WQ0002857_Monitoring - 10-2021_20211130

Monitoring Report Submittal
Permit Number #*
Name of Facility:*
Month: * October
Report Information
WQ0002857
Piedmont Custom Meats WWTF
Type *
NDMR, NDAR-1, NDAR-2, NDMLR
Confirmation Email Address:*
Name of Submitter: *
Signature:
Date of submittal:
Initial Review
Year:* 2021
Upload Document*
Piedmont Custom.pdf 1.7MB
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
[e-mail]
Jessica Mize
jemdf & lip
Reviewer: Zhong, Vivien
11 /30/2021
This will be filled in automatically

Is the project number correct?* WQ0002857
Is the monitoring report accepted?* Yes No
Regional Office* Winston-Salem
Accepted Date:
12/9/2021

Page 1
of 3
NON -DISCHARGE WASTE WATER
MONITORING REPORT
PERMIT NUMBER: W 0002857
MONTH:
October YEAR: 202I
FACILITY NAME: Piedmont Custom Meats WWTF
COUNTY: Caswell
Flow Monitoring Point: Effluent: LJ Influent:
Parameter Monitoring Point: Effluent: Influent:
Surface Water (SW):
El SW Code/Name:
Was There Effluent Flow for this Month Generated At This Facility:
Yes:
No: FXA
Operator 50050 00400 50060
00310
00610
00530 3181E
70300
00620 00625
OOFi40
00600 00665
D Arrival []ally Rate
Fecal
A Time Operator ORC (Flow) into
Coliform
Tpat
T 2400 Time on on Treatment Residual
Site? System pH Chlorine
00D-5
20°C
NH-3-N
(Geoanctric
M Mean-)
DS
NO-3-N TKN
Chlorite
Nitrogen Phosphorus
cl-k sm
UNITS UGR,
KiclT
PUT
MC I. 11000L
hIC'L
%1GfL MGJL
MGIL
MGlL MGrL
IIRS YIN GALLr3N5
1 900
900
3 900
3 900
5 900
n 900
7 900
S 0847 0.25 1' 91111 6.1; <10
9 1000
L 0 0 0
u
11 1,01)()
12 1,000
1.1 1,000
14 1 1 16 4.25 R 1,1100 6.4 <I U
t5
8U0
th
800
17
1;oa
18
800
19
800
2e
]050
0.25
1
800
6.4
�111
21
11100
22
1,100
23
1,100
23
1,100
25
1,100
26
1,100
27
(1950
1.00
Y
11I10
6.5
<10
76A
1.6
56.0
236
453
18.4
7.2
91,4
26.5
0.68
28
1,000
29
1 000
3U
1,00
31
A
1 000
958
<10
76.1
Lfi
56.0
236
453
18A
7.2
91.4
26.5
11.611
rerrgc
Daily Marlmam
1 100
6.50
<10
76.1
1,6
56.0
236
453
18.4
1 7.2
1 91.4
26.5
0.68
HallyNlinimuaa
800
6.40
<10
76A
1.6
5G.0
236
453
18.4
7.2
91.4
26.5
0.68
Monthly Limits ( Avg) 5000
Composite C I Grab (G)
Operator in Responsible Charge (ORC): Glenn Price
Grade: SI
Pbone: 336-996-2841
Check Box if ORC Has Changed:
ORC Certification
Number: 987931/20771
Certified Laboratories (I): Pace Analytical Services
(2)
Person(s) Collecting Samples: Glenn Price
Mail ORIGINAL and Two COPIES to.
ATTN: Non -Discharge Compliance Unit X
DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CI IA
Division of Water Quality By this signature, I certify that this report is accurate and
1617 Mail Service Center complete to the best of my knowledge.
RALEIGH, NC 27699-1617
DENR Form NDAR-1 (5/2003)

NON DISCHARGE WASTEWATER MONITORING REPORT
FACILITY STATUS:
Please answer the following question: Compliant ,N)
L Does all monitoring data and sampling frequencies meet permit requirements?
If the facility is non -cam, please explain in the space below the reason(s) the facility was not in compliance with its
permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach
additional sheets if necessary.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
I- 36 - � Baron Neal McDuffie
(Signature ofPermitee)* Date (Name of Signing Official -Please print or type)
Field Services Director (Pace Analytical Services)
Baron Neal McDuffie (Authorized Agent)
(Permittee-Please print or type)
9683 Kerr's Chapel Road
Gibsonville NC
(Permittee Address)
01002 Arsenic
01022 Boron
00310 BOD5
01027 Cadmium
00916 Calcium
00940 Chloride
50060 Chlorine, Total
Residual
01034 Chromium
00340 COD
PARAMETER CODES
31504
Coliform, Total
00094
Conductivity
01042
Copper
00300
Dissolved Oxygen
31616
Fecal Coliform
01051
Lead
00927
Magnesium
71900
Mercury
00610
NH3 as N
01067
Nickel
(Position or Title)
336-582-8247
(Phone Number)
00600 Nitrogen, Total
00630 NO2 & NO3
00620 NO3
00556 Oil & Grease
W 09 PAN Plant Available
00400 pH
32730 Phenols
00665 Phosphorus, Total
00937 Potassium
00545 Settleable Matter
03/31 /21
(Permit Exp. Date)
00929
Sodium
00931
SAR
00745
Sulfide
00515
TDS
00010
Temperature
00625
TKN
00680
TOC
00530
TSS/TSR
00076
Turbidity
01092
Zinc
Parameter Code assistance may be obtained by calling the Water Quality Compliance/Enforcement Unit at [phone], extension 529.
The monthly average for Fecal Coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data.
* If signed by other dean the Permittee, delegation of signatory authority must be on file with the state per ISA NCAC 2B.0506 (b) (2) (D).

Page 2 of 3
NON -DISCHARGE APPLICATION REPORT
SPRAY IRRIGATION SITE(S)
THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED
PERMIT NUMBER•. W 0002857 MONTH: October YEAR: 2021
FACILITY NAME:Piedmont Custom Mcats WWTF COUNTY: Caswell
Formulas:
Daily Loading (inches) = [Volume Applied (gallons) x 0.1336 (cubic feetigallon) x 12 (incheslfoot)] I [Area Sprayed (acres) x 43,560 (square feetlacre) or
= [Volume Applied (gallons) I [Area Sprayed (acres) x 27,152 (gallonslacre-inch).
Maximum Hourly Loading (inches) = Daily Loading (inches) I (rime Irrigated (minutes) I6D (minutes/hour)] Monthly Loading (inches) =Sum of Daily Loading (inches)
12 Month Floating Total (inches) = Sum of this month's Monthly Loading (inches) and previous 11 month's Monthly Loadings (inches}
Average Weekly Loading (inches) = [Monthly Loading (incheslmonth) l Number of days in the month (dayslmonth )] x 7 {daysMeek)
Did Irrigation Occur At This Farilily�
Did Irrigation Oocur On This Field:
D�d Irrigation Occur On This Field:
Yol—Al
■
Field Number.
Yid
• • •IN
MArMT.,®
®!
1
;.
"Weather Coder C-clear, PC -partly cloudy, CI-rloudy, R-raln, Smsnow, Sl-Meer
Spray Irrigation Operator in Responsible Charge (ORC): Glenn Price Phone: [phone]
ORC Certification Number: 987931/20771 Check Box if ORC HastChanged: El
Mail ORIGINAL and Two COPIES to:
ATTN: Non -Discharge Compliance Unit
DENR
Division of Water Quality
1617 Mail Service Center
RALEIGH, NC 27699-1617
(SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE)
By this signature, 1 certify that this report is accurate and
complete to the best or my knowledge.
DENR Form NDAR-1 (5/2003)

FACILITY STATUS:
Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been compliant_
with the following permit requirements: (Note: If a requirement does not apply to your facility put (NA) in the
compliant box.)
Compliant (Y,N)
1. The application rate(s) did not exceed the limit(s) specified in the permit.
[�0
2. Adequate measures were taken to prevent wastewater runoff from the site(s).
4
3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit.
4
4. All buffer zones as specified in the permit were maintained during each application.
4
5. The freeboard in the treatment and/or storage lagoon(s) was not less than the
4
limit(s) specified in the permit.
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance with its
permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach
additional sheets if necessary.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permiee) Date
Baron Neal McDuffie (Authorized Agent)
(Permittee-Please print or type)
9683 Kerr's Chapel Road
Gibsonville. NC
(Permittee Address)
Baron Neal McDuffie
(Name of Signing Official -Please print or type)
Field Services Director (Pace Analytical Services)
(Position or Title)
336-582-8247
(Phone Number)
03/31/21
(Permit Exp. Date)
* If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506 (b) (2) (D).
DENR Form NDAR-1 (5/2003)

Page 3 of 3
NON -DISCHARGE APPLICATION REPORT
SPRAY IRRIGATION SITE(S)
THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED
PERMIT NUMBER: W 0002857 MONTH: October YEAR: 2021
FACILITY NAME: Piedmont Custom Heats V4 WTF COUNTY: Caswell
Formulas:
Daily Loading (inches) = [Volume Applied (gallons) x o.1336 (cubic feeUgallon) x 12 (inche5Maol)] I (Area Sprayed (acres) x 43.560 (square feeyacre) or
= [Volume Applied (gallons) I [Area Sprayed (acres) x 27.152 (galfonsracre-Inch).
Maximum Hourly Loading (inches) = Daily Loading (inches)! [Time irrigated (mil 160 (minuleslhourl] Monthly Loading (inches) =Sum of Daily Loading (inches)
12 Month Floating Total (inches) = Sum of this months Monthly Loading (inches) and previous 11 moni Monthly Loadings (inches)
Average Weekly Loading (inches) = {Monthly i.oading (inchoslmonth) I Number of days in the month (dayslmonth )] x 7 (dayshveek)
•
■. • 6•
■. " • •
•. • On
w
Yes !
■
.
Field Number
Permitted Hourly ate (inMOS17
1
��
��
��
m
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��
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��
��
��
mow.
�I■
��
I'1
•Weather CodL�: C-clear, PC -partly cloudy, CI-eluudy, n-raie, Sn-nnun, SI-sleet
Spray Irrigation Operator in Responsible Charge (ORC): Glenn Price Phone: [phone]
ORC Certification Number: 987931/20771 Check Box if ORC Has C anged: ❑
Mail ORIGINAL and Two COPIES to:
ATTN: Non -Discharge Compliance Unit X `
DENR (SIGNATURE OFOPERATOR 1N RESPONSIBLE CHARGE)
Division of Water Quality By this signature, 1 certify that this report is accurate and
1617 Mail Service Center complete to the best of my knowledge.
RALEIGH, NC 27699-1617
DENR Form NDAR-1 (5/2003)

FACILITY STATUS:
Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been compliant
with the following permit requirements: (Note: If a requirement does not apply to your facility put (NA) in the
compliant box.)
Compliant (Y,N)
1. The application rate(s) did not exceed the limit(s) specified in the permit. EIP
2. Adequate measures were taken to prevent wastewater runoff from the site(s).
3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit. 4
4. All buffer zones as specified in the permit were maintained during each application.
5. The freeboard in the treatment and/or storage lagoon(s) was not less than the 4
limit(s) specified in the permit.
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance with its
permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach
additional sheets if necessary.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Baron Neal McDuffie
( ignature of Permitee)* Date (Name of Signing Official -Please print or type)
Baron Neal McDuffie (Authorized Agent) Field Services Director ( Pace Analytical Services
(Permittee-Please print or type) (Position or Title)
9683 Keres Chapel Road 336-582-8247 03/31/21
Gibsonville NC (Phone Number) (Permit Exp. Date)
(Pennittee Address)
* If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506 (b) (2) (D).
DENR Form NDAR-1 (5/2003)

aceAnalytical
WM.pacalabs.cam
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
ANALYTICAL RESULTS
Project: Piedmont Custom Meats
Pace Project No.: 92569014
Sample: Effluent Lab ID: 92569014004 Collected: 10/27/21 10:45 Received: 10/27/21 12:37 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2015
Pace Analytical Services - Eden
Total Dissolved Solids
453 mg/L 25.0
1
11/02121 17:26
2540D Total Suspended Solids
Analytical Method: SM 2540D-2015
Pace Analytical Services - Eden
Total Suspended Solids
56.0 mg/L 16.7
1
10/28/21 16:07
350.1 Ammonia EDN
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, Ammonia
1.6 mg/L 0.10
1
10/27/21 15:12 7664-41-7
353.2 NO2/NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.01993
Pace Analytical Services - Eden
Nitrogen, NO2 plus NO3
19.3 mg/L 0.20
5
10/28/21 09:03
Nitrogen, Nitrate
18.4 mg/L 0.20
5
10/28/21 09:03 14797-55-8
5210E BOD, 5 day EON
Analytical Method: SM 5210B-2016 Preparation Method: SM 521 OB-2016
Pace Analytical Services - Eden
BOD, 5 day
76.1 mg/L 2.0 1 10/28/21 10:37 11/02/21 10:56 R6
Colilert-18 Fecal Coliform EDN
Analytical Method: Colilert-18 Preparation Method: Colilert-18
Pace Analytical Services - Eden
Fecal Coliforms
236 MPN/100mL 1.0 1 10/27/21 12:50 10/28/21 09:05
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services -Asheville
Total Nitrogen
26.5 mg/L 0.52 1 11/11/21 15:17
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
Chloride
91.4 mg/L 1.0 1 10130/2117:08 16887-00-6
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.01993
Pace Analytical Services - Asheville
Phosphorus
0.68 mg/L 0.050 1 11/08/2122:56 11/09/2119:54 7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/11/2021 03:27 PM without the written consent of Pace Analytical Services, I.I.C.
Page 13 of 49

Pace Analytical Services, LLC
acenMalidical
1377 South Park Drive
Kernersville, NC 27284
www.pawab st=
[phone]
CERTIFICATIONS
Project: Piedmont Custom Meats
Pace Project No.: 92569014
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
North Carolina Drinking Water Certification #: 37712
Virginia/VELAP Certification #: 460222
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Wastewater Certification #: 633
North Carolina Drinking Water Certification M 37738
VirginiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. LLC. Page 2 of 49

0
( --- aceAnalytical
Report of Analysis
Pace Analytical LLC
1377 South Park Drive
Kernersville, NC 27284
Attention: Stephanie Knott
Project Name: Piedmont Custon Meats
Project Number: 92569014
Lot Number:WJ30050
Date Completed: 11/11/2021
11/11/2021 1:41 PM
Approved and released by:
Project Manager I: Biaire M. Gagne
� ^ ``ll
_ �1
AJ=-
�Y
A C L R E D I T E D
7ES71NO LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Pax: 803-791-9111 www.pacelabs.com
Page 39 of 49
Page 1 of 11

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Pace Analytical LLC
Lot Number: WJ30060
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation:
Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium,
Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, Fecal
Coliform SM 9221 C E-2006 & SM 922213-2006, Strontium SW 846 601 OD, VOC SM 6200 B-2011,
Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, Solid
Chemical Material: TOC Walkley-Black.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.paoelabs.com
Page 40 of 49
Page 2 of 11

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Pace Analytical LLC
Lot Number: WJ30050
Project Name: Piedmont Custon Meats
Project Number: 92569014
Sample Number Sample ID Matrix Date Sampled Date Received
001 Effluent Aqueous 10/27120211045 10/28/2021
(1 Sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
108 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com Page 41 of 49
Page 3 of I i

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Pace Analytical LLC
Lot Number: WJ30050
Project Name: Piedmont Custon Meats
Project Number: 92669014
Sample Sample ID Matrix Parameter Method Result 0 Units Page
001 Effluent Aqueous TKN 351.2 7.2 mgiL 5
(1 detection)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia. SC 29172 [phone] Fax [phone] www.pacelabs.com Page 42 of 49
Page 4 of 11

Inoraanic non-metals
Client: Pace Analytical LLC Laboratory ID:WJ30050-001
Description: Effluent Matrix: Aqueous
Date Sampled:1012712021 1045 Project Name: Piedmont Custon Meats
Date Received:1012812021 Project Number: 92569014
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date aatcn
1 351.4 (TKN) 351.2 2 1Ili 0/2021 1647 DMA 11/10/2021 0910 21839
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
TKN 351.2 7.2 0.20 0.20 mg/L 1
LOQ = Limit of Quarddation 8 - Detected in the method blank E = Quentilation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate Failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > OL L = LCSILCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 43 of 49
Page 5 of I i

QC Summary
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: WJ30060
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com Page 44 of 49
Page 6 of 11

Inorganic non-metals - MB
Sample ID: W021839-001 Matrix: Aqueous
Batch: 21839 Prop Method: 351.4
Analytical Method: 351.2 Prep Date: 11/10/2021 0910
Parameter Result Q Dil LOQ DL Units Analysis Date
TKN ND 1 0.10 0.10 mg/L 11/10/2021 1513
LQQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limb J = Estimated result - LQQ and >_ DL P = The RPD between two GC columns exceeds 40%
• = RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, inc.) QC Data for Lot Number: WJ30050
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 45 of 49
Page 7 of I 1

Inorganic non-metals - LCS
Sample ID: W021839-002 Matrix: Aqueous
Batch:21839 Prep Method: 351.4
Analytical Method: 351.2 Prep Date: 1111012021 0910
Spike
Amount Result %Rec
Parameter (mg1L) (mg1L) Q Dil % Roc Limit Analysis Date
TKN 2.0 2.0 1 102 90-110 11/10/20211513
LOG - Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOG and i DL P = The RPD between two GC columns exceeds 40%
• = RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: WJ30050
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 46 of 49
Page 8 of I 1