WQ0035049_Monitoring - 10-2021_20211123

Monitoring Report Submittal
Permit Number #*
Name of Facility:*
Month: * October
Report Information
WQ0035049
Maple Hill WWTP
Type *
NDMR, NDAR-1, NDAR-2, NDMLR
Confirmation Email Address:*
Name of Submitter: *
Signature:
Date of submittal:
Initial Review
Year:* 2021
Upload Document*
October2021 _N DM R_N DA... 7.06MB
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
[e-mail]
Kenny Keel
Reviewer: Lloyd, Chloe D
11 /23/2021
This will be filled in automatically

Is the project number correct?* WQ0035049
Is the monitoring report accepted?* Yes No
Regional Office* Wilmington
Accepted Date:
12/6/2021

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Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Pender County Utility Operations
Date of Report: Nov 10, 2021
Post Office Box 995
Customer PO #:
Burgaw NC 28425
Customer ID: 08100095
Attention: Chris Pickett
Report #: 2021-18738
Project ID: Maple Hill WWTP
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
21-46918 Site: Effluent
10/22/2021
9:00 AM Water Walker Diab
Test
Method
Results Date Analyzed
Ammonia Nitrogen
EPA 350,1, Rev. 2.0,1993
0.5 mg/L
10/29/2021
Total Kjeldahl Nitrogen (TKN)
EPA351.2, Rev. 2.0,1993
2.0 mg/L
11/03/2021
Residue Suspended (TSS)
SM 2540 D-2015
<2.5 mg/L
10/25/2021
BOD
SM 5210 B-2016
5 mg/L
10/22/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0, 1993
0.34 mg/L
10/22/2021
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0, 1993
13.9 mg/L
10/26/2021
Nitrate Nitrogen
Subtraction Method
13.6 mg/L
11/05/2021
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
21-46919 Site: Effluent - Grab
10/22/2021
9:00 AM Water Walker Diab
Test
Method
Results Date Analyzed
Fecal Coliform IdexxColilert-18
<1 MPN/100ml
10/22/2021
Temperature SM 2550 B-2010
19.4 C
10/22/2021
pH SM 4500 H B-2011
7.7 units
10/22/2021
Total Phosphorus SM 4500 P (F-H)-2011
0.15 mg/L
11 /02/2021
Comment:
Reviewed by:
Report #. 2021-18738 Page 1 of 1

flare: �r A � Pi�l CertiOcattanp 94
faettin Name:
slnat�st: b.1F` yA�t
Permit ii: Yy Q
Reference Method Skt45on H-B ?01 I �!
4 a . ,ati• n Time
Cal Buflar 4 , s u
tat l3uftbr 10.0 s u
Check Huffer 7 it s u
instrument ID V17
Comments
ro {%!
L
.pit check buffer must read
a ithin ± 0 i pH units orthc
buffer's true %alue -
4 su buffer Loie : Ricca 2001920
Exit 1/20?2
7 su buffer Lot--
Ricca 2009993 Exp 7 2022
10 su buffer Lot-- LCi2siO4 12012
Sample location
Sample Collection
Sample$ h sis
pH Result b. sis Her
Time e
Check %slue au
Comments Data Qualifiers
ers
A Post anall sis buffer check is required tehen performing anal} ses at multiple sampling locations and must be %ohm 0 1 units orthe buffer's true %alue
All pit %aloes In PI units (i e. s u ) Record all data to the nearest 0 01 s u and capon to the nearest 0 1 s u
Total Residual Chlorine (TRC)
Refrcnce Atelhod. s53 4500 Ct-G201 I Bach 81 7 HR { Please circle an") Icable :vdethad instrument ID
Dath Check Post -analysis Time chactr
Check Std. Sample Sample
Standard Result Standard Sample TRC Result
i i%th naval}zing t.ocattan Collection Anal) Comments Data µ_'L are mgL at mute le sites} Analizcd Tinto Time pS L or mg L
I IM r.rail% c. necs Standard true value µg/L or mg/i, acceptance range_ . _., _112 i. or mg I,
Check standard, mint reca er within; i0", nrtiic check ctnnd lyd-c trip it niir,
,-Annual LahbrationLure Verification hate. I Ur
atc
Reagent thank tre Value. _ (ll'hen applicable Analand document a reagent blank %%hen standards, sample dilutions or PT S mples art pri�iarerl)
Dissolved Oxygen (DO)
Reference Method SM 45000 G.-201 I Instrument ID
Calibration Calibrationranable 0leterreading opost-anOlt sticalibration
Verification or °a efricienc% t,nficalni I (Ithcn necessan r
Time after cahbrali - Comments
Temperature Barometric Thcarehcat Calculated
Iressure Value mz L Value me't.
Sample location I Sample Collection
Anahsis j D0
I. se this roii %lien
a i erification instead of
Comments Data Qualifiers
0 When performing anahses at multiple locations. the meter must be recahbrated at each site berore analysis or a post-anahsts calibration yenlicatton must be performed
If sample is measured directl% In the stream and or ansite. onh time anatt zed uould be recorded %tth a note that ahe% are measured to situ or immr diate t
Temperature
R�tin+nra16+0-4 c%r'r.•;r,oi..� ..
Sample Location I Collection
i
li sample is melts d
Annual Verification Date
Field Personnel Note:
Rev 9-2020
•Samptc Temperai=
Analysis .0
Time
i
i
in the 3ircam and or on site only tame ana%zed %%ould be
Comments Data Qualifiers
with a note that the% are measurer) in situ or tmmediateh
Q %.001

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receil t Checklist
Client. Date10 OZI Report Number:
6602 Windmill Way
Wilmington, NC 28405
910-392-t)2;11
[Receipt of sample:
❑
ECHEM_ P' ickup Client Delivery 0
JUPS 0 FedEx 0 Other U
YES
1
0 NO
N/A 1. Were custody seals present on the cooler?
0 YES
10 NO
If custody
IR NIA 2. If custody seals were present, were they intact/unbroken?
JOriginal temperature upon receipt - a C Corrected temperature upon receipt
How temperature taken:
0 Temperature Blank es
JIR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor *C: 0.0
13 YES
CO1NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
JW YES
1103 NO
4. Were proper custody procedures (relinquished/received) followed?
YES
113 NO
S. Were sample ID's listed on the COC?
YES
NO
6, Were c=mnine ID's listed on sample containers?
YES
10 NO
7. Were collection date and time listed on the COC?
YES
10 NO
B. Were tests to be performed listed on the COC?
YES
10 NO
9. Did samples arrive in proper containers for each test?
Ilk YES--
E3 NO
10. Did samples arrive in good condition for each test?
YES
0 NO
11. Was adequate sample volume availableT
YES
13 NO
12. Were samples received within proper holding time for requested tests?
YES
13 NO
33 Were acid preserved samples received at a pH of <2?
YES
0 NO
14 Were cyanide samples receivedata pH >12?
11 YES
0 NO
15. Were sulfide samples received at a pH >9?
YES
Ei NO
16. Were NH1 TKN/Phenol received at a chlorine residual of <0.5 m/L?
YES
13 NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
113 NO
I8. Were orthophosphate samples filtered in the field within 15 minutes?
TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any -sample(s) incorrectly preserved or N7with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCl NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service Immediately for incorrectly preserved samples. Obtain anew sample or
notify the - state lab If directed to analyzed by the customer. Who was notified, date and time:
Volatiles Samples)
were received with hea;soaca
COMMENTS:
DOC. QA.002 Rev 1

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