HomeMy WebLinkAboutWQ0036723_Modification_20210922Initial Review
Reviewer Thornburg, Nathaniel D
Is this submittal an application? (Excluding additional information.)*
r Yes r No
Permit Number (IR)* WQ0036723
Applicant/Permittee Town of Mooresville
Applicant/Permittee Address 369 Johnson Dairy Rd , Mooresville NC 28115
Is the owner in BIMS? r Yes r No Is the facility in BIMS? r Yes r No
Owner Type Municipal
Facility Name Town of Mooresville DCAR
County Iredell
Fee Category Major Fee Amount $395
Is this a complete
application?*
r Yes r No Complete App Date 09/16/2021
Signature Authority
Signature Authority Title
Signature Authority Email
Document Type (if non -application)
Email Notifications
Does this need review bythe hydrogeologist?* r Yes r No
Regional Office
CO Reviewer
Admin Reviewer
Below list any additional email address that need notification about a new project.
Email Address
Comments to be added to email notfication
Comments for Admin
Comments for RO
Comments for Reviewer
Comments for Applicant
Submittal Form
Project Contact Information
Rease provide information on the person to be contacted by N B Staff regarding electibnittal, confirmation of receipt, other
.......................................................... electronic surece, aner correspondence.
_ -
Name * James Levis
Email Address*
jlevis@mooresvillenc.gov
Phone Number*
7046638341
Project Information
........ ..................................................................................................................................................... ......... ............ .... .... ........ ... ... .... .... .... ... ... ... .... .... .... ... .... .... ......... ......
Application/Document Type* r New (Fee Req ui red)
c Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* WO0036723
Fbs Current Existing pernit number
Applicant/Permittee * Town of Mooresville
Applicant/Permittee Address* 369 Johnson Dairy Rd , Mooresville NC 28115
Facility Name * Town of Mooresville DCAR
Please provide comments/notes on your current submittal below.
The Town of Mooresville wishes to modify our Distribution of Class A residuals permit to
increase our maximum residuals distribution from 900 Dry Tons/year to 1600 Dry Tons/year.
In this application package, we believe that all the requested information has been provided.
If additional information is needed, please see contact info at the bottom of this letter.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at nathaniel.thornburg@ncdenr.gov.
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Spedications, Calculations, Bc.)
Class A mod whole scan.pdf 25.59MB
upload only 1 RJFdocurnert (less than 250 M3). Mafliple documents rust be corrbined into one RDFfile unless file is larger than
upload lirit.
* W By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 9/8/2021
To: NCDWQ/AQtJIFER PROTECTION SECTION/LAND APPLICATION UNIT
Re: Modification for Class A Distribution Permit - Permit# WQO�036723
The Town of Mooresville wishes to modify our Distribution of Class A residuals permit
to increase our maximum residuals distribution from 900 Dry Tons/year to 1600 Dry
Tons/year. In this application package, we believe that all the requested information has
been provided, If additional information is needed, please see contact info at the bottom
of this letter.
Please see the attached documents referenced in the application, one original and two
copies.
A check in the amount of $395.00 made payable to NCDEQ.
Completed Distribution of Class A Residuals (DCAR 06-16) form.
Attachment t - Program inforination and flow diagram
Attachment 2 - Marketability Statement
Attachment 3 — Product label/information sheet.
Attachment 4 — Operation and Maintenance Plan.
Completed Residuals Source Certification (RSC 06-16) form
Attachment 5 — Vicinity Map.
Attachment 6 — Quantitative justification statement.
Attachment 7 — Sampling Plan.
Attachment 8 — Laboratory analytical data.
Thank you for your time and consideration.
Allison Kraft, Utilities Director
Phone 704-799-4066
Jamie Levis, WWTP Plant Manager
Phone 704-662-8341
Larry Hendren, WWTP Biosolids Coordinator
Phone 704-799-4063
1 lene.
--goA/.
State of North Carolina
DWR Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS
INSTRUCTIONS FOR FORM: DCAR 06-16 & SUPPORTING DOCUMENTATION
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted, the ADDlicant shall submit one original and two copies of the application and
supporting documentation
For more information, visit the Water Quality Permitting,5ection's Lon-DLY�hat' Per naittin�sx ChitIve.&qtg
General — This application is for treatment, storage, transport, distribution, land application, and/or marketing of Class A (or Equivalent}
residuals under 115AA -NC CQ r',1100.
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Distribution of Class A Residuals (FORM: DCAR 06-16):
Submit the completed and appropriately executed Distribution of Class A Residuals (FORM: DCAR 06-16) form. Please do
not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to
the application may be made, as long as the attachments are numbered to correspond to the section and item to which they
refer,
Z The project name should be consistent on the plans, specifications, etc,
Z The Applicant's Certification on Page 3 of this form shall be signed in accordance with 15A "" C NCA02T.0 1 Qom. An alternate
person may be designated as the signing official if a delegation letter, is provided from a person who meets the criteria in 15A
T LCA;C 02T ,o LQ0LbJ.
Z If this project is for a modification of an existing permit, submit one copy of the existing permit.
Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to
operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units.
B. Application Fee (New and Major Modification Application Packages)
N Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental
Quality (NCDEQ).
Facility Classification
Major (residuals permitted for distribution >— 3,000 dry tons/year) I
Minor (residuals permitted for distribution < 3,000 dry tons/year)
New Permit
$1,310
ME
Major Modification
$395
$245
' - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage;
adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted.
There is no fee for minor permit modifications.
C. Cover Letter (All Application Packages)
Z I,ist all items included in the application package, as well as a brief description of the requested permitting action,
INSTRUCTIONS FOR FORM: DCAR 06-16 Page] of3
D. Program Information (All Application Packages)
Provide a narrative explaining the following:
Z How the materials will be handled and transported from where the residuals were produced to where it will be treated.
How the residuals will be processed/treated (attach process flow diagram).
How leachate collection will be handled.
Where the residuals will be stored until processed,
How the final product will be distributed (packaging, bulk, etc.)
What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the
limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause
contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality.
Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed.
Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the
person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following
information:
Name and address of the person who prepared the residual that is sold or given away.
A statement that application of the residuals to the land shall be in accordance with the instructions on the label or
information sheet.
Z A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered.
Z A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored
residuals into any surface waters.
Z Information on all applicable setbacks in accordance with 15A NCAC 02T, I 108(b).
[g A statement that the residuals shall be applied at agronomic or recommended rates for intended uses,
E. Detailed Plans and Specifications (Application Involving New or Changes to Treatment or Storage Units)
El Submit detailed plans and specifications that have been signed, sealed, and dated by a NC Professional Engineer per .15A '
NC AC 02T .1 104(q). Specifications for standard equipment may only be omitted for municipalities with approved standard
specifications, but use of the standard specifications must be noted on each sheet of the plans.
El Plans must include the following minimum items: a general location map, a topographic map, plan and profile view of the
residuals treatment and storage units as well as the proximity of the residuals treatment and storage units to other utilities and
natural features within 500 feet of all treatment and storage facilities, and detail drawings of all items pertinent to the residuals
treatment and storage units. Depict minimum separations required in 15A NCAC 02T . I-L081q) on the plans,
El Specifications must include, at a minimum, the following for all items pertinent to residuals treatment and storage units:
description of materials to be used, methods of construction, quality of construction testing procedures to ensure the integrity
of the final product in accordance with 15 A NCAC 02T .1 104(a)(2)(13), including leakage and pressure testing as appropriate,
E] Plans and specifications must not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR
CONSTRUCTION, etc.) that indicate that they are anything other than final plans and specifications. However, the plans and
specifications may be labeled with the phrase: FINAL DESIGN — NOT RELEASED FOR CONSTRUCTION.
F. Engineering Calculations (Application Involving Now or Changes to Treatment or Storage Units)
El Submit all design calculations that have been signed, sealed, and dated by a NC Professional Engineer per .1 5A NCAC 02T
_L104U
G. Environmental Assessments (May be Required — See 15A C NAQ IC,0300)
Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include
information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals
treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for
the construction. of the subject facilities.
INSTRUCTIONS FOR FORM: DCAR 06-16 Page 2 of 3
H. Operation and Maintenance Plan (New and Renewal Application Packages)
EJ For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan.
Submit the O&M Plan in accordance with 15A N - CAC 02T I I - 10 and include at a minimum:
Operational functions; describe the operation of the program to show what operations are necessary for the program to function
and by whom the functions are to be conducted.
Maintenance schedules; may include equipments calibration, maintenance of signs, etc.
Safety measures; may include safety training program, manuals, signs, etc.
Z Spill response plan; including control, containment, remediation, emergency contact information, etc.
Z Inspection plan including the following information;
Z Names and titles of personnel responsible for conducting the inspections.
Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected
location(s) and inspection frequency are representative of the residuals management program.
Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event
that noncompliance is observed.
Sampling and monitoring plan including the following information;
Names and titles of personnel responsible for conducting the sampling and monitoring.
Detailed description of monitoring procedures including parameters to be monitored.
Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow,
and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling
plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet
pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual
sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected
by cold temperatures,
ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL
SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS:
F _E31"T T", 7T171 TAL 1�14ALITI
DIVISION OF WATER RESOURCES
WATER QUALITY PERMITTING SECTION
NON -DISCHARGE PERMITTING UNIT
By U.S. Postal Service:
1617 MAIL SERVICE CENTER
RALEIGH, NORTH CAROLINA 27699-1617
TELEPHONE NUMBER: (919) 807-6464
By Courier/Special Delivery:
512 N. SALISBURY STREET
RALEIGH, NORTH CAROLINA 27604
FAX NUMBER: (919) 807-6496
INSTRUCTIONS FOR FORM: DCAR 06-16 Page 3 of 3
I. APPLICANT INFORMATION:
1. Applicant's name: Town of Mooresville
Applicant type: El Individual M Corporation M General Partnership
M Federal M State Municipal 0 County
Signature authority's name per .1 5A NCAC 02T,0 106: Title:
Applicant's mailing address: PO Box 878
City: Mooresville State: NC Zip: 28115
Telephone number: Email Address:
2. Consultant's name: License Number (for P.E,):
Affiliation: [] On Staff Retained (Firm:
Consultant's mailing address: -
City: - State., Zip.
Telephone number: (—) = Email Address:
3. Fee submitted: $395.00 (See Instruction B)
M Privately -Owned Public Utility
1. Application is for (check all that apply):E] new, Z modified, El renewed permit
1 If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: WQ0036723
Date of most -recently issued pen -nit: 10/7/2013
Date of most -recently certified Attachment A (if different than the permit):
1. Name of residuals processing facility: Rocky River Wastewater Treatment Facility
City: Mooresville State: NC Zip: 28115-
Coordinates: Latitude: 35' 3 1'33 Longitude; 80' 46'56"
Datum: Level of accuracy:
Method of measurement: QPS
County where facility is located- Iredell
2. Facility contact (person familiar with residuals preparation):
Name: Larry Hendren Title: Biosolids, Coordinator
Mailing address: PO Box 878
City: Mooresville State: NC Zip: 28115-
Telephone number: (104) 799-4063 E-mail address: Iliendren@mooresvillene.gov
FORM: DCAR 06-16 Page I of 3
3. Is the residual process facility also the generator? 0 Yes; [:] No
If No, please specify delivery frequency and quantity of residual to be processed:
4. Length of residuals storage at facility: 180 days (Note: the Division requires minimum 30 days storage in units that are separate
from treatment system, i,e, not in clarifiers, aeration basins, etc.)
IV. RESIDUALS QUALITY INFORMATION:
Specify how these residuals will be distributed:
El sold or given away in bags or other containers; [I lawn (bulk); home garden (bulk);
Z other (explain); local farms for non-food cr_qps
Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a
load capacity of one metric ton or less.
2. Complete the following if residuals are to be mixed with other materials:
3
Approximate amounts of the residuals received and processed at the facility: 1600 dry tons per year.
4. Approximate amounts of the final product (processed residuals) to be distributed: 1600 dry tons per year.
5, Provide a description of the onsite storage management plan for the treated residuals (including estimated average and
maximum storage times prior to distribution): Mora e-is on a covered, and paved pad with dimensions I I F x 79' Average
storage time as �60d s. 1vlaximum story getime 180 days.
6. Does the facility have a stormwater management plan? Z Yes; [] No
Explain whether the treatment and storage areas are under roof or how storinwater runoff will be handled: Storage area is under
pgrmenant steel erected roof Pad .isalso slg2pd in the event of water intrusion so that the runoffwould be directed to a drainage
line that goes back to the head of the_plant,
V. RESIDUALS SOURCE INFORMATION- (Required for all new, renewed, or modified residuals source)
Complete and submit the attached Residuals Source Certification and all associated documentation,
Residuals Source
Certification
FORM: DCAR 06-16 Page 2 of 3
Professional Engineer's Certification: (Application Involving Now or Changes to Treatment or Storage Units)
attest that this application for
has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge
the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package
may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed
this material and have judged it to be consistent with the proposed design.
North Carolina Professional Engineer's Seal, Signature, and Date:
Applicant's Certification:
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T.0 105.
QkYes F-1 No, Explain;_
A -A Jr IVV k-lp llvq,�A 4,1
(Signature Authority's Name — PLEASE PRINT) (Title)
11(1— e-t-- Y.
attest that this application for O-U1V-
K a I
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or, the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water
Resources should condition of this permit be violated. I also understand that if all required parts of this application are not completed
and that if all required supporting information and attachments are not included, this application package will be returned to me as
incomplete.
Note: In accordance with North Carolina General Statutes §143-215.6A and §143-215.613, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed. $ 10,000 as well as civil penalties tip to $25,000 per violation.
Signature. Date:
FORM: DCAR 06-16 Page 3 of 3
State of North Carolina
WIT"M mlirtymNT
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
INSTRUCTIONS FOR FORM: RSC 0646
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted, the Applicantshall submit one original and two copies of the application and
supporting documentation
For more information, visit the Water Quality Permitting Section's lvoil-Disc&jr&.. Perinitting Unit
General — This certification provides detailed information of residuals source generating facility and its residuals quality for land
application, distribution, or disposal in accordance with 15A NCAC 02T, I 100. Do not submit this certification for review without
a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SIR 11-15).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Residuals Source Certification (FORM: RSC 11-15):
Z Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not
make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the
application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer.
For new or renewed permits, submit a separate certification for each source facility.
❑ For modified permits„ submit a separate certification for only those facilities that are affected by the proposed modification.
Complete the residuals source facility summary page. List all new, renewed, or modified facilities.
B. Residuals Source -Generating Facility Information:
For each source facility, attach the following:
Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Quidance for
Residuals Land ADDlication Pen -nits".
Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals
are to be generated, treated, processed, and stored at the facility.
Z Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item 1. 8.
Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of
the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed,
and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during
processing.
Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies
sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition,
ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and
vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as
they are to be land applied, distributed, and/or disposed.
C. Residuals Quality Information:
For each source facility, attach the following:
M Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification.
M Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector
attraction reduction requirements.
F For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please
attach analytical results of residuals generated from a similar facility along with the description of similarities of the two
facilities.
INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of I
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State of North Carolina
Department of Environmental Quality
Division of Water Resources
Division of Water Resources
FORM: RC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction 13.):
1. Facility Name: Rocky River Wastewater Treatment Facility
2. Facility permit holder is: r_1 Federal, Ej State, M Local Government, or Ej Private.
Facility permit issued by: 0 Div. of Water Resources, Div. of Environmental Health,
or � Other (explain:
3. Facility contact person and title: Larry Hendren
Complete mailing address: PO Box 878
City: Mooresville State: NC Zip: 28115
Telephone number: (204) 799-4063 E-mail address: Ihendren@mooresvillene.gov
4, Facility physical address: 369 Johnson Dairy Rd.
City: Mooresville State: NC Zip: 28115-
Coordinates: Latitude: 3 5' 3 V 3 3 Longitude: 80'46'56"
Datum: Level of accuracy:
Method of measurement; GPS
5. Purpose of the facility:
treatment of municipal wastewater, [I treatment of 100% domestic wastewater,
treatment of potable water, E] treatment of 100% industrial wastewater,
E] treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: _ % industrial and % domestic)
E] other (explain: _ ).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: 75 MGD and facility average daily flow: 5 MGD
8, Average amount of residuals being generated at this facility 1600 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: LIMA aerobic digestion. belt press to 14% solids, heatt(
Type and volume of residuals storage (i.e., outside of residuals treatment units): I1I'x79'covprLdpa
11. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1, Specify if residuals are regulated under:
Z 40 CFR Part 503 or 40 CFR Part 257.
Note: Only residuals that are generated during domestic/i-nunicipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257,
2, Specify if residuals are defined under fl 5 A..N.C.AC 02T. 1102(151 as:
Z Biological � Non -Biological
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, aninial
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems),
FORM: RSC 06-16 Page 1 of 5
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRk (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: M yes JE no.
If yes, list the number(s): _
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR �261,2 1 -
261.24: 11 yes E' no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Vvaypoint Anal tical and Date of analysis: 01/19/2021
Passed corrosivity test-, yes R no. pH: s.u. (2 pH < 12.5)
Passed ignitability test: yes R no. Flashpoint: - 'F (> 1401F)
Passed reactivity test: 0 yes Rno. FICN: mg/kg (<250) & H2S: - mg/kg (<500)
TCLP Parameter
Limit
(mg/1)
Result
(mg1l)
TCLP Parameter
Limit
(mg/1)
Result
(nigll)
Arsenic
5.0
<0.50
Hexachlorobenzene
0.13
"0.020
Barium
100.0
Hexachloro-1,3-Butadiene
0.5
<0.050
Benzene
0.5
<0.025
Hexachloroethane
3.0
<0.050
Cadmium
1.0
<0.050
Lead
5.0
-'0.050
Carbon Tetrachloride
0.5
<0.025
Lindane
0.4
Na
Chlordane
0.03
-0.0025
Mercury
0.2
<0.010
Chlorobenzene
100.0
<5
Methoxycblor
10.0
<0.00050
Chloroform
6.0
-0.30
Methyl Ethyl Ketone
200.0
<10
Chromium
5.0
--0.25
Nitrobenzene
2.0
'U50
m-Cresol
200.0
Na
Pentachlorophenol
100.0
<0,25
O-Cresol
200,0
Na
Pyridine
5.0
-0.25
p-Cresol
200.0
Na
Selenium
1.0
<0. 12
Cresol
200,0
Na
Silver
5.0
-0.25
2,4-D
10.0
Na
Tetrachloroethylene
0.7
<0.025
1,4-Dichloroberizene
7.5
<0.38
Toxaphene
0.5
<0.025
1,2-Dichloroethane
1, 1 -Dichloroethylene
2,4-Dinitrotoluene
Endrin
Heptachlor and its d:ro�x ide
I- :y�
0.5
0.7
0.13
0.02
�O008
<0.025
<0.035
Na
0.00050
�<O�_0005��
Trichlorocthylene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4,5-TP (Silvex)
Vinyl Chloride
0.5
400.0
2.0
1.0
0.2
<0.025
<0.25
<0. 10
Na
-'0.020
FORM: RSC 06-16 Page 2 of 5
4. Metals Determination. Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAQ 02T...,-J....I 0.5..
a. For DistributiotVLand Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory bVyponi Analytical and Date of analysis: 7/19/2021
Parameter
Ceiling
Monthly Average
Result
Concentration Limits
Concentration Limits
(ClassA & ClassB)
(Class A Only)
(mg1kg)
(mglkg)
(n7glkg)
Arsenic
75
41
2.80
Cadmium
85
39
-,1.06
Copper
4,300
1,500
287
Lead
840
300
11.3
Mercury
57
17
0346
Molybdenum
75
n✓a
14.8
Nickel
420
420
14.3
Selenium
100
100
4.24
Zinc
—
7,500
.............. ...
2,800
625
b. ror VurLace Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e,, on a dry weight
basis) for the following metal parameters:
Laboratory: _ and Date of analysis:
Distance from Disposal
Arsenic
Chromium
Nickel
Unit to Boundary to
Closest Property Line
(meters, check one)
(inglkg)
(niglkg)
(mg/kg)
E] > 0 but- 25
30
200
210
1- 25 but < 50
34
220
240
50 but - 75
39
260
270
75 but < 100
46
300
320
100 but< 125
53
360
390
125
62
450
420
Result (mg1kg)
FORM: RSC 06-16 Page 3 of 5
5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 95 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Wa pint Analytical and bate of analysis: 07/19/2021
Parameter
Result
(inglkg)
Aluminum
25300
Ammonia -Nitrogen
2810
Calcium
Magnesium
15100
2320
Nitrate -Nitrite Nitrogen
3.02
pH (Standard Unit)
6.1.9
Phosphorus
18700
Potassium
Sodium
2290
881
Total 1C.jeldahl Nitrogen
16200
Using the results listed in Item 11. 5b. above, calculate the sodium adsorption ration (SAR): 18
[Note: if residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This
rate is a (check one): X default value, or El actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
e. Calculate the :PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (111) Year PAN
Five -"Year
Maximum Adjusted PAN
(mg✓kg)
(mg1kg)
Surface
9,640
Injection/Incorporation
10,90
Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:
FORM: RSC 06-16 Page 4 of 5
7, Pathogen Reduction: Per 15A NCAC 02T. 11.06, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or EquivaIen
A fecal coliforin density that is demonstrated to be less than 1,000 MPN per grain of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
F1 Alternative I [ I 5A NCAC 02T. I 106(b)(3)(A)] - Time/Temperature Compliance.
[I Alternative 2 [15A NCAC 02T.1 106(b)(3)(B)l - Alkaline Treatment.
El Alternative 3 [15A NCAC 02T. I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
[] Alternative 4 (15A NCAC 02T.1 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova,
Z Alternative 5 [15A NCAC 02T. I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFR-P).
Specify one: composting, Z heat drying, heat treatment,
then-nophilic aerobic digestion, beta ray irradiation,
gamma ray irradiation, or pasteurization.
b. For Land Aolication of Class B:
El Alternative I [I 5A NCAC 02T. I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02TJ 106(c)(2)] - Process to Significantly Reduce Pathogens (PSR,P).
Specify one: E] aerobic digestion, 0 air drying, El anaerobic digestion,
El composting, or M lime stabilization.
c. For Surface Disposal:
,X Select One of the Class Act Equivalent Pathogen Reduction Alternatives in Item 11. 7a. above.
[] Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item If. 7b. above.
n Exempt - If Daily Cover Alternative is chosen in Item 11.8. below [15A NCAC 02T.1 106(a)(2)].
n Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution,
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02TJ 107, specify how residuals will meet the VAR requirements:
Fj Alternative I [15A NCAC 02T.1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
Alternative 2 [15A NCAC 02T.1 107(a)(2)1- 40-Day Bench Scale Test (Anaerobic Digestion),
Alternative 3 [15A NCAC 02T.1 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion),
E] Alternative 4 [15A NCAC 02T.1 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
Alternative 5 [15A NCAC 02T. I 107(a)(5)] - 14-Day Aerobic Processes.
Alternative 6 [15A NCAC 02T. I 107(a)(6)] - Alkaline Stabilization.
Alternative 7 [15A NCAC 02T. I 107(a)(7)] - Drying of Stabilized Residuals.
Alternative 8 [15A NCAC 02T. I 107(a)(8)] - Drying of Unstabilized Residuals,
Alternative 9 [15A NCAC 02T. I 107(a)(9)] - Injection.
Alternative 10 D 5A NCAC 02T. I 107(a)(I 0)] - Incorporation,
El Alternative for Surface Disposal Units Only - Soil/Other Material Cover [I 5A NCAC 02T. I 107(b)(2)].
0 Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution,
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5
Processed residual pellets are transported from dryer to covered facility where they
are stored from 30 — 180 days until recipients/end users are ready for delivery.
Recipients coordinate bulk hauling of residuals to their final destination through
correspondence with the Biosolids Coordinator.
Suggested nutrient limiting factors could be nitrogen, phosphorus, calcium and
aluminum.
Leachate is not a concern due to cover storage pad. However, pad is sloped to drainage
line as an extra safety precaution.
Process flow is explained below:
Waste activated sludge is pumped from WAS basin to one of two aerobic digesters.
Sludge is held in digesters before being pumped to a belt press.
The sludge is dewatered and pressed to achieve an approximate 14-16% cake which is
conveyed to a storage hopper.
The cake is than conveyed to the belt dryer system where it is heated for 4 hours at —20OF
to achieve 90% - 98% dry Class A pellet.
Dry pellets are conveyed to a dump truck.
Dump truck transfers product to the covered storage facility until ready for final bulk
shipping. Loaded trucks leaving the facility contain 4 — 8 tons of residuals depending on
the vehicle.
All Class A residuals are distributed to local farmers who land apply in accordance with
the Town of Mooresville Utilization Agreement. Residuals were applied at predetermined
agronomic rates by their own equipment. A total of 898 dry tons left the facility in 2020.
For 2021 we have more fainers signed up to use our product and are limited by our
permit distribution capacity of 900 dry tons per year.
No product label — Current Class A Utilization Agreement Included
Operations and Maintenance
The Town of Mooresville's Rocky River WWTP is permitted to discharge 7.5mgd. The
current average flow is 4.Omgd. The incoming waste stream is protected from excessive
fats, oils, and grease by our FOG program though a system of monitoring and permitting
local dischargers.
The incoming waste stream is further protected from heavy metals and other toxins through
our industrial Pretreatment program system of permitting and monitoring.
The plant's extended air activated sludge is managed by our Operations Supervisor and
Biosolids Coordinator. This sludge is pumped to one of two digesters. We operate the
digesters on a rotational basis filling and digesting one while removing sludge from the
other via our belt press. We rotate the digester functions approximately every 30 days.
The belt press solids are then transferred to the belt dryer system where we achieve an
average dryness of 95%.
All maintenance and calibration schedules are based on manufacturer's recommendations.
Safety protocols are based on OHSA requirements.
All wet processes are either contained or directed to an internal drainage system that leads
back to the head of the plant.
Inspection Plan
Daily inspections are performed by the Biosolids Coordinator of all equipment, safety, and
records. Any problems are reported to the Operations Supervisor.
Weekly inspections are perfonned by the Operations Supervisor of all equipment, safety,
and records. Any problems are reported to the Plant Manager.
Monthly inspections are performed by the Plant Manager of all equipment, safety, and
records. Any problems are reported to the Utilities Director.
Annual review performed by the Utilities Director.
Annual safety inspection performed by the Town's Safety Committee,
During operational inspections if any noncompliant solids are observed they will be
reintroduced to the system of disposed of in a lined landfill.
All safety issues will be corrected in house as soon as noted.
All records will be verified monthly by at least three people.
Sampling Plan
In house percent solids testing will be done by the Biosolids Coordinator and verified by
our Laboratory Analyst.
Samples will be sent to a certified commercial lab for WIT analyses.
Ignitability, corrosivity and reactivity will be conducted annually.
Metals, nutrients, VOC, SVOC, herbicides, pesticides, pH and pathogens will be conducted
quarterly.
Heat drying will use to meet pathogen reduction.
Drying of stabilized residuals will be used to meet vector attraction reduction.
Sample location will be at the exit of the dryer.
Sample type will be grab.
The figure presented in Section 1.8. was based upon the 2020 Class A Annual Sludge
Report. We are currently permitted to distribute 900 dry tons, and records state that a
total of 898 dry tons left the facility in 2020. Over the last 2 years we have been working
with Huber USA to make minor adjustments to the dryer to increase capacity and hourly
throughput. We are currently operating the dryer on a 24/7 basis except during periods of
maintenance or malfunction. Residuals distribution in 2020 was greater than any single
year in our records and with additional capacity we could have continued to dispense
farther into the fall and winter months. We currently have a high demand for our product
from local farmers and expect more growth in and around our community in the coming
years. For these reasons we are requesting to increase our annual residuals distribution to
1600 Dry Tons per year. We feel that elevated ceiling will allow us to serve our farmers
through the entire year without interruption and reduce the amount of Class A product we
would have to pay to dispose of via our landfill contract with BFI landfill in Concord.
Sampling Plan
In house percent solids testing will be done by the Biosolids Coordinator and verified by
our Laboratory Analyst,
Samples will be sent to Waypoint Analytical, a certified commercial lab for, TCLP
analyses.
Ignitability, corrosivity and reactivity will be conducted annually.
Metals, nutrients, VOC, SVOC, herbicides, pesticides, pH and pathogens will be conducted
quarterly,
Heat drying will use to meet pathogen reduction.
Drying of stabilized residuals will be used to meet vector attraction reduction,
Sample location will be at the exit of the dryer.
Sample type will be grab.
25;
;
Attachment S — Laboratory Data
The attached laboratory data was used to complete Residuals Source Certification (RS C
O6- !.
NORTH ROY COOPER QuCAROLINAality
Govr'Ilw
MIC14AEL S, REGAN
Saerptwy
UNDA CULPEPPER
S'n teHm A rw."Or
August 30, 2018
JAmEs ANDREW LEVIS — WWTP MANAGER
TOWN OF MOORESVILLE
POST OFFICE BOX 878
MOORESVILLE, NORTH CAROUNA 28115
Dear Mr. Levis:
Subject: Permit No. WQG036723
Town of Mooresville DCAR
Distribution of
Class A Residuals
Iredell County
In accordance with your permit renewal request received May 22, 2018, and subsequent additional
information received July 16, 2018, we are forwarding herewith Pemit No. WQ0036723 dated August 30,
2018, to the Town of Mooresville for the continued operation of the subject residuals management program.
Please note that this renewed pen. -nit shall become effective on October 1, 2018 (i.e, the day after the
expiration date of the existing permit).
This permit shall be effective from October 1, 2018 until September 30�, 2023, shall void Permit
No,, WQ0036723 issued November 7, 2013, and shall be subject to the conditions and limitations as
specified therein. Please pay particular attention to the monitoring requirements listed in Attachment A for
they may differ from the previous permit issuance, Failure to establish an adequate system for collecting
and maintaining the required operational information shall result in future compliance problems.
Please note the following permit conditions have been removed since, the last permit issuance
dated November 7,2013:
> Old Conditions 111.9. and 111.10, — The utilization agreement conditions are replaced by
Condition 111.9,
North Carolina Department of Environmental Quality I Division of Water Resources I Non -Discharge Branch
512 North Salisbury Street � 1617 Mait Service Center I Raleigh, North Carolina 27699-1617
919.707,3654
Mr, James Andrew Levis
August 30, 2018
Page 2 of 2
Please note the following permit conditions are new since the last permit issuance dated
Novem her 7, 2 013:
Condition 111.9. —This condition requires the Permitteeto inform all bulk receivers of residuals
that they are to comply with Conditions 11,8, (application at agronomic rate) and 111.8.
(conditions under which bulk residuals are not to be applied) of this permit,
If any parts, requirements or limitations contained in this permit are unacceptable, the Ponnittee
has the right to request an adjudicatory bearing upon written request within 30 days following receipt of
this permit, This request shall be in the form of a written petition, conforming to Chapter 150B of the North
Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail Service
Center, Raleigh, NC 27699-6714, Unless such demands are made, this pen -nit shall be final and binding.
If you need additional information concerning this permit, please contact Troy Doby at (919) 707-
3655 or troy .doby(amcderingov.
Sincerely,
?Dipda Culpepper, Interim Director
nLivision of Water Resources
cc: Iredell County Health Department (Electronic Copy)
Mooresville Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Laserfiche File (Electronic Copy)
Digital Permit Archive (Electronic Copy)
Central Files
fill
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as
amended, and other applicable Laws, Rules, and Regulations
• - �L �61•11,
Town of Mooresville
Iredell County
IN-96-H-0
continued operation of a residuals management program for the Town of Mooresville and consisting of the
distribution of Class A residuals generated by the approved facility listed in Attachment A with no discharge
of wastes to surface waters, pursuant to the application received May 22, 2018, and subsequent additional
information received by the Division of Water Resources, and in conformity with other supporting data
subsequently filed and approved by the Department of Environmental Quality and considered a part of this
permit. The use and disposal of residuals are regulated under Title 40 Code of Federal Regulations Part
503. This permit does not exempt the Pennittee fiorn complying with the federal regulations.
This permit shall be effective from October 1, 2018 until September 30, 2023, shall void Permit No,
WQ0036723 issued November 7, 2013, and shall be subject to the following specified conditions and
limitations:
I . No later than six months prior to the expiration of this permit, the Permittee shall request renewal of
this permit on official Division forms. Upon receipt of the request, the Division will review the
adequacy of the facilities described therein, and if warranted, will renew the permit for such period of
time and under such conditions and limitations as it may deem appropriate. Please note Rule 15A
NCAC 02T.0 I 05(d) requires an updated site map to be submitted with the permit renewal application.
[I 5A NCAC 02T .01 08(b)(2), 02T .0 1 05(d), 02T.0 109]
A �t
I . The subject residuals management program shall be effectively maintained and operated at all times so
there is no discharge to surface waters, nor any contravention of groundwater or surface water
standards, In the event the facilities fail to perform satisfactorily, including the creation of prolonged
nuisance conditions due to improper operation and maintenance, the Permittee shall immediately cease
distribution of residuals, contact the Mooresville Regional Office supervisor, and take any immediate
corrective actions,. [G.S. 143-215, 1]
WQ0036723 Version 2.0 Shell Version 180711 Page 1 of 10
2. This permit shall not relieve the Permittee of responsibility for damages to groundwater or surface
water resulting from the operation of this residuals management program. [15A NCAC 028 0200,
02L.0100]
3. Only residuals generated by the facility listed in Attachment A are approved for distribution in
accordance with this permit. [G. S , 143-215. 1 ]
4. Pollutant concentrations in residuals distributed or applied to any land application site shall not exceed
the following Ceiling Concentrations or Monthly Average Concentrations (i.e., dry weight basis):
Parameter
Ceiling Concentration
(milligrams per kilogram)
Monthly Average
Concentration
(milligrams per kilogram)
Arsenic
75
41
Cadmium
85
39
Copper
4,300
1,500
Lead
840
300
Mercury
57
17
Molybdenum
75
n/a
Nickel
420
420
Selenium
100
100
Zinc
7,500
2,800
[15A NCAC 02T. 1105]
5. Residuals that are distributed shall meet Class A pathogen reduction requirements in 15A NCAC 02T
.1106 (a) and (b), Exceptions to this requirement shall be specified in Attachment A. [ 15A NCAC 02T
.1106]
6. Biological residuals (i.e, residuals generated during the treatment of domestic or animal processing
wastewater, or the biological treatment of industrial wastewater, and as identified in Attachment A)
that are distributed shall meet one of the vector attraction reduction alternatives in 15A NCAC 02T
.1107(a). Exceptions to this requirement shall be specified in Attachment A. [15ANCAC 02T.1107]
WQ0036723 Version 2.0 Shell Version 180711 Page 2 of 10
7, Setbacks for Class Aland applied bulk residuals shall be as follows:
Setback by residual type
Setback Description
(feet)
Liquid Cake'
Private or public water supply
100
100
Surface waters (streams — intermittent and perennial,
perennial waterbodies,.Lnd wetlands...
100
25
Surface water diversions (ephemeral streams,
waterw , ditches)....
25
0
Groundwater lowering ditches (where the bottom of
the ditch intersects the SHWT)
25
0
Wells with exception to monitoring wells
100
100
Bedrock outcrops
25
0
Unless otherwise noted in Attachment A, "cake" residuals are those that have greater than 15%
solids by weight and can be stacked without flowing, as well as can be handled, transported and
spread as a solid (e,g, using a backhoe, front end loader, stinger spreader, broadcast spreader or
other equipment designed for handling solid materials) without leaving any significant liquid
fraction behind.
[I 5A NCAC 02T .11081
8. Bulk residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in exceedance
of agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen
requirements based on the determined Realistic Yield Expectations (RYE) using any of the following
methods:
a. Division's pre -approved site specific historical data for specific crop or soil types by calculating
the mean of the best three yields of the last five consecutive crop harvests for each field.
b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State
University Department of Soil Science (h //nutrients ) A copy
t!p�_ "h �
shall be kept on file and reprinted every five years in accordance with Condition IV.6.
c, If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the: RYE
and appropriate nutrient application rates reported in any of the following documents:
i. Crop management plan as outlined by the local Cooperative Extension Office, the North
Carolina Department of Agriculture and Consumer Services, the Natural Resource
Conservation Service, or other agronomist,
iL Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance
Document: Chapter I
(h4pL-//w-_vvNv-gU ,o _nca �v/SWC/tech/documents/9th Guidance Dog. �O0109�,df).
iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation
Services (MRCS), These plans must meet the USDA -MRCS 590 Nutrient Management
Standards
If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall
contact the Division to determine necessary action.
[I 5A NCAC 02T . I 109(b)(1)(k)]
WQ0036723 Version 10 Shell Version 180711 Page 3 of 10
The Permittee shall not distribute Class A residuals that have a sodium adsorption ratio (SAID) of I or
higher without prior written Division approval, The Permittee may seep approval by demonstrating
that the entity accepting the residuals is: aware of the effects of a high SAIL content- has agreed on
proper residual application rates; and has agreed to operational considerations to ensure that the high
SAR content will not adversely impact the receiving sites. Recommendations regarding sodium
application rate, soil amendments (e.g., gypsum, etc.) or a mechanism for maintaining site integrity and
conditions conducive to crop growth, can be obtained from the local Cooperative Extension Office, the
Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, allorth
Carolina Licensed Soil Scientist, or an agronomist, [15A NCAC 02T .0108(b)(1)]
(( I � I
tti M; 49"a= Or
1, The residuals management program shall be properly maintained and operated at all times, The
program shall be effectively maintained and operated as a non -discharge system to prevent any
contravention of surface water or groundwater standards. [ I SA NCAC 02T .1110]
2. The Permittee shall maintain an approved Operation and Maintenance Plan (O&M Plan) Modifications
to the O&M Plan shall be approved by the Division prior to utilization of the new plan, The O&M Plan,
at the minimum, shall include:
a, Operational functions-,
b. Maintenance schedules;
c. Safety measures;
d. Spill response plan;
e. Inspection plan including the following information:
i. Names and/or titles of personnel responsible for conducting the inspections;
ii. Frequency and location of inspections, including those to be conducted by the ORC, and
procedures to assure that the selected location(s) and inspection frequency are representative
of the residuals management program;
iii. Detailed description of inspection procedures including record keeping and actions to be taken
by the inspector in the event that noncompliance is observed pursuant to the noncompliance
notification requirements under the monitoring and reporting section of the permit;
f. Sampling and monitoring plan including the following information:
i. Names and/or titles of personnel responsible for conducting the sampling and monitoring,
ii. Detailed description of monitoring procedures including parameters to be monitored;
iii. Sampling frequency and procedures to assure that representative samples are being collected.
Fluctuation in temperature, flow, and other operating conditions can affect the quality of the
residuals gathered during a particular sampling event. The sampling plan shall account for any
foreseen fluctuations in residuals quality and indicate the most limiting times for residuals, to
meet pathogen and vector attraction reduction requirements (e.g, facilities that distribute
multiple times per year but have an annual sampling frequency, may need to sample during
winter months when pathogen reduction is most likely to be negatively affected by cold
temperatures).
[I 5A NCAC 02T. I 100]
WQO 03 6723 Version 2.0 Shell Version 180711 Page 4 of 10
3, Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC)
classification of the facility, the Permittee shall designate and employ a certified operator in responsible
charge (ORC) and one or more certified operators as back-up ORCs in accordance with 15A NCAC
08G.020 1, The ORC or his back-up shall visit the facilities in accordance with 15A NCAC 08G. 0204,
or as specified in the most recently approved O&M plan (i.e., see Condition IIL2), and shall comply
with all other conditions of 15A NCAC 08G. 0204. For more information regarding classification and
designation requirements, please contact the Division of Water Resources' Protection and Enforcement
Branch at (919) 707-9105. At the time of this permit issuance, a certified ORC is not required for the
subject Distribution of Class A Residuals program. [15ANCAC 02T.0117]
4. When the Permittee land applies bulk residuals, a copy of this permit and a copy of O&M Plan shall be
maintained at the land application sites during land application activities, [15A NCAC 02T
.0108(b)(1)]
5. When the Permittee transports or land applies bulk residuals, the spill control provisions shall be
maintained in all residuals transport and application vehicles, [15ANCAC 02T.1110]
6. When the Permittee land applies bulk residuals, adequate measures shall be taken to prevent wind
erosion and surface runoff from conveying residuals from the land application sites onto adjacent
properties or into surface waters. [G.S. 143-215.1]
7. When the Pennittee land applies bulk residuals, a suitable vegetative cover shall be maintained on land
application sites onto which residuals are applied, or application shall be in accordance with the crop
management plan outlined by the local Cooperative Extension Office, the Department of Agriculture
and Consumer Services, the Natural Resource Conservation Service, or an agronomist and as approved
by the Division. [15A NCAC 02T .1109(b)(1)]
8. Bulk residuals shall not be land applied under the following conditions:
a. If the residuals are likely to adversely affect a threatened or endangered species listed under section
4 of the Endangered Species Act or its designated critical habitat;
b, If the application causes prolonged nuisance conditions;
c. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface
water or, groundwater standards;
d. If the land is flooded, frozen or snow-covered, or is otherwise in a condition such that runoff of the
residuals would occur;
e. Within the I 00-year flood elevation, unless the bulk residuals are injected or incorporated within a
24-hour period following a residuals land application event;
f During a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours
following a rainfall event of 0.5 inches or greater in a 24-hour period;
& If the slope is greater than 10% for surface applied liquid residuals, or if the slope is greater than
18 % for injected or incorporated bulk liquid residuals;
h. If the land does not have an established vegetative cover unless the residuals are incorporated or
injected within a 24-hour period following a residuals land application event. Any field that is in a
USDA no -till program shall be exempted from meeting this vegetative cover requirement;
i. If the vertical separation between the seasonal high water table and the depth of residuals
application is less than one foot;
j. If the vertical separation of bedrock and the depth of residuals application is less than one foot;
k. Application exceeds agronomic rates.
[15A NCAC 02T .1109]
WQ0036723 Version 2.0 Shell Version 180711 Page 5 of 10
9. The Permittee shall notify all third -party entities receiving bulk distributed Class A residuals that land
application activities occurring on the third-party's property shall meet the requirements in 15A NCAC
02T .1 108(b)(1) and 02T .1 109(b) (i.e., Conditions 11.8. and RIX, respectively). [I 5A NCAC 02T
.114i3 (4)]
10, All residuals shall be adequately stored to prevent untreated leachate runoff. The finished product may
be placed on a concrete pad, placed under shelter or physically covered until it is distributed to a third -
party entity. If bulk residuals are to be applied, the residuals may be staged at the application site for
up to 30 days for biological residuals,, and 60 days for non -biological residuals. If an alternate storage
site is used, approval must be obtained from the Division. [15ANCAC 02T.0108(bXl)]
11. A label shall be affixed to the bag or other container in which residuals are sold or given away for land
application, or an information sheet shall be provided to the person who receives Class A residuals. At
a minimum, the label or information sheet shall contain the following:
a. The name and address of the person who prepared the residuals;
b. A statement that residual land application is prohibited except in accordance with the instructions
on the ➢abel or information sheet;
c. A statement identifying that this material shall be prevented from entering any public or private
water supply source (including wells) and any surface water (e.g., stream, lake, river, wetland, etc.);
d. A statement that the residuals shall be applied at agronomic rates and recommended rates for its
intended use,
[I 5A NCAC O2T.1109(a)]
12. The Permittee shall not distribute bulk residuals to any person or entity known to be applying residuals
contrary to the conditions of this permit. The Permittee shall report to the Mooresville Regional Office
as per reporting conditions under Condition IV. 8. any person or entity known to be applying residuals
contrary to the condition of this permit, [I 5A NCAC 02T .I 103(a)]
WQ0036723 Version 2,0 Shell Version 180711 Page 6 of 10
1, Any Division -required monitoring (including groundwater, plant tissue, soil and surface water
analyses) necessary to ensure groundwater and surface water protection shall be established, and an
acceptable sample reporting schedule shall be followed. [15A NCAC 02T .0108(c)]
1 Residuals shall be analyzed to demonstrate they are non -hazardous under the Resource Conservation
and Recovery Act (RCRA). Residuals, that tests or is classified as a hazardous or toxic waste under 40
CFR Part 261 shall rant be used or disposed under this permit. The analyses [corrosivity, ignitability,
reactivity, and toxicity characteristic leaching procedure (TCLP)l shall be performed at the
frequency specified in Attachment A, and the Permittee shall maintain these results for a minimum of
five years. Any exceptions from the requirements in this condition shall be specified in Attachment A.
The TCLP analysis shall include the following parameters (the regulatory level in milligrams per liter
is in parentheses):
Arsenic (5.O1)
1,4-Dichlorobenzene (7.5)
Nitrobenzene (2.0)
Barium (100.0)
1,2-Dichloroethane (0.5)
Pentachloropheno,l (10H)
Benzene (0.5)
1, 1 -Dichloroethylene (0.7)
Pyridine (5.0)
Cadmium (1,0)
2,4-Dinitrotoluene (0.13)
Selenium (1.0)
Carbon tetrachloride (0,5)
Endrin (0.02)
Silver (5.0)
Chlordane (0.03)
Hexachlorobenzene (0,13)
Tetrachloroothylene (03)
Chlorobenzene (100.0)
Heptachlor (and its hydroxide)
(0.008)
Toxaphene (0.5)
Chloroform (6,0)
Chromium (5.0)
Hexachloro-1,3-butadiene (0'.5)
Hexachloroethane (3.0)
Trichloroethylene (0.5)
2,4,5-Trichlorophenol (400'.0)
m-Cresol (200.0)
Lead (5.0) 1
2,4,6-Trichloropbenot (2.0)
o-Cresol (200.0)
Lindane (0.4)
2,4,5-TP (Silvex) (1,0)
p-Cresol (200.0)
Mercury (0.2)
Vinyl chloride (0.2)
Cresol (2001.0)
Methoxychlor (10.0)
2,4-D (10,0),
Methyl ethyl ketone (200,0)
Once the residuals have been monitored for two years at the frequency specified in Attachment A, the
Permittee may submit a permit modification request to reduce the frequency of this monitoring
requirement. In no case shall the monitoring frequency be less than once per permit cycle,
[15A NCAC 13A.0102(b), 02T.1 101, 02T.1 105]
WQ0036723 Version 2,0 Shell Version 180711 Page 7 of 10
3. An analysis shall be conducted on the residuals from each source generating facility at the frequency
specified in Attachment A, and the Permittee shall maintain the results for a minimum of five years.
The analysis shall include the following parameters:
Aluminum
. . ........
Mercury
Potassium
Ammonia -Nitrogen
Molybdenum
Selenium
Arsenic
Nickel
Sodium
Cadmium
Nitrate -Nitrite Nitrogen
Sodium Adsorption Ratio
(SAR)
Calcium
Percent Total Solids
TKN
Copper
pH
Zinc
Lead
Phosphorus
Magnesium
Plant Available Nitrogen
(by calculation)
[15A NCAC 02T,, 11011
4. Residuals shall be monitored for compliance with pathogen and vector attraction reduction
requirements at the frequency specified in Attachment A, and at the time indicated in the sampling and
monitoring sections of the approved O&M plan. The required data shall be specific to the stabilization
process utilized, and sufficient to demonstrate compliance with the Class A pathogen reduction
requirements in 15A NCAC 02T .1106 (a) and (b), and one vector attraction reduction requirement in
15A NCAC 02T .1107 (a) shall be met. Any exceptions from the requirements in this condition shall
be specified in Attachment A. [15ANCAC 02T.1106,02T,1107,02T.1111(c)]
5, Laboratory parameter analyses shall be performed on the residuals as they are distributed, and shall be
in accordance with the monitoring requirements in 15A NCAC 02B .0505. [15A NCAC 02B M051
6. The Permittee shall maintain records tracking all bulk residual distribution or land application events
performed by the Permittee, At a minimum, these records shall include the following:
a. Source of residuals;
b. Date of distributionfland application;
c. Name and address of recipient of residuals,
d. Volume of residuals distributed to: each recipient;
e. Intended use of residuals;
f If land application events performed by the Permittee -Nitrogen Application Rate based on RYES
(if using data obtained from the North Carolina State University Department of Soil Science
Website, the printout page shall be kept on file and reprinted every five years),
[15A NCAC 02T.0108(a)]
WQ0036723 Version 10 Shell Version 180711 Page 8 of 10
T Three copies of an annual report shall be submitted on or before March 1". The annual report shall
meet the requirements described in the Instructions for Residuals Ap
Instructions for reporting and annual report forms are available at
h�t �-//de n�c.gov/about/divisions,/water-resources/water-resources-pe nits/wistewater-branch/non-
di scharge- Lerm ittJ or can be obtained by contacting the Non -Discharge
Permitting Unit directly. The annual report shall be submitted to the following address:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[I 5A NCAC 02T. I 11 I (a)]
8. Noncompliance Notification
The Permittee shall report by telephone to the Mooresville Regional Office, telephone number (704)
663 -1699, but in no case more than 24 hours or on the next working day following
the occurrence or first knowledge of the occurrence of any of the following:
a. Distribution of residuals abnormal in quantity or characteristic.'
b. Any failure of the distribution program resulting in a release of material to surface waters,
c. Any time self -monitoring indicates the facility has gone out of compliance with its permit
limitations.
d. Any process unit failure, due to known or unknown reasons, rendering the facility incapable of
adequate residual treatment,
e. Any spill or discharge from a vehicle or piping system during residuals transportation.
Any emergency requiring immediate reporting (e,g., discharges to surface waters, imminent failure of
a storage structure, etc.) outside normal business hours shall be reported to the Division's Emergency
Response personnel at telephone number (800) 662-7956, (800) 858-0368, or (919) 733-3300.Persons
reporting such occurrences by telephone shall also file a written report in letter form within five days
following first knowledge of the occurrence. This report shall outline the actions taken or proposed to
betaken to ensure that the problem does not recur. [15ANCACO2T.0105(1),02T.0108(b)(1)]
1, The Permittee shall provide adequate inspection and maintenance to ensure proper operation of the
subject facilities and shall be in accordance with the approved O&M Plan, [15ANCACO2T,0108(b)]
2. Prior to each bulk residuals distribution event, the Permittee or his designee shall inspect the residuals
processing, storage, transport and distribution facilities to identify malfunctions, facility deterioration
and operator errors that could result in discharges to the environment, a threat to human health or a
public nuisance, The Permittee shall maintain an inspection log that includes, at a minimum, the date
and time of inspection, observations made, and any maintenance, repairs, or corrective actions taken.
The Pen-nittee shall maintain this inspection log for a period of five years from the date of inspection,
and this log shall be made available to the Division upon request. [15A NCAC 02T .0108(b)]
1 Any duly authorized Division representative may, upon presentation of credentials, enter and inspect
any property, premises or place on or related to the distribution sites or facilities permitted herein at
any reasonable time for the purpose of determining compliance with this permit; may inspect or copy
any records required to be maintained under the terms and conditions of this permit; and may collect
groundwater, surface water or leachate samples, [G.S. 143-215,3(a)(2)]
WQ0036723 Version 2.0 Shell Version 180711 page of 10
1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to an
enforcement action by the Division in accordance with North Carolina General Statutes 143-215,6A to
143-215.6C� [G.S, 143-215,6A to 143-215.6C]
1 This permit shall become voidable if the residuals distribution events are not carried out in accordance
with the conditions of this permit, [15ANCAC 02T.0110]
3. This permit is effective only with respect to the nature and volume of residuals described in the permit
application and other supporting documentation, [G.S. 143-215.1]
4. The issuance of this permit does not exempt the Permittee, from complying with any and all statutes,
rules, regulations, or ordinances, which may be imposed by other jurisdictional government agencies
(e.g, local, state, and federal). Of particular concern to the Division are applicable river buffer rules in
15A NCAC 02B .0200; erosion and sedimentation control requirements in I SA NCAC Chapter 4 and
under the Division's General Permit NCGO 10000; any requirements pertaining to wetlands under 15A
NCAC 0213.0200 and 02H.0500; and documentation of compliance with Article 21 Part 6 of Chapter
143 of the General Statutes. [15A NCAC 02T .0105(c)(6)]
5, In the event the residuals program changes ownership or the Permittee changes his name, a formal
permit modification request shall be submitted to the Division. This request shall be made on official
Division forms, and shall include appropriate documentation from the parties involved and other
supporting documentation as necessary, The Permittee of record shall remain fully responsible for
maintaining and operating the residuals program permitted herein until a permit is issued to the new
owner, [ISANCAC 02T,01041
6. This permit is subject to revocation or unilateral modification upon 60-day notice from the Division
Director, in whole or part for the requirements listed in 15A NCAC 012T.01 10. [15ANCAC 02T,0110]
7. Unless the Division Director grants a variance, expansion of the permitted residuals program contained
herein shall not be granted if the Permittee exemplifies any of the criteria in 15A NCAC 02T.0120(b),
[15A NCAC 02T.01201
8. The Permittee shall pay the annual fee within 30 days after being billed by the Division. Failure to pay
the annual fee accordingly shall be cause for the Division to revoke this permit. [I 5A NCAC 02T
.0105(c)(3)]
Permit issued this the 30' day of August 2018
(Linda Culpepper, Interim Director
Division of Water Resources
By Authority of the Environmental lvlanagcJent Commission
WQ0036723 Version 2.0 Shell Version 180711 Page 10 of 10
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0 NC Certification No. 402 Case Narrative
Waypointe) NC Drinking Water Cert No. 37735 2/10121 10:17
ANALYTICAL SC Certification No. 99012
Town of Mooresville/RR WWTP
Whitney Munroe
P. 0. Box 878
Mooresville, NC 28115
Project: Class A Dried Sludge
Lab Submittal Date: 01/19/2021
Work Order 1010286
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Herbicides TCLP analysis was subcontracted to Waypoint Memphis. Laboratory report is attached.
PAN Equation = 0.3 * (TKN - Ammonia) + 0.5 * (Ammonia) +
Nitrate -Nitrite
PAN = 0.3 * (26000 - 1200) + 0.5 * (1200) + 2.6
PAN = 8200 mg/kg
Equation uses Mineralization Rate (MR) for Aerobically Digested
Solids (0.3)
Analysis note for SAR:
SAR = Na ] / 'SQRT i ( [Ca] + [Mg] ) 12
SAR = 15/23 ]1 SQRT [140/20] + [5,9/122] 2
SAR = 0.34
ConcentraVons for Na, Ca, and Mg are expressed in milliequivatents per liter, and SQRT designates
taking the square root of the operand in parentheses.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Spriingbrook Road - P.D. Box 240543 - Charlotte, NC 28224.0543
Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 Pc gD 1 of 17
Please call if you have any questions relating to this analytical report.
Respectfully,
WAYPOIINT ANALYTICAL
Terri W. Cole
Project Manager
Data Qualifiers Key Reference:
B Analyte is found in the associated blank at a concentration >1/2 RL.
B2 Analyte is found in the blank at a concentration > 1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MS.
HT Sample received and analyzed outside of the hold time.
MC Sample concentration too high for recovery evaluation,
SE Surrogate recovery outside of the CSC limits due to emulsion.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
Results reported to the reporting limft. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent ofWaypointAnalyticaJ.
449 Springbrook Road - P-0, Box 240543 - Charlotte, NC 28224-0543
Phone: 7041529-6364 -Toll Free Number; 1-8001529-6364 - Fax: 704/525-0409, Page 2 of
Work Order: 1010286
Client Sample ID Lab Sample iD Matrix DatefTime Sampled Date/Time Received
Class A
1010286-01 Solid 01/19/21 8:26 01/19/21 12:30
Samples were received in good condition at 4.9 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent Of Waypoint Analytical,
449 Springbrook Road - P.0, Box 240543 - Charlotte, No 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529.6364 - Fax: 7041525-0409 17
0 0 Laboratory Report
Waypoint. 02110/2021
ANALYTICAL
Town of Mooresville/RR WWTP Project: Class A Dried Sludge Client Sample ID: Class
Attn: Whitney Munroe Sample ID: 1010286-01
P, 0. Box 878 Work Order: 1010286
Mooresville, NC 28115 Sample Matrix: Solid Time Collected: 01/19/21 08:26
Time Submitted: 01/19/21 1230
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Plant Available Nitrogen
8200
mgikg dry
3100
1100
20
*Calculation,
1127121 14;57
CLB
(CALC]
% Solids
95.7
% by
0.100
0.100
1
*SM2540 0
1122121 13,50
EDV
PlA0789
Weight
Ammonia as N
1200
mg/kg dry
9.7
2.4
1
*SM4500-NH3 C 1/27121 14:57
BMS
PlAO911
Nitrate/Nitrite as N
BRL
mg/kg dry
5.2
1A
1
*SM4500-NO3 F 1/25/21 12:18
CLB
PIA0861
pH
6.3
pH Units
1
*9045D
1/20121 11:50
CLB
PIA0738
Phosphorus -Total
11000
mg/kg dry
520
210
100
*SM4500-P F
1125/21 9:06
CLB
PlAO835
Temperature
20.2 HT
C
1
*SM2550 B
1/20121 11:50
CLB
PIA0738
Total Kjeldahl Nitrogen
26000
mg/kg dry
10000
3600
20
*351.2
1/22121 11:32
CLB
PlAO801
Microbiological Parameters
Fecal Coliforms
2
MPN/g dry
01
1
*SM9221 E
1/19121 13:43
ENM
PIA0777
TCLP Extraction by EPA 1311
TCLP Extraction
Complete
N/A
1
*1311 ZHE
1/21/21 6:54
TBL
PIA0751
TCLP Extraction
Complete
N/A
1
1311
1/22121 810
EDV
PIA0798
TCLP Metals
mercury
SRL
mg/L
0,010
0.000034
1
*7470A
1/25121 15:50
EDV
PIA0863
Arsenic
BRL
mg/L
050
0,021
5
*6020B
1125/21 23;30
JAB
PIA0817
Barium
BRL
mg/L
5.0
0.079
5
*6020B
1125121 23:30
JAB
PlAO817
Cadmium
BRL
mg1L
0.060
0.016
5
*60208
1/25121 23:30
JAB
PIA0817
chromium
BRL
mg/L
0.25
0.023
5
*60208
1/25/21 23:30
JAB
PlAO817
Lead
BRL
mg/L
0.050
0.011
5
*60208
1/25/21 23:30
JAB
PIA0817
Selenium
BRL
mg/L
0,12
0.024
5
*6020B
1/25/21 23:30
JAB
PIA0817
Silver
BRL
mg1L
0.25
0.0084
5
*6020B
1/25121 23:30
JAB
P I A0817
TCLP Organochlo dine Pesticides by GC/ECD
Chlordane
BRL
mg/L
0.0025
0.00090
1
*8081B
1/25/21 17:11
NMB,
PlA0849
Dieldrin
BRL
mg/L
0.00050
0,000068
1
*80816
V25/21 17:11
NMB
PIA0849
Endrin
BRL
mg/L
0.00050
0,000068
1
*8081B
1/25/21 17:11
NMB
PlA0849
gamma-13HC
BRL
mg/L
0.00050
0,000030
1
*8081B
1/25/21 17:11
NMB
PlAO849
Heptachlor
BRL
mg/L
0.00050
0,000065
1
*8081B
1/25/21 17:11
NMB
PlAO849
Heptachlor Epoxide
BRL
mg/L
0.00050
0,00011
1
*8081B
1126121 17:11
NMB
PlAO849
Methoxyrhdr
BRL
mg1L
0.00050
0.000090
1
*8081B
1/25121 17:11
NMB
PlA0849
Toxaphene
BRL
mg/L
0.025
0.0018
1
*8081B
1/25/21 17:11
NMB
PIA0849
Surrogate
Recovery
Control Limits
Decachlorobiphenyl
30%
13-186
Tetrachloro-m-xylene
52%
40-134
TCLP Serinivolatile Organic Compounds by GCIMS
2,4,5-T6chloropherol
BRL
mg/L
0,25
0,0036
1
*8270E
1125121 16:03
JMV
PlAC812
2,4,6-Trichlorophenoi
BRL
mg1L
0.10
0.0045
1
*8270E
1125/21 16:03
JMV
PIA0812
2,4-Dinitrotoluene
BRL
mg/L
0.012
0.0042
1
*827GE
1/25/21 16:03
JMV
PlAD812
This report should not be reproduced, except in its entirety, without the written consent of Waypoini Analytical.
449 Springbrook
Road - P.0, Box 240543 - Charlotte, No 28224-0543
Phone: 704/529-6364 -Toll Free Number;
1-8001529-6364 - Fax:
704/525-0409
EEag:4::C
Town of Mooresville/RR WWTP
Attn: Whitney Munroe
R U. Box 878
Mooresville, NC 28115
Project: Class A Dried Sludge
Sample Matrix: Solid
Client Sample ID: Class
Sample ID: 1010286-01
Work Order: 1010286
Time Collected: 01/19/21 08:26
Time Submitted: 01/19/21 12:30
M&T 11 77I
02/1012021
Parameter
Result
Units
Report
MDL
Dilution
Method
Anafysis
Analyst
Batch
Limit
Factor
Date/Time
ID
2-Methylphenol
EIPL
mg/L
0.050
0,0024
1
*8270E
1/25/21 16:03
JMV
PlAD812
314-Methylphenal
BRL
mgIL
0.050
0,0025
1
*8270E
1/25/21 16:03
JMV
PlAO812
Hexachlorobenzene
BRL
mg/L
0.020
0.0039
1
*8270E
1/25/21 16:03
JMV
PlAO812
Hexachlorobutadiene
BRL
mgJL
0.050
0,0045
I
*8270E
1125121 16:03
JMV
P1 A0812
Hexachloroethane
BRL
mg/L
0.050
0.0037
1
'8270E
1/25/21 16:03
JMV
PlAO812
Nitrobenzene
BRL
mg/L
0.050
0.0038
1
*8270E
1/25121 16:03
JMV
PlAO812
Pentachlorophenol
BRL
mg1L
0.26
Ull
1
*8270E
1/25121 16:03
JMV
PlAO812
Pyridine
BRL
mg/L
0.25
0.0016
1
*8270E
1J25121 16:03
JMV
PIA0812
Surrogate
Recovery
Control Limits
2,4,6-Tribrornophenol
13%
43-140
SE
2-Fluorobiphenyl
100
44-119
SE
2-Fluorophenol
5%
19-119
SE
Nitrobenzene-d5
9%
44-120
SE
Phenol-d5
7%
11-52
SE
Terphenyl-d14
11 %
50-134
SE
TCLP Volatile Organic Compounds by GCIMS
1,1-Dichloroethylene
BRL
mg/L
0.035
0.00083
10
*8260D
1/22121 20:38
JLB
PlA0831
1,2-Dichloroethane
BRL
mgIL
0.0215
0.00066
10
*8260D
1/22/21 20:38
JLB
PlA0831
1,4-Dichicra benzene
BRL
mg/L
0.38
0.00050
10
*8260D
1/22/21 20:38
JLB
PIA0831
Benzene
BRL
MgIL
0.025
0.00048
10
*8260D
1122/21 20:38
JLB
PlAO831
Carbon Tetrachloride
BRL
mg/L
0,025
0.0011
10
*8260D
1122121 20:38
JLB
PIA0831
Chlorobenzene
BRL
mgIL
5.0
0.00062
10
*8260D
1/22/21 20:38
JLB
PlAO831
Carbon disulfide
BRL
mg/L
0.050
0.00075
10
*8260D
1/22/21 20:38
JLB
PlAO831
Chloroform
BRL
mg/L
0.30
0.00076
10
*8260D
1122/21 20:38
JLB
PlAO831
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/L
10
0.0024
10
*8260D
1122121 20:38
JLB
PlAC831
7etrachloroothyiene
BRL
mg/L
0.035
0.00098
10
*8260D
1/22/21 20:38
JLB
PlAO831
Trichloroethylene
BRL
mg/L
0.025
0.00078
10
*8260D
1/22/21 20:38
JLB
PlA0831
Vinyl chloride
BRL
mg/L
0.020
0.00097
10
*8260D
1122121 20:38
JLB
PlAO831
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
99%
80-124
Dibromofluoromethane
99%
75-129
Toluene-c!8
98%
77-123
Total Metals
Aluminum
17000
mg/kg dry
260
29
100
*6020B
1126121 16 :31
JAB
PlAO842
Mercury
BRL
mg/kg dry
0.52
0.16
10
*7471 B
1121121 1318
EDV
PIA0790
SAR Soil Preparation
Complete
9
1
*2-78-054
1/22/21 15:05
EDV
PIA0800
SAR Percent Moisture
75.7
% by
0.100
0.100
1
*2-78-054
1/25121 8:20
EDV
PlAO829
Weight
Arsenic
2.1
mglkg dry
1.0
0.088
10
*6020B
1125/21 19:12
JAB
PIA0842
Sodium Absorption Ratio
BRL
[blank]
1.0
0.016
1
-2-78-054
1/27/21 9:40
JAB
PlAO827
Cadmium
0.54
mg/kg dry
0.52
0.039
10
*6020B
1125/21 19:12
JAB
PlAO842
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
"S Springbrook Road - P,O, Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 -Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Page 5 of 17
0 G
Laboratory Report
Waypoi,nt.
02110/2021
ANALYTICAL
Town of MooresvilleIRR WWTP
Project: Class A Dried
Sludge
Client Sample lD:
Mass
Attn: Whitney Munroe
Sample ID, 1010286-01
P, O. Box 878
Work Order: 1010286
Mooresville, NC 28115
Sample Matrix: Solid
Time Collected: 01/19121 08:26
Time Submitted: 01/19/21
12:30
Parameter
Result
Units
Report
MDL
Dilution Method
Analysis Analyst
Batch
Limit
Factor
Dale/Time
ID
Calcium
13000
mg/kg dry
100
20
110 *6020B
1126/21 116:37
JAB
PIA0842
Calcium, SAR
140
mg1L
10
0A73
10 *60208
1127/21 9:40
JAB
PlAO827
Copper
170
mglkg dry
2.6
0,28
10 *60205
1125121 19:12
JAB
PIA0842
Lead
8.1
mg/kg dry
1.0
U79
10 *60205
1/26/21 16:37
JAB
PlAO842
Magnesium
2400
mglkg dry
26
5,5
10 *60208
1125121 19:12
JAB
PlAO842
Magnesium, BAR
5.9
mg/L
0.10
0.00072
1 *6020B
1/27121 9:40
JAB
PIA0827
Molybdenum
71
mg/kg dry
1.0
0.18
10 *6020B
1/25/21 19:12
JAB
PlA0842
Nickel
9.8
mglkg dry
1.0
0A2
10 *6020B
1125121 19:12
JAB
PlAO842
Potassium
3400
mglkg dry
100
15
10 *6020B
1125i21 19:12
JAB
PIA0842
Selenium
3.2
mglkg dry
1.0
0.24
10 *60208
1/25/21 19:12
JAB
PlAO842
Sodium
990 B2 mglkg dry
100
24
10 *6020B
1/26121 16:37
JAB
PIA0842
Sodium, SAR
15 B
mg1l-
0.10
0.0047
1 *6020B
1/27/21 9:40
JAB
PIA0827
Zinc
400
mg/kg dry
10
2.1
10 *60205
1126121 16:37
JAB
PlAO842
This report shouW not be reproduced, except in its entirety, without the written consent cf Waypoint Analytical,
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone; 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
I Pap 6 of 17
Sample Extraction Data
Prep Method: 351.2
Lab Number Batch Initial Final Date/Time
1010286-01 PIA0801 0.05 g 25 mL 01121/21 10:50
Prep Method: SM4500•NN3 B
Lab Number Batch Initial Final Date/Time
1010286-01 PlAO911 1.08 g 50 mL 01127/21 9:43
Prep Method. SM4500-PB5
Lab Number Batch Initial Final Date/Time
1010286-01 PIA0835 I g 50 mL 01/23121 10A5
Prep Method: Solids, Dry Weight
Lab Number Batch Initial Final Date/Time
1010286-01 PlA0789 30 g 30 9 01/21/21 9:57
Prep Method: 1311
Lab Number Batch Initial Final DatelTime
1010286-01 PlA0751 12.5 g 250 mL 01/20121 12:10
1010286-01 PlA0798 100 g 2000 mL 01/21121 16:08
Prep Method; 3010A
Lab Number Batch Initial Final DatefTime
1010286-01 PIA0817 10 mL 50 mL 01122/21 10:31
Prep Method: 7470A
Lab Number Batch Initial Final Date1nme
1010286-01 PIA0863 20 mL 30 mL 01/26/21 11:08
Prep Method: 3$10C GC
Lab Number Batch Initial Final Datefrime
1010286-01 PlA0949 200 mL 10 mL 01125121 8:30
Prep Method: 3510C MS
Lab Number Batch Initial Final Date/Time
1010286-01 PIA0812 200 mL 1 mL 01/22121 8:30
Prep Method: 5030B
Lab Number Batch Initial Final Date/Time
1010286-01 PlAO831 10 mL 10 mL 01122121 10:00
Prep Method: 3010A
Lab Number Batch Initial Final DateMme
1010286-01 RIA0827 50 mL 50 mL 01/22121 15:05
1010286-01 PIA0827 50 mL 50 mL 01122121 15:05
Prep Method: 30505
Lab Number Batch Initial Final DateMme
1010286-01 PIA0842 2 g 60 mL 01125/21 8A6
1010286-01 PlA0842 2 g 60 mL 01/25/21 8:46
...........
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
44,9 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 7041529.6364 - Tell Free Number; 1-800/529-6364 - Fax: 704/525-0409 Pag
Sample Extraction Data
Prep Methoch 305oB
Lab Number
Batch
Initial
Final
DaterTime
1010286-01
PlAO842
2 g
50 ni
01/25/21 8:46
Prep Method: 74715
Lab Number
Batch
Initial
Final
Date/Time
1010286-01
PlAO790
0.6 g
50 n-L
01/21121 10:30
Prep Method; SAR 2.78-054
Lab Number
Batch
initial
Final
Date/Time
1010286-01
PlAO800
250 g
250 g
01/21121 15:05
Subcontracted Analyses
The following analyses were subcontracted to Waypoint Analytical
i Number• Analysis
1010286-01 llcrbicidc5 TCLP (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrock Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Page of 17
C- UA
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Waypoint-,,(2)
ANALYTICAL
2/5/2021
Waypoint Analytical Charlotte
Ms. Terri Cole
P.O. Box 240543
Charlotte, NC, 28224-0543
2790 Whitten Road, Memphis, TN 38133
Main 901.213,24001 0 Fax 901,213�.2440
www.waypointanalytical,com
Ref: Analytical Testing
Lab Report Number- 21-029-0083
Client Project Description: Subcontract Order # 1010286
Dear Ms. Terri Cole:
Waypoint Analytical, LLC. received sample(s) on 1/29/2021 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions, The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method, Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol, These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Andrea R Brownfield
Project manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis,
I Page 11 of 17 ]
Page 1 of 7
2790 Whitten Road, Memphis, TN 38133
Main 901,213.2400 0 Fax 901,213.244,0
www.waypoinitanalyticaill.com
State
Program
Lab ID
. .
.. . ............. . . Expiration Date
Alabama
State Program
40750
02/28/2021
Arkansas
State Program
88-0650
02/07/2021
California
State Program
2904
06/30/2021
Florida
State Program - NELAP
E871157
06/30/2021
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2021
Illinois
State Program - NELAP
200078
10/10/2021
Kentucky
State Program
80215
06/30/2021
Kentucky
State Program
KY90047
12/31/2021
Louisiana
State Program - NELAP
LA037
12/31/2021
Louisiana
State Program - NELAP
04015
06/30/2021
Mississippi
State Program
IVIS
02/11/2023
North Carolina
State Program
415
12/31/2021
Oklahoma
State Program
9311
08/31/2021
Pennsylvania
State Program - NELAP
68-03195
05131/2021
South Carolina
State Program
84002
06/30/2021
South Carolina
State Program
84002
06/30/2021
Tennessee
State Program
02027
02/11/2023
Tennessee
A21LA ISO 17025:2017
4313.01
10/31/2021
Texas
State Program - NELAP
T104704180
09/30/2021
Virginia
State Program
00106
06/30/2021
Virginia
State Program - NELAP
460181
09/14/2021
Page I of 1 004 Page 12 of 17
Page 2 of 7
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 FaX 901.213.2440
www.waypointanaiytical.com
Sample Summary Table
Report Number: 21-029-0083
Client Project Description,: Subcontract Order # 1010286
Lab No Client Sample ID Matrix Date Collected Date Received
91164 Class A Solid 01/19/202108;26 01/29/2021
Page 13 of 17�'
Page 3 of 7
2790 Whitten Road, Memphis, TN 38133
Main 901,213.2400 ® Fax 901.213.2440
www.wayp o in tanalytical. co m
Ms., Terri Cole Project Subcontract Order # 1010286
P.O, Box 240543 Information
Charlotte , NC 28224-0543
Report Number : 21-029-0083 ,REPORT OFAIVAL YSIS
Report Date 02/05/2021
Received 01/29/2021
Lab No : 91164 Matrix: Solid
Sample ID : Class A Sampled; 1/19/20218:26
Analytical Method: 1311
Test
TCLP Herbicide Extraction
Analytical Method: 8151A
Prep Method: 8151A
Test
TCLP 2,4-D
TCLP 2,4,5-TP (Silvex)
Surrogate: DCAA
Results Units MDL MQL DF Date / Time By Analytical.
Analyzed Batch
Leachate 1 02/01/21 16:30 PHE L534263
Prep Batches}: 1-534722 02/03/21 15:00
Results Units MOL MQL DF
Date I Time By
Analytical
Analyzed
Batch
<0,0100 mg/L 0,0100 0.0200 1
02/04/21 15;44 VIC
L534973
<0.0010 mg/L 0,0010 0.0020 1
02/04/21 15:44 VIC
L534973
70,80 Limits: 20-120%
1 02/04/2115:44 VIC
L534973
Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit
Page 4 of 7
(2)
Waypoint
2790 Whitten Road, Memphis,
TN: 38133
rVain 901.213.2400 0 Fax
901,213.2440
ANALYTICAL
www.waypointanalytical.com
Quality Control Data
Client ID-
Waypoint Analytical Charlotte
Project Description.
Subcontract Order# 1010286
Report No:
21-029-10083
QC Prep:
L534722
QC Analytical Batch(es). L534973
QC Prep Batch Method:
8151A
Analysis Method; 8151A
Analysis Description: Phenoxy Acid Herbicides - GC/ECD (TCLP)
Lab Reagent Blank
LRB-L534722
Matrix: TCL
Associated Lab Samples;
91164
Parameter
Blank JMDL
Units Result
MQL Analyzed
0/0
0/4 Rec
Recovery
Limits
TCLP 2,4-D
mg/L <0.0100 0.0100
0.0200 02/04/21 12:03
TCLP 2,4,5-TP (Siivex)
mg/L <0.0010 0.0010
0.0020 02/04/21 12:03
DCAA (5)
02/04/21 12:03
88.8
20-120
Laboratory Control Sample
& LCSD LCS-LS34722 LCSD-L534722
Parameter
Spike
Units Conc„'
LCS LCSD LCS LCSD
Result Result G/bRec % Rec
% Rec
Limits
RPD Max
RPD
TCLP 2,4-D
mg/L 0.1000
0.0808 0.0772 80.8 77.2
20-120
4.5 20.00
TCLP 2,4,5-TP (Silvex)
mg/L 0.0100
0.0076 0.0074 76.0 74.0
20-120
2.6 20,00
DCAA (S)
83.8 81.6
20-120
Date: 02/05/202103:47 PM Page 15 of 17
Page 5 of 7
(Ol 2790 Whitten Road, Memphis, TN 38133
Waypoint, Main 901.213.2400 0 Fax 901.213,24411
ANALYTICAL wwwwavpointanalybcal,com
Shipment Receipt Form
Customer Number; 25657
Customer Name: Waypoint Analytical Charlotte
Report Number: 21-029-0083
Shipping Method
49 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
F--
F _00--
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
f —1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
Yes
0 No
COO properly completed
Yes
0 No
Samples in proper containers?
Yes1
No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding tame?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
(a N/A
Water - VOA vials free of headspace
Yes
0 No
40 N/A
—0
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
Yes
0 No
N/A
—0
F High concentration container (48 hr)
F High concentration pre -weighed (methanol -14 d)
F Low
[' Low
concentration EnCore samplers (48 hr)
cons pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
@ No
Comments:
Signature: cry Phillips Date & Time: 51
I Page 16 of 17 �
Page 5 of 7
Wayp ' inA t
LYTICAL
suBcovi-R,kci, ORDER
:Certification:
NFLAC USACE.
Waypoint Analytical
NC X SC Other
1010286
NiA
S F. N I[) I N G, 1, A Ji _O R,,M'O R Y:
RECEIVING 1.ABQ&.AT0RY-.
Way point Analy6cal
'Waypoint Analy,fical
11. 0, Box 240543
2790 Whitten Road
Charlotte. NC 28224-0543
Memphis- "TN 38133
Phone: 800-529-6364
Phone 190 1 ) 2 l 3-2400
Fax: 704-525-0409
Fav (901) 213.2440
Protect Mandeer Terri A". Cole
Analysis
Duc Expires Laboratory ID
Lommerats
Sample M, 1010296-01 Solid San'PIM: 011012108-26 ClassA
I lcrbicide,'WLP (Sub 02M2121 08 20
ComainersSupplied:
21029-0083
25651 0,_2. 2021
'
�Vavmlnt Anal0cal Charictle
11 51 42
SuDcal MAO ornef 9 10 10-1136
f l -)-. �, l -2- (
Date Recewed By
Date
m
Rage 7 of 7
Page I ut, I
Page 17 of77
Town of Mooresville/RR WWTP
Whitney Munroe
P. O. Box 878
Mooresville, NC 28115
NC Certification No, 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Project: Class A TCLP
Lab Submittal Date: 01/19/2021
Work Order: 1010287
2/10/21 10:38
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods,
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Reactivity analysis was subcontracted to Waypoint Memphis. Laboratory report is attached.
Please call if you have any questions relating to this analytical report.
Respectfully,
WAYPOINT ANALYTICAL
Terri W. Cole
Project Manager
Data Qualifiers Key Reference:
HT Sample received and analyzed outside of the hold time,
IGN The test results of this method cannot be used to directly classify a waste as a D001 hazardous waste, nor can the
results be used by themselves to definitively classify a waste as non -hazardous. 40 CFR 26121
INEG Negative Ignitability result according to DOT regulations,
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report shouid not be reproduced, except in its entirety, without the written consent of WaypointAnatytical
449 Springbrook Road - P.O, Box 240543 - Charlotte, NC 28224-0543
Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax; 7041525-0409 Page 1 of 1=5
Gi
Waypoint.
ANALYTICAL
Sample Receipt Summary
02/10/2021
Work Order: 1010287
Client Sample ID Lab Sample ID Matrix Datefrinne Sampled DatelTime Received
Class A TCLP
1010287-01 Solid 01/19/21 8:26 01/19/21 12:30
Samples were received in good condition at 4.9 degrees C uNess otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Ana I ytieg L
449 Spriingbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 7041$29•6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 15
0 G Laboratory Report
Waypolint. 02110/2021
ANALYTICAL
Town of Mooresville/RR WWTP Project: Class A TCILP Client Sample ID: Class ATCLP
Attm Whitney Munroe Sample ID: 1010287-01
P. 0. Box 878 Work Order: 1010287
Mooresville, NC 28115 Sample Matrix: Solid Time Collected: 01/19/21 08-26
Time Submitted: 01/19/21 12:30
Parameter
Result
Units
Report
IVDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
95.6
% by
0.100
0.100
1
*SM2540 G
1129121 15:12
EDV
PlA0977
Weight
Corrosivity-pH
6.3
pH Units
I
*9045D
1120121 11:50
CLB
PlA0737
Ignitability
E3RL IGN, IINEG
mm/sec
0.10
1
*1030
1120121 15:15
BMS
PIA0775
Temperature
20.2 HT
c
1
*SM2550 B
1/20/21 11;50
CLS
PlA0737
TCLP Extraction by EPA1311
TCLP Extraction
Ccrnplete
N/A
1122/21 8:10
EDV
PlA0798
TCLP Sernivolatile Organic Compounds by GCIMS
2,4,5-Trichlorophenol
BRL
mg1L
0.25
0,0036
1
'8270E
1125121 11:33
JMV
PIA0812
2,4,6-Trichlorophenol
BRL
mg/L
010
0.0045
1
*8270E
1/25/21 11:33
JMV
PlA0812
2,4-Dr)itrotoluene
BRL
mg1L
0.012
0.0042
1
*8270E
1/25121 11:33
JMV
PIA0812
2-Methylphenol
BRL
mg/L
0,050
0.0024
1
*8270E
1/25/21 11:33
JMV
PlAO812
314-Methylphenol
BRL
mg/L
0,050
0.0025
1
*8270E
1126121 11:33
JMV
PlA0812
Hexachlorobenzene
BRL
mg/L
0.020
0.0039
1
*8270E
1/25/21 11:33
JMV
PlAO812
Hexachlorobutadiene
BRL
mg1L
0.050
0.0045
1
*8270E
1125/21 11.33
JMV
PlAO812
Hexach[oroethane
BRL
mg/L
0.050
0.0037
1
*8270E
1/25121 11:33
JMV
P 1 A0812
Nitrobenzene
BRL
mgIL
0.050
0.0038
1
*8270E
1/25/21 11:33
JMV
PlAO812
Pentachlorophenol
BRL
mg/L
0,25
0.011
1
*8270E
1125/21 11:33
JMV
PlAO812
Pyridlne
BRL
mg/L
0.25
0.0016
1
*8270E
1/25121 11:33
JMV
PlA0812
Surrogate Recovery Control Limits
2,4,6-Tribrornophenol
127%
43-140
2-Fluorobiphenyl
91%
44-119
2-FluarophenoJ
53%
19-119
Nitrobenzene-d5
83%
44-120
Phenol-d5
35%
11-52
Terphenyl-d14
99%
50-134
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.0, Box 240543 - Charlotte, NC 28224-0543
Phone: 7041529-6364 -Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch Initial Final Date/Time
1010287-01
P1A0977
30 g
30 g
01/29/21 7:54
Prep Method: 1311
Lab Number
Batch
Initial
Final
Date/Time
1010287-01
PlA0798
100 g
2000 mL
01121/21 16:08
Prep Method: 3510C MS
Lab Number
Batch
Initial
Final
DatelTime
1010287-01
PIA0812
200 mL
1 mL
01122121 8:30
Subcontracted Analyses
The following analyses were subcontracted to Waypoint Analytical
Lab Number Analysis
1010287-01 Reactivity, Cyanide (Sub)
10 10287-0 1 Reactivity, Sulfide (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0543
Phone. 7041529-6364 -Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Page 4 of ILJ
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llaypoint
ANALYTICAL
2/2/2021
Waypoint Analytical Charlotte
Ms, Terri Cole
P.O. Box 240543
Charlotte, NC, 28224-0543
Ref: Analytical Testing
Lab Report Number: 21-026-0044
Client Project Description: Subcontract# 1010287
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax 901.213.2440
www.waypointanalytical.com
Dear Ms, Terri Cole;
Waypoint Analytical, LLC. received sample(s) on 1/26/2021 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a'—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling, Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
1 & A* k
Andrea R Brownfield
Project manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
I Page 6 of 1-5—D'I
Page 1 of 10
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 rax 901.213.2440
www.waypointanalytical,com
Laboratory 11): WP MTN: Waypoint Analytical, ILL.C., Memphis, TIN
State
Pre rg m
Lab I D
Expi ation- Date
Alabama
State Program
40750
02/28/2021
Arkansas
State Program
88-0650
02/07/2021
California
State Program
2904
06/30/2021
Florida
State Program - NELAP
E871157
06/30/2021
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2021
Illinois
State Program - NELAP
200078
10/10/2021
Kentucky
State Program
80215
06/30/2021
Kentucky
State Program
KY90047
12/31/2021
Louisiana
State Program - NELAP
LA037
12/31/2021
Louisiana
State Program - NELAP
04015
06130/2021
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
415
12/31/2021
Oklahoma
State Program
9311
08/3112021
Pennsylvania
State Program - NELAP
68-03195
05/31/2021
South Carolina
State Program
84002
06/30/2021
South Carolina
State Program
84002
06/30/2021
Tennessee
State Program
02027
02/11/2023
Tennessee
A21-A ISO 17025:2017
4313.01
10/31/2021
Texas
State Program - NELAP
T104704180
09/30/2021
Virginia
State Program
00106
06/30/2021
Virginia
State Program - NELAP
460181
09/14/2021
Page I of 1 00q- , Page 7 of 15
Page 2 of 10
0 (D
Waypoint,
ANALYTICAL
Report Number:
Client Project Description-,
Lab No Client Sample ID
89334 Class A TCLP
2790 Whitten Road, Memphis, TN 381.13
Main 901.213.24010 " Fax 901.213.2440
www.waypointaniallytical.com
Sample Summary Table
Subcontract # 1010287
Matrix Date Collected Date Received
Sohds 01/19/2021 08;26 01/26/2021
Page 3 of 10
2790 Whitten Road, Memnphis, TM 3,8133
Main 901.213.2400 0 Fax 901.213.2440
www.waypointanalytical.corn
Ms, Terri Cole Project Subcontract # 1010287
P.O. Box 240543 Information
Charlotte , NC 28224-0543
Report Number ; 21-026-0044
Report Date 02/02/2021
Received 01/26/2021
Lab No : 89334
Sample ID : Class, A TCLP
Matrix: Solids
Sampled; 1/19/20218:26
Analytical Method: SW-7.33
Test
Results
Units
MDL MOL OF
Date / Time By
Analytical
Analyzed
Batch
Cyanide, Reactive
<0A25
mg/Kg
0.125 0.125 1
01/26/21 12:46 FMM
L533272
Sulfide (Reactivity)
<25.0
mg/Kg
25.0 25.0 1
01/26/21 12:46 FMM
L533273
Moisture
4.04
%
1
02/01/21 17:57 FMM
L534252
Quailifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 9 oF1 5
Page 4 of 10
Waypoint.0
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901,213.2400 ' Fax 901.213.2440
www.waypointanalytical.com
Client ID:
Waypoint Analytical Charlotte
Project Description:
Subcontract # 1010287
Report No;
21-026-004,4
QC Analytical Batch:
L533272
Analysis Method:
SW-7.33
Analysis Description, Reactive Cyanide
Lab Reagent Blank LRB Matrix: SOL
Associated Lab Samples: 89334
Parameter
Cyanide, Reactive
Laboratory Control Sample
Parameter
Cyanide, Reactive
Blank
Units Result
mg/Kg <0A25
LCS
Spike
Units Conc.
mg/Kg 1000
wa�lffl
0.125 0.125
LCS
Result
166
Analyzed
01/26/21 12:46
LCS O/oRec 0/0 Rec
Limits
17.0 5-75
Date: 02/02/2021 03:51 PM Page 10 of I
Page 5 of 10
QC Analytical Batch: L533273
Analysis Method: SW-7.3.4
Analysis Description: Sulfide Reactivity
Lab Reagent Blank LRB Matrix: SOL
Associated Lab Samples: 89334
Blank MDL MQL Analyzed
Parameter Units Result
Sulfide (Reactivity) mg/Kg <25.0 25,0 25.0 01/26/21 12:46
Laboratory Control Sample LCS
Spike LCS LCS 0/aRec O/o Rec
Parameter Units Conc. Result Limits
Sulfide (Reactivity) mg/Kg 254 231
91,0 50-130
Date: 02/02/2021 03:51 PM
Page 6 of 10
[ Page 11 of 15 1
Waypolinto
ANALYTICAL
2790 whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax 901,213.2440
www.waypointanalytical.com
Client ID.-
Waypoint Analytical Charlotte
Project Description:
Subcontract# 1010287
Report No:
21-026-0044
QC Analytical Batch.
L534252
Analysis Method:
SW-DRYWT
Analysis Description:
Dry Weight Determination
Duplicate
Parameter
Moisture
L 90869-DUP
Result DUIP
Units Result
% 10.1 6.73
RPD Max RPD Analyzed
40.0* 20.0 02/01/21 17:57
QC Fail Date: 02/02/202103:51 PM
Page 12 of " -0
Page 7 of 10
Wyrp
NLTCL(D 90W:ttenRo.ad,MeapTnt M90200maph0is, TN 3,841430
AYA3
wwmwavpointanalyticaLcom
Shipment Receipt Form
Customer Number: 25657
Customer Name: Waypoint Analytical Charlotte
Report Number; 21-026-0044
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
Yes
0 No
Number of coolers/boxes received
1.
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
40 Yes
0 No
COC agrees with sample labei(s)?
9 Yes
0 No
COG properly completed
4D Yes
0 No
Samples in proper containers?
9 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
9 Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 - compliance criteria met
0 Yes
0 No
N/A
High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) � - Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
@ No
Comments:
Signature: Kr:i:s:t:i:n:a:::A-McAdams Date &Time: 16-1-/2-6/6_21 _09:32:1_9]
F—P—age 13 o-f-1 —5-]
Page 8 of 10
MMW
SUBCONTRACT ORDER
Certification: NELAC— "'ACE
Waypoi tit Ana lytica I NC SC— Other
1010287 N/A.
SENDING LABORATORY-, RECEIVING LABORkYORN:
Waypoint Analytical
Waypoint Analytical
P. OBox 240543
2790 Whitten Road
Charlotte, NC28224-0543
Nfemphis, IN 38133
Phone: 800-529-6364
Phone:(901) 213-2400
Fax: 704-525-0409
Fax: (901) 213-2440
Prpject,\Ianager; Terri W. Cole
Anatvsis Due Expires Laboratoq ID
Comments
Sample III; 1010287-01 Solid San, pled: 01119/2108:26 (TAMS ATCLP
Reactivity, Cyanide { S ub) 02/0 2/21 08:26
�aratcadra S SI ipvl hN. (1:
I N 60,L-
21-026-0044
26657
01-26-2021
Wavy oml AnWiCal CharRohe 09'31 46
SUbconTrart # 1010287
Releas"I By
_ Bate
Page I of 2
Page 14 of 15
Page 9 of 10
Waypoint Analytical Cerlificatiow NELAC— USACE
-
NC SC Other
1010287 NIA
SLN
,L)ING 1,AV0RVr0RV,
RECEIV1,NG LABOkATQRY,
Waypoint Analytical Waypoint Analytical, LLC
P. 0. Box 24054") 2790 Whitten Road
Charlotte, NC 28224-0543 Memphis, TN 38133
Phone: 8,00-529-6364 Phone -,(901) 213-2400
Fax: 70,4-525-0409 Fax: (901) 213-2440
Projeci Manager: Terri W. Cole
Analysis
Due Expires Laboratory ID Comments
Sample ID: 1010287-41 Solid sampk&O 1/] 9/2108.26 Class A TCLP
Reactivity, Sulfide (Sktb) 0 1126Q] 08:26
Containers S4 1 U d
1 K7 tM
21-026-0044
25657
01 '26-207.1
WavDtwni AnaNlical Charlotte 09.31:46
Subconlract # 1010287
Page 10 of 10
Page 2 of 2
L Page 15 oF1 5
Waypoint.(2)
ANALYTlC,4,L--
8/13/2021
Town of Mooresville/RR WWTP
Whitney Munroe
369 Johnson Dairy Rd.
Mooresevifle, NC, 28115
Ref. Analytical Testing
Lab Report Number: 21-200-0031
Client Project Description: Class A
Dear Whitney Munroe:
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
war w.waypointan,aiyticall.com
Waypoint Analytical, LLC (Charlotte) received sample(s) on 7/19/2021 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2012) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
60A'd
Terri W Cole
Laboratory Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page I of 21
Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.5291.6364
www,waypolintanalytical.com
MIN
Laboratory ID: WP CNIC: Waypolinit Analytical Carolina, Inc. (C), Charlotte, NC
State
Program
Lab ID
Expiration Date
North Carolina
State Program
37735
07/31/2022
North Carolina
State Program
402
12/31/2021
South Carolina
State Program
99012
07/31/2021
South Carolina
State Program
99012
12/31/2021
Laboratory ID: WP M'TN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2022
Arkansas
State Program
88-0650
02/07/2022
California
State Program
2904
06/30/2022
Forida
State Program - NELAP
E871157
06/30/2022
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2021
Illinois
State Program - NELAP
200078
10/10/2022
Kentucky
State Program
80215
06/30/2022
Kentucky
State Program
KY90047
12/31/2021
Louisiana
State Program - NELAP
LA037
12/31/2021
Louisiana
State Program - NIELAP
04015
06130/2022
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
415
12/31/2021
Oklahoma
State Program
9311
08/31/2021
Pennsylvania
State Program - NELAP
68-03195
05/31/2022
South Carolina
State Program
84002
06/30/2022
South Carolina
State Program
84002
06/30/2022
Tennessee
State Program
02027
02/11/2023
Tennessee
A21-A ISO 170252017
4313.01
10131/2021
Texas
State Program - NELAP
T104704180
09/30/2021
Virginia
State Program
00106
06/30/2022
Virginia
State Program - NELAP
460181
09/14/2021
Page 1 of 1 00016/21-200-0031
Page 2 of 21
0 (D
Waypoint
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Maln 704,529,6364
wwwwaypointanal"cal,com
Sample Summary Table
Report Number: 21-200-0,031
Client Project Description: Class A
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab 111)
91977
Class A
Sludge
07/19/2021 08:55
07/19/2021 13:45
91977
Class A
Sludge
07/19/2021 08:55
07/19/2021 13:45
6010D
WP MTN
91977
Class A
Sludge
07/19/2021 08:55
07/19/2021 13:45
SW-1311
WP MTN
91977
Class A
Sludge
07/19/2021 08:55
07/19/2021 13:45
8081A
WP MTN
91977
Class A
Sludge
07/1912021 08:55
07/19/2021 13:45
8151A
WP MTN
91977
Class A
Sludge
07/19/2021 08:55
07/19/2021 13:45
8270C
WP MTN
91977
Class A
Sludge
07/19/2021 08:55
07/19/2021 13:45
7470A
WP MTN
91978
Class A
Solids
07/19/2021 08:55
07/19/2021 13:45
91978
Class A
Solids
07/19/2021 08:55
07/19/2021 13:45
350.1
AES
91978
Class A
Solids
07/19/202108:55
07/19/2021 13:45
6010D
WP MTN
91978
Class A
Solids
07/19/2021 08:55
07/19/2021 13:45
4500NORGD-2011
WP MTN
AES: Analytical Environmental Services, Inc., Atlanta, GA
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 21
Waypoint(2)
ANALYTlCAL
Client-, Town of Mooresville/RR WWTP
Project, Class A
Lab Report Number: 21-200-0031
Date: 8/13/2021
449 Springbrook Rd, Charlotte, NC 28217
Main 704,529.16,364
www.waypointanalyticai.com
CASE NARRATIVE
Fecal Coliform MPN Method 9221E-2011
Sample 91978 (Class A)
QC Batch No: V6750
Sediment from sample likely inhibited gas collection in the inverted tubes of the 10 mL sample volume. Bubbles
were observed in the MPN tube; however, they were absent from the inverted capture tube.
Metals Analyses Method 6020B
QC Batch No: V6931A/6905
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly,
QC Batch No: V6983N6905
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Sample 92143
Analyte: Potassium
QC Batch No: V6983N6905
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Nickel
QC Batch No: V6931/V6905
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Zinc
QC Batch No: V6931/V6905
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control
acceptance ranges. Matrix interference is suspected
Solids Total Mercury Analysis - CVAA Method 7471B
Sample 91978 (Class A)
Analyte: Mercury
QC Batch No: V6703/V6690
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly
Analysis note for PAN
PAN Equation = 0.3 * (TKN — Ammonia) + 0.5 * (Ammonia) + Nitrate -Nitrite
PAN = 0.3 * (16200 — 2810) + 0.5 * (2810) + 3.02
PAN = 5425 mg/Kg
Equation uses Mineralization Rate (MR) for Aerobically Digested Solids (0.3)
Page 4 of 21
Wayl'Ont(2)POI
ANALYTICAL
Analysis note for SAR
449 Springbrook Rd, Chadotte, NC 28217
Main 704-529.6364
www.waypointanalytical.com
SAR = [ Na ] / SQRT f ( [Ca] + [Mg) ) / 2)
Concentrations for Na, Ca, and Mg are expressed in milli -equivalents per liter, and SQRT designates taking the
square root of the operand in parentheses,
SAR = (881/23) / SQRT ((l 5100/20 + 2320/12.2)/2)
SAR = 38 / SQRT ((755 + 190) / 2)
SAR = 38121.7
SAR = 1,72
Page 5 of 21
449 $pringbrook Rd, Charlotte, NC 28217
Main 704,529,6364
wwwwaypointanalytfcal.co rn
Report Date 08/13/2021
Received 07/19/2021
Report Number : 21-200-0031 REPORTOFAIVALYSIS
Lab No : 91977 Matrix: Sludge
Sample ID : Class A Sampled: 7/19/20,218.55
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
TCLP Herbicide Extraction
Leachate
1
07/21/21 13:00
JAN
SW-1311
TCLP Metals Extraction
Leachate
1
07/21/21 13:00
JAN
SW-1311
TCLP Pesticide Extraction
Leachate
1
07/21/21 13:00
JAN
SW-1311
TCLP SVOC Extraction
Leachate
1
07/21/21 13:00
JAN
SW-1311
TCLP VOC ZHE Extraction
leachate
1
07/20/21 13:45
TBL
SW-1311 (ZHE)
Analytical Method. 6010D
Prep Batch(es):
L565880 07/27/21 13:00
Prep Methods 3015A
Test
Results Units
MDL MOIL DF
Date / Time
By
Analytical
Analyzed
Batch
TCLP Arsenic
<0.250
mg/L
0,056
0.250
1
07/28/21 12:49
TJS
L566040
TCLP Barium
<0.250
mg/L
0.040
0.250
1
07/28/21 12:49
TJS
L566040
TCLP Cadmium
< 0. 0500
mg/L
0.0030
0,0500
1
07/28/21 12:49
TJS
L566040
TCLP Chromium
<0.100
mg/L
0.038
01100
1
07/28/21 12:49
TJS
L566040
TCLP Lead
<0.100
mg/L
0,024
0.100
1
07/28/21 12:49
TJS
L566040
TCLP Selenium
<0.500
mg/L
0,034
0.500
1
07/28/21 12:49
TJS
L566040
TCLP Silver
<0.0500
mg/L
0.023
0.0500
1
07/28/21 12:49
TJS
L566040
Qualifiers/ DF Dilution Factor J Estimated value
Definitions MQL Method QuantitaUon Limit
Page 6 of 21
Report Number : 21-200-0031
Lab No : 91977
Sample ID : Class A
Analytical Method: 7470A
Prep Method: 7470A
Test
TCLP Mercury
Analytical Method: 8081A
Prep Method: 3510C
Test
TCLP Endrin
TCLP gamma-61-1C
TCLP Methoxychlor
TCLP Toxaphene
TCLP Chlordane
TCLP Heptachlor Epoxide
TCLP Heptachlor
Surrogate: Decachlorobiphenyl
Surrogate: Tetra cftro-m-xylen e
Analytical Method: 8151A
Prep Method: 8151A
Test
449 Sp,ringbrook Rd, Charlotte, NC 28217
Main 704.52!9.6364
www,waypointanalytical.com
Report Date 08/13/2021
Received 07/19/2021
REPORT OFANAL YSIS
Matrix: Sludge
Sampled: 7/19/20218:55
Prep Batch(es): L565308 07/23/21 10:00
Results Units MDL MOL DF Date / Time By Analytical
Analyzed Batch
<0,0200 mg1L 0.0017 0.0200 1 07/23/2113:55 DDB L565450
Prep Batch(es): L565400 07/23/21 13:00
Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
<0,001600
mg/L
0.()0()800
0.001600
10
07/26/21
19:54
VIC
L565844
<0.001600
mg/L
0,000800
0.001600
10
07/26/21
19:54
VIC
L565844
<0.001600
mg/L
0.000800
0.001600
10
07/26/21
19:54
VIC
L565844
<0.01200
mg/L
0,006000
0.01200
10
07/26/21
19:54
VIC
L565844
<0.008000
mg/L
0,004000
0.008000
10
07/26/21
19:54
VIC
L565844
<0.001600
mg/L
0,000800
0.001600
10
07/26/21
19:54
VIC
L565844
<0.001600
mg/L
0,000800
0.001600
10
07/26/21
19:54
VIC
L565844
52.29
Limits: 34-116%
10 07/26/21 19:54
L565844
54.29
Umits: 25-123%
10 07/26/21 19:54
L565844
Prep Batch(es)-,
L565473 07/23/21
16:15
Results Units MDL MQL DF Date I Time By Analytical
Analyzed Batch
TCLP 2,4-D <0.0200 mg/L 0.0100 0.0200 1 07/27/21 02:36 VIC L565886
TCLP 2,4,5-TP (Silvex) <0.0020 mg/L 0.0010 0.0020 1 07/27/2102:36 VIC L565886
Surrogate: DCAA 56,00 Limits: 20-120% 1 07/27/2102:36 L565886
Qualifiers/ DF Dilution Factor 3 Estimated value
Definitions MQL Method Quantitation Limit
Page '7 of 21
Report Number: 21-200-0031
449 Springbrook Rd, Charlotte, NIC 28217
Main 704,529,6364
www.waypo�inta:na:lyVcal.com
REPORT OFANAL YSIS
Report Date 08/13/2021
Received 07/19/2021
Lab No : 91977 Matrix: Sludge
Sample ID: Class A Sampled: 7/19/20218:55
Analytical Method.- 8260D Prep Satch(es): V6806 07/21/21 09:30
Prep Method: 5030E
Test Results Units MDL MQL DF Date I Time By Analytical
Analyzed Batch
TCLP Benzene
<0.0050
mg/L
0.0033
0.0050
10
07/21/21 20:12
JLB
V6807
TCLP Carbon Tetrachloride
<0.0200
mg/L
0.0054
0.0200
10
07/21/21 20:12
JLB
V6807
TCLP Chlorobenzene
<0,0050
mg/L
0.0033
0.0050
10
07/21/2120:12
JLB
V6807
TCLP Chloroform
<0.0050
mg/L
0.0047
0.0050
10
07/21/2120:12
)LB
V6807
TCLP 1,4-Dichlorobenzene
<0.0050
mg/L
0.0042
0.0050
10
07/21/2120:12
JLB
V6807
TCLP 1,2-Dichloroethane
<0.0050
mg/L
0.0040
0.0050
10
07/21/2120:12
JLB
V6807
TCLP IJ-Dichloroethene
<0.0050
mg/L
0.0034
0.0050
10
07/21/2120:12
JLB
V6807
TCLP Methyl Ethyl Ketone (MEK)
0.156
mg/L
0,0078
0,0050
10
07/21/2120:12
JLB
V6807
TCLP Tetrachloroethene
<0.0050
mg/L
0,0030
0.0050
10
07/21/2120:12
JLB
V6807
TCLP Trichloroethene
<0,0050
mg/L
0.0046
0,0050
10
07/21/21 20:12
JLB
V6807
TCLP Vinyl Chloride
<0.0050
mg/L
0.0041
0,0050
10
07/21/21 20:12
JLB
V6807
Surrogate: 4-Bromofluorobenzene
103
Limlts:
80-124%
10 07/21/2120:12
JLB
V6807
Surrogate: Dibromofluaromethane
105
Limits:
75-129%
10 07/21/21 20:12 JLB
V6807
Surrogate! Toluene-dS
95.2
Limits:
77-123%
10 07/21/21 20:12
JLB
V6807
Analytical Method: 8270C
Prep Satch(es):
L565579
07/26/2109:00
Prep Metlhod, 3510C
Test
Results
Units
MDL
MOL
DF
Date I Time
By
Analytical
Analyzed
Batch
TCLP 2-Methylphenol
<0.100
mg/L
0.025
0.100
5
07/26/21 18:13
BGV
L565794
TCLP 3&4 Methylphenol
<0.200
mg/L
0.025
0.200
5
07/26/21 18:13
BGV
L565794
TCLP 2,4-Dinitrotoluene
<0.100
mg/L
0.025
0.100
5
07/26/21 18:13
BGV
L565794
TCLP Hexachlorobenzene
<0A00
mg/L
0.025
0.100
5
07/26/21 18:13
BGV
L565794
Qualifiers/ DF
Dilution Factor
j
Estimated value
Definitions MQL
Method Quantitation Limit
Page 8 of 21
Report Number : 21-200-00,31
449 Sprin:gbrook Rd', Charlotte, NC 28217'
Main 704,529,6364
www�waypointanalytical.com
REPoRr OFANAL YSrS
Report Date 08/13/2021
Received 07/19/2021
Lab No : 91977 Matrix: Sludge
Sample ID : Class A Sampled: 7119/20218:55
Analytical Method: 8270C Prep Batch(es): L565579 07/26/21 09:()0
Prep Method: 3510C
Test Results Units MDL MQL DIF Date I Time By Analytical
Analyzed Batch
TCLP HexacWorobutadiene
<0.100
mg/L
0.025 0.100
5
07/26/21 18:13 BGV
L565794
TCLP Hexachloroethane
<0.100
mg/L
0.025 0.100
5
07/26/21 18J3 .BGV
L565794
TCLP Nitrobenzene
<0.,100
mg/L
0.025 0,100
5
07/26/21 18:13 BGV
L565794
TCLP Pentachlorophenol
<0.200
mg/L
0.025 0.200
5
07/26/21 18:13 BGV
L565794
TCLP Pyridine
<0.100
mg/L
0.025 0100
5
07/26/21 18:13 BGV
L565794
TCLP 2,4,5-Trichlorophenol
<0.100
mg/L
0.025 0.100
5
07/26/21 18:13 BGV
L565794
TCLP 2,4,6-Trichlarophenol
<0.100
mq/L
0.025 0.100
5
07/26/21 18:13 BGV
L565794
Surrogate: TCLP 2,4,6-Tribromophenol
54,3
Limits: 42-102%
5 07/26/21 18:13 BGV
L565794
Surrogate: TCLP 2-Fluorobiphenyl
410
Limits: 24-86%
5 07/26/21 18:13 BGV
L565794
Surrogate. TCLP 2-Fluorophenal
16,,8
Limits: 13-37%®
5 07/26/21 18:13 BGV
L565794
Surrogate: TCLP 4-Terphenyl-cI14
66.8
Limits: 30-122%
5 07/26/21 18:13 BGV
L565794
Surrogate: TCLP Nitrobenzene-d5
44.3
Limits; 25-78%
5 07/26/21 18:13 BGV
L565794
Surrogate: TCLP Phenol-d6
12,0
Limits: 9-27%
5 07/26/21 18:13 BGV
L565794
Qualifiers/ DF Dilution Factor 7 Estimated value
Definitions MQL Method Quantitation Limit
Page 9 of 21
Report Number: 21-200-0031
449 Springbrook Rd, Charlotte, NC 28217'
Main 704,529.6364
www.waypointanailytiCal.com
REPoRrOFANALYSIS
Report Date 08/13/2021
Received 07/19/2021
Lab No : 91978
Matrix: Solids
Sample ID : Class A
Sampled: 7/19/2021 Sz55
Test
Results
Units
MDL
MOL
DF
Date / Time
By
Analytical
Analyzed
Method
Fecal Coliform MPN/g
17.8
MPN/g - dry
2.0
2.0
1
07/19/21 14:34
ENM
9221E-2011
Sodium Absorption Ratio
1.72
Ratio
0.010
0.010
20
07/26/2121:02
CALCULATION
Plant Availabie Nitrogen
5680
mg/Kg - dry
1
08/13/2100:00
CALCULATION
Moisture
4.57
%
1
07/26/21 16:30
EDV
SW-DRYVVT
Nitrate+Nitrite-N
3.02
mg/Kg - dry
1.06
1
07/22/21 10:50
9056A
pH
6.19
SM°
1
07/23/21 11:15
CL3
9045D
Total Solids
95.4
%
0
0.010
1
07/26Y21 16:30
EDV
2540G-2011
Total Kjeldahl Nitrogen
16200
mg/Kg - dry
322
649
10
07/27/21 15:58
CLP 4500NORGD-2011
Phosphorus
18700
mg/Kg - dry
28,9
52.4
10
07/29/2123:11
TJS
6010D
Aluminum
25300
mg/Kg - dry
8.02
52.7
20
07/26/2121:02
EDV
6020B
Arsenic
2.80
mg/Kg - dry
0,198
2A1
20
07/26/2121:02
EDV
6020B
Cadmium
<1.06
mg/Kg - dry
0,116
1.06
20
07/26/21 21:02
EDV
6020E
Calcium
15100
mg/Kg - dry
48.4
211
20
07/26/2121:02
EDV
6020B
Copper
287
mg/Kg - dry
0.948
5.27
20
07/26/2121:02
EDV
6020E
Lead
11.3
mg/Kg - dry
0,738
5.27
50
07/27/21 18:09
EDV
6020B
Magnesium
2320
mg/Kg - dry
13.9
52.7
20
07/26/2121:02
EDV
6020B
Mercury (Total)
0.346
mg/Kg - dry
0.0251
0.0629
2
07/20/21 14:37
EDV
7471B
Molybdenum
14.8
mg/Kg- dry
0.358
2.11
20
07/26/2121:02
EDV
6020B
Nickel
14.,3
mg/Kg - dry
0.505
111
20
07/26/2121:02
EDV
6020E
Potassium
2290
mg/Kg - dry
73.8
527
50
07/27/21 18:09
EDV
6020B
Selenium
4.24
mg/Kg - dry
1.90
4.21
20
07/26/21 21�02
EDV
6020B
Sodium
Sal
mg/Kg - dry
42.1
211
20
07/26/2121:02
EDV
60206
Quallifiers/ DF
Dilution Factor
j
Estimated value
Definitions L
Limit Exceeded
MQL
Method Quantitation
Limit
Page 10 of 21
449 Springb:rook Rd, Charlotte, NC 28217
Mlain, 704.529,636A
www.waypointanalytical,corn,
Report Date 08/13/2021
Received 07/19/2021
Report Number : 21-200-0031 REPORTOFANALYSIS
Lab No : 91978 Matrix: Solids
Sample ID : Class A Sampled: 7/19120218:55
Test Results Units MDL MOIL DF Date I Time By Analytical
Analyzed Method
Zinc 625 mg/Kg - dry 4.84 21.1 20 07/26/21 21:02 EDV 6020E
Qualifiers/ DF Dilution Factor i Estimated vaiue
Definitions L Limit Exceeded MQL Method Quantitation Limit
Page 11 of 21
F4 *
ANAt,,y-riCAL, INC.
NUM"
Way.point Analytical
PO Box 240543
Charlotte NC 282240543
ATTENTION
Terri W Cole
ffil Ion
LABORATORY REPORT NUMBER
2107N67
DATE
July 28, 2021
Pritnary Data Review By Secondary Data Review By
Chris Pafford
Project Manager, AES
PLEASE NOTE:
Ashley Amick
Project Manager, Access Analytical
aamick@axs-ine.com
Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc),,
3080 Presidential Drive, Atlanta, GA 30340.
AES is SCDHEC certified laboratory # 98016, NCDENR certified tab # 562, GA certified tab # FL-E87582,
NFLAP certified laboratory # E87582
AIHA-LAP,LLC Laboratory ID: 100671 for Industriall-lygiene samples (Organics, Metals, PCM Asbestos,
Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal)
Direct Examination.
Local support services for this project are provided by Access Analytical, Inc, Access Analytical is a
representative ofAES serving client in the SC/NC/GA areas. All questions regarding this report should be directed
to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243
Page 12 of 21 Pagel of 7
—Z cn
C-3
0 0 MN� I ri
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0
Analytical Environmental Services, Inc
Date: 28-Jul-21
Client: Waypoint Analytical
Project: 21-200-0031 Case Narrative
Lab ID: 2107N67
Sample Receiving Nonconformance:
An additional unlabeled 250ml plastic bottle filled with aqueous matrix was received but not listed on the Chain of Custody.
The laboratory did not proceed with analysis on this bottle per Ashley Amick via email 07-22-21 as it was a temperature blank.
Page 14 of 21 Page 3 of 7
Analytical Environmental Services, Inc Date: 28-7ul-2.1
Client:
Waypoint Analytical
Client Sample 1D:
91978
Lab Order
2107N67
`rag Number:
Class A
Project Name.
21-200-0031
Collection bate:
7/1912021 8:55.00 AM
Lab ID:
21071`wT67-001A
Matrix:
Soil
Analyses Result Reporting
Y tual fiIDL Limit Units BatchID Dl late Analyzed Analyst
Nitrogen, Ammonia (as N) Extractable E350.1 MOD (E350.1)
Nitrogen, Ammonia (As N) Extractable 2810 53.2 101 -g/Kg dry 319533 10 07/27/2021 18:32 KV
PERCENT MOISTURE D2216
Percent Moisture 5.80 0 0 wt R460502 1 07123/2021 00:00 J"W
Quali:fiers:. . Value exceeds maximum contaminant level
BRL Nat Dmcted at MDL
ll holding [:noes for preparation or analysis exceeded
N Anedyac not NE:LAC certified
B Analyte detected in the associated method bla lk
ki Estimated value alcove ynanaatation. range
S Spike Recovery outside holes due to matrix.
> Greater than Result value
J Estimated value detected below Reporting Limit
Less than. Result value
Page 15 of 21
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Page 18 of 21 Page 7 of 7
0 0
Waypoint
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 282:L7
Main 704.529,6364
www,waypointanalytical.com
Shipment Receipt Form
Customer Number: 012�05
Customer Name: Town of Mooresville/RR WWTP
Report Number: 21-200-0031
Shipping Method
0 Fed Ex 0 US Postal (# Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
ff-_15ER
Shipping container/cooler uncompromised?
Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
Yes
0 No
COC properly completed
Yes
0 No
Samples in proper containers?
Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun,
Yes
0 No
Water - Sample containers properly preserved
Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
[_ Low
[_ Low
concentration EnCore samplers (48 hr)
conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments: — — - — -------- — ----
Signature: 1Stacy LCruz Date & Time: L07/:19_/202_1 _14:0.45
Page 19 of 21
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Page 21 of 21