Loading...
HomeMy WebLinkAboutWQ0005603_GWrw, yl rermit $ Wfsl00fl5inp3 (Submit one each umnfloring period with GiF59 farms.) 1 ' Enter date monitoring results were due. - - Will this monitoring report (GW-59 and GW-59A) III YES NO be submitted after the established due date? I x 2 Was any required information missing on the GW-59 report forms? YES NO I;I X IF the answer to question f or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. i I 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing IYES NO identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Once for guidance. II I I y /� 4 Are any monitored constituents equal to or above the established standards? (IYES I NO If the answer to question 4 is "NO", skip to section 8. . if the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) II exceeding standards in the space provided below: P HtW /3 m�"j3 Mw-/1 snr~-fz rh.a^9•/.b'/ /hw•/S 'NAp-/S8n•/C /!tW-/Y Irao.ef-2.l5 l /rr,a -O. yro 5 For the constituents identified In question 4 above, have standards been exceeded previously for the 1 YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is "NO", skip to section 8. if the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). 74/6 - f-/d y-ip y.oci y-°9 8-09 fi`o9 /zb9 mM w9 - ros in a 17 To3 Est w"s r4� 2 /2. !Y r2 2 /Z IY 2 /2 /D 2 /2 ro !y Jr /3 /5 // /3 /S tl /S it /3 /s Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES N9 x If the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. if the answer is "NO", monitoring wells maybe improperly I located; contact the Regional Office. I Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is 'YES'; describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties. Ix to RECEIVE�:.m to m �; r 6 1A1 3 1 2011 g. c g The person completing this portion (GW-59A) of the monitoring report should i n be �{ gdisubmitlthis+_ _ form with GW 59 forms for required wells to the address provided at the top of the current GW-59 fortR I°herebyackno' leiig at theabove Inforrnatlon was evaluated and the inforattatioti submltted7n this ti' report,(Cotriphance,Re _ rt GW 59A� Is true . , •complete to the'best of my knowledge t �'•; 3 Signature of Peitnitteeror Authorized Agent) Dale 11 PC G%V-59A 12/8/2003 - - — -- -- �I -I-- GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: L' 0(]l1 < Permit Name (if different): Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type Telephone #: Yabf- JSfa - No. of Wells to be Sampled: Well Identification Number (from Permit): _D� f.) ;L For Groundwater Treatment Systems Well Depth:�,�V ft. Well Diameler _� in. Check One; ❑ Influent (98) Screened Interval:It. to nJ A it Depth to Water Level: ❑ Effluent (99) ft. below measuring point. Measuring Point (M.P.) is:..LI o3. It, above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 73 Date sample collected: /a - /O Field analysis: pH 7,1 Specific Conductance ' uMhos Temp. �_,5°C.Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #:l )Q000br003 EXPIRATION DATE: 5 -ao/ Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING Milrr O(j,ED� -_� Lagoon _flemedialiom{-Inii ra—lion Gallery I Spray Field _Remediation: 1 Ty W Rotary Distributor _Land Application oT-Sludoe NOTE: Values should reflect dissolved and -- � rj'l colloidal concentrations. -D eft Date sample analyzed: _See T2� I n, m aN-' n _l Laboratory Name: IA. O:Jpr T,-(Ik Ir = r Certification No. So PARAMETERS (Samples for metals were collected unfiltered-LX—YES _NO and field acidified COD mg/I Nitrite (NO2) as N mg /I Coliform: MF Fecal /100ml Nitrate (NO3) as N m/I Coliform: MF Total /1 nOml Phncnhnn ic• Total n¢ ID 'M-J-r_i.. .,.---11 (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total_0-9-/o S/8? mg/I pH (When analyzed) /a -7—/o 7 units TOC_ 41,0 mg/I Chloride is-a)-ln 5.5 mg/I Arsenic la-in-IC7 4o.0ms mg/l Grease and Oils mg/I Phenol mg/I Sulfate 1R -lo-lo to I mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Orthophosphate mg/I Al - Aluminum / io 10 0,990 mg/I Ba-Barium /-A-io io 4 o 0ar mg/I Ca - Calcium /a -/n-lo a.e _ mg/I Cd - Cadmium is-/0 /4 40.009 mg/I Chromium: Total _)a -io-)o L o.co5 mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/l K - Potassium mg/I Mg -Magnesium Ia-lo-10 1,toa mg/I Mn- Manganese.IQ -Io-lo o.00t, ma/I A YES _ NO) Ni- Nickel /d-/o-/e Pb -Lead /a-/o-yn 240.00S mg/I 4 0-o 5 mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) Sodro.. 1 a-10-10 ffc to ma 1 Q Se�en�un, la-lo-lo 40•cu5 em q 1JZ ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes-Y.(1) No _ (0) VOC '8 QL : method # = (pp) fh d CArtAr fhAt In Ohm hec%ni ..... r.......e-�-_ __-. �_,. _. .. ... .. ..! GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT Facility Name:_ Permit Name (if Contact Person: Yh(II Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County LDEIhl.wL1 Telephone N: 1�28r-15/e -Ll I I No. of Wells to be Sampled:,,. �7 „ Well Identification Nu er (from Permit): fY W - 10 Well Depth: I For Groundwater Treatment Systems ft. Well lameler: a in. Check One: ❑ Influent (98) Screened Interval: __A� �_ ft. to . tj A ft. ❑ Effluent (99) Depth to Water Level:/6-7 ft. below measuring point. Measuring Point (M.P.) is: a 13 It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 3 Dale sample collected:�a-%-/o Field analysis: pH _(G mac_ , Specific Conductance ' uMhos Temp. /7,2°C,Odor Appearance PARAMETERS (Samples for metals were collected COD mg/I Coliform: MF Fecal /100ml Coliform: MFTotal /loom[ (Note: Use MPH method for highly turbid samples) Dissolved Solids: Total la A-Io JOIG mg/l pH (when analyzed) la-')-)o te.q units TOC ia•aa-lo Gl, o mg/1 Chlorides -a/ -/o /o o mg/I Arsenic /3 -lo -/o L o 006 mg/I Grease and Oils mg/1 Phenol mg/I Sulfate 1 -/G /o mg/I ,3`7 Specific Conductance LlMhos Total Ammonia mg/I TKN as N mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT ft: Q 01)05(o?) 3 EXPIRATION DATE: 6 -.� 1 11 1 Non -Discharge UIC NPDES TYPE PERMITTED OPERATION BEING MONITORED Lagoon _Remediation: Infiltration Gallery Spray Field _Remediation: Rotary Distributor —Land Application of Sludge Other: NOTE• Values should reflect dissolved and colloidal concentrations. Date sample analyzed: S & P_ ar, t .1 Laboratory Name: LA)an-ec TCn Certification No. SO YES _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/1 Phosphorus: Total as P /0- -/0 LQ./bmg/l Orthophosphate mg/I Al -Aluminum /a -/o io n o &T mg/I Ba - Barium )-q-)6-16 12,00 mg/I Ca - Calcium Ja -16 -io f3. 305 mg/I Cal- Cadmium Z.240 /a <o ooA mg/1 Chromium: Total /a-do-io Ga.00s mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium /a-/o-In p )mG mg/I Mn -Manganese L oa5 mg/I KYES _ NO) Ni - Nickel /a -io -to <o oCG mg/I Pb -Lead /a 1D io L o ooS mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) fin ii)r. ia_Ie-/e 416,e1 ___ a -- Seltniitryl a-lo-/rl Gn OSm���Q ORGANICS: (GC,GC/MS,HPLC) (Specify test and method If. Attach lab report.) ROC ReportAttached? Yes X (1) No _ (0) BQ1_ : method #=/eaJp n method B = m.thnH If - GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Permit Name (if Contact Person:. T/)i/1t Well Locatiord Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County /flc 1 11t I I Telephone ft: 4a06 =�A No. of Wells to be Sampled: Well Identification Number (from Permit): inn 1 For Groundwater Treatment Systems Well Depth: fl. Well Iameler: �_ in. Check One: ❑ Influent (98) Screened Interval: It. to� ft. ❑ Effluent (99) Depth to Water Level: 06 ft. below measuring point. Measuring Point (M.P.) is: 73.lo ft. above land surface. Relative M.P. Elevation in R.: Gallons of water pumped/bailed before sampling: . 5 Date sample collected: /9 - —1 D Field analysis: pH_(0,9 , Specific Conductance uMhos Temp. 15. 1 °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT#: LA)&000S�1?03 EXPIRATION DATE: 5 Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED _ Lagoon _Remedialion: Infiltration Gallery Spray Field ' _Remediation: Rotary Distributor —Land Application of Sludge Other. NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: 5Ce &I ht Laboratory Name: 1 K)Ca�rn r -reCh Certification No. Sa PARAMETERS (Samples for metals were collected unfiltered YES _NO and field acidified _YES COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P_/a-/7-10 46.1 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total 129-o 1o?9 mg/I AI -Aluminum 12-1640 O,alo mg/I pH (when analyzed) /a 1 -`7 -/o P units Ba - Barium 19 -l0-/0 O.OIpq mg/I TOC a9-la 317D mg/I Ca-Calcibm_IB-10-fo /9t3 mg/I Chloride _19.91 -lb 2.3 mg/I Cd - Cadmium /a-/o-/0 4.0.00a mg/I Arsenic 19-10-10 <0.oa5 mg/l Chromium: Total /a-/0-/0 /-0•o0S mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate 1R -lb -tb 4/1.7 mg/I Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium '1840-10 ql&r mg/I TKN as N mg/I Mn -Manganese. J8-/O-10 0,151 mg/I NO) Ni - Nickel- /,9 /6-/e 40.005 mg/I Pb - Lead /a /O -/O G o oe)5 mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) � itlh / -la-10 molL S�lrni��m la-10-/D Go.oeS moL-Q ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes X (1) No _ (0) VOC pj QL, : method #= (oPIC D method # mpthnrl U — GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Permit Name (if Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County Ir I`-( )OL-Dt• Telephone #: gib$ -'7" No. of Wells to be Sampled: Well Identification Number (from Permit): tY1t/J-1�_ For Groundwater Treatment Systems Well Depth: 40W /3 ft. Well Diameter: in. Check One: ❑ Influent (98) Screened Interval: JJA ft. to_p?_it. ❑ Effluent (99) Depth to Water Level: -- Lf, 10 ft. below measuring point. Measuring Point (M.P.) is: S • (Q It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: _L Date sample Field analysis: pH (0, 8— , Specific Conductance Temp. 14•S -C, Odor /`/� Appearance _ uMhos DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT#: l.Jgoao5(p03 EXPIRATION DATE: Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED X Lagoon _Remedialion: Infiltration Gallery Spray Field _Remedialion: Rotary Distributor —Land Application of Sludge Other: NOTE Values should reflect dissolved and colloidal concentrations. Date sample analyzed: See Se ku ) Laboratory Name: li)ctIr TP )- Certification No. .z ( PARAMETERS (Samples for metals were collected unfiltered_A YES _NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total _ /l nnml Phncnhnn icr-rntnl oc D ko-/9.)ft ♦n./I ...,.e (Note: Use MPN method for highly turbid samples) Dissolved Solids: Totally-9-le 33o mg/I pH (when analyzed) /2-7-/n (018' units TOC_/�2-aa-)A / 7S mg/I Chloride Je a)-!o ! A mg/I Arsenic /S -/o -/ n 40.45C)5 mg/I Grease and Oils mg/I Phenol mg/1 Sulfate AP-/e -in /�/ m /I 9 Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Orthophosphate mg/I AI- Aluminum /2-Je-/o ,).1?6 mg/I Ba - Barium /a -/o -/d o- o roT mg/I Ca - Calcium /.P-/o-/D -sa 9 mg/I Cd - Cadmium /a ae -In Ge oo 0 mg/I Chromium: Total /2 -/D-!o Lo 005 mg/I Cu -Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg -Magnesium /2-/6 -/O E. o mg/I Mn - Manganese AR46-/0 ! 5? mo/I YES _ NO) Ni- Nickel -/;2-)o-in 40-065 mg/I Pb-Lead/,2-)D-/0 L6.60S mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/1 Other (Specify Compounds and Concentration Units) 5exi;sln. 10-I0-10 `l o mo Stltilium )9.-)D-/A Lo,�oS rnq P ORGANICS: (GC,GC/MS,HPLC) (Specify test and method N. Attach lab report.) Report Attached? Yes X (1) No_(0) VOC Q QL : method # = Ic a) D p method # method # GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Permit Name (if Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County Ir l`�kxu ue_l l Telephone 0: (i6ra' - No. of Wells to be Sampled: Well Identification Number (from Permit): 17Y1 W -/3 For Groundwater Treatment Systems Well Depth: Ab /Z it. Well lameler: Q in. Check One: ❑ Influent (98) Screened Interval: �R _ it. to AA ft. El Effluent (99) Depth to Water Level: L�_ft, below measuring point. Measuring Point (M.P.) is:(o ft. above land surface. Relative M.P. Elevation in it.: Gallons of water pumped/bailed before sampling: Date sample collected: /e Field analysis: pH /P -�q, Specific Conductance ' uMhos � Temp. 11¢Z OC, Odor Appearance /D DEPARTMENT Of ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT Y: I.V Q0065r0 L EXPIRATION DATE: S • a01 ! Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED _ Lagoon _Remedialion: Infiltration Gallery Spray Field _ Remedialion: Rotary Distributor _Land Application of Sludge Other: NOTE. Values should reflect dissolved and colloidal concentrations. Dale sample analyzed: 53 �e t J Laboratory Name: �ln*-z. eo k. Certification No. 56 PARAMETERS (Samples for metals were collected unfiltered -___YES _NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MFTotal /100ml Phosphorus: Total as P/2-/2-/e to.lt. m9 /I (Nose: Use MPN method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total /9-9-/o 590 mg/I Al -Aluminum La-/o •/o 0.05S mg/1 pH (when analyzed) 12 -?-1 D (,,.9 units Ba - Barium /a-/o -io o- 10 6 mg/1 TOC 10-dP-/o `i mg/I Ca - Calcium/a -ro -/A 33.9 mg/I Chloride /19 mg/I Cd-Cadmium /a-/o-/0 6.009 mg/I Arsenic /;) -/o -/o [ o.00S mg/I Chromium: Total la -to -lo Lo. oos mg/l Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate la-to-10��. 510-10 5 mg/I Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium MAO-lo a3I5 mg/I TKN as N mg/I Mn - Manganese la-to-lo 1 r a I mg/I _,0_YES _NO) Ni - Nickel /a-/A-10 <0.0o5 m I Pb - Lean /a -/o -/o o .006 mg/1 Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) Sel��;���1��0��<0 ooSS m ORGANICS: (GC,GC/MS,HPLC) (Specify test and method 0. Attach lab report.) Report Attached? Yes__,X_(1) No _ (0) VOC 2 GI_ : method 0= Iva lO 0 method 0 = method It = GROUNDWATER QUALITY MONITORING: COMPLIANCE Facility Name: — Permit Name (if t Facility Address: Well Location/ Site Name: •� •Cu SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County f f I" 4101i1e 1' Telephone #: $a$ • rl S(c - No. of Wells to be Sampled: Well Identification Number (from Permit): N - t4 Well Depth: is It. Well Diameter: a Screened Interval: IA It. to A It. DepthN_ to Water Level:'1-a_ft. below measuring point. Measuring Point (M.P.) is: r_ It. above land surface. Gallons of water pumped/bailed before sampling: ec. Field analysis: pH—lat00, Specific Conductance , Temp. /S -C, Odor A PARAMETERS (Samples for metals were collected COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total_J9-4-1n 935 mg/I pH (when analyzed) /9-7-/0 61F units TOC -5.0-5 mg/I Chloride 12-a\-1O 4S.0 mg/) Arsenic J6-to-lo Lo.005 mg/I Grease and Oils mg/) Phenol mg/I Sulfate IQ-t n -f o 410 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I For Groundwater Treatment Systems in. Check One:❑ Influent (98) ElEffluent (99) Relative M.P. Elevation in ft.: Date sample collected: /a -/0 uMhos ppearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PER ITN: LOG.0o0 toll, EXPIRATIONDATE: -a011 Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED _,X Lagoon _Remedialion: Infiltration Gallery Spray Field _Remedialion: Rotary Distributor —Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: Sep 13f l n J Laboratory Name: t. c= , aenh Certification No. SD tered_�A YES _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P 12-11-ID <o.lb mg/I Orthophosphate mg/I Al - Aluminum IP-10 -lo o, a33 mg/1 Ba-Barium t9-lb-lo 0.140 mg/I Ca-'Calcium_Ia-10-10 S6 mg/I Cd -Cadmium I21-10-1 tj L-o. 00a mg/I Chromium: Total 19-lo-1 o 4 C, 00S mg/I Cu - Copper - mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium la-10-l0 5"1 8 mg/I Mn - Manganese _I a-10 -10 6 LI to mg/I YES _ NO) Ni- Nickel Go oo mg/I Pb- Lead /2.-10-10 Go oD mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ion, I'a-In-In r.Jl .. p Selanlnr„ 19-10-10 <0.00[ m�lyD,- ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes X (1) No_(0) VOC B QL : method # = (oa 10 CD method # = method # = GW-59 Rev. 03/2000 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FO Facility Name:_ Permit Name (if Contact Person: — Well Location/ Site SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County Mcf)IO41s/) Telephone #: !RAk:056 -4!/ No. of Wells to be Sampled: Well Identification Number (from Permit): --Zr) W -/5 For Groundwater Treatment Systems Well Depth: 1(10 ft. Well Diameter: _a— in. Check One: ❑ Influent (98) Screened Interval: —A) jR ft. to AAA ft. ❑ Effluent (99) Depth to Water Level:Z1, 1� ft. below measuring point. Measuring Point (M.P.) is: -9 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: I Date sample collected: 1A-7-10 Field analysis: pH 0 S Specific Conductance uMhos Temp. ' r5'C, Odor Appearance PARAMETERS (Samples for metals were collected COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 19-9-16 -Ago mg/I PH (when analyzed) )5-)-10 6-1 units TOC NW;Lg-to a.-)9 mg/I Chloride IA-2)-)o 45.0 mg/I Arsenic 19-I6-10 40.00S mg/I Grease and Oils mg/I Phenol mg/I Sulfate 19-10-10 1'S•1 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I PERMIT #: 1.J Non -Discharge DEPARTMENT OF ENVIRONMENT t; NATURAL RESOURCES WATER DUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER EXPIRATION DATE: S -a6 { ) NPDES TYPE OF PERMITTED OPERATION BEING MONITORED —X Lagoon _Remedialion: Inlillialion Gallery Spray Field _Remedialion: Rotary Distributor —Land Application of Sludge Other: _ NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: Sce f6P lA •) Laboratory Name: Certification No. so lered /% YES _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P_la-)0-/D 4o•Ib mgll Orthophosphate mg/I AI-Aluminum)a-)6-to 46,060 mg/I Ba - Barium 19 -16-16 0.115 mg/I Ca - Calcium IB-Io-lo '7q.o mg/I Cd - Cadmium1a-16-1 o 40,00P mg/I Chromium: Total la-lo-lo /0,005 mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg -Magnesium 1a-16.-16 310 mg/I Mn- Manganese 13-1DAD a.15 mg/I YES _NO) Ni- Nickel Y9-l0-/o 46,066 mg/I Pb - Lead lA-10-1o 40.00s mg/l Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) _ odium I'a-t0-16 14.$ mgT elenl _, 14-10-I� Lo oo< met ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes_X_(1) No _ (0) VOC f,. 0 L, : method # = Jo alb D method # = method N = I. Volatile Organics Quantitation EPA Method 6210D Limit MW2 MW10 MWIl. MW12 MW13 MW14 MWIS Parameter (oob) (pPb) (vobl {pobl oahl (oob) (P�i iP� 1,1-Dichlomethane 2,2-Dichloropropane Chloroform 1,1,1-Trichloroedwe I,l-Dichloropropene Carbon Tetrachloride Benzene 1,2-Dichlomethane Trichloroethene 1,2-Dichlompmpane Dibromotnethane Toluene 1,1,2 Trichlomedtane 1,3-Dicbloropropane Tetrachloroethene 1,1,1,2-Tetrachlomethane 1,1,2,2-Tet meW omethane 1,2,3-Trichloropropane Hezachlorobutadiene Bmrmbemene Ethylbenzene Styrene 2-Chloromluene 4-Chloromluem Tert-Butylbenzene Sec-Butylbenzene 1,4-Dichlombenzene 1,2-Dichlombenzene Total Xylenes I-Propylbemene N-Propylbencene 1,3-Dichlorobenzew Dibrornochloromethane Diddoroditluoromethane Chloroaethane Vinyl Chloride Brommrethane Chloroethane Trichlorofluoromelhane I,1-Dichloroethene Methylene Chloride Tr I,2-Dichloroctheae Cis-1,2-Dichloroethcue Bmmodichlomrnethwe Bromochloromethane Cis-1,3-Diebloropmpene Trans-1,3-Dichlompropene Methyl-Tert-Butyl ether (MTBE) Isopropyl ether (IPE) Dilution Factor Sample Number Sample Date Sample Time (hrs) Analyst Date Analyzed Time Analyzed 0.5. 0.5 0.5 0.5 0.5 0.5 0.5 0.5 05 0.5 0.5 0.5 OS 05 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 OS 0.5 0.5 0.5 0.5 OS 0.5 0.5 0.5 0.5 0.5 0.5 OS 0.5 0.5 0.5 0.5 0.5 0.5 5.0 5.0 690868 690869 690870 690971 690872 690873 690874 12/07/10 12/07/10 12/07/10 12/07/10 12/07/10 12/07/10 12/07/10 0700 0730 0800 0830 0900 0930 1000 NM NM NM NM NM NM NM GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Permit Name (if Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County I I ,-- i C) CI Telephone #: 0'6* -7'1, Y No. of Wells to be Sampled: Well Identification Number (from Permit): )Y)t O 9 Well Depth: 7 S it. Well Diameter. _1,0 Screened Interval: A )1 A It. to U) it. Depth to Water Level: 32,3 _ft. below measuring point. Measuring Point (M.P.) is:_Q�j ft. above land surface. Gallons of water pumped/bailed before sampling:9 Field analysis: pH I- - 1 Specific Conductance Temp. °C,Odor A PARAMETERS (Samples for metals were collected COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 8-Cl -1 D � 1 mg/I pH (when analyzed) ? -tU l b units TOC _ u a 3 -t u 11 I 0 mg/I Chloride_ s-lz-la 4 S.o mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate ems_- C S mg/l Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I For Groundwater Treatment Systems in. Check one: ❑ Influent (98) ❑ Effluent (99) Relative M.P. Elevation in ft.: _� Date sample collected: 3 -10 uMhos Poearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT#:WLYQCb5(oC)3 EXPIRATIONDATE: ,S-a00 Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED -- Lagoon _Remedialion: Infiltration Gallery Spray Field _Remedialion: rn Rotary Distributor -Land Application of Sludge>33 O Other: NOTE: Values should reflect dissolved and . lu A7 colloidal concentrations. to a O tp Date sample analyzed: See Q001_J 03 PV Laboratory Name: Wo=k itc 'TPch o rO o Certification No. 50 )--� tered A YES _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P g It -1D blb mg/I Orthophosphate mg/I AI - Aluminum 2 4o -1 D 9.: 5 mg/I Ba-Barium� -to -10 n•Olq mg/I Ca -Calcium to-tD 1Q,4 mg/I Cd - Cadmium S -to - I D G n CCD mg/I Chromium: Total (o-ID GG,bUS mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium 4-ln -1a la.(0 mg/I Mn - Manganese 10 U, ioi� mg/I _YES NO) L— Ni - Nickel 8 la -Ib 0•007 mg/I Pb - LearL x-(c -Ib O'Cao mg/( Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) `�nrti�lm -to-lc) O `1fr tmc 0 rng Q ScIPniOm `t -lo -t Za•Cos ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes_(1) No_(0) VOC : method # = method # = method If = GROUNDWATER QUALITY MONITORING: COMPLI Facility Name:_ Permit Name (it Facility Address: Well Location/ Site CE REPORT FORM SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County. r T klL JN.1 Telephone 6: to No. of Wells to be Sampled: Well Identification Number (from Permit): MV) -I O For Groundwater Treatment Systems Well Depth: fl. Well Diameter: i in. Check One: ❑ Influent (98) Screened Interval: 0 Il. to /J (� it. ❑ Effluent (99) Depth to Water Level: )to below measuring point. Measuring Point (M.P.) is:2LLa 1t. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: ' Date sample collected: - ID Field analysis: pH 'I. 1_ , Specific Conductance Umhos Temp. \HOC, Odor Appearance PARAMETERS (Samples for metals were collected COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /loom[ (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total S:9-ID ol-yD mg/I pH (when analyzed) �s -3 -to units TOC !3-a3..11 I n mg/I Chloride Ss -it) 13.0 mg/I Arsenic 4} l0 -1 O /,o.005 mg/I Grease and Oils mg/I Phenol mg/I Sulfate Fs -1c-lid 03 mg/I Specific Conductance uMhos Total Ammonia mg/1 TKN as N mg/1 GW-59 Rev. 0312000 SEP207010 Ittformatfon Processing U Dlrvq/R0 nit PERMIT 0: W Non -Discharge DEPARTMENT OF ENVIRONMENT& NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER EXPIRATION DATE: S -a01 1 NPDES Magoon F PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field . _Remedialion: Rotary Distributor _ Land Application of Sludge Other: NOTE• Values should reflect dissolved and colloidal concentrations. Date sample analyzed: Scb Laboratory Name: t �J (n�cr A T P n Certification No. SO tered & YES _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P-2-II-10 40-1 mg/I Orthophosphate mg/l Al- Aluminum 2 -to-1 l0 01119 mg/I Ba - Barium a -Lo-lb mg/I Ca -Calcium ',--Le -to 0•`190 mg/I Cd - Cadmium S -to -IO Lo. (` ,)q mg/I Chromium: Total 2-10-10 40.CD5 mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium S b-ID 01,240 mg/I Mn - Manganese a-L -10 4C) s mg/I n YES NO) Ni - Nickel_ -(c -IU l-Od)(-S mg/I Pb - Lead $ (c -10 LO Uo5 mg/I Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) �orltL)nti R-40-10 CHI rr 0 Se\en;Om e PL ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) ReportAttached? Yes_([) No _(0) VOC : method a = method N = mclhnrt ll — GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: - Permit Name (it Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County. it Y') I ,,-y Telephone No. of Wells to be Sampled: Well Identification Number (from Permit): (Y\W -11 For Groundwater Treatment Systems Well Depth: I�S��p,'ft. WellDiameter. in. Check One: ❑ Influent (98) Screened Interval: ==fly ft. to it. El De Ih to Water Level: � i Effluent (99) P ft. below measuring point. Measuring Point (M.P.) is: tL it. above land surface. Relative M.P. Elevation in It.: Gallons of water pumped/bailed before sampling:. S Date sample collected: g -3 - I Field analysis: pH (3.10 , Specific Conductance uMhos Temp, f °C, Odor Aooearance PARAMETERS (Samples for metals were collected COD mg/I Coliform: MF Fecal /100m1 Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total k -Q -1 l> R 9 mg/I pH (when analyzed) 2-3 -I(> (n . Ln units TOC -10 --i,13 mg/I Chloride 19-?, mg/I Arsenic 5s-( - 10 �D.CO5 mg/I Grease and Oils mg/I Phenol mg/1 Sulfate 2 -(o -10 3 mg/1 Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/1 DEPARTMENT OF ENVIRONMENT 3 NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMITfl:-'Ja000S(o03 EXPIRATIONDATE: S-380 Non -Discharge UIC NPDES P RMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field _Remediation: Rotary Distributor —Land Application of Sludge Other: NOTE• Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: SPr Laboratory Name:—L-L>Ct- (' eC-1 1 Certification No. .5D YES _NO and field acidified Nitrite (NO2) as N mg/1 Nitrate (NO3) as N mg/I Phosphorus: Total as P 8-11 )0 03img/I Orthophosphate mg/I AI - Aluminuml-ID n, t-f10 mg/I Ba - Barium - -10 n, I I mg/I Ca - Calcium S -Lo -10 I I mg/I Cd - Cadmium Lo 1 n L I� mg/I Chromium: Total �s to -ID D, oOS mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg Mg - Magnesium 8 -(D-10 10,(03 mg/I Mn-Manganese 2;-(o-ID 0-a- mg/I A YES NO) Ni - Nickel _R do -10 / ,b(s mg/I PID - Lean Sn -(n -I o mg/I Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) SCxjiu)rr) "�_-(c-)U 4SIav_ncII �-Nek- lit�m k - n-1D Z0•` S Ma Q ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) ReportAttached? Yes_(1) No _ (0) VOC : method tl = method 0 = method N = GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Permit Name (if Well Location/ Site SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County rrlc i• xAQe* I Telephone It: n, No. of Wells to be Sampled: Well Identification Number (from Permit): fhlal-la For Groundwater Treatment Systems Well Depth: 13 ft. Well Diameter. in. Check One: ❑ Influent (98) Screened Interval:A.)).A- ft. to_A)) [-1 It. ❑ Effluent (99) Depth to Water Level:q , L, ft. below measuring point. Measuring Point (M.P.) ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 9 Date sample collected: $ -3 -10 Field analysis: pH D 1 , Specific Conductance uMhos . Temp. t °C, Odor ADoearance PARAMETERS (Samples for metals were collected COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPH method for highly turbid samples) Dissolved Solids: Total S'4-10 109n mg/I pH (when analyzed) 4;2-10 ''1 1 units TOC mg71 Chloride -1 - tp 4 r 0 mg/I Arsenic _� -(v -ICE 40.005 mg/I Grease and Oils - mg/I Phenol mg/I Sulfate Ln -I I b mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT n: LOU OW&,303 EXPIRATION DATE: 5 •610 11 Non -Discharge UIC NPDES TYPE OF PERnMECT D OPERATION BEING MONITORED —� Lagoon Remedialion: Infiltration Gallery Spray Field Remedialion: Rotary Distributor _ Land Application of Sludge NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: V) e Laboratory Name: U)11 oa TP Certification No. .SO tered_ A YES _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P S-II-/0 6,33 mg/I Orthophosphate mg/I At - Aluminum Sl-10-10 LO,050 mg/I Ba - Barium n, Oq 1 mg/I Ca - Calcium 113r 9 mg/I Cd - Cadmium Q, o09 mg/I Chromium: Total -6-)0 4n•D05 mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium -U-10 11 In mg/I Mn - Manganes( - mg/I f YES _ NO) Ni- Nickel S -LD-Itb 0. `C-1.0 mg/I Pb - Lean Ss -la -10 mg/( Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) -10 I1�5 ma 1 J. _SP1Pr\i Jn� ' -lo -Its �0.(.Y�S ✓r,c,. ,�. ORGANICS: (GC,GC/MS,HPLC) (Specify test and method If. Attach lab report.) Report Attached? Yes_(1) No _ (0) VOID : method M = method # = method N = z a GW-SU SEP zolo Signature ofPermillee (Or AuthorizedAgent) - Rev. 03/2000 Infarm�lt.,.. o--- GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Permit Name (if Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County- )Telephone f): M=I&, No, of Wells to be Sampled: Well Identification Number (from P89�T7 For Groundwater Treatment Systems Well Depth: 1p 1CheckOne:❑ InflUent (98) Screened Interval: It. ❑ Effluent (99) Depth to Water Level: ft. below measuring point. Measuring Point (M.P.) is: -5 It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 15 Date sample collected: � •3 -1 D Field analysis: pH • to Specific Conductance uMhos Temp. °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT 0: W(AbC05tP03 EXPIRATION DATE: 5-20 1 1 Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED x Lagoon Remediallon: Infiltration Gallery Spray Field _Remediation: Rotary Distributor —Land Application of Sludge Other. NOTE, Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: • Y'P Below low Laboratory Name: 1 JC =CC -I-) Certification No. 5D PARAMETER$ (Samples for metals were collected unfiltered_-1, YES _NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N m /I Coliform: MF Total /100ml Phnsnhnnrs• Tntal aq P 9-11-11) fi.`XI ,, /l (Note: Use MPN method for highl turbid samples) Dissolved Solids: Total -- -)0 51r7 mg/I pH (when analyzed)_`�-3-16 h l units TOC_3-)c) O at^ mg/I Chloride �`-1°s-10 C. o mg/I Arsenic a-(o-IG mg/I Grease and Oils mg/I Phenol mg/I Sulfate ';,-D -Irt G� mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Orthophosphate mg/I Al - Aluminum 2-(n-10 C O. DSG mg/I Ba - Barium V -(n-to 0. 131 mg/I Ca - Calcium_A -to -10 2 1 mg/I Cd - Cadmium R-Io -ID Lb -La mg/I Chromium: Total 8-(o-10 L D, mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese VS -(n-10 mall m1orrnation Processing Uno YES NO) Ni - Nicker to IO C,CCOS mg/I Pb - Lean-1.,-IO ��'S mg/I Zn - Zinc mg/l Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) • � 1 ORGANICS: (GC,GC/MS,HPLC) (Specify test and method If. Attach lab report.) Report Attached? Yes-_(J) No _ (D) VOC : method N = method N = method H = GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ ( Permit Name (if diff Facility Address:_ Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type PERMIT #: County 17\� VGWPI Telephone w S O,S 75 b No. of Wells to be Sampled: Well Identification Number (from Permit): MirJ - For Groundwater Treatment Systems Well Depth: r1 it. Well Diameter, to in. Check One: ❑ Influent (98) Screened Interval: N ft. tom DeDepth to Water Level:- r� 1 ft.❑Effluent (99) P _ft. below measuring point. Measuring Point (M.P.) is:` a� ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: (00 Date sample collected:14 -6 •-1 C7 Field analysis: pH I ' , Specific Conductance ' Temp. IS °C, Odor Appearance PARAMETERS (Samples for metals were collected COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 4f-io lo'2 mg/I pH (when analyzed) S-.bG units TOC �/ -/'s -r o 4 /. o mg/I Chloride _�/ / / l0 5 mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate y-9-/[) 1-10.y mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Rev. 03/2000 uMhos DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER , EXPIRATION DATE: Non -Discharge UIC_ NPDES _ TYPE OF PERMITTED OPERATION BEING MOI• k Lagoon Remedialion:lnfilla Spray Field Remediation: Rotary Distributor _ Land Application of Other: NOTE' Values should reflect dissolved and . m p {� colloidal concentrations. p cL -_2 �} Date sample analyzed: 5ce 1➢Y'�rlls) .+ O N 0 fv Nra G Laboratory Name:—10(14917 'TPPh to n Certification No. SO n .YES _NO and field acidified YES -A_ NO) Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P 9_ -1 o I ,l to mg/I Orthophosphate mg/I AI - Aluminum y -9 to i -i3 mg/I Be - Barium 9-t0 d•tnty$ mg/I Ca - Calcium y - 9 -)a Q'9, a mg/I Cd - Cadmium y 4-In Gos_ . o mg/I Chromium: Total `/-y-lb La, Uo 5 mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - MaaLLesium_ �� . I mgll Ni - Nickel `a -9-i6 Lo. o05 mg/I Pb - Lean y -9 /o Q' 01 / mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/1 Other (Specify Compounds and Concentration Units) r-I -q-to u5mct 1 Sc Iff ear LA -Q -I O L.O. alai; 1 ORGANICS: (GC,GC/MS,HPLC) ' (Specify test and method #. Attach lab report.) Report Attached? Yes_(1) No _ (0) VOC : method # = SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Print Clearly or Type __ Facility Name:_ Permit Name (if a.ol County f>1 Contact Person: t nio ' Telephone S(n • Well Location/ Site Name: Pd J2��"Y_ 1?608 No. of Wells to be Sampled:_ e J 1-am Well Identification mber(fromPermit): MIA) -ID For Groundwater Treatment Systems Well Depth: 1�! 4it. Well DjryMIA)Diameterin. Check One:❑ Influent (98) Screened Interval: zU A ft. to 1v�7—_ ft. ❑ Effluent (99) Depth to Water Level: f ' ft. below measuring point. Measuring Point (M.P.) is:'r •. It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 1_ Date sample collected: t -l9 10 Field analysis: pH -1. ` Specific Conductance UMhos Temp. I l 'C, Odor Appearance PARAMETERS (Samples for metals were collected COD mg/I Coliform: MF Fecal A00ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 4-9' /n 035 mg/I pH (when analyzed) -),:LD units TOC L-f -/•5 -i(` 4 1 n mg/I Chloride '/-Iy-Ili L') o mg/I Arsenic LA --CI -I u L 0. WS mg/I Grease and Oils mg/I Phenol mg/I Sulfate L4 "i -1 is 13 y mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Rev. 03/2000 DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: L0 G00051r U3 EXPIRATION DATE: 5 '�1 O t Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED —� Lagoon _Remedialion: Infiltration Gallery Spray Field ' _Remediation: Rotary Distributor —Land Application of Sludge NOTE' Values should reflect dissolved and colloidal concentrations. Date sample analyzed: SnP l_�r•�/r ' Laboratory Name: _I A)41 P r `rP C h Certification No. 5 f_� tered_A YES _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as LO-II`rn /I Orthophosphate mg/I AI - Aluminum -9 / o < 0, oSCD mg/I Ba - Barium 14 -9 -1 v L p oDC mg/I Ca- Calcium _y-9-/0 /+39 mg/I Cd - Cadmium- q - 9 -1 o <a. 00a mg/I Chromium: Total 4J-9-/o /,o.o65 mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium 43 0.936 Mn Manganese `) - -/o 44),005 mg/I - mg/I _X YES _ NO) Ni- Nickel `4-4-JD zp:tiOS mg/1 Pb - Leant 4-9-/o 40,00S mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) oA orn y -Q -1 0 9 n.Ld rn l 4 c) 00A rn (I ORGANICS: (GC,GC/MS,HPLC) (Specify test and method If. Attach lab report.) Report Attached? Yes -_(I) No _(0) VOC method # = method # = method # = -/ v GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Permit Name (if Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type _ . County 1Yne 1 Telephone #: R �n --7'sto No. of Wells to be Sampled: Well Identification Nu ber (from Permit): Mt For Groundwater Treatment Systems Well Depth: I it. Well Diameter: `,) in. Check One: ❑ Influent (98) Screened Interval: ft. to it. '11T 0 Effluent (99) Depth to Water Level: It tH i ft. below measuring point. Measuring Point (M.P.) is•L•1.n ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: I Date sample collected: LA -6 -16 Field analysis: pH 1� -i_ , Specific Conductance uMhos . Temp. �°C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER DUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: LO (S L'4)" La(N 3 EXPIRATION DATE: c�-,3L 1 I Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED —� Lagoon _Remedialion: Infiltration Gallery Spray Field ' _Remedialion: Rotary Distributor Land Application of Sludge Other: NOTE' Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: Ste Laboratory Name: bray P r '-re Cn Certification No. _S(7 PARAMETERS (Samples for metals were collected unfiltered -YES _NO and field acidified COD mg/I Coliform: MF Fecal /100m1 Coliform: MF Total /100ml (Note: Use MPH method for highly turbid samples) Dissolved Solids: Total 4-9-A) /63 mg/I pH (when analyzed) (�.'7� units TOC -%-l.5 iil C 9G mg/I Chloride %-1-V- n 91 ` mg/l Arsenic 4 -R - I o c , 005 mg/l Grease and Oils mg/I Phenol mg/I Sulfate q --9 -10 o mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P q a7 Id U,a� mg/I Orthophosphate mg/I Al - Aluminum i4 -Q_I o qSb mg/I Ba - Barium -(P -R) t).n 7 o mg/I Ca - Calcium Ll -A -1 b /S '7 mg/I Cd - Cadmium y -q -1 r3 40, uoa mg/I Chromium: Total 'i o1-lb 4o•60S mg/I Cu - Copper mg/I Fe - Iron mg/1 Hg - Mercury mg/1 K - Potassium mg/I Mg - Magnesium 4 P- ifs 4411 mg/I Mn - Manganese 9 -9.1 co d Imo' -moil YES _ NO) Ni - Nickel ` "9 /o 0,0/'7 mg/I Pb - Lead l -9 -lo 46,005 mg/1 Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) .Srct i 'C rv� LA -9 -10 13 . g- m o L eler,i Jn., -rl -Q -Iy LU.Ji:S m��L ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) ReportAttached? Yes --(I) No_(0) VOC : method # = 01-1(f Rev. 03/2000 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT Facility Name: - Permit Name (if Contact Person: u n • \ Well Location/ Site Name: Please Print Clearly or Type _ County i f�Lp 4 aC:,uJ 2 I 1 Telephone #: _Orris --)Ste, .LI W No. of Wells to be Sampled:.. `7 ,. Well Identification Number (from Permit)1: 1Q - 02 Well Depth: j _ft. Well Diameter: Screened Interval: d) iT ft. to r i ]<= ft. DeDepth to Water Level: P _�_,�ft. below measuring point . Measuring Point (M.P.) is: A ft, above land surface: Gallons of water pumped/bailed before sampling: Field analysis: pH , t_ , Specific Conductance . Temp. I 'A °C, Odor A PARAMETERS (Samples for metals were collected COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPH method for highly turbid samples) Dissolved Solids: Total-/-4-10 9V,12 mg/I pH (when analyzed) l,-f; units TOC _ -el-IA • !r, S n4 mg/I Chloride i/S mg/I Arsenic 4 -t, - I h,OOS mg/I Grease and Oils mg/I Phenol mg/I Sulfate it) ^ (o.L4 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I For Groundwater Treatment Systems in. Check One:❑ Influent (98) ❑ Effluent (99) Relative M.P. Elevation in It.: �_ Date sample collected: LA - -1 O uMhos ooearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER EXPIRATION DATE: Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED _ Lagoon Remediation: Infiltration Gallery Spray Field - _ Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal. concentrations. Date sample analyzed: 5ef ipwI , \ LaboratoryName: k.A=j-er"iF(h Certification No. so .YES _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P 4 -��-I b �,a�ng/I Orthophosphate mg/I AI - Aluminum -1r -Ct -ID Ol Dloi`s mg/I Ba - Barium 14 -q - 0 6, Ock q 10 Ci(a,SS mg/I Ca - Calcium -Q - mg/I Cd - Cadmium 4 -61' -l0 1-6,n0a mg/I Chromium: Total 4 -q -It) L0, 0D8 mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg -Magnesium -it) la,d_ mg/I __).YES NO) Ni- Nickel 5'-9-/o n,UDC mg/I Pb - LearL mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) SAr.1ioo" 4-Q- I O I I S rnrA I Selen�o;r 4-q-16 L.b,O mtJ, L ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes—_(1) No _ (0) VOC : method # = method # = method If = ++edify that, lathe best of my knowledgeand belief, the information submiffedin this reportfs true, accurate,.and complete, and that thedaboratory analyficafdata was produced using approved.methods ofanalysis by a.North Carolina DWO (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including.the possibility of fines and imprisonment for knowing violations. r 41 11, 1 111 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: — Permit Name (if Facility Address: Contact Person:- Well Location/ Site Please Print Clearly or Type County Inc: 1-)Ch Ze t� Telephone #: S91 - % No. of Wells to be Sampled: Well Identification Number (from Permit): Mt, -IS For Groundwater Treatment Systems Well Depth: 1 S it. Well Diameter. 2_ in. Check One: ❑ Influent (98) Screened Interval: —ft. to it. ❑ Effluent (99) Depth to Water Level: (,-'s it. below measuring point. Measuring Point (M.P.) ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: _a_ Date sample collected:t-I -(o -10 Field analysis: pH S�i • , Specific Conductance ' uMhos Temp. —lam 'C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: W (AUL'USIsG 0 EXPIRATION DATE: i 1 Non -Discharge UIC TYPE OF PERMITTED OPERATION BEING MONITORED X Lagoon Remedialion: Infiltration Gallery Spray Field _Remediation: Rotary Distributor _Land Application of Sludge Other: _ N TE� Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: ` Pe f eti t,,j Laboratory Name: _ + pc- Tev Certification No. so PARAMETERS (Samples for metals were collected unfiltered A YES _NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /loom] Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as PQ-r97-Ih r„Igmg/I (Note: Use MPN method for highly turbid samples) - Orthophosphate mg/I Dissolved Solids: Total 4-91) a95 mg/I Al - Aluminum -10 D,D .5 mg/I pH (when analyzed) 4-/3-1� 5 units Ba - Barium I-- --) p 0 ,O mg/I TOC ,t-� mg/I Ca - Calcium � -�f -f I i mg/1 Chloride -4 / /-/i) Iq Q mg/I Cd - Cadmium -q -10 L-D coo mg/I Arsenic -1 -Q - ID 4C> OU mg/I Chromium: Total 4-cl'-I0 40.ODS mg/I Grease and Oils mg/I Cu - Copper mg/l Phenol mg/I Fe - Iron mg/I Sulfate 4 -G - tb mg/I Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium ` -C1- t? 10, mg/I TKN as N mg/I Mn— Mang- ese --4 -q -16 0, laCQ m ) 'YES NO) Ni - Nickel -Ip LU.GOS mg/I Pb - Lead C/ -r7 -1 O 4. O ci.5 mg/1 Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) Srkd I iXh -c1 -to (nC, Mra L, me L Scler,, o, , ct-IU Z.n:005 ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) ReportAttached? Yes --(I) NO_(0) VOC : method # = SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM rMl UI r uyrVnmAlIL)N Please Print Clearly or Type Facility Name:. (COCAS AIN-\jC1 C&t Permit Name (if different): Facility Address:_'i) h I'D 3(e�b (Ylr ! hr1 ISveep . r f Est 15 c1.pt County C P l \ Contact Person: ht(Y + ti !�[ 1 i� �r� Telephone #: Smla -7tL -U 11 1 Well Location/ Site Name: -3Y0� pry i-ern + No. of Wells to be Sampled: (from Permllj Well Identification Number (from Permit): IV)L'0-10 ForGroundwaterTreatmentSystems Well Depth: I s ft. Well Diameter: � in. Check One: ❑ Influent (98) Screened Interval: AlInAl It. to ;vl 8 tL 11 Effluent (99) Depth to Water Level: _ 7 ft. below measuring point. Measuring Point (M.P.) is:7+5 ` ft. above land surface. Relative M.P. Elevation in N.: Gallons of water pumped/(bailed before sampling: '3 Date sample collected: L -(o -it," � Field analysis: pHL�'i , Specific Conductance ' uMhos Temp. ll— °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER 3 EXPIRATION DATE: Non -Discharge NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Y Lagoon Remedialion: Infiltration Gallery Spray Field Remedialion: Rotary Distributor _ Land Application of Sludge Other: NOTE' Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: �See a2tn ,' Laboratory Name: 1100 1 er Tech Certification No. 5 PARAMETERS (Samples for metals were collected unfiltered_ YES _NO and field acidified COD mg/1 Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MFTotal /100ml Phosphorus: Total as Psi /D i)0013mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total f-9-/0 45-6 mg/I Al -Aluminum 9 -9 J U / , 93 mg/I pH (when analyzed) 4-13•-io ( 4 1 units Ba -Barium 13S mg/I TOC S•3`- mg/I Ca -Calcium k(c,0 mg/I Chloride 7 I '" /i 45. o mg/I Arsenic -61 -)t7 Cd - Cadmium, -9 -10 4-9-10 [.a 00q mg/I rrig/I Chromium: Total LOr0o5 mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate mg/I Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium 4- --)O S3. 1 mg/I TKN as N mg/I MrT—M nga Cl-/0 orygl/ mg) Rev. 0312000 AYES NO) Ni - Nickel 4 - -I1) L�",UGC mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) rng Se I eni om -9-/rl 4 r/),nos m /L ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes_(1) No _ (0) yOC : method # = method # = method # = ry SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Prinf Clearly or Type Facility Name:_ 0rl`tA-,, AfY-tociortn Permit Name (if different): Well Location/ Site Name: County MO UntOe't Telephone #: �aa-,),�i' No. of Wells to be Sampled: Well Identification Number (from Permit): M W - 1 5 LForundwater Treatment Systems Well Depth: ft.WellDiameter: 1 in.One: ❑ Influent (98) Screened Interval: N A• ft. to I , 44 ft. ❑ Effluent (99) Depth to Water Level: 5 ft. below measuring point. Measuring Point (M.P.) is: 16 ft. above land surface. Relative M.P. Elevation in fl.: Gallons of water pumped/bailed before sampling: 31 LI Date sample collected: Field analysis: pH� , Specific Conductance uMhos Temp. 12'C, Odor Appearance PARAMETERS (Samples for metals were collected COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total q -9 -JD 5 ) to mg/I pH (when analyzed) I (n \ units TOC `/ - ) 3 .-11) D I t S mg/I Chloride 9-1 4 -1 n Z-5.0 mg/1 Arsenic _J -fi -in S0.0051 mg/I Grease and Oils mg/I Phenol mg/I Sulfate 1-9 -) 6 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I -r, - DEPARTMENT OF ENVIRONMENT 8, NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: W aoOG5 ia03 EXPIRATION DATE: _S - R01 1 Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED X_ Lagoon Remediation: Infiltration Gallery Spray Field Rotary Distributor Other: Remediation: Land Application of Sludge NOTE• Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: 'Sec. Laboratory Name:-+-i>rk� Tech Certification No. 5�, tered/\ YES _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/1 Phosphorus: Total as P � -'q�-/o co.11�gA Orthophosphate mg/I AI - AluminulT� 4 -R -1 t) 40,050 mg/I Ba -Barium �l -Q -10 C> UPS tG mg/I Ca - Calcium 9 -q - f D g P S% mg/I Cd - Cadmium ! -C —l) <0' 00 mg/l Chromium: Total q -q -11) 4b. UO5 mg/I Cu - Copper. mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesfum <.-Q -/0 YES NO) Ni - Nickell-9-10 0, oc>1 mg/I Pb - Leart -C/ -l0 4 Q , 005 mg/I Zn - Zinc mg/1- Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes_(1) No_(0) VOC : method # = method # = method # = GW-59 Rev. 03/2000 -��r. vtrirLitllVl 1v to ruK'1' FORM Permit # !✓ 06 60 5-403 (Submit one each nroaitarfng period will, Gil=59 jorms.J 1 Enter date monitoring results were due. ( 1 Will this monitoring report (GW59 and GW-59A) YES be submitted after the established due date? NO i Was any required information missing on the GW-59 report forms? YES NO IF the answer to question 1 or 2 is 'YES", list in the space provided below the welt identification number(sJ and explain the problems encountered in obtaining the required information. Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing identification plate, area overgrown, etc.)? Ifthe answer is •'Yes'", YES NO contact the Regional Officefor guidance. 4; Are any monitored constituents equal to or above the established standards? Y NO If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES "list the affected wells individually with constituents) and concentration(s) exceeding standards in the space provided below., )TI A , G•S 3 /rr [u A 11n 0 XL 'ir7 /a, /s" : M-1 : 0.7 Y d I" �ryrtr: a•99s mw-ID 7135 X0 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is NO ,skip to " section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceedi g standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). 1 tJ-2 = /NA' o•m7rr ro.3sy o M4/nr° inwfo = Tr45 S.?o. W 12: m-v 22- Su/F 37e 1"W 13 = Mn d•yvy Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES'; a groundwater quality problem maybe occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO'; monitoring wta!!s maybe improperly located; contact the Regional Office. i Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? ff the answer to question 7 is "YES'; describe those actions in the space provided below. If the answer to question 7is "NO'; contact the Regional Office within 90 days., an evaluation maybe required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may sub ect the oermittee to a Notice of Violation fines, and/or penalties. l ,.. _. `,� _. ✓ y ( jj�'�q SAP 2 2d5- 3 ,... 5tr 1 5 "Z009 n c) Mice Unit fun Processing g The person completing this portion (GW--59A) of the monitoring report shout signs ibtlo difd submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. herebyacknowledge fhatahaabove;informatlon was evaluated and thelnfornJation submitted•�nthis - t 3 a'a report (Compliance,Rdpd GW 59A)°Isi(rue and complete to theibas; of my ktuowledge _ _Ytir! Signature of Pe itlee (or Autho ' ed Agent) Date CW-59A 121812003 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION -Please Print Clearly or Type Facility Name: `-b A+ S fA vv% e r C A qj Permit Name (if different): Facilih, AAH,.o e• Contact Person: I-^•' Well Location/ Site Name: County /ter= NoweIt Telephone #: �Zg''75Yo-ylr I No. of Wells to be Sampled:,,_ Well Identification Number (from Permit): �w�2 — For Groundwater TrealmenlSyslems Well Depth: 176 r 1l. Well Diameter to in. Check One: ❑ influent (98s Screened Interval; 1A It. to , _ft . Depth to Water Level: 2 g point. S ft. below measuring El Effluent (99) Measuring Point (M.P.) is: 2_3 It. above land surface. Relative M.P. Elevation in ft.: Gallons of water railed before sampling: 3 2. Dale sample collected: -09 Field analysis: pH 7, o Specific Conductance uMhos Temp. /.S °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT#: WCy006St. o3 EXPIRATION DATE: .5--2o// Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field _Remedialion: Rotary Distributor _Land Application of Sludge / Other:_ � NOTE Values should reflect dissolved and . / `� .05 colloidal concentrations. e Date sample analyzed: Laboratory Name: W weer Te th o Certification No. 157-6_ .� PARAMETEaS (Samples for metals were collected unfiltered �ES _NO and field acidified YES NO) COD mg/I /100ml Nitrite (NO2) as N Nitrate (NO3) as N mg/I mg/I _ Ni - Nickel 2-9-09 .Co•oe r mg/I Pb Lear] A- 7. 09 Coliform: MF Fecal Coliform: MF Total /100ml Phosphorus: Total as PSIo 09 Le.lb mg/I - el.00(2 mg/I Zn - Zinc mg/I (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 9 1// mg/I Orthophosphate Al S-'T •o9 mg/I Ammonia Nitrogen mg/I _8-1-o pH (when analyzed) 8-9-o9 7-0 -Aluminum o r/2 mg/I Other (Specify Compounds and Concentration Units) TOC_ IS-I4-o9 units A&S'D mg/I Ba - Barium 2-9-o9 Ca - Calcium Sl-7•o9 6.oYy- mg/I mg/I .50d;�� 2-9.09 /0.2 /6.7 SeLeA-;Q'n 9-11•09 0,0 Chloride-& -0 9 7.3 mg/I Cd - Cadmium—`7- )-09 .c6•00Z mg/I ill Arsenic5?-`7-04 •oosmg/I Chromium: Total 3-7-09 Co. 0,57 mg/l Grease and Oils mg/I Cu - Copper mg/I Phenol Sulfate mg/I 426.1) mg/I Fe - Iron Hg - Mercury mg/I mg/I ORGANICS: (GC,GC/MS,HPLC) Specific Conductance uMhos K - Potassium mg/I (Specify test and method If. Attach lab report.) ReportAttached? Yes_(1) No Total Ammonia mg/I Mg- Magnesium 8'7"0 9 /o. m /I _(0) VOC method # TKN as N mg/I Mn - Manganese -0 0-o7 mg/I = method # = 11-1 mot h"I h _ A, 0 rC G W -59 Rev. 03/2000 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: — Permit Name (if Facility Address: Contact Person: i Well Location/ Site SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type w- County /'Fo" VD We- r t Telephone #:92V*7 - /r / No. of Wells to be Sampled:,,_ Well Identification Number (from Permit): rn4) -10 For Groundwater Treatment Systems Well Depth: l R it. Well Diameter:? in. Check One: ❑ Influent (98) Scrleened Interval: It. to '" /1 it.. ❑ Effluent (99) Depth to Water Level: _ 12,_ft. below measuring point. Measuring Point (M.P.) is: 2.3 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 16 Date sample collected: -D 9 Field analysis: pH 4' � , Specific Conductance ' uMhos Temp. _J_*_°C, Odor Appearance PARAMETERS (Samples for metals were collected unfiltered COD mg/I Nitri Coliform: MF Fecal /100ml Nitr Coliform: MF Total /100ml Pho (Nole: Use MPN method for highly turbid samples Dissolved Solids: Total -a9 S mg/I pH (when analyzed) 8 y o9 6,9 units TOC _914- 0 C 0 90 mg/I Chloride 8-r,49 try mg/I Arsenic 2-?-09 40.om- mg/I Grease and Oils mg/I Phenol mg/I Sulfate�`9-o9 ?7A m9 /I Specific Conductance Mhos Total Ammonia mg/I TKN as N mg/I PERMIT #: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER OUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER EXPIRATION DATE: .S- 20!/ Non -Discharge UIC NPDES TY E F P RMITT D OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field . _Remediation: Rotary Distributor _ Land Application of Sludge Other:_ colloidal concentrations.-V •�V ~ V Date sample analyzed: 5 l!o ry Laboratory Name: w A e ^ '?sec f, Certification No. 5-0 _ZYES _NO and field acidified to (NO2) as N mg/I ate (NO3) as N mg/I sphorus: Total as P 9-10-69 ./re mg/I Orthophosphate mg/I At - Aluminum S oa ZO.050 mg/I Ba - Barium 04 a•03d mg/I Ca -Calcium 8-9-01? (--G3 mg/I Cd - Cadmium.V-9.04 Le•002. mg/I Chromium: Total 8-9.09 46•005' mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg -Magnesium 8-?-0 1' 3• /9 mg/I Mn- Manganese- 9-7-69 0,00V mg/I i YES _ NO) <11 Ni - Nickel 7-7.09 40•06s_ mg/I Pb - Lead_2-9 -09 te, dos mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Com ounds and Concentration Units) s,rd;c, S- boat Z�0h+o1/ _Sr41on,io,rl u 7•09 Go•o03 m L ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes --(I) , No _ (0) VOC method # = method # = method # = GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ A Permit Name (if different): Facility Address: Well Location/ Site SUBMIT FORM ON YELLOW PAPER ONLY Please Prinr Clearly or Type `Dry` County L"= veafff N (zip) Telephone #: 878-756 `S _96—ru-T No. of Wells to be Sampled: Well Identification Number (from Permit): j0j ld- // For Groundwater Treatment Systems Well Depth: lay ft. Well Diameter: `Z in. Check One: ❑ Influent (98) Screened Interval: fp It. to Wg it. ❑ Effluent (99) Depth to Water Level: ft. below measuring point. Measuring Point (M.P.) is:a.( ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: I Date sample collected: i I— _ Field analysis: pH /,• 9 , Specific Conductance Temp. / 7 -C. Odor Appearance uMhos DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: WBc)Od 67403 EXPIRATION DATE: 5-20// Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon _Remediation: Infiltration Gallery Spray Field . _Remediation: Rotary Distributor _Land Application of Sludge Other: JnTF• Valucc chnn Ll •oft . t .lr­1. A .....r .<i colloidal concentrations. Date sample analyzed: Se birlip w Laboratory Name: f j wi e 0 T'2 c Certification No. SD PARAMETERS (Samples for metals were collected unfiltered "" YES _NO and field acidified NO) 01V —YES to COD mg/I /100ml Nitrite (NO2) as N mg/I _ Ni-Nickel 5-7'09 40• o°s' mg/I Coliform: MF Fecal Coliform: MF Total /100m( Nitrate (NO3) as N Phosphorus: Total as P 8-10.09 mg/I 0.35' mg/I Pb - Lean 9-1.09 to•dos-mg/I Zn - Zinc mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Ammonia Nitrogen mg/I Dissolved Solids: Total $-1-o9 /2L mg/I pH (when analyzed) 8.9•d9 6.5 Al- Aluminum 8•'1-09 o•9z3 mg/I Othe (Specify Compounds and Concentration Units) TOC_ 47-AI-og units Ba - Barium R-'I-oz O. /0!1- mg/I S;Cim g-7.09 I7..s mo/i Chloride ?-fn o4 t of mg/I Ca- Calcium _8•`1.09 /7./ mg/I 5A/e�)Oz✓7 54•'j•09 e.a r -3 mg/I Cd-Cadmium 22-7-69' 46.002 mg/I Arsenic ss- r7- 0 y 40.00mg/I Chromium: Total I? g-67 <6.003- mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol Sulfate 7. 09 mg/I 2 Fe - Iron mg/I ORGANICS: (GC,GC/MS,HPLC) _$• Specific Conductance ( j mg/I uMhos Hg - Mercury K - Potassium mg/I mg ll (Specify test and method #. Attach lab report.) Report Attached? Yes Total Ammonia mg/I Mg - Magnesium -2-0 9 S' O/ mg/I —(I) No _(0) VOC method If = TKN as N mg/I Mn - Manganese -169 P . mg/I method # = method # = tow rC i oris GW-59 \ k —✓� g (D —� Rev. 03/2000 Sgnature a rmlllee (or Author d Agent) (Dal( SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: IIIIIIIIIIllIN DEPARTMENT OF ER QUALITY DIVISIENVIRONMENT NATERAL RESOURCES COMPLIANCE REPORT FORM 1636 MAIL SERVICE CENTER AGILITY INFORMATION Please Print Clearly or Type RALEIGH NC 27699-1636 Phone:919 733-32: Facility Name: — Permit Name (if Facility Address: W1 An. r,n Well Location/ Site Name: cn ro L County -Lyl^ k/O w GL( A� (ZIP) Telephone #: 92x- 9S'6 -S ff" r "' No. of Wells to be Sampled: Well Identification Number (from Permit): /7'1z-/2 For Groundwater Treatment Systems Well Depth: wit. Well Diameter: 2 in. Check One: ❑ Influent 98) Screened Interval: '•'/" It. to �'k It. ElEffluent (99) Depth to Water Level:_ft. below measuring point. Measuring Point (M.P.) is: It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumpeed�3�ailed before sampling: 2 Date sample collected: �� Field analysis: pH_(._L , Specific Conductance ' uMhos Temp. /7 *C, Odor Appearance PARAMETER$ (Samples for metals were collected COD mg/l Coliform: MF Fecal /100m1 Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total $-1-09 �66 mg/1 pH (when analyzed) 9-LvOcr units TOC _V-lq-° / mg/I ChlorideN-id-09 /o mg/1 Arsenic `d-7•o9 eb.00s mg/I Grease and Oils mg/I Phenol mg/I Sulfate -7-oci /o / mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I PERMIT#:Wri0005603 EXPIRATION DATE: 20// Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED —� Lagoon Remedialion: Infiltration Gallery Spray Field _Remedialion: Rotary Distributor —Land Application of Sludge Other: NOT i Values should reflect dissolved and colloidal concentrations. Date sample analyzed: 5 e br I (b 4 Laboratory Name: rue+. , —re C_I Certification No. So tered � YES _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P S-Io-OG d-'G mg/I Orthophosphate mg/I At- Aluminum _8-1•1)9 o-csz mg/I Ba - Barium `3-'1'0 Q 0 -o s0 mg/I Ca- Calcium 9-7-0 9 (/z 9 mg/I Cd - Cadmium q-7-09 mg/I Chromium: Total 9-7•69 46.005 mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium 8 by I mg/I Mn-Manganese 8-1-b9 1.7 g/I _YES _ NO) '< Ni- Nickel- 2-7.o 9 0-01s' mg/I Pb - Learl 8 oS _16•00 mg/1 Zn - Zinc mg/I Ammonia Nitrogen mg/I Other(Specify Compounds and Concentration Units) Soc)V t $-i-O% o i ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) ReportAttached? Yes_(1) No_(0) VOC : method # = method If = mathM e — Gl ; l� t' �-7LY- (1)/t c Permihee!o�rAulhonzed g_ent)Namearr lle-Please print or type (} GW-59 \ Y CVO --- Rev.03/2000 wqnaiuiVemidlee (OrAulhorizedA Agent) (Dale) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Co 4f3 %i m e Permit Name (if dilfere t): Facility Address:__ O Vu m A n , r9 N tsireep - Well Location/ Site SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type 14 4' County //I Telephone #:. No. of Wells to be Well Identification Number (from Permit): /22 k/-/ For Groundwater Treatment Systems Well Depth: /S ft. Well Diameter. 2 in. Check One: ❑ Influent (98) Screened Interval: 0-/A ft. to "'//+ ft. ❑ Effluent (99) Depth to Water Level:(40_ft. below measuring point. Measuring Point (M.P.) is: 7•�_ It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: ---I Date sample collected: 'C 9 Field analysis: pH 4 , Specific Conductance uMhos Temp. 'C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT 0:WL'0 EXPIRATION DATE: S-2orl Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Spray Field Rotary Distributor Other: _Remedialion: Infiltration Gallery Remedialion: _Land Application of Sludge NOTE: Values should reflect dissolved and . colloidal concentrations."•' a Date sample analyzed: Laboratory Name: Certification No. PARAMETERS (Samples for metals were collected unfiltered /YES _NO and field acidified _ NO) COD mg/1 Nitrite (NO2) as N mg/I Ni - Nickel 9-9-09 <o• ouS mg/I Coliform: MF Fecal Coliform: MF Total /100ml /100ml Nitrate (NO3) as N Phosphorus: Total as P.Y-10-49 D./7 mg/I mg/I Pb - Lead 9-1.09 tu•oo5 mg/1 Zn - Zinc mg/I (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 8•1-o9 Orthophosphate J/ mg/1 Ammonia Nitrogen mg/I pH (when analyzed) 9-9.04 3-51 mg/I 6.3 units At - Aluminum 8 •)-0 Ba - Barium 4 7'tl� o•09/ mg/I m /I Other (Specify Compounds and Concentration Units) sbd'Un1 '-7-v 9 6•059 TOC_9r4'09 7Z mg/I Ca - Calcium - 4"'1•69 X-3 mg/I Selen ;um k-7 09 koI , �= Chloride_-W'o9 mg/I Cd- Cadmium `3-7-09 46.a62- mg/I Arsenic.-7-oy <o•oos mg/I Chromium: Total 6-1•0 9 L6.605` mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol Sulfate -7. 0 9 mg/I 43 % Fe - Iron mg/I ORGANICS: (GC,GC/MS,HPLC) Specific Conductance mg/I uMhos Hg - Mercury K - Potassium mg/I mg/I (Specify test and method if. Attach lab report.) ReportAttached? Total Ammonia mg/I Mg - Magnesium �'7 0`/ / 7• G mg/I Yes—(1) No _ (0) VOC TKN as N mg/I Mn - Manganese o i d• ° mg/I method s = methods = u 0312000 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: (,OAf /` rsu p Permit Name (if dilferent) Well Location/ Site SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County ///-il/Owelt Telephone #: (fZfr' 9d7e -Y No. of Wells to be Sampled: Well Identification Number (from Permit): Dw- /y Far Groundwater Treatment Systems Well Depth: Is it. Well Diameter; �_ in. Check One: ❑ Influent (98) Screened Interval: e"/r4 II, to _ ✓`14 It. ❑ Effluent (99) Depth to Water Level: _ 7 ft. below measuring point. Measuring Point (M.P.) is: 2, (o it. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: ! Dale sample collected: Field analysis: pH L •1 Specific Conductance ' uMhos Temp.°C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT fl: t-'"6e Sl ° EXPIRATION DATE: S'26 N Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED —Lagoon Remedialion: Infiltration Gallery Spray Field ' _Remedialion: Rotary Distributor Land Application of Sludge Other: icucl•1 uioaulvGu Ullu colloidal concentrations. Date sample analyzed: Laboratory Name: — Certification No. PARAMETERS (Samples for metals were collected unfiltered AYES _NO and field acidified �" YES NO) COD mg/I /100m1 Nitrite (NO2) as N Nitrate (NO3) as N mg/I _ Ni - Nickel 8 7 09 to•oaSg/ •oC/ m I Coliform: MF Fecal Coliform: MF Total /100ml Phosphorus: Total as P F-10-09 6•22 mg/I mg/I Pb - Leac -� ampnq Zn - Zinc mg/I mg/I (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total -1-0? r Orthophosphate mg/I Ammonia Nitrogen mg/I pH (when analyzed) _8 �l �q mg/I units AI - Aluminum 9-7•62 Ba -Barium 9-? a$ d>.9G/ mg/I Other (Specify Compounds and Concentration Units) dale/ TOC_9-1y•dy 77mg/I Ca -Calcium 4•7•69 93.2. mg/I mg/I 5e�;v rn S-7-oq ,S/•�r n,o/I- ,l„IL SIFICAi , -16-60 Chloride 9-6'•o9 1 •S mg/I Cd - Cadmium 9-7-o9 t6•002 Rig/I -' Arsenic . 0-2- o? -,Co•oos mg/I Chromium: Total T-7•o i -Co'oaS mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol Sulfate `Sop 1 mg/I 9 Fe - Iron mg/I ORGANICS: (Gc,GCIMs,HPLC) Specific Conductance mg/I uMhos Hg -Mercury K - Potassium mg/I mg/I (Specify test and method #. Attach lab report.) Report Attached? Total Ammonia mg/I Mg - Magnesium -9-69 mg/I Yes. —(I) No VOC method # = _ (0) TKN as N mg/I Mn - Manganese o 6 g/I method # = method 0 = GW-59 12- 9-V/'L9 Rev. 03/2000 Sgnatwe of Permatee ( homed Agent (Date) GROUNDWATER QUALITY MONITORING: COMPLIANCE R Facility Name:_ Permit Name (if Facility Address Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type C 09. A'-• County !V7-; J/dwa(l Telephone #: 929- iJ 1, -S No. of Wells to be Sampled: Well Identification N�ber(from Permit): 1"&)-JS` For Groundwater Treatment Systems Well Depth: 6 it. Well Diameter: 2- in. in. Check One: El Influent (98) Screened Interval: wiry ft. to Ab A it. ❑ Effluent (99) Depth to Water Level: .S ft. below measuring point. Measuring Point (M.P.) is:__j_ ft. above land surface. Relative M.P. Elevation in IL: Gallons of water pumped/bailed before sampling: �r� Dale sample collected: 8 Y'� i Field analysis: pH •`7 , Specific Conductance uMhos Temp. A 7 °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT#: w'aO006*603 EXPIRATIONDATE:.T-2 Non -Discharge UIC NPDES TYPE OF P RMITT D OPERATION BEING MONITORED it agoon _Remediation: Inlillration Gallery Spray Field '_Remediation: Rotary Distributor —Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations."•°' Q� Date sample analyzed: - - j cc GE/l04L,/ Laboratory Name: r, l a tEr �6 C 11 * x ='S, Certification No. 5-6 f. PARAMETERS (Samples for metals were collected unffltered___e:!'_�YES _NO and field acidified �' YES NO) v?5 COD Coliform: MF Fecal mg/I /100ml Nitrite (NO2) as N Nitrate (NO3) as N mg/1 _ Ni - Nickel 2-7•6 % 4e ..To5- mg/I Coliform: MF Total /100m( Phosphorus: Total as P 9feb9 4o•/G mg/I _ mg/1 Pb - Lead Q oS <o•oos m I Zn - Zinc mg/I (Note: Use MPN method for highly Dissolved Solids: Total turbid samples) 8-7 D9 30 Orthophosphate mg/1 Ammonia Nitrogen mg/I pH (when analyzed) 8 mg/I y o 9 6.7 units At - Aluminum 9-7•69 Ba -Barium -� d 9 n ��� mg/I Other (Specity Compounds and Concentration Units) O,14W TOCAINa�j Chloride ?S4 mg/I Ca - Calcium X-7•09 96•40 mg/I mg/I Sod: vm fs 7 ooi JS• 9 _.S.ren.lun, 6•bt15"�n J Arsenic _V-9-oi mg/I 49•D06- mg/I Cd- Cadmium g-7.3q Chromium: Total 8-7.0? <orcbZ mg/I Zo•ooS mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol Sulfate 09 mg/I JD•S Fe - Iron mg/I ORGANICS: (GC,GC/MS,HPLC) _2-7 Specific Conductance p mg/I uMhos Hg - Mercury K Potassium m /I 9 mg/1 (Specify test and method #. Attach lab report.) Report Attached? Total Ammonia mg/I Mg - Magnesium 8-7-0 9 37• / mg/I Yes_(1) No_(0) VOC TKN as N mg/I Mn - Manganese •7•6 F m /I 9 method # = :method # _ method # = 4 K Q GW-59 Rev. 03/2000 im 0 GW-59A COMPLIANCE REPORT F0Rly1 na; is # Gl B eop 6 6 03 (Submit one each mouftoring period with GW-59 farms) 1 Enter date monitoring results were due. ( 1 Will this monitoring report (GW-59 and GW-59A) be, submitted after the established due date? YES NO i Was any required information missing on the GW'-59 report forms? IF the answer to question 1 or 2 is 'YES'; list in the space provided below the well idenL'fication number(s) and explain the problems encountered in YES obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing identification plate, area overgrown, etc.)? Ifthe answer is "Yes-, YES NO contact the Regional Ofce forglddance. _ 4 Are any monitored constituents equal to or above the established standards? If the answer to question 4 is 'lVO'; skip to section B. 1: YES NO if the answer to question 4 is "YES" the affected wells individually with consituent(s) and concentration(s) exceeding standards in the space provided below: Mw'Z /j%W-e.o90 /?+cb.-.5 a rtN= 0.4,3Z Al W-tt /77/U-af,g%,(, into-/Z ^N V_ /,/z 5 For the constituents identified in question 4 above, have standards been exceeded previously for the same constituent(s) in the same wells) in the last two YES NO years? If the answer to question 5 is 'NO- s to section 8. If the answer to question 5 is 'YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). /Yjt✓ 2- /vW 0„-.TyV Mw-///,V,v=O,/2l✓ Led) o.o/fv 1,YAO-/21NIP9 0.99S✓ /%�4ifSemnJz0,78c7. /yftu- /tJ 7-45= sq0' Aiv-/ y !Pot: c-056 t/a wr 0✓ C8 = 0,002 Mw 13 anti=o.o59 ✓ Are the monitoring ells listed in section 5 located at or beyond t�p review boundary? r^N = 0. sq If the answer is "YES", a groundwater qualityproblem maybe occurring. CONTACT THE REGIONAL OFFICE IMMEDiATELYFOR GUIDANCE. If the answer is `NO'; monitoring wells maybe improperly located,- contact the RegionalOfce. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is 'YES', describe those actions in the space provided below. if the answer to question 7 is 'NO", contact the ReoionalOffice within an The person completing this portion (GW-59A) or the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. M M FIN CW-59A 12/8/2003 GROUNDWATER QUALITY MC COMPLIANCE REPORT FORM Facility Name: ow4- Permit Name (if differed) Facility Address: r- p_ ISUR 1019DMFN YE -ORING:'111e Regional Office L_ Acruif�Pctinn Please Print Clearly or Type PAPER ONLY r••in r•.ow ^ - 8t . 4'•r3Z Count MS fdowell YI !'�s: It . �•{.�,s�xr1� W .^' u.v1 y t cil Contact Person: ' � Telephone N: 82Y-7SG^ /(// Well Location/ Site Name:.56v; ee r/ BACK Gi C"� No. of Wells to be Sampled: 7 Ihom evmll) Well Identification Number (from Permit): M W - Z LFGoundwater Treatment Systems Well Depth:{f, WeIlhDiameter% ink One: ❑ Influent (98) Screened Interval: /.4 It. to /r% ft. ❑ Effluent (99) Depth to Water Level: 36 ft. below measuring point. Measuring Point (M.P.) is:3. -1 It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 3C Date sample collected: y-/4-oq Field analysis: pH ?•o , Specific Conductance ' uMhos Temp. �°C, Odor Appearance DEPARTMENT OF ENVIRONMENT h NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT ff:6/Ooeose03 EXPIRATION DATE: S-2or/ TYPE OF PERMITTED OPERATION —G Lagoon _Rem( Spray Field _ Reme Rotary Distributor _Land Other: NOTE: Values should reflect disso colloidal concentrations. a MONITORED ��II� is Infill jjAi V" tu09 Office and . Ty., r••- v pI t� Date sample analyzed: $kE be/f o w Viu ( 2 p 2009 Laboratory Name: W.¢ Ar i 7Y e L Certification No. So cC'r ION Inferaracon 1�mrrssincl Unit PARAMETERS (Samples for metals were collected unfiltered YES _NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P 0•26 Y-21ro mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/1 Dissolved Solids: Total 112 y-iy-o9 mg/I AI - Aluminum 4 (,a 9-/709 mg/I pH (when analyzed) 7•o v-/von units Ba - Barium 46-o2o 'Y-17•09 mg/I TOC40•So V-ztroq mg/I Ca-Calcium_23.s mg/I Chloride lS .5 y-Is, o9 mg/I Cd - Cadmium !c d• ooz y-17-0 9 mg/I Arsenic < o•ooS yv7-a 9 mg/I Chromium: Total o• 60s v /7 0 mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate - 410.6 yv7-o9 mg/I Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium /el• Z. y-/7-o9 mg/I TKN as N mg/I Mn - Manganese 0.539 vv7-094 mg/I YES _ NO) Ni - Nickel 0.007 1/-/7-c 9 mg/I PID - Lead o. mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) Sp/rn %uwt <o. /7•09 sow -'Um i0.1 m�/ y-/7-a9 ORGANICS: (GC,GC/MS,HPLC) (Specify test and method It. Attach lab report.) ReportAttached? YeS_(1) No_(0) VOC : method k = method ft = methnri it = GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Permit Name (it Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type le — County Telephone #: 1329-215'Y 4r4r No. of Wells to be Sampled: Well Identification Nu bar (from Permit): P4141_/ Fo. Groundwater Treatment Systems Well Depth: 1 g ft. Well Diameter. 2 in. CheckOnc: ❑ Influent 98) Screened Interval: ^1r� It. to 0"/4 It. El Effluent (99) Depth to Water Level: t0 ft. below measuring point. Measuring Point (M.P.) is: 2— It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 10 Date sample collected: / �9 Field analysis: pH _6 , Specific Conductance ' uMhos Temp. _12— eC, Odor Appearance PARAMETERS (Samples for metals were collected unfiltered COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 9 /y oq F 6 mg/I pH (when analyzed) 6,2 units TOC Lf, io- oc9 D 0 mg/I Chloride -'rs- Der 2-1.22 mg/1 Arsenic Li-iri-cq 1-000' mg/I Grease and Oils mg/1 Phenol Sulfate !I I-o9 ��� m9g/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Rev. 03/2000 DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1676 MAIL SERVICE CENTER PERMIT #: L.Wt9e0oS403 EXPIRATION DATE: 5--20r / Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED ---� Lagoon Remedialion: Infiltration Gallery Spray Field Rotary Distributor Other: _ Remedialion: Land Application of Sludge NOTE: Values should reflect dissolved and colloidal concentrations. V10 IOH Date sample analyzed: SEE belle w ;x nv_1 Unit. Laboratory Name: Certification No. S C� _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as Py ?1 a9 moo./bmg/I Orthophosphate , mg/I Al - Aluminum. mg/1 Ba - Barium y-17-o 9 e.o2o mg/I Ca - Calcium H-t,7-e9 9---te 5 mg/I Cd - Cadmium 9-/7-o9 G6,66Z mg/I Chromium: Total 9-1767 zao•etc�l- mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium y /7-c? /.99 mg/I Mn -Manganese n I mg/I ./ YES _ NO) Ni - Nickel y-/7-69 ta.00-Sm I Pb - Lean y-/7-o4 Co.oec mg/( Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) .se�:anr c1-1?-n4 J357. ..�i. ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes—(1) No _ (0) VOC : method # = method # = method # = GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Permit Name (if 44s me-, c.aK- Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County / r Telephone #: 329-75G -y/// No. of Wells to be Sampled:,_ Well Identification Number (from Permit): M -// For Groundwater Treatment Systems Well Depth: l 3 it. Well Diameter: 2 in. Check One: ❑ Influent (98) Screened Interval: A -lit It, to � ft. ❑ Effluent (99) Depth to Water Level: 9 It. below measuring point. Measuring Point (M.P.) isYA_-_(_ it. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: I Date sample collected: -/r -o Field analysis: pH L• 9 , Specific Conductance uMhos Temp. /7- °C, Odor Appearance PARAMETERS (Samples for metals were collected Lin COD mg/I Coliform: MF Fecal /100m1 Coliform: MF Total /100m1 (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total Y-/y°9 n mg/I pH (when analyzed) 9-/v-o9 6.4 units TOC y-2o-o9 7.91 mg/I Chloride y=/5-09 .<S•o mg/1 Arsenic)-i7-e9 to.eos-mg/l Grease and Oils mg/I Phenol mg/I Sulfate L-/-17-6y V4, m /I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: O°05403 EXPIRATION DATE: S Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field _Remediation: Rotary Distributor —Land Application of Sludge IVV I G. values snoula renect mssolved and . ,( % ;4 LVI"-' colloidal concentrations. t�Q ;,�•,•,,')bt Date sample analyzed: _ �E E be//oc.J Laboratory Name: /✓s ,'T�+c Certification No. S-O .eyed_ 'YES _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P Y-s/ ev O.(oo mg/1 Orthophosphate mg/I Al - Aluminum 9-/7-a9 /.SL mg/I Ba - Barium Y-t7-o9 o. /a/ mg/I Ca -Calcium 7-17• 02 i(..9 mg/I Cd - Cadmium )'/7b q c e• WZ mg/1 Chromium: Total y-/7.09• eoao5-- mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg -Magnesium y-/7-o 7 y.?7 mg/I Mn- Manganese /7-off 0./2/ mg/I YES _ NO) Ni - Nickel y-/7-o9r 4,6.025- mg/I Pb - Lead_SI•/?•o7 6.a4t mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) I ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes —(I) No _ (0) yOC : method # = method # = method # = Rev. 0312000 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION- ,/� Please Print Clearly or Type Facility Name: DAYS An+er"O", PERMITN:li% Permit Name (if dilferenik _ Non. Discharge Facility Adgress ♦N A 0 / vxC Contact Person: T r Well Location/ Site Name: County Telephone k:YZ$-9S41-t, No. of Wells to be Sampled: Well Identification Number (from Permit): A7 -1 For Groundwater Treatment Systems Well Depth: / :3 It. Well Diameter _� in. Check One: ❑ Influent (98) Screened Interval: 1- It. to w R it. ❑ Effluent (99) DepthA to Water Level: Il. below measuring point. Measuring Point (M.P.) is:2fL It. above land surface. Relative M.P. Elevation in It.: Gallons of water pumped/bailed before sampling: 2 Date sample collected:-7 ollected:%44 Field analysis: pH 6 1 , Specific Conductance uMhos Temp. _jD__°C, Odor Appearance PARAMETERS (Samples for metals were collected unfilte COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 7-/9•e9 Z3G mg/I pH (when analyzed) V-/y-o9 6•9 units TOC _ 9- 20-09 14 7 m /I Chloride i-�S-o t19 3Smg/I Arsenic y /7-og <o.aaSmg/I Grease and Oils mg/I Phenol g Sulfate V-/?-09 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I NPDES DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER EXPIRATION DATE: TYPE F P -RMI D OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field _ Remedialion: Rotary Distributor —Land Application of Sludge Other: e NOTE' Values should reflect dissolved and'"="-:�)` t colloidal concentrations. / � /�p •10(19 Date sample analyzed: a50 r 4 k i11 (W�, Laboratory Name: 6d/► fe / %Pc h yy Certification No. S-6 _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P !V og o-zl mg/I Orthophosphate mg/I AI - Aluminum 11-/7-sv a•o99 mg/I Ba - Barium y-/7-e9 e.oyo mg/I Ca - Calcium 6/-1,7- ey 229 mg/I Cd- Cadmium 11-17•69 .co.cez mg/I Chromium: Total Y-/7•69 440.eeS mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg -Magnesium 4-/7-0 9 475 mg/I Mn - Manganese y-/7-09 B,99tmg/I i YES _ NO) Ni- Nickel `/-/7-09 ;Cd•0pZ mg/I Pb - Leafi U- /9.0 9 e D-ooSmgll Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) 5Cle, ; urn c9(-/7•eW f7r" ORGANICS: (GC,GC/MS,HPLC) (Specify test and method ff. Attach lab report.) ReportAttached? Yes_(1) No _ (0) VOC : method k = method N = method ft = GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Permit Name (if rj ti SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type Contact Person: rh/r/�p '-ri fyr,yn "" Telephone #: 9'28­7SG-9 Well Location/ Site Name. 5ZIEr1/ r tir/utarNo. of Wells to be Sampled: Well Identification Number (from Permit): MM-l.i For Groundwater Treatment Systems Well Depth: /S ft. Well^iameter: 2 in. Check One:❑ Influent (98) Sclfeened interval. /� It. to �_ ft. El Effluent (99) Depth to Water Level: '7 ft. below measuring point. Measuring Point (M.P.) is:_I_ It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/b led before sampling: / Dale sample collected: y ly_o9 Field analysis: pH L • � Specific Conductance uMhos . Temp. �'C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT#:EXPIRATION DATE: .S-2tl// Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Rotary Distributor Other: Remedialion: Land Application or Sludge �. k'F., or 4. i,) NOTE: Values should reflect dissolved and . ��� G7.Z = colloidal concentrations. ' mm 7. 4t /p09 Date sample analyzed: ga „rS Laboratory Name: rv'We j^ 7-er A Certification No. SO tr�ter.r- PARAMETERS (Samples for metals were collected unfiltered "� YES _NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as Pmg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total Y-/Y-os you7 mg/I AI - Aluminum - 917•09 (7.0 1 mg/I pH (when analyzed) q-19•69 61 units Ba - Barium yto- o S 0,452 mg/I TOC y-20-02 Z/9' mg/I Ca - Calcium 9-17. 09 17. z mg/I Chloride y-/S dD 9 //0 mg/I Cd - Cadmium 11-17•09 <o•oez. mg/I Arsenic v-)ti-oq ta•aaS mg/I Chromium: Total _ 1-17•o9 46-0e5- mg/I Grease and Oils mg/I Cu - Copper mg/1 Phenol mg/I Fe - Iron mg/1 Sulfate V-0-o4 yc•/ mg/I Hg- Mercury mg/1 Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium y-11-09 /'l, 2 mg/I TKN as N mg/I Mn - Manganese y-/7•69 01,05? mg/I YES _ NO) Ni-Nickel `1-/7n 9 O•oa F mg/I Pb - Lean &1./9.69 to.00S mg/I Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) 5P/r/�; M �/-/7'09 A6,Ns-"-#2 ,5aM:1 27-3msIL ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) ReportAttached? Yes_(1) No_(0) VOC method # = method # = method It = Rev. 03/2000 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION /� II�//// Please Print Clearly or Type Facility Name: (o.1 3 `7 M e r `c rg ✓� Permit Name (if different): _ - (cur) r I rJt of County ///2//0 ruc n• t,;C[,. „ v...4 nr Contact PercnTelephone #:828-'7.F6' f{ Well Location/ Site Name: No. of Wells to be Sampled: Well Identification Number (from Permit): For Groundwater Treatment Systems Well Depth: Af- ft. Well Diameter.— in. Check One: ❑ Influent (98) Screened Interval: "/4 ft. to _ ^/A ft, ❑ Effluent (99) Depth to Water Level: _7 ft. below measuring point. Measuring Point (M.P.) is: 2• � It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bg{Ied before sampling: Date sample collected: / -o 'y Field analysis: pH //. Specific Conductance uMhos Temp. —LL°C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636MAIL SERVICE CENTER PERMIT #: L.% 6"' 06-S443 EXPIRATION DATE: S- 2'D// Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED �G Lagoon Remedialion: Infiltration Gallery Spray Field _Remedialion: Rotary Distributor —Land Aoolication of Sludoe Other: NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: 3rC bP�l�^ •f rn9•�°'-" j1°}�tru, Laboratory Name: Tpc Certification No. S-0 PARAMETERS (Samples for metals were collected unfiltered �YES _NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100mi Phosphorus: Total as P y-2/•o? 0,87 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total _q-i7 -Y y07 mg/I AI - Aluminum Y-17• 03.23 mg/I pH (when analyzed) N /yDg 6OPunits Ba - Barium y l7 oq o,2/ mg/I TOC y-26b 9 08 mg/I Ca - Calcium y /9 0 9 7/. / mg/I Chloride y-rs-02 Zs,0 mg/I Cd- Cadmium mg/I Arsenic H /7-oy to.eof mg/I Chromium: Total /'/?-09 6.008 mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate N-/7-6 9 t/a o mg/I Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium y'17•6-9' mg/I TKN as N mg/I Mn - Manganese y-/i •o? 6,998mg/I _YES _ NO) Ni - Nickel `/-/7•es 6.02y m I Pb - Lead 11-/9•0 9 C. mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) c��,�r•�ro��n �[-/7.09 �o oaS�i+./L ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) ReportAttached? Yes—(1) No _ (0) VOC : method # = method If = mpthnd if = SUBMIT FORM ON YELLOW PAPER ONLY t DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: WATER QUALITY DIVISION, GROUNDWATER SECTION COMPLIANCE REPORT FORM 1636 MAIL SERVICE CENTER FACILITY INFORMATION '�1 Please Print Clearly or Type RALEIGH NC 27699-1636 Phone:919 733-3221 Facility Name: �m A,; if A, r r I C A PERMIT #: B mD-5463 EXPIRATION DATE: S- 26/1 Permit Name (if different);,_ Non -Discharge UIC Well Location/ Site Name: County Telephone #: No. of Wells to be Sampled: Well Identification Number (from Permit): A14/- /.S For Groundwater Treatment Systems Well Depth: I /p it. Well Diameter.: 2- in. Check One: ❑ Influent (98) Screened Interval: A ft. to /rr it. ❑ Effluent (99) Depth VA to Water Level: _4! it. below measuring point. Measuring Point (M.P.) is:It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/b filed before sampling: %_ Date sample collected: 9•/Y-07 Field analysis: pH G Specific Conductance uMhos Temp. 10 °C, Odor Appearance PARAMETERS (Samples for metals were collected un COD mg/I Coliform: MF Fecal /loom( Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 3 t mg/I pH (when analyzed) -62 units TOC mg/I Chloride 4-r5•ocl cT.o mg/1 Arsenic q-oy �o.aoS mg/l Grease and Oils mg/I Phenol Sulfate y-17-09 g 51-91 mg/I Specific Conductance uMhos Total Ammonia mg/1 TKN as N mg/I NPDES TYEE PE PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor _ Land Application of Sludge Other: NOTE, Values should reflect dissolved and .tom' " " colloidal concentrations. Pfl(•1 'f, �'%()�4 Dale sample analyzed: SE r 5r//o w Unit Laboratory Name: WAfrr -7-P M Certification No. SO lerecl ✓ YES _NO and field acidified Nitrite (NO2) as N mg/1 Nitrate (NO3) as N Phosphorus: Total as P _ mg/I mg/I Orthophosphate mg/1 AI - Aluminum 2-0-o9 46-oyo mg/1 Ba - Barium 09 0./6X mg/I Ca - Calcium y-/9-o 9 9c.7 mg/I Cd -Cadmium- y-1" 9 e4•642 mg/1 Chromium: Total 4-f9 a 9 46: a6s mg/1 Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/l Mg -Magnesium `/-/7-02 12.tj mg/I Mn-Manganese. 0,7519 mg/I _YES _ NO) Ni - Nickel 9-/,>-a7 D.en mg/1 Pb - Lean y-/'7• e9 -44• e6• ' mg/( Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ,v'��r `-I �e moo• OS L ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes_(1) No_(0) VOC : method # = method # = method # = GROUNDWATER COMPLIANCE RI Facility Name,:_ Permit Narne (if Well Location/ Site SUBMIT FORM ON YELLOW PAPER ONLY , QUALITY MONITORING: :PORT FORM Please Print Clearly or Type n c ais . CountyL? u (ZIP) Telephone #: $2 — No. of Wells to be Well Identification Number (from Permit): M&/- /.S For Groundwater Treatment Systems Well Depth: (� it. Weihiameter in. Check One: ❑ Influent (98) Screened Inl(3 val: IA ' it. to lyt fl. I] Effluent (99) Depth to Water Level: 4_1t. below measuring point. Measuring Point (M.P.) is:_5 It. above land surface. RelativalM.P. Elevation in It.: Gallons of water pumped/b fled before sampling: � _ Date sample collected:. 9'JY-0`j Field analysis: pH 4 , Specific Conductance uMhos Temp. C, Odor Appearance PARAMETERS (Samples for metals were collected COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPH melhod for highly lurbld samples) Dissolved Solids: Total 1-1 -09 3 t mg/I pH (when analyzed)—!J. y-p9 e• units y-aD-09 c0.1/ mg/I Chloride N-15-ag so mg/I Arsenic N-11 • op 66,685- mg/l Grease and Oils mg/I Phenol mg/I Sulfate H-17-09 54 °L mg/l Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Rev. 0312000 DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT it: OJ00000_54K3 ''EXPIRATION DATE: Non -'Discharge UIC NPDES IYEE PE.PERMITTED OPERATION BEING MONITOIPED'> — Lagoon _Remediallon: Infiltration Gallery Spray Field _Remediallon: m Rotary Distributor _Land Applicalion*,ol Sludge ='� Other:—_ Iro r0 M NOTE: Values should reflect dissolved and , o o colloidal concentrations. w o Date sample analyzed: SE E bwo w O Laboratory Name: tu.o fee '7-8 Certification No. SO (o filtered �YES _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I ?-'Phosphorus: Total as P J�y=al-ov �bjiiTtg/1 Orthophosphate mg/I Al- Aluminum y'19-m9 40•oso mg/I Ba - Barium W-(� e9 O,/_y mg/I Ca - Calcium Y i7-D 9 9d."1 mg/I Cd - Cadmium 14-67 9 <e•s02_ mg/I Chromium: Total Y-0-09 4d'.005- mg/1 Cu - Copper mg/l Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium `/-/7-°2 mg/I Mn - Manganese- �/-17-09 0,71V6 mg/1 YES _ NO) Ni - Nickel ai d•a�� mg/I Pb - Lead t1-!ry-69 46•065* mg/1 Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ,v1001 °- to Lo• OS L N rd #. Attach lab report.) (1) No_(0) method # _ method If _ method # _ SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY VF MA O tt Please Print Clearly or Type Facility Name: A A LT r»G a C .a ~- Permit Name (if differerit): Well Location/ Site Name: Telephone #: 321-7% No. of Wells to be Sampled: Well Identification Number (from Permit): /'/1W-/0 For Groundwater Treatment Systems Well Depth::: 1 8 ft. Well Diameter: Z in. Check One: ❑ Influent (98) Screened Interval: �`/� ft. to /-9 it. 11 Effluent (99) Depth to Water Level: 18 _ft. below measuring point. Measuring Point (M.P.) is: I 3 ft. above land surface. Relative M.P. Elevation in IL: Gallons of water pumpediballed before sampling: L— Date sample collected: / �9 Field analysis: pH (e •9 , Specific Conductance uMhos . Temp. �eC, Odor I. Appearance. DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: [J19aooS4o3 EXPIRATION DATE: 5 -2o r I NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon _Remediallon: Infillralion Gallery Spray Field ' _Remediallon: Rotary Distributor _Land Application of Sludge Other: NOTE, Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: SEE %J c //e o� Laboratory Name: t Certification No. S PARAMETERS (Samples for metals were collected unfiltered :�f—YES NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MFTotal /loom[ Phosphorus: Total as PZ21-ey /o./bmg/I (Note: Use MPH method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total _9vy-og r b mg/I Al - Aluminum 6`/ •9?' [.0.C'D mg/I pH(when analyzed) 91-ry-o9 L.}7 units Ba-Bar)um�-rl•o9 Le.020 mg/f TOC Lf, 20- 09 0.100 mg/l Ca - Calcium ,3 43 mg/I Chloride �F25 mg/I Cd - Cadmium�tllzn i ^LD o02 mg/I Arsenic Y-t� 04 c0,00s mg/I Chromium: Total 9-1767 co.0gr mg/I Grease and Oils mg/1 Cu - Copper mg/I Phenol mg/I Fe - Iron- mg/I Sulfate `1-/9-09 3QC mg/I Hg- Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/1 Mg - Magnesium' /1-02- _ / 99 mg/I TKN as N mg/I ✓Mn - Manganese-R-O_�9 tDar�mg/I YES _ NO) Ni - Nickel 9-/?-o9 4,0-00.smg/I Pb - Lead V 09 4a.0eS mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify- Compounds and Concentration. Units) 5f/PN;une 9-17.09 to,easn.�IL AUG II 2_004 ORGANICS: (GC,GC)Ms,HPLC) (Is$i oll I r tWMN(48 #. Attach lab report.) ReI a e ? Yes_(1) No_(0) VOC : method # = method # = method # = --- s- ?U7GW-59 SynawreofP Tee nt) Rev. 0312000 (orAmhori r FEB 0 2 20RL _ I SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITO COMPLIANCE REPORT FORM Facility Name:_ Permit Name (if Well Location/ Site Name: Please Print,Clearly or Type Telephone #: $2N 7$(o Yn► No. of Wells to be Sampled: _ I Well Identification Number (from Permit): Mkt-2 Well Depth: 75: _ft. Well Diameler. Screened Interval: N/A• it. to rv/A ft. Depth to Water Level: 9 n ft. below measuring point. Measuring Point (M.P.) is:%, ft. above land surface. Gallons of water pumped/bailed before sampling: Field analysis: pH 'b , Specific Conductance S Temp. _ I°C, Odor A PARAMETERS (Samples for metals were collected COD mg/1 Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPH method for highly turbid samples) Dissolved Solids: Total 12�204o9 lot mg/I pH (when analyzed) h/�lot� 7.%S units TOC_ 1213nlos7 so-so mg/I Chloride i_ z61os? 7:75 mg/1 Arsenic 12� l to / on/ Z-o o/o mg/I Grease and Oils mg/I Phenol mg/I Sulfate ( /os7 /o.0 mg/l Specific Conductance UMhos Total Ammonia mg/I TKN as N mg/I For Groundwater Treatment Systems in. Check One:❑ Influent (98) ❑ Effluent (99) Relative M.P. Elevation in ft.: Date sample collected: 12 UMhos Doearance DEPARTMENT OF ENVIRONMENT 6 NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT#: tJo 0oos- 663 EXPIRATION DATE: .5- Z O// Non -Discharge UIC NPDES TYPE 9F PER D OPERATION BEING MONITORED Lagoon Remediatlon: Infiltration Gallery Spray Field ' _Remediatlon: Rotary Distributor _Land Application of Sludge \ Other:_ NIOTFt t/a IIIAQ chn.,l.l .ene-r At --- t..-.a --� colloidal concentrations. .IAN 2 8 2009 Date sample analyzed: See 136 r (o n Processing Unit Laboratory Name: td A e Tee t, nwnrr n� Certification No. S in tered_ZYES _NO and field acidified Nitrite (NO2) as N mg/l Nitrate (NO3) as N mg/I Phosphorus: Total as P�h/a V cd./� mg/I Orthophosphate mg/( AI -Aluminum JLZL&1o9 < o•/m mg/I Ba - Barium yz//�l a 5� e o 0�6mg/I Ca -Calcium ylk4 o a 7.3 mg11 Cd - Cadmium IWA/c Y �a.00/ mg/I Chromium: Total /?jgVoB <o•o/o mg/l Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/l K - Potassium Ing/I Mg - Magnesium /Z1�/a9 9. t8 mg/1 Mn - Manganese J�/� o B < 0,010 mg/l _YES -"' NO) Ni- Nickel /z//a/oy to.o/o g/ Pb- Lead LZJ14�/aJl 4 o 06s mg/l Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) o,n St <o o/o .,,�L Saolrum V 9L7 / ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes ✓(1) No _ (0) VOC method # = EPN 62/o Q method # = method # = - • - ice, P ngc.ur name an a - riease print or Type GW-59 i (� r 1- 21-a 9 Rev. 03/2000 Y/` Srgnalure of ermiltee (o ulnonzed Agent) (Date) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER, QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: l Permit Name (if different): Facility Address: Well Location/ Site Name: Print Clearly or Type N County jFrr=NOWCrL Telephone if: 82 Sy- ZS6 -91 r / No. of Wells to be Sampled:,, Well Identification Number (from Permit): iY1 d-/O For Groundwater Treatment Systems Well Depth: / 9S it. Well Diameter: 2- in. Check One: ❑ Influent (98) Screened Interval: ^'/q ft. to "' a ft. ❑ Effluent (99) Depth to Water Level: _/0 ft. below measuring point. Measuring Point (M.P.) is: 13 ft. above land surface. Relative M.P. Elevation in ft: Gallons of water pumped/bailed before sampling: _� Date sample collected: /2 /G -o � Field analysis: pH %•°1 , Specific Conductance uMhos Temp. 12- °C, Odor Appearance DEPARTMENT OF ENVIRONMENT 3 NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE -CENTER PERMIT#: W0800S 03 EXPIRATION DATE: .S-20// Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: infiltration Gallery Spray Field Remediation: Rotary Distributor —Land Application of Sludge NOTE: Values should reflect dissolved add. " colloidal concentrations. BAN 2 8 2009 Date sample analyzed: _ SEE IOel to r..lgp;it on Processing Unit Laboratory Name: w af-& - r er h MA1011400 Certification No. S-d PARAMETERS (Samples for metals were collected unflltered_k!!fYES _NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /loom[ Phosphorus: Total as P 12ZYOles lo,it, mg/I (Note: Use MPH method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total /2 zo oy 3oi mg/I AI -Aluminum <a.roo mg/I pH (when analyzed) '7.0/ units Ba -Barium-/�/os7 <o.e•fo mg/I TOC L/3o/D 8 D• GS mg/I Ca -Calcium ram/o�7 /• 3/ mg/I Chloride Iz sc' o mg/I Cd - Cadmium 12/16/on/ A 0•06/ mg/I Arsenic _/ / �o`i <o,o/o mg/I Chromium: Total l2//r ay ti p•o10 mg/I Grease and Oils mg/I Cu - Copper _ mg/I Phenol mg/I Fe - Iron mg/I Sulfate 121/9to? 248 mg/I Hg- Mercury mg/1 Specific Conductance - uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium-11//G/0V ei•?oo mg/I TKNasN mg/I Mn-Manganese)zr/4/ems �Orolr)mgll /I; _YES ! NO) Ni - Nickel 12//6/" 8 0•01 ° mg/I Pb - Lear[ /7//6/0y <e.dos' mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) i / 2271116 40 ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #_ Attach lab report.) ReportAttached? Yes ✓ (1) No _(0) VOC : method#=_[pA �2/0p : method # = : 'method # = 6r G W-59 Rev. 0312000 /- 2/•o 7 \� SUBMIT FORM ON YELLOW PAPER ONLY ti GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM ACILITY INFORMATION_ Please Facility Name: Permit Name (if different): Well Location/ Site Name: or Type e-x% County M_ /„tor S r c n wv1 t �-�—/- Telephone q: S'28•%56- No. of Wells to be Sampled: Well Identification Number (from Permit): MO-11 � For Groundwater TreatmentSyslepts Well Depth: I .3 ft. Well Diameter:?- in. Check One: ❑ Influent tuo) Screened InlervN: P-1A ft. to �' A ft. ❑Effluent (99) Depth to Water Level: tl. below measuring point. Measuring Point (M.P.) is: It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 2- Date sample collected: G-o Field analysis: pH /, .9 9 , Specific Conductance ' uMhos Temp. _JL°C, Odor Appearance PARAMETERS (Samples for metals were collected COD mg/I Coliform: MF Fecal /100m1 Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total /g2gotr lo9mg/I pH (when analyzed) /z//o/ounits —' J TOC213o) o57 2.45?mg/1 Chloride' /zrze�oV �25' mg/I Arsenic i '—'asT <o.oio mg/I Grease and Oils mg/I Phenol Mgt[ Sulfate 12�/o5J �.9_ mgA Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER DUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: 40 6 eoo 6-6o3 EXPIRATION DATE: .S= 2 d 1 / Non -Discharge UIC NPDES LYE ED OPERATION BEING MONITORED — Lagoon Remedlation: Infiltration Gallery Spray Field ' _ Remediation: Rotary Distributor —Land Application of u'IC �6 \1 tl Other: i= rl3 NOTE• Values should reflect dissolved and . .I.�I� 2 $ 2009 colloidal concentrations. Information Processing Unit Date sample analyzed: S C t b P//e0 OWOJBOG Laboratory Name: Ld A fr r r e e h Certification No. b-D YES _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/1 Phosphorus: Total as P /2/10IPY 6./7mg/I Orthophosphate mg/I AI -Aluminum /2��og <0160mg/I Ba - Barium 11-11416$1 .z.osX mg/I Ca - Calcium it I wol? /r. Z . mg/1 Cd-Cadmium <o•oo/ mg/I .��E/"� Chromium: Totall,? )i;ou 1-d.61e mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/l K - Potassium - mg/I Mg- Magnesium _Lz/r4/Of� 3,re m /I Mn Manganese 1�i j( �m9/I _YES / NO) Ni - Nickell zll�.16Y Co. r,io mg/I Pb - LeadJ Z-1416' 6 .00 mg/l Zn - Zinc mg/I Ammonia Nitrogen mg/1 Other (specify Compounds and Concentration Units) Self ;um /211lrFoe,9 <e oioncL _Seri : V rrn 7 7/r A $E .1 52 - y'. t ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes✓✓(1) No _ (0) VOC , : method # = ,EPA (,21o4 19Ar d iC method # = method # = GW-59 Rev. 0312000 SlQnature of Parmdtee (arA ihorized Age (Date) N SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY -MONITORING: COMPLIANCE REPORT FACILITY INFORMATION !r Please Prinf Clearly or Type Facility Name:- - C rs a % 5 men ' c r4 r - Permit Name (if different): Contact Person:- )P Telephone #:X2il- "/SG •, Well Location/ Site Name: $Fy, a //.'FA-/ oraf No. of Wells to be Sampled: Well Identification Number (from Perm It): /?'/ -12 r roundwalerTreatmentSystems Well Depth: 13 ft. Well Diameter:? in. eck One: ❑ Influent (98) Screened Interval: ^ /N ft. to�� ft. El Effluent (99) Depth to Water Level: ft. below measuring point. Measuring Point (M.P.) is:2_(L ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: _L Date sample collected: Field analysis: pH "7 -e b , Specific Conductance ' uMhos Temp. It eC, Odor Appearance DEPARTMENT OF ENVIRONMENT 3 NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: Wig 000 S--La 3 EXPIRATION DATE: X-2e// Ndn-Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remedlation: Infiltration Gallery Spray Field _ Remediaticn: Rotary Distributor _Land Application of Sludge Other: 01r'r%... _ ♦araca a,ruuru rcucm alssutvea ana JAN 2 8 2009 colloldal concentrations. Date sample analyzed: Sz'F be//e ru Information Processing Unit Laboratory Name: P✓,ufer _F&CL Ow4/8OG Certification No. 5-0 PARAMETERS (Samples for metals were collected unfiltered AYES _NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total 1100ml Phosphorus: Total as PJzligl. ep-f6 mg/I (Note: Use MPH method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total /Moa' tot. mg/I AI -Aluminum /ZZ//r/ey 44.1ed mg/1 pH (when analyzed) /zIA/6 9 2e0 units Ba - Barium /za4 my 0 r041 mg/I TOC L% 3oloy / y,Y mg/1 Ca - Calcium /z//z/ey Zo.z mg/I Chloride 1�r�ieu mg/I Cd - Cadmium /z,//41.4 Xaao l mg/I Arsenic �f/ey ezcs eo,jo mg/I Chromium: Total _/z/�a/os/ _-o,o/o mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mg/l Fe - Iron mg/I Sulfate-17il!19JAV /3 X mg/1 Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I _ Mg - Magnesium /y/4/ob :YZ mg/I TKN as N mg/I Mn -Manganese /z//e/or'-mg/I ._YES - NO) Ni -Nickel /zl/!,/erp ! e.0 /d m I Pb - Lean /2,/61e rV [e-e � mg/1 Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) m Z L e Le. o/dq, L ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. A,tach lab report.) Report Attached? Yes _(1) No—(C) VOC method # = &g •L z/o p method # _ method # _ .i} m'4r1 ....... ngcay rvenm ana i we - rjease prim or Type GW-59 01%/�� e Rev. 0312000 Signature of Per a (or AUthorizea Agent) (Dale) SUBMIT FORM ON YELLOW PAPER ONLY r - • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: WATER DUALITY DIVISION, GROUNDWATER SECTION COMPLIANCE REPORT FORM _— ------ tfi36MAILSERVICE CENTER RALEIGH NC FACILITY INFORMATION Please Print Clearly or Type 27fi99.1636 Phone: 919 733.3221 Facility Name: Co•a 1s /-� m e ,. (` rqr" .r � •' PERMIT 9: 4J c9 06bS403 EXPIRATION DATE: J - 20// Permit Name (if different): Non -Discharge UIC Facility dress: r 3 0 /4m a r-c.a % br•radr PCof 7 19raep H�Ad�e,,. if.r 25J7'2 Count /y/r�oo--r/) .� Coniact Person: La 40 hpti Ili! Telephone Telephonefl: $2X-75G'y/J/ Well Location/ Site Name: t = yr ,1 T FI✓ew No. of Wells to be Sampled:_ bom Pe,m I) Well Identification Number (from Permit): Mkj-/g For Groundwater Treatment Systems Well Depth: / e . ft. Well Diameter:?. in. Check One: ❑ Influent (98) Screened Interval: w/r ft. to ^b4 ft. ❑ Effluent (99) Depth to.Water Level: ft. below measuring point. Measuring Point (M.P.) is: 2. 4 ft. above land surface. Relative M.P. Elevation In it.: Gallons of water pumped/bailed before sampling: [_ Date sample collected:/24[Aloe Field analysis: pH � .s % , Specific Conductance ' uMhos Temp. °C, Odor Appearance NPDES TYPE OF PERMITTED OPERATION BEING MONITORED —Lagoon Remediation: Infiltration Gallery Spray Field ' _ Remediation: Rotary Distributor —Land Application of Sludge Other. NOTE• Values should reflect dissolved and , JQ VFD colloidal concentrations. N 2 8 2009 / Date sample analyzed: SEc tie //dal Information proc Laboratory Name: ru•u f e r 7_ivc I WO/n a Irig Unit Certification No. So PARAMETERS (Samples for metals were collected unfiltered '— YES _NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Coliform: MF Total /100m1 Phosphorus: Total as P� 3yd8 z0,/G mg/I (Note: Use MPH method for highly turbid sampl�y- Orthophosphate mg/I Dissolved Solids: Total/2 zo o 1 mg/I Al - Aluminum /z/jr/eN Iro, /o o mg/I pH (when analyzed) �� 0 S units Ba - Barium / 2 , ie� M. z 17- Mg/1 TOC 12Pc lo mg/I Ca - Calcium 1-2111.1ood 59.3 mg/I Chloride /_z; /4r/oV czo mg/I Cd - Cadmium_ 2/ /olo 8 [d.00/ mg/I Arsenic i o a mg/I Chromium: Total l? /clog CO•040 mg/I Grease and its Im Cu - Copper mg/I Phenol mgill Fe - Iron mg/I Sulfate LZ,//9,169 Jo mg/I Hg - Mercury mg/I Specific donductance uMhos K - Potassium Mg Total Ammonia mg/I Mg - Magnesium /2 / k mg/I TKN-asN mg/I Mn- Manganese. i2ujilet? _mgill _YES --NO) Ni -Nickel / Z1 /Mort L e.O le mg/I Pb - Lead le /oy < n, c o.S mg/1 Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) Sr/ert.:a.n /zlJt [o o)e JZ OR (GC,GC/MS,HPLC) (Specify test and method ft. Attach lab report.) Report Attached? Yes / (1) No_(0) VOC : method #=_£PA-G2/a4 : method N = : method N = GW-59 Slgnalute of Pe(mit ee (Or Azed gnl1� Rev. 03/2000 (Date) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Permit Name (if Facility Address Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type mericw .t County 1J A rd oa,e ( % Telephone #: V29-` ,Ti -yrl l No, of Wells to be Sampled:,_L, Well Identification Number (from Permit): /'N!d^/N For Groundwater Treatment Systems Well Depth: /S it. Well Diameter: 2- in. Check One: ❑ Influent (98) Screened Interval: ,-/R it. to '-14_ it. ❑ Effluent (99) Depth to Water Level: _& _ft. below measuring point. Measuring Point (M.P.) is: 2.40 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 2 Date sample collected: 12yod 8 Field analysis: pH G •$D , Specific Conductance Umhos Temp. /6 °C, Odor Appearance PARAMETERS (Samples for metals were collected Lin COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbld samples) Dissolved Solids: Total lzlzalo 3916 mg/I pH (when analyzed) tz//c/es L.so units TOC 12/ 30o8 3.91 mg/I Chloride lz/�io8 cs.o mg/I Arsenic /21/6_/rq8 e&.o/0 mg/I Grease and Oils mg/I Phenol mg/I Sulfate a'jglof,' /4.7 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1696-MAIL SERVICE CENTER PERMIT#: W49000560.3 EXPIRATION DATE: e -20// Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED —GLagoon Remedialion: Infiltration Gallery Spray Feld ' _Remedialion: Rotary Distributor _Land Application of Sludge Other: NOTE• Values should reflect dissolved and . I4'1-ei1 vppti colloidal concentrations. /qN 2 200 LL_.. Date sample analyzed: $ c e br //cl�rnauD p 9 Laboratory Name: W a f e r C b rw"�rocebm Certification No. SU r tered / YES _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Orthophosphate img/I Al -Aluminum /2//4/vid Ze• i0v mg/I Ba -Barium IU;tile8 o,/rs" mg/I Ca - Calcium - /z//c/oft Ir4l mg11 Cd - Cadmium /2//�/ort < .60/ mg/I Chromium: Total /W/oar < 6.910 mg/I Cu - Copper "mg/I Fd - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese g/i _YES ✓ NO) NI-Nickel/c,/08 <o•o/o mg/I Pb - Learf /zlze ldY e e . oQS mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) e vti;ejn 12//6Ia8 Lo.614 �iii leg y'3 17 � ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes ✓(1) No_(0) VOC : method # = EpA -42mh method # = method # = Rev. 03/2000 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Permit Name (if Well Location/ Site Name: SUBMIT FORM ON Please Print Clearly or Type Telephone #: R-25?-a.s1 - r No. of Wells to be Sampled:. Well Identification Number (from Permit): A10-/5 For Groundwater Treatment Systems Well Depth: I ag w It. t Well Diameter. Z in. Check One: ❑ Influent (98) Screened Interval: /A ❑ Effluent (99) Depth to Water Level:_Ltt. below measuring point. Measuring Point (M.P.) is: ft. above land surface. Relative M.P. Elevation in It.: Gallons of water pumped/bailed before sampling: I_ Date sample collected: 121IV49 V Field analysis: pH 4— 9 S , Specific Conductance ' uMhos Temp. / e °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT#:WeOOOSGo3 EXPIRATION DATE: 1 - Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infillrallon Gallery Spray Field . _Remediation: Rotary Distributor _, Land Application of Slud Other. _ % 6 t�!'� r, NOTE• Values should reflect dissolved and 14 . AN 9 �Tv_kh�. colloidal concentrations. Jnrorr 8 2009 Date sample analyzed: x6e 6 e ll k w na01NQscessin9 Vn,t Laboratory Name: i.�./far Tee A Certification No. S-0 PARAMETERS (Samples for metals were collected unfiltered_�YES _NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N - mg/I Coliform: MF Total /100ml Phosphorus: Total as P /zr/.3e/nsr zo./� mg1l (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total z Zo o mg/I Al - Aluminum /T�o� �c•/0° mg/I pH (when analyzed) units Ba - Barium /z/i rs. n6 mg/I TOC a13aloiir 1/0 IN mg/I .NO Ca - Calcium z;%2oR y4• z m /I g/I Chloride z zn o mg/I Cd - CadmiumJ2i,/eX 6.00 m 4 9 Arsenic 12-iwo v 4A.O/6 mg/I Chromium: Total /Va o? w•o /D mg/l Grease and Oils mg/I Cu - Copper mg/l Phenol mg/I Fe - IrorY -mg/I Sulfate /�l/g�o 8 /Z 2 mg/I Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg Total Ammonia mg/I Z Mg - Magnesium o 2 •1 mg/I TKN as N mg/I Mn - Manganese v e m /I 9 _YES NO) Ni-Nickel /z//G/°rt zo.o/'o mg/I Pb - Lean /z/ieleu 46.e06'mg/1 Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) rSe/ee;ow.� 2Z�loS to 0//9mo/t ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) RepottAttached? Yes __t'(1) No_(0) VOC method #=_9p//-6 2/0 D method # = method it = Rev_ n3/20nn I. Volatile Organics Quantitation MW2 EPA Method 6210 D Limit Parameter (oob) (pnb) 1,1-Dichloroethane 0.5 BQL 2,2-Dichloropropane 0.5 BQL Chloroform 0.5 4.0 1,1,1-Trichloroethane 0.5:' BQL l,l-Dichlompropene 0.5 BQL Carbon Tetrachloride 0.5 • BQL Benzene 0.5 ' BQL 1,2-Dichloroetharre 0.5 BQL TricNoroedtene 0.5 BQL 1,2-Dichlompropane 0.5 BQL Dibrotmmethane 0.5 BQL Toluene 0.5 BQL 1,1,2-Trichlorocdwre 0.5 BQL I,3-Dichlompropane 0.5 BQL Tetrachloroethene 0.5 BQL 1,1,1,2-Tetrachloroethane 0.5 BQL. 1,1,2,2-Tetrachloroethane 0.5 BQL 1,2,3-Trichlompropane 0.5 BQL Heaacblorobutadiene 0.5 BQL Brormbenzane 0.5 BQL Ethylbeazece 0.5 BQL Styrene 0.5 BQL Bromoform 0.5 BQL P1sopropyltoluene 0.5 BQL' N-Butylbenzene 0.5 BQL Naphthalene 0.5 BQL 1,3,5-Trimethylbenzeoe 0.5 BQL 1,2,4-Trimethylbenzenc� 0.5 BQL 1,2,4-TrichIprohemrne 0.5 BQL 1,2,3-Trichlorobenzene 0.5 BQL Chlombeofene l 0.5 BQL 2-Chlorotoluene - 0.5 BQL 4-Chlorotoluene 0.5 BQL Tert-Butylbemene 0.5 BQL Sec-Bwylbetzene 0.5 BQL 1,4-Dichloroberzene ) -- 0.5 BQL. 1,2-Dichlorobeozene , ' 0.5 BQL Total Xylenes - 0.5 BQL I-Propylbemene 0.5 BQL N-Propylbenzene 0.5 BQL 1,3-Dichlorobenzene 0.5 BQL D'bromochlorome0rane 0.5 BQL Dichlorodifluoromethane 0.5 BQL Chloromethme ' 0.5 BQL Vinyl Chloride 0.5 BQL Brumomethane 0.5 BQL Cidoroethana 0.5 BQL Ttichlorofluoromethane 0.5 BQL 1,1-Dichloroethene _ 0.5 BQL Methylene Chloride 0.5 BQL Trans-1,2-Dichlomethene 0.5 BQL Cis-1,2-Dichloroethene 0.5 BQL Bromodichloromethane 0.5 BQL Bromochlommethane 0.5 BQL Cis-1,3-Dichloropropene 0.5 BQL Trans-1,3-Dichloropropene 0.5 BQL Methyl-Tert-Butyl ether (MTBE) 5.0 BQL Isopropyl ether (1PE) 5.0 BQL Dilution Factor 1 Sample Number 634655 Sample Date 12/16/08 Sample Time (hrs) 0700 Analyst NM BQL = Below Quantitation Limits - = Not Available A M*10 0 a 0 MWll MW12 MW13 MWA MW15 fmmbl fnnb2 fmmbl bpbl 1 1 1 1 1 634656 634657 634658 634659 634660 12/16/08 12/16/08 12I16/08 12/16/08 12/16/08 0730 0800 0830 0900 0930 NM NM NM NM NM ppb = partsperbillion inmbl 1 634661 12 I6108 1000 NM GW-59A COMMIANCE PEPORT FOMI Perm:t#t✓C91000S'60;3 (Submit one each monitoringperiod With GW-59jorms) 1 2 3 4 5 ",.mil aaia munnanng results were due. ( 1 Will this me be.submitted after the established due date? Was any required information missing on the G)i`-59 repof`f forms? IF the answer to question 1 or 2 is 'YES ; list in the space provided belt explain the problems encountered in obtaining the required information. Are dny of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing tap, missing identification plate, area overgrown, etc.)? Ijthe answer is "Yes'; contoct the Regional Ofce jorguidmse Are any monitored constituents equal to or.above the established standards? if the answer to question 41, "NO; skip to secton 8. If the answer to question 4 is "YES"list the affected wells individually with consfftuent(s) and concentration(s) exceeding standards in the space provided below. MLL7� 13 = TO s113f22oo mL �1 sTee f9,//lMy • 13 = Cl,brW¢ ll aP OZjiny/1 f2 Gr`/5' h7FA3A111r SP /3 " 2•i3 A7,ilyA /y same constituents) In the same wells) in the last two years?moo u� �..Jj ezceeoea previously for the If the answer to question 31 sskip to section 8. if the answer to question 5 is 'YES", list in the space provided below, each well with constituenl(s) exceeding standards, concentrations) reported, and sample collection datefor each occurrence (for the last two years). j2 6,y76 A" 4V 13 /.1 z l y „ N'. IS /s• v 6 1 Are b7 IN or ff the answer is 'YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAi OFFICE iMMEDiATELYFOR GUIDANCE. If the answer is 'NO'; monitoring wells maybe improperly located; contact the Regional Office. Is the permittee implementing previously approved actions required by the Division involving this groundwater quality problem? ff the answer to question 7 is 'yES, describe those actions in the space provided below. If the answer to question 7 fs 'WO-, contact the Reninnal ofnec ,.,ur:., on i ne person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. YES ti ce IlMe G%V-59A 1218/2003 CW-59ACOMPLIANCEREPORT FORM Pe:t9oD6513 (Submit one each In oil itoringperiod with GW-59jorms.) r+l Enter date monitoring results were due. ( 1 Will this monitoring report (GW-59 and GW-59A) YES be,submitted after the established due date? Was any missing on the GW-59 report it- ine answer to question 1 or 2 is 'YES; list in the space provided below the welt identificatior,tiumbers) znd explain the problems encountered in obtaining the re wired information. bed,n, � /Z�+ /S' 4- ivoj h0v� eNv�Sh Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES identification plate, area overgrown, etc.)? Ijthe answer is "Yes-', cauact the Regional Ofee jorgntdmice. 4 1 Are any 5 or above the it ine answer to question 4 is NO', skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentrations) exceeding standards in the space provided below: m49 /3 -T105- `7:22) nkslL- rVl the constituents ieentitieci in question 4 above, have standards same constituent(s) in the same well(s) in the last two years? it me answer to question 5 is "NO" skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). in at or n the answer is -'rts••, a groundwater quality problem maybe OFFICE IMMEDIATELYFOR GUIDANCE. If the answer is "NO'; located; contact the Regional Office. Is the permittee imps groundwater quality It the answer to question 7 is 'YES, describe those actions in the space If the answer to question 7 is "NO", contact the Reoional Office will by the :ONTACT THE REGIONA/ wells maybe improperly The person completing this portion (GW-59A) of the monitoring report shoulc'sign below and submit th s form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. NO C W-59A 12/8/2003 SUBMIT FORM ON GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Office -- —FACILITY INFORMATION //�� /n Please P_ririf Clearfy: or -Type -I FacililyName:_ l_ O/O�S f7!' Permit Name Name (if different): PAPER ONLY ��•2' /•vc ea iso County /1/d"0 r✓ Cont•e •' tcactnrt Person: (s,.,) %� %f l r �.•rt°w 00 Telephone if:92 X- 25'L - 4 / 1 I m .ti _ Well Location/ Site Name: Sr ui P'� 415 A D'j- No. of Wells to be Sampled: (,cm P-11) Well Identification Number (from Permit): Mkj- IS For Groundwater Treatment Systems Well Depth: / 6 ft. Well Diameter:?- in. Check One: ❑ Influent (98) Screened Interval: ft. to f A ft. ❑ Effluent (99) Depth to Water Level: 8•s ft. below measuring point. Measuring Point (M.P.) is: 3 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/billed before sampling: / Date sample collected: 8.26-d N Field analysis: pH ? D (J , Specific Conductance uMhos Temp. _12- °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMITS: EXPIRATION DATE: .57. 2611 Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED ,/ Lagoon Remedialion: Inlilhalion Gallery Spray Field _Remediation: Rotary Distributor _ Land Application of Sludge Other: NOTE• Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: •,SrP hellerd LaboratoryName: !vl rF ier Tech ,....r*uun I•'rou:;,,tt)r; t:)., Certification No. IS-y .u"t PARAMETERS (Samples for metals were collected unfiltered AYES _NO and field acidif^ri _YES NO) COD mg/1 Nitrite (NO2) as N mg/ -(<ol 9.2q.oN 4'0.0e,5 m I Coliform: MF Fecal /100ml Nitrate (NO3) as N �.p mg tgCp `'a _ c a. oo,y—r�mg/I Coliform: MF Total /100ml Phosphorus: Total as P_ (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total T-/2•a8 9.99 mg/I pH (when analyzed) units TOC mg/I Chloride mg/I Arsenic $• L9-wg <0.066- mg/I� Grease and Oils mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/1 Orthophosphate AI- Aluminum 8-z9.09 10.050 Ba- Barium 0'9 /3 Ca - Calcium 8'2Y-08 G9. ✓ Cd - Cadmiumg-2g•08 <0-oozy Chromium: Total 8.29.08 Zo.00Stf Cu - Copper I Fe - Iron / Hg - Mercury 1 nc mg/1 j �( _ In �Ct in Units) ;z" Tb(- K - Potassium 15 Mg - Magnesium N z5 �8 31 C�nlo�fd Mn -Manganese F 29 08 �2.0 M 14 ^ i 1 tb report.) No _ (0) UZd cJ l' 1 j o-1A( p> , Rev. 03/2000 S)gnalure oI Permd (or Authorized ent) (Date) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: PLIANCE REPORT FORM FACILITY INFORMATION �/] Please Print Clearly or Type Facility Name: CoFf5 /`/r-vricv42 Permit Name (if different): Facility Address: 3 a Th r p . Well Location/ Site Name: County orn = /JOwfL r t Telephone #: No. of Wells to be Sampled: •, __ _ Well Identification Number (from Permit): Mu-'/y For Groundwater Treatment Systems Well Depth: J ,, it. Well Diameter: 2 in. ck One: ❑ Influent (98) Screened Interval: 'IA- It. to rt'/A ft. ( Dep'"'IA-Che th to Water Level: %, 3 f1blow measuriEl Effluent 9) . e ng point. Measuring Point (M.P.) is: 2_41 ft. above land surface. Relative M.P. Elevation in It.: Gallons of water pumped/bailed before sampling: 2• Date sample collected: Field analysis: pH1 •9S , Specific Conductance uMhos Temp. // °C, Odor Appearance Q] DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: LOOCC"5G03 EXPIRATION DATE: Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field _Remediation: Rotary Distributor _ Land Application of Sludge Other: Iry _k (" NOTE: Values should reflect dissolved and . OCT f, 0 2008 colloidal concentrations. hltarrna6> I1'rnrc_srtq Ono Date sample analyzed: rSF6 8et(erd Laboratory Name: G� afr TPcI, Certification No. 3-0 PARAMETERS (Samples for metals were collected unfiltered AYES _NO and field acidified COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100m1 (Note: Use MPH method for highly turbid samples) Dissolved Solids: Total 8-29-oS L/9/ mg/I pH (when analyzed) 9-26-63 701 units TOC_9-)2-og y.W' mg/I Chloride_1-24LO$ <s.a mg/I Arsenic 2.2ci-o6 &Cos' mg/I Grease and Oils mg/I Phenol Sulfate A-2ef-eg g eld.v mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P9-2-08 o.zomg%I Orthophosphate mg/I Al - Aluminum a-29•o8 leo•cso mg/I Ba - Barium S- 27- 69 o• //!o mg/I Ca - Calcium 29 0$ 7;.2. mg/I Cd - Cadmium N• z9 0 8 eo.0o 2. mg/I Chromium: Total a-2-9-a� Z&OaS mg/I Cu - Copper mg/I Fe - Iron mg/I Fig - Mercury mg/I K - Potassium mg/I Mg - Magnesium •2112% 4 3 mg/I Mn - Manganese5- 22-0f 0.581 g/I /I _YES NO) Ni-Nickel 8 2Y-o8 eo•oos mg/I Pb - Lead S-2161il' mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other 11r(Specify Compounds and Concentration Units) d.0 r» il-2q-Ots 4e Na mrlL �PLe�-iuM 4>''Z9•tl6� LA 04Snr9 tj ORGANICS: (GC,GC/MS,HPLC) (Specify test and method If. Attach lab report.) Report Attached? Yes—i(l) No _(0) VOC : method # = ✓4-• 0 rc method # = method It = GW-59 Rev. 03/2000 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: l 6 W 't s -t-4 m e Permit Name (if different): Facility Address: - o D rh 1° n C q n- { l 40 i 0 ti so -an w C 2 IT 2 tC'IY) ISIa1e1 (iivl Contact Person: tt Well Location/ Site Name: Se v', Er '-C',,, F I.,•rw-F SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type .ti County IYl s Oowe It Telephone N: A28-756-I n r No. of Wells to be Sampled:,, _ Well Identification Number (from Permit): h•. W - 13 For Groundwater Treatment Systems Well Depth: / 3— it. Well Diameter•:? in. Check One: ❑ Influent (98) Screened Interval: —14 It. to a/.J, it. ElEffluent (99) Depth to Water Level: V ft. below measuring point. Measuring Point (M.P.) is: 2IP ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: _L Date sample collected: 9 - ZG -o Field analysis: pH 1• zS , Specific Conductance ' Temp. _/I 'C, Odor Appearance uMhos DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT ff: GJ©0605bo3 EXPIRATION DATE: Non -Discharge UIC TYPE OF PERMITTED OPERATION BEING MONITORED Lago� Remediation: Infiltration Gallery Spray Field _Remediation: Rotary Distributor —Land Application of Sludge Other: r-%r- , . -. IVV 1 n- values snouw reuect dissolved and . 0f f r? 0 Z�C��i colloidal concentrations. Date sample analyzed: Laboratory Name: 0✓..T�r �c h r''Ij`'"• I Certification No. 5-0 PARAMETERS (Samples for metals were collected unfiltered AYES _NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I (Note: Use MPN method for highly turbid sample Orthophosphate mg/I Dissolved Solids: Total •29•°� 72� g/I AI -Aluminum -2y-ois <o•osom /I pH (when analyzed) 2-2VOS 7;39units Ba -Barium 9.Z9•D o, o(-/3 mg/I TOC mg/I Ca - Calcium IS- Z9-o8 31•S mg/I Chloride mg/I Cd- Cadmium S'21,05 .<6.602 mg/1 Arsenic 2-n-og —�o•msmg/I Chromium: Total-z9'•o8 ZD•oo mg/1 Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate mg/I Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg -Magnesium R 20•09 g/l TKN as N mg/I Mn - Manganese $-z -e) 8 /• /2 g/I _YES � NO) Ni - Nickel 8-Zyo1s 40-0as mg/l Pb - Learf A- 29.09 •Co• Dos mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) -_5_Dd.um 8 Z`-oe yg.2 n 11 SPLNNr.�m V-29-e GD.985"�I( ORGANICS: (GC,GC/MS,HPLC) (Specify test and method fl. Attach lab report.) Report Attached? Yes-_(1) No _ (0) VOC : method # = method # = method N = FAYA "GW-59 Rev. 03/2o00 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Permit Name (if Facility Address Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type � •� r r9 ✓t' �ct4A- -I hrpvteJ Kof FV76•2 County�1IS10~011 A N (rn) Telephone #: 82K• 9S'G - y/// 7ffluc114' No. of Wells to be Sampled:,_L— Well Identification Number (from Permit): MW -12 For Groundwater Treatment Systems Well Depth: 13 it. Well Diameter: T- in. Check One: ❑ Influent (98) Screened Interval: ^-/.a it. to �" �/} It. ❑Effluent (99) Depth to Water Level:-9—ft. below measuring point. Measuring Point (M.P.) is:Z. ( It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 2- Date sample collected: •24.0 Field analysis: pH 7. 3D Specific Conductance Temp. / 0 °C, Odor Appearance . uMhos DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT If: /"(76000 s 603 EXPIRATION DATE: Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED _CLagoon Remediation: Infiltration Gallery Spray Field _Remediation: Rotary Distributor Land Application Other: NOTE: Values should reflect dissolved and 21)0l3 colloidal concentrations. •ntCKlrL,l•J'� !>r,,• ^.;S h}(j I !nr Date sample analyzed: sx,- 4elle / OvrO,r;O"', Laboratory Name: W afri iP e h Certification No. 6`D PARAMETERS (Samples for metals were collected unfiltered AYES _NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/1 Coliform: MF Total /100ml Phosphorus: Total as P 9--r/-e 8 6.2! m9 /I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total9-29.08 2,jl mg/I Al - Aluminum 16-29. J9 _�e.050 mg/I pH (when analyzed) 9-2b•eX 7.31 units Ba - Barium S-2-9.0b C"0vV mg/I TOC 9-12-W3 7• 2- mg/I Ca - Calcium St •Z9.0-8 30.9 mg/I Chloride 9-27-6 a -es•0 mg/I Cd - Cadmium 9•z4.0 t; 6.00 z mg/I Arsenic !6-29-old t0.00 mg/I Chromium: Total F-0-66 Cy.00S mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate 9-29.09 mg/I Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg- Magnesium 9-251.0 8 g/I TKN as N mg/I ///�//r7.16-, Mn - Manganese 8.29 -oE ccc,rhg/l �GW-59 _YES / NO) Ni - Nickel SP-z9-08 .40•06Smg/I Pb - Lead 8.29.0$ -eo•066- mgA Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) Sad 2ne F-4?-09 �(y.3 M514 SrLea;oxr 8!-z5,-og LO.15457sn9j ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes_(1) No _ (0) VOC : method # = method # _ method If = SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT Facility Name:_ Permit Name (it °' t L Contact Person: f'•� Well Location/ Site Name: Please Print Clearly or Type eo%CA ej Z County /D e d n rJ e l l — Telephone #: _82 S' ?S b •- bff / 1 — No. of Wells to be Sampled:,, Well Identification Number (from Permit): /N &J -// For Groundwater Treatment Systems Well Depth: 1 It. Well Di meter: 2 in. Check One: ❑ Influent (98) Screened Interval: r //} It. to " fr It. ❑ Effluent (99) Depth to Water Level: _AD ft. below measuring point. Measuring Point (M.P.) is%24 ft. above land surface. Relative M.P. Elevation in it.: Gallons of water pumped/bailed before sampling: 2. Date sample collected: •24•0 Field analysis: pH I °1 , Specific Conductance uMhos Temp. °C, Odor Appearance DEPARTMENT OF ENVIRONMENT 6 NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT#:WeoPaSGa3 EXPIRATION DATE: .S-?0 Non -Discharge UIC TYPE OF PERMITTED OPERATION BEING MONITORED _GLagoon _Remediation: Infiltration Gallery Spray Field _Remediation: Rotary Distributor _ Land Application of —Sludge Other: �3' 6-0 mnra colloidal concentrations. r,lh,t.1160:: Date sample analyzed: $ k ! br i!° eJ Laboratory Name: W A P r t c h Certification No. S e) PARAMETERS (Samples for metals were collected unfiltered ""YES _NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P 9-fi•6 9 0.2bm9 /I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total 5724 08 259S mg/I Al - Aluminum $-29-o9 Zo. oso mg/I pH (when analyzed) 9-26.OV (,•9y units Ba -Barium $•29.Ox O•og9 m /I TOC _9 /2• 08 •/ mg/1 Ca - Calcium _9-29• 09 16.3 mg/I Chloride 9.27:08 9.0 mg/1 Cd- Cadmium V-29•ore 40•oo2 mg/I Arsenic R 29 OS LD•oOS mg/I Chromium:Total`d-2q•o8 Z6•065mg/I Grease and Oils mg/l Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate A•29-0S /o/ mg/I Hg- Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium-29 e 8 S oS 9/1 TKN as N mg/I Mn - Manganese $ 29 0�3 f0.7s`cj/I _YES efNO) Ni - Nickel 21-Z92`1? G 0.0(56' mg/I Pb - Lead MO. Zn - Zinc mg/1 Ammonia Nitrogen mg/I, Other (Specify Compounds and Concentration Units) 5eriiuw R 01? 176-Y mq// SfI PA"UM V-29. c) 6-66LTr.;61 n ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) ReportAttached? Yes—(1) No_(0) vOC : method # = �4 m d rc-- d (` C. method # = method If = GW-59 Rev. 03/2000 /0-9-03 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: LoA Jr 5 H rn rl c f Permit Name (if different): Facility Address:_ (v 3 14 rh o n•r c A n. T _lM pn't o N.1 I5b"0 L 289 -z lla I •° Ll.) ILO) Contact Person: �Is'� maw . Well Location/ Site Name: V • r Rs ti f6AJ SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type N County ✓/I + ve td c / I Telephone if: V 26-'7S6 -1/11 1 No. of Wells to be Sampled:. Well Identification Number (from Permit): M w-/D For Groundwater Treatment Systems Well Depth: Z R it. Well Diameter:_ in. Check One: ❑ Influent (98) Screened Interval: • I"IA- ft. to "'14 It. ❑ Effluent 99 Depth to Water Level: / Z- ft. below measuring point. ( ) Measuring Point (M.P.) is:?. 3 It. above land surface. Relative M.P. Elevation in It.: Gallons Of water pumped/bailed before sampling: Date sample collected: -26-09 Field analysis: pH'7- (P 7 , Specific Conductance uMhos Temp. f—°C, Odor Appearance PARAMETERS (Samples for metals were collected COD mg/1 Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total'9-24-oP so mg/I pH (when analyzed) 9-2yo? 7.72 units TOC 9-(z•oy cp b mg/I Chloride-8.2?:o8 9.3 mg/I Arsenic 2-29-07 c o.00 mg/I Grease and Oils mg/I Phenol mg/I Sulfate 9-29°6g 157 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT N: /v o0Qar609 EXPIRATION DATE: r 26// Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED -� Lagoon _Remediation: Infiltration Gallery Spray Field . _ Remediation: Rotary Distributor _Land Application ;o6.Sludge,,,-- Other: _ NOTE, Values should reflect dissolved and . OCT 3 Py, ZOOS colloidal concentrations. J 1ii Date sample analyzed: Sc'c` b E/%e a! Laboratory Name: w AV g o, Te c h Certification No. 3 a YES _NO and field acidified _YES Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P A-y•08 mg/I Orthophosphate mg/I Al - Aluminum E- 29-o8 t0.0so mg/I Ba - Barium 9-29-0'6 40.020 mg/I Ca - Calcium 19-21-02 6.930 mg/I Cd - Cadmium 9-Z9-o19 < 0°oo2- mg/I Chromium: Total8-24-6e to -cos mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium F-29.0x 6,111 mg/I Mn - Manganese K-21-08 415.00.5- mg/I NO) Ni - Nickel 2-zg-e9 40.00mg/I Pb - Learf 2-29-08 GO.00s- mg/I Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) Soot%um g-Z9-o8 /2S--m�/L _5PL6n,;Om �j•29•o8 ca.00s ORGANICS: (GC,GC/MS,HPLC) (Specify test and method C Attach lab report.) Report Attached? Yes_(1) No — (0) VOC : method ft % i L l i r7 't__11 +k),14 L� method N m olhnrt N _ / d Rev.03/2000 Signalur es P rmmeejot Au)rybrrzedAgent) (Date: SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM - Facility Name:_ Permit Name (if Facility Address Well Location/ Site Name: ri N Please Print Clearly or Type County Fri= {iowe If Telephone #: 8 2ff - 7S6 - 9 t I 1 No. of Wells to be Sampled:,,„—L;, Well Identification Number (from Permit): M W - 7L Well Depth: i5 ft. Well Diameter: & in. Screened Interval: N/it ft. to w/pv ft. Depth to Water Level: 3 S' ft. below measuring point. Measuring Point (M.P.) is: Z•3 ft. above land surface. Rel Gallons of water pumped/bailed before sampling: _ y_g_ Field analysis: pH 7- 2 / , specific Conductance Temp. ��'C, Odor •App PARAMETERS (Samples for metals were collected un COD mg/I Coliform: MF Fecal Coliform: MF Total /100ml /100m1 (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 8-29•eg /1S mg/I pH (when analyzed) 9.26-o9 TOC 9-12-0$ 9.3y units Las'a mg/I Chloride2-27-oV <s:o mg/I Arsenic <o.eQ�Fmg/I Grease and Oils Phenol mg/I mg/I Sulfate o mg/I Specific Conductance uMhos Total Ammonia TKN as N mg/I mg/I GW-59 For Groundwater Treatment Systems Check One: ❑ Influent (98) El Effluent (99) alive M.P. Elevation in It.: D ate sample collected: _9-26-69 uMhos earance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER DUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #:WO000,gG, 3 EXPIRATIONDATE: 5--2011 Non -Discharge UIC NPDES TYPEg-)E PERMITTED OPERATION BEING MONITORED / Lagoon Remediation: Infiltration Gallery Spray Field _Remedialion: Rotary Distributor _ Land Application of Sludge Other: NOTE• Values should reflect dissolved and „CT ZQI)� colloidal concentrations. 11 Dale sample analyzed: Laboratory Name: [r) A+r e Tech Certification No. S-o :ered -� YES _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P 7 �-o9 Zo.16 mg/1 Orthophosphate mg/I AI- Aluminum _T-29-os1 co.oso mg/I Ba - Barium - 29- a .037 mg/I Ca - Calcium 9. 29- oy? /. G mg/I Cd- Cadmium 2-29-o8 40.002- mg/I Chromium: Total 8-29•o59 4acoy, mg/1 Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium -29.0 V L9 os mg/I Mn -Manganese. 8 29 0 0.0o mg/I _YES ! NO) Ni -Nickel 2-29-os Z6•p0S mg/I Pb - Lean Y-29-o9 co.00 mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) z9 opt 9 g`l"t— �P�BNi�M 5i-29•68 . zo.OAs t%'^ ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) ReportAttached? Yes_(1) No_(0) VOID method # = method # = method # = /`/ r/r C rt,a col SUBMIT FORM ON YELLOW PAPER ONLY WITT• DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: WgTER QUALITY DIVISION, GROUNDWATER SECTION COMPLIANCE REPORT FORM 1636 MAIL SERVICE CENTER 1 FACILITY INFORMATION Please Pr RALEIGH NC 27699-1636 Phone:t 919 733.32: Print Clearly or Type Facility Name: ('�,�.�J d olio nI c *!I PERMIT Ii: meo4S4°3 EXPIRATION DATE: Permit Name (if different): Non -Discharge UIC i? Facility Address: 616 M_P N 'c.rrt�J i FK NPDES�- Well Location/ Site Name: County = c.� ll Telephone N: 2lir`- 9S L No. of Wells to be Sampled: Well Identification Number (from Permit): /Y/!✓'/f For Groundwater Treatment Systems Well Depth: / G it. Well Diameter:? in. Check One: ❑ Influent (98) Screened Interval: � /� ft. to ' /R II. 0 Effluent (99) Depth to Water Level: �—fl, below measuring point. Measuring Point (M.P.) is: 3 It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: / Date sample collected: 2 -O Field analysis: pH 700 , Specific Conductance ' uMhos Temp. / 2 °C, Odor Appearance PARAMETERS (Samples for metals were collected unfiltered COD mg/I Nitri Coliform: MF Fecal /100m1 Nitr Coliform: MF Total /100ml Pho (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/1 pH (when analyzed) units TOC 9-/2• eY C �s9 mg/I Chloride mg/I Arsenic 1' 29, of 40•oes mg/I Grease and Oils mg/I Phenol mg/I Sulfate mg/1 Specific Conductance uMhos Total Ammonia mg/1 TKN as N mg/1 TYPE OF PERMITTED OPERATION BEING MONITOF�Eb Lagoon Remediation: infiltration GallerryJ- iV Spray Field _Remedialion: Rotary Distributor Other: —Land Application of Sludge] w cr'o I� O NOTE' Values should reflect dissolved colloidal concentrations. RECE Date sample analyzed: SFr JUN 1 6 2009 Laboratory Name: �ccii r1 -- Certification No. Sy Inrormatwn Processing Unfl _te,� YES _NO and field acidified to (NO2) as N mg/I ate (NO3) as N mg/I sphorus: Total as P mg/I Orthophosphate mg/I Al - Aluminum 11-27•01? e e.dfd mg/I Ba-Barium_f-zg•0Y 6./3Y mg/1 Ca - Calcium- _Q 29•m� G9• y mg/I Cd- Cadmium Ar4•Dst 40.oD2 mg/I Chromium: TotalR-29•DSr s0.00r mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/l K - Potassium mg/l Mg-MagnesiumB•29'•05' 3/•G mg/l Mn - Manganese!?• ?I- it ? 2. "S mg/I on VL71 0 _YES ___,�NO) Ni-Nickell•29.0ti c0.ao " mg/I Pb - Lean X. 291• a b- 40. na,N-- mg/I Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) fir• lew.;,,,n T!• Lv •0 7L �a •�!L'r"p�.( G ORGANICS: (GC,GC/MS,HPLC) (Specify test and method If. Attach lab report.) ReportAttached? Yes —(I) No _(0) VOC : method # = method If = method If = /Y/neA,d,ca SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: C Permit Name (if different): A Well Location/ Site Name: r�. Please Print Clearly or Type County & Oowr f f Telephone #: YZY-73 i- r/ No. of Wells to be Sampled: Well Identification Number (from Permit): /hu-/3 For Groundwater Treatment Systems Well Depth: / 6 ft. Well Diameter: 2 in. Check One; ❑ Influent (98) Screened Interval: "�� ft. to /'gyp ft. El Effluent (9) Depth to Water Level: fr ft. below measuring point. Measuring Point (M.P.) is:?4 It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: / Date sample collected: - 4 -o N Field analysis: pH 2•2-1— , Specific Conductance ' uMhos Temp. __L _/°C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER DUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: W &OOOS-40 EXPIRATION DATE: 47'2e// Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon _Remedialion: Infiltration Gallery Spray Field ',_Remedialion: Rotary Distributor —Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. RECEIVED Date sample analyzed: SEF QE�lo�l I, N s Z��9 Laboratory Name: AveCv/Toc Certification No. 5y yw_.1 •'I. C. _cJ i iON PARAMETERS (Samples for metals were collected unfiltered 'YES _NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal J100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/l Dissolved Solids: Total 8-29-6y 72d mg/I AI - Aluminum y29•o8 La054 mg/I pH (when analyzed) 9-4-01 2.3? units Ba-Barium 9.29-oA 6oa%S mg/I TOC mg/1 Ca - Calcium 9-29-58 3/-s mg/I Chloride mg/I Cd- Cadmium t29-o9 ea. ooz mg/I Arsenic 9.29.o R «oe,s' mg/I Chromium: Total 2-2$oV LG•GG.S mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mg/i Fe - Iron mg/I Sulfate mg/I Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium 9-27-41d / mg/I TKN as N mg/I Mn - Manganese Y 29 • a 1 /. / 2- mg/I _YES l NO) Ni- Nickel 9-29-aV <e.00s mg/I Pb-Leari 9!-29•61 [a•oo< mg/I Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) 29, yYz w �t ORGANICS: (GC,GC/MS,HPLC) (Specify test and method If. Attach lab report.) ReportAttached? Yes_(1) No _ (0) VOC : method # = method # = method # = Rev. 03/2000 U W--'!1yA UL)MPLiANCE .REPORT FORM Permit # (Submit one each u'onitoringperiod with GPr=59 forms.) 1 Enter date monitoring results were due. ( 1 Will this monitoring report (GW-59 and GW-59A) be submitted after the established due date? YES NO Was any required information missing on the GW'-59 report forms? YES NO IF the answer to question f or 2 is 'YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. We1tS /3.1-/S t7-oD A p-f hwa+e fb�gt w44,, Td syf:f r %fA 5-;l(.ok /)Im-/3-(/uOJ 70C i.P 501 f4iC I Cblvpij- SranIQ�C /t%wl: zoc� �lw-/S(/"v, TOS 7`0 50";fl' Ph/ca'�tP 3 Are any of the monitorwells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing identification plate, area overgrown, etc.)? If the answer is -yes", YES NO contact the Regional O�ce forguidance. 4 Are any monitored constituents equal to or above the established standards? YES NO If the answer to question 4 is NO , skip to section 8. if the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: 720 r•gl L I 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES same constituent(s) in the same well(s) in the last two years? I If the answer to question 5 is IN skip to section 8. If the, answer to question 5 is "YES'; list in the space provided below, each well with constituent(s) exceeding standar s, concentration(s) reported, and sample collection date for each occurrence (for the last two years). I 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YE NO If the answer is "YES'; a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELYFOR GUIDANCE. If the answer is "NO'; monitoring wells may be improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? lr the answer to question 7 is 'YES'; describe those actions in the space provided below. If the answer to question 7 is "NO" _contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facthty. Failure to do so may subject the permittee to a Notice of Violation fines andlor penalties g The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. l I herebyackngwle�ge that(they�above'informatlon was evaluate, rid the inoraiat(onsubmItted�nYh3s' r'eport.(Comphanc_ _ ort GW 59Aa Isfrue d complete,to the best of my kr owledge_ _ 01 Q Signature Pennittee (or oriz Agent) Date CNV-59A 12/8/2003 GROUNDWATER QUALITY MONITORING: wk r SUBMIT FORM ON YELLOW PAPER ONLY I I I vrvny H I I VIN ( Please print Clearly or Type Facility Name: r9R is rn ev) c vL Permit Name (if different): Well Location/ Site Name: County lr1= rJow• [-t Telephone-#: 5 2 g- 9 b-0 No. of Wells to be Sampled: Well Identification Number (from Permit): 17110For Groundwater Treatment Systems Well Depth: % (/i_it. Well Di meter: in. Check One: ❑ Influent 98 Screened Interval: /"/r>` fL to. ft. ( ) Depth to Water Level: to ❑Effluent (99) —�-it. below measuring point. Measuring Point (M.P.) is: I ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped ailed before sampling: �_ Date sample collected: 2-// 0 7 Field analysis: p..G' Specific Conductance ' uMhos Temp. 7 'C, Odor Appearance PARAMETERS (Samples for metals were collected COD COliform: MF Fecal /100m/I Coliform: MF Total . /100ml (Note: Use MPN method for highly t amples) Dissolved Solids: Total 3/ /.07 mg/I pH (when analyze" LZO 1-2-11-67 units TOC 3•(v 2-I1-o7 mg/I Chloride 57V 12-11-07 mg/I Arsenic < -0,o o s- )7-/l-c mg/I Grease and Oils mg/I Phenol g Sulfate 9. ( -U-o7 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I IJ eta L'Oe l 1 DEPARTMENT OF ENVIRONMENT& NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT#:EXPIRATIONDATE: S--2011 Non-Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING -MONITORED Lagoon _Remedialion: Infiltration Gallery Spray Field Remedialion: Rotary Distributor _Land AoDlicalion of Sludnp NOTE• Values should reflect dissolved Ind , colloidal concentrations. JAN 2 9 2000 Date sample analyzed: See be /(Oa Laboratory Name: r_ r _ pc 1 Abliuville Regional Office Certification No. _.Sd I Ant dfar Prntaetinn _NO and field acidified Nitrite (NO2) as N mg /I Nitrate (NO3) as N mg/I Phosphorus: Total as P_ D,/9 /1-/rod mg/I Orthophosphate m/I AI : Aluminum < o . oS /z-//•e7 mg/I Ba - Barium /7-ll•67 mg/I Ca - Calcium SY• y lz•u•n'Y mg /I Cd- Cadmium 4o.00z /2,//-o'7 m/I g Chromium: Total zo•0.S 1z-//-ofj m g/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium 13 / 2 Il ui mg/I Mn - Manganese z 2 //• a` mg/I _YES =NO) Ni- Nickel «'•ooS' /7•r/-a7 mg/I Pb'- Lead to•oos Zn -Zinc mg/I Ammonia Nitrogen mg/1 Other (Specify Compounds and Concentration Units) .�ocl'utsn ' Sr4 n /Z /I-6 yd ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Att h lab report.) Report Attached? Yes / (1) No _ (0) VOC : method #= 6.2/D 4 Parameter 1,1-Dichloroethane 2,2-Dichloropropane Chloroform 1, 1, 1-Trichloroetmne 1,1-Dichlompropene Carbon Tetrachloride Benzene I Toluene Bromobenzene Ethylbenzene Styrene Bromoform p-Isopropyltoluene N-Butylbenzene i Naphthalene I 1,3,5-Tritnethylbenzene 1,2,4-Trnrethylbenzene 1 _,4-Trichlorobenzene 1,2,3-Trichlombemene Chlorobenzene 2-Chlorotoluene 4-Chlamtoluene Ten-Butylbernene Sec-Butylbenzene IA-Dichlombenzene 1,2-Dichlorobenzene Total Xylenes I-Propylbemene N-Propylbenzene 1,3-Dichlorobenzebe Dibromochloromethane Dichlorodi0uoromethane Chloromedtane Vinyl Chloride Bromomethane Chlomethane Trichloro0uoromcthane I,I-Dichlomethene Methylene Chloride Trans-1,2-Dichloroethene Cis-1,2-Dichlomcthene Bromodichloromethane Bromochloromethane, Cis-1,3-Dichlompropene, Trmu-1,3-Dichlompropene Methyl -Ten -Butyl ether (MTBE) Isopropyl ether (IPE) Dilution Factor Sample Number Sample Date Sample Time (hrs) Analyzed Date Analyzed Time (hrs) Analyst BQL = Below Quantitation Limits = Not Available (ppb) 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.51 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 5.0 5.0 ip1 b) IPPI IPp-bl (pE1 (PPb) (Vpb) iPP1 I I 1 I 1 1 1 605735 605736 605737 605738 605739 605740 605741 12/11/07 12/11/07 12/11/07 12/11/07 12/11/07' 12/11/07 12/11/07 12/19/07 12/19/07 12/19/07 12/19/07 12/19/07 12/19/07 12/19/07 1442 1511 1540 1608 1637 1706 1735 NM NM NM NM NM NM NM ppb = pansperhillion SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: Ca a-1 S mC' P i C p 1ti Permit Name (if different): Farflily Arldrasc• ✓P3a l4mp o\CJl,L riven, i Site Name: Well Depth: Screened Interval: _ Depth to Water Level: Measuring Point (M.P.) Gallons of water pump Field analysis: pH-¢ Temp. ca %y TelCount yrt� ,Juo wet vwk :") ephone #: g 23'`YS !0`411 1 5 vl er era }) N No. of Wells to be Sampled:_ • erom Pertnln (from Permit): 411t)-1 ForGroundwaterTreatment Systems eft. Well Diameter:? In, Check One: ❑ Influent (98) n. to it. ❑ Effluent (99) �ft. be �1low measuring point. �10 ft. above land surface. Relative M.P. Elevation in ft.: ailed before sampling: I Date'sample collected: 2-I Specific Conductance ' uMhos °C, Odor Appearance PARAMETERS (Samples for metals were collected unfiltered r YES COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for hight urblds mpies) Dissolved Solids: Totai .2- 2-11-6 mg/I pH (when analyzed) 2.1-0units TOC to r 2 b 19-11-01 mg/I Chloride G_S'.'b IZ-)i-rM mg/I Arsenic e•o6,5- 12-IID7 mg/I Grease and Oils mg/I Phenol mg/I Sulfate - $r tfa 12-11-0 m /I Specific Conductance uMhos Total Ammonia m g /i TKN as N C --rr ,�. DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT#: LO0cDo°5003 EXPIRATION DATE: Non -Discharge UIC NPDES TYPE QF PERMITTED OPERATION BEING MONITORED Lagoon _Remediation: Infiltration Gallery Spray Field _Remediation: _ Rotary Distributor —Land. Application of Sludge Other:___ NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: 5'ee 6c I ( o rJ LaboratoryName: W9447.1 -7'7,r h Certification No. rLy _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P 0,13 12-11-07 mg/I Orthophosphate mg/I Al -:Aluminum - Z0,0576 17-11•o7 mg/I Ba - Barium a e)3 b 2-11-07 mg/I Ca - Cal� 2-11.07 mg/I Cd - Cadmium <0•moz 12-)J-01 mg/I Chromium:, otal to.af:6- Jr-nn7mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium gll Mn -Manganese 1.5 /z 11-67mg1l _YES —NO) Ni - Nickel 1-0.605 12�11-4img/1 Pb - Lead < 6,ez,5- 12-11•07 mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) (P i 4� •r70S - 1-0 ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes / (1) No _ (0) VOC : method # = 621,9 b : method # = : method # = GW-59 ' �QwQ9��� %�5`� Rev. 0312000 Signawre of Penn'HtZ dr Anlltvnzed A n (Date) Parameter I,I-Dichloroethane 2,2-Dichloropropane Chloroform 1,1,1-Trichloroethane l,l-Dichloropropene Carbon Tetrachloride Benzene 1,2-Dichloroethane Trichloroethene 1,2-Dichloropropane Dibromomethane Toluene 1,1,2-Trichloroethane 1,3-Dichloropropane Teuachloroethene I, 1, 1,2-Tetrachlaroethme I, 1,2,2-Teuachloroedume I.2,3-Trichloropropare Hexachlorobutadiene Bromobemene Ethylber¢ene Styrene Bromoform p-Isopropyltoluene N-Butylbenzene' Naphthalene 1,3,5-Trimethylbenzene 12,4-Trimethylbenzene 1,2,4-Trichlorobemme 1,2,3-Trichlorobemene Chlorobenzene 2-Chlorotoluene 4-Chlorotoluene Tert-Butylbenzene Sec-Butylbenzene 14-Dichlorobenzene 1,2-Dichlorobemene Total Xylenes 1-Propylbenzene N-Propylbenzene 1,3-Dichlorobenzene Dibrovuchloromethane Dichlorodifluorometlune Chloromedume Vinyl Chloride Bromomethane Chloroethane Trichlorofluc romethane I,I-Dichloroethene Methylene Chloride Tmns-1,2-Dichloroethene Cis-1,2-Dichloroethene Bromodichloromethane Bromochloromethane Cis-1,3-Dichloropropene Tmms-1,3-Dichloropropene Methyl-Tert-Butyl ether (MTBE) Isopropyl ether(IPE) Dilution Factor Sample Number Sample Date Sample Time (hrs) Analyzed Date Analyzed Time (hrs) Analyst BQL = Below Quantitation Limits -- = Not Available iPPb? (aobl (oobl (o0b) (lipb) (uub) (nob) ippb) n 0 e i I 1 I I I I 1 605735 605736 605737 605738 605739 605740 605741 12/11/07 12/11/07 12/11/07^ 12/11/07 12/11/07 12/11/07 12/11/07 12/19/07 12/19/07 12/19/07 12/19/07 12/19/07 12/19/07 12/19/07 1442 1511 1540 1608 1637 1706 1735 NM NM NM NM NM NM NM ppb = pansperbillion SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Clearly or Type Facility Name:_ Permit Name (if Facility Addres 14mo n\CAd Ft a q ,AA fq . rt n O s""°° W C 734 2 tcnrl Is ml tziol County = c we l l Contact Person:— �� lam14 Telephone#: WelLLocation/ Site Name: SP°ree xn, Ff Oea't No: of Wells to be Sampled:_{ ev.mq Well IdentificationNumber(fromPermit): 1V110—)3 For Groundwater Treatment Systems Well Depth: /• D it. Well Djia�meter: 2 in. Check One: ❑ Influent (98) Screened Interval: �" ft. to-��— It. ❑ Effluent (99) Depth to Water Level: ft. below measuring point. Measuring Point (M.P.) is:_24- ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before,sampling: Z Date sample collected: /2-11•-n 7 Field analysis: pH 6 Specific Conductance ' uMhos Temp. °C, Odor Appearance PERMIT#: W Non -Discharge NPDES DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER EXPIRATION DATE: .5 -26r1 YMMED OPERATION BEING -MONITORED Lagoon _Remedialion: Infiltration Gallery Spray Field _Remediation: Rotary Distributor _Land Application of Sludge Other: NOTE; Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: SEE G%[ ll'o Laboratory Name: U) a Ter N ct, Certification No. ,S75 (Samples for metals were collected unfiltered ✓ YES _NO and field acidified COD mg/I Nitrite-(NO2) as N mg/1 Coliform: MF Fecal /loom] Nitrate (NO3) as N mg/1 Coliform: MF Total /100ml Phosphorus: Total as P a• 11 12-11�d mg/1 (Note: Use MPH method for highly t amples) Orthophosphate mg/1 Dissolved Solids: Total l -11'z mg/I A(=Aluminum <'0•050 12-11-07 mg/I pH (when analyzed.) -N-c units Ba - Barium 0.256 12-11.6r7 mg/f TOC D ' -r1 mg/I Ca - Calcium Ll4 , L I2 1ra'> mg/1 Chloride mg Cadmium±��a / -n a mg/I Arsenic 4o•oo5 /�-nd7 mg/I Chromium: Total raj%oo'sl �R', -ro o7 mg/I Grease and Oils mg/1 Cu - Copper - mg/1 Phenol mg/I Fe - Iron �A wu mg/I Sulfate /211ai mg/I Hg- Mercdrpr�� mg/I Specific Conductance uMhos K - Potassium i'q% ocesnin_ •.. mg/1 Total Ammonia mg/1 Mg - Magnesium - - `L ii'o7 mg/I TKN as N mg/I Mn - Manganese Z //"e mg/I It _YES ! NO) Ni - Nickel 4' e•dos 12-IH7 mg/1- Pb - Lead <o.oe /2-/1-07 m I Zn - Zinc mg/I Ammonia Nitrogen mg/1 Other (Specify Compounds and Concentration Units) ffe/em),vM eo,00,Spl"n J7-/1-07 S'ar/:f,m 1-124, eh' ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes ✓1) No _ (0) VOC : method # = ,b 21D D yl-- CY r method # = method 1i = Gw-59 Signature of Pormillee (or AWH dzed Agent - (Date) Rev. 03/2000 cr n Iveww uem v Parameter l,l-Dichloroetlive 2,2-DieWoropropane Chloroform 1, 1, 1-Trieldomethane I,1-Dichloropropene Carbon Tetmcbloride Benzene 1,2-Dichloroethane Trichloroethene 1,2-Dichloropropane Dibromornethane Toluene 1,12-Trichloroeduvte 1,3-Dichloropropane Tetrachloroethene 1,1, 1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane 1,2,3-Trichloropropane H"achlorobutadiene Bromobenzene Ethylbenzene Styrene Bromofurm ' p-lsoprppyltoluepe N-Butylbenzene Naphthalene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene 1,2,4-Trichlorobenzene 1r,3-Trichlorobemene Chlorobenzene 2-Chlorotoluene 4-Chlomtolume Tert-Butylbenzene Sec-Butylbenzene 1,4-Dichlorebenzene 1,2-Dichlorobenzene Total Xylenes I-Propylbemene N-Propylbenzene 1,3-Dichlorobenzene Dibromochloromethane Dichlorodifluoronethane Chloromethane Vinyl Chloride Bro rnmethane Chloroethane Trichlorofluorumethane I,I-Dichlomethene Methylene Chloride Turns-1,2-Diddoroethene Cis-1,2-Dichloroethene Bromodichlommethane Bromochlommethane Cis-1,3-Dichloropropene Trans-1,3-Dichloropropene Methyl-Tert-Butyl ether (MTBE) Isopropyl ether (IPE) Dilution Factor Sample Number Sample Date Sample Time (hrs) Analyzed Date Analyzed Time (hrs) Analyst BQL = Below Quantitation Limits Not Available LLfalt fppbl L-r� bilb) fnmbl frmb) fnpbl (oob) Ombj i I 605735 I 605736 I 605737 I 605738 I 605739 1 605740 1 605741 12/ 11 /07 12/ l 1 /07 12/ 11 /07 12/ 1 1 /07 12/ I 1 /07 12111 /07 12/ 1 1 /07 12/19/07 12/19/07 12/19/07 12/19/07 12/19/07 12/19/07 12/19/07 1442 1511 1540 1608 1637 1706 1735 NM NM NM NM NM NM NM ppb = partsperbillion SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or`Type Facility Name: <o A is 1. c ^ C W" Permit Name (if different): Facility Address: 171—r11,14ti 7� 1,VwK _ yh A is n. 's"Ro"q �St']SZ County /Yl s' CWeI itac — ii, L i Rios 2 ConlactPerson: �� t�� �1r`- Telephonefl: -& 41/1 WelhLocation/ Site Name:'iu;re GY/uCw' No, of Wells to be Sampled: I eT map Well'Identification Number (from Permit): M Q- 12 For Groundwater Treatment Systems Well Depth: It.. Well Di meter: 2- in. Check One: ❑ Influent (98) Screened Interval: ft. to rr'± ft. ❑Effluent (99) Depth to Water Level: q ft. below measuring point. Measuring Point (M.P.) is:z ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/b iled before sampling: a Date sample collected: 2-11-o Field analysis: pHW • Specific Conductance ' uMhos Temp. _9 OC, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMITS: Id6'CC05403 EXPIRATIONDATE: 6-2011 Non -Discharge UIC TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon _RemediAtion: Infiltration Gallery Spray Field _Remedialion: Rotary Distributor—LandApplication of Sludge Other. NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: SEt he ylo a.) Laboratory Name: Ldg4e., Pr h Certification No. $-O PARAMETERS (Samples for metals were collected unfiltered '' YES _NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P 0,32 12.11•0'1 mg/1 (Note: Use MPN method for highly.turbid samples) Orthophosphate mg/I ` Dissolved Solids: Total 260 12-1ho mg/I AI ='Aluminum e 0.0s•o 12-/1r67 mg/I pH (when analyzed) m12 12-0-07units Ba - Barium o'- 6(03 12.11.67 mg/I _ TOC 1,53 12-11-o7 mg/I Ca - Calcium 21.'D . Chloride 2q /2-02�7 mg/I Cd - Cadmium / 0, aoz 12-u-67mg/l. Arsenic - - 0.605 12-N-4 mg/I Chromium: Total Lo•00 u-rr07mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate 53 ,7(b. .qf'% � 2.jjIF - �mg/I Hg - Mercury mg/I Specific Conductance "'ilfvlhoS K - Potassium mg/I Total Ammonia . 14hl ! 9 2ffl mg/I Mg - Magnesium / �-/-o mg/I TKN as N mg/I Mn - Manganese - mg/I ,. InfoFinafion Processing Unit f GW-59 r Rev.0312000 _YES NO)' Nf - Nickel 0 ,005 /2-i/-o7 mg/I Pb - Lead- t 0. O09 / 7-/i•o'7 mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) e/e,r-rurn �o,or,s-ppm i�_ii-o7 ORGANICS: (GC,GC/MS,HPLC) (Specify test and method If. Attach lab report.) Report Attached? Yes._! (1) No _ (0) VOC : method N = 621D Q : method N = : method H = C i Parameter (n)b) I,I-Dichloroethane 0.5 2,2-Dichloropmpane 0.5 Chloroform 0.5 I,1,1-Trichloroethane 0.5 1,1-Dichloropropene 0.5 Carbon Tetrachloride 0.5 Benzene 0.5 1,2-Dichloroethane 0.5 Trichloroethene' 0.5 I,2-Dichloropropane 0.5 Dibromomethane 0.5 Toluene 1,1,2-Trichloroethane 0.5 0.5 1,3-Dichloropropane 0.5 Teunchloroethene 0.5 I,I,I,2-Tetrachloroethane 0.5 1, 1,2,2-Tetrachloroctlme 0.5 1,2,3-Trichloropmpam 0.5 Henchlombutadiene 0.5 Bromobenzene 0.5 Ethylbenzene 0.5 Styrene 0.5 Brommform 0.5 p-Isopropyltoluene 0.5 N-Butylbemene 0.5 Naphthalene 0.5 0,5-Trimethylbenzene 0.5 1,2,4-Trimethylbenzene 0.5 1,2,4-Trichlorobemene 0.5 1,2,3-Trichlorobenzene 0.5 Chlorobenzene 0.5 2-Chlorotolume 0.5 4-Chlomtoluene 0.5 Tert-Butylbenzene 0.5 Sec-Butylbenzene 0.5 1,4-Dichlorobenzene 0.5 1,2-Dichlorobenzene 0.5 Total Xylenes 0.5 I-Propylbenzene 0.5 N-Propylbenzene 0.5 I,3-Dichlorobenzene 0.5 Dibromochlommethane 0.5 DichlorodiBuoromethane 0.5 Chloromethane 0.5 Vinyl Chloride 0.5 Bromorrethane 0.5 Chloroethzne 0.5 TrieldoroBuoromethane 0.5 1,1-Dichloroethene 0.5 Methylene Chloride 0.5 Tans-1,2-Dichloroethene 0.5 Cis-1,2-Dichlorocthenc 0.5 Bromodichloromethane 0.5 Bromochloromethane 0.5 Cis-1,3-Dichloropropene 0.5 Tans-1,3-Dichloropropene 0.5 Methyl-Tert-Butyl ether(MTBE) 5.0 Isopropyl ether (IPE) 5.0 Dilution Factor Sample Number Sample Date Sample Time (hrs) Analyzed Date Analyzed Time (hrs) Analyst BQL = Below Quantimtion Limits -- = Not Available (npb) (ppb) (pub) (orb) (npb) ipmb) (pobl I I 1 I I 1 1 605735 605736 605737 605738 605739 605740 605741 12/11/07 IVI 1/07 12/11/07 12/11/07 12/11/07 12/11/07 12/11/07 12/19/07 12/19/07 12/19/07 12/19/07 12/19/07 12/19/07 12/19/07 1442 1511 1540 1608 1637 1706 1735 NM NM NM NM NM NM NM ppb = pans per billion ' SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY IN M ON [� Please Print Clearly or Type Facility Name: O P 3 ��I m p y; c p Permit Name (if different): Facility Address: .- 0 \ V_ 'TY) A D v(-, �"'°`0 n, c z8�g'Z� M S (Jo.w't i- (City)i e,et County Contact Person: Telephonelk SZS %S6 f)II) Well Location/ Site Name: at Fr h 8ti No. of Wells to be Sampled:I WelfldentificationNumber (from Permit): Rlv-// ForGroundwaterTreatmentSystems Well Depth: f3 ft. Well Diameter. -in. Check One: ❑ Influent (913) x Screened Interval: !L . % ft. to L&M ft. El Effluent {99) Depth to Water Level: ft. below measuring point. Measuring Point (M.P.) is:a-'% ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 2 Date sample collected: /2 1•0 Field analysis: pH � .9 7 Specific Conductance uMhos' Temp. -4L-_°C, Odor Appearance PARAMETERS (Samples for metals were collected u _ COD mg/1 Coliform: MF Fecal /100m1 Coliform: MF Total /100m1 (Note: Use MPN method for highly turbid samples) ` Dissolved Solids: Total 344 12.11. mg/I pH (when anal zed) 4.95 IIII-qunits TOC '.71 11-0-o•7 mg/I Chloride 915' 12-A-a`7 mg/I 655 Arsenic 4-0,0 - rz-ff•v7 mg/1 Grease and Oils mg/I Phenol mg/I Sulfate 14b �+fy/1 Specific Conductance t)Iv11iS?s Total Ammonia mg/I TKN as N 7f1(}E}g/I Rev. 03/2000 DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER DUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT#:Oe0",4703 EXPIRATION DATE: .720// Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING -MONITORED Lag= _Remediation: Infiltration Gallery Spray Field _Remediation: Rotary Distributor _ Land Application of Sludge NOTE• Values should reflect dissoived and . colloidal concentrations. Date sample analyzed: � F E A e l I h w Laboratory Name: _. W A- Q G -T'12 c br Certification No. , 0 YES _NO and field acidified Nitrite (NO2) as N mg/1 Nitrate (NO3) as N mg/I Phosphorus: Total as P 6.15 /z rf a7 mg/I, Orthophosphate mg/I At -'Aluminum Zv uSio /2-u-67 mg/I Ba - Barium 0 43(a` n-/I-67 mg/I Ca - Calcium 1'&21 / 2-//-a7 mg/I Cd- Cadmium �c•r;oz /2-u•a7 mg/I Chromium: Total 0, ob 8 /2-//•d 7 mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg -Magnesium S,4/ /2 -_47mg/I Mn - Manganese // d7 mg/I _YES NO) Ni - Nickel ! 6,006' /2-//ti7 mg/I Pb - Lead -eO. oo 5 r 2-/1-47 mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) Soli u to in ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes f (1) No _(0) VOC method # = G 2 /D,d method # = ,t. RESEARCh & ANALyTOCAt LABORATORIES, INC. Analytical/Process Consultations Chemical Analysis for Selected Parameters and Water Sample Identified as Coats American (A Water Tech Labs, Inc. Project, collected 11 December 20 I. Volatile Organics Quantitation MW2 MW10 MWII MW12 MW13 MW14 MWIS EPA Method 6210 D Limit Parameter (opbl (ppb) (oob) (pob) (pnb) (opbl iP� (Dnb) 41-Dichloroethane 0.5 BQL BQL BQL BQL BQL BQL BQL 2,2-Dichloropropane 0.5 'BQL BQL BQL BQL. BQL BQL BQL Chloroform 0.5 _' BQL BQL BQL BQL BQL BQL BQL I,I,I-Tdchloroethme 0.5 BQL BQL BQL BQL BQL BQL BQL l,l-Dichloropropene 0.5 BQL BQL BQL BQL BQL BQL BQL Carbon Tetrachloride 0.5 BQL BQL BQL BQL BQL BQL BQL Benzene 0.5 BQL BQL - BQL BQL BQL BQL BQL 1,2-Dichlomethane 0.5 BQL BQL BQL BQL BQL BQL BQL Trichloroethene 0.5 BQL BQL BQL BQL BQL BQL BQL 1,2-Dichloropr6pane 0.5 BQL BQL BQL BQL BQL BQL BQL Dibromernethane 0.5 BQL BQL BQL BQL BQL BQL BQL Toluene 0.5 BQL BQL BQL BQL BQL BQL BQL 1,1,2-Trichloroethane 0.5 BQL BQL BQL BQL BQL BQL BQL 1,3-Dichloropr6pane 0.5 BQL BQL BQL BQL BQL BQL BQL Tetmchlorocthene 0.5 BQL BQL BQL BQL BQL BQL BQL 1,1,1,2-Tetrachloroethane 0.5 -BQL BQL BQL BQL BQL BQL. BQL I,I,2,2-TetracNoroethane , 0.5 BQL . BQL BQL BQL BQL BQL BQL 111,3-Trichloropmpane 0.5 BQL BQL BQL BQL BQL BQL BQL Hexachlorobutadiene 0.5 BQL BQL BQL BQL BQL BQL BQL Bromobenzene 0.5 BQL BQL BQL BQL SQL BQL BQL Ethylbemene 0.5 BQL BQL BQL BQL BQL BQL BQL Styrene 0.5 BQL BQL BQL BQL BQL BQL BQL Bromoform 0.5 BQL BQL BQL BQL BQL BQL BQL p-Isopropyltoluene 0.5 BQL BQL BQL r BQL BQL BQL BQL N-Butylbenzene 0.5 BQL BQL BQL BQL BQL BQL BQL Naphthalene 0.5 BQL BQL BQL BQL BQL BQL BQL 1,3,5-Trimedylbenzene 0.5 BQL BQL BQL BQL BQL BQL BQL 1,2,4-Trimethylbenzene 0.5 BQL BQL BQL BQL BQL BQL BQL 1,2,4.Tricblorobemene 0.5 BQL BQL BQL BQL BQL BQL BQL lA3-Trlchlombenzene 0.5 BQL BQL BQL BQL BQL BQL BQL Chlorobenzene 0.5 BQL BQL BQL BQL BQL BQL BQL 2-Chlorotoluene 0.5 BQL BQL BQL BQL BQL BQL BQL 4-Chlorotoluene 0.5 BQL BQL BQL BQL BQL BQL BQL Ten-Butylbenzene 0.5 BQL BQL BQL BQL BQL BQL BQL Sec-Butylbenzene 0.5 BQL . BQL BQL BQL BQL BQL BQL 1,4-Dichlorobenzene 0.5 BQL BQL BQL BQL BQL BQL BQL 1,2-Dichlorobemene 0.5 BQL BQL BQL BQL BQL BQL BQL Total Xylenes 0.5 BQL. BQL BQL BQL BQL BQL - BQL I-Propylbenzene 0.5 BQL BQL BQL BQL BQL BQL BQL N-Propylbenzene 0.5 BQL BQL BQL BQL BQL BQL BQL LS-Dichlorobenzene 0.5 BQL BQL BQL BQL BQL BQL BQL Dibrormchlaromethane 0.5 BQL BQL BQL BQL BQL BQL BQL Dichlorodi0uoromethane 0.5 ' BQL BQL BQL BQL BQL BQL BQL Chloromethane 0.5 BQL BQL BQL BQL BQL BQL BQL Vinyl Chloride 0.5 BQL BQL BQL BQL BQL BQL BQL Bromomethane 0.5 BQL BQL BQL BQL BQL BQL BQL Chloroethane 0.5 BQL BQL BQL BQL BQL BQL BQL Trichloro0uoromethane 0.5 BQL BQL BQL BQL BQL BQL BQL 1,1-Dichlomethene 0.5 BQL BQL BQL BQL BQL BQL BQL Methylene Chloride 0.5 BQL BQL BQL BQL BQL BQL BQL Trans-1,2-Dichloroethene 0.5 BQL BQL BQL BQL BQL BQL BQL Cis-1,2-Dichloroethene 0.5 BQL BQL BQL BQL BQL BQL BQL Bromodichloromethane 0.5 BQL BQL BQL BQL BQL BQL BQL Bromochloromethane 0.5 BQL BQL BQL BQL BQL BQL BQL Cis-1,3-Dichloropropene 0.5 BQL BQL BQL BQL BQL BQL BQL Trans-1,3-Dichloropropene 0.5 , - BQL BQL BQL BQL BQL BQL BQL Methyl -Ten -Butyl ether(MTBE) 5.0 BQL BQL BQL BQL BQL BQL BQL Isopropyl ether (IPE) 5.0 BQL BQL BQL BQL BQL BQL BQL Dilmion Factor 1 1 I 1 I I 1 Sample Number 605735 605736 605737 605738 605739 605740 605741 Sample Date 12/11/07 12/11/07 12/11/07 12/11/07 12/11/07 12/11/07 12/11/07 Sample Time (hrs) --- - - - -- - -- Analyud Date 12/19/07 12/19/07 12/19/07 12/19/07 12/19/07 12/19/07 12/19/07 Analyzed Time (hrs) 1442 1511 1540 1608 1637 1706 1735 Analyst NM NM NM NM NM NM NM BQL = Below Quanlimtion Limits ppb = pausperbillion -- = Not Available SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: I RT FORM FACILITY INFORMATION 2 i /� Please Print Clearly or Type Facility Name: o t4 5 1�I�e r 1 C >4 ti Permit Name (if different): Facility Address: to 3 a is M e a` c'A 1 UXI Welf;Location/ Site Name: Telephone fl: 829-2S6' No. of Wells to be Sampled: Well lldentificationNumber (from Permit): /Yltd'10 For Groundwater Treatment Systems Well Depth: /-ft. Well Diameter. 2- in. Check One: ❑ Influent (98) Screened Interval:to ti ' it. ❑ Effluent (99) Depth to Water Level: ft. below measuring point. Measuring Point (M.P.) is: 2.3 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/b filed before sampling: � Date sample collected: / 2-//'07 Field analysis: . Specific Conductance —'uMhos Temp. --� _°C, Odor Appearance PARAMETERS (Samples for metals were collected COD mg/I Coliform: MF Fecal A00ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 291-1 )2-11-0-/mg/I pH (when analyzed) 6.92 /a-/Edunits TOC <D. .e -v mg/I Chloride 8• iz-I)-o'y mg/I Arsenic �Q�eS" 12-11-09 mg/I Grease and Oils mg/I Phenol mg/I Sulfate 1 ?b 1 -0•07 mg/I Specific Conductance �r"'�- ulvtp,os °°n�' Total Ammonia l��-.?rn�/I TKN as N mg/I PERMIT ff: W DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER EXPIRATION DATE: Non -Discharge UIC TYPE OF PERMITTED OPERATION BEING MONITORED _Lagoon _Remediation: Infiltration Gallery Spray Field _Remedialion: Rotary Distributor _Land Application of Sludge Other: NOTE, Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: Stt /�e e,c ry Laboratory Name: Gera cr Tee Certification No. SD tered / YES _NO and field acidified Nitrite (NOZ) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P B•/a P-J,1-e7mg/I Orthophosphate mg/I All = Aluminum C 0.050 12-//•07mg/1 Ba - Barium 0•037- j2-//-o7 mg/f Ca - Calcium Lot 12-//•07 mg/I Cd -'Cadmium < 4,06 z 1 z-11-07 mg/l Chromium: Total 40r00 S )2 /I o7 mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg ' Magnesium Dr `l93 12-II•07mg/I Mn - Manganese [a.o©S t;01-47 mg/I _YES ZNO) Ni - Nickel— /-0-6G5E /Z-//-e%mg/I Pb - Lead <Oroo 5- /ai/o7 mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units): 6elPwiorn .GQ.Oo.S 12-/I O% ,9100 gi.2 12.-11-6O 7 ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes✓✓(1) No _ (0) VOC method B = G Z /O �J method # = method f/ = Y Chemical RESEA1iCh & ANA1YTICAL •o°ca6"""i} oivi LABORATORIES INC. �,•'��� lNC#34 Anowical/Process Consultations _ t Selected Parameters and Water Sample ldentifed as Coats American I. Volatile Organics EPA Method 6210 D Parameter l,l-Dichloroethane 2,2-Dichloropropane Chloroform 1,1,1-Trichloroethane 1,1-Dichloropropene Carbon Tetrachloride Benzene 1,2-Dichloroethane Tdchloroethene 1,2-Dichloropropane Dibromomethane Toluene 1, 1,2-Trichloroethane 13-Dichloropropane Tetrachloroethene 1, 1, 1,2-Tetrachloroethane 1, 1,2,2-Tetracbloroethane + 1,2,3-Trichloropropane Nexachlorobutadiene Bromobenzene Ethylbetaene Styrene Brotmform p-Impropyltoluene N-Butylbenzene Naphthalene 1,3,5-Trimethylbenzene 1,2,4-Trlmethylbenzene 12,4-Trichlorobemene 1,2,3-Trichloroben wrte Chlorobenzene 2-Chlorotoluene 4-Chlorotoluene Tert-Butylbenzene Sec-Butylbeazene 1,4-Dichlombenzene 1,2-Dichlorobenzene Total Xylenes 1-Propylbenzene N-Propylbenzene 1,3-Dichlorobenzene Dibromwchloromethane D ichlorodifluoromed+ane Chloromethane Vinyl Chloride Bromonethane Chlomethane Trichlorofluoromethane I,[-Dichloroethene Methylene Chloride Trans-1,2-Dichloroethene Cis1,2-1)ichloroethme Bromodichloromethane Bromochloromethane Cis1,3-Dichloropropene, Trans 1,3-Dichloropropene Methyl -Ten -Butyl ether (RTIBE) Isopropyl ether (IPE) Dilution Factor Sample Number Sample Date Sample Time (hrs) Analyzed Date Analyzed Time (hrs) Analyst BQL = Below Quantitation Limits = Not Available Quantitation Limit (Ppb) 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5, 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 , 0.5 0.5! 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 5.0 5.0 MW2 ( 'MW10' ) MWII MW12 MW13 111IW14 MW15 (Dob) (P41 (r)[3) inabl (PP, (P�) (12pbj 1 I 1 1 1 1 I 605735 605736 605737 605738 605739 605740 605741 12/11/07 12/11/07 12/11/07 12/11/07 12/11/07 12/11/07 12/11/07 12/19/07 12/19/07 12/19/07 12/19/07 12/19/07 12/19/07 12/19/07 1442 1511 1540 1608 1637 1706 1735 NM NM NM NM NM NM NM ppb = partsperbillion 0 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Permit Name (if Please Print Clearly or Type w .rrirv.•)a_ 11,% �..(ziCounty 117- UD LUC1( Contact Person:- 1 ti'� (LIP i�w. Mw Telephone #: 9 2q-'15b Welf.Location/ Site Name:- SEVlYP / ]9 5 h o1Ld- No. of Wells to be Sampled: I e,em Pe,mle WelllldentificationNumber (from Permit): W)a1-2 For Groundwater Treatment Systems Well Depth: 'J .S' ft. Well Diameter.. _(0 in. Check One: ❑ Influent (98) Screened Interval: �/.r ft. to f"1& ft. Depth to Water Level: 2 1 ft. below measuring point. Effluent (99) Measuring Point (M.P.) is: 7,3 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: �c Dale sample collected: 12-11-e 7 Field analysis: pH (7,01 , Specific Conductance ' uMhos_ Temp. _/L_°C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT#: 0490065603 EXPIRATION DATE: S- 2o1J Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED 1� Lagoon _Remedialion: Infiltration Gallery Spray Field ' _Remediation: Rotary Distributor _Land Application of Sludge Other: NOTE: Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: s'iF %e.1Gc-0 Laboratory Name: CdAFeP JecA Certification No. Sb PARAMETERS (Samples for metals were collected unfiltered_Z�_YES _NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /10om1 Nitrate (NO3) as N mg/1 Coliform: MF Total - /100ml Phosphorus: Total as P o.la /z /1 07 mall (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 315 /2-0-7 m /I pH (when analyzed) 7.o/ i7-r/�7unitts TOC -1 -d mg/I Chloride R,o 12-//'0 mg/I Arsenic <0'00s l2-11-07 mg/I Grease and Oils mg/I Phenol mg/I Sulfate 7rb9 Jz-/ro7 mg/I Specific Conductance t•= f N dt FrOMhos — °®IITg/I Total Ammonia TKN as N fp N t !R ')nn , mg/I Orthophosphate mg/I A[ -:Aluminum t0.05e3 /2-//-&7 mg/I Ba - Barium 0.0 `12. J 2-0,j 7 mg/f Ca - Calcium 2' 6 / / 2-11.07 mg/l Cd - Cadmium -40.001 /z-/1.07 mg/I Chromium:Tota1_co.00S /z-/1.07mg/I Cu --Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium AD % /2-1/-L7 mg/I Mn - Manganese - - D 7o J z -a-j7 mg/I _YES / NO) Ni - Nickel 46.00.5- /7-//-07 mg/l Pb - Lead <D•005S / -11-67 mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) Edee.iotn ' D.dd5 rpm >z-/1-Di � Dot: Vrn S%O.D flnpm 12�//-d ORGANICS: (GC,GC/MS,HPLC) (Specify test and method ff. Attach lab report.) Report Attached? Yes � (1) No _ (0) VOC : method N = (n 2 /17 /) : method 0 = method N = Rev. 0312000 n aaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaa r z m mmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmm mmmmmmmmmmmmmmmmmmmm ��, a aaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaa z mmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmm � _, a _ aaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaa rn m ^ mmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmm � ? a _ aaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaa � _ �°`� z mmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmm � � a _ aaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaa aaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaa N ^�dn z mmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmm � y a aoo aa.aaaaa.�..�..iaaaaaa.aa.aaaaa.a.aaaa.a.aa(yaa.a.1.lc�acycyclo clacac aaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaa aaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaa N ^�dn z mmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmm � y a aoo aa.aaaaa.�..�..iaaaaaa.aa.aaaaa.a.aaaa.a.aa(yaa.a.1.lc�acycyclo clacac aaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaaa m�mmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmm a O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O.O O O O O O O O O N N C 2e yes E$eg 00€ olu o dog ao�? q'o _off 95oE -riU-�C�m _I-^❑ y SY ��q tlk C C G _oc ToEc�-vE,N aaa s'E Q 2E2`FFFFO-,'Eo�U�X�nU C$ r g m O.Z.I--_mavrn o�smm00^ eEC] E� ,g 6 [{N CLL Ci (JY '?�Y oI w a 41NZ.ju__VNJ'I-V)_.. Z_p❑ 1J' y �sooQOC d S d O e V� p'+0 u o Coo V>mVF�-.��FVm 1 W N d U W L s E o �o Z G d Q1+1 F' T 6 C d ofg mUF�= .G Va Vam6QQ ' { i GW-59ACOMP1,IANCEREPQIZTj'0j;U%2 Permff#0c9aoos(,os (Submit one each monitoring period with GW-59 forms) 7 truer uate monitoring results were due. be, submitted after the established due c any missing on the GW-59 report this IF the answer to question i or 2 k 'YES'; I in the space provided belt explain the problems encountered in obtaining the required information. Are any of the monitorwells in need ofrepair or maintenance (damaged casing, unlocked or missing cap, identification plate, area overgrown, etc.)? If the answer is "Yes-. coitact the Regional Ofce forgr<idairce. any to or YES NO YES NO >er(s) and / missing YES NO, ITS" NO ,, .,,� "„swer ru quesoon 4 is -NO-, skip to section a. If the answer to question 4 is "YES" list the affected wells individually with consiftuent(s) and concentration(s) exceeding standards in the space provided below: - >nw z mru= o.oga /rww-13�iy=7s99 W /77r13 CL- yq/Yl a ly=/5 Tdc_3. rniw•q /,,.�= o.37f /n= is-� nlw-ft) 7A5=52 • ntw=/5 TAS=531 For the constituents identified in question 4 above, have standards been exceeded previously for the same constituent(s) in the same well(s) in the last two years? rr rrr� answer io quesnon o is -NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last. two years). M tw rS c j aC t(- to- 0 7 /974J vY �.i 9/io o7�lz-sc(� Mu/Ir= rpry �/_/D•0Y/ /?-S'Euf SO�tl M u, l3 = MN tl -lo-a'1 / 17.5--" Are If the answer is "YES'; a groundwab OFFICE IMMEDIA TEL Y FOR GUIDAA located; contact the Regional Office. groundwater quality problem it me answer to question 7 is 'TES-, d If the answer to question 7 is 'WO", at or iaury prourem may be occurring. CONTACT THE REGIONAL If the answer is 'NO'; monitoring wells may be improperly approved actions required by the Division space JAN 18 2008 Information Processing Unit DWO/SOG this i ne person completing this portion (GW-59A) or the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I 71Qr nn1 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION /� t Please Print Clearly or Type Facility Name: LoA7s Iravter'ICN✓� Permit Name (If dif(arent . Facility Address:_l6e Isb 1 $ 6 3O me n f�dw 'TA ,L Is ) — tcuri a,o) z County lam- /Jocry e rC Contact Person: ti Well Location/ Site Name: Yeiephone #: 53ZR-'7s - ,io/ 4 gZ6 le� Ac r o. of Wells to be Sampled: _L Well Identification Number (from Per7Diameter. pcmr,mu) Well Depth: `71� tt. Win. For Groundwater Treatment Systems Screened Interval: � ft. to Check One: ❑ Influent (98) Depth to Water Level: ft. below measuring point. El Effluent (99) Measuring Point (M.P.) is: 2— ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/�ailed before sampling: Z Date sample collected: �S 9 Field analysis: pH_ fO.9Y , Specific Conductance uMhos Temp, t'3°C, Odor Appearance PARAMETERS (Samples for metals were collected COD mg/I Calif orm: MF Fecal /100ml Coliform: MF Total " /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 9-0 O mg/I PH (when analyzed) 7 07 (r.?Gunits TOG S'^lSo CO, D mg/I Chloride_ 27-02 2g Mg/1 Arsenic "R-lo-o% 4n eoC mg/I Grease and 011s mg/I Phenol mg/I Sulfate -lo- 0 7 90 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT#:ev(gotDSba3 EXPIRATIO NDATE: S� Non -Discharge UIC NPDES T PE P R ITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field ' Remediation: Rotary Distributor Land Application of Slud!R I Other:_ Z. ___EC NOT • Values should reflect dissolved colloidal concentrations. Date sample analyzed: Laboratory Name: Certification No. YES _NO and field acidified VrQ Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg /I Phosphorus: Total as P t--22:c7 0,07 mg/1 Orthophosphate mg/I AI = Aluminum - ajb-o7 C o. a -To mg/I Ba- Barium '6-/0•060096 Ca - Calcium_ mg/I 4-I6-67 1 1 • mg/I Cd - Cadmium 2-/o-n7 o,002 g Chromium: Total 8-)o-07 46.006 mg /I Cu - Copper m/I Fe - Iron mg/I Hg - Mercury m /I K - Potassium mg/I Mg - Magnesium - 0-0 2 mg 1I Mn - Manganese -18-ti 6,00 m9/I E! N( - Nickel `-16-6 7 m Pb-Lead "2-16-b7Cd,p©S m I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other fsPecify Compounds and Concentration Units) 07 -,59 me/c 5 olpN�vwl x /a 0< D co P41L ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes_(1) No —(a) VOC : method # = method # method # G W-59 Rev. 03/2000 SUBMIT FORM ON YE_ LLOW PAPER ONLY IGROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION___ _ /)_ /� Please Print Clearly or Type Facility Name:_ C O 9,5 { �S /ym P n Permit Name (if different): nJ ISveeq 111 2 P • G O}<t p fi __—lcirl N ¢ 2 LCOUnIy —/2J� dW('!i Contact Persnn•_ �},',L t' n ��yr. W.•t, Iziol Well Location/ Si[e Name: - !�� �> � oN No. of Wells to be Sampled:_ Well Identification Number (from Permit): /7� RJ-/ io-o v.�,�„ WeII Depth: / Q it. Well Diameter: Z in. For Groundwater Treatment Systems Screened Interval: �`/ ft. to ti<� ft Check One: ❑ Influent (98) Depth t0 Water Level: r2./ it. below measuring point. Effluent (99) Measuring Point (M.P.) ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water Pumped/balled before sampling: :3 Date sample collected: Field analysis: pH 2. n/ , Specific Conductance ' UMhcs Temp. _ / c 'C, Odor Appearance PARAMETERS (Samples for metals were collected u COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: use MPN method for highly turbid samples Dissolved Solids: Total 0 8 Ing", PH (when analyzed) 8 0 7,01 units) TOC 4T (as, mg/I Chloride_ 84Z9-oh (% mg/Il Arsenic W-10-07 ' 40.605' mg/I Grease and Oils mg/l Phenol mg/I Sulfate mg/l Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I G W-59 Rev. 03/2000 DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT#: W®e665605 EXPIRATIONDATE: -?o// Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED ,GLagoon-____Remedialion: Infiltration Gallery Spray Field ' _Remediation: Rotary Distributor _Land Application of Sludge Other. __ 9:11/rr, NOTE' Values should reflect dissolved and , • ee "I'llZROIJAL colloidal concentrations. SEP 2 4 2002 Date sample analyzed: Laboratory Name: tz >r — Certification No. S /) Itered_4e'__YES _NO and field acidified Nitrite (NO2) as N mg /I Nitrate (NO3) as N mg/I ii/?9 Phosphorus. Total as P o,o mg/I> —smg/I Orthophosphate Al -'Aluminum _?-la•o7 •Cd•osv m/I g Ba - Barium 9-/D-67 o,vSb m g/I Ca - Calcium_ 10-07 O 7/6d mg/I Cd- Cadmium g-1o•o7 Go•o0z mg/I Chromium: Total R-A-oq t 0.00 mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury m /I K - Potassium mg/I Mg - Magnesium -1 -D '0-D 6.2 g/I Mn - Manganese - Go,o Mg/I !l- —YES _ENO) Ni - Nickel Y /0-07 O• o /1 mg/I Pb-Lead. 2-W-07 C 00£ m I Zn - Zinc mg/I Ammonia Nitrogen mgp Other (Specify Compounds and Concentration Units) So r&*v 'y o !!�mcpIt ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) ReportAttached? YeS_(1) No _ (0) VOC : method # = : method # = : method # = ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) ReportAttached? YeS_(1) No _ (0) VOC : method # = : method # = : method # = SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: INOn-MDip DEPARTMENT OF ENVIRONMENT B NATURAL RESOURCES COMPLIANCE REPORT FORM WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER ACIL I RMAT ON, RALEIGH NC 27699-1636 Phone: 919 733.3221 �Please Prinf Clearly or Type Facility Name_ �t?iS /Y%Y)�Y r A iL ERIT#: W ovo�Gg3 EXPIRATION DATE: -27f!Permit Name (if different): scharge UIC Well Location/ Site Name: Telephone#: `Zi ff-764- No. of Wells to be Sampled: vom rermn7 Well Identification Number (from Permit): �// Well De the / :3 For Groundwater Treatment Systems P ft. Well Diameter:—Z in. Check One: ❑ Influent (98) Screened interval: IV& ft. to "'44 ft. Depth to Water Level: q.2 ft. below measurin Effluent (99) .�� g point. Measuring Point (M.P.) is: ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/balled before sampling: 2 Date sample collected: Field analysis: pH 4S Specific Conductance ' UMhos Temp. /,5 °C, Odor Appearance NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon _Remedialion: Infiltration Gallery Spray Field _Remediation: Rotary Distributor _ Land Application of Sludge Other: NOTE Values should reflect dissolvad an-f)IV. colloidal concentrations. Date sample analyzed: 5Eyc bPIIO a/ SEP 2 4; 2007 Laboratory Name: U e c /, Certification No. S C7 PARAMETERS (Samples for metals were collected unfiltered DYES COD mg/I _NO Nitrite (NO2) as N and field acidified m /I Coliform: MF Fecal Coliform: MF Total /100ml /100ml Nitrate (NO3) as N mg/l Phosphorus: Total as P -29-0`7 O./Smg/I (Note: Use MPH method for highly turbid samples) Dissolved Solids: Total - Orthophosphate mg/I g PH (when analyzed) 7 D z . mg/I units Al -'Aluminum ro-o Ba - Barium -1D •0 lo.g5 mg/I 0 •'7 9 TOC 53- / S or7 / mg/I Ca - Calcium ID-O Cd - Cadmium '8-la o02 mg/I 15, mg/I Chloride R-22- 07 —�50 mg/I Arsenic �- I� 09 46 deLs mg/I Chromium: Total g"/a D7 mg/I Z�,oas mg/I Grease and Oils Phenol mg/I Cu - Copper m /I g Sulfate R- I o- 0 / N7 mg/I mg/1 Fe - Iron Hg - Mercury mg/I mg/I Specific Conductance uMhos K - Potassium m g/I Total Ammonia TKN as N mg/I Mg -Magnesium ' -fo-o $/ /I mg/I Mn - Manganese - e-o �c�6 xmg/I _YES ! NO) Ni - Nickel 8-1D-a7 zo, oaS g/ Pb - Lead 5� /o•07 4e9 nd5, m I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other1(Specify Compounds and Concentration Units) SIIDc�ivrrt -lo-a'-9 //4 ew ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) ReportAttached? Yes --(I) No _ (0) VOC : method # = method # = method # = IGROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMAT[ON n Please Facility Name:_ ( eA4'5 e Permit Name (if diffe,(e0t): SUBMIT FORM ON YELLOW PAPER ONLY or _it i s Lpl' County rh_ U�weC Contact Person• ti-GUP ,1`�'eJ`><nrwn. Telephone #:82£'-75'H-z///! 6✓33C$ Well LocatioN Site Name: SFyi Fr /�FFCvNrt f No. of Wells to be Sampledt Well Identification Number (from Permit): / For Groundwater Treatment Systems Well Depth: / 3 ft. Well Diameter:? in. Screened Interval: //z tL to Check One: ❑ Influent (98) Depth to Water Level: q O ft. below measuring point. Effluent (99) Measuring Point (M.P.) is: 2 It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pump d/bailed before sampling: 2- Date sample collected: R i-07 Field analysis: pH 9 / Specific Conductance uMhos Temp. / 0 C, Odor. Appearance PERMIT #: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER EXPIRATION DATE: Non -Discharge NPDES TYPE OF PERM177ED OPERATION BEING MONITORED —, /Lagoon _,Remedialion: Infiltration Gallery Spray Field ' _Remedialion: Rotary Distributor __Land Application of Sludge NOTE, Values should reflect dissolved and . fRECEIVEE) colloidal concentrations. OI!/.OFWATEPOIJALITY Date sample analyzed: 5si (p/(p yJ SEP 2 4 2007 Laboratory Name: pycr iPrti Certification No. 6-a PARAMETERS (Samples for metals were collected unfiltered YES COD _NO and field acidified Coliform: MF Fecal mg/I /100ml Nitrite (NO2) as N Nitrate (NO3) as N m /I Coliform: MF Total (Note: Use /100ml Phosphorus: Total as P 9-2 .67 0.68 mg/I mg/I MPN method for highly Dissolved Dissolved Solids: Total turbid samples) 67 32 Orthophosphate — g mg/I PH (when analyzed)-'I•o�7 (c• ( units TOC f3-IS-o7 AI = Aluminum. /0-o7 <o s0 Ba -Barium 8-/6D cryR mg/I mg/t 51-22-D y, mg/1 <S a mg/I Ca - Calcium_ 6/D-07 y/,2 Cd - Cadmium- A-io-o7 <000Z mg/1 ArseChlonic Arsenic __ d Otis Grease and Oils �p,o0� mg/I Chromium: Total JYo- d 7 �o,60-mg/I b mg/I Phenol mg/I Cu - Copper, mg/I Sulfate ��/o 07 mg/I $ 4o X mg/I Fe - Iron Hg - Mercury mg/I Specific Conductance Ammonia uMhos mg/I K - Potassium Mg -Magnesium Arlo -o 9 i m /I g/I mmg/I TotalKN N mg/I Mn - Manganese_8 /D-o7 /-5 '7Xmg/I GW-59 Rev. 03/2000 _YES NO) Ni - Nickel {a• o 66- g/ Pb - Lead£?-/0-07 •zp OOS m I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) SB/e r vrn /D 07 C D rio s mfZL ORGANICS: (GC,GC/MS,HPLC) (Specify test and method If. Attach lab report.) ReepCort Attached? Yes_(1) No _ (0) method # = method # = method If = ✓L- SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION/7 Please Prfnt Clearly or Type Facility Name:— It r Permit Name (d different): Facility Address: D fo 3a e� a eif- N,, N ISveei tac rti��o) .z ,nPZ County ��r C)o C C Contact Person:— l7 L , P i ti � � Telephone #: 828-?5'I - yrll ff 336, Well Location/ Site Name: S1,11, u No. of Wells to be Sampled:— Irom Permit) Well Identification Number (from Permit):/hCJ- / Well Depth: /Sri it. WeIlDiameter 2 in For Groundwater Treatment Systems Screened Interval: _ "/r] ft. to Dia Check One: ❑ Influent (98) _—� It' ❑Effluent (99) Depth to Water Level: 7�ft. below measuring point. Measuring Point (M.P.) is: 2•49 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bai ed before sampling: 2 Date sample collected: • Field analysis: P. G- Sf� , Specific Conductance ' uMhos Temp. -C, Odor Appearance PARAMETERS (Samples for metals were collected COD mg/I Coliform: MF Fecal /100m1 Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 4 a7 g/I PH (when analyzed) `T44`1 G 99, units TOC_ 8 r5 c"! 2 '/7 mg/I Chloride `d-22 D7 mg/I Arsenic?-/o-oy �� oaS mg/I Grease and Oils mg/I Phenol mg/I Sulfate-_ /D-07 23' mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I GW-59 Rev. 03/2000 _NO DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: 66SODO S5 00:3 EXPIRATION DATE: S , Non -Discharge UIC NPDES PE F PERMITTED OPERATION BEING MONITORED LagJ oon _Remedialion:Infiltration Gallery Spray Field ' _Remedialion: Rotary Distributor _ Land Application of Sludge NOTE' Values should reflect dissolved and . MC:UrIVtU colloidal concentrations. DIV. OF WATER OUALITY Date sample analyzed: StE`hr'//o iu SEP 2 41 2D07 Laboratory Name: /iJN Ni TPc Certification No. S l� and field acidified Nitrite (NO2) as N mg /1 Nitrate (NO3) as N mg/I Phosphorus: Total as P. (j-29-67 0•N mg/I Orthophosphate mg/I AI -:Aluminum Id o°I 666 mg/I Ba - Barium_ -0'67 o /sY mg/I Ca - Calcium -lD o 29.1 -/D-o mg/I Cd - Cadmium V y 4rj rdOz mg/I Chromium: Total I-10-57 zb.00ur mg/l Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium Vb,t7 5g3 a mg/1 Mn - Manganese L'-/o-o% /• 45 Xmg/I ' / /" _YES NO) Ni - Nickel 8 /o-a7 Z©,60S' mg/I Pb - Leali£t-/o 07 c o.00cs mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) S"oOri ur7J 8-/0`o C/'!`/ilr��/t 1SP/o.vrvpl LU' UQS me/L ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes. —(I) No _ (0) VOC : method # = or C method # = method If = SUBMIT FORM ON YELLOW PAPER ONLY IGROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY R_ _ _A I /] Please Print Clearly or Facility Name:_ r7 /1 /s N rn P ^ c /q ✓L Permit Name (If ddferAnt):_ Well Location/ Site Z�County. elf ✓✓ove[ L tnvl —� Telephone #: e2S1->56''1// No. of Wells to be Sampled: Well Identification Number (from Permit): Well Depth: Z For Groundwater InfTrealuent Systems P ft. Well Diameter:_ in. Check One: ❑ Influent Screened Interval; �'• � ft. to �ti/R- f(, (98) Depth to Water Level: �ft. below measuring point. Effluent (99) Measuring Point (M.P.) is: & ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped ailed before sampling: /-, Date sample collected: Field analysis: pH , Specific Conductance ' UMhos Temp. /b °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: �✓ `� °0 °� U EXPIRATION DATE. Non -Discharge UIC NPDES TYPE OF PFgMITTED OPERATION BEING MONITORED T LLagooh _Remediation: Infiltration Gallery Spray Field _Remedialion: Rotary Distributor Land Application of Sludge NOTE: Values should reflect disscived and . colloidal concentrations. Date sample analyzed: ,J/ i E- bell '� e/ Laboratory Name: __ W I e r iPC Certification No. .S l) PARAMETER$ (Samples for metals were collected unfiltered IYES and field acidified COD COliform: MF Fecal mg/1 /100ml _NO Nitrite (NO2) as N Nitrate (NO3) as N m /I Coliform: MF Total /100ml Phosphorus: Total as P f Zy °7 d/ mg/I mg/I (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 5-9•b 7 7/X �_ Orthophosphate mg/1 g E mg/I PH (when analyzed) 4 9•°7 /v7,i_units T At =Aluminum 8'/� �r1 Co oso Ba - Barium 8 /n'07 ®•/y mg/I TOC 15-07 Chloride1 2Z D > 5` 72 mg/1 Ca - Calcium $ /° D7 /D/ m / g Arsenic �1-1 D D0 7 r - mg/I 4 p mg/1 Cd - Cadmium_ R-ro-o 4ho02 Chromium: Total. S'/d-D7 < a.605 mg/1 9 mg/1 Grease and Oils Phenol mg/I Cu - Copper m /I rg-Io-D Sulfamg/1 q 1 mg/I Fe - Iron Hg - Mercury mg/1 mg/I Specific Conductance uMhos K - Potassium g Total Ammonia TKN as N mg/1 Mg - Magnesium �'-/o d" % ,2 m /I mg/I Mn - Manganese -/o'd7 6413 pg/I 9 _YES - NO) Ni - Nickel vo v 7 40oo,5- g/I Pb - Lead_8-/19 _o <o•od mg/1 Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) Sod;, to g-/o 0 / 0 P G SP/w.f v100 '?-/0-0 CO o /Ir4 ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes._(1) No _ (0) VOC : method If : method # _ method # = GW-59 Rev. 0312000 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATIO ',, // //�� Please Print Clearly or Type Facility Name:- �© 4).5 /4 2 r )'- e r"1- Permit Name (If differgrtt): v ri,� Telephone #:BZ� 75/o-yG Well Location/ Site Name: /7 oti No. of Wells to be Sampled: Well Identification Number (from P:Wel ): Well Depth: /a tI.l D'ameter _Z Screened Interval: !9 ft. ° f(• Depth to Water Level —it, below measuring point. Measuring Point (M.P.) is: 3 ft. above land surface. Gallons of water pumped/balled before sampling: Field analysis: pH _Le �Z , Specific Conductance Temp. /'-j °C, Odor A PARAMETERS (Samples for metals. were collected COD mg/I Coliform: MF Fecal Coliform: MF Total /100m1 /100m1 (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total $`9'd% 4/SZ mg/I PH (when analyzed) L-7.0.7 6132 units TOC8-/S-o� 32yK mg/I Chloride S 2z•y`7 Arsenic-la-o`7 S• D mg/I o•oo15- mg/I Grease and Oils Phenol mg/I mg/I Sulfate `lD'a 7 l o m /I Specific Conductance Total Ammonia TKN as N uMhos mg/I mg/I I For Groundwater Treatment Systems in. Check One: ❑ Influent (98) ❑ Effluent (99) Relative M.P. Elevation in ft.: Date sample collected: S- uMhos ooearance DEPARTMENT OF ENVIRONMENT $ NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: G/ d o'fd 0 /v06 EXPIRATION DATE: Non -Discharge UIC TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon _Remediation: Infiltration Gallery Spray Field ' _Remediation: Rotary Distributor _Land Application of Sludge other. NOTE Values should raflact dissolved and colloidal concentrations. Date sample analyzed: r_ E Gel h) rU Laboratory Name: Lri 0 -e + ec A Certification No. b�l YES _NO and field acidified Nitrite (NO2) as N mg /I Nitrate (NO3) as N m/I Phosphorus: Total as P z4 o7 b mg/I Orthophosphate mg/l A1= Aluminum- R-Id-o% <o oso m /I Ba- Barium 8 (D-D? O-/9� mg/I Ca - CalciumR- D-Y7 /oZ mg/I Cd -Cadmium -/0-a r7 002 mg/I Chromium: Total 07 �.o mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg -Magnesium $-I o-vr7 t2.Y mg/I Mn - Manganese_ 2'-/o-07 2.3 mg/I 'GL _YES �-- NO) Ni - Nickel- C6'60,5- mg/I Pb - Lead _ S-/D-o7 G 6.0 0 mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (specify Compounds and Concentration Units) Ser om S-/D O(o 'q b4m G SPlwrL7um •/D�pO CD•/,aS��L ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes_(1) No _ (0) VOC : method # = method # = method # = GW-59 Rev. 0312000 u W-59A COMPLIANCE REPORT FORM Perm (Snbnnit one each monitoring period wljli G1i-59 jo m mlt # G✓ 0 D p5 �o D 3 0 b-- --• -- —mw: mg resuits were due.( 1 Will this monitoring report (GW-59 and GW.59A) YES NO e;submitted after the established due date? Was any required information missing on the GW-59 report forms? 1/ IF the answer to question 1 or 2 is "YES'; list in the space provided below the weft identif cation numbers) and YES N0 explain the problems encountered in obtaining the required information. t/ 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? ythe answer is -yes ' contact the I Regional OJ�ce jot guidance, 4 Are any monitored constituents equal to crab-.- the estahifeh-- ------ , It the answer to question 4 is NO'; skip to section 8. YES NO If the answer to question 4 is 'TES" list the affected wells individually with constituents) and concentration(s) Y exceeding standards in the space provided below: rn�-f3 iAs=sue/ jYilV/2 ry7A2yrltipser /,ri% MN�'Artrye=/./r7 if9/rl-/S 70(f= 32-y S d%sY12 8 y /Yll1 / / T/ 5 - S-'7/ //�N = 7.3 V For the constituents identified in question 4 ab-.-, ve standards been exceeded reviou5l for the same constituent(s) in the same well(s) in the last two years? p y YES NO if the answer to quest/on 5 is NO , skip to section 8. /f the answer to question 5 is `TES", list in the space provided below, each well with constituents) exceeding standards, concentration(s) reported, and sample collection date for each occurrence if the last two years). Are the monitoring wells listed in section 5located at or it me answer is "YES" a ring. CONTACT THE REGIONA! groundwater quality problem maybe occur OFFICE IMMEDIATELY FOR GUIDANCE. ff the answer is `NO`; ccurtorfng wefts may be improperly located; contact the Regional Office. groundwater quality problem? -- '-:-r....`� �`""""' requirea oy the Division involving this YES NO if the answer to question 7 is 'YES describe those actions rn the space provided below. If the answer to question 7is `NO", contact the Rentnnnt nrr._ ...:.�._ fines. and/oraenaltfes The person completing this portion (Gw-59AJ of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current rw_so s . G1V`I59A 12/8/2003 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM r H%.14,1I r INLVHMA I I N �n Please Print Clearly or Type Facility Name: ('. 01� >L5 An ee rO AN Permit Name (it different) - Facility Address: - I'C Id, oy 3 (a 56 n o ,fxne or cN 'nrertc/ R m4ri0ti Isv .q I -AY' � :t �/Urc Z87St County- /X% Oowe t Contact Person: Telephone #: 8 2&'- io -Ili Well Location/ Site Name: S1=v; r:r J69c J! 6"O"tj No. of Wells to be Sampled: Well Identification Number (from Permit): MU-2- Well Depth: ' %S ft. Well Diameter: /O Screened Interval: /"/n It. to ^'/A ft. Depth to Water Level:._ ft. below measuring point. Measuring Point (M.P.) is:2-3_ It. above land surface. Gallons of water pumped/bailed before sampling: S-3 Field analysis: pH 2S Specific Conductance Temp. 13.9 °C, Odor. A PARAMET_ ERS (Samples for metals were collected COD mg/1 Coliform: MF Fecal Coliform: MF Total 1100ml /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 12-2-or< //� mg/1 pH (when analyzed) 12-5--e& 7.25 units TOC_ 1-11-oq 7 mg/1 Chloride /2-22-etc Arsenic /2•/9-66 S 6•mg/l Zo,oto mg/I Grease and Oils Phenol mg/I Sulfate __ /Z- �� g/ 7 2D mg/I Specific Conductance Total Ammonia TKN as N. uMhos mg/l mg/I For Groundwaler Treatment Systems in. Check One:❑ Influent (98) ElEffluent (99) Relative M.P. Elevation in ft.: Date sample collected: 2-3- eG uMhos ooearancA DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER FLHMIT It: EXPIRATION DATE: , 2n// Non -Discharge 100eooSG63 UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remedia(lon: Inliltration Gallery Spray Field Rotary Distributor Other: Remediation: Land Application of Sludge NOTE: Values should reflect dissolved an(yIw'� Ce- colloidal concentrations. JAN 200-/ Date sample analyzed: S r f 1c� F to U-) Laboratory Name: L ATEr Tec )_ 4 (� Certification No. 5(3 YES _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/l Phosphorus: Total as P /2-21-e6 1n.z2 mg/I Orthophosphate mg/I AI - Aluminum_ 12-/9-66 1-6•1L0 mg/l Ba -Barium... / z-19a4 o.o,s 1 mg/1 Ca - Calcium 12-19•06 /y9 mg/l Cd - Cadmium 12-19-vG eo.002. mg/I Chromium: Total /2-19'-4 40.0/6 mg/I Cu - Copper m9/l Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium /2-19-4 7,Q m9 /I Mn -Manganese. /2-/9-o6 ze,o 1a mg/I certfy that to the best of my knowledne and ballot ihn I f .t M w FEB 21 M7 GW-59 Rev. 03/2000 /1L ;1'i'I ' ( :. 0":k:. _.YES NO) Ni - Nickel /2-/9-4 Pb - Lean /2-/9•06 GD•O/o mg/l to, oos mg/l Zn - Zinc mg/I Ammonia Nitrogen mg/l Other (Specify Compounds and Concentration Units) _SQL v/ uv✓�1z /5w6 o 01 nq�L Ski -/Y aG R VC) rh ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) ROC Report Attached? Yes ✓(1) No ._ (0) method # = (0 2/0Q method it = �"�' opc SUBMIT FORM ON -YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Permit Name (if 1L_ Well Location/ Site Name: Please Print Clearly or Type e -,'C )4 r ' .3 ma.icr4a .,eo?r 28TS2 Count (zip)y 0Telephone #: b"?S/ 9f6 /I//, 0 No. of Wells to be Sampled:., Well Identification Number (from Permit): - I94/- /d Well Depth: /ft. Well Diameter: 2- Screened Interval: It. to N//><A ft. Depth to Water Level: 1. 7 it. below measuring point. Measuring Point (M.P.) is: 2, 3 It. above land surface. Gallons of water ed/b ' d before sampling: _,r Field analysis: H o 3 Specific Conductance Temp. S 'C, Odor A For Groundwater Treatment Systems in. Check One: ❑ Influent (9li) ❑ Effluent (99) Relative M.P. Elevation in ft.: Date sample collected: 12-S -o G uMhos ooearanre PARAMETERS (Samples for metals were collected unit COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid sa es Dissolved Solids: Total ZZ -o mg/I pH (when analyzed) /z- -e& t!3 units TOC__ /-Y-07 9 mg/1 Chloride / 2- 22 -e e 9.3 mg/1 Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate /Z-V-oS 7y mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/l DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT#:. EXPIRATION DATE: -Zo// Non -Discharge 'V606e, /o 03 UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED — Lagoon _Remediallon: Infiltration Gallery Spray Field ' _Remediation: Rotary Distributor _Land Application of Sludge Other: NOTE: Values should reflect dissolved and 'DI colloidal concentrations. Date sample analyzed: SSE Ze. le, /v JAN 24 2911 Laboratory Name: L_).4e r 7-rr L i9 Certification No. ,S-O tered_kYES _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P /2-21-64, r7,03 mg/I Orthophosphate mg/I At -'Aluminum /2-/9-o(F 4-0,100 mg/I Ba - Barium /2-/9.0 6 0.01/7 mg/1 Ca - Calcium /2-/,9ro6 6-.78 mg/I Cd- Cadmium 12-Of' Lo.00? mg/1 Chromium: Total /2-/9•o4, e-lo,e/o mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/1 K - Potassium mg/I Mg - Magnesium /2 /9 2.82 mg/I Mn- Manganese, ,cd 610 mg/I _YES NO) Ni - Nickel !2-/9•0 ¢ L0,0/0 mg/I Pb - Lear) ! 2 ig-a6 OQT m I Zn - Zinc mg I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) SN/en , rn /2-19'-04 L D.0/O /7-19-06 / 8 ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes'! (1) No _ (0) VOC : method # = G 2 / 0-1) method # = method # = 7 GROUNDWATER QUALITY MONITORING: COMPLIAN( FACILITY INFORN Facility Name: — Permit Name (if diff Facility Addregs:_ yy/ Ari D� Contact Person:— Well Location/ Site I RT SUBMIT FORM ON YELLOW PAPER ONLY — / Please Prin( Clearly or Type Telephone #: 9zP 7SG 5a �� No. of Wells to be Sampled: Well Identification Number (from Permit): M4) For GroundwaterTrealmenlSystems Well Depth: 13 ft. Well Diameter: in. Check One: ❑ Influent (9B) Screened Interval: /A ft. to ^' /9- ft. Effluent (99) Depth to Water Level:- 9 f�„ ft. below measuring point. Measuring Point (M.P.) fs: 6 ft. above land surface. Relative M,P. Elevation in ft.: Gallons of water pumped/bailed before sampling: / Dale sample collected: /2 Field analysis: pH s!E , Specific Conductance Temp. /1125 'C, Odor ' Appearance . uMhos DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: EXPIRATION DATE: _, -- 2 0// Non -Discharge 6)0onos-6a3 UIC NPDES PEPERMITTED OPERATION BEING MONITORED Lagoon _Remediation:Infiltration Gallery Spray Field _ Remediation: Rotary Distributor _ Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: cSez &I b o IV.O� \IVATSR QUAW Laboratory Name: 4JF�er T C,P Certification No. .57,61. PARAMETERS (Samples for metals were collected unfiltered ✓YES _NO and field acidified COD mg/I /100ml Nitrite (NO2) as N Nitrate (NO3) as N mg/I mg/I Coliform: MF Fecal Coliform: MF Total /100ml Phosphorus: Total as P /0-11-o6 0.07 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total z-a o mg/I At - Aluminum /2-/9' ,n6 46,roa mg/I pH (when analyzed) /2 s=o.¢ units Ba - Barium [ 2-19 0/r 0 179 mg/1- TOO. /-y-o 7 mg/I Ca - Calcium_ /2-/9-06 9,35 mg/I Chloride /2--ez-00 cro mg/I Cd- Cadmium 1'2V9-0�, L("CcZmg/I Arsenic /z-/a-cF co,ela rng/I Chromium: Total/2-/9-06 0,0/a mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate /2-9-0� '72 0 mg/I Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/l Mg - Magnesium /2-19- 04, mg/I TKN as N mg/I Mn - Manganese- /2-r9-o6 (25,126 )mg/I _YES ✓ NO) Ni - Nickel /2-/9-06 40,0/ a mg/I Pb - Lead / 2-/9-ep Z0.00s mg/( Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) -56 ,iUjrr /2-/9-66 e- o 01 =SDdi C /2-/9-oG / i 3 Mo/L ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. tach lab report.) Report Attached? Yeses/ (1) No _ (0) VOC : method ft= 62/01 : method # = : method if = GW-59c Rev.03/2000 s "" '�1"` g ) / (Date) �yii4 mrnn mace orn ma edA enl SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Permit Name (if Facility Address: J11Anro, Well Location/ Site Name: Please Print Clearly or Type 75 tf /rr p r i c 4 rt- County. /77 - Uo we / t Telephone #: 82!;! %S ,-W// ry. 5)368 No. of Wells to be Sampled:I . Well Identification Number (from Permit): _1>7 W-12- For Groundwater Treatment Systems Well Depth: 1 3 it. Well Diameter.. Z in. Check One: ❑ Influent (98) Screened Interval: ^"6M- ft. to '-/H it. ❑ Effluent (99) Depth to Water Level: 9 ft. below measuring point. Measuring Point (M.P.) is:-?-,�— ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: Z Date sample collected: /2 5 0 Field analysis: PH La � , Specific Conductance ' uMhos Temp. 1?,q °C,Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: EXPIRATION DATE: .S - Oo 1 / Non -Discharge w&000J603 UIC NPDES— TYPE PF PERMITTED OPERATION BEING MONITORED Lagoon _Remedialion: Infiltration Gallery Spray Field ' Remedialion: Rotary Distributor _ _ Land Application of Sludge Other: NOTE; Values should reflect dissolved and . RECEIVED colloidal concentrations. DIV.t)FWATER OUALIT) Date sample analyzed: - rE hf /o uJ �A� 2 4 2��� Laboratory Name: &)ig y / e&?='02 (� Certification No. L5- PARAMETERS (Samples for metals were collected unfiltered AYES _NO and field ai:idified COD mg/I /loom[ Nitrite (NO2) as N Nitrate (NO3) as N mg /I mg/I Coliform: MF Fecal Coliform: MF Total /loom[ Phosphorus: Total as P 12-21-06 0•13 m/I (Note: Use MPN method for highly turbid samples) Orthophosphate - mg/I Dissolved Solids: Total 1-2-- 06 . C mg/I - AI =Aluminum_ /z-t9-oc -o, tao mg/I g PH analyzed) fy oqD c nits Ba - Barium 1 2-19-04 ©.07 mg/I TC/When O mg/I 36 Ca -Calcium /2-/7-0 6 mg/I Chloride /2-22-c6 _ Arsenic 12-19-06 mgA 'C' 010 mg/I Cd- Cadmium Chromium: Total _ /2-/7-o(, 12-(?-o6 40.002 < o.o I p mg/I mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol Sulfate /Z -8 0� mg/I /<•2 mg/I Fe - Iron Hg -Mercury m p g mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium / z, /C-c� %•21 m /I TKN as N mg/I Mn - Manganese 12 -/ -d • /3 m9g/I _YES ENO) Ni - Nickel_ !z-/y-od Za• 6/0 mg/I Pb - Lear[ /n-/9-6 6 L O.80S mg/1 Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) 1 'r- 1E/Li e M 6 L(91 0/6 o , trr✓, 12-/9-06 -yry' / ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. A tach lab report.) ReeportAttached? Yes V(1) No_(0) C method # =_ (Z/O `117 ✓d/!- method # = method # = GW-59 Rev. 03/Z000 SUBMIT FORM ON YELLOW PAPER ONLY _YES ' ' NO) Ni - Nickel_ /2-/9-66 L6.0/0 mg/I Pb - Lean /2-/9-el, 0.0015, mg/I Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) SE! n 6;,n l/2-/4ok 4(9,61 L ORGANICS: (GC,GC/MS,HPLC) (Specify test and method If. Attach lab report.) Report Attached? Yes l/(1) No _ (0) VOC : method # = 62/01) GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: Permit Name (if differe Well Location/ Site Name: Print Clearly or Type JS /7fYIPr, zCounty /9P9o&)e_1L Telephone it: L2ft-76-4i9d P9336 E" No. of Wells to be Sampled:..-/ _ Well identification Number (from Permit): Info-/3 For Groundwater Treatment Systems Well Depth: / S ft. Well Diameter:_2- in. Check One: ❑ Influent (98) Screened Interval:——ft. to ^'//q it. ❑ Effluent 99 Depth to Water Level: - Y j ft. below measuring point. ( ) Measuring Point (M.P.) is: 2_4 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/balled before sampling: / Date sample collected: /2-S-e4 Field analysis: pH T 9 V , Specific Conductance ' uMhos Temp. 621 °C, Odor Appearance PERMIT #: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER EXPIRATION Non -Discharge GuB0006603 UIC TYPE OF PERMITTED OPERATION BEING MONITORED •Lagoon _Remediation: infiltration Gallery Spray Field ' _Remediation: Rotary Distributor _ Land Application of Sludge Other. NOTE7 Values should reflect dissolved anlv colloidal concentrations. Date sample analyzed: C�� (jrley JAN 9 4 2007 wg 1 Laboratory Name: 1 T_f �� 6:4 Certification No. 15-6 PARAMETERS (Samples for metals were collected unfiltered / YES _NO and field acidified COD mg/I Coliform: MF Fecal /100m1 Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total /2-R-ob Sky mg/1 pH (when analyzed) 2-. -0 units TOCt l-y-cr7 .•a mg/1 Chloride /2-22-ob q6 mg/1 Arsenic /2-r9-a y <e.o/D mg/I Grease and Oils mg/I Phenol g Sulfate /2-s3'o6 `16,7 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/1 Phosphorus: Total as P /2-21-06 o,oS mg/I Orthophosphate mg/I At -'Aluminum /2-/9 ed 46,1OP mg/I Ba - Bariumy2-19 Flo 6.660 mg/I Ca - Calcium /2-/9-66 2/•5 /I mg/I Cd - Cadmium /2-/P-66 002 mg/I Chromium: Total /2-/9-96 4,nzlp mg/I Cu - Copper mg/I Fe - Iron mg/l Hg - Mercury mg/I K - Potassium mg/1 Mg - Magnesium /2-/9-OC l `1 9 mg/I Mn - Manganese /2-/9 otc 1. 625) mg/1 7 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION n/% Facility Name:- `0AL5 h Permit Name (if different),. rel Well Location/ Site Name: Please Print Clearly or Type C'I°iCAzZ 10 = County /n //ocue t (zip) Telephone If: 6P29-9S-G -C/l No. of Wells to be Sampled: Well Identification Number (from Permit): /i1GrJ-/ / For Groundwater Treatment Systems Well Depth: / ft. Well Diameter.. 2 in. Check One: ❑ Influent (98) Screened Interval: /N ft. to 11-/4 ft. ❑ Effluent (99) Depth to Water Level: (0• 7 ft. below measuring point. Measuring Point (M.P.) is:2, 6 It. above.land surface. Relative M.P. Elevation Gallons of water pump d/b iled before sampling: 2. s Date sample collected: ' 2�— Field analysis: pH 2A Specific Conductance ' uMhos Temp. /9.3 °C, Odor Appearance DEPARTMENT OF ENVIRONMENT $ NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT#: EXPIRATION DATE: S zd)/ Non -Discharge W606OS663 UIC NPDES TYPE OF PERMITTED OPERATION BEING -MONITORED Lagoon _ Remedialion: Infiltration Gallery Spray Feld ' _ Remedialion: Rotary Distributor _Land Application of Sludge Other. NOTEA Values should reflact dissolved and colloidal concentrations. ��O 'Y Date sample analyzed: S£cr F /c 0��' OFkfgA'ER �li[a1�1 LaboratoryName i Ixm 2 A NG Certification No. SC7 ", PARAMETERS (Samples for metals were collected unfiltered f-YES ' _NO and field acidified COD mg/I Coliform: MF Fecal /100m1 Coliform: MF Total I/100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total. /2 S rk ZZ mg/I pH (when analyzed) /2-S-,D6 Inits TOC /-S a '7 mg/I Chloride 2-2•z-o6 LS'd mg/I Arsenic 12-f9-6b L0,610 mg/I Grease and Oils mg/I Phenol mgp Sulfate /2 R 0 6 9 6S1 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P_ /2 21'dk 0-0' mg/I Orthophosphate mg/I A[ -'Aluminum /2-19-ob 6,lob mg/I Ba - Barium f 2-19 • D b 0,136 mg/I Ca - Calcium 12-17-0 GS-/ mg/I Cd- Cadmium fz 14 06 LO>oo2 mg/I Chromium: Total I2-19-6 b <(5,010 mg/1 Cu - Copper mg/1 Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg -Magnesium mg/I Mn-Manganese 12-M-0(v ,7 6 )mg/I _YES ✓ NO) Ni - Nickel /2-/9-06 40.016 mg/I Pb - Lead /z-/9-06 Zd'rIDS mg/I Zn - Zinc mg/1 Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) Sod) O m 2 /9 O/o 7/• 9 m� ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) ReportAttached? Yes t-'(1) No (0) VOC : method # = 6 Z/D method # = .method If = RESEARCh & ANAIYIFiCA[ LABORATORIES INC. Analytical/Process Consultations Chemical Andlysis for Selected Parameters and Water Sample Identified as Coats American (A Water Tech Labs, In Pro�ectr collected 05 December 2006) I. Volatile Organics Quantitation MW2 MW10 MWII MW12 MW13 MW14 EPA Method 6210 D Limit Parameter (oob) (nob) (nob) (mob) (oob) fpobl obi 1,1-Dichloroethane 0.5 BQL BQL BQL BQL BQL BQL 2,2-Dichloropropane 0.5 BQL BQL BQL BQL. BQL Chloroform 0.5 8.00' BQL BQL BQL BQL BQL I,1,1-Trichloroeth=e 0.5 BQL BQL BQL BQL BQL I,1-Dichloropropene 0.5 J - BQL BQL BQL BQL BQL BQL Carbon Tetrachloride 0.5 BQL BQL BQL BQL BQL BQL Benzene 0.5 BQL BQL BQL BQL BQL BQL 1,2-Dichloroethane 0.5 BQL BQL BQL BQL BQL BQL Trichloroethene 0.5 BQL BQL BQL BQL BQL BQL I,2-Dichloropropane 0.5 BQL BQL BQL BQL BQL BQL Dibronomethane 0.5 BQL BQL BQL BQL BQL BQL Toluene 0.5 BQL BQL • BQL BQL BQL BQL 1,1,2-Trichloroethane 0.3 BQL BQL BQL BQL BQL BQL 1,3-Dichloropropane 0.5 BQL BQL BQL BQL BQL BQL Tetmchloroethene 0.5 BQL BQL BQL BQL BQL BQL 1,1,1,2-Tetiachloroetbane 0.5 BQL BQL BQL BQL BQL BQL l,lr_-Tetmchloroeth=e 0.5 BQL BQL BQL BQL BQL BQL 1,2,3-Trichloropropane 0.5 BQL BQL BQL BQL BQL BQL Hezachiambutadiene 0.5 BQL BQL BQL BQL BQL BQL Brormbe=ene 0.5 BQL BQL BQL BQL BQL BQL Ethylbenzene - 0.5 BQL BQL BQL BQL BQL BQL Styrene 0.5 BQL BQL BQL BQL BQL BQL Bromoform 0.5 BQL BQL BQL BQL BQL BQL p-Impropyltoluene 0.5 BQL BQL BQL BQL. BQL BQL N-Butylbenzene 0.5 BQL BQL BQL BQL BQL BQL Naphthalene 0.5 BQL BQL BQL BQL ` BQL BQL 1,3,5-Tnmethylbemene 0.5 BQL BQL BQL BQL BQL BQL 1,2,4Trimethylbe=ene 0.5 BQL BQL BQL BQL BQL BQL 1,2,4-Trichlorobe=ene 0.5 BQL BQL BQL BQL BQL BQL 1,Y3-Trichlorobemene 0.5 BQL BQL BQL BQL BQL BQL Chlorobemene 0.5 BQL BQL BQL BQL BQL BQL 2-Chlorotoluene 0.5 BQL BQL BQL BQL BQL BQL 4Lhlorotoluene 0.5 BQL BQL BQL BQL BQL BQL Tert-Butylbemene 0.5 BQL BQL BQL BQL BQL BQL Sec-Butylbemene 0.5 BQL BQL BQL BQL BQL BQL 14-Dichlorobemene 0.5 BQL BQL BQL BQL BQL BQL 1,2-Dichlorobemene 0.5 BQL BQL BQL BQL BQL BQL Total Xylenes 0.5 BQL BQL BQL BQL BQL BQL I-Propylbe=ene 0.5 BQL BQL BQL BQL BQL BQL N-Propylbemene 0.5 BQL BQL BQL BQL BQL BQL 1,3-Dichlorobemene 0.5 BQL BQL BQL BQL BQL BQL Dibromochloromethane 0.5 BQL BQL BQL BQL BQL BQL DicWoradifluoromethane 0.5 BQL BQL BQL BQL BQL BQL Chlorornethane - 0.5 BQL BQL BQL BQL BQL I BQL Vinyl Chloride 0.5 BQL BQL BQL BQL BQL BQL Bromomethane 0.5 BQL BQL BQL BQL BQL BQL Chloroethane 0.5 BQL BQL BQL BQL BQL BQL Trichlorofluaromethane 0.5 BQL BQL BQL BQL BQL BQL 1,1-Dichlaroethene 0.5 BQL BQL BQL BQL BQL BQL Methylene Chloride 0.5 BQL BQL BQL BQL BQL BQL Trans-1,2-13ichloroethene 0.5 BQL BQL BQL BQL BQL BQL Cis-1,2-Dichloroetheae 0.5 BQL BQL BQL BQL BQL BQL Brormdichloromethane 0.5 BQL BQL BQL BQL BQL BQL Bromochloromethane 0.5 BQL BQL BQL BQL BQL BQL Cis-1,3-Dichloropropene 0.5 BQL BQL BQL BQL BQL BQL TraL,1,3-Dichloropropene 0.5 BQL BQL BQL BQL BQL BQL Methyl-Tert-Butyl ether(MTBE) 5.0 BQL BQL BQL BQL BQL BQL Isopropyl ether (IPE) 5.0 BQL BQL BQL BQL BQL BQL Dilution Factor 1 I - 1 1 1 I Sample Number 577796 577797 577798 577799 577800 577801 Sample Date 12/05/06 12/05/06 12/05/06 12/05/06 12/05/06 12/05/06 Sample Time (hrs) 0700 0730 0800 0830 0900 0930 Analyzed Date 12I9106 12/19/06 12/19/06 12/19/06 12/19/06 12/19/06 Analyzed Time (hrs) 1419 1451 1522 1554 1625 1657 Analyst NM NM NM NM NM NM BQL = Below Quantitation Limits Fab = partsperbillion - = Not Available ' RESEARCtJ & ANA1Y-FiCA1 L.AbORATORIES, INC. Analytical/Process Consultations Chemical Analysis for Selected Parameters and Water (A Water Tech Labs, Inc. Project, collected 05 Decemb, I. Volatile Organics Quantitation MW2 EPA Method 6210 D Limit Parameter - (nnb) (oob) Identified as Coats American MW10 MW11 1PPbi (m)b) MW12 MW13 Irk fnp6) MW14 bkbl 1,1-Dichloroethane 0.5 BQL BQL BQL BQL BQL BQL 2,2-Dichloropropane 0.5 BQL BQL BQL BQL BQL Chloroform 0.5 8.00' BQL BQL BQL BQL BQL 1,1,1-Trichlomethane 0.5 BQL BQL BQL BQL - BQL 1,1-Dichlompropene 0.5 BQL BQL BQL BQL BQL BQL Carbon Tetrachloride OS BQL BQL BQL BQL BQL BQL Benzene 0.5 BQL BQL BQL BQL BQL BQL 1,2-Dichloroethane 0.5 ' BQL BQL BQL BQL BQL BQL Trichloroethene - 0.5 BQL., BQL BQL BQL BQL BQL ir-Dichlorepropane, 0.5 BQL BQL BQL BQL BQL BQL Dibromarrethane 0.5 BQL BQL BQL BQL BQL BQL Toluene 0.5 BQC BQL BQL BQL BQL BQL 1, 1,2.Trichloroethane 0.5 BQL BQL BQL BQL BQL BQL I,3-Dichloropropme 0.5 BQL BQL BQL BQL BQL BQL Tenachloreetbeae 0.5 _ BQL BQL BQL BQL BQL BQL l,l,lr-Teunchloroedune 0.5 BQL BQL BQL BQL BQL BQL 1,1.2_-Tetrachloroedme 0.5 BQL BQL BQL BQL BQL BQL 1 _,3-Trlchloropropane 0.5 BQL BQL BQL BQL - BQL BQL Hexacltlorobutadiene 0.5 BQL BQL BQL BQL BQL BQL Brormbcmene 0.5 BQL BQL BQL BQL BQL - BQL Ethylbemene 0.5 BQL BQL BQL BQL BQL BQL Styrene 0.5 BQL BQL BQL BQL BQL BQL Bromoform 0.5 BQL BQL BQL BQL BQL BQL p-Impropyltoluene 0.5 BQL BQL BQL BQL BQL BQL N-Butylbeazene OS BQL BQL BQL BQL . BQL BQL Naphthalene - 0.5 BQL BQL BQL BQL BQL BQL 1,3,5-Tnmerhylbemene 0.5 BQL BQL BQL BQL BQL BQL 1,2,4-Trirrethylbeazene 0.5 BQL BQL BQL BQL BQL BQL 1,2,4-Trichlombemene 0.5 BQL BQL BQL BQL BQL BQL 1,2,3-Trichlorobenzem: 0.5 BQL BQL BQL BQL BQL BQL Chlorobenzenc 0.5 BQL BQL BQL BQL BQL BQL 2-Cblomtoluene 0.5 BQL BQL BQL BQL BQL BQL 4Lhloretoluene 0.5 BQL BQL BQL BQL BQL BQL Tert-Butylbenzene 0.5 BQL BQL BQL BQL BQL BQL Sec-Butylbemene 0.5 BQL BQL BQL BQL • BQL BQL 1,4-Dichlorobemene OS BQL BQL BQL BQL BQL BQL I _-Dichlorobemene 0.5 BQL BQL BQL BQL BQL BQL Total Xylenes 0.5 BQL BQL BQL BQL BQL BQL 1-Propylbemene 0.5 BQL- BQL BQL BQL BQL BQL N-Propylbemene 0.5 BQL BQL BQL BQL BQL BQL 1,3-Dichlorobenzene 0.5 BQL BQL BQL BQL BQL BQL Dibromocldoromethane 0.5 BQL BQL BQL BQL BQL BQL Dichlerudifluoromethane 0.5 BQL BQL BQL BQL BQL BQL Chlorometbane 0.5 BQL BQL BQL BQL BQL BQL Vinyl Chloride 0.5 BQL BQL BQL BQL BQL BQL Brotromethane 0.5 BQL BQL BQL BQL BQL BQL Chloroethane 0.5 BQL BQL BQL BQL BQL - BQL Trichlorotluoromethane 0.5 BQL BQL BQL BQL BQL BQL LI-Dichloroethene 0.5 BQL EQL BQL BQL BQL BQL Methylene Chloride 0.5 BQL BQL BQL BQL BQL BQL Tm 1,2-Dichloroethene 0.5 BQL BQL BQL BQL BQL BQL Cis-I,2-Dichlorocthene 0.5 BQL BQL BQL BQL BQL BQL Brormdichloromedume 0.5 BQL BQL BQL BQL BQL BQL Bromochloronethane - 0.5 BQL BQL BQL BQL BQL BQL Cis-1,3-Dichloropropene 0.5 BQL BQL BQL BQL BQL BQL Tm 1,3-Dicldoropropene 0.5 BQL BQL BQL BQL BQL BQL Methyl-Tert-Butyl ether(MTBE) 5.0 BQL BQL BQL BQL BQL BQL Isopropyl ether(IPE) 5.0 BQL BQL BQL BQL BQL BQL Dilution Factor 1 1- 1 1 1 I Sample Number 577796 577797 577798 577799 577800 577801 Sample Date 12/05/06 12/05/06 12/05/06 12/05/06 12/05/06 12/05/06 Sample Time (hrs) 0700 0730 0800 0830 0900 0930 Analyzed Date 12/19/06 12/19/06 12/19/06 12/19/06 12/19/06 12/19/06 Analyzed Time (hrs) 1419 1451 1522 1554 1625 1657 Analyst NM NM NM NM NM NM BQL = Below Quantitation Limits ppb = parts per billion - = Not Available RESEARCh & ANAly-FiCAI a LAboRATORIES, INC. Analytical/Process Consultations Chemical Analysis for Selected Parameters and Water (A Water Tech Labs, Inc. Project, collected 05 Decemb, as Coats American I. Volatile Organics . Quantitation MW2 MW10 MWll MW12 MW13 MW14 EPA Method 6210 D Limit Parameter JUb) (oob) (oob) frmb) (oob) (oob) (ppb) 1,1-Dichlomethane 0.5 BQL BQL BQL BQL BQL BQL 2r-Dichloropropme 0.5 BQL BQL BQL BQL BQL Chloroform 0.5 9.00• BQL BQL BQL BQL BQL 1,1,1-Trichlaroedme 0.5 BQL BQL BQL BQL BQL 1,1-Dichloropropene OS J • BQL BQL BQL BQL BQL BQL Carbon Tetrachloride 0.5 BQL BQL BQL BQL BQL BQL Benzene 0.5 BQL BQL BQL BQL BQL BQL 1,2-Dichloroethane 0.5 BQL BQL BQL BQL _ BQL BQL Trichloroethene 0.5 BQL BQL BQL BQL BQL BQL 1,2-Dichloropropane 0.5 BQL BQL BQL BQL BQL BQL Dibromcmethane 0.5 BQL BQL BQL BQL BQL BQL Toluene 0.5 BQL BQL BQL BQL BQL BQL 1,Ir•Trichloroethane 0.5 BQL BQL BQL BQL BQL BQL 1,3-Dichlompropme 0.5 BQL BQL BQL BQL BQL BQL Tetmchloroethene OS BQL BQL BQL BQL BQL - BQL I, I,lyTenchloroethme 0.5 BQL BQL BQL BQL BQL BQL I, 1 rr•Tetrachloroethme 0.5 BQL BQL BQL BQL BQL BQL 1 _,3-Trlchloropropme 0.5, BQL BQL BQL BQL BQL BQL Hexacblorobumdiene 0.5 BQL BQL BQL BQL BQL BQL Bromobenzece - 0.5 BQL BQL BQL BQL BQL - BQL Ethylbemene 0.5 BQL _ BQL BQL BQL BQL BQL Styrene 0.5 BQL BQL BQL BQL BQL BQL Bromoform 0.5 BQL BQL BQL BQL BQL BQL p-lsopropyltoluene 0.5 BQL BQL BQL BQL BQL BQL N-Burylbenzene OS BQL BQL BQL BQL BQL Naphthalene 0.5 BQL BQL BQL BQL ,BQL BQL BQL 1,3,5-Trimethylbenzene 0.5 BQL BQL BQL BQL BQL BQL 1,2,4-Trimethylbermene 0.5 BQL BQL BQL BQL BQL BQL l _,4-Trlchlorobenzeae 0.3 BQL BQL BQL BQL BQL BQL 1,2,3-Trichlorobenzene 0.5 BQL BQL BQL BQL BQL BQL Chlorobenzene 0.5 BQL BQL BQL BQL BQL BQL 2-Chlorotoluene 0.5 BQL BQL BQL BQL BQL BQL 4-Chlorotoluene 0.5 BQL BQL BQL BQL BQL BQL Tert-Butylber¢ene 0.5 BQL BQL BQL BQL BQL BQL Sec-Butylbeazene 0.5 BQL BQL BQL BQL BQL BQL IA-Dichloroberame 0.5 BQL BQL BQL BQL BQL BQL 1,2-Dichlorobenzene 0.5 BQL BQL BQL BQL BQL BQL Total Xyleoes " 0.5 BQL BQL BQL BQL BQL BQL I-Propylbenzene - 0.5 ' BQL BQL BQL BQL BQL BQL N•Propylbenzene 0.5 BQL BQL BQL BQL BQL BQL 1,3-Dichlorobenzene 0.5 BQL BQL BQL BQL BQL BQL Dibromochloromethane 0.5 BQL BQL BQL BQL BQL BQL Dichlorodifluorometbane 0.5 BQL BQL BQL BQL BQL BQL Chloromethane 0.5 BQL BQL BQL BQL "BQL BQL Vinyl Chloride 0.5 BQL BQL BQL BQL BQL BQL Brorromethme 0.5 BQL BQL BQL BQL BQL BQL Chloroeduane OS BQL BQL BQL BQL BQL - BQL Tdchlorotluaromethme 0.5 BQL BQL BQL' BQL BQL BQL l,l-Dichloroethene, 0.5 BQL BQL BQL BQL BQL BQL Methylene Chloride 0.5 BQL BQL BQL BQL BQL BQL Tans-1-•Dichloroethene 0.5 BQL BQL BQL BQL BQL BQL Cis-1,2-Dichloroetheae 0.5 BQL BQL BQL BQL BQL BQL Bromodichloromethane 0.5 BQL BQL BQL BQL BQL BQL Bronochloromethme 0.5 BQL BQL BQL BQL BQL BQL Cis-1,3-Dichloropropene 0.5 BQL BQL BQL BQL BQL BQL Trms•I,3-Dichloropropene 0.5 BQL BQL BQL BQL BQL BQL Methyl-Tert-Butyl ether(IvIBE) 5.0 BQL BQL BQL BQL BQL BQL Isapmpyl ether (IPE) 5.0 BQL - ' BQL BQL BQL BQL BQL Dilution Factor I I -. I I I I Sample Number 577796 577797 577798 577799 577800 577801 Sample Date 12/05/06 12/05/06 12/05/06 12/05/06 12/05/06 12/05/06 Sample Time (hrs) 0700 0730 0800 0830 0900 0930 Analyzed Date 12/19/06 12/19/06 12/19/06 12/19/06 12/19/06 12/19/06 Analyzed Time (hrs) 1419 1451 1522 - 1554 1625 1657 Analyst NM NM NM NM NM NM BQL = Below Quantitation Limits ppb = pamper billion - = Not Available RESEARCH & ANAIyT1CAI LAboFtA--ORIESo INC. +t Analytical/Process Consultations Chemical Analysis for Selected Parameters and Water Sample Identified as Coats American (A Water Tech Labs. Inc. Proiect, collected 05 December 2006) I. Volatile Organics Quantitation MW2 MW10 MWI1 MW12 MW13 MW14 • EPA Method 6210 D Limit Parameter (Drib) (oob) (Dab) (oob) (oob) (oob) (oob) 1,1-Dichloroethane 0.5 BQL BQL BQL BQL BQL BQL 2,2-Dichlompropane 0.5 BQL BQL BQL BQL BQL Chloroform 0.5 8.00' BQL BQL BQL BQL BQL l,l,l-Trichloroethane 0.5 BQL BQL BQL BQL BQL I,1-Dichloropropene 0.5 j BQL BQL BQL BQL BQL BQL Carbon Tetrachloride 0.5 BQL BQL BQL BQL BQL BQL Benzene 0.5 BQL BQL BQL BQL BQL BQL 1,2-Dichloroethaae 0.5 BQL BQL BQL BQL BQL BQL Trichloroethene 0.5 BQL BQL BQL BQL BQL BQL !r-Dichloropropane 0.5 BQL BQL BQL BQL BQL BQL Dibrorrmmethnne OS BQL BQL BQL BQL BQL BQL Toluene 0.5 BQL BQL BQL BQL BQL BQL 1,1r-Trichlomethane 0.5 BQL BQL BQL BQL BQL BQL 1,3-Dicblompropaue 0.5 BQL BQL BQL BQL BQL BQL Tetrachloroethene 0.5 BQL BQL BQL BQL BQL' BQL _1,1,1,2-Tetrachloroethane 0.5 BQL BQL BQL BQL BQL BQL, 1,11_7-Tetrnchlcroedmne 0.5 BQL BQL BQL BQL BQL BQL 1 _,3-Trichloropropme 0.5 BQL BQL BQL BQL BQL BQL Hexachlorobutadiene 0.5 BQL BQL BQL BQL BQL BQL Bromobemene - 0.5 BQL BQL BQL BQL BQL - BQL Ethylbemene 0.5 BQL BQL BQL BQL BQL BQL Styrene 0.5 BQL BQL BQL BQL BQL BQL Bromotonv 0.5 BQL BQL BQL BQL BQL BQL p-Isopropyltoluene 0.5 BQL BQL BQL BQL BQL BQL N-Butylbenzene 0.5 BQL BQL BQL BQL , BQL BQL Naphthalene 0.5 BQL BQL BQL BQL BQL BQL 1,3,5-Trimethylbenzeoe 0.5 BQL BQL BQL BQL BQL BQL 1,2,4-Trimethylbenzene 0.5 BQL BQL BQL BQL- BQL BQL I _,4-Trichlorobenzene 0.5 BQL BQL BQL BQL BQL BQL 1,2,3.Trichlorobemene 0.5 BQL BQL BQL BQL BQL BQL Chlorobemene 0.5 BQL BQL BQL BQL BQL BQL 2-Chlorotoluene 0.5 BQL BQL BQL BQL BQL BQL 4-Chlorotoluene 0.5 BQL BQL BQL BQL BQL BQL Tert-Butylbenzene 0.5 BQL BQL BQL BQL BQL BQL Sec-Butylbemene 0.5 BQL SQL BQL BQL BQL BQL 1,4-Dichlombemene 0.5 BQL BQL BQL BQL BQL BQL 12-Dichlarobemene 0.5 BQL BQL BQL BQL BQL BQL Total Xylenes 0.5 BQL BQL BQL BQL - BQL BQL I-Propylbemene 0.5 ' BQL BQL BQL - BQL BQL BQL N-Propylbemene 0.5 BQL BQL BQL BQL BQL BQL I,3-Dichlorobemene 0.5 BQL BQL BQL BQL BQL BQL Dibromochlaromethane 0.5 BQL BQL BQL BQL BQL BQL Dichloradifluoromethane 0.5 BQL BQL BQL BQL BQL BQL Chloromethane - 0.5 BQL BQL BQL BQL 'BQL BQL Vinyl Chloride 0.5 BQL BQL BQL BQL BQL BQL Bromomethane 0.5 BQL BQL BQL BQL BQL BQL Chloroethane 0.5 BQL BQL BQL BQL BQL - BQL Tdchlorotluoromethaae 0.5 BQL BQL BQL BQL BQL BQL I,]-Dichlaroediene 0.5 BQL BQL BQL BQL BQL BQL Methylene Chloride 0.5 BQL BQL BQL BQL BQL BQL Trans•Ir-Dichloroethene 0.5 BQL BQL BQL BQL BQL BQL Cis-12-Dichloroethene 0.5 BQL BQL BQL BQL BQL BQL Bromodichloromethane 0.5 BQL BQL BQL BQL BQL BQL Bromochloromethane 0.5 BQL BQL BQL BQL BQL BQL Cis-1,3-Dichloropropme 0.5 BQL BQL BQL BQL BQL BQL Trans-I,3-Dichlompropene 0.5 BQL BQL BQL BQL BQL BQL Methyl -Teri -Butyl ether(MTBE) 5.0 BQL BQL BQL BQL BQL BQL Isopropyl ether(IPE) 5.0 BQL BQL BQL BQL BQL BQL Dilution Factor I I - I I I I Sample Number 577796 577797 577798 577799 577800 577801 Sample Date 12/05/06 12/05/06 12/05/06 12/05/06 12/05/06 12/05/06 Sample Time (hrs) 0700 0730 0800 0830 0900 0930 Analyzed Date 12/19/06 12/19/06 12/19/06 12/19/06 12/19/06 12/19/06 Analyzed Time (hrs) 1419 1451 1522 1554 1625 1657 Analyst NM NNI Nlv1 NM NM NM ' BQL = Below Quantitation Liudts ppb = parts perbillion -- = Not Available Parameter (pr)b) 1,1-Dichloroethane 0.5 2,2-Dichloropropane 0.5 Chloroform 0.5 I,1,1-Trichloroethane 0.5 l,l-Dichloropropene 0.5 J Carbon Tetrachloride 0 5 Bemene 0.5 1,2-Dichloroethane 0.5 Trichloroethene 0.5 1 2-Dichloropropme 0.5 Dibrumoacthane 0.5 Toluene 0.5 1.1 r-Trichloroethane 0.5 I,3-Dichloropropane 0.5 Tenachloreethene 0.3 1, 1, 1,2-Tenachloroethane 0.5 1,1.2,2-Tetrachloroethane 0.5 1,2,3-Trlchlompropane 0.5 Hezaci lorobutadiene 0.5 Bromobemeae 0.5 Ethylbenzene 0.5 Styrene 0.5 Brormform 0.5 p-Isopropyholuene 0.5 N-Butylbenzene 0.5 Naphthalene 0.5 1,3,5-Trimethylbemene 0.5 42,4-Trimethylbemene 0.5 Ir,4-Trichlombemene 0.5 42,3-Trichlorobenzene 0.5 Chlombemem 0.5 2-Chlorotoluene 0.5 4-Chlorotoluene 0.5 Tert-Butylbemene 0.5 Sec-Butylbenzene 0.5 1,4-Dichlorobemene 0.5 - 1,2-Dichlerobemene 0.5 Total Xylenes 0.5 I-Propylbemene 0.5 N-Propylbemene 0.5 1,3-Dichlorobemene 0.5 Dibromochloromethane 0.5 Dichlorodifluorotnethane 0.5 Chloromethane 0.5 Vinyl Chloride 0.5 Brormmethane 0.5 Chloroethane 0.5 Trichlorofluotomethane 0.5. I,I-Dichloroethene 0.5 Methylene Chloride 0.5 Trans-1,2-Dichloreethene 05 Cis-1,2-Dichloroethene 0.5 Brormdichloromethane 0.5 Bromochlorornethane 0.5 Cis-1,3-Dichloropropene 0.5 Trans-13-Dichloropropene 0 0.5 Methyl-Tert-Butyl ether (MTBE) Isopropyl ether (IM) .5 5.0 Dilution Factor Sample Number Sample Date - Sample Time (hrs) Analyzed Date Analyzed Time (hrs) Analyst BQL = Below Quantitation Limits - = Not Available (Pp) (m)b) (13pb) (nob) (013b)' (Pob) BQL BQL BQL BQL BQL, BQL BQL BQL BQL BQL BQL 8.00' BQL BQL BQL BQL I BQL BQL BOL RQL BQL BQL BQL I I I I 1 1 577796 577797 577798 577799 577800 577801 12/05/06 12/05/06 12/05/06 12/05/06 12/05/06 12/05/06 0700 0730 0800 0830 0900 0930 12/ 19/06 12/19/06 12J 19106 12/ 19/06 12/ 19/06 12/ 19/06 1419 1451 1522 1554 1625 1657 NM NNI NM NM NM NM ppb = partsperbillion RESEARCh & ANA1Y-riCA1 LAbORATORIESP INC. Analytical/Process Consultations Chemical Analysis for Selected Parameters and Water Sample Identified as Coats American (A Water Tech Labs, Inc. Project, collected 05 December 2006) I. Volatile Organics Quantitation MW2 MW10 NIWll MW32 MW13 MW34 EPA Method 6210 D Limit Parameter (pnb) (omb) fmahl (nmb) (P.P-b) (mob) Ippb) l,l-Dichlomethane 0.5 BQL BQL BQL BQL BQL SQL 2,2-Dichlompropme 0.5 BQL BQL BQL BQL SQL Chloroform 0.5 8.00' BQL BQL BQL BQL BQL I,1,1-Trichloroetbane 0.5 BQL BQL BQL BQL BQL I,1-Dichloropropene 0.5 • BQL BQL BQL BQL BQL BQL Carbon Tetrachloride 0.5 BQL BQL BQL BQL BQL BQL Benzene 0.5 BQL BQL BQL BQL BQL BQL 1,2-Dichloroethane 0.5 BQL BQL BQL BQL BQL BQL Trichloroethene 0.5 BQL BQL BQL BQL BQL BQL l 2-Dicideropropane 0.5 BQL BQL BQL BQL BQL ' BQL Dibrommrethane OS BQL BQL BQL BQL BQL BQL Toluene 0.5 BQL BQL BQL BQL BQL BQL 1, 1,2-Trichloroethane 0.5 BQL; BQL BQL BQL BQL BQL 1,3-Dichloropmpme 0.5 BQL BQL BQL BQL BQL BQL Tenachloroethene OS BQL HQL BQL BQL BQL BQL 1, 1, 1,2-Tetrachloroethin 0.5 BQL BQL BQL BQL BQL BQL I,1,2,2.Tetrachloroethane 0.5 BQL BQL BQL BQL BQL BQL 1,2,3-Tricbloropropme 0.5 BQL BQL BQL BQL BQL BQL Hesachlorobutadiene 0.5' BQL BQL BQL BQL BQL BQL Bromobemene - 0.5 BQL BQL BQL BQL BQL - BQL Etylbenzene 0.5 BQL BQL BQL BQL BQL BQL Styrene 0.5 BQL BQL BQL BQL BQL BQL Bromform 0.5 BQL BQL BQL BQL BQL BQL p4sopropyholuene 0.5 BQL BQL BQL BQL BQL BQL N-Butylbenzene 0.5 BQL BQL BQL BQL -BQL BQL Naphthalene 0.5 BQL BQL, BQL BQL BQL BQL 1,3,5-Trimethylbenzene 0.5 - BQL BQL BQL BQL BQL BQL l _,4-Trimethylbenzene 0.5 BQL BQL BQL BQL BQL BQL Ir,4-Trichlombenzene 0.5 BQL BQL BQL BQL BQL BQL 1,2,3-Trichlorobenzene 0.5 BQL BQL BQL BQL BQL BQL Chlorobenzene 0.5 BQL BQL BQL BQL BQL BQL 2-Chlormtoluene 0.5 BQL BQL BQL BQL BQL BQL 4-Chlorotoluene 0.5 BQL BQL BQL BQL BQL BQL Ter-Butylbenzene 0.5 BQL _ BQL BQL BQL BQL BQL Sec-Butylbenzene 0.5 BQL BQL BQL BQL BQL BQL 1,4-Dichlmmbenzene 0.5 BQL BQL BQL BQL. BQL BQL I2-Dichlombeanne 0.5 BQL BQL BQL BQL ' BQL BQL Total Xylenes 0.5 BQL BQL BQL BQL BQL BQL I-Propylbenzene 0.5 BQL- BQL BQL BQL BQL BQL N-Propylbenzene ' 0.5 , BQL BQL BQL BQL BQL BQL 1,3-Dichlmrobenzene 0.5 BQL BQL BQL BQL. BQL BQL' Dibromoebloromethane 0.5 BQL BQL BQL BQL BQL BQL Dichlorodifluaromethane 0.5 BQL BQL BQL BQL BQL BQL Chloromethane 0.5 BQL BQL BQL BQL BQL BQL Vinyl Chloride 0.5 BQL BQL BQL BQL BQL BQL Bromometbane 0.5 BQL BQL BQL BQL BQL BQL Chloroethane OS BQL BQL BQL BQL BQL - BQL Trichlorofluoromethane 0.5 BQL BQL BQL BQL BQL BQL 1,1-Dichlomethene 0.5 BQL BQL BQL BQL BQL BQL Methylene Chloride 0.5 BQL BQL BQL BQL BQL BQL Trans-1,B-Dichloroethene 0.5 BQL BQL BQL BQL BQL BQL Cis-1,2-Dichloroethene 0.5 BQL BQL BQL BQL BQL BQL Bromodichloromethane 0.5 BQL BQL BQL BQL BQL BQL Bromochloromethane 0.5 BQL BQL BQL BQL BQL BQL Cis-1,3-Dichloropropene 0.5 BQL BQL BQL BQL BQL BQL Trans-1,3-Dichloropropene 0.5 BQL BQL BQL BQL BQL BQL Methyl-Tert-Butyl ether(MTBE) 5.0 BQL BQL BQL BQL BQL BQL Isopropyl ether (IPE) 5.0 BQL BQL BQL BQL BQL BQL Dilution Factor I 11 I 1 I Sample Number 577796 577797 577798 577799 577800 577801 Sample Date 12/05/06 12/05/06 12/05/06 12/05/06 12/05/06 12/05/06 Sample Time (hrs) 0700 0730 0800 0830 0900 0930 Analyzed Date 12/19/06 12/19/06 12/19/06 12/19/06 12/19/06 12/19/06 Analyzed Time (hrs) 1419 1451 1522 1554 1625 1657 Analyst NM NNI KM NM NM NM BQL = Below Quantitation Limits ppb = parts perbillion -- = Not Available GW-59A CO1kM ANCE �pORI T FORPr� '13,it # 'Voe oas 6a3 (Submit one each monitoring perid4l with GW-59 forms) /LeooO yZ y3 -,ter date monitoring results were due. TRR 31 07 Will this monitoring report (GW-59 and GW-59A) YES ple. submitted after the established due date? YES :Was any r39 report forms? re information missing on the GW- F the answer to question i or 2 is YES ;list in the space provided below the well Its- Tificaf 1ion numbers) end 2Xplain the problems encountered in obtaining the required information. the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing "Y'es", the Regional Office jor guidance. AYES NO Y A,re any of contact identification plate, area overgrown, etc.)? if the answer is i e establisd standards? constituents equal to or above thhe YE NO p,re any monitored if the answer to question 4 is "NO ; skip to section 8. "ves" the affected wells individually with constftuent(s) and concentration(s) If the answer to question a is list exceeding standards in the space provided below: // to 2 (�w-2 rnw_ip m i iN4/= //h //ihW/3 /�fdl�� s� $'� 7p5 , os on Ppb C)nLcrpr r Sui6✓i'fL-=37 rr l 4 above, have standards been exceeded previously for the YES NO For the constituents identified in question in the same well(s) in the last two years? rj same constituent(s) If the answer to question 5 is "NO" skip to section 8. exceeding in the sPac a provided eoccurretn etf(for othe tlast two Years). 5 is " ESand sample collection dlist ethos ate forieach If tndards, content 9� . k )�: H-f tAc h E the monitoring wells listed in section 5 located at or beyond the review boundary? YES NC Are 6 a roundwater qualftyproblem be occurring. CONTACT THE REGIONAL is `NEs'; g ,No,,, welts maybe improperly If the answer monitoring OFFICE IMMEDIATELY FOR GUIDANCE. if the answer is located,' contact the Regional Office. actions required by the Division involving this YES Is the permittee implementing previously approved '7 groundwater quality problem? to question 7 is "YES", d conibe those ons in Office within 90 da s/ an evaluation may be act the Retr If the answer oval If the answer to question 71 "NO'; to determine the im act the waste disposal s stem is having a[ The review and como ranee subject the ermittee to a Notice of trolation required boundaries surroundin this facfli . Failure to do so ma fines and/oroenaltles. tom feting this ortion (GW-59A) of the Monitorirtg report shoulc'sign below and submit this P p at the top of the 9 form. �current Thep erson 8 form with G W-59 forms for required wells to the address provided hm n dsnthl's "-? `21 -r/ Agent) r MW2 CHLOROFORM 12/05 4.3ugl 12.04 10 ugl PH 4/05 6.30 MW 10 PH -TDS SULFATE 4/05 6.30 4/04 530 mg/l 8/04 410 mg/l MW 13 PH 8/05 6.40 MW 14 PH 8/05 6.10 GROUNDWATER Q PLIANCE REP Facility Name:_ Permit Name (if Well Location/ Site Name: nEcrzivED ITY MONITORING: - ( 30 fJrn�nT SUBMI'j FORM ON YELLOW PAPER ONLY Print Ofearfy or Type County 41c0e1we 1t Telephone 11:829:211, •iNN Fy 33h8 No. of Wells to be Sampled: /_ Well Identification Number (from Permit): M W -2 For Groundwater Treatment Systems Well Depth: 767 ft. Well Diameter: (o— in. Check One: El Influent (98) Screened Interval: a/A ft. to N A4 it. El Effluent (99) Depth to Water Level: 39 • 3It. below measuring point. Measuring Point (M.P.) is: 0.3 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 3:X Date sample collected: 8 S OG Field analysis: pH 7.G 9 , Specific Conductance uMhos Temp. 1y11 °C, Odor Appearance PERMIT If: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES- I WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER EXPIRATION DATE: ZZ 26 //// Non-Discharge&19e005,003 U NPDES TYPE OF PERMITTED OPERATION BE114G MONITORED Lagoon Remediallon: Infiltration Gallery Spray Field _Remedialion: Rotary Distributor —Land Application of Sludge NOTE: Values should reflect dissolved and . ro09 colloidal concentrations. 0 rn Date sample analyzed: SEE iOE�ouJ LaboratoryName: _Fou%n..nL:b. At Tas Ll• a Certification No. boa PARAMETERS (Samples for metals were collected unfiltered ✓ YES _NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100m1 PhnsnhnnLs• Tnfal as P21/29/e0-ZA.o'm n (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total RM- 81/ m 406g/I pH (when analyzed)//06— 7.69 units TOC_S120oG— /•Bo ✓mg/I Chloride 8��/ei r.6, .1mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate _S jishore — // "�mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Orthophosphate mg/I At - Aluminurn mg/I Ba - Barium mg/I Ca - Calcium 22 fob— / 6'�mg/I Cd - Cadmium mg/I Chromium: Tota( mg/I Cu - Copper mg/I Fe - Iron mg/I Fig - Mercury mg/I K - Potassium mg/I Mg - Magnesium 81221ail, — g•7'mg/I, Mn - Manganese mq/I YES _ NO) Ni - Nickel mg/t Pb - Lead mg/1 Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method ff. Attach lab report.) ReportAttached? Yes._(1) No_(0) VOC method U = method 0 = method It = (;W-Rg (' Y)X K _49 1.. /\-� v� 9-,7-Q6 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM ."Please Print Clearly or Type Facility Name: Cp A -5 IVI e n ) G ja w Permit Name (if different): Facility Address: PO fat- - h3a 14~o'cA•—rhepAr NAribkv tcub I I II i1+ c 1-7 ae County _ M COe�It Co2021 ntact Person: 1L1� p '�I I mti Telephone 11:8_29•TSi-4/rl ie�K33G8 Well Location/ Site Name: Sevlgr/ 6A _Po�No. of Wells to be Sampled: _[_wm Pmmle Well Identification Number (from Permit): IOW -/o Well Depth: IS 1l. Well Diameter: 2 in. For Groundwater Treatment Systems Screened Interval: /y /tD ft.L to A,4 Check Oe: ❑ Influent (9 n ft. ❑Effluent (99) Depth to Water Level: /S 8 "tl. below measuring point. Measuring Point (M.P.) is: 2_3 It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pa ped7bail d before sampling: 6 -D Date sample collected: ?f�OG Field analysis: pl-17 •z Specific Conductance uMhos Temp' . * ' *C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT ll: EXPIRATION DATE: 240/ Non -Discharge LJ9 000sN_g3 UIC NPDES TYPE PERMITTED OPERATION BEING MONITORED Lagoon _Remediatlon:Infiltration Gallery Spray Field _ Remediation: Rotary Distributor _ Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: LaboratoryName: Ervus's, Certification No. (vOD PARAMETERS (Samples for metals were collected unfiltered ✓YES _NO COD and field abldified Coliform: MF Fecal mg/I /100ml Nitrite (NO2) as N Nitrate (NO3) as N mg/I Coliform: MF Total ' /100ml mg/I Phosphorus: Total as PoG-Caa mg/I (Note: use MPN method for highly turbid samples) Dissolved Solids: Total8/ t6iii- oo mg/I Orthophosphate AI =Aluminum m /I PH (when analyzed)8/�1,1pL 6.2 Y �unils Ba - Barium mg/I mg/I TOC 8/zoho G - Chloride /o%, L /• oo mg/I 2� ✓mg/I Ca - Calcium.6/22 j0G - t. mg/I _8//g Arsenic �— Cd - Cadmium mg/I Grease and Oils mg/I mg/I Chromium: Total Cu - Copper mg/I mg/I Phenol Sulfate.v/ i"` - /1 / 27o%mg/I Fe - Iron mg/I Specific Conductance uMhos Hg - Mercury /I K - Potassium r g TKNTotaIas N Ammonia mg/I Mg -Magnesium _642 02. mg/I mg/I Mn - Manganese g/I fV _AYES _ NO) as ' r Ni - Nickel Pb - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method fl. Attach lab report.) Report Attached? Yes _(1) No_(0) VOC : method tt =_ method If = method 1) = GW,-59 -- 1l ( Ire Ie uzo L� u v LQ 6o OCT 0 5 2006 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Permit Name (if Facility Address Well Location/ Site Name: SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Telephone if: 8trl'9S i-N/r/ No. of Wells to be Sampled: Well Identification Number (from Permit): /N4i-// For Groundwater TrealmenlSyslem Well Depth: / 3 s ft. Well Diameter: �_ in. Check One; ❑ Influent (98 Screened Interval: l/h- It. to a/x ft. ❑Effluent (9) Depth to Water Level: ^Lp (� fl. below measuring point. Measuring Point (M.P.) is:&'�- It. above land surface. Relative M.P. Elevation in It.: Gallons of water pumpgd/bailed before sampling: b D Date sample collected: Field analysis: pH •yy , Specific Conductance ' uMhos Temp. l7TX OC, Odor Appearance PERMIT N: DEPARTMENT OF EIIVIRPgl WATER DUALITY-DIVISIONL( 1636 MAIL SERVICE CENTER EXPIRATION DATE: Non -Discharge_ Wq 060S603 UIC NPDES aPE OF PERMITTED OPERATION BEING MONITORED Lagoon _Remediation: Infillralion Gallery Spray Field _Remedialion: Rotary Distributor _ Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: ,SEk bE Laboratory Name: iMw �• Certification No. (a d O PARAMETERS (Samples for metals were collected unfiltered • YES _NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /l00ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as Pg,/�2VA -o.0" mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total / oG- 3 go 'Mg/l Al - Aluminum 8&UPA- /•2 "mg/I pH (when analyzed)tff R 06 - � • I/ -"units Ba - Barium - o -o mg/I TOC �/Zolafo - 2: 33 ✓mg/1 Ca - Calcium f .27 - / g/l Chloride B%/fi; b� - ll' 33 Vmg/I Cd - Cadmium - 0.007 g/I Arsenic g/22 �o.olo,rng/I Chromium: Total vvmg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate i7V&/ LD10- / 90 'mg/I Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/1 Mg - Magnesium 1?/221o6 - 7• Z mg/I TKN as N mg/I Mn - Mangan ese.!/2�,o4 - 1--!-VIMg/I to ER rV ✓ YES NO) "1- Ni-Nickel to- 4 D•ID g/I Pb - Lead Fi'/22/66 - D . z) glI Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) v.ui+r_R/22106- LO.020mo{L" g12.�lai — 22 mg& ORGANICS: (GC,GC/MS,HPLC) (Specify test and method N. Attach lab report.) Report Attached? Yes --(I) No _ (0) VOC : method ft = method it = method It = Ile -Please ant or type SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM • - — ­1 Ulm/� Please Print Clearly or Type Facility Name: l [ot4TS A Me �iCA ✓t Permit Name (if ddfprent): Facility Address: ?batik 3G8- G,30 rhPr+�te4� ThoQ�a b _ nir4n�e.t .Co wC 2R7 County-�Mf Qcwp[t ntacJuly' t Person: �t+1 AIM prt tZ'"I Telephone it: Well Location/ Site Name- 15L[�I E PFl v ek'4 No. of Wells to be Sampled: f mm ve,m q Depth: Well Identification Number (from Permit): tit to—/2 I Well De 13 For Groundwater Treatment Systems P ft. Well Diameter: _?- in. Check One: ❑ influent (96) Screened Interval: /V /r4 It. to � r4 Ill. Depth to Water Level: fl. below measuring point. Effluent (99) Measuring Point (M.P.) is: ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/balled before sampling: /s Date sample collected: 8 D (e Field analysis: pH 6.71 Specific Conductance umhos Temp. /74 °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMITS: EXPIRATION DATE: Non -Discharge WQ0003(o A UIC NPDES T_ YPE OF PERMITTED OPERATION BEING MONITORED Lagoon _Remedialion: Inlillratton Gallery Spray Field _Remediation:__ Rotary Distributor Land Application of Sludge Other: NOTE• Values should reflect dissolved and . colloidal concentrations. Date sample analyzed: 5EE 6 /, Laboratory Name: ,6.y tn'r•o rti in e. Certification No. fc 0 e PARAMETERS (Samples for metals were collected unfiltered EYES and field acidified COD mg/I /100ml _NO Nitrite (NO2) as N Nitrate (NO3) as N mg/I /I Coliform: MF Fecal Coliform: MF Total /100ml m Phosphorus: Total as PV? �- e,o 0 mg/I (Note: Use MPN method for highly turbid samples) Dissolved Solids: TotalWap- 386 m9/1 Orthophosphate A( - Aluminum �l?2,/�- mg/I PH (when analyzed) "Jo 4- /c•7/ units Ba - Barium�J2vne - 6•29 mg/I ogs �mg/I TOC-.4 f ofa- s y mg/I co Ca - Calcium_f>J»/oG - —vi mg/I Chloride g�/R &l. - 17 mg/I Arsenic 8/2z,/o 6- Z D o/D''mg/I Cd - Cadmium_sJzz/c6 - / Chromium: Total /vs� o.caG m /I �o.oe`s'y �mg/I Grease and Oils mg/I Cu - CoPhenolpper m /I Sulfate i - o - �mg/I mg/I Fe - Iron Fig - Mercury mg mg/I Specific onductance uMhos K - Potassium g Total Ammonia TKN as N mg/I Mg - Magnesium fffz��eY, - �'.h m /I mg/I Mn - Manganeses{zi - //•7 m9/I L� 30 YES _ NO) Ni - Nickel_ga-y-� Pb - Lead2J06 - < o. des j( Zn - Zinc 1 mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) S wlw-r- SP 2z o - te•e b ORGANICS: (GC,GC/MS,HPLC) (Specify test and method S. Attach lab report.) Report Attached? Yes --(I) No _ (0) VOC : method N = method S = method It = u u G= %O lrz u V = ILU GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM - Facility Name:. ( 0.47" 5 11jWD Permit Name (if different): Facility Address: 100 g- (y 3c1 gr p ^ 1 D'%i (Street) ' 2 % z tc" y)4 Contact Person: _ r Well Location/ Site Name: ✓/ it fl VrA,-t SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type 'iC4 � T6pd I(J - County-/9d cQowp (C Telephone if:L28-')S6-9d/ jry9ttfl No. of Wells to be Sampled: _-_J._- °m Pumlq Well Identification Number (from Permit): _y114J^/ Well Depth: / 5 For Groundwater Treatment Systems P it. Well Diameter-. 2 in. Chec Screened Interval: !V r1• It. to A,A k One: ❑ Influent 98 It. ( ) Depth to Water Level: below measuring point. Effluent (99) Measuring Point (M.P.) is: 2!^ It. above (and surface. Relative M.P. Elevation in ft.: Gallons of water pumped/balled before sampling: /•S Date sample collected: -D6 1=1e1d analysis: pH_ , Specific Conductance ' UMhos Temp. J - °C, Odor Appearance OCT 0 5 2006 DEPARTMENT OF ENVIRONI WATER QUALITY DIVISION, C 1636 MAIL SERVICE CENTER PERMIT it: EXPIRATION DATE: Non -Discharge G/QOeng ¢O3 UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED —Pet Lagoon _Remedialion: Infiltration Gallery Spray Field ' _Remediallon: Rotary Distributor _Land Application of Sludge Other: - NOTE• Values should reflect dissolved and . colloidal concentrations. C0 R� r*m Dale sample analyzed SCE Laboratory Name: 2c, Certification No, to o!, o , rn, PARAMETERS (Samples for metals were collected 'Unfiltered- ✓ YES _NO and field acidified COO mg/I Nitrite (NO2) as N mg /I Coliform: MF Fecal /100rn1 N.itrate (NO3) as N m/I Coliform: MF Total /1 nnmi Phnenh nr, 7 d 1 n 0 4r1 ✓ g (Note: Use MPH method for highly turbid saa)pfe Dissolved Solids: Total I? /rob- mg/1 pH (when analyzed)o nits TO C D - ✓ g Chloride bV /I Arsenic 00 -` � C,- 6 - mg/I Grease and Oils g mg/I Phenol mg/I Sulfate 8//5'/nG - 7.9 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Orthophosphate mg/I Al = Aluminum 9422Lge- O ./o I mg/l Ba - Barium gw�JoG- o• mg/I Ca - Caicium-ro�- . /s9 mg/I Cd - Cadmium 0123Z66 - 9.'oo7mg/I Chromium: TotaliZ 21,cG- Gb 3 KTIg/I Cu - Copper m9 /I Fe - Iron mg/I Fig - Mercury m /I K - Potassium mg/I Mg - Magnesium 06- 2 8'`mg/I Mn - Manganese 1-9-1°Smn/l ✓YES _ NO) NI -Nickel B,/23/0& - Z o oea mg/I Pb - Lead sr9!2.7 46 - to 00S2) mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method V. Attach lab report.) Repoli Attached? YeS_0) No _(0) VOC : method tt = method N = method It = G W-59 K-\-)O.. n r , '�2 l i'- --> SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:—_( 12A71S Permit Name (if diffe ell[: s: A Facility Addres� (C }�(___� hltf n)p Is 1 A� 2 tr9SL Contact Person:— ;-L-(-p rl (E'°) 'Nell Location/ Site Name:_lul icy eopc a,DA_ Please Prinr Clearly or Type dti County IAcOour tC Telephone t1:829-9S1 No. of Wells to be Sampled: Well Identification Number (from Permit): Ylk)-/ _ Well Depth: / It. Well Diameter: Z in For Groundwater Treatment Systems Screened Interval: H- f!. to n g ft. Check one: ❑ Influent (96) Depth to Water Level:ft. below measuring point. Effluent (99) Measuring Point (M.P.) is: z It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/balled before sampling: :1 -1) Dale sample collected: 8. p Field analysis: pH L(cZ , Specific Conductance uMhos Temp. l7•�^C, Odor Appearance DEPARTMENT OF EIIVInONMENT A NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMITY: EXPIRATION DATE:. S 10/ Non-Discharge1.4-ApodSG07 UIC NPDES TYPE OF PEBMITTED OPERATION BEING MONITORED Lagoon ___Remedlallon: Infiltration Gallery Spray Field _Remedialion: Rolary Distributor —Land Application of Sludge Other: NOTE- Values should reflect dissolved rind, colloidal concentrations. Dale sample analyzed:CC/mu/ 2i Laboratory Name: dl 7Z—T_J_, Ci Certification No. D b PARAMETERS (Samples for metals were collected unfiltered YES _NO and field acidlffed COD Coliform: MF Fecal Coliform: mg/I /10Um1 Nitrite (NO?) as N Nitrate (NO3) as N MF Total (Note: Use MPN method for hlrgbly lurbtd /100ml mg/I Phosphorus: Total as Pff/ts�0 -0,03 mg/I samples) Dissolved Solids: Total // pb- G6� mg/I Orthophosphate At = Aluminum m /I g pH (when analyzed) p -—_4�units TOCSz12o a[ ` Ba - Barium mg/I mg/I Chloride / ��-�� - 9 G7 mg/I S R mg/I Ca - Calcium�S/� fo6 � Cd Cadmium mg/I Arsenic - mg/I Grease and Oilsmg/1 mg/I Chromium: Total Phenol mg/1 Cu - Copper m g /1 Sulfate - — rng/I mg/l Fe - Iron I Ig -Mercury mg/I Specific onductance Total Ammonia uMhos K - Potassium mg/I mg/I TKN as N rn /I M 2-6, J Magnesium 6- r mg/I M9 - Ma9ganese mg/I 9 Y_ � YES _ NO) ry Nf - Nickel o fir g/I Pb - Lead I Zn - Zinc - -9/i Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ------------- ORGANICS: (GC,GC/MS,HPLC) (Specify test and method 0. Attach lab report.) Report Attached? Yes-_(1) No _ (0) VOC method 0 = method 0 = method f) = GW,59 �.... ............. � � �„ A„��,..,. GW-59A CO?JPIJA-NCE REPORT FORD Perm it # ALI ooase (Snhmit one each monitoring period with GW-59 forms) -•••- -- u."m—illy results were due. (— be.submitted after the established due date? Was any required on the monitoring report (GW-59 and YES it the answer to question Y or 2 is 'YES", list in the space provided bets explain the problems encountered in obtaining the required information. J Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing I ES identification plate, area overgrown, etc)? IJthe mower is 'Yes-, contact the Regional Office for guidance. I NO Are any monitored constituents equal to or above the established standards? ✓ NO !f the answer to question 9 is NO; skip to section 8. YES � If the answer to question 4 is `YES"list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below. rui one constituents identified in question 4 above, have stan same constituent(s) in the same well(s) in the last two years? the YES NO it the answer to question 5 is NO ;skip to section 8. IF the answer to question 5 is `YES", list in the space provided -below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). Are the monitoring wells listed in section 5 located at or beyond the review boundary? I YES NO /f the answer is `YES'; a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFr'7CE IMMEDIATELY FOR GUIDANCE. If the 'No'; answer is monitoring wells may be improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required bythe Division involving this groundwater quality problem? i YES NO If the answer to question'YES; describe those actions in the space provided -below_ If the answer to 7fs `NO'; question contact the Regional Office within 90,da sr,an-evaluation m be- reguired to determine the imoact the waste dis osa! system is Navin at' fhe•revidwi`and,cdmolfance boundaries surrounding this facility. Failure to do so may subiebt the oermittee to a Notice of Violation fines and/oroenalbes. OCT O 5 2006 Asheville Regional Office —_ A uifer Protection e rya.,erg_.,...:.,m,.�,.<:__.�:---_•__ -- - r•-•--•• ��••r-L-v ""- pur"on Ivvv-ayA) or me monitoring report shoula'sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. CW-59A 12/812003 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Prinf Clearly or Type Facility Name: rm E PI e a nl Permit Name (it different): Facility Address: _. 'MPiON wreeq rt,:L Zgry Z N O41f L( Icuyt ; t 1: si ° L°t' County �= i) Contact Person:_Q ) m afv Telephone #:92E-75E -y/n Bz3�GP Well Location/ Site Name: r1clC s re u ry No. of Wells to be Sampled: 1 Well Identification Number (from Permit): 7te Weli Depth; _ ,S _ {l, �n/ell DiameFor Groundwater Treatment Systems Screened Interval: ^ R ft. to j'/yCheckOne:❑ InflUettt (98) ❑ Effluent (99) Depth to Water Level: 3ry•cl it. below measu Measuring Point(M.P.) is: 2.3 ft. above land surface. Relative M.P. Elevationin ft.: Gallons of water pumped/balled before sampling: 9D Date sample collected v-y'e 6 Field analysis: pH 2 6 , Specific Conductance uMhos Temp. S °C, Odor Appearance PARAMETERS (Samples for metals were collected COD Coliform:'MF Fecal /1 mg/ Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total(L-S--6h) q,S' mg/I pH (when analyzed) f y-LI eb) 7.26 units TOC f °1-12-e 11 1.11 Chloride f y-(o o b )—_ mg/1 _ Arsenic mg/I mg/I Grease and Oils mg/1 Phenol mg/I Sulfate —-7 0l0) mg/1 Specific Conductance uMhos Total Ammonia moll TKN as N mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: EXPIRATION DATE; Non -Discharge- 1A- 60o S 603 UIC NPDES /uC 049G y2L/3 TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon _Remediation: Infiltration Gallery Spray Field _Remediation: Rotary Distributor Land Application of Sludge Other. 4 L1QM Values should reflect dissolved and colloidal concentrations, < Date sample analyzed: S IFE IOEL0 Lt) '�< Laboratory Name: EIV• Ie5}, t>60L• Certification No. boo >- r- Itered ✓ YES _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P. mg/I Orthophosphate mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium y-11 eb mg/I Cd - Cadmium mg/I Chromium: Total mg/1 Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium Mg - Magnesium (4 /1 or, 9.3 mg/I _ Mit- Manganese mg/I mg/I v YES _ NO) -G Ni'- Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) (Specify test nt %61 Report Atta hed? F" VOC method # G W-59 Rev. 0312000 SUBMIT FORM ON Y LL W PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM. Facility Name: L 0A+'5 141'n E r; C a Permit Name (if different): Facility Address: l0 3 F m E n i a �. tM A., `� e N? Isreeq ----__._ Icuy) C 2 2 -2 `51 10) - Contact Person: `1 h; Llr 1} rn,e � Iv°1 Well Location! Site Nama• 5ti Q r or Type rJ County. 11'LLoJecL611 Telephone#:8256K//r/ r=,34ER No. of Wells to be Sampled: Well Identification Number (from Permit): 14lo- / u om Fem l) Well Depth: j' ForG'oundwaterTreatment Systems n P Iw ft. WeIIlDiameler•: 2 in. Check One:❑ Influent (98) Screened Interval: rrt- ft. to IAL ft..11 Depth to Water Level: J,'.3 ft. below measuring point. Effluent (99) Measuring Point (M.P.) is: 7_3 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/balled before sampling: Date sample collected: -el-00 Field analysis: pH r .23 , Specific Conductance uMhos Temp. C, Odor Appearance DEPARTMENT OF ENVIRONMENT& NATURAL. RESOURCES WATER QUALITY DIVISION, GROUNDWATER _SECTION 1636MAIL SERVICE CENTER PERMIT#: EXPIRATION DATE: "3J-6G Non -Discharge UIC NPDES NC Op0 yzy� TYPE OF PERMITTED OPERATION BEING. MONITORED Lagoon _Remeciaiion:Infiltration Gallery Spray Field _ Remediation: Rotary Distributor Land Application of Sludge Nam'. Values should reflect dissolved and ._4 , *M colloidal concentrations. I —arn Date sample analyzed: �EF i�F�a sJ ro om Laboratory Name: 7 Certification No. / 00 PARAMETERS (Samples for metals were collected unfiltered_ ✓✓ YES COD Coliform: MF Fecal mg/I _NO and field Nitrite (NO2) as N acidified Coliform: MF Total /100m1 /100ml Nitrate (NO3) as N Phosphorus: Total as P. mg/I mg/I (Note: Use MPN,method for highly turbid samples) D's;;oived $ocl : Iota ti',-06 Orthophosphate mg/I PH(whenanalyzed) c o� a mg/I G:23 units AlAI - Aluminum Ba - Barium mg/l y-2u-ct Chloride �I r,� mg/1 Ca - Calbium_ y-//-off /y mg/l. m /I _ �N b oil Arsenic °° ! 2 mg/I Cd - Cadmium, mg/I Grease and.0ils mg/I mg/I Chromium: Total Cu - Copper mg/I Phenol Sulfate � w/ � mg/I 3�0�, mg/I Fe - Iron Hg - Mercury mg/I mg/I Specific Conductance Total Ammonia uMhos mg/I K - Potassium Mg - Magnesium y /1•0 6 •7,/ mg/I mg/I TKN as N mg/I Mn - Manganese mg/I mg/I YES — NO) NF- Nickel mg/I Pb - Lear[ mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes_(1) No _ (0) VOC : method # : method # = method # = GW-56 - Rev. 03/2000 7.06 SUBMIT FORM ONLLOVV PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATIONn (� Please Print clearly or Type Facility Name: I n f3 Li Ft m E n: CAN Permit Name (if different): Facilityy Address: - (o Iri me ^� c>F1r, iti+`w� _ (cIIrYYv Ar ioro Is ) w 292 - County IY1S100&w,t: I Contact Person: ti.tt Q 034-mov-, z"t Telephone It:i3'L8.7S✓y'4rlf >r336R Well Location/ Site Name: Vo N No. of Wells to be Sampled: f emm Pe min Well Identification Number (from Permit): /�7 lJ -/ For Groundwater Treatment Systems Well Depth: ) it. Well Diameter: 2 in. Check One: ❑ Influent (98) Screened Interval: r /r>0 it. to " ft. ❑ Effluent (99) Depth to Water Level: ft. below measuring point. Measuring Point (M.P.) is:2 It. above land surface. Relative M.P. Elevation in It.: Gallons of Water pumped/bailed before sampling: r Date sample collected: tz-y-o6 Field analysis: pH_ Specific Conductance uMhos Temp. /3 'C, Odor Appearance DEPARTMENT OF ENVIRONMENT& NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: EXPIRATION DATE: 3'3 f -ID G Non -Discharge_ LcJL 6(9 bo UIC NPDES /'UC 606 c/2y ,3 TYPE OF PERMITTED OPERATION BEING MONITORED —jG Lagoon _Remediation: Infiltration Gallery Spray Field _Remediation: Rotary Distributor _Land Application of Sludge o Other: _ NOTE, Values should reflact dlssoiv6d find colloidal concentrations. -gin co rn Date sample analyzed: S6E QElo aJ zm� Laboratory Name; v • i o r . Certification No. G60 _ r PARAMETERS (Samples for metals were collected unfiltered DES NO and fielrf al i liras �"u mg/I Coliform: MF Fecal /100m) Coliform: MFTotal /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total La,fo4 0 PpH OCWhen analyzed)_(y 2 ao6) ,;.U5- 1—% 07 frig/1 units mg/I Chloride _ ( y-6-66) /o mg/I Arsenic mg/I Grease and Oils Phenol mg/I mg/I Sulfate `I //roG /8d mg/I Specific Conductance uMhos Total Ammonia TKN as N mg/I mg/I Nitrite (NO2) as N m /I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Orthophosphate mg/I AI -'Aluminum mg/I Ba - Barium mg/I Ca - Calcium. 4-//-06) t S mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Fig - Mercury mg/I K - Potassium Mg - Magnesium y-//-dro y.l mg/1 mg/I Mn - Manganese mn/I v YES _ NO) -L Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc -._ m /I Ammonia Nitrog� m I Other (Specify CarrfDC SSe -nf . I, Ic (Specify test and method #. Attach lab report.) Report Attached? YeS_0) No _ (0) VOC : method # = A r— method # _ method If G W-59 �4 p(" - /j 2 7 0 6 Rev. 03/2000 Slgnalure of Pe m llee (r Aveto. I Agent SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: ° COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print clearly or Type Facility Name:_ C'n a >< y rn e c. A PERMIT #: Permit Name (If different): Non-Discha Lamy Auuress:— N V T+-M Q A PA AN 1 h ti (SIX. -ill .e. TelephoneMak-756-4//i e,�5 Well Location/ Site Name: 65F1 ub' Af- No. of Wells to be Sampled: �� .M I mm 1—.1 Well Identification Number (from Permit): 94J-)2 Well De ih: I . For Groundwater Treatment Systems P —_ �_ft. Well �in. Check One:❑ Influent 98 Screened Interval: � ft. to /'Q ( ) Depth to Water Level: 9 S ft. below measuring point. Effluent (99) Measuring Point (M.P.) is: 2 • � fL above land surface. Relative M.P. Elevation in ft.: Gallons o�pwaterpumped/� fled before sampling: 1, 6' Date sample collected: Field anal sis: H Specific Conductance ' uMhos Temp. I ?- °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOuRCEs WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER EXPIRATION TYPE OF PERMITTED OPERATION BEING -MONITORED Lagoon __Remediation: Infiltration Gallery Spray Field _Remediation: Rotary Distributor _Land Application of Sludge Other: __ NOTE- Values should reflect dissolved as -id . colloidal concentrations. _+c C:)>7:u < *171 Date sample analyzed: S.F5 B� 110 kl t :m Laboratory Name: ��� ies a� C MD Certification No. % O 0 ^, mr-ri PARAMETERS (Samples for metals were collected unflltered_L�YES COD mg/I _NO and field Nitrite (NO2) as N abidlfied m if Coliform: MF Fecal COliform: MFTotal /100m1 /loom[ Nitrate (NO3) as N mg/I (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total t-s-ot,) coo Phosphorus: Total as P. Orthophosphate mg/1 mg/1 pH (when analyzed) a ,o b mg/I r76 units AlAI - Aluminum Ba - Barium mg/I TOC _ (v-12-o4 3,57 mg/I Ca - Calcium z/ /1-06 )i' mg/I mg/I Chloride C y (r-o6) Arsenic 41 mg/I Cd - Cadmium mg/1 Grease and Oils mg/I mg/I Chromium: Total Cu - Copper mgll Phenol Sulfate N-R-at mg/I Fe - Iron mg/1 mg/I — Specific Conductance mg/I uMhos Hg - Mercury K - Potassium mg/I Total Ammonia mg/l Mg -Magnesium - e6 /c) mg/I TKN as N mg/1 Mn - Manganese mg/I m9 /I _!L-YES _ NO) Ni - Nickel -Ag/I Pb - Lead mg/l Zn - Zinc mg/1 Ammonia Nitrogen mg/l Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Repoli Attached? Yes _(1) No _ (0) VOC : method # = tL;.o i }frnpw O method # = method # = ...... yon,r ��..... IIO I Ile -r e e print or GW-59 r p yrJLrzygcp Rev.03/2000 Signature Ofvermdte AUlhorizedAge SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Fes""-" ' 1141­"^ ° " I IUIN /� / /] Please Print Clearly or Type Facility Name:_.._ l CA4 T H.m e n 1 C q k'v Permit Name (if different): Facility Address: _. 420( Well Location/ Site Name: County m=:)d4J a-rC Telephone No. of Wells to be Sampl Well identification Number (from Permit): ihtl-/.3 . _. _. oundwater Treatment Systems Well Depth: /.S it. Well Diameter: P_- in. Check One: ❑ Influent 96) Screened Interval: '/i4 it. to !VA ft. ❑ Effluent (99) Depth to Water Level:- 145 ft. below measuring point. Measuring Point (M.P.) is: 2. (o ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/balled before sampling: 2 Date sample collected: 4/-V-64 Field analysis: pH S. 9,q , Specific Conductance ' uMhos Temp. -19-`/ °C,Odor Appearance PARAMETERS (Samples for metals were collected COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 290 mg/I pH (when analyzed) -q-eG 98 units TOC 9-11-e/ ..L mg/I Chloride _ Lr C-oL 13 mg/I Arsenic mg/I Grease and Oils Phenol mg/I mg/I Sulfate C '1-N-ot-) L�/ mg/I Specific Conductance uMhos Total Ammonia TKN as N mg/I mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT1f: EXPIRATION DATE:_, Non -Discharge /✓QDa6En3 UIC NPDES /UC660t12y3 TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon _Remedialion: infiltration Gallery Spray Field _Remediation: Rotary Distributor _Land Application of Sludge NOTE, Values should reflect dissolved and colloidal concentrations. Date sample analyzed: Laboratory Name: Certification No. tered_ZYES _NO and field abldifled Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Orthophosphate mg/I Al = Aluminum mg/I Ba - Barium mg/I Ca - Calcium. ( y-/(-oO / F mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium y-l! 06) // mg/I Mn - Manganese mg/I YES _ NO) 4 >a ' n rp rrtm N prn Ni - Nickel mg/I Pb - Lear) mg/I Zn - Zinc_ mg/I MI IIII IV[ Ild IV1trUyerl Other (Specify OompoUjj9EgEdA&nTrt>Dn Units) I IJUN U 12006 . ^.._•. ra 40 l ORGANICS: '(Gc,G (ML+h#tFLr¢))tection (Specify test and method If. Attach lab report.) Report Attached? Yes. --(I) No _ (0) VOC method # = method # = method # = G W-59 Rev. 03/2000 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM f-NGILI I r INI-UMMA I IUN Please Print Clearly or Type Facility Name: ( 3 i7 /Y e r) C /V /L� Permit Name (if different): Faclli1vAddress: f 96 n+Pn'cA2 77.eeA YYlgr?erJ � SeeOw 2$%5Z' County %n`l!owel( Contact Person: r�, L� % P I"U' M w ✓i (Zip) P � Telephone #:Sz8!A:6 1jV ( fx 3 9 Well Location/ Site Name: de" /e=u No. of Wells to be Sampled:_ emm Pcrmlp Well Identification Number (from Permit): M40-/y For Groundwater Treatment Systems Well Depth: iS ft. Well Diameter: 2 in. Check One: ❑ Influent (98) Screened Interval: /R ft. to '"41 ft. ElInEffluent(99) Depth to Water Level: �' `I ft. below measuring point. Measuring Point (M.P.) is: ?_� ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/b Iled before sampling: 3 Dale sample collected: LI-1-06 Field analysis: pH �'� � , Specific Conductance uMhos Temp. 12.3 °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER DUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMITff: EXPIRATION DATE:• Non -Discharge wQOoorj 60'3 UIC NPDES /LC e6092g3 TYPE QF PERMITTED OPERATION BEING MONITORED Lagoon _Remedlation: Infiltration Gallery Spray Field ' _ Remedialion: Rotary Distributor _ Land Application of Sludge Other: rry I ". WaIUUb SIIUUIU r2IIUGi aissclvea ana CD colloidal concentrations. so Date sample analyzed: J`c'E BC loco t —� Laboratory Name: ANCO M Certification No. H 04 N ED PARAMETERS (Samples for metals were collected unfiltered AYES _NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosnhorus TntRl as P mn/I (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 4( Zr6rif) SSasrag/I pH (when analyzed) (11- 00 140 units TOC — (9-t2sQ7 mg/I Chloride y-tc 3 L- mg/I Arsenic mg/I Grease and Oils mg/1 Phenol mg/I Sulfate Y-B-cG 2 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Orthophosphate m6/1 At - Aluminum mg/l Ba - Barium mg/I Ca - Calcium N'//'oG) ( mg/l Cd - Cadmium mg/I Chromium: Total mgll Cu - Copper mg/l Fe - Iron mg/I Hg - Mercury mg/I K - Potassium Mg - Magnesium -1VG 92 mg/I mg/I Mn - Manganese mq/l 1--IES _ NO) Nt- Nickel `mg/I Pb -Leant mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes_(1) No _ (0) VOC : method # = : method # = or 0fC method # = GW-59 t-° Rev. 0312000 GW-59A COMPLIANCE REPORT FORM_ Per ii It # � / C�SGo 3 (Submit one each monitoringperiad with GIF-59forms.) /VCd(9092y3 1 Enter date monitoring results were due. (M.4r- oe ) Will this monitoring report (GW-59 and GW-59A) YES NO be.submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES NO IFthe answer to question 1 or 2 is "YES", list in the space provided below the welt identification numbers) and explain the problems encountered in obtaining the required information. i 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? Irthe answer is "Yes", contact the Regional Office for guidance. I ✓ 4 Are any monitored constituents equal to or above the established standards? YES N If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below., 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s).in the same well(s) in the last two years? If the answer to question 5 is "NO" skip to section B. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentrations) reported, and sample collection date for each occurrence (for the last two years). 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. if the answer is `NO", monitoring wells maybe improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this i YES NO groundwater quality problem? If the answer to question 7 is `YES, describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days: an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so maysubiect the permittee to a Notice of Violation Fines, and/or penalties. I� i g The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. i 'he febyacknpwledgelhatrt rf a above:9nfo—mat lor :was evaluated aril the Infocma'""`- "ffon submitted Inthls K repprt`(Comphar ce Repoli-�GWr5%A true and compleI LZ ttie�best of my knowledge x":•_ �_<,. ys z7-o� Signature of Permitte' (or Authorized Agent) Date GNV-59A 12lSR003 SUBMIT FORM ON YELLOW PAPER ONLY lam^ GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION _ Please Print Clearly or Type Facility Name: Lorafl Hmc zN Permit Name (If different): t-aoIIllyAddress: 'O t `5f,5E &— Cn3o owElme+-rceN (k erg R,( to-r O+ /V c: Z55'75Z Count Contact Person: lull. , tfM Nam) tL') Telephone #: Well Location/ Site Name: `�e+/i :k ae+� No. of Wells to be Sampled: / Well Identification Number (from Permit): M W Nem R.11) Well Depth: 75 it. Well Diameter: & in For Groundwater Treatment systems Screened Interval: A/1q ft. to A//i ft' Check One: ❑ Influent (98) J6ra Depth to Water Level: ❑ Effluent (99) fL below measuring point. Measuring Point (M.P.) is:;?. -5 It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: �— Date sample collected: Z 8 0 Field analysis: pH "�7`3 ,Specific Conductance uMhos Temp. MI °C, Odor Appearance DEPARTMENT OF ENVIRONMENT R NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: EXPIRATION DATE:,`):'I R!L Non-Discharge_60 ca CecSb o �) UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon _Remediation: Infiltration Gallery Spray Field ' __Remediation: Rotary Distributor _Land Application of Sludge Other: NOTE' Values should reflect dissolved and v - colloidal concentrations. + w Date sample analyzed: -Sc e bt'/r J ca - Laboratory Name: �L�/v�o-ONrnr a 7'�sf+,us g' fiovlS Certification No. _ 606 PARAMETERS (Samples for metals were collected unfiltered t� YES COD Coliform: Mt- Fecal mg/I _NO Nitrite (NO2) as N and field acidified mg /I Coliform: MF Total /100ml /100ml Nitrate (NO3) as N Phosphorus: Total as P m g/I (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 9De,c5 Orthophosphate mg/I mg/I pH (when analyzed) too mg/I Al -Aluminum mg/I TOC 171)"OS units 5 31 mg/1 Ba - Barium Ca - Calcium14Dcdos mg/I f R mg/I Arsenic 9a`c5 G 5 mg/I Cd - Cadmium m /I g Grease and Oils mg/I Chromium: Total mg/I Phenol mg/I Cu - Copper m g Sulfate — 3o Ncb, mg/I tit mg/I Fe -Iron Hg -Mercury Specific Conductance Total Ammonia uMhos K - Potassium mg/I g TKN as N mg/l Mg - Magnesium 14d� L!S 9 2 in mg/I Mn - Manganese mg/I GW-59 Rev. 03/20oo FEB 13 2006 Asheville-Redonal Office YES _ NO) Ni - Nickel mg/I Pb - Learf mg/l 7_n - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method H. Attach lab report.) RePoROC rt Attached? Yes_;G(1) NC_ (0) method # = E•Pra�D method # _ method # GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Facility Name:_ Permit Name (if Contact Person:. Well Location! Site SUBMIT FORM ON YELLOW PAPER ONLY or Type DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT,#: EXPIRATION DATE:3f Ae din Non -Discharge (ell 0005GG 3 UIC NPDES /1/cC00gt243 TYPE OF PERMITTED OPERATION BEING MONITORED —�G Lagoon _Remediation: Infiltration Gallery Spray Field ' _Remedialion: Rotary Distributor .__ Land Application of Sludge Other: 1 NOTE' Values should reflect dissolved and ca colloidal concentrations. CD Cl Date sample analyzed: Sic 2zlow Laboratory Name: L-'+.rvro-��r Certification No. boo PARAMETER$ (Samples for metals were collected unfiltered ✓ YES COD R _NO and field acidifiamg/I Coliform: MF Fecal /1 mg/I Coliform: MFTotal ' /loom1 County—1 N ` f2rwe.1 I Telephone If: 628- 75'6r4 No. of Wells to be Sampled: Well Identification Number (from Permit): /Y! (. t /C Well Depth: ( For Groundwater Treatment Systems p —ft, t Well Diameter., in. Check One; ❑ Influent (98) Screened Interval: R ft Depth to Water Level: .7 ft. below measuring point. 11 Effluent (99) Measuring Point (M.P.) is: 2_3 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/balled before sampling: ' Date sample collected: 12 5-05 Field analysis: pH 'i br d`''Specific Conductance uMhos Temp._'C, Odor Appearance (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total_4D�G� 14o mg/I PH (when analyzed) is TOC 1-7DecDec DS —units (� m Chloride q eS Arsenic f'y 3 5 mg/I =�)r �����e� Grease and Oils mg/I Phenol mg/1 Sulfate - 3017e< n mg/I Z mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/1 GW-59 I FEB 13 2006 Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/1 Phosphorus: Total as P. mg/I Orthophosphate mg/I At - Aluminum mg/I Sa - Barium mg/I Ca - Calcium r4lk. cS 1! mg/1 Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/1 Hg - Mercury mg/1 K - Potassium mg/I Mg - Magnesium l Dec0$ 2.9 mg/I Mn - Manganese mg/I e YES NO) Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method R. Attach lab report.) Report Attached? Yes ✓ (1). No _ (0) VOC method ft = 2A method If = method II = or Rev. 03/2000 S 9na u e of P rmillee (or Authorized Agent) ' Z / Asheville Regional Office GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Permit Name (if Facility Address: SUBMIT FORM ON YELLOW PAPER ONLY Please Prinf Clearly or Type I$Ia1C) ` County L"t cJe-1 Contact Person:-J--, G, M�k ,vc,� (Z'°) Telephone It: _Si_'o•-Z5G-4171x33/� Well Location/ Site Name:Soulce (J, —&o -- --r------- No. of Wells to be Sampled: prom Pemip Well Identification Number(from Permit):.filw 11 Well Depth: /_3 it. Well Diameter: 5_ in. For Groundwater Treatment Systems Screened Interval: It. to Check One: ❑ Influent (98) —f� fl. Depth to Water Level: 14a S ft. below measuring point. El Effluent (99) Measuring Point (M.P.) is: Zft. above land surface. Relative M.P. Elevation in It.: Gallons of water pumped/bailed before sampling: _ IDate sample collected: Field analysis: pH ro,�1 , Specific Conductance ' uMhos Temp. `C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT#: EXPIRATION DATE: 31 Mnr oG Non -Discharge GJ0000,'[,og UIC NPDES AIC Loe-4py'; TYPE OF PERMITTED OPERATION BEING MONITORED —� Lagoon _Remedialion: Infiltration Gallery Spray Field '_Remediation: Rotary Distributor _ Land Application of Sludge f Other: -Tt T' LQTE: Values should reflect dissolved and . colloidal concentrations, w LD s: Date sample analyzed: J�e CSelow Cn -- LaboratoryName: Ct. ury Certification No. �Oo PARAMETERS (Samples for metals were collected unfiltered -/YES COD Coliform: MF Fecal mg/I _NO Nitrite (NO2) as N and field acidified m /I Coliform: MF Total /100ml /100m1 Nitrate (NO3) as N Phosphorus: Total as P. mg/I (Note: Use MPN method for highly Dissolved Solids: Total turbid samples) I O��05 Soo mg/I Orthophosphate At mg/I mg/I g PH (when analyzed) units -'Aluminum Ba - Barium TOC _ 17 ',A- Dp� LS 1 0'7 mgChlo/I es 2 Ca -Calciumt4 DtrS mg/I 9.0 mg/I .Arsenic �' Arsenic mg/I Cd - Cadmium mgll Grease and Oils men otal mg/1 Phenomg/I Cur�Co p Sulfate 4 1a-n o6 I4-o mg/I mg/l Fe - Iron Hg - Mercury mg/I Specific Conductance Total Ammonia uMhos I< - Potassium /I mg/1 TN mg/I Mg - Magnesium I D-Y-05 x/ `i m g/1 mg/I Mn -Manganese mg/I G W-59 Rev. 0312000 —)NBC- y L--' YES Ni - NickE Pb - Leac Z_n - Zinc Ammonia Other (sor ORGANIC : (GC (Specify test and m Report Attached? VOC or r, NO) mg/I mg/1 mg/I lS✓✓ (l) No—(0) method 0= EP46z30 £) method 9 = method If = 1 7_f -0 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Permit Name (if SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or L V,QL _ (City) 121p1 County '<✓�-ll Contact Person: ��« r /f)=e- u� a Telephone V: 888-7S6-/lNl X 3363 Well Location/ Site Name: rev / FC lue r'� —�� F No. of Wells to be Sampled: _L Petmll) Well Identification Number (from Permit): MiJ 12 Well Depth: I i it. Well Diameter: in. For Groundwater Treatment Systems Screened Interval: .3 ft. to fCheck One: ❑ Influent (98) _—.1'i Depth to Water Level: e / it. below measuring g point. p Effluent (99) Measuring Point (M.P.) is: 2_& ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/balled before sampling: 2 Date sample collected: r2-8-OCc Field analysis: pH ' • 7r Specific Conductance Temp. IS °C, Odor uMhos Appearance DEPARTMENT OF ENVIRONMENT $ NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1536 MAIL SERVICE CENTER PERMIT #: EXPIRATION DATE: _3j, Non -Discharge _,!­'Qoce,S,;,o UIC NPDES 61G6e01(pi1--�) TYKE QF PERMITTED OPERATION BEING MONITORED Lagoon _Remediation: Infiltration Gallery Spray Field _Remedialion: Rotary Distributor —Land Application of Sludge Other:_ NOTE Values should reflact dissolved and T colloidal concentrations. t w - Date sample analyzed: S s = iooJ 0 Laboratory Name: i=n�rvmNmr.0 - Tcs ,u. of • Certification No. ec PARAMETERS (Samples for metals were collected unfiltered ✓ YES _NO COD and field acidified if Coliform: MF Fecal mg/I /100ml Nitrite (NO2) as N Nitrate (NO3) as N ci Coliform: MF Total (Note: use /100m1 Phosphorus: Total as P mg/I mg/I MPN method for highly turbid samples) Dissolved Solids: Total °t 0ec OS : D Orthophosphate mg/I' g pH (when analyzed) mg/I AI = Aluminum mg/I units TOC I7 sec 05 .3 r 3 mg/I Be - Barium Ca - Calcium __ !U Deco z/9 m/I gChloride_ 9sOS 5-7 Arsenic M--- mg/I mg/IChromium: mum Total mg/1G Grease and Oils Phenol mg/I Cu -Copper mg/I mg/I Sulfate - 3oD, 05 I S mg/1 mg/I Fe - Iron Fig - Mercury mg/I Specific Conductance Total Ammonia u os - K Potassium mg/I mg/I TKN as N mg/I g/I Mg -Magnesium 14Dec05 R 6. mg/1 mg/I Mn - Manganese mg/I I t, G W -59 Rev. 0312000 G L-- YES _ NO) Ni - Nickel mg/I Pb - Lead mg/I 7_n - Zinc--TTig/I AmmoniaFjIYCOIE�Pounds ECEI�ItE_D A Other (Spa and Concentration Units ORGANICS.- - - - (Specify test and method 1t. Attach lab report.) Report Attached? Yes (1) No _ (0) VOC : method#=(--P66230D : method # = M or method H = —21-04 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: • DEPARTMENT OF ENVIRONMENT B NATURAL RESOURCES COMPLIANCE REPORT FORM WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER FACILITY INFORMATION r //)) Facility Cc Please Print Clearly or Type RALEIGH NC 27699-1636 Phone: (919) 733-3221 Name: LTS i`l"+rfer-ICZrJ Permit Name (If different):Non-Discharge_t-Utz PERMITN: EXPIRATIONDATE:.31 �Dcc o0U 121 3 Facility Address: o G,x 3E V — 6 3c �trC4L /o (Sveeq UIC 'mot b, Crj C (City) NL�JL Contact Person: ��- G �(s'°'°), (Z;,) ft�1 clJe County .7 (` TYPE OF PERMITTED OPERATION BEING MONITORED Well Location/ Site Name:vrP a+•- Telephone R; �6�ri- �-`�!( x33C.$ , ✓' Lagoon __Remediation: Infiltration Gallery No. of Wells to be Sampled: p Spray Field _Remedlation: .� Well Identification Number (from Permit): _A71,�1 /4 Imm P,,.n) ForGroundwalerTreatmenlSystems Rotary Distributor ._ Land Application of Sludge�',�t Well Depth: /5. ft. Woil Diame(er: Z Screened Intervalto — . ft--ice ft. in Check One; ❑ Influent (98) Other: cn Depth to Water Level: 17;,4 ft. below measuring point. Effluent (99) NOTE. Values should r effect dissolved and Measuring Point (M.P.) is: ft. above land surface. Relative M.P. Elevation in ft.: colloidal concentrations. C m Gallons of water pumped/bailed before sampling: 4 Date sample collected: IR-?-OS Field analysis: pH ) Date sample analyzed: 5e e �jelotJ , Specific Conductance Temp. 15 °C, Odor uMhos Laboratory Name: EN 5vil�ls Appearance Certification No, l C) 0 COD PARAMETERS (Samples for metals were collected unfiltered YES _NO and field acidified ;AYES mg/I Coliform: MF Fecal /100ml Coliform: Nitrite (NO2) as N Nitrate NO as N ( _ NO mg/I Ni - Nickel ) mgll MF Total /100m1 (Note: Use MPN method for highly turbid 3) Phosphorus: Total as P. mg/I Pb - Lean mg/1 mg/I Zn - Zinc samples) Dissolved Solids: Total `tDOS r{r7e mg/1 Orthophosphate At Aluminum mg/I Ammoni ItrO g/l g/I pH (when analyzed) units TOC_ I�n��cS Ba -Barium mg/I Other (S city C d ncenl�ration nits) & mg/I Chloride— q:D• c ; f U Ca - Calcium 1G�ea 5 ia� mg/I g mg/I Arsenic Cd - Cadmium mg/1 FEB 13 2- Grease and Oils mg/1 Chromium: Total mg/I Phenol mg/I Cu - Copper mg/I As evt e Sulfate - 30 l7ec OS t (o mg/I Fe -Iron mg/I ORGANI ton Specific Conductance UMhos Total Ammonia Kg Pota stium mg/1 (Specify test and method tF. Attach lab report.) mg/I Report mg/I TKN as N Mg - Magnesium Attached? Yes-_ (1) No _ (0) mg/I VOC mg/I Mn -Man anese g : method II= ElPA&23an mg/I method 0 = ■940rtnw arns■■�. _ _ _ - - method N = c ......... ^ -_.. (.y .„w uuu ...re. rlease print or type GW-59 U_.= G.—)"�z-�ct: nL - Rev. 03/2000 SIi 9 1an t iIa^ , i tint Pet rnhee forA Ih ( �I GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Permit Name (it SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type Icily) t Islale) F County /r/ `-Cls�e!( Contact Person: -1-✓ G k:.. e z'ol —, Tel. O one Wells to be milled:/f/x'366 Well Location/ Site Name: Sf�rel- _ «:L�i�sY'i�n No. of Wells to be Sampled: / Irom Permlp Well Identification Number (from Permit): /224J /3 Well Depth: / 5 ft. Well Diameter: � in Far Groundwater Treatment Systems Check One: ❑ Influent (98) Screened Interval: 5 ft. to IS_ ft. Depth to Water Level: 17 ft. below measuring point. � Effluent (99) Measuring Point (M.P.) is:2.6 It. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/balled bef?re sampling: 2.5 Date sample collected: 124 - oS. Field analysis: pH "7.� `&pecific Conductance - uMhos Temp. _IIm OC, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT#: EXPIRATION DATE: 31 .17o_c09 Non -Discharge W C0U004�43 UIC NPDES LJCg0c424 :� TYPE OF PERMITTED OPERATION BEING MONITORED L_� Lagoon _Remedialion: Infiltration Galleryt' Spray Field _Remedialion: Rotary Distributor __Land Application of Sludga�� Other: '� UQTE• Values should reflect dissolved and , w colloidal concentrations. C ) Dale sample analyzed: 5�' &-1OLj --•� Laboratory Name: ENT Certification No. G-Cav PARAMETERS (Samples for metals were collected unfiltered YES COD —NO and field acidified Coliform: MF Fecal m /100ml Nitrite (NO3NO2) as N Nitrate NO3) as N ( mg/I Coliform: MF Total (Note: Use /100MI Phosphorus: Total as P. mg/I mg/I MPN method for highly turbid samples) Dissolved Solids: Total 2D«�5 :5,5o mg/I Orthophosphate Al mg/I PH (when analyzed) Y ) units -'Aluminum Ba - Barium mg/I lily 4�S n �5 mg/I Ca - CalciumlL , ; oS m /l. I mg/I Chloride qj&e c5 Arsenic r� mg/I Cd - Cadmium mg/I Grease and Oils mg/I mg/I Chromium: Total Cu - Capper mg/I Phenol Sulfate — 3 mg/I Hg - IMercu mg/I mg/I Specific Conductance Total Ammonia uMhos K - Potassium mg/I mg/I TKN as N mg/I Mg -Magnesium I4 Dec 0 I � mg/I — mg/I Mn - Manganese mg/I C. GW-59 Rev.0312000 YES _ NO) Ni - Nickel mg/I Pb - Lead mg/I 7_n -Zinc Ammonia Nitro en g/I Other (Specify C mpounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC r�«a uvrr (Specify test and method S. Attach lab report.) Report Attached? Yes ✓(1) No _ (0) VOC method#= EP12 6Q07 method 9 = method It = NU int or I-Z_I-61/3 GW-59A COMPLIANCE REPORT FORM Permit # Coo Sao 3 (Submit one each monitoring period WhI, G V-59 jorms.) iv'Cc�ce �tz3 1 Enter date monitoring results were due. (7)sc c g ) WIII thi be. submitted after the established due date? s mentonng report (GIN-59 and GIN-59A) YES NO 2 Was any required information missing on [he CW-59 report forms? - V� YES NO IF the answer! question 1 or 2 is "YES'; list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing c identification plate, area overgrown, etc.)? Ythe mrswer is •'Yes", missingp, missing YES NO cartact the V 4 Are any monitored constituents equal to or above the established s±andards? - If the answer to question 4 is NO", skip to section 8. YES NO If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s), exceeding standards in the space provided below. 5 For the constituents identified in question 4 above, have standards been exceeded previously for the same constituent(s) in the same well(s) in the last two years? YES NO If the answer to question 5 is NO'; skip to section 8. if the answer to question 5 is "YES'; list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). 6 Are the monitoring wells listed in section S located at or beyond the review boundary? i YES NO If the answer is "YES" a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFF/CEIMMEDiATELYFOR GUIDANCE. If the `NO'; answer is monitoring wells maybe improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this groundwater quality problem? YES NO If the answer to question, 7 is 'YES ; descrbe Lyose actions in the space provided below. If the answer to question 7 is `NO", contact the Regional Office within 90 days- an evaluation may be required todetermine the impact the waste dfSpQSaI system rs having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation Tines and/or penalties g The person completing this portion (GW-59A) of the monitoring report should sign below and submit thf form with GW-59 forms for required wells to the ? address provided at the top of the current GW-59 form. ' herebyacknowledge�that the above Iriforma±ioh was eva afed aril the infofanation submCtted Inthls - `_+ ' N� m repprt„(CompliariceReport�GW59A);Iszeue nd,completetofite siofm'ykmowledge ,- �,.;�-'.,ro,� W � l- Zl-D6 DO N Sigri'tureW permittee(or Authorized ) Date o - to G«`-59A ra/sI?nnst i n n Environmental Testing Solutions, Inc. PO Box 7565 Phone: (828) 350-9364 Asheville, NC 28802 Fax: (828) 350-9368 Certificate of Analysis Results: Sample identification: MW #12 Sample number: 28940 Parameters Meinod Result 1VID'L 'Units Date Analys Footnotes Analyzed Solids, Total Dissolved EPA 160.1 390 1.0 ai°-L 9-Dcc-05 AAB Chloride, Total EPA 325.3 57 2.0 mg/L 9-D..-os AAB Sulfate, Total 9056 15 1.0 mg/L 30-NC-05 Mlaadrelh 1 Calcium EPA 200.7 49 0.10 mg/L 14-DeFo5 .vmempbell I Magnesium EPA 200.7 8.6 0.050 mg/L 14-Dcc,05 Mcanpball 1 6230D EPA 6230D See Attached Sheet n-D. --M EmsseE 1 Total Organic Carbon 9060 3.63 1.00 me& n-Dc os MzC 2 Results: Sample identification: b11i' #13 Sa-nple number: 28941 Parameters Method Result MDL Units --" Analyst Footnotes Analyzed Solids, Total Dissolved EPA 160.1 350 1.0 mg/L 9-D�oos AAB Chloride, Total EPA 325.3 29 1.0 mg/L s-D. os AAB - Sulfate, Total 9056 89 10 mg/L 30-Dec-0S M =dmth 1 Calcium EPA 200.7 17 0.10 mg/L 14-Dce05 Mean bell 1 Magnesium EPA 200.7 12 0.050 mg/L 1a-Deo05 Mcampbell 1 6230D EPA 6230D See Attached Sheet n-Ikuos Erasell 1 Total Organic Catbon 9060 3.95 1.00 mg/L 17-D.F05 Idw 2 Results: Sample identification: MW #14 Sample number: 28942 Parameters Method Result MDL Units Analyst Footnotes Analyzed Solids, Total Dissolved EPA 160.1 470 1.0 mg/L 9-i .w AAB Chloride, Total EPA 325.3 10 1.0 mg/L 9-Dcc-Os AAB Sulfate, Total 9056 16 1.0 mg/L 30-NwS W.&eLh I Calcium EPA 200.7 67 0.50 mg/L ie-oe os w ..pbea 1 Magnesium EPA 200.7 41 0.050 mg/L 14-ixc-os Mcaaq.bell 1 6230D EPA 6230D See Attached Sheet 18-1cc-05 E.assen I Total Organic Carbon 9060 5.64 1.00 mg/L 17-> e.os Mac 2 Footnotes: 1. Analyzed by Prism Laboratories, Inc. 2. Pnsm subcontracted to Test America, Inc. 7 NC CertificatioaNumber. 600 NC Drinking Water Certification Number. 37786 0 Environmental Testing Solutions, Inc PO Box 7565 Phone: (828) 350-9364 Asheville, INC 28802 Fax: (828) 350-9368 Certificate of Analysis Project name: Coats American Collection date: 8-Dec-05 Date received: 8-Dec-05 Results: Sample identification: NIW #2 Project number: 051208.511 Sample number: 28937 Parameters Method Result MDL Units I.. Analyst Footnotes Analyzed Solids, Total Dissolved EPA 160.1 100 1.0 mg/L 9-mw5 AAB Chloride, Total EPA 325.3 6.5 1.0 mg/L 9- b,o5 AAB Sulfate, Total 9056 14 1.0 mg/L 30-Rc-05 Mleadreth 1 Calcium EPA 6010B 18 0.10 mg/L 14-Dee-e5 Mcampben 1 Magnesium EPA 6010B 9.2 0.050 mg/L 14-Dcc-05 Mee.r ll I 6230D EPA 6230D See Attached Sheet 17-Dews Emesell 1 Total Organic Carbon 9060 5.31 1.00 mg/L 19-Deoos MLc 2 Results: Sample identification: MW #10 Sample number: 28938 Parameters Method Result MDL Units heed Analyst Footnotes An Y Solids, Total Dissolved EPA 160.1 140 1.0 mg/L 9-Dew5 AAB Cldoade, Toral EPA 325.3 3.5 1.0 mg/L 9-news AAB Sulfate, Total 9056 32 10 mg/L 3o-Dee-os Mleadreth 1 Calcium EPA 6010B 11 0.10 mg/L 14-ixF05 Mcampbell 1 Magnesium EPA 6010B 2.9 0.050 mg/L 14-Ixoas mc,cp It 1 6230D EPA 6230D See Attached. Sheet n-Dee-os Ern. sell 1 Total Orgame Carbon 9060 5.62 1.00 mg/1. 17-Dee-os Nac 2 Results: Sample identiiacatfmh: M V #i1 Sample number: 28939 I Parameters Method Result MDL Units Date Analyst Footnotes Analyzed Solids, Total Dissolved EPA 160.1 310 1.0 mg/L 9-Dec-os AAB , Chloride, Total EPA 325.3 12 1.0 mg/L 9-Dec-os AAB Sulfate, Total 9056 140 10 mg/L 4-raa-os ,needc�f 1 Calcium EPA 6010B 9.0 0.10 mg/L t4-Dcc-as Mcaapbdi 1 Magnesium EPA 6010B 4.9 0.050 mg/L 14-D< 05 Mcampbell 1 6230D EPA 6230D See Attached Sheet 17-De.05 Eraseell 1 S Total Organic Carbon 9060 1.87 1.00 mg/L n-Dee-os imc 2 ID CO ,t8 C W 7 N s NC CefificationNumber. 600 NCD 'moag Water CertificatonNumber. 37786 NC Certification No. 402 SC Certification No. 99012 .ALMS- NC Drinking Water Cart. No. 37735 F0 Smi MaW.l S.EmLvn,rcnhl UN . Environmental Testing Solutions Project Name: Coat's American MWs Attn: Kelley Keenan Project ID: GW Samples PO Box 7565 Sample Matrix: Water Asheville, NC 28802 Laboratory Report 01/06/06 Client Sample ID �_#2,_..J Prism Sample ID: 1367761 COC Group: G1205263___ Time Collected-- 12/08/05 7:00 1 Time Submitted:-12/09/05 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Aromatic and Halogenated Volatiles by GC/PID-ELCD 1,1,1,2-Tetmchlorcethane BRL pg/L 1,1,1-Tdchloroethane BRL pg1L 1,1,2,2-Tetrachloroethane BRL pg/L 1,1,2 Trichlorcethane BRL pg/L 1,1-Dichloroethane BRL pg/L 1,1-Dichloroethene BRL pg/L 1,1-Dlchloropmpane BRL pg/L 1,2,3-Trichlombenzene BRL pg/L 1,2,3-Trichicroprop2ne BRL pg/L 1,2,4-Tdchlorobenzene BRL pg/L 1,2,4-Trimethyibenzene BRL pg/L 1,2-Dibromo3chlorcpropane BRL pg/L 1,2-Dibromoethane (EDB) BRL pg/L 1,2-Dlchlorobenzene BRL pg/L 1,2-Dichloroethane BRL pg/L 1,2-Dichloropropane BRL pg/L 1.3,5-Tdmethylbenzene BRL pg/L 1,3-DIeWorobenzene BRL pg/L 1,3-Dichloropmpane BRL pg/L 1,4-Dichlorobenzene BRL pg/L 2,2-Dichloropropane BRL pg/L 2-Chlorotoluene BRL pg/L 4-Chlorotaluene BRL pg/L Benzene BRL pg/L Bromobenzene BRL pg/L Bmmochlorcmethane BRL pg/L 13mmadichloromethane BRL pg/L 0.50 0.17 1 6230D 12/17/05 19:58 erussell Q11207 0.50 0.080 1 6230D 12/17/05 19:58 erussell Q11207 0.50 0.11 1 62300 12/17/05 19:58 erussell Q11207 0.50 0.080 1 6230D 12/17105 19:58 erussell Q11207 0.50 0.11 1 6230D 12/17/05 19:58 erussell Q11207 0.50 0.13 1 6230D 12117MS 10:56 erussell Q11207 0.50 0.090 1 6230D 12/17/05 19:58 emssell Q11207 0.50 0.12 1 6230D 12/17/06 19:58 erussell Q11207 0.50 0.11 1 6230D 12/17/05 19:58 'enlssell Q11207 0.50 0.040 1 6233D 12/17/05 19:58 erussell 011207 0.50 0.10 1 62300 12/17/05 19:58 erussell Q11207 0.50. 0.14 1 6230D 12/17/05 19:58 eruwell Q11207 0.50 0.12 1 6230D 12/17/05 19:58 erussell Q11207 0.50 0.12 1 6230D 12/17/05 19:58 erussell Q11207 0.50 0.070 1 62300 12/17/05 19:58 erussell I Q11207 - 0.50 0.12 1 6230D 12/17/05 19:58. erussell Q11207 0.50 0.10 'I 6230D 12f17/05 19:58' ennmli Q11207 0.50 0.050 1 62300 12117/05 19:58 erussell Q11207 0.50 0.070 1 6230D 12/17/05 19:58 erussell 011207 0.50 0.060 1 6230D 12/17/05 19:58 er=ell Q11207 0.50 0.13 1 6230D 12/17/05 19:58 erussell Q11207 0.50 021 1 6230D 12/17/05 19:58 erussell Q11207 0.50 0.090 1 62300 12/17/05 19:58 ermsell Q11207 0.60 0.060 1 6230D 12/17/05 19:58 enuse0 Q11207 0.50 0.13 1 6230D 12117/05 19:58 erussell Q11207 0.50 0.090 1 6230D 12/17/05 19:58 erussell Q11207 0.50 0.090 1 6230D 12/17/05 19:58 erussell Q11207' This report should not be reproduced, except in Itsentirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: "00/529-6364 - Fax: 7041625-MS Page 1 of 24 NC Certification No. 402 SC Certification No. 99012 M NC Drinking Water Cart. No. 37735 Full e.M.M d.l SEmvervnenW eolullmu Environmental Testing Solutions Project Name: Coat's American MWs Attn: Kelley Keenan Project ID: GWSamples PO Box7565 Sample Matrix: Water Asheville, NC 28802 Laboratory Report 01/06/06 Client Sample ID: MW #2 Prism Sample ID: 136776 CDC Group: G1205263 Time Collected: 12/08/05 7:00 Time Submitted: 12/09/0� 12:00 Parameter Result Units Report MDL Limit Dilution Factor Method Analysis Analyst Date/Time Batch ID Bromolorm BRL pg/L 0.50 0.050 1 62300 12/17/05 19:58 erussell Q11207 Bromomethane BRL pglL 0.50 0.27 1 6230D 12/17/05 19:58 emssell 011207 Carbon Tetrachloride BRL p91L 0.50 0.060 1 6230D 12/17/05 19:58 erussell Q11207 Chlorobenzene BRL pg/L 0.50 0.17 1 6230D 12/17/05 19:58 erussell Q11207 Chloroethane BRL pg/L 0.50 0.41 1 6230D 12/17/05 19:58 erussell Q11207 Chloroform 4.3 pg/L 0.50 0.060 1 6230D 12/17/05 19:58 erussell Q11207 Chloromethane BRL pg/L 0.50 0.14 1 6230D 12/17/05 19:58 emssell Q11207 cis-1,2-Dichlcmethene BRL pglL 0.50 0.13 1 6230D 12/17/05 19:58 erussell Q11207 cis-1,3-Dichloropropene BRL pg/L 0.50 0.14 1 6230D 12/17/05 19:58 emssell Q11207 Dibromochloromethane BRL pg/L 0.50 0.080 1 62300 12/17/05 19:58 erussell Q11207 Dibromomethane BRL pg/L 0.50 0.13 1 62300 12/17/05 19:58 ewssell Q11207 Dichlorodiflucromethane BRL pglL 0.50 0.14 1 6230D 12/17/06 19:58 erussell Q11207 Ethylbenzene BRL pg/L 0.50 0.16 1 6230D 12/17/05 19:58 emu ll Q11207 Hexachlorobutadiene BRL pg/L 0.50 0.17 1 6230D 12/17/05 19:58 erussell Q11207 Isopropyl ether(IPE) BRL pg/L 0.50 0.24 1 6230D 12/17/05 19:58 erussell Q11207 Isopropylbenzene BRL pg/L 0.50 0.10 1 62300 12/17/05 19:58 emssell Q11207 m,p-Xylenes BRL pg/L 1.0 0.43 1 6230D 12h V05 19:58 erussell Q11207 Methyl t-butyl ether(MTBE) BRL pg/L 0.50 0.14 1 6230D 12/17/05 19:58 erussell Q11207 Methylene chloride BRL pg/L 2.0 0.75 1 6230D 12/17/05 19:58 erussell Q11207 n-Butylbenzene BRL pg/L 0.50 0.19 1 6230D 12/17/05 19:58 erussell Q11207 n-Propylbenzene BRL pg/L 0.50 0.10 1 6230D 12/17/06 19:58 erussell 011207 Naphthalene BRL pg/L 0.50 0.10 1 6230D 12/17/05 19:58 erussell Q11207 c-Xylene BRL pg/L 0.50 0.16 1 62300 12/17/05 19:58 erussell Q11207 p-Isopropyltoluene BRL pg/L 0.50 0.17 1 6230D 12/17/05 19:58 erussell Q11207 sec-Butylbenzene BRL pg/L 0.50 0.12 '1 6230D 12/17/05 19:58 erussell i Q11207 Styrene BRL pg/L 0.50 0.050 1 6230D 12/17/05 19:58 enassell I Q11207 tert-Butylbenzene BRL pg/L 0.50 0.13 1 6230D 12/17/05 19:58 erussell Q11207 Tetrachloroethene BRL pgrL 0.50 - 0.11 1 6230D 12117/05 19:58 enussell Q11207 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbruok Road - P.O. Box 240M - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number:1-800/529.63" - Fax: 7041525-0409 Page 2 of24 NC Certification No. 402 i Laboratory Report LMS SC Certification No. 99012 NC Drinking Water Cert. No. 37735 01/06/06 WO Smlm AndY9.1 b Eovleonmwfal 8.10 m ' Environmental Testing Solutions Project Name: CoaCs American MWs Client Sample ID: MW #2 Attn: Kelley Keenan Project ID: GW Samples Prism Sample ID: 136776 PO Box 7565 Sample Matrix: Water COG Group: G1205283 Asheville, NC 28802 Time Collected: 12/08/05 7:00 Time Submitted: 12/09/05 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Datelrime Batch ID Toluene BRL pg/L 0.50 0.11 1 6230D 12/17/05 19:58 erassell Q11207 transd,2-Dfohloroethene BRL pg/L 0.50 0.27 1 6230D 12/17/05 19:58 enm;ell Q11207 trans-1,3-Dichloropropens BRL pg/L 0.50 0.070 1 6230D 12/17/05 19:58 emwell Q11207 Tdchloroethene BRL pg/L 0.50 0.10 1 6230D 12/17/05 19:58 emssell Q11207 I Tichloroflucromethane BRL pg'L 0.50 0.19 1 6230D 1Zm 17/05 19:58 essell 011207 Vinyl chloride BRL pg/L 0.50 0.24 1 6230D 12/17105 19:58 enusell Q11207 Surrogate % Recovery Control Limits Bromochlarobenzene-ELCD 95 60-144 1,4-Difluornbenzene-PID 104 50-141 Metals by TOP Calcium Magnesfum Sample Preparation: Sulfate by Ion Chromatonranhv Sulfate 18 mg/L . 0.10 0,027 1 6010B 12/14/05 19:50 mcampbell 011119 9.2 mg/L 0.050 0.0054 1 6010B 12114105 19:50 mrampbell' Q11119 50 mL / 50 mL 3010A 12114/05 6:15 cnguyen P14177 14 mg/L 1.0 0.095 1 9056 12130105 15:22 mlandreth i Q11530 Total Oraanlc Carbon Subcontract Report See attached 1 See Attached • Analysis Note for Subcontract Report: Subcontracted to SC certified laboratory rD 387. This report should not be reproduced, except In Its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O..Box240543 - Charlotte, NO 28224-0543 Phone: 704/529-6364 -.To]] Free Number: 1-a88j529.6384 - Fax: m525-048s Page 3.of 24 NC CerOfimlion No. 402 I 1 Laboratory Report SC Certification No. 99012 _ NC Drinking Water Cerl. No. 37735 01/06/06 Full S.M. M*ftal i Emlrvnm ers>t S.n Environmental Testing Solutions Project Name: Coat's American MWs Client Sample ID: MW #2 Attn: Kelley Keenan _ Project ID: GW Samples Prism Sample ID: 136776 PO Box 7565 Sample Matrix: Water COC Group: G1205263 Asheville, NC 28802 Time Collected: 12/08/05 7:00 Time Submitted: 12/09/05 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Sample Comment(s): This report is a revision and supercedes our original report dated 12/28/05. BRL = Below Reporting Limit J = Estimated value between the Reporting Limit and the MDL The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than NELAC certification except for those instances indicated in the case narrative and/or test comments. Angela D. Overcash, V.P. Laboratory Services This report should not be reproduced, except In its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0543 - Phone: 7041529-6364 - Toll Free Number. 1-8001629-6364 - Fax: 7041525-0409 Page 4 of 24 NC Codification No. 402 SC Certification No. 99012 Laboratory Report NC Drinking Water Cert. No. 37735 01/06/06 wu s.,,,e. a,eryua a snvw,wm,w sanm=r.. _ Environmental Testing Solutions Project Name: Coafs American MWs Client Sample ID:`MW,,#10. i Attn: Kelley Keenan Project ID: GW Samples Prism Sample ID: 936777 PO Box 7565 Sample Matrix: Water COC Group: G4205263..-, Asheville, NC 28802 Time Collected: /'17 8105 =7:30 .�----- Time Submitted: '---12/09/05 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DateMme I❑ Aromatic and Halogenated Volatiles by GC/PID-ELCD 1,1,1,2-Tetrachloroethane BRL Pg/L 0.50 0.17 1 6230D 12/17/05 20:49 erussell' Q11207 1,1,1-Trichleroethane BRL pg/L 0.50 0.080 1 6230D 12/17/05 20:49 ewu ll Q11207 1,1,2.2-Tetrachloroethane BRL Pg/L 0.50 0.11 - 1 62300 12/17/05 20:49 emsvll Q11207 1,1,2-Tdchloroethane BRL Pg/L 0.50 0.080 1 6230D 12117/05 20:49 em=dl Q11207 1,1-0ichiomethane BRL PgIL 0.50 0.11 1 6230D 12117/05 20:49 erussell 011207 1,1-1)ichloroethene BRL PULL 0.50 0.13 1 623CD 12/17/05 20:49 emssell Q11207 1,1-Dichloropropene BRL .Pg/L 0.50 0.090 1 6230D 12/17/05 20:49 emssell Q11207 1,2.3-Trichlorobenzene BRL pg/L 0.50 0.12 1 6230D 12/17/05 20:49 erussell Q11207 1,2,3-Tdchloropropane BRL Pg/L 0.50 0.11 • 1 6230D 12/17/05 20:49 emssel! 011207 1,2A.Trichlorobenzene BRL pg/L 0.50 0.040 1 6230D 12117/05, 20:49 emssell Q11207 1,2,4-Tdmethyibenzene BRL pg/L o.50 0.10 1 62300 12/17/05 20:49 er s ell Q11207 1,2-01bromo3-chloropropane BRL pg/L 0.50 0.14 1 6230D 12/17/05 20:49 emssell Q11207 1,2-Dibromoethane (EDB) BRL Pg/L 0.50 0.12 1 62300 12/17/05 20:49 erussell Q11207 1.2-Dichiorobenzene BRL PgIL 0.50 0.12 1 6230D 12/17/05 20:49 erussell Q11207 1,2-Dichloroethane BRL pg/L 0.50 0.070 1 6230D 12/17/05 20:49 emssell Q11207 1,2-Dlchloropropane BRL Pg/L 0.50 0.12 1 6230D 12M7/05 20:49 erussell Q11207 1,3,5-Trnethylbenzena ERL pgP 0.50 0.10 1 6230D 12/17/05 20:49 emssell Q11207 1,3-Dichlorobenzene BRL PgIL 0.50 0,050 1 6230D 12/17/05 20:49 emssell Q11207 1,3-Dichloropropane BRL pg/L 0.50 0.070 1 6230D 12/17/05 20:49 emsmIl Q11207 1,4-Dichlorobenzens BRL Pg/L 0.50 0.060 1 6230D 12/17/05 20:49 emssell Q11207 2,2-131chloropmpane BRL pg/L 0.50 0.13 1 6230D 12M 7105 20:49 emssell Q11207 2-Chlorotoluene BRL pg/L 0.50 021 1 6230D 12/17/05 20:49 emssell Q11207 4-Chlorotoluene BRL pg/L 0.50 0.090 .1 62300 12/17/05 20:49 enj sdl Q11207 Benzene BRL Pg/L 0.50 0.060 1 6230D 12/17/05 20:49 erussell 1 Ql1207 Brcmobenzene BRL Pg/L 0.50 0.13 1 6230D 12/17/05 20:49 emssell Q11207 Bromochloromethane BRL pg/L 0.50 0.090 1 6230D 12/17/05 20:49 erussell Q11207 Bromedichloromethane BRL Pg/L 0-50 0.090 1 6230D .12117105 20t49 erussell Q11207 Bromoform BRL Pg/L 0.50 0.050 1 6230D 12/17/05 20:49 erussell Q11207 This report should not be reproduced• except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 5 of 24 402 NC Certification No990Laboratory SC Certification No. 99032 NC Drinking Water Cart No. 37735 A Fu11 ft,k Ana,BF 'momm315oA,liao Environmental Testing Solutions Project Name: Coat's American MWs Attn: Kelley Keenan Project fD: GIN Samples PO Box 7665 Sample Matrix: Water Asheville, NC 28802 Report 01/06/06 Client Sample ID: MW #10 Prism Sample ID: 136777 COC Group: G1205263 Time Collected: 12/08/05' 7:30 Time Submitted: I=9105 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Datelrime ID Bromomethane SRL Pg/L 0.50 0.27 1 6230D 12117105 20:49 emssell Q11207 Carbon Tetrachloride BRL Pg/L 0.50 0.060 1 6230D 12/17/05 20:49 emssell Q11207 Chlorcbenzene BRL Pg/L 0.50 0.17 1 6230D 12/17/06 20:49 emssell Q11207 Chloroethane BRL pg/L 0.50 0.41 1 6230D 12/17/05 20:49 erussell Q11207 Chloroform BRL pg/L 0.50 0.060 1_ 62301) 12/17/05 20:49 ews l •011207 Chloromethane BRL Pg/L 0.50 0.14 1 6230D 12/17/05 20:49 emssell Q11207 cis-1,2-Dfchloroethene BRL pg/L 0.50 0:13 1 6230D 12/17/05 20A9 emssell Q11207 cis-1,3-Dichloropropene BRL pg/L 0.50 0.14 1 6230D 12/17/05 20.49 emssell Q11207 Dibromochlommethane _ BRL P91L 0.50 0.080 1 6230D 12117105 20:49 emssell Q11207 Dibromomethane ` BRL Pg/L 0.50 0.13 1 6230D 12/17/05 20:49 erussell Q11207 DichlorodiFluoromethane BRL pg/L 0.50 0.14 1 6230D 12117/05 20A9 emsse0 Q11207 Ethylbenzena BRL Pg/L 0.50 0.16 1 6230D 12117/05 20:49 emssell Q11207 Hexachlorobutadiene BRL pg/L 0.50 0.17 1 6230D 12/17/05 20-49 erussell Q11207 Isopropyl ether(IPE) BRL Pg/L 0.60 0.24 1 6230D 12117105 20:49 emsse0 011207_ Isopropylbenzene BRL pg/L 0.50 0.10 1 6230D 12/17/05 20:49 emssell Q11207 m,p-Xylenes BRL Pg/L 1.0 0.43 1 6230D 12/17/05 20:49 erussell Q11207 Methyl t-butyl ether (MTBE) BRL Pg(L 0.50 0.14 1 6230D 12/17/05 20:49 erusseii ,Q11207 Methylene chloride BRL pg/L 2.0 0.75 1 6230D i2/37i05 20:49 erus di Q11207 n-Butylbenzene BRL Pg/L 0.50 0.19 1 6230D 12/17/05 20:49 erusselt Q11207 n-Propylbenzene BRL Pg/L 0.50 0.10 1 6230D 12117105 20:49 emssell Q11207 Naphthalene BRL Pg/L. 0.50 0.10 1 6230D 12/17/05 20:49 erussell Q11207 a-Xylene BRL yg/L 0.50 0.16 1 6230D 12/17/05 20:49 erussell Q11207 p-Isopropyltoluene BRL Pg/L 0.50 0.17 1 6230D 12/17/05 20.49 erussell Q11207 sec-Butylbenzene BRL pglL 0.50 0.12 1 6230D 12/17/05 20:49 erussell Q11207 Styrene BRL pg1L Mo 0.050 1 6230D 12/17/05 20:49 emssell Q11207 tart-Butylbenzene BRL Pg/L 0.50 0.13 1 6230D 12/17/05 20:49 emssell Q11207 Tetrachlorcethene BRL Pg/L 0.50 0.11 1 6230D 12/17/05 20:49 emssell Q11207 Toluene BRL Pg/L 0.50 0.11 1 �` 62300 12/17/05 20:49 emssell Q11207 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 704/529.6364 - Toll Free Number: 1.8001529-6364 - Fax: 7041525-0409 Page 6 of 24 i NC Certification No. 402 � �/ `^s - SC CertiOcaL'en LaboratoReport No. 99012 • dl S� - NC Drinking Water Cert No. 37735 01/06/06 FUY 4ents fwlyec e18 frn'veno,enld SduUam Environmental Testing Solutions Project Name: Coat's American MWs Client Sample ID: MW #10; Attn: Kelley Keenan Project ID: GW Samples Prism Sample ID: 136777 PO Box 7665 Sample Matrix: Water COC Group: G1205263 Asheville, NC 28802 Time Collected: 12/08/05! 7:30 Time Submitted: 12/09105, 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID bans-1;2-Dichloroethene BRL lig/L 0.50 0.27 1 6230D 12/17/05 20.49 emssell Q11207 trans-1,3-Dichloropropene BRL lig/L 0.50 0.070 1 6230D 12/17/05 20:49 emssell ' Q11207 Trichloroethene BRL Pg/L 0.50 0.10 1 6230D 12/17/05 20:49 emssell Q11207 , Trichlorofluoromethane BRL Pg/L 0.50 0.19 1 6230D 12/17/05 20r49 emssell Q11207 Vinyl chloride BRL* Pg/L 0.50 0.24 1 6230D 12l17105 20:49 emssell Q11207 Surrogate %Recovery Control Limits Bromochlorobenzene-ELCO 1,4-Difluorobenzene-PID 92 97 i 60-144 ; 50 - 141 Metals by ICP Calcium 11 mglL 0.10 0.027 1 6010B 12/14/05 19:57 mcampbell Q11119 Magnesium 2.9 mgA 0.050 0.0054 1 60108 12/14l05 19:57 mcampbe➢ g11119 Sample Preparation: 50 mL / 50 mL 3010A 12/14/05 6:15 cnguyen P14177 Sulfate by Ion Chromatooranhv Sulfate 32 mg/L 10 0.95 10 9056 12/30/05 15:41 mlandreth' I Q11530 Total Organic Carbon Subcontract Report See attached 1 See Attached i + Analysis Nate for Subcontract Report: subcontracted to SC certified laboratory ID 387. I I I I This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. ! 449 Springbrook Road -P.O. Box 240543 -Charlotte, NC 28224-0643 Phone: 7041529-6364 - Tell Free Number: 1-3001529-6364 - Fax: 7641525-0409 Page 7 of 24 NC Certification No. 402 SC Certification No. 99012 NC Drinking Water Cert. No. 37735 FWrservkeAmMdra� a EmlmommdtSauCoeu Environmental Testing Solutions Project Name: Coat's American MWs Attn: Kelley Keenan Project ID: GW Samples PO Box 7565 Sample Matrix: Water Asheville, NC 28802 Parameter Laboratory! Report 1 01/06/06 Client Sample ID: MW #101 Prism Sample ID: 136777 CDC Group: G1205263 Time Collected: 12/08/051 7:30 Time Submitted: 12109/05' 12:00 Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Dateffime ID Sample Commengs): This report Is a revision and supercedes our original report dated 12128/05. BRL = Below Reporting Limit J = Estimated value between the Reporting Limit and the MDL The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than NELAC certification except for thoseinstances indicated in the case narrative and/or test comments. t Angela D. Overcash, V.P. Laboratory Services This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 - Toll Free Number: 1-8001629-6354 - Fax: 7041525-0409 Page 8 of 24 i NC Certification No. 402 SC Certification No. 99012 - NC Drinking Water CerL No. 37735 Foil ServceavMna&ErzrimnmuMi'wY Nma Environmental Testing Solutions Project Name: Coat's American MWs Attn: Kelley Keenan Project ID: GW Samples PO Box 7565 Sample Matrix: Water Asheville, NC 28802 i i Laboratory; Report 01/06/06 Client Sample Prism Sample COG Group: Time Collected Time Submittei A Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Aromatic and Halogenated Vola6les by GCIPID•ELCD 1, 1,12-Tetrachloroethane BRL pg/L 0.50 0.17 1 6230D 12/17/05 21:40 eruesell Q11207 1,1,1-Trichlomethane BRL pg/L ozo 0.080 1 6230D 12/17/05 21:40 erussell Q11207 1,1,2,2-Tetrachioroethane". BRL pg/L 0.50 0.11 1 6230D 12/17/05 21:40 erusse7 Q11207 1,1,2-Tdchloroethane. BRL pg/L 0.50 0.080 1 6230D I 12/17/05 21:40 encase] Q11207 10-Dichloroethane BRL pg/L 0.50 0.11 1 62300 12/17/05 21:40 erusse0 Q11207 1,1-Dichloroethene BRL pg/L 0.50 0.13 1 62300 12/17/05 21:40 erussell I Q11207 1,1-Dichlcropropene BRL pg/L 0.50 0.090 1 62300 12/17/05 21:40 erussell Q11207 1,2,3-Trichlorobemene BRL pg/L 0.50 0.12 1 6230D 12/17/05 21:40 erussell Q11207 1,2,3-Trichloropropane BRL pg/L 0.50 0.11 1 6230D 12/17/05 21:40 er s ell Q11207 1,2,4-Trfchlcrobenzene BRL pg/L 0.50 0.040 1 6230D 12/17/05 21:40 erussell Q11207 1,2,4-Trfinethylbenzene BRL pg/L 0.50 0.10 1 6230D 12/17/05 21:40 erusseil Q11207 1,2-Dlbromo-3-chloropropane BRL pg/L 0.50 0.14 1 6230D 12/17/05 21:40 erussell i Q11207 1,2-Dibromoethane (EDB) BRL pg/L 0.50 0.12 1 6230D 12/17105 21:40 erussell Q11207 1,2-Dichlorobenzene BRL pg/L 0.50 0.12 1 6230D 12/17/05 21:40 amwell Q11207 1,2-Dichloroethane BRL pg/L 0.50 0.070 1 6230D 12/17/05 21:40 erussetl Q11207 1,2-Dichicropropane BRL pg/L 0.50 0.12 1 623CD 12117/05 21:40 erussell Q+, 1207 1,3,5-Trimethylbenzene BRL pg/L 0.50 0.10 16230D 12/17105 21.40 erussell Q11207 1,3-Dichiorobenzene BRL pg/L 0.50 0.050 1 6230D 12/17/05 21:40 erussell Q11207 1,3-Dichloropmpane BRL pg/L 0.50 0.070 1 62300 12/17/05 21:40 erussell 1 Q11207 1,4-Dlchlorobenzene BRL pg/L 0.50 0.060 1 6230D 12/17/05 21:40 erussell Q11207 2,2-Olchlorapropane BRL pg/L 0.50 0.13 1 6230D 12/17/05 21.40 erussell I Q11207 2-Chlorotoluene BRL pg/L 0.50 021 1 6230D 12/17/05 21:40 erussell I Q11207 ,4-Chlomtoluene BRL' pg/L 0.50 0.090 1 62300 12/17/05 21:40 erussell i Q11207 Benzene BRL pg/L 0.50 0.060 1 62300 12117105 21:40 erussell Q11207 Bromobenzene BRL pg/L 0.50 0.13 1 6230D 12/17/05 21:40 erussell i g11207 Bromochloromethane BRL pg/L 0.50 0.090 1 6230D 12/17/05 21:40 enrsseii Q11207 Bmmodichioromethane BRL pg/L 0.50 0.090 1 6230D 12/17105 21:40 erussell I Q11207 Bromoform BRL pg/L 0.50 0.050 1 6230D 12/17/05 21'40 missell I g11207 This report should not be reproduced, except In its entirety, without the mitten consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7ON529-6364 - Tall Free Number. 1-800/529-6364 - Fax: 7041525-0409 Page 9 0f 24 NC Certification No. 402 Laboratory Report SC Certification No. 99012 "Ant.-M NO Drinking Water Cart. No.37735 01/06/06 FWl3.ik. mwydm SEmim's w56 d .f Environmental Testing Solutions Project Name: Coats American MWs Client Sample ID: MW #11 Attn: Kelley Keenan Project ID: GW Samples Prism Sample ID: 136778 PO Box 7565 Sample Matrix: Water COC Group: G1205263 Asheville, NC 28802 Time Collected: 12/08/05 8:00 ' Time Submitted: 12/09/06 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Datelfime Batch ID Bramomethane BRL pg/L 0.50 0.27 1 62300 12/17/05 21:40 emssell Q11207 Carbon Tetrachloride BRL pg/L 0.50 0.060 1 62300 12/17/05 21:40 emssell 011207 chicrobenzene BRL pg/L 0.50 0.17 1 6230D 12/17/05 21AU emssell Q11207 Chioroethane BRL pg/L 0.50 0A1 1 62300 12/17/05 21:40 a sen Q11207 Chloroform BRL pg/L 0.50 0.060 11 6230D 12/17/05 21:40 eruasell Q11207 Chlommethane BRL pg/L 0.50 0.14 1 6230D I 12/17/05 21:40 emssell Q11207 cis-1,2-Dichloroethene BRL pg/L 0.60 0.13 1 6230D 12/171 1 Q11207 cis-1,3-Dichloropropene _ BRL pg/L 0.50 0.14 1 6230D 12/17/05 21:40 eru 11 Q11207 Dibromochloromethane BRL pg/L 0.50 0.080 1 6230D 12/17/05 21:40 emssell Q11207 . Dibromomethane BRL ' pg/L ' 0.50 0.13 1 ' 6230D 12/17/05 21:40 erirssell Q11207 Dichlorodi8uorom ethane BRL pg/L 0.50 0.14 1 6230D 12/17/05 21:40 emssell Q11207 Ethylbenzene BRL pg/L 0.50 0.16 1 6230D 12/17/05 21:40 emssell Q11207 Hexachiorobutadlene BRL pg/L 0.50 0.17 1 6230D 12/17/05 21:40 emssell Q11207 Isopropyl ether(IPE) BRL pg/L 0.50 0.24 1 6230D 12/17/05 21:40 emssell Q11207 Isopropylbenzene BRL pg/L 0.50 0.10 1 6230D 12/17/05 21:40 emssell QI1207 m,p-Xylenes BRL pg/L 1.0 0.43 1 6230D 12/17/05 21:40 emssell 011207 Methyl t-butyl ether(MTBE) BRL pg/L 0.50 0.14 1. 6230D 12/17/05 21:40 emssell Q11207 Methylene chloride BRL pg/L 2.0 0.76 1 6230D 12/17105 21:40 emssell Q11207 n-Butylbenzene BRL pg/L 0.50 0.19 1 6230D 12/17/05 21:40 erussell Q11207 n-Propylbenzene BRL pg/L 0.50 0.10 1 6230D 12/17/05 21:40 emssell Q11207 Naphthalene BRL pg/L 0.50 0.10 1 6230D 12117/05 21:40 erussell .Q11207 o-Xylene BRL pg/L 0.50 0.16 1 6230D 12/17/05 21:40 emssell Q11207 p-Isopropyltoluene BRL pg/L 0.50 0.17 1 62300 12/17/05 21:40 errs en Q11207 sec-Butylbenzene BRL pg/L 0.50 0.12 1 5230D 12/17/05 21:40 emssell Ql1207 Styrene BRL pg/L 0.50 0.050 1 6230D 12/17/05 21:40 emssell 011207 tert-Butylbenzene BRL pg1L 0.50 0.13 1 6230D 12/17/05 21:40 emssell Q11207 Tetrachloroethene BRL pg/L 0.50 0.11 1 6230D 12/17/05 21:40 emssell Q11207 Toluene BRL pgfL 0.50 0.11 1 6230D 12/17/05 21:40 emssell Q11207 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. ` 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6384 - Toll Free Number: 1.8001529-6364 - Fax: 7041525-0409 Page 10 of 24 - NC Certification No. 402 SC Certification No. 99012 NC Drinking Water Cert. No. 37735 FUV setvlra MahMcal a Ewlmnme�l SqutlOrti Environmental Testing Solutions Project Name: Coat's American, MWs Attn: Kelley Keenan Project ID: GW Samples PO Box 7565 Sample Matrix: Water . Asheville, NC 28802 Laboratory 'Report 1 01/06/06 Client Sample ID: MW #11 i Prism Sample ID: 136778 COC Group: G1205263 Time Collected: 12/08/05 1 8:00 Time Submitted: 12/09/05 j 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Batch Date/Time ID trans-1,2-Dichloroethene BRL pg/L 0.50 027 1 6230D 12/17/05 21:40 emssell Q11207 trans-1,3-Dichloropropene BRL pg/L 0.50 0.070 1 6230D 12/17/05 21:40 erussell Q11207 Trichloroethene BRL pg/L 0.50 6.10 1 6230D 12/17/05 21:40 emssell 1111207 Trichlorofluoromethane BRL pg/L 0.50 0.19 1 6230D 127i7105 21:40 emssell Q11207 Vinyl chloride BRL pglL 0.50 0.24 1 6230D 12/17/05 21:40 emssell i Q11207 Surrogate %Recovery Coltr0l Limits Bromochlorobenzene-ELCD 94 60-144 1,4-Diflucrobenzene-PID 102 150-141 Metals by ICP Calcium . 9.0 mg/L 0.10 0.027 1 60108 12/14/05 20:14 rn a pbell Q11119 Magnesium 4.9 mg/L 0.060 0.0054 1 6010B 12/14/05 20:14 mcampbell Q11119 Sample Preparation: 50 mL / 50 mL 3010A 12/14/05 6:15 cnguyen . P14177 Sulfate by Ion Chromatooraohv Sulfate 140 , mg/L 10 0.95 10 9056 01/04/06 13:02 mlandreth Q11572 Toiai Organic Carbon Subcontract Report See attached 1 See Attached * Analysis Note for Subcontract Report: Subcontracted to SC certified laboratory ID 387I This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Ina _ 449 Springbrook Road • P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-63" -,Toll Free Number. 1-8001529-6364 - Fax: 7041525-0409 Page 11 of 24 W NC Certification No. 402 SC Certification No. 99012 _..'NO Drinking Water Cert. No. 37735 FW 9enke MairG:dB Enr4vmnnW Sa4sslmo Environmental Testing Solutions Project Name: Coats American MWs Attn: Kelley Keenan Project ID: GW Samples PO Box 7565 Sample Matrix: Water Asheville, NC 28802 Laboratory Report 01/06/06 Client Sample 11): MW ##11 Prism Sample ID: 136778 COC Group: G1206263 Time Collected: 12/08/05 8:00 Time Submitted: 12/09/05 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Datelrime ID Sample Comment(s): This report is a revision and supercedes our original report dated 12128/05. BRL= Below Reporting Limit J = Estimated value between the Reporting Limll and the MDL' The results in this report rate (a only to the samples submitted for anatysls and meet state certfication requiremants other than NELAC certification except for those instances indicated in the case narrative and/or test comments. M Angela D. Overcash, V.P. Laboratory Services This report should not be reproduced, except in its entirety, without the mitten consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NO 28224-0543 Phone: 704/529.6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525.0409 Page 12 of 24 e - o' NO Certification No. 402 Laboratory Report SC Certification No. 99012 ' - NO Drinking Water Cart. No. 37735 01/06/06 FWI ServIrn MWyd.W b Emi -.v S$.e , Environmental Testing Solutions Project Name: Coat's American MWs Client Sample(ID:' MW #12 , Attn: Kelley Keenan Project ID: GW Samples Prism Sample ID: 136779 L-- ` PO Box 7565 Sample Matrix: Water COO Group: � G1205263 Asheville, NO 28802 Time Collected ,112108/05 8:30 . Time Submitted: 12/09%O5 12:00 Parameter Result Units Report MDL Limit Dilution Factor Method Analysis Analyst Date/Time Batch ID Aromatic and Halogenated Volatiles by GCIPID-ELCD 1,1,1,2-Tetrachloroethane BRL pg/L 0.50 0.17 1 6230D 12/17105 22:32 erussell 011207 1,1,1-Trichloroethane BRL pg/L 0.50 0.080 1 6230D 12/17/05 22:32 erussell Q11207 1,1,22-Tetrachloroethane BRL pg/L 0.50 0.11 1 6230D 12/17/05 22:32 erussell Q11207 1,1,2-Trichioroethane BRL pg/L 0.50 0.080 1 6230D 12/17/05 22:32 erussell Q11207 1,1-DIchlomethane BRL pg/L 0.50 0.11 1 6230D 12/17/05 2232 erussell Q11207 1,1-Dichieroethene BRL pg/L 0.50 0.13 1 6230D 12/17/05 22:32 enusell Q11207 1,1-Dlchlompropene _ BRL pg/L 0.50 0.090 1 62300 12/17/05 22:32 erussell Q11207 1,2,3 Trichlorobenzene BRL pg/L 0.50 0.12 1 6230D 12/17/05 22:32 erussell Q11207 1,2,3-Trichloropropane BRL pg/L 0.50 0.11 1 • 6230D 12/17/05 22:32 erussell Q11207 1,2,4-Trichlorobenzene BRL pg/L 0.50 0.040 - 1 6230D 12117/05 22:32 erussell Q11207 1,2,4-Trimethylbenzene BRL pg/L 0.50 0.10 1 6230D i 12/17/05 22:32 erussell Q11207 1,2-Dibromo-3-chieropropane BRL pglL 0.50 0.14 1 6230D 12/17/05 22:32 erussell Q11207 1,2-Dibromoethane(EDB) BRL pg/L 0.50 0.12 1 6230D 12/17/05 22:32 e,usseil Q11207 1,2-Dichlorobenzene BRL pg/L 0.50 0.12 1 6230D 12117/05 22:32 erussen Q11207, 1,2-Dichloroethane BRL pg/L 0.50 0.070 1 6230D 12/17/05 22:32 erussell Q11207 1,2-Dichloropropane BRL PA 0.50 0.12 1 6230D 12/17/05 22:32 erussell Q11207 1,3.5-Trim athyltoarzera BRL pg/L Q50 0.?0 ? 6230D 12/17/05 22:32 erusv_9 Q 112 07 1,3-Dichlorobenzene BRL pg/L 0.50 0.050 1 6230D 12/17/05 22:32 erussell Q11207 1,3-Dichloropropane BRL pg/L 0.50 0.070 1 6230D 12/17/05 22:32 erusse0 Q11207 1,4-Dichlorobenzene BRL pg/L 0.50 0.060 1 6230D 12/17/05 22:32 erussell Q11207 2,2-Dichloropropane BRL pglL 0.50 0.13 1 62300 12117/05 22:32 emwell Q11207 2-Chlorotoluene BRL pg/L 0.50 0.21 1 6230D 12I7105 22:32 enuseli Q11207 4-Chlorotoluene . BRL pg/L 0.50 0.090 1 6230D 12/17/05 22:32 erussell Q11207 Benzene BRL pg/L 0.50 0.060 1 6230D 12N7105 22:32 erussell Q11207 Bromcbenzene BRL pglL 0.50 0.13 1 6230D 12/17/05 22:32 erussell Q11207 Bromochloromethane BRL pg/L 0.50 0.090 1 6230D 12/17/05 22:32 erussell Q11207 Bromodichloromethane BRL pg/L 0.50 0.090 1 6230D 12/17/05 22:32 erussell 011207 Bromoform BRL pg/L 0.50 0.050 1 6230D 12M7105 22:32 emwell Q11207 This report should not be reproduced, except in Us entirety, without the written consent of Prism Laboratories, Inc. ,449 Springbrook Road - P.O. Box 240543 - Charlotte, NO 28224-0543 - Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 13 of 24 NC Certification No. 402 SC Certification No. 99012 NC Drinking Water Cart. No, M35 PoII9mW MYYr�l6 Fm4an,vmtl SaluOev Environmental Testing Solutions Project Name: Coat's American MWs Attn: Kelley Keenan Project ID: GW Samples PO Box 7565 Sample Matrix: Water Asheville, NC 28802 Laboratory Report 01/06/06 Client Sample ID: MW #12 Prism Sample ID: 136779 COC Group: G1205263 Time Collected: 12/08/05 8:30 Time Submitted: 12/09/06 12:00 Parameter Result Units Report Limit MOL 'Dilution Factor Method Analysis Analyst Date/Time Batch ID Bromomethane BRL pg/L 0.60 0.27 1 6230D 12/17/05 22:32 emssell Q11207 Carbon Tetrachloride BRL pg/L 0.50 0.060 1 6230D 12/17/05 22:32 er=ell Q11207 Chlombenzene BRL pg/L 0.50 0.17 1 62300 12/17/05 22:32 emssell 011207 Chloroethane BRL pg/L 0.50 0.41 1 6230D 12/17/05 22:32 emssell Q11207 Chloroform BRL pg/L 0.50 0.060 1 6230D 12/17/05 22:32 emssell Q11207 Chloromethane BRL pg/L 0.50 0.14 1 6230D 12/17/05 22:32 emssell Q11207 cis-1,2-Dichloroethene BRL pg/L 0.50 0.13 1 6230D 12/17/05 22:32 emssell Q11207 cis-1,3-Dichloroprapene BRL pg/L 0.50 0.14 1 6230D 12/17/05 22:32 emssell Q11207 Dibromochlcromethane BRL pgfL 0.50 0.080 1 6230D 12/17/05 22:32 emssell Q11207 • Dibromomethane _ • BRL pg/L 0.50 0.13 1 6230D 12/17/05 22:32 emsse0 Q11207 Dichlorodiflucromethane BRL pg/L 0.50 0.14 1 6230D 12/17/05 22:32 emssell Q11207 Ethylbenzene BRL pg/L 0.60 0.16 1 6230D 12/17/05 22:32 emssell Q11207 Hexachlorobutadiene BRL pg1L 0.50 0.17 1 6230D 12f17/05 22:32 emssell Q11207 Isopropyl ether(IPE) BRL pg/L 0.50 024 1 6230D 12/17/05 22:32 emssell Q11207 Isopropylbenzene BRL pg/L 0.50 0.10 1 6230D 12/17/05 22:32 emssell Q11207 m,p-Xylenes BRL pg/L 1.0 0.43 1 6230D 12/17/05 22:32 emssell Q11207 Methyl t-butyl ether (MTBE) BRL pg/L 0.50 0.14 1 6230D 12/17/05 22:32 emssell Q11207 Methylene chloride BRL p9/1 2.0 0.75 1 6230D 12 I7105 22:32 er=e0 Q11207 n-Butylbenzene BRL pg/L 0.50 0.19 1 6230D 12117/05 22:32 enasell Q11207 n-Propylbenzene BRL pg/L 0.60 0.10 1 6230D 12/17/05 22:32 enasell Q11207 Naphthalene BRL pg/L 0.50 0.10 1 6230D 12/17/05 22:32 emssell Q11207 o-Xylene BRL p91L 0.50 0.16 1 6230D 12/17/05 22:32 emssell Q11207 p-Isopropyltoluene BRL pg/L 0.50 0.17 1 6230D 12/17/05 22:32 emssell Q11207 sec-Butylbenzene BRL pgR 0.50 0.12 1 6230D 12/17/05 22:32 emssell Q11207 Styrene BRL pg/L 0.50 0.050 1 6230D 12117/05 22:32 emsse0 Q11207 left-Butylbenzene BRL pg/L 0.50 0.13 1 6230D 12/17/05 22:32 emsselt Q11207 Tetrachlcroethene BRL pg/L 0.50 0.11 1 6230D 12/17/05 22:32 emssell Q11207 Toluene BRL pg/L 0.50 0.11 1 6230D 12/17/06 22:32 emssell Q11207 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543. Phone: 70415294364 - Toll Free Number: 1-8001529-6364 - Fax: 7041626-0409 Page 14 of 24 44yfNC Certification No. 402 Laboratory Report 01/06/06 nvironmen a e ' stIng 6Mons Project Name: Coafs American MWs Client Sample ID: MW #12 Attn: Kelley Keenan Project ID: GW Samples Prism Sample ID: 136779 PO Box 7565 Sample Matrix: Water CDC Group: G1205263 Asheville, NC 28802 Time Collected: 12/08/05 8:30 Time Submitted: 12/09/05 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Daterrime Batch ID trans-1,2-Dichloroethene BRL Pg/L 0.50 0.27 1 6230D 12/17/05 22:32 erussell 011207 trans-1,3-Dichlorcpropene BRL Pg/L 0.50 0.070 1 6230D 12/17/05 22:32 erussell Q11207 Trichlcroethene BRL Pg/L 0.50 0.10 1 6230D 12/17/05 22:32 erussell' Q11207 Trichiorofluoromethane BRL Pg/L 0.50 0.19 1 6230D 12/17/05 22:32 erussell Q11207 Vinyl chloride BRL Pg/L 0.50 0.24 1 6230D 12/17/05 22:32 erussell Q11207 Metals by ICP Calcium Magnesium Sample Preparation: Sulfate by Ion Cbromatograin Sulfate Surrogate °% Recovery Control Limits Bromochlarobenzene-ELCD 96 60 - 144 14-DiOuarobenzene-PID 103 50 - 141 49 mg/L 0.10 0.027 1 8.6 mg/L 0.050 0.0054 1 50 mL / 50 mL 15 mg/L 1.0 0,095 1 6010B i 12/14/05 20.20 mcampbeft Q11119 6010B 12/14/05 20:20 mcampbell Q11119 3010A 12/14/05 6:15 cnguyen P14177 9058 12/30/05 16:01 mtandrelh Q11530 Total Organic Carbon ' Subcontract Report See attached 1 ' See Attached • Analysis Note for Subcontract Report: Subcontracted to SC certified laboratory ID 387. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number. 1-8001529-6364 - Fax: 7041525-0409 Page 15 of 24 Certification No. 402 SC Certification No. 99012 NC Drinking Water Cert. No. 37735 o4LMINC FWI Ze.I-MWVMA 6 EW.na w5 Wl Environmental Testing Solutions Project Name: Coat's American MWs Attn: Kelley Keenan Project ID: GW Samples PO Box 7565 Sample Matrix: Water Asheville, -NC 28802 Laboratory Report 01/06/06 Client Sample ID: MW #12 Prism Sample ID: 136779 COC Group: G1206263 Time Collected: 12/08/05 8:30 Time Submitted: 12/09/05 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time I ID Sample Comment(s): This report is a revision and supen:edes our original report dated 12128/05. BRL = Below Reporting Limit J = Est/mated value between the Reporting Limit and the MDL The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than NELAC cerffcadon except for those instances ind/cated in the case narrative and/or test comments. M-M Angela D. Overcash, V.P. Laboratory Services This report should not be reproduced, except In its entirety, without the written consent of Prism Laboratories, Ina 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 - — - Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 70415250409 Page 16 of 24. NC Certiiicatlon No. 402 SC Certification No. 99012 NC Drinking Water Ced. No. 37735 Fu05> EEmnmwend4alutlaru- Environmental Testing Solutions Project Name: Coat's American MWs Attn: Kelley Keenan Project ID: GW Samples PO, Box 7565 Sample Matrix: Water Asheville, NC 28802 Laboratory Report 01/06/06 Client Sample ID: 'MW #13 Prism Sample ID: 136780 CDC Group: G_1205263 Time Colle.c.e ,t- -tea te� d =_;. 12/Ofi/O5 9:00. Time Submitted: 12/09/05 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DateTime ID Aroma_tic and Halogenated Volatiles by GC/PID-ELCD 1.1.1.2-Tetraehlomethane BRL Pg/L 0.50 0.17 1 6230D 12117/05 23:23 erussell Q11207 1,1,1-Trichloroethane BRL pg/L 0.50 0.080 1 6230D 12117/06 2323 erossell Q11207 1.1,2.2-Tetrachlomethane BRL Pg/L 0.50 0.11 1 6230D 12/17/05 23.23 erussell Q11207 1,1,2-Trichlorcethane BRL pg/L 0.50 0.080 1 62300 . 12/17/05 23:23 ems ll Q11207 1,1-Dlchloroethane BRL Pg/L 0.50 0.11 1 6230D 12/17/05 23:23 erussell Q11207 . 1,1-Dlchloroethene BRL Pg/L 0.50 0.13 1 6230D 12/17/05 23:23 erossell Q11207 1,1-Dlchieropropene BRL Pg/L 0.50 0.090 1 6230D 12/17/05 23:23 erossell Q11207 1,2,3-Trichlombenzene BRL WE- 0.50 0.12 1 6230D 12/17/05 23:23 erossell Q11207 1,2.3-Trichloropropane BRL . pg/L 0.50 0.11 1 6230D 12/17/05 23:23 erossell Q11207 1.2,4-Trichiorobenzene BRL pglL 0.50 0.040 1 6230D 12(17/05 23:23 enusell ' Q11207 1,2,4-Trimethylbenzene BRL 141- 0.50 0.10 1 6230D 12/17/05 2323 enusetl Q11207 1,2-Dibromo-3- hloropropane BRL Pg/L 0.50 0.14 1 6230D 12/17/05 23:23 erossell Q11207 1.2-Dibromoethane (EDB) BRL Pg/L 0.50 0.12 1 6230D 12/17/05 23:23 erossell Q11207 1,2-Dichlorobenzene BRL P91L 0.50 0.12 1 6230D 12/17/05 2323 erossell Q11207 1,2-Dichlomethane BRL Pg/L 0.50 0.070 1 6230D 12/17/05 23.23 erossell Q11207 1,2-Dichloropropane BRL Pg/L 0.50 0.12 1 6230D 12/17/05 23:23 enusell g11207 1,3,5-Tdmethylbenzare BP.L P5'L 0.50 0.}0 1 62300 12/1?!05 23:23 erossell Q11207 1,3-Dichlorobenzene BRL Pg/L 0.50 0.050 1 6230D 12/17/05 23:23 erusself Q11207 1,3-Dichlaropropane BRL pg/L 0.50 0.070 1 6230D 12/17/05 23:23 erussell I Q11207 1.4-Dichlorobenzene BRL Pg/L 0.50 0.060 1 6230D 12117/05 2323 erossell Q11207 2,2-Dichlaropropane BRL Pg/L 0.50 0.13 1 6230D 12/17/05 23:23 erossell Q11207 2-Chlorotoluene BRL Pg/L 0.50 0.21 1 6230D 12/17/05 23:23 enusefl Q11207 4-Chiomtoluene BRL' Pg/L 0.50 0-090 1 6230D 12117/05 23:23 enasell Q11207 Benzene BRL Pg/L 0.50 0.060 1 6230D 12/17/05 23.23 erossell Q11207 Bromobenzene BRL Pg/L 0.50 0.13 1 6230D 12/17/05 23:23 enrssell Q11207 Bromochlcmmethane BRL pg/L 0.50 0.090 1 6230D 12/17/05 23:23 erossell Q11207 Bromodichloromethane BRL Pg/L 0.50 0.090 1 6230D 12/17/05 23:23 erussell Q11207 Bromoform BRL Pg/L MO 0.050 1 6230D 121M05 23:23 erossell 611207 This report should not be reproduced, except In its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 2405" -Charlotte, NC 28224-0543 _ Phone_ 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax:.7041525-0409 -- Page 17 of 24 - NC Certification No. 402 Laboratory Report - SC Certification No. 99012 y NC Drinking Water Cart. No. 37735 01/06/06 FA S.M.. An ildal1 Em ...lS .l . Environmental Testing Solutions Project Name: Coats American MWs Client Sample ID: MW #13 Attn: Kelley Keenan Project ID: GW Samples Prism Sample ID: 136780 PO Box 7565 Sample Matrix: Water COC Group: G1205263 Asheville, NC28802 Time Collected: 12l08/05 9:00 Time Submitted: 12/09/05 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst DateTme Batch ID Bromomethane BRL pg/L 0.50 0.27 1 6230D 12/17/05 23:23 emssell Q11207 Carbon Tetrachloride BRL pgfL 0.50 0.060 1 6230D 12/17/05 23:23 erussell Q11207 Chlorobenzene BRL Pg/L 0.50 0.17 1 6230D 12/17/05 23:23 ert,.sell Q11207 Chlorcethane BRL pg/L 0.50 OA1 1 6230D 12/17/05 23:23 emssell Q11207 Chloroform BRL pglL 0.60 0.060 1 6230D 12/17/06 23:23 erussell Q41207 Chloromethane BRL Pg/L 0.50 0.14 1 6230D 12/17/05 23:23 erussell Q11207 cis-1,2-Dichloroethene BRL pg/L 0.50 0.13 1 6230D 12/17/05 23:23 emssell Q11207 cis-1,3-Diohloropropene BRL Pg/L 0.50 0.14 1 6230D 12/17/05 23:23 erussell Q11207 Dibromochloromethane BRL Pg/L 0.50 0.080 1 6230D 12/17/05 23:23 emsell Q11207 Dibromomethane • BRL P91L 0.60 0.13 1 6230D 12117105 23:23 emssell Q71207 Dlchloradiflucromethane BRL pg/L 0.50 0.14 1 6230D 12/17/05 23:23 emssell I Q11207 Ethylbenzene BRL Pg/L 0.50 0.16 1 6230D 12/17/05 23:23 emssell 011207 Hexachlarobutadiene BRL pg/L 0.50 0.17 1 6230D 12/17/05 23:23 emssell Q11207 Isopropyl ether ()PE) BRL Pg/L 0.50 0.24 1 6230D 12/17/05 2323 emssell Q11207 Isopropylbenzene BRL Pg/L 0.50 0.10 1 6230D 12/17/05 23:23 emssell Q11207 rn,p-Xylenes BRL Pg/L 1.0 OA3 1 62300 12/17/05 2323 enssell Q11207 Methyl t-butyl ether(MSE) BRL Pg/L 0.50 0.14 1 6230D 12/17/05 23:23 emssell Q11207 Methylene chloride BRL PgPL 2.0 0.75 1 6230D 12/17/05 2323 emssell Q11207 n-Buylbenzene BRL Pg/L 0.50 0.19 1 6230D 12/17/05 23:23 emssell Q71207 n-Propylbenzene BRL Pg1L 0.50 0.10 1 6230D 12/17/05 23:23 emssell Q11207 Naphthalene BRL Va 0.50 0.10 1 6230D 12/17/05 2323 emssell Q11207 o-Xylene BRL P91L 0.50 0.16 1 6230D 12/17/05 2323 emssell Q11207 p4sopropyltoluene BRL Pg/L 0.50 0.17 1 62300 12/17/05 23:23 emssell Q11207- sec-Butylbenzene BRL pg/L 0.50 0.12 1 6230D 12/17/05 23:23 emssell I Q11207 Styrene BRL pg/L 0.50 0.050 1 6230D 12/17/05 23:23 emssell Q11207 lert-Butylbenzene BRL Pg/L 0.50 0.13 1 62300 12/17105 23:23 emssell Q11207 Tetrachlorcethene BRL pg/L 0.50 0.11 1 62300 12/17/05 2323 emssell Q11207 Toluene BRL Pg/L 0.50 0.11 1 6230D 12/17/05 2323 enssen i Q11207 This report should not be reproduced, except in Its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number. 1-8001529-6364 - Fax: 7041526-0409 Page 18. of 24 _ �� 402 NC Certification No.990 SC Certification No. 9012 Laboratory Report NO Drinking Water Cart. No. 37735 01/06106 Full UO a Aaalrtlol B Emfivvmnfal Ufa'= Environmental Testing Solutions Project Name: CoaPs American MWs Client Sample ID: MW #13 Attn: Kelley Keenan Project ID: GW Samples Prism Sample ID: 136780 PO Box 7565 Sample Matrix: Water CDC Group: G1205263 Asheville, NO 28802 Time Collected: 12/08/05 9:00 Time Submitted: 12/09/05 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID trans-1,2-Dichloroethene BRL pg/L 0.50 027 1 6230D 12/17/05 23:23 erussell Q11207 trans-1,3-Dichlcropropene BRL pglL 0.50 0.070 1 6230D 12117/05 23:23 enlssell Q11207 Trichlomethene BRL pg/L 0.50 0.10 1 6230D 12/17/05 23:23 elussell Q11207 Tdchlomfluoromethane BRL pg/L 0.50 0.19 1 6230D 12/17/05 23:23 eru sell Q11207 Vinyl chloride BRL pg/L 0.50 0.24 1 6230D 12/17/05 23:23 erussell Q11207 Surrogate % Recovery Control Limits Bmmochlorobenzene-ELCD 88 60 - 144 IA-Difluorobenzene-PID 95 50-141 Metals by ICP Calcium .17 mglL 0.10 0.027 1 6010B 12/14/05 20:28 mcampbell Q11119 Magnesium 12 mg/L 0.050 0.0054 1 6010B 12/14/05 20:28 mcampbe0 Q11119 Sample Preparation: 50 mL / 50 mL 3010A 12/14/05 6:15 cnguyen P14177 Sulfate by Ion Chromatouraohv .. Sulfate 89 mg/L 10 0.95 10 9056 12/30/05 16:20 mlandreth Q11530 Total Organic Carbon Subcontract Report See attached 1 See Attached * Analysis Note for Subcontract Report: Subcontracted to SC certified laboratory ID 387. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Ina 449 Springbrock Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number. 1-8001529-6364 - Fax: 70415250409 Page 19 of 24 NC Certification No. 402 SC Certification No. 93012 _ffiNC Drinking. Water Cert. No. 37735 FO se� Nita a E. ,.. Ws . Environmental Testing Solutions Project Name: Coat's American MWs Attn: Kelley Keenan Project ID: GW Samples PO Box 7665 Sample Matrix: Water .Asheville, NC 28802 Laboratd; 6 Report 01/06/06 Client Sample ID: MW #131 Prism Sample ID: 1367801 COC Group: G1205263 Time Collected: 12/08/05 9:00 Time Submitted: 12/09/05 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Datefiime ID Sample Comment(s): This report Is a revision and supercedes our original report dated 12128105. BRL = Below Reporting limit J = Estimated value between the Reporting Limit and the MDL i The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than NELAC certification except for those instances Indicated in the case narrative and/or test comments. Angela D. Overcash, V.P. Laboratory Services This report should not be reproduced, except in its entirety, without the written consent of Prism laboratories, Inc.. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6304 - Toll Free Number. 1-800/529.6364 - Fax:.704/525A409 Page 20 of 24 NC Certification No. 402 SC Certification No. 99012 NC Drinking Water Cert. No. 37735 Fu0S .M M.IyEof Sa We., Environmental Testing Solutions Project Name: Coat's American MWs Attn: Kelley Keenan Project ID: GW Samples PO Box 7665 Sample Matrix: Water Asheville, NC28802 Laboratory Report 01/06/06 Client S o e.ID; MW #14' Prism Sample ID: 136781 COC Group_, G1205263 _ Time Collecfddi 12/08/05 9:30 Time Submitted: 12/09/05 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Datelfime ID Aromatic and Halogenated Volatiles by GClPID.ELCD 1,1,1,2-Tetmchlomethane BRL pg/L 0.50 0.17 1 6230D 12/18/05 0:15 en ell Q11207 1,1,1 Trichloreethane BRL Pg/L 0.50 0.080 1 6230D 12/18/05 0:15 erussell Q11207 1,1,2,2-Tetrachlotoethane BRL pg/L 0.50 0.11 1 6230D 12/18/05 0:15 emnell Q11207 1,1,2-Tdchloroethane BRL pg/L 0.50 0.080 1 6230D 12/18/05 0:15 erussell ,Q11207 1,1-Dichloroethane BRL pg/L 0.50 0.11 1 6230D 12/18/05 0:15 emnell Q11207 1,1-Dichioroethene BRL Pg/L 0.50 0.13 1 6230D 12/18/05 0:15 emmeli 011207 1,1-Dlchloropropene BRL pg/L 0.50 0.090 1 6230D 12118/05 0:15 erussell QM07 1,2,3-Trichlorobenzene BRL pg/L 0.50 0.12 1 6230D 12/18/05 0:15 erussell Q11207 1,2,3-Trichloropropane. BRL pg/L 0.50 0.11 1 6230D t2MS= 0:15 enuseu Q11207 1,2,4-Tdchlombenzene BRL pg/L 0.50 0,040 1 6230D 12/18/05 0:15 enasell Q11207 1,2,4-Trimethylbenzene BRL pg/L 0.50 0.10 1 6230D 12/18/05 0:15 enssell Q11207 1,2-Dibromo-3-chloropmpane BRL P91L 0.50 0.14 1 6230D 12/18/05 0:15 enasell Q11207 1,2-Dibromoelhane (EDB) BRL Pg/L 0.50 0.12 1 6230D 12/18/05 0:15 erussell Q11207 1,2-Dlchlorobenzene BRL Pg/L 0.50 0.12 1 6230D 12118/05 0:15 emwell Q11207 1,2-Dichloreethane . BRL pg/L 0.50 0.070 1 6230D 12/18/05 0:15 emsWl Q11207 1,240ichloropropane BRL pg.R. 0.50 0.12 1 6230D 12/18/05 0:15 erussell Q11207 1 3,5-Trlmethylberzene BRL pg(L 0.50 0.10 1 6230D 12/18/06 0:15 erussell *Q11207 1,3-Dichlorobenzene BRL Pg/L 0.50 0.050 1 6230D 12/18/05 0:15 enusell 011207 1,3-Dichloropropane BRL pg/L 0.50 0.070 1 6230D 12118/05 0:15 emssell Q11207 1,4-Dieblorobenzene BRL WE- 0.50 0.060 1 6230D 12/18/05 0:15 erussell Q11207 2,2-Dichloropropane BRL Pg/L 0.50 0.13 1 6230D 12118/05 0:15 er=ell Q11207 2-Chlorotoluene BRL Pg/L 0.50 021 1 6230D 12/18/05 0:15 er 11 Q11207 4-Chlorotoluens BRL pg/L 0.50 0.090 1 6230D 12118/05 0:15 onusell Ql1207 Benzene BRL pg/L 0.50 0.060 1 6230D 12/18/05 0:15 erussell Ql1207 Bromobenzene BRL pg/L 0.50 ' 0.13 1 6230D 12/18/05 0:15 a fl Q11207 Bromochloromethane BRL pg/L 0.50 0.090 1 6230D 12/18/05 0:15 erussell Q11207 Bromodlchloromethane BRL pg/L 0.50 0.090 1 62300 12/18/05 0:15 erussell Q11207 Bromoform BRL pg/L 0.50 0.050 1 6230D 12118/05 0:15 en H Q11207 This report should not be reproduced, except In its entirety, yritheut the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.G. Box 240643 - Charlotte, NC 28224-0643 Phone: 704/529-6364 - Toil Free Number: 1-800/529-6364 - Fax: 7041525-0409 Page 21. of 24 No. - NC Certification 90 12 SC Certification No. 990 NC Drinking Water Cert. No. 37735 M S.ka Matgp 8FnWmmmWSaluUam Environmental Testing Solutions Project Name: Coat's American MWs Attn: Kelley Keenan Project (D: GW Samples PO Box 7565 Sample Matrix: Water Asheville, NC 28802 Laboratory Report 01/06/06 Client Sample ID: MW #14 Prism Sample ID: 136781 COC Group: G1205263 Time Collected: 12/08/05 9:30 Time Submitted: 12/09/05 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Datelfime ID Bromomethane BRL pg/L 0.50 0.27 1 6230D 12/18/05 0:15 emsell' Q11207 Carbon Tetrachloride BRL pg/L 0.50 0.060 1 6230D 12118/050:15 emssell Q11207 Chlombenzene BRL pg/L 0.50 0.17 1 6230D 12/18/05 0:15 erussell Q11207 Chlorcethane BRL pg/L 0.50 0.41 1 6230D 12118/05 0:15 emuell Q11207 ' Chloroform BRL pg/L 0.50 0.060 1 6230D 12/18/05 0:15 e<ussell Q11207 Chlommethane BRL pg/L 0.50 0.14 1 6230D 12118/05 0:15 emssell Q11207 cis-1,2-01chlomethene BRL pg/L 0.50 0.13 1 .6230D 12/18/05 0:15 erus Jl Q11207 cis-1,3-01chlompropene BRL pg/L 0.50 0.14 1 6230D 12/18/05 0:15 eamsell Q11207 Dibromochloromethane BRL pg/L 0.50 0.080 1 6230D 12/18/05 0:15 emwell Q11207 Dibmmomethane ' BRL pg/L 0.50 0.13 1 62300 12/18/05 0:15 erusre0 Q11207 Dlchlomdl0uoromethane BRL pg/L 0.50 0.14 1 6230D 12118/05 0:15 emsssell 011207 Ethylbenzene BRL pg/L 0.50 0.16 1 6230D 12/18/05 0:15 emssell Q11207 Hexachlorobutadiene BRL pg/L 0.50 0.17 1 6230D 12/18/05 0:15 erussell Q11207 Isopropyl ether(IPE) BRL pg/L 0.50 0.24 1 6230D 12118/05 0:15 erussell Q11207 Isopropylbenzene -BRL pg/L 0.50 0.10 1 6230D 12118/05 0:15 eruwall Q11207 m,p-Xylenes BRL pg/L 1.0 0.43 1 6230D 12118/05 0:15 enu c1l Q11207 Methyl t-butyl ether (MTBE) BRL pg/L 0.50 0.14 1 6230D 12/18/05 0:15 erussell 011207 Methylene chlorldo BRL W, 2.0 0.75 1 6230D 12/18/05 0:15 eru5 all Q11207 n-Butylbenzene BRL pg/L 0.50 0.19 1 6230D 12/18/05 0:15 entsse0 Q11207 n-Propylbenzene BRL pg/L 0.50 0.10 1 6230D 12J18/05 0:15 emssell Q11207 Naphthalene BRL pg/L 0.50 0.10 1 6230D 12I8105 0:15 emwell Q11207 o-Xylene BRL pg/L 0.50 0.16 1 6230D 12/18/05 0:15 emssell Q11207 p4sopropyltoluene BRL pg/L 0.50 0.17 1 6230D 12/18/05 0:15 erur ll Q11207 sec-Butylbenzene BRL pg/L 0.50 0.12 1 6230D 12/18/05 0:15 emwell Q11207 Styrene BRL. pg/L 0.50 0.050 1 6230D 12/18/05 0:15 emssell Q11207 tert-Butylbenzene BRL pg/L 0.50 0.13 1 6230D 12tl8105 0:15 erusses Q11207 Tetrachloroethene BRL pg/L 0.50 0.11 1 62306 12118/05 0:15 eruusell Q11207 Toluene BRL pg/L 0.50 0.11 1 6230D 12118/05 0:15 emssell - Q11207 This report should not be reproduced, except in its entirety, w8hout the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543- ' Phone: 704/529-6364 - Tall Free Number. 1-800/529-6364 - .Fax: 704/525-0409 Page 22 of 24 -- _ NC Certification No. 402 SC CerOficaticn No. 99012 990 Laboratory Report ° NC Drinking Water Cert. No. 37735 01/06/06 Fa S eMm M,lyrcal d envrmmeenut sauUvm Environmental Testing Solutions Project Name: CoaPs American MWs Client Sample ID: MW #14 Attn: Kelley Keenan Project ID: GW Samples Prism Sample ID: 136781 . PO Box 7665 Sample Matrix: Water COC Group: G1205263 . Asheville, NC 28802 Time Collected: 12/08/05 9:30 ' Time Submitted: 12/09/05 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis DatetTme Analyst Batch ID trans-1,2-Dichlorcethena BRL pg/L 0.50 0.27 1 6230D 12/18/05 0:15 erussell Q11207 trans-1,3-Dichlcropropene BRL pg/L 0.50 0.070 1 6230D 12/18/05 0:15 emssell Q11207 Tdchloroethene BRL pg/L 0.50 0.10 1 6230D 12/18/05 0:15 emssell Q11207 Tdchloro6uoromethane BRL pg/L 0.50 0.19 1 62300 12/18/05 0:15 erueseli Q11207 Vinyl chloride BRL pg/L 0.50 0.24 1 6230D 12/18/05 0:15 emmen Q11207 Surrogate % Recovery Control Limits Bromochlorcbenzene-ELCD 92 60-144 . 1,4-61Fluoroberaene-PID 103 50-141 Metals by ICP Calcium 67 mg/L 0.50 0.14 5 6010B 12/16/05 17:40 mcampbell Q11119 Magnesium 41 mg/L 0.050 0.0054 1 6010B 12/14/05 20:34 mcampbell Q11119 Sample Preparation: 50 mL / 50 mL 3010A 12/14/05 6:15 cnguyen P14177 Sulfate by Ion Chromatocraohv Sulfate 16 mg/L 1.0 0.095 1 9056 12/30/05 16:40 mlandreth 011530 Total Ortianic Carbon Subcontract Report See attached 1 See Attached * Analysis Note for Subcontract Report: Subcontracted to SC certified laboratory ID 387. This report should not be reproduced, except in Its entirety, without the written consent of Prism Laboratories, Inc 449 Spdngbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number. 1-89tll529.6364 - Fax: 7041525-0409 Page 23 of 24 - CCertiflca990cnNo. S SC Cenlra0flon No. 99012 Laboratory Report NC Drinking Water Cert. No. 37735 01/06/06 rJl9ervke Analgtlpl66nhv,mm W �duVam Environmental Testing Solutions Project Name: CoaVs American MWs Client Sample ID: MW #14 Attn: Kelley Keenan Project ID: GW Samples Prism Sample ID: 136781 PO Box 7565 Sample Matrix: Water CDC Group: G1205263 Asheville, NC 28802 Time Collected: 12/08/05 9:30 r Time Submitted: 12/09/05 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DateFFime ID Sample Comment(s) This report Is a revision and supercedes our odgfnal reportdated 12128/05. BRL = Below Reporting Limit •J = Estimated value between the ,Reporting limit and the MDL The resu@s In thlsreport relate only to the samples submitted for analysis and meet state certification requirements other than NELAC certification except for those instances indicated in the case narrative and/or test comments. Angela D. Overcash, V.P. Laboratory Services This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inm 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224.0543 Phone: 704/529-6364 - Toll Free Number.'1-800/529-6364 - Fax: 7041525-0409 Page 24 of 24 /. I GROUNDWATER QUALITY MONITORING: l COMPLIANCE REPORT FORM FACILITY INFORMATION /� Please Print Clearly or Type Facility Name: Co,4J 5 6 m it ; C A N Permit Name (if differen_t): _ Facility Address• �' (3dK 3tc$ AmFrleg T6rfad f� 11'1Ar9p" 'sv ' /u 2T75� Count lie Dow11t Contact Person: �E''t'y G lY1cCOY)tK;rut%JE 1�01 y � � Telephone #:82�i-9SG-ylrr £x 3&F Well Location/ Site Name:+r!sr /QAc rdoN No. of Wells to be Sampled: I--� p from rermitl Well Identification Number (from Permit): IhW xk 2 For Groundwater Treatment Systems Well Depth: 7 ft. Well Diameter: (6 in, Screened Interval: /�R ft. to V' it. Check One: ❑ Influent (9 ❑ Effluent (99) Depth to Water Level: 3G..5 ft. below measuring point. Measuring Point (M.P.) is: 2.3 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: .S-9 Date sample collected: 8-2- 05 Field analysis: pH 0•'76 , Specific Conductance—.____uMhos Temp. IS- 'C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT It: EXPIRATION DATE: Non -Discharge GJOdc o.R UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediafion: Infiltration Gallery Spray Field Remediafion: �i Rotary Distributor Land Application of @fmdge m Other: NV I t• values snould reflect dissolved and - A colloidal concentrations, can Date sample analyzed:€F I�tlyrat Laboratory Name: Fvv;rcn ntFv�n[ 7 crj .cc Certification No. fecd -� PARAMETERS (Samples for metals were collected unfiltered --- t/ YES _NO and field acldifled COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P mnll (Ndte: Use MPN method for highly turbid samples) Dissolved Solids: Tota(8-3-D5 too mg/I pH (when analyzed) units TOC (9"6-05) ,f /.00 mg/I Chloride C 84-e5) b S mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate C S-7c-os) i mg/1 Specific Conductance " uMhos Total Ammonia mg/I TKN as N ..._. mg/I Gw-59 11 LI OCT 18 2005 Rev. 03/2000 Orthophosphate mg/I AI - Aluminum mg/I Ba - Barium mg/I Ca - Calcium (2-12-e51 20 mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury - mg/I K - Potassium mg/I Mg - Magnesium _(9-Iz-o5) 9.9 mg/I Mn - Manganese mq/I (L C— _k YES _ NO) Ni - Nickel mg/I Pb - Learl mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method P. Attach lab report.) Report Attached? Yes _(1) No r/ (0) VOC : method f) = method It = method 0 = GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Permit Name (if Facility Address Well Location/ Site /t Please Print Clearly or Type N"'Telephone #: g�f1->S�"Ll//I Fx334Fi ` No. of Wells to be Sampled: i Well Identification Number (from Permit): /h td;Fj /o For Groundwater Treatment Systems Well Depth: /8 ft. Well Diameter: 2 in. Check One: ❑ Influent (98) Screened Interval: S It. to 15r It. ❑ Effluent (99) Depth to Water Level: /7. $ N. below measuring point. Measuring Point (M.P.) is: L3_ ft. above land surface. Relative M.P. Elevation in It.: Gallons of water pumped/bailed before sampling: 2 Date sample collected: 8-2 -e.S Field analysis: pH 6.71 , Specific Conductance . Temp. I�7 °C, Odor - Appearance PARAMETERS (Samples for metals were collected COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total(9-3-o3) 32a mg/I pH (when analyzed) units TOC _ C (9 dSJ ZGJ.00 mg/1 Chloride mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate C8 ra cs) 15'0 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N . _ mg/I uMhos PERMIT It: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER EXPIRATION D_A_T_I Non-Discharge-GJBoad,56o3 U - NPDES TYPE OF PERMITTED OPERATION BEING MONITORED —� Lagoon Remedialion: Infiltration Gallery Spray Field Remedialion: Rotary Distributor Land Application of Sludge Other: colloidal concentrations. c') < —a Date sample analyzed: SEE Qt e(azo Laboratory Name; FNv;roi,.vre A! �SfJNg Certification No. od YES _NO and field acidified _AYES _ NO) Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as'PT mg/I Orthophosphate mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium (8-rz-e5) 2; z mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium (9-/2-c5) Ll mg/I Mn - Manganese mg/I McV'—l"Wa Ni - Nickel mg/I Pb - Lead mg/1 Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes _(1) No V (0) VOC : method it = method ft = method # = ut G W-59 1 5n\ � r`eG�or numod Agent)q- 3 a- 0 1g Rev. 03/2000 �� �jm GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name:_ Permit Name (if Facility Address 1 (� Please Print Clearly or Type 10145 Arhen�l co'� c _. III MVI a N we cit7SZ Countyedcwe11 (CYy) (SM10) ILo) Contact Person:—� r� G m N n ' Telephone #: 929-756-li/1/ Ft331,9 Well Location/ Site Name: -��° h�51, eti No. of Wells to be Sampled:) omoe M ) Well Identification Number (from Permit): M W # // For Groundwater Treatment Systems Well Depth: /3 ft. Well Diameter: in. Check one: ❑ Influent (98) Screened Interval: 3 It. to 13 ft. ❑ Effluent (99) Depth to Water Level: 12, 2 ft. below measuring point. Measuring Point (M.P.) is: Z• � ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: ,25 Date sample collected: 9-2-0-5- Field analysis: pH G L ; Specific Conductance uMhos Temp. /7 °C, Odor Appearance DEPARTMENT OF ENVIRONMENT a NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: EXPIRATION DATE: Non -Discharge Gl6 o ocS'6 03 UIC TYPE OF PERMITTED OPERATION BEING MONITORED —t,' Lagoon Remedialion: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: IVV 1 C, values snoula reTlect alssoivea ang tF, colloidal concentrations. c) ,.t Date sample analyzed: SEF_ �e10U , Laboratory Name: kA0retimexe-1rl 7?54%N5 Certification No. d -, EARAMETERS (Samples for metals were collected unfiltered ✓YES NO and field acidified �ES — NO) COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: use MPN method for highly turbid samples) Dissolved Solids: Total (9-3 os) /7o mg/I pH (when analyzed) units TOC 6-05-) 2.6G mg/I Chloride (A-ti-os) 45- mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/1 Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N .. — mg/I Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/l Orthophosphate mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium (,I-/z-°-s) r X mg/I Cd : Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab repo w Report Attached? Yes—(1) No ✓ (0) VOC : method # = method # = method # = GROUNDWATER QUALITY MONITORING: ICE REPORT FORM t-AUI1.1 I Y Mt-UHMA I IUN Please Print Clearly or Type Facility Name: . ...... C /4 +� Permit Name (if different): Facility Address: /0,9 'goy 3 G r`3 1 o, ericA -7-1711,4 /%Ia�iow Istnep %rve 2.9 2 County— /J9c�dwe!( -uw 5 �I n�1 Contacte Person: Tc�w %c K%n weLr_ Telephone 8:928-7f4fll/l F)e 9 Well Location/ Site Name:%E�Fl�eti f No. of Wells to be Sampled:_ Well Identification Number (from Permit): _MJV--! /2 Well Depth: 13 ft. Well Diameter:_ Screened Interval: 3 ft. to.. L3 ft. Depth to Water Level: 9-lr H. below measuring point. Measuring Point (M.P.) is: 2, 4 ft. above land surface. Gallons of water pumped/bailed before sampling: l• 25 Field analysis: pH , Specific Conductance Temp. .°C, Odor A PARAMETERS (Samples for metals were collected COD mg/I Coliform: MF Fecal /100m1 Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples Dissolved Solids: Total (�3� ""s= m l pH (when analyzed) units TOC (rd-G-os) /,bl mg/f Chloride ! ) mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate C S-Id-oS) l7 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N...­-------------- mg/I I For Groundwater Treatment Systems in, Check One: ❑ Influent (98) ❑ Effluent (99) Relative M.P. Elevation in ft.: Date sample collected: 8 -2-05 uMhos ooearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT It: EXPIRATION DATE: a-3/-o 9' Non -Discharge W d?o°a SG 0 3 UIC NPDES ir/COOd Y2V 3 TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Remediation:_ Rotary Distributor .Land App(iRption of, Sludge Other: c- NOTE: Values should reflect dlssoived(i d ' colloidal concentrations. o Date sample analyzed: ,SEE Qela .j Laboratory Name: /�-V%eA,UmPR7 al ­1—esfJej;Z Certification No. Ina a tered /L._YES _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P_- mg/1 Orthophosphate mg/I AI - Aluminum mg/I Ba - Barium mg/I Ca -Calcium--.... ( 8-zs-oS) /26 mg/I Cd - Cadmium _mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury- mg/I K - Potassium mg/I Mg - Magnesium < 8va=es) /6 mg/I Mn - Manganese mg/I --t,ZYES _ NO) Ni - Nickel mgll Pb - Lean mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Corlcentralion Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method P. Attach lab report) Report Attached? Yes —(1) No (0) VOC method it = or method R = method It = GW-59 Rev. 03/2000 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION nn n Please Print Clearly or Type Facility Name: - (O iZ �S /-9 M e n )"fA Permit Name (if different): - Facility Address: ,�2,0 46 X 31-g my n iylK 7-z"" c 7'y1A-Pier jwovj /Uc 29752 /?yc,0awelL la�Yl ¢. a 17.ip1 County Contact Person: del'-y G I�ICJwtiev_Telephone #:22$`7sb-1//119x3346 Well Location/ Site Name: . il.11 — No. of Wells to be Sampled: �L— Irom evma) Well Identification Number (from Permit): h'74'#13 For Groundwater Treatment Systems Well Depth: /S ft. Well Diameter: 2 in. Check one: ❑ Influent (98) Screened Interval: S It. to /S- ft: ❑ Effluent (99) Depth to Water Level: /0- 9 ft. below measuring point. Measuring Point (M.P.) is: 2 66 ft. above land surface. Relative M.P. Elevation in It.: ,Gallons of water pumped/bailed before sampling: `7, 0 Date sample collected: Field analysis: pH • ` O , Specific Conductance uMhos Temp. /7 °C, Odor Appearance PERMIT #: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER EXPIRATION DATE: Non -Discharge 4'dceoyP_.r,/3 UIC - NPDES 17iCeoocyze/3 TYPE P ITT D OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: N T • Values should reflect dissolved and colloidal concentrations. Date sample analyzed: Laboratory Name: F m�; rRom PK A 7Ps �i Certification No. /.00 PARAMETERS (Samples for metals were collected unfiltered— _,-'�YES NO 'and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total (3�3-oS) 36o mg/I Al - Aluminum mg/I pH (when analyzed) units Ba - Barium mg/I TOC ( -G bs) 3. w mg/1 Ca - Calcium ( R-12-e3-) 22. mg/I Chloride (8 y ss) 23 mg/I Cd - Cadmium mg/1 Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mg/1 Fe - Iron mg/I Sulfate / pia-os) 90 mg/I Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium (B-12-as) /3 mg/I TKN as N .. mg/I Mn - Manganese mg/I ✓ YES _ NO) Ni - Nickel mg/I Pb - Lear) mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) J l ORGANICS: (GC,GC/MS Jg-IPLC)�� (Specify test and method #LrAttadfi lab report ) Report Attached? Yes _(1)' No VOC : method 07. method # = method ft = r re ntee ( fir Aatnonzea Agent) Name and fife - Please print or type ' GW-59 G. `mL+7 9-3a Rev. 03/2000 ) Sign T11 re a mittee (or Authorized Agent) GROUNDWATER QUALITY MONITORING: COMPLIA RT FORM FACILITY INFORMATION /I Please Print Clearly or Type 9 Facility Name:_. Permit Name,(lf-different)z - - FacilnyAddress: 51PE0 0 13o 3I°8 mcviar 76�ead l< _ /Y/RniA'* /fie 2st952 Count 49c#0ee0rze Contacyj t Person:. J P� 0—Itll KC: � yl'Pt Telephone 7S6Y/// eN3 C-A Well Location/ Site Name: Sexier' 6yr-4"/s.< No. of Wells to be Sampled: „ _ o •m Well Identification Number (from Permit): &'W* /y For Groundwater Treatment Systems Well Depth: f.S ft. Well Diameter: 2 in. Check one: ❑ Influent (98) Screened Interval: ft, to /,S` ft. El Effluent (99) Depth to Water Level: Z'K ft. below measuring point. Measuring Point (M.P.) is:2,� ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/balled before sampling: 3 Date sample collected: 9-2'4 S Field analysis: pH , /D , Specific Conductance uMhos Temp. / 7 °C, Odor Appearance PERMIT It: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER EXPIRATION DATE: Non -Discharge — - UIC-- NPDES-- /vC G'O4 V2-1,3 TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Remedialion: Rotary Distributor Land Application of Sludge Other: NOTE* Values should reflect dissolved and colloidal concentrations. Date sample analyzed: .SFt %EPIC w Laboratory Name: 6a ;etie Certification No_ y/.Ao PARAMETER (Samples for metals were collected unfiltered YES _NO and field acidified _YES COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Coliform: MF Total /looml Phosnhorus: Tntal as'P mn/I (Note: Use MPN method for highly turbid pies) Dissolved Solids: Total 3_,sa co mg/1 pH (when analyzed) units TOC_ ff G c3 35-/ mg/1 Chloride Arsenic mg/I mg/1 Grease and Oils Phenol mg/I mg/1 Sulfatemg/l Specific Conductance uMhos Total Ammonia TKN as N-----_---_-_-- mg/I mg/I Orthophosphate mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium 5"12-e5) 79 mg/I Cd - Cadmium _ mg/I Chromium: Total mg/1 Cu - Copper mg/1 - Fe - Iron mg/I Hg Mercury mg/I K - Potassium mg/I Mg - Magnesium (B-Ia-43) 9.3 mg/1 Mn - Manganese mq/1 _ NO) Nt - Nickel mg/1 Pb - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen Q' mg/I Other (Specify Compounds and Concentration Units) o G, _i o ORGANICS: (GC,GC/MS,HPLC) (Specify test and method $. Attach Rob report.) Report Attached? Yes_(1) No ;-' (0) VOC : method If = V method It = method 11 = GW-59 ) (>. rvl` r ` —30-0 Rev. 03/2000 Signaler f Per i ee (or Authorized Agent) ---- �W=...,�� rvxln Permit# wcaoo.5-603 (Submit one each nme,iforing period with GPo=59 forma.) yc000 Yzv3 1 2 3 0 5 --- --•� ••�•...,,,y resuics were due. g report GW- ( i Will this monitorin be submitted after the established due date? ( 59 and GW-59A) YEE Was any required Information missing on the CN 59 report forms lain the pr to question 1 or 2 is "YES'; list in the space provided below the well identification numbers) and YE` explain the problems encountered in obtaining the required information. Are anI of the moni[or wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES identification plate, area overgrown, etc.)? If the answer is "3'e1•', comact the Regional OjjT,ce jorguidance. Are — monitored constituents equal to or above the established standards? If the answer to question 4 is NO'; skip to section 8. YE If the answer to question 4 is "YES"fist the affected wells individually with constituent(s) and concentrations) exceeding standards in the space provided below: ••• •,���••�+duuve, nave standards been exceeded previously same constituent(s) in the same well(s) in the last two years? for the YES - the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentrations) reported, and sample collection date for each occurrence (for the last two years). See AAA -kee) 6 Are the moniti if the answer i OFFICE IMME located; conta 7 I Is the permitte groundwater q 0 n section 5 located at or beyond the review its••, a groundwater quality problem may be occurring. CONTACT THE REGIONA, iTELY FOR GUIDANCE. If the answer is "NO-, monitoring wells may be improperly the Regional Office. uuy previously approved problem? If the answer to question 7 is "NO", the space , ne person completing this portion (GW--59A) of the monitoring report should sign below and submit this form with GW 59.forms for required wells to the address provided at the top of the current GW-59 form. heretiy acknowledge that ,[lRetFi'eabo7nfo-nwmapseportmeuated:and thelnona _rueportGW 59A) Isfe tioh submlYted Inthis to the best of knowled e Sicnatture o n v/ CN1'-59A 12%8/2003 -n nwaj I IQ11\ Samples Exceeding The Ground Water Standards I , 04/23/2002. MW 10 MW 11 MW 12 MW 13 MW 14 TDS Sulfate 08/06/2002 530 mg\I 370 mg\I 300 mg\I 520 mg\I TDS 510 mg\I Sulfate 12/03/2002 290 mg\I 370 mg\I . TDS Sulfate 560 mg\I 850 mg\I a630mg\l 12/03/2 003 TDS Sulfate 620 mg\I . 650 mg\I 620 mg\I 04/14/2004 TDS Sulfate 710 mg\I 440 mg\I 530 mg\I 610 mg\I 780 mg\I . 780 mg\l 08/30/2004 T,DS Sulfate 410 mg\I 548 mgM 503 mg\I Note: GrounId water standard for TDS 500 mg.M Ground water standard for Sulfate 250 mg\I tz/3l/e rnw 01LO iL F D 5 T D 5 — 546I-j Q i it I sample water.. 3 i Inwt3 n'ttif�� Environmental Testing Solutions, Inc Asheville, NC 28802 Certificate of Analysis Project name: Coats American Cullectimmdate: 2-Aug-05 Date received: 2-Aug-05 Results: Sample identification: MW #2 Phone: (828) 350-9364 Fax: (828) 350-9368 Project number: 050902.519 Sample number: 24320 .Parameters Method Result MDL Units Date Analyst Footnotes Analyzed Solids, Total Dissolved EPA 160.1 100 1.0 mg/L ;.pug -as KEK Chloride, Total EPA 325.3 6.5 - 1.0 mg/L &Aeg-as KEK, Sulfate, Total EPA 300.0 15 1.0 mg/L lo"Aag-os Mtaadrdh 1 Calcium EPA 200.7 20 0.10 mg/L 12-Aug-05 Pfitzgerald I Magnesium EPA 200.7 9.8 0.050 mg/L 12-Avg-05 PLtzguald 1 Total Organic Carbon EPA415.1 <1.00 1.00 mg/L &Aug-o5 MZC 2 Results: Sample identification: MW #10 Sample number: 24321 Parameters Method Result MDL Units Date Analyst Footnotes Analyzed Solids, Total Dissolved EPA 160.1 320 1.0 mg/L 3-Aug.05 KEK Chloride, Total EPA 325.3 14 1.0 mg/L &Aug.os KEK Sulfate, Total EPA 300.0 150 10 mg/L IaAug-05 Mlmdreth 1 Calcium EPA 200.7 2.3 0.110 mg/L 12-Aug-05 Phtzguatd 1 Magnesium' EPA 200.7 1.1 0.050 mg/L 12-pug-05 Pfitzguatd 1 Total Organic Carbon EPA415.1 <1.00 1.00 mg/L &Aug-05 MZC 2 Results: Sample identification: MW #11 Sample number: 24321 Parametem Method Result MDL Units Analyst Footnotes rLudyzc�l Solids, Total Dissolved EPA 160.1 170 1.0 mg/L 3-Aug-05 KEK Chloride, Total - EPA 325.3 6.5 1.0 mg/L &Aug-05 KEK_, Suffate, Total EPA 300.0 _ 59 2.0 mg/L laAug-05 Mlandreth I Calcium EPA 200.7 14 0.10 mg/L I2.Aug-05 Ptitzguald 1 Magnesium, EPA 200.7 3.0 0.050 mg/L 12-ms,-05 Pfitzgerald 1 Total Organic Carbon EPA415.1 2.66 1.00 mg/L 6-Aug-o5 MZC 2 i Numoer: ()UV Environmental Testing Solutions, Inc. PO Box 7565 Phone: (828) 350-9364 Asheville, NC 28802 Fax: (828) 350-9369 Certificate of Analysis Results: Sample identification: MW #12 Sample number:, 24323 Parameters Method Result M Units DateDL Analyst Footnotes Analyzed Solids, Total Dissolved EPA 160.1 580 1.0 mg/L 3-Au9 05 KEK Chloride, Total EPA 325.3 130 4.0 mg/L 4-Avg-as KEK Sulfate, Total EPA 300.0 17 1.0 mg/L mAug-os mudradt 1 Calcium EPA 200.7 120 0.20 mg/L is-Avg-o5 P6tzgmld 1 Magnesium EPA 200.7 16 0.050 mg/L 15-Aug-05 Pfi zgmld 1 Total Organic Carbon EPA 415.1 1.83 1.00 ma/L &Avg-w MZC 2 Results: Sample identification: MW#13 Sample number: 24324 Parameters Method Result MDL Units Date Analyst Footnotes Analyzed So&ds,TotalDissolved EPA 160.1 360 1.0 mg/L 3-Avg-05 KEK Chloride, Total EPA 325.3 25 1.0 mg/L aA Os KEK Sulfate, Total EPA 300.0 90 , 2.0 mg/L ]aAug-05 MLvtdreth 1 Calcium EPA 200.7 22 0.10 mg/L 12-Avg-05 Pfitzgrald 1 Magnesiun EPA 200.7 13 0.050 mg/L 12-Avg-05 PfitZprald 1 Total Organic Carbon EPA 415.1 3.79 1.00 mg/L 6-Aug 05 MZC 2 " Results: Sample identific Lion: M W #14 Sample number: 24325 Parameters Method Result MDL Units DateAnalyzed Analyst Footnotes Solids, Total Dissolved EPA 160.1 460 1.0 mg/L 3-Aug 05 KEK Chloride, Total EPA 325.3 12 1.0 mg/L 4-Avs-os KEK Sulfate, Total EPA 300.0 12 1.0 mg/L 10,Aug-05 MlaadreW 1 Calcium EPA 200.7 76 0.10 mg/L t2-Aug os P61zgerald 1 Magnesium EPA 200.7 43 0.050 mg/L m2 ag-05 P6tzgerald 1 Total Organic Carbon EPA 415.1 3.51 1.00 mg/L &Aug-os MZC 2 Footnotes: 1. Analyzed by Prism Laboratories, Inc. 2. Prism subcontracted to Test America, Inc. i NC Certification Number: 600 NC Drinking Water Certification Number: 37786 GROUNDWATER QUALITY MONITORING: c0 i FACIL j Facility Contact Person: eYry Well Location/ Site Name: Please Print Clearly or Type County-,-,' `,yow=rr Telephone #: Sz8-756-YG No. of Wells to be Sampled: Well Identification Number (from Permit): WO # 12_ For Groundwater Treatment Systems Well Depth: /3 0. Well Diameter:_2 in. Check One: ❑ Influent (98) Screened Interval: 3 ft. to I I ft. ❑ Effluent (99) Depth to Water Level: 2, °/ ft. below measuring point. Measuring Point (M.P.) is:^& ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampfing:, 16C Date sample collected: Field analysis: pH (0. 5 , Specific Conductance uMhos Temp. __12_°C, Odor Appearance PERMIT If: NPDES DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER EXPIRATION DATE: /Z 3/- _UIC TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gall a Spray Field Remediation: Rotary Distributor Land Application of Sludge r w, Other: N T • Values should reflect dissolved and C� __- colloidal concentrations, o tY - tr m Date sample analyzed: 4 - 5 - o S t� LaboratoryName: E12ulg0tJ )'&. t certification No. (�00 PARIAMETE (Samples for metals were collected unfiltered AYES —NO and field acidified ✓YES _ NO) COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turhld samples) Dissolved Solids: Total (N-(O-oS) .5bo mg/I pH (when analyzed) units TOC S-e5)2.5E Chloride .mg/l ip-o mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfated 19 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N ... V __.. mg/I Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as.PT mg/I Orthophosphate mg/I AI - Aluminum .r�'— mg/I Ba - Barium Ca - Calcium6q-13 -oOT�G—ta mg/I mg/I Cd - Cadmium _ mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury, mg/I K - Potassiu mg/I Mg- Magnesium -05 /7 mg/I Mn - Manganese mg/I FA u Ni - Nickel mg/I Pb - Lead mg/l Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes_(1) No tl (0) VOC method # = method # = method # = GW-59 uIIIIII - Z - O Rev. 0312000 � Sign. ire o ermittee r Authorized Agent I 1 _ (Da GROUNDWATER QUALITY MONITORING: Facility Name: L­ .Permit Name_(if dif FaMAddress:— l I oy"y (city) Contact Person:� Well Location/ Site SPORT FORM Please Print Clearly or Type � PERMIT It: County —/ ° I —.Ile 4,41 1 I Telephone #:162A- 75-S-4 No. of Wells to be Sampled: Well Identification Number (from Permit): /// 40 a /j For Groundwater Treatment Systems Well Depth: 14_ft. Well Diameter:_i in. Check One: ❑ Influent (98) Screened Interval: S ❑ Effluent (99) Depth to Water Level: 917 ft. below measuring point. Measuring Point (M.P.) is: 2,& ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/balled before sampling: /• 9 Date sample Collected: zf 5-0 Field analysis: pH L & , Specific Conductance uMhos Temp. 13 °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER EXPIRATION DATE: NPDES TYPE OF PERMITTED OPERATION BEING MONITORED ✓ lagoon Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: , NOTE: Values should reflect dissolved and colloidal concentrations. 9 JG+t1 ,o Date sample analyzed: -�—d ' ,$e c (�e/ ^'A LaboratoryName: ENvrreAr/ye r /4 T s1z � � Certification No. lvQ'� `'''I— PA_R.AMETE (Samples for metals were collected unfiltered <✓ YES _NO and field acidified Cmg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as PT mg/I (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total /1+-t,-o5) o511 mg/I pH (when analyzed) units TOC z/-8-o5 /•66 mg/I Chloride 4-7-05 II mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate g'OS A I mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I urtnopnospnate mg/I Al - Aluminum mg/I Be - Barium mg/1 Ca - Calcium -13 oS Zl mg/I Cd - Cadmium —mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassiu mg/I Mg - Magnesi mg/I Mn - Manganese mg/I C 'YES _NO) Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method P. Attach lab report.) Report Attached? Yes_(1) No _,�—(0) VOC method # = method # = method # = t` nl L'IR 0AJMc!✓1 rentm a (or Numunzeu Agent) Name ant; i me • mease print or type + GW-59 51gnalt of Polliltee (or Authorized Agent) (De Rev. 0312000 1 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Namt ,_Permit Name Well Location/ Site Name: Please Print Clearly or Type County—rfr Telephone #: No. of Wells to be Sampled: Well Identification Number (from Permit): /r6i�cJ YA /,'/ For Groundwater Treatment Systems Well Depth: 15' ft. Well Diameter: 2_ in- Check One: ❑ influent (98) Screened interval: .r ft. to I� ft. ❑ Effluent (99) Depth to Water Level: 712 ft. below measuring point. Measuring Point (M.P.) is: Z_(e ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 2. 5 Date sample collected: 1/- 5--D4 Field analysis: pH 61 S , Specific Conductance uMhos Temp. /P— °C, Odor Appearance DEPARTMENT OF ENVIRONMENT S NATURAL RESOURCES WATER DUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT it: EXPIRATION DATE: Non -Discharge— UIC NPDES NC-oaolie Z 1/3 1'YP F PERMITTED OPERATION BEING MONITORED NZ Lagoon Remediafion: Infiltration Gallery Spray Field Remediafion: Rotary Distributor Land Application of Sludge Other: AV1Tc• 1/.. b.,.,. .-1.....1.1 .sl....• dl-_�L.-u _.--1 colloidal concentrations.VV V~ y„~ co Date sample analyzed: /e/0k/ Laboratory Name: <, "VC ,. Certification No. SOD 7. 0"'b PARAMETE (Samples for metals were collected unfiltered_L/ _YES _NO and field acidified ✓YES _ NO) COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100m1 (Note: Use MPN method for highly urbld sem lee) Dissolved Solids: Total `/-�-os 370 mg/I pH (when analyzed) units TOC y-Ff o5 2,10 mgrl Chloride4-7-05 10 mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate (`f-g a$ l9 mg/I Specific Conductance uMhos Total Ammonia mg/l TKN as N mg/I GW-59 Rev. 03/2000 Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P__ . mg/I Orthophosphate mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassiu GS 42 mg/I Mg - Magnesium -I - mg/I Mn - Manganese mg/I "N Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report, Report Attached? Yes_(1) No_(0) VOC : method # = u i ret,1 yvte-4,i method d = method # = �Q GW-59A COMPLIANCE REPORT FORM Permit # lsjq 000 SGo !� (Submit one each monitoring period with 0N-59 jorms.) Ale p pp Jf I,4.3 I Enter date monitoring results were due. ( NpA•/3i 1 Will this monitoring report (GW-59 and GW-59Aj YES be. submitted after the established due date? NO ci Z Was any required information missing on the GW-59 report forms? YES NO IF the answer to question f or 2 is 'YES", list in the space provided below the well identification - umber(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)?I%dre answer is "Yes", contact the Regional Ojricejor guidance. 4 Are any monitored constituents equal to or above the established standards? YES ✓ NO If the answer to question 4 is "NO", skip to section B. If the answer to question 4 is "YES" list the affected wells individually with crinstituent(s) and concentration(s) exceeding standards in the space provided below. M04 12.: 1 DS = S&c V. n3/-11 5 For the constituents identified In question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is "NO", skip to section 8. if the answer to question 5 is `YES" list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). `Jee i4 tl rt��n�� Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO !f the answer is "YES", a groundwater qualityproblem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is 'NO", monitoring wells may be improperly located,, contact the Regional Office. - 7 is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is 'YES", describe those actions in the space provided below. If the answer to question 7is "NO'; contact the Regional Office within 90 days: an evaluation maybe required to determine the impact the waste disposal system Is having at the review and compliance - boundaries surrounding this facility. Failure to do so may subfect the permittee to a Notice of Violation fines. and/or penalties. , g The person completing this portion (G W-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. Thereby acknowledge thatkthe above nf6rm8tlon was evaluated and'thelnfoimaflon submltte� n this" ieport (Compllance report GW 59A),Is tru Arid complete to the best_o�rty kno 1 de gem, Sig ure(T Permittee (or Authorized nt) Date GW-59A 12/9/2nn7 Sevier Finishing Plant Samples Exceeding The Ground Water Standards MW10 MW11 MW12 MW13 MW14 04/23/2002. TDS 530 mg\I 520 mg\I Sulfate 370 mg\I 300 mg\I 08/06/2002 TDS 510 mg\I Sulfate 290 mg\I 370 mg\I 12/03/2002 TDS 850 mg\I 630 mgU Sulfate 560 mg\I 12/03/2003 TDS 620 mg\I . 650 mg\I 620 mg\I Sulfate. 04/14/2004 TDS 710 mg\I 530 mg\I 610 mg\I 780 mg\I „ 780 mg\I Sulfate 440 mg\I 08/30/2004 TDS 548 mgU 503 mg\I Sulfate 410 mg\I Note: Ground water standard for TDS 500 mg\I Ground water standard for Sulfate 250 mgU r 213ole I -r D 5 sample water.123 m W fC (yi LO i I mw, iz mW mw� Environmental Testing Solutions, Inc PO Box 7565 Phone: (828) 350-9364 Asheville, NC 28802 Fax: (828) 350-9368 Certificate of Analysis Projectname: Coats American Collection (late: 5-Ayr-05 Date received: 5-Apr-05 Results: Sample identification: MW #2 Project number: 050405.506 Sample number: 21096 Parameters Method Result MDL Units mare Analyst Footnotes Analyzed Solids, Total Dissolved EPA 160.1 110 1.0 mg/L 6Apna5 KEK Chloride, Total EPA 325.3 5.5 1.0 mg/L 7-Apr-as KEK Sulfate, Total 9056 15 1.0 mg/L 8-A,.-m Mlmdmh 1 Calcium 6010B 19 0.10 mg/L I3Apr-05 M=Vbell 1 Magnesium 6010 B 10 0.050 mg/L 1g.Apr-05 Mcampbell 1 Total Organic Carbon 9060 4.00 1.00 mg/L 8-Ap -05 T A 2 Results: Sample identification: MW#10 Sample number: 21097 Parameters Method Result MDL Units Date Analyst Footnotes Analyzed Solids, Total Dissolved EPA 160.1 120 1.0 mg/L eA,-a5 KEK Chloride, Total EPA 325.3 13 1.0 mg/L 7.Apr-as KEK Sulfate, Total 9056 35 1.0 mg/L 8-A4r-as Mlaadreth 1 Calcium 6010 B 1.1 0.10 mg/L ia-Apwos Mwaq)bell 1 Magnesium 6010 B 0.53 0.050 mg/L I3-Apc-05 Mcmipbell 1 Total Organic Carbon 9060 <100 1.00 mg/L 8-Ap-05 T a 2 Results: Sample identification: MW #11 Sample number: 21098 Parameters Method Result MDL Units "ace Analyst Footnotes Analyzed Solids, Total Dissolved EPA 160.1 280 1.0 mg/L 6Apr-0s KEK Chloride, Total EPA 325.3 7.0 1.0 mg/1. 7.Ap.- KEK Sulfate, Total 9056 52 2.0 mg/L a-Apn05 Miaadreth 1 Calcium 6010 B 15 0.10 mg/L 13-Apr.05 Mcampbeli 1 Magnesium 6010B 3.7 0.050 mg/L n.Apr-a5 Meaaph6l 1 Total Organic Carbon 9060 239 1.00 mg/L &Apr-a5 Ten� 2 NC Certification Number. 600 NC Drinking Water Certification Number: 37786 Environmental Testing Solutions, Inc. PO Box 7565 Phone: (928) 350-9364 Asheville, NC 28802 Fax: (928) 350-9368 Certificate of Analysis Results: Sample identification: MW #12 Sample number: 21099 Parameters Method Result MDL Units Date Analyst Footnotes Analyzed Solids, Total Dissolved EPA 160.1 560 1.0 mg/L 6-Apr-os KEK Chloride, Total EPA 325.3 120 0.4 mg/L 7-Apr-05 KEK Sulfate, Total 9056 19 1.0 mg/L s-Apr-os Mwiaaa, 1 Calciwn 6010 B 100 0.10 mg/L 13-Apr-05 Mealnpbe➢ 1 Magnesium 6010 B 17 0.050 mg/L 13-Apr-05 Mcampbcu 1 Total Organic Carbon 9060 2.58 1.00 mg/L s.Apr-o5 Tma 2 Results: Sample identification: MW #13 Sample number: 21100 Parameters Method Result MDL Units Analyst Footnotes A1lyzed Solids, Total Dissolved EPA 160.1 250 1.0 mg/L 6-Apr-05 KEK Chloride, Total EPA 325.3 11 1.0 mg/L 7-Apr-05 KEK Sulfate, Total 9056 61 2.0 mg/L' s-Apr-os MlandaW 1 Calcium 6010 B 21 0.10 mg/L 13-Apr-05 Mcampbell 1 Magnesium 6010 B 14 0.050 mg/L 13-Apr-05 Mcampbell 1 Total Organic Carbon 9060 1.66 1.00 mg/L s-Apr-o5 TaA 2 Results: Sample identification: MW #14 Sample number: 22001 Parameters Method Result MDL Units Date Analyst Footnotes Analyzed Solids, Total Dissolved EPA 160.1 370 1.0 mg/L 6-Apr-05 KEK Chloride, Total EPA 325.3 10 1.0 mg/L 7-Apr-05 KEK Sulfate, Total 9056 19 1.0 mg/L s.Apr-o5 Mbndrem 1 Calcium 6010 B 64 0.10 mg/L 13-Apr-05 Mcampbcll 1 Magnesium 6010 B 42 0.050 mg/L 13.Apr-05 Mcampbell 1 Total Organic Carbon 9060 2.84 1.00 mg/L 8.Apnos T� 2 Footnotes: 1. Analyzed by Prism laboratories, Inc. 2. Prism subcontracted to Test America, Inc. NC Certification Number. 600 NC Drinking Water Certification Number: 37786 GROUNDWATER QUALITY MONITORING: lR�ll'1 l _ R _ f r. FACILITY INFORMATIONPlease Print Clearly or Type Facility Name: CQP-+5 /- mcPlc,.6L PermitName(if different): —T -- C....f,:r.. I, .1 il...... r. Pn ,�e --r ld LL ✓lYl (.2P1 / i1 h/Jn RC it "+nro"v - rv1_ wrote County Jrc-.'�owe.lr (CO) IS�Ie) RIP) Contact Person: Jz rr• c k 1 0) s Telephone #: V-? 756 - `t t l l x 33 1 Well Location/ Site Name: Sev1eR IT (3A s PAN No. of Wells to be Sampled: r Irom Ve,mlq Well Identification Number (from Permit): M(J XZ For Groundwater Treatment Systems Well Depth: _f5f. t Well�Diameter: 67 in. Check One: ❑ Influent (98) Screened Interval: 3 NIT' ❑ Effluent (99) Depth to Water Le>t�l. � n. below measuring point. Measuring Point (M.P.) is: 23 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 60 Date sample collected: !4- 5 -o S Field analysis: pH__yZfib1 Specific Conductance — uMhos Temp. _Cq°C, Odor Appearance PARAMETERS (Samples for metals were collected COD mg/I Coliform: MF Fecal /100ml Colfform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total (�1-6-Cs) 110 mg/I pH (when analyzed) units TOG q-8-cs <hoemg/I Chloride Ll-7-os .5.5 mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate C# -8-05 !.S mg/I Specific Conductance uMhos Total Ammonia mg11 TKN as N mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: EXPIRATION DATE: 3-.3 i -ac- Non-Discharge.."G05lo03 UIC NPDES TYPEF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Remediation:— Rotary Distributor Land Application of Sludge Other: C- NOTE: Values should reflect dissolved and colloidal concentrations, o I Ul Date sample analyzed: Sea belo L ) Laboratory Name: —10�tiruj RO"rmE�✓t 4 ics N� Certification No. boo tiered v YES —NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/1 Orthophosphate mg/I Al - Aluminum mg/I Ba - Barium Ca - Calcium mg/I mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury - mg/I K - Potassium Mg - Magnesium Ll-13 mg/I mg/I Mn - Manganese mg/I YES _ NO) Ni - Nickel mg/I Pb - Learl mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes_(1) No _t-1 (0) VOC method # = method # = method # = GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION n�J Please Print Clearly or Type (nx15 /yrNeY/CeZN PEAMIT#: Facility Name: / - Well Location/ Site Name: County Irl—.y0e.Jerr Telephone #: T9`75E- No. of Wells to be Sampled: Well Identification Number (from Permit): /y/W4' /C Well Depth: t ft. Well Diameter: Z Screened Interval: $ ft, to 18 ft, Depth to Water Level: 14-3 ft. below measuring point. Measuring Point (M.P.) is;i_,_;� ft. above land surface. Gallons of water pumped/balled before sampling: 35 Field analysis: pH &•o , Specific Conductance Temp. I_°C, Odor A For Groundwater Treatment Systems In Check One: ❑ Influent (98) ❑ Effluent (99) Relative M.P. Elevation in ft.: Date sample collected: `f -5 --05 uMhos ppearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER OUALRY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER EXPIRATION DATE: S -31- NPDES TYPE OF PERMITTED OPERATION BEING MONITORED ✓Lagoon Remediaiion: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other. NOTE: Values should reflect dissolved and colloidal concentrations. Z i a Date sample analyzed: Laboratory Name: c -dU, e 6NrvC44 7L.7 r Certification No. hp o f s PA AMETERS (Samples for metals were collected unfiltered&_�'_YES —NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I (Note: Use MPN method for highly turbid aample8) Dissolved Solids: Total C -�Z fZc mg/I pH (when analyzed) units TOG 4-8-05 l.evmg/I Chloride mg/1 Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia - mg/l TKN as N mg/I Urthophosphate mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium CI4-/3-eS !.! mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassiu mg/I Mg - Magnesiu mg/I Mn - Manganese mg/I JG YES _ NO) Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Goncentralion Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes_(1) No ✓ (0) VOC : method # = method # = method # = GROUNDWATER QUALITY MONITORING: FACILITY INFORMATION Please Print Clearly or Type Facility Name: Cc )J 5 /-lmerte.6-1k.) - `Permit-Name=(if°different); Fagility Address: Pb P;c A A LR A30 i/.rerlc3 u %!tt e J l�e� /liARfO v 19tree0 A/C'. 097� _ County00 i Contact Person: Jer,-.a Mektp_%Z ,�1t —Telephone #:RES"75G-ylllx3369 Well Location/ Site Name: Sevier NSA Dowd No. of Wells to be Sampled: „ Well Identification Number (from Permit): MO l( For Groundwater Treatment Systems Well Depth: /Z. ft. Well Diameter: _ in. Check One: ❑ Influent (98) Screened Interval: .3 ft. to 1�; ft, ❑ Effluent (99) Depth to Water Level: '3, ft. below measuring point. Measuring Point (M.P.) is: ft. above land surface. Relative M.P. Elevation in ff: Gallons of water pumped/bailed before sampling: /,5• Date sample collected: 4-5-06- Field analysis: pH&__ , Specific Conductance uMhos Temp. 13°C, Odor Appearance PAft METE (Samples for metals were collected unfiltered ✓YES —NO r . ! " + . DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH, NO 27699-1636 Phone:(919) 733.3221 PERMIT #:WQooe5ric3 EXPIRATION DATE: 3-31-c6- Non -Discharge- UIC TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallay Spray Field Remediation: Rotary Distributor Land Application of Sled e NOTE: Values should reflect dissolved and C3 wd colloidal concentrations. - Y Date sample analyzed: See �x'aaJ Laboratory Name: t a u t raev men al t es t-7 Certification No. (aC© and field acidified COD mg/I Nitrite (NO2) as N mgA Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P mgA (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total q-6-05) Apo mg/I Orthophosphate AI - Aluminum mg/I mg/I pH (when analyzed) units Be - Barium mg11 TOC 4-s=C52,39 mgA Ca - Calcium fj-13-e5 1.5 mg/I Chloride 4---7-os 72 mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate mg/I Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia mg/I Mg - Magnesium 4�os 7 mg/I TKN as N _ mg/I Mn - Manganese mg/I YES _ NO) Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GG,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes_(1) No VOC : method # = : method # = method # = UNDWATER QUALITY MONITORING: PLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: Coa%s Awtct tc�2rt Permit Name (if different): --- Factlity Address: PO tbe,r 348 - Avtaricaou f7 rca AR10A1 I51`°0 A]C. 2-5 m�.nowL1 U tsmi0t tart County. Contact Person: Je-r� a Ic � -tNe Telephone #: RP$ 756 - y!f I x 331-$ Well Location/ Site Name: e ie ck rcaw No. of Wells to be Sampled: . ir Well Identification Number (from Permit): /rl0 For Groundwater Treatment Systems Well Depth:.. 5 ft. Well Diameter: in. Check One: ❑ Influent (98) Screened Interval: 9 A ft, to hZ19 _ ft. ❑ Effluent (99) Depth to Water Le39l. � ft. below measuring point. Measuring Point (M.P.) is: _2. 3 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/balled before sampling: b 0 Data sample collected: 4- S -o S Field analysis: Specific Conductance uMhos Temp. °C, Odor Appearance PARAMETER (Samples for metals were collected u COD mg/I Coliform: MF Fecal /100MI Coliform: MF Total /100MI (Note: Use MPN method for hlehly turbid samples) Dissolved Solids: Total LK-(-'s� !10 mg/I pH (when analyzed) units TOC 4f - 8 <(,oe mg/I Chloride (4-7-05) S.5 mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate tl -S o5 f5 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: EXPIRATION DATE: Non -Discharge_+ 0056C3 UIC NPDES ,TYPE OF PERMITTED OPERATION BEING MONITORED _7l- Lagoon Remediafion: Infiltration Gallery Spray. Field Remediation: Rotary Distributor Land Application of Sludge t; Other:- - - C_ M NOTE: Values should reflect dissolved and . I - colloidal concentrations, 03 I /I � t Date sample analyzed: Sez pe1o� LaboratoryName: -EAJv1 R0^'mE1L1ra i cs vN!7 Certification No. 600 tered v YES —NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as PT mg/I Orthophosphate mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium-L3 - 05 Iq mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium _ mg/I Mg -Magnesium Y-13-o5 /0 mg/I Mn - Manganese mg/I `kt _tom YES _ NO) Ni - Nickel mg/I Pb - Lean mg/I Zn - Zinc mg/I Ammonia Mir Other (specify t uun�wii_ ORGANICS: ( , _T (Specify test and method #. Attach lab report,) Report Attached? Yes._(1) No _ / (0) VOC : method # = : method # = : method # = r, GW-59 Rev. 03/2000 ROUNDWATER QUALITY MONITORING: OMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: o x f 5 American/ Permit Name. (if_different): - Fac ity Address r° 0 %3ox 3 b P 34rdevreglu Deea ..AQ/D/i Wrleq C ZgG% ounty G.�oWC' poavl c (SM10) Rio) r Contact Person: J / Telephone fl: gEg-7.56-W!/n3369 Well Location/ Site Name: aWells to be Sampled: ,,• r Well Identification Number (from Permit): /ylW rt /0 For Groundwater Treatment Systems Well Depth: tp ft. Well Diameter: Z in. Check One: I] Influent (98) Screened Interval: 8 ft. to 18 ft, ❑ Effluent (99) Depth to Water Level: _ 14-3 ft. below measuring point. Measuring Point (M.P.) is:_2_•_1i ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: .35 Date sample collected: Lf-S -05 Field analysis: pH 6,0 , Specific Conductance _uMhos Temp. IS °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER GUALITY DIVISION, GROUNDWATER SECTION 1536 MAIL SERVICE CENTER PERMIT 0: EXPIRATION DATE: 3 -3/-d o Non-Discharge__QDO6S663 UIC-- NPDES TYPE OF PERMITTED OPERATION BEING MONITORED ✓Lagoon Remediation: Infiltration Gallery Spray Field Remediation: Fye Rotary Distributor Land Application of Sludge Other: I_ NOT Values should reflect dissolved and ca colloidal concentrations, a Date sample analyzed: 6=e %e%�✓ i LaboratoryName: .uurr6,vm� tc27 -7-,= n' Certification No. s60 o L3ARA-M-ETE (Samples for metals were collected unfiltered_g", YES _NO and field acidified COD mg/l Nitrite (NO2) as N mg/I Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as PT mg/I (Note; Use MPN method for highly turbid samples) Dissolved Solids: Total [`(-6-45) /i?o mg/I pH (when analyzed) units TOC 4-S-oS�mg/1 Chloride 63 mg/l Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate (q-B-Ds 35�5 mg/1 Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Urtnophospnate mg/I AI - Aluminum mg/1 Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potasslu Mg - Magnesium -0-05.53 mg/I mg/I Mn - Manganese mg/I e-x, _tom YES _ NO) Nf - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method If. Attach lab report) Report Attached? Yes—(1) No r/ (0) VOC method tf = method N = method if = rA ti �v 3`2 7- 0 Rev. 03l2000 I signalilr or rr miltee (or Authorized Agen Rev. `GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FAC IJ_ IIY INFORMAT_rP ION //�� Please Print Clearly or type Facility Name:Caa.T5 MOPlecalJ Permit Name (if different): - - Facc��i�lity Address —PO gax .��^� A 36 !rI 4Rloy svuen It/C`77 Z�S75 County w e ry e-l p7+v1 2 'L1C[NN2 RIM Contact Person: y Telephone #: g2C -756-4111 x 3369 Well Location/ Site Name:,50-wer l ° No. of Wells to be Sampled: i c 6) Well Identification Number (from Permit): M GJ Il For Groundwater Treatment Systems Well Depth:. 0 ft. Well Diameter:in. Checkpne: ❑ influent (98) Screened Interval: 3 ft, to �?L it. ' ❑ Effluent (99) Depth to Water Level: 9.4 ft. below measuring point. Measuring Point (M.P.) is: P. 6 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/balled before sampling: /,5. Date sample collected: 11-5-0S Field analysis: pH 6, , Specific Conductance uMhos Temp. _13_00, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT it: LJQ 000S1co3 EXPIRATION DATE: 3 31-0 Non -Discharge UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Remediation:° Rotary Distributor Land Application of Sludge ` Other �r z VV VV F 1Y colloidal concentrations.t Date sample analyzed: See b�IOCJ can Laboratory Name: En ui ov w en a Iz5 rN�1 Certification No. �6bC) PARAMETERS (samples for metals were collected unfiltered AYES —NO and field acidified OYES _ NO) COD mg/I Coliform: MF Fecal /100m1 Coliform: MF Total /100ml (Note; Use MPN method for highly turbid samples) Dissolved Solids: Total �4-6�05) �o mgfl pH (when analyzed) units TOC -'8-c5)2,39 mg/l Chloride 4-3-DS, 70 mg/1 Arsenic mg/1 Grease and Oils mg/I Phenol mg/1 Sulfate KZ mgll Specific Conductance uMhos Total Ammonia mg/I TKN as N ... _—--_ mg/1 Nitrite (NO2) as N mg/1 Nitrate (NO3) as N mg/1 Phosphorus: Total as P mg/I Orthophosphate mg/I AI - Aluminum mg/I Ba - Barium mg/1 Ca - CalciumN-13-e51q mg/l Cd - Cadmium mg/1 Chromium: Total mg/1 Cu - Copper mg/1 Fe - Iron mg/1 Hg - Mercury, mg/1 K - Potassium 14-13-05 7 mg/I Mg - Magnesium .1, mg/I Mn - Manganese mg/I Ni - Nickel mg/1 Pb - Lead mg/1 Zn - zinc mg/1 Ammonia Nitrogen_ mg/1 Other (Specify Compounds and Goncentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes_(1) No t/(0) VOC method It = method # method It = ON GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM raclr_I IT INr uVHMA I tuN n Please Print Clearly or Type Facility Name:..C-c2in'lt5 Otmerf�ar.j Permit Name (if different): /'(NgrQrou Nr_ Z-`d757- Counly--m�7�nwe Contact Person: J�rr nC �G�„ I< aal Telephone tY: $z8- 7$6 Well Location/ Site Name: zV1�+t S - quo No. of Wells to be Sampled: i Well Identification Number (from Permit): M l=J t" 2 For Groundwaler Treatment Systems Well Depth: .75 ft. Well Diameter: & if). Check One: ❑ Influent (98) Screened Interval:_dL1i_ ft. to.Ald_ it. El Effluent (99) Depth to Water Level: �° ft. below measuring point. Measuring Point (M.P.) is:.2.3 ft. above land surface, Relative M.P. Elevation in ft.: j Gallons of water pumped/bailed before sampling: .ram 78 Date sample collected: 1.2-30-6 Field analysis: pH 7, 3 , Specific Conductance —uMhos Temp. —t"f 00, Odor Appearance DEPARTMENT OP ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAILS ERVICE CENTER PERMIT ti: EXPIRATION DATE: 3 Non -Discharge G141UIC NPDES PF F PERMITTED OPERATION BEING MONITORED LaUoon Remedialion:Infiltratioh-rAttmv----• Spray Field _Remediation: Rotary Distributor _ Land Application of Other: _ NOTE- Values should reflect dissolved and z t colloidal concentrations. ipe�u Date sample analyzed: 5e c I? :An1 (_; Laboratory Name: c- r c f - ~i �+ C�( Certification No. 4o PAff ±METERS (Samples for metals were collected unfiltered / YES —NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml PhOSDhorus: Total as P mn/l (Note: Use MPN method for highly turhld samples) Dissolved Solids: Total ll- t-os) Iq0 mg/I pH (when analyzed) units TOC 4-5 mg/I Chloride Z- 3 -as) /b mg/I Arsenic mg/I Grease and Oils_ ^ mg/I Phenol _ mg/I Sulfate 1-3 �5 .5 Z mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N .. -_ mg/I Orthophosphate mg/I Al - Aluminum mg/I Ba - Barium Ca - Calcium mg/I mg/l Cd - Cadmium -_ mg/I Chromium: Total mg/I Cu - Copper__ mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassiu Mg - Magnesium I-lSf-os mg/I mg/l Mn - Manganese mull G, M"f; rjijIe-Y` - YES _NO)r- Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/l Other (Specify Compounds and ConAentratioii units) w �n ORGANICS: (GC,GC/MS,HPLC) r:- tv (Specify test and method N. Attach 11"D orh;) Report Attached? Yes I/ (1) No ' {0) VOC method ft = -�,,,o � rummiznu „6�-en77q��n�rvem�e�e-nrn nue -Please print ar GW-59 Signah 01 . miltee (or Authored geN) Rev. 03/2000 i method tt = method It = lace'Analyfical" Pace Analytical Services, Inc. 2225 Riverside Drive Asheville, 28804 Phone: 828.2.204.7176 www.pacelabs.com Fax 828.252.4616 - Lab Project Number: 9284858 Client Project ID: MONITORING WELLS Lab Sample No: l 925136863 Project Sample Number: 9284858-005 Date Collected: 12/30/04 11:56 Client Sample ID: MW #2 #4040 Matrix: Water Date Received: 12/30/04 14:10 Parameters i Results Units Report Limit Analysed By CAS No. Qual RegLmt GUMS Volatiles - 6230 VOCs by 8260, low level Method: EPA 8260 Benzene NO ug/l 0.50 01/05/05 10:38 BCK 71-43-2 Bromobenzene NO ug/1 0.50 01/05/05 10:38 BCK 108-86-1 Bromochloromethane NO ug/l 0.50 01/05/05 10:38 BCK 74-97-5 Bromodichlohoimethane NO ug/l 0.50 01/05/05 10:38 BCK 75-27-4 Bromoform NO ug/l 0.50 01/05/05 10:38 BCK 75-25-2 Bromomethane NO ug/l 0.50 01/05/05 10:38 BCK 74-83-9 n-Butylbenzene NO ug/l 0.50 01/05/05 10:38 BCK 104-51-8 sec-Butylbenzene NO ug/l 0.50 01/05/05 10:38 BCK 135-98-8 tert-Butylbenzene ND ug/l 0.50 01/05/05 10:38 BCK 98-06-6 Carbon tetrachloride NO ug/l 0.50 01/05/05 10:38 BCK 56-23-5 Chlorobenzene' NO ug/l 0.50 01/05/05 10:38 BCK 108-90-7 Chloroethane NO ug/l 0.50 01/05/05 10:38 BCK 75-00-3 Chloroform 10. ug/l 0.50 01/05/05 16:38 BCK 67-66-3 Chloromethanel NO ug/l 0.50 01/05/05 10:38 BCK 74-87-3 2-Chlorotoluene NO ug/l 0.50 01/05/05 10:38 BCK 95-49-8 4-Chlorotoluene NO ug/l 0.50 01/05/05 10:38 BCK 106-43.4 1,2-Dibromo-3tchloropropane NO ug/l 2.0 01/05/05 10:38 BCK 96-12-8 Dibromochloromethane NO ug/l 0.50 01/05/05 10:38 BCK 124-48-1 1,2-Oibromoe4ane (EDB) NO ug/l 0.50 01/05/05 10:38 BCK 106-93-4 Dibhomomethane ND ug/l 0.50 01/05/05 10:38 BCK 74-95-3 1,2-Dichlorobenzene NO ug/l 1.0 01/05/05 10:38 BCK 95-50-1 1,3-Dichlorobenzene NO ug/1 1.0 01/05/05 10:38 BCK 541-73-1 1.4-Dichlorobenzene NO ug/l 1.0 01/05/05 10:38 BCK 106-46-7 Dichlorodifluoromethane NO ug/l 0.50 01/05/05 10:38 BCK 75-71-8 1.1-Dichloroethane NO ug/l 0.50 01/05/05 10:38 BCK 75-34-3 1,2-Dichloroethane NO ug/l 0.50 01/05/05 10:38 BCK 107-06-2 1,2-Dichloroethene (Total) NO ug/l 0.50 01/05/05 10:38 BCK 540-59-0 1,1-Dichloroethene NO ug/l 0.50 01/05/05 10:38 BCK 75-35-4 cis-1,2-Dichloroethene NO ug/l 0.50 01/05/05 10:38 BCK 156-59-2 trans-1,2-Dichloroethene NO ug/l 0.50 01/05/05 10:38 BCK 156-60-5 1,2-Dichloropropane NO ug/l - 0.50 01/05/05 10:38 BCK 78-87-5 1,3-Dichloropropane NO ug/l 0.50 01/05/05 10:38 BCK 142-28-9 2,2-Dichloropropane ND ug/l 0.50 01/05/05 10:38 BCK 594-20-7 1,1-Dichloropropene NO ug/l 0.50 01/05/05 10:38 BCK 563-58-6 cis-1.3-Dichloropropene NO ug/l 0.50 01/05/05 10:38 BCK 10061-01-5 trans-1,3-Dichloropropene NO ug/l 0.50 01/05/05 10:38 BCK 10061-02-6 Diisopropyl efher NO ug/l 0.50 01/05/05 10:38 BCK 108-20-3 Date: 01/17/05, Page: 5 of 48 Asheville Certification IDs NC Wastewater 40 1 NC Drinking Water 377,12 SC Environmental 99030 FL NELAP Ed1648 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. �E tpq bal Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 aceAnalXical www.pacelabs.cem Lab Sample No: 925136863 Client Sample ID: MW 02 #4040 Pace Analytical Services, Inc. 2225 Riverside Drive Asheville, NC 28804 Phone: 828.254.7176 Fax: 828.252,4618 Lab Project Number: 9284858 Client Project ID: MONITORING WELLS Project Sample Number: 9284858-005 Date Collected: 12/30/04 11:56 Matrix: Water Date Received: 12/30/04 14:10 Parameters Results Units Report Limit Analyzed By CAS No. Dual RegLmt Ethylbenzene NO ug/l 0.50 01/05/05 10:38 BCK 100-41-4 Hexachloro=l,3-butadiene NO ug/l 2.0 01/05/05 10:38 BCK 87-68-3 Isopropylbenzbne (Cumene) NO ug/1 0.50 01/05/05 10:38 BCK 98-82-8 p-Isopropyltoluene NO ug/1 0.50 01/05/05 10:38 BCK 99-87-6 Methylene chloride NO ug/1 2.0 01/05/05 10:38 BCK 75-09-2 Methyl-tert-butyl ether NO ug/l 0.50 01/05/05 10:38 BCK 1634-04-4 Naphthalene NO ug/l 2.0 01/05/05 10:38 BCK 91-20-3 n-Propylbenzene NO ug/l 0.50 01/05/05 10:38 BCK 103-65-1 Styrene NO ug/l 0.50 01/05/05 10:38 BCK 100-42-5 1,1.1,2-Tetrachloroethane NO ug/l 0.50 01/05/05 10:38 BCK 630-20-6 1,1.2.2-Tetrachloroethane NO ug/l 0.50 01/05/05 10:38 BCK 79.34-5 Tetrachloroethene NO ug/l 0.50 .01/05/05 10:38 BCK 127-18-4 Toluene NO ug/l 0.50 01/05/05 10:38 BCK 108-88-3 1.2.3-Trichlorobenzene NO ug/l 2.0 01/05/05 10:38 BCK 87-61-6 1,2,4-Trichlorobenzene NO u9/l 2.0 01/05/05 10:38 BCK 120-82-1, 1,1,1-Trichloroethane NO ug/l 0.50 01/05/05 10:38 BCK 71-55-6 1,1,2-Trichloroethane NO ug/l 0.50 01/05/05 10:38 BCK 79-00-5 Trichloroethene NO ug/1 0.50 01/05/05 10:38 BCK 79-01-6 Trichlorofluoromethane NO ug/1 0.50 01/05/05 10:38 BCK 75-69-4 1,2,3-Trichloropropane NO ug/l 0.50 01/05/05 10:38 BCK 96-18-4 1.2,4-Trimethylbenzene NO ug/l 0.50 01/05/05 10:38 BCK 95-63-6 1.3,5-Trimethylbenzene NO ug/l 0.50 01/05/05 10:38 BCK 108-67=8 Vinyl chloride NO ug/l 0.50 01/05/05 10:38 BCK 75-01-4 Xylene (Total) - NO ug/1 0.50 01/05/05 10:38 8CK 1330-20-7 m&p-Xylene NO ug/1 1.0 01/05/05 10:38 BCK o-Xylene NO ug/l 0.50, 01/05/05 10:38 BCK 95-47-6 Toluene-d8 (S) 85 % 01/05/05 10:38 BCK 2037-26-5 4-13romofluorobenzene (S) 102 % 01/05/05 10:38 BCK 460-00-4 Dibromofluoromethane (S) 97 % 01/05/05 10:38 BCK 1868-53-7 1,2-Dichloroethane-d4 (S) 92 % 01/05/05 10:38 BCK 17060-07-0 Date: 01/17/05 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 FL NELAP E87648 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Oq b ac, Page: 6 of 48 Charlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 1 7 3 4 ki 0 7 0 -- ---- _ 1-11, rermit e Gyq 00 o 3 . (Subinir —One each mm"iloring period wirl. GW 59 forms.) /l%C 000 1/7-cf 7j Enter date monitoring results were due. (-J� „-, 31 I Will tho is monitoring repo GW- be submitted after the established due date? ( 59 and GW-59A) .yES NO Was any required information missing on the GW-59 report forms? IF the answer to question 1 or 2 is'YES', list -the space provided below the well identification number(s) and YES explain the problems encountered in obtaining the required information. Are any of the monitor welts in need of repair or maintenance (damaged casing, unlocked or p, missing the Regions/ O�ace for guiinging sscami identification plate, area overgrown, etc.)? If the. answer is "Yes ", contact ca Are any monitored constituents equal to or above the established standards? If the answer to question 4 is '%VO ;skip to section 8. If the answer to question 4 is "YES"fist the affected wells individually with constituent(s) and concentrations) exceeding standards in the space provided below.- Mw a 12 i Ds = 520 rMg(-e - - -••- -,- =IRO .aenuneo in question 4 above, have standards been exceeded previouslyfo —the same constituent(s) in the same well(s) in the last two years? - the answer to question 5 is "NO" skip to section 8. If the answer to question 5-is "YES", list in the space provided below, each well with constituent(s) exceeding standards; conceentration(s) reported, and sample collection date for each occurrence (for the last two years). 1 / the monitoring wells listed in section 5located at or beyond the review boun rr me answer is "YES'; a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office. • •- r ........ rr unpiementing previously approved actions required by the Division involving this groundwater quality problem? YES n me answer to question 7 is 'yES ; describe those actions in the space orowded hetnw Ifthe ancwn. •.. ...... _.:__ ...._.. - •- r- —....ornpteung this portion (G W.59A) off e monitoring report should sign below and submit it form with GW-59'forms for required wells to the address provided at the top of the current GW-59 form. Glermittee(Or AumOriZeC ue 1 7-7 0 NO t/ GW-59A I2%8/2003 Sevier Finishing Plant Samples Exceeding The Ground Water Standards MW 10 MW 11 MW 12 MW 13 MW 14 04/23/2002 TDS 530 mg\I 520 mg\I Sulfate 370 mg\I 300 mg\I 08/06/2002 T,DS 516 mgU Sulfate 290 mg\I 370 mg\I 12/03/2002 T,DS 850 mg\I 630 mg\I Sulfate 560 mg\I 12/03/2003 TDS 620 mg\I 650 mg\I 620 mg\I Sulfate 04/14/2004 TDS 710 mg\I 530 mg\I 610 mgU 780 mg\I 780 mg\I Sulfate '440 mg\I 08/30/2004 TDS 548 mg11 503 mg\I Sulfate 410 mg\I Note: 1 Ground water standard for TDS 500 mg\I Ground water standard for Sulfate 250 mgU sample water.1 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facillty Name:._.S_.o a7 5 KcYlept Permit Name (it different): Nddress:— r40 /3ok 364 Well Location/ Site Name: Please Print Clearly or Type County _/rr-<Joa�cll Telephone #: No. of Wells to be Sampled:,,._ / Well Identification Number (from Permit): 97010E to Well Depth: ($ ft. Well Diameter: 3 Screened Interval: 8 ft. to , / S It. Depth to Water Level:.�ft. below measuring point. Measuring Point (M.P.) is:-x�j3 ft. above land surface. Gallons of water pumped/balled before sampling: 4v Field analysis: pH 7" r , Specific Conductance Temp. 1_°C, Odor A For Groundwater Treatment Systems In. CheokOne:❑ Influent (98) ❑ Effluent (99) Relative M.P. Elevation in ft.: Date sample collected: / ------uMhos ooearance P_.ABAMETER (Samples for metals were collected unff COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 6-y-o5) 171P mg/I pH (when analyzed) units TOC /-�-n < S mg/1 Chloride_ 1-3--052 < 5 mg/I Arsenic mg/I Grease and Oils ^ mg/I Phenol.. mg/I Sulfate __ J-3-oSi ! mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N .� mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES - WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT If: EXPIRATION DATE: .3`3/-DG Non -Discharge /JQ!0O 5(�p3 UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field _ Remediation: Rotary Distributor —Land Application of Sludge ..Other: — NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: sec &(o�j Laboratory Name: cc ft Certification No. — HQ Itered 6' YES _,NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P_ mg/I Orthophosphate mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper m9 /I Fe - Iron mg/I Hg -. Mercury mg/I K - Potassiu Mg - Magnesium - IL 4=°S r 5°7 mg/I mg/I Mn - Manganese mg/I Pe itlee rAuthorized Agent Name nd Tiae GW-59 e.yy G • ��)Gr�Ne Rev. 03/2000 Signature of P rmittee (or Authorized Agent) YES _ NO) Nf - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen_ n-_-mg/I Other (Specify Compounds and CIO Units N c'ca ORGANICS: (GC,GC/MS,HPLC) u1 (Specify test and method #. Attach leb report.) Report Attached? Yes_(1) No — (0) VOC method # = method 8 = method # = or E -Z7—o ace Analytical www.pacelabs.com Lab Sample No: 925136913 Client Sample ID: MW #10 #4045 Pace Analytical Services, Inc. 2225 Riverside Drive Asheville, NC 28804 Phone., 828.254.7176 Fax: 828.252.4618 Lab Project Number: 9284858 Client Project ID: MONITORING WELLS Project Sample Number: 9284858-010 Date Collected: 12/30/04 12:05 Matrix: Water Date Received: 12/30/04 14:10 Parameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt GUMS Volatiles 6230 VOCs by 8260, low level Method: EPA 8260 Benzene ND ug/l 0.50 01/05/05 11:04 BCK 71-43-2 Bromobenzene ND ug/l 0.50 01/05/05 11:04 BCK 108-86-1 Bromochloromethane NO ug/l 0.50 01/05/05 11:04 BCK 74-97-5 Bromodichloromethane ND ug/l 0.50 01/06/05 11:04 BCK 75-27-4 Bromoform NO ug/l 0.50 01/06/05 11:04 BCK 75-25-2 Bromomethane NO ug/l 0.50 01/05/05 11:04 BCK 74-83-9 n-Butylbenzene ND ug/l 0.50 01/05/05 11:04 BCK 104-51-8 sec-Butylbenzene ND ug/l 0.50 01/05/05 11:04 BCK 135-98-8 tert-Butylbenzene ND ug/l 0.50 01/05/05 11:04 BCK 98-06.6 Carbon tetrachloride ND ug/l 0.50 01/05/05 11:04 BCK 56-23-5 Chlorobenzene NO ug/l 0.50 01/06/05 11:04 BCK 108-90-7 Chloroethane NO ug/l 0.50 01/05/05 11:04 BCK 75-00-3 Chloroform NO ug/l 0.50 01/05/05 11:04 BCK 67-66-3 Chloromethane ND ug/l 0.50 01/05/05 11:04 BCK 74-87-3 - 2-Chlorotoluene ND ug/l 0.50 01/05/05 11:04 BCK 95-49-8 4-Chlorotoluene NO ug/l 0.50 01/05/05 11:04 BCK 106-43-4 1,2-Dibromo-3-chloropropane ND ug/l 2.0 01/05/05 11:04 BCK 96-12-8 Dibromochloromethane ND ug/l 0.50 01/05/05 11:04 BCK 124-48-1 1,2-Dibromoethane (EDB) ND ug/l 0.50 01/05/05 11:04 BCK 106-93-4 Dibromomethane ND ug/l 0.50 01/05/05 11:04 BCK 74-95-3 , 1,2-Dichlorobenzene ND ug/l 1.0 01/05/05 11:04 BCK 95-50.1 1.3-Dichlorobenzene NO ug/l 1.0 01/05/05 11:04 BCK 541-73-1 1.4-Dichlorobenzene NO ug/l 1.0 01/05/05 11:04 BCK 106-46-7 Dichlorodifluoromethane NO ug/l 0.50 01/05/06 11:04 BCK 75-71-8 1,1-Dichloroethane ND ug/l 0.50 01/05/05 11:04 BCK 75-34-3 1,2-Dichloroethane ND ug/l 0.50 01/05/05 11:04 BCK 107.06-2 , 1,2-Dichloroethene (Total) NO ug/l 0.50 01/05/05 11:04 BCK 540-59-0 1,1-Dichloroethene ND - ug/l 0.50 01/05/05 11:04 BCK 75-35-4 cis-1,2-Dichloroethene ND ug/l 0.50 01/05/05 11:04 BCK 156-59-2 trans-1,2-Dichloroethene ND ug/l 0.50 01/05/05 11:04 BCK 156-60-5 1.2-Dichloropropane NO ug/l 0.50 01/05/05 11:04 BCK 78-87-5 1,3-Dichloropropane NO ug/l 0.50 01/05/05 11:04 BCK 142-28-9 2.2-Dichloropropane ND ug/l 0.60 01/05/05 11:04 BCK 594.20-7 1.1-Dichloropropene ND ug/1 0.50 01/05/05 11:04 BCK 563-58-6 cis-1,3-Dichloropropene ND ug/l 0.50 01/05/05 11:04 BCK 10061-01-5 trans-1,3-Dichloropropene NO ug/l 0.50 01/05/05 11:04 BCK 10061-02.6 Diisopropyl ether NO ug/l 0.50 01/05/05 11:04 BCK 108-20.3 Date: 01/17/05 Page: 11 of 48 REPORT OF LABORATORY ANALYSIS Asheville Certification IDs This report shall not be reproduced, except in full, Charlotte Certification IDs NO Wastewater 40 without the written consent of Pace Analytical Services, Inc. NO Wastewater 12 NO Drinking Water 37712 «,, NO Drinking Water 37706 SC Environmental 99030 "' �'��� SC 99006 FI NIFI AP FA7AAA Ph r= n aio no va�em ace Analytical www.pacelabs.com Lab Sample No: 925136913 Client Sample ID: MW #10 #4045 Pace Analytical Services, Inc. 2225 Riverside Drive Asheville, NO 28804 Phone: 828.254.7176 Fax: 828.252.4618 Lab Project Number: 9284858 Client Project ID: MONITORING WELLS Project Sample Number: 9284858-010 Date Collected: 12/30/04 12:05 Matrix: Water Date Received: 12/30/04 14:10 Parameters Results Units Report Limit Analyzed By CAS No. ual ReoLmt Ethylbenzene NO ug/l 0.50 01/05/05 11:04 BCK 100-41.4 Hexachloro-1,3-butadiene NO ug/l 2.0 01/05/05 11:04 BCK 87.68-3 Isopropylbenzene (Cumene) NO ug/l 0.50 01/05/05 11:04 BCK 98-82-8 p-Isopropyltoluene NO ug/l 0.50 01/05/05 11:04 BCK 99-87-6 Methylene chloride NO ug/l 2.0 01/05/05 11:04 BCK 75-09.-2 Methyl-tert-butyl ether NO ug/l 0.50 01/05/05 11:04 BCK 1634-04-4 Naphthalene NO ug/l 2.0 01/05/05 11:04 BCK 91-20-3 n-Propylbenzene NO ug/l 0.50 01/05/05 11:04 BCK 103-65-1 Styrene NO ug/l 0.50 01/05/05 11:04 BCK 100-42-5 1,1,1,2-Tetrachloroethane NO ug/l 0.50 01/05/05 11:04 BCK 630-20-6 1,1,2,2-Tetrachloroethane NO ug/l 0.50 01/05/05 11:04 BCK 79-34-5 Tetrachloroethene NO ug/l 0.50 01/05/05 11:04 BCK 127-18-4 Toluene NO ug/l 0.50 01/05/05 11:04 BCK 108.88-3 1,2,3-Trichlorobenzene NO ug/l 2.0 01/05/05 11:04 BCK 87.61.6 1,2,4-Trichlorobenzene NO ug/l 2.0 01/05/05 11:04 BCK 120.82-1 1.1,1-Trichloroethane NO ug/l 0.50 01/05/05 11:04 BCK 71-55-6 1,1.2-Trichloroethane NO ug/l 0.50 01/05/05 11:04 BCK 79-00-5 Trichloroethene NO ug/l 0.50 01/05/05 11:04 BCK 79-01.6 Trichlorofluoromethane NO ug/l 0.50 01/05/05 11:04 BCK 75-69-4 1,2,3-Trichloropropane NO ug/l 0.50 01/05/05 11:04 BCK 96-18-4 1.2,4-Trimethylbenzene NO ug/l 0.50 01/05/05 11:04 BCK 95-63-6 1,3.5-Trimethylbenzene NO ug/l 0.50 01/05/05 11:04 BCK 108-67-8 Vinyl chloride NO - ug/l 0.50 01/05/05 11:04 BCK 75-01-4 Xylene (Total) NO ug/l 0.50 01/05/05 11:04 BCK 1330-20.7 m&p-Xylene NO ug/l 1.0 01/05/05 11:04 BCK o-Xylene NO ug/l 0.50 01/05/05 11:04 BCK 95-47-6 Toluene-d8 (S) 86 % 01/05/05 11:04 BCK 2037-26-5 4-Bromofluorobenzene (S) 103 % 01/05/05 11:04 BCK 460-00-4 Dibromofluoromethane (S) 99 % 01/05/05 11:04 BCK 1868-53-7 1,2-Dichloroethane-d4 (S) 91 % 01/05/05 11:04 BCK 17060-07.0 Date: 01/17/05 REPORT OF LABORATORY ANALYSIS Asheville Certification IDs This report shall not be reproduced, except in full, NO Wastewater 40 without the written consent of Pace Analytical Services, Inc. NO Drinking Water 37712 SC Environmental 99030 FL NFL AP FKUR Ahip 1117�` Page: 12 of 48 Charlotte Certification IDs NO Wastewater 12 NO Drinking Water 37706 SC 99006 M hirl AD PA7997 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM racn.t i x mrunmH I lUN Please Print Clearly or Type Facility Name: �c af5 �naerrcan/ Permit Name (if different): /JV1149104Kj `""""' It^ G875t✓ County (CM (Smle) (hp) Contact Person: cierrK N Telephone #: Well Location/ Site Name:No. of Wells to be Sampled:-i- ��__ Ilrom Permle Well Identification Number (from Permit): /t4d-.i! I I ForGroundwaterTreatmentSystems Well Depth: 1, ft. Well Diameter: Z in. Check One: ❑ Influent (98) Screened Interval: .3 ft. to 1.3 ft. ❑Effluent (99} Depth to Water Level: 10, o ft. below measuring point. Measuring Point (M.P.) is: 2_&- ft..above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/Ted before sampling: - 3 Date sample collected: Field analysis: pH 71 '� , Specific Conductance _ uMhos Temp. 16 °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION. GROUNDWATER SECTION 1696 MAIL SERVICE CENTER PERMIT it: EXPIRATION DATE: 3- 31 -d �a Non-Discharge_W_n 6oU 6c' UIC NPDES F F P I ITED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Rotary Distributor Other: Remediation: Land Application of Sludge NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: See L$J 7 Laboratory Name: 19ACZ Certification No. ` C PARAMETERS (Samples for metals were collected unfilteredr,,�_YES —NO and field acidified ✓ YES COD mg/1 Coliform: MF Fecal /100m1 Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total (/-I/-llo mg/1 pH (when analyzed units TOC /- 6 --05 3,7 mg/1 Chloride (1-3-0 -55.5 mg/I Arsenic mg/1 Grease and Oils _ mg/I Phenol mg/I Sulfate mg/l Specific Conductance uMhos Total Ammonia mg/I TKNas N .... -- .--------------------------- mg/i Nitrite (NO2) as N mg/1 Nitrate (NO3) as N mg/1 Phosphorus: Total as P _ mg/1 Orthophosphate _ mg/I AI - Aluminum mg/I Ba - Barium mg/I Ca - Calcium /-14-os 97 mg/I Cd - Cadmium _ mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/1 K - Potassiu Mg -Magnesium l-lk o5 4 mg/I Mn - Manganese mg/I — NO) Ni - Nickel mg/1 Pb - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen rr /I Other (Specify Compounds and Concert alien Units ORGANICS: (GC,GC/MS,HPLC) N w (Specify test and method #. Attach lab report.) cr Report Attached? Yes, (1) No_(0) , VOC method 0 _ method ff = I acMnalytical ® www-pacelabs.coin Lab Sample No: 925136962 Client Sample1ID: MW #11 #4050 uufmMJ voIaLl Ies 6230 VOCs by i8260, low level Benzene Bromobenzene Bromochloromethane Bromodichlorlomethane Bromoform I Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzen�e Chloroethane Chloroform Chloromethane 2-Chlorotolulene 4-Chlorotoluene 1,2-Dihromo-3-chloropropane Dibromochloromethane 1,2-DibromoeIthane (EDB) Dibromomethane 1.2-Dichlorobenzene i 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,2-Dichloroethene (Total) 1.1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-0i'chloroethene 1,2-Oichloropropane 1.3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene , cis-1,3-Dichloropropene trans-1.3-Dichloropropene Diisopropyl ether Date: 01/171 1 05 I I Asheville Certification) IDs NC Wastewater 4b NC Drinking Water 37712 SC Environmental 99030 FL NFLAP FR784R Pace Analytical Services, Inc. 2225 Riverside Drive Asheville, X 28804 Phone: 828.254.7176 Fax., 628.252.4618 Lab Project Number: 9284858 Client Project ID: MONITORING WELLS Project Sample Number: 9284858-015 Date Collected: 12/30/04 12:20 Matrix: Water Date Received: 12/30/04 14:10 Results Units Report Limit Analyzed By CAS No. Qual RegLmt Method: EPA 8260 NO ug/l 0.50 01/05/05 11:30 BCK 71-43-2 NO ug/,1 0.50 01/05/05 11:30 BCK 108-86-1 NO ug/l 0.50 01/05/05 11:30 BCK 74-97-5 NO ug/l 0.50 01/05/06 11:30 BCK 75-27-4 NO ug/l 0.50 01/05/05 11:30 BCK 75-25-2 NO ug/l 0.50 01/05/05 11:30 BCK 74-83-9 NO ug/l 0.50 01/05/05 11:30 BCK 104-51-8 NO ug/l 0.50 01/05/05 11:30 BCK 135-98-8 NO ug/l 0.50 01/05/05 11:30 BCK 98.06-6 NO ug/l 0.50 01/05/05 11:30 BCK 56-23-5 NO ug/l 0.50 01/05/05 11:30 BCK 108-90-7 NO ug/l 0.50 01/05/05 11:30 BCK 75-00-3 NO ug/l 0.50 01/05/05 11:30 BCK 67-66-3 NO ug/l 0.50 01/05/05 11:30 BCK 74-87-3 NO ug/l 0.50 01/05/05 11:30 BCK 95-49-8 NO ug/l 0.50 01/05/05 11:30 BCK 106-43-4 NO ug/l 2.0 01/05/05 11:30 BCK 96-12-8 NO ug/l 0.50 01/05/05 11:30 BCK 124-48-1 NO ug/l 0.50 01/05/05 11:30 BCK 106-93-4 NO ug/l 0.50 01/05/05 11:30 BCK 74-95-3 NO ug/l 1.0 01/05/05 11:30 BCK 95-50-1 NO ug/l 1.0 01/05/05 11:30 BCK 541-73-1 NO ug/l 1.0 01/05/05 11:30 BCK 106-46-7 NO ug/l 0.50 01/05/05 11:30 BCK 75-71-8 NO ug/l 0.50 01/05/05 11:30 BCK 75-34-3 NO ug/l 0.50 01/05/05 11:30 BCK 107-06-2 NO ug/l 0.50 01/05/05 11:30 BCK 540-59-0 NO ug/l 0.50 01/05/05 11:30 BCK 75-35-4 NO ug/l 0.50 01/05/05 11:30 BCK 156-59-2 NO ug/l 0.50 01/05/05 11:30 BCK 156-60-5 NO u9/l 0.50 01/05/05 11:30 BCK 78-87-5 NO ug/l 0.50 01/05/05 11:30 BCK 142-28-9 NO ug/l 0.50 01/05/05 11:30 BCK 594-20-7 NO ug/l 0.50 01/05/05 11:30 BCK 563-58-6 NO ug/l 0.50 01/05/05 11:30 BCK 10061-01-5 NO ug/1 0.50 _01/05/05 11:30 BCK 10061-02-6 NO ug/l 0.50 01/05/05 11:30 BCK 108-20-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. p�-Cpq Page: 17 of 48 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706, SC 99006 FI NIFI AP FR7R97 aceAnalytical www.pacelabs.com Lab Sample No: 925136962 Client Sample ID: MW #11 #4050 Pace Analytical Services, Inc. 2225 Riverside Drive Asheville, All? 28804 Phone: 828.254.7176 Fax: 828.252.4618 Lab Project Number: 9284858 Client Project ID: MONITORING WELLS Project Sample Number: 9284858-015 Date Collected: 12/30/04 12:20 Matrix: Water Date Received: 12/30/04 14:10 Parameters Results Units Report Limit Analyzed By CAS No. Qual ReaLmt Ethylbenzene NO ug/l 0.50 01/05/05 11:30 BCK 100-41-4 Hexachloro-1,3-butadiene ND ug/l 2.0 01/05/05 11:30 BCK 87-68-3 Isopropylbenzene (Cumene) ND ug/l 0.50 01/05/05 11:30 BCK 98-82-8 p-Isopropyltoluene ND ug/1 0.50 01/05/05 11:30 BCK 99-87-6 Methylene chloride NO ug/l 2.0 01/05/05 11:30 BCK 75-09-2 Methyl-tert-butyl ether NO ug/l 0.50 01/05/05 11:30 BCK 1634-04-4 Naphthalene NO ug/l 2.0 01/05/05 11:30 BCK 91.20-3 n-Propylbenzene NO ug/l 0.50 01/05/05 11:30 BCK 103.65-1 Styrene NO ug/l. 0.50 01/05/05 11:30 BCK 100-42-5 1.1.1,2-Tetrachloroethane NO ug/l 0.50 01/05/05 11:30 BCK 630-20-6 1,1.2,2-Tetrachloroethane ND ug/l 0.50 01/05/05 11:30 BCK 79-34-5 Tetrachloroethene ND ug/l 0.50 01/05/05 11:30 BCK 127-18-4 Toluene ND ug/l 0.50 01/05/05 11:30 BCK 108-88-3 1.2,3-Trichlorobenzene ND. ug/l 2.0 01/05/05 11:30 BCK 87-61-6 1.2,4-Trichlorobenzene NO ug/l 2.0 01/05/05 11:30 BCK 120-82-1 1,1.1-Trichloroethane ND ug/l 0.50 01/05/05 11:30 BCK 71-55-6 1,1.2-Trichloroethane ND ug/l 0.50 01/05/05 11:30 BCK 79-00-5 Trichloroethene NO ug/l 0.50 01/05/05 11:30 BCK 79-01-6 Trichlorofluoromethane NO ug/l 0.50 01/05/05 11:30 BCK 75-69-4 1,2,3-Trichloropropane NO ug/l 0.50 01/05/05 11:30 BCK 96-18-4 1.2,4-Trimethylbenzene - ND ug/l 0.50 01/05/05 11:30 BCK 95-63.6 1.3.5-Trimethylbenzene ND ug/l 0.50 01/05/05 11:30 BCK 108-67-8 Vinyl chloride ND ug/l 0.50 01/06/05 11:30 BCK 75-01-4 Xylene (Total) NO ug/l 0.50 01/05/05 11:30 BCK 1330.20-7 m&p-Xylene NO ug/l 1.0 01/05/05 11:30 BCK o-Xylene NO ug/l 0.50 01/05/05 11:30 BCK 95-47-6 Toluene-d8 (5) 97 9 01/05/05 11:30 BCK 2037-26-5 4-Bromofluorobenzene (S) 99 R 01/05/05 11:30 BCK 460-00-4 Dibromofluoromethane (S) 100 X 01/05/05 11:30 BCK 1868-53-7 1.2-Dichloroethane-d4 (S) 93 % O1/05/05 11:30 BCK 17060-07-0 Date: 01/17/05 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 FI KIM AP FA79AA REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. min n Page:. 18 of 48 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC^r 99006 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: CF)AT-5 4r•7e P/cyit1 Permit Name (if different): Contact Person: l Fd Well Location/ Site Name: County_. /'I : u uwe.I r Telephone #: gag- 756 - No. of Wells to be Sampled:,,,.-._„ Well Identification Number (from Permit): Mill/ 0 11 For Groundwater Treatment Systems Well Depth: /3 ft. Well Diameter: - 42- in. Check One: ❑ Influent (98) Screened Interval: 3 ft. to 1-3 it. ❑ Effluent (99) Depth to Water Level: eft. below measuring point. Measuring Point (M.P.) is: a. G ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: . 75Date sample collected: Field analysis: pH 1• `/ , Specific Conductance _.. uMhos Temp. _/ 9 OC, Odor Appearance PARAMETERS (Samples for metals were collected COD mg/l Coliform: MF Fecal /looml Coliform: MF Total /loom) (Note: Use MPN method for highly turbl samples) Dissolved Solids: Total rr n a mg/I pH (when analyzed) units TOG 15r7r7 q 3, 3 mg/I Chloride M3.ldqmg/I Arsenic mg/I Grease and Oils mg/I Phenol - mg/I Sulfate 1 Dy 1 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N ... mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT It: EXPIRATION DATE:.3 Non -Discharge WQQO�SIo 03 UIC - NPDES TYPE QF ERMITTED OPERATION BEING MONITORED t/ Lagoon Remedialion: Infiltration Gallery Spray Field Rotary Distributor Other: Remediation: Land Application of Sludge NOTE: Values should reflect dissolved and colloidal concentrations. N t Date sample analyzed: .SEE AO t.J Laboratory Name: 'Ptice p Certification No. `aL9 O tered' YES _,NO and field acidified Nitrite (NO2) as N mg/1 Nitrate (NO3) as N mg/I Phosphorus: Total as P _ mg/I Orthophosphate mg/1 Al - Aluminum mg/1 Ba - Barium Ca - Calcium _£(19 0 `1 I q mg/I mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassiu mg/I Mg - Magnesium ?h0 oy 3• mg/I Mn-Ma nganese I mg/I YES NO) Ni - Nickel mg/I Ph - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) O (Specify test and method Ii. Attach le Report Attached? Yes_(1) r VOC : method It =_ method It = method 0 = GROUNDWATER QUALITY MONITORING: FACILITY INFORMATION Please Print Clearly or Type Facility Name: CDIITS 1jA9VrCd / Permit Name (if different): - Facllity Address: P D Bolt 363 MAR,fa �s'r°`0 ejr 01875d County /11 ` J7owell (CRY) c woo) Rnl Contact Person: 3'£R� a4_, /Z' � ��e✓ Telephone #: >L<ig-75"6 'y/// Well Location/ Site No. of Wells to be Sampled:-1 _ Well Identification Number (from Permit): M -Al d /a For Groundwater Treatment Systems Well Depth: 13 ft. Well Diameter: in. Checkone: ❑ Influent (98) Screened Interval: 3 ft. to 13 ft. ❑ Effluent (99) Depth to Water Level: 9,8 ft. below measuring point. Measuring Point (M.P.) is: 3 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/balled before sampling: /. aS Date sample collected: -'/- O Field analysis: pH 7.5 , Specific Conductance uMhos Temp. _/ $_°C, Odor Appearance PARAMETERS (Samples for metals were collected unfiltered ✓ YES COD mg/I Nitrite (NO2) Coliform: MF Fecal /100ml Nitrate (NO3) Coliform: MF Total /100ml Phosphorus: (Note: Use MPN method for highly turbl samples O) Dissolved Solids: Total /I 47G mg/I pH (when analyzed) 314Y 7.5 units TOC Elf 710 mg/I Chloride )3 110 mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate 13 1 y r/. S mg/I Specific Conductance uMho_,; Total Ammonia mg/I TKN as N ... mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT M EXPIRATION DATE: /c7-3 J - £ Non -Discharge UIC NPDES A1C60044R5r3 TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remedialton: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: S£E' ,BE /Oi.) Laboratory Name: PAGC N Certification No. ` o .91 _NO and field acidified as N mg/I as N mg/I Total as P mg/I Orthophosphate mg/I Al - Aluminum Mg/1 Ba - Barium mg/I Ca - Calciumum Cd _ Cadmi�— mg/I Chromium: Total mg/l Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassiu mg/l Mg - Magnesium R /o oy J3 mg/I Mn - Manganese mg/I La _tGYES _NO) O Ni - Nickel I— mg/I Pb - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC). (Specify test and method #. Attach lab 1 Report Attached? Yes --(I) No VOC method # method # method It �iiL)I print or type GW-59 Sig rl ire of P Mee (or Authorized Agen ) Rev. 03/2000 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: coa-T arr e-A; carj PERMIT Well Location/ Site Name: County iyr = tiara E-I/ Telephone #: 8a8-956 - t1/l/ No. of Wells to be'Sampled: ,.: I �_._.. Well Identification Number (from Permit): /N W F /3 For Groundwater Treatment Systems Well Depth: /s ft. Well Diameter: a in. Cheek One: ❑ Influent (98) Screened Intervals S ft, to /-5 ft. . [] Effluent (99) Depth to Water Level: //. f ft. below measuring point. Measuring Point (M.P.) is: Q. 7 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: /. / Date sample collected: R- y-O S1 Field analysis: pH 7• y , Specific Conductance _uMhos Temp. / 9 °C, Odor Appearance I'_ARAMETE (Samples for metals were collected COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly t rb d samples) Dissolved Solids: Total B 10 S mg/I pH (when analyzed) 3 DN 7. `iunits TOC 8 /7 mg/I Chloride V1 310 306 mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate 8 l ON .< S. 0 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N ... mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION; GROUNDWATER SECTION 1636 MAIL SERVICE CENTER EXPIRATION DATE: NPDES NCCOUY,dYJ TYTYPE.QF PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Remedialion: Rotary Distributor Land Application of Sludge NOTE: Sr Values should reflect dissolved and CP colloidal concentrations. CD Date sample analyzed: C !3 r o cd C:) CP Laboratory Name: /9 Certification No. e/0 YES —NO and field acidified r/ YES _ NO) Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P ___ mg/I Orthophosphate mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium A /D oy yG mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassiu mg/I Mg - Magnesium j,hq o t/ WnT mg/I Mn - Manganese mg/I Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) v2 v�lJ,�lps (Specify test and method #. Attach lab'te*oti't`" Report Attached? Yes_(1) No lfG(Kj VOC : method # = method # method # = GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name:-- COAT.5 Arno-,q CAN Well Location/ Site County-- M - jL-'0WC- Telephone #: SR 8. 73'6 - No. of Wells to be Sampled:; Well Identification Number (from Permit):,Mbt( l`1 For Groundwater Treatment Systems Well Depth: /.S ft. Well Diameter: c2 in. Check One: ❑ Influent (98) Screened Interval: S ft. to /3 ft, ❑ Effluent (99) Depth to Water Level: 7 le_ ft. below measuring point. Measuring Point (M.P.) above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/balled before sampling: a•75, Date sample collected: $- V- o `i Field analysis: pH 7• q , Specific Conductance _uMhos Temp. 19 °C, Odor Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT it: EXPIRATION DATE: TYPE.OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE• Values should reflect dissolved and t colloidal concentrations. 0% O Date sample analyzed: SEE 13E00tti O Laboratory Name: A4E en Certification No. y0 L3AFIAMETERS (Sample's for metals were collected unfiltered_ie!�'—YES —NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100m1 Phosphorus: Total as P—_ mg/I (Note: Use MPN method for highly t hi' samples) Orthophosphate mg/l Dissolved Solids: Total S IP 5a3mgll Al - Aluminum mg/I pH (when analyzed) 3 TOG 911710 0 7. `!units V so mg/I Be - Barium mg/I Ca — Calcium7(a mg/l Chloride 6 11.3 lb I9 mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate 8_71 SAO q 0 mg/I Hg - Mercury mg/I Specific Conductance Total Ammonia uMhos mg/I K - Potasstu mg/I Mg - Magnesium $410,10 y1 mg/I TKN as N ... ___ mg/I Mn - Manganese mg/l V'YES _NO) Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Gortcentralion Units) ORGANICS: (GC,GC/MS,HPLC) Fail JF�lG (Specify test and method #. Attach lab QDrt.) � Report Attached? Yes_(1) No �(0 VOC method # = method # _ method # _ GW-59A COMPLIANCE REPORT FORM Permit # W6000051,03 (Submit one each monitoring period with GfV-59forms.) (Jc 00o j4,Z+43 1 Enter date monitoring results were due: (Scg 30 ) Will this monitoring report (GW-59 and GW-59A) YES NO be submitted after the established due date? I � 2 Was any required information missing on the GW-59 report forms? YES NO IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. I i 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing I YES NO identification plate, area overgrown, etc.)? Ijthe answer is "Yes ", contact the. Regional Ofce jorguidance. 4 Are any monitored constituents equal to or above the established standards? YES NO If the answer to question 4 is NO",, skip to section B. if the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentrations) exceeding standards in the space provided below: Fin fl-} l l .$wl.fe�fe = 4i (o wweJ /� i m W i3 ; OtEsofv�f Soles = 5�!$ rmy/e M10 14 ' DiS5oiuc4 Sol cds 5503 0$12 -e 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is NO", skip to section B. If the answer to question 5 is `7ES'; list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). `J�� ATfi4c�t>'1rtP�st� 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO rr If the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUiDANCE, if the answer is "NO", monitoring wells maybe improperly located; contact the Regional Office. i Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? i ✓ If the answer to question 7is'YES", describe those actions in the space provided below. If the answer to question 7 is "NO'; contact the Regional Office within 90 days: an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation; Fines, and/orpena/ties. 8 The person completing this portion (G W-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that fhe above information was evaluated and the Infotriatign subm(tte��his •y T L Y "c F "tti w5 iW`` ri] repgrt,(Compiiance Repoli GW 5C istrue and complete-to�the besi'pf my knowlec)ge z c Sig tureof Permittee (or Authorized Agent) Date Gw'-59A 12/8/2003 Coats American Sevier Finishing Plant Samples Exceeding The Ground Water Standards MW 10 MW 11 MW 12 MW 13 MW 1'4 04/23/2002 TDS 530 mg/I 520 m9/1 Sulfate 370 mg/I 300 m9/1 08/06/2002 TDS 510 mg/1 Sulfate 290 mg/I 370 mg/l 12/03/2002 TDS 850 m9/1 630 m' /I Sulfate 560 mg/I 12/03/2003 TDS 620 mg/I 650 mg/I 620 mgll Sulfate 04/14/2004 TDS 710 530 610 780 mg/I 780 mg/I Sulfate 440 Note: Ground water standard for TDS 500 mg\I Ground water standard for Sulfate 250 mg\I sample water.123 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION I Please Print Clearly or Type Facility Name: CORD-S AM£Rrr-AN PERMIT #: -----�Y•`===----`�_ - -Non--Disrhe Faci Contact Person: IF-K Well Location/ Site Name: County /N = t7Owe-ll Telephone #:696782756 - 1//// No. of Wells to'be Sampled: Well Identification Number (from Permit): 41 Wy a Well Depth: 7S ft. Well Diameter: Screened Interval: A/ A ft. to m& _ It. Depth to Water Level: q6 ft. below measuring point. Measuring Point (MR) is:-" ft. above, land surface. Gallons of water pumped/bailed before sampling: Field analysis: pH 79 , Specific Conductance Temp. —hL°C, Odor - A PA.f1AMETE (Samples for metals were collected COD mg/I Coliform: MF Fecal /100ml Colfform: MF Total /100ml (Note: Use MPN method for highly turbi samples) Dissolved Solids: Total Al 0 mg/I pH (when analyzed) 8 units TOC l7 0 0.5 IT Chloride 7,� 81 o mg/1 Arsenic mg /l Grease and Oils mg/l Phenol mg/I Sulfate 9 r D� .45.0 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N. ...... mg/I. For Groundwater Treatment Systems in. Check One:❑ Influent (98) ❑ Effluent (99) Relative M.P. Elevation in ft.: Date sample collected: 0V —uMhos ppearance NPDES DEPARTMENT OF ENVIRONMENT 6 NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER EXPIRATION DATE:3 - TYPE-F PERMITTED OPERATION BEING MONITORED; Lagoon Remediation: Infiltration Galletya Spray Field Remediation: t 'Rotary Distributor Land Application of Sludge CIN Other: C3 NOTE: Values should reflect dissolved and colloidal concentrations. nn a E C E Date sample analyzed: 6-jr �Vf Laboratory Name; P r- Certification No. y0 l SEP 10 2004 tered v YES _NO and ffold acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P— _ ___ mgA Orthophosphate mg/l Al - Aluminum mg/l Ba - Barium mg/I Ca - Calciu070 mg/l Cd - Cadmium —mg/I Chromium: Total mg/l Cu - Copper mg/l Fe -Iron mg/I Hg - Mercury' mg/I K - Potassiu mg/I Mg - Magnesium — mg/I Mn - Manganese mg/I ✓ 'YES NO GROUNDWATER SECTION Ni - Nickel ASHEVILLE REGIONAL OFnT l Pb - Lead mg/I Zn - Zinc mg/l Ammonia Nitrogen mg/l Other (Specify Compounds anAm-*1ration Units) ORGANICS: (GC,GG/MS,HPLC) `v 1 (Specify test and method #. Attach lab report.) Report Attached? Yes_(1) No ✓ (0) VOC : method H = method 8 = method # = GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INE RO MATION Please Print Clearly or Type Facility Name: COATS AMFR/CAN Permit Name (if different): Facility Address; P O sox 369 MAR;eIA strae° AlC County— --- M `- Dowe'l% —� ' Contact E Stale Iz�M Contact Person: M" .Telephone #:gd8•SG - 5/1// Well Location/ Site Name: AS No. of Wells to be Sampled:—�_ Well Identification Number (from Permit): MW s I U For Groundwater Treatment Systems Well Depth: I S ft. Well Diameter:Q in. Check One: ❑ Influent (98) Screened Interval: S ft, to _ ) S_ it. ❑ Effluent (99) Depth to Water Level: f y , ft. below measuring point. Measuring Point (M.P.) is:,Q�J ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 13 7 Date sample collected: R- `I- 0 Field analysis: pH 7.6 Specific Conductance —.uMhos Temp. ) 9 . °C, Odor Appearance PAgAMETER (Samples for metals were collected u COD mg/I Coliform: MF Fecal /loom[ Coliform: MF Total /looml (Note: Use MPN method for highly turhl samples) Dissolved Solids: Total 81, 0 160 mg/l pH (when analyzed) 8 3 0r 7. L units TOC 7 OY 1--a-mg/I _ Chloride 8 /3 < 5, 6 mg/I Arsenic mg/I Grease and Oils mg/I Phenol - Sulfate 8 / De! .53 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N.. mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: EXPIRATION DATE: 3 - 3 / - D 6 Non -Discharge W G 000,5 !0 03 UIC NPDES D(PEDEPERULTTIFD OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge NOTE: Values should reflect dissolved and CZ) - colloidal concentrations. N F Date sample analyzed: 5EE ZE)O rJ Laboratory Name: PACF- 8 Certification No. 4/0 O tered_// YES —NO and field acidified Nitrite (NO2) as N mg/1 Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Orthophosphate mg/I Al - Aluminum mg/l Be - Barium Ca - Calcium le /0 D 5.07 mg/I mg/1 Cd - Cadmium mg/I Chromium: Total mg/l Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/1 K - Potassiu mg/I Mg - Magnesium 8L o51 a. SI mg/I Mn - Manganese mg/l YES _ NO) Nf - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC)`e,o,, FCT (Specify test and method #. Attach la ts Port Report Attached? Yes_([) No ✓ (0) VOC method # = _ method # = method It = tr ar GW-59 G -h J `3 0 Rev. 0312000 a Sig ure ermiltee (or Authorized .gent) e ✓ GROUNDWATER QUALITY MONITORING: RT FORM FACILITY INFORIAATION Please Print Clearly or Type Facility Name: COATS flTvl fJ� Permit,Name (if different): Contact Person: Well Location/ Site Telephone 9: ARE756 No. of Wells to be Sampled: Well Identification Number (from Permit): M W Well Depth: is ft. Well Diam ter:_ Screened Interval: __L it. to It. Depth to Water Level: _7 ft. below measuring point. Measuring Point (M.P.) is: °—`� ft. above land surface. Gallons of water pumped/bailed before sampling: 3. 0 Field analysis: pH V. I , Specific Conductance Temp. _L.°C, Odor A p.ABAMETER (Samples for metals were collected COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for Wanly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) S•%-oy 2—, units TOC mg/1 Chloride mg/I Arsenic mg/I Grease and Oils mg/I Phenol _ mg/I Sulfate mg/1 Specific Conductance uMhos Total Ammonia mg/1 TKN as N ... _ mg/1 For Groundwater Treatment Systems in• Check One:❑ Influent (98) ElEffluent (99) Relative M.P. Elevation in n.: Date sample collected: ______._ uMhos ppearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT it: EXPIRATION DATE: La( 3/—v7 Non-DischargeUIC NPDES8LGO tlat,_ TYPE F PF IM TTED OPERATION BEING MO ITORED Lagoon Remediation: InRltr �gn Gaile Spray Field Remedialion: ��' Rotary Distributor Land Application of S`k� e c Other:r� z z NOTE: values should reflect dissolved and zM 1 o colloidal concentrations. D-M o o-i 4a Date sample analyzed: Se5jE Zf)ln te 2 -z Tn Laboratory Name: M Certification No. Bred t/ YES _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P — mg/I Orthophosphate mg/I At - Aluminum mg/I Ba - Barium mg/1 Ca - Calcium mg/1 Cd - Cadmium _mg/I Chromium: Total mg/1 Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I V IIf ,' iris YES _ NO) Ni - Nickel mg/I Pb - Lead mg/1 Zn - ZincIg/l,. ; Ammonia Nitrogen ng/l Other (Specify Compounds and Concentration Units'} C co fr.;ti ORGANICS: (GC,GC/MS,HPLC)v.- (Specify test and method #. /attach lab�report.) Report Attached? Yes v, (1) No — (0) VOC : method It = 6 c; ,JO DD : method it = : method If = or GW-59 Rev. 0312000 �FaceAnalytical ° www.pacelabs.com Lab Sample No: 924210867 Client Sample ID: MW #14 GRAB #1915 Pace Analytical Services, Inc. 2225Riverside Drive Asheville, NC 28804 Phonei 828.254.7176 Faxt 828.252.4618 Lab Project Number: 9266660 Client Project ID: MONITORING WELLS Project Sample Number: 9266660-003 Date Collected: 05/07/04 08:05 Matrix: Water Date Received: 05/07/04 11:19 Parameters Results Units Report Limit Analyzed By CAS No. Qual R.eoLmt GC Volatiles GC VOCs in Water Method: SM 6230D Benzene ND ug/l 0.50 05/18/04 06:40 STC 71-43-2 Bromobenzene ND ug/l 0.50 05/18/04 06:40 STC 108-86-1 Bromochloromethane ND ug/l 0.50 05/18/04 06:40 STC 74-97-5 _ Bromodichloromethane ND ug/l 0.50 05/18/04, 06:40 STC 75-27-4 Bromoform ND ug/l 0.50 05/18/04 06:40 STC 75-25-2 Bromomethane ND ug/1 0.50 05/18/04 06:40 STC 74-83-9 n-Butylbenzene ND ug/l 1.0 05/18/04 06:40 STC 104-51.8 sec-Butylbenzene NO ug/l 0.50 05/18/04 06:40 STC 135-98-8 tert-Butylbenzene ND ug/l 0.50 05/18/04 06:40 STC 98-06-6 Carbon tetrachloride ND ug/1 0.50 05/18/04 06:40 STC 56-23-5 Chlorobenzene ND ug/l 0.50 05/18/04 06:40 STC 108-90-7 Chloroethane ND ug/l 0.50 05/18/04 06:40 STC 75-00-3 Chloroform NO ug/l 0.50 05/18/04 06:40 STC 67-66-3 Chloromethane ND ug/l 2.0 06/18/04 06:40 STC 74-87-3 2-Chlorotoluene ND ug/l 0.50 05/18/04 06:40 STC 95-49-8 4-Chlorotoluene ND ug/l 0.50 05/18/04 06:40 STC 106-43-4 1,2-Dibromo-3-chloropropane NO ug/l 2.0 05/18/04 06:40 STC 96-12-8 Dibromochloromethane ND ug/l 0 50 05/18/04 06.40 STC 124-48-1 a m m, <= L mp Z mm OSl iV o z�, � N o T nz ^ uYu m 1,2-Dibromoethane (EDB) NO ug/l 0.50 05/18/04 06:40 STC 106.93-4 Dibromomethane ND ug/1 0.50 05/1B/04 06:40 STC 74-95-3 1.2-Dichlorobenzene ND ug/l 1.0 05/18/04 06:40 STC 95-50-1 1.3-Dichlorobenzene NO ug/l 1.0 05/18/04 06:40 STC 541-73-1 1,4-Dichlorobenzene ND ug/l 1.0 05/18/04 06:40 STC 106-46-7 Dichlorodifluoromethane NO ug/1 0.60 05/18/04 06:40 STC 75-71-8 1,1-Dichloroethane ND ug/1 0.50 05/18/04 06:40 STC 75-34-3 1,2-Dichloroethane NO ug/l 0.50 05/18/04 06:40 STC 107-06-2 1,1-Dichloroethene NO ug/l 0.50 05/18/04 06:40 STC 75-35-4 cis-1.2-Dichloroethene ND ug/l 0.50 05/18/04 06:40 STC 156-59-2 trans-1,2-Dichloroethene ND ug/l 0.50 05/18/04 06:40 STC 156-60-5 1,2-Dichloropropane NO ug/l 0.50 05/18/04 06:40 STC 78-87-5 1,3-Dichloropropane NO ug/l 0.50 05/18/04 06:40 STC 142-28-9 2.2-Dichloropropane NO ug/l 0.50 05/18/04 06:40 STC 594-20-7 1.1-Dichloropropene ND ug/l 0.50 05/18/04 06:40 STC 563-58-6 cis-1,3-Dichloropropene ND ug/l 0.50 05/18/04 06:40 STC 10061-01-5 trans-1,3-Dichloropropene ND ug/l 0.50 05/18/04 06:40 STC 10061-02-6 Diisopropyl ether NO ug/l 0.50 05/18/04 06:40 STC 108-20-3 Ethylbenzene ND ug/l 0.50 05/18/04 06:40 STC 100-41-4 Date: 05/19/04 Page: 5 of 14 REPORT OF LABORATORY ANALYSIS Asheville Certification IDs This report shall not be reproduced, except in full, Charlotte Certification IDs NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 ' NC Drinking Water 37712 _, NC Drinking Water 37706 SC Environmental 99030 ���. SC 99006 FL NELAP E87648 "(�eC FL NFI AP Fn7n97 ceAnaWicai www.pacelahs.cem Lab Sample No: 924210867 Client Sample ID: MW #14 GRAB #1915 Pace Analytical Services, Inc. 2225 Riverside Drive Asheville, NC 28804 Phone: 828.254.7176 Fax.' 828.252.4618 Lab Project Number: 9266660 Client Project ID: MONITORING WELLS Project Sample Number: 9266660-003 Date Collected: 05/07/04 08:05 Matrix: Water Date Received:'05/07/04 11:19 Parameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt Hexachloro-1,3-butadiene ND ug/l 2.0 05/18/04 06:40 STC 87-68-3 Isopropylbenzene (Cumene) NO ug/l 0.50 05/18/04 06:40 SIC 98-82-8 p-Isopropyltoluene ND ug/l 1.0 05/18/04 06:40 STC 99-87-6 Methylene chloride ND ug/l 2.0 05/18/04 06:40 STC 75-09-2 Methyl-tert-butyl ether NO ug/l 0.50 05/18/04 06:40 SIC 1634-04.4 h h l ND /1 2 0 05/18/04 06 40 STC 91-20 3 Nap t a ene ug n-Propylbenzene ND ug/l 0.50 05/18/04 06:40 STC 103-65-1 Styrene ND ug/l 0.50 05/18/04 06:40 STC 100-42-5 1,1.1,2-Tetrachloroethane ND ug/l 0.50 05/18/04 06:40 STC 630-20-6 1,1,2,2-Tetrachloroethane ND ug/l 0.50 05/18/04 06:40 STC 79-34-5 Tetrachloroethene ND ug/l 0.50 05/18/04 06:40 STC 127-18-4 Toluene ND ug/l 0.50 05/18/04 06:40 STC 108-88-3 1.2,3-Trichlorobenzene NO ug/l 2.0 05/18/04 06:40 STC 87-61-6 1,2,4-Trichlorobenzene ND ug/l 2.0 05/18/04 06:40 SIC 120-82-1 1.1,1-Trichloroethane ND ug/l 0.50 05/18/04 06:40 STC 71-55-6 1.1,2-Trichloroethane ND ug/l 0.50 05/18/04 06:40 SIC 79-00-5 Trichloroethene ND ug/l 0.50 05/18/04 06:40 STC 79-01-6 Trichlorofluoromethane ND ug/l 0.50 05/18/04 06:40 SIC 75-69-4 1,2,3-Trichloropropane ND ug/l 0.50 05/18/04 06:40 STC 96-18-4 c F== m p c Z m Y I O N o D m O o a =z I c� m 1.2,4-Trimethylbenzene NO ug/l 0.50 05/18/04 06:40 SIC 95-63-6 1,3.5-Trimethylbenzene ND ug/l 0.50 05/18/04 06:40 STC 108-67-8 Vinyl chloride ND ug/l 0.50 05/18/04 06:40 STC 75-01-4 m&p-Xylene NO ug/l 0.50 05/18/04 06:40 STC o-Xylene ND ug/l 0.50 05/18/04 06:40 STC 95-47-6 1-Chloro-3-fluorobenzene (S) 108 % 05/18/04 06:40 STC 625-98-9 Date: 05/19/04 Asheville Certification IDs NO Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 FL NELAP E87648 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. M CCOq Page: 6 of 14 i Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 h MR AP LR79W GROUNDWATER QUALITY MONITORING: CE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: CnR'f5 AMEA i colt% Permit Name (if different).,. Well Location/ Site Name: County Telephone #: RRS-756 No. of Wells to be Sampled: Well Identification Number (from Permit): M kW 'f l-j For Groundwater Treatment Systems Well Depth: 15 ft. Well Diameter: in. Check One: ❑ Influent (98) Screened Interval: r it, to /'�: ft. ❑ Effluent (99) Depth to Water Level: 10. S ft. below measuring point. Measuring Point (M.P.) is:Q. 2 ft. above land surface. Relative M.P. Elevation in It.: Gallons of water pumped/bailed before sampling: /. 6 Date sample collected: ' 7- D`l Field analysis: pH , Specific Conductance---.._.._._uMhos Temp. °C, Odor Appearance PAFIA IETERS (Samples for metals were collected COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total pH (when analyzed) -Oy mg/I 7. 1units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/1 Phenol _ mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia — mg/I TKN as N ... — mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT it: EXPIRATION DATE: /�!- f/-✓`, Non -Discharge-_ UIC NPDES M00124VA2 y � TYPE F PERMITTED OPERATION BEING MONITO6rn- DLagoon Remedialiolt:lnfiltrafionlMSpray Field Remediation: M Rotary Distributor . Land Application of Slu ao z Other: NOTE: Values should reflect dissolved and 25^ z" N colloidal concentrations. o o Date sample analyzed: cE " %O U) mz Laboratory Name: Certification No. y0 YES _NO and field acidified _jZ YES _ NO) Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P — mg/I Orthophosphate mg/I Al - Aluminum mg/I Ba - Barium mg/1 Ca - Calcium mg/I Cd - Cadmium _ mg/l Chromium: Total mg/I Cu - Copper_ mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I WE 01m Ni - Nickel mg/I Pb - Lead 91fl/I Zn - Zincrlg/lc Ammonia Nitrogen Other (Specify Compounds and Concentr;%iJn 1.1.4 ): ORGANICS: (GC,GC/MS,FIPLC) (Specify test and method #. A tach lab report.) Report Attached? Yes(1) No(o) VOC : method 1t = 4d30 -D method 11 = method it = �PaceAnalytical www.pacelabs.com Lab Sample No: 924210842 Client Sample ID: MW #13 GRAB #1914 Pace Analytical Services, Inc. 2225�iiverside Drive Asheville, NC 28804 Phone., 828.254.7176 Fax.• 828.252.4618 Lab Project Number: 9266660 Client Project ID: MONITORING WELLS Project Sample Number: 9266660-002 Date Collected: 05/07/04 07:55 Matrix: Water Date Received: 05/07/04 11:19 Parameters Results Units Report Limit Analyzed By CAS No. - Qual RegLmt GC Volatiles GC VOCs in Water Method: SM 6230D Benzene ND ug/l 0.50 05/18/04 05:58 STC 71-43-2 Bromobenzene NO ug/l 0.50 05/18/04 05:58 STC 108-86-1 Bromochloromethane NO ug/l 0.50 05/18/04 05:58 STC 74-97-5 Bromodichloromethane ND ug/l 0.50 05/18/04 05:58 STC 75-27-4 Bromoform ND ug/l 0.50 05/18/04 05:58 STC 75-25-2 Bromomethane ND ug/l 0.60 05/18/04 05:58 STC 74-83.9 n-Butylbenzene NO ug/l 1.0 05/18/04 05:58 STC 104.51.8 sec-Butylbenzene NO ug/l 0.50 05/18/04 05:58 STC 135-98-8 tert-Butylbenzene ND ug/1 0.50 05/18/04 05:58 STC 98-06-6 Carbon tetrachloride NO ug/l 0.50 05/18/04 05:58 STC 56-23-5 Chlorobenzene NO ug/l 0.50 05/18/04 05:58 STC 108-90-7 Chloroethane ND ug/1 0.50 05/18/04 05:58 STC 75-00-3 Chloroform NO ug/l 0.50 05/18/04 05:58 STC 67-66-3 Chloromethane NO Ilg/l 2.0 05/18/04 05:58 STC 74-87-3 2-Chlorotoluene NO ug/l 0.50 05/18/04 05:58 STC 95-49-8 T m ill <o Mz � z Sn? m o MD I I nr� o TO f� 4-Chlorotoluene ND ug/l 0.50 05/18/04 05:58 STC 106-43-4 1,2-Dibromo-3-chloropropane NO ug/l 2.0 05/18/04 05:58 STC 96-12-8 Dibromochloromethane NO ug/l 0.50 05/18/04 05:58 STC 124-48-1 1,2-Dibromoethane (EDB) ND ug/1 0.50 65/18/04 05:58 STC 106-93-4 Dibromomethane ND ug/l 0.50 05/18/04 05:58 STC 74-95-3 1,2-Dichlorobenzene ND ug/l 1.0 05/18/04 05:58 STC 95-50-1 1.3-Dichlorobenzene NO ug/l 1.0 05/18/04 05:58 STC 541.73-1 1,4-Dichlorobenzene ND ug/l 1.0 05/18/04 05:58 STC 106.46-7 Dichlorodifluoromethane NO 'ug/l 0.50 05/18/04 05:58 STC 75-71-8 1,1-Dichloroethane ND ug/1 0.50 05/18/04 05:58 STC 75-34-3 1,2-Dichloroethane ND ug/l 0.50 05/18/04 05:58 STC 107.06.2 1.1-Dichloroethene NO ug/l 0.50 05/18/04 05:58 STC 75.35.4 cis-1.2-Dichloroethene NO ug/l 0.50 05/18/04 05:58 STC 156-59-2 trans-1.2-Dichloroethene ND ug/l 0.50 05/18/04 05:58 STC 156.60-5 1,2-Dichloropropane ND ug/l 0.50 05/18/04 05:58 STC 78-87-5 1,3-Dichloropropane ND ug/l 0.50 05/18/04 05:58 STC 142-28-9 2,2-Dichloropropane NO ug/l 0.50 05/18/04 05:58 STC 594-20-7 1.1-Dichloropropene ND ug/l 0.50 05/18/04 05:58 STC 563.58.6 cis-1,3-Dichloropropene ND ug/l 0.50 05/18/04 05:58 STC 10061-01-5 trans-1.3-Dichloropropene NO ug/l 0.50 05/18/04 05:58 STC 10061-02-6 Diisopropyl ether NO ug/1 0.50 05/18/04 05:58 STC 108-20-3 Ethylbenzene ND ug/l 0.50 05/18/04 05:58 STC 100-41-4 Date: 05/19/04 Page: 3 of 14 REPORT OF LABORATORY ANALYSIS Asheville Certification IDs This report shall not be reproduced, except in full, Charlotte Certification IDs NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NG Drinking Water 37712 «j„ NC Drinking Water 37706 SC Environmental 99030 Sc 99006 FL NELAP E87648 r 7�{pQ������a. "/�1GICL41 FI NFI API FA7R97 aceAnalytical° www.pacelabs.com Lab Sample No: 924210842 Client Sample ID: MW #13 GRAB #1914 Pace Analytical Services, Inc. 2225AIverside Drive Asheville, NC 28804 Phone: 828.254.7176 Fay': 828.252.4618 Lab Project Number: 9266660 Client Project ID: MONITORING WELLS Project Sample Number: 9266660-002 Date Collected: 05/07/04 07:55 Matrix: Water Date Received: 05/07/04 11:19 Parameters Results Units Report Limit Analyzed By CAS No. Qual 022Lmt Hexachloro-1,3-butadiene ND ug/l 2.0 05/18/04 05:58 STC 87-68-3 Isopropylbenzene (Cumene) ND ug/l 0.50 05/18/04 05:58 STC 98-82-8 p-Isopropyltoluene NO ug/l 1.0 05/18/04 05:58 STC 99.87-6 Methylene chloride NO ug/l 2.0 05/18/04 05:58 STC 75-09-2 Methyl-tert-butyl ether ND ug/l 0.50 05/18/04 05:58 STC 1634-04-4 Naphthalene ND ug/l 2.0 05/18/04 05:58 STC 91-20-3 n-Propylbenzene ND ug/l 0.50 05/18/04 05:58 STC 103-65-1 w� Styrene ND ug/l 0.50 05/18/04 05:58 STC 100-42-5 o 1,1,1,2-Tetrachloroethane ND ug/l 0.50 05/18/04 05:58 STC 630-20-6 �Iz� 1,1,2,2-Tetrachloroethane ND ug/l 0.50 05/18/04 05:58 STC 79-34-5 Tetrachloroethene NO ug/1 0.50 05/18/04 05:58 STC 127-18-4 Toluene .ND ug/l 0.50 05/18/04 05:58 STC 108.88-3 0 1,2,3-Trichlorobenzene ND ug/l 2.0 05/18/04 05:58 STC 87-61.6 m 1.2.4-Trichlorobenzene ND ug/1 2.0 05/18/04 05:58 STC 120-82-1 0 1,1,1-Trichloroethane ND ug/l 0.50 05/18/04 05:58 STC 71-55-6 z 1,1,2-Trichloroethane ND ug/l 0.60 05/18/04 05:58 STC 79-00-5 Trichloroethene ND ug/l 0.50 05/18/04 05:58 STC 79-01-6 Trichlorofluoromethane ND ug/l 0.50 05/18/04 05:58 STC 75-69-4 1,2,3-Trichloropropane ND ug/1 0.50 05/18/04 05:58 STC 96-18-4 1,2,4-Trimethylbenzene ND ug/1 0.50 05/18/04 05:58 STC 95-63-6 1,3,5-Trimethylbenzene ND ug/l 0.50 05/18/04 05:58 STC 108-67-8 Vinyl chloride ND ug/l 0.50 05/18/04 05:58 STC 75-01-4 m&p-Xylene ND ug/l 0.50 05/18/04 05:53 STC o-Xylene NO ug/l 0.50 05/18/04 05:58 STC 95-47-6 1-Chloro-3-fluorobenzene (S) 102 X 05/18/04 05:58 STC 625-98-9 Date: 05/19/04 Asheville Certification IDs NO Wastewater 40 NO Drinking Water 37712 SC Environmental 99030 FL NFI_AP F8784R REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. ai` ryry� i Page: 4 of 14 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 Sc 99006 FI NFI 6P P27907 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION [I n I Please Print Clearly or Type Facility Name: CoA l �i�ERr CArU Permit Name (if differenceO: _ Well Location/Site County "t �'r'� Telephone #: WE- 75la ` `/LII No. of Wells to be Sampled: —1. Well Identification Number (from Permit): Mtn/ /d For Groundwater Treatment Systems Well Depth: /_3 ft. Well Diameter: in. Check One: ❑ Influent (98) Screened Interval: 3 ft. to _1-S_ it. ❑ Effluent (99) Depth to Water Level: /D ft. below measuring point. Measuring Point (M.P.) is: 3 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/balled before sampling: _/1.3 Date sample collected: 5-7-0 Field analysis: pH 7.) , Specific Conductance uMhos Temp. )_3 ...°C, Odor Appearance PARAMETERS (Samples for metals were collected COD mg/1 Coliform: MF Fecal 1100ml Coliform: MF Total /100ml (Note: Use MPH method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) 5-6-D 7. / units TOC mg/I Chloride mg/I Arsenic mg/1 Grease and Oils mg/I Phenol mg/I Sulfate mg/1 Specific Conductance uMhos Total Ammonia mg/I TKN as N ..— — mg/I GW-59 Rev. 03/2000 DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER DUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT It: " EXPIRATION DATE: /9'-s r - ri y Non -Discharge__ UIC NPDES 1N/Cooe2v0L13 TYP F PERMITTED OPERATION BEING MONI ORED Lagoon Remediafion: Infiltrat =�G ery Spray Field Remediafion: Rotary Distributor — Land Application of 16dg� z Other: NOTE: Values should reflect dissolved and nm o colloidal concentrations. � Date sample analyzed: SEE ttiJ Tz Laboratory Name: C Certification No. ` Q YES —NO and field acidified Nitrite (NO2) as N mg/l Nitrate (NO3) as N mg/I Phosphorus: Total as P_ 1119/1 Orthophosphate mg/1 Al - Aluminum mg/l Ba - Barium mg/I Ca - Calcium mall Cd - Cadmium mg/l Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/l K - Potassium mg/l Mg - Magnesium mg/I Mn - Manganese mg/l lZYES _NO) Ni - Nickel mg/I Pb - Leal �mgll Zn - Zinc m /1 Ammonia Nitrogen r4 Other (specify Compounds and Gonce tiog anits ORGANICS: (GC,GCIMS,HPLC) ' (Specify test and method #. aqttttach lab report.) Report Attached? Yes_Y_(1) No _ (0) VOC : method # = l cZ30 D Permittee (or Authorized Agent) Name and Title - Please print or type method # = method # = Signature of Permittee (or Authorized Agent) (Date) a Paoce Analytical ° wvvm pacelahs.com Lab Sample No: 924210776 Client Sample ID: MW #12 GRAB #1913 Pace Analytical Services, Inc. 2225'Riverside Drive Asheville, NC 28804 Phone: 828.254.7176 Fax: 828.252.4618 Lab Project Number: 9266660 Client Project ID: MONITORING WELLS Project Sample Number: 9266660-001 Date Collected: 05/07/04 07:45 Matrix: Water Date Received: 05/07/04 11:19 Parameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt GC Volatiles GC VOCs in Water Method: SM 6230D Benzene ND ug/1 0.50 05/18/04 05:17 STC 71-43-2 Bromobenzene ND ug/l 0.50 05/18/04 05:17 STC 108-86-1 Bromochloromethane ND ug/1 0.50 05/18/04 05:17 STC 74-97-5 Bromodichloromethane NO ug/1 0.50 05/18/04 05:17 STC 75-27-4 Bromoform NO ug/l 0.50 06/18/04 05:17 STC 75-25-2 Bromomethane ND ug/l 0.50 05/18/04 05:17 STC 74-83-9 n-Butylbenzene ND ug/l 1.0 05/18/04 05:17 STC 104-51-8 sec-Butylbenzene NO ug/l 0.50 05/18/04 05:17 STC 135-98-8 tert-Butylbenzene ND ug/1 0.50 05/18/04 0517 STC 98-06-6 Carbon tetrachloride ND ug/l 0.50 05/18/04 05:17 STC 56-23-5 Chlorobenzene ND ug/l 0.50 05/18/04 05:17 STC 108-90-7 Chloroethane ND ug/1 0.50 05/18/04 05:17 STC 75-00-3 Chloroform ND ug/l 0.50 05/18/04 05:17 STC 67-66-3 Chloromethane NO ug/l 2.0 05/18/04 05:17 STC 74-87-3 2-Chlorotoluene ND ug/l 0.50 05/18/04 05:17 STC 95-49-8 4-Chlorotoluene ND /1 0 50' OS/18/04 05.17 4 `T � M c ml*m z !a I mlm IV O31 o Z ^c C~ oo T nz I� m ug STC 106-43 REPORT OF LABORATORY ANALYSIS Asheville Certification IDs This report shall not be reproduced, except in full, Charlotte Certification IDs NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 , +==o NC Drinking Water 37706 SC Environmental 99030 0 SC 99006. FL NELAP E87648 FI NFI AP Gn7ao� Pace Analytical Services, Inc Analytical e222� Asheville, Riverside Drive Aville, NC 28804 Phone: 828,254.7176 www.pacelabs.com Fax 828.252.4618 Lab Project Number: 9266660 Client Project ID: MONITORING WELLS Lab Sample No: 924210776 Project Sample Number: 9266660-001 Date Collected: 05/07/04 07:45 Client Sample ID: MW #12 GRAB #1913 Matrix: Water Date Received; 05/07/04 11:19 Parameters Results Units Report Limit Analyzed By CAS No. Qual 'RegLmt Mexachloro-1.3-butadiene ND ug/l 2.0 05/18/04 05:17 SIC 87-68-3 Isopropylbenzene (Cumene) 1.1 ug/l 0.50 05/18/04 05:17 STC 98-82-8 p-Isopropyltoluene NO ug/l 1.0 05/18/04 05:17 STC 99-87-6 Methylene chloride NO ug/l 2.0 05/18/04 05:17 STC 75-09-2 Methyl-tert-butyl ether NO ug/l 0.50 05/18/04 05:17 STC 1634-04.4 Naphthalene NO ug/l 2.0 05/18/04 05:17 STC 91-20-3 n-Propylbenzene NO ug/l 0.50 05/18/04 05:17 STC 103-65-1 Styrene NO ug/l 0.50 05/18/04 05:17 SIC 100-42-5 1,1,1,2-Tetrachloroethane NO ug/l 0.50 05/18/04 05:17 STC 630-20-6 1,1,2.2-Tetrachloroethane NO ug/l 0.50 05/18/04 05:17 STC 79-34-5 Tetrachloroethene NO ug/l 0.50 05/18/04 05:17 STC 127-18-4 Toluene ND ug/l 0.50 05/18/04 05:17 STC 108-88-3 1,2.3-Trichlorobenzene NO ug/l 2.0 05/18/04 05:17 STC 87-61-6 1,2,4-Trichlorobenzene NO ug/l 2.0 06/18/04 05:17 STC 120-82.1 1,1,1-Trichloroethane NO ug/l 0.50 05/18/04 05:17 STC 71-55-6 1,1.2-Trichloroethane NO ug/l 0.50 05/18/04 05:17 STC 79-00-5 Trichloroethene NO ug/l 0.50 05/18/04 05:17 STC 79-01.6 Trichlorofluoromethane NO ug/l 0.50 05/18/04 05:17 STC 75-69-4 1,2,3-Trichloropropane NO ug/l 0.50 05/18/04 05:17 STC 96-18-4 1,2,4-Trimethylbenzene NO ug/l 0.50 05/18/04 05:17 STC 95-63-6 1.3,5-Trimethylbenzene NO ug/l 0.50 05/18/04 05:17 STC 108-67-8 Vinyl chloride NO ug/l 0.50 05/18/04 05:17 STC 75-01-4 m&p-Xylene NO ug/l 0.50 05/18/04 05:17 STC o-Xylene NO ug/l 0.50 05/18/04 05:17 STC 95-47-6 1-Chloro-3-fluorobenzene (S) 110 % 05/18/04 05:17 STC 625-98-9 Date: 05/19/04 Asheville Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 FL NELAP E87648 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. \M AL p Jy O� ' Page: 2 of 14 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI AIPI AP cv7c07 Pace Analytical Services, Inc. 2225 Riverside Drive Analytical® Asheville, NC 28804 Phone. 828,254.7176 www.pacelahs.com Fax. 828.252.4618 Lab Project Number: 9266660 Client Project ID: MONITORING WELLS PARAMETER FOOTNOTES Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic testing was performed at our Pace Charlotte laboratory unless otherwise footnoted. Method 9071B modified to use ASE. All pH, Free Chlorine, Total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended immediate hold time. ND Not detected at or above adjusted reporting limit NC Not Calculable J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit MDL Adjusted Method Detection Limit (S) Surrogate Date: 05/19/04 Asheville_ Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 FL NELAP E87648 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. it IC1A.�1= a ✓v m � < o L c � z z m O ma I 031 N o r-n O = Z ll l�Il O m Page: 7 of 14 Charlotte Certification IDs NC Wastewater 12 PVC Drinking Water 37706 SC 99006 h NCI AO C07907 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: C'Q,97- fl/1 eAicald Permit Name (if different): Well Location/ Site Name: Well Identification Number (from Permit): Mbl 47' eR Well Depth: 75 It. Well Diameter: Screened Interval: WA ft. to AL;j It. Depth to Water Level: y0• 1 It. below measuring point. Measuring Point (M.P.) is:—Q_2 ft. above land surface. Gallons of water pumped/bailed before sampling: 69' Field analysis: pH 7. a , Specific Conductance Temp. IV. I °C,Odor A PAf AMETERS (Samples for metals were collected COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total y/ty/oT ►t) mg/l pH (when analyzed) N 7. units TOC 'f� nN < 0, 60 mg/I Chloride s/I5/0q 7,6mg/I Arsenic mg/I 'Grease and Oils mg/I Phenol mg/I Sulfate Liflal 04 -4 S. 0 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N ._ mg/I County nS b041e-.1 / Telephone #: 8199 -754 - No. of Wells to be Sampled:,,.__.,._„ �_ in. For Groundytaler Treatment Systems CheckOne:[] Influent (98) ❑ Effluent (99) Relative M.P. Elevation in ft.: Date sample collected: '! uMhos ppearance DEPARTMENT OF ENVIRONMENT S NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: EXPIRATION DATE: 3 -3 / - 06 Non-DischargejA[a6nOS6 63 UIC NPDES P F PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: SF_er L3r l ou/ Laboratory Name: e4e c Certification No. go YES _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Orthophosphate mg/I AI - Aluminum mg/I Ba - Barium mg/I Ca - Calcium N oN a a mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassiu mg/I Mg - Magnesium Yda oy / d mg/I Mn - Manganese mg/I c. Ni- Nickel Pb - Lead Zn - Zinc Ammonia Nitrogen Other (Specify Comp( amE rr CO w mg/I mg/I mg/I and Cdncenjrah`or) Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach JJ��I Report Attached? Yes_(1) ��)o VOC : method # 5< . method # method If = GW-ss . Y `—C S— Z_ —o Rev. 0312000 Sig ire of rmiltee (of Authorized Agent) (0) GROUNDWATER QUALITY MONITORING: Please Print Clearly or Type Facility Name: Coars Ann ea; r 9,J Permit Name (if different):_ --- Well Location/ Site Name: County M ` Qou/Gl) Telephone #: 919- 75'k - 4// I No. of Wells to be Well Identification Number (from Permit): AA W tiP I 0 For Groundwater Treatment Systems Well Depth: 18 ft. Well Diameter:- in. Check One: ❑ Influent (98) Screened Interval: S it. to )9 ft. ❑ Effluent (99) Depth to Water Level: /5• 5 ft. below measuring point. Measuring Point (M.P.) is: ell 3 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: _ Y2 Date sample collected: y-/y- 0 Field analysis: pH 7. / , Specific Conductance uMhos Temp. la. 8 °C, Odor Appearance PAFRIMETER (Samples for metals were collected COD mg/I Coliform: MF Fecal 1100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samplos) Dissolved Solids: Total N 7/0 mg/I pH (when analyzed) 11 7.1 units TOC y V < mg/l Chloride S mg/1 Arsenic mg/I Grease and Oils mgll Pheno1 Sulfe a W.21 04 0110 mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N . — mg/I DEPARTMENT OF ENVIRONMENT& NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: EXPIRATION DATE: 3 - s/. D tb Non-DischargeW40005'603 UIC NPDES — --- - -- TYPE_ �F PERMITTED OPERATION BEING MONITORED _� Lagoon Remedialion: Infiltration Gallery Spray Field Remedialion: Rotary Distributor Land Application of Sludge Other: n .r. N T • Values should reflect dissolve _ colloidal concentrations. so � w rz D C D C4 m� Date sample analyzed: CZ)Laboratory Name: M" Certification No. z� NO and field acidified _L YES Nitrite (NOp) as N mg/I Nitrate (NO3) as N mg/1 Phosphorus: Total as P mg/1 Orthophosphate mg/I Al - Aluminum mg/1 Ba - Barium mg/I Ca - Calcium N oN (o. Smg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassiu mg/I Mg - Magnesium '! SIN J.3mg/I Mn - Manganese mg/I Ni - Nickell Pb - Lead I l C Zn - Zinc' Ammonia Nitrogen Other (Specify Compounds and IME ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes_(1) .No ��(0) VOC : method # = method # = method # = GROUNDWATER QUALITY MONITORING: r L • i L FACILITY INFORMATION Please Print Clearly or Type Facility Name: CI)AT S rqMr-R j r and Permit Name (if different):_ Well Location/ Site Name: County- M s t tuwcr Telephone #: 9Ag -7S4 ' St/ 1 / r No. of Wells to be Sampled:...__ Well Identification Number (from Permit): Anur/ W / / I For Groundwater Treatment Systems Well Depth: 13 ft. Well Diameter: a ill. Check One: ❑ Influent (98) Screened Interval: 3 It. to L-3 ft. 1 ❑ Effluent (99) Depth to Water Level: _1_0 ft. below measuring point. Measuring Point (M.P.) is:R. 4 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 1.0 Date sample collected: y-rq- 0 Field analysis: pH 6,9 , Specific Conductance Temp. 13. 2 °C, Odor Appearance . pA�RAJ IET -_a (Samples for metals were collected COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbl sem les) Dissolved Solids: Total �5 9/1 pH (when analyzed)11 69 units TOC N/23/nu ),7 mg/I Chloride Y/ J.,�I17o Q I mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N .— —._ mg/I uMhos DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: EXPIRATION DATE: 3 - 3 / - OG Non-Discharge1V0000 s G03 UIC TYPE J F PERMITTED OPERATION BEING MONITORED Lagoon Remediation:Iroftfagon4alle Spray Field Remediation: Rotary Distributor Land Applic Other. NOTE: Values should reflect dissolved and my - colloidal concentrations. �m a o� Date sample analyzed: E F_/ n1 oti Laboratory Name: c o 0 Certification No. ered ✓ YES NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Orthophosphate mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium 1A mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassiu mg/I Mg - Magnesium A g mg/I Mn - Manganese mg/I YES Ni - Nickel mg/I Pb - Lean Zn - Zinc -Oia/I Ammonia Nitrogen —4 g/I Other (Specify Compounds and Concentration Uri@ ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes—(1) No_(0) VOC method # = method # ,tJrJr i or Noe method # = GW-59 Rev. 0312000 GROUNDWATER QUALITY MONITORING: CO EPORT FORM Facility Name: COi}TS rgFvl ERt Glf.ti Permit Name (if different): Well Location/ Site Name: Print Clearly or Type County An's Uorae I I Telephone #:. OAS -?S6 -J/ll1 No. of Wells to be Sampled:.._- ._.. Well Identification Number (from Permit): ' 105 Well Depth: 13 N. Well Diameter: Screened Interval: J ft. to 13 It. Depth to Water Level: eft. below measuring point. Measuring Point (M.P.) is: 3 ft. above land surface. Gallons of water pumped/bailed before sampling: 1. a Field analysis: pH 7• 0 , Specific Conductance Temp. 14, H °C, Odor A PARAMETERS (Samples for metals were collected COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total A00ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total gh(410N (610 mg/I pH (when analyzed) ylr,2lot/ 7.ounits TOC g1A(144 13 mg/I Chloride %&/ /Oq 180_ mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate glAVoy 4-5, 1) mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N . __ mg/1 For Groundwater Treatment Systems in• check One:❑ Influent (98) ElEffluent (99) Relative M.P. Elevation in ft.: Date sample collected: _cZ uMhos ppearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT if: EXPIRATION DATE: /a(-1I -u I Non -Discharge UIC NPDES /dC o00 Na (13 TYPE PERMITTED nED OPERATION BEING MONITORED Lagoon Remediatio ;• Infiltration rAllnry Spray Field Reme Rotary Distributor _ Land Other: NOTE: Values should reflect dissolved a d� ITS colloidal concentrations. m A Date sample analyzed: S ,r341Otrl Laboratory Name: Ham " o Certification No. zi0 �z T ]ir ered L/ YES _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/1 Phosphorus: Total as P _ mg/1 Orthophosphate mg/I AI - Aluminum mg/I Ba - Barium mg/1 Ca - Calcium 7//mg/l Cd - Cadmium mg/1 Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Ni - Nickel mg/I Pb - Lead mgfl Zn - Zinc rol o Ammonia Nitrogen moll o� Other (Specify Compounds and ConcentratioQnitW, ORGANICS: (GC,GCIMS,HPLC) cam" (Specify test and method #. Attach lab report.) Report Attached? Yes_(1) No _ (0) VOC : method # = : method ft = or : method # = IVA—WI] GW-59 Rev. OMOOO GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: GoATz ,04NfPri; /,4"2 Permit Name (if different): _ Well Location/ Site Name: Please Print Clearly or Type County Al C- 150tc%l 1 Telephoneft: 929-Wk-yer r No. of Wells to be Sampled: _ I Well Identification Number (from Permit): MW 0 7.3 For Groundwater Treatment Systems Well Depth: ft. Well Diameter:'_ in. Check One: ❑ Influent (98) Screened Interval: 5 It. to_L45* it. ❑ Effluent (99) Depth to Water Level: 16• S ft. below measuring point. Measuring Point (M.P.) is: &?v 7 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: 1,7 Date sample collected: Field analysis: pH G, A , Specific Conductance uMhos Temp. 13. 6 OC, Odor Appearance PARAMETERS (Samples for metals were collected I COD mg/I Coliform: MF Fecal /100m1 Coliform: MF Total /100m1 (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 4/ly/0U ISomg/I pH (when analyzed) og 4,91 units TOC mg/I Chloride N mg/I Arsenic mg/I Grease and Oils mg/l Phenol mg/I Sulfate 4 al y 49mg/I Specific Conductance uMhos Total Ammonia mg/l TKN as N .._ — mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT ft: EXPIRATION DATE: /A Non -Discharge UIC NPDES a iQQQ ya y3 TYPE FIRERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Feld Remediation: _ Rotary Distributor Land Application of Slud e,� Other: a NOTEa Values should reflect dissolved and `- colloidal concentrations.( Date sample analyzed: B.F 1 o^, � Laboratory Name: Ph ce- f-" g Certification No. 1/0 YES _NO and field acidified Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/l Orthophosphate mg/I Al - Aluminum mg/I Be - Barium mg/I Ca - Calcium %414 l/ Lf of q mg/I Cd - Cadmium mg/l Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassiu mg/I Mg - Magnesium __q -1or( lsmgll Mn - Manganese mg/I YES _ NO) Ni - Nickel Pb - Lead mg/1 Zn - Zinc mg/I Ammonia Nitrogen mg/l Other (Specify Compounds and Concentratlg&Unitt ORGANICS: (GC,GC/MS,HPLC) ry (Specify test and method If. AttaclLleb Report Attached? Yes_(1f-7 Nt VOC : method H = method tf = method 8 = (0) F rTU C Fru GROUNDWATER QUALITY MONITORING: Please Print Clearly or Type Facility Name: CaA'r.S AmLR;L a,,d Facility Well Location/ Site County M `:' "Uwel r Telephone#: $z6-7S6—�llr No. of Wells to be Sampled:; T Well Identification Number (from Permit): MW 'lv' )14 For Groundwater Treatment Systems Well Depth: /S It. Well Diameter: A in. Check One: ❑ Influent (98) Screened Interval: 3' It. to 15, it. ❑ Effluent (99) Depth to Water Level: 7, ( R. below measuring point. Measuring Point (M.P.) is:- ft. above land surface. Relative M.P. Elevation in It.: Gallons of water pumped/bailed before sampling: __J,-L Date sample collected: - ry N-pri Field analysis: pH 6,2 , Specific Conductance uMhos Temp. / Q. t0 °C, Odor Appearance PARAMETERS (Samples for metals were collected COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 4/tyloy 1190 mg/I pH (when analyzed) r)tf tp, 9 units TOC V 4 1/n mg/I Chloride yr(lt nr-I 13 mg/l Arsenic mg/1 Grease and Oils mg/I Phenol mg/I Sulfate y ON /-5'mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N — mg/I PERMIT ff: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER DUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER EXPIRATION DATE: TYPE F P .RMITTED OPERATION BEING MONITORED Lagoon Remediation:Infiltration Gallery Spray Field Remediadon: Rotary Distributor Land Application of Sludge R , Other. NOTE: Values should reflect dissolved and W colloidal concentrations. Date sample analyzed: S xza 1 Laboratory Name: Certification No. Al0 :eyed ✓ YES _NO and field acidified Nitrite (NO2) as N mg/1 Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Orthophosphate mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium/AA-/04 69 mg/I Cd - Cadmium� mg/1 Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/l Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium y/a-7,10V yy mg/1 Mn - Manganese mg/I L/ YES _N, Ni - Nickel PID - qri Zn - Zinc Ammonia Nitrogen_ Other (Specify Compoli r tit ng/1 n ng/I ng/I Units) a c, ORGANICS: (GC,GC/MS,HPLC) �" ^tI�V (Specify test and method #. Attar lab !i rt.) Report Attached? Yes_( NO(0) VOC : method # = ay method # =, method If = `.IV.ai r2-7 3 El 5 G7 7 UVY-59A Coi\' P ' L�NCERch.FORM Permit#'WQ000$6o3 ' (Submit o_�.r each neourtvrine period with Gf{• g a t - 9jorms) NG000�/Lr{3 Enter date monitor results P. ' be sub g were due, t o Will this monitoring report (GW-59 and GW-59q miffed after the established due date? ) :� Was any required the missing on th+ Ow•-59 report forms? IF the answer to question i.or 2 is'yCS•; fist in the space provided beicw the welt id entificationnumber(s) and exp/ain the problems encountered in ob'aining the required information. r Are any of the monitor Oells in need of repair ar maintenance (damaged casing, unlocked or missio ca identification plate, area overgrown, etc.)? lithe answer is "Yes ", con[ccr the Rggionaf Or Ice or g .p, missing Are any J I guidance. y monitored constituents equal to or above the established standards? • If the answer to question 4 is NO'; skip to section 8. if the answer to question 4 is "YES"list the affected wells individually with constituents) and concentrations) exceeding standards in the space provided below: rnwto TD5--110nn?/p - S• If te.: 4Ko +t.ta(-e t1l4112 ` TD5 - 4 to ^4 ( Q ►r1+1It -7M5 - 53oebI �74113-T95^7sorK to For the constituents identified in uestion &J f •TD5 7 $o e-I (,e q 4 above, have standards been exceeded previously for the same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is "NO , skip to section 8. , the answer to question 5 is "YES-, list in the space provided below, each well with constituents) exceeding standards, concentration(s) reported; and sample collection date for each well (for the last twe years). t�'a4, eel the monitoring we� in at or u me answer is :"YES I a11?1 .' OFFICE IMMEDIATELY FOR GUIDANCE. If the answer Is "N0", y be occurring. CONTACT THE REGIONq, located; contact the Regional Office. monitoring wefts may be improperly Ca,�a<�ee! �(� f}s�•�i(!. Rej(ON Q 641cc S-3-0i groundwater qualit yproblem?N,evtouslyapproved actions require, If the answer to question If the ans7 IS "YES ; describe those actions wer to question 7is "NO in the space con�n..,,t.., t ne person completing this portion G the mot form with GW_59.forms for required well 5oahefaddress at the top of the current GW-59 form, -5-0 [I X\ NO X NO YES I NO X 1218/1-003 'y County: MCDOWELL River Basin Report To AROAP Collector. J VANN Region: ARO Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Emergency Yes/No CDC Yes/No Location ID: IP059W00005603MWI l �"WED � P 22 2CG8 ^c'logional Office ..�'- Pro cC.tion VisitlD Loc. Descr.: COATS AMERICAN MW-11 Collect Dale: 0812612008 Collect Time:: Sample Qualifiers and Comments Routine Qualifiers Sample ID: AB34864 PO Number# 8G1208 _ Date Received: 0812812008 Time Received: 07:45 Labworks LoginlD HPARKER D'ate Reported: f I I Repo ,Generated: 9117108 09/17/2008 10:12 1 Sample Depth For a more detailed description of these qualifier codes refer to www.dwqlab.org under Staff Access A -Value reported is the average of two or more determinations B1-Countable membranes with <20 colonies; Estimated B2- Counts from all filters were zero. B3- Countable membranes with more than 60 or 80 colonies; Estimated B4-Filters have counts of both >60 or 80 and < 20; Estimated B5-Too many colonies were present; too numerous to count (TNTC) J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated J3-The sample matrix interfered with the ability to make any accurate determination; Estimated J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated NI -The component has been tentatively identified based on mass spectral library search and has an estimated value LAB N3-Estimated concentration is < PQL and>MDL NE -No established PQL P-Elevated PQL due to matrix interference and/or sample dilution Q1-Holding time exceeded prior to receipt at lab. 02- Holding time exceeded following receipt by lab PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity U. Samples analyzed for this compound but not detected X1- Sample not analyzed forthis compound Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 1 of 3 ROUNDWATER FIELD/LAB FORM Location code ! 1i`017`1'VJU 000Sf.D i `NI W- I I SAMPLE TYPE County M��nwsl( I!—XW/ater Quad No Serial No. ❑ Soil Lat., i 47 9b, q'I Long. Fia o 0 ❑ Other ❑ Chain of Custody North Carolina Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION SAMPLE PRIORITY Routine Lab Number nrJS`(�O I El Emergency (,Gd�77 �}mgvlca Date Received $• ZG•aY Time: -II Rec d By: )0/4/ From:Bus, Courier, Hand Del., Other: Report To: ARO RO, MRO, RRO, WaRO, WiRO, WSRO, Kinston FO, Fed. Trust, Central Off., Other: Shipped by: Bus,ourier tHand D�el1, Other: Purpose: Collector(s): ulle V.;n✓� Date fr R Time 10i iZ F FIELD ANALYSES Owner_ pH 40o Spec. Cond.s4 at 260C Location or Sit Temp.lo °C Odor Description of Appearance Sampling Metl Field Analysis By: Remarks_ I ARnP ATr7RY ANAI YSFS - Data Entry By: Date Reportec Ck: iT,-Pesticide Study, Federal Trust, Other: ono) BOD 310 mg/L iss. Solids 70300 mg/L Ag-Silver46566 u /L O anochlodne Pesticides COD High 340 mg/L Fluoride 951 mg/L AI -Aluminum 46557 u /L O ano hos horns Pesticides COD Low 335 mg/L Hardness: Total 900' mg/L As -Arsenic 46551 u /L Nitrogen Pesticides Colifonn: MF Feca131616 /100m1 Hardness (nonurb) 902 mg/L Ba-Barium 46558 u /L Acid Herbicides Colifoun: MF Total 31504 /100m1 Phenols 32730 ug/i Ca -Calcium 46552 no/L PCBs OC 680 mg/L Specific Cond. 95 pMhos/cm Cd-Cadmium 46559 u /L Turbitlity 76 NTU Sulfate 945 mg/L Cr-Chromium 46559 u )L Residue, Total Suspended 530 mg/L Sulfide 745 . mg/L Cu-Copper 46562 u /L Fe -Iron 46563 u /L Semivolatile Organics Oil and Grease mg/L Hg-Mercury 71900 u /L I TPH-Dlesel Range pH 403 units K-Potassium 46565 m /L Alkalinity to pH 4.5 410 mg/L - Mg -Magnesium 46554 mg/L Alkalinity to pH 8.3 415 mg/L Mn-Manganese 46565 u /L Volatile Organics(VOA bottle Carbonate 445 119/L NH3 as N 610 mg/L Na-Sodium 46556 mg/L TPH-Gasoline Range _ Bicarbonate 440 mg/L TKN as N 625 mglL Ni-Nickel u /L TPH-STEX Gasoline Range Carbon dioxide 405 mg/L NOz+ No, as N 630 mg/L Pb-Lead 46564 u /L Chloride 940 mg/L P: Total as P 665 mg/L Se -Selenium u /L Chromium: Hex 1032 u9/L Nitrate (NO, as N) 620 mg/L Zn-Zinc 46557 u !L Color: True 80 Cu Nitrite (NO2 as N) 615 mg/L LAB USE ONLY .Temperature on arrival (°C): 2• Cyanide 720 mg/L Lab GW.54 REV. 7103 For Dissolved Analysis -submit filtered sample and write'DIS• in block. County: MCDOWELL River Basin Report To AROAP Collector. J VANN Region: ARC Sample Matrix: GROUNDWATER Loc. Type: Monitoring Well Emergency Yes/No CDC Yes/No F WAp Sample ID: r� 4� �p �Q 9O PO Number # F17 C E I" O® y Date Received: 7 r—y Time Received: 0 _P 09 2GG8 C Y Labworks LoginlD Date Reported: Asheville Regional office Report Generated: Aquifer Protection ,aitlD Fly Loc. Descr.: COATS AMERICAN MW-12 zfa Il Location ID: 1P059WQ0005603MWI2 I Collect Date: 08/26/2008 Collect Time:: 10:25 Sample Depth . Sample Qualifiers and Comments AB34815 ARC 0812612008 14:15 KJIMISON 914108 0910c412008 Id 1 J 1QO Routine Qualifiers For a more detailed description of these qualifier codes refer to www.dwqlab.org under Staff Access A -Value reported is the average of two or more determinations , Bi-Countable membranes with <20 colonies; Estimated N3-Estimated concentration is < PQL and>MDL B2-Counts from all filters were zero. NE -No established PQL B3- Countable membranes with more than 60 or 80 colonies; Estimated P-Elevated PQL due to matrix interference and/or sample dilution B4-Filters have counts of both >60 or 80 and < 20; Estimated Q1-Holding time exceeded prior to receipt at lab. BS-Too many colonies were present; too numerous to count (TNTC) Q2- Holding time exceeded following receipt by lab J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity J3-The sample matrix interfered with the ability to make any accurate determination; Estimated U- Samples analyzed for this compound but not detected Js-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated Xi- Sample not analyzed for this compound NI -The component has been tentatively identified based on mass spectral library search and has an estimated value ARO Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 1 of 2 County: MCDOWELL River Basin Report To AROAP Collector. J VANN Region: ARO Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Emergency Yes/No COC Yes/No Location ID: IP059W00005603MW12 -- _ Sample ID: (CY la ; V I"= ® PO Number# r Dale Received: y Time Received: vamp 2 2 2008 ti - . C Labworks LoginlD ' Date Reported: Asheville Regional Office Report Generated: —emu Loc. Descr.: COATS AMERICA MW-12 Collect Date: 08/26/2008 Collect Time:: 10:25 Sample Depth Sample Qualifiers and Comments AB34865 BG1209 08/28/2008 07:45 HPARKER 9117/08 09/17/2008 9 (lgla(�) Routine Qualifiers For a more detailed description of these qualifier codes refer to www.dwglab.org under Staff Access A -Value reported is the average of two or more determinations B7-Countable membranes with <20 colonies; Estimated N3-Estimated concentration is < PQL and >MDL B2-Counts from all filters were zero. NE -No established PQL 63- Countable membranes with more than 60 or 80 colonies; Estimated P-Elevated PQL due to matrix interference and/or sample dilution B4-Filters have counts of both >60 or 80 and < 20; Estimated QI-Holding time exceeded prior to receipt at lab. BS-Too many colonies were present; too numerous to count (TNTC) Q2- Holding time exceeded following receipt by lab J2-Reported value failed to meet QC criteria for either precision or accuracy; Estimated PQL- Practical Quantitafion Limit -subject to change due to instrument sensitivity J3-The sample matrix interfered with the ability to make any accurate determination; Estimated U- Samples analyzed for this compound but not detected J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated X1- Sample not analyzed for this compound N1-The component has been tentatively identified based on mass spectral library search and. has an estimated value LAB Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 1 of 3 rr1 I D: 1 P 059 W 00005603 M W 12 oc. Desc-.: COATS AMERICA MW-12 Visit ID CAS # Analyl Sample temperature Method Reference MIC NC (DWWQ Laboratory Section 12esufts TOC In Ilquld Method Reference APHA5310B-201h Ion Chromatography ILL 2.0 Collect Date: Collect Tune:: 08/26/2008 10:25 Qualifier Units Analyst/Dale Approved By 11 0.9 'C DSAUNDERS MMATHIS 8128108 828108 2.4 mgfL BSWANSON MOVERMAN 82SM8 9/8/08 TITLE_ mgfL MIBRAHIMl MOVERMAN Method Reference EPA300.0 9/4/OB 9/15M8 Chloride 1.0 33 mg/L MIBRAHIMt MOVERMAN Method Reference EPA300.0 9/4108 9115/08 Fluoride 0.4 2.0 U,P mg/L MIBRAHIMt MOVERMAN Method Reference EPA 300.0 9/4108 9115/08 Sulfate 2.0 3.9 mg/L MI13RAHIM1 MOVERMAN Method Reference EPA 300.0 914/08 9115108 Phosphoms_lotal as P In Ilquld 0.02 0.11 mgiL as P MAJAYI CGREEN Method Reference Lac10-115-01-1EF 829108 913108 MET 7429-90-5 AIby ICP 50 86 ug/L PGAUTHIER ESTAFFORD Method Reference EPA 200.7 9/3108 9/11108 7440-38-2 Asby ICPMS 5.0 5.0 U ugfL DSTANLEY ESTAFFORD Method Reference EPA200.8 9/3108 9111108 7440-38-3 Be by ICP 10 53 ugfL PGAUTHIER ESTAFFORD Method Reference EPA200.7 9rM8 9111108 7440-70-2 Caby ICP 0.10 35 mglL PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3108 9111108 7440-43-9 Gdby ICPMS 1.0 1.0 U ugfL DSTANLEY ESTAFFORD Method Reference EPA200.8 913/08 9/11108 7440-47-3 Crby ICPMS 10 10 U ugfL DSTANLEY ESTAFFORD Method Reference EPA200.8 9008 9111/08 7440-50-8 Cuby ICPMS 2.0 4.7 ugtL DSTANLEY ESTAFFORD Method Reference EPA 200.8 M/08 9/11/08 7439-95-4 Mg by ICP 0.10 7.7 mg/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 913/08 9111108 7439_96-5 Mnby_ICP _ _ _ 10 __- 1100 uglL PGAUTHIER ESTAFFORD-- - ---- Methad Reference EPA200.7 - - - - M/08 9111/08 7440-23-4 Na by ICP 0.10 60 mgfL PGAUTHIER ESTAFFORD Method Reference EPA200.7 913103 9111108 Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 2 of 3 NC (JDWQ Laboratory Section Results Sample ID AB34865 F,rmt 1P059WQD005603MW12 Collect Dale: 0812612008 COATS AMERICA MW-12Collect Time:: 10:25 --- nuuq.v..a,oe rul nesuit uua9ner Units Analyst/Date Approved By (Date Method Reference EPA 200.8 913109 9/11/03 7439-92-1 Pb by ICPMS 10 10 U u g2 DSTANLEY ESTAFFORD Method Reference EPA200.8 913108 9111/08 7782-49-2 Be by ICPMS 5.0 5.0 U ugfL DSTANLEY ESTAFFORD Method Reference EPA200.8 913/08 9/11108 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 3 of 3 NC (DWWQ La6oratory Section 12esufts Sample ID AB34815 lion ID: 1 P059WO0005603MW72 Collect Date: 0812612008 Loc. Descr.: COATS AMERICAN MW-12 Collect Time:: 10:25 7011t ID ^�^ ^=•r• ^•= rer� Resort uuannur units nnarysvuate .Approved By/Date Method Reference 8r26108 828/08 Total Dissolved Solids In liquid 12 268 mg1L KJIMISON CGREEN Method Reference APHA2540C.18TH 8/28108 914/08 Laboratory Section>> 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 733-1908 Page 2 of 2 GROUNDWATER FIELD/LAB FORM Location code �Yl3h`1 HJ �[300.SGDiVJ'I tiV-I-� SAMPLE TYPE SAMPLE PRIORITY nty CouM�7eWel� I/� Itlr Routine ❑ L ��)y Quad No _ Serial No. ❑ Soil Emergency �mgrrca Lat. �S L1 133 Long. 89L. 01 lie. & ❑ Other ❑ Chain of Custody Report To: ARO 'FRO, MRO, RRO, WaRO, WiRO, WSRO, Kinston FO, Fed. Trust, Central Off., Other: Shipped by: Bus, owner Hand Del Other: Purpose: Collector(s): JLilie inn ate Time i0. 2., Baseline, - FIELD ANALYSES Owner i mis A "}c pH 40o Spec. Cond.9a at 25°C Location or Site_/ Temp.lo °C Odor Description of sampling Appearance Sampling Method_ Field Analysis By: Remarks I ARr1RATn RY ANAI YSFS of Environment and Natural Resources TER QUALITY -GROUNDWATER SECTION Lab Number 1M!ge1'y Dale Received S-Zfo.cS Time: t�4t� Rec'd By: 1GN� From:Bus, Courier, Other: Data Entry By: Ck: Date Reported: Complaint, Cam fiance LUST, Pesticide Study, Federal Trust, Other: r, rn (urcla one) BDo 310 mg1L D . Solids 70300 mg/L Ag-Silver 4656 u /L Or anochlonne Pesticides COD'High 340 mg/L Fluoride 951 mg/L Aluminum 6557 u /L Or ano hos horns Pesticides COD Low 335 mg/L Hardness: Total 900 mg/L . ✓ As- sent 46551 u /L Nitro en Pesticides Coliform: MF Fecal 31616 /t00m1 Hardness (non-carb) 902 mg/L Ba-Ba " 46558 u /L Acid Herbicides Colifortn: MF Total 31504 1100m1 Phenols 32730 ugll 9 Ca-C ci 46552 molt. PCBs mg/L Specific Cond. 95 pMhos/cm C admiu 46559 u /L Turbidity 76 NTU mg/L ✓ r-Chromium 559 u /L Residue, Total Suspended 530 mg/L Sulfide 745 . mg/L Cu-Copper 46562 u /L Fe -Iron 46563 u /L Semivolatile Organics Oil and Grease mg/L Hg-Mercury71900 u /L 7PH-Oiesel Range 03 units -Potassium 6555 mg/L Alkalinity to pH 4.5 410 mg/L M agnes m 46554 m 1L Alkalinity to pH 8.3 415 mg1L Mn-M nese 46565 u /L Volatile Organics(VOA bottle Carbonate 445 mg/L NH3 as N 610 mg/L Na-Sod' 46556 m /L TPH-Gasoline Range Bicarbonate 440 mg/L TKN as N 625 mg/L elu /L TPH-BTFX Gasoline Ran e Carbon dioxide 405 mg/L NO, t NO, as N'630 mg/L !M-Nic ad46564 u /L mg/L Selenium u /L Chromium: Hex 1032 ug/L Nitrate (NO3 as N) 620 mg/L -Zinc46567 u /L ' Color. True 80 Cu Nitrite (NO2 as N) 615 mg/L LAB USE ONLY .Temperature on arrival (°C): J Cyanide 720 mgJL LaD GW-54 REV. 7103 For Dissolved Analysis -submit filtered sample and write'DIS' in block. GROUNDWATER FIELD/LAB FORM Location code I V(3h`1`A U GOQ5 3Vy1W- I s County MCDQweil Quad No Serial No. Lat. 3.5-47' 33S" Long. ka OI ' f(v, $ Report To: ARO FRO, MRO, RRO, WaRO, WiRO, WSRO, Kinston FO, Fed. Trust, Central Off., Other: Shipped by: Bus, ourier Hand D'e11, Other: Collector(s): �L11ieyanY� I FIELD ANALYSES ❑ Soil ❑ Other ❑ Chain of Custody pH 400 Spec. Cond.9a at 25°C Temo.,o °C Odor Analysis SAMPLE PRIORITY Routine ❑ Emergency Location or Situ Description of sampling Sampling Method_ North Carolina Department of Environment and Natural Resources L Lab Number !J LJ -fa0?/ B�J� V b S Date Received $_oggfQg Time: �}mP. •rica W-1 Redd By: From urier Hand Del., Other: Data Entry By: Ck: Date Reported: iT, Pesticide Study, Federal Trust, Other: one) Sample LABORATORY ANALYSES r t (Pwnpingtime,alr torn" .lc') BOD 310 mg/L Diss. Solids 70300 mg/L Ag-Silver 46566 u /L O anochlorine Pesticides COD High 340 mg/L Fluoride 951 mg/L AI -Aluminum 46557 u /L Or ano hos horns Pesticides COD Low 335 mg/L Hardness: Total 900 mg/L As -Arsenic 46551 ugIL Nitro en Pesticides Colifoon: MF Fecal 31616 /100ml Hardness (non-carb) 902 mg/L Ba-Barium 46558 u L Acid Herbicides Colifonn: MF Total 31504 /loom] Phenols 32730 ug4 Ca -Calcium 46552 mg/L PCBs TOC 680 mg/L Specific Cord. 95 pMhos/cm Cd-Cadmium 46559 u qfL Turbidity 76 NTU Sulfate 945 mg/L Z Cr-Chromium 46559 ugfi, Residue, Total Suspended 530 mg/L Suede 745 mg/L Cu-Copper 46562 u /L Fe -Iron 46563 u /L Semivolable Comics Oil and Grease mg/L Hg-Mercury 71900 u /L TPH-Diesel Ran e pH 403 units K-Potassium 46555 m 2 Alkalinity to pH 4.5 410 mg/L Mg -Magnesium 46554 m /L Alkalinity to pH 8.3 415 mg/L Mn-Manganese 46565 u /L Volatile Or anics(VOA botde Carbonate 445 mg/L NH3 as N 610 mg/L Na-Sodium 46556 m L TPH-Gasoline Range Bicarbonate 440 mg/L TKN as N 625 mg/L Ni Nickel u /L TPH-BTEX Gasoline Range Carbon dioxide 405 mg/L NO2 + NO3 as N 630 mg/L Pb-Lead 46564 u /L Chloride 940 mg/L P: Total as P 665 mg/L Se -Selenium u 2 Chromium: Hex 1032 ug/L Nitrate (N%as N) 620 mg/L Zn-Zinc 46567 u /L Color. True 80 cU Nitrite (NO2 as N) 615 mg/L LAB USE ONLY - .Temperature on arrival (°C): Cyanide 720 mg/L Lab GW-54 REV. 7103 For Dissolved Analysis -submit filtered sample and write'DIS- in block. County: MCDOWELL SampleID:be AB34866 River Basin AROAP-� WAIF �O 9 �G PO Numr# 867210 Retort To rr,, E C'' V E ® V Ito p� y Date Received: 001281200t1 Collector. J VANN `' 4a y Time Received: 07:45 Region: Sample Matrix: ARO GROUNDWATER rr 6 20�8 Jar 1 U U Y ,_, ^ �1-I• r 1,��%J Labworks LoginlD Date Reported: HPARKER 9112/08 Loc.Type: MONITORING WELL Emergency Yes/No ?,shevill� Re_J nal Office Report Generated: 09/1212008 COC Yes/No ¢ protection YisitlD H�]J I Loc. Oescr.: COATS AMERICA MW-13 ^ / Location ID: 1PO59W00005603MW13 Collect Date: 08/26/2008 Collect Time:: 10:35 Sample Depth Sample Qualifiers and Comments Routine Qualifiers For a more detailed description of these qualifier codes refer to www.dwqlab.org under Staff Access A -Value reported is the average of two or more determinations B1-Countable membranes with <20 colonies; Estimated 92- Counts from all filters were zero. 83- Countable membranes with more than 60 or 80 colonies; Estimated 84-Filters have counts of both >60 or 80 and < 20; Estimated BS-Too many colonies were present; too numerous to count (TNTC) J2- Reported value failed_to meet QC criteria for either precision or accuracy; Estimated J3-The sample matrix interfered with the ability to make any accurate determination; Estimated J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated Nt-The component has been tentatively identified based on mass spectral library search and has an estimated value N3-Estimated concentration is < PQL and>MDL NE -No established PQL P-Elevated PQL due to matrix interference and/or sample dilution 01-Holding time exceeded prior to receipt at lab. Q2- Holding time exceeded following receipt by lab PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity U-Samples analyzed for this compound but not detected X1- Sample not analyzed for this compound LAB Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 1 of 2 County: MCDOWELL River Basin Report To AROAP Collector. J VANN Region: ARC Sample Matrix: GROUNDWATER Loc. Type: Monitoring Well Emergency Yes/No CDC Yes/No Location to 1P059W00005603MW73 �OF wArFgo RECEIVE® � r y 6 Y SEP 09 2GG8 Asheville Regional office Loc. Descr.: COATS AMERICAN MW-13 Collect Date: 0812612008 Collect Time:: 10:35 Sample Qualifiers and Comments Sample ID: PO Number # Date Received: Time Received: Labworks LoginlD Date Reported: Report Generated Sample Depth A834816 ARO 08/26/2008 14:15 KJIMISON 914/08 09/04/2008 Um Routine Qualifiers For a more detailed description of these qualifier codes refer to www.dwqlab.org under Staff Access A -Value reported is the average of two or more determinations Bt-Countable membranes with <20 colonies; Estimated 1,13-Estimated concentration is < PQL and >MDL B2-Counts from all filters were zero. NE -No established PQL B3- Countable membranes with more than 60 or 80 colonies; Estimated P-Elevated PQL due to matrix interference and/or sample dilution B4-Filters have counts of both >60 or 80 and <20: Estimated Q1-Holding time exceeded prior to receipt at lab. B5-Too many colonies were present; too numerous to count (TNTC) Q2- Holding time exceeded following receipt by lab J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated PQL- Practice[ Quanlitation Limit -subject to change due to instrument sensitivity J3-The sample matrix interfered with the ability to make any accurate determination; Estimated U- Samples analyzed for this compound but not detected J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated Xt- Sample not analyzed for this compound N1-The component has been tentatively identified based on mass spectral library search and has an estimated value ARO Laboratory Section» 1623 Mail Service Center, Raleigh, INC 27699.1623 (919) 733-3908 Pagel of 2 NC IDWQ La6oratory Section Results Sample ID As34866 n ID: 1P059WQ0005603MW73 Collect Data: O8I26I2008 c. Descc; COATS AMERICA MW-13 Collect Time:: 10:35 VsitlQ Method Reference 7429-90-5 At by ICP 50 Method Reference EPA 200.7 8128108 M8108 84 - ug/L PGAUTHIER ESTAFFORD 913/08 9/11108 7440-38-2 As by ICPMS - 5.0 5.0 U ug/L DSTANLEY ESTAFFORD Method Reference EPA 200.8 9/2/08 9/11/08 7440-38-3 Be by ICP 10 130 ugfL PGAUTHIER - ESTAFFORD Method Reference EPA200.7 913/08 9/11108 7440-70-2 Ca by ICP 0.10 - 33 mglL PGAUTHIER ESTAFFORD Method Reference EPA 200.7 _ M108 9/11108 744043-9 Cd by ICPMS 1.0 1.0 U ugfL DSTANLEY ESTAFFORD - Method Reference EPA 200.8 9Y1J08 9/11/O8 744047-3 Cr by ICPMS 10 10 U ugf- DSTANLEY ESTAFFORD Method Reference EPA200.8 9/2108 9/11/08 7440-50-8 Cu by ICPMS 2.0 390 ug/L DSTANLEY ESTAFFORD Method Reference EPA200.6 90O8 91111O8 7439-954 Mg by ICP 0.10 22 mg/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3N8 '91111O8 7439-96-5 Mn by ICP 10 1000 ug/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 9!3/08 9117/08 7440-234 Na by ICP 0.10 170 mg1L PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3/08 9111108 7440-02-0 NI by ICPMS 10 10 U ugfL DSTANLEY ESTAFFORD Method Reference EPA200.8 912/08 9/11/08 7439-92-1 Pb by ICPMS 10 10 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9008 9/11/08 778249-2 Se by ICPMS 5.0 5.0 U ugfL DSTANLEY ESTAFFORD Method Reference EPA200.8 9/2108 9/11/08 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699.1623, (919) 733-3908 Page 2 of 2 NC DWQ Laboratory Section ResultsSample ID AB34816 n ID: 1P059W00005603MW13 Collect Date: 08f2612008 c. Descr.: COATS AMERICAN MW-13 Collect Time:: 10:35 Vsit ID uuanner units Method Reference M6108 . 8/28108 Total Dissolved Solids In liquid 12 767 mg/L KJIMISON CGREEN Method Reference APHA2540C-18TH 828/08 914108 Laboratory Section>> 1623 Mail Service. Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 2 of 2 GROUNDWATER FIELD/LAB FORM County - MCDOWell ater Quad No Serial No. ❑ Soil Lat.T5- q-7140.8" Long. AF2 ol'17" El Other El Chain of Custody Report To: ARO FRO, MRO, RRO, WaRO, WiRO, WSRO, Kinston FO, Fed. Trust, Central Off., Other: Shipped by: Bus, ourler Hand Del , Other: Purpose: Collector(s): tulle znn Date C Time G: 3S FIELD ANALYSES Owner_ PH 400 Spec. Cond.s, at 250C Location or SI Temp.lo °C Odor Description of Appearance Sampling Mel Boo 310 mg/L COD High 340 mg/L COD Low 335 mg/L Coliform: MF Fecal 31616 /t00ml C liform: MF Total 31504 /loom[ mg/L Turbidity 76 NTU Residue. Total Suspended 530 mg/L pH 403 units Alkalinity to pH 4.5410 mg/L Alkalinity to pH 8.3 416 mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L Carbon dioxide 406 mg/L mg/L Chromium: Hex 1032 ug/L Color: True 80 Cu Cyanide 720 mg/L Lab of Environment and Natural Resources SAMPLE PRIORITY Routine L Lab Numb( ❑ Emergency Cam' Date Recei Rec'd By: Other: Data Entry Date Repo 1 ,)Pesticide Study, Federal Trust, Other: (Pumping time. Del., Diss. Solids 70300 mg/L Ag-Silver 46566 u /L Orilanochlonne Pesticides Fluoride 951 mg/L )/ AI -Aluminum 46557 u /L Or ano hos horns Pesticides Hardness: Total 900 mg/L L,, As -Arsenic 46551 u /L Nitrogen Pesticides Hardness (non-carb) 902 mg/L Sa-Banum 46558 uq1L Acid Herbicides Phenols 32730 ugn Ca -Calcium 46552 mg1L PCBs Specific Cond. 95 pMhos/cm Cd-Cadmium 46559 u L mg/L Cr-Chromium 46559 u /L Sulfide 745 mg/L Cu-Copper 46562 u /L Fe -Iron 46563 u /L Semivolabie Organics Oil and Grease mg/L Hg-Mercury 71900 u /L TPH-Diesel Range K-Potassium 46655 milli. Mg -Magnesium 46554 m gJL Mn-Manganese 46565 u /L Volatile Organics(VOA bottle NH3 as N 610 mg/L Na-Sodium 46556 m /L TPH-Gasoline Range TKN as N 625 mg/L 111,NI-Nickel u /L TPH-BTEX Gasoline Range NO2- N%as N 630 mg)L Pb-Lead 46564 u /L mg/L Se -Selenium u fL Nitrate (NO3 as N) 620 mg/L Zn-Zinc 46567 u/L wiii Nitrite (NO2 as N) 615 mg/L arrival (°C): � �� I ROUNDWATER FIELD/LAB FORM Department of Environment and Natural Resources Location code S N04 'VW0 0005 WI W-13 SAMPLE TYPE SAMPLE PRIORITY County Mr-7C M41ter Routine /a LL Lab Number3`fii��O El Soil ❑ Emergency L..ta'l7 Quad No / Serial No. r, El /�r1TQ.NCIt Date Received T• ZS>•4'7� Time: Lat. oS `t% 3L'.<'+ Long. q 01 • -7 W-13 Reed By: 1Gik� From:Bus, Courier, Hand Del., ❑ Chain of Custody Other: Report To: RO RO, MRO, RRO, WaRO, WiRO, Data Entry By: Ck: WSRO, Kinston FO, Fed. Trust, Central Off., Other: Date Reported: Shipped by: Bus, n:er Hand D�el1, Other: Purpose: Collector(s): •JLLI12yanrt Date 26 Time in, 3� Bas line, Comraint, Corn liance LUST, Pesticide Study, Federal Trust, Other: _11FIELD ANALYSES Owner _oa� fimerlca fGtie«e> pH 4ee Spec. Cond.94 at 25°C Location or Site I` i On c;Y� i Temp.to °C Odor Description of sampling point nylon r iArP Appearance Sampling Method PuvnD - Sample Interval Field Analysis By: Remarks SPkl Ole - I ARC)RATORY ANAI YRFR I I (P°mai°9 Gme, all rem°.. emJ SOD 310 mg/L b iss. Solids 70300 mg/L ill, Ag-Silver46566 u /L Or anochlorine Pesticides COD High 340 mg/L Fluoride 951 mg/L AI -Aluminum 55! u !L Oroano has hams Pesticides COD Low 335 mg/L Hardness: Total 900 mg/L ,' -Arsenic 6551 - u !L' Nitrogen Pesticides Colifonn: MF Fecal 31616 AoOmI Hardness (noncarb) 902 ni Be. du 46556 uqn. Acid'Herbiddes Cplifonn: MF Total 31504 /100ml Phenols 32730 ug1l Ca-C m 46552 m !L PCBs mg/L Specific Cond. 95 pMhos/cm Cd admiu 46559 u fL Turbidity 76 NTU mg/L r-Chromium h559 u !L Residue. Total Suspended 530 mg/L Sulfide 745 . mg/L Cu-Copper 46562 u 1L Fe -Iron 46563 u2tl. Semivolatile Organics Oil and Grease mg/L Hg-Mercury 71900 u /L TPH-Diesel Range H 403 units K-Potassium 46555 m 1L Alkalinity to pH 4.5 410 mg/L j,� MQ-MagrigIsium 46554 m 1L Alkalinity to pH 6.3 415 mg/L Mn- n anese 46565 ugfL Volatile Organics(VOA bottle Carbonate 445 mg1L NH3 as N 610 mg/L Na-So 46556 m fL TPH-Gasoline Range Bicarbonate 440 mg/L TKN as N 625 mg/L Ni-N' el u /L TPH.BTEX Gasoline Range Carbon dioxide 405 mg/L NOz t NOa as N 630 m92 Pb eatl 46564 u gfL 0 mg/L P 665 mg/l. -Selenium u /L Chromium: Hex 1032 ug/L Nitrate (14%as N) 620 mg/L Zn-Zinc 46567 u fL Color. True 60 CU Nitrite (NOi as N) 615 mg/L LAB USE ONLY .Temperature on arrival (°C): Cyanide 720 1 LCu GW-54 REV. 7103 For Dissolved Analysis -submit filtered sample and wnte'DIS' in block County: MCDOWELL River Basin Report To AROAP 1 Collector. J VANN { Region: ARO Sample Matrix: GROUNDWATER Loc.Type: MONITORING WELL rat; VED L,cp 2 2 2008 Emergency Yes/No Psheville regional office CDC Yes/No f�c'+1,111'fi Proteclon V�tA7F�OG of r YsitlD Loc. Descr.: COATS AMERICA MW-14 Sample ID: AB34867 PO Number# BG1211 Date Received: 08/28/2008 Time Received: 07:45 Labworks LoginlD HPARKER Date Reported: 9117/08 Report Generated: 09117/2008 ILLocation to: 1P059W00005603MW14 I Collect Date: 08/26/2008 (Collect Time:: 10.45 Sample Depth Sample Qualifiers and Comments Routine Qualifiers For a more detailed description of these qualifier Codes refer to www.dwqlab.org under Staff Access A -Value reported is the average of two or more determinations - B1-Countable membranes with <20 colonies; Estimated B2- Counts from all filters were zero. B3- Countable membranes with more than 60 or 80 colonies; Estimated B4-Filters have counts of both >60 or 80 and <20; Estimated B5-Too many colonies were present; too numerous to count (TNTC) J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated J3-The sample matrix interfered with the ability to make any accurate determination; Estimated J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated Nl-The component has been tentatively identified based on mass spectral library search and has an estimated value LAB 0 9II sI©� N3-Estimated concentration is < PQL and >MDL NE -No established POL P-Elevated PQL due to matrix interference and/or sample dilution Q1-Holding time exceeded prior to receipt at lab. Q2- Holding time exceeded following receipt by lab PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity U- Samples analyzed for this compound but not detected X1- Sample not analyzed for this compound Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 1 of 3 County: MCDOWELL River Basin Report To AROAP Collector. J VANN Region: ARC Sample Matrix: GROUNDWATER Loc.Type: Monitoring Well Emergency Yes/No CDC Yes/No RECEIVED SEP 09 2608 Asheville Regional Office Aquifer Protection Loc. Descr.: COATS AMERICAN MW-14 Sample ID: AB34817 PONumber# - ARO Date Received: 08126/2008 Time Received: 14:15 Labworks LoginlD KJIMISON Date Reported: 9/4/08 Report Generated: 09104/2008 q 1 S5 02 II Location ID: iP059W00005603MW14 I Collect Date: 08126/2008 I Collect Time:: 10:45 I Sample Depth Sample Qualifiers and Comments Routine Qualifiers For a more detailed description of these qualifier codes refer to www.dwqlab.org under Staff Access A -Value reported is the average of two or more determinations B7-Countable membranes with <20 colonies; Estimated B2- Counts from all filters were zero. B3- Countable membranes with more than 60 or 80 colonies; Estimated 84-Filters have counts of both >60 or 80 and <20; Estimated B5-Tao many colonies were present; too numerous to count (TNTC) J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated J3-The sample matrix interfered with the ability to make any accurate determination; Estimated J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated NI -The component has been tentatively identified based on mass spectral library search and has an estimated value ARO 1,13-Estimated concentration is < PQL and>MDL NE -No established PQL P-Elevated PQL due to matrix interference and/or sample dilution Q7-Holding time exceeded prior to receipt at lab. Q2- Holding time exceeded following receipt by lab PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity U- Samples analyzed for this compound but not detected X7- Sample not analyzed for this compound Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 1 of 2 V it D: 1 P 059 W 00005603 M W 7 4 Descr.: COATS AMERICA MW44 ID CAS # Analyl Sample temperature Method Reference NC (DWWQ La6oratory Section 12esufts TOC In liquid Method Reference APHA5310B-20th W�a 2.0 Collect Date: Collect Time:: Qualifier Units AnalysUDate 0.9 °C DSAUNDER: 828108 5.6 mg/L BSWANSON MV08 081262008 10:45 8128108 MOVERMAN 9/8/08 Ion Chromatography TITLE-, mg/L MIBRAHIM7 MOVERMAN Method Reference EPA300.0 9/4108 9/15I08 Chloride 1.0 30 mgfL MIBRAHIM7 MOVERMAN Method Reference EPA300.0 914/08 9/15/0B Fluoride 0.4 2.0 U,P mg1L MIBRAHIMt MOVERMAN Method Reference EPA 300.0 - 9/4/09 9/15/08 Sulfate 2.0 2.0 mg/L MIBRAHIMI MOVERMAN Method Reference EPA300.0 914108 9115/08 14U Phosphorus total as P In liquid 0.02 0115 mglL as P MAJAYI CGREEN Method Reference La00-115-01-1EF 829/08 9008 7429-90-5 AI by ICP 50 1600 ug/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3/08 9/11108 744038-2 As by ICPMS 5.0 5.0 U ugfL DSTANLEY ESTAFFORD Method Reference EPA200.8 VMS 9111108 744038-3 Be by ICP 10 140 ugfL PGAUTHIER ESTAFFORD Method Reference EPA200.7 9008 9111108 7440-70-2 Caby IGP 0.10 60 mgfL PGAUTHIER ESTAFFORD Method Reference EPA200.7 9ld/08 9/11/96 744043-9 Cd by ICPMS 1.0 1.0 U ug1L DSTANLEY ESTAFFORD Method Reference EPA200.8 M/08 9111/08 7440-47-3 Crby ICPMS 10 10 U ugfL DSTANLEY ESTAFFORD Method Reference EPA200.8 9008 9/11/08 7440-50-8 Cu by ICPMS 2.0 210 ugfL DSTANLEY ESTAFFORD Method Reference EPA200.8 92/08 9111108 7439-95-4 Mg by ICP 0.10 38 mgfL PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3/08 9/11108 7439 96 5 Mn by ICP 10 530 ug/L PGAUTHIER _ _ _ ESTAFFORD__-- - Method Reference EPA200.7 - - -- - - --- _ 9008 9/11108 - 7440 23-4 Na by ICP 0.10 64 mgfL PGAUTHIER ESTAFFORD Method Reference EPA200.7 9008 9111108 Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733.3908 Page 2 of 3 ED 1P059WQ0005603MW14 COATS AMERICA MW-14 NC D WQQ Laboratory Section 12esufts Collect Date: Collect Time:: 0812612008 10:45 ....�,. ..,,a,y.e Hanle VUL Result Qualifier Units Analyst/Date Aoorovad Rv bate Method Reference EPA200.8 9/3108 9111108 7439-92-1 Pb by ICPMS 10 22 ug/L DSTANLEY ESTAFFORD Method Reference EPA 200.8 9/3108 9111108 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L DSTANLEY ESTAFFORD Method Reference EPA 200.8 9/3108 9/11108 Laboratory Sectic >> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 3 of 3 Pi ID: 1P059WO0005603MWi4 Descr.: COATS AMERICAN MW-14 ID .. o.r— n..". NC DWQ Laboratory Section Results Kesun Collect Date: Collect Time:: 08/2612008 10:45 Method Reference w6N8 828/08 Total Dissolved Solids In liquid 12 446 mgfL KJIMISON CGREEN Method Reference APHA2540C-18TH 828/08 9/4108 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 2 of 2 GROUNDWATER FIELD/LAB FORM Locationcode 1Y0h'1vJ00QQ5_W3`"D/V_l't SAMPLE TYPE County M°7o Wei ater Quad No Serial No. ❑ Soil Lat. 35' 4 Long. $a' UI ' 19.7° ❑Other ❑ Chain of Custody Report To: ARO FRO, MRO, RRO, WaRO, WiRO, WSRO, Kinston FO, Fed. Trust, Central Off., Other: Shipped by: Bus, ouner Hand D�elf , Other: _ Purpose: Collector(s): lulte XKIl1rl Date G Time�U:US FIELD ANALYSES Owner SAMPLE PRIORITY Routine ❑ Emergency pH 400 Spec. Cond.94 at 25*C Location or Sit Terri eC Odor Description of Appearance Sampling Metl fn Boo 310 mg/L COD High 340 mg/L COD Low 335 mg/L Coliforrn: MF Fiscal 31616 /100m1 biqliform: MF Total 31504 /100ml 7 C 680 mg/L Tumidity 76 NTU Residue, Total Suspended 630 mg/L units Alkalinity to pH 4.5 410 mg/L Alkalinity to pH 8.3415 mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L arbon dioxide 405 mg/L 0 mg/L Chromium: Hex 1032 ug/L Color: True 80 CU Cyanide 720 mg/L Lab Comments GW-54 REV. 7103 For Dissolved Analy North Carolina Department of Environment and Natural Resources (i) Lab Number UT M I m\ ` 16 I Date Received 0t Ti 5 Rec d By: From: s, Courier Hand Del., Other: Data Entry y: Ck: Date Reported: Study, Federal Trust, Other: trumping ume, an temp., e¢.l Diss. Solids 70300 mg/L 66 u L Or anochlorine Pesticides Fluoride 951 mg/L ✓ AI- uminum 46557 u /L Or ano hos horns Pesticides Hardness: Total 900 mg/l As -A enic46551 u /L Nitrogen Pesticides Hardness (non-carb) 902 mg/L Ba-B dum 46558 ugiL Acid Herbicides Phenols 32730 ug8 Ca- Icium 46552 m PCBs S�cCond.95 pMhos/cm Cd- admium 46559 uq1t. mg/L 5AChmmium 46559 u 1L Sulfide 745 mg/L Cu-Copper46562 u /L Fe -Iron 46563 u I Semivolalile Organics Oil and Grease mg/L Hg-Mercury 71900 uqtL TPH-Diesel Range K-Potassium 46555 mqfL -Magnesium 46554 m fL Mr -Manganese 46555 uq1t. Volatile Organics(VOA bottle) NH3 as N 610 mg/L Na-S dium 46556 mqfL TPH-Gasoline Range TKN as N 625 mg/L Ni-Ni kel ugIL TPH-STEX Gasoline Range NO2 + NO3 as N 630 mg/L b-L ad 46564 u /L G 5 mg/L Se- elenium u /L Nitrate (NO3 as N) 620 mg/L -Zinc 46567 u /L Nitrite (NO2 as N) 615 mg/L LAB USE ONLY Temperature on arrival ("C):D f �LpW� II.I`l 111fLt�.-ib cm- '5 0;L1,f °'i i 521, e,l- UNDWATER FIELD/LAB FORM Location code S YOh`I W 4 (iCQS (rfl i W I W- I `f SAMPLE TYPE County 1Ac 1 /O 1Ate ater Quad No Serial No. ❑ Soil Lat. �� LF 1 27. /n ` Long. a - of 19 % n ❑ Other ❑ Chain of Custody Department of Environment and Natural Resources SAMPLE PRIORITY Routine I ��L Lab Number �` kk �% El Emergency �7 Date Received %-Ar-C9 'Time: A - I Rec'd By: 414From:Bus, Courier, Hand Del., Report To: ARO RO, MRO, RRO, WaRO, WIRO, Data Entry By: Ck WSRO, Kinston FO, Fed. Trust, Central Off., Other. Date Reported: Shipped by: Bus, owner Hand Del , Other. - Purpose: Collector(s): JLLIIe DI Date Time Ill %4C Baseline, Complaint, Corn liance LUST, -Pesticide Study, Federal Trust, Other. FIELD ANALYSES Owner G°°°°) pH 400 Spec. ConoLm at 25°C Location or Site Temp.lo °C Odor Description of sampling point Appearance Sampling Method - Sample Interval Field Analysis By'. Remarks Sol,l- ! m2 "m°' b2fler.° I I LABORATORY ANALYSES tpvmpem time, ar temp.. etc) BOD 310 mg/L ss. Solids 70300 mg/L 66 'u /L O anochlorine Pesticides COD High 340 mg/L Fluodtle.951 mg/L N,41uminum 57 ugL Or ano hos horns Pesticides COD Low 335 mg/L Hardness: Total 900 mg/L - As- rsenic 6551 u /L Nitroen Pesticides Colifomt: MF Fecal 31616 /loom[ Hardness (non-carb) 902 mg/L Ba-e ' 46558 u /L Acid Herbicides Colifonn: MF Total 31504 - 110Dm1 Phenols 32730 ugA Ca-C/1"'i'OT 46552 m rL PCBs mglL Specific Cond. 95 pMhos/an -Cadmiu 6559 u /L Turbidity 76 NTU s mg/L Cr-Chromium 4 59 u L Residue. Total Suspended 530 mg/L Sulfide 745 mg/L Cu-Copper 46562 u /L - Fe -Iran 46563 u /L Semivolatile O anics Oil and Grease mg/L Hg-Merwry71900 u A TPH-Diesel Range r/ H 403 units K-Potassium 46555 m IL Alkalinity to pH 4.5470 mg/L g-Magnesium 46 54 m Alkafnity to pH 8.3415 mglL M Manganes 46565 ugfL Volatile Organics(VOA bottle Carbonate 445 mg/L NH, as N 610 M91L - Na-5 lu 6556 m IL TPH-Gasoline Range Bicarbonate 440 mg/L TKN as N 625 mg/L Nl-Nick u 1L TPH-BTEX Gasoline Range Carbon dioxide 405 M91L NOi. NO3 as N 630 mg/L 1pb-tAd 465 - u IL M91L mg/L SqeSelenlum 1 u tL Chromium: Hex 1032 ug/L Nitrate (NO3 as N) 620 mg/L ZD-Zinc 46567 u Color. True 80 Cu Nitrite (NO2 as N) 615 mg/L _ LAB USE ONLY - .Temperature on amval (°C): 2. 1 Cyanide 720 mg/L Lab GW-54 REV. 7/03 For Dissolved Analysis-submfl filtered sample and write'DIS' in block. MCDOWELL Basin tTo AROAP Collector: J VANN Region: ARO Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Emergency Yes/No COC Yes/No RECEIVED SAP 16 2OOB Asheville Regional Office Sample ID: AB34868 PO Number# BG1212 Date Received: 08/28/2008 Time Received: 07:45 Labworks LoginlD HPARKER Date Reported: 9/11/08 Report Generated: 09/11/2008 II Location ID: IP059W00005603MWIS Collect Date: 08/2612008 I Collect Time:: 10:55 I Sample Depth Sample Qualifiers and Comments Routine Qualifiers For a more detailed description of these qualifier codes refer to www.dwqlab.org under Staff Access A -Value reported is the average of two or more determinations B1-Countable membranes with <20 colonies; Estimated B2- Counts from all filters were zero. B3- Countable membranes with more than 60 or 80 colonies; Estimated B4-Filters have counts of both >60 or 80 and <20; Estimated B5-Tao many colonies were present; too numerous to count (TNTC) J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated J34he sample matrix interfered with the ability to make any accurate determination; Estimated J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated N1-The component has been tentatively identified based on mass spectral library search and has an estimated value LAB N3-Estimated concentration is < PQL and >MDL NE -No established PQL P-Elevated PQL due to matrix interference and/or sample dilution Qi-Holding time exceeded prior to receipt at lab. Q2- Holding time exceeded following receipt by lab PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity U- Samples analyzed for this compound but not detected X1- Sample not analyzed for this compound Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699.1623 (919) 733-3908 Page 1 of 2 IL) NC (D WQ Laboratory Section 12esufts 1P059W00005603MW15 Collect Date: Collect Time:: 0812612008 10:55 Ana a Amnyxe name PUL Res01t Qualifier Units Analyst/Date Approved By (Date sampletemperature at receipt by lab 0.9 °C DSAUNDERS MMATHIS Method Reference 8/28108 8/28108 TOC In liquid 2.0 4A mg/L BSWANSON MOVERMAN Method Reference APHA53108-20th 828/08 9/8/08 7429-905 AIby ICP 50 50 U ugfL PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3108 9/11108 7440-38-2 Asby ICPMS 5.0 5.0 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 913108 9111108 744038-3 Be by ICP 10 140 ugr- PGAUTHIER ESTAFFORD Method Reference EPA200.7 9008 9111/08 7440-70-2 Ca by ICP 0.10 67 mg/L PGAUTHIER ESTAFFORD Method Reference EPA 200.7 1 9/3/08 9111/08 7440-43-9 Cd by ICPMS 1.0 1.0 U ug1L DSTANLEY ESTAFFORD Method Reference EPA200.8 92/08 9111/08 7440-47-3 Cr by ICPMS 10 10 U uglL DSTANLEY ESTAFFORD Method Reference EPA200.8 92108 9/11108 7440-50-8 Cu by ICPMS 2.0 2.0 U ug1L DSTANLEY ESTAFFORD Method Reference EPA200.8 9008 9111108 7439-95-4 Mg by ICP 0.10 30 mg/L PGAUTHIER ESTAFFORD Method Reference EPA200.7 913108 9/11/08 7439-96-5 Mn by ICP 10 20DO ugfI- PGAUTHIER ESTAFFORD Method Reference EPA200.7 M108 9/11108 7440-23-4 Na by ICP 0.10 52 mgfL PGAUTHIER ESTAFFORD Method Reference EPA200.7 9/3/08 9/11/08 7440-02-0 NI by ICPMS 10 10 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 9/2108 9111108 -_ - 7439-92-1 Pbby ICPMS 10 10 U ugll- DSTANLEY ESTAFFORD Method Reference EPA200.8 92/08 9111108 7782-49-2 Seby ICPMS 5.0 5.0 U ug/L DSTANLEY ESTAFFORD Method Reference EPA200.8 913108 9/11108 Laboratory Section 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 2 of 2 NDWATER FIELD/LAB FORM R6cation code d YU�h "I W N UOU,S a) 5 W I VV — I� SAMPLE TYPE SAMPLE PRIORITY County mci)OweA ater Routine Quad No `I Serial No.T_ ❑ Soil El Emergency 3l Lat. S %7..24. 4 Long. 1 ❑ Other ❑ Chain of Custody Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SEC �cn/5 Lab Numl y7me,1 Oa Date Rec W-IS Reed By: nrHe.• M-_6gi o From:Bus, jCourier„ Eland Del., Report To: ARO FRO, MRO, RRO, WaRO, WiRO, I Data Entry By: I Ck WSRO, Kinston FO, Fed. Trust, Central Off., Other: Date Reported: Shipped by: Bus, ouner Hand Dell, Other: Purpose: Collector(s): tulleyClnYy Date Time IU;S� Baseline, Complaint, Corn Hance LUST, Pesticide Study, Federal Trust, Other. rci FIELD ANALYSES Owner Id ewe) pH 40o Spec. Cond.e4 at 250C Location or Site Temp.lo °C Odor Description of sampling point Appearance Sampling Method Sample Interval Field Analysis By: RemarksGr)14cr?mD)e umo. Miter. etc.) C _ABORATORY ANALYSES """'P"'s ""'a' a" `a"'P.. a"' BOD 310 mg/L Diss. Solids 70300 mg/L Ng -Silver 46566 u /L Or anochlorine Pesticides COD High 340 mg/L Fluoride 951 mg/L ,jANAluminum 46557 u /L O ana hos horns Pesticides COD Low 335 mg/L Hardness: Total 900 mg/L s rsenic46551 uq1L Nitrogen Pesticides Colifonn: MF Fecal 31616 /100ml Hardness (non-carb) 902 ' mg/L Ba- adum 46558 u /L Acid Herbicides oliform: MF Total 31504 /100m1 Phenols 32730 ug/l Ca alcium 46552 m /L PCBs OC 680 mg/L Specific Cond. 95 pMhos/cm C Cadmium 46559 u /L Turbidity 76 NTU mg/L -Chromium 46559 u !L Residue, Total Suspended 530 mg/L Sulfide 745 mg/L Cu-Copper 46562 u IL Fe -Iron 46563 u /L Semivolalile Organics Oil and Grease mg/L Hg-Mercury 71900 u /L TPH-Diesel Rance pH 403 units K-Potassium 46555 m /L Alkalinity to pH 4.6 410 mg/L -Magnesium 46554 m fL Alkalinity to pH 8.3 415 mg/L Mn Manganese 46565 u /L Volatile Organics(VOA bottle Carbonate 445 mg/L NH3 as N 610 mg/L Na- odium 46556 m /L TPH-Gasoline Range Bicarbonate 440 mg/L TKN as N 625 mg/L Ni- ickel u IL TPH-BTEX Gasoline Range Carbon dioxide 406 mg/L NO,+ NO3 as N 630 mg/L P Lead 46564 u /L mg/L mg/L -Selenium a /L Chromium: Hex 1032 ug/L Nitrate (No, as N) 620 mglL Zn-Zinc 46567 u /L Color. True 80 CU Nitrite (Not as N) 615 mg/L LAB USE ONLY .Temperature on arrival (°C): Oil Cyanide 720 mg/L Lab GW-54"REV: 7/03 For Dissolved Analysis -submit filtered sample and write'DIS' in block. - - / - - - - -- , I Ill County: MCDOWELL Sample ID: I AB34862 River Basin pF WATFS, PO Number# 8G1206 Report To AROAP y Date Received: Time Received: 08/26/2008 07:45 Collector: J VANN O Y Labworks Logm1D HPARKER Region: ARO Report Generated: 5/19/09 Sample Matrix: GROUNDWATER Dale Reported: 1212012011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN MW-2 Location ID: 1P059W00005603MW2 Collect Date: 08/26/2008 Collect Time: 09:25 Sample Depth Result/Units Method Analysis CAS # Analvte Name P(�. LL Validated by ualifer Reference Date LAB Sample temperature at receipt by lab 0.9 °C 8/28/0e MMATHIS MIC TOC in liquid 2.0 2 U mg/L APHA53106-20m 8/28/os MOVERMAN WET Ion Chromatography _TITLE mg/L EPA 300.0 9/4108 MOVERMAN Chloride 1.0 5.8 mg/1- EPA300.0 9/4/08. MOVERMAN Fluoride 0.4 0.4U mg/L EPA 300.0 9141081 MOVERMAN Sulfate 2.0 5.3 mg/L EPA 300.0 9/4108 MOVERMAN NUT Phosphorus -total as P in liquid 0.02 0.04 mg/L as P Lacl O-115-01-lEF 8/29/08 CGREEN MET 7429-90-5 Al by ICP 50 50 U ug/L EPA 200.7 9/3108 ESTAFFORD 7440-38-2 AS by ICPMS 5.0 5.0 U ug/L EPA200.8 9/3108 ESTAFFORD 7440-38-3 Ba by ICP 10 47 ug/L EPA200.7 9/3/08 ESTAFFORD 7440-70-2 Ca by ICP 0.10 19 mg/L EPA200.7 9/3108 ESTAFFORD 744043-9 Cd by ICPMS 1.0 1.0 U ug/L EPA200.8 913108 ESTAFFORD 7440-47-3 Cr by ICPMS 10 101.1 ug/L EPA200.8 9/3108 ESTAFFORD 7440-50-8 Cu by ICPMS 2.0 4.6 ug/L EPA200.8 9/3108 ESTAFFORD 7439-954 Mg by ICP 0.10 10 mg/L EPA 200.7 9/3108 ESTAFFORD 7439-96-5 Mn by ICP 10 68 ug/L EPA200.7 9/3/08 ESTAFFORD 7440-23-5 Na by ICP 0.10 9.9 mg/L EPA200.7 9/3108 ESTAFFORD 7440-02-0 Ni by ICPMS 10 10 u ug/L EPA200.8 9/3108 ESTAFFORD 7439-92-1 Pb by ICPMS 10 10 u ug/L EPA200.8 9/3/08 ESTAFFORD 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 9/3/08 ESTAFFORD Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed desotiptlon of the quari0er codes infer to hm r/°ercetn<d•nr e.etwW-Ad a/:nh°sort«nnssuep}lpt�yier,r C�s-.,er/°erc°LnM-er°,awee�.°n nl•mfien°rmm°vun Page 1 of 1 MCDOWELL River Basin Report To AROAP Collector: J VANN Region: ARO Sample Matrix: GROUNDWATER Lac. Type: MONITORING WELL Emergency Yes/No COC Yes/No Sample to: Ab34801 OF PO Number# ARO QG �02 h Date Received: Time Received: 081126/2008 14:15 -i O Y Labworks LoginlD KJIMISON Report Generated: 5/19/09 Date Reported: 12/20/2011 VisitlD Loc. Descr.: COATS AMERICAN MW-2 Location ID: 1P059W00005603MW2 Collect Data: 0812612008 Collect Time: 09:25 Sample Depth CAS # Analyte Name PQL Result/ Units Method Analysis Validated by Qualifier Reference Date Others Sample temperature at receipt by lab 2.1 °c 8/26108 SMATHIS 1. Total Dissolved Solids in liquid 12 110 mg/L APHA2540C-18TH 8128108 CGREEN Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Fore deviled descdprwn oftee qualifier codes refer to Inim. aei < wailll Page 1 of 1 County: MCDOWELL Sample to: AI334863 WATER River Basin pF O� QG PO Number# 8G1207 Report To AROAP r Date Received: Time Received: 08/28/2008 07:45 Collector: J VANN 0 Y Labworks LoginlD HPARKER Region: ARO Report Generated: 5/19/09 Sample Matrix: GROUNDWATER Date Reported: 12/20/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD CDC Yes/No Loc. Descr.: COATS AMERICAN MW-10 Location ID: 1P059W00005603MW10 Collect Date: 08/26/2008 Collect Time: 09:60 Sample Depth Result/Units Method Analysis CAS # Analvte Name PQL validated by Qualifier Reference Date LAB Sample temperature at receipt by lab 0.9 °C 8128/08 MMATHIS MIC TOC In liquid 2.0 2 U mg/L APHA5310B-20th 8/28/08 MOVERMAN WET Ion Chromatography _TITLE mg/L EPA 300.0 9/4/08 CGREEN Chloride 1.0 10 mg/L EPA 300.0 9/4/08' .CGREEN Fluoride 0.4 2.0 U,P mg/L EPA 300.0 914/08 CGREEN Sulfate 2.0 150 mg/L EPA300.0 9/4/OB CGREEN NUT Phosphorus -total as P in liquid 0.02 0.02 U mg/L as P Lacl G-115-01-1EF 8129108 CGREEN MET 7429-90-5 Al by ICP 50 50 U ug/L EPA200.7 9/3/08 ESTAFFORD 7440-38-2 As by ICPMS 5.0 6.0 U ug/L EPA200.8 9/3108 ESTAFFORD 7440-38-3 Be by ICP 10 16 ug/L EPA200.7 9/3/08 ESTAFFORD 7440-70-2 Ca by ICP 0.10 1.1 mg/L EPA200.7 913/08 ESTAFFORD 744043-9 Cd by ICPMS 1.0 1.0 U ug/L EPA200.8 913/08 ESTAFFORD 7440-473 Cr by ICPMS 10 10 U ug/L EPA200.8 913/08 ESTAFFORD 7440-50-8 Cu by ICPMS 2.0 4.6 ug/L EFA200.8 9/3/08 ESTAFFORD 7439-95-4 Mg by ICP 0.10 0.43 mg/L EPA200.7 9/3/0B ESTAFFORD 7439-96-5 Mn by ICP 10 10 U ug/L EPA200.7 9/3/08 ESTAFFORD 7440-23-5 Na by ICP 0.10 110 mg/L EPA200.7 913/08 ESTAFFORD 7440-02.0 Ni by ICPMS 10 10 U ug/L EPA200.8 9/3108 ESTAFFORD 7439-92-1 Pb by ICPMS 10 10 U ug/L EPA200.8 9/3/08 ESTAFFORD 778249-2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 9/3/08 ESTAFFORD Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For ad eta iled deeatlpllan of tha qualifier codes refer to mo r/°°nn ommrnrtLy°yw9/jno1 'e/+a5a-ar'd-Ourin.•e.,'I/no nm.•. °.u/«ectr an°u4mnnno/tgq [-. Page 1 of 1 County: MCDOWELL Sample ID: River Basin WATFq PO Number# Report To apt G AROAP ,�O h Dale Received: Time Received: Collector: J VANN O Y Labworks LoginlD Region: ARO Report Generated: Sample Matrix: GROUNDWATER Date Reported: Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN MW-10 Location ID: 1P059W00006603MW10 Collect Date: 08/26/2008 Collect Time: 09:50 CAS # Analvte Name POL Result/Units Method Qualifier Reference Others Sample temperature at receipt by lab 2.1 °C Total Dissolved Solids in liquid 12 316 12/20/2011 Sample Depth Analysis. Validated by Date I I' B/26/08 II MMATHIS 8/28108 CGREEN Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Fora detailed desedptlen Ditto qualifier codes reform heo L,, l.nvde°ear o Lti,Ltpfinfil t—Iliaouanner epees o-anl/rorca net<nro o/wen/.°1�n'-ae.fl°/mma-:�:n Page 1 of 1 County: MCDOWELL Sample ID: AB34864 River Basin pF WATF9 PO Number# 8137208 Report To AROAP �O� pG Date Received: 08/28/2008 y Time Received: 07:45 Collector: J VANN O C Labworks LoginlD HPARKER Region: ARO Report Generated: 5/19/09 Sample Matrix: GROUNDWATER Dale Reported: 12/2012011 Loc. Type: MONITORING WELL Emergency Yes/No VlsitlD CDC Yes/No Loc. Descr.: COATS AMERICAN MW-11 Location ID: 1P059W00005603MWIl Collect Date: 08/2612008 Collect Time: 10:12 Sample Depth Result/Units Method Analysis CAS # Analvte Name P(�. LL Validated by Qualifier Reference Date' LAB Sample temperature at receipt by lab 0.9 °C 8/28/0811 1 MMATHIS MIC I. TOC In liquid 2.0 4.4 mg/L APHA531OB-20th 8/28/08 MOVERMAN WET Ion Chromatography _TITLE_ mg/L EPA300.0 9/4/08 i. MOVERMAN Chloride 1.0 5.4 mg/L EPA300.0 9/4/08 MOVERMAN Fluoride 0.4 0.4U mg/L EPA 300.0 9/4/08„ MOVERMAN Sulfate 2.0 33 mg/L EPA 300.0 9/4/10B MOVERMAN NUT Phosphorus_ total as P in liquid 0.02 0.20 mg/Las P LacIO-115-01-lEF 8129/08 CGREEN MET 7429-90-5 Al by ICP 50 460 ug/L EPA 200.7 9/3/08 ESTAFFORD 7440-38-2 As by ICPMS 5.0 5.0 U ug/L EPA 200.8 9/3108 ESTAFFORD 7440-38-3 Ba by ICP 10 100 ug/L EPA 200.7 9/3/OB ESTAFFORD 7440-70-2 Ca by ICP 0.10 18 mg/L EPA 20D.7 9/3/0B ESTAFFORD 7440.43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA 200.8 9/3/08 ESTAFFORD 7440A7-3 Cr by ICPMS 10 IOU ug/L EPA 200.8 913106 ESTAFFORD 7440-50-8 Cu by ICPMS 2.0 11 ug/L EPA 200.8 9/3/08 ESTAFFORD 7439-95A Mg by ICP 0.10 5.2 mg/L EPA 200.7 9/3/013 ESTAFFORD 7439-96-5 Mn by ICP 10 890 ug/L -EPA 200.7 9/3/08 ESTAFFORD 7440-23-5 Na by ICP 0.10 84 mg/L EPA 200.7 9/3/08 ESTAFFORD 10U 7439-92-1 Pb by ICPMS 10 IOU ug/L EPA 200.8 9/3108 ESTAFFORD 7782-49-2 Se by ICPMS 5.0 6.0 U uglL EPA 200.8 913108 ESTAFFORD Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Fora detailed adsorption olthe qualifier codes all to ne .ue,m°<Kn.,::.a re1rcmem._.. wmw maese .em Page 1 of 1 County: River Basin Report To MCDOWELL AROAP Collector: J VANN Region: ARO Sample Matrix: GROUNDWATER Lac. Type: MONITORING WELL Emergency Yes/No COC Yes/No Visi9D Loc. Descr.: COATS AMERICAN MW-11 Sample ID: PO Number# Date Received: Time Received: Latraorks LoginlD Report Generated: Date Reported: 5/19109 12/20/2011 Location to: 1PO59W00006603MWII Collect Date: 08/26/2008 Collect Time: 10:12 Sample Depth CAS At Analvte Name PAL Units Result/ Method Analysis Validated by Qualifier Reference Date Others f Sample temperature at receipt by lab 2.1 C MMATHIS Total Dissolved Solids in liquid 12 280 mg/L APHA254OC-18TH 8/28/0811 CGREEN Laboratory Section>> 1623 Mail Service Center, Raleigh, NO 27699-1623 (919) 733-3908 Fora delaikd descdptlanafthe qualiferendesreferta Q.Aftm cme .I. _ r.e.,ge can ssi Page 1 of 1 County: MCDOWELL Sample ID: A634865 River Basin OF WA7E;9 PO Number# BG1209 Report To pG AROAP �O� h r Date Received: OB/28/2008 Collector: J VANN 0 Y Time Received: 07:1 1 46 Labworks LoginlD HPARKER Region: ARO Report Generated: 5119/09 Sample Matrix: GROUNDWATER Date Reported: 12/20/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc.Descr.: COATS AMERICA MW-12 Location ID: 1P059W00006603MW12 Collect Date: 08/26/2008 Collect Time: 10:25 Sample Depth Result/ Method Analysis CAS # Analvte Name PQL - Qualifier Units Reference Validated by Date LAB Sample temperature at receipt by lab 0.9 °c 8/28/081 MMATHIS I MIC TOC In liquid 2.0 2.4 mg/L APHA5310B-20th 8/28/0811 MOVERMAN WET p Ion Chromatography _TITLE mg/L EPA 300.0 914/08 MOVERMAN Chloride 1.0 33 mg/L EPA 300.0 914/08 MOVERMAN Fluoride 0.4 2.0 U,P mg/L EPA300.0 914/08 MOVERMAN Sulfate 2.0 3.9 mg/L EPA 300.0 9/4/08 MOVERMAN NUT Phosphorus -total as P in liquid 0.02 0.11 mg/L as P Lacl O-115-01-1EF 8/29/138 CGREEN MET 7429-90-5 Al by ICP 50 86 ug/L EPA200.7 913/08 ESTAFFORD 7440-38-2 As by ICPMS 5.0 5.0 U ug/L EPA200.8 9/3/08 ESTAFFORD 7440-38-3 Be by ICP 10 53 ug/L EPA 200.7 9/3108 ESTAFFORD 7440-70-2 Ca by ICP 0.10 35 mg/L EPA200.7 9/3/08 ESTAFFORD 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA 200.8 9/3/08 ESTAFFORD 7440-47-3 Cr by ICPMS 10 10 U ug/L EPA 200.8 9/3108 ESTAFFORD 7440-50-8 Cu by ICPMS 2.0 4.7 ug/L EPA 200.8 9/3/08 ESTAFFORD 7439-95-4 Mg by ICP 0.10 7.7 mg/L EPA 200.7 9/3108 ESTAFFORD 1100 7440-23-5 Na by ICP 0.10 60 mg/L EPA 200.7 913108 ESTAFFORD 7440-02-0 Ni by ICPMS 10 10 U ug/L EPA200.8 913108 ESTAFFORD 7439-92-1 Pb by ICPMS 10 10 u ug/L EPA 200.8 9/3108 ESTAFFORD 778249-2 Se by ICPMS 5.0 5.0 U ug/L EPA 200.8 9/3108 ESTAFFORD Laboratory Section>> 1623 Mail Service Center, Raleigh, NO 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes rerer to h, amma i. Page 1 of 1 MCDOWELL River Basin Report To AROAP Collector: J VANN Region: ARO Sample Matrix: GROUNDWATER Lac. Type: MONITORING WELL Emergency Yes/No COC YesrNo Sample ID: A63481t OF WATFq PO Number# ARO O� 09 Date Received: Time Received: 08/26/2008 14:16 ON Y Lebworks LcginlD KJIMISON Report Generated: 5119/09 Date Reported: 12/20/2011 VisitlD Lac. Descr.: COATS AMERICAN MW-12 Location ID: 1P059W00005603MW72 Collect Date: 08/2612008 Collect Time: 10:26 Sample Depth CAS # Analyte Name PQL Rei Units Method Analysis Validated by Qualifier Reference Date, Others Sample temperature at receipt by lab 2.1 °C 8126/08' MMATHIS 268 Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699.1623 (919) 733-3908 Fora detalled description orthe qualifier codes rererw n,. °m°l. a<m.e, tan .,mne°rsne.ss,eoam uiwe °nm.°m.°.° Page 1 of 1 County: MCDOWELL Sample ID: A634866 River Basin pF WATFA PO Number# BG1210 Report To AROAP QGy Date Received: 08/128/2008 �0 ^u [ Time Received: 07:45 Collector J VANN p Labworks LoginlD HPARKER Region: ARO Report Generated: 5/169 Sample Matrix: GROUNDWATER D ale Reported: 12/20/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD CDC Yes/No Loc.Descr.: COATS AMERICA MW-13 Location to: 1P059W00006603MW13 Collect Dale: 08/2612008 Collect Time: 10:35 Sample Depth CAS # Analvte Name Result/ P(�. LL Method Units Analysis Validated by Qualifier Reference Date LAB Sample temperature at receipt by lab 0.9 °C 8/28/08 MMATHIS MET 7429-90-5 Al by ICP 50 84 ug/L EPA 200.7 913/08' ESTAFFORD 7440-38-2 AS by ICPMS 5.0 5.0 U ug/L EPA 200.8 912108 ESTAFFORD 7440-38-3 Be by ICP 10 130 ug/L EPA 200.7 913/08 ESTAFFORD 7440-70-2 Ca by ICP 0.10 33 mg/L EPA 200.7 9/3/08 ESTAFFORD 744043-9 Cd by ICPMS 1.0 1.0 U ug/L EPA 200.8 912108' ESTAFFORD 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA 200.8 912/08 ESTAFFORD 74413-50-8 Cu by ICPMS 2.0 390 ug/L EPA 200.8 912/OB ESTAFFORD 7439-95-4 Mg by ICP 0.10 22 mg/L EPA 200.7 913108 ESTAFFORD 7439-96-5 Mn by ICP 10 1000 ug/L EPA 200.7 913/08 ESTAFFORD 7440-23-5 Na by ICP 0.10 170 mg/L EPA 200.7 9/3/08 ESTAFFORD 7440-02-0 Ni by ICPMS 10 IOU ug/L EPA200.8 9/2/08 ESTAFFORD 7439-92-1 Pb by ICPMS 10 IOU ug/L EPA200.8 9/2/0B" ESTAFFORD 7782A9-2 Se by ICPMS 5.0 5.0 U ug/L EPA 200.8 9/2/08' ESTAFFORD Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description ofthe QuallOer eades rererto neo U..e°r..d... ... /w. �nl;me.e.nr<n°ssatN°u o�igj�r1.r7, all°°mrKd:m°.a/wrt/wype/w,�P�Po/°ma•sisn Page 1 of 1 County: River Basin Report To MCDOWELL AROAP Collector: J VANN Region: ARO Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Emergency Yes/No COC Yei O�C� W AT �9 of f � y O Y VisitlD Loc. Descr.: COATS AMERICAN MW-13 Sample ID: PO Number # Date Received: Time Received: Labworks LoginlD Report Generated: Date Reported: AB34816 ARO 08/26/2008 14:16 KJIMISON 5/19109 12/20/2011 I I Location ID: 1P059W00005603MW13 I Collect Date: 08/26/2008 1 Collect Time: 10:36 1 Sample Depth I I CAS # Analvte Name PQL Result/ Qualifier Units Method Analysis Validated by Reference Date Others Sample temperature at receipt by lab 2.1 °C 8/26/08 MMATHIS Total Dissolved Solids in liquid 12 767 mg/L APHA2540C-18TH 8/28/08 CGREEN I I I it Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description orthe Qualifier codes reterto lno/Ir i..a°.. n° •ma..ro °°Iii m.°m.°.°webw eaMaa Page 1 of 1 County: MCDOWELL River Basin Report To AROAP Collector: J VANN Reglow ARO Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Emergency Yes/No VisigD COC Yes/No Sample ID: AB34861 WATFiQO �pF PO Number# 8G1211 O G� Date Received: 08/28/2008 h r Time Received: 07:45 O Y Labworks LoginlD HPARKER Report Generated: 5/19/09 Date Reported: 12/20/2011 Loc.Descr.: COATS AMERICA MW-14 Location ID: 1PG59WQ0006603MW14 Collect Date: 08/26/2008 Collect Time: 10:45 Sample Depth CAS # Analvte Name PQL Result/Units Method Analysis Validated by Qualifier Reference Date LAB Sample temperature at receipt by lab 0.9 °C I 8/28/08 MMATHIS MIC 1! TOC in liquid 2.0 5.6 mg/L APHA5310B-20N 8/28108 ' MOVERMAN 11 WET Ion Chromatography _TITLE me/L EPA 300.0 91 MOVERMAN Chloride 1.0 30 mg/L EPA 300.0 9/4/08 MOVERMAN Fluoride 0.4 2.0 U,P mg/L EPA 300.0 9/41081, MOVERMAN Sulfate 2.0 2.0 mg/L EPA300.0 9/4/08i MOVERMAN 21g1 Phosphorus_ total as P in liquid 0.02 0.26 mg/Las P Lac10-115-01-1EF 8129108 CGREEN MET 7429-90-5 At by ICP 50 1600 ug/L EPA200.7 9/3/08 ESTAFFORD 7440-38.2 As by ICPMS 5.0 5.0 U ug/L EPA 200.8 9/3/08 ESTAFFORD 7440-36-3 Be by ICP 10 140 ug/L EPA200.7 9/3/OB ESTAFFORD 7441 Ca by ICP 0.10 60 mg/L EPA200.7 9/3/08 ESTAFFORD 7440.43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA200.8 913/08 ESTAFFORD 7440.47-3 Cr by ICPMS 10 10 U ug/L EPA200.8 9/3/08 ESTAFFORD 7440-50-8 Cut by ICPMS 2.0 210 ug/L EPA200.8 9/3/08 ESTAFFORD 7439-95-4 Mg by ICP 0.10 38 mg/L EPA200.7 9/3108 !, ESTAFFORD 7439-96-5 Mn by ICP 10 530 ug/L EPA200.7 9/3108II ESTAFFORD 7440-23-5 Na by ICP 0.10 64 mg/L EPA 200.7 9/3108 1 ESTAFFORD 7440-02-0 Ni by ICPMS 10 10 U ug/L EPA 21 9/3/08 ESTAFFORD 7439-92-1 Pb by ICPMS 10 22 ug/L EPA 200.8 9/3/08I ESTAFFORD 778249.2 Se by ICPMS 5.0 5.0 U ug/L EPA 200.8 9/3/08 ESTAFFORD Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Fare detailed deseeption of the qualifier Codes referto htlY1ona11,1-rrr oi,alix.r cmo,+nme�ooml.xa<�..o,ar«eni.a�mernne�nonmha;PfC Page 1 of 1 County: MCDOWELL River Basin Report To AROAP Collector: J VANN Region: ARO Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Sample ID: Of WATFq PO Number# Date Received: r Time Received: O Y Labwodcs LoginlD Report Generated: Date Reported: 511 Emergency Yes/No VisitlD CDC Yes/No Loc. Descr.: COATS AMERICAN MW-14 L,;t,n ID: 1P059W00005603MW14 Collect Dale: 08/26/2008 Collect Time: 10:45 Sample Depth Result/Method Analysis CAS # Analvte Name PQL - Units Validated by Qualifier Reference � Date Others Samnle temnereture nt recaint by lah 91 °C 8/2610 III MMATHIS Total Dissolved Solids in liquid 12 446 mg/L APHA254OC-18TH 8/28/081 CGREEN Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description ofitie qualifier codes reterto Q(atnc ndr.r,e„nor n ca o-,ve. c...... -n, °mom°. °.Ls1y°me fift+iecna5p)P Page 1 of 1 County: MCDOWELL Sample ID: AB34861 W'4TF.Q River Basin pF OF PO Number # 8G1212 Report To AROAP Date Received: 08/28/2008 �O� =° r � Time Received: 07:45 Collector: J VANN 'y Y Labworks LoginlD HPARKER Region: ARO Report Generated: 5/19/09 Sample Matrix: GROUNDWATER t Date Reported: 12/20/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitID CDC Yes/No Loc. Descr.: Location to: 1P059=0005603MW15 Collect Dale: 08/26/2008 Collect Time: 10:65 Sample Depth CAS # Analyte Name POL Result/ Units Method Analysis Validated by Qualifier Reference Date LAB Sample temperature at receipt by lab 0.9 C 8/28108, MMATHIS MIC I TOC in liquid 2.0 4.4 mg/L APHA5310B-20th 8/28/08iMOVERMAN MET 7429-90-5 Al by ICP 50 50 U ug/L EPA200.7 913/08 / ESTAFFORD 7440-38-2 AS by ICPMS 5.0 5.0 U ug/L EPA200.8 9/3/0B ESTAFFORD 7440-38-3 Be by ICP 10 140 ug/L EPA200.7 9/3/08 ESTAFFORD 7440-70-2 Ca by ICP 0.10 67 mg/L EPA 200.7 9/3/08 ESTAFFORD 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA200.8 9/2108 ESTAFFORD 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA200.8 9/2/08 ESTAFFORD 7440-50-8 Cu by ICPMS 2.0 2.0 U ug/L EPA200.8 9/2108 ESTAFFORD 7439-95-4 Mg by ICP 0.10 30 mg/L EPA200.7 9/3/08 ESTAFFORD 7439-98-5 Mn by ICP 10 2000 ug/L EFA200.7 9/3108 ESTAFFORD 7440-23-5 Na by ICP 0.10 52 mg/L EPA 200.7 9/3/08 ESTAFFORD 7440-02-0 Ni by ICPMS 10 IOU ug/L EPA200.8 9/2108 ESTAFFORD 7439-92-1 Pb by ICPMS 10 IOU ug/L EPA200.8 9/2108 ESTAFFORD 7782-48-2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 9/3/08 ESTAFFORD I Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier Codes far to Ica., sze�s/on'lgog"°n..ei es ng;:_ Page 1 of 1 County: River Basin Report To Collector. Region: Sample Matrix: MCDOWELL AROAP B LAVERTY ARO GROUNDWATER OFWATF9 f�0� QG >_ Sample ID: PO Number# Dale Received: Time Received: Labworks LogInID Report Generated: Date Reported: AB56685 10GO162 0410812010 08:25 SMATHIS 4/23/10 12/20/2011 Loc.Type: MONITORING WELL Emergency Yes/No Visi8D COC Yes/No Loc.Descr.: COATSAMERICAN Location to: 1P59MW2COATS Collect Date: 04/0612010 Collect Time: 10:00 Sample Deptti ResulU Method Analysis CAS # Analvte Name PQL Units Validated by Qualifier Reference Date LAB Sample temperature at receipt by lab 1.7 C 418/10 SMATHIS MET 7429-90-5 Al by ICP 50 640 ug/L EPA200.7 4/14110 ESTAFFORD 7440-38-2 As by ICPMS 2.0 2.0 U ug/L EPA200.8 4112/10 ESTAFFORD 7440-38-3 Be by ICP 10 66 ug/L EPA200.7 4/14110 ESTAFFORD 7440-70-2 Ca by ICP 0.10 19 mg/L EPA200.7 4114/10 ESTAFFORD 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA200.8 4/12/10 ESTAFFORD 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA200.8 4112110 ESTAFFORD 7439-89-6 Fe by ICP 50 5800 ug/L EPA200.7 4114/10 ESTAFFORD 7439-954 Mg by ICP 0.10 9.9 mg/L EPA 200.7 4/14110 ESTAFFORD 7439-96-5 Mn by ICP 10 380 ug/L EPA 200.7 4114110 ESTAFFORD 7440-23-5 Na by ICP 0.10 9.2 mg/L EPA 200.7 4114/10 ESTAFFORD 7440-02-0 Ni by ICPMS 10 IOU ug/L EPA 200.8 4/12110 ESTAFFORD 7439-92-1 Pb by ICPMS 10 13 ug/L EPA200.8 4112/10 ESTAFFORD 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 4112/10 ESTAFFORD Laboratory Section» 1623 Mali Service Center, Raleigh, NC 27699-1623 (919( 733-3908 For a detailed desalpaon of the quafflflercoEes refer to r ml/mnnLnm«, lvdCAnS,1ustsmac Page 1 of 1 County: MCDOWELL River Basin Report To AROAP Collector. 8 LAVERTY Region: ARO Sample Matra: GROUNDWATER Loc. Type: MONITORING WELL Emergency Yes/No VlsitlD CDC Yes/No Sample ID: AB5668( pFWA7Fq qy PO Number# 10GO163 �Oa Date Received: Time Received: 0410812010 08:25 O Y Labworks LoginiD SMATHIS Report Generated: 4123110 Date Reported: 12/20/2011 Loc.Descr.: COATSAMERICAN Location ID: 1P59MW2C0ATS Collect Date: 0410612010 Collect rime: 10:00 Sample Depth CAS # Analyte Name PP Result/Units Method Analysis Validated by _L Qualifier Reference Date lA8 T — Sample temperature at receipt by lab 1.7 C 4/8/10 SMATHIS MET 7429-90-5 AI by ICP 50 120 ug/I. EPA200.7 4114110 ESTAFFORD 7440-38-2 AS by ICPMS 2.0 2.0 U ug/L EPA200.8 4112110 ESTAFFORD 7440-38-3 Ba by ICP 10 34 ug/L EPA200.7 4114110 ESTAFFORD 7440-70-2 Ca by ICP 0.10 18 mg/L EPA200.7 4/14110 ESTAFFORD 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA200.8 4/12/10 ESTAFFORD 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA200.8 4112110 ESTAFFORD 7439-89-6 Fe by ICP 50 170 ug/L EPA 200.7 4/14110 ESTAFFORD 7439-95-4 Mg by ICP 0.10 8.8 mg/L EPA 200.7 4114/10 ESTAFFORD 7439-96-5 Mn by lCP 10 10 ug/L EPA 200.7 4/14/10 ESTAFFORD 7440-23-5 Na by ICP 0.10 9.3 mg/L EPA 200.7 4/14110 ESTAFFORD 7440-02-0 Ni by ICPMS 10 IOU ug/L EPA 200.8 4/12/10 ESTAFFORD 7439-92-1 Pb by ICPMS 10 IOU ug/L EPA 200.6 4/12/10 ESTAFFORD 7782A9-2 Se by ICPMS 5.0 5.0 U ug/L EPA 200.E 4/12110 ESTAFFORD Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699.1623 (919( 733-3908 For a Eetalled choalption of the qua after codes refer to xig( mltnsPs°nx�a. "gfilp/[ya.�i nRp¢.pefMttRRLwx/!as/•�•s•e°n°mao¢u Page 1 of 1 County: MCDOWELL River Basin Report To AROAP Collector: B LAVERTY Region: ARO Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Emergency Yes/No COC Yes/No VIsIOD Loc.Descr.: COATSAMERICAN Sample ID: PO Number # Date Received: Time Received: Lobworks LoginlD Report Generated: Date Reported: 08:25 1 SMATHIS 4/23/10 12/20/2011 Location ID: lP59MW1000ATS Collect Date: 0410612010 Collect Time: 10:15 Sample Depth CAS # Analvte Name S ualResi lU ifier LAB Sample temperature at receipt by lab 1.7 °c Units Method Analysis Validated by Reference Date 4/8/10 SMATHIS 7429-90-5 Al by ICP 50 50 U ug/L EPA 200.7 4/14110 ESTAFFORD I. 7440-38-2 As by furnace 2.0 2.0 U ug/L EPA 200.9 4113110 ESTAFFORD 7440-38-3 Be by ICP 10 19 ug/L EPA200.7 4114110 ESTAFFORD 7440-70-2 Ca by ICP 0.10 0.95 mg/L EPA200.7 4/14/10 ESTAFFORD 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA 200.8 4/12/10 ESTAFFORD 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA200.8 4/12/10 ESTAFFORD 7439-89-6 Fe by ICP 50 56 ug/L EPA200.7 4/14/10 ESTAFFORD 7439-95-4 Mg by ICP 0.10 0.46 mg/L EPA 200.7 4/14/10 ESTAFFORD 7439-96-5 Mn by ICP 10 IOU ug/L EPA200.7 4114110 ESTAFFORD 7440-23-5 Na by ICP 0.10 96 mg/L EPA200.7 4114110 ESTAFFORD 7440-02-0 Ni by ICPMS 10 IOU ug/L EPA200.8 4/12110 ESTAFFORD 7439-92-1 Pb by ICPMS 10 IOU ug/L EPA 200.8 4112110 ESTAFFORD 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA 200.8 4/12110 ESTAFFORD 7440-66-6 Zn by ICPMS 10 IOU ug/L EPA200,8 4/12110 ESTAFFORD Laboratory Section» 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 733-3903 Fore 4ela0eJ 4esNpYon ofOq queGfermEea rebrlo °:nre eb n w Page 1 of 1 County: MCDOWELL Sample ID: AB56688 River Basin �OF WA7F90 PO Number# 10G0165 Report To AROAP �O v Date Received: 0410812010 t— Time Received: 08:25 Collector. 8 LAVERTY P Y Labworks LoginlD SMATHIS Region: ARO Sample Matrix: GROUNDWATER Report Generated: 4123110 Loc. Type: MONITORING WELL ' Date Reported: 12120/2011 Emergency Yes/No MOD CDC Yes/No Loc.Descr.: COATSAMERICAN Location ID: 1P59MWIICOAT5 I Collect Date: 04/0612010 Collect Time: 10:27 Sample Depth CAS # LAB Analvte Name Sample temperature at receipt by lab PQL Result/ ualifer 1.7 Units °C Method Reference Analysis Date 4/8110 Validated by SNIATHIS MET 7429-90-5 At by ICP 50 500 ug/L EPA200.7 4114110 ESTAFFORD 7440-38-2 AS by furnace 2.0 2.0 U ug/L EPA 200.9 4113110 ESTAFFORD 7440-38-3 Be by ICP 10 70 ug/L EPA200.7 4114110 ESTAFFORD 7440-70-2 Ca by ICP 0.10 12 mg/L EPA200.7 4114110 ESTAFFORD 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA200.8 4112110 ESTAFFORD 7440-47-3 Cr by ICP 10 IOU ug/L EPA200.7 4/14/10 ESTAFFORD 7439-89-6 Fe by ICP 50 550 ug/L EPA200.7 4114/10 ESTAFFORD 7439-95-4 Mg by ICP 0.10 3.6 mg/L EPA 200.7 4/14/10 ESTAFFORD 7439-96-5 Mn by ICP 10 59 ug/L EPA200.7 4114110 ESTAFFORD 7440-23-5 Na by ICP 0.10 15 mg/L EPA200.7 4/14/10 ESTAFFORD 7440-02-0 Ni by ICP 10 IOU ug/L EPA 200.7 4114/10 ESTAFFORD 7439-92-1 Pb by ICPMS 10 IOU ug/L EPA200.8 4/12110 ESTAFFORD 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA 200.E 4/12/10 ESTAFFORD Laboratory Section 1623 Mall Service Center, Raleigh, NC 27699.1623 (919) 733-3908 For a deloled desudpt]on of the quarter Wes rotor to Page 1 of 1 County: MCDOWELL Sample ID: A135666E River Basin WATF9O PO Number # 1000166I �pF O Report To AROAP CO 9 Date Received: Time Received: 0410812010 08:26 Collector. BLAVERTY O C Lebwarks LoginlD SMATHIS Region: ARO Report Generated: 4/23/10 Sample Matrix: GROUNDWATER Date Reported: 1212012011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc.Descr.: COATSAMERICAN Location ID: 1P69MW12COATS I Collect Date: 0410612010 CollectTime: 10:41 Sample Depth Result/Method Analysis CAS # Analvte Name Units Validated by Qualifier Reference Date LAB Sample temperature at receipt by lab 1.7 C 4/8110 SMATNIs NUT NO2+NO3 as N In liquid 0.02 0.02 U mg/L as N Lac10-107-04-1-c 4/12110 CGREEN Nitrate as N in liquid 0.02 0.02 U mg/L as N Lachat107-04-1c 4/13/10 CGREEN Nitrite as N in liquid 0.01 0.01 U mg/L as N Lachal107-04-1-c 418/10 CGREEN MET 7429-90-5 Al by ICP 50 52 ug/L EPA200.7 4114110 ESTAFFORD 7440-38-2 As by ICPMS 2.0 2.0 U ug/L EPA 200.8 4112110 ESTAFFORD 7440-38-3 Be by ICP 10 97 ug/L EPA 200.7 4114110 ESTAFFORD 7440-70-2 Ca by ICP 0.10 48 mg/L EPA 200.7 4114110 ESTAFFORD 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA 200.8 4112110 ESTAFFORD 744047-3 Cr by ICPMS 10 IOU ug/L EPA 200.8 4112/10 ESTAFFORD 7439-89-6 Fe by ICP 50 11000 ug/L EPA 200.7 4/14110 ESTAFFORD 7439-95A Mg by ICP 0.10 10 mg/L EPA 200.7 4114110 ESTAFFORD 7439-96-5 Mn by ICP 10 2100 ug/L EPA 200.7 4/14/10 ESTAFFORD 7440-23-5 Na by ICP 0.10 130 mg/L EPA 200.7 4/14/10 ESTAFFORD 7440-02-0 Ni by ICPMS 10 IOU ug/L EPA 200.8 4/12/10 ESTAFFORD 7439-92-1 Pb by ICPMS 10 IOU uglL EPA 200.8 4/12110 ESTAFFORD 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 4/12J10 ESTAFFORD I i Laboratory Section» 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 733.3908 Fw B dMbd&Bw,10„ d Uh. 05w N., RW t. Ifl irttle fl l Page 1 of 1 1 County: MCDOWELL Sample ID: AB56690 River Basin pF WATFq �� 0� PO Number# 10GO167 Report To AROAP =' r Date Received: 04/08/2010 Time Received: 08:25 Collector. a LgVERTY O Y Labworks LoginlD SMATHIS Region: ARO Report Generated: 4/23/10 Sample Matrix GROUNDWATER Date Reported: 12202011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc.Descr.: COATSAMERICAN Location ID: 1P59MW13COAT$ Collect Date: 0410612010 CollectTime: 10:61 Sample Depth CAS # LAB Analvte Name Sample temperature at receipt by lab PgL Result/ 0ualifier 1.7 Units 'C Method Reference Analysis Date 4/6/10 validated by SMATHIS NUT NO2+NO3 as N in liquid 0.02 0.02 U mg/Las N Le010-107-04-1-c 4/1W10 1 CGREEN Nitrate as N in liquid 0.02 0.02 U mg/L as N Lachat107-04-1c 4113/10 1 CGREEN Nitrite as N in liquid 0.01 0.01 U mg/L as N Lachat107-04-1-c 4/8/10 CGREEN MET 7429-90-5 At by ICP 50 110 ug/L EPA200.7 4114110 ESTAFFORD 7440-38-2 As by furnace 2.0 2.0 U ug/L EPA200.9 4/13110 ESTAFFORD 7440-38-3 Be by ICP 10 34 ugll. EPA200.7 4114110 ESTAFFORD 7440-70.2 Ca by ICP 0.10 13 mg/L EPA200.7 4/14110 ESTAFFORD 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA200.8 4112110 ESTAFFORD 744"7-3 Cr by ICPMS 10 IOU ug/L EPA200.8 4/12110 ESTAFFORD 7439-89.6 Fe by ICP 50 470 ug/L EPA200.7 4/14/10 ESTAFFORD 7439-95-4 Mg by ICP 0.10 8.7 mg/L EPA200.7 4/14/10 ESTAFFORD 7439-96-5 Mn by ICP 10 200 ug/L EPA2003 4/14/10 ESTAFFORD 7440-23-5 Na by ICP 0.10 74 mg/L EPA200.7 4114/10 ESTAFFORD 7440-02-0 Ni by ICPMS 10 IOU ug/L EPA200.8 4112110 ESTAFFORD 7439-92-1 Pb by ICPMS 10 IOU ug/L EPA200.8 4/12/10 ESTAFFORD 7782-09-2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 4112110 ESTAFFORD Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Fore EeleAW Ee5ai0�on or Ne 9vaRar wOea refer to ptyl/wrlo nen b n i Page 1 of 1 County: River Basin Report To Collector. MCDOWELL AROAP 8 LAVERTY OF WAT'F9 O� �G� > � T Sample ID: PO Number# Date Received: Time Received: Labworks LogInID AB56691 10GO168' 0410812010 SMA SMATHIS Region: Sample Matrix: Loc. Type: ARO GROUNDWATER MONITORING WELL Report Generated: Date Reported: 10 12/20/2011 12/2 Emergency Yes/No VisitlD COC YeslNo Loc.Descr.: COATSAMERICAN Location ID: 1P59MW13COATS I Collect Date: 04/06/2010 Collect Time: 11:17 Sample Depth CAS # Analvte Name PQL Result/Units Method Analysis Validated by Qualifier Reference Dale LAB Sample temperature at receipt by lab 1.7 °c 4/8/10 SMATHIS MET 7429-90-5 Al by ICP 50 1700 ug/L EPA200.7 4114/10 j ESTAFFORD 7440-38.2 As by ICPMS 2.0 2.0 U ug/L EPA 200.8 4/12/10 I ESTAFFORD 7440-38-3 Be by ICP 10 140 ug/L EPA200.7 4/14/10 1 ESTAFFORD 7440-70-2 Ca by ICP 0.10 74 mg/L EPA200.7 4114110 ESTAFFORD 744043-9 Cd by ICPMS 1.0 1.0 U ug/L EPA 200.8 4112110 ESTAFFORD 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA200.8 4/12/10 ESTAFFORD 7439-89-6 Fe by ICP 50 9900 ug/L EPA 200.7 4114110 ESTAFFORD 7439-95-4 Mg by ICP 0.10 47 mg/L EPA 200.7 4/14/10 ESTAFFORD 7439-96-5 Mn by ICP 10 470 ug/L EPA 200.7 4114/10 ESTAFFORD 7440-23-5 Na by ICP 0.10 51 mg/L EPA 200.7 4114110 ESTAFFORD 7440-02-0 Ni by ICPMS 10 IOU ug/L EPA 200.8 4112110 ESTAFFORD 7439-92-1 Pb by ICPMS 10 21 ug/L EPA200.8 4/12110 ESTAFFORD 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 4112110 I ESTAFFORD SEM 7439-96-5 Semivolatile Organics (BNAs) in liquid _TITLE_ ug/L EPA625/827013510 4/12/10 NGOOD 62-53-3 Aniline 12 Not detected ug/L EPA625/8270/3510 4112/10 I' NGOOD 108-95-2 Phenol 10 Not detected ug/L EPA625/827013510 4/12/10 NGOOD 111-44-4 BIs(2-chloroethyl)ether 10 Not detected ug/L EPA6251827013510 4112110 NGOOD 95-57-8 Chlorophenol, 2- 10 Not detected ug/L EPA625/827013510 4/12/10 NGOOD 541-73-1 Dichlorobenzene, 1,3 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 106-46-7 Dichlorobenzene, 1,4- 10 Not detected ug/L EPA625/827013510 4112110 NGOOD 100-51-6 Benzyl alcohol 20 Not detected ug/L EPA625/827013510 4112/10 NGOOD 95-50-1 Dichlorobenzene, 1,2- 10 Not detected ug/l. EPA625/8270/3510 4/12110 NGOOD 95-48-7 Methylphenol, 2- 10 Not detected ug/L EPA625/8270/3510 4112110 NGOOD 39638-32-9 Bis(2-chloroisopropyl)ether 10 Not detected ug/L EPA62518270/3510 4112110 NGOOD 106-44-5 Methylphenol, 4- 10 Not detected ug/L EPA625/827013510 4112/10. NGOOD 621-64-7 N-nitrosodi-n-propylamine 12 Not detected ug/L EPA625/827013510 4/12110 NGOOD 67-72-1 HeXachloroethane 10 Not detected ug/L EPA625/827013510 4/12/10 NGOOD 98-95-3 Nitrobenzene 10 Not detected ug/L EPA625/8270/3510 4112/10 NGOOD 78-59-1 Isophorone 12 Not detected ug/L EPA6251027013510 4/12110 NGOOD Laboratory Section 1623 Mail Service Center, Raleigh, NO 27699-1623 (919)733.3908 For a delafled deserlpdon of the qualldermdes refer to m// mna ewe ° er.°nm9n°o/noxnnoh man: owm a�° n� c°ae.an °>/ oortai nMen.e MrccE/w°nabM°none/rcmonsn Page 1 of 3 NCfD'WQ-La6oratorySection ftsults Location ID: 1P69MW13COATS Sample 10: AB66691 Collect Date: 04/0612010 Collect 7me:: 11:17 SEM Result/Units Method Analysis CAS # Analvte Name PQL Validated by ualifier Reference Date 88-75-5 Nitrophenol, 2- 10 Not detected ug/L EPA625/827013510 4/12110 NGOOD 105-67-9 Dimethylphenol, 2,4- 10 Not detected ug/L EPA62518270/3510 4/12110 NGOOD 65-85-0 Benzoic acid 50 Not detected ug/L EPA6251827013510 4/12/10 NGOOD 111-91-1 Bis(2-chloroethoxy)methane 12 Not detected ug/L EPA625/8270/3510 4/12110 NGOOD 120-83-2 D'Ichlorophenol, 2,4- 10 Not detected ug/L EPA625/8270/3510 4/12110 NGOOD 120-82-1 Trichlorobenzene, 1,2,4- 10 Not detected ug/L EPA625/827013510 4/12/10 NGOOD 91-20-3 Naphthalene(SV) 10 Not detected ug/L EPAS251827013510 4112110 NGOOD 106-47-8 Chloroaniline,4- 20 Not detected ug/L EPA6251827013510 4/12/10 WOOD 87-68-3 Hexachlorobutadiene(S\o 10 Not detected ug/L EPA625/827013510 4112110 NGOOD 59-50-7 Chloro-3-methyl phenol, 4- 20 Not detected ug/L EPA625/627013510 4112110 WOOD 91-57-6 Methylnaphthalene, 2- 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 77-47-4 Hexachlorocyclopentadiene 10 Not detected ug/L EPA625/827013510 4/12110 WOOD 88-06-2 Trichlorophenol, 2,4,6- 10 Not detected ug/L EPA625/827013510 4/12/10 NGOOD 95-95-4 Trichlorophenol,2,4,5- 10 Not detected ug/L EPA625/8270/3510 4/12/10 WOOD 91-58-7 Chloronaphthalene, 2- 10 Not detected ug/L EPA625/8270/3510 4/12/10 WOOD 88-744 Nltroanlllne, 2- 50 Not detected ug/L EPA625/827013510 4/12/10 NGOOD 131-11-3 Dimethyl phthalate 10 Not detected ug/L EPA625/827013510 4112110 NGOOD 208-96-8 Acenaphthylene 10 Not detected ug/L EPA625/827013510 4/12110 NGOOD 606-20-2 Dinitrotoluene, 2,6- 10 Not detected ug/L EPA625/8270/3510 4112/10 NGOOD 99-09-2 Nitroaniline, 3- 50 Not detected ug/L EPA62518270/3510 4112110 NGOOD 83-32-9 Acenaphthene 10 Not detected ug/L EPA625/827013510 4/12/10 WOOD 51-28-5 Dinitrophenol, 2,4- 50 Not detected ug/L EPAS25/827013510 4/12110 NGOOD 100-02-7 Nitrophenol, 4- 50 Not detected ug/L EPA625/827013510 4112/10 NGOOD 132-64-9 Dibenzofuran 10 Not detected ug/L EPA625/827013510 4112110 WOOD 121-14-2 Dinitrotoluene, 2,4- 10 Not detected ug/L EPA62518270/3510 4112/10 NGOOD 84-66-2 Diethyl phthalate 10 Not detected uglL EPA625/827013510 4112/10 NGOOD 7005-72-3 Chlorophenyl phenyl ether, 4- 10 Not detected ug/L EPA625/827013510 4/12/10 NGOOD 86-73-7 Fluorene 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 100-01-6 Nitroaniline, 4- 50 Not detected ug/L EPA625/827013510 4/12/10 NGOOD 534-52-1 Dinitro-2-methyl phenol, 4,6- 50 Not detected ug/L EPA6251827013510 4/12/10 NGOOD 86-30-6 N-nitrosodiphenylamine 10 Not detected ug/L EPA62518270/3510 4/12/10 NGOOD 101-55-3 Bromophenyl phenyl ether, 4- 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 118-74-1 Hexachlorobenzene 10 Not detected ug/L EPA625/827013SI0 4/12/10 NGOOD 87-86-5 Pentachlorophenol 60 Not detected ug/L EPA625/827013510 4112110 NGOOD 85-01-8 Phenanthrene 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 120-12-7 Anthracene 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 84-74-2 Di-n-butyl phthalate 10 Not detected ug/L EPA625/8270/3510 4112110 NGOOD 206-44-0 Fluoranthene 10 Not detected ug/L EPA62518270/3510 4/12/10 NGOOD 129-00-0 Pyrene 10 Not detected ug/L EPA625/8270/3510 4/12/10 NGOOD 85-68-7 Butylbenzyl phthalate 10 Not detected ug/L EPAG25/0270/3510 4/12110 NGOOD 91-94-1 Dichlorobenzidine, 3,3'- 20 Not detected ug/L EPA625/8270/3510 4112/10 NGOOD 56-55-3 Benzo(a)anthracene 10 Not detected ug/L EPA6251827013510 4112/10 NGOOD Laboratory Section» 1623 Mall Service Center, Raleigh, NC 27699-1623 (9191 733-3908 For adetaAM desMpgan of No qualifier woes refer to ff 111,11 ld. Page 2 of 3 NC(E)T,P -La6oratorySectionIRSmfts Location lD: 1P69MW13COATS Sample ID: AB56691 Collect Date: 04/0612010 Collect Time:: 11:17 SEM CAS # 218-01-9 Analvte Name Chrysene PQL 10 Result/ Qualifier Not detected Units ug/L Method Reference EPA625/8270/3510 Analysis Date 4112/10 validated by NGOOD 117-81-7 Bis(2-ethylhexyl)phthalate 10 Not detected ug/L EPA625/827013510 4/12110 NGOOD 117-84-0 Di-n-octyl phthalate 10 Not detected uglL EPA62518270/3510 4112110 NGOOD 205-99-2 Benzo(b)fluoranthene 10 Not detected ug/L EPA625/827013510 4112110 NGOOD 207-08-9 Benzo(k)fluoranthene 10 Not detected ug/L EPA625/827013610 4112110 NGOOD 50-32-8 Benzo(a)pyrene 10 Not detected ug/L EPA6251827013510 4/12110 NGOOD 193-39-5 Indeno(1,2,3-cd)pyrene 10 Not detected ug/L EPA62518270/3510 4112110 NGOOD 53-70-3 Dlbenzo(a,h)anthracene 10 Not detected ug/L EPA62518270/3510 4112/10 NGOOD 191-24-2 Benzo(g,h,l)perylene 10 Not detected ug/L EPA625/8270/3510 4112/10 NGOOD sv1- Hexamethyl cyclotrisiloxane 7 N1 ug/L EPA625/8270/3510 4112/10 NGOOD Laboratory Section» 1623 Mail Service Center, Raleigh, INC 27699-1623 (919) 733.3908 For a 4etaUM desvipton o(Ne auet4arwos toter to r,,a b ae n Page 3 of 3 County: MCDOWELL River Basin ReportTo AROAP Collector. B LAVERTY Region: ARO Sample Matrix: GROUNDWATER Loc.Type: MONITORINGWELL Emergency Yes/No VisitlD COC Yes/No Sample to: I AB56692 VJAI'F9Q �OF PO Number # 10GO169 9 � Date Received: Time Received: 0410812010 08:25 y Labworks LoginlD SMATHIS Report Generated: 516110 Date Reported: 12202011 Loc. Descr.: COATS AMERICAN Location ID: 1P59MW14COATS I Collect Date: 0410612010 Collect Time: 11:17 Sample Depth CAS # Analute Name LAB S Results Units Method Analysis Validated by Qualifier Reference Date Sample temperature at receipt by lab 1.7 °C 4/8110 SMATHIS MET 7429-90-5 Al by ICP 50 64 ug/L EPA200.7 4/14/10 ESTAFFORD 7440-38-2 As by furnace 2.0 2.2 ug/L EPA 200.9 4/13/10 ESTAFFORD 744D-38-3 Be by ICP 10 130 ug/L EPA 200.7 4/14110 ESTAFFORD 7440-70-2 Ca by ICP 0.10 72 mg/L EPA 200.7 4/14110 ESTAFFORD 744G43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA 200.8 4112110 ESTAFFORD 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA 200.8 4112110 ESTAFFORD 7439-89-6 Fe by ICP 50 7200 ug/L EPA2001 4114110 ESTAFFORD 7439-954 Mg by ICP 0.10 46 mg/L EPA200.7 4114110 ESTAFFORD 7439-96-5 Mn by ICP 10 450 ug/L EPA200.7 4114110 ESTAFFORD 7440-23.5 Na by ICP 0.10 50 mg/L EPA2013.7 4/14110 ESTAFFORD 7440-02-0 Ni by ICPMS 10 IOU ug/L EPA200.8 4/12110 ESTAFFORD 7439-92-1 Pb by ICPMS 10 IOU ug/L EPA20D.8 4112/10 ESTAFFORD 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 4/12/10 ESTAFFORD Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a dWde desatp4on ome yuatiAeraes refertotmll1,new oa/web/xv/lee/s monanea,rmsw - n nno i. Page 1 of 1 County: River Basin Report To MCDOWELL AROAP Collector. 8 LAVERTY Region: ARO Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Emergency Yes/No COC Yes/No oaOF WATF,9QG h P T VisitlD Sample ID: PO Number # Date Received: Time Received: Labworks LoginlD Report Generated: Data Reported: Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD RD MARION NC AB74917 ARO 0810912011 08:25 KAMISON 8123/11 11/14/2011 Location 10: 1P59COATSMW2 Collect Date: 0810812011 Collect Time: 09:08 Sample Depth ResulU Method Analysis CAS # Analvte Name S Units Validated by Qualifier Reference Date Others Sample temperature at receipt by lab 1.1 °C 8/9/11 DLEAVITT Turbidity 1 6.0 NTU APHA2130B-20th 8110/11 CGREEN Residue_Suspended in liquid 6.2 6.2 U mg/L APHA25400-20th 8/9/11 CGREEN Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699.1623 (919) 733-3908 For a dolalled descoplion ofdle qualllbr moos refer o W Brorri.roderr o lea dabrslafinfotl Cbe.elat#gala QjAlifeE CNes<htaWstaffnfoftnhnm�t> Page 1 of 1 County: MCDOWELL Sample ID: AB74918 River Basin apP WATFgO O PO Number# ARO Report To AROAP Date Received: 0810912011 Collector. B LAVERTY Y Time Received: 08:25 t? Lebworks LoginlD KJIMISON Region: ARO Report Generated: 8/23/11 Semple Matrix: GROUNDWATER Date Reported: 11/14/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisilID CDC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD RD MARION NO Location ID: 1P69COATSINW2 Collect Date: 0810812011 Collect Time: 09:11 Sample Depth Result/ Method Analysis CAS # Analyte Name S Units Validated by ualifier Reference Date Others Sample temperature at receipt by lab 1.1 °C 8/9111 DLEAVITT Turbidity 1 1000 NTU APHA213oB-20th 8/10/11 CGREEN Residue —Suspended in liquid 6.2 41100 mg/L APHA25400-20th 819111 CGREEN Laboratory Section» 1623 Mail Service Center, Raleigh, NO 27699-1623 (919) 733-3908 For a aet.110 desaiptloO Of the puau0arcoes rekrto Wn rl QO,r1jfi.1c e a it // tlal. Mery Av ela,a nto as le Page 1 of 1 �I County: MCDOWELL Sample ID: AB74928 River Basin WATEgO PO Number # ARO aOF Report To AROAP `O Dale Received: 0810912011 j Time Received: 15:55 Collector: LAVERTY Y p Lebworks LoginlD KJIMISON RARO Region: Report Generated: 8/23/11 Sample Matrix: GROUNDWATER Date Reported: 11/142011 Loc. Type: MONITORING WELL Emergency Yes/No VisigD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD RD MARION NC Location to: 1P59COATSMW2 I Collect Date: 0810912011 1 Collect Time: 09:05 Sample Depth CAS # Analvte Name PQL Result/ Units Method Analysis Validated by Qualifier Reference Date Others Sample temperature at receipt by lab 1.9 °C 819/11 ' DLEAVITT Turbidity 1 150 NTU APHA2130B-20th 8110111 CGREEN Residue —Suspended in liquid 6.2 164 U mg/L APHA2540D-20th 819111 ' CGREEN Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a delared descrimlon ofma qualllkr m es reWlo htt,1/ al n� x Nye na I eP o osskl# elo enxln Mes n' nal.n e M b su mfo na Page 1 of 1 County: MCDOWELL River Basin Report To AROAP Collector. B LAVERTY Region: ARO Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Emergency Yes/No VisitlD CDC Yes/No Sample ID: AB75029 WA7E19 aOF O PO Number# 11G0688' y 9 Date Received: 0811112011 Time Received: 08:00 Labworks LoginlD HMORGAN Report Generated: 9/12111 Date Reported: 11/14/2011 Loc. Descr.: COATS AMERICAN Location ID: 1P59COATSMW2 Collect Date: 0810912011 Collect Time: 09:05 Sample Depth Result/Method Analysis CAS # Analvte Name PQL Units Validated by Qualifier Reference Date LAB Sample temperature at receipt by lab 1.9 °C 8/11/11 DLEAVITT MET 7440-22-4 Ag by ICPMS 5 5.0 U ug/L EPA 200.8 8/15111 ESTAFFORD1 7429-90-5 Al by ICP 50 1300 ug/L EPA 200.7 8/15/11 ESTAFFORD1 7440-38-2 As by ICPMS 2 2.0 U ug/L EPA 200.8 8/15111 ESTAFFORD7 7440-38-3 Be by ICP 10 89 ug/L EPA 200.7 8115/11 ESTAFFORD7 7440-70-2 Ca by ICP 0.1 23 mg/L EPA 200.7 8115111 ESTAFFORD7 7440-43-9 Cd by ICPMS 1 1.0 U ug/L EPA 200.8 8115111 ESTAFFORD1 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA 200.8 8/15/11 ESTAFFORD1 7440-50-8 Cu by ICPMS 2 12 ug/L EPA 200.8 8115111 ESTAFFORDt 7439-89-6 Fe by ICP 50 9100 ug/L EPA 200.7 8115/11 ESTAFFOROI 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA 245.1 9/1/11 ESTAFFORD1 7440-09-7 K by ICP 0.1 1.1 mg/L EPA 200.7 8/15111 ESTAFFORD1 7439-954 Mg by ICP 0.1 12 mg/L EPA 200.7 8/15/11 ESTAFFORD1 7439-96-5 Mn by ICP 10 680 ug/L EPA 200.7 8115111 ESTAFFORD1 7440-23-5 Na by ICP 0.1 11 mg/L EPA 200.7 e/15/11 ESTAFFORD1 7440-02-0 Ni by ICPMS 2 5.7 ug/L EPA 200.8 8/15/11 ESTAFFORD1 7439-92-1 Pb by ICPMS 2 19 ug/L EPA 200.8 8/15/11 ESTAFFORD1 7782-49-2 Se by ICPMS 5 5.0 U ug/L EPA 200.8 8/15111 ESTAFFORD1 7440-66-6 Zn by ICPMS 10 33 ug/L EPA 200.8 8/15111 ESTAFFORD1 Laboratory Section 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a deleted descdpten of the qualifier woes refer ld hft, ll orte nAen a Iwe dabl, R Ise#enln Ounrder C atom n o /w.e rnNsla rnronec Page 1 of 1 County: River Basin Report To MCDOWELL AROAP Collector: B LAVERTY Region: ARO Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Emergency YesJNo COC Yes/No Sample ID: PO Number # Date Received: Time Received: Labworks LoginlD Report Generated: Date Reported: VisiOD Loc. Descl.: COATS AMERICAN 630 AMERICAN THREAD RD MARION NC AB74919 ARO 0810912011 08:25 KJIMISON 8/23111 11/14/2011 Location ID: 1P59COATSMW10 Collect Data 0810812011 Collect Time: 09:26 Sample Dept Result/ Method Analysis CAS # Analvte Name P�(L Units Validated by ualifier Reference Date Others Sample temperature at receipt by lab 1.1 °C 819111 DLEAVITT Turbidity 1 1.9 NTU APHA2130B-20th 8110111 CGREEN Residue —Suspended In liquid 6.2 6.211 mg/L APHA2540D-20th 819111 CGREEN Laboratory Section>> 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For o detahed description of rim qualifier codes refer to Mo, 11rQM,f.nr4evro Ixe� now �' on s9ttt al eual oe c /I al +w awstal ml na Page 1 of 1 County: River Basin Report To MCDOWELL AROAP Collector: B LAVERTY Region: ARO Semple Matrix: GROUNDWATER Loc. Type: MONITORING WELL Emergency Yes/No COC Yes/No Sample ID: PO Number 0 Date Received: Time Received: Lebwarks LoginlD Report Generated: Date Reported: VisiOD Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD RD MARION NC AB74929 ARC) ' 08/0912011 15:55 KJIMISON 8/23/11 11/14/2011 LocaOonlD: IP59COATSMWID Collect Date: 0810912011 Collect Time: 09:15 Sample Depth CAS # Analvte Name P(�'. LL Result/ Units Method Analysis Validated by ualifier Reference Date Others Sample temperature at receipt by lab 1.9 °c 8/9/11 DLEAVITT Turbidity 1 7.0 NTU APHA2130B-20th 8/10/11 CGREEN Residue —Suspended In liquid 6.2 15 mg/L APHA2540D-20th 819/11 CGREEN Laboratory Section 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detaOed description of Me 9uafflor codes refer to Mt 11yonal. no /stxlri odee asslsldoala Oualn codes <hraL Msla orlon nas Ise Page 1 of 1 County: MCDOWELL Sample ID: AB75030 River Basin OF WA 7-F9 11 9y PO Number# 11GO689 Report To AROAP h >_ r Date Received: Time Received: 0811112011 08:00 Collector: B LAVERTY ti Lebworks LoginlD HMORGAN Region: ARO Report 11 Sample Matrix: GROUNDWATER Date Reported: ported: 1111 11/14/2011 Loc. Type: MONITORING WELL Emergency Yes/No Visitlo COC Yes/No Loc. Descr.: COATS AMERICAN Location ID: 1P59C0ATSMW10 Collect Date: 08/0912011 Collect Time: 09:15 Sample Depth Result/Units Method Analysis CAS # Analvte Name P(�. LL Validated by Qualifier 'Reference Date LAB Sample temperature at receipt by lab 1.9 °C 8/11111 DLEAVITT MET 1, 7440-224 Ag by ICPMS 5 5.0 U ug/L EPA 200.8 8/15/11 ESTAFFORD1 7429-90-5 At by ICP 50 180 ug/L EPA 200.7 8/15111 ESTAFFORD7 7440-38.2 As by ICPMS 2 2.0 U ug/L EPA 200.8 8/18/11 ESTAFFORD1 7440-38-3 Be by ICP 10 31 ug/L EPA200.7 8115111 ESTAFFORD1 7440-70-2 Ca by ICP 0.1 0.20 mg/L EPA200.7 8/15/11 ESTAFFORD1 7440-43-9 Cd by ICPMS 1 1.0 U ug/L EPA 200.8 8/15/11 ESTAFFORDt 7440-47-3 Cr by ICPMS 10 11 ug/L EPA 200.8 8/15/11 ESTAFFORD1 7440-50-8 Cu by ICPMS 2 4.3 ug/L EPA 200.8 8/15/11 ESTAFFORD1 7439-89-6 Fe by ICP 50 350 ug/L EPA 200.7 8/15111 ESTAFFORD1 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA 245.1 9/1111 ESTAFFORD1 7440-09-7 K by ICP 0.1 0.46 mg/L EPA 200.7 8/15/11 ESTAFFORD1 7439-954 Mg by ICP 0.1 0.10 U mg/L EPA 200.7 8/15/11 ESTAFFORD1 7439-96-5 Mn by ICP 10 IOU ug/L EPA 200.7 8115/11 ESTAFFORD1 7440-23.5 Na by ICP 0.1 45 mg/L EPA 200.7 8/15/11 ESTAFFORD1 7440-02-0 Ni by ICPMS 2 2.0 U ug/L EPA 200.8 8115111 ESTAFFORD1 7439-92-1 Pb by ICPMS 2 2.0 U ug/L EPA 200.8 8115111 ESTAFFORD1 7782-49-2 Se by ICPMS 5 5.0 U ug/L EPA 200.8 8115111 ESTAFFORD7 7440-66-6 Zn by ICPMS 10 IOU ug/L EPA 200.8 8116111 ESTAFFORD1 Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699.1623 (919) 733J908 Fora deaUeddescdpuon prthe qualldercodesmkrtohn ll o alnWeMe,Aabl.slat,WoAeMassisitOeta QuAliflyr CWesh datnWenr.o ee IIANStaffnfOAeOaSSISI> Page 1 of 1 County: MCDOWELL Sample ID: AB7 River Basin �pF WA�e•90 Gy PO Number# ARO Report To ARDAP h L- Date Received: 08109, Time Received: 08:25 Collector.BLAVERTY p Y Labworks LoginlD KJIMI Region: Region::RO Report Generated: 8/23P Semple Matrix: G GROUNDWATER Date Reported: 11114 Loc. Type: MONITORING WELL Emergency Yes/No VisiOD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD RD MARION NC Location ID: 1P59COATSMW11 Collect Date: 0810812011 Collect Time: 09:39 Sample Depth ResuIV Method Analysis' CAS # Analvte Name PQL Units Validated by Qualifier Reference Date i Others Sample temperature at receipt by lab 1.1 C 8/9/11 1 DLEAVITT Turbidity 1 4-5 NTU APHA2130B-20th 8/10111 ' CGREEN Residue —Suspended in liquid 6.2 6.2 tJ mg/L APHA2540D-20th 8/9111 i CGREEN Laboratory Section>> 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Fora demeed desoapnco arms quaAMrcoaes reterta hop llroOaLroderrM analslnF o e ism nie ,wmer II J aln a Me ad la nr s.h Page 1 of 1 County: MCDOWELL Sample ID: AB74930 River Basin �OF WATFgO O PO Number# ARO Report To AROAP Date Received: 0810912011 Time Received: 15:55 Collector. BLAVERTY p T Labworks LoginlD KJIMISON Region: ARO Report Generated: 8/23111 Sample Matnx: GROUNDWATER D ate Reported: 11/14/2011 Loc. Typo: MONITORING WELL Emergency Yes/No VlsitlD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD RD MARION NO Location ID: IP59COATSMWll Collect Data 0810912011 Collect Time: 09:31 Sample Depth CAS # Analyte Name S Result/ Units Method Analysis Validated by Qualifier Reference Date Others Sample temperature at receipt by lab 1.9 C 819/11 1 DLEAVITT Turbidity 1 1.9 NTU APHA2130B-20th 8110111 II ' CGREEN Residue —Suspended in liquid 6.2 5.5 mg/L APHA2540D-201h 8/9111 1 CGREEN Laboratory Section» 1623 Mali Service Center, Raleigh, NO 27699.1623 (919) 733-3908 Fora delalled deamp0an of NO Qua00ereodoa referto nit / onn nme na / al! lonedia Isip le Ide / onal.nmenr.o Me naw la m! ne n Page 1 of 1 County: MCDOWELL Sample ID: AB75031 WATF9O River Basin �OF G PO Number# 11GO690 Report To AROAP �O j Date Received: Time Received: 0811112011 08:00 Collector.GROUNDWATER p -c Labworks LoglnlD HMORGAN Region::RO Region: Report Generated: 9112/11 Sample Matrix: GROUNDWATER Date Reported: 11/14/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN Location ID: IP59COATSMWll Collect Date: 0810912011 Collect Time: 09:31 Sample Depth CAS # Analvte Name PQL Result/ Units Method Analysis Validated by Qualifier Reference Date LAB Sample temperature at receipt by lab 1.9 °C 8/11111 DLEAVITT MET 7440-22A Ag by ICPMS 5 5.0 U ug/L EPA200.8 ! 8115/11 '' ESTAFFORDI 7429-90-5 Al by ICP 50 50 U ug/L EPA 200.7 8/15111 ESTAFFORDI 7440-38-2 As by ICPMS 2 2.0 U ug/L EPA 200.8 8115/11 ESTAFFCRD1 7440-38-3 Ba by ICP 10 100 ug/L EPA 200.7 8/15/11 ESTAFFORDI 7440-70-2 Ca by ICP 0.1 26 mg/L EPA 200.7 8116111 ESTAFFORDI 744043-9 Cd by ICPMS 1 1.0 U ug/L EPA 200.8 8/15/11 ESTAFFORDI 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA 200.8 8116111 ESTAFFORDI 7440-50-8 Cu by ICPMS 2 7.9 ug/L EPA 200.8 8/15/11 ESTAFFORDI 7439-BM Fe by ICP 50 2000 ug/L EPA 200.7 8/16/11 ESTAFFORDI 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA 245.1 911111 ESTAFFORDI 7440-09-7 K by ICP 0.1 6.3 mg/L EPA 200.7 8/15/11 ESTAFFORD1 7439-95-4 Mg by ICP 0.1 9.1 mg/L EPA 200.7 8/15111 ESTAFFORD1 7439-96-5 Mn by ICP 10 590 ug/L EPA 200.7 8115111 ESTAFFORDI 7440-23-5 Na by ICP 0.1 77 mg/L EPA 200.7 8/15/11 ESTAFFORD1 7440-02-0 Ni by ICPMS 2 2.0 U ug/L EPA 200.8 8/16111 ESTAFFORDI 7439-92-1 Pb by ICPMS 2 2.0 U ug/L EPA 200.8 8115/11 ESTAFFORD1 7782-49-2 Se by ICPMS 5 5.0 U ug/L EPA 200.8 8115/11 ESTAFFORDI 7440-66-6 Zn by ICPMS 10 IOU ug/L EPA 200.8 8/15MI ESTAFFORD1 Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699.1623 (919( 733-39D8 Fare OeleOeE aesalption otlpe 9uzGlarcaEes,akrio n ! nNe r ed nam afinla asalsiPenla wx40. cm < , nal. /w. aNSUlfnfMe nuu, Page 1 of 1 County: MCDOWELL Sample ID: AB74921 River Basin �OF WArF19 PO Number # ARO Report To AROAP 1 Date Received: 0810912I11 Collector.a LAVERTY O Y Time Received: 08:25 Lebwarks LoginlD KJIMISON Region: ARO Report Generated: 6/23111� Sample Matra: GROUNDWATER Data Reported: 11/14126111 Loc.Type: MONITORING WELL Emergency YesMo VisitlD j CDC Yes/No Lac. Descr.: COATS AMERICAN 630 AMERICAN THREAD RD MARION NO Location ID: 1P59COATSMW72 Collect Date: 08/08/2011 Collect Time: 09:48 Sample Depth Result/ Method Analysis CAS # Analyte Name POL Units Validated by ualifier Reference Dale Others Sample temperature at receipt by lab 1.1 so 8/22111 CGREEN 120 Residue —Suspended in liquid 6.2 26 mg/L APHA2540D-20th 8/9111 CGREEN Laboratory Section» 1623 Mali Service Center, Raleigh, NO 27699-1623 (919) 733.3908 For a detailed description of the quatworwdes.%,to are Irmtrol rincarr Q1111alar Code, le flor,111tianr /w OaNsla 'nlonecha sl Page 1 of 1 County: MCDOWELL Sample ID: AB74931 River Basin �OF WA7F9O O PO Number# ARO Report To AROAP y Date Received: 08/09/2I11 Collector. LAVERTY Time Received: 15:55 p Y Labworks LoginlD KJIMISON Region: RO A Sample Matrix: Report Generated: 8123111II GROUNDWATER D ate Reported: 11/14/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD RD MARION NC Location ID: 1P59COATSMWI2 Collect Date: 0810912011 Collect Time: 09:42 Sample Depth Result/Method Analysis CAS # Analvte Name P L Units Validated by ualifier Reference Date Others Ili Sample temperature at receipt by lab 1.9 °C 8/22/11 CGREEN Residue —Suspended in liquid 6.2 17 mg/L APHA2540D-20th 8/9111 CGREEN Laboratory Section>> 1623 Mall Service Center, Raleigh, NC 27699.1623 (919) 733-3908 Faredelelled d.eWptlon arm. q. tftr.des re Wo h9p Nporni0iinfirerCod / e /la sl nfonern .. Is Page 1 of 1 County: MCDOWELL River Basin Report To AROAP Collector: B LAVERTY Region: ARO Sample Matrix: GROUNDWATER Loc.Type: MONITORING WELL Emergency Yes/No COC Yes/No oa�F W ATFjr,OG h O Y VisitlD Loc. Descr.: COATS AMERICAN Sample ID: PO Number # Date Received: Time Received: Labworks LoginlD Report Generated: Date Reported: AB75032 1100691 08/1112011 08:00 HMORGAN 9/12111 11/14/2011 Location ID: 1P59COATSMWI2 Collect Date: 08/09/2011 Collect Time: 09:42 Sample Depth CAS # Analyle Name LAB S Units ResulU Method Analysis Validated by Qualifier Reference Date Sample temperature at receipt by lab 1.9 °C 8111111 DLEAVITT MET 7440-224 Ag by ICPMS 5 6.0 U ug/L EPA 200.8 8115111 1 ESTAFFORD1 7429-90-5 Al by ICP 50 90 ug/L EPA 200.7 8115/11 ESTAFFORD1 7440-38-2 As by ICPMS 2 2.0 U ug/L EPA 200.8 8/15/11 ESTAFFORD1 7440-38-3 Be by ICP 10 110 ug/L EPA 200.7 8/15/11 ESTAFFORD1 7440-70-2 Ca by ICP 0.1 47 mg/L EPA 200.7 8/15/11 ESTAFFORD1 7440-43-9 Cd by ICPMS 1 1.0 U ug/L EPA 200.8 8/15111 ESTAFFORD1 7440-47-3 Cr by ICPMS 10 10 U ug/L EPA 200.8 8/15111 ESTAFFORD1 7440-50-8 Cu by ICPMS 2 6.5 ug/L EPA 200.8 8115/11 ESTAFFORD1 7439-89-6 Fe by ICP 50 7900 ug/L EPA 200.7 8/15/11 ESTAFFORD1 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA 245.1 9/1111 ESTAFFORD1 7440-09-7 K by ICP 0.1 4.4 mg/L EPA 200.7 8/15/11 ESTAFFORD1 7439-95-4 Mg by ICP 0.1 9.8 mg/L EPA 200.7 8115/11 ESTAFFORD1 7439-96-5 Mn by ICP 10 1900 ug/L EPA 200.7 8115/11 ESTAFFORD1 7440-23-5 Na by ICP 0.1 190 mg/L EPA 200.7 8/15/11 ESTAFFORD1 7440-02-0 Ni by ICPMS 2 7.7 ug/L EPA 200.8 8/15111 ESTAFFORD1 7439-92-1 Pb by ICPMS 2 2.0 U ug/L EPA 200.8 8/15/11 ESTAFFORDI 7782-49-2 Se by ICPMS 5 5.0 U ug/L EPA 200.8 8/15/11 ESTAFFORD1 7440-66-6 Zn by ICPMS 10 10 U ug/L EPA 200.8 8115111 ESTAFFORD1 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a dole Had! deaulpuon of the qualifier coins ranee hit,L nl.nedo M1M naOtstaRnfo assislx atea i in we odes 011ip Pool a I r men ro meb a betuflneAechilssuir,o Page 1 of 1 County. River Basin Report To Collector. MCDOWELL AROAP B LAVERTY �OF > O t Sample ID: PO Number Date Received: Time Received: Lobworks LoginlD AB74922 ARO 0810912011 08:25 KJIMISON Region: ARO Report Generated: 8123/11 Sample Matrix. Loc.Type: GROUNDWATER MONITORINGWELL Dale Reported: 11/14/2011 Emergency Yes/No VIsHID CDC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD RD MARION NC Location ID: 1P59COATSMWI3 Collect Date: 0810812011 Collect Time: 09:64 Sample Depth CAS # Anaivte Name PgL ResulU Units Method Analysis Validated by ualifier Reference Dale Others Sample temperature at receipt by lab 1.1 'C 8/9111 DLEAVITT Turbidity 1 25 NTU APHA21306-20th e/10/11 CGREEN Residue —Suspended in liquid 6.2 34 m9/L APHA2540D-20th 819/11 CGREEN Laboratory Section>> 1623 Mall Service Center, Raleigh, NC 27699-1623 (919( 733-3908 For a detelled dosvlplioo orNe quarlercode3 raterto h1p "Porlof PoloIrBaNsdKb 't0 a TheeC t' In MWslart fM �a s' Page 1 of 1 County: River Basln Report To Collector. Region: MCDOWELL AROAP B LAVERTY ARO �OF WAIQ9 O G7E P < SemplelD: PO Number# Date Received: Time Received: Labworks LoginlD AB74923 ARO 08/0912011 08:25� KJIMISON Sample Matrix: GROUNDWATER Report Generated: Date Reported: 8/23/11 11114/2011 Loc.Type: MONITORING WELL Emergency Yes/No VisiUD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD RD MARION NC Location ID: 1P59COATSMW74 Collect Dale: 08108/2011 Collect Time: 10:00 Sample Depth CAS # Analvte Name S Result/ Units Method Analysis Validated by Qualifier Reference Date Others Sample temperature at receipt by lab 1.1 C 819111 DLEAVITT Turbidity 1 80 NTU APHA2130B-20ih 8/10111 CGREEN Residue —Suspended in liquid 6.2 47 mall- APHA2540D-20th 819111 CGREEN Laboratory Section>> 1623 Mall Service Center, Raleigh, NC 27699.1623 (919( 7334908 Far a detIM dlsuIPgn V the gnlmreww.%r to bft0.Mr,,Iwe eh seine In 0mlll a Aveh , MelI in VI,k Page 1 of 1 County: MCDOWELL Sample ID: AB74932 River Basin pF W A7Fq O� PO Number # ARO Report To AROAP r�0� Date Received: 0810912011 Received: 15:55 CollectoTime B LAVERTY t p Labworks Lo9inlD KJIMISON Region; Region:; ARO Report Generated: 8123111 Sample Matrix: GROUNDWATER D ale Reported: 11/14/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD RD MARION NC Location To: 1P59COATSMW74 Collect Date: 0810912011 Collect Time: 10:12 Sample Depth CAS # Analyte Name S Result/ Units Method Analysis Validated by Qualifier Reference Date Others I Sample temperature at receipt by lab 1.9 C e/9/11 i DLEAVITT Turbidity 1 49 NTU APHA2130B-20th 8/10/11 1 CGREEN Residue Suspended in liquid 6.2 16 mg/L APHA2540D-20th 6/9/11i CGREEN Laboratory Section» 1623 Mall Service Center, Raleigh, NO 27699.1623 (919) 733-3908 For a detaoed description ortne quaReroodes Rrertp hITp r aE Tinto ceassl la ete unr a CM aln o Ave Msla mton ssist I Page 1 of 1 County: MCDOWELL Sample ID: A875033 River Basin apF WATFi1+Q O Gy PO Number# 11GO692 Report To AROAP h Date Received: 08/11/2011 �_ y Time Received: 08:00 Collector: B LAVERTY p Labworks LoginlD HMORGAN Region: ARO Report Generated: 9/12/11 Sample Matrix: GROUNDWATER Date Reported: 11/14/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisitiD COC Yes/No Loc. Descr.: COATS AMERICAN Location ID: 1P59COATSMW14 Collect Dale: 0810912011 Collect Time: 10:12 Sample Depth CAS # AnalYte Name PQL Result/ Units Method Analysis Validated by Qualifier Reference Date LAB Sample temperature at receipt by lab 1.9 °C 8/11/11 DLEAVITr MET 7440-22-4 Ag by ICPMS 5 5.0 U ug(L EPA 200.8 8/15/11 ESTAFFORDI 7429-90-5 At by ICP 50 62 ug/L EPA 200.7 8/15/11 ESTAFFORD1 7440-38-2 As by ICPMS 2 2.0 U ug/L EPA 200.8 8/15/11 ESTAFFORDI 7440-38-3 Be by ICP 10 110 ug/L EPA 200.7 8/15/11 ESTAFFORDI 7440-70-2 Ca by ICP 0.1 69 mg/L EPA 200.7 8/15/11 ESTAFFORDI 744043-9 Cd by ICPMS 1 1.0 U ug/L EPA 200.8 8/15111 ESTAFFORDI 744047-3 Cr by ICPMS 10 IOU ug/L EPA 200.8 8115111 ESTAFFORDI 7440-50-8 Cu by ICPMS 2 18 ug/L EPA 200.8 8/15111 ESTAFFORDI 7439-89-6 Fe by ICP 50 5800 ug/L EPA 200.7 8/15/11 ESTAFFORDI 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA 245.1 911/11 ESTAFFORDI 7440-09-7 K by ICP 0.1 1.2 mg/L EPA 200.7 8/15111 ESTAFFORDI 7439-95-4 Mg by ICP 0.1 44 mg/L EPA 200.7 8115111, ESTAFFORDI 7439-96-5 Mn by ICP 10 990 ug/L EPA 200.7 8/16111 ESTAFFORDI 7440-23-5 Na by ICP 0.1 50 mg/L EPA 200.7 8/15/111 ESTAFFORDI 7440-02-0 Ni by ICPMS 2 2.5 ug/L EPA 200.8 8/15111 I ESTAFFORDI 7438-82-1 Pb by ICPMS 2 2.0 U ug/L EPA 200.8 8/15/11 1, ESTAFFORDI 7782-49-2 Se by ICPMS 5 5.0 U ug/L EPA 200.8 0/15/11' ESTAFFORDI 7440-66-6 Zn by ICPMS 10 IOU ug/L EPA 200.8 8115/11 ESTAFFORDI Laboratory Section 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 733.3908 Fora 4eleDe44ezvryNon afNe quafif rmEez relerlo Fn R o al [Oe na Flo .id auouatrer cwp, nn :/ al N ulgnfo/1 Page 1 of 1 County: MCDOWELL Sample ID: AB74924 River Basin OF WATe9 PO Number# ARC Report To �� q� AROAP H Date Received: 081091201; Collector. B LAVERTY p Time Received: 08:25 -~c Labworks LoginlD KAMISON Region: RO Report Generated: 8123/11 Sample Matrix: G GROUNDWATER D ate Reported: 11114/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisIOD CDC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD RO MARION NC Location ID: IP59COATSMWIS Collect Date: 08/0812011 Collect Time: 10:09 Sample Depth CAS # Analvte Name POL Result/Units Method Analysis Validated by ualifier Reference Date Others Sample temperature at receipt by lab 1.1 °C 8/9111 DLEAVITT Turbidity 1 15 NTU APHA213OB-20th 8/10111 CGREEN Residue —Suspended in liquid 6.2 6.2 U mg/L APHA2540D-20th 819111 CGREEN Laboratory Section» 1623 Mall Service Center, Raleigh, NC 27699.1623 (919) 7334908 Foradv.sW da,Wsonomequeflfief UEes Rwto hl I nai nw2 fn MB. 'IPdSlnRinlO RIPIK Pld rcMec <MI'/ aln nf0 /wP /IT6'Id n(O/I IITssi Page 1 of 1 County: MCDOWELL Sample ID: AB94211 River Basin OFWprF9 tit, OG PO Number # 13GO265 Report To AROAP _y Dale Received: 0411112013 Time Received: 08:00 Collector. B LAVERTY P Y Labworks LoginlD HMORGAN Region: ARO Final Report Dale; 4127113 Sample Matrix: GROUNDWATER Final Report Report Print Date: 0 2 Loc. Type: MONITORING WELL i'— Emergency Yes/No VlslllD 1 '-i E C rE e VE: U CDC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD ROAD MARION, NC I I ,,,r Location ID: 1P69C0ATSMW2 Collect Dale; 0410912013 Collect Time: 09:22 , Sample Depth esheville Regions Office If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purpo _ Aquifer Protection -- Result/ Method Analysis # Analyte Name POL ualifier Units Reference Validated byCAS Date LAB Sample temperature at receipt by lab 2.0 C 4/11113 HMORGAN Volatile Organics in liquid _TITLE_ ug/L EPA50301824/8260 4/lV13 ACHANDLER 75-71-8 Dichlorodifluoromethane 1.0 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 74-87-3 Chloromethane 1.0 Net detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 75-014 Vinyl Chloride 0.50 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 74-83-9 Bromomethane 1.0 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 75-00-3 Chloroethane 0.50 Not detected ug/L EPA5030/624/8260 4111/13 ACHANDLER 75-694 Trichlorofluoromethane 0.50 Not detected ug/L EPA5030/62418260 4/11113 ACHANDLER 75-35-4 1,1-Dichloroethene 0.25 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 75-09-2 Methylene Chloride 10 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 156-60-5 trans-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 1834-04-4 Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPA5030/624/8260 4111113 ACHANDLER 75-34-3 1,1-Dichloroethane 0.25 Not detected ug(L EPA5030/624/8260 4111/13 ACHANDLER 156-59-2 CIS-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 4M1/13 ACHANDLER 74-97-5 Bromochloromethane 0.25 Not detected ug/L EPA5030162418260 4/11/13 ACHANDLER 67-66-3 Chloroform 0.25 1.6 ug/L EPA5030162418260 4111113 ACHANDLER 594-20-7 2,2-Dichloropropane 0.25 Not detected ug/L EPA5030/62418260 4111/13 ACHANDLER 107-06-2 1,2-Dichloroethane 0.25 Not detected ug/L EPA5030/62418260 4/11113 ACHANDLER 71-55-6 1,1,1-Trichloroethane 0.25 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 563-SM 1,1-Dichloropropene 0.25 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 71-43-2 Benzene 0.25 Net detected ugli. EPA50301624/8260 4/11/13 ACHANDLER 74-95-3 Dibromomethane 1.0 Not detected ug/L EPAS030/624/8260 4/11/13 ACHANDLER 78-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPAS030/624IB260 M11113 ACHANDLER 79-01-6 Trichloroethene 0.25 Not detected ug/L EPA5030/62418260 4/11113 ACHANDLER 75-27-4 Bromodichloromethane 0.25 Not detected ug/L EPA5030162418260 4111/13 ACHANDLER 10061-01-5 cis-1,3-Dichloropropene 0.25 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 10061-02-6 trans-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 4/11113 i ACHANDLER 79-00-5 1, 1,2-Trichloroethane 0.25 Not detected ug/L EPA50301624/8260 4/11/131 ACHANDLER 108-88-3 Toluene 0.25 Not detected ug/L EPAS030162416260 4111113 ACHANDLER Laboratory Secllon» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Fora deowdesWpoon oftee quahfiereWes,ererl0tw.&s.m!!.nKsa.mLw-e/^'�/^=/,1x^^en Page 1 of 2 NC rD'KQ- La6onitory Section P,?sults Location ID: 1P69COATSMW2 Sample ID: AB94211 Collect Date: 04/0912013 Collect Time:: 09:22 VOL ResulU Method Analysis CAS # Analvte Name Units Validated by qualifier Reference Date 142-28-9 1,3-Dichloropropane 0.25 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 124-48-1 Dibromochloromethane 0.50 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 106-93-4 (EDB)1,2-Dibromoethane 0.50 Not detected ug/L EPA5030162418260 4/11113 ACHANDLER 127-18-4 Tetrachloroethene 0.25 Not detected ug/L EPA5030/624/8260 4111/13 ACHANDLER 108-90.7 Chlorobenzene 0.25 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 100-41.4;,- , Ethylbenzene 0.26 Not detected ug/L EPA5030182418260 4111113 ACHANDLER 75-25-2 Bromoform 1.0 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 108-38-3 m,p-Xylene 1.0 Not detected ug/L EPA50301624/8260 4111/13 ACHANDLER 100-42-5 Styrene 0.25 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 79-34-5 1,1,2,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 630-20-6 1,1,1,2-Tetrachloroelhane 0.25 Not detected ug/L EPAS0301624/8260 4/11/13 ACHANDLER 9547-6 o-Xylene 0.25 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 96-184 1,2,3-Trichloropropane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 98-82-8 Isopropylbenzene 0.25 Not detected ug/L EPAS030/624/8260 4/11113 ACHANDLER 108-86-1 Bromobenzene 0.25 Not detected uglL EPA50301624/8260 4/11/13 ACHANDLER 103-65-1 n-Propylbenzene 0.25 Not detected ug/L EPAS030/62418260 4/11/13 ACHANDLER 95-49.8 2-Chlorotoluene 0.25 Not detected ug/L EPA50301624/8260 4111/13 ACHANDLER 106-43-4 4-Chlorotoluene 0.25 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 108-67-8 1,3,5-Trimethylbenzene 0.25 Not detected ug/L EPAS0301624/8260 4111113 ACHANDLER 98-06-6 tert-Butylbenzene 0.25 Not detected ug/L EPAS0301624/8260 4111113 ACHANDLER 95-63-6 1,2,4-Trmethylbenzene 0.25 Not detected ug1L EPA50301624/8260 4/11113 ACHANDLER 135-98-8 sec-Butylbenzene 0.25 Not detected ug/L EPAS0301624/8260 4111113 ACHANDLER 541-73.1 m-Dichlorobenzene (1,3) 0.25 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 106-46.7 p-Dichlorobenzene (1,4) 0.25 Not detected ug/L EPA5030/62418260 4111113 ACHANDLER 95-50.1 o-Dichlorobenzene (1,2) 0.25 Not detected ug/L EPA5030162418260 4111/13 ACHANDLER 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 104-51-8 n-Butylbenzene 0.25 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 96-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 120-82-1 1,2,4-Tdchlorobenzene 0.50 Not detected ug/L EPA6030162418260 4111113 ACHANDLER 91-20.3 Naphthalene 0.50 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 87-68-3 Hexachlorobutadiene 0.50 Not detected ug/L EPA5030162418260 4111/13 ACHANDLER 87-61-6 1,2,3-Trichlorobenzene 1.0 Not detected ug/L EPA50301624/8260 4/11113 ACHANDLER Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Far a eHalleE aesmpeon a/lea qualifier eoaea re(erto Il@.IL.Para.to!�.rse.ns/s3AGeMnDLnb99pv�t�iW n.0 w,+o 5y;i-n1p:u .n �.e.�,a.r..Y.nnz+rranb'.mgya Page 2 of 2 GROUNDWATER FIELD/LAB FORM Location code: 1 P59CoatsMW2 County: McDowell Quad Serial Water (Ground Water) ❑ Soil ❑ Other ❑ Chain of Custody Department of Environment and Natural Resources , DIVISION OF WATER QUALITY -GROUNDWATER SECTION SAMPLE PRIORITY Do Routine Lab Number ❑ Emergency Date Received Time: Rec'd By: From:Bus, Courier, Hand Del., Other: Report To: ARO, FRO, MRO, RRO, WaRO, WiRO, Data Entry By: Ck:_ WSRO, Kinston FO, Fed. Trust, Central Off., Other: Date Reported: Shipped by: Bus, Courier, Hand Del., Other: Purpose: Collector(s): Brett Laverty Date: 4/9/2013 Time: 9:22 AM Baseline, Complaint, Compliance. LUST, Pesticide Study, Federal Trust, Other: FIELD ANALYSES Owner: Coats American—`irdeone) pH 4ob Spec. Cond.94 at 250C Location or Site: 630 American Thread Road Marion, NC Temp.lo eC Odor Description of sampling point: Monitoring Well MW2 Appearance DO, mg/L ORP, mV Sampling Method: External Well Pump Sample Interval Field Analysis By: Remarks LABORATORY ANALYSES (Pumping time, air temp., etc.) BOD 310 mgfL COD High 340 mg/L COD Low 335 mg/L Coliform: MF Feca131616 /100ml Coliform: MF Total 31504 /100ml TOC 680 mg/L Turbidity 76 NTU Residue, Total Suspended 530 mg/L DOC pH 403 units Alkalinity to pH 4.5410 mg/L Alkalinity to pH 8.3415 mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L Carbon dioxide 405 mg/L Chloride 940 mg/L Chromium: Hex 1032 ug/L Color: True 80 Cu Cyanide 720 mg/L Lab Diss. Solids 70300 mg/L Ag-Silver46566 u /L Or anochlonne Pesticides Fluoride 951 mg/L AI -Aluminum 46557 u /L Or ano hos horns Pesticides Hardness: Total 900 mg/L As -Arsenic 46551 u /L Nitrogen Pesticides Hardness (non-carb) 902 mg/L Ba-Barium 46558 u /L Acid Herbicides Phenols 32730 ug/I Ca -Calcium 46552 m /L PCBs Spec Cord. 95 pMhos/cm Cd-Cadmium 46559 u /L Sulfate 945 mg/L Cr-Chromium 46559 u /L MBAs Sulfide 745 mg/L I Cu-Copper 46562 u /L Boron Fe -Iron 46563 u /L Semivolable Organics Oil and Grease mg/L Hg-Mercury 71900 u /L TPH-Diesel Range K-Potassium 46555 m /L Mg -Magnesium 46554 m /L PO4 as P Mn-Manganese 46565 u /L X Volatile Organics VOA bottle NH3 as N 610 mg/L Na-Sodium 46556 m /L TPH-Gasoline Range TKN as N 625 mg/L Ni-Nickel u /L TPH-BTEX Gasoline Range NO2+ NO3 as N 630 mg/L Pb-Lead 46564 u /L P: Total as P 665 mg/L Se -Selenium u /L Nitrate (NO3 as N) 620 mg/L Zn-Zinc46567 u /L Nitrite (NOs as N) 615 mg/L LAB USE ONLY Temperature on arrival (eC): NH4-ammonium Silica GW-54 REV. 7/03 For Dissolved Analysis -submit filtered sample and wnte'DIS' in block. _ _ - County: MCDOWELL wATF9 Sample ID: AB94212 River Basin OF OG PO Number # 13GO266 0 Report To AROAP H Date Received: 04/11/2013 -1 Time Received: 08:00 Collector. 8 LAVERTY Y Lelrxorks LogInID HMORGAN Region: ARO Final Report Date: 5/9/13 Sample Matrix: GROUNDWATER Final Report Report PfinlD Loc.Type: MONITORING WELL � g 0 E C E Y '17 ap��+ E RECEIVED Emergency Yes/No VisitlD CDC Yes/No Loc. Descr.: COATS AERICAN 630 AMERICAN THREAD ROAD MARION. N JUL 17 2013 Location 10: 1P69COATSMW10 I Collect Date: 0410912013 1 Collect Time: 09:3 Sample Depth I IC t V Q l i-1 If this report is labeled preliminary report the results have not been validated. Do not use for Regulatory pure �rifer Protection CAS Analyte Name # ResulU P L Units Method Analysis Validated by Qualifier Reference Date LAB Sample temperature at receipt by lab 2.0 C 4111113 HMORGAN MET 744047-3 Cr- Dissolved Chromium by ICPMS 10 IOU ug/L EPA200.8 4/18113 ESTAFFORDI 7440-224 Ag by ICPMS 1.0 1.0 U ug/L EPA 200.8 4/18/13 ESTAFFORDI 7429-9D-5 Al by ICP 50 50 U ug/L EPA 200.7 4116113 ESTAFFORDI 7440-38-2 AS by ICPMS 2.0 2.0 U ug/L EPA200.8 4118113 ESTAFFORDI 7429-90-5 B by ICP 50 84 ug/L EPA 200.7 4/18113 ESTAFFORDI 7440-38-3 Ba by ICP 10 IOU ug/L EPA 200.7 4/15/13 ESTAFFORDI 7440-70-2 Ca by ICP 0.10 0.46 mg/L EPA 200.7 4115/13 ESTAFFORD1 7440-43-9 Cd by ICPMS 0.50 0.50 U ug/L EPA 200.6 4118113 ESTAFFORD1 7440-50-8 Cu by ICPMS 2.0 2.6 ug/L EPA200.8 4118/13 ESTAFFORDI 7439-89-6 Fe by ICP 50 50 U ug/L EPA200.7 4116/13 ESTAFFORDI 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA245.1 4/17113 ESTAFFORD1 7440-09-7 K by ICP 0.10 0.36 mg/L EPA 200.7 4115/13 ESTAFFORDI 7439-954 Mg by ICP 0.10 0.20 mg/L EPA200.7 4115113 ESTAFFORDI 7439-96-5 Mn by ICP 10 IOU ug/L EPA 200.7 4116/13 ESTAFFORDI 7440-23-5 Na by ICP 0.10 58 mg/L EPA 200.7 4/15113 ESTAFFORDI 7440-02-0 Ni by ICPMS 2.0 2.0 U ug/L EPA 200.8 4/18/13 ESTAFFORDI 7439-92-1 Pb by ICPMS 2.0 2.0 U ug/L EPA 200.8 4118/13 ESTAFFORDI 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA 200.8 4/18113 ESTAFFORD1 7440-28-0 Thallium (TI) ICPMS 2.0 2.0 U J2 ug/L EPA 200.8 4118113 ESTAFFORD1 7440-56-6 Zn by ICPMS 10 IOU ug/L EPA 200.8 4/1a/13 ESTAFFORD1 VOL 7429-90-5 Volatile Organics in liquid TITLE ug/L EPA5030/624/8260 4111113 ACHANDLER 75-71-8 Dichlorodifluoromelhane 1.0 Not detected ug/L EPA50301624/8260 4111/13 ACHANDLER 74-87-3 Chloromethane 1.0 Not detected ug/L EPA5030/62418260 4/11113 ACHANDLER 75-014 Vinyl Chloride 0.50 Not detected ug/L EPA5030162418260 4/11/13 ACHANDLER 74-83-9 Bromomethane 1.0 Not detected ug/L EPA5030/62418260 4/11/13 ACHANDLER 75-OD-3 Chloroethane 0.50 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 75-694 Trichlorofluoromethane 0.50 Not detected ug/L EPA5030/624/8260 4111113 ACHANDLER 75-354 1,1-Dichloroethene 0.25 Not detected ug/L EPA50301624/8260 4/11113 ACHANDLER Laboratory Section>> 1623 Mali Sorvice Center, Raleigh, NC 27699-1623 (919) 733.3908 For adetmteddescpwn orree9va5fercodes rererto p,�¢7(¢yasLorfiee.°^Mw.annn•.nn,n n.°�.v,.n Ma<�me w.n/.M.p/.t nly/y-�svti Page 1 of 3 NC 0$WQ, La6oratorySection tRSsulu Locaflon ID: IP69COATSMW10 Sample ID: AB94212 Collect Date: 0410912013 Collect Time:: 09:33 VOL CAS # 75-09-2 Analvte Name Methylene Chloride P(�L 10 Result/ Qualifier Not detected Units ug/L Method Reference EPA5030162418260 Analysis Date 4111/13 Validated by ACHANDLER 156-60-5 trans-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030162418260 4/11/13 ACHANDLER 1634-044 Methyl Teri -Butyl Ether 0.25 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 75-34-3 1,1-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 4111113 ACHANDLER 156-59-2 CIS-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030162418260 4/11113 ACHANDLER 74-97-5 1 18romochlor6riiethane 0.25 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 67-66-3 Chloroform 0.25 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 594-20-7 2,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 4111113 ACHANDLER 107-06-2 1,2-Dichloroethane 0.25 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 71-55-6 1, 1, 1-Trichloroethane 0.25 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 563-58-6 1,1-Dichloropropane 0.25 Not detected ug/L EPA5030/62418260 4111/13 ACHANDLER 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L EPAS030/624/8260 4/11/13 ACHANDLER 7143.2 Benzene 0.25 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 74-95-3 Dibromomelhane 1.0 Not detected ug/L EPA5030/624/8260 4111/13 ACHANDLER 78-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPA50301624/8260 4/11113 ACHANDLER 79-01-6 Trichloroethene 0.25 Not detected ug/L EPAS0301624/8260 4/11/13 ACHANDLER 75-274 Bromodichloromethane 0.25 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 10061-01-5 Cis-1,3-Dlchloropropene 0.25 Not detected ug/L EPA5030/62418260 4111113 ACHANDLER 10061-02-8 trans-1,3-Dichloropropene 0.25 Not detected ug/L EPAS030/62418260 4/11113 ACHANDLER 79-00-5 1,1,2-Trichloroethane 0.25 Not detected ug/L EPA5030/62418260 4/11/13 ACHANDLER 108-88-3 Toluene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 142-28-9 1,3-Dichloropropane 0.25 Not detected ug/L EPAS030/624/8260 4111113 ACHANDLER 12448-1 Dibromochloromethane 0.50 Not detected ug/L EPA5030/62418260 4111113 ACHANDLER 106-934 (EDB)1,2-Dibromoethane 0.50 Not detected ug/L EPA5030/62418260 4111/13 ACHANDLER 127-184 Tetrachloroethene 0.25 Not detected ug/L EPAS030/624/8260 4/11/13 ACHANDLER 108-90.7 Chlorobenzene 0.25 Not detected ug/L EPA5030/824/8260 4/11113 ACHANDLER 100-41-4 Ethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4111/13 ACHANDLER 75-25-2 Bromoform 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 108-38-3 m,p-Xylene 1.0 Not detected uglL EPA5030/624/8260 4111113 ACHANDLER 100.42-5 Styrene 0.25 Not detected ug/L EPA5030162418260 4111/13 ACHANDLER 79-34-5 1,1,2,2-Tetrachloroelhane 0.25 Not detected ug/L EPA5030/62418260 4111113 ACHANDLER 630-20-6 1,1, 1,2-Tetrachloroelhane 0.25 Not detected ug/L EPA5030/62418260 4/11/13 ACHANDLER 95-47-6 o-Xylene 0.25 Not detected ug/L EPA5030/62418260 4/11/13 ACHANDLER 96-18-4 1,2,3-Trichloropropane 0.25 Not detected ug/L EPA5030/624/8260 4111/13 ACHANDLER 98-82-8 Isopropylbenzene 0.25 Not detected ug/L EPA5030162418260 4/11/13 ACHANDLER 108-86-1 Bromobenzene 0.25 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 103-65-1 n-Propylbenzene 0.25 Not detected ug/L EPA503D/624/8260 4111113 ACHANDLER 95-49-8 2-Chlorotoluene 0.25 Not detected ug/L EPA50301624/8260 4/11113 ACHANDLER 106-43-4 4-Chlorotoluene 0.25 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 109-67.8 1,3,5-Trimethylbenzene 0.25 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 98.06-6 tert-Butylbenzene 0.26 Not detected ug/L EPA5030/62418260 4111/13 ACHANDLER 95-63-6 1,2,4-Trimethylbenzene 0.25 Not detected ug/L EPA5030/62418260 4111113 ACHANDLER Laboratory Section>> 1623 Mall Service Center, Raleigh, NC 27699.1623 (919) 733-3908 Fore Celalk44esulptbn of lea 9uafifiar¢oEea reler to dz//. amrrW!Ksetsu[niDLwlUfP4J�[2B�n:t:!�`tam.�n..cee-,mpl[p¢is!,¢cllmLca✓-�xfhL•iMe¢4a.M-bQ �•+'� Page 2 of 3 1i Location ID: • 1P69C0ATSMW10 NC/DWIQ La6oratorySectiouWjv=ftr Sample ID: AB94212 Collect Date: 04/09/2013 Collect Time:: 091-33 j VOL CAS # 135-98-8 AnalVte Name sec-Butylbenzene PQL 0.25 Result/ Qualifier Not detected Units ug/L Method Reference EPA5030/624/8260 Analysis Date 4111/13 I Validated by ACHANDLER (ACHANDLER 541-73-1 m-Dichlorobenzene (1,3) 0.25 Not detected ug/L EPA50301624/8260 4111/13 106-46-7 p-Dichlorobenzene (1,4) 0.25 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 95-5(1-1 o-Dichlorobenzene (1,2) 0.25 Not detected ug/L EPA5030162418260 4/11113 (ACHANDLER 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA50301624/8260 4111113 (ACHANDLER 104-51-8 n-Butylbenzene 0.25 Not detected ug/L EPA5030/62418260 4111113 (ACHANDLER 96-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA5030/624/8260 4111113 (ACHANDLER 19rLazd i o n n cn un/L EPA5030/62418260 4111113 (ACHANDLER 91-20-3 Naphthalene 0.50 Not detected ug/L EPA5030/624/8260 4111113 (ACHANDLER 87-68-3 Hexachlorobutadiene 0.50 Not detected ug/L EPA5030/62418260 4/11113 I ACHANDLER 87-61-6 1,2,3-Trichlorobenzene 1.0 Not detected ug/L EPA5030/62418260 4/11113 I ACHANDLER IMET:Thallium-J2-estimated-QC Sample Comments failure due to Cl inter. from 3030C digestion. Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699.1623 (919) 733-3908 Fore delelteddeecdption.1ttiequalifiercoft. refer to nJp7(,pgrstl,et4.m! /+-/+„+/�.=rnpgmggSn;vanw, nee ner cmpSJe:fLn01 •nn. are,ws9/Pg�a4G:a-�L�w1.�Atv�L> Page 3 of 3 County: MCDOWELL River Basin Report To AROAP Collector. B LAVERTY Region: ARC, Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Emergency Yes/No VsitlD COC Yes/No OF NNgpF9 Sample ID: AB942471 O? PG PO Number# ARO OJ Date Received: 04110120131 O T Time Received: 08:30 Labworks LoginlD KJIMISON Final Report Date: 4/22/13 1� Final Report Report Print Date: 05/16/2013 Loc. Descr.: Location ID: 1P69COATSMW10 Collect Date: 0410912013 Collect Time: 09:33 Sample Depth If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. CAS # Result/ Method Analysis Analyte Name PQL Units 'Validated by Qualifier Reference Date Others Sample temperature at receipt by lab 1.6 °C 4110113 RBYRD Turbidity 1 1 U NTU APHA2130B-20th 4/10M3 CGREEN Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For adetalled desorption Of the qualifier codes refer to h-,Vw rcem.mMw/wy�,e,c.n�,nenn.a (r,n�Mh.:nnmo Page 1 of 1 GROUNDWATER FIELD/LAB FORM Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION Location code: 1P59CoatsMW10 SAMPLE TYPE SAMPLE PRIORITY County: McDowell �J Water (Ground Water) DO Routine Lab Number Quad No Serial No. ❑ Soil ❑ Emergency 2 Date Received Time: Lat. Long. ❑ Other Redd By: From:Bus, Courier, Hand Del., ❑ Chain of Custody Other: Report To: ARO, FRO, MRO, RRO, WaRO, WiRO, Data Entry By: Ck: WSRO, Kinston FO, Fed. Trust, Central Off., Other: Date Reported: Shipped by: Bus, Courier, Hand Del., Other: Purpose: Collector(s): Brett Laverty Date: 4/9/2013 Time: 9:33 AM Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other: FIELD ANALYSES Owner: Coats American jurcle one) pH 400 Spec. Cond.94 at 250C Location or Site: 630 American Thread Road Marion, NC Temp.lo eC Odor Description of sampling point: Monitoring Well MW10 Appearance DO, mg/L ORP, mV Sampling Method: External Well Pump Sample Interval Field Analysis By: Remarks P f t t time LABORATORY ANALYSES umping air emp, a c. Boo 310 mg/L Diss. Solids 70300 mg/L Ag-Silver46566 u /L Or anochlorine Pesticides COD High 340 mg/L Fluoride 951 mglL AI -Aluminum 46557 u /L Organophosphows Pesticides COD Low 335 mg/L Hardness: Total 900 mg/L X As -Arsenic 46551 u /L Nitro en Pesticides Colifonn: MF Fecal 31616 /100ml Hardness (non-carb) 902 mg/L Ba-Barium 46558 u /L Arad Herbicides Colifomr. MF Total 31504 /100MI Phenols 32730 ugn Ca -Calcium 46552 m /L PCBs TOC 680 mg1L Specific Cord. 95 pMhos/cm Cd-Cadmium 46559 u /L Turbidity 76 NTU Sulfate 945 mg/L X Cr-Chromium 46559 u /L MBAS Residue, Total Suspended 530 mg/L Sulfide 745 mg1L X Cu-Copper 46562 u /L X Boron DOC X I Fe -Iron 46563 u /L Semivolatile Or anics Oil and Grease mg/L X Hg-Mercury71900 u /L TPH-Diesel Range pH 403 units X K-Potassium 46555 m /L Alkalinity to pH 4.5410 mg1L X Mg -Magnesium 46554 m /L Alkalinity to pH 8.3 415 mg/L PO4 as P X Mn-Manganese 46565 u /L X Volatile Organics(VOA bottle Carbonate 445 int NH3 as N 610 mg/L X Na-Sodium 46556 moll. TPH-Gasoline Range Bicarbonate 440 mg1L TKN as N 625 mg1L NkNickel u /L TPH-BTEX Gasoline Range Carbon dioxide 405 mg/L NO3+ NO3 as N 630 mg1L XPb-Lead 46564 u /L Chloride 940 mg/L P: Total as P 655 mg/L 1 Se -Selenium u /L Chromium: Hex 1032 ug/L Nitrate (1,103as N) 620 mg/L Zn-Zinc 46567 u /L Color: True 60 CU Nitrite (NO3 as N) 615 mg1L x I Please add thallium LAB USE ONLY Temperature on arrival(eC): Cyanide 720 mg/L NH4-ammonium I Silica Lab GW-54 REV. 7/03 — For Dissolved Analysis -submit filtered sample and write -DIS' in block. -- - GROUNDWATER FIELD/LAB FORM Location code:1 P59CoatsMW10 County: McDowell Quad No Serial No. Lat. Long. X Water (Ground Water) ❑ Soil ❑ Other ❑ Chain of Custody Report To: ARO, FRO, MRO, RRO, WaRO, WiRO, I WSRO, Kinston FO, Fed. Trust, Central Off., Other: Shipped by: Bus, Courier, Hand Del., Other: Collector(s): Brett Laverty Date: 4/9/2013 FIELD ANALYSES Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION SAMPLE PRIORITY Routine Lab Number ❑ Emergency 2 Date Received Time: Rec'd By: From:Bus, Courier, Hand Del., Other: Data Entry By: Ck: Date Reported: Purpose: Time: 9:33 AM Baseline, Complaint, Compliance LUST, Pesticide Study, Federal Trust, Other: pH 400 Spec. Cond.94 at 25eC Terri eC Odor mg/L ORP, mV Lab ameone) Diss. Solids 70300 ri Ag-Silver46566 u /L Organochlonne Pesticides Fluoride 951 mg/L AI -Aluminum 46557 u /L Or ano hos horns Pesticides Hardness: Total 900 mg/L As -Arsenic 46551 u /L Nitrogen Pesticides Hardness (non-carb) 902 ri Ba-Barium 46558 u /L Acid Herbicides Phenols 32730 ug/I Ca -Calcium 46552 m /L PCBs Specific Cord. 95 pMhos/cm Cd-Cadmium 46559 u /L Sulfate 945 mg/L Cr-Chromium 46559 u /L MBAS Sulfide 745 mg/L Cu-Copper46562 u /L I Boron Fe -Iron 46563 u /L Semlvolatile Organics Oil and Grease mg/L Hg-Mercury71900 u /L TPH-Diesel Range K-Potassium 46556 m /L Mg -Magnesium 46554 ri PO4 as P Mn-Manganese 46566 u /L Volatile Organics(VOA bottle NH3 as N 610 mg/L Na-Sodium 46556 ri TPH-Gasoline Range TKN as N 625 mg/L Ni-Nickel u /L TPH-BTEX Gasoline Range NO2 + NO3 as N 630 mg/L Pb-Lead 46564 u /L P: Total as P 665 ri Se -Selenium u /L Nitrate (NO3 as N) 620 mg/L Zn-Zinc46567 u /L Nitrite (NO2 as N) 615 mg/L LAB USE ONLY Temperature on arrival (°C): NH4 -ammonium Silica GW-54 REV. 7103 For Dissolved Analysis -submit filtered sample and write'DIS' in block. County: MCDOWELL wgTE9 Sample ID: AB94213 River Basin OF Oa OG PO Number# 13G0267 Report To AROAP y Date Received: 04111/2013 Time Received: 08:00 Collector. B LAVERTY Latrworks LoginlD HMORGAN Region: ARO Final Report Dal 9113 Sample Matrix: GROUNDWATER Final Report Report Print Dat: 1661 2013 Loc. Type: MONITORING WELL R.A5/16/FG` 11R•'*r pV�ED Emergency Yes/No VisitlD 171 CDC Yes/No Loc. Daacr.: COATS AMERICAN 630 AMERICAN THREAD ROAD MARION. NO JUL 17 2013 1 Location ID: IP59COATSMW11R Collect Date: 0410912013 Collect Time: 09:46 AS1,690Nr�pyl}.,;,.,��„-ram If this report is labeled preliminary report, the results have not been validated. Do not use for CAS # Analvte Name PQI Result/Units Method Analysis Validated by Qualifier Reference Date LAB Sample temperature at receipt by lab 2.0 C 4111113 HMORGAN 7440A7-3 Cr- Dissolved Chromium by ICPMS 10 ICU ug/L EPA 200.8 4118/13 ESTAFFORD1 7440-22.4 Ag by ICPMS 1.0 1.0 U ug/L EPA200.8 4/18113 ESTAFFORDI 7429-90-5 Al by ICP 50 50 U ug/L EPA 200.7 4/16/13 ESTAFFORDI 7440-38-2 As by ICPMS 2.0 2.0 U ugfL EPA 200.8 4/18/13 ESTAFFORDI 7429-SD-5 B by ICP 50 50 U ug/L EPA200.7 4/18113 ESTAFFORD1 7440-38-3 Be by ICP 10 53 ugfL EPA 200.7 4115113 ESTAFFORD1 7440-70-2 Ca by ICP 0.10 47 mg/L EPA 200.7 4115113 ESTAFFORDI 7440-43-9 Cd by ICPMS 0.50 0.50 U ug/L EPA 200.8 41la/13 ESTAFFORD1 7440-50-8 Cu by ICPMS 2.0 2.0 ugfL EPA 200.8 4/18/13 ESTAFFORD1 7439-BM Fe by ICP 50 50 U ugfL EPA 200.7 4/16/13 ESTAFFORD1 7439-97-6 Hg 245.1 0.2 0.20 U ugfL EPA 245.1 4117113 ESTAFFORDI 7440-09-7 Kby ICP 0.10 2.7 mg/L EPA200.7 4115113 ESTAFFORDI 7439-95A Mg by ICP 0.10 19 mg/L EPA 200.7 4/15/13 ESTAFFORDI 7439-96-5 Mn by ICP 10 10 U ug/L EPA 200.7 4116/13 ESTAFFORDI 7440-23-5 Na by ICP 0.10 17 mg/L EPA 200.7 4/15113 ESTAFFORDI 7440-02-0 NI by ICPMS 2.0 2.0 U ugfL EPA200.8 4/18/13 ESTAFFORDI 7439-92-1 Pb by ICPMS 2.0 2.0 U ugfL EPA 200.8 4/18/13 ESTAFFORDI 778249-2 Se by ICPMS 5.0 5.0 U ug/L EPA 200.8 4/18/13 ESTAFFORDI 7440-28-0 Thallium (TI) ICPMS 2.0 2.0 U J2 ug/L EPA 200.8 4/18/13 ESTAFFORDI 7440-66-6 Zn by ICPMS 10 14 ugfL EPA 200.8 4118113 ESTAFFORD1 VOL 7429-90-5 Volatile Organics in liquid _TITLE_ ugfL EPA5030162418260 4111/13 ACHANDLER 75-71-8 Dichlorodifluoromelhane 1.0 Not detected ug/L EPAS030/624/8260 4111113 ACHANDLER 74-87-3 Chloromethane 1.0 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 75-01-4 Vinyl Chloride 0.50 Not detected ug/L EPA5030/62418260 4111113 ACHANDLER 74-83-9 Bromomethane 1.0 Not detected ug/L EPAS0301624/8260 4/11113 ACHANDLER 75-00-3 Chlorcethane 0.50 Not detected ug/L EPA5030/62418260 4111113 ACHANDLER 75-69-4 Trichlorofluoromelhane 0.50 Not detected ugfL EPA5030/624/8260 4111113 ACHANDLER 75-35-4 1,1-Dichloroethene 0.25 Not detected ug/L EPA5030162418260 4/11113 ACHANDLER Laboratory Section 1623 Mall service Center, Raleigh, NO 27699-1623 (919) 733-3908 Foraaeraileddesoprion or the quarorcooes reler to Il@:/LB.Af1d a5G.MlR]JSSDL t4,b/.nsn4a, •dmsY �• ^- Page 1 of 3 WC(Z)IKQ La6orntorySection I�(psalts , . Location to: IP59COATSMWIIR Sample ID: AB94213 Collect Date: 0410912013 Collect Time:: 09:46 VOL CAS # 75-09.2 Analvte Name Methylene Chloride P(�L, 10 ResulU Qualifier Net detected Units ug/L Method Reference EPA5030162416260 Analysis Date 4111 113 Validated by ACHANDLER 156-60-5 trans-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/62418260 4111/13 ACHANDLER 1634-044 Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPA5030/62418260 4/11/13 ACHANDLER 75-34-3 1,1-Dichloroethane 0.25 Not detected ug/L EPAS030/62418260 4/11/13 ACHANDLER 156-59-2 cis-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030162418260 4/11/13 ACHANDLER 74-97-5 Brof ochloi0methane 0.25 Net detected ug1L EPA50301624/8260 4111113 ACHANDLER 67.6E3 Chloroform 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 594-20-7 2,2-Dichloropropane 0.25 Not detected ug/L EPA5030162418260 4/11/13 ACHANDLER 107-06-2 1,2-Dichloroethane 0.25 Not detected ug/L EPAS030/624/8260 4111113 ACHANDLER 71-55-6 1,1,1-Trichloroethane 0.25 Not detected ug/L EPAS0301624/8260 4/11113 ACHANDLER 563-58-6 1,1-Dichloropropene 0.25 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L EPA5030162416260 4111/13 ACHANDLER 71-43-2 Benzene 0.25 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 74-95-3 Dlbromomethane 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 78-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 79-01-6 Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11A3 ACHANDLER 75-274 Bromodichloromethane 0.25 Not detected ug/L EPAS030/624/8260 4111113 ACHANDLER 10061-01-5 Cis-1,3-Dichloropropene 0.25 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 10061-02-6 trans-1,3-Dichloropropene 0.25 Not detected ug(L EPA50301624/8260 4111113 ACHANDLER 79-00.5 1,1,2-Trichloroethane 0.25 Not detected ug/L EPA5030162418260 4/11113 ACHANDLER 108-88.3 Toluene 0.25 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 142-28-9 1,3-Dichloropropane 0.25 Not detected ug/L EPA5030162418260 4/11/13 ACHANDLER 124-4a-1 Dibromochloromethane 0.50 Not detected ug/L EPA5030162418260 4/11113 ACHANDLER 106-934 (EDB)1,2-Dibromoethane 0.50 Not detected ug/L EPA5030162418260 4/11/13 ACHANDLER 127-184 Tetrachloroethene 0.25 Not detected ug/L EPAS030/62418260 4111113 ACHANDLER 1OB-90-7 Chlorobenzene 0.25 Not detected ug/L EPA5030/62418260 4111113 ACHANDLER 100.41-4 Ethylbenzene 0.25 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 75-25-2 Bromoform 1.0 Not detected ug/L EPA5030/62418260 4111113 ACHANDLER 108-38-3 m,p-Xylene 1.0 Not detected ug/L EPA5030/62418260 4111113 ACHANDLER 100-42-5 Styrene 0.25 Not detected ug/L EPA5030/624/8260 4111113 ACHANDLER 79-34-5 1,1,2,2-Tetrachloroethane 0.25 Not detected ug/L EPA50301624/8260 4/11113 ACHANDLER 630-20-6 1,1,1,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/62418260 4/11/13 ACHANDLER 95-47-6 o-Xylene 0.25 Not detected ug/L EPA5030/624/6260 4/11/13 ACHANDLER 96-18-4 1,2,3-Trichloropropane 0.25 Not detected ug/L EPA5030/624/6260 4/11/13 ACHANDLER 98-82-B Isopropylbenzene 0.25 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 10MB-1 Bromobenzene 0.25 Not detected ug/L EPA5030/62418260 4/11/13 ACHANDLER 103-65-1 n-Propylbenzene 0.25 Not detected ug/L EPA5030162418260 4/11113 ACHANDLER 95-49-8 2-Chlorotoluene 0.25 Not detected ug/L EPA5030162418260 4/11113 ACHANDLER 106-43-4 4-Chlorotoluene 0.25 Net detected ug/L EPA5030/62418260 4111/13 ACHANDLER 108-67-8 1,3,5-Trimethylbenzene 0.25 Not detected ug/L EPA50301624/8260 4111/13 ACHANDLER 98-06-6 tert-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4111/13 ACHANDLER 95-63-5 1,2,4-Trimethylbenzene 0.25 Not detected ug/L EPA5030/62418260 4/11113 ACHANDLER Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Fore delaned deeorreton of the 9ua0fiercodes refer to 6N.;(L.2o!;.iLL194t59u1bxPlwM.ip/g.��unr-ne,::uo.y}ye nor( I�r.Mnuo+n e.L..eMarnh annmhrcnn,�rc> Page 2 of 3 NC 014,Q La6oratory Seaton �ksurts Location ID: 11`69COATSMW11R Sample ID: AB94213 Collect Date: 0410912013 Collect Time:: 09:46 CAS # Analyte Name 135-98-8 sec-Butylbenzene PQL Result/ Qualifier Units 0.25 Not detected ug/L Method Analysis Reference Date EPA5030162418260 4111/13 541-73-1 m-Dichlorobenzene (1,3) 0.25 Not detected ug/L EPA5030/624/8260 4111113 ACHANDLER 106-46-7 p-Dichlorobenzene (1,4) 0.25 Not detected ug/L EPA5030/624/8260 4111/13 ACHANDLER 95-50-1 o-Dichlorobenzene (1,2) 0.25 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 104-51-8 n-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 96-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 120-82-1 1,2,4-Trichlorobenzene 0.50 Not detected ug(L EPA5030/62418260 4/11113 ACHANDLER 91-20-3 Naphthalene 0.50 Not detected ug/L EPA5030/624/6260 4/11/13 ACHANDLER 87-68-3 Hexachlorobutadiene 0.50 Not detected uglL EPA5030/624/8260 4111/13 ACHANDLER 87-61-6 1,2,3-Trichlorobenzene 1.0 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER Sample Comments IMET:Thallium-J2-estimated-QC failure due to Cl Inter. from 3030C digestion. Laboratory Section>> 1623 Mall Service Canter, Raleigh, NC 27699-1623 (919) 733.3908 For a delalled descretlon of the Quallfler wiles refer to 9t y dipa�.areLwx➢b.NJn�/a m�nommge,r,,. ev II, CW-, �booavm��me Page 3 of 3 County: MCDOWELL River Basin Report To AROAP Collector. B LAVERTY Region: ARO Sample Matrix: GROUNDWATER Loa Type: MONITORING WELL Emergency Yes/No COC Yes/No W ATF9 Sample ID: AB94248 OF O� OG PO Number# ARID �i Date Received: 04/1012013 O Y Time Received: 08:30 Laberorks LoginlD KJIMISON Final Report Date: 4/22113 Final Report Report Print Date: 1511112113 VIsitID Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD ROAD MARION, NC Location ID: 1P59COATSMWIIR I Collect Date: 0410912013 I Collect Time: 09:46 Sample Depth If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. I Resultl Method Analysis Validated CAS # Analvte Name P(�. L Units by ualifier Reference Date Others Sample temperature at receipt by lab 1.6 C 4110/13 RBYRD Turbidity 1 1.1 NTU APHA2130B-20th 4/10/13 CGREEN Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733.3908 For a detailed desuretbn of qualifier miles refer to Me//nee, nme+•an(asp[yrya •e°Tin nr_•. ee °n!na Page 1 of 1 GROUNDWATER FIELD/LAB FORM Location code: 1 P59CoatsMW11 R County: McDowell Quad Serial No. Long. Report To: ARO, FRO, MRO, RRO, WaRO, WiRO, WSRO, Kinston FO, Fed. Trust, Central Off., Other Shipped by: Bus, Courier, Hand Del., Other: Collector(s): Brett Laverty FIELD ANALYSES Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION 4 SAMPLE TYPE SAMPLE PRIORITY X Water (Ground Water) W Routine Lab Number ❑ Soil ❑ Emergency 3 Date Received Time: ❑ Other Rec'd By: From Courier, Hand Del., ❑ Chain of Custody Other: Data Entry By: Ck: Date Reported: Purpose: Date: 4/9/2013 Time: 9:46 AM Baseline, Complaint, Compliance LUST, Pesticide Study, Federal Trust, Other: Owner: Coats American tclrcle one) pH 400 Spec. Cond.94 at 250C Location or Site: 630 American Thread Road Marion, NC Terri aC Odor Description of sampling point: Monitoring Well MW11 R Appearance DO, mg/L ORP, mV Sampling Method: External Well Pump Sample Interval Field Analysis By I GRr)PATOPY BOD 310 mg/L COD High 340 ni COD Low 335 mg/L Colifonn: MF Feca131616 /100ml Colifonn: MF Total 31504 /100ml _ TOC 680 ni Turbidity 76 NTU Residue, Total Suspended 530 mg/L DOC pH 403 units Alkalinity to pH 4.5410 mg/L Alkalinity to pH 8.3 415 mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L Carbon dioxide 405 mg/L Chloride 940 mg/L Chromium: Hex 1032 ug/L Color: True 80 CU Cyanide 720 mg/L Lab (Pumping time, air temp., etc.) Diss. Solids 70300 mg/L AgSilver46566 u /L Or anochlorine Pesticides Fluoride 951 mg/L AI -Aluminum 46557 ug1l. Organophosphoms Pesticides Hardness: Total 900 mg/L X As -Arsenic 46551 u L Nitrogen Pesticides Hardness (non-carb) 902 mg/L Ba-Barium 46558 ug/L Acid Herbicides Phenols 32730 ugn Ca -Calcium 46552 mg/L PCBs Specific Cond. 95 pMhos/cm Cd-Cadmium 46559 u /L Sulfate 945 mg/L X Cr-Chromium 46559 u /L MBAs Sulfide 745 mg/L X Cu-Copper46562 u /L X Boron X Fe -Iron 46563 u /L I Semivolatile Or anics Oil and Grease mg/L X Hg-Mercury 71900 u /L TPH-Diesel Range X K-Potassium 46555 mg/L X Mg -Magnesium 46554 mg/L PO4 as P X Mn-Manganese 46565 u /L X Volatile Organics(VOA bottle NH, as N 610 mg/L X Na-Sodium 46556 mg/L TPH-Gasoline Range TKN as N 625 mg/L Ni-Nickel u /L TPH-BTEX Gasoline Range NOa+ NO3 as N 630 mg/L X Pt Lead 46564 u /L P: Total as P 665 mg I XSe-Selenium u /L Nitrate (NO3 as N) 620 mg/L X Zn-Zinc 46567 u /L Nitrite (NO2 as N) 615 mg/L Please add thallium LAB USE ONLY Temperature on arrival (aC): NH4-ammonium Silica GW-54 REV. 7103 For Dissolved Analysis -submit filtered sample and write'DIS' in block. GROUNDWATER FIELD/LAB FORM Location code: 1 P59CoatsMW11 R County: McDowell Quad Serial No. Long. SAMPLE TYPE N Water (Ground Water) ❑ Soil ❑ Other ❑ Chain of Custody Department of Environment and Natural Resources - DIVISION OF WATER QUALITY -GROUNDWATER SECTION SAMPLE PRIORITY N Routine Lab Number ❑ Emergency 3 Date Received Time: Rec'd By: From Courier, Hand Del., Other: Report To: ARO, FRO, MRO, RRO, WaRO, WiRO, Data Entry By: Ck: WSRO, Kinston FO, Fed. Trust, Central Off., Other: Date Reported: Shipped by: Bus, Courier, Hand Del., Other: Purpose: Collector(s): Brett Laverty Date: 4/912013 Time: 9:46 AM Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other: FIELD ANALYSES Owner: Coats American 7crzcle one) pH ,oft Spec. Cond.94 at 25eC Location or Site: 630 American Thread Road Marion, NC Temp.lo eC Odor Description of sampling paint: Monitoring Well MW11 R Appearance DO, mg/L ORP, mV Sampling Method: External Well Pump Sample Interval B DD 310 mg/L CODOD High 340 ni CLow 335 mg/L Coliform: MF Fecal 31616 /loom] Coffering: MF Total 31504 /loom[ TOC 680 mg/L Tumidity 76 NTU Residue, Total Suspended 530 mg/L DOG pH 403 units Alkalinity to pH 4.5410 mg/L Alkalinity to pH 8.3415 mg/L Carbonate 445 mg/L Bicarbonate 440 ni Carbon dioxide 405 mg/L Chloride 940 mg/L Chromium: Hex 1032 ug/L Color. True 80 CU Cyanide 720 mg/L Lab (Pumping time, air temp., etc) Diss. Solids 70300 mg/L Ag-Silver 46566 u /L Organochlodne Pesticides Fluoride 951 ni AI -Aluminum 46557 u /L Or ano hos horns Pesticides Hardness: Total 900 ni As -Arsenic 46551 u /L Nitrogen Pesticides Hardness (non-carb) 902 mg/L Ba-Barium 46558 u IL Acid Herbicides Phenols 32730 ugA Ca -Calcium 46552 m /L PCBs Specific Cord. 95 pMhos/cm Cal -Cadmium 46559 u /L Sulfate 945 mglL Cr-Chromium 46559 u /L MBAS Sulfide 745 mg/L Cu-Copper 46562 u /L Boron Fe -Iron 46563 u /L Sem]volat le 0 anics Oil and Grease mg/L Hg-Mercury 71900 u /L TPH-Diesel Range K-Potassium 46555 m IL Mg -Magnesium 46554 gt A Poo as P Mn-Manganese 46565 u /L Volatile Organics(VOA bottle NH3 as N 610 ni Na-Sodium 46556 m /L TPH-Gasoline Range TKN as N 625 ni Ni-Nickel u /L TPH-BTEX Gasoline Range NO2 + NO3 as N 630 ni Pb-Lead 46564 u /L P: Total as P 665 ni Se -Selenium u /L Nitrate (NO3 as N) 620 mg/L Zn-Zinc 46567 u /L Nitrite (NO2 as N) 615 1 LAB USE ONLY Temperature on arrival aG): NH4 - ammonium Silica GW-54 REV. 7103 For Dissolved Analysis -submit filtered sample and write'DIS' in block. County: MCDOWELL River Basin �F WATF9 Sample ID: AB94214 Q PO Number# 13GO268 Report To AROAP � Date Received: 04111/2013 '/ Time Received: 08:00 Collector: B LAVERTY O Y Labworks LoginlD HMORGAN Region: ARO Final Report Dale: 4/27/13 Sample Matrix: S GROUNDWATER Final Report Report Print Date: 07/18/2013 Loc. Type: MONITORING WELL Emergency Yes/No VlsitlD CDC YeslNo Lac. Descr.: COATS AMERICAN 630 AMERICAN THREAD ROAD MARION, NC Location ID: 1P59C0ATSMW12 Collect Dale: 0410912013 CollectTime: 10:00 Sample Depth If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes Result/Method Analvsi CAS # Analvte Name P(�L, Units Qualifier Reference Date LAB VOL Sample temperature at receipt by lab 2.0 C 4/11113 HMORGAN Volatile Organics in liquid _TITLE_ ug/L EPA50301624/8260 4/11113 ;ACHANDLER 75-71-8 Dichlorodifluoromethane 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 74-87-3 Chloromethane 1.0 Not detected ug/L EPA5030/62418260 4111113 ACHANDLER 75-014 Vinyl Chloride 0.50 Not detected ug/L EPA5030162418260 4/11/13 ACHANDLER 74-83.9 Bromomethane 1.0 Not detected ug/L EPA5030162418260 4/11113 ACHANDLER 75-00-3 Chloroethane 0.50 Not detected ug/L EPA5030/62418260 4111/13 ACHANDLER 75-60-4 Trichlorofluoromethane 0.50 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 75-35-4 1,1-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 4111113 ACHANDLER 75-09-2 Methylene Chloride 10 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 156-60-5 trans-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/62418260 4111113 ACHANDLER 1634-04-4 Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPA5030162418260 4/11113 ACHANDLER 75-34-3 1,1-Dichloroethane 0.25 Not detected ug/L EPA5030162418260 4/11/13 ACHANDLER 156-59-2 CIS-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 4111113 ACHANDLER 74-97-5 Bromochloromethane 0.25 Not detected ug/L EPA503Ot624/8260 4/11113 ACHANDLER 67-66-3 Chloroform 0.25 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 594-20-7 2,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 4111113 ACHANDLER 107-06-2 1,2-Dichloroethane 0.25 Not detected ug/L EPA5030162418260 4/11/13 ACHANDLER 71-55-6 1,1,1-Trichloroethane 0.25 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 553-58-6 1,1-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L EPA5030/624/8260 4111/13 ACHANDLER 7143-2 Benzene 0.25 Not detected ug/L EPA5030/62418260 4/11113 ACHANDLER 74-95-3 Dibromomethane 1.0 Not detected ug/L EPA5030/624/8260 4111113 ACHANDLER 78-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 4111113 ACHANDLER 79-01-6 Trichloroethene 0.25 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 75-27-4 Bromodichloromethane 0.25 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 10061-01-5 cis-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030162416260 4/11113 ACHANDLER 10061-02-6 trans-1,3-Dichloropropene 0.25 Not detected ug/L EPA50301624/8260 4/11113 ACHANDLER 79-00-5 1,1,2-Trichloroethane 0.25 Not detected ug/L EPA5030/62418260 4111/13 ACHANDLER 108-88-3 Toluene 0.25 Not detected ug/L EPA5030/62418260 4/11113 ACHANDLER Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699.1623 (919) 733-3908 Fina delaJed dsswpwnorlaa quaeflerp es 2(erlo pl¢J/eenarcee,vd.al Page 1 of 2 NC,D1NQ La6oratorySection /Fsufts Location ID: 1P59COATSMWI2 Sample ID: AB94214 Collect Date: 0410912013 Collect Time:: 10:00 VOL CAS # 142-28-9 Analvte Name 1,3-Dichloropropane P(�, LL 0.25 Result/Units Qualifier Not detected ug/L Method Reference EPA5030/624/8260 Analysis Date 4111113 Validated by ACHANDLER 124-48-1 Dibromochloromethane 0.50 Not detected ug/L EPA5030/62418260 4/11/13 ACHANDLER 106-93A (EDB)1,2-Dibromoethane 0.50 Not detected ug/L EPA5030162418260 4/11113 ACHANDLER 127-18A Telrachloroethene 0.25 Not detected ug/L EPA50301624/8260 4/11113 ACHANDLER 10840-7 Chlorobenzene 0.25 0.59 ug/L EPA50301624/8260 4111113 ACHANDLER 100-41A Ethylbenzene 0.25 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 75-25-2 Bromoform 1.0 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 108-38-3 m,p-Xylene 1.0 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 100-42-5 Styrene 0.25 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 79-34-5 1, 1,2,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 630-20-6 1, 1, 1,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 9547-6 o-Xylene 0.25 Not detected ug/L EPA5030/62418260 4111113 ACHANDLER 96-18-4 1,2,3-Trichloropropane 0.25 Not detected ug/L EPA5030/62418260 4111113 ACHANDLER 98-82.8 Isopropylbenzene 0.25 0.42 ug/L EPA5030/62416260 4/11113 ACHANDLER 108-86-1 Bromobenzene 0.25 Not detected ug/L EPA50301624/8260 4/11113 ACHANDLER 103-65-1 n-Propylbenzene 0.25 Not detected ug/L EPA5030/62418260 4111113 ACHANDLER 95-49-8 2-Chlorotoluene 0.25 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 106-434 4-Chlorotoluene 0.25 Not detected ug/L EPAS030162418260 4111/13 ACHANDLER 108-67-8 1,3,5-Trimethylbenzene 0.25 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 9B-066 tert-Butylbenzene 0.25 Not detected ug/L EPA50301624/8260 4111/13 ACHANDLER 95-63-6 1,2,4-Trimethylbenzene 0.25 Not detected ug/L EPAS030/62418260 4/11/13 ACHANDLER 135-98-8 see-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4111113 ACHANDLER 541-73-1 m-Dichlorobenzene (1,3) 0.25 Not detected ug/L EPAS030/62416260 4111/13 ACHANDLER 106 46-7 p-Dichlorobenzene (1,4) 0.25 Not detected ug/L EPA5030/62418260 4/11/13 ACHANDLER 95-50-1 o-Dichlorobenzene (1,2) 0.25 Not detected ug/L EPA5030/624/8260 4111113 ACHANDLER 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA5030/624/8260 4111113 ACHANDLER 104-51-8 n-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 86-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPAS0301624/8260 4111113 ACHANDLER 120-82-1 1,2,4-Trichlorobenzene 0.50 Not detected ug/L EPA5030/624/8260 4111/13 ACHANDLER 91-20-3 Naphthalene 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 87-68.3 Hexachlorobutadiene 0.50 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 87-61-6 1,2,3-Trichlorobenzene 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699.1623 (919) 733-3908 Fore delal6dd.b., bDries Quaffer wdee relel106f1J/J�It!_�6C 122AM.9etCLatr^_2bG[Mas%L.oy„L¢.a.nn ca!•..n•_ii r. (gap ays_yjyolf„im Page 2 of 2 GROUNDWATER FIELD/LAB FORM Department of Environment and Natural Resource —Location code 1 P59CoatsMW12__ _ SAMPLE TYPE County: McDowell Do Water (Ground Water) Quad No Serial No. El soil ❑ Emergency Date Rece Lat. Long. ❑ Other ❑ Chain of Custody Report To: ARO, FRO, MRO, RRO, WaRO, WiRO, Data Entry By: Ck:_ WSRO, Kinston FO, Fed. Trust, Central Off., Other. Date Reported: Shipped by: Bus, Courier, Hand Del., Other: Purpose: Collector(s): Brett Laverty Date: 4/9/2013 Time: 10:60 AM Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other. FIELD ANALYSES Owner: Coats American (d deana) pH 400 Spec. Cond.e4 at 250C Location or Site: 630 American Thread Road Marion, NC TemD.,n eC Odor Description of sampling point: Monitoring Well MW12 s � Routine Lab Number ived Time: DIVISION OF WATER QUALITY -GROUNDWATER SECTION SAMPLE PRIORITY 4 Redd By: From:Bus, Cour er, Hand Del., Other: _DO, mg/L ORP, mV Sampling Method: External Well Pump Sample Interval LABORATORY ANALYSES BOD 310 mg/L COD High 340 mg/L COD Low 335 mg/L Colifonn: MF Fecal 31616 1100MI Colifom: MF Total 31504 1100m1 TOC 680 mg/L Turbidity 76 NTU Residue, Total Suspended 530 mg/L DOC pH 403 units Alkalinity to pH 4.5 410 mg/L Alkalinity to pH 8.3.415 mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L Carbon dioxide 405 mg/L Chlodde 940 mg/L Chromium: Hex 1032 ug/L Color: True 80 Cu Cyanide 720 mg/L Lab (Pumping time, air temp., etc) Lab (Pumping time, air temp., etc) Din. Solids 70300 mg/L Ag-Silver 46566 u L Organochlodne Pesticides Fluoride 951 mg/L AI -Aluminum 46657 u L Or ano hos horus Pesticides Hardness: Total 900 mg/L As -Arsenic 46551 u L Nitrogen Pesticides Hardness (nonrarb) 902 mg/L Ba-Barium 46558 u /L Add Herbicides Phenols 32730 ugn Ca -Calcium 46552 mgtL PCBs Specific Cond. 95 pMhos/cm Cd-Cadmium 46559 u /L Sulfate 945 mg/L Cr-Chromium 46559 u 2 MBAs Sulfide 745 mg/L Cu-Copper 46562 u /L Boron Fe -Iron 46563 u IL Semivolafile Orrianics Oil and Grease mg/L Hg-Mercury 71900 u TPH-Diesel Ran e K-Potassium 46555 rn gfL Mg -Magnesium 46554 mg/L PO4 as P Mn-Manganese 46565 u IL x Volatile Organics(VOA bouts NH3 as N 610 mg/L Na-Sodium 46556 m TPH-Gasoline Range TKN as N 625 mg/L Ni-Nickel u /L TPH-BTD( Gasoline Ran e N%+ NO, as N 630 mg/L Pb-Lead 46564 u IL P: Total as P 665 mg/L Se -Selenium u /L Nitrate (NO3 as N) 620 mg/L Zn-Zinc46567 u /L Nitrite (NO, as N) 615 mg/L LAB USE ONLY Temperature on arrival (eC): NH4 -ammonium Silica JUL L % 1013 Asheville Regional Office County: WATF9 River Basin OF Report To AROAP Collector. B LAVERTY O Y Region: ARO Sample Matrix: BLANKWATER Loa Type: TRIP BLANK Final Report Emergency Yes/No VisitlD CDC Yes/No Loc. Descr.: VOATRIP BLANK Sample ID: PO Number# Date Received: Time Received: Labworks LoginlD Final Report Date: Report Print Date: AB94210 13GO264 04/1112013 08:00 HMORGAN 4/22113 RECEEIVE I Location ID: VOATRIPBLANK I Collect Date: 0410912013 1 Collect Time: 07:51 1 1 Sample Depth I If this report is labeled preliminary report the results have not been validated. Do not use for CAS # Analvte Name S Result/ Units Method Analysis Validated by ualifier Reference Date LAB Sample temperature at receipt by lab 2.0 C 4/11/13 HMORGAN VOL Volatile Organics in liquid _TITLE ug/L EPA5030/624/8260 4/11113 ACHANDLER 75-71-8 Dichlorodifluoromethane 1.0 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 74-87-3 Chloromethane 1.0 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 75-014 Vinyl Chloride 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 74-83-9 Bromomethane 1.0 Not detected ug/L EPA50301624/8260 4/11113 ACHANDLER 75-00-3 Chloroethane 0.50 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 75-69-4 Trichlorofluoromethane 0.50 Not detected ug/L EPA5030162418250 4/11113 ACHANDLER 75-35-4 1,1-Dichloroethene 0.25 Not detected ug/L EPA50301624/8260 4111/13 ACHANDLER 75-09-2 Methylene Chloride 10 Not detected ug1L EPA5030162418260 4/11113 ACHANDLER 156-60-5 trans-1,2-Dichloroethene 0.25 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 1634-044 Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPA50301624/8260 4/11113 ACHANDLER 75-34-3 1,1-Dichloroethane 0.25 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 156-59-2 cis-1,2-Dichloroethene 0.25 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 74-97-5 Bromochloromethane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 67-66-3 Chloroform 0.25 Not detected ug/L EPA50301624/8260 4111/13 ACHANDLER 594-20-7 2,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 107-06-2 1,2-Dichloroethane 0.25 Not detected uglL EPA5030/62418260 4111/13 ACHANDLER 71-55-6 1, 1,1-Trichloroethane 0.25 Not detected ug/L EPA5030162418260 4/11/13 ACHANDLER 563-58-6 1,1-Dichloropropene 0.25 Not detected ug/L EPA5030/62418260 4/11113 ACHANDLER 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 71-43-2 Benzene 0.25 Not detected ug/L EPA5030/624/8260 4111113 ACHANDLER 74-95-3 Dibromomethane 1.0 Not detected ug/L EPA50301624/8260 4/11/13 ACHANDLER 78-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPA5030162418260 4/11/13 ACHANDLER 79-01-6 Trichloroethene 0.25 Not detected ug/L EPA5030/624/8260 4111113 ACHANDLER 75-274 Bromodichloromethane 0.25 Not detected ug/L EPA5030/62418260 4111/13 ACHANDLER 10061-01-5 cis-1,3-Dichloropropene 0.25 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 10061-02-6 trans-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 79-00-5 1,1,2-Trichloroethane 0.25 Not detected ug/L EPA50301624/8260 4/11113 ACHANDLER 108-88-3 Toluene 0.25 Not detected ug/L EPA5030162418260 4111113 ACHANDLER Laboratory Section» 1623 Mall Service Center, Raleigh, NC 27699-1623 (919)733-3908 For a dmaikd dosOpfion of tee quamorcodes wfor lot!{p.;l(.py¢a6pW.et.mllxxpLwNiaf @1 xa Page 1 of 2 5VC/WVQ La6oratorySection q?fsv6ts Ir Location ID: VOATRIPBLANK Sample 10: AB94210 Collect Date: 04/09/2013 CollectTme:: 07:51 VOL CAS At 142-28-9 Analvte Name 1,3-Dichloropropane PSG L, 0.25 Result/Units ualifier Not detected ug/L Method Reference EPAS0301624/8260 Analysis Date 1/11/13 Validated by ACHANDLER 124-48-1 Dibromochloromethane 0.50 Not detected ug/L EPA50301624/8260 4/11113 ACHANDLER 106-93-4 (EDB)1,2-Dibromoethane 0.50 Not detected ug/L EPAS0301624/8260 4/11113 ACHANDLER 127-184 Tetrachloroethene 0.25 Not detected ug/L EPAS030/624/8260 4111/13 ACHANDLER 10B-90-7 Chlorobenzene 0.25 Not detected ug/L EPA5030162418260 4/11/13 ACHANDLER 100-41-0i l .,Ethlpenzene 0.25 Not detected ug/L EPA50301624/B260 4/11/13 ACHANDLER 75-25.2 Bromoform 1.0 Not detected ug/L EPA50301624/8260 4111/13 ACHANDLER 108-38-3 m,p-Xylene 1.0 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 10042-5 Styrene 0.25 Not detected ug/L EPA5030162418260 4/11113 ACHANDLER 79-34-5 1,1,2,2-Tetrachloroethane 0.25 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 630.20-6 1, 1, 1,2-Tetrachloreethane 0.25 Not detected ug/L EPA50301624/8260 4/11113 ACHANDLER 95-47-6 o-Xylene 0.25 Not detected ug/L EPA5030/624/8260 4111/13 ACHANDLER 96-194 1,2,3-Trichloropropane 0.25 Not detected ug/L EPA5030162418260 4111/13 ACHANDLER 98-82-8 Isopropylbenzene 0.25 Not detected ug/L EPA5030162418260 4111113 ACHANDLER 108-86-1 Bromobenzene 0.25 Not detected ug/L EPA5030/62418260 4/11113 ACHANDLER 103-65-1 n-Propylbenzene 0.25 Not detected ug/L EPA5030162418260 4/11113 ACHANDLER 95-49-8 2-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 4111113 ACHANDLER 10543-4 4-Chlorotoluene 0.25 Not detected ug/L EPA5030162418260 4/11/13 ACHANDLER 108-67-6 1,3,5-Trimethylbenzene 0.25 Not detected ug/L EPA50301624/8260 4111113 ACHANDLER 98-06.6 tert-Butylbenzene 0.25 Not detected ug/L EPA50301624/8260 4/11113 ACHANDLER 95-63.6 1,2,4-Trimethylbenzene 0.25 Not detected ug/L EPA50301624/8260 4111/13 ACHANDLER 135-98-8 sec-Butylbenzene 0.25 Not detected ug1L EPA50301624/8260 4111/13 ACHANDLER 541-73-1 m-Dichlorobenzene (1,3) 0.25 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 106-46-7 p-Dichlorobenzene (1,4) 0.25 Not detected ug/L EPA5030162418260 4111/13 ACHANDLER 95-50.1 o-Dichlorobenzene (1,2) 0.25 Not detected ug/L EPA5030/62418260 4/11/13 ACHANDLER 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA5030162418260 4111/13 ACHANDLER 104-51-8 n-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 4111/13 ACHANDLER 96-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA50301624/8260 4/11113 ACHANDLER 120-82-1 1,2,4-Trichlorobenzene 0.50 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 91-20-3 Naphthalene 0.50 Not detected ug/L EPA5030/624/8260 4/11/13 ACHANDLER 87-88-3 Hexachlorobutadiene 0.50 Not detected ug/L EPA5030/624/8260 4/11113 ACHANDLER 87-61-6 1,2,3-Trichlorobenzene 1.0 Not detected ug/L EPA5030/62418260 4111/13 ACHANDLER Laboratory Sectlon» 1623 Mail Service Center, Raleigh, INC 27699.1623 (919) 733-3908 For a delafled dosedpdon of the quafifier codes refer to pl2dll!a[nLn-LAfecxeLwsEf»:NIM1RGV Lt+Mc•e rm•a w.mer [oa•,m•�gvonn Me nem.nl.�n,e/mfi /•:nnan> Page 2 of 2 GROUNDWATER FIELD/LAB FORM Location code: VOA Trip Blank SAMPLE TYPE County: Do Water (Ground Water) Quad No Serial No. ❑ Soil Lat. Long. ❑ Other ❑ Chain of Custody Report To: ARO, FRO, MRO, RRO, WaRO, WiRO, WSRO, Kinston FO, Fed. Trust, Central Off., Other. Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION SAMPLE PRIORITY Routine pp Lab Number ❑ Emergency Tp Date Received Time: Redd By: From:Bus, Courier, Hand Del., Other: Data Entry By: Ck: Date Reported: Shipped by: Bus, Courier, Hand Del., Other. Purpose: Collector(s): Brett Laverty Date: 4/9/2013 Time: 7:51 AM Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other: FIELD ANALYSES Owner: VOA Trip Blank lLU pH 4w Spec. Cond.94 at 25°C Location or Site: Temp.lo °C Odor Description of sampling point: Appearance DO, mg/L ORP, mV Sampling Method: Sample Interval LABORATORY ANALYSES (Pumping time, a rtemp., eta) 310 mg/LD rBOD High 340 mg/LD Low 335 mg/L Colifortn: MF Fece131616 /100ml Colifonn: MF Total 31504 1100ml TOC 680 mg/L Turbitlity 76 NTU Residue, Total Suspended 530 mg/L OOC PH403 units Alkalinity to pH 4.6 410 mg/L Alkalinity to pH 8.3 415 mg/L Camonate 445 mg/L Bicarbonate 440 mg/L Carbon dioxide 405 mg/L Chloride 940 mgr. Chromium: Hex 1032 ug/L Color. True 80 Cu Cyanide 720 mg/L Lab Diss. Solids 70300 mg/L Ag-Silver46566 u L Organochlorine Pesticides Fluoride 951 mg/L AI -Aluminum 46557 u /L Organophosphows Pesticides Hardness: Total 900 mg/L As -Arsenic 46551 u L Nitrogen Pesticides Hardness (non -cart) 902 mg/L Ba-Barium 46556 u L Acid Herbicides Phenols 32730 ug/l Ca -Calcium 46552 m 2 PCBs Specific Cord. 95 Whos/cm Cd-Cadmium 46559 u lL Sulfate 945 mg/L Cr-Chromium 46559 u /L MBAs Sulfide 745 mg/L Cu-Copper46562 a /L Boron Fe -Iron 46563 u /L Semivolatile0 ants Oil and Grease mg/L Hg-Merwry 71900 u L I TPH-Diesel Ran e K-Potassium 46555 mg/L Mg -Magnesium 46554 mgr- PO4 as P Mn-Manganese 46565 u /L Volatile Organics(VOA bottle NH3 as N 610 mg/L Na-Sodium 46556 mgr. TPH-Gasoline Range TKN as N 625 mg/L Ni-Nickel uq1L TPH-BTEX Gasoline Range NO2+NO3 as N 630 mg/L Pb-Lead 46564 u L P: Total as P 665 mg/L SeSelenlum ugn. Nitrate (NO3 as N) 620 mg/L Zn-Zinc465s7 uqf- Nibite (NO2 as N) 615 mg/L LAB USE ONLY Temperature on arrival (°C): NH4 -ammonium Silica GW-54 REV. 7103 For Dissolved Analysis -submit filtered sample and wnte'DIS'in block. __ _ Countya . _MCDOWELL F•fjgpF 9QG Sample ID: ACOO6a River Basin OHO PO Number # 13G0783 Report To AROAP Date Received: 091261201 Time Received: 08:16 Collector: B LAVERTY O Y Labworks LoginlD MSWIFT Region: ARO Final Report Date: 1 /1 Sample Matrix: GROUNDWATER Final Report Report Print Dale: 11l15120/20' Loc.Type: MONITORINGWELL Emergency Yes/No VisitlD CDC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD ROADD MARION, NC Location ID: IPSSCOATSMW10 Collect Date: 0912312013 Collect Time: 11:11 Sample Depth If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. CAS # Analvte Name P(�L Result/Units Method Analysis Validated by Qualifier Reference Date LAB Sample temperature at receipt by lab 1.6 'c 9/25/13 HMORGAN MIC Turbidity 1.0 1 U NTU APHA2130B-20th 9/25/13 ESTAFFORDI WET Residue -Suspended In liquid 6.2 12 U,P mg/L APHA2540D-20th 9126/13 CGREEN MET 7440-22-4 Ag by ICPMS 1.0 1.0 U ug/L EPA 200.8 1011113 ESTAFFORDI 7429-90-5 At by ICP 50 60 U ug/L EPA 200.7 10/3/13 ESTAFFORD11 7440-38-2 As by ICPMS 2.0 2.0 U ug/L EPA200.8 1011113 ESTAFFORDI 7429-90-5 B by ICP 50 150 ug/L EPA200.7 10/8/13 ESTAFFORDI 7440-38-3 Ba by ICP 10 11 ug/L EPA200.7 1013/13 ESTAFFORDI 7440-70-2 Ca by ICP 0.10 0.20 mg/L EPA 200.7 1013113 ESTAFFORD1 7440-43-9 Cd by ICPMS 0.50 0.60 U ug/L EPA200.8 10/1113 ESTAFFORDI 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA200.8 10/1113 ESTAFFORDI 7440-50-8 Cu by ICPMS 2.0 2.0 U ug/L EPA 200.8 10/1/13 ESTAFFORD'i 7439-89-6 Fe by ICP 50 50 U ug/L EPA 200.7 10/3/13 ESTAFFORDI 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA 245.1 10/10/13 ESTAFFORD1 7440-09-7 K by ICP 0.10 0.36 mgfL EPA 200.7 1013/13 ESTAFFORDI 7439-95-4 Mg by ICP 0.10 0.10 U mg/L EPA 200.7 1013/13 ESTAFFORD1 7439-96-5 Mn by ICPMS 10 IOU ug/L EPA 200.8 10/3/13 ESTAFFORDI 7440-23-5 Na by ICP 0.10 40 mg/L EPA 200.7 10/3/13 ESTAFFORDI 7440-02-0 NI by ICPMS 2.0 2.0 U ug/L EPA200.8 1011/13 ESTAFFORD1 7439-92-1 Pb by ICPMS 2.0 2.0 U ug/L EPA 200.8 10/1/13 ESTAFFORDI 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 10/1113 ESTAFFORDI 7440-28-0 Thallium (TI) ICPMS 2.0 2.0 U ug/L EPA 200.8 10/1113 ESTAFFORDI 7440-66.6 Zn by ICPMS 10 IOU ug/L EPA200.8 1011/13 ESTAFFORD'I VOL 7440-50-8 Volatile Organics in liquid _TITLE_ ug/L EPA50301624/8260 9125/13 VANDREWS 75.71-8 Dichlorodifluoromethane 1.0 Not detected ug/L EPA5030/62418260 9/25113 VANDREWS 74-87-3 Chloromethane 1.0 Not detected ug/L EPA5030/624/8260 9125/13 VANDREWS 75-01-4 Vinyl Chloride 0.50 Not detected J2 ug/L EPA5030/624/8260 9125/13 VANDREWS Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Far a detailed loaf PW. dit e.a.e1.ert1.11. .enuenm!..1.,om Page 1 of 3 NC /DWQ Ga6oratory Section.&mIts Location 10: 1P69COATSMWIO Sample ID: AC00648 Collect Dale: 09/2312013 Collect Time:: 11:11 VOL CAS # 74-83-9 Analvte Name Bromomethane P(�L 1.0 ResulU Qualifier Not detected Units ug/L Method Reference EPA5030162418260 Analysis Date 9/25/13 validated by VANDREWS 75-00-3 Chloroethane 0.50 Not detected ug/L EPA50301624/8260 9/25113 VANDREWS 75-69-4 Trichlorofluoromethane 0.50 Not detected ug/L EPA5030/62418260 9125/13 VANDREWS 75-35-4 1,1-Dichloroethene 0.25 Not detected J2 ug/L EPA5030/624/8260 9/25113 VANDREWS 75-09-2 Methylene Chloride 10 Not detected ug/L EPA50301624/8260 9125113 VANDREWS 156-60-5 trans-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/62418260 9125113 VANDREWS 1634-04-4 Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPA50301624/8260 9/25/13 VANDREWS 75-34-3 1,1-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 9125/13 VANDREWS 156.59-2 cis-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/62418260 9125113 VANDREWS 74-97-5 Bromochloromethane 0.25 Not detected ug/L EPAS030/62418260 9125113 VANDREWS 67-66-3 Chloroform 0.25 Not detected ug/L EPA5030162418260 9125113 VANDREWS 594-20-7 2,2-Dichloropropane 0.25 Not detected ug/L EPA50301624/8260 9/25/13 VANDREWS 107-06-2 1,2-Dichloroethane 0.25 Not detected ug/L EPA5030162418260 9/25113 VANDREWS 71-55-6 1,1,1-Trichloroethane 0.25 Not detected ug/L EPA5030/62418260 9/25113 VANDREWS 563-58-6 1,1-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L EPA5030/62418260 9/25/13 VANDREWS 71-43-2 Benzene 0.25 Not detected ug1L EPA5030162418260 9125113 VANDREWS 74-95-3 Dibromomethane 1.0 Not detected ug/L EPA5030/624/8260 9125113 VANDREWS 78-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPA5030/62418260 9125/13 VANDREWS 79-01-6 Trichloroethene 0.25 Not detected ug/L EPA50301624/8260 9125113 VANDREWS 75-27A Bromodichloromethane 0.25 Not detected ug/L EPA50301624/8260 9/25113 VANDREWS 10061-01-5 cis-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 9/25113 VANDREWS 10061-02-6 trans-1,3-Dichloropropene 0.25 Not detected ug/L EPA50301624/8260 9125113 VANDREWS 79-00-5 1,12-Trichloroethane 0.25 Not detected ug/L EPA5030162418260 9/25113 VANDREWS 108-58-3 Toluene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 142-28-9 1,3-Dichloropropane 0.25 Not detected ug/L EPA50301624/8260 9/25/13 VANDREWS 124-48-1 Dibromochloromethane 0.50 Not detected ug/L EPA5030/62418260 9125/13 VANDREWS 106.93-4 (EDB)1,2-Dibromoethane 0.50 Not detected ug/L EPA5030/62418260 9125113 VANDREWS 127-18-4 Tetrachloroethene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 10840-7 Chlorobenzene 0.25 Not detected ug/L EPA5030/824/8260 9/25/13 VANDREWS 100-414 Ethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9125/13 VANDREWS 75-25-2 Bromoform 1.0 Not detected ug/L EPA5030/62418260 9/25/13 VANDREWS 10848-3 m,p-Xylene 1.0 Not detected ug/L EPA5030/62418260 9/25113 VANDREWS 100-42-5 Styrene 0.25 Not detected ug/L EPA5030/62418260 9/25/13 VANDREWS 79-34-5 1, 1,2,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/62418260 9/25/13 VANDREWS 630-20.6 1, 1, 1,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 9125/13 VANDREWS 9547-6 o-Xylene 0.25 Not detected ug/L EPA50301624/8260 9/25113 VANDREWS 96-18-4 1,2,3-Trichloropropane 0.25 Not detected ug/L EPA5030162418260 9125/13 VANDREWS 98-82-8 Isopropylbenzene 0.25 Not detected ug/L EPAS0301624/8260 9125113 VANDREWS 108-86-1 Bromobenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25113 VANDREWS 103-65-1 n-Propylbenzene 0.25 Not detected ug/L EPA50301624/8260 9125113 VANDREWS 9549-8 2-Chlorotoluene 0.25 Not detected ug/L EPA5030/62418260 9125/13 VANDREWS Laboratory Section 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a doWlf,d deswplbn of Me quarter emes refer to n:,,110 nixern. n ImoMam>MePnfanetlw,^nvo-a in.cm n.rvn Page 2 of 3 .NCOTPQ Laboratory Section Pfmfts Location ID: IP69COATSMWIO Sample ID: AC00648 Collect Date: 09/23/2013 Collect Time:: 11:11 CAS # 10643-4 Analvte Name 4-Chlorotoluene PQL 0.25 ResulU ualifier Not detected Units ug/L Method Reference EPA5030/624/8260 Analysis Date 9125113 validated by i VANDREWS 108-87-8 1,3,5-Trimethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9125/13 VANDREWS 98-06-6 tert-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9125113 VANDREWS 95-63-6 1,2,4-Trimethylbenzene 0.25 Not detected ug/L EPA5030162418260 9125/13 VANDREWS 135-98-8 sec-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9125/13 VANDREWS 541-73-1 m-Dichlorobenzene (1,3) 0.25 Not detected ug/L EPA50301624/8260 9/25113 VANDREWS 106-46-7 p-Dichlorobenzene (1,4) 0.25 Not detected ug/L EPA5030162418260 9125113 VANDREWS 95-50-1 o-Dichlorobenzene (1,2) 0.25 Not detected ug/L EPA5030162418260 9/25113 VANDREWS 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA5030/62418260 9/25113 VANDREWS 104-51-8 n-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9/25113 VANDREWS 96-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA5030/624/B260 9/26/13 VANDREWS 120-82-1 1,2,4-Trichlorobenzene 0.50 Not detected ug/L EPA5030162418260 9/25/13 VANDREWS 91-20-3 Naphthalene 0.50 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 87-68-3 Hexachlorobutadiene 0.50 Not detected ug/L EPA50301624/8260 9/25113 VANDREWS 87-61-6 1,2,3-Trichlorobenzene 1.0 Not detected uglL EPA5030/624/8260 9/25113 VANDREWS Sample Comments VOA-J2-estimated-2 analyte(s) failed < LCL in the CV. f:TSS-U, P-Sample was duplicated. PQL elevated for volume. Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699.1623 (919( 733-3908 ForedMWTedd.0 PWn an. peGfiero .d relor Ion .irce . •m h K• Page 3 of 3 County: MCDOWELL WATF9 Sample ID: AC01053 River Basin OF i0� QG PO Number# 13G0816 Report To AROAP 6j Date Received: 10/1012013 Time Received: 08:11 Collector. B LAVERTY O Y Labworks LoginlD MSWIF7 Region: ARO Finalport Dale: 1 3 Sample Matrix: GROUNDWATER Final Report r Report t Print Date: 11/21/2/2112013 Lot Type: MONITORING WELL Emergency Yes/No VisitlD COC YeslNo Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD ROADD MARION NC Location ID: 1P69COATSMWI6 Collect Date: 10/0812013 Collect Time: 14:14 Sample Depth If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. __,,a_^,___ Result/ I Method Analysis . "'""" ualifier Reference Date LAB Sample temperature at receipt by lab 1.7 C 10/10/13 HMORGAN MET 7440-22-4 Ag by ICPMS 1.0 1.0 U ug/L EPA200.8 10/16/13 ESTAFFORDI 7429-90-5 Al by ICP 50 130 ug/L EPA 200.7 10/21113 ESTAFFORDI 7440-38-2 As by ICPMS 2.0 2.0 U ug/L EPA 200.8 10/16/13 ESTAFFORD1 7429-90-5 B by ICP 50 56 ug1L EPA 200.7 10/24/13 ESTAFFORDI 7440-38-3 Be by ICP 10 150 ug/L EPA 200.7 10/21/13 ESTAFFORDI 7440-70-2 Ca by ICP 0.10 80 mg/L EPA200.7 10/21/13 ESTAFFORDI 744043-9 Cd by ICPMS 0.50 0.50 U ug/L EPA200.8 10/16/13 ESTAFFORDI 7440-47-3 Cr by ICPMS 10 IOU ugfL EPA200.8 10116/13 ESTAFFORDI 7440-50-8 Cu by ICPMS 2.0 2.0 U ug/L EPA200.8 10/16/13 ESTAFFORD1 7439-89-6 Fe by ICP 50 5600 ug/L EPA200.7 10121/13 ESTAFFORDI 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA245.1 10/18/13 ESTAFFORD1 7440-09-7 K by ICP 0.10 1.9 mg/L EPA 200-7 10/21/13 ESTAFFORD1 7439-95-4 Mg by ICP 0.10 28 mg/L EPA200.7 10/21/13 ESTAFFORDI 7439-96-5 Mn by ICP 10 1700 ug/L EPA 200.7 10/21/13 ESTAFFORDI 7440-23-5 Na by ICP 0.10 39 mg/L EPA 200.7 10/21/13 ESTAFFORDI 7440-02-0 Ni by ICPMS 2.0 6.8 ug/L EPA 200.8 10/22/13 ESTAFFORD7 7430-92-1 Pb by ICPMS 2.0 2.0 U ug/L EPA 200.8 10/16/13 ESTAFFORD1 7782A9-2 Se by ICPMS 5.0 6.0 U ug/L EPA 200.8 10/16/13 ESTAFFORD1 7440-28-0 Thallium (TI) ICPMS 2.0 2.0 U ug/L EPA200.8 10/16/13 ESTAFFORDI 7440-66-6 Zn by ICP 10 IOU ug/L EPA200.7 10/21113 ESTAFFORDI VOL Volatile Organics in liquid _TITLE_ ug/L EPA5030/62418260 10/10113 VANDREWS 75-71-8 Dichlorodifluoromethane 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 74-87-3 Chloromethane 1.0 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 75-014 Vinyl Chloride 0.50 Not detected J2 ug/L EPA5030/624/8260 10/10/13 VANDREWS 74-83-9 Bromomethane 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-00-3 Chloroethane 0.50 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 75-69-4 Trichlorofluoromethane 0.50 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 75-35-4 1,1-Dichlorcethene 0.25 Not detected ug/L EPAS0301624/8260 10/10/13 VANDREWS Laboratory Section» 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Foie d�ddesctlpO.n orlee q.wr..rmdecmrww / ^r Page 1 of 3 NC /D'WQ La6oratory Section IRSsuas Location ID: 1PSSCOATSMW15 Sample ID: AC01053 Collect Dale: 1010812013 Collect Time:: 14:14 VOL CAS # 75-09-2 Analvte Name Methylene Chloride P(�. LL 10 Result/Units ualifier Not detected ug/L Method Reference EPA5030162418260 Analysis Date 10/10/13 Validated by VANDREWS 156-60-5 trans-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 1634-D4-4 Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-34-3 1,1-Dlchloroethane 0.25 Not detected ug/L EPA5030162418260 10/10113 VANDREWS 156.59-2 cis-1,2-Dichloroethene 0.25 Not detected ugr- EPA5030162418260 10/10113 VANDREWS 74-97-5 Bromochloromethane 0.25 Not detected ug/L EPA5030152418260 10110/13 VANDREWS 67-66-3 Chloroform 0.25 Not detected ug/L EPAS0301624/8260 10/10/13 VANDREWS 594-20-7 2,2-Dichloropropane 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 107-06-2 1,2-Dichloroethane 0.25 Not detected uglL EPA5030162418260 10/10/13 VANDREWS 71-55-6 1,1,1-Trichloroethane 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 563-58-6 1,1-0ichloropropene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L EPAS030162418260 10/10/13 VANDREWS 7143.2 Benzene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 74-95.3 Dibromomethane 1.0 Not detected ug/L EPAS030/62418260 10/10/13 VANDREWS 78-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 79.01-6 Trchloroethene 0.25 Not detected ug1L EPA5030/62418260 10/10/13 VANDREWS 75-27A Bromodichloromethane 0.25 Not detected ug/L EPAS030/624/8260 10/10/13 VANDREWS 10061-01-5 Cis-1,3-Dichloropropene 0.26 Not detected ug/L EPAS0301624/8260 10/10/13 VANDREWS 10061-02-6 trans-1,3-Dichloropropene 0.25 Not detected ug/L EPAS0301624/8260 10/10113 VANDREWS 79-ON5 1,1,2-Trichloroethane 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 108-88-3 Toluene 0.25 Not detected ug/L EPA50301624IB260 10/10/13 VANDREWS 142-28.9 1,3-Dichloropropane 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 12448-1 Dibromochloromethane 0.50 Not detected ug/L EPA503Ot624/8260 10/10/13 VANDREWS 106-934 (EDB)1,2-Dibromoethane 0.50 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 127-18-4 Tetrachloroethene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 108-90-7 Chlorobenzene 0.25 Not detected ug/L EPA50301624/8260 10/10113 VANDREWS 100-414 Ethylbenzene 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 75-25-2 Bromoform 1.0 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 10B.38-3 m,p-Xylene 1.0 Not detected ug/L EPA5030/62418260 10110/13 VANDREWS 1ON42-5 Styrene 0.25 Not detected ug/L EPAS030/624/6260 10/10/13 VANDREWS 79-34-5 1,1,2,2-Tetrachloroethane 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 630-20-8 1,1,1,2-Tetrachloroethane 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 95-47-6 O-Xylene 0.25 Not detected ug/L EPAS0301624/8260 10/10/13 VANDREWS 96-18-4 1,2,3-Trichloropropane 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 98-82-8 Isopropylbenzene 0.25 Not detected ug/L EPA60301624/8260 10/10/13 VANDREWS 108.86-1 Bromobenzene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 103-65-1 n-Propylbenzene 0.25 Not detected ug/L EPAS0301624/8260 10/10/13 VANDREWS 9549.8 2-Chlorotoluene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 106-43-4 4-Chlorotoluene 0.25 Not detected ug/L EPAS0301624/8260 10/10/13 VANDREWS 108-67-8 1,3,5-Trimethylbenzene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 98-06-6 tert-Butylbenzene 0.25 Not detected uglL EPA503016241826D 10/10/13 VANDREWS 95-63-6 1,2,4-Trimethylbenzene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS Laboratory Section>> 1623 Mall Service Center, Raleigh, NC 27699.1623 (919) 733-3908 Fora OH.Woeectlpaon WOa... lifiw COEIW.rtolm (ygy rc- �.e<, m am ne> ne Page 2 of 3 7YC(DOQ, Ga6oratorySection Pssuks LocattonlDr ' 1P69COATSMWI6 Sample ID: AC01063 Collect Date: 1010812013 Collect Time:: 14:14 VVL CAS # 135-98-8 Analvte Name sec-Butylbenzene PQL 0.25 Result/ Qualifier Not detected Units ug/L Method Reference EPA50301624/8260 Analysis Date 10/10/13 Validated by VANDREWS 541-73-1 m-Dichlorobenzene(1,3) 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 106-46.7 p-Dichlorobenzene (1,4) 0.25 Not detected ug/L EPA5030/62418260 10/10113 VANDREWS 95-50-1 o-Dichlorobenzene (1,2) 0.25 Not detected ug/L EPA50301624/8260 10110/13 VANDREWS 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA50301624/8260 10110/13 VANDREWS 104-51-8 n-Butylbenzene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 96-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 120.82-1 1,2,4-Tichlorobenzene 0.50 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 91-20-3 Naphthalene 0.50 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 87-58-3 Hexachlorobutadiene 0.50 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 87-61-6 1,2,3-Tichlorobenzene 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS Sample Comments :VOA-J2-estimated-1 analyte(s) failed < LCL in the CV. Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699.1623 (919) 733J908 Ftta damped d.W,*n amd queOfiercodea refer ldh% Page 3 of 3 County: MCDOWELL INArF9 Sample ID: AC01107 River Basin OF 0�. OG PO Number# ARO Report To AROAP I -Date Rammed: 1010912013 "1 Time Received: 10A0 Collector. B LAVERTV O Y Labworks LoginlD KJIMISON2 Region: ARO Final Report Date: 10/29H3 Sample Matrix: GROUNDWATER Final Report Report Print Date: 11/2112013 Loc. Type: MONITORING WELL Emergency Yes/No VisBID COG Yes/No Loc. Descr.: Location ID: IP69COATSMWIS I Collect Date: 1010812013 Collect Time: 14:14 Sample Depth If this report is labeled preliminary report the results have not been validated. Do not use for Regulatory purposes. Result/ Method_ Analysis 'wi- ualifier Reference Date Others Sample temperature at receipt by lab 1.7 'C 1019113 RBYRD Turbidity 1 33 NTU APHA2130B-20th 10110/13 CGREEN Residue —Suspended In liquid 6.2 12 mg/L APHA2540D-20th 10110/13 CGREEN Laboratory Section 1623 Mall Service Center, Raleigh, NC 27699.1623 (919) 733-3908 rota E¢IalleE ae¢uipllon olrae auaMarootle¢relerta➢.NIL.¢¢2e^9�^:�l?!�+_*0/+,'d�WII+6�6e<^'•^:.o.. evnme. coa...n eu eer r..mo.r.m(�¢g(y�¢ey/r¢u¢y��p, Page 1 of 1 County: McDOWELL WATF9 Sample ID: AC00650 River Basin OF O� OG PO Number # 13GO786 Report To AROAP r^q T� Date Received: 09/512013 '-i Time Received: 08:16 Collector: B LAVERTY O Y Lallworks LoginlD MSWIFT Region: ARO Final Report Date: / 11/1520 Sample Matrix: GROUNDWATER Final Report Report Print Date: 1l/13 Loc.Type: WATERSUPPLY Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD ROAD MARION, NC Location ID: 1P59COATSSUMP Collect Date: 0912312013 Collect Time: 13:54 Sample Depth If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. Result/ Method Analysis ualifier Reference Date LAB Sample temperature at receipt by lab 1.6 C 9/25/13 HMORGAN MET 7440-224 Ag by ICPMS 1.0 1.0 U ug/L EPA200.8 10/1113 ESTAFFORDI 7429-90-5 Al by ICP 50 SOU ug/L EPA 200.7 10/3113 ESTAFFORDI 7440-38-2 AS by ICPMS 2.0 2.0 U ug/L EPA200.8 10/1113 ESTAFFORDI 7429-90-5 B by ICP 50 50 U ug/L EPA200.7 1013113 ESTAFFORDI 7440-38-3 Be by ICP 10 44 ug/L EPA 200.7 10/3113 ESTAFFORDI 7440-70-2 Ca by ICP 0.10 39 mg/L EPA 200.7 1013/13 ESTAFFORDI 7440-43-9 Cd by ICPMS 0.50 0.50 U ug/L EPA 200.8 1011/13 ESTAFFORD1 7440-47-3 Cr by ICPMS 10 IOU uglL EPA 200.8 10/1M3 ESTAFFORD1 7440-50-8 Cu by ICPMS 2.0 2.0 U ug/L EPA 200.8 10/1/13 ESTAFFORDI 7439-89-6 Fe by ICP 50 50 U ug/L EPA200.7 10/3/13 ESTAFFORDI 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA 245.1 10/10/13 ESTAFFORDI 7440-09-7 K by ICP 0.10 1.9 mg/L EPA 200.7 10013 ESTAFFORDI 7439-954 Mg by ICP 0.10 19 mg/L EPA 200.7 10/3113 ESTAFFORDI 7439-96-5 Mn by ICPMS 10 IOU ug/L EPA 200.8 1013113 ESTAFFORD1 7440-23-5 Na by ICP 0.10 31 mg/L EPA 200.7 1013/13 ESTAFFORD1 7440-02-0 Ni by ICPMS 2.0 2.0 U ug/L EPA 200.8 1011113 ESTAFFORD1 7439-92-1 Pb by ICPMS 2.0 2.0 U ug/L EPA 200.8 10/1l13 ESTAFFORDI 7782.49.2 Se by ICPMS 5.0 6.0 U ug/L EPA 200.8 10/1113 ESTAFFORD1 7440-28-0 Thallium (TI) ICPMS 2.0 2.0 U ug/L EPA 200.8 1011/13 ESTAFFORDI 7440-66-6 Zn by ICPMS 10 IOU ug1L EPA 200.8 1011/13 ESTAFFORDI VOL 7440-50-8 Volatile Organics in liquid TITLE_ ug/L EPA5030162418260 9125113 VANDREWS 75-71-8 Dichlorodifluoromelhane 1.0 Not detected ug/L EPA5030162418260 9/25/13 VANDREWS 74-87-3 Chloromethane 1.0 Not detected ug/L EPA5030/624/8260 0125113 VANDREWS 75-01-4 Vinyl Chloride 0.50 Not detected J2 ug/L EPA50301624/8260 9/25/13 VANDREWS 74-83.9 Bromomethane 1.0 Not detected ug/L EPA5030/624/8260 9125/13 VANDREWS 75-00-3 Chloroethane 0.50 Not detected ug/L EPAS0301624/8260 9125113 VANDREWS 75-69-4 Trichlorofluoromethane 0.50 Not detected ug/L EPAS0301624/8260 9125113 VANDREWS 75-35-4 1,1-Dlchloroethene 0.25 Not detected J2 ug/L EPA5030/62418260 9/25113 VANDREWS Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699.1623 (919) 733-3908 Fora4elaltetl Eesulptlan of NoqueGferrAEea relerlo�jyJl oma nWm. wv/w.eadntlemnrwn�nr °in. _.n. b ne Page 1 of 3 NC /D`WQ La6oratorySection 9([!sults Location ID: IP59COATSSUMP Sample ID: AC00660 Collect Date: 09/23/2013 Collect Time:: 13:54 VOL Result/Method Analysis CAS # Analvte Name POLL Units Validated by ualifier Reference Date 75-09-2 Methylene Chloride 10 Not detected ug/L EPA50301624/8260 9/25113 VANDREWS 156-60-5 trans-1,2-Dichloroethene 0.25 Not detected ug/L EPAS0301624/8260 9/25113 VANDREWS 1634-04-4 Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPA5030/624/6260 9/25/13 VANDREWS 75-34-3 1,1-Dichloroelhane 0.25 Not detected ug/L EPA5030/62418260 9125/13 VANDREWS 156-59-2 cis-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/62418260 9125/13 VANDREWS 74-97-5 Bromochloromethane 0.25 Not detected ug/L EPA5030/62418260 9/25/13 VANDREWS 67-66-3 Chloroform 0.25 Not detected uglL EPA5030/62418260 9125/13 VANDREWS 594.20-7 2,2-Dichloropropane 0.25 Not detected uglL EPA5030/62418260 9125113 VANDREWS 107-06-2 1,2-Dichloroethane 0.25 Not detected ug/L EPAS030/624/8260 9125113 VANDREWS 71-55-6 1, 1. 1 -Trichloroethane 0.25 Not detected ug/L EPA5030162416260 9/25113 VANDREWS 563-SM 1,1-Dichloropropene 0.25 Not detected ug/L EPA50301624/8260 9/25113 VANDREWS 56-23.5 Carbon Tetrachloride 0.25 Not detected ug/L EPA50301624/8260 9125/13 VANDREWS 714S-2 Benzene 0.25 Not detected ug/L EPA50301624/8260 9125113 VANDREWS 74-95-3 Dibromomethane 1.0 Not detected ug/L EPA5030/624/8260 9125/13 VANDREWS 76-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPA50301624/8260 9/25113 VANDREWS 79-01.6 Trchloroethene 0.25 Not detected ug/L EPAS030182410260 9125113 VANDREWS 75-27-4 Bromodichloromethane 0.25 Not detected ug/L EPA50301624/8260 9/25/13 VANDREWS 10061-01-5 CIS-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030162418260 9125/13 VANDREWS 10061-02-6 Vans-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030162418260 9125/13 VANDREWS 79-00.5 1,1,2-Trichloroethane 0.25 Not detected ug/L EPAS030/62418260 9125/13 VANDREWS 108-88-3 Toluene 0.25 Not detected ug/L EPA5030162418260 9125/13 VANDREWS 142-28-9 1,3-Dichloropropane 0.25 Not detected ug/L EPAS0301624/8260 9125113 VANDREWS 124-48-1 Dibromochloromethane 0.50 Not detected ug/L EPA50301624/8260 9P25/13 VANDREWS 106-93-4 (EDB)1,2-Dibromoethane 0.50 Not detected ug/L EPA5030/62418260 9/25/13 VANDREWS 127-184 Tetrachloroehene 0.25 Not detected ug/L EPA50301624/8260 9125/13 VANDREWS 106-90-7 Chlorobenzene 0.25 Not detected ug/L EPAS030162418260 9/25113 VANDREWS 100-414 Ethylbenzene 0.25 Not detected ug/L EPA50301624/8260 9125113 VANDREWS 75-25-2 Bromoform 1.0 Not detected ug/L EPA5030162418260 9125/13 VANDREWS 108.38-3 m,p-Xylene 1.0 Not detected ug/L EPA5030/62418260 9/25113 VANDREWS 100.42-5 Styrene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 79-34-5 1,1,2,2-Tetrachloroethane 0.25 Not detected ug/L EPAS030162418260 9125/13 VANDREWS 630-20-6 1,1, 1,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 9125/13 VANDREWS 9547'6 o-Xylene 0.25 Not detected ug/L EPA50301624/8260 9125/13 VANDREWS 96-164 1,2,3-Trichooropropane 0.25 Not detected ug/L EPA50301624/8260 9125113 VANDREWS g5-82-8 Isopropylbenzene 0.25 Not detected ug/L EPAS030162418260 9/25/13 VANDREWS 108-86-1 Bromobenzene 0.25 Not detected ug/L EPAS0301624/8260 9125113 VANDREWS 103-65-1 n-Propylbenzene 0.25 Not detected ug/L EPA5030162418260 9125113 VANDREWS 95-49.8 2-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 9/25/13 VANDREWS 106-43-4 4-Chlorotoluene 0.25 Not detected ug/L EPA5030162418260 9125113 VANDREWS 108-67-8 1,3,5-Trimethylbenzene 0.25 Not detected ug/L EPAS030162418260 9125/13 VANDREWS 98-00-g tert-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9125/13 VANDREWS 95-63-6 1,2,4-Trimethylbenzene 0.26 Not detected ug(L EPA50301624/8260 9/25113 VANDREWS Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Fora EeWWCesWpW o(Ne 9uaG0eroasesrelerlo n3//ronei.veenaan/..emvismen+a<n..n.a-,.oa wa erc+tl•,.nag/o-ea�wfm,ner,.,eMxna>/,•ie+5on•muaro Page 2 of 3 NCID` IQGa6oratorySectionPgults Lomlion ID: a IP69COATSSUMP Sample ID: AC00550 Collect Date: 0912312013 CollectTintJ 13:64 VOL ResulU Method Analysis CAS # Analvte Name S Qualifier Units Validated by Reference Date' 135'88-8 sec-Butylbenzene 0.25 Not detected ug/L EPA5 330162418260 9/251131,- VANDREWS 0.25 Not detected 106-46-7 p-Dichlorobenzene (1,4) 0.25 Not detected ug/L EPA50301624/8260 9/25113I VANDREWS 95-50-1 o-Dichlorobenzene (1,2) 0.25 Not detected ug/L EPA5030162418260 9125113 j VANDREWS 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA5030162418260 9/25/13 VANDREWS 104-51-8 n-Butylbenzene 0.25 Not detected ug/L EPA50301624/8260 9125/13 VANDREWS 96-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA50301624/8260 9/25/13 VANDREWS 120-82-1 1,2,4-Tdchlorobenzene 0.50 Not detected ug/L EPA5030162418260 9125/13 VANDREWS 91-20-3 Naphthalene 0.50 Not detected uglL EPA5030/62418260 9125113 VANDREWS 87-68-3 Hexachlorobutadiene 0.50 Not detected ug/L EPA50301624/8260 9/25/13 VANDREWS 87-61-6 1,2,3-Tdchlorobenzene 1.0 Not detected ug/L EPA50301624/8260 9/25113 VANDREWS Sample Comments :VOA-J2-estimated-2 analyte(s) failed < LCL in the CV. Laboratory Section» 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detalad dessdptbn ortoo 9uatteroadea rarer to r Page 3 of 3 acolDSo NCQMAXLadorato Section rysuCts County: MCDOWELL Sample ID: AC01050 River Basin PO Number # 13GOB12 Report To AROAP Date Received: 10110112013 Time Received: 08:11 Collector: B LAVERTY Labworks LoginlD MSWIFT Region: ARO Division of Water Resources Final Report Date: 10/30113 SR Sample Matrix: GROUNDWATE Loc. Type: MONITORING WELL Final Report Report Print Date: 10/30/2013 , Emergency Yes/No VIsJdD COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD ROADD MARION NC Location 10: IF69COATSMW12 Collect Dale: 1010812013 Collect Time: 10:32 Sample Depth If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes Result! Method Analysis CAS # Analvle Name PQL Units Validated by Qualifier Reference Dale LAB Sample temperature at receipt by lab 1.7 °C 10110/13 HMORGAN 7440-22-4 Ag by ICPMS 1.0 1.0 U uglL EPA200.8 10/16113 ESTAFFORDI 7440-38-2 As by ICPMS 2.0 2.0 U ug/L EPA200.8 10/16/1,3 ESTAFFORDI 7429-90-5 B by ICP 50 220 ug/L EPA 200.7 10/24/13 ESTAFFORDI 7440-38-3 Ba by ICP 10 190 ug/L EPA 200.7 10121/13 ESTAFFORDI 7440-70-2 Ca by ICP 0.10 93 mg/L EPA 200.7 10/21113 ESTAFFORDI 7440-43-9 Cd by ICPMS 0.50 0.50 U ug/L EPA200.8 10/16113 ESTAFFORDI 7440-47.3 Cr by ICPMS 10 10 U ug/L EPA 200.8 10/16/13 ESTAFFORDI 7440- M Cu by ICPMS 2.0 2.0 U ug/L EPA200.8 10/16/13 ESTAFFORDI 7439-89-6 Fe by ICP 50 12000 ug/L EPA200.7 10/21/13 ESTAFFORDI 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA245.1 10/18/13 ESTAFFORDI 7440-09-7 K by ICP 0.10 6.3 mg/L EPA200.7 10/21/13 ESTAFFORDI 7439-95-4 Mg by ICP 0.10 17 mg/L EPA200.7 1001113 ESTAFFORDI 7439-96-5 Mn by ICP 10 4400 ug/L EPA 200.7 10/21113 ESTAFFORDI 7440-23-5 Na by ICP 0.10 160 mg/L EPA200.7 10/21113 ESTAFFORDI 7440-02-0 Ni by ICPMS 2.0 11 ugli. EPA200.8 10/22113 ESTAFFORDI 7439-92-1 Pb by ICPMS 2.0 2.0 U ug/L EPA200.8 10116/13 ESTAFFORDI 7782-49-2 Se by ICPMS 5.0 5.0 U uglL EPA200.8 10/16/13 ESTAFFORDI 7440-28-0 Thallium (TI) ICPMS 2.0 2.0 U ug/L EPA200.8 10116113 ESTAFFORDI 7440.6G6 Zn by ICP 10 13 ug/L EPA 200.7 10121113 ESTAFFORDt Volatile Organics in liquid _TITLE_ ug/L EPA50301624/8260 10/10113 VANDREWS 75-71-8 Dichlorodifluoromethane 1.0 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 74-87-3 Chloromelhane 1.0 Not detected ug/L EPA5030162418260 10/10M3 VANDREWS 75-01-4 Vinyl Chloride 0.50 Not detected J2 ug/L EPA5030/624/8260 10/10/13 VANDREWS 74-83-9 Bromomethane 1.0 Not detected ug/L EPA5030162418260 10/10113 VANDREWS 75-00-3 Chloroethane 0.50 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 75-69-4 Tdchlorofluoromethane 0.50 Not detected ug/L EPA5030/624/8260 10/10113 VANDREWS 75-35-4 1,1-Dichloroethene 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS Laboratory Section 1623 Mall Service Center, Raleigh, NO 27699-1623 (919) 733-3908 For a Catered dewriptim of tegw1r1erccWm refer to Page 1 of 3 5VC,DW/L La6oratory Section Pfw&r I Location 10: 1P59COATSMWI2 Sample ID: AC01050 Collect Date: 1010812013 Collect Tme:: 10:32 VOL Result/ Method Analysis CAS # Analyte Name PQL Units Validated by Qualifier Reference Date 75-09.2 Methylene Chloride 10 Not detected ug/L EPA50301624/8260 10110113 VANDREWS 156-60-5 trans-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 1634-04-4 Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 75-34-3 1,1-Dlohloroethane 0.25 Not detected ug/L EPA5030162418260 10/10113 VANDREWS 156-59.2 cis-1,2-Dichloroethene 0.25 Not detected ug/L EPA50301624/8260 10/10113 VANDREWS 74-97-5 Bromochloromethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 67-66-3 Chloroform 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 594-20-7 2,2-Dichloropropane 0.25 Not detected ug/L EPA5030/62418260 10110/13 VANDREWS 107-06-2 1,2-Dichloroethane 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 71-55-6 1,1,1-Trichloroethane 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 563-58-6 1,1-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 56-23.5 Carbon Tetrachloride 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 71-43.2 Benzene 0.25 Not detected ug/L EPAS030/62418260 10/10113 VANDREWS 74-953 Dibromomethane 1.0 Not detected ug/L EPA50301624/8260 10/10113 VANDREWS 78-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPA5030162418260 10110113 VANDREWS 7s-0I-6 Tdchloroethene 0.25 Not detected ug/L EPA5030/62418260 10/10113 VANDREWS 75-27-4 Bromodichloromethane 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 10061-01-5 cis-1,3-Dichloropropane 0.25 Not detected uglL EPA50301624/8260 10/10/13 VANDREWS 10061-02-6 trans-1,3-Dichloropropene 0.25 Not detected uglL EPA50301624/8260 10/10/13 VANDREWS 79-00-5 1,1,2-Trichloroethane 0.25 Not detected ug/L EPA50301624/8260 10110/13 VANDREWS 108-88-3 Toluene 0.25 Not detected ug/L EPA50301624/8260 10110/'13 VANDREWS 142-28-9 1,3-Dichloropropane 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 124-48-1 Dibromochloromethane 0.50 Not detected ug/L EPA50301624IB260 10/10/13 VANDREWS 106-93-4 (EDB)1,2-Dibromoethane 0.50 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 127-18-4 Tetrachloroethene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 108-90-7 Chlorobenzene 0.25 1.6 ug/L EPA5030/624/8260 10/10113 VANDREWS 100-41-4 Ethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-25-2 Bromoform 1.0 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 108-38-3 m,p-Xylene 1.0 Not detected uglL EPA5030/624/8260 10110/13 VANDREWS 100-42.5 Styrene 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 79-34-5 1,1,2,2-Tetrachloroethane 0.25 Not detected ug/L EPA50301624/8260 10/10113 VANDREWS 630-20.6 1,1,1,2-Tetrachloroethane 0.25 Not detected ug/L EPA50301624/8260 10/10t13 VANDREWS 95-47.6 o-Xylene 0.25 Not detected ug/L EPAS0301624/8260 10/10/13 VANDREWS 96-18-4 1,2,3-Trichloropropane 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 98-82-8 Isopropylbenzene 0.25 0.30 ug/L EPA50301624/8260 10/10/13 VANDREWS 108-86-1 Bromobenzene 0.25 Not detected ug/L EPA5030/624/8260 10110/13 VANDREWS 103-65.1 n-Propylbenzene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 9549-8 2-Chlorotoluene 0.25 Not detected ug/L EPAS030/624/8260 10/10/13 VANDREWS 10643-4 4-Chlorotoluene 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 108-67-8 1,3,5-Tdmethylbenzene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 98-06.6 tert-Butylbenzene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 95-63-6 1,2,4-Trimethylbenzene 0.25 Not detected uglL EPA5030162418260 10/10/13 VANDREWS Laboratory SecOon» 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 7333908 For a debled deunptim of teequel fercodes refer to Page 2 of 3 .NCORAk Ga5oratory Section PS ru&s Location ID: 1P69COATSMWI2 Sample ID: AC01050 Collect Date: 10/08/2013 Collect Time:: 10:32 VUL CAS AtReResult/Method 135-98-8 Analvte Name sec-Butylbenzene PAL 0.25 Qualifier Not detected Units ug/L Reference EPA50301624/8260 Analysis Date 10/10113 Validated by VANDREWS 541.73-1 m-Dichlorobenzene (1,3) 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 10646-7 p-Dichlorobenzene (1,4) 0.25 0.51 ug/L EPA5030162418260 10/10113 VANDREWS 95-50-1 o-Dichlorobenzene (1,2) 0.25 0.71 ug/L EPA50301624/8260 10/10/13 VANDREWS 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA5030162418260 10/10113 VANDREWS 104-51-8 n-Butylbenzene 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 96-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 120-82-1 1,2,4-Trichlorobenzene 0.50 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 91-20-3 Naphthalene 0.50 Not detected ug/L EPA50301624/6260 10/10/13 VANDREWS 87-68-3 He%achlorobutadlene 0.50 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 87-61-6 1,2,3-Trichlorobenzene 1.0 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS Sample Comments analyte(s) failed a LCL in the CV. Laboratory Section 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 7333908 For a& MOM deuriptim Were qualiterccees refer to Page 3 of 3 AC01104_ NC DllkLa6oratory Section County: MCDOWELL River Basin Report To AROAP Collector. B LAVERTY Region: ARO Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Emergency Yes/No COC Yes/No D- Division of Water Resources Final Report VisitlD Loc. Descr.: Sample ID: AC01104 PO Number# ARO Date Received: 10/09/2013 Time Received: 10:00 Labvrorks LoginlD KJIMISON2 Final Report Date: 10/29/13 Report Print Dale: 10/292013 II Locafion ID: 1p59cOA-rsMWI2 I Collect Dale: 1010812013 I CollectTlme: 10:32 I Sample Depth I If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. CAS # Analyte Name PQL Result/Method Units Analysis Validated by Qualifier Reference Date Others Sample temperature at receipt by lab 1.7 °G 10/9H3 RBYRD Turbidity 1 150 NTU APHA2130B.20th 10/10/13 CGREEN Residue Suspended In liquid 6.2 18 mg/L APHA2540D-20th 10/10/13 CGREEN Laboratory Section 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 7333908 Fored IW descripaen of Ne4uelifercodmreferto Page 1 of 1 vvt 1 wo auararory ve t7on lwrud e I County: McDOWELL WgTF9 Sample ID: AC00649 River Basin OF QG PO Number # 13G0784 Report To AROAP \Q� r� Date Received: 0912512013 >_ "i Time Received: 1 08:16 Collector. B LAVERTY O Y i Latrxorks Loginl0 MSWIFT Region: ARO Final Report Dale: 10/16/13 Sample Matdx: GROUNDWATER I Final Report Report Print Date: 11/1512013 Loa Typo: MONITORING WELL Emergency Yes/No Visitlo COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD ROAD MARION, NC Location ID: IP59COATSMWIIR I Collect Date: 09123/2013 Collect Time: 12:30 Sample Depth If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes Result/Method Analysis CAS # Analvte Name PgL Units Validated by ualifier Reference Date LAB Sample temperature at receipt by lab 1.6 C 9/25113 HMORGAN MIC Turbidity 1.0 1 U NTU APHA21308-20th 9/25/13 ESTAFFORDI WET Residue -Suspended In liquid 6.2 6.20 mg/L APHA2540D-20th 9/26/13 CGREEN MET 744D-22-4 Ag by ICPMS 1.0 1.0 U ug/L EPA 200.8 10/1/13 ESTAFFORDI 7429-90.5 At by ICP 50 50 U ug/L EPA 200.7 10/3113 ESTAFFORD1 7440-38-2 As by ICPMS 2.0 2.0 U ug/L EPA 200.8 10/1113 ESTAFFORD1 7429-90-5 B by ICP 50 50 U ug/L EPA 200.7 10/3113 ESTAFFORD1 7440-38-3 Ba by ICP 10 39 ug/L EPA200.7 10/3/13 ESTAFFORD1 7440-70-2 Ca by ICP 0.10 38 mg/L EPA200.7 10/3113 ESTAFFORD1 7440-43-9 Cd by ICPMS 0.50 0.50 U ug/L EPA 200.8 10/1113 ESTAFFORDI 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA 200.8 1011113 ESTAFFORDI 7440-50-8 Cu by ICPMS 2.0 2.00 ug/L EPA 200.8 10/1/13 ESTAFFORDI 7439-89-6 Fe by ICP 50 50 U ug/L EPA 200.7 1013113 ESTAFFORDI 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA245.1 10/10/13 ESTAFFORDI 7440-09-7 K by ICP 0.10 2.2 mg/L EPA200.7 1013/13 ESTAFFORDI 7439-95-4 Mg by ICP 0.10 17 mg/L EPA200.7 10/3/13 ESTAFFORD1 7439-96-5 Mn by ICPMS 10 IOU ug/L EPA200.8 1013/13 ESTAFFORD1 7440-23-5 Na by ICP 0.10 17 mg/L EPA 200.7 1013113 ESTAFFORD1 7440-02-0 Ni by ICPMS 2.0 2.0 U ugr- EPA 200.8 1011113 ESTAFFORDI 7439-92-1 Pb by ICPMS 2.0 2.0 U ug/L EPA 200.8 1011/13 ESTAFFORDI 778249.2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 1011113 ESTAFFORD1 7440-28-0 Thallium (TI) ICPMS 2.0 2.0 U ug/L EPA 200.8 101V13 ESTAFFORD1 7440-66-6 Zn by ICPMS 10 IOU ug/L EPA200.8 10/1113 ESTAFFORD1 VOL 7440-50-8 Volatile Organics in liquid _TITLE_ ug/L EPA50301624/8260 9125113 VANDREWS 75-71-8 Dichlorodiflueromethane 1.0 Not detected ug/L EPA5030162418260 9/25/13 VANDREWS 74-87-3 Chloromethane 1.0 Not detected ug/L EPA5030/62418260 9125113 VANDREWS 75-01-4 Vinyl Chloride 0.50 Not detected J2 ug/L EPA5030162418260 9125113 VANDREWS Laboratory section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Forede Mdeec WndlN qud4fermdde relerlp a e lann na. n5..a m i Page 1 of 3 .NC (DI+Q La6oratory Section 'Pfsufts Location ID: IP69COATSMWIIR Sample 10: A000649 Collect Date: 0912312013 Collect Time:: 12:30 VOL ResulU Method Analysis CAS # Analvte Name P(�L Units Validated by Qualifier Reference Date 74-83.9 Bromomethane 1.0 Not detected uglL EPA5030162418260 9/25113 VANDREWS 75-00-3 Chloroethane 0.50 Not detected ug/L EPA5030162418260 9125113 VANDREWS 75-69-4 Trichlorofluoromethane 0.50 Not detected ug/L EPA5030/62418260 9125113 VANDREWS 75-35.4 1,1-Dichloroethene 0.25 Not detected J2 ug/L EPA5030/62418260 9125/13 VANDREWS 75-09-2 Methylene Chloride 10 Not detected ug/L EPA50301624/8260 9125113 VANDREWS 156-60-5 trans-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030162418260 9/25/13 VANDREWS 1634-044 Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPA5030/62418260 9125/13 VANDREWS 75-34-3 1,1-Dichloroethane 0.25 Not detected ug/L EPA50301624/8260 9/25/13 VANDREWS 156-59-2 cis-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 9125113 VANDREWS 74-97-5 Bromochloromethane 0.25 Not detected ug/L EPA50301624/8260 9125113 VANDREWS 67-66-3 Chloroform 0.25 Not detected ug/L EPA5030/624/6260 9125/13 VANDREWS 594-20-7 2,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 9125/13 VANDREWS 107-06-2 1,2-Dlchloroelhane 0.25 Net detected ug/L EPA5030162418260 9/25/13 VANDREWS 71-55.6 1,1,1-Trichleroethane 0.25 Not detected ug/L EPA5030162418260 9125113 VANDREWS 563-58-8 1,1-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 9/2SM3 VANDREWS 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L EPA5030162418260 9125113 VANDREWS 7143-2 Benzene 0.25 Not detected ug/L EPA5030/62418260 9/25113 VANDREWS 74-95-3 Dibromomethane 1.0 Net detected ug/L EPA5030/62418260 9125113 VANDREWS 78-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPA50301624/8260 9125113 VANDREWS 79-01-6 Trichloroethene 0.25 Not detected ug/L EPA50301624/8260 9/25113 VANDREWS 75-27-4 Bromodichloromethane 0.25 Not detected ug/L EPA5030162418260 9125113 VANDREWS 10061-01-5 cis-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/62418260 9125113 VANDREWS 10061-02-6 trans-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 9/25113 VANDREWS 79-00-5 1, 1,2-Trichloroethane 0.25 Not detected ug/L EPA5030/62418260 9125113 VANDREWS 108-88-3 Toluene 0.25 Not detected ug1L EPA5030/024/8260 9/25/13 VANDREWS 142-28-9 1,3-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 9/25113 VANDREWS 12448-1 Dibromochloromethane 0.50 Not detected ug/L EPA5030/624/8260 9/25113 VANDREWS 106.93-4 (EDB)1,2-Dibromoethane 0.50 Not detected ug/L EPA5030/624/8260 9/25113 VANDREWS 127-18-4 Tetrachloroethene 0.25 Not detected ug/L EPA5030/62418260 9125/13 VANDREWS 108-90-7 Chlorobenzene 0.25 Not detected ug/L EPAS030/624/8260 9125113 VANDREWS 100-41-4 Ethylbenzene 0.25 Not detected uglL EPA50301624/8260 9125113 VANDREWS 75-25-2 Bromoform 1.0 Not detected ug/L EPA5030/62418260 9/25113 VANDREWS 108-38-3 m,p-Xylene 1.0 Net detected ug1L EPA50301624/8260 9125113 VANDREWS 100-42-5 Styrene 0.25 Not detected ug/L EPA5030/624/8260 9125113 VANDREWS 79-34-5 1, 1,2,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 9/25113 VANDREWS 630-20.6 1,1, 1,2-Tetrachloroethane 0.25 Not detected ug/L EPA50301624/8260 9125113 VANDREWS 95-47-6 O-Xylene 0.25 Not detected ug/L EPA5030162418260 9/25113 VANDREWS 96-184 1,2,3-Tdchloropropane 0.25 Not detected ug/L EPA5030162418260 9125/13 VANDREWS 98.82-8 Isoprepylbenzene 0.25 Not detected ug/L EPA50301624/8260 9125/13 VANDREWS 108-66-1 Bromobenzene 0.25 Not detected uglL EPA5030/624/8260 9/25113 VANDREWS 103-65-1 n-Propylbenzene 0.25 Not detected ug/L EPA50301624/8260 9125113 VANDREWS 95-49-8 2-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 9125/13 VANDREWS Laboratory Section 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 731J908 Fina de fled desaipWn ofthequaGOercodes referlo G;S.(/� rrr �111-fb Page 2 of 3 NC /D`WiZ, La6oratorySection Rfm(ts I. Location to: 1P69COATSMW11R Sample to: A000649 Collect Date: 0912312013 Collect Time!: 12:30 VOL Result/ Method Analy I is CAS # AnalVte Name PQL Qualifier Units Reference Date Validated by 106-434 4-Chlorotoluene 0.25 Not detected ug/L EPA5030/62418260 9/25/13 VANDREWS 108-67-8 1,3,5-Trimethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 9/251131 VANDREWS 98-06-6 tert-Butylbenzene 0.25 Not detected ug/L EPA50301624/8260 9/25/131 VANDREWS 95-63-6 1,2,4-Thmethylbenzene 0.25 Not detected ug/L EPA5030/62418260 9/25/13i VANDREWS 135-98-8 sec-Butylbenzene 0.25 Not detected ug/L EPA50301624/8260 9/25/131 VANDREWS 541-73-1 m-Dichlorobenzene (1,3) 0.25 Not detected ug/L EPA5030162418260 9/25/131 VANDREWS 10646-7 p-Dichlorobenzene (1,4) 0.25 Not detected ug/L EPA5030/624/8260 9/25/131 VANDREWS 95-50-1 o-Dichlorobenzene (1,2) 0.25 Not detected ug/L EPA50301624/8260 9/25/13 I VANDREWS 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA5030/624/8260 9/25113 VANDREWS 104-51-8 n-Butylbenzene 0.26 Not detected ug/L EPA5030/624/8260 9125113 VANDREWS 96-12.8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA5030/82418260 9/25113 VANDREWS 120-82-1 1,2,4-Trichlofobenzene 0.50 Not detected ug/L EPA5030162418260 9/25113 VANDREWS 91-20-3 Naphthalene 0.50 Not detected Wt. EPA5030162418260 9/25/13 VANDREWS 87-68-3 Hexachlorobutadiene 0.50 Not detected ug/L EPA50301624/8260 9/25/13 VANDREWS 87-61-6 1,2,3-Tdchlorobenzene 1.0 Not detected ug/L EPA50301624/8260 9/25113 VANDREWS Sample Comments .:VOAJ2-esfimated-2 analyte(s) failed < LCL in the CV. Laboratory Section» 1623 Mail Service Center, Raleigh, NO 27699-1623 (919) 733-3908 Fora dH gad deaWp4on e(me 9oaufier codes m(arto hmlLoea9auJ ^ • Page 3 of 3 County: MCDOWELL WATF9 Sample ID: AC01051 River Basin QF PO Number # 13GO813 Report To AROAP ti r Date Received: 10110/2013 O Time Received: 08:11 Collectora LAVERTY Y Labworks LoglnlD MSWIFT Region: ARO Final Report Date: 10/30/13 Sample Matrix: GROUNDWATER Final Report Report Print Date: 11/2112013 Loc. Type: MONITORING WELL Emergency Yes/No Malin) COC Yes/No Loc. Descr.: COATS AMERICAN 630 AMERICAN THREAD ROADD MARION NC Location ID: 1P59COATSMWI3 I Collect Date: 10/0812013 Collect Time: 12:12 Sample Depth If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. Result/ Method Analysis F W" Qualifier Reference Datd LAB Sample temperature at receipt by lab 1.7 'C 10/10/13 HMORGAN MET 7440-224 Ag by ICPMS 1.0 1.0 U ug/L EPA 200.8 10/16/13 ESTAFFORDI 7429-90-5 Al by ICP 50 50 U ug/L EPA 200.7 10/21/13 ESTAFFORD1 7440-38-2 AS by ICPMS 2.0 2.0 U ug/L EPA200.8 10/16113 ESTAFFORDI 7429-90-5 B by ICP 50 180 ug/L EPA 200.7 10/24/13 ESTAFFORDI 7440-38-3 Be by ICP 10 79 ug/L EPA 200.7 10/21/13 ESTAFFORDI 7440-70-2 Ca by ICP 0.10 27 mg/L EPA 200.7 10/21/13 ESTAFFORD1 7440-43-9 Cd by ICPMS 0.50 0.50 U ug/L EPA200.8 10/16/13 ESTAFFORD1 744047-3 Cr by ICPMS 10 IOU ug/L EPA 200.8 10/16/13 ESTAFFORDI 7440-50-8 Cu by ICPMS 2.0 3.4 ug/L EPA 200.8 10/16/13 ESTAFFORDI 7439-89-6 Fe by ICP 50 3500 ug/L EPA 200.7 10/21/13 ESTAFFORDI 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA 245.1 10/18/13 ESTAFFORD1 7440-09-7 Kby ICP 0.10 0.71 mg/L EPA 200.7 10/21/13 ESTAFFORD1 7439-95-4 Mg by ICP 0.10 19 mg/L EPA 200.7 10/21/13 ESTAFFORD1 7439-96-5 Mn by ICP 10 670 ug/L EPA200.7 10/21/13 ESTAFFORDI 744D-23-5 Na by ICP 0.10 89 mg/L EPA 200.7 10/21113 ESTAFFORDI 7440-02-0 Ni by ICPMS 2.0 2.8 ug/L EPA200.8 10/22/13 ESTAFFORDI 7439-92-1 Pb by ICPMS 2.0 2.0 U ug/L EPA200.8 10/16/13 ESTAFFORD1 778249-2 Se by ICPMS 5.0 5.0 U ug/L EPA200.8 10/16/'13 ESTAFFORDI 7440-28-0 Thallium (TI) ICPMS 2.0 2.0 U ug/L EPA 200.8 10/16/13 ESTAFFORDI 7440-66-6 Zn by ICP 10 13 ug/L EPA 200.7 10/21/13 ESTAFFORD1 VOL Volatile Organics in liquid _TITLE_ ug/L EPA5030/62418260 10/10/13 VANDREWS 75-71-8 Dichlorodifluoromethane 1.0 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 74-87-3 Chloromethane 1.0 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 75-01-4 Vinyl Chloride 0.50 Not detected J2 ug/L EPA5030/62418260 10/10/13 VANDREWS 74-83-9 Bromomethane 1.0 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 75-00-3 Chloroethane 0.50 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 75-69-4 Trichlorofluoromethane 0.50 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 753r'4 1,1-DIChloroethene 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS Laboratory Section» 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Fore Eelalletl tles[tlp0on of iha qua0fer [titles refarlo � pLw�s/: ,nnnoheaAnfrxpgpiade .fir pp@ Page 1 of 3 NC OWQ La6oratory Section Results I Location ID: IP59COATSMWI3 Sample ID: AC01051 Collect Date: 10/0812013 Collect Time% 12:12 VOL CAS # 75-09-2 Analvte Name Methylene Chloride PAL 10 Result/Units ualifer Net detected ug/L Method Reference EPAS030/62418260 Analysis Date 10/10/13 Validated by VANDREWS 156-50-5 trans-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 1634-044 Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-34-3 1,1-Dlchloroethane 0.25 Not detected ug/L EPA5030/6241826D 10/10/13 VANDREWS 156-59-2 cis-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 74-97-5 Bromochloromethane 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 67-66-3 Chloroform 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 594-20-7 2,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 107-06-2 1,2-Dichloroethane 0.25 Not detected ug/L EPAS030/624/8260 10/10/13 VANDREWS 71-55-6 1,1,1-Triahloroethane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 563.58-8 1,1-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 7143-2 Benzene 0.25 Not detected ug/L EPA5030/624/826D 10/10/13 VANDREWS 74-95-3 Dibromomethane 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 78-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 79-01-6 Trichloroethene 0.25 Not detected uglL EPA5030162418260 10/10/13 VANDREWS 75-27-4 Bromodichloromethane 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 10051-01-5 Cis-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 10061-02-6 trans-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 79-00-5 1,1,2-Trichloroethane 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 108-88-3 Toluene 0.25 Net detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 142-28-9 1,3-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 12448-1 Dibromochloromethane 0.50 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 106-934 (EDB)1,2-Dibromoethane 0.50 Not detected ugh. EPA5030/62418260 10/10/13 VANDREWS 127-184 Tetrachloroethene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 108-90-7 Chlorobenzene 0.25 Net detected ug/L EPA5030162418260 10/10M3 VANDREWS 100-414 Ethylbenzene 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 75-25-2 Bromoform 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 108-38-3 m,p-Xylene 1.0 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 10042-5 Styrene 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 79-34-5 1, 1,2,2-Tetrachloreethane 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 630-20-6 1,1,1,2-Tetrachloreethane 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 95-47-6 o-Xylene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 96-184 1,2,3-Trichloropropane 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 98-82-8 Isopropylbenzene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 108-86-1 Bromobenzene 0.25 Not detected ug/L EPA5030/62418260 10/10113 VANDREWS 103-65-1 n-Propylbenzene 0.25 Net detected ug/L EPA5030/62418260 10/10/13 VANDREWS 95-49.8 2-Chlorotoluene 0.25 Not detected ug/L EPA5030/62418260 10/10H3 VANDREWS 106-434 4-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 108-67-8 1,3,5-Trimethylbenzene 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 98-06-e tert-Butylbenzene 0.25 Not detected ugh. EPA5030/624/8260 10/10/13 VANDREWS 95-63-6 1,2,4-Trimethylbenzene 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 73349DS Far s dMINd der[Aptio of ft 9vallller[odes rd., to lliPiIi 6w Sl .(y+,p1r:'lab'e:WSLHLA3hR-r±oyq,ytyplsiGSAsf �InelLesnal rc.9vnr.we,weeMofzn(n,nnno/mnaay� Page 2 of 3 XC VWQ La6oratory Section Pesuas Locabon ID: 1P59COATSMWI3 Sample ID: AC01051 Called Date: 1010812013 Collect Time:: 12:12 VUL Result/ Method Analysis CAS # AnalVte Name PQL Units Validated by Qualifier Reference Date 135-98-8 sec-Butylbenzene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 541-73-1 m-Dichlorobenzene (1,3) 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 106-46-7 p-Dichlorobenzene (1,4) 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 95-50.1 o-Dichlorobenzene (1,2) 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 104-51.8 n-Butylbenzene 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 96-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA5030162418260 10110/13 VANDREWS 120-82-1 1,2,4-Tdchlorobenzene 0.50 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 91-20.3 Naphthalene 0.50 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 87-68-3 Hexachlorobutadiene 0.50 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS Laboratory Suction» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For addaaed dederc,tcn or the quallfier cod es rotor to e• rWffi Page 3 of 3 County: MCDOWELL River Basin Report To AROAP Collector. B LAVERTY Region: ARO Sample Matrix: GROUNDWATER Loc. Type: MONITORING WELL Emergency Yes/No Visitlo COG Yes/No Loc. Descr.: Sample ID: AC01105 �OPWATFhQ O G PO Number# ARO v� Data Received: 10612013 Y Time Received: 10:00 Labworks LoginlD KJIMISON2 Final Report Date: I 10/29/13 Final Report Report Print Date: 11/2112013 Location ID: 1P59COATSMWI3 Collect Date: 1010812013 Collect Time: 1212 Sample Depth If this report Is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. CAS At Analyte Name Others S Result/Uits Method Analysis Validated by ualifier nReference Date, I Sample temperature at receipt by lab 1.7 'C 1019113 RBYRD Turbidity 1 4.3 NTU APHA2130B-20th 10/10/13 CGREEN Residue —Suspended in liquid 6.2 6.2 U mg/L APHA2540D-20th 10/10/13 CGREEN Laboratory Section» 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 733.3908 Fora dnelbddewipwnortee quefifiercodeafererto Page 1 of 1 County.' MCDOWELL INA)p9 Sample ID: AC01052 River Basin Op QG PO Number# 13GO814 C� Report To AROAP Dale Received: 10110/2013 '1 Time Received: 08:11 Collector: B LAVERTY O '� Labworks Loginl0 MSWIFT Region: ARO Final Report Date: 1 3 Sample Matrix: GROUNDWATER Final Report Report Print Date: 1112V2/21/2013 Loc. T Type: MONITORING WELL Emergency YesfNo MOO CDC Yes/No Loc. Doscr.: COATS AMERICAN 630 AMERICAN THREAD ROADD MARION NC Location ID: 1P69COATSMWI4 I Collect Date: 10/08/2013 I Collect Time: 13:46 Sample Depth If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. Result/ Method Analysis -`- Qualifier Reference Date LAB Sample temperature at receipt by lab 1.7 'C 10110/13 HMORGAN MET 7440-22-4 Ag by ICPMS 1.0 1.0 U ug/L EPA200.8 10/16/13 ESTAFFORDI 7429-90-5 At by ICP 50 320 ugf- EPA200.7 10/21113 ESTAFFORDI 7440-38-2 AS by ICPMS 2.0 2.0 U ug/L EPA 200.8 10/16/13 ESTAFFORDI 7429-90-5 B by ICP 50 180 ug/L EPA 200.7 10/24113 ESTAFFORDI 7440-38-3 Ba by ICP 10 170 ug/L EPA 200.7 10/21/13 ESTAFFORD1 7440-70-2 Ca by ICP 0.10 52 mg/L EPA 200.7 10121/13 ESTAFFORDI 7440-43-9 Cd by ICPMS 0.50 0.50 U ugfL EPA 200.8 10/16/13 ESTAFFORD1 7440-47-3 Cr by ICPMS 10 IOU ugfL EPA 200.8 10116/13 ESTAFFORD1 7440-50-8 Cu by ICPMS 2.0 36 ug/L EPA200.8 10/16/13 ESTAFFORDI 7439-89.6 Fe by ICP 50 4700 ug/L EPA 200.7 10/21/13 ESTAFFORDI 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA 245.1 10/18/13 ESTAFFORDI 7440-09-7 K by ICP 0.10 3.2 mgfL EPA200.7 10/21/13 ESTAFFORDI 7439-954 Mg by ICP 0.10 34 mg/L EPA200.7 10/21/13 ESTAFFORDI 7439-95-5 Mn by ICP 10 530 ug/L EPA 200.7 10/21/13 ESTAFFORD1 7440-23-5 Na by ICP 0.10 100 mg/L EPA 200.7 10121/13 ESTAFFORD1 7440-02-0 Ni by ICPMS 2.0 2.8 ug/L EFA200.8 10/16/13 ESTAFFORD1 7439-92-1 Pb by ICPMS 2.0 12 ug/L EPA200.6 10116/13 ESTAFFORDI 7782-49-2 Se by ICPMS 5.0 5.0 U ug/L EPA 200.8 10/16/13 ESTAFFORDI 7440-26-0 Thallium (TI) ICPMS 2.0 2.0 U ug/L EPA 200.8 10/16/13 ESTAFFORDI 7440-66.6 Zn by ICP 10 19 ug/L EPA 200.7 10/21/13 ESTAFFORDI VOL Volatile Organics in liquid _TITLE_ ugf- EPA5030/62418260 10/10/13 VANDREWS 75-71-8 Dichlorodifluoromethane 1.0 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 74-87-3 Chloromethane 1.0 Not detected uglL EPA5030/62418260 10/10/13 VANDREWS 75-01-4 Vinyl Chloride 0.50 Not detected J2 ug/L EPA5030/624/8260 10/10/13 VANDREWS 74-83-9 Bromomethane 1.0 Not detected ug/L EPA5030162416260 10/10/13 VANDREWS 75-00-3 Chloroethane 0.50 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 75-69-4 Trichlorofluoromethane 0.50 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 75-35-4 1,1-Dichloroethene 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Fmiidetailed dosalpeon of eNe 9uatifiercodas rarer to / •A�� �' S Page 1 of 3 VC /D`WQ La6oratory Section (Bssufts Location to: 1P69COATSMW14 Sample ID: AC01052 Collect Date: 1010812013 Collect Time:: 13:46 VOL CAS # 75-09-2 Analvte Name Methylene Chloride 10 Resulf/ Qualifier Not detected Units ug/L Method Reference EPA5030/624/8260 Analysis Date 10/10/13 Validated by VANDREWS 156-60-5 trans-1,2-DIChloroethene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 1634-04-4 Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPAS030/62418260 10/10/13 VANDREWS 75-34-3 1,1-Dichloroethane 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 156-59-2 Cis-1,2-Dichloroethene 0.25 Not detected ug/L EPA50301624/8260 10110/13 VANDREWS 74-97-5 Bromochloromethane 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 67-66-3 Chloroform 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 594-20-7 2,2-Dichloropropane 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 107-06-2 1,2-Dichloroethane 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 71-55-8 1,1,1-Trichloroethane 0.25 Not detected uglL EPAS030/624/8260 10/10/13 VANDREWS 563.58-6 1,1-Dichloropropene 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 71-43-2 Benzene 0.25 Not detected ug/L EPAS030/624/6260 10/10/13 VANDREWS 74-95-3 Dibromomethane 1.0 Not detected ugA. EPA5030/62418260 10/10/13 VANDREWS 78-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPAS030162418260 10/10/13 VANDREWS 794)1-8 Trichloroethene 0.25 Not detected ug/L EPASD301624/8260 10/10/13 VANDREWS 75-27-4 Bromodichloromethane 0.25 Not detected ug/L EPA50301624/8260 10110/13 VANDREWS 10061-01-5 cis-1,3-Dichloropropene 0.25 Not detected ug/L EPA503D/624/8260 10/10/13 VANDREWS 10061-02-6 trans-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 70-00-5 1,1,2-Trichloroethane 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 108-88-3 Toluene 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 142-28-9 1,3-Dichloropropane 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 124-48-1 Dibromochloromethane 0.50 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 106-93-4 (EDB)1,2-Dibromoethane 0.50 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 127-18-4 Tetrachloroethene 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 108-90-7 Chlorobenzene 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 100-41-4 Elhylbenzene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 75-25-2 Bromofonn 1.0 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS 108-38-3 m,p-Xylene 1.0 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 100-42-5 Styrene 0.25 Not detected ug/L EPAS030/624/8260 10/10/13 VANDREWS 79-34-5 1,1,2,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 10/10113 VANDREWS 630-20-6 1,1,1,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 9547-6 o-Xylene 0.25 Not detected ug/L EPA5030/624/8260 10/10113 VANDREWS 95-18-4 1,2,3-Trichloropropane 0.25 Not detected ug/L EPA5030/024/8260 10/10/13 VANDREWS 9M2-8 Isopropylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 108-88-1 Bromobenzene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 103-8S-1 n-Propylbenzene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 95-49-8 2-Chlorotoluene 0.25 Not detected ug/L EPAS0301624/8260 10/10/13 VANDREWS 106-43A 4-Chlorotoluene 0.26 Not detected ug/L EPAS030/624/8260 10/10/13 VANDREWS 108-67-8 1,3,5-Trimelhylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 98-08.6 tert-Butylbenzene 0.26 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 95-63-6 1,2,4-Trimethylbenzene 0.25 Not detected ug/L EPA5030162418260 10/10/13 VANDREWS Laboratory Section>> 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 733-3908 ForaddlaitM&wptbnot Ne quau0er cones relertn hLty!-aublrt4sc ew/r.¢A6�yla *� nY1e Page 2 of 3 . NC (D WQ La6oratorySection %m(ts Location ID: 1P59COATSMWI4 Sample ID: AC01052 Collect Date: 1010812013 Collect Time:: 13:46 VOL CAS # 135-98-8 Analvte Name sec-Butylbenzene PQL 0.25 Result/ Qualifier Net detected Units ug/L Method Reference EPA5030/624/8260 Analysis Date 10/10/13 Validated by VANDREWS 541-73-1 m-Dichlorobenzene (1,3) 0.26 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 106-48-7 p-Dichlorobenzene (1,4) 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 95-50-1 o-Dichlorobenzene (1,2) 0.26 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 89-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 104-51-6 n-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 10/10/13 VANDREWS 96-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 120-82-1 1,2,4-Tdchlorobenzene 0.50 Not detected ug/L EPA50301624/8260 10/10/13 VANDREWS 91-20-3 Naphthalene 0.50 Not detected uge- EPA50301624/8260 10/10/13 VANDREWS 87-68-3 Hexachlorobutadiene 0.50 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS 87-61-6 1,2,3-Tichlorobenzene 1.0 Not detected ug/L EPA5030/62418260 10/10/13 VANDREWS Sample Comments analyte(s) failed < LCL in the CV. Laboratory Section>> 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 733.3908 For a delayed CesmpO of Oa pudfierco0a3 referto is no eerVn Page 3 of 3 County MCDOWELL Sample ID: AC01106 River Basin OF\NAT-E9 Oa pG PO Number 9 ARO Report To AROAP h r Date Received: 1010912013 '1 Time Received: 10:00 Collector. B LAVERTY O Y Labworks LoginlD KJIMISON2 Region: ARO Final Report Date: 10/29/13 Sample Matrix: GROUNDWATER Final Report Report Print Dale: 11/21/2013 Loc. Type: MONITORING WELL Emergency Yes/No VlsitlD CDC Yes/No Loc. Descr.: Location ID: 1P59COATSMWI4 I Collect Date: 1010812013 Collect Tlme: 13:45 Sample Depth If this report is labeled preliminary report the results have not been validated. Do not use for Regulatory purposes. CAS # Analvte Name Pam( L_ Result/ Units metriotl Analysis validated by ualifier Reference Date Others Sample temperature at receipt by lab 1.7 °C 10/9113 RBYRD Turbidity 1 20 NTU APHA21306-20th 10/10/13 CGREEN Residue —Suspended In liquid 6.2 40 mg/L APHA2540D-20th 10/10/13 CGREEN Laboratory Section 1623 Mail Service Canter, Raleigh, NC 27699.1623 (919) 733-3908 Fw a deleted aesodpoon or the 9uetfier codes rotor to Me//e ,y M• �- Page 1 of 1