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HomeMy WebLinkAboutNCG100080_2021 DMR_20211026MAKING COMPLEX EASY Date: August 26, 2021 Omar Castilla 3525 Piedmont Road N.E., LKQ Salisbury Suite 417, Bldg. 7 1212 Webb Road Atlanta GA 30305 Salisbury, NC 28146 T +1 404 812 0001 Re: 2021 Third Quarter Storm Water Sampling Results LKQ Salisbury — Salisbury, NC Permit No. NCG100080 Dear Mr. Castillo: Enclosed is your 2021 third quarter Stormwater Discharge Monitoring Report (DMR). Please note this is the second sample submitted for this monitoring period. You are required by the permit to submit your DMR to the Mooresville Regional DEMLR Office. A cover letter to the DWQ for transmittal of the DMR is also attached here for your convenience. Please print the cover letter and a copy of the DMR, and sign and date inside the gray boxes of the cover letter. Please also sign and date the certification sections on the bottom of the page of the DMR. A copy of the signed DMR also must also be electronically uploaded to this link; https://edocs.deg.nc.gov/Forms/SW-DMR This link is also available on the DMR form and in the email that contained this DMR. Please fill out the date the form was uploaded at the top of the page before submittal. The original signed cover letter and DMR should be sent via certified mail with a return receipt or via Fed - Ex to the Mooresville Regional DEMLR Office at the address shown on the cover letter. You should make copies of the letter and form and file them in the monitoring section of your Storm Water Pollution Prevention Plan (SPPP). The original signed cover letter and the DMR should be sent via certified mail with a return receipt or via Fed -Ex to the DWQ at the address shown on the cover letter by November 161" 2021 If you should have any questions or comments, please do not hesitate to contact me at (404) 809-3878 or colby.geil6a rpsgroup com. Sincerely, Colby Geil Consultant I Attachment 1 — Cover Letter to State Attachment 2 — DMR Attachment 3 — Test America Analytical Report and Chain of Custody rpsgroup.com RIPS Group, Inc.. Registered in United States No. 76-0539898, Page 1 CERTIFIED MAIL, RETURN RECEIPT REQUESTED Mooresville Regional Office Attn: Central Files 610 East Center Avenue Mooresville, NC 28115 RE: LKQ Salisbury Salisbury, NC Permit # NCG100080 2021 Third Quarter Stormwater Discharge Monitoring Report Dear Sir/Madam: Please find attached the 2021 Third Quarter Stormwater Discharge Monitoring Report (DMR) for the LKQ Full -Service facility located in Salisbury, North Carolina. This submittal covers the reporting period July 31 s' to September 30'h, 2021. A sample was collected previously in July 2021. However, COD was not analyzed. Therefore, an additional sample was collected so that COD could analyzed and submitted for the 2021 third quarter. A copy of the DMR was also uploaded electronically as required. Please call me at (912) 313- 2720 or Mr. Colby Geil of RPS at 404-809-3878 if you have any comments, questions, or concerns about the information lkesented in this submittal. Since Omar Castillo Plant Manager Attachment NCDEQ Division of Energy, Mineral and Land Resources Stormwater Discharge Monitoring Report (DMR) Form for NCG100000 Used Motor Vehicles Click here for instructions Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office. Certificate of Coverage No, NCG10 0080 Person Collecting Samples: Omar Castillo Facility Name: LKQ Salisbury Laboratory Name: Eurofins TestAmerica, Savannah Facility County: Rowan Laboratory Cert. No.: 490 Discharge during this period: Yes No (if no, skip to signature and date) Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? 0Yes , ✓' No If so, which Tier (I, II, or III)? A copy of this DMR has been uploaded electronically via https://edocs.deLnc.gov/Forms/SW-DMR ✓, Yes M No Date Uploaded: Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red) Parameter Code , Parameter Outfall 001 Outfall Outfall Outfall Outfall N/A Receiving Stream Class B N/A Date Sample Collected MM/DD/YYYY 9/22/21 46529 24-Hour Rainfall in inches 4.6 C0530 TSS in mg/L (100 or 50*) 730 00400 pH in standard units (6.0 — 9.0 FW, 6.9 6.8 — 8.5 SW) 00340 Chemical Oxygen Demand in mg/L (120) 23 01051 Lead, total recoverable (as Pb)in mg/ L (0.075 FW, 0.22 SW) 0.0065 Ethylene Glycol in mg/ L (any amount 77023 detected Tier One; 8,000 mg/L Tier 5.0(Less than detectable limit) Two and Three) 00552 Non -Polar Oil & Grease in mg/L (15) 1.3 NCOIL Estimated New Motor/Hydraulic Oil Usage in gal/month 5-10 weans to Outstanding Resource waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA) have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 mg/L FW (Freshwater) SW (Saltwater) Notes (optional): A sample was collected earlier in the Third Quarter (July 2021). However, COD was not analyzed. Therefore an additional sample was collected to analyze COD. "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted i , the bestjff my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false info r a on, inclu ng the possibility of fines and imprisonment for knowing violations." of Per(4iittee or Delegated Authorized Individual _ (!U$fjo PL90 � Copt Email Address /0 - Z & —x7_-t Date Phone Number eurofins Environment America Eurofins TestAmerica, Savannah 5102 LaRoche Avenue Savannah, GA 31404 Tel: (912)354-7858 Laboratory Job ID: 680-205006-2 Laboratory Sample Delivery Group: 212417/41676 Client Project/Site: 1140A - LKQ SALISBURY For: RPS Group Inc 3525 Piedmont Rd NE Suite 520 Bldg 6 Atlanta, Georgia 30305 Attn: Seth Ailiff Authorized for release by. 1011912021 5:15:36 PM Bernard Kirkland, Lab Director (912)250-0274 Bernard.Kirkland@Eurofinset.com Designee for Jim Knapp, Project Manager II (630)758-0262 Jim.Knapp@Eurofinset.com The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. Definitions/Glossary Client: RPS Group Inc Project/Site: 1140A- LKQ SALISBURY Job ID: 680-205006-2 SDG: 212417/41676 Qualifiers --- General Chemistry Qualifier Qualifier Description HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request. Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. ° Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level" MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit MIL Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative / Absent POS Positive / Present PQL Practical Quantitation Limit PRIES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEO Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Eurofins TestAmerica, Savannah Page 2 of 11 10/19/2021 Sample Summary Client: RPS Group Inc Project/Site: 1140A - LKQ SALISBURY Lab Sample ID Client Sample ID Matrix Collected Received 680-205006-1 Water Sample Water 09/22/21 1,3 00 0912512 110:10 Job ID:680-205006-2 S DG: 212417141676 Eurofins TestAmerica, Savannah Page 3 of 11 10/19/2021 Case Narrative W s Client: RPS Group Inc Job ID: 680-205006 2 Project/Site: 1140A- LKQ SALISBURY SDG: 212417/41676 o io: sso-zosoas-� Laboratory: Eurofins TestAmerica, Savannah Narrative Receipt The sample was received on 9/25/2021 10:10 AM. Unless otherwise noted below, the sample arrived in good condition, and where is required, properly preserved and on ice. The temperature of the cooler at receipt was 0.1 ° C. General Chemistry No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. Eurofins TestAmerica, Savannah Page 4 of 11 10/19/2021 Client: RPS Group Inc Project/Site: 1140A - LKQ SALISBURY Client Sample Results: Job ID: 680-205006-2 SDG: 212417/41676 Client Sample ID: Water Sample Lab Sample ID: 680-205006-1 Date Collected: 09/22/21 18:00 Date Received: 09/25121 10:10 Matrix: Water General Chemistry Analyte Result Qualifier NONE NONE Unit D Prepared Analyzed Dil Fac pH 6.9 HF Su 10/08/2112:33 1 Analyte l Chemical Oxygen Demand Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fa. 23 10 5.0 mg/L 10/19/21 08:55 1 Eurofins TestAmerica, Savannah Page 5 of 11 10/19/2021 Client: RPS Group Inc QC Sample Results Project/Site: 1140A- LKQ SALISBURY lVietnod: 410.4-1993 R2.0 - COD Lab Sample ID: MB 680-689904/3 Matrix: Water Analysis Batch: 689904 Analyte Chemical Oxygen Demand Lab Sample ID: LCS 680-689904/4 Matrix: Water Analysis Batch: 689904 Analyte Chemical Oxygen Demand .. .......... Method: 4500 H+ B-2011 - PH Job ID: 680-205006-2 SDG: 212417/41676 ....... . ... . ....... ..... ---------- - --- -------- Client Sample ID: Method Blank V�5 Prep Type: Total/NA MB M13 Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <10 10 5.0 mg/L 10/19/21 08:55 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits 50.0 49.0 mg/L 98 90-110 ... . ...... Lab Sample ID: LCS 680-688596/31 Matrix: Water Analysis Batch: 688596 Spike LCS LCS Analyte Added Result Qualifier pH - - 7.01 7.1 .. ....... . .... . . ........ Client Sample ID: Lab Control Sample Prep Type: Total/NA %Rec. Unit D %Rec Limits S-U— — —101 —63-158 Eurofins TestAmerica, Savannah Page 6 of 11 10/19/2021 Client: RPS Group Inc QC Association Summary Project/Site: 1140A - LKQ SALISBURY General Chemis Analysis Batch: 688596 Lab Sample ID Client Sample ID 680-205006-1 Water Sample LCS 680-688596/31 Lab Control Sample Analysis Batch: 689904 Lab Sample ID Client Sample ID 680-205006-1 Water Sample MB 680-68990413 Method Blank LCS 680-68990414 Lab Control Sample Prep Type Matrix Total/NA Water Total/NA Water Job ID: 680-205006-2 SDG: 212417141676 Method Prep Batch 4500 H+ B-2011 4500 H+ B-2011 i Prep Type Matrix Method Total/NA Water 410.4-1993 R2.0 Total/NA Water 410.4-1993 R2.0 Total/NA Water 410.4-1993 R2.0 Eurofins TestAmerica, Savannah Page 7 of 11 10/19/2021 Lab Chronicle r# Client: RPS Group Inc Job ID: 680-205006 2 Project/Site: 1140A - LKQ SALISBURY SDG: 212417/41676 Client Sample ID: Water Sample Lab Sample ID: 680-205006-1 Date Collected: 09/22/21 18:00 Matrix: Water Date Received: 09125/21 10:10 Batch Batch Dil Initial Final Batch Prepared t Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab }� Total/NA Analysis 410.4-1993 R2.0 1 2 mL 2 mL 689904 10/19/21 08:55 ALG TAL SAV N:.t Instrument ID: SPC7 7X t� x1 Total/NA Analysis 4500 H+ B-2011 1 688596 10/08/21 12:33 DR TAL SAV Instrument ID: MANTECH Laboratory References: TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins TestAmerica. Savannah Page 8 of 11 10/19/2021 AccreditationlCertification Summary Client: RPS Group Inc Job ID: 680-205006-2 Project/Site: 1140A - LKQ SALISBURY SDG: 212417/41676 Laboratory: urofins TestAmerica, Savannah All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report. Authority Alabama Alaska (UST) ANAB ANAB Arkansas DEQ California Connecticut Florida Georgia Georgia (DW) Guam Hawaii Illinois Indiana Iowa Kentucky (UST) Louisiana Louisiana (DW) Maine Maryland Massachusetts Michigan Mississippi Nebraska New Jersey New Mexico New York North Carolina (DW) North Carolina (WW/SW) Pennsylvania Puerto Rico South Carolina Tennessee Texas Texas USDA Virginia Washington Wisconsin Wyoming Program Identification Number Expiration Date AFCEE SAVLAB State 41450 06-30-22 State 17-016 09-22-22 Dept. of Defense ELAP L2463 09-22-22 ISO/IEC 17025 1-2463.01 09-22-22 State 19-015-0 02-01-22 State 2939 06-30-22 State PH-0161 03-31-23 NELAP E87052 06-30-22 State E87052 06-30-22 State 803 06-30-22 State 19-007R 04-17-22 State <cert No.> 06-30-22 NELAP 200022 11-30-21 State C-GA-02 06-30-22 State 353 06-30-22 State NA 06-30-22 NELAP 02011 06-30-22 State LA009 12-31-21 State GA00006 09-25-22 State 250 12-31-21 State M-GA006 06-30-22 State 9925 03-05-22 State <cert No.> 06-30-22 State NE-OS-7-04 06-30-22 NELAP GA769 06-30-22 State GA00006 06-30-22 NELAP 10842 04-01-22 State 13701 07-01-22 State 269 12-31-21 NELAP 68-00474 06-30-22 State GA00006 01-01-22 State 98001 06-30-22 State 02961. _ 06-30-22 NELAP T1047004185-19-14 11-30-21 TCEQ Water Supply T104704185 06-30-22 US Federal Programs P330-18-00313 09-03-24 NELAP 10509 06-29-22 State C805 06-10-22 State 999819810 08-31-22 State 8TMS-L 06-30-22 Eurofins TestAmerica, Savannah 19 1 Page 9 of 11 10/19/2021 Client: RIPS Group Inc Project/Site: 1140A - LKQ SALISBURY Method Method Description 410.4-1993 R2.0 COD 4500 H+ B-2011 pH Protocol References: Method Summary Job ID:680-205006-2 SDG: 212417/41676 Protocol Laboratory MCAWW TAL SAV SM TAL SAV MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions. SM = "Standard Methods For The Examination Of Water And Wastewater' Laboratory References: TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins TestAmerica, Savannah Page 10 of 11 10/19/2021 Login Sample Receipt Checklist Client: RIPS Group Inc Login Number: 205006 List Number: 1 Creator: Sims, Robert D Question Answer Radioactivity wasn't checked or is </= background as measured by a survey N/A meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. N/A There is sufficient vol. for all requested analyses, incl, any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is True <6mm (1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A Job Number: 680-205006-2 SDG Number: 212417/41676 List Source: Eurofins TestAmerica, Savannah Comment No Eurofins TestAmerica, Savannah Page 11 of 11 10/19/2021 eurofins Environment Testing America Eurofins TestAmerica, Savannah 5102 LaRoche Avenue Savannah, GA 31404 Tel: (912)354-7858 Laboratory Job ID: 680-205006-1 Laboratory Sample Delivery Group: 212417/41676 Client Project/Site: 1140A - LKQ SALISBURY For: RPS Group Inc 3525 Piedmont Rd NE Suite 520 Bldg 6 Atlanta, Georgia 30305 Attn: Seth Ailiff � K_"� Authorized for release by: 101112021 4:04:33 PM Jim Knapp, Project Manager II (630)758-0262 Jim.Knapp@Eurofinset.com The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. Client: RPS Group Inc Definitions/Glossary Project/Site: 1140A- LKQ SALISBURY wuaiirlers Metals Qualifier Qualifier Description i Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. General Chemistry Qualifier Qualifier Description J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. Ulossary Abbreviation These commonly used abbreviations may or may not be present in this report. a Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoDIDOE) LOQ Limit of Quantitation (DOD/DOE) MCL EPA recommended "Maximum Contaminant Lever' MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative/Absent POS Positive / Present PQL Practical Quantitation Limit PRIES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Job ID: 680-205006-1 S DG: 212417/41676 Eurofins TestAmerica, Savannah Page 2 of 14 10/1/2021 Client: RPS Group Inc Project/Site: 1140A- LKQ SALISBURY Lab Sample ID Client Sample ID 680-205006-1 Water Sample Sample Summary Job ID: 680-205006-1 S DG: 212417/41676 Matrix Collected Received Water 09/22/2118:00 09/25/2110:10 9 EurofinsTestAmerica1Savannah Pa e3of14 Case Narrative Client: RPS Group Inc Project/Site: 1140A- LKQ SALISBURY Job ID: 680-205006-1 Laboratory: Eurofins TestAmerica, Savannah Narrative Job Narrative 680-205006-1 Comments No additional comments. Job ID: 680-205006-1 SDG: 212417/41676 Receipt The sample was received on 9/25/2021 10:10 AM. Unless otherwise noted below, the sample arrived in good condition, and where required, properly preserved and on ice. The temperature of the cooler at receipt was 0,10 C. GC Semi VOA No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. Metals No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. General Chemistry Method SM 2540D: The sample duplicate precision for the following sample associated with analytical batch 680-687021 was outside control limits: (680-204833-A-1 DU). The associated Laboratory Control Sample / Laboratory Control Sample Duplicate (LCS/LCSD) precision met acceptance criteria. Methods 1664A, 166413: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated with preparation batch 680-687438. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. Eurofins TestAmerica, Savannah Page 4 of 14 10/1/2021 Client Sample Results Client: RPS Group Inc Project/Site: 1140A- LKQ SALISBURY Client Sample ID: Water Sample Date Collected: 09/22121 18:00 Date Received: 09/25/21 10:10 Method: 8015C - Nonhalogenated Organic using GC/FID (Direct Aqueous Injection) Analyte Result Qualifier RL MDL Unit Ethylene glycol <5.0 5.0 1.2 mg/L Method: 200.7 Rev 4.4 - Metals (ICP) - Total Recoverable Analyte Result Qualifier RL MDL Unit Lead 0.0065 J 0.010 0.0039 mg/L General Chemistry Analyte Result Qualifier RL MDL Unit Oil & Grease 1.3 J 2.5 0.70 mg/L Analyte Result Qualifier RL RL Unit Total Suspended Solids 730 50 50 mg/L D Prepared Analyzed Dil Fac 09/27/21 18:54 1 D Prepared Analyzed oil Fac 09/2812115:07 09129/2122:57 1 >. D Prepared Analyzed Dil Fac r 10/01/21 07:04 10/01 /21 09: 06 1 D Prepared Analyzed Dil Fac 09/28/21 18:14 1 Eurofins TestAmerica, Savannah Page 5 of 14 10/1/2021 QC Sample Results Client: RPS Group Inc Job ID: 680-205006-1 Project/Site: 1140A- LKQ SALISBURY SDG: 212417/41676 , Method: 8015C - Nonhalogenated Organic using GCIFID (Direct Aqueous Injection) Lab Sample ID: MB 680-686766/11 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 686766 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Ethylene glycol <5.0 r n -1,) ..,.,n NIS Lab Sample ID: LCS 680-68676617 Matrix: Water Analysis Batch: 686766 Analyte Spike Added LCS LCS Result Qualifier Unit Client Sample ID: Lab Control Sample Prep Type: Total/NA «' %Rec. D %Rec Limits Ethylene glycol 20.0 19.5 mg/L 97 61 - 148 Lab Sample ID: LCSD 680-686766/8 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: TotaIINA Analysis Batch: 686766 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Ethylene glycol 20.0 19.6 mg/L 98 61 - 148 1 50 Lab Sample ID: 680-205006-1 MS Client Sample ID: Water Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 686766 Sample Sample Spike MS MS %Rec. Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits Ethylene glycol <5.0 20.0 18.3 mg/L 91 61 _ 148 Lab Sample ID: 680-205006-1 MSD Client Sample ID: Water Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 686766 Sample Sample Spike MSD MSD %Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Ethylene glycol <5.0 20.0 18.6 mg/L 93 61 - 148 2 50 Method: 200.7 Rev 4.4 - Metals (ICP) Lab Sample ID: MB 680-686994/1-A Matrix: Water Analysis Batch: 687289 Analyte Lead Lab Sample ID: LCS 680-686994/2-A Matrix: Water Analysis Batch: 687289 Analyte Lead MB MB Result Qualifier RL MDL Unit <0.010 0.010 0.0039 mg/L Client Sample ID: Method Blank Prep Type: Total Recoverable Prep Batch: 686994 D Prepared Analyzed Dil Fac 09/28/2115:07 09/29/2122:48 1 Client Sample ID: Lab Control Sample Prep Type: Total Recoverable Prep Batch: 686994 Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits 0.505 0.492 mg/L 98 85 - 115 Eurofins TestAmerica, Savannah Page 6 of 14 10/1 /2021 Qo QC Sample Results ON Client: RPS Group Inc Job ID: 680-205006 1 Project/Site: 1140A - LKQ SALISBURY SDG: 212417/41676 Method: 200.7 Rev 4.4 - Metals (ICP) (Continued) Lab Sample ID: 680-205006-1 MS Matrix: Water Analysis Batch: 687289 Sample Sample Spike MS MS Analyte Result Qualifier Added Result Qualifier Unit Lead 0.0065 J 0.505 0.502 mg/L Lab Sample ID: 680-205006-1 MSD Matrix: Water Analysis Batch: 687289 Sample Sample Spike MSD MSD Analyte Result Qualifier Added Result Qualifier Unit L Lead 0.0065 J 0.505 0.501 mg/L Method: 1664A - HEM and SGT-HEM Lab Sample ID: MB 680-68743811-A Matrix: Water Analysis Batch: 687484 MB MB Analyte Result Qualifier RL MDL Unit Ir Oil & Grease <5.0 5.0 1,4 mg/L Lab Sample ID: LCS 680-68743812-A Matrix: Water j Analysis Batch: 687484 Spike LCS LCS Analyte Added Result Qualifier Unit Oil & Grease 40,0 34.40 mg/L Lab Sample ID: LCSD 680-687438/3-A Matrix: Water Analysis Batch: 687484 Spike LCSD LCSD Analyte Added Result Qualifier Unit i Oil & Grease 40.0 34.00 mg/L -- .......... .__....... - ......... -----..._...._.._._......... _..__....... — ........... _ Method: 2540 D-2011 - Total Suspended Solids (Dried at — ---- - - --..._._....... _.... 103-105°C) - Lab Sample ID: MB 680-687021/1 Matrix: Water Analysis Batch: 687021 MB MB Analyte Result Qualifier RL RL Unit Total Suspended Solids <2,5 2.5 2.5 mg/L Lab Sample ID: LCS 680-687021/2 Matrix: Water Analysis Batch: 687021 Spike LCS LCS Analyte Added Result Qualifier Unit Total Suspended Solids 951 834 mg/L Client Sample ID: Water Sample Prep Type: Total Recoverable Prep Batch: 686994 %Rec. s Ws D %Rec Limits L� a 98 75 _ 125 Client Sample ID: Water Sample Prep Type: Total Recoverable Prep Batch: 686994 %Rec. RPD D %Rec Limits RPD Limit 98 75. 125 0 20 Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 687438 D Prepared Analyzed Dil Fac 10/01/21 07:04 10/01/21 09:06 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 687438 %Rec. D %Rec Limits 86 78 _ 114 Client Sample ID: Lab Control Sample Dup Prep Type: Total1NA Prep Batch: 687438 %Rec. RPD D %Rec Limits RPD Limit 85 78 _ 114 1 18 Client Sample ID: Method Blank Prep Type: Total/NA D Prepared Analyzed Dil Fac 09/28/21 18:14 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA %Rec. D %Rec Limits 88 80. 120 Eurofins TestAmerica, Savannah Page 7 of 14 10/1 /2021 Client: RPS Group Inc Project/Site: 1140A- LKQ SALISBURY QC Sample Results Job ID: 680-205006-1 SDG: 212417/41676 Method: 2540 D-2011 - Total Suspended Solids (Dried at 103-105°C) (Continued) Lab Sample ID: LCSD 680-687021/3 Client Sample ID: Lab Control Sample Dup ... Matrix: Water Prep Type: TotaI/NA Analysis Batch: 687021 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D % Rec Limits RPD Limit F Total Suspended Solids 951 830 mg/L 87 80 - 120 0 25 m Eurofins TestAmerica, Savannah Page 8 of 14 10/1/2021 QC Association Summary r, Client: RPS Group Inc Job ID: 680-205006 1 Project/Site: 1140A - LKQ SALISBURY SDG: 212417/41676 Analysis Batch: 686766 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-205006-1 Water Sample Total/NA Water 8015C MB 680-686766/11 Method Blank Total/NA Water 8015C LCS 680-68676617 Lab Control Sample Total/NA Water 8015C LCSD 680-686766/8 Lab Control Sample Dup Total/NA Water 8015C 680-205006-1 MS Water Sample Total/NA Water 8015C 680-205006-1 MSD Water Sample -- Total/NA --- Water 8015C Metals - — Prep Batch: 686994 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-205006-1 Water Sample Total Recoverable Water 200.7-1994 R4.4 MB 680-686994/1-A Method Blank Total Recoverable Water 200.7-1994 R4.4 LCS 680-686994/2-A Lab Control Sample Total Recoverable Water 200.7-1994 R4.4 680-205006-1 MS Water Sample Total Recoverable Water 200.7-1994 R4.4 68D-205006-1 MSD Water Sample Total Recoverable Water 200.7-1994 R4.4 Analysis Batch: 687289 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-205006-1 Water Sample Total Recoverable Water 200.7 Rev 4.4 686994 MB 680-686994/1-A Method Blank Total Recoverable Water 200.7 Rev 4.4 686994 LCS 680-686994/2-A Lab Control Sample Total Recoverable Water 200.7 Rev 4.4 686994 680-205006-1 MS Water Sample Total Recoverable Water 200.7 Rev 4.4 686994 680-205006-1 MSD Water Sample Total Recoverable Water 200.7 Rev 4.4 686994 General Chemistry ......... _._—........ _..._._ ........... ..... — _._.._...__.... __ Analysis Batch: 687021 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-205006-1 Water Sample Total/NA Water 2540 D-2011 MB 680-687021/1 Method Blank Total/NA Water 2540 D-2011 LCS 680-687021/2 Lab Control Sample Total/NA Water 2540 D-2011 LCSD 680-687021/3 Lab Control Sample Dup Total/NA Water 2540 D-2011 Prep Batch: 687438 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-205006-1 Water Sample Total/NA Water 1664A MB 680-687438/1-A Method Blank Total/NA Water 1664A LCS 680-68743812-A Lab Control Sample Total/NA Water 1664A LCSD 680-68743813-A Lab Control Sample Dup Total/NA Water 1664A Analysis Batch: 687484 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-205006-1 Water Sample Total/NA Water 1664A 687438 MB 680-687438/1-A Method Blank Total/NA Water 1664A 687438 LCS 680-68743812-A Lab Control Sample Total/NA Water 1664A 687438 LCSD 680-687438/3-A Lab Control Sample Dup Total/NA Water 1664A 687438 Eurofins TestAmerica, Savannah Page 9 of 14 10/1 /2021 Client: RPS Group Inc Project/Site: 1140A- LKQ SALISBURY Client Sample ID: Water Sample Date Collected: 09/22/21 18:00 Date Received: 09/25/21 10:10 Lab Chronicle Job ID: 680-205006-1 S DG: 212417/41676 Lab Sample ID: 680-205006-1 Matrix: Water Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab �t u4,s Total/NA Analysis 8015C Y 1 686766 09/27/21 18:54 EHS TAL SAV Instrument ID: CVGG2 Total Recoverable Prep 200.7-1994 R4.4 50 mL 50 mL 686994 09/28/21 15:07 JE TAL SAV Total Recoverable Analysis 200.7 Rev 4.4 1 687289 09/29/21 22:57 BCB TAL SAV Instrument ID: ICPE Total/NA Prep 1664A 993 mL 500 mL 687438 10/01/21 07:04 JAS TAL SAV • Total/NA Analysis 1664A 1 687484 10/01/21 09:06 JAS TAL SAV Instrument ID: NoEquip Total/NA Analysis 2540 D-2011 1 50 mL 1000 mL 687021 09/28/21 18:14 PG TAL SAV Instrument ID: NOEQUIP Laboratory References: TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins TestAmerica, Savannah Page 10 of 14 10/1/2021 Accreditation/Certification Summary Client: RPS Group Inc Job ID: 680-205006-1 Project/Site: 1140A- LKQ SALISBURY SDG: 212417/41676 Laboratory: Eurofins TestAmerica, Savannah All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report. Authority Program AFCEE Alabama State Alaska (UST) State ANAB Dept. of Defense ELAP ANAB ISO/IEC 17025 Arkansas DEQ State California State Connecticut State Florida NELAP Georgia State Georgia (DW) State Guam State Hawaii State Illinois NELAP Indiana State Iowa State Kentucky (UST) State Louisiana NELAP Louisiana (DW) State Maine State Maryland State Massachusetts State Michigan State Mississippi State Nebraska State New Jersey NELAP New Mexico State New York NELAP North Carolina (DW) State North Carolina (VW/SW) State Pennsylvania NELAP Puerto Rico State South Carolina State Tennessee State Texas NELAP Texas TCEQ Water Supply USDA US Federal Programs Virginia NELAP Washington State Wisconsin State Wyoming State Identification Numbe SAVLAB 41450 17-016 L2463 L2463.01 19-015-0 2939 PH-0161 E87052 E87052 803 19-007 R <cert No.> 200022 C-GA-02 353 NA 02011 LA009 GA00006 250 M-GA006 9925 <cert No.> N E-OS-7-04 GA769 GA00006 10842 13701 269 68-00474 GA00006 98001 02961 T1047004185-19-14 T104704185 P330-18-00313 10509 C805 999819810 8TMS-L Expiration Date 06-30-22 09-22-22 09-22-22 09-22-22 02-01-22 06-30-22 03-31-23 06-30-22 06-30-22 06-30-22 04-17-22 06-30-22 11-30-21 06-30-22 06-30-22 06-30-22 06-30-22 12-31-21 09-25-22 12-31-21 06-30-22 03-05-22 06-30-22 06-30-22 06-30-22 06-30-22 04-01-22 07-01-22 12-31-21 06-30-22 01-01-22 06-30-22 06-30-22 11-30-21 06-30-22 09-03-24 06-29-22 06-10-22 08-31-22 06-30-22 Eurofins TestAmerica, Savannah 'EfiM 4 Page 11 of 14 10/1/2021 Method Summary Client: RPS Group Inc Project/Site: 1140A- LKQ SALISBURY Job ID: 680-205006-1 SDG: 212417/41676 Method Method Description Protocol Laboratory 8015C Nonhalogenated Organic using GC/FID (Direct Aqueous Injection) SW846 TAL SAV 2003 Rev 4.4 Metals (ICP) 40CFR136A TAL SAV 1664A HEM and SGT-HEM 1664A TAL SAV 2540 D-2011 Total Suspended Solids (Dried at 103-105°C) SM TAL SAV 1664A HEM and SGT-HEM (Aqueous) 1664A TAL SAV 200.7-1994 R4.4 Preparation, Total Recoverable Metals EPA TAL SAV Protocol References: 1664A = EPA-821-98-002 40CFR136A = "Methods for Organic Chemical Analysis of Municipal Industrial Wastewater", 40CFR, Part 136, Appendix A, October 26, 1984 and subsequent revisions. EPA = US Environmental Protection Agency SM = "Standard Methods For The Examination Of Water And Wastewater" SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins TestAmerica, Savannah Page 12 of 14 10/1 /2021 "3 c z z Z: z 20a Oa 0 > 2 E E LD (D u < o 0 x 0 cq U- u ID a. < co a sioulplUO3 10 JeqLunN 19101 t—tz'pEt, -2 z 4! 0 0 M -r' Q0 ry IF:3 An a cr (V 0 S94,- (30*SZ Peal vm 3 COE 0 OTO * V119V w o Lli —,AV, 2 pzAID - Iva-39toR C) z x U� E CL m AON jo roA) 9ydwcs pajalllA plalzi 4) 0 m 4t E E M Etc E E 01 0 m 00 0 ca 76 0 1 cn r w z 0 " v LL E 0 C) c b- N N C' E pp �z w — Ln m D E C<, E 75 2� CL E y i w 'f IN Page 13 of 14 10/l/2021 Login Sample Receipt Checklist Client: RIPS Group Inc Login Number: 205006 List Number: 1 Creator: Sims, Robert D Question Answer Radioactivity wasn't checked or is </= background as measured by a survey NIA meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection dateltimes are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. N/A There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is True <6mm (114"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. NIA List Source: Eurofins TestAmerica, Savannah : -- Comment Eurofins TestAmerica, Savannah Page 14 of 14 10/1 /2021