HomeMy WebLinkAboutNC0024911_Solube BOD and Tox Results_20210624Action History (UTC-05:00) Eastern Time (US & Canada)
Submit by Anonymous User 6/24/2021 9:50:27 AM (Supplemental Submittal)
Submit by Bennett, Tilman B 11/24/2021 9:24:04 AM (Supplemental Info Submittal)
IN Tox Lab Reports and Soluble BOD Results
Bennett, Tilman B assigned the task to Bennett, Tilman B 11/24/2021 9:23 AM
• The task was assigned to Thedford, Wren, Bennett, Tilman B 6/24/2021 9:50 AM
Initial Review Information
Updated ID#: * IMPORTANT: REVIEWER SHOULD VERIFY and revise here if necessary.
NCO024911
How should this project be handled?*
File Discard
Information Submitted on 6/24/2021
Submitter Information
Name: Roger Edwards
Who is submitting the information?
Email Address:* RogerE@msdbc.org
Submittal Information
The Division of Water Resources (DWR) is providing this site to allow for the upload of required supplemental information
associated with discharge monitoring reports (DMR). All DMR data is required to be submitted electronically through
the eDMR system and should not be submitted here. Division staff will review all uploaded documents and will only
maintain required information. Documents such as laboratory reports are not required to be submitted and will not be
maintained in the system.
Project Information:
Please supply the permit number for this project.
......................................................................................................................................................................................................................................................................................................................................................................................................
Existing ID#* Permit Number
NCO024911
Examples: NCxxxxxxx or NCGxxxxxx
Facility Name: * Metropolitan Sewerage District of Buncombe County
County: Buncombe
Please upload all files that need to be submited.*
Click the upload button or drag and drop files here to attach document
May 2021 Toxicity.pdf 971.83KB
5 - May 2021 Soluble BOD Results.pdf 25.51 KB
Only pdf files are accepted.
Comments about the attachments:
* By checking the box and signing box below, I certify that:
o I have given true, accurate, and complete information on this form;
a I agree that submission of this Supplemental Information form is a "transaction" subject to Chapter 66, Article 40 of the
NC General Statutes (the "Uniform Electronic Transactions Act)
a I agree to conduct this transaction by electronic means pursuant to Chapter 66, Article 40 of the NC General Statutes
(the "Uniform Electronic Transactions Act');
a I understand that an electronic signature has the same legal effect and can be enforced in the same way as a written
signature; AND
o I intend to electronically sign and submit the Supplemental Information form."
Full Name: Roger Edwards
Signature:
Date Submitted: 06/24/2021
Metropolitan Sewerage District of Buncombe County
Soluble BOD Results
Date
Effluent Soluble BOD
(Mg/L
5/5/2021
7.7
5/12/2021
4.6
5/19/2021
5.0
5/26/2021
6.4
Average
5.9
Analytical
www,pecelebs.com
June 08, 2021
Mr. Roger Edwards
Metropolitan Sewerage District
2028 Riverside Drive
Asheville, NC 28804
RE: Project: MSD NC0024911
Pace Project No.: 92537883
Dear Mr. Edwards:
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
Enclosed are the analytical results for samples) received by the laboratory between May 11, 2021 and May 13, 2021. The
results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC
Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
lorri.patton@pacelabs, com
1(828)254-7176
Project Manager
Enclosures
cc: Ms. Shannon Bergeron, Metropolitan Sewerage District
Mr. John Gosnell, Metropolitan Sewerage District
Mr. Chad Ledford, Metropolitan Sewerage District
Mr. Dwayne Martin, Metropolitan Sewerage District
Ms. Cassandra McKnight, MSD of Buncombe County
Patrick Smith, MSD of Buncombe County, NC
Mr. Alan Taylor, Metropolitan Sewerage District
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
out the written consent of Pace Analytical Services, LLC.
Page 1 of 13
Document Name:
Sample Condition Upon Recei
Document No.:
F-CAR-CS*033•Rev,07
Document Revised: October 28, 2020
Page 1 of 2
issuing Authority:
Pace Carolinas Quality Office
Laboratory receiving samples;
Asheville Eden❑ Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville[]Atlanta❑ Kernersyilie❑
III • � II, � Client Name; 11 r W0# 0 92537883
_. \ Project #: il
Courier: ❑Fed Ex LJUPS UUSPS �(Cli
❑ Commercial ❑Pace ❑Other:_
Custody Seal Present? ❑Yes 496 Seals Intact? ❑Yes ^ joNo
Packing Material: ❑Bubble Wrap ❑Bubble Bags�ne ❑ Other
Thermometer:+l�vet ❑Blue
❑ IR Gun ID: q 3 ((j 7 I Type of Ice:
Correction Factor:
Cooler Temp: 't 'Ed Add/Subtract (°C)
r'
Cooler Temp Corrected ('C);
USDA Regulated Soil (M N/A, water sample)
Did samples originate in a quarantine zone within the United States, CA, NY, or SC (check maps)?
Chain of Custody Present?
Samples Arrived within Hold Time?
Short Hold Time Analysis (<72 hr,)'
Rush Turn Around Time Requester
Sufficient Volume?
Correa ontalners lJsod?
-Pace Containers Used?
Intact?
Sample Labels Match COC1
-Includes
Headspace in
Trip Blank Present?
Blank Custody Seals
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFI[ATIO
Person contacted:
Mona
SCURF Review:
Project Manager SRF Review:
1.
Yes ❑No ❑N/A
)Yes ❑No ❑N/A —I 6.
�res ❑No ❑N/A 7.
❑Yes ❑No j�N/A 8.
Yes []No❑N/A 9,
1111111111111111
37883
Dale/Initials Person EKamining Contents: ( T, 11 I
giologicaiTissue Frozen?
❑Yes ❑No EMN/A
❑None
Tempshould be above freezing to 6°C
]Samples out of temp criteria. Samples on Ice, cooling process
hasbegun
❑Yes ❑No. INN/A 10.
❑Yes ❑No �]NJA 11,
Date/Time:
Did
In
samples originate from a foreign source (Internationally,
dingHawali and Puerto Rico)? ❑Yes No
it containers:
Date:
Date:
Field Data Required? ❑Yes ❑Nd
Page 2 of 13
Document Name:
Condition Upon Recei
Document No,,
F-CAR-CS-033-Rev.07
*Check mark top half of box if pH and/ dechlorination is
verified and within the acceptance range for preservation
samples,
Exceptions; VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
*Bottom half of box is to list number of bottles
g
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3
4
5
6
7
8
9
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it
Document Revised: October 28, 2
t(SCUR) Page 2 of 2
Issuing Authority:
Pace Carolinas Quality Office
Project # WO# : 92537
PM: LJP Due Date; 05/25/21
CLIENT: 93vii
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Log for Preserved Samples
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Page 3 of 13
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Document Name:
Document Revised: October 28, 2020
Sample Condition Upon Recelpt(SCUR)
Page 1 of 2
aceAnalytical
Document No,:
issuing Authority:
1
F•CAR•CS-033•Rev.07
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheviile�o*4�Eden❑ Greenwood ❑ Huntersviile ❑ Raleigh❑ Mechanicsville❑ Atlanta[] Kernersville❑
w � Sample condition " �`
Upon Receipt .: ' <`
Courlent ■.. Ex
■ commercial []Pace
ustody■
Project :
Seals Intact? ❑Yes �lo
Packing Material; ❑eubbie Wrap ❑Bubble Bags -}None ❑ Other
Thermometer;
❑ IR Gun ID• 3Tt;� ( i@Wet ❑Blue
• Type office:
Correction Factor: ,e
Cooler Temp: �' �- Add/Subtract (°C)y
Cooler Temp Corrected (°C): � . / o C
USDA
U5 (®T�/A, water
Did
C� 5 Z 4 �
Date/Initials Person Examining Contents: s'
Biological Tissue Frozen?
❑Yes ❑No +RN/A
❑None
Temp should be above freezing to 6°C
❑samples out of temp criteria, Samples on ice, cooling process
fiasbegun
Regulated Soil
sample)
samples originate in a quarantine zone within the United States: CA, NY, or SC(check maps)? Did samples originate from a foreign source (internationally,
[]Yes ❑No IncludingHawaii and Puerto Rico)? ❑Yes ❑No
Comments/Discrepancy:
Chain of Custody Present? &Yes []NO ❑N/A 1.
Samples Arrived within Hold Time? Yes ❑No ❑N/A 2.
Short Hold Time Analysis (02 hr.)? []Yes &o ❑N/A 3.
Rush Turn Around Time Requested? []Yes &No ❑N/A 4.
Sufficient Volume? ayes []No ❑N/A 5.
Correct Containers Used? 4Tes ❑No ❑N/A 61
*Pace Containers Used? &Yes []No ❑NIA
Containers Intact? (�rYes j[3No ❑N/A 7.
Dissolved analysis: Samples Field Filtered? ❑Yes o [Bt/A 8.
Sample Labels Match COC? Des ❑No ❑N/A 9.
•Includes Date/Time/ID/Analysis Matrix: W
Headspace in VOA Vials (>5.6mm)? ❑Yes ❑Pin N/A 10.
Trip Blank Present? ❑Yes []No i O/A
Trip Blank Custody Seals Present? Des ❑No ®N?A
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFI
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Raview;
Date/Time;
Lot ID of split contain
Date:. CJ
bate:
Field Data Required? ❑Yes ❑No
Page 6 of 13
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFI
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Raview;
Date/Time;
Lot ID of split contain
Date:. CJ
bate:
Field Data Required? ❑Yes ❑No
Page 6 of 13
Document Name;
Sample Condition Upon Recell
Document No.:
F•CAR-CS-033,,Rev07
*Check mark top half of box If pH and/or dechlorination is
verified and within the acceptance range for preservation
samples,
Exceptions; VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottles
Project if
Docume October 28, 2020
Page 2 of 2
Issuing Authority,
nsi.o rnrnlinas Quality Office
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Adjustment
Sample ID Type of Preservative pH upon receipt
Log for Preserved Samples
Date preservation adjusted Time preservation Amount of Preservative Lot tf
adjusted added
rif thin fnrm will b ont to rhp North Carolina DEHNR Certification Office (La,
ivoce;vvnenevercnereisaaiscrepancyanc�.uu6ivul,1
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Page 7 of 13
Ceriodaphilia dubia Survival and Reproduction Test
EPA-821-R-02-013 Method 1002
Client: MSD OF BUNCOMBE COUNTY
Facility: WRF
NPDES #: NC0024911
Test Date: 12-May-21
Laboratory ID #: T59190
Test Reviewed and Approved By:
Robert W, Kelley, Ph.D.
Ifficer
Certification #E87819
Test results presented in this report conform to all requirements of
NELAC, conducted under NELAC Certification Number E87819
Certification #23104
Florida Dept. of Health, Included results pertain only to provided sam les.
rage 1 of 6
Certification # 022 Page 8 of 13
Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50
Date 31-May-21
Facility: MSD OF BUNCOMBE CO. WRF NPDES#NCO024911 Pipe# 001 County: Buncombe
Laboratory Performing Test: Comments
X
Signatu e o Aerator in Responsible Charge
X
Signature of Laboratory Supervisor
MAIL ORIGINAL TO Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test FChron!cTestsults
0
2.508
CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 0.0%
# Young Produced 22 17 21 22 19 20 22 18 21 22 21 17
Adult (L)Ive (D)ead L L L L L L L L L L L L
Effluent %
TREATMENT 2 ORGANISMS
# Young Produced
Adult (L)Ive (D)ead
pH
Control
Treatment 2
D.O.
Control
Treatment 2
23
18
22
19
22
17
22
19
20
19
22
19
L
L
L
L
L
L
L
L
L
L
I L
L
1st sample
7.8 7.9
8.0 8.1
start end
1 sl samola
8.2
7.8
8.2
7.8
LC50IAcute Toxicity Test
(Mortality expressed as %, combining replicates)
1 sl sample
7.8 8.3
7.8 8.5
start and
lslsam le
7.5 8,1
7.6 8.6
2nd sample
7.8 8.3
8.0 8.5
start end
9nd samola
8.0
7,9
7.7
8.5
�n (Startl Date
1 10-May-21
to This for Either Test
Sample 1 X 24hrs.
Sample 2 X 24hrs.
Hardness (mg/L)
Spec. Cond. (pmhos)
Chlorine (mg/L)
at
0%
20.2
Control
Control
0%
20.2
Treatment 2
Treatment 2
Control CV
9.7%
3rd Brood PASS FAIL
1
1st 2nd
Tox Tox
Dilution Sample Sample
85.1
326 500 489
<0.05 <0.05
1.7 0.9
slart/end slart/end
Control
High Cone.
pH D.O.
Page 9 of 13
DEM Form AT-1
Page 2 of 6
STATISTICAL ANALYSIS RESULTS
Facility: MSD xPOESa NCO024911
Sample 11): WWTP LTTH T59190 Date; 12-May-21
Laborato : i Certification #: NCO22 Ex . Date: l l/1/2021
val Data
7 Day Survival Test Used: FISHERS TEST
Control 100% Test Statistic: P= 1.000
Effluent 100% Critical Value: P= 0.01
PASS: The effluent does not reduce survival of the test organisms.
Reproduction Data
Raw Data Test for Normality
Mean young/female Std. Dev. Test Used: Shapiro-Willcs Test;
Control 20.2 1,95
Effluent 20.2 1.95 W: 0.889
Critical Value: 0.884
Analysis for Differences in Reproduction Test for Homogeneity of Variance
Test Used: Equal Variance t Test, Test Used: F Test
Calculated t= 0.00 F= 1.00
Critical Value= 2.51 Critical Value= 5.32
The data are homogeneous in variance
PASS: The effluent is not chronically toxic.
Page 10 of 13
Page 3 of 6
1
Control
2
Mortality
3
and Reproduction by
4 5
Test Day
6
7
8
Total
source
rep
115
5-5
1
+4+7
11
22
W24-30
2
+3+5
9
17
02 4-29
3
+4+7
101
21
HH6 5-5
4
+4+6
121
22
V1 4-30
5
+3+5
111
19
N14-29
6
4
+7+9
20
B8 4-28
7
4
+8+10
22
P2 4-29
8
3
+7+8
18
V2 4.30
9
+4+6
11
21
O1 4-29
10
+3+7
12
22
A10 4-30
11
+4+6
11
21
LL9 5-5
12
+3+5
9
17
13
N/A
0
14
N/A
0
15
N/A
0
16
N/A
0
17
N/A
0
18
N/A
0
19
N/A
o
Mean
20
N/A
0
20.2
12
1
% Effluent
2
Mortality and Reproduction by Test Day
3 4 5 6
7
8
Total
115 5-5
1
+4+7
12
23
W2 4-3
2
+3+6
9
18
02 4-2
3
+4+7
11
22
HH6 5-
4
+3+6
10
19
V1 4-30
5
+4+7
11E22
N1 4 29
s
3
+s+6
B8 4-28
7
q
+7+11
P2 4-29
8
3
+7+9
V2 4-30
9
+3+7
10Q1
4-2
10
3
+6+10A10
4-3
11
+4+6
12
LL9 5-5
12
+3+7
9
19
0
13
N/A
0
0
14
N/A
0
0
15
N/A
0
0
16
N/A
0
0
17
N/A
0
0
18
N/A
0
0
19
N/A
o
Mean
0
20
NIA
0
20.2
rd11a4v
AM
AM
fSi
JC
AM
AM
JC
AM
JC
19-May-21
y
07:46 AM
02:06 PM
06:56 AM
0614 AM
11:20 AM
17:36 AM
12:54 PM
JC
A7a1v lam
, .
24.9
25.2
Old temp. °C
25.3
25.3
24.9
Control New tamp.
°C
24.6
24.8
190
5-2200
Comments
inl
dubia
JID=Dead N/A•Losl or not used I�
Page 4 of 6
Page 11 of 13
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