) specified in the permit. If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting -false information, including the possibility of fines and imprisonment for knowing violations." (Sigriature of Permitee)* Date Baron Neal McDuffie (Authorized Agent) (Permittee-Please print or type) 2N Riverside Plaza Suite 800 Chicago. Il 60606 (Permittee Address) Baron Neal McDuffie (Name of Signing Official -Please print or type) Field Services Director (Pace Analytical Services) (Position or Title) 3/31/2021 (Permit Exp. Date) * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per I SA NCAC 2B.0506 (b) (2) (D). aOAnalytical WWW'Pacelabs-Com Tracy Overdurf Forest Lake 192 Thousand Trails Dr. Advance, NC 27006 RE: Project: Forest Lake Pace Project No.92569304 Dear Tracy OverdurE Pace AnalyficM Services, LLC 1377 SoWh Park Drive Kernersville, NC 27284 (704)977-0981 Enclosed are the analytical results for sarriple(s) received by the laboratory on October 28, 2021, The results relate only to the samples included in this report, Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report, The test results provided in this final report were generated by each of the following laboratories within the Pace Network: Pace Analytical Services -Asheville Pace Analytical Services - Eden If you have any questions concerning this report, please feel free to contact me. Sincerely, Stephanie Knott stephariie.knott@pacelabs.corn 704-977-0981 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, J without Viio written consent of Pace Analytical Services, LLC. I 4"m Page 1 of 16 aneAnalytICalWmimidahm o Project: Forest Lake Pace Project No.: 92569304 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 M^rfh Romlinn nrinkinn Water Certification #: 37712 CERTIFICATIONS North Carolina Wastewater Certification #: 40 South Carolina Certification M 99030001 VrginiaNELAP Certification #: 460222 Pace Analytical Services Eden 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633 North Carolina Drinking Water Certification #: 37738 VirginiaNELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Servloes, LLC. Pace Analytical Services, LLC 1377 South Park Drive Kemersviile, NC 27284 (704)977-0981 Page 2 of 16 aLU*U ytical www Pellabs.tetit PAO SAMPLE ANALYTE COUNT Project: Forest Lake Pace Project No.: 92569304 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92569304001 Effluent SM 254OD-2015 AED 1 PASI-E EPA 353.2 Rev 2.01993 SRS 1 PASI-E SM 521OB-2016 SRS 1 PASI-E Colilert-18 AMI 1 PASI-E TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 350.1 Rev 2.0 1993 NGP 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.01993 KDF1 1 PASI-A EPA 365.1 Rev 2.01993 MDW 1 PASI-A PASI-A = Pace Analytical Services - Asheville PASI-E = Pace Analytical Services - Eden REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 16 aceAnalyticai wtrtvpatnl�hsr:ont ANALYTICAL RESULTS Project: Forest Lake Pace Project No.: 92569304 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977.0981 Sample: Effluent Parameters Lab ID: 92669304001 Collected: 10/28/21 13:22 Received: 10/28/21 13:45 Matrix: Water Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 254OD-2015 Pace Analytical Services - Eden Total Suspended Solids 7.2 mg/L 5.8 1 10/29/21 11:16 353.2 NO2/NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Nitrate 12.7 mg/L 0.20 5 10/29/21 12:07 14797-55-8 5210E BOD, 5 day EDN Analytical Method: SM 521OB-2016 Preparation Method: SM 521OB-2016 Pace Analytical Services - Eden BOD, 5 day 2.5 mg/L 2.0 1 10/29/21 12:08 11103/21 10:57 Colilert-18 Fecal Coliform EDN Analytical Method: Colilert-18 Preparation Method: Cotllert-18 Pace Analytical Services - Eden Fecal Coliforms 2420 MPN/100rnL 1.0 1 10/28/21 18:35 10/29/21 12:48 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services - Asheville Total Nitrogen 15.0 mg/L 0.52 1 11/10/21 17:02 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Ammonia 0.26 mg/L 0.10 1 11/05/21 12:33 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Kjeldahl, Total 3.0 mg/L 0.50 1 11/09/21 15:58 11/10/21 04:14 7727-37-9 353.2 Nitrogen, NO2/NO3 pros. Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, NO2 plus NO3 12.0 mg/L 0.20 5 11/04/21 12:19 366.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 2.0 mg/L 0.050 1 11/08/2122:56 11109/2121:44 7723-14-0 Date: 11/1012021 05:06 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 16 aceAnalyttcal wrnr.paa1rt61.coiA QUALITY CONTROL DATA Project: Forest Lake Pace Project No.: 92569304 Pace Analytical Services, LLC 1377 South Park Drive Komersvitle, NC 27284 (704)977-0981 QC Batch: 656173 Analysis Method: SM 254OD-2015 QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92569304001 METHOD BLANK: 3439852 Matrix: Water Associated Lab Samples: 92569304001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L NO 2.5 10129/21 11:08 LABORATORY CONTROL SAMPLE: 3439853 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 232 93 90-110 SAMPLE DUPLICATE: 3439854 92569191001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 38.7 36.8 5 SAMPLE DUPLICATE: 3439855 92569254001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 133 133 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/10/2021 05:06 PM without the written consent of Pace Analytical Services, I.I.C. Page 5 of 16 aceArralytical tvwPacelabamm Project: Forest Lake Pace Project No.: 92569304 QC Batch: 656204 QC Batch Method: EPA 353.2 Rev 2.0 1993 QUALITY CONTROL DATA Analysis Method: EPA 353.2 Rev 2.01993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92569304001 METHOD BLANK: 3440034 Matrix: Water Associated Lab Samples: 92569304001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/L ND 0.040 10129/21 12:05 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: Parameter Nitrogen, Nitrate 3440035 Units mg/L Spike Conc. 1.5 LCS Result 1.4 LCS % Rae 94 % Rae Limits Qualifiers 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3440036 3440037 MS MSID 92569504010 Spike Spike MS MSD MS MSD % Rae Parameter Units Result Cone. Conc. Result Result % Rae % Rae Limits RPD Qual Nitrogen, Nitrate mg/L 4.7 1.5 1.5 6.1 6.2 98 100 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3440038 3440039 MS MSD 92569504009 Spike Spike MS MSD MS MSD % Rae Parameter Units Result Conc. Conc. Result Result % Rae % Rae Limits RPD Qua[ Nitrogen, Nitrate mg/L 4.7 1.5 1.5 6.1 6.1 98 95 90-110 1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11110/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 16 8C@Analyt%Cato tnrw.patcu�0><.eora QUALITY CONTROL DATA Project: Forest Lake Pace Project No.: 92569304 QC Batch: 656192 Analysis Method: SM 521OB-2016 QC Batch Method: SM 521OB-2016 Analysis Description: 5210E BOD, 5 day Final EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92569304001 METHOD BLANK: 3439949 Matrix: Water Associated Lab Samples: 92569304001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers BOD, 5 day mg/L ND 2.0 11/03/21 10:11 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3439950 Spike LCS LCS % Rec Parameter Units Conc. Result % Rao Limits Qualifiers BOD, 5 day mg/L 196 193 97 84.6-115 SAMPLE DUPLICATE: 3439952 92569254001 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg/L 160 170 7 R6 Results presented on this page are in the units Indicated by the "Unite' column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11110/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 16 (�Iace Anaiytical wtrtrpttult<Its.colu QUALITY CONTROL DATA Project: Forest Lake Pace Project No.: 92569304 QC Batch: 656078 Analysis Method: Colilert-18 QC Batch Method: Colilert-18 Analysis Description: Colilert-18 Fecal Coliform EON Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92569304001 SAMPLE DUPLICATE: 3439622 Parameter Fecal Coliforms 92569453001 Dup Units Result Result RPD Qualifiers MPN/100mL NO NO Pace Analytical Services, PLC 1377 South Park Drive Kemersville. NC 27284 (704)977-0981 Results presented on this page are In the unite Indicated by the "Units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 11/10/2021 05:06 PM without the written consent of Pace Analytical Services. I.I.C. Page 8 of 16 aceAnaJytical 1tww.Ptc1Itb&= Project: Forest Lake Pace Project No.: 92569304 QC Batch: 657751 QC Batch Method: EPA 350.1 Rev 2.0 1993 Associated Lab Samples: 92569304001 METHOD BLANK: 3447860 Associated Lab Samples: 92569304001 QUALITY CONTROL DATA Analysis Method: EPA 350.1 Rev 2.01993 Analysis Description: 350.1 Ammonia Laboratory: Pace Analytical Services - Asheville Matrix: Water Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Ammonia mg/L ND 0.10 11/05/21 10:57 LABORATORY CONTROL SAMPLE: 3447861 Spike LCS LCS °!o Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Ammonia mg/L 5 5.0 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3447862 3447863 MS MSD 92569249001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L NO 5 5 5.1 5.1 101 101 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3447864 MS 92569250001 Spike Parameter Units Result Conc. Nitrogen, Ammonia mg/L 24.2 5 3447865 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD Qual 5 28.4 28.5 85 88 90-110 0 M1 Results presented on this page are In the units Indicated by the "Units' column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/10/2021 05:06 PM without the written consent of Pace Analytical Services, I.L.C. Page 9 of 16 (�IaceAnalytical W pacoltbs.com QUALITY CONTROL DATA Project: Forest Lake Pace Project No.: 92569304 QC Batch: 658510 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92569304001 METHOD BLANK: 3451371 Matrix: Water Associated Lab Samples: 92569304001 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L NO 0.50 11/10/21 03:55 LABORATORY CONTROL SAMPLE: 3451372 Spike LOS LCS % Rae Parameter Units Conc. Result % Rae Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 9.6 96 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3451373 3451374 MS MSD 92569193001 Spike Spike MS MSD MS MSD % Rae Parameter Units Result Conc. Cone. Result Result % Rae % Rae Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 5.9 10 10 16.6 16.4 107 106 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3451375 3451376 MS MSD 92569233001 Spike Spike MS MSD MS MSD % Rae Parameter Units Result Cone. Cone. Result Result % Rae % Rae Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L ND 10 10 10.3 IDA 99 100 90-110 1 Results presented on this page are In the units indicated by the "Unite" column except where an alternate unh is presented to the right of the rasuit. REPORT OF LABORATORY ANALYSIS This report shall riot be reproduced, except in full. Date: 11/10/2021 05:06 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 16 (�Ia'neAnalytical wwwwwafti n Project: Forest Lake Pace Project No.: 92569304 QC Batch: 657412 QC Batch Method: EPA 353.2 Rev 2.01993 Associated Lab Samples: 92569304001 METHOD BLANK: 3446176 Associated Lab Samples: 92569304001 Parameter Units Nitrogen, NO2 plus NO3 mg/L LABORATORY CONTROL SAMPLE: 3446177 Parameter Nitrogen, NO2 plus NO3 QUALITY CONTROL DATA Analysis Method: EPA 353.2 Rev 2.01993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Laboratory: Pace Analytical Services - Asheville Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.040 11/0412111:40 Spike Units Conc. mg/L 2.5 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LCS LCS % Rec Result % Rec Limits Qualifiers 2.5 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3446178 3446179 MS MSD 92567965002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rac Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L NO 2.5 2.5 2.3 2.3 92 93 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3446180 3446181 MS MSD 92567965003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg1L ND 2.5 2.5 2.4 2.4 95 97 90-110 1 Results presented on this page are In the units Indicated by the 'Unite column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shell not be reproduced, except in full, Date: 11/10/2021 05:06 PM without the written consent of Pace Analytical Services, I.I.C. Page 11 of 16 aceAnalyticat www.pwNUf c= QUALITY CONTROL DATA Project: Forest Lake Pace Project No.: 92569304 QC Batch: 658334 Analysis Method: EPA 365.1 Rev 2.01993 QC Batch Method: EPA 365.1 Rev 2.01993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92569304001 METHOD BLANK: 3450643 Matrix: Water Associated Lab Samples: 92569304001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L NO 0.050 11/09/2120:30 Pace Analytical Services, LLC 1377 South Park Drive Kernersvilie. NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3450644 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.6 104 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3450645 3450646 MS MSD 92569237001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 4.7 2.5 2.5 7A 7.1 110 98 90-110 4 MATRIX SPIKE $ MATRIX SPIKE DUPLICATE: 3450647 3450648 MS MSD 92569249001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 3.3 2.5 2.5 5.8 6.9 103 107 90-110 2 Resutts presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/10/2021 05:06 PM without the written consent of Pace Analytical Services, I.I.C. Page 12 of 16 aclAna/ytical" nerve paetlatbieao QUALIFIERS Project: Forest Lake Pace, Prniwct NM: 92569304 DEFINITIONS OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MOIL - Adjusted Method Detection Limit. Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 PQL - Practical Quantitation Limit. RL- Reporting Limit _-The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenythydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphanylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is. a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN - The NELAC Institute. ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R6 The RPD between valid sample dilutions exceeded 30%. Date: 11/10/2021 05:06 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.I.C. Page 13 of 16 (�Iaci.Anayical www.patcNatncom QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Forest Lake Pace Project No.: 92569304 Pace Analytical Services, LLC 1377 South Park Drive Kernersvilie, NC 27284 (704)977-0981 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92569304001 Effluent SM 254OD-2015 656173 92569304001 Effluent EPA 353.2 Rev 2.0 1993 656204 92569304001 Effluent SM 521OB-2016 656192 SM 52108-2016 656246 92569304001 Effluent Colitert-18 656078 Colilerl-18 656079 92569304001 Effluent TKN+NO3+NO2 658936 Calculation 92569304001 Effluent EPA 350.1 Rev 2.0 1993 657751 92569304001 Effluent EPA 351.2 Rev 2.01993 658510 EPA 351.2 Rev 2.0 1993 658664 92569304001 Effluent EPA 353.2 Rev 2.0 1993 657412 92569304001 Effluent EPA 365.1 Rev 2.0 1993 658334 EPA 365.1 Rev 2.0 1993 658622 Date: 11/10/2021 05:06 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 14 of 16 CHAIN -OF -CUSTODY Analytical Request Document 1 LAB USE ONLY -Affix Workorder/togin babel Here or List Pace Workorder Number or -" Chain -of -Custody is a LEGAL DOCUMENT - Complete all relevent fields Company- Forest st Lakes III information: ALLSHADED Ia 111111 All, 11111111111 fit Report To: Email To: Copy To:Site Collection lnfd/Address: Customer Project Name/Number: State: CountyjCity, Time Zone Collected: i [ ]PT[ ]MT[ ]CT [ ]ET Phone: Site P / ayiiity iD �: —r -ia Compliance M©rttpting7 Email: [ V6es [ ]No Col eco- y (print): Purchase Order #: F DW PWS ID . � DW Location Code. i f Quote R: CoNec-ed ey signature): Turnaround Date Required: Immediately Packed on .ee: t ��Vlpsal [ ]Yes [ ] Nd3 Rush: Field Filtered (if applicable): ( j mspme as appropriate ( I Return [ ]Same Day [ Next Lay [ ] Yes [ ]No I ( ) Archive: ] ] 2 Day [ 13 Lay [ ] 4 DAY [ ] 5 Day Analysis I ] Hold: (Expedite Charges APPIY) £ Matrix Codes (insert in Matrix box below): tar inking Water (DW), Ground Water (GW), Wastewater (WW), $ Product WE SoHISolid (SL). (ail f©L), Wipe (WP), Air (AR), Tissue (fS), Bioassay (B), Vapor (V), Other (OT) •, Presentative Types: O nitric atid, 12) sulturic aci. ,'j:., (6) methanaL 17) sodium b€sulfate, (S) Sodium .. iosulfate, (9) hexane, IA) ascorbic acid, iti) ammon.urn suN$te, IQ a-mvniLm hyd oxide, ID) TSP,,U) Unpresen'taf, M) Other 3 n; : I >�a �.�m� � rccF<•e'ng� �r s?a�aaF��:: t study° Seals r ue t/lnt t N t,A E. 1 i [ custom{ Signatures PreventF CullecLar 5 anat�I_e irte n w t-- 3 _ I RVILtiog i ,€ace '' ; (� orrect aorr"Ie =4 NA i Sufficient V� it:� NA 1 l arFrlea e€ vent on Tee.: U,a � I I [ 1 IV0.1% - Hein a .� Acc ptabie ar`f I -.( MADA veesulated so 2 v Y ] F sa>•1ttF #r H€rrl T.r tom, - t.. I Residual rr1.?rsia4 s; nt 5°com �t rp� [ swrie.FAH c � �� tF: PH St Sul=lac pr.oanr Y h �f ( I,ea'd Acetate Strips:. Comp l Collected (or Res d of I- a carpi :'r nr t r: Sample ID Matrix I Customer Sam P " ) Composite Ent) Gran Composite p _ GI Gtns C] A) € ( t D to Time I Date Time 0(_ Z r 1 `LMue t Ia - t ( 1 0 E i , f I 1 E r Customer Remarks / Sp¢c"sal Conditions / Possible Hazards: 'Type of ice Used: kWel IBlue Dry None i� !Packing Material Used: ( Radchent sample(s) screened (<Soo cpm): Y N NA by/Com ny:(Signature) f by/Company: (Signature) j f ze_eived by/Co ��ny: (Signature) Received oy/Company: (Signature) SHORT HOLDS PRESENT (c72 hourS). Y i N N/A Lab Tracking M. pies recehmd via: €DID'* U'S Client Courier r r Tall 3 j 'Acc,num: {" Fa`f # i 'rem plate: ePrelo�in: Date) ai, ,, l N: Dp- Lap Sample Iel pp r€#1 tge into: ernp Blank PpcPi r Y N NA berets 4Dp tI� Coolt r l Temp V n Recelp InG Cooler I T hprm C r Factor. CC Cooler : Correct Tem�p. tC Comments: Trip San, Rect ived: t N NA HCL M.oOl-I TSP Other - Aeon volors -,,r, ej t. Page: YtS / -N c D%W"ent Name Document Revised: February 1, i,mer� taredkren IMti a.w.re.�IR�I tC l page 1 of 2 Document No.: I fsurfng authartty: •Chuk mark top half of box If pH and/or dechlorinatlon Is Project I -werlffed and.within the 4=0101tance range for-preserNtlon - — - - samples. faaapdov. VOA+ Catffam, MC CO and Grease, OW/8015 (water) OM 11Hy **Bottom hall of box Is to list number of bottle 96 46 96 E o d s o 6 pH Adjustment Log for Preserved Samples WV4 ID tW of Prostrative plf apan receipt Dow presuvatlen adjuttad itt a presemttan adjultid Anmurtt of proservaUve lot N added NOU: WMneVir trrdra U a aRQe�t7RGY arriGUn6 naru, tirCUM cwopnar+c� iuntn■,, ■ wyr w w.r .■..n mw vc .any w u..+ nv.... ....--.. ��... _. __. _.--r- - �..- .---- out at hall, tnoarrrat p 4orraow, aut of temp, k1correct eanuiners. Page 16 of 16