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aceAnalytical
www.pacelabs.cm
October 04, 2021
Kaline Davis
Covanta Environmental Solutions
2503 N. Fayetteville St.
Asheboro, NC 27203
RE: Project: MONTHLY TESTING GW
Pace Project No.: 92563284
Dear Kaline Davis:
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Enclosed are the analytical results for sample(s) received by the laboratory on September 24, 2021. The results relate only
to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless
otherwise footnoted.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services -Asheville
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyler Forney
tyler.forney@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: RANDY ATKINS, COVANTA ENV. SOL
Vicki Zamudio
REPORT OF LABORATORY ANALYSIS
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Project: MONTHLY TESTING GW
Pace Project No.: 92563284
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TNO0003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TNO0003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TNO0003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: A130792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification M M-TNO03
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TNO0003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TNO02
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification M R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification M TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LA000356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DWIChem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification M LABO152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TNO0003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification M 998093910
Wyoming UST Certification #: via A21-A 2926.01
A21-A-ISO 17025 Certification #: 1461.01
A21-A-ISO 17025 Certification #: 1461.02
AIHA-LAPILLC EMLAP Certification #:100789
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
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aceAnalj&al
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Project: MONTHLY TESTING GW
Pace Project No.: 92563284
Lab ID Sample ID
92563284001 OUTFALL 1
92563284002 OUTFALL 2
92563284003 OUTFALL 3
PAN = Pace National - Mt. Juliet
PAS I -A = Pace Analytical Services - Asheville
SAMPLE ANALYTE COUNT
Method
EPA 1664E
SM 254OD-2011
EPA 9040C
EPA1664B
SM 254OD-2011
EPA 9040C
EPA 1664B
SM 254OD-2011
EPA 9040C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLG
6701 Conference Ddve
Raleigh, NC 27607
(919)834-4984
Ana lytes
Analysts
Reported
Laboratory
ERK, WAW
2
PAN
MJP
1
PASI-A
SMK
1
PASI-A
ERK, WAW
2
PAN
MJP
1
PASI-A
SMK
1
PASI-A
ERK, WAW
2
PAN
MJP
1
PASI-A
SMK
i
PASI-A
Page 3 of 14
leAnalytical e
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ANALYTICAL RESULTS
Project: MONTHLY TESTING GW
Pace Project No.: 92563284
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Sample: OUTFALL 1
Lab ID: 92563284001 Collected: 09/23/21 10:00
Received: 09/24/21 07:31 Matrix: Water
Parameters
Results Units Report Limit DF
Prepared
Analyzed CAS No. Qual
Wet Chemistry 1664B
Analytical Method: EPA 1664E Preparation Method: 1664E
Pace National - Mt. Juliet
Oil & Grease (Hexane Extr)
ND ug1L 5000 1
10/01/21 09:27
10/01/21 16:14 OG_SGT
Oil and Grease
ND ug1L 5000 1
10/01/21 09:27
10/01/21 18:47
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services -Asheville
Total Suspended Solids
21.6 mg1L 2.5 1
09/30/21 13:06
9040 pH
Analytical Method: EPA9040C
Pace Analytical Services -Asheville
pH at 25 Degrees C
6.7 Std. Units 0.10 1
10/03/21 16:54 H3
Sample: OUTFALL 2
Lab ID: 92563284002 Collected: 09/23/21 10:15
Received: 09/24/21 07:31 Matrix: Water
Parameters
Results Units Report Limit DF
Prepared
Analyzed CAS No. Qual
Wet Chemistry 1664E
Analytical Method: EPA 1664B Preparation Method: 1664B
Pace National - Mt. Juliet
Oil & Grease (Hexane Extr)
ND uglL 5000 1
10/01/21 09:27
10/01/21 16:14 OG_SGT
Oil and Grease
ND uglL 5000 1
10/01/21 09:27
10/01/21 18:47
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services -Asheville
Total Suspended Solids
27.8 mglL 4.2 1
09/30/21 13:06
9040 pH
Analytical Method: EPA9040C
Pace Analytical Services -Asheville
pH at 25 Degrees C
6.4 Std. Units 0.10 1
10/03/21 17:00 H3
Sample: OUTFALL 3
Lab ID: 92563284003 Collected: 09/23/21 10:40
Received: 09/24/21 07:31 Matrix: Water
Parameters
Results Units Report Limit DF
Prepared
Analyzed CAS No. Quaff
Wet Chemistry 1664B Analytical Method: EPA 1664E Preparation Method: 16646
Pace National - Mt. Juliet
Oil & Grease (Hexane Extr) ND ug1L 5000 1 10/01/21 09:27 10/01/21 16:14 OG_SGT
Oil and Grease ND uglL 5000 1 10/01/21 09:27 10/01/21 18:47
2540D Total Suspended Solids Analytical Method: SM 254OD-2011
Pace Analytical Services -Asheville
Total Suspended Solids 7.7 mglL 2.7 1 09/30/21 13:07
REPORT Of LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/04/2021 12:54 PM without the written consent of Pace Analytical Services, LLC.
Page 4 of 14
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Project: MONTHLY TESTING GW
Pace Project No.: 92563284
Sample: OUTFALL 3 Lab ID: 92563284003 Collected: 09/23/21 10:40 Received: 09/24/21 07:31 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
9040 pH Analytical Method: EPA 9040C
Pace Analytical Services -Asheville
pH at 25 Degrees C 6.3 Std. Units 0.10 1 10/03/21 17:12 D6,H3
REPORT OF LABORATORY ANALYSIS
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Date: 10/04/2021 12:54 PM without the written consent of Pace Analyticai Services, LLC. Page 5 of 14
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QUALITY CONTROL DATA
Project: MONTHLY TESTING GW
Pace Project No.: 92563284
QC Batch: 1749796 Analysis Method:
QC Batch Method: 1664E Analysis Description:
Laboratory:
Associated Lab Samples: 92563284001, 92563284002, 92563284003
METHOD BLANK: R3711468-1 Matrix: Water
Associated Lab Samples: 92563284001, 92563284002, 92563284003
Blank Reporting
Parameter Units Result Limit
Oil & Grease (Hexane Extr) ND
EPA 1664B
Wet Chemistry 1664E
Pace National - Mt. Juliet
Analyzed Qualifiers
10/01/21 16:14
Pace Analytical Services, Ll-C
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
LABORATORY CONTROL SAMPLE & LCSD:
R3711468-2
R3711468-3
Spike LCS
LCSD
LCS LCSD
% Rec
Max
Parameter
Units
Conc. Result
Result
% Rec % Rec
Limits
RPD RPD Qualifiers
Oil & Grease (Hexane Extr)
40.0 ND ND
90.5 86.3
78.0-114
4.81 20
MATRIX SPIKE SAMPLE: R3711468-4
L1409732-02
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Oil & Grease (Hexane Extr)
uglL
1470
40000
36100
86.6
78.0-114
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/04/2021 12:54 PM without the written consent of Pace Analytical Services, L.LC.
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I e
Analytical
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QUALITY CONTROL DATA
Project: MONTHLY TESTING GW
Pace Project No.: 92563284
QC Batch: 1750244 Analysis Method:
QC Batch Method: 1664B Analysis Description:
Laboratory:
Associated Lab Samples: 92563284001, 92563284002, 92563284003
METHOD BLANK: R3711517-1 Matrix: Water
Associated Lab Samples: 92563284001, 92563284002, 92563284003
Blank Reporting
Parameter Units Result Limit
Oil and Grease ND
EPA 1664B
Wet Chemistry 1664B
Pace National - Mt. Juliet
Analyzed Qualifiers
10/01/21 18:47
LABORATORY CONTROL SAMPLE & LCSD: R3711517-2 R3711517-3
Spike LCS LCSD LCS LCSD % Rec
Parameter Units Conc. Result Result % Rec % Rec Limits
Oil and Grease 20.0 ND ND 101 90.5 84.0-132
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Max
RPD RPD Qualifiers
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 10/04/2021 12:54 PM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: MONTHLYTESTING GW
Pace Proiect No.: 92563284
QC Batch: 650125 Analysis Method: SM 254OD-2011
QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92563284001, 92563284002, 92563284003
METHOD BLANK: 3409731 Matrix: Water
Associated Lab Samples: 92563284001, 92563284002, 92563284003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg1L ND 2.5 09/30/21 13:05
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
LABORATORY CONTROL SAMPLE: 3409732
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg/L 250 254 102 90-110
SAMPLE DUPLICATE: 3410063
Parameter
Total Suspended Solids
SAMPLE DUPLICATE: 3410064
Parameter
Total Suspended Solids
92563420001 Dup
Units Result Result RPD Qualifiers
mg/L 38.0 37.6 1
92563497001 Dup
Units Result Result RPD Qualifiers
mg/L 286 278 3
Results presented on this page are in the units indicated by the -UnIW" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/04/2021 12:54 PM without the written consent of Pace Analytical Services, LLC.
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Project:
MONTHLY TESTING GW
Pace Project No.:
92563284
QC Batch:
650563
QC Hatch Method:
EPA 9040C
Associated Lab Samples: 92563284001, 92563284002
SAMPLE DUPLICATE: 3412133
Parameter
Units
pH at 25 Degrees C
Std. Units
SAMPLE DUPLICATE: 3412134
Parameter
Units
pH at 25 Degrees C
Std, Units
QUALITY CONTROL DATA
Analysis Method: EPA9040C
Analysis Description: 9040 pH
Laboratory: Pace Analytical Services -Asheville
92562457001 Dup
Result Result RPD Qualifiers
4.8 4.6 3 D6,H3
92562970003 Dup
Result Result RPD Qualifiers
6.3 5.8 9 D6,113
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/04/2021 12:54 PM without the written consent of Pace Analytical Services, LLC.
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Project: MONTHLY TESTING GW
Pace Project No.: 92563284
QC Batch: 650564
QC Batch Method: EPA 9040C
Associated Lab Samples: 92563284003
SAMPLE DUPLICATE: 3412135
Parameter Units
pH at 25 Degrees C Std. Units
QUALITY CONTROL DATA
Analysis Method: EPA 9040C
Analysis Description: 9040 pH
Laboratory: Pace Analytical Services - Asheville
92563284003 Dup
Result Result RPD Qualifiers
6.3 5.9 7 D6,H3
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Results presented an this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/04/2021 12:54 PM without the written consent of Pace Analytical Services, LLC.
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QUALIFIERS
Project: MONTHLY TESTING GW
Pace Project No.: 92663284
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)8344984
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
'Total' may vary slightly from the sum of the reported component parameters.
SAMPLE QUALIFIERS
Sample: 92563284001
[1] Wet Chemistry by Method 1664E - Total Oil&Grease is non -detect. Extract was not processed through silica gel.
Sample: 92563284002
[1] Wet Chemistry by Method 1664B - Total Oil&Grease is non -detect. Extract was not processed through silica gel.
Sample: 92563284003
[1] Wet Chemistry by Method 1664B - Total Oil&Grease is non -detect. Extract was not processed through silica gel.
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
REPORT OF LABORATORY ANALYSIS
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Date: 10/04/2021 12:54 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 14
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: MONTHLY TESTING GW
Pace Project No.: 92563284
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
92563284001
OUTFALLI
1664B
1749796
EPA1664B
92563284001
OUTFALLI
1664B
1750244
EPA1664B
92563284002
OUTFALL 2
1664B
1749796
EPA1664B
92563284002
OUTFALL 2
1664B
1750244
EPA1664B
92563284003
OUTFALL 3
1664B
1749796
EPA1664B
92563284003
OUTFALL 3
1664B
1750244
EPA1664B
92563284001
OUTFALLI
SM 2540D-2011
650125
92563284002
OUTFALL 2
SM 2540D-2011
650125
92563284003
OUTFALL 3
SM 254OD-2011
650125
92563284001
OUTFALLI
EPA 9040C
650563
92563284002
OUTFALL 2
EPA 9040C
650563
92563284003
OUTFALL 3
EPA 9040C
650564
Date: 10/04/2021 12:54 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
1749796
1750244
1749796
1750244
1749796
1750244
Page 12 of 14