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HomeMy WebLinkAboutWQ0036723_Modification_20210922Initial Review Reviewer Thornburg, Nathaniel D Is this submittal an application? (Excluding additional information.)* r Yes r No Permit Number (IR)* WQ0036723 Applicant/Permittee Town of Mooresville Applicant/Permittee Address 369 Johnson Dairy Rd , Mooresville NC 28115 Is the owner in BIMS? r Yes r No Is the facility in BIMS? r Yes r No Owner Type Municipal Facility Name Town of Mooresville DCAR County Iredell Fee Category Major Fee Amount $395 Is this a complete application?* r Yes r No Complete App Date 09/16/2021 Signature Authority Signature Authority Title Signature Authority Email Document Type (if non -application) Email Notifications Does this need review bythe hydrogeologist?* r Yes r No Regional Office CO Reviewer Admin Reviewer Below list any additional email address that need notification about a new project. Email Address Comments to be added to email notfication Comments for Admin Comments for RO Comments for Reviewer Comments for Applicant Submittal Form Project Contact Information Rease provide information on the person to be contacted by N B Staff regarding electibnittal, confirmation of receipt, other .......................................................... electronic surece, aner correspondence. _ - Name * James Levis Email Address* jlevis@mooresvillenc.gov Phone Number* 7046638341 Project Information ........ ..................................................................................................................................................... ......... ............ .... .... ........ ... ... .... .... .... ... ... ... .... .... .... ... .... .... ......... ...... Application/Document Type* r New (Fee Req ui red) c Modification - Major (Fee Required) r Renewal with Major Modification (Fee Required) r Annual Report r Additional Information r Other O Modification - Minor C Renewal C GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 r Residual Annual Report r Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* r Wastewater Irrigation r High -Rate Infiltration r Other Wastewater r Reclaimed Water r Closed -Loop Recycle r Residuals r Single -Family Residence Wastewater r Other Irrigation Permit Number:* WO0036723 Fbs Current Existing pernit number Applicant/Permittee * Town of Mooresville Applicant/Permittee Address* 369 Johnson Dairy Rd , Mooresville NC 28115 Facility Name * Town of Mooresville DCAR Please provide comments/notes on your current submittal below. The Town of Mooresville wishes to modify our Distribution of Class A residuals permit to increase our maximum residuals distribution from 900 Dry Tons/year to 1600 Dry Tons/year. In this application package, we believe that all the requested information has been provided. If additional information is needed, please see contact info at the bottom of this letter. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form Engineering Rans, Spedications, Calculations, Bc.) Class A mod whole scan.pdf 25.59MB upload only 1 RJFdocurnert (less than 250 M3). Mafliple documents rust be corrbined into one RDFfile unless file is larger than upload lirit. * W By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date 9/8/2021 To: NCDWQ/AQtJIFER PROTECTION SECTION/LAND APPLICATION UNIT Re: Modification for Class A Distribution Permit - Permit# WQO�036723 The Town of Mooresville wishes to modify our Distribution of Class A residuals permit to increase our maximum residuals distribution from 900 Dry Tons/year to 1600 Dry Tons/year. In this application package, we believe that all the requested information has been provided, If additional information is needed, please see contact info at the bottom of this letter. Please see the attached documents referenced in the application, one original and two copies. A check in the amount of $395.00 made payable to NCDEQ. Completed Distribution of Class A Residuals (DCAR 06-16) form. Attachment t - Program inforination and flow diagram Attachment 2 - Marketability Statement Attachment 3 — Product label/information sheet. Attachment 4 — Operation and Maintenance Plan. Completed Residuals Source Certification (RSC 06-16) form Attachment 5 — Vicinity Map. Attachment 6 — Quantitative justification statement. Attachment 7 — Sampling Plan. Attachment 8 — Laboratory analytical data. Thank you for your time and consideration. Allison Kraft, Utilities Director Phone 704-799-4066 Jamie Levis, WWTP Plant Manager Phone 704-662-8341 Larry Hendren, WWTP Biosolids Coordinator Phone 704-799-4063 1 lene. --goA/. State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS INSTRUCTIONS FOR FORM: DCAR 06-16 & SUPPORTING DOCUMENTATION Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the ADDlicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting,5ection's Lon-DLY�hat' Per naittin�sx ChitIve.&qtg General — This application is for treatment, storage, transport, distribution, land application, and/or marketing of Class A (or Equivalent} residuals under 115AA -NC CQ r',1100. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Distribution of Class A Residuals (FORM: DCAR 06-16): Submit the completed and appropriately executed Distribution of Class A Residuals (FORM: DCAR 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer, Z The project name should be consistent on the plans, specifications, etc, Z The Applicant's Certification on Page 3 of this form shall be signed in accordance with 15A "" C NCA02T.0 1 Qom. An alternate person may be designated as the signing official if a delegation letter, is provided from a person who meets the criteria in 15A T LCA;C 02T ,o LQ0LbJ. Z If this project is for a modification of an existing permit, submit one copy of the existing permit. Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units. B. Application Fee (New and Major Modification Application Packages) N Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental Quality (NCDEQ). Facility Classification Major (residuals permitted for distribution >— 3,000 dry tons/year) I Minor (residuals permitted for distribution < 3,000 dry tons/year) New Permit $1,310 ME Major Modification $395 $245 ' - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage; adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted. There is no fee for minor permit modifications. C. Cover Letter (All Application Packages) Z I,ist all items included in the application package, as well as a brief description of the requested permitting action, INSTRUCTIONS FOR FORM: DCAR 06-16 Page] of3 D. Program Information (All Application Packages) Provide a narrative explaining the following: Z How the materials will be handled and transported from where the residuals were produced to where it will be treated. How the residuals will be processed/treated (attach process flow diagram). How leachate collection will be handled. Where the residuals will be stored until processed, How the final product will be distributed (packaging, bulk, etc.) What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality. Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed. Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following information: Name and address of the person who prepared the residual that is sold or given away. A statement that application of the residuals to the land shall be in accordance with the instructions on the label or information sheet. Z A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered. Z A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored residuals into any surface waters. Z Information on all applicable setbacks in accordance with 15A NCAC 02T, I 108(b). [g A statement that the residuals shall be applied at agronomic or recommended rates for intended uses, E. Detailed Plans and Specifications (Application Involving New or Changes to Treatment or Storage Units) El Submit detailed plans and specifications that have been signed, sealed, and dated by a NC Professional Engineer per .15A ' NC AC 02T .1 104(q). Specifications for standard equipment may only be omitted for municipalities with approved standard specifications, but use of the standard specifications must be noted on each sheet of the plans. El Plans must include the following minimum items: a general location map, a topographic map, plan and profile view of the residuals treatment and storage units as well as the proximity of the residuals treatment and storage units to other utilities and natural features within 500 feet of all treatment and storage facilities, and detail drawings of all items pertinent to the residuals treatment and storage units. Depict minimum separations required in 15A NCAC 02T . I-L081q) on the plans, El Specifications must include, at a minimum, the following for all items pertinent to residuals treatment and storage units: description of materials to be used, methods of construction, quality of construction testing procedures to ensure the integrity of the final product in accordance with 15 A NCAC 02T .1 104(a)(2)(13), including leakage and pressure testing as appropriate, E] Plans and specifications must not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR CONSTRUCTION, etc.) that indicate that they are anything other than final plans and specifications. However, the plans and specifications may be labeled with the phrase: FINAL DESIGN — NOT RELEASED FOR CONSTRUCTION. F. Engineering Calculations (Application Involving Now or Changes to Treatment or Storage Units) El Submit all design calculations that have been signed, sealed, and dated by a NC Professional Engineer per .1 5A NCAC 02T _L104U G. Environmental Assessments (May be Required — See 15A ­C NAQ IC,0300) Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for the construction. of the subject facilities. INSTRUCTIONS FOR FORM: DCAR 06-16 Page 2 of 3 H. Operation and Maintenance Plan (New and Renewal Application Packages) EJ For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan. Submit the O&M Plan in accordance with 15A N - CAC 02T I I - 10 and include at a minimum: Operational functions; describe the operation of the program to show what operations are necessary for the program to function and by whom the functions are to be conducted. Maintenance schedules; may include equipments calibration, maintenance of signs, etc. Safety measures; may include safety training program, manuals, signs, etc. Z Spill response plan; including control, containment, remediation, emergency contact information, etc. Z Inspection plan including the following information; Z Names and titles of personnel responsible for conducting the inspections. Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program. Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed. Sampling and monitoring plan including the following information; Names and titles of personnel responsible for conducting the sampling and monitoring. Detailed description of monitoring procedures including parameters to be monitored. Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures, ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS: F _E31"T T", 7T171 TAL 1�14ALITI DIVISION OF WATER RESOURCES WATER QUALITY PERMITTING SECTION NON -DISCHARGE PERMITTING UNIT By U.S. Postal Service: 1617 MAIL SERVICE CENTER RALEIGH, NORTH CAROLINA 27699-1617 TELEPHONE NUMBER: (919) 807-6464 By Courier/Special Delivery: 512 N. SALISBURY STREET RALEIGH, NORTH CAROLINA 27604 FAX NUMBER: (919) 807-6496 INSTRUCTIONS FOR FORM: DCAR 06-16 Page 3 of 3 I. APPLICANT INFORMATION: 1. Applicant's name: Town of Mooresville Applicant type: El Individual M Corporation M General Partnership M Federal M State Municipal 0 County Signature authority's name per .1 5A NCAC 02T,0 106: Title: Applicant's mailing address: PO Box 878 City: Mooresville State: NC Zip: 28115 Telephone number: Email Address: 2. Consultant's name: License Number (for P.E,): Affiliation: [] On Staff Retained (Firm: Consultant's mailing address: - City: - State., Zip. Telephone number: (—) = Email Address: 3. Fee submitted: $395.00 (See Instruction B) M Privately -Owned Public Utility 1. Application is for (check all that apply):E] new, Z modified, El renewed permit 1 If this application is being submitted to renew or modify an existing permit, provide the following: Permit number: WQ0036723 Date of most -recently issued pen -nit: 10/7/2013 Date of most -recently certified Attachment A (if different than the permit): 1. Name of residuals processing facility: Rocky River Wastewater Treatment Facility City: Mooresville State: NC Zip: 28115- Coordinates: Latitude: 35' 3 1'33 Longitude; 80' 46'56" Datum: Level of accuracy: Method of measurement: QPS County where facility is located- Iredell 2. Facility contact (person familiar with residuals preparation): Name: Larry Hendren Title: Biosolids, Coordinator Mailing address: PO Box 878 City: Mooresville State: NC Zip: 28115- Telephone number: (104) 799-4063 E-mail address: Iliendren@mooresvillene.gov FORM: DCAR 06-16 Page I of 3 3. Is the residual process facility also the generator? 0 Yes; [:] No If No, please specify delivery frequency and quantity of residual to be processed: 4. Length of residuals storage at facility: 180 days (Note: the Division requires minimum 30 days storage in units that are separate from treatment system, i,e, not in clarifiers, aeration basins, etc.) IV. RESIDUALS QUALITY INFORMATION: Specify how these residuals will be distributed: El sold or given away in bags or other containers; [I lawn (bulk); home garden (bulk); Z other (explain); local farms for non-food cr_qps Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a load capacity of one metric ton or less. 2. Complete the following if residuals are to be mixed with other materials: 3 Approximate amounts of the residuals received and processed at the facility: 1600 dry tons per year. 4. Approximate amounts of the final product (processed residuals) to be distributed: 1600 dry tons per year. 5, Provide a description of the onsite storage management plan for the treated residuals (including estimated average and maximum storage times prior to distribution): Mora e-is on a covered, and paved pad with dimensions I I F x 79' Average storage time as �60d s. 1vlaximum story getime 180 days. 6. Does the facility have a stormwater management plan? Z Yes; [] No Explain whether the treatment and storage areas are under roof or how storinwater runoff will be handled: Storage area is under pgrmenant steel erected roof Pad .isalso slg2pd in the event of water intrusion so that the runoffwould be directed to a drainage line that goes back to the head of the_plant, V. RESIDUALS SOURCE INFORMATION- (Required for all new, renewed, or modified residuals source) Complete and submit the attached Residuals Source Certification and all associated documentation, Residuals Source Certification FORM: DCAR 06-16 Page 2 of 3 Professional Engineer's Certification: (Application Involving Now or Changes to Treatment or Storage Units) attest that this application for has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed this material and have judged it to be consistent with the proposed design. North Carolina Professional Engineer's Seal, Signature, and Date: Applicant's Certification: The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T.0 105. QkYes F-1 No, Explain;_ A -A Jr IVV k-lp llvq,�A 4,1 (Signature Authority's Name — PLEASE PRINT) (Title) 11(1— e-t-- Y. attest that this application for O-U1V- K a I (Facility Name) has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or, the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Resources should condition of this permit be violated. I also understand that if all required parts of this application are not completed and that if all required supporting information and attachments are not included, this application package will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes §143-215.6A and §143-215.613, any person who knowingly makes any false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to exceed. $ 10,000 as well as civil penalties tip to $25,000 per violation. Signature. Date: FORM: DCAR 06-16 Page 3 of 3 State of North Carolina WIT"M mlirtymNT Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 0646 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicantshall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's lvoil-Disc&jr&.. Perinitting Unit General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T, I 100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SIR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 11-15): Z Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. For new or renewed permits, submit a separate certification for each source facility. ❑ For modified permits„ submit a separate certification for only those facilities that are affected by the proposed modification. Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source -Generating Facility Information: For each source facility, attach the following: Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Quidance for Residuals Land ADDlication Pen -nits". Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. Z Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item 1. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: For each source facility, attach the following: M Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. M Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. F For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of I o o iy 90 CCf 21 40- 0 0 U En State of North Carolina Department of Environmental Quality Division of Water Resources Division of Water Resources FORM: RC 06-16 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction 13.): 1. Facility Name: Rocky River Wastewater Treatment Facility 2. Facility permit holder is: r_1 Federal, Ej State, M Local Government, or Ej Private. Facility permit issued by: 0 Div. of Water Resources, Div. of Environmental Health, or � Other (explain: 3. Facility contact person and title: Larry Hendren Complete mailing address: PO Box 878 City: Mooresville State: NC Zip: 28115 Telephone number: (204) 799-4063 E-mail address: Ihendren@mooresvillene.gov 4, Facility physical address: 369 Johnson Dairy Rd. City: Mooresville State: NC Zip: 28115- Coordinates: Latitude: 3 5' 3 V 3 3 Longitude: 80'46'56" Datum: Level of accuracy: Method of measurement; GPS 5. Purpose of the facility: treatment of municipal wastewater, [I treatment of 100% domestic wastewater, treatment of potable water, E] treatment of 100% industrial wastewater, E] treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: _ % industrial and % domestic) E] other (explain: _ ). 6. Does the facility have an approved pretreatment program: Yes No 7. Facility permitted/design flow: 75 MGD and facility average daily flow: 5 MGD 8, Average amount of residuals being generated at this facility 1600 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: LIMA aerobic digestion. belt press to 14% solids, heatt( Type and volume of residuals storage (i.e., outside of residuals treatment units): I1I'x79'covprLdpa 11. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1, Specify if residuals are regulated under: Z 40 CFR Part 503 or 40 CFR Part 257. Note: Only residuals that are generated during domestic/i-nunicipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257, 2, Specify if residuals are defined under fl 5 A..N.C.AC 02T. 1102(151 as: Z Biological � Non -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, aninial processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems), FORM: RSC 06-16 Page 1 of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRk (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: M yes JE no. If yes, list the number(s): _ b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR �261,2 1 - 261.24: 11 yes E' no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Vvaypoint Anal tical and Date of analysis: 01/19/2021 Passed corrosivity test-, yes R no. pH: s.u. (2 pH < 12.5) Passed ignitability test: yes R no. Flashpoint: - 'F (> 1401F) Passed reactivity test: 0 yes Rno. FICN: mg/kg (<250) & H2S: - mg/kg (<500) TCLP Parameter Limit (mg/1) Result (mg1l) TCLP Parameter Limit (mg/1) Result (nigll) Arsenic 5.0 <0.50 Hexachlorobenzene 0.13 "0.020 Barium 100.0 Hexachloro-1,3-Butadiene 0.5 <0.050 Benzene 0.5 <0.025 Hexachloroethane 3.0 <0.050 Cadmium 1.0 <0.050 Lead 5.0 -'0.050 Carbon Tetrachloride 0.5 <0.025 Lindane 0.4 Na Chlordane 0.03 -0.0025 Mercury 0.2 <0.010 Chlorobenzene 100.0 <5 Methoxycblor 10.0 <0.00050 Chloroform 6.0 -0.30 Methyl Ethyl Ketone 200.0 <10 Chromium 5.0 --0.25 Nitrobenzene 2.0 'U50 m-Cresol 200.0 Na Pentachlorophenol 100.0 <0,25 O-Cresol 200,0 Na Pyridine 5.0 -0.25 p-Cresol 200.0 Na Selenium 1.0 <0. 12 Cresol 200,0 Na Silver 5.0 -0.25 2,4-D 10.0 Na Tetrachloroethylene 0.7 <0.025 1,4-Dichloroberizene 7.5 <0.38 Toxaphene 0.5 <0.025 1,2-Dichloroethane 1, 1 -Dichloroethylene 2,4-Dinitrotoluene Endrin Heptachlor and its d:ro�x ide I- :y� 0.5 0.7 0.13 0.02 �O008 <0.025 <0.035 Na 0.00050 �<O�_0005�� Trichlorocthylene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4,5-TP (Silvex) Vinyl Chloride 0.5 400.0 2.0 1.0 0.2 <0.025 <0.25 <0. 10 Na -'0.020 FORM: RSC 06-16 Page 2 of 5 4. Metals Determination. Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAQ 02T...,-J....I 0.5.. a. For DistributiotVLand Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory bVyponi Analytical and Date of analysis: 7/19/2021 Parameter Ceiling Monthly Average Result Concentration Limits Concentration Limits (ClassA & ClassB) (Class A Only) (mg1kg) (mglkg) (n7glkg) Arsenic 75 41 2.80 Cadmium 85 39 -,1.06 Copper 4,300 1,500 287 Lead 840 300 11.3 Mercury 57 17 0346 Molybdenum 75 n✓a 14.8 Nickel 420 420 14.3 Selenium 100 100 4.24 Zinc — 7,500 .............. ... 2,800 625 b. ror VurLace Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e,, on a dry weight basis) for the following metal parameters: Laboratory: _ and Date of analysis: Distance from Disposal Arsenic Chromium Nickel Unit to Boundary to Closest Property Line (meters, check one) (inglkg) (niglkg) (mg/kg) E] > 0 but- 25 30 200 210 1- 25 but < 50 34 220 240 50 but - 75 39 260 270 75 but < 100 46 300 320 100 but< 125 53 360 390 125 62 450 420 Result (mg1kg) FORM: RSC 06-16 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 95 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Wa pint Analytical and bate of analysis: 07/19/2021 Parameter Result (inglkg) Aluminum 25300 Ammonia -Nitrogen 2810 Calcium Magnesium 15100 2320 Nitrate -Nitrite Nitrogen 3.02 pH (Standard Unit) 6.1.9 Phosphorus 18700 Potassium Sodium 2290 881 Total 1C.jeldahl Nitrogen 16200 Using the results listed in Item 11. 5b. above, calculate the sodium adsorption ration (SAR): 18 [Note: if residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This rate is a (check one): X default value, or El actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: e. Calculate the :PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (111) Year PAN Five -"Year Maximum Adjusted PAN (mg✓kg) (mg1kg) Surface 9,640 Injection/Incorporation 10,90 Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: FORM: RSC 06-16 Page 4 of 5 7, Pathogen Reduction: Per 15A NCAC 02T. 11.06, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or EquivaIen A fecal coliforin density that is demonstrated to be less than 1,000 MPN per grain of total dry solids, or A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): F1 Alternative I [ I 5A NCAC 02T. I 106(b)(3)(A)] - Time/Temperature Compliance. [I Alternative 2 [15A NCAC 02T.1 106(b)(3)(B)l - Alkaline Treatment. El Alternative 3 [15A NCAC 02T. I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. [] Alternative 4 (15A NCAC 02T.1 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova, Z Alternative 5 [15A NCAC 02T. I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFR-P). Specify one: composting, Z heat drying, heat treatment, then-nophilic aerobic digestion, beta ray irradiation, gamma ray irradiation, or pasteurization. b. For Land Aolication of Class B: El Alternative I [I 5A NCAC 02T. I 106(c)(1)] - Fecal Coliform Density Demonstration. Alternative 2 [15A NCAC 02TJ 106(c)(2)] - Process to Significantly Reduce Pathogens (PSR,P). Specify one: E] aerobic digestion, 0 air drying, El anaerobic digestion, El composting, or M lime stabilization. c. For Surface Disposal: ,X Select One of the Class Act Equivalent Pathogen Reduction Alternatives in Item 11. 7a. above. [] Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item If. 7b. above. n Exempt - If Daily Cover Alternative is chosen in Item 11.8. below [15A NCAC 02T.1 106(a)(2)]. n Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution, 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02TJ 107, specify how residuals will meet the VAR requirements: Fj Alternative I [15A NCAC 02T.1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). Alternative 2 [15A NCAC 02T.1 107(a)(2)1- 40-Day Bench Scale Test (Anaerobic Digestion), Alternative 3 [15A NCAC 02T.1 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion), E] Alternative 4 [15A NCAC 02T.1 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). Alternative 5 [15A NCAC 02T. I 107(a)(5)] - 14-Day Aerobic Processes. Alternative 6 [15A NCAC 02T. I 107(a)(6)] - Alkaline Stabilization. Alternative 7 [15A NCAC 02T. I 107(a)(7)] - Drying of Stabilized Residuals. Alternative 8 [15A NCAC 02T. I 107(a)(8)] - Drying of Unstabilized Residuals, Alternative 9 [15A NCAC 02T. I 107(a)(9)] - Injection. Alternative 10 D 5A NCAC 02T. I 107(a)(I 0)] - Incorporation, El Alternative for Surface Disposal Units Only - Soil/Other Material Cover [I 5A NCAC 02T. I 107(b)(2)]. 0 Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution, Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 Processed residual pellets are transported from dryer to covered facility where they are stored from 30 — 180 days until recipients/end users are ready for delivery. Recipients coordinate bulk hauling of residuals to their final destination through correspondence with the Biosolids Coordinator. Suggested nutrient limiting factors could be nitrogen, phosphorus, calcium and aluminum. Leachate is not a concern due to cover storage pad. However, pad is sloped to drainage line as an extra safety precaution. Process flow is explained below: Waste activated sludge is pumped from WAS basin to one of two aerobic digesters. Sludge is held in digesters before being pumped to a belt press. The sludge is dewatered and pressed to achieve an approximate 14-16% cake which is conveyed to a storage hopper. The cake is than conveyed to the belt dryer system where it is heated for 4 hours at —20OF to achieve 90% - 98% dry Class A pellet. Dry pellets are conveyed to a dump truck. Dump truck transfers product to the covered storage facility until ready for final bulk shipping. Loaded trucks leaving the facility contain 4 — 8 tons of residuals depending on the vehicle. All Class A residuals are distributed to local farmers who land apply in accordance with the Town of Mooresville Utilization Agreement. Residuals were applied at predetermined agronomic rates by their own equipment. A total of 898 dry tons left the facility in 2020. For 2021 we have more fainers signed up to use our product and are limited by our permit distribution capacity of 900 dry tons per year. No product label — Current Class A Utilization Agreement Included Operations and Maintenance The Town of Mooresville's Rocky River WWTP is permitted to discharge 7.5mgd. The current average flow is 4.Omgd. The incoming waste stream is protected from excessive fats, oils, and grease by our FOG program though a system of monitoring and permitting local dischargers. The incoming waste stream is further protected from heavy metals and other toxins through our industrial Pretreatment program system of permitting and monitoring. The plant's extended air activated sludge is managed by our Operations Supervisor and Biosolids Coordinator. This sludge is pumped to one of two digesters. We operate the digesters on a rotational basis filling and digesting one while removing sludge from the other via our belt press. We rotate the digester functions approximately every 30 days. The belt press solids are then transferred to the belt dryer system where we achieve an average dryness of 95%. All maintenance and calibration schedules are based on manufacturer's recommendations. Safety protocols are based on OHSA requirements. All wet processes are either contained or directed to an internal drainage system that leads back to the head of the plant. Inspection Plan Daily inspections are performed by the Biosolids Coordinator of all equipment, safety, and records. Any problems are reported to the Operations Supervisor. Weekly inspections are perfonned by the Operations Supervisor of all equipment, safety, and records. Any problems are reported to the Plant Manager. Monthly inspections are performed by the Plant Manager of all equipment, safety, and records. Any problems are reported to the Utilities Director. Annual review performed by the Utilities Director. Annual safety inspection performed by the Town's Safety Committee, During operational inspections if any noncompliant solids are observed they will be reintroduced to the system of disposed of in a lined landfill. All safety issues will be corrected in house as soon as noted. All records will be verified monthly by at least three people. Sampling Plan In house percent solids testing will be done by the Biosolids Coordinator and verified by our Laboratory Analyst. Samples will be sent to a certified commercial lab for WIT analyses. Ignitability, corrosivity and reactivity will be conducted annually. Metals, nutrients, VOC, SVOC, herbicides, pesticides, pH and pathogens will be conducted quarterly. Heat drying will use to meet pathogen reduction. Drying of stabilized residuals will be used to meet vector attraction reduction. Sample location will be at the exit of the dryer. Sample type will be grab. The figure presented in Section 1.8. was based upon the 2020 Class A Annual Sludge Report. We are currently permitted to distribute 900 dry tons, and records state that a total of 898 dry tons left the facility in 2020. Over the last 2 years we have been working with Huber USA to make minor adjustments to the dryer to increase capacity and hourly throughput. We are currently operating the dryer on a 24/7 basis except during periods of maintenance or malfunction. Residuals distribution in 2020 was greater than any single year in our records and with additional capacity we could have continued to dispense farther into the fall and winter months. We currently have a high demand for our product from local farmers and expect more growth in and around our community in the coming years. For these reasons we are requesting to increase our annual residuals distribution to 1600 Dry Tons per year. We feel that elevated ceiling will allow us to serve our farmers through the entire year without interruption and reduce the amount of Class A product we would have to pay to dispose of via our landfill contract with BFI landfill in Concord. Sampling Plan In house percent solids testing will be done by the Biosolids Coordinator and verified by our Laboratory Analyst, Samples will be sent to Waypoint Analytical, a certified commercial lab for, TCLP analyses. Ignitability, corrosivity and reactivity will be conducted annually. Metals, nutrients, VOC, SVOC, herbicides, pesticides, pH and pathogens will be conducted quarterly, Heat drying will use to meet pathogen reduction. Drying of stabilized residuals will be used to meet vector attraction reduction, Sample location will be at the exit of the dryer. Sample type will be grab. 25; ; Attachment S — Laboratory Data The attached laboratory data was used to complete Residuals Source Certification (RS C O6- !. NORTH ROY COOPER QuCAROLINAality Govr'Ilw MIC14AEL S, REGAN Saerptwy UNDA CULPEPPER S'n teHm A rw."Or August 30, 2018 JAmEs ANDREW LEVIS — WWTP MANAGER TOWN OF MOORESVILLE POST OFFICE BOX 878 MOORESVILLE, NORTH CAROUNA 28115 Dear Mr. Levis: Subject: Permit No. WQG036723 Town of Mooresville DCAR Distribution of Class A Residuals Iredell County In accordance with your permit renewal request received May 22, 2018, and subsequent additional information received July 16, 2018, we are forwarding herewith Pemit No. WQ0036723 dated August 30, 2018, to the Town of Mooresville for the continued operation of the subject residuals management program. Please note that this renewed pen. -nit shall become effective on October 1, 2018 (i.e, the day after the expiration date of the existing permit). This permit shall be effective from October 1, 2018 until September 30�, 2023, shall void Permit No,, WQ0036723 issued November 7, 2013, and shall be subject to the conditions and limitations as specified therein. Please pay particular attention to the monitoring requirements listed in Attachment A for they may differ from the previous permit issuance, Failure to establish an adequate system for collecting and maintaining the required operational information shall result in future compliance problems. Please note the following permit conditions have been removed since, the last permit issuance dated November 7,2013: > Old Conditions 111.9. and 111.10, — The utilization agreement conditions are replaced by Condition 111.9, North Carolina Department of Environmental Quality I Division of Water Resources I Non -Discharge Branch 512 North Salisbury Street � 1617 Mait Service Center I Raleigh, North Carolina 27699-1617 919.707,3654 Mr, James Andrew Levis August 30, 2018 Page 2 of 2 Please note the following permit conditions are new since the last permit issuance dated Novem her 7, 2 013: Condition 111.9. —This condition requires the Permitteeto inform all bulk receivers of residuals that they are to comply with Conditions 11,8, (application at agronomic rate) and 111.8. (conditions under which bulk residuals are not to be applied) of this permit, If any parts, requirements or limitations contained in this permit are unacceptable, the Ponnittee has the right to request an adjudicatory bearing upon written request within 30 days following receipt of this permit, This request shall be in the form of a written petition, conforming to Chapter 150B of the North Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail Service Center, Raleigh, NC 27699-6714, Unless such demands are made, this pen -nit shall be final and binding. If you need additional information concerning this permit, please contact Troy Doby at (919) 707- 3655 or troy .doby(amcderingov. Sincerely, ?Dipda Culpepper, Interim Director nLivision of Water Resources cc: Iredell County Health Department (Electronic Copy) Mooresville Regional Office, Water Quality Regional Operations Section (Electronic Copy) Laserfiche File (Electronic Copy) Digital Permit Archive (Electronic Copy) Central Files fill In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, and other applicable Laws, Rules, and Regulations • - �L �61•11, Town of Mooresville Iredell County IN-96-H-0 continued operation of a residuals management program for the Town of Mooresville and consisting of the distribution of Class A residuals generated by the approved facility listed in Attachment A with no discharge of wastes to surface waters, pursuant to the application received May 22, 2018, and subsequent additional information received by the Division of Water Resources, and in conformity with other supporting data subsequently filed and approved by the Department of Environmental Quality and considered a part of this permit. The use and disposal of residuals are regulated under Title 40 Code of Federal Regulations Part 503. This permit does not exempt the Pennittee fiorn complying with the federal regulations. This permit shall be effective from October 1, 2018 until September 30, 2023, shall void Permit No, WQ0036723 issued November 7, 2013, and shall be subject to the following specified conditions and limitations: I . No later than six months prior to the expiration of this permit, the Permittee shall request renewal of this permit on official Division forms. Upon receipt of the request, the Division will review the adequacy of the facilities described therein, and if warranted, will renew the permit for such period of time and under such conditions and limitations as it may deem appropriate. Please note Rule 15A NCAC 02T.0 I 05(d) requires an updated site map to be submitted with the permit renewal application. [I 5A NCAC 02T .01 08(b)(2), 02T .0 1 05(d), 02T.0 109] A �t I . The subject residuals management program shall be effectively maintained and operated at all times so there is no discharge to surface waters, nor any contravention of groundwater or surface water standards, In the event the facilities fail to perform satisfactorily, including the creation of prolonged nuisance conditions due to improper operation and maintenance, the Permittee shall immediately cease distribution of residuals, contact the Mooresville Regional Office supervisor, and take any immediate corrective actions,. [G.S. 143-215, 1] WQ0036723 Version 2.0 Shell Version 180711 Page 1 of 10 2. This permit shall not relieve the Permittee of responsibility for damages to groundwater or surface water resulting from the operation of this residuals management program. [15A NCAC 028 0200, 02L.0100] 3. Only residuals generated by the facility listed in Attachment A are approved for distribution in accordance with this permit. [G. S , 143-215. 1 ] 4. Pollutant concentrations in residuals distributed or applied to any land application site shall not exceed the following Ceiling Concentrations or Monthly Average Concentrations (i.e., dry weight basis): Parameter Ceiling Concentration (milligrams per kilogram) Monthly Average Concentration (milligrams per kilogram) Arsenic 75 41 Cadmium 85 39 Copper 4,300 1,500 Lead 840 300 Mercury 57 17 Molybdenum 75 n/a Nickel 420 420 Selenium 100 100 Zinc 7,500 2,800 [15A NCAC 02T. 1105] 5. Residuals that are distributed shall meet Class A pathogen reduction requirements in 15A NCAC 02T .1106 (a) and (b), Exceptions to this requirement shall be specified in Attachment A. [ 15A NCAC 02T .1106] 6. Biological residuals (i.e, residuals generated during the treatment of domestic or animal processing wastewater, or the biological treatment of industrial wastewater, and as identified in Attachment A) that are distributed shall meet one of the vector attraction reduction alternatives in 15A NCAC 02T .1107(a). Exceptions to this requirement shall be specified in Attachment A. [15ANCAC 02T.1107] WQ0036723 Version 2.0 Shell Version 180711 Page 2 of 10 7, Setbacks for Class Aland applied bulk residuals shall be as follows: Setback by residual type Setback Description (feet) Liquid Cake' Private or public water supply 100 100 Surface waters (streams — intermittent and perennial, perennial waterbodies,.Lnd wetlands... 100 25 Surface water diversions (ephemeral streams, waterw , ditches).... 25 0 Groundwater lowering ditches (where the bottom of the ditch intersects the SHWT) 25 0 Wells with exception to monitoring wells 100 100 Bedrock outcrops 25 0 Unless otherwise noted in Attachment A, "cake" residuals are those that have greater than 15% solids by weight and can be stacked without flowing, as well as can be handled, transported and spread as a solid (e,g, using a backhoe, front end loader, stinger spreader, broadcast spreader or other equipment designed for handling solid materials) without leaving any significant liquid fraction behind. [I 5A NCAC 02T .11081 8. Bulk residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in exceedance of agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen requirements based on the determined Realistic Yield Expectations (RYE) using any of the following methods: a. Division's pre -approved site specific historical data for specific crop or soil types by calculating the mean of the best three yields of the last five consecutive crop harvests for each field. b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State University Department of Soil Science (h //nutrients ) A copy t!p�_ "h � shall be kept on file and reprinted every five years in accordance with Condition IV.6. c, If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the: RYE and appropriate nutrient application rates reported in any of the following documents: i. Crop management plan as outlined by the local Cooperative Extension Office, the North Carolina Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, or other agronomist, iL Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance Document: Chapter I (h4pL-//w-_vvNv-gU ,o _nca �v/SWC/tech/documents/9th Guidance Dog. �O0109�,df). iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation Services (MRCS), These plans must meet the USDA -MRCS 590 Nutrient Management Standards If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall contact the Division to determine necessary action. [I 5A NCAC 02T . I 109(b)(1)(k)] WQ0036723 Version 10 Shell Version 180711 Page 3 of 10 The Permittee shall not distribute Class A residuals that have a sodium adsorption ratio (SAID) of I or higher without prior written Division approval, The Permittee may seep approval by demonstrating that the entity accepting the residuals is: aware of the effects of a high SAIL content- has agreed on proper residual application rates; and has agreed to operational considerations to ensure that the high SAR content will not adversely impact the receiving sites. Recommendations regarding sodium application rate, soil amendments (e.g., gypsum, etc.) or a mechanism for maintaining site integrity and conditions conducive to crop growth, can be obtained from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, allorth Carolina Licensed Soil Scientist, or an agronomist, [15A NCAC 02T .0108(b)(1)] (( I � I tti M; 49"a= Or 1, The residuals management program shall be properly maintained and operated at all times, The program shall be effectively maintained and operated as a non -discharge system to prevent any contravention of surface water or groundwater standards. [ I SA NCAC 02T .1110] 2. The Permittee shall maintain an approved Operation and Maintenance Plan (O&M Plan) Modifications to the O&M Plan shall be approved by the Division prior to utilization of the new plan, The O&M Plan, at the minimum, shall include: a, Operational functions-, b. Maintenance schedules; c. Safety measures; d. Spill response plan; e. Inspection plan including the following information: i. Names and/or titles of personnel responsible for conducting the inspections; ii. Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program; iii. Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed pursuant to the noncompliance notification requirements under the monitoring and reporting section of the permit; f. Sampling and monitoring plan including the following information: i. Names and/or titles of personnel responsible for conducting the sampling and monitoring, ii. Detailed description of monitoring procedures including parameters to be monitored; iii. Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals, to meet pathogen and vector attraction reduction requirements (e.g, facilities that distribute multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures). [I 5A NCAC 02T. I 100] WQO 03 6723 Version 2.0 Shell Version 180711 Page 4 of 10 3, Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC) classification of the facility, the Permittee shall designate and employ a certified operator in responsible charge (ORC) and one or more certified operators as back-up ORCs in accordance with 15A NCAC 08G.020 1, The ORC or his back-up shall visit the facilities in accordance with 15A NCAC 08G. 0204, or as specified in the most recently approved O&M plan (i.e., see Condition IIL2), and shall comply with all other conditions of 15A NCAC 08G. 0204. For more information regarding classification and designation requirements, please contact the Division of Water Resources' Protection and Enforcement Branch at (919) 707-9105. At the time of this permit issuance, a certified ORC is not required for the subject Distribution of Class A Residuals program. [15ANCAC 02T.0117] 4. When the Permittee land applies bulk residuals, a copy of this permit and a copy of O&M Plan shall be maintained at the land application sites during land application activities, [15A NCAC 02T .0108(b)(1)] 5. When the Permittee transports or land applies bulk residuals, the spill control provisions shall be maintained in all residuals transport and application vehicles, [15ANCAC 02T.1110] 6. When the Permittee land applies bulk residuals, adequate measures shall be taken to prevent wind erosion and surface runoff from conveying residuals from the land application sites onto adjacent properties or into surface waters. [G.S. 143-215.1] 7. When the Pennittee land applies bulk residuals, a suitable vegetative cover shall be maintained on land application sites onto which residuals are applied, or application shall be in accordance with the crop management plan outlined by the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, or an agronomist and as approved by the Division. [15A NCAC 02T .1109(b)(1)] 8. Bulk residuals shall not be land applied under the following conditions: a. If the residuals are likely to adversely affect a threatened or endangered species listed under section 4 of the Endangered Species Act or its designated critical habitat; b, If the application causes prolonged nuisance conditions; c. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface water or, groundwater standards; d. If the land is flooded, frozen or snow-covered, or is otherwise in a condition such that runoff of the residuals would occur; e. Within the I 00-year flood elevation, unless the bulk residuals are injected or incorporated within a 24-hour period following a residuals land application event; f During a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period; & If the slope is greater than 10% for surface applied liquid residuals, or if the slope is greater than 18 % for injected or incorporated bulk liquid residuals; h. If the land does not have an established vegetative cover unless the residuals are incorporated or injected within a 24-hour period following a residuals land application event. Any field that is in a USDA no -till program shall be exempted from meeting this vegetative cover requirement; i. If the vertical separation between the seasonal high water table and the depth of residuals application is less than one foot; j. If the vertical separation of bedrock and the depth of residuals application is less than one foot; k. Application exceeds agronomic rates. [15A NCAC 02T .1109] WQ0036723 Version 2.0 Shell Version 180711 Page 5 of 10 9. The Permittee shall notify all third -party entities receiving bulk distributed Class A residuals that land application activities occurring on the third-party's property shall meet the requirements in 15A NCAC 02T .1 108(b)(1) and 02T .1 109(b) (i.e., Conditions 11.8. and RIX, respectively). [I 5A NCAC 02T .114i3 (4)] 10, All residuals shall be adequately stored to prevent untreated leachate runoff. The finished product may be placed on a concrete pad, placed under shelter or physically covered until it is distributed to a third - party entity. If bulk residuals are to be applied, the residuals may be staged at the application site for up to 30 days for biological residuals,, and 60 days for non -biological residuals. If an alternate storage site is used, approval must be obtained from the Division. [15ANCAC 02T.0108(bXl)] 11. A label shall be affixed to the bag or other container in which residuals are sold or given away for land application, or an information sheet shall be provided to the person who receives Class A residuals. At a minimum, the label or information sheet shall contain the following: a. The name and address of the person who prepared the residuals; b. A statement that residual land application is prohibited except in accordance with the instructions on the ➢abel or information sheet; c. A statement identifying that this material shall be prevented from entering any public or private water supply source (including wells) and any surface water (e.g., stream, lake, river, wetland, etc.); d. A statement that the residuals shall be applied at agronomic rates and recommended rates for its intended use, [I 5A NCAC O2T.1109(a)] 12. The Permittee shall not distribute bulk residuals to any person or entity known to be applying residuals contrary to the conditions of this permit. The Permittee shall report to the Mooresville Regional Office as per reporting conditions under Condition IV. 8. any person or entity known to be applying residuals contrary to the condition of this permit, [I 5A NCAC 02T .I 103(a)] WQ0036723 Version 2,0 Shell Version 180711 Page 6 of 10 1, Any Division -required monitoring (including groundwater, plant tissue, soil and surface water analyses) necessary to ensure groundwater and surface water protection shall be established, and an acceptable sample reporting schedule shall be followed. [15A NCAC 02T .0108(c)] 1 Residuals shall be analyzed to demonstrate they are non -hazardous under the Resource Conservation and Recovery Act (RCRA). Residuals, that tests or is classified as a hazardous or toxic waste under 40 CFR Part 261 shall rant be used or disposed under this permit. The analyses [corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)l shall be performed at the frequency specified in Attachment A, and the Permittee shall maintain these results for a minimum of five years. Any exceptions from the requirements in this condition shall be specified in Attachment A. The TCLP analysis shall include the following parameters (the regulatory level in milligrams per liter is in parentheses): Arsenic (5.O1) 1,4-Dichlorobenzene (7.5) Nitrobenzene (2.0) Barium (100.0) 1,2-Dichloroethane (0.5) Pentachloropheno,l (10H) Benzene (0.5) 1, 1 -Dichloroethylene (0.7) Pyridine (5.0) Cadmium (1,0) 2,4-Dinitrotoluene (0.13) Selenium (1.0) Carbon tetrachloride (0,5) Endrin (0.02) Silver (5.0) Chlordane (0.03) Hexachlorobenzene (0,13) Tetrachloroothylene (03) Chlorobenzene (100.0) Heptachlor (and its hydroxide) (0.008) Toxaphene (0.5) Chloroform (6,0) Chromium (5.0) Hexachloro-1,3-butadiene (0'.5) Hexachloroethane (3.0) Trichloroethylene (0.5) 2,4,5-Trichlorophenol (400'.0) m-Cresol (200.0) Lead (5.0) 1 2,4,6-Trichloropbenot (2.0) o-Cresol (200.0) Lindane (0.4) 2,4,5-TP (Silvex) (1,0) p-Cresol (200.0) Mercury (0.2) Vinyl chloride (0.2) Cresol (2001.0) Methoxychlor (10.0) 2,4-D (10,0), Methyl ethyl ketone (200,0) Once the residuals have been monitored for two years at the frequency specified in Attachment A, the Permittee may submit a permit modification request to reduce the frequency of this monitoring requirement. In no case shall the monitoring frequency be less than once per permit cycle, [15A NCAC 13A.0102(b), 02T.1 101, 02T.1 105] WQ0036723 Version 2,0 Shell Version 180711 Page 7 of 10 3. An analysis shall be conducted on the residuals from each source generating facility at the frequency specified in Attachment A, and the Permittee shall maintain the results for a minimum of five years. The analysis shall include the following parameters: Aluminum . . ........ Mercury Potassium Ammonia -Nitrogen Molybdenum Selenium Arsenic Nickel Sodium Cadmium Nitrate -Nitrite Nitrogen Sodium Adsorption Ratio (SAR) Calcium Percent Total Solids TKN Copper pH Zinc Lead Phosphorus Magnesium Plant Available Nitrogen (by calculation) [15A NCAC 02T,, 11011 4. Residuals shall be monitored for compliance with pathogen and vector attraction reduction requirements at the frequency specified in Attachment A, and at the time indicated in the sampling and monitoring sections of the approved O&M plan. The required data shall be specific to the stabilization process utilized, and sufficient to demonstrate compliance with the Class A pathogen reduction requirements in 15A NCAC 02T .1106 (a) and (b), and one vector attraction reduction requirement in 15A NCAC 02T .1107 (a) shall be met. Any exceptions from the requirements in this condition shall be specified in Attachment A. [15ANCAC 02T.1106,02T,1107,02T.1111(c)] 5, Laboratory parameter analyses shall be performed on the residuals as they are distributed, and shall be in accordance with the monitoring requirements in 15A NCAC 02B .0505. [15A NCAC 02B M051 6. The Permittee shall maintain records tracking all bulk residual distribution or land application events performed by the Permittee, At a minimum, these records shall include the following: a. Source of residuals; b. Date of distributionfland application; c. Name and address of recipient of residuals, d. Volume of residuals distributed to: each recipient; e. Intended use of residuals; f If land application events performed by the Permittee -Nitrogen Application Rate based on RYES (if using data obtained from the North Carolina State University Department of Soil Science Website, the printout page shall be kept on file and reprinted every five years), [15A NCAC 02T.0108(a)] WQ0036723 Version 10 Shell Version 180711 Page 8 of 10 T Three copies of an annual report shall be submitted on or before March 1". The annual report shall meet the requirements described in the Instructions for Residuals Ap Instructions for reporting and annual report forms are available at h�t �-//de n�c.gov/about/divisions,/water-resources/water-resources-pe nits/wistewater-branch/non- di scharge- Lerm ittJ or can be obtained by contacting the Non -Discharge Permitting Unit directly. The annual report shall be submitted to the following address: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 [I 5A NCAC 02T. I 11 I (a)] 8. Noncompliance Notification The Permittee shall report by telephone to the Mooresville Regional Office, telephone number (704) 663 -1699, but in no case more than 24 hours or on the next working day following the occurrence or first knowledge of the occurrence of any of the following: a. Distribution of residuals abnormal in quantity or characteristic.' b. Any failure of the distribution program resulting in a release of material to surface waters, c. Any time self -monitoring indicates the facility has gone out of compliance with its permit limitations. d. Any process unit failure, due to known or unknown reasons, rendering the facility incapable of adequate residual treatment, e. Any spill or discharge from a vehicle or piping system during residuals transportation. Any emergency requiring immediate reporting (e,g., discharges to surface waters, imminent failure of a storage structure, etc.) outside normal business hours shall be reported to the Division's Emergency Response personnel at telephone number (800) 662-7956, (800) 858-0368, or (919) 733-3300.Persons reporting such occurrences by telephone shall also file a written report in letter form within five days following first knowledge of the occurrence. This report shall outline the actions taken or proposed to betaken to ensure that the problem does not recur. [15ANCACO2T.0105(1),02T.0108(b)(1)] 1, The Permittee shall provide adequate inspection and maintenance to ensure proper operation of the subject facilities and shall be in accordance with the approved O&M Plan, [15ANCACO2T,0108(b)] 2. Prior to each bulk residuals distribution event, the Permittee or his designee shall inspect the residuals processing, storage, transport and distribution facilities to identify malfunctions, facility deterioration and operator errors that could result in discharges to the environment, a threat to human health or a public nuisance, The Permittee shall maintain an inspection log that includes, at a minimum, the date and time of inspection, observations made, and any maintenance, repairs, or corrective actions taken. The Pen-nittee shall maintain this inspection log for a period of five years from the date of inspection, and this log shall be made available to the Division upon request. [15A NCAC 02T .0108(b)] 1 Any duly authorized Division representative may, upon presentation of credentials, enter and inspect any property, premises or place on or related to the distribution sites or facilities permitted herein at any reasonable time for the purpose of determining compliance with this permit; may inspect or copy any records required to be maintained under the terms and conditions of this permit; and may collect groundwater, surface water or leachate samples, [G.S. 143-215,3(a)(2)] WQ0036723 Version 2.0 Shell Version 180711 page of 10 1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to an enforcement action by the Division in accordance with North Carolina General Statutes 143-215,6A to 143-215.6C� [G.S, 143-215,6A to 143-215.6C] 1 This permit shall become voidable if the residuals distribution events are not carried out in accordance with the conditions of this permit, [15ANCAC 02T.0110] 3. This permit is effective only with respect to the nature and volume of residuals described in the permit application and other supporting documentation, [G.S. 143-215.1] 4. The issuance of this permit does not exempt the Permittee, from complying with any and all statutes, rules, regulations, or ordinances, which may be imposed by other jurisdictional government agencies (e.g, local, state, and federal). Of particular concern to the Division are applicable river buffer rules in 15A NCAC 02B .0200; erosion and sedimentation control requirements in I SA NCAC Chapter 4 and under the Division's General Permit NCGO 10000; any requirements pertaining to wetlands under 15A NCAC 0213.0200 and 02H.0500; and documentation of compliance with Article 21 Part 6 of Chapter 143 of the General Statutes. [15A NCAC 02T .0105(c)(6)] 5, In the event the residuals program changes ownership or the Permittee changes his name, a formal permit modification request shall be submitted to the Division. This request shall be made on official Division forms, and shall include appropriate documentation from the parties involved and other supporting documentation as necessary, The Permittee of record shall remain fully responsible for maintaining and operating the residuals program permitted herein until a permit is issued to the new owner, [ISANCAC 02T,01041 6. This permit is subject to revocation or unilateral modification upon 60-day notice from the Division Director, in whole or part for the requirements listed in 15A NCAC 012T.01 10. [15ANCAC 02T,0110] 7. Unless the Division Director grants a variance, expansion of the permitted residuals program contained herein shall not be granted if the Permittee exemplifies any of the criteria in 15A NCAC 02T.0120(b), [15A NCAC 02T.01201 8. The Permittee shall pay the annual fee within 30 days after being billed by the Division. Failure to pay the annual fee accordingly shall be cause for the Division to revoke this permit. [I 5A NCAC 02T .0105(c)(3)] Permit issued this the 30' day of August 2018 (Linda Culpepper, Interim Director Division of Water Resources By Authority of the Environmental lvlanagcJent Commission WQ0036723 Version 2.0 Shell Version 180711 Page 10 of 10 > M 4 B Ao Zo U's. 0 34 W GA c) C:) C> C) 94 . . . ........ . dS u z O IV R E. 4. 0 " 04 rl; 4 wi 49 42 NIA UA 42 u -M J! Nu .5 E C: 40- OD cd cr 0 NC Certification No. 402 Case Narrative Waypointe) NC Drinking Water Cert No. 37735 2/10121 10:17 ANALYTICAL SC Certification No. 99012 Town of Mooresville/RR WWTP Whitney Munroe P. 0. Box 878 Mooresville, NC 28115 Project: Class A Dried Sludge Lab Submittal Date: 01/19/2021 Work Order 1010286 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Narrative Notes: Herbicides TCLP analysis was subcontracted to Waypoint Memphis. Laboratory report is attached. PAN Equation = 0.3 * (TKN - Ammonia) + 0.5 * (Ammonia) + Nitrate -Nitrite PAN = 0.3 * (26000 - 1200) + 0.5 * (1200) + 2.6 PAN = 8200 mg/kg Equation uses Mineralization Rate (MR) for Aerobically Digested Solids (0.3) Analysis note for SAR: SAR = Na ] / 'SQRT i ( [Ca] + [Mg] ) 12 SAR = 15/23 ]1 SQRT [140/20] + [5,9/122] 2 SAR = 0.34 ConcentraVons for Na, Ca, and Mg are expressed in milliequivatents per liter, and SQRT designates taking the square root of the operand in parentheses. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical 449 Spriingbrook Road - P.D. Box 240543 - Charlotte, NC 28224.0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 Pc gD 1 of 17 Please call if you have any questions relating to this analytical report. Respectfully, WAYPOIINT ANALYTICAL Terri W. Cole Project Manager Data Qualifiers Key Reference: B Analyte is found in the associated blank at a concentration >1/2 RL. B2 Analyte is found in the blank at a concentration > 1/2 RL. BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MS. HT Sample received and analyzed outside of the hold time. MC Sample concentration too high for recovery evaluation, SE Surrogate recovery outside of the CSC limits due to emulsion. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference Results reported to the reporting limft. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent ofWaypointAnalyticaJ. 449 Springbrook Road - P-0, Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 -Toll Free Number; 1-8001529-6364 - Fax: 704/525-0409, Page 2 of Work Order: 1010286 Client Sample ID Lab Sample iD Matrix DatefTime Sampled Date/Time Received Class A 1010286-01 Solid 01/19/21 8:26 01/19/21 12:30 Samples were received in good condition at 4.9 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent Of Waypoint Analytical, 449 Springbrook Road - P.0, Box 240543 - Charlotte, No 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529.6364 - Fax: 7041525-0409 17 0 0 Laboratory Report Waypoint. 02110/2021 ANALYTICAL Town of Mooresville/RR WWTP Project: Class A Dried Sludge Client Sample ID: Class Attn: Whitney Munroe Sample ID: 1010286-01 P, 0. Box 878 Work Order: 1010286 Mooresville, NC 28115 Sample Matrix: Solid Time Collected: 01/19/21 08:26 Time Submitted: 01/19/21 1230 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters Plant Available Nitrogen 8200 mgikg dry 3100 1100 20 *Calculation, 1127121 14;57 CLB (CALC] % Solids 95.7 % by 0.100 0.100 1 *SM2540 0 1122121 13,50 EDV PlA0789 Weight Ammonia as N 1200 mg/kg dry 9.7 2.4 1 *SM4500-NH3 C 1/27121 14:57 BMS PlAO911 Nitrate/Nitrite as N BRL mg/kg dry 5.2 1A 1 *SM4500-NO3 F 1/25/21 12:18 CLB PIA0861 pH 6.3 pH Units 1 *9045D 1/20121 11:50 CLB PIA0738 Phosphorus -Total 11000 mg/kg dry 520 210 100 *SM4500-P F 1125/21 9:06 CLB PlAO835 Temperature 20.2 HT C 1 *SM2550 B 1/20121 11:50 CLB PIA0738 Total Kjeldahl Nitrogen 26000 mg/kg dry 10000 3600 20 *351.2 1/22121 11:32 CLB PlAO801 Microbiological Parameters Fecal Coliforms 2 MPN/g dry 01 1 *SM9221 E 1/19121 13:43 ENM PIA0777 TCLP Extraction by EPA 1311 TCLP Extraction Complete N/A 1 *1311 ZHE 1/21/21 6:54 TBL PIA0751 TCLP Extraction Complete N/A 1 1311 1/22121 810 EDV PIA0798 TCLP Metals mercury SRL mg/L 0,010 0.000034 1 *7470A 1/25121 15:50 EDV PIA0863 Arsenic BRL mg/L 050 0,021 5 *6020B 1125/21 23;30 JAB PIA0817 Barium BRL mg/L 5.0 0.079 5 *6020B 1125121 23:30 JAB PlAO817 Cadmium BRL mg1L 0.060 0.016 5 *60208 1/25121 23:30 JAB PIA0817 chromium BRL mg/L 0.25 0.023 5 *60208 1/25/21 23:30 JAB PlAO817 Lead BRL mg/L 0.050 0.011 5 *60208 1/25/21 23:30 JAB PIA0817 Selenium BRL mg/L 0,12 0.024 5 *6020B 1/25/21 23:30 JAB PIA0817 Silver BRL mg1L 0.25 0.0084 5 *6020B 1/25121 23:30 JAB P I A0817 TCLP Organochlo dine Pesticides by GC/ECD Chlordane BRL mg/L 0.0025 0.00090 1 *8081B 1/25/21 17:11 NMB, PlA0849 Dieldrin BRL mg/L 0.00050 0,000068 1 *80816 V25/21 17:11 NMB PIA0849 Endrin BRL mg/L 0.00050 0,000068 1 *8081B 1/25/21 17:11 NMB PlA0849 gamma-13HC BRL mg/L 0.00050 0,000030 1 *8081B 1/25/21 17:11 NMB PlAO849 Heptachlor BRL mg/L 0.00050 0,000065 1 *8081B 1/25/21 17:11 NMB PlAO849 Heptachlor Epoxide BRL mg/L 0.00050 0,00011 1 *8081B 1126121 17:11 NMB PlAO849 Methoxyrhdr BRL mg1L 0.00050 0.000090 1 *8081B 1/25121 17:11 NMB PlA0849 Toxaphene BRL mg/L 0.025 0.0018 1 *8081B 1/25/21 17:11 NMB PIA0849 Surrogate Recovery Control Limits Decachlorobiphenyl 30% 13-186 Tetrachloro-m-xylene 52% 40-134 TCLP Serinivolatile Organic Compounds by GCIMS 2,4,5-T6chloropherol BRL mg/L 0,25 0,0036 1 *8270E 1125121 16:03 JMV PlAC812 2,4,6-Trichlorophenoi BRL mg1L 0.10 0.0045 1 *8270E 1125/21 16:03 JMV PIA0812 2,4-Dinitrotoluene BRL mg/L 0.012 0.0042 1 *827GE 1/25/21 16:03 JMV PlAD812 This report should not be reproduced, except in its entirety, without the written consent of Waypoini Analytical. 449 Springbrook Road - P.0, Box 240543 - Charlotte, No 28224-0543 Phone: 704/529-6364 -Toll Free Number; 1-8001529-6364 - Fax: 704/525-0409 EEag:4::C Town of Mooresville/RR WWTP Attn: Whitney Munroe R U. Box 878 Mooresville, NC 28115 Project: Class A Dried Sludge Sample Matrix: Solid Client Sample ID: Class Sample ID: 1010286-01 Work Order: 1010286 Time Collected: 01/19/21 08:26 Time Submitted: 01/19/21 12:30 M&T 11 77I 02/1012021 Parameter Result Units Report MDL Dilution Method Anafysis Analyst Batch Limit Factor Date/Time ID 2-Methylphenol EIPL mg/L 0.050 0,0024 1 *8270E 1/25/21 16:03 JMV PlAD812 314-Methylphenal BRL mgIL 0.050 0,0025 1 *8270E 1/25/21 16:03 JMV PlAO812 Hexachlorobenzene BRL mg/L 0.020 0.0039 1 *8270E 1/25/21 16:03 JMV PlAO812 Hexachlorobutadiene BRL mgJL 0.050 0,0045 I *8270E 1125121 16:03 JMV P1 A0812 Hexachloroethane BRL mg/L 0.050 0.0037 1 '8270E 1/25/21 16:03 JMV PlAO812 Nitrobenzene BRL mg/L 0.050 0.0038 1 *8270E 1/25121 16:03 JMV PlAO812 Pentachlorophenol BRL mg1L 0.26 Ull 1 *8270E 1/25121 16:03 JMV PlAO812 Pyridine BRL mg/L 0.25 0.0016 1 *8270E 1J25121 16:03 JMV PIA0812 Surrogate Recovery Control Limits 2,4,6-Tribrornophenol 13% 43-140 SE 2-Fluorobiphenyl 100 44-119 SE 2-Fluorophenol 5% 19-119 SE Nitrobenzene-d5 9% 44-120 SE Phenol-d5 7% 11-52 SE Terphenyl-d14 11 % 50-134 SE TCLP Volatile Organic Compounds by GCIMS 1,1-Dichloroethylene BRL mg/L 0.035 0.00083 10 *8260D 1/22121 20:38 JLB PlA0831 1,2-Dichloroethane BRL mgIL 0.0215 0.00066 10 *8260D 1/22/21 20:38 JLB PlA0831 1,4-Dichicra benzene BRL mg/L 0.38 0.00050 10 *8260D 1/22/21 20:38 JLB PIA0831 Benzene BRL MgIL 0.025 0.00048 10 *8260D 1122/21 20:38 JLB PlAO831 Carbon Tetrachloride BRL mg/L 0,025 0.0011 10 *8260D 1122121 20:38 JLB PIA0831 Chlorobenzene BRL mgIL 5.0 0.00062 10 *8260D 1/22/21 20:38 JLB PlAO831 Carbon disulfide BRL mg/L 0.050 0.00075 10 *8260D 1/22/21 20:38 JLB PlAO831 Chloroform BRL mg/L 0.30 0.00076 10 *8260D 1122/21 20:38 JLB PlAO831 Methyl Ethyl Ketone (2-Butanone) BRL mg/L 10 0.0024 10 *8260D 1122121 20:38 JLB PlAC831 7etrachloroothyiene BRL mg/L 0.035 0.00098 10 *8260D 1/22/21 20:38 JLB PlAO831 Trichloroethylene BRL mg/L 0.025 0.00078 10 *8260D 1/22/21 20:38 JLB PlA0831 Vinyl chloride BRL mg/L 0.020 0.00097 10 *8260D 1122121 20:38 JLB PlAO831 Surrogate Recovery Control Limits 4-Bromofluorobenzene 99% 80-124 Dibromofluoromethane 99% 75-129 Toluene-c!8 98% 77-123 Total Metals Aluminum 17000 mg/kg dry 260 29 100 *6020B 1126121 16 :31 JAB PlAO842 Mercury BRL mg/kg dry 0.52 0.16 10 *7471 B 1121121 1318 EDV PIA0790 SAR Soil Preparation Complete 9 1 *2-78-054 1/22/21 15:05 EDV PIA0800 SAR Percent Moisture 75.7 % by 0.100 0.100 1 *2-78-054 1/25121 8:20 EDV PlAO829 Weight Arsenic 2.1 mglkg dry 1.0 0.088 10 *6020B 1125/21 19:12 JAB PIA0842 Sodium Absorption Ratio BRL [blank] 1.0 0.016 1 -2-78-054 1/27/21 9:40 JAB PlAO827 Cadmium 0.54 mg/kg dry 0.52 0.039 10 *6020B 1125/21 19:12 JAB PlAO842 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. "S Springbrook Road - P,O, Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 -Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Page 5 of 17 0 G Laboratory Report Waypoi,nt. 02110/2021 ANALYTICAL Town of MooresvilleIRR WWTP Project: Class A Dried Sludge Client Sample lD: Mass Attn: Whitney Munroe Sample ID, 1010286-01 P, O. Box 878 Work Order: 1010286 Mooresville, NC 28115 Sample Matrix: Solid Time Collected: 01/19121 08:26 Time Submitted: 01/19/21 12:30 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Dale/Time ID Calcium 13000 mg/kg dry 100 20 110 *6020B 1126/21 116:37 JAB PIA0842 Calcium, SAR 140 mg1L 10 0A73 10 *60208 1127/21 9:40 JAB PlAO827 Copper 170 mglkg dry 2.6 0,28 10 *60205 1125121 19:12 JAB PIA0842 Lead 8.1 mg/kg dry 1.0 U79 10 *60205 1/26/21 16:37 JAB PlAO842 Magnesium 2400 mglkg dry 26 5,5 10 *60208 1125121 19:12 JAB PlAO842 Magnesium, BAR 5.9 mg/L 0.10 0.00072 1 *6020B 1/27121 9:40 JAB PIA0827 Molybdenum 71 mg/kg dry 1.0 0.18 10 *6020B 1/25/21 19:12 JAB PlA0842 Nickel 9.8 mglkg dry 1.0 0A2 10 *6020B 1125121 19:12 JAB PlAO842 Potassium 3400 mglkg dry 100 15 10 *6020B 1125i21 19:12 JAB PIA0842 Selenium 3.2 mglkg dry 1.0 0.24 10 *60208 1/25/21 19:12 JAB PlAO842 Sodium 990 B2 mglkg dry 100 24 10 *6020B 1/26121 16:37 JAB PIA0842 Sodium, SAR 15 B mg1l- 0.10 0.0047 1 *6020B 1/27/21 9:40 JAB PIA0827 Zinc 400 mg/kg dry 10 2.1 10 *60205 1126121 16:37 JAB PlAO842 This report shouW not be reproduced, except in its entirety, without the written consent cf Waypoint Analytical, 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone; 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 I Pap 6 of 17 Sample Extraction Data Prep Method: 351.2 Lab Number Batch Initial Final Date/Time 1010286-01 PIA0801 0.05 g 25 mL 01121/21 10:50 Prep Method: SM4500•NN3 B Lab Number Batch Initial Final Date/Time 1010286-01 PlAO911 1.08 g 50 mL 01127/21 9:43 Prep Method. SM4500-PB5 Lab Number Batch Initial Final Date/Time 1010286-01 PIA0835 I g 50 mL 01/23121 10A5 Prep Method: Solids, Dry Weight Lab Number Batch Initial Final Date/Time 1010286-01 PlA0789 30 g 30 9 01/21/21 9:57 Prep Method: 1311 Lab Number Batch Initial Final DatelTime 1010286-01 PlA0751 12.5 g 250 mL 01/20121 12:10 1010286-01 PlA0798 100 g 2000 mL 01/21121 16:08 Prep Method; 3010A Lab Number Batch Initial Final DatefTime 1010286-01 PIA0817 10 mL 50 mL 01122/21 10:31 Prep Method: 7470A Lab Number Batch Initial Final Date1nme 1010286-01 PIA0863 20 mL 30 mL 01/26/21 11:08 Prep Method: 3$10C GC Lab Number Batch Initial Final Datefrime 1010286-01 PlA0949 200 mL 10 mL 01125121 8:30 Prep Method: 3510C MS Lab Number Batch Initial Final Date/Time 1010286-01 PIA0812 200 mL 1 mL 01/22121 8:30 Prep Method: 5030B Lab Number Batch Initial Final Date/Time 1010286-01 PlAO831 10 mL 10 mL 01122121 10:00 Prep Method: 3010A Lab Number Batch Initial Final DateMme 1010286-01 RIA0827 50 mL 50 mL 01/22121 15:05 1010286-01 PIA0827 50 mL 50 mL 01122121 15:05 Prep Method: 30505 Lab Number Batch Initial Final DateMme 1010286-01 PIA0842 2 g 60 mL 01125/21 8A6 1010286-01 PlA0842 2 g 60 mL 01/25/21 8:46 ........... This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 44,9 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 - Tell Free Number; 1-800/529-6364 - Fax: 704/525-0409 Pag Sample Extraction Data Prep Methoch 305oB Lab Number Batch Initial Final DaterTime 1010286-01 PlAO842 2 g 50 ni 01/25/21 8:46 Prep Method: 74715 Lab Number Batch Initial Final Date/Time 1010286-01 PlAO790 0.6 g 50 n-L 01/21121 10:30 Prep Method; SAR 2.78-054 Lab Number Batch initial Final Date/Time 1010286-01 PlAO800 250 g 250 g 01/21121 15:05 Subcontracted Analyses The following analyses were subcontracted to Waypoint Analytical i Number• Analysis 1010286-01 llcrbicidc5 TCLP (Sub) This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrock Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Page of 17 C- UA W am ta to0 C- lu Z 0 ¢ 0 q g z z i,- uj W, :0 �z ¢-Zt.=,g8gE 0 z of>- § (5 Lu = L, -, CL a -0 0 -1 of F- LLJ A0 LU IL -N N0' c2 >0 11 Ll� 411 lu zvja C)fS 0 CL o U-C z Z 0 CL w LL Ul 0 =0 GL z 0) x (D Off 0 a. 0,22 >2 > L CL 0 iL ai OMfl 0 x 24 - E z rMo zM cp C 0 0 0 CL M J uj 0 U; 9L I z 0 a . z Z. 0 >- LU z LL uj c w t Ljj uj c LU 2 ul Ul IZ A = 61. L N -, ca 'M LU .40 0-2 C L � 3 qy ,q�l AULU C, z -0 2 .13 U, Z Cl •'a) "LO La W, w Ec IL cuig UJ 0. UJ uj IL w I S. 0 QED 0 0 V ll ki ujx E � M U. o 0 m M 0 �q w w U) to 611 0 u Z 0 P p- r.L w z 0 El Cl z z r u Cdi LL C3 (1) 0 S lz 10- (no Z M =Lu J-- Of fl u LU 25KI 0 U) OR a. LU M x 0 a M ro z n L. LL 1L 'w C, Cl > 0 If zo Aw '10 o0 u �z ag 0 z W 'uj 4 a 0 0 oa 2 z cry 0 UJ z 0. M 0 0� uj U) LU 0 (j z 0 L2 L 0 CL z 0 cl P LU nz 4:z co tn� I t 0 m ct g) z z lu 0, cr Ca 0 pia th m th CDO =0 �KW 0 a 0L 0 C .j LU z z 0 0 1=1 LUJ IL z 2 z 0 j Ir ca U, z lu wz r cy LU m cL am cl so; mzci F., 0 LU j cr) 41 Q zj� ON .0 Z< ran 14 Al o7, .- .6 � Alo w 0, -Z WX m r- 53 mE a. CCj O x m wx Us z cc 2 .-0 to U U 0 0 =0 II CL uj LU 9) W i7w ME i to i a. ul N to z Fa FF LU LU can yw os 0 cd c z 0ii So 9 = E m 02 m S 04) 0 IC KNO Waypoint-,,(2) ANALYTICAL 2/5/2021 Waypoint Analytical Charlotte Ms. Terri Cole P.O. Box 240543 Charlotte, NC, 28224-0543 2790 Whitten Road, Memphis, TN 38133 Main 901.213,24001 0 Fax 901,213�.2440 www.waypointanalytical,com Ref: Analytical Testing Lab Report Number- 21-029-0083 Client Project Description: Subcontract Order # 1010286 Dear Ms. Terri Cole: Waypoint Analytical, LLC. received sample(s) on 1/29/2021 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions, The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method, Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol, These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Andrea R Brownfield Project manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis, I Page 11 of 17 ] Page 1 of 7 2790 Whitten Road, Memphis, TN 38133 Main 901,213.2400 0 Fax 901,213.244,0 www.waypoinitanalyticaill.com State Program Lab ID . . .. . ............. . . Expiration Date Alabama State Program 40750 02/28/2021 Arkansas State Program 88-0650 02/07/2021 California State Program 2904 06/30/2021 Florida State Program - NELAP E871157 06/30/2021 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2021 Illinois State Program - NELAP 200078 10/10/2021 Kentucky State Program 80215 06/30/2021 Kentucky State Program KY90047 12/31/2021 Louisiana State Program - NELAP LA037 12/31/2021 Louisiana State Program - NELAP 04015 06/30/2021 Mississippi State Program IVIS 02/11/2023 North Carolina State Program 415 12/31/2021 Oklahoma State Program 9311 08/31/2021 Pennsylvania State Program - NELAP 68-03195 05131/2021 South Carolina State Program 84002 06/30/2021 South Carolina State Program 84002 06/30/2021 Tennessee State Program 02027 02/11/2023 Tennessee A21LA ISO 17025:2017 4313.01 10/31/2021 Texas State Program - NELAP T104704180 09/30/2021 Virginia State Program 00106 06/30/2021 Virginia State Program - NELAP 460181 09/14/2021 Page I of 1 004 Page 12 of 17 Page 2 of 7 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 FaX 901.213.2440 www.waypointanaiytical.com Sample Summary Table Report Number: 21-029-0083 Client Project Description,: Subcontract Order # 1010286 Lab No Client Sample ID Matrix Date Collected Date Received 91164 Class A Solid 01/19/202108;26 01/29/2021 Page 13 of 17�' Page 3 of 7 2790 Whitten Road, Memphis, TN 38133 Main 901,213.2400 ® Fax 901.213.2440 www.wayp o in tanalytical. co m Ms., Terri Cole Project Subcontract Order # 1010286 P.O, Box 240543 Information Charlotte , NC 28224-0543 Report Number : 21-029-0083 ,REPORT OFAIVAL YSIS Report Date 02/05/2021 Received 01/29/2021 Lab No : 91164 Matrix: Solid Sample ID : Class A Sampled; 1/19/20218:26 Analytical Method: 1311 Test TCLP Herbicide Extraction Analytical Method: 8151A Prep Method: 8151A Test TCLP 2,4-D TCLP 2,4,5-TP (Silvex) Surrogate: DCAA Results Units MDL MQL DF Date / Time By Analytical. Analyzed Batch Leachate 1 02/01/21 16:30 PHE L534263 Prep Batches}: 1-534722 02/03/21 15:00 Results Units MOL MQL DF Date I Time By Analytical Analyzed Batch <0,0100 mg/L 0,0100 0.0200 1 02/04/21 15;44 VIC L534973 <0.0010 mg/L 0,0010 0.0020 1 02/04/21 15:44 VIC L534973 70,80 Limits: 20-120% 1 02/04/2115:44 VIC L534973 Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit Page 4 of 7 (2) Waypoint 2790 Whitten Road, Memphis, TN: 38133 rVain 901.213.2400 0 Fax 901,213.2440 ANALYTICAL www.waypointanalytical.com Quality Control Data Client ID- Waypoint Analytical Charlotte Project Description. Subcontract Order# 1010286 Report No: 21-029-10083 QC Prep: L534722 QC Analytical Batch(es). L534973 QC Prep Batch Method: 8151A Analysis Method; 8151A Analysis Description: Phenoxy Acid Herbicides - GC/ECD (TCLP) Lab Reagent Blank LRB-L534722 Matrix: TCL Associated Lab Samples; 91164 Parameter Blank JMDL Units Result MQL Analyzed 0/0 0/4 Rec Recovery Limits TCLP 2,4-D mg/L <0.0100 0.0100 0.0200 02/04/21 12:03 TCLP 2,4,5-TP (Siivex) mg/L <0.0010 0.0010 0.0020 02/04/21 12:03 DCAA (5) 02/04/21 12:03 88.8 20-120 Laboratory Control Sample & LCSD LCS-LS34722 LCSD-L534722 Parameter Spike Units Conc„' LCS LCSD LCS LCSD Result Result G/bRec % Rec % Rec Limits RPD Max RPD TCLP 2,4-D mg/L 0.1000 0.0808 0.0772 80.8 77.2 20-120 4.5 20.00 TCLP 2,4,5-TP (Silvex) mg/L 0.0100 0.0076 0.0074 76.0 74.0 20-120 2.6 20,00 DCAA (S) 83.8 81.6 20-120 Date: 02/05/202103:47 PM Page 15 of 17 Page 5 of 7 (Ol 2790 Whitten Road, Memphis, TN 38133 Waypoint, Main 901.213.2400 0 Fax 901.213,24411 ANALYTICAL wwwwavpointanalybcal,com Shipment Receipt Form Customer Number; 25657 Customer Name: Waypoint Analytical Charlotte Report Number: 21-029-0083 Shipping Method 49 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: F-- F _00-- Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers/boxes received f —1 Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? Yes 0 No COC agrees with sample label(s)? Yes 0 No COO properly completed Yes 0 No Samples in proper containers? Yes1 No Sample containers intact? Yes 0 No Sufficient sample volume for indicated test(s)? Yes 0 No All samples received within holding tame? Yes 0 No Cooler temperature in compliance? Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No (a N/A Water - VOA vials free of headspace Yes 0 No 40 N/A —0 Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met Yes 0 No N/A —0 F High concentration container (48 hr) F High concentration pre -weighed (methanol -14 d) F Low [­' Low concentration EnCore samplers (48 hr) cons pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes @ No Comments: Signature: cry Phillips Date & Time: 51 I Page 16 of 17 � Page 5 of 7 Wayp ' inA t LYTICAL suBcovi-R,kci, ORDER :Certification: NFLAC USACE. Waypoint Analytical NC X SC Other 1010286 NiA S F. N I[) I N G, 1, A Ji _O R,,M'O R Y: RECEIVING 1.ABQ&.AT0RY-. Way point Analy6cal 'Waypoint Analy,fical 11. 0, Box 240543 2790 Whitten Road Charlotte. NC 28224-0543 Memphis- "TN 38133 Phone: 800-529-6364 Phone 190 1 ) 2 l 3-2400 Fax: 704-525-0409 Fav (901) 213.2440 Protect Mandeer Terri A". Cole Analysis Duc Expires Laboratory ID Lommerats Sample M, 1010296-01 Solid San'PIM: 011012108-26 ClassA I lcrbicide,'WLP (Sub 02M2121 08 20 ComainersSupplied: 21029-0083 25651 0,_2. 2021 ' �Vavmlnt Anal0cal Charictle 11 51 42 SuDcal MAO ornef 9 10 10-1136 f l -)-. �, l -2- ( Date Recewed By Date m Rage 7 of 7 Page I ut, I Page 17 of77 Town of Mooresville/RR WWTP Whitney Munroe P. O. Box 878 Mooresville, NC 28115 NC Certification No, 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Project: Class A TCLP Lab Submittal Date: 01/19/2021 Work Order: 1010287 2/10/21 10:38 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods, Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Narrative Notes: Reactivity analysis was subcontracted to Waypoint Memphis. Laboratory report is attached. Please call if you have any questions relating to this analytical report. Respectfully, WAYPOINT ANALYTICAL Terri W. Cole Project Manager Data Qualifiers Key Reference: HT Sample received and analyzed outside of the hold time, IGN The test results of this method cannot be used to directly classify a waste as a D001 hazardous waste, nor can the results be used by themselves to definitively classify a waste as non -hazardous. 40 CFR 26121 INEG Negative Ignitability result according to DOT regulations, BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report shouid not be reproduced, except in its entirety, without the written consent of WaypointAnatytical 449 Springbrook Road - P.O, Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax; 7041525-0409 Page 1 of 1=5 Gi Waypoint. ANALYTICAL Sample Receipt Summary 02/10/2021 Work Order: 1010287 Client Sample ID Lab Sample ID Matrix Datefrinne Sampled DatelTime Received Class A TCLP 1010287-01 Solid 01/19/21 8:26 01/19/21 12:30 Samples were received in good condition at 4.9 degrees C uNess otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Ana I ytieg L 449 Spriingbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041$29•6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 15 0 G Laboratory Report Waypolint. 02110/2021 ANALYTICAL Town of Mooresville/RR WWTP Project: Class A TCILP Client Sample ID: Class ATCLP Attm Whitney Munroe Sample ID: 1010287-01 P. 0. Box 878 Work Order: 1010287 Mooresville, NC 28115 Sample Matrix: Solid Time Collected: 01/19/21 08-26 Time Submitted: 01/19/21 12:30 Parameter Result Units Report IVDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 95.6 % by 0.100 0.100 1 *SM2540 G 1129121 15:12 EDV PlA0977 Weight Corrosivity-pH 6.3 pH Units I *9045D 1120121 11:50 CLB PlA0737 Ignitability E3RL IGN, IINEG mm/sec 0.10 1 *1030 1120121 15:15 BMS PIA0775 Temperature 20.2 HT c 1 *SM2550 B 1/20/21 11;50 CLS PlA0737 TCLP Extraction by EPA1311 TCLP Extraction Ccrnplete N/A 1122/21 8:10 EDV PlA0798 TCLP Sernivolatile Organic Compounds by GCIMS 2,4,5-Trichlorophenol BRL mg1L 0.25 0,0036 1 '8270E 1125121 11:33 JMV PIA0812 2,4,6-Trichlorophenol BRL mg/L 010 0.0045 1 *8270E 1/25/21 11:33 JMV PlA0812 2,4-Dr)itrotoluene BRL mg1L 0.012 0.0042 1 *8270E 1/25121 11:33 JMV PIA0812 2-Methylphenol BRL mg/L 0,050 0.0024 1 *8270E 1/25/21 11:33 JMV PlAO812 314-Methylphenol BRL mg/L 0,050 0.0025 1 *8270E 1126121 11:33 JMV PlA0812 Hexachlorobenzene BRL mg/L 0.020 0.0039 1 *8270E 1/25/21 11:33 JMV PlAO812 Hexachlorobutadiene BRL mg1L 0.050 0.0045 1 *8270E 1125/21 11.33 JMV PlAO812 Hexach[oroethane BRL mg/L 0.050 0.0037 1 *8270E 1/25121 11:33 JMV P 1 A0812 Nitrobenzene BRL mgIL 0.050 0.0038 1 *8270E 1/25/21 11:33 JMV PlAO812 Pentachlorophenol BRL mg/L 0,25 0.011 1 *8270E 1125/21 11:33 JMV PlAO812 Pyridlne BRL mg/L 0.25 0.0016 1 *8270E 1/25121 11:33 JMV PlA0812 Surrogate Recovery Control Limits 2,4,6-Tribrornophenol 127% 43-140 2-Fluorobiphenyl 91% 44-119 2-FluarophenoJ 53% 19-119 Nitrobenzene-d5 83% 44-120 Phenol-d5 35% 11-52 Terphenyl-d14 99% 50-134 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.0, Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 -Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Sample Extraction Data Prep Method: Solids, Dry Weight Lab Number Batch Initial Final Date/Time 1010287-01 P1A0977 30 g 30 g 01/29/21 7:54 Prep Method: 1311 Lab Number Batch Initial Final Date/Time 1010287-01 PlA0798 100 g 2000 mL 01121/21 16:08 Prep Method: 3510C MS Lab Number Batch Initial Final DatelTime 1010287-01 PIA0812 200 mL 1 mL 01122121 8:30 Subcontracted Analyses The following analyses were subcontracted to Waypoint Analytical Lab Number Analysis 1010287-01 Reactivity, Cyanide (Sub) 10 10287-0 1 Reactivity, Sulfide (Sub) This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0543 Phone. 7041529-6364 -Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Page 4 of ILJ 0 ro w >w Cl j,2 L to oJ L) s 9 l,� A ' C3 o 0 a, 0 -1 A-0 st 0. a F. U o'20 Dy COL E J rn Z5 LU or- .0 LL. 0 0c d 16 Z-4 o 05 z,- I earw -6 z-4 -0 6 o w - = E I E = a- m E p CL 0 * CL E a,. �T 'o p cv 0 Z.x A A 0,4 rz E z mR Cz 14 1> . t; E t ml c 0 0 0 Q. CL = u rs L —6 V Z x w E LL z m CL r- M ti 0 E- E I w Lu R LU N w z LU Lu LU w 0) 0 W B LU u Lu n p -30 ol 11 u i� cq !Y w w .j %n 0. 2 ww ms CL M E c co cu 0 -0 CD a E cu :3 a. ?,-a cn.-Q .- 'rh 'to 0. eqmwm l m -S CLC E E 5.0 co CU m CL= in E E kk LU 0 0 Cl cs -j CO u eD -� 0 LL X z Z d, ci 9 U. z R 9z w r U Z -C W C.1 cl c Z 13 z 0 R z LZ A iul z 0 Z ar o 1:� zu Iu fn O U) z z z D 7ww 0 (2) llaypoint ANALYTICAL 2/2/2021 Waypoint Analytical Charlotte Ms, Terri Cole P.O. Box 240543 Charlotte, NC, 28224-0543 Ref: Analytical Testing Lab Report Number: 21-026-0044 Client Project Description: Subcontract# 1010287 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 1 Fax 901.213.2440 www.waypointanalytical.com Dear Ms, Terri Cole; Waypoint Analytical, LLC. received sample(s) on 1/26/2021 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a'—' symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling, Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, 1 & A* k Andrea R Brownfield Project manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. I Page 6 of 1-5—D'I Page 1 of 10 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 rax 901.213.2440 www.waypointanalytical,com Laboratory 11): WP MTN: Waypoint Analytical, ILL.C., Memphis, TIN State Pre rg m Lab I D Expi ation- Date Alabama State Program 40750 02/28/2021 Arkansas State Program 88-0650 02/07/2021 California State Program 2904 06/30/2021 Florida State Program - NELAP E871157 06/30/2021 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2021 Illinois State Program - NELAP 200078 10/10/2021 Kentucky State Program 80215 06/30/2021 Kentucky State Program KY90047 12/31/2021 Louisiana State Program - NELAP LA037 12/31/2021 Louisiana State Program - NELAP 04015 06130/2021 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2021 Oklahoma State Program 9311 08/3112021 Pennsylvania State Program - NELAP 68-03195 05/31/2021 South Carolina State Program 84002 06/30/2021 South Carolina State Program 84002 06/30/2021 Tennessee State Program 02027 02/11/2023 Tennessee A21-A ISO 17025:2017 4313.01 10/31/2021 Texas State Program - NELAP T104704180 09/30/2021 Virginia State Program 00106 06/30/2021 Virginia State Program - NELAP 460181 09/14/2021 Page I of 1 00q- , Page 7 of 15 Page 2 of 10 0 (D Waypoint, ANALYTICAL Report Number: Client Project Description-, Lab No Client Sample ID 89334 Class A TCLP 2790 Whitten Road, Memphis, TN 381.13 Main 901.213.24010 " Fax 901.213.2440 www.waypointaniallytical.com Sample Summary Table Subcontract # 1010287 Matrix Date Collected Date Received Sohds 01/19/2021 08;26 01/26/2021 Page 3 of 10 2790 Whitten Road, Memnphis, TM 3,8133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.corn Ms, Terri Cole Project Subcontract # 1010287 P.O. Box 240543 Information Charlotte , NC 28224-0543 Report Number ; 21-026-0044 Report Date 02/02/2021 Received 01/26/2021 Lab No : 89334 Sample ID : Class, A TCLP Matrix: Solids Sampled; 1/19/20218:26 Analytical Method: SW-7.33 Test Results Units MDL MOL OF Date / Time By Analytical Analyzed Batch Cyanide, Reactive <0A25 mg/Kg 0.125 0.125 1 01/26/21 12:46 FMM L533272 Sulfide (Reactivity) <25.0 mg/Kg 25.0 25.0 1 01/26/21 12:46 FMM L533273 Moisture 4.04 % 1 02/01/21 17:57 FMM L534252 Quailifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 9 oF1 5 Page 4 of 10 Waypoint.0 ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901,213.2400 ' Fax 901.213.2440 www.waypointanalytical.com Client ID: Waypoint Analytical Charlotte Project Description: Subcontract # 1010287 Report No; 21-026-004,4 QC Analytical Batch: L533272 Analysis Method: SW-7.33 Analysis Description, Reactive Cyanide Lab Reagent Blank LRB Matrix: SOL Associated Lab Samples: 89334 Parameter Cyanide, Reactive Laboratory Control Sample Parameter Cyanide, Reactive Blank Units Result mg/Kg <0A25 LCS Spike Units Conc. mg/Kg 1000 wa�lffl 0.125 0.125 LCS Result 166 Analyzed 01/26/21 12:46 LCS O/oRec 0/0 Rec Limits 17.0 5-75 Date: 02/02/2021 03:51 PM Page 10 of I Page 5 of 10 QC Analytical Batch: L533273 Analysis Method: SW-7.3.4 Analysis Description: Sulfide Reactivity Lab Reagent Blank LRB Matrix: SOL Associated Lab Samples: 89334 Blank MDL MQL Analyzed Parameter Units Result Sulfide (Reactivity) mg/Kg <25.0 25,0 25.0 01/26/21 12:46 Laboratory Control Sample LCS Spike LCS LCS 0/aRec O/o Rec Parameter Units Conc. Result Limits Sulfide (Reactivity) mg/Kg 254 231 91,0 50-130 Date: 02/02/2021 03:51 PM Page 6 of 10 [ Page 11 of 15 1 Waypolinto ANALYTICAL 2790 whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901,213.2440 www.waypointanalytical.com Client ID.- Waypoint Analytical Charlotte Project Description: Subcontract# 1010287 Report No: 21-026-0044 QC Analytical Batch. L534252 Analysis Method: SW-DRYWT Analysis Description: Dry Weight Determination Duplicate Parameter Moisture L 90869-DUP Result DUIP Units Result % 10.1 6.73 RPD Max RPD Analyzed 40.0* 20.0 02/01/21 17:57 QC Fail Date: 02/02/202103:51 PM Page 12 of " -0 Page 7 of 10 Wyrp NLTCL(D 90W:ttenRo.ad,MeapTnt M90200maph0is, TN 3,841430 AYA3 wwmwavpointanalyticaLcom Shipment Receipt Form Customer Number: 25657 Customer Name: Waypoint Analytical Charlotte Report Number; 21-026-0044 Shipping Method Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: Shipping container/cooler uncompromised? Yes 0 No Number of coolers/boxes received 1. Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? 40 Yes 0 No COC agrees with sample labei(s)? 9 Yes 0 No COG properly completed 4D Yes 0 No Samples in proper containers? 9 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 9 Yes 0 No All samples received within holding time? Yes 0 No Cooler temperature in compliance? Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 - compliance criteria met 0 Yes 0 No N/A High concentration container (48 hr) F Low concentration EnCore samplers (48 hr) High concentration pre -weighed (methanol -14 d) � - Low cone pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes @ No Comments: Signature: Kr:i:s:t:i:n:a:::A-McAdams Date &Time: 16-1-/2-6/6_21 _09:32:1_9] F—P—age 13 o-f-1 —5-] Page 8 of 10 MMW SUBCONTRACT ORDER Certification: NELAC— "'ACE Waypoi tit Ana lytica I NC ­­ SC— Other 1010287 N/A. SENDING LABORATORY-, RECEIVING LABORkYORN: Waypoint Analytical Waypoint Analytical P. OBox 240543 2790 Whitten Road Charlotte, NC28224-0543 Nfemphis, IN 38133 Phone: 800-529-6364 Phone:(901) 213-2400 Fax: 704-525-0409 Fax: (901) 213-2440 Prpject,\Ianager; Terri W. Cole Anatvsis Due Expires Laboratoq ID Comments Sample III; 1010287-01 Solid San, pled: 01119/2108:26 (TAMS ATCLP Reactivity, Cyanide { S ub) 02/0 2/21 08:26 �aratcadra S SI ipvl hN. (1: I N 60,L- 21-026-0044 26657 01-26-2021 Wavy oml AnWiCal CharRohe 09'31 46 SUbconTrart # 1010287 Releas"I By _ Bate Page I of 2 Page 14 of 15 Page 9 of 10 Waypoint Analytical Cerlificatiow NELAC— USACE - NC SC Other 1010287 NIA SLN ,L)ING 1,AV0RVr0RV, RECEIV1,NG LABOkATQRY, Waypoint Analytical Waypoint Analytical, LLC P. 0. Box 24054") 2790 Whitten Road Charlotte, NC 28224-0543 Memphis, TN 38133 Phone: 8,00-529-6364 Phone -,(901) 213-2400 Fax: 70,4-525-0409 Fax: (901) 213-2440 Projeci Manager: Terri W. Cole Analysis Due Expires Laboratory ID Comments Sample ID: 1010287-41 Solid sampk&O 1/] 9/2108.26 Class A TCLP Reactivity, Sulfide (Sktb) 0 1126Q] 08:26 Containers S4 1 U d 1 K7 tM 21-026-0044 25657 01 '26-207.1 WavDtwni AnaNlical Charlotte 09.31:46 Subconlract # 1010287 Page 10 of 10 Page 2 of 2 L Page 15 oF1 5 Waypoint.(2) ANALYTlC,4,L-- 8/13/2021 Town of Mooresville/RR WWTP Whitney Munroe 369 Johnson Dairy Rd. Mooresevifle, NC, 28115 Ref. Analytical Testing Lab Report Number: 21-200-0031 Client Project Description: Class A Dear Whitney Munroe: 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 war w.waypointan,aiyticall.com Waypoint Analytical, LLC (Charlotte) received sample(s) on 7/19/2021 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, 60A'd Terri W Cole Laboratory Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page I of 21 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.5291.6364 www,waypolintanalytical.com MIN Laboratory ID: WP CNIC: Waypolinit Analytical Carolina, Inc. (C), Charlotte, NC State Program Lab ID Expiration Date North Carolina State Program 37735 07/31/2022 North Carolina State Program 402 12/31/2021 South Carolina State Program 99012 07/31/2021 South Carolina State Program 99012 12/31/2021 Laboratory ID: WP M'TN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2022 Arkansas State Program 88-0650 02/07/2022 California State Program 2904 06/30/2022 Forida State Program - NELAP E871157 06/30/2022 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2021 Illinois State Program - NELAP 200078 10/10/2022 Kentucky State Program 80215 06/30/2022 Kentucky State Program KY90047 12/31/2021 Louisiana State Program - NELAP LA037 12/31/2021 Louisiana State Program - NIELAP 04015 06130/2022 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2021 Oklahoma State Program 9311 08/31/2021 Pennsylvania State Program - NELAP 68-03195 05/31/2022 South Carolina State Program 84002 06/30/2022 South Carolina State Program 84002 06/30/2022 Tennessee State Program 02027 02/11/2023 Tennessee A21-A ISO 170252017 4313.01 10131/2021 Texas State Program - NELAP T104704180 09/30/2021 Virginia State Program 00106 06/30/2022 Virginia State Program - NELAP 460181 09/14/2021 Page 1 of 1 00016/21-200-0031 Page 2 of 21 0 (D Waypoint ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Maln 704,529,6364 wwwwaypointanal"cal,com Sample Summary Table Report Number: 21-200-0,031 Client Project Description: Class A Lab No Client Sample ID Matrix Date Collected Date Received Method Lab 111) 91977 Class A Sludge 07/19/2021 08:55 07/19/2021 13:45 91977 Class A Sludge 07/19/2021 08:55 07/19/2021 13:45 6010D WP MTN 91977 Class A Sludge 07/19/2021 08:55 07/19/2021 13:45 SW-1311 WP MTN 91977 Class A Sludge 07/19/2021 08:55 07/19/2021 13:45 8081A WP MTN 91977 Class A Sludge 07/1912021 08:55 07/19/2021 13:45 8151A WP MTN 91977 Class A Sludge 07/19/2021 08:55 07/19/2021 13:45 8270C WP MTN 91977 Class A Sludge 07/19/2021 08:55 07/19/2021 13:45 7470A WP MTN 91978 Class A Solids 07/19/2021 08:55 07/19/2021 13:45 91978 Class A Solids 07/19/2021 08:55 07/19/2021 13:45 350.1 AES 91978 Class A Solids 07/19/202108:55 07/19/2021 13:45 6010D WP MTN 91978 Class A Solids 07/19/2021 08:55 07/19/2021 13:45 4500NORGD-2011 WP MTN AES: Analytical Environmental Services, Inc., Atlanta, GA WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 3 of 21 Waypoint(2) ANALYTlCAL Client-, Town of Mooresville/RR WWTP Project, Class A Lab Report Number: 21-200-0031 Date: 8/13/2021 449 Springbrook Rd, Charlotte, NC 28217 Main 704,529.16,364 www.waypointanalyticai.com CASE NARRATIVE Fecal Coliform MPN Method 9221E-2011 Sample 91978 (Class A) QC Batch No: V6750 Sediment from sample likely inhibited gas collection in the inverted tubes of the 10 mL sample volume. Bubbles were observed in the MPN tube; however, they were absent from the inverted capture tube. Metals Analyses Method 6020B QC Batch No: V6931A/6905 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly, QC Batch No: V6983N6905 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Sample 92143 Analyte: Potassium QC Batch No: V6983N6905 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Nickel QC Batch No: V6931/V6905 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Zinc QC Batch No: V6931/V6905 The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control acceptance ranges. Matrix interference is suspected Solids Total Mercury Analysis - CVAA Method 7471B Sample 91978 (Class A) Analyte: Mercury QC Batch No: V6703/V6690 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly Analysis note for PAN PAN Equation = 0.3 * (TKN — Ammonia) + 0.5 * (Ammonia) + Nitrate -Nitrite PAN = 0.3 * (16200 — 2810) + 0.5 * (2810) + 3.02 PAN = 5425 mg/Kg Equation uses Mineralization Rate (MR) for Aerobically Digested Solids (0.3) Page 4 of 21 Wayl'Ont(2)POI ANALYTICAL Analysis note for SAR 449 Springbrook Rd, Chadotte, NC 28217 Main 704-529.6364 www.waypointanalytical.com SAR = [ Na ] / SQRT f ( [Ca] + [Mg) ) / 2) Concentrations for Na, Ca, and Mg are expressed in milli -equivalents per liter, and SQRT designates taking the square root of the operand in parentheses, SAR = (881/23) / SQRT ((l 5100/20 + 2320/12.2)/2) SAR = 38 / SQRT ((755 + 190) / 2) SAR = 38121.7 SAR = 1,72 Page 5 of 21 449 $pringbrook Rd, Charlotte, NC 28217 Main 704,529,6364 wwwwaypointanalytfcal.co rn Report Date 08/13/2021 Received 07/19/2021 Report Number : 21-200-0031 REPORTOFAIVALYSIS Lab No : 91977 Matrix: Sludge Sample ID : Class A Sampled: 7/19/20,218.55 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method TCLP Herbicide Extraction Leachate 1 07/21/21 13:00 JAN SW-1311 TCLP Metals Extraction Leachate 1 07/21/21 13:00 JAN SW-1311 TCLP Pesticide Extraction Leachate 1 07/21/21 13:00 JAN SW-1311 TCLP SVOC Extraction Leachate 1 07/21/21 13:00 JAN SW-1311 TCLP VOC ZHE Extraction leachate 1 07/20/21 13:45 TBL SW-1311 (ZHE) Analytical Method. 6010D Prep Batch(es): L565880 07/27/21 13:00 Prep Methods 3015A Test Results Units MDL MOIL DF Date / Time By Analytical Analyzed Batch TCLP Arsenic <0.250 mg/L 0,056 0.250 1 07/28/21 12:49 TJS L566040 TCLP Barium <0.250 mg/L 0.040 0.250 1 07/28/21 12:49 TJS L566040 TCLP Cadmium < 0. 0500 mg/L 0.0030 0,0500 1 07/28/21 12:49 TJS L566040 TCLP Chromium <0.100 mg/L 0.038 01100 1 07/28/21 12:49 TJS L566040 TCLP Lead <0.100 mg/L 0,024 0.100 1 07/28/21 12:49 TJS L566040 TCLP Selenium <0.500 mg/L 0,034 0.500 1 07/28/21 12:49 TJS L566040 TCLP Silver <0.0500 mg/L 0.023 0.0500 1 07/28/21 12:49 TJS L566040 Qualifiers/ DF Dilution Factor J Estimated value Definitions MQL Method QuantitaUon Limit Page 6 of 21 Report Number : 21-200-0031 Lab No : 91977 Sample ID : Class A Analytical Method: 7470A Prep Method: 7470A Test TCLP Mercury Analytical Method: 8081A Prep Method: 3510C Test TCLP Endrin TCLP gamma-61-1C TCLP Methoxychlor TCLP Toxaphene TCLP Chlordane TCLP Heptachlor Epoxide TCLP Heptachlor Surrogate: Decachlorobiphenyl Surrogate: Tetra cftro-m-xylen e Analytical Method: 8151A Prep Method: 8151A Test 449 Sp,ringbrook Rd, Charlotte, NC 28217 Main 704.52!9.6364 www,waypointanalytical.com Report Date 08/13/2021 Received 07/19/2021 REPORT OFANAL YSIS Matrix: Sludge Sampled: 7/19/20218:55 Prep Batch(es): L565308 07/23/21 10:00 Results Units MDL MOL DF Date / Time By Analytical Analyzed Batch <0,0200 mg1L 0.0017 0.0200 1 07/23/2113:55 DDB L565450 Prep Batch(es): L565400 07/23/21 13:00 Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch <0,001600 mg/L 0.()0()800 0.001600 10 07/26/21 19:54 VIC L565844 <0.001600 mg/L 0,000800 0.001600 10 07/26/21 19:54 VIC L565844 <0.001600 mg/L 0.000800 0.001600 10 07/26/21 19:54 VIC L565844 <0.01200 mg/L 0,006000 0.01200 10 07/26/21 19:54 VIC L565844 <0.008000 mg/L 0,004000 0.008000 10 07/26/21 19:54 VIC L565844 <0.001600 mg/L 0,000800 0.001600 10 07/26/21 19:54 VIC L565844 <0.001600 mg/L 0,000800 0.001600 10 07/26/21 19:54 VIC L565844 52.29 Limits: 34-116% 10 07/26/21 19:54 L565844 54.29 Umits: 25-123% 10 07/26/21 19:54 L565844 Prep Batch(es)-, L565473 07/23/21 16:15 Results Units MDL MQL DF Date I Time By Analytical Analyzed Batch TCLP 2,4-D <0.0200 mg/L 0.0100 0.0200 1 07/27/21 02:36 VIC L565886 TCLP 2,4,5-TP (Silvex) <0.0020 mg/L 0.0010 0.0020 1 07/27/2102:36 VIC L565886 Surrogate: DCAA 56,00 Limits: 20-120% 1 07/27/2102:36 L565886 Qualifiers/ DF Dilution Factor 3 Estimated value Definitions MQL Method Quantitation Limit Page '7 of 21 Report Number: 21-200-0031 449 Springbrook Rd, Charlotte, NIC 28217 Main 704,529,6364 www.waypo�inta:na:lyVcal.com REPORT OFANAL YSIS Report Date 08/13/2021 Received 07/19/2021 Lab No : 91977 Matrix: Sludge Sample ID: Class A Sampled: 7/19/20218:55 Analytical Method.- 8260D Prep Satch(es): V6806 07/21/21 09:30 Prep Method: 5030E Test Results Units MDL MQL DF Date I Time By Analytical Analyzed Batch TCLP Benzene <0.0050 mg/L 0.0033 0.0050 10 07/21/21 20:12 JLB V6807 TCLP Carbon Tetrachloride <0.0200 mg/L 0.0054 0.0200 10 07/21/21 20:12 JLB V6807 TCLP Chlorobenzene <0,0050 mg/L 0.0033 0.0050 10 07/21/2120:12 JLB V6807 TCLP Chloroform <0.0050 mg/L 0.0047 0.0050 10 07/21/2120:12 )LB V6807 TCLP 1,4-Dichlorobenzene <0.0050 mg/L 0.0042 0.0050 10 07/21/2120:12 JLB V6807 TCLP 1,2-Dichloroethane <0.0050 mg/L 0.0040 0.0050 10 07/21/2120:12 JLB V6807 TCLP IJ-Dichloroethene <0.0050 mg/L 0.0034 0.0050 10 07/21/2120:12 JLB V6807 TCLP Methyl Ethyl Ketone (MEK) 0.156 mg/L 0,0078 0,0050 10 07/21/2120:12 JLB V6807 TCLP Tetrachloroethene <0.0050 mg/L 0,0030 0.0050 10 07/21/2120:12 JLB V6807 TCLP Trichloroethene <0,0050 mg/L 0.0046 0,0050 10 07/21/21 20:12 JLB V6807 TCLP Vinyl Chloride <0.0050 mg/L 0.0041 0,0050 10 07/21/21 20:12 JLB V6807 Surrogate: 4-Bromofluorobenzene 103 Limlts: 80-124% 10 07/21/2120:12 JLB V6807 Surrogate: Dibromofluaromethane 105 Limits: 75-129% 10 07/21/21 20:12 JLB V6807 Surrogate! Toluene-dS 95.2 Limits: 77-123% 10 07/21/21 20:12 JLB V6807 Analytical Method: 8270C Prep Satch(es): L565579 07/26/2109:00 Prep Metlhod, 3510C Test Results Units MDL MOL DF Date I Time By Analytical Analyzed Batch TCLP 2-Methylphenol <0.100 mg/L 0.025 0.100 5 07/26/21 18:13 BGV L565794 TCLP 3&4 Methylphenol <0.200 mg/L 0.025 0.200 5 07/26/21 18:13 BGV L565794 TCLP 2,4-Dinitrotoluene <0.100 mg/L 0.025 0.100 5 07/26/21 18:13 BGV L565794 TCLP Hexachlorobenzene <0A00 mg/L 0.025 0.100 5 07/26/21 18:13 BGV L565794 Qualifiers/ DF Dilution Factor j Estimated value Definitions MQL Method Quantitation Limit Page 8 of 21 Report Number : 21-200-00,31 449 Sprin:gbrook Rd', Charlotte, NC 28217' Main 704,529,6364 www�waypointanalytical.com REPoRr OFANAL YSrS Report Date 08/13/2021 Received 07/19/2021 Lab No : 91977 Matrix: Sludge Sample ID : Class A Sampled: 7119/20218:55 Analytical Method: 8270C Prep Batch(es): L565579 07/26/21 09:()0 Prep Method: 3510C Test Results Units MDL MQL DIF Date I Time By Analytical Analyzed Batch TCLP HexacWorobutadiene <0.100 mg/L 0.025 0.100 5 07/26/21 18:13 BGV L565794 TCLP Hexachloroethane <0.100 mg/L 0.025 0.100 5 07/26/21 18J3 .BGV L565794 TCLP Nitrobenzene <0.,100 mg/L 0.025 0,100 5 07/26/21 18:13 BGV L565794 TCLP Pentachlorophenol <0.200 mg/L 0.025 0.200 5 07/26/21 18:13 BGV L565794 TCLP Pyridine <0.100 mg/L 0.025 0100 5 07/26/21 18:13 BGV L565794 TCLP 2,4,5-Trichlorophenol <0.100 mg/L 0.025 0.100 5 07/26/21 18:13 BGV L565794 TCLP 2,4,6-Trichlarophenol <0.100 mq/L 0.025 0.100 5 07/26/21 18:13 BGV L565794 Surrogate: TCLP 2,4,6-Tribromophenol 54,3 Limits: 42-102% 5 07/26/21 18:13 BGV L565794 Surrogate: TCLP 2-Fluorobiphenyl 410 Limits: 24-86% 5 07/26/21 18:13 BGV L565794 Surrogate. TCLP 2-Fluorophenal 16,,8 Limits: 13-37%® 5 07/26/21 18:13 BGV L565794 Surrogate: TCLP 4-Terphenyl-cI14 66.8 Limits: 30-122% 5 07/26/21 18:13 BGV L565794 Surrogate: TCLP Nitrobenzene-d5 44.3 Limits; 25-78% 5 07/26/21 18:13 BGV L565794 Surrogate: TCLP Phenol-d6 12,0 Limits: 9-27% 5 07/26/21 18:13 BGV L565794 Qualifiers/ DF Dilution Factor 7 Estimated value Definitions MQL Method Quantitation Limit Page 9 of 21 Report Number: 21-200-0031 449 Springbrook Rd, Charlotte, NC 28217' Main 704,529.6364 www.waypointanailytiCal.com REPoRrOFANALYSIS Report Date 08/13/2021 Received 07/19/2021 Lab No : 91978 Matrix: Solids Sample ID : Class A Sampled: 7/19/2021 Sz55 Test Results Units MDL MOL DF Date / Time By Analytical Analyzed Method Fecal Coliform MPN/g 17.8 MPN/g - dry 2.0 2.0 1 07/19/21 14:34 ENM 9221E-2011 Sodium Absorption Ratio 1.72 Ratio 0.010 0.010 20 07/26/2121:02 CALCULATION Plant Availabie Nitrogen 5680 mg/Kg - dry 1 08/13/2100:00 CALCULATION Moisture 4.57 % 1 07/26/21 16:30 EDV SW-DRYVVT Nitrate+Nitrite-N 3.02 mg/Kg - dry 1.06 1 07/22/21 10:50 9056A pH 6.19 SM° 1 07/23/21 11:15 CL3 9045D Total Solids 95.4 % 0 0.010 1 07/26Y21 16:30 EDV 2540G-2011 Total Kjeldahl Nitrogen 16200 mg/Kg - dry 322 649 10 07/27/21 15:58 CLP 4500NORGD-2011 Phosphorus 18700 mg/Kg - dry 28,9 52.4 10 07/29/2123:11 TJS 6010D Aluminum 25300 mg/Kg - dry 8.02 52.7 20 07/26/2121:02 EDV 6020B Arsenic 2.80 mg/Kg - dry 0,198 2A1 20 07/26/2121:02 EDV 6020B Cadmium <1.06 mg/Kg - dry 0,116 1.06 20 07/26/21 21:02 EDV 6020E Calcium 15100 mg/Kg - dry 48.4 211 20 07/26/2121:02 EDV 6020B Copper 287 mg/Kg - dry 0.948 5.27 20 07/26/2121:02 EDV 6020E Lead 11.3 mg/Kg - dry 0,738 5.27 50 07/27/21 18:09 EDV 6020B Magnesium 2320 mg/Kg - dry 13.9 52.7 20 07/26/2121:02 EDV 6020B Mercury (Total) 0.346 mg/Kg - dry 0.0251 0.0629 2 07/20/21 14:37 EDV 7471B Molybdenum 14.8 mg/Kg- dry 0.358 2.11 20 07/26/2121:02 EDV 6020B Nickel 14.,3 mg/Kg - dry 0.505 111 20 07/26/2121:02 EDV 6020E Potassium 2290 mg/Kg - dry 73.8 527 50 07/27/21 18:09 EDV 6020B Selenium 4.24 mg/Kg - dry 1.90 4.21 20 07/26/21 21�02 EDV 6020B Sodium Sal mg/Kg - dry 42.1 211 20 07/26/2121:02 EDV 60206 Quallifiers/ DF Dilution Factor j Estimated value Definitions L Limit Exceeded MQL Method Quantitation Limit Page 10 of 21 449 Springb:rook Rd, Charlotte, NC 28217 Mlain, 704.529,636A www.waypointanalytical,corn, Report Date 08/13/2021 Received 07/19/2021 Report Number : 21-200-0031 REPORTOFANALYSIS Lab No : 91978 Matrix: Solids Sample ID : Class A Sampled: 7/19120218:55 Test Results Units MDL MOIL DF Date I Time By Analytical Analyzed Method Zinc 625 mg/Kg - dry 4.84 21.1 20 07/26/21 21:02 EDV 6020E Qualifiers/ DF Dilution Factor i Estimated vaiue Definitions L Limit Exceeded MQL Method Quantitation Limit Page 11 of 21 F4 * ANAt,,y-riCAL, INC. NUM" Way.point Analytical PO Box 240543 Charlotte NC 282240543 ATTENTION Terri W Cole ffil Ion LABORATORY REPORT NUMBER 2107N67 DATE July 28, 2021 Pritnary Data Review By Secondary Data Review By Chris Pafford Project Manager, AES PLEASE NOTE: Ashley Amick Project Manager, Access Analytical aamick@axs-ine.com Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc),, 3080 Presidential Drive, Atlanta, GA 30340. AES is SCDHEC certified laboratory # 98016, NCDENR certified tab # 562, GA certified tab # FL-E87582, NFLAP certified laboratory # E87582 AIHA-LAP,LLC Laboratory ID: 100671 for Industriall-lygiene samples (Organics, Metals, PCM Asbestos, Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal) Direct Examination. Local support services for this project are provided by Access Analytical, Inc, Access Analytical is a representative ofAES serving client in the SC/NC/GA areas. All questions regarding this report should be directed to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243 Page 12 of 21 Pagel of 7 —Z cn C-3 0 0 MN� I ri Amy. in qLrl Ln CU 0 36 CL E Y I rGM14 a 0 (D .ff 0- u 0 -0 J3 u < CA m , c T OL 0� rq Ln U L6 Ln w 44 0 Analytical Environmental Services, Inc Date: 28-Jul-21 Client: Waypoint Analytical Project: 21-200-0031 Case Narrative Lab ID: 2107N67 Sample Receiving Nonconformance: An additional unlabeled 250ml plastic bottle filled with aqueous matrix was received but not listed on the Chain of Custody. The laboratory did not proceed with analysis on this bottle per Ashley Amick via email 07-22-21 as it was a temperature blank. Page 14 of 21 Page 3 of 7 Analytical Environmental Services, Inc Date: 28-7ul-2.1 Client: Waypoint Analytical Client Sample 1D: 91978 Lab Order 2107N67 `rag Number: Class A Project Name. 21-200-0031 Collection bate: 7/1912021 8:55.00 AM Lab ID: 21071`wT67-001A Matrix: Soil Analyses Result Reporting Y tual fiIDL Limit Units BatchID Dl late Analyzed Analyst Nitrogen, Ammonia (as N) Extractable E350.1 MOD (E350.1) Nitrogen, Ammonia (As N) Extractable 2810 53.2 101 -g/Kg dry 319533 10 07/27/2021 18:32 KV PERCENT MOISTURE D2216 Percent Moisture 5.80 0 0 wt R460502 1 07123/2021 00:00 J"W Quali:fiers:. . Value exceeds maximum contaminant level BRL Nat Dmcted at MDL ll holding [:noes for preparation or analysis exceeded N Anedyac not NE:LAC certified B Analyte detected in the associated method bla lk ki Estimated value alcove ynanaatation. range S Spike Recovery outside holes due to matrix. > Greater than Result value J Estimated value detected below Reporting Limit Less than. Result value Page 15 of 21 Page 4 of 7 z Pa E O 11, 7E v [-] 7: a d, (U u U za CL CL 2�ro fu (U u u CJ O ug r- E -6 cp@� o C�co cc. * 0 C4# C- ti et E cr ai w c E 0 F= Ld 73 0 0 u u to c " U 'E ❑ C: 0 �v CL do 2L W 11 I a m M C 11 U C) 0 CL cu U Qj U V Q'i u -0 C, CL w 0 as E E 0 E u0 2 E CL E u . u . u U U kn ai E cu w -6 -o 0 0 Q u u u is :3 a) Q. CL E w w E 0 6 E 0 0 0 u u u El u Ll D u u 0 cu 0 fl w 0 u 0 "a -6 ai 103 "a 15 s ..c G000446 c 0 t co cc 0 E) C- ai 73 m w �u c 0 43 m 0 Cc Fv -M CL > -r- o -M CL W ftl Pam. E cL L iu IL ai > ro O E < C) ca E > 0 0 cu a 0 < m 3: w w C.) c j 2 c E CL co GJ to r cc ci 0 u m -E O U) w ej - :13 Ln vj -14 uc u) 0 Q> z �6 r-: 06 Cr C� N m L'n lt5 r-- 06 6 6 7A 20: 7T 0 6 cqof lt N CN ca u R CY o P4 ai rn aka Cd r- a. < Ln en ho Eli u O LaI cn 5 5 air cr cn U) V�l C/ Cl) oo a> r- 00 �o C> tn E z z Z Z 0. CL CD bf) bb Ln tc ON —bh CZ, C7, C�l C7, C) 00 0 iat 7acaa E E t4 cl) V) V) V) 75 ro cc Page 18 of 21 Page 7 of 7 0 0 Waypoint ANALYTICAL 449 Springbrook Rd, Charlotte, NC 282:L7 Main 704.529,6364 www,waypointanalytical.com Shipment Receipt Form Customer Number: 012�05 Customer Name: Town of Mooresville/RR WWTP Report Number: 21-200-0031 Shipping Method 0 Fed Ex 0 US Postal (# Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: ff-_15ER Shipping container/cooler uncompromised? Yes 0 No Number of coolers/boxes received Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? Yes 0 No COC agrees with sample label(s)? Yes 0 No COC properly completed Yes 0 No Samples in proper containers? Yes 0 No Sample containers intact? Yes 0 No Sufficient sample volume for indicated test(s)? Yes 0 No All samples received within holding time? Yes 0 No Cooler temperature in compliance? Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun, Yes 0 No Water - Sample containers properly preserved Yes 0 No 0 N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) [_ Low [_ Low concentration EnCore samplers (48 hr) conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes * No Comments: — — - — -------- — ---- Signature: 1Stacy LCruz Date & Time: L07/:19_/202_1 _14:0.45 Page 19 of 21 (jL L ZL 0 z Z 10 00 � M L m L L C cn 0 Cl) L m 01 L 0 m L .1. L - 0 Z n, 0 > L 0 MI L L 0 Z m 0 Z 0 L 0 R L:X 0 -61, z 0 L 0 w! 0 6 L L 7j' z > L < L. 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M. 3 lPPY z 0 rn CN C: Mc M -CM 2 r- Mo- x M M M M fy M Zz 0 0 L z z 'M N M I I 0 i dC. mM L L 9 FE P, W a L > M i: C) ui 'D 0 0' M 0 S > z > On I— rn z fir fA T (A zz M < M 0 _4 0 0 0 rM 6 2 'IF lx� 4 0, "09 CD 0 7: (D F 0 0 61 M M 0 10 Z4 T c: 0 z — z I () > z r7l Tb 0 0 7; U) <, rt nc 0 z :;I R z rn 'A z z 0 M M 0 Z z Page 21 of 21