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HomeMy WebLinkAboutNCG080839_2021 DMR_20211005W N 0' O N w TI 0 v 3 as a rn 0 Q 0 a n Go m 3 N 3 T7Q ro O C e••f O c c IA cr 3 '•r Q. n as rD 3 O 0 aq m 0 r�• 7 Ol n ro n 77 a3i S rD m m 3 O � Z � W N 3 0 m N ry N cL a m CD CD N M m O. Ln 0i � N 0 m O v N N 0¢ O oa m W m O C CL r 3. rr S 30. O W A V CL O C � 3 o a 0 z �0 0 CL W O 4h 3 O z z z Q. tn a a o Ln � m m 01 ryryQQ Y r m a 7 Z m C a � 90 C et d 0 m O m c m 0 El i Q u+ S io n O O -O s m CU � O N C m = M N ro C r CA �. r m m rt M s n m � C, m ru CL fD c 3 M O o m s d 7 V'7 U� 47 rrn m 9 m W m O N m z O z m m m C m M Ln m H 0 O N m � m m rt 3 4 0 CD 4A CD 3 •o � m o n m O o � �c 0 3 0 y O1 F, m O z A 0 m n 1 z G) n v m fA m m 0 N A O C Z n m m n mm O m n C m n G) m z O z n ul O 00 IC) � as n n m m Gl rrn O Z m O 7o r O m M-1 tG q ElLj o {p "' 0 �3 3 m Ln rt m S R �. C n O ❑ � v m 4A c Cr o. O CD 0 z o s 3 0 �. 0 4� C H� f+ 3 Q a, v 0 O A C =r n � N Gi �p m 1A y O M O 3 z GO O G) o o 0 C O N 0 D O.. 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CD 0) CD N O :U o_ (D O a N 0 3' fl] N 0 O 0)Wlp 0 O x m 61 0 z n r O -C T `m n = m D O m z -< D0 z z D -1 m m Dq m v x m v A m m 0 z D r 0 T rn =!Nn M X Co m m 2 n n r„zD O n x _ m � z n m D m ` - 'on r z T m 2 0 ❑ _ m G� m A n m 0 m m m D m ZF+ K m _ M C > :;o m D m 2 n m LA m rn 0 D Ln m m m m n 0 m m G T 7'1 O D r b r m G) N GI K m m m v x o z D N W rri m m A X - Im n 3 z z O E9 mLA 0 m � m T D � r � n W N ❑ M z O0 nz m jT 0 v m m -4v a m �c fD w rt N m n C+ O CD 3 7 S 3 m 13 •N C. w� LA O rn C m n x m m aceAnalytical www.pacelabs.cm October 04, 2021 Kaline Davis Covanta Environmental Solutions 2503 N. Fayetteville St. Asheboro, NC 27203 RE: Project: MONTHLY TESTING GW Pace Project No.: 92563284 Dear Kaline Davis: Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Enclosed are the analytical results for sample(s) received by the laboratory on September 24, 2021. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace National - Mt. Juliet • Pace Analytical Services -Asheville If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyler Forney tyler.forney@pacelabs.com (704)875-9092 Project Manager Enclosures cc: RANDY ATKINS, COVANTA ENV. SOL Vicki Zamudio REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 14 ceAnalytical www.pjkcalabs.com Project: MONTHLY TESTING GW Pace Project No.: 92563284 Pace Analytical Services National 12065 Lebanon Road, Mt. Juliet, TN 37122 Alabama Certification #: 40660 Alaska Certification 17-026 Arizona Certification #: AZ0612 Arkansas Certification #: 88-0469 California Certification #: 2932 Canada Certification #: 1461.01 Colorado Certification #: TNO0003 Connecticut Certification #: PH-0197 DOD Certification: #1461.01 EPA# TNO0003 Florida Certification #: E87487 Georgia DW Certification #: 923 Georgia Certification: NELAP Idaho Certification #: TNO0003 Illinois Certification #: 200008 Indiana Certification #: C-TN-01 Iowa Certification #: 364 Kansas Certification #: E-10277 Kentucky UST Certification #: 16 Kentucky Certification #: 90010 Louisiana Certification #: A130792 Louisiana DW Certification #: LA180010 Maine Certification #: TN0002 Maryland Certification #: 324 Massachusetts Certification M M-TNO03 Michigan Certification #: 9958 Minnesota Certification #: 047-999-395 Mississippi Certification #: TNO0003 Missouri Certification #: 340 Montana Certification #: CERT0086 Nebraska Certification #: NE-OS-15-05 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Nevada Certification #: TN-03-2002-34 New Hampshire Certification #: 2975 New Jersey Certification #: TNO02 New Mexico DW Certification New York Certification #: 11742 North Carolina Aquatic Toxicity Certification #: 41 North Carolina Drinking Water Certification #: 21704 North Carolina Environmental Certificate #: 375 North Dakota Certification M R-140 Ohio VAP Certification #: CL0069 Oklahoma Certification #: 9915 Oregon Certification M TN200002 Pennsylvania Certification #: 68-02979 Rhode Island Certification #: LA000356 South Carolina Certification #: 84004 South Dakota Certification Tennessee DWIChem/Micro Certification #: 2006 Texas Certification #: T 104704245-17-14 Texas Mold Certification M LABO152 USDA Soil Permit #: P330-15-00234 Utah Certification #: TNO0003 Virginia Certification #: VT2006 Vermont Dept. of Health: ID# VT-2006 Virginia Certification #: 460132 Washington Certification #: C847 West Virginia Certification #: 233 Wisconsin Certification M 998093910 Wyoming UST Certification #: via A21-A 2926.01 A21-A-ISO 17025 Certification #: 1461.01 A21-A-ISO 17025 Certification #: 1461.02 AIHA-LAPILLC EMLAP Certification #:100789 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Page 2 of 14 aceAnalj&al www.paeelahs.com Project: MONTHLY TESTING GW Pace Project No.: 92563284 Lab ID Sample ID 92563284001 OUTFALL 1 92563284002 OUTFALL 2 92563284003 OUTFALL 3 PAN = Pace National - Mt. Juliet PAS I -A = Pace Analytical Services - Asheville SAMPLE ANALYTE COUNT Method EPA 1664E SM 254OD-2011 EPA 9040C EPA1664B SM 254OD-2011 EPA 9040C EPA 1664B SM 254OD-2011 EPA 9040C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLG 6701 Conference Ddve Raleigh, NC 27607 (919)834-4984 Ana lytes Analysts Reported Laboratory ERK, WAW 2 PAN MJP 1 PASI-A SMK 1 PASI-A ERK, WAW 2 PAN MJP 1 PASI-A SMK 1 PASI-A ERK, WAW 2 PAN MJP 1 PASI-A SMK i PASI-A Page 3 of 14 leAnalytical e www.pecdahs.eaa ANALYTICAL RESULTS Project: MONTHLY TESTING GW Pace Project No.: 92563284 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: OUTFALL 1 Lab ID: 92563284001 Collected: 09/23/21 10:00 Received: 09/24/21 07:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Wet Chemistry 1664B Analytical Method: EPA 1664E Preparation Method: 1664E Pace National - Mt. Juliet Oil & Grease (Hexane Extr) ND ug1L 5000 1 10/01/21 09:27 10/01/21 16:14 OG_SGT Oil and Grease ND ug1L 5000 1 10/01/21 09:27 10/01/21 18:47 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services -Asheville Total Suspended Solids 21.6 mg1L 2.5 1 09/30/21 13:06 9040 pH Analytical Method: EPA9040C Pace Analytical Services -Asheville pH at 25 Degrees C 6.7 Std. Units 0.10 1 10/03/21 16:54 H3 Sample: OUTFALL 2 Lab ID: 92563284002 Collected: 09/23/21 10:15 Received: 09/24/21 07:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Wet Chemistry 1664E Analytical Method: EPA 1664B Preparation Method: 1664B Pace National - Mt. Juliet Oil & Grease (Hexane Extr) ND uglL 5000 1 10/01/21 09:27 10/01/21 16:14 OG_SGT Oil and Grease ND uglL 5000 1 10/01/21 09:27 10/01/21 18:47 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services -Asheville Total Suspended Solids 27.8 mglL 4.2 1 09/30/21 13:06 9040 pH Analytical Method: EPA9040C Pace Analytical Services -Asheville pH at 25 Degrees C 6.4 Std. Units 0.10 1 10/03/21 17:00 H3 Sample: OUTFALL 3 Lab ID: 92563284003 Collected: 09/23/21 10:40 Received: 09/24/21 07:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Quaff Wet Chemistry 1664B Analytical Method: EPA 1664E Preparation Method: 16646 Pace National - Mt. Juliet Oil & Grease (Hexane Extr) ND ug1L 5000 1 10/01/21 09:27 10/01/21 16:14 OG_SGT Oil and Grease ND uglL 5000 1 10/01/21 09:27 10/01/21 18:47 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services -Asheville Total Suspended Solids 7.7 mglL 2.7 1 09/30/21 13:07 REPORT Of LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/04/2021 12:54 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 14 aceAnalytical www.pacelabo.com ANALYTICAL RESULTS Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: MONTHLY TESTING GW Pace Project No.: 92563284 Sample: OUTFALL 3 Lab ID: 92563284003 Collected: 09/23/21 10:40 Received: 09/24/21 07:31 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 9040 pH Analytical Method: EPA 9040C Pace Analytical Services -Asheville pH at 25 Degrees C 6.3 Std. Units 0.10 1 10/03/21 17:12 D6,H3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/04/2021 12:54 PM without the written consent of Pace Analyticai Services, LLC. Page 5 of 14 ceAnalytical www.pacel&bs.com QUALITY CONTROL DATA Project: MONTHLY TESTING GW Pace Project No.: 92563284 QC Batch: 1749796 Analysis Method: QC Batch Method: 1664E Analysis Description: Laboratory: Associated Lab Samples: 92563284001, 92563284002, 92563284003 METHOD BLANK: R3711468-1 Matrix: Water Associated Lab Samples: 92563284001, 92563284002, 92563284003 Blank Reporting Parameter Units Result Limit Oil & Grease (Hexane Extr) ND EPA 1664B Wet Chemistry 1664E Pace National - Mt. Juliet Analyzed Qualifiers 10/01/21 16:14 Pace Analytical Services, Ll-C 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 LABORATORY CONTROL SAMPLE & LCSD: R3711468-2 R3711468-3 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Oil & Grease (Hexane Extr) 40.0 ND ND 90.5 86.3 78.0-114 4.81 20 MATRIX SPIKE SAMPLE: R3711468-4 L1409732-02 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil & Grease (Hexane Extr) uglL 1470 40000 36100 86.6 78.0-114 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/04/2021 12:54 PM without the written consent of Pace Analytical Services, L.LC. Page 6 of 14 I e Analytical www.pacelaba.ctaa QUALITY CONTROL DATA Project: MONTHLY TESTING GW Pace Project No.: 92563284 QC Batch: 1750244 Analysis Method: QC Batch Method: 1664B Analysis Description: Laboratory: Associated Lab Samples: 92563284001, 92563284002, 92563284003 METHOD BLANK: R3711517-1 Matrix: Water Associated Lab Samples: 92563284001, 92563284002, 92563284003 Blank Reporting Parameter Units Result Limit Oil and Grease ND EPA 1664B Wet Chemistry 1664B Pace National - Mt. Juliet Analyzed Qualifiers 10/01/21 18:47 LABORATORY CONTROL SAMPLE & LCSD: R3711517-2 R3711517-3 Spike LCS LCSD LCS LCSD % Rec Parameter Units Conc. Result Result % Rec % Rec Limits Oil and Grease 20.0 ND ND 101 90.5 84.0-132 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Max RPD RPD Qualifiers Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 10/04/2021 12:54 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 14 aceAnalytical trww.puefebs.eon QUALITY CONTROL DATA Project: MONTHLYTESTING GW Pace Proiect No.: 92563284 QC Batch: 650125 Analysis Method: SM 254OD-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92563284001, 92563284002, 92563284003 METHOD BLANK: 3409731 Matrix: Water Associated Lab Samples: 92563284001, 92563284002, 92563284003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 09/30/21 13:05 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 LABORATORY CONTROL SAMPLE: 3409732 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 254 102 90-110 SAMPLE DUPLICATE: 3410063 Parameter Total Suspended Solids SAMPLE DUPLICATE: 3410064 Parameter Total Suspended Solids 92563420001 Dup Units Result Result RPD Qualifiers mg/L 38.0 37.6 1 92563497001 Dup Units Result Result RPD Qualifiers mg/L 286 278 3 Results presented on this page are in the units indicated by the -UnIW" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/04/2021 12:54 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 14 aceAnalytical www.patelabs.com Project: MONTHLY TESTING GW Pace Project No.: 92563284 QC Batch: 650563 QC Hatch Method: EPA 9040C Associated Lab Samples: 92563284001, 92563284002 SAMPLE DUPLICATE: 3412133 Parameter Units pH at 25 Degrees C Std. Units SAMPLE DUPLICATE: 3412134 Parameter Units pH at 25 Degrees C Std, Units QUALITY CONTROL DATA Analysis Method: EPA9040C Analysis Description: 9040 pH Laboratory: Pace Analytical Services -Asheville 92562457001 Dup Result Result RPD Qualifiers 4.8 4.6 3 D6,H3 92562970003 Dup Result Result RPD Qualifiers 6.3 5.8 9 D6,1­13 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/04/2021 12:54 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 14 PjceAnalytical WW.pacidabs.com Project: MONTHLY TESTING GW Pace Project No.: 92563284 QC Batch: 650564 QC Batch Method: EPA 9040C Associated Lab Samples: 92563284003 SAMPLE DUPLICATE: 3412135 Parameter Units pH at 25 Degrees C Std. Units QUALITY CONTROL DATA Analysis Method: EPA 9040C Analysis Description: 9040 pH Laboratory: Pace Analytical Services - Asheville 92563284003 Dup Result Result RPD Qualifiers 6.3 5.9 7 D6,H3 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Results presented an this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/04/2021 12:54 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14 aceAnalytrcal www.pacelabs.com QUALIFIERS Project: MONTHLY TESTING GW Pace Project No.: 92663284 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)8344984 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as 'Total' may vary slightly from the sum of the reported component parameters. SAMPLE QUALIFIERS Sample: 92563284001 [1] Wet Chemistry by Method 1664E - Total Oil&Grease is non -detect. Extract was not processed through silica gel. Sample: 92563284002 [1] Wet Chemistry by Method 1664B - Total Oil&Grease is non -detect. Extract was not processed through silica gel. Sample: 92563284003 [1] Wet Chemistry by Method 1664B - Total Oil&Grease is non -detect. Extract was not processed through silica gel. ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H3 Sample was received or analysis requested beyond the recognized method holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/04/2021 12:54 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 14 1aceAnalytical www.paeollbs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: MONTHLY TESTING GW Pace Project No.: 92563284 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92563284001 OUTFALLI 1664B 1749796 EPA1664B 92563284001 OUTFALLI 1664B 1750244 EPA1664B 92563284002 OUTFALL 2 1664B 1749796 EPA1664B 92563284002 OUTFALL 2 1664B 1750244 EPA1664B 92563284003 OUTFALL 3 1664B 1749796 EPA1664B 92563284003 OUTFALL 3 1664B 1750244 EPA1664B 92563284001 OUTFALLI SM 2540D-2011 650125 92563284002 OUTFALL 2 SM 2540D-2011 650125 92563284003 OUTFALL 3 SM 254OD-2011 650125 92563284001 OUTFALLI EPA 9040C 650563 92563284002 OUTFALL 2 EPA 9040C 650563 92563284003 OUTFALL 3 EPA 9040C 650564 Date: 10/04/2021 12:54 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Batch 1749796 1750244 1749796 1750244 1749796 1750244 Page 12 of 14