WQ0039053_Renewal Application_20210818

Initial Review
Reviewer Thornburg, Nathaniel D
Is this submittal an application? (Excluding additional information.)*
r Yes r No
Permit Number (IR)* WQ0039053
Applicant/Permittee Bio-Nomic Services, Inc.
Applicant/Permittee Address 530 Woodlawn Street, Belmont, NC 28012
Is the owner in BIMS? r Yes r No Is the facility in BIMS? r Yes r No
Owner Type Organization
Facility Name Bio-Nomic Services, Inc.
County Gaston
Fee Category Major Fee Amount $0
Is this a complete
application?*
r Yes r No Complete App Date 08/18/2021
Signature Authority
Signature Authority Title
Signature Authority Email
Document Type (if non -application)
Email Notifications
Does this need review bythe hydrogeologist?* r Yes r No
Regional Office
CO Reviewer
Admin Reviewer
Below list any additional email address that need notification about a new project.
Email Address
Comments to be added to email notfication
Comments for Admin
Comments for RO

Comments for Reviewer
Comments for Applicant

Submittal Form
Project Contact Information
Rease provide information on the person to be contacted by N B Staff regarding electronic receipt, another correspondence. ittal, confirmation of iptd othd
.......................................................... ronc su_ -
Name * Martin Mabe
Email Address*
[e-mail]
Project Information
........ ......... ..........................................................................................................................................
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
3363121396
O Modification - Minor
G Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
r Wastewater Irrigation
r High -Rate Infiltration
r Other Wastewater
r Reclaimed Water
r Closed -Loop Recycle
r Residuals
r Single -Family Residence Wastewater
r Other
Irrigation
Permit Number:*
WQ0039053
Fbs Current Existing perm[ number
Applicant/Permittee*
Bio-NomicServices, Inc.
Applicant/Permittee Address*
530 Woodlawn Street, Belmont, NC28012
Facility Name *
Bio-Nomic Services DCAR
Please provide comments/notes
on your current submittal below.
Please contact Martin Mabe with questions
or comments about this permit application.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Spec'rfications, Calculations, Rc.)
WQ0039053 Permit Renewal Application.pdf 27.76MB
Upload only 1 RDF docurrent (less than 250 tVB). Mitiple documents nest be corrbined into one RDF file unless file is larger than
upload limit.
* W By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
�Wa4&_;r ew'?*
Submission Date 8/18/2021

APPLICATION FOR
DISTRIBUTION OF CLASS A RESIDUALS
PERMIT RENEWAL
BIO-NOMIC SERVICES, INC.
NON -DISCHARGE PERMIT NO. WQ0039053
Willcox & Mabe Soil Solutions, PLLC Project No. 15-18
Prepared for:
Bo-Nomic Services, Inc.
530 Woodlawn Street
Belmont, North Carolina 28012
Prepared by:
Willcox & Mabe Soil Solutions, PLLC
7231 B Surnmerfield Road
Summerfield, North Carolina 27'358
willcox&mabe
SO I L SOLUTIONS
August, 2021

August 18, 2021
NCDEQ/DWR
Water Quality Pennitting Section
5112 N. Salisbury Street
91h Floor, Office #942W
Raleigh, North Carolina 27604
Attention: Non -Discharge Permitting Unit
Reference: Renewal for Distribution of Class A Residuals
Bio-Nornic Services, Inc. WQ0039053
Willcox & Mabe Soil Solutions, PLLC Project No. 15-18, Phase: 14
Non -Discharge Permitting Unit:
Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting the enclosed application to
renew the existing Distribution of Class A Residuals permit WQ0039053 for Bio-Nomic
Services, Inc. (BNS) on behalf of BNS. The application package includes information for
renewing two Class A sources at this time: Greenville Utilities WTP — 2,000 Dry Tons and
City of Lenoir WTP - 2,000 Dry Tons. WMSS and BNS are requesting to delete the
following sources from the permit: Williams WTP — 4,000 Dry Tons, Chatham County
WTP — 500 Dry Tons, and McCall Farrns WTP — 6,000 Dry Tons.
It should be noted that Greenville Utilities WTP and City of Lenoir VV7P have not
distributed any Class A biosolids during the 2021 calendar year. Therefore, the most recent
analytical results that were collected during distribution events in the 2020 calendar year
were utilized for the renewal application. All analytical required by pen -nit will be
conducted in the future prior to any land application distribution events.
If there is any further information required or questions regarding this application please do
not hesitate to contact Bio-Nomic's, Mr. Vaughn "Buck" Stevenson at [phone] or
WMSS's Mr. Martin Mabe at 336-312-1396 for further assistance.
Sincerely,
Willcox & Mabe Soil Solutions, PLLC
Martin Mabe
Agronomist
cc: Bio-Nomic Services, Inc.
Rob Willcox, L.S.S.
Licensed Soil Scientist
15-18 Bio-NorniesThase 09 - BNS Class A PermitQ021 Permit Renewalkl 5-18 Bionornics Distribution of Class A Residuals Application
Package,doc
Willcox & Mabe Soil Solutions, PLLC / 7231 B Summeffield Road / Surnmerfield, NC 27358 / Rob 336.339.9128 or
Martin 336,312.1396 / www.willcoxmabesoil.com

TABLE OF CONTENTS
APPENDIX TITLE
DISTRIBUTION OF CLASS A RESIDUALS
APPLICATION FORM
(FORM: DCAR 06-16)
II FORM DCAR 06-16 (ITEM D. - PROGRAM INFORMATION)
III FORM DCAR 06-1.6 (ITEM H. - OPERATION AND MAINTENANCE
PLAN)
IV RESIDUALS SOURCE CERTIFICATION
APPLICATION FORM
GR.EENVILLE UTILITIES WTP
(FORM: RSC 06-1.6)
V RESIDUALS SOURCE CERTIFICATION
APPLICATION FORM
CITY OF LENOIR'TP
(FORM: RSC 06-16)

APPENDIX 1
DISTRIBUTION OF CLASS A RESIDUALS
APPLICATION FORM (DCAP 06-16)

State of North Carolina
DWR
Department of'Environmental Quality Division of Water Resources
Division of Water Resources 15A NCAC 02T.1100 — DISTRIBUTION OF CLASS A RESIDUALS
INSTRUCTIONS FOR FORM: DCAR 06-16 & SUPPORTING DOCUMENTATION
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce: the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and
Mpporting documentation
For snore information, visit the Water Quality Permitting Section's Non-Dischar�e Pennitting Unit website
General — This application is for, treatment, storage, transport, distribution, land application, and/or marketing of Class A (or Equivalent)
residuals under 15A NCAC 02T .1100.
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Distribution of Class A Residuals (FORM: DCAR 06-16):
Submit the completed and appropriately executed Distribution of Class A Residuals (FORM: DCAR 06-16) form. Please do
not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to
the application may be made, as long as the attachments are numbered to correspond to the section and item to which they
refer.
The project name should be consistent on the plans, specifications, etc,
The Applicant's Certification on Page 3 of this form shall be signed in accordance with 15A NCAC 02T,0I 06(b). An alternate
person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A
NCAC 02T.0106(b).
If this project is for a modification of an existing permit, submit one copy of the existing permit,
El Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to
operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units.
B. Application Fee (New and Major Modification Application Packages)
0 Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental
Quality (NCDEQ).
Facility Classification I New Permit I Major Modification'
Major (residuals permitted for distribution > 3,000 dry tons/year) $1,310 $395
Minor (residuals permitted for distribution < 3,000 dry tons/year) � $810 1 $245
' - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage;
adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted.
There is no fee for minor permit modifications.
C. Cover Letter (All Application Packages)
M List all items included in the application package, as well as a brief description of the requested permitting action.
INSTRUCTIONS FOR FORM: DCAR 06-16 Paget of3

D. Program Information (All Application Packages)
Provide a narrative explaining the following:
How the materials will be handled and transported from where the residuals were produced to where it will be treated.
How the residuals will be processed/treated (attach process flow diagram).
How leachate collection will be handled.
❑ Where the residuals will be stored until processed.
How the final product will be distributed (packaging, bulk, etc.)
What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum, calcium, etc.,) are used or recommended as the
limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause
contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality.
Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed.
Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the
person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following
information:
Name and address of the person who prepared the residual that is sold or given away,
A statement that application of the residuals to the land shall be in accordance with the instructions on the label or
information sheet.
A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered.
A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored
residuals into any surface waters.
Information on all applicable setbacks in accordance with 15A NCAC - 02T_J 108(b).
A statement that the residuals shall be applied at agronomic or recommended rates for intended uses.
E. Detailed Plans and Specifications (Application Involving New or Changes to Treatment or Storage Units)
El Submit detailed plans and specifications that have been signed, sealed, and dated by a NC Professional Engineer per 15A
NCAC 02T .1104(a). Specifications for standard equipment may only be omitted for municipalities with approved standard
specifications, but use of the standard specifications must be noted on each sheet of the plans.
0 Plans must include the following minimum items: a general location map, a topographic map, plan and profile view of the
residuals treatment and storage units as well as the proximity of the residuals treatment and storage units to other utilities and
natural features within 500 feet of all treatment and storage facilities, and detail drawings of all items pertinent to the residuals
treatment and storage units,. Depict minimum separations required in 15A NCAC 02T. I 108(a) on the plans,
Ej Specifications must include, at a minimum, the following for all items pertinent to residuals treatment and storage units:
description of materials to be used, methods of construction, quality of construction testing procedures to ensure the integrity
of the final product in accordance with 15A NCAC 02T . I 104(a)(2)(B), including leakage and pressure testing as appropriate.
El Plans and specifications must not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR
CONSTRUCTION, etc.) that indicate that they are anything other than final plans and specifications. However, the plans and
specifications may be labeled with the phrase: FINAL DESIGN — NOT RELEASED FOR CONSTRUCTION.
F. Engineering Calculations (Application Involving New or Changes to Treatment or Storage Units)
F1 Submit all design calculations that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T
.1 104(a).
G. Environmental Assessments (Maybe Required— See 15A NCAC 1C.0300)
........................
El Submit a copy of the Findings of No Significant impact (FONSI) or Environmental Impact Statement (EIS). Also, include
information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals
treatment and storage facilities, An EA may also be required for private systems if any public funds and/or lands, are used for
the construction of the subject facilities.
INSTRUCTIONS FOR FORM: DCAR 06-16 Page 2 of 3

H. Operation and Maintenance Plan (New and Renewal Application Packages)
Ll For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan,
Z Submit the O&M Plan in accordance with 15A NCAC 02T. 1110 and include at a minimum:
Operational functions; describe the operation of the program to show what operations are necessary for the program to function
and by whom the functions are to be conducted.
Maintenance schedules; may include equipments calibration, maintenance of signs, etc.
Safety measures; may include safety training program, manuals, signs, etc.
Spill response plan; including control, containment, remediation, emergency contact information, etc.
Inspection plan including the following information;
Names and titles of personnel responsible for conducting the inspections.
Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected
location(s) and inspection frequency are representative of the residuals management program.
Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event
that noncompliance is observed.
Sampling and monitoring plan including the following information;
Names and titles of personnel responsible for conducting the sampling and monitoring.
Detailed description of monitoring procedures including parameters to be monitored.
Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow,
and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling
plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet
pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual
sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected
by cold temperatures.
ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL
SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS:
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF WATER RESOURCES
WATER QUALITY PERMITTING SECTION
NON -DISCHARGE PERMITTING UNIT
By U.S. Postal Set -vice:
1617 MAIL SERVICE CENTER
RALEIGH, NORTH CAROLINA 27699-1617
TELEPHONE NUMBER: [phone]
By Courier/Special Delivery;
512 N. SALISBURY STREET
RALEIGH, NORTH CAROLINA 27604
FAX NUMBER: [phone]
INSTRUCTIONS FOR FORM: DCAR 06-16 Page 3 of 3

State of North Carolina
Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T.1 IOU — DISTRIBUTION OF CLASS A RESIDUALS
FORM: DCAR 06-16
I. APPLICANT INFORMATION:
1. Applicant's name: Bio-Nomic Services, Inc
Applicant type: El Individual Z Corporation El General Partnership El Privately -Owned Public Utility
M Federal 0 State n Municipal F] County
Signature authority's name per 15A NCAC 02T.0106: Mr, Vaughn Stevenson Title: Vice President
Applicant's mailing address: 530 Woodlawn Street
City. Belmont State: NC Zip: 28012-
Telephone number: [phone] Email Address: [e-mail]
2. Consultant's name: Martin Mabc License Number (for P.E.): _
Affiliation:E] On Staff Z Retained (Firm: Willcox & Mabe Soil Solutions, PLLC)
Consultant's mailing address: 7231 B Summerfield Road
City: Summerfield State: NC Zip: 27358-.
Telephone number: [phone] Email Address: [e-mail]
3. Fee submitted: $0.00 (See Instruction B)
II. PERMIT INFORMATION:
1. Application is for (check all that apply): El new, F modified, M renewed permit
2. If this application is being submitted to renew or modify an existing pen -nit, provide the following:
Permit number: W00039053
Date of most -recently issued permit: March 22, 2017
Date of most -recently certified Attachment A (if different than the permit): March 9, 2020
111. FACILITY INFORMATION:
I . Name of residuals processing facility: Bio-Nomic Services, Inc.
City: Belmont State: NC Zip: 28012-
Coordinates: Latitude: 35' 16' 32" Longitude: 81'3' 7"
Datum: NAD 83
Method of measurement: MAP
Level of accuracy: Nearest Second
County where facility is located: Gaston
2. Facility contact (person familiar with residuals preparation):
Name: VauFhn "Buck" Stevenson Title: Vice President
Mailing address: 530 Woodlawn Street
City: Belmont State: NC Zip: 28012-
Telephone number: (LO4) 529-0000 E-mail address: [e-mail]
FORM: DCAR 06-16 Page I of 3

3. Is the residual process, facility also the generator? ❑ Yes; ❑ No
If No, please specify delivery frequency and quantity of residual to be processed: NIA
4. Length of residuals storage at facility: N/A days (Note: the Division requires minimum 30 days storage in units that are separate
from treatment system, i.e. not in clarifiers, aeration basins, etc.)
IV. RESIDUALS QUALITY INFORMATION:
1. Specify how these residuals will be distributed:
❑ sold or given away in bags or other containers; ❑ lawn (bulk),- ❑ home garden (bulk);
Z other (explain); Land Application
Note: Bulk residuals, shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a
load capacity of one metric ton or less.
2. Complete the following if residuals are to be mixed with other materials:
Type of Materials Amounts to be added
per 1.0 dry ton of residuals (dry ton)
3. Approximate amounts of the residuals received and processed at the facility: N/A dry tons per year,
4. Approximate amounts of the final product (processed residuals) to be distributed: N/A dry tons per year.
5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and
maximum storage times prior to distribution): N/A
6. Does the facility have a stormwater management plan? ❑ Yes; ❑ No
Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled: N/A
V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and submit the attached Residuals Source Certification and all associated documentation.
Residuals Source
Certification
FORM: DCAR 06-16 Page 2 of 3

Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units)
attest that this application for
has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge
the proposed design has been prepared in accordance with the applicable regulations,. Although certain portions of this submittal package
may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed
this material and have judged it to be consistent with the proposed design.
North Carolina Professional Engineer's Seal, Signature, and Date:
Applicant's Certification:
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T.01 05.
0 Yes [:1 No, Explain;
Vaughn Stevenson Vice President
(Signature Authority's Name — PLEASE PRINT) (Title)
attest that this application for Bio-Nom.ic.S.ervices, Inc. — Distribution of Class A Residuals
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water
Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed
and that if all required supporting information and attachments are not included, this application package will be returned to me as
incomplete.
Note, In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.6B, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil penalties up to $25,000 per violation.
Signature:
47
Date: d —
FORM. DCAR 06-16 Page 3 of 3

Water Resources
ENVIRONMENTAL QUALITY
March 22, 2017
PETER. P. FLEETWOOD - PRESIDENT
Bio-Nook SERVICES, INC,
516 RoUNTREE ROAD
CI-LA,RLo'rrE, NORTI-1 CAROLINA 28217
Dear Mr. Fleetwood:
ROY COOPER
Gove)-nor
MICHAEL S. REGAN
secrLICIly
S. JAY ZIMMERMAN
Dii-eclor
Subject: Permit No. WQ0039053
Bio-Nomic Services DCAR
Distribution of Class A Water
Treatment Plant Residuals
Mecklenburg County
In accordance with your permit application request received February 7, 2017, we areforwarding,
herewith Permit No. WQ0039053 dated March 22, 2017, to Bio-Nomic Services, Inc. for the operation of
the subject residuals management program.
This permit shall be effective from the date of issuance until February 28, 2022, and shall be subject
to the conditions and limitations as specified therein. Please pay particular attention to the monitoring
requirements listed in Attachment A, Failure to establish an adequate system for collecting and maintaining
the required operational information shall result in future compliance problems.
If any parts, requirements or limitations contained in this permit are unacceptable, the Permittee
has the right to request an adjudicatory hearing upon written request within 30 days following receipt of
this permit. This request shall be in the form of a written petition, conforming to Chapter 150E of the North
Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail Set -vice
Center, Raleigh, NC 27699-6714. Unless such demands are made, this permit shall be final and binding.
If you need additional information concerning this permit, please contact Troy Doby at (919)
8076336 or tro),,[e-mail],
Sincerely,
S . Jay Zimmerman, P,G,, Director
Division of Water Resources
cc: Chatham County Health Department (Electronic Copy)
Durham County Health Department (Electronic Copy)
Raleigh Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Nothing Cornpares'--'.-
State of North Carolina I Environmental Quality I Water Resources I Water Quality Permitting I Non-Dischiarge Permitting
1617 Mail Service Centrr I Raleigh, North Carolina 27699-1617
919-807-6332
711
�'p
Im

Mr. Peter P. Fleetwood
March 22, 2017
Page 2 of 2
Mooresville Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Martin Mabc, Rob Wilcox— Wilcox & Mabe: Soil Solutions (Electronic Copy)
Beth Buffington —Protection and Enforcement Branch (Electronic Copy)
Digital Permit Archive (Electronic Copy)
Central Files

NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF ENVIRONMENTAL QUALITY
RALEIGH
DISTRIBUTION OF CLASS A WATER TREATMENT PLANT RESIDUALS PERMIT
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as
amended, and other applicable Laws, Rules, and Regulations
PERMISSION IS HEREBY GRANTED TO
Bio-Nomic Services, Inc.
Mecklenburg County
FOR THE
operation of a residuals management program for Bits-Nomic Services, Inc. and consisting of the
distribution. of Class A Water Treatment Plant residuals generated by the approved facilities listed in
Attachment A with no discharge of wastes to surface waters, pursuant to the application received February
7, 2017, and in conformity with other supporting data subsequently filed and approved by the Department
of Environmental Quality and considered a part of this permit. The use and disposal of residuals are
regulated under Title 40 Code of Federal Regulations Part 257. This permit does not exempt the Permittee
from complying with the federal regulations.
This permit shall be effective from the date of issuance until February 28, 2022, and shall be subject to the
following specified conditions and limitations:
I. SCHEDULES
I . No later than six months prior to the expiration of this permit, the Permittee shall request renewal of
this permit on official Division forms. Upon receipt of the request, the Division will review the
adequacy of the facilities described therein, and if warranted, will renew the permit for such period of
time and under such conditions and limitations as it may deem appropriate. Please note Rule 15A
NCAC 02T.0 I 05(d) requires an updated site map to be submitted with the permit renewal application.
[I 5A NCAC 02T.01 08(b)(2), 02T.01 05(d), 02T.01091
II. PERFORMANCE STANDARDS
The subject residuals management program shall be effectively maintained and operated at all times so
there is no discharge to surface waters, nor any contravention of groundwater or surface water
standards. In the event the facilities fail to perform satisfactorily, including the creation of prolonged
nuisance conditions due to improper operation and maintenance, the Permittee shall immediately cease
distribution of residuals, contact the Raleigh Regional Office supervisor, and take any immediate
corrective actions. [G.S. 143-215,1]
1 This permit shall not relieve the Permittee of responsibility for damages to groundwater or surface
water resulting from the operation of this residuals management program, [15A NCAC 02B .02001,
02L .0100]
WQ0039053 Version 1.0 Shell Version 160210 Page 1 of 9

Only residuals generated by the facilities listed in Attachment A are approved for distribution in
accordance with this permit, [G,S. 143-215, 11
4. Pollutant concentrations in residuals distributed or applied to any land application site shall not exceed
the following Ceiling Concentrations or Monthly Average Concentrations (i.e., dry weight basis):
Parameter
Ceiling Concentration
(in illigrams per kilogranz)
Monthly Average
Concentration
(milligrams per kilogram)
Arsenic
75
41
Cadmium
85
39
Copper
4,300
1,500
Lead
840
300
Mercury
57
17
Molybdenum
75
n/a
Nickel
420
420
Selenium
too
100
Zinc
7,500
2,800
[ 15A NCAC 02T.11051
5. Residuals that are distributed shall meet Class A pathogen reduction requirements in 15A NCAC 02T
.1106 (a) and (b)(2). Exceptions to this requirement shall be specified in Attachment A. [15ANCAC
02T.1 106]
6. Setbacks for Class A land applied bulk residuals shall be as follows:
Setback Description
Setback by residual type
(feet)
Liquid
Cake I
Private or public water supply
too
100
Surface waters (streams — intermittent and perennial,
perennial waterbodies, and wetlands)
100
25
Surface water diversions (ephemeral streams,
waterwaLs, ditches)
25
0
Groundwater lowering ditches (where the bottom of
the ditch intersects the SHWT)
25
0
Wells with exception to monitoring wells
too
100
Bedrock outcrops
25
0
Unless otherwise noted in Attachment A, "cake" residuals are those that have greater than 15%
solids by weight and can be stacked without flowing, as well as can be handled, transported and
spread as a solid (e.g., using a backhoe, front end loader, clinger spreader, broadcast spreader or
other equipment designed for handling solid materials) without leaving any significant liquid
fraction behind.
[15A NCAC 02T. 1108]
WQ0039053 Version . 1.0 Shell Version 160210 Page 2 of 9

7, Bulk residuals and other sources of Plant. vailable Nitrogen (PAN) shall not be applied in exceedance
of agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen
requirements based an the determined Realistic Yield Expectations (RYE) using any of the following
methods:
a. Division's pre -approved site specific historical data for specific crop or soil types by calculating
the mean of the best three yields of the last five consecutive crop harvests for each field.
b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State
University Department of Soil Science (httl2://nutrients.soil.nesu.edu/yields/l*ndex.ph ). A copy
shall be kept on file and reprinted every five years in accordance with Condition rv.6.
c. If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the RYE
and appropriate nutrient application rates reported in any of the following documents:
i. Crop management plan as outlined by the local Cooperative Extension Office, the North
Carolina Department of Agriculture and Consumer Services, the Natural Resource
Conservation Service, or other agronomist,
ii. Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance
Document: Chapter I
http://www.ncagr.ggv/SWC/tech/documents/9th Guidance Doc 100109.pd-0,
iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation
Services (MRCS), These plans must meet the USDA -MRCS 590 Nutrient Management
Standards (ftp://ftp-fc.sc.nov.u.sda.gov/NHO/pi-actice-standards/standards/59O.Rda.
d, If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall
contact the Division to determine necessary action.
I 5A NCAC 02T .I 109(b)(1)(k)]
8, The Permittee shall not distribute Class A Water Treatment Plant residuals that have a sodium
adsorption ratio (SAR) of 10 or higher without prior written Division approval. The Permittee may
seek approval by demonstrating that the entity accepting the residuals is: aware of the effects of a high
SAR content; has agreed on proper residual application rates; and has agreed to operational
considerations to ensure that the high SAR content will not adversely impact the receiving sites.
Recommendations regarding sodium application rate, soil amendments (e.g., gypsum, etc,) or a
mechanism for maintaining site integrity and conditions conducive to crop growth, can be obtained
from the local Cooperative Extension Office, the Department of Agriculture and Consumer, Services,
the Natural Resource Conservation Service, allorth Carolina Licensed Soil Scientist, or an agronomist.
[15A NCAC 02T.0108(b)(1)]
WQ0039053 Version 1.0 Shell Version 16021.0 Page 3 of 9

111. OPERATION AND MAINTENANCE REQUIREMENTS
1. The residuals management program shall be properly maintained and operated at all times. The
program shall be effectively maintained and operated as a non -discharge system to prevent any
contravention of surface water, or groundwater standards, [15ANCAC 02T,1110]
2. The Permittee shall maintain an approved Operation and Maintenance Plan (O&M Plan) Modifications
to the O&M Plan shall be approved by the Division prior to utilization of the new plan. The O&M Plan,
at the minimum, shall include:
a. Operational functions;
b. Maintenance schedules;
c. Safety measures;
d. Spill response plan;
e. Inspection plan including the following information:
i. Names and/or titles of personnel responsible for conducting the inspections;
iL Frequency and location of inspections, including those to be conducted by the ORC, and
procedures to assure that the- selected location(s) and inspection frequency are representative
of the residuals management program;
iii. Detailed description of inspection procedures including record keeping and actions to be taken
by the inspector in the event that noncompliance is observed pursuant to the noncompliance
notification requirements under the monitoring and reporting section of the permit;
f. Sampling and monitoring plan including the following information:
i. Names and/or titles of personnel responsible for conducting the sampling and monitoring;
ii. Detailed description of monitoring procedures including parameters to be monitored;
iii. Sampling frequency and procedures to assure that representative samples are being collected.
Fluctuation in temperature, flow, and other, operating conditions can affect the quality of the
residuals gathered during a particular sampling event. The sampling plan shall account for any
foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to
meet pathogen reduction requirements (e.g. facilities that dispose multiple times per year but
have an annual sampling frequency, may need to sample during winter months when pathogen
reduction is most likely to be negatively affected by cold temperatures).
[I 5A NCAC 02T.1100]
Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC)
classification of the facility, the Permittee shall designate and employ a certified operator in responsible
charge (ORC) and one or more certified operators as back-up ORCs in accordance with I SA NCAC
08G .0201. The ORC or his back-up shall visit the facilities in accordance with 15A NCAC 08G. 0204„
or as specified in the most recently approved O&M plan (i.e., see Condition 111.2.), and shall comply
with all other conditions of 15A NCAC 080. 0204. For more information regarding classification and
designation requirements, please contact the Division of Water Resources' Protection and Enforcement
Branch at [phone]. At the time of this permit issuance, a certified ORC is not required for the
subject Distribution of Class A Residuals program, [ISANCAC 02T.0117]
4. When the Permittee land applies bulk residuals, a copy of this permit and a copy of O&M Plan shall be
maintained at the land application sites during land application activities. [15A NCAC 02T
.0108(b)(1)]
5. When the Permittee transports or land applies bulk residuals, the Spill control provisions shall be
maintained in all residuals transport and application vehicles. [15ANCAC 02T.1110]
WQ0039053 Version 1.0 Shell Version 160210 Page 4 of 9

6. When the Permittee land applies bulk residuals, adequate measures shall be taken to prevent wind
erosion and surface runoff from conveying residuals from the land application sites onto adjacent
properties or into surface waters. [G,S. 143-215. 1 ]
7. When the Permittee land applies bulk residuals, a suitable vegetative cover shall be maintained on land
application sites onto which residuals are applied, or application shall be in accordance with the crop
management plan outlined by the local Cooperative Extension Office, the Department of Agriculture
and Consumer Services, the Natural Resource Conservation Service, or an agronomist and as approved
by the Division. [15A NCAC 02T .1109(b)(1)]
8. Bulk residuals shall not be land applied under the following conditions:
a. If the residuals are likely to adversely affect a threatened or endangered species listed under section
4 of the Endangered Species Act or its designated critical habitat;
b. If the application causes prolonged nuisance conditions;
c, If the land fails to assimilate the bulk residuals or the application causes the contravention of surface
water or groundwater standards;
d. If the land is flooded, frozen or snow-covered, or is otherwise in a condition such that runoff of the
residuals would occur;
e. Within the 100-year flood elevation, unless the bulk residuals are injected or incorporated within a
24-hour period following a residuals land application event;
f During a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours
following a rainfall event of 0.5 inches or greater in a 24-hour period;
g. If the slope is greater than 10% for surface applied liquid residuals, or if the slope is greater than
18% for injected or incorporated bulk liquid residuals;
h. If the land does not have an established vegetative cover unless the residuals are incorporated or
injected within a 24-hour period following a residuals land application event. Any field that is in a
USDA no -till program shall be exempted from meeting this vegetative cover requirement;
i. If the vertical separation between the seasonal high water table and the depth of residuals
application is less than one foot;
j . If the vertical separation of bedrock and the depth of residuals application is less than one foot-,
k. Application exceeds agronomic rates.
[I 5A NCAC 02T. 1109]
9. The P'en-nittee shall notify all third -party entities receiving bulk distributed Class A Water Treatment
Plant residuals that land application activities occurring on the third-party's property shall meet the
requirements in 15A NCAC 02T .1 108(b)(1) and 02T .1 109(b) (i.e., Conditions 11.8. and 1118.,
respectively), [15A NCAC 02T .1103(5)]
10. All residuals shall be adequately stored to prevent untreated leachate runoff. The finished product may
be placed on a concrete pad, placed under shelter or physically covered until it is distributed to a third -
party entity, If bulk residuals are to be applied, the residuals may be staged at the application site for
up to 30 days for biological residuals, and 60 days for non-biologica[ residuals. If an alternate storage
site is used, approval must be obtained from the Division. [15A NCAC 02T .0108(b)(1)]
WQ0039053 Version 1.0 Shell Version 160210 Page 5 of 9

11, A label shall be affixed to the bag or other container in which residuals are sold or given away for land
application, or an information sheet shall be provided to the person who receives Class A residuals, At
a minimum, the label or information sheet shall contain the following:
a. The name and address of the person who prepared the residuals;
b. A statement that residual land application is prohibited except in accordance with the instructions
on the label or information sheet;
c. A statement identifying that this material shall be prevented from entering any public or private
water supply source (including wells) and any surface water (e.g., stream, lake;
- river, wetland, etc.);
d. A statement that the residuals shall be applied at agronomic rates and recommended rates for its
intended use,
[15A NCAC 02T .1 109(a)]
12. The Permittee shall not distribute bulk residuals to any person or entity known to be applying residuals
contrary to the conditions of this permit. The Permittee shall report to the Raleigh Regional Office as
per reporting conditions under Condition IV.8. any person or entity known to be applying residuals
contrary to the condition of this permit. [I 5A NCAC 02T. I 103(a)]
IV. MONITORING AND REPORTING REQUIREMENTS
I. Any Division -required monitoring (including groundwater, plant tissue, soil and surface water
analyses) necessary to ensure groundwater and surface water protection shall be established, and an
acceptable sample reporting schedule shall be followed. [15ANCACO2T.0108(c)]
2. Residuals shall be analyzed to demonstrate they are non -hazardous under the Resource Conservation
and Recovery Act (RCRA). Residuals that tests or is classified as a hazardous or toxic: waste under 40
CFR Part 261 shall not be used or disposed under this permit. The analyses [corrosivity, ignitability,
reactivity, and toxicity characteristic leaching procedure (TCLP)] shall be performed at the
frequency specified in Attachment A, and the Pen-nittee shall maintain these results for a minimum of
five years. Any exceptions from the requirements in this condition shall be specified in Attachment A.
The TCLP analysis shall include the following parameters (the regulatory level in milligrams per liter
is in parentheses):
Arsenic (5.0)
1,4-Dichlorobenzene (7.5)
Nitrobenzene (2.0)
Barium (100.0)
1,2-Dichloroethane (0.5)
Pentachlorophe:nol (100.0)
Benzene (0,5)
1, 1 -Dich loroethylene (0.7)
Pyridine (5,0)
Cadmium (1,0)
2,4-Dinitrotoluene (0.13)
Selenium (1.0)
Carbon tetrachloride (0.5)
Endrin (0,02)
Silver (5.0)
Chlordane (0.03)
Hexachlorobenzene (0.13)
Tetrachloroethylene -(0,7)
Chlorobenzenc (100.0)
Heptachlor (and its hydroxide)
(0.008)
Toxaphene (0,5)
Chloroform (6.0)
Hexachloro-1,3-butadiene (0,5)
Trichloroethylene (0.5)
Chromium (5.0)
Hexachloroethane (3.0)
2,4,5-Trichlorophenot (400.0)
m-Cresol (200.0)
Lead (5.0)
2,4,6-Trichlorophenol (2.0)
o-Cresol (200,0)
Lindane (0.4)
2,4,5-TP (Silvex) (1,0)
p-Cresol (200.0)
Mercury (0,2)
Vinyl chloride (0.2)
Cresol (200.0)
Methoxychlor (10.0)
;-D (I(
Methyl ethyl ketone (200.0)
WQ003,9053 Version 1.0 She]] Version 160210 Page 6 of 9

Once the: residuals have been monitored for two years at the frequency specified in Attachment A, the
Permittee may submit a permit modification request to reduce the frequency of this monitoring
requirement. In no case shall the monitoring frequency be less than once per permit cycle.
[ I SA NCAC 13A .01 02(b), 02T , 1101, 02T. 1105]
3. An analysis shall be conducted on the Class A residuals at the frequency specified in Attachment A,
and the Permittee shall maintain the results for a minimum of five years. The analysis shall include the
following parameters:
Aluminum
Mercury
Potassium
Ammonia -Nitrogen
Molybdenum
Selenium
Arsenic
Nickel
Sodium
Cadmium
Nitrate -Nitrite Nitrogen
sodium Adsorption Ratio
(SAR)
Calcium
Percent Total Solids
TKN
Copper
pH
Zinc
Lead
Phosphorus
Magnesium
L . . ................ . ..
Plant Available Nitrogen
(by calculation)
[I 5A NCAC 02T, I 101]
4. Residuals shall be monitored for compliance with pathogen reduction requirements at the frequency
specified in Attachment A, and at the time indicated in the sampling and monitoring sections of the
approved O&M plan, The required data shall be specific to the stabilization process utilized, and
sufficient to demonstrate compliance with the Class A pathogen reduction requirements in 15A NCAC
02T. 1106 (a) and (b)(2) shall be met. Any exceptions from the requirements in this condition shall be
specified in Attachment A. [15ANCAC 02T.1106,02T.1107,02T.1111(c)]
5. Laboratory parameter analyses shall be performed on the residuals as they are distributed, and shall be
in accordance with the monitoring requirements in 15A NCAC 02B ,0505. [15A NCAC 0213,0505]
6. The Permittee shall maintain records tracking all bulk residual distribution or land application events
performed by the Permittee. At a minimum, these records shall include the following:
a. Source of residuals;
b. Date of distribution/land application;
c. Name and address of recipient of residuals;
d. Volume of residuals distributed to each recipient;
e. lntended use of residuals;
f. If land application events performed by the Permittee -Nitrogen Application Rate based on RYES
(if using data obtained from the North Carolina State University Department of Soil Science
Website, the printout page shall be kept on file and reprinted every five years),
I 5A NCAC 02T.0109(a)]
WQ003 9053 Version I .O Shell Version 160210 Page 7 of 9

V.
7. Three copies of an annual report shall be submitted on or before March I'. The annual report shall
meet the requirements described in the Instructions for Residuals Application Annual Reporting Forms,
Instructions for reporting and annual report - forms are available at
http,Hportal.ncdenr,orgtweb/wq/aps/lau/roorting, or can be obtained by contacting the Land
Application Unit directly, The annual report shall be submitted to the following address-,
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[I 5A NCAC 02T. I I I I(a)]
8. Noncompliance Notification
The Permittee shall report by telephone to the Raleigh Regional Office, telephone number (919) 791 -
4200, as soon as possible, but in no case more than 24 hours or on the next working day following the
occurrence or first knowledge of the occurrence of any of the following:
a. Distribution of residuals abnormal in quantity or characteristic.
b. Any failure of the distribution program resulting in a release of material to surface waters.
c. Any time self -monitoring indicates the facility has gone out of compliance with its permit
limitations.
d. Any process unit failure, due to known or unknown reasons, rendering the facility incapable of
adequate residual treatment.,
e. Any spill or discharge from a vehicle or piping system during residuals transportation.
Any emergency requiring immediate reporting (e.g., discharges to surface waters, imminent failure of
a storage structure, etc.) outside normal business hours shall be reported to the Division's Emergency
Response personnel at telephone number [phone], [phone], or [phone].Persons
reporting such occurrences by telephone shall also file a written report in letter foam within five days
following first knowledge of the occurrence, This report shall outline the actions taken or proposed to
betaken to ensure that the problem does not recur. [15ANCACO2T.0105(1),02T.0108(b)(1)]
1. The Permittee shall provide adequate inspection and maintenance to ensure proper operation of the
subject facilities and shall be in accordance with the approved O&M Plan. [15ANCACO2T.0108(b)]
2. Prior to each bulk residuals distribution event, the Permittee or his designee shall inspect the residuals
storage, transport and distribution facilities to identify malfunctions, facility deterioration and operator
errors that could result in discharges to the environment, a threat to human health or a public nuisance.
The Permittee shall maintain an inspection log that includes, at a minimum, the date and time of
inspection, observations made, and any maintenance, repairs, or corrective actions taken. The Permittee
shall maintain this inspection log for a period of five years from the date of inspection, and this log
shall be made available to the Division upon request, [ 15A NCAC 02T .0108(b)]
3. Any duly authorized Division representative may, upon presentation of credentials, enter and inspect
any property, premises or place on or related to the land application sites or facilities permitted herein
at any reasonable time for the purpose of determining compliance with this permit-, may inspect or copy,
any records required to be maintained under the terms and conditions of this permit; and may collect
groundwater, surface water or leachate samples, [G.S. 143-215.3(a)(2)]
WQ0039053 Version I .O Shell Version 1602 10 Page 8 of 9

VT. GENERAL CONDITIONS
1. Failure: to comply with the conditions and limitations contained herein may subject the Permittee to an
enforcement action by the Division in accordance with North Carolina General Statutes 143-215,6A to
143-215.6C. [G.S. 143-215.6A to 143-215.6C]
2. This permit shall become voidable if the residuals distribution events are not carried out in accordance
with the conditions of this permit. [15A NCAC 02T .0110]
3. This permit is effective only with respect to the nature and volume of residuals described in the permit
application and other supporting documentation. [G,S. 143-215.1]
4. The issuance of this permit does not exempt the Permittee from complying with any and all statutes,
rules, regulations, or ordinances, which may be imposed by other jurisdictional government agencies
(e.g., local, state, and federal). Of particular concern to the Division are applicable river buffer rules in
15A NCAC 02B .0200; erosion and sedimentation control requirements in 15A NCAC Chapter 4 and
under the Division's General Pen -nit NCG010000; any requirements pertaining to wetlands under 15A
NCAC 02B.0200 and 02H,0500; and documentation of compliance with Article 21 Part 6 of Chapter
143 of the General Statutes. [15A NCAC 02T .0105(c)(6)]
5. In the event the residuals program changes ownership or the Permittee changes his name, a formal
permit modification request shall be submitted to the Division. This request shall be made on official
Division forms, and shall include appropriate documentation from the parties involved and other
supporting documentation as necessary. The Permittee of record shall remain fully responsible for
maintaining and operating the residuals program permitted herein until a permit is issued to the new
owner. [15A NCAC 02T .0104]
6. This permit is subject to revocation or unilateral modification upon 60-day notice from the Division
Director, in whole or part for the requirements listed in 15A NCAC 02T.01 10. [15ANCAC 02T.0110]
7. Unless the Division Director grants a variance, expansion of the permitted residuals program contained
herein shall not be granted if the Permittee exemplifies any of the criteria in 15A NCAC 02T,0120(b).
[I 5A NCAC 02T.0 120]
S. The Permittee shall pay the annual fee within 30 days after being billed by the Division. Failure to pay
the annual fee accordingly shall be cause for the Division to revoke this permit, [15A NCAC 02T
.0 1 05(e)(3)]
Permit issued this the 22nd day of March 2017
NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION
d-S. Jay Zimmerman, RG, Director
Division of Water Resources
By Authority of the Environmental Management Commission
Permit Number WQ0039053
WQ0039053 Version 1.0 Shell Version 160210 Page 9 of 9

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i�fJY C 0 P E R
Governor
441CHAEL S, REGM,l
:Seca ctnrY
S. DAT',IIEL SMITH
Director
VAUGHN STEVENSON —VICE PRESIDENT
Bio-Nomic SERVICES, INC.
530 WOODLAWN STREET
BELMONT, NORTH CAROLINA 28012-2130
Dear Mr. Stevenson:
�10RTH CAROL1111A
March 9, 2020
Subject: Permit No. WQ0039053
Bio-Nomic Services DCAR
Attachment A Certification
Gaston County
In accordance with your permit major modification request received December 3, 2019, and
subsequent additional information received January 31, 2020, we are forwarding herewith a modified
Attachment A certified March 9, 2020, to Bio-Nomic Services, Inc. for the subject residuals management
program.
Modifications to the subject Attachment are as follows: Addition of 2,000 dry tons/year from
George L. Bernhardt, Sr. Lake Rhodhiss WTP (Permit No. NCO 114010) located in Caldwell County.
The modified Attachment Ashall be effective from the date of certification until February 28, 2022
(i.e., expiration date of the current permit), shall void Attachment A of Permit No. WQ0030953 issued
March 22, 2017 that was previously certified on April 16, 2019, and shall be subject to the conditions and
limitations as specified therein, as well as those specified in the above -referenced permit. Please replace
Attachment A of Permit No. WQ0039053 that was certified on April 16, 2019 with the modified
Attachment A. Please note that the Permittee shall submit a renewal application no later than
September 1, 2021.
If any parts, requirements or limitations contained in this certification are unacceptable, the
Permitter, has the right to request an adjudicatory hearing upon written request within 30 days following
receipt of this permit. This request shall be in the form of a written petition, conforming to Chapter 150B
of the North Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail
Service Center, Raleigh, NC 27699-6714. Otherwise, this certification shall be final and binding.
If you need any additional information concerning this matter, please contact Poonarn Giri at (919)
707-3656 orocat,llyda.1
Sincerely,
:72S. Daniel Smith, Director
6 Division of Water Resources
Ncyr'lh (:..mAkaj o
.A2 Nol 0) .weld 'Aluvy I K'i7 I tAl Clroi�m„ , i.('17

Mr. Vaughn Stevenson
March 9, 2020
Page 2 of 2
cc: Caldwell County Health Department (Electronic Copy)
Asheville Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Mooresville Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Raleigh Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Martin Mabe — Willcox and Mabe Soil Solutions, PLLC (Electronic Copy)
Laserfiche File (Electronic Copy)
Digital Permit Archive (Electronic Copy)
Central Files

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APPENDIX II
FORM DCAR 06-16 (ITEM DM - PROGRAM INFORMATION)

FORM DCAR 06-16 (ITEM D. PROGRAM INFORMATION)
D. Program Information (Bio-Nomic Services, Class A Residuals)
Currently, Biro-Nomic Services is proposing to renew two source: Greenville Utilities
WTP and the George L. Bernhardt, Sr. Lake Rho.dhiss WTP (in association with
dewatering WTP residuals on an as -needed basis.)
• How the materials will be handled and transported from where the residuals
were produced to where it will be treated.
The operational functions of this program involve removing Class A Residuals from the
respective WTP's and beneficially recycling the biosolids to land application sites which
meet NCDEQ-DVvR regulatory requirements. Class A Residuals will be land applied at
or below agronomic rates.
0 How the residuals will be processed/treated (attach process flow diagram).
The Class A Residuals will be tested at the respective treatment plants prior to hauling for
land application.
• How leachate collection will be handled.
Leachate will not be generated
• Where the residuals will, be stored until processed.
Class A Residuals will be stored at the respective treatment plants
0 How the final product will be: distributed (packaging, bulk, etc.)
Class A Residuals will be land applied, not distributed
• What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum,
calcium, etc.) are used or recommended as the limiting parameter for
determination of residuals loading rate to ensure that it does not overload the
soil and cause contravention of surface water or groundwater standards, limit
crop growth, or adversely impact soil quality.
Product Information Labels and Application Information Sheets are attached.

D. Program Information (Bio-Nomic Services Class A Residuals) Page 2
• Attach a marketability statement detailing destinations and approximate
amounts of the final product to be distributed.
Product Information Labe -Is and Application Information Sheets are attached
• Provide either a label that shall be affixed to the bagged processed residual or an
information sheet that shall be provided to the person who receives the
processed residual. The label or information sheet shall contain, at a minimum,
the following information:
• Name and address of the person who prepared the residual that is sold or given away.
• A statement that application of the residuals to the land shall be in accordance with
the instructions on the label or information sheet.
• A statement that the residuals shall not be applied to any site that is flooded, frozen or
snow-covered.
• A statement that adequate procedures shall be provided to prevent surface runoff from
carrying any disposed or stored residuals into any surface waters.
• Information on all applicable setbacks in accordance with 15A NCAC 02T I 108(b).
• A statement that the residuals shall be applied at agronomic or recommended rates for
intended uses.
Product Information Labels and Application Information Sheets are attached

APPENDIX III
FORM TAP. 061-1.6 (ITEM H. OPERATION AND MAINTENANCE PLAN)

BIO-NOMIC SERVICES, INC.
NON -DISCHARGE PERMIT NO. WQ0039053
OPERATIONS AND MAINTENANCE PLAN
CLASS A RESIDUALS
I. Purpose
To put into place a plan that implements the requirements of North Carolina Department
of Environmental Quality — Division of Water Resources (NCDEQ-DWR) Permit No,
WQ0039053 for Bio-Nomic Services, Inc. (Rio-Nomic Services). Requirements are
included for the Class, A source(s) (WWTP's and WTP's) and Bio-Nomic Services (land
application contractor). Class A source(s) are listed within the permit.
11. . Operational Functions
The operational functions of this program involve hauling Class A Residuals from the
respective WWTP's and WTP's to land application sites which meet NCDEQ-DWR
regulatory requirements. Class A Residuals, will be land applied at or below agronomic
rates. Bio-Nomic Services will also account for any nutrient sources the
landowner/lessee has applied. Some source(s) may be land applied as either a liquid or
cake material utilizing either pumper trucks, vacuum trucks, tractor trailer, tractor and
cake spreader and/or tractor and pull tank. Class A Residuals will be spread evenly and
at consistent rates. Class A Residuals will be larid applied on fields that are used for hay
production, grazing, or row crop production harvested for animal feed. In the case where
Class A Residuals are land applied on fields utilized for grazing, applications rates will
be reduced by 25% in accordance with USDA-NRCS 590 Nutrient Management
Standards. Grazed fields will be determined by Bio-Nomic Services Operations Manager
on site.
The Bio-Nornic Services Class A Residuals will be monitored to confirm its compliance
with conditions in Non -Discharge Permit No. WQ0039053 to include,
• 15A NCAC 02T. 1105 Pollutant Limits and nutrient, analysis,
• Toxicity Characteristics Leaching Procedure (TCLP), and
0 Reactivity, Ignitability and Corrosivity
111. Maintenance Schedules
Bio-Nomic Services will follow the maintenance schedule as recommended by the
manufacturer for the equipment utilized to complete the job within the limits of the permit.
IV, Safety Measures
Bio-Nomic Services takes pride in operating in a safety conscious manner. Employees
participate in regular safety training that is designed to help employees recognize safety
issues and take steps to prevent potential accidents from occurring. Bio-Nomic Services
employees have the authority to stop operations if they think any aspect of the operation
is going to lead to the cause of an environmental or personal accident.
C:WsersWartinkWillcox and Mabe Soil SolutionMRob Willcox - Shared=MSS PrOjects=l 5115-18 Bio-NomicskPhase 09 - Class A Permift2019 Permit
Modirication (Lenoir WrP)kBio.Nomlc Services Class A O&M Plan 20 1 8.doc 11-21 .19

B10-NOMIC SERVICES, INC.
NON -DISCHARGE PERMIT N6. WQ0039!053
OPERATIONS AND MAINTE NANCE PLAN
CLASS A RESIDUALS
V. Spill Response Plan
• Halt the source of the spill: Such as a ruptured line or valve, or damaged transportation
unit.
Contain spill: Use straw bales to form a barrier. Straw or hay bales can be obtained
from several sources for this purpose. Soil near the site can also be used to form a barrier
for containment.
Clean up: Use Class A Residuals application equipment to recover as much of the
material as possible. After the application equipment has recovered as much material as
possible, it will be land applied as per the management plan. A temporary sump pit may
be dug in the containment area and spilled material washed into it to enhance recovery.
Final Clean up: The ultimate goal will be to restore the spill area to its original
condition if possible.
0 Notification: As soon as possible after a spill occurs notify:
• Bio-Nomic Services — Home Office
704-529-0000
Andy Taylor
704-907-7933
Joel Coert
704-904-9704
Buck Stevenson
704-930-8886
• Department of Environmental Quality
Division of Water Resources
Applicable Regional Office (See Pen -nit)
Management of clean-up efforts: The field superintendent shall take immediate charge
of the clean-up activities. Additional labor will be requested from Bio-Nomic Services as
needed.
VI. Reporting
Within 24 hours of a spill the field superintendent shall present a written report detailing the
cause of the spill and all action taken in response to the spill. Bio-Nornic Services will notify
the appropriate Regional Office as soon as possible, but not more than 24 hours after, or on the
next working day following the occurrence
V11. Inspection Plan
Inspections for the land application of Class A Residuals will be conducted at a minimum of
daily at the land application site during land application events. Inspections will consist of
inspecting the currentfield(s) that are being applied on, as well as inspecting random fields
that have previously received Class A Residuals applications. Inspections will be performed
by Bio-Nomic Services personnel on a rotational basis to ensure that all employees are
familiar with the inspection processes. At a minimum, these inspections will consist of the
following:
CAUsersWartinkWillcox and' Mahe Soil Solutlonsftb Willcox - Shared\WMSS Prqjects2015115-18 Bio-Nomics%Phase 09 - Class A Permit12019 Permit
Modification (Lenoir VVTP)\Sio-Nomic services Class A O&M Plan 201 BAOC 11-21-19
2

BIO-NOMIC SERVICES, INC.
NON -DISCHARGE PERMIT NO. WQ0039053
OPERATIONS AND MAINTENANCE PLAN
CLASS A RESIDUALS
• Verify that a residuals analysis has been collected prior to land application
activities being performed and that it meets the criteria for land application,
• Verify that pathogen reduction data has been collected for the source to be land
applied and that it meets the criteria for land application.
• Verify the crop that is planted or is to be planted on the respective field(s).
• Confirm that the correct amount of Class A Residuals are being land applied.
• Confirm that transport and application vehicles have a copy of the spill control plan.
• Confirm that a copy of the permit and the operations and maintenance plan are
maintained at the land application sites during land application activities.
• Check that the field has, been properly flagged and that buffers are adhered to.
• Confirm that records are turned in at the end of each business day.
Inspections will also be conducted by the respective employees of the Class A Residuals
generating facilities (at the source generating facility). Bio-Nomic Services is not
responsible for inspections at the source generating facilities. These inspections
should be conducted by the respective ORC of each facility and should fall under
their own Operations and Maintenance Plans.
VIII. Sampling and Monitoring Plan
All sampling and monitoring shall be performed in accordance with current Permit No,
WQ0039053, Bio-Nomic Services Class A Residuals.
Pollutant concentrations for Class A Residuals shall not exceed the following Ceiling
Concentrations or Monthly Average Concentrations (i.e,, dry weight basis):
Parameter
Ceiling Concentration
(milligramsper
kilogram)
Monthly Average
Concentration
(milligranis per kilogram)
Arsenic
75
41
Cadmium
85
39
Copper
4,300
1,500
Lead
840
300
Mercury
57
17
Molybdenum
75
n/a
Nickel
420
420,
Selenium
100
100
Zinc
7,500
2,800
3

BIO-NOMIC SERVICES, INC.
,NON -DISCHARGE PERMIT NO. WQ,0039053
OPERATIONS AND MAINTENANCE PLAN
CLASS A RESIDUALS
Class A Residuals shall be analyzed to demonstrate it is non -hazardous under the Resource
Conservation and Recovery Act (RCRA). The analyses [corrosivity, ignitability, reactivity,
and toxicity characteristic leaching procedure (TCLP)] shall be performed prior to land
application of Class A Residuals.
TCLP analysis of Class A Residuals shall include the following parameters (the regulatory level in
milligrams per liter is in parentheses):
_-Arsenic (5.0)
1,4-Diclilorobenzene (7.5)_
Nitrobenzene (2.0)
Barium (100.0)
1,2-Dichloroethane(0.5)
-Pentacliforopheno](100.0)
Benzene (0.5)
1, 1 -Dichloroethylene (0.7)
Pyridine (5.0)
Cadmium (1.0)
2,4-Dinitrotoluen,- (0,13)
Selenium (1.0)
Carbon tetrachloride (0.5)
- Endrin (0.02)
Silver (5.0)
--ie-trachloroethylene
Chlordane (0.03)-
-Hexach lorobenzene (0.13)
(0.7)
Chlorobenzene (100.0)
Heptachlor (and its
- hydroxide).0.008)
Toxaphene (0.5)
Chloroform (6.0)
Hexachloro-1,3-butadione
- ( 0.5)
Trichloroeth lene (0.5)
y
Chromium (5.0)
Hexa loroethane (3,0)
2,4,5-Tricliloroplienol (400.0)
m-Cresol (200.0)
Lead (5.0)
-Lindane
2,4,6-Trichlorophenol (2.0)
o-Cresol (200.0)
(0.4)
2,4,5-TP (Silvex) (1.0)
P-Cresol (200.0)
-.Mercury (0.2)
Vinyl chloride (0.2)
Cresol (200.0)
Methoxychl or (10,0)
2,4-D (10.0)
iVlethyl ethylketone(200.0).
An analysis shall be conducted on the Class A Residuals based on conditions set forth in Permit No,
WQ0039053. The analysis shall include the following parameters:
Aluminum
Mercury
Potassium
Ammonia -Nitrogen
Molybdenum-
Selenium
Arsenic
Nickel
Sodium
Cadmium
Nitrate -Nitrite Nitrogen
Sodium Adsorption Ratio
(SAR)
Calcium
Percent Total Solids
TIN
Copper
pH
Zinc
Lead
Phosphorus
Magnesium
Plant Available Nitrogen
(by calculation)
Pathogen Reduction,: Per 15A NCAC 02T. 1106,
For DistributionlLand Application of Class A or E ditivalent:
Z A fecal co[iform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids

BIO-NOMIC SERVICES PRODUCT INFORMATION LABEL
ProducedlLandApplied By: Prepai-ei-:
Bio-Nomic Services, Inc, Respective WWTP's and WTP's
530 Woodlawn Street
Belmont, North Carolina 28012
For information on these products contact Bio-Nomic Services, Inc,
Vaughn "Buck" Stevenson, Vice President [phone]
The Bio-Nomic Services Class A Residuals are WTP Plant Residuals and VvTWTP Biosolids that
meet NCDEQ-DWR Class A land application requirements. The Bio-Nomic Services Class A
Residuals and Biosolids contain varying values of Nitrogen, Phosphorus and Potassium. Each
permitted Source will have a laboratory sample analyzed, with current nutrient values made
available prior to land application of the product,
Provisions for Application
Application of the Bid-Noinic Services Class A Residuals are prohibited except in accordance with
the provisions specified in the Application Information Sheet Application must conform to
standards identified in Permit WQ0039053 and include but are not limited to:
Setback Description
Private or public water supply sources
Setback
(feet)
100
Surface waters (streams — intermittent and Perennial, perennial waterbodies,
and wetlands)
25
Surface water diversions (ephemeral streams, waterways, ditches)
0
Groundwater lowering ditches (where the bottom intersects the SHWT)
0
Wells with exception to monitoring wells
100
Bedrock outcrops
0
Bio-Nomic Services Class A Residual Product Information Label

Application Information Sheet
1. Bio-Nomic Services Class A Residuals are intended for use as a fertilizer product.
Applications of Bio-Nomic Services Class A Residual should be made in accordance with
approved application standards and WQ0039053 permit conditions,
2. Bio-Nomic Services Class A Residuals shall not be applied to flooded, frozen, or snow
covered areas.
3. Application and storage of Rio-Nomic Services Class A Residuals must be conducted in
such a way as to prevent runoff from the application or storage site to any surface water.
4. Applications and loading rates of Rio-Nomic Services Class A Residuals shall be
applied at agronomic or recommended rates.
Contact Bio-Nomic Services for a copy of the most recent Class A Residuals analysis and
loading rates.
Bio-Nomic Services Class A Residual Product Information Label

BIO-NOMIC SERVICES CLASS A RESIDUALS RECEIPT FORM
1 1- (printed name) have received
pounds and/or gallons of the Bio-Nomic Services Class A Residuals, a copy of the Bio-Noinic
Services Class A Residual product information label, and a copy of the most recent analysis of
the product (if requested). I have read these documents and agree to adhere to the directions
specified on the Application Information Sheet and the Product Information Label.
Signature of Receiver Date of Receipt
Address of Receiver
BiD-N'omic Services Class A Residual Product Information Label

APPENDIX IV
RESIDUALS SOURCE CERTIFICATION
APPLICATION FORM
GREENVILLE UTILITIES WTP
(FORM: RSC 06-16)

State of North Carolina
DWR
Department of Environmental Quality Division of'Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
INSTRUCTIONS FOR FORM: RSC 06-16
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested.Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and
supporting documentation
For snore inforniation, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit
General — This certification provides detailed information of residuals source generating facility and its residuals quality for land
application, distribution, or disposal in accordance with 15A NCAC 02T .1.100. Do not submit this certification for review without
a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Residuals Source Certification (FORM: RSC 11-15):
Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) forrn. Please do not
make any unauthorized content changes to this form. if necessary for clarity or due to space restrictions, attachments to the
application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer.
For new or renewed permits, submit a separate certification for each source facility,
F] For modified pen -nits, submit a separate certification for only those facilities that are affected by the proposed modification.
Z Complete the residuals source facility summary page. List all new, renewed, or modified facilities,
B. Residuals Source -Generating Facility Information:
Z For each source facility, attach the following:
Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "CViap Guidance 6or
Residuals Land Application llermits",
Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals
are to be generated, treated, processed, and stored at the facility.
Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item L 8.
Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of
the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed,
and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during
processing.
Z Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies
sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition,
ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and
vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as
they are to be land applied, distributed, and/or disposed,
C. Residuals Quality Information:
For each source facility, attach the following:
Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification.
Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector
attraction reduction requirements,
El For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please
attach analytical results of residuals generated from a similar facility along with the description of similarities of the two
facilities.
INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of I

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I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Greenville Utilities Commission
2. Facility permit holder is: El Federal, F1 State, E Local Government, or [] Private.
Facility permit issued by: Z Div. of Water Resources, D Div. of Environmental Health,
or F-1 Other (explain: _),
3. Facility contact person and title: Julius Patrick, WTP Superintendent
Complete mailing address: PO Box 1847
City. Greenville State: NC Zip: 27835-1847
Telephone number: [phone] E-mail address: [e-mail]
4. Facility physical address: 1721 Waterway Road
City: Greenville State: NC Zip: 27834
Coordinates: Latitude: 35'38' 26.31" Longitude: 77'23' 55.74"
Datum: NAD83 Level of accuracy: Nearest hundredths of second
Method of measurement: MAP
5. Purpose of the facility -
El treatment of municipal wastewater, E] treatment of 100% domestic wastewater,
E treatment of potable water, n treatment of 100% industrial wastewater,
El treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: - % industrial and % domestic)
El other (explain:_).
6. Does the facility have an approved pretreatment program: El Yes No
7. Facility permitted/design flow: 22.5 MGD and facility average daily flow: 10.54 MGD
8. Average amount of residuals being generated at this facility 2000 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment., N/A
Type and volume of residuals storage (i.e., outside of residuals treatment units): 23 acres with a depth of 14 feet from the
invert to grade with a 350,000 cubic yard capacity.
11. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1, Specify if residuals are regulated under:
El 40 CFR Part 503 or 40 CFR Part 257,
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257,
2. Specify if residuals are defined under 15ANCAC 02T.1 102(6) as:
0 Biological 0 Non -Biological
FORM: RSC 06-16 Page 1 of 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems),
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be: completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: E] yes 0 no.
If yes, list the number(s): _
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.2 1 -
261.24: ❑ yes 0 no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Eurofins Test America and Date of analysis: 3/12/20
Passed corrosivity test: 0 yes El no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: ED yes [1' no, Flashpoint: > 176 OF (> 1400F)
Passed reactivity test. Z yes Elno. HCN: <0.01, mg/kg (<250) & H2S: 37.6 mg/kg (<500)
TCLP Parameter
Limit
(n,911)
Result
(mg/1)
TCLP Parameter
Limit
(n,911)
Result
(nigll)
Arsenic
5.0
<0.05
Hexachlorobenzene
0.13
<0.005
Barium
100.0
<0.5
Hexachloro- 1,3-Butadiene
0.5
<0,.05
Benzene
0.5
<0.02
Hexachloroethane
3.0
<0.05
Cadmium
1.0
<0.005
Lead
5.0
<0.05
Carbon Tetrachloride
0.5
<0.02
Lindane
0.4
<0.005
Chlordane
0.03
<0.0 1
Mercury
0.2
<0.2
Chlorobenzene
100.0
<0.02
Methoxychlor
10.0
<0.0 I
Chloroform
6.0
<0.04
Methyl Ethyl Ketone
200.0
<0. I
Chromium
5.0
<0.025
Nitrobenzene
2.0
<0.01
m-Cresol
200.0
< 0.02
Pentachlorophenol
100.0
<0.2
o-Cresol
200.0
< 0.02
Pyridine
5.0
<02
p-Cresol
200.0
< U2
Selenium
1.0
<0.05
Cresol
200.0
< 0.02
Silver
5.0
<0,025
2,4-D
10.0
<U
Tetrachloroethylene
0.7
<0.02
1,4-Dichlorobenzene
7.5
<0.02
Toxaphene:
0.5
<0.05
1,,2-Dichloroethane
0.5
<0.02
Trichloroethylene
0.5
<0,02
I,I-Dichloroethylene
0.7
<0.02
2,4,5-Trichlorophenol
400.0
<0. I
2,4-Dinitrotoluene
0,13
<0.,0I
2,416-Trichlorophenol
2,0
<0.05
Endrin
0,02
<0.005
2,4,5-TP (Silvex)
Lo
<0. I
Fleptachlor and its Hydroxide
0.008
<0.004
Vinyl Chloride
0.2
<0.02
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T.1 105.
a. For DistributionlLand Applicatio : Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Waypoint Analytical and Date of analysis: 9/11/20
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(M911T)
Monthly Average
Concentration Limits
(Class A Only)
(mg1kg)
Result
(nI91k9)
Arsenic
75
41
16.1
Cadmium
85
39
<0.613
Copper
4,300
1,500
319
Lead
840
300
23.1
Mercury
57
17
0.313
Molybdenum
75
n/a
1.53
Nickel
420
420
13.6
Selenium
100
100
4.93
Zinc
7,500
2,800
58.8
b. For Surface Disposal Unit (lantIrill): Fill in the following table with the results of the latest analyses (he,, on a dry weight
basis) for the following metal parameters:
Laboratory: - and Date of analysis: -
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(nag/kg)
Chromium
(ing1kg)
Nickel
(inglkg)
> 0 but< 25
30
200
210
El > 25 but < 50
34
220
240
El 50 but < 75
39
260
270
[-] 75 but < 100
46
300
3320
El3 100 but< 125
53
360
390
> 125
62
450
420
Result (niglkg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 16.3 %�
b. Fill in the: following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Waypoint Analytical and Date of analysis: 9/11/20
Parameter
Result
(mg1kg)
Aluminum
152,000
Ammonia -Nitrogen
307
Calcium
1,870
Magnesium
650
Nitrate -Nitrite Nitrogen
36.1
pH (Standard Unit)
6.2
Phosphorus
3,260
Potassium
549
Sodium
267
Total e1dahl Nitrogen
13,200
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 0.545
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g,, gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth],
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 20 %. This
rate is a (check one): N default value, or E3 actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (111) Year PAN
Five -Year
(ing4g)
Maximum Adjusted PAN
(mg/kg)
Surface
2,768
4,752
Injection/Incorporation
2,922
4,906
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses: NIA
FORK RSC 06-16 Page 4 of 5

7. Patho2en Reduction: Per 15A NCAC 02T.1 106, specify how residuals will meet the pathogen reduction requirements:
a, For Distribittiotilf.aiidApBlictition of Class A orEquivalent.
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,,
or
El A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
Alternative I [ 1 5A NCAC 02T. I 106(b)(3)(A)] - Time/Temperature Compliance,
Alternative 2 [15A NCAC 02T. 1 106(b)(3)(13)] - Alkaline Treatment,
El Alternative 3 [15A NCAC 02T. I 106(b)(3)(C)] - Prior Testing for Enteric VirusNiable Helm inth Ova.
Alternative 4 [15,A NCAC 02T. I 106(b)(3)(D)] - No Prior Testing for Enteric VirusNiable Helminth Ova.
Alternative 5 [15A NCAC 02T. I 106(b)(3)(E)-(K)l - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, F -1 heat drying, El heat treatment,
thermophilic aerobic digestion, El beta ray irradiation,
El gamma ray irradiation, or [] pasteurization.
b. For Land Application of Class B:
0 Alternative I [15A NCAC 02T.1106(c)(1)] -Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T. 1 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one. n aerobic digestion, El air drying, n anaerobic digestion,
El composting, or El lime stabilization.
c. For Surface Absposal.
El Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item 11. 7a. above,
E3 Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item 11. 7b. above.
El Exempt - If Daily Cover Alternative is chosen in Item 11.8. below [15A NCAC 02T.1 106(a)(2)],
M Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
& Vector Attraction Reduction (VAR): Per 15A NCAC 02T. 1107, specify how residuals will meet the VAR requirements:
[I Alternative I [15A NCAC 02T. 1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
El Alternative 2 [15A NCAC 02T. I 107(a)(2)) - 40-Day Bench Scale Test (Anaerobic Digestion),
E] Alternative 3 [15A NCAC 02T., 1 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
F] Alternative 4 [15A NCAC 02T.1 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
El Alternative 5 [15A NCAC 02T. I 107(a)(5)] - 14-Day Aerobic Processes.
Alternative 6 [15A NCAC 02T. I 107(a)(6)] - Alkaline Stabilization.
Alternative 7 [15A NCAC 02T. 1 107(a)(7)] - Drying of Stabilized Residuals,
Alternative 8 [15A NCAC 02T. I 107(a)(8)] - Drying of Unstabilized Residuals.
El Alternative 9 (15A NCAC 02T. 1 107(a)(9)] - Injection,
Alternative 10 [ 15A NCAC 02T. I 107(a)(I 0)] - Incorporation.
Alternative for Surface Disposal Units Only - Soil/Other Material Cover [ 1 5A NCAC 02T. I 107(b)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5
C,

BIO-NOMIC SERVICES, INC.
Specializing in today's needs for environmental protection.
530 Woodlawn Street - Belmont, North Carolina 28012 - (704) 5290000 - [phone]
GREENVILLE UTILITIES COMMISSION (GU'C)
GREENVILLE UTILITIES WATER TREATMENT PLANT
Residuals Source- Generating Facility Information
- Process Flow Narrative
Greenville Utilities Commission operates an existing water treatment plant at 1721 Waterway
Road, which produces drinking water for the local community. The source of raw water
originates from the Tar River,
The Greenville Utilities Water Treatment Plant has been operational since 1985 and has a
capacity of 10.5 MGD. In 1995, the plant was upgraded to accommodate, the treatment of an
additional 12 MGD bringing the plant's capacity to 22.5 MGD. The average daily flow is 10,54
million gallons per day.
Raw water from Greenville's sources is pumped into a 63-million-gallon impoundment where it
settles for five days to facilitate sedimentation. Then the introduction of a coagulant allows
particles to clump together allowing additional sedimentation to occur with the aid of
flocculators.
Upon the completion of settled water receiving ozone for primary disinfection, clear, sediment
free water is, pumped into 2 three -million -gallon storage tanks ready for distribution. The
collected sediment is discharged into a holding lagoon, GUC also utilizes eight deep
groundwater wells that have a combined capacity of 2.0 MGD which have previously been used
to meet the increasing water demands of the city.
The lagoon will hold the sediment until removal is necessary. A portable hydraulic dredge is
placed in the lagoon, to pump the materials out of the basin. The floating hydraulic dredge is
advantageous as it allows the lagoon to remain in service during the process. The sediment is
pumped in Slurry form to a 20,000-gallon receiving tank. The tank is fitted with mixers to
homogenize the materials for mechanical dewatering.
The mechanical dewatering process is accomplished with a mobile belt filter press system. An
anionic or catanionic polymer is introduced to concentrate the slurry during the dewatering
process. The belt filter press further removes water by compressing the residuals between filter
belts generating a filter cake. The filtrate water resulting from the process can be returned to the
lagoon.
The filter cake, is now suitable for either onsite land application or for loading into dump trucks
for transportation to a secondary application site as a soil amendment,
- Quantitative Justification for Residuals Production Rate
A minimum of 1,250 dry tons may be removed and land applied annually,
A Carylon Company

SAMPLING PLAN
Sampling Procedures
Accurate sampling is essential for valid laboratory test results.. All samples collected at the respective
Water Treatment Plant's (WTI'} are grab samples, which are samples taken at selected intervals to
represent conditions at a given location at a particular point in time.
Grab samples of residuals are stored in a manner that will not alter sample characteristics. Proper
preservatives are Used for specific parameters, The samples are kept under refrigeration at 4' C until
delivered to laboratory for analysis.
Sampling Log
Sampling information is recorded on a chain of custody (COG) form by Bio-Nornic Services personnel
provided by the respective laboratory that is performing the required testing required by the permit, Log
book entries include, at a inininium:
• Purpose of sampling
• Location of sampling point
• Type of sample (grab or composite)
• Name of person collecting samples
• Type of residuals sampled (undigested, post -digestion, post -storage)
• Number and volume of sarnple(s) collected
• Description of sampling point
• Date and: time of collection
The residual solids analysis will be conducted for, but not limited to, the following parameters, percent total
solids, phosphorus, lead, copper, cadmium, sodium, total Kjeldahl nitrogen, nitrate nitrogen, nitrite nitrogen,
rna g nesium, potassiLim, ziilc, nickel, arsenic, meremy, selenium, molybdellUrn, calcium, ammonia nitrogen,
aluminum and pH on an AnnLial Basis, or as required by permit Conditions based upon annual tons land
applied,

Review your project A
results through
Total Accem
Have a Question?
eurofins
Env irourient Tyr sflng
I'estrAmerica
Eurofins TestAmerica, Chicago
2417 Bond Street
University Park, IL 60484
Tel: [phone]
Laboratory Job ID: 500-179338-1
Client Project/Site: Greenville Utility Water Plant
For:
Bio-Nomics Services., I'nc.
530 Woodlawn Street
Belmont, North Carolina 28012
Attn: Vaughn Stevenson
Authorized for release by.-
313012020 3:20.,03 PM
Ken Hayes, Project Manager 11
[phone]
ken.hayes @testamericainc.corn
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are rioted in this report. This report may not be reproduced except in full,
and with written approval from the laborafoty. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratoty

Client: Blo-Nomics Services., Inc.
Project/Site: Greenville Utility Water Plant
Laboratory Job ID: 500-179338-1
Table of Contents
CoverPage ..............................................
1
Table of Contents .........................................
2
Case Narrative ...........................................
3
Detection Summary ........................................
4
Method Summary .........................................
Sample Summary .........................................
5
s
Client Sample Results ......................................
7
Definitions ...............................................
QC Association ...........................................
10
Surrogate Summary .......................................
13
QC Sample Results ........................................
Chronicle ................................................
17
26
Certification Summary ......................................
Chain of Custody .................................. . .......
27
28
Receipt Checklists .........................................
29
Page 2 of 29
Eurofins TestAmeriCa, chlcago
3/34/20

Case Narrative
Client: Bio-Nornics Services., Inc.
ProjectlSite: Greenville Utility Water Plant
Job ID: 500-179338-1
Laboratory: Eurofins TestAmieri:ca, Chicago
Narrative
Job Narrative
500-179338-1
Comments
No additional comments.
Job ID: 500-179338-1
Receipt
The samples were received on 3/1412020 12:10 PM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperature of the cooler at receipt was 1.8° C.
GCIMS VIDA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page,
GC/MS Semi VOA
No analytical or quality issues were noted, other than those described in the Definition s/Glossary page,
GC Semi VOA
Method 808113: DCB Decachlorobiphenyl Surrogate recovery for the following samples were outside the upper control limit: Greenville
Utility (500-179338-2) and (MB 500-535163/1-A). This samples did not contain any target analytes; therefore, re -extraction and/or
re -analysis was not performed.
Method 8082A: The RPD of the laboratory control sample (LCS) and laboratory control sample duplicate (LCSD) for preparation batch
500-535414 and analytical batch 500-535496 recovered outside control limits for the following analytes: PCB-1016 and PCB-1!260;
however, %recovery was within control limits for both the LCS and LCSD.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page,
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page,
General Chemistry
No analytical or quality issues were noted, other than those described in the Definition s1G lossa ry page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Eurofins TestArnerica, Chicago
Page 3 of 29 3/30/2090

Detection Summary
Client: Bio-Comics Services., Inc,
Job ID: 500-179338-1
ProjectlSite: Greenville Utility Water Plant
Client Sample ID: Greenville Utility
Lab Sample ID: 500-179338-2
Analyte Result Qualifier
RL
MDL Unit
DllFac D Method Prep Type
Flashpoin >176
Degrees F
I 1010A Total/NA
I IM',
Sulfide 37.6
5.00
mg/L
1 9034 Total/NA
pH 5,56 HF
0.200
su
I 9040C Total/NA
This Detection Summary does not include radiochemical test results.
Eu!rofins TestArnerica, Chicago
Page 4 of 2�9 3/30/2020

Method Summary
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville Utility Water Plant
. . .... ... ... -
Method Method Description
Job ID: 500-179338-1
Protocol Laboratory
8260D Volatile Organic Compounds by —GC/MS—"
9W846
TAL CHI
8270E Sernivolatile Organic Compounds (GCIMS)
SW846
TAL CHI
8081 B Organochlorine Pesticides (GC)
SW846
TAL CHI
8082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography
SW846
TAL CHI
8151A Herbicides (GC)
SW846
TAL CHI
60I0D Metals (ICP)
SW846
TAL CHI
7470A Mercury (CVAA)
SW846
TAL CHI
1010A Ignitability, Pensky-Martens Closed -Cup Method
SW846
TAL CHI
9014 Cyanide
SW846
TAL CHI
9034 Sulfide, Acid soluble and Insoluble (Titrimetric)
SW846
TAL CHI
9040C pH
SW846
TAL CHI
1311 TCLP Extraction
SW846
TAL CHI
3010A Preparation, Total Metals
SW846
TAL CHI
3510C Liquid -Liquid Extraction (Separatory Funnel)
SW846
TAL CHI
5030E Purge and Trap
SW846
TAL CHI
7470A Preparation, Mercury
SWB46
TAL CHI
8151A Extraction (Herbicides)
SW846
TAL CHI
9010E Cyanide, Distillation
SW846
TAL CHI
Protocol References-
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third' Edition, November 1986
And Its Updates,
Laboratory References:
TAL CHI = Eurofins TestAmerica, Chicago, 2417 Bond Street, University Park, IL 60484, TEL [phone]
Eurofins TestArnerica, Chicago
Page 5 of 29 3/30/2020

Sample Summary
Client: Bio-No,mics Services., Inc.
Project/Site: Greenville Utility Water Plant
Job ID: 500-179338-1
Lab Sample ID Client Sample ID Matrix Collected Received Asset ID
500-179338-2 Greenville.Utility Sludgeb-31-12/2000,00 6-3if4/20 —1110
Eurofins TestAmerica, Chicago
Page 6, of 29 3/30/2020

Client Sample Results
Client: Bio-Nomics Services,, Inc.
Project/Site: Greenville Utility Water, Plant
ClientSampleID: Greenville . Utility
Date Collected: 03112/20 00:00
Date Received: 03/14120 12:10
Method: 8260D - Volatile Organic Compounds by GC/MS - TCILP
Analyte
Result Qualifier
RL
T'T'Dichloroethene
NO
20,0
1,2-Dichloroethane
ND
20,0
2-Butanone (MEK)
ND
100
Benzene
ND
20.0
Carbon tetrachloride
ND
20.0
Chlorobenzene
ND
20.0
Chloroform
ND
40.0
Tetrachloroethene
ND
20.0
Trichloroethene
ND
20.0
Vinyl chloride
ND
20.0
Surrogate
%Recovery Qualifier
Limits
1,2-Dichlaroethane-d4 (Surr)
104
75-126
4-Bromofluorobenzone (Surr)
92
72-124
Dibromofluoromethane (Surr)
97
75-120
Toluene-d8 (Surr)
91
75-120
Method: 8270E - Sernivolatile Organic Compounds
(GC/MS) - TCLP
Analyte
Result Qualifier
RL
1,4-Dichlorobenzene
ND
-
—20-0
2,4,5-Trichlorophenol
ND
100
2,4,6-Trichlarophenol
ND
50.0
2,4-Dinitrotoluene
ND
10.0
Hexachlorobenzenie
ND
5,00
Hexachlorobutadiene
ND
50.0
Hexachloroethane
ND
50.0
Cresols
ND
20.0
Nilrobenzene
ND
10.0
Pentachlorophenol
ND
200
Pyridine
ND
200
Surrogate
%Recovery Qualifier
Limits
2,4,6-Tribromophenol (Surr)
--66 —
40-145
2-Fluorabiphenyl
60
34-110
2-Fluorophonol (Surr)
47
27-110
Nitrobenzene-d5 (Surr)
70
36-120
PhenoW5 (Surr)
29
20-100
Terphenyl-dN (Surr)
96
40-145
I
Method: 8081 B - Organochlorine Pesticides (GC) - TCLP
Analyte
Result Qualifier
RL
Chlordane (technical)
ND
10.0
Endrin
ND
5.00
Heptachlor
ND
4.00
Heptachlor epoxide
ND
4.00
gamma-BHC (Lindane)
ND
5.00
Methoxychlor
ND
10,0
Toxaphene
ND
50.0
Surrogate
%Recovery Qualifier
Limits
DCB Decachlorobiphenyl
140 X
30-130
Job ID: 600-179338-1
Lab Sample ID: 500-179338-2
Matrix. Sludge
MDL Unit
D Prepared
Analyzed
Dil Fac
ug/L
03126/20 17;09
20
ug/L
03/2612!0 17:09
20
ug/L
03/26120 17:09
20
ug/L
03126120 17:09
20
lyfo
ug/L
03/26120 17:09
ug/L
03/26/20 17:09
20
ug/L
03126/20 17:09
20
ug/L
03/26/20 17:09
20
ug/L
03/26/20 1T09
20
ug/L
03/26/20 17:09
20
Prepared
Analyzed
Dil Fac
b Y 72-6; ff "i 7.-'0-9
20
03126120 17:09
20
03126120 17:09
20
03126120 17:09
20
MDL Unit
D Prepared
Analyzed
Dil Fac
ug/L
03/24/20 0812
03/24/20 17:21
1
ug]L
03124/20 08:12
03/24/20 17:21
1
ug/L
03/24120 08A2
03/24/20 17:21
1
ug/L
03124120 0812
03/24120 1721
1
ug:/L
03124120 08:12
03/24/20 17:21
1
ug/L
03/24/20 08:12
03124120 17:21
1
ug/L
03/24/20 08:12
03124120 17:21
1
ug/L
03124/20 08:12
03/24120 17:21
1
ug/L
0,3124/20 08,12
03/24/20 17:21
1
ug/L
03/24/20 08:12
03/24/20 17:21
1
ug/L
03124120 05:12
03/24/20 17:21
1
Prepared
Analyzed
Dil Fac
�4120 08 �12
03124120 17,2-1
1
03/24/20 08:12
03124120 17:21
1
03124120 08:12'
03124120 17:21
1
03124120 08:12
03124120 17:21
1
03124120 08:12
03124120 17:21
1
03124120 08:12
03124120 17:21
1
MDL Unit
D Prepared
Analyzed
Dil Fac
mm ugIL
03/24/20 09:29
03/24120 21:31
ug/L
03124120 09:29
03124/20 21:31
ug/L
03/24120 0929
03/24/20 21:31
1
ug/L
03/24/20 09:29
03124120 21:31
1
ug/L
03/24120 09:29
03/24/20 21, 31
1
ug/L
03/24120 09:29
0312412!0 21:31
1
ug/L
03/24/20 09;29
03124/20 21:31
1
Prepared
Analyzed
Dil Fee
03124120 09:29
(53-124✓202 1:31
1
Eurofins TestAmerica, Chicago
Page 7 of 29 3/30/2020

Client Sample Results
Client: Bio-Nordics Services,, inc,
Job ID: 500-179338-1
Project/Site: Greenville Utility Water Plant
Client Sample ID: Greenville Utility
Lab Sample
ID: 500-179338-2
Date Collected: 03112120 00:00
Matrix:
Sludge
Date Received: 03/14/20 12.10
Method: 8081 B - Organochlorine Pesticides (GC) - TCLP (Continued)
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene 110
30-120
03_1_24120 _09-29
ON �412021:3?
—1
Method: 8082A - Polychlorinated Biphenyls (PCBs)
by Gas Chromatography
Analyte
I Result Qualifier
RL
IVIDL Unit
D
Prepared
Analyzed
Dill Fac
Hills
PC­B_1 0 i 6 91—
5. b
5g _/L
b-3—/26T2-6-1868
ow26/2o _oq 31
—1
PCB-1221 ND
5,00
uq1L
03125/20 18:08
03/26/20 M31
1
PCB-1232 NO
5.00
ug/L
03/25120 18,:08
03/26/20 09:31
1
PCB-1242 NO
5.00
ug/L
03/25120 18:08
03/26/20 M31
1
PCB-1248 NO
5.00
ug/L
03/25120 18:08
03/26/20 09:31
1
P'CB-1254 NO
5.00
ug/L
03125120 18:08
03/26/20 09:31
1
PCB-1260 NO *1
5.00
ug/L
0312512D 18M
03/26/20 09:31
1
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-rn-xylene 93
30-120
03J25120 16:08
b-3 �6120 09�.-31
1
DCB Decachlorobiphenyl 83
30-140
03125120 18:08
03126120 09:31
1
Method. 8151A - Herbicides (GC) - TCLP
Analyte Result Qualifier
—D
RL
IVIDL Unit
D
Prepared
Analyzed
Dil Fac
2,_4 - N b __
—0.100
—mgIL
-
03123/2-0 09:51
-63­124-720­13: 1­0
1
i Silvex (2,4,5-TP) NO
0.100
mg/L
03/23/20 09:51
03/24/20 13:10
1
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCAA 67
25-130
03123120 09.51
03a4120 1310
Method: 6010D - Metals (ICP) - TCLP
Analyte Result Qualifier
RL
IVIDL Unit
D
Prepared
Analyzed
Dil Fac
I Arsenic NO
0.0500
mg/L
03122120 16:15
03/23120 09-26
1
Barium NO
0.500
mg/L
03/22120 16:15
03123/20 09:26
1
Cadmium ND
0.00500
mg/L
03122120 16:15
03/23120 09:26
1
Chromium NO
0.0250
mgIL
03122/2:0 16:15
03/23120 09:26
1
Lead ND
0.0500
mg/L
03122/20 16:15
03/23120 09:26
1
Selenium NO
0,0500
mg/L
03122/20 16:15
03123/20 09,26
1
-Silver ND
0.0250
mg/L
03122/20 16:15
03123120 09:26
1
Method: 7470A - Mercury (CVAA) - TCLP
Analyte Result Qualifier
RL
IVIDL Unit
D
Prepared
Analyzed
Dil Fac
Mercury NO
0100
ug/L
03/23/20 07;50
03123120 12:04
1
General Chemistry
Analyte Result Qualifier
RL
MDL Unit
D
Prepared
Analyzed
Dil Fac
flashpoini>176
99.0
Degrees F
03127/20 08:27
1
Cyanide, Total ND
0.0100
mg/L
03123120 MOO
03/23/20 13;13
1
Sulfide 37.6
5.00
mg/L
03/17/20 12:37
1
pH 5.56 HF
0.200
su
03/30/20 10:22
1
Eurofins TestAmerica, Chicago
Page 8 of 29 3/30/2020

Definitions/Glossary
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville Utility Water Plant
Qualifiers
GC Semi VOA
Qualifier Qualifier Description
.1 LCS1LCSD RPD exceeds control limits,
X Surrogate recovery exceeds control limits
Metals
Qualifier Qualifier Description
i Result is less than the RL but greater than or equal, to the MDL and the concentration is an approximate value,
General Chemistry
Qualifier Qualifier Description
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request,
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report
13 Listedunder the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNIF Contains No Free Liquid
DER Duplicate Error Ratio (normalized' absolute difference)
Dil Fac Dilution Factor
OIL Detection Limit (DoDIDOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metalslanion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoDIDOE)
LOQ Limit of Quantitation (DoDIDOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MOIL Method Detection Limit
ML Minimum Level (Dioxin,)
NC Not Calculated
NO Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemilstry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
Job 0: 500-179338-1
Eurofins TestAmerica, Chicago
Page 9 of' 29 3/30/2020

QC Association Summary
Client: Bio-Nornics Services., Inc.
Job ID: 500-179338-1
Project/Site: Greenville Utility Water Plant
GC/MS VOA
--- — ------ --- - --- ..... .....
..........
-- - ----------
. ......
Leach Batch: 535216
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-179338-2 Greenville Utility
TCLP
Sludge
1311
LB 500-535216/1-A Method Blank
TCLP
Water
1311
Analysis Batch: 535461
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
179338-2 Greenville Utility
TCLP
Sludge
8260D
535216
LB 500-53521611-A Method Blank
TCLP
Water
8260D
635216
MB 500-535461/6 Method Blank
Total/NA
Water
8260D
LCS 500-535461/4 Lab Control Sample
Total/NA
Water
8260D
GC/MS Semi VOA
Leach Batch: 534637
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
179338-2
Greenville Niiii
TCLP
Sludge
1311
LB 500-534637/1-E
Method Blank
TCLP
Water
1311
500-179338-E-2-F MS
500-179338-E-2-F MS
TCLP
Sludge
1311
Prep Batch: 535134
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-179338-2
Greenville Utility
TCLP
Sludge
3510C
534637
LB 500-534637/1-E
Method Blank
TCLP
Water
3510C
534637
MB 500-53513411 -A
Method Blank
Total/NA
Water
3510C
LCS 500-535134/2-A
Lab Control Sample
Total/NA
Water
3510C
500-179338-E-2-F MS
500-179338-E-2-F MS
TCLP
Sludge
3510C
5,34637
Analysis Batch: 535155
Lab Sample, ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
�65-'179338-2
Greenville Utility
TCLP
Sludge
8270E
535134
LB 500-534637/1-E
Method Blank
TCLP
Water
8270E
535134
MB 500-53513411-A
Method Blank
Total/NA
Water
8270E
535134
LCS 500-535134/2-A
Lab Control Sample
TotalINA
Water
8270E
535134
500-179338-E-2-F MS
500-179338-E-2-F MS
TCLP
Sludge
8270E
535134
GC Semi VOA
............
Leach Batch: 534637
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-179338-2
Greenville Utility
TCLP
'§k!d_9e
1311
LB 500-534637/1-D
Method Blank
TCLP
Water
1311
LB 500-534637/1-F
Method Blank
TCLP
Water
1311
Prep Batch: 534960
Lab Sample to
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-179338-2
Greenville Utility
fC_iJFT"
Sludge
8151A
_5346_3_7
LB 500-53463711-E)
Method Blank
TCLP
Water
8151A
534637
MB 500-534960/1-A
Method Blank
Total/NA
Water
8151A
LCS 500-534960/2-A
Lab Control Sample
Total/NA
Water
8151A
Analysis Batch, 535129
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-179338-2
Greenville Utility
TCLP
Sludge
8151A
534966
Eurofins TestAmerica, Chicago
Page 10 of 29 3/30/2020

QC Association Summary
Client: Bio-Nomics Services., Inc. Job ID: 500-179338-1
Project/Site: Greenville Utility Water Plant
GC Semi VOA (Continued
Analysis Batch: 535129 (Continued)
Lab Sample ID
—
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
LB 00-53463711-E)
Method Blank
TCLP
Water
8151A
5,34960
MB 500-53496011 -A
Method Blank
Total/NA
Water
8151A
534960
LCS 500-534960/2-A
Lab Control Sample
Total/NA
Water
8151A
534960
Prep Batch: 535163
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
500-179338-2
Greenville Utility
TCLP
Sludge
3510C 534637
LB 500-534637/1-F
Method Blank
TCLP
Water
3510C 534637
i M B 500-535163/1 -A
Method Blank
Total/NA
Water
3510C
LCS 500-53516312-A
Lab Control Sample
Total/NA
Water
3510C
ME
LCS 500-535163/3-A
Lab Control Sample
TotaYNA
Water
3510C
Analysis Batch: 535231
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500 179338-2
Greenville Utility
TCLP
Sludge
8081E
535163
LB 500-534637/1-F
Method Blank
TCLP
Water
8081E
535163
MB 500-535163/1 -A
Method Blank
Total/NIA
Water
80818
535163
LCS 500-53516312-A
Lab Control Sample
Total/NA
Water
8081E
535163
LCS, 500-53516313-A
Lab Control Sample
Total/NA
Water
8081B
535163
Prep Batch: 535414
Lab Sample lD
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-179338-2
Greenville Utility
Total/NA
Sludge
3510C
MB 500-535414/1 -A
Method Blank
Total/NA
Water
3510C
LCS 500-535414/2-A
Lab Control Sample
Total/NA
Water
3510C
LCSD 500-535414/3-A
Lab Control Sample Dup
TotaltNA
Water
3510C
Analysis Batch: 535496
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
179338-2
Greenville Utility
Total/NA
Sludge
8082A
535414
MB 500-53541411 -A
Method Blank
Total/NA
Water
8082A
535414
LCS 500-53541412-A
Lab Control Sample
Total/NA
Water
8082A
535414
LCSD 500-53541413-A
Lab Control Sample Dup
Total/NA
Water
8082A
535414
Metals
.. ........
-
Leach Batch: 534637
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-179338-2
Greenville Utility
TCLP
Sludge
1311
LB 500-534637/1-B
Method Blank
TCLP
Water
1311
LB 500-534637/1-C
Method Blank
TCLP
Water
1311
Prep Batch: 534857
Lab Sample ID
Client Sample I!D
Prep Type
Matrix
Method
Prep Batch
500-179338-2
Greenville Utility
LP
Sludge
3i) 1-0 A
534637
LB 500-534637/1-B
Method Blank
TCLP
Water
3010A
534637
LCS 500-534857/2-A
Lab Control Sample
Total/NA
Water
3010A
Prep Batch: 534911
Lab Sample ID —
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-179338-2
Greenville Utility
TCLP
Sludge"
7470A
5-34-637
Eurofins TestArnerica, Chicago
Page 11 of 29 3/30/2020

QC Association Summary
Client: Bio-Norrics Services., Inc.
Project/Site: Greenville Utility Water Plant
Metals (Continued
Prep Batch: 534911 (Continued)
Job ID: 500-179338-1
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
LB 00-53463711-C
Method Blank
TCLP
Water
7470A 534637
MB 500-534911/12-A
Method Blank
Total/NA
Water
7470A
LCS 500-534911114-A
Lab Control Sample
Total/NA
Water
7470A
Analysis Batch: 534991
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-179338-2
Greenville Utility
TCLP
Sludge --
74-7 0 —A
534911
LB 500-534637/1-C
Method Blank
TCLP
Water
7470A
534911
1 MB 500-53491'1/12-A
Method Blank
TotalINA
Water
7470A
534911
LCS 500-534911114-A
Lab Control Sample
Total/NA
Water
7470A
534911
Analysis Batch: 535002
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-179338-2
Greenville Utility
TCLP
Sludge
6 0-10 —D
534857
LB 500-53463711-B
Method Blank
TCLP
Water
60101)
534857
LCS 500-534857/2-A
Lab Control Sample
Total/NA
Water
6010D
534857
General'Cheap
Analysis Batch: 534269
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
179338-2
Greenville Utility
TotalINA
Sludge
9034
MB 500-534269/1
Method Blank
TotalINA
Water
9034
LCS 500-53426912
Lab Control Sample
Total/NA
Water
9034
Prep, Batch: 534916
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
179338-2
Greenville Utility
Total/NA
S I uid—ge
90I —OB
MB 500-53491611 -A
Method Blank
Total/NA
Water
9010B
LCS 500-534916/2-A
Lab Control Sample
Total/NA
Water
90108,
500-179338-2 MS
Greenville Utility
Total/NA
Sludge
901 OB
500-179338-2 MSD
Greenville Utility
TotalINA
Sludge
9010E
Analysis Batch: 535016
Lab Sample ID —
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-179338-2
Greenville Utility
Total/NA
Sludge
9014
--9-34-9fig
MB 500-534916/1-A
Method Blank
Total/NA
Water
9014
534916
LCS 500-534916/2-A
Lab Control Sample
Total/NA
Water
9014
534916
500-179338-2 MS
Greenville Utility
Total/NA
Sludge
90,14
534916
500-179338-2 MSD
Greenville Utility
Total/NA
Sludge
9014
534916
Analysis Batch: 535749
Lab Sample 10 —
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500 179338-2
i3reenvilte Utility
Total/NA
Sludge
101-0A
Analysis Batch: 535938
Lab Sample ID —
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
179338-2
Greenville Utility
Total/NA
9-1UT94—
9040C
LCS 500-535938/5
Lab Control Sample
Total/NA
Water
9040C
LCSD 500-535938/6
Lab Control Sample Dup
TotalINA
Water
9040,C
500-179338-2 DU
Greenville Utility
Total/NA
Sludge
9040C
Eurofins T'estAmerica, Chicago
Page 12 of 29 3/30/2020

Surrogate Summary
Client: Bio-Nornics Services., Inc.
Project/Site: Greenville Utility Water Plant
Job ID: 500-179338-1
. . .. . .......
Method: 8260D - Volatile Organic Compounds by GC/MS
Matrix: Sludge
............. .......... -----------------Pre Type: TCLP
— ----------
Percent Surrogate Recovery (Acceptance Limits)
DCA BFB DBFM TOL
Lab Sample ID Client Sample ID (75-126) (72-124) (76-120) (75-120)
500-179338-2 Greenville Utility 104 92 97 91
Surrogate Legend
DCA = 1,2-Dichtoroethane-d4 (Surr)
BFB 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane (;Surr)
TOL = Toluene-d8 (Surr)
Method: 8260D - Volatile Organic Compounds by GC/MS
Matrix: Water
I..... -------------
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
I DCA
BFB
DBFM
TOL
Lab Sample ID Client Sample ID (75.126)
(72-124,)
(75-120)
(75-120)
LCS 500-53546114 Lab Control Sample i 101
91
96
95
MB 500-535461/6 Method Blank 103
96
95
94
Surrogate Legend
DCA = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane (Surr)
TOL = Toluene -dB (Surr)
Method: 8260D - Volatile Organic Compounds by GC/MS
Matrix: Water
Percent Surrogate Recovery (Acceptance Limits)
DCA BFB DBFM TOL
Lab Sample ID Client Sample ID (75-126) (72-124) (75-120) (75-120)
LB 500-53521611 -A Method Blank 101 93 —94 ­_ - 9-4
Surrogate Legend
DCA = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane (Surr)
TOL = Toluene-d8 (Surr)
Method: 8270E - Semivolatile Organic Compounds (GCIMS)
Matrix: Sludge
Pre
Percent Surrogate Recovery (Acceptance Limits)
TBP FBP 2FP
NEZ
PHL
TPHL
Lab Sample ID Client Sample ID
(40-145) (34-110) (27-110)
(36-120)
(20-100)
(0-145)
500-179338-2 Greenville Utility
68 80 47
70
29
96
500-179338-E-2-F MS 500-179338-E-2-F MS
80 85 51
86
35
88
Surrogate Legend
TBP = 2,4,6-Tribromophenol (Surr)
FBP = 2',Fluorobiphenyl
2FP = 2-Fluorophenol (Surr)
NBZ = Nitrobenzene-d5 (Surr)
PHL = Phenol-d5 (Surr)
TPHL = Terphenyl-04 (Surr)
TCLP
: TCLP
Eurofins TestArnerica, Chicago
c
Page 13 of 29 3/30/2020

Surrogate Summary
Client: Bio-Nornics Services., Inc.
Job ID: 500-179338-1
Project/Site: Greenville Utility Water Plant
Method: -8 -2-70 E-S e m i vo I a t- i' I e-, - 6 rg an ic Compounds (GC/MS)
Matrix: Water
- — ---- --- -------- ...... . ... . .................... -
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
TBP FBP 2FP
NBZ
PHL
TPHL
Lab Sample ID Client Sample ID
(40-145) (34-110) (27.110)
(36-120)
(20-100)
(40-145)
S 500-535134/2-A Lab —(5 o""n'trol Sample
8-5 ­79-8— 6-2
9-9
—41
9-8
MB 500-53513411-A Method Blank
71 84 63
75
33
105
Surrogate Legend
I TBP = 2,4,6-Tribromophenol (Surry '--'
FBP = 2-Fluorobiphenyl
2FP = 2-Fluorophenot (Surr)
NBZ = Nitrobenzene-d5 (Surr)
PHL = Phenol-d5 (Surr)
TPHL = Terphenyl-d 14 (Surr)
Method: 8270E - Sernivolatile Organic Compounds (GC/MS)
Matrix: Water
Prep Type: TCL,P
Percent Surrogate Recovery (Acceptance Limits)
TBP FBP 2FP NBZ PHL TPHL
Lab Sample ND Client Sample ID (40-145) (34-110) (27-110) (36-120) (20-100) (40-145)
LB 500-534637/1-E Method Blank 73 86 56 7-5 —30 --- 101
Surrogate Legend
TBP = 2,4,6-Tribrom,ophenol (Surr)
FBP = 2-Fluorobiphenyl
2FP = 2-Fluorophenol (Surr)
NBZ = Nitrobenzene-d5 (Surr)
PHL = Phenol-d5 (Surr)
TPHL = Terphenyl-d14 (Surr)
Method: 8081B - Organoch,lorine Pesticides (GC)
Matrix: Sludge Prep Type, TCLP
Percent Surrogate Recovery (Acceptance Limits)
DCBP1 TCx1
Lab Sample ID Client Sample ID (30-130) (30-120)
6-0-0-179338-2 Greenville Utility —140-g— —110
Surrogate Legend
DClBP1
TCX1
Lab Sample ID
Client Sample ID
(30-130),
(30-120)
UGS- 500-53516312-A
Lab Control Sample
103
LCS 500-535163/3-A
Lab Control Sample
99
79
MB 500-535163/1 -A
Method Blank
131 x
106
Surrogate Legend
QCBP = DCB Decachloro,biphenyl
TCX =: Tetrachloro-m-xylene
Total/NA
Eurofins TestArnerica, Chicago
Page 14 of 29 3/30/2020

Surrogate Summary
Client: Bio-Nornics Services., Inc. Job ID: 500-179338-1
Project/Site: Greenville Utility Water Plant
Method: 80816 -Organochlorine Pesticides (GC)
Matrix: Water, - Prop Type: TCLP
Percent Surrogate Recovery (Acceptance Limits)
DCBP1
TCX1
Lab Sample ID Client Sample ID (30-130)
(30-120)
500-179552-B-1-M MS1Matrix Spike 60
70
1 LB 500-53463711-F Method Blank 112
1
92
Surrogate Legend
I DCBP = DCB Decachforobiphenyl
TCX = Tetrachloro-m-xylene
Method: 8082A - Polychlorinated Biphenylls (PCBs) by Gas Chromatography -ii-i--- _­--'-""-
Matrix: Sludge
Percent Surrogate Recovery (Acceptance Limits)
TCX1 DCBP1
Lab Sample ID Client Sample ID (30-120) (30-140)
5b0-179338-2 Greenville Utility �d_ - 83
Surrogate Legend
TCX = Tetrachlor6__­m­_Xyl(;we
DCBP = DCB Decachlorobiphenyl'
Method: 8082A - Polychlorinated Biphenylls (PCBs) by Gas Chromatography
Matrix: Water
— ----------- . — P
Percent Surrogate Recovery (Acceptance Limits)
TCX1
DCBP1
Lab Sample ID
Client Sample ID
(30-120)
(30-140)
LCS 500-535414/2-A
Lab Control Sample
82
100
LCSD 500-53541413-A
Lab Control Sample Dup
59
74
MB 500-535414/1-A
Method Blank
68
95
Surrogate Legend'
X = Tetrachloro-m-_xylene­
DCBP = DCB Decachlorobiphenyt
Method: 8151A - Herbicides (GC)
Totall/NA
Total/NA
Matrix: Sludge
. . . ............ ..... . . . ....... Type: TCLP
Percent Surrogate Recovery (Acceptance Limits)
DCPAA11
Lab Sample ID Client Sample ID (25-130)
500-179338-2 Greenville Utility 67
Surrogate Legend
DCPAA = DCAA
Method: 8151A - Herbicides (GC)
Matrix: Water
DCPAA1
Lab Sample ID Client Sample ID (25-130)
LCS 500-53496012-A - LaE_Control Sample 67
MB500-534960/1-A Method Blank 70
Surrogate Legend
Prep Type. Total/NA
Percent Surrogate Recovery (Acceptance Limits)
Eurofins TestAmerica, Chicago
Page 15 of 29 3/30/2020

Surrogate Summary
Client: Bio-Nomics Services., Inc.
ProjectlSite: Greenville Utility Water Plant
DCPAA = DCAA
Method: 8-1 5-1A ---Herbicides- - (—G- - 6)
Matrix: Water
DCPAA1
Lab Sample ID Client Sample ID (25-130)
SfDtl-179563-B-1-F MS Matrix Spike 6-5
LB 500-534637/1-0 Method Blank 65
Surrogate Legend
DCPAA = DCAA
Job ID: 500-179338-1
Type. TCLP
Percent Surrogate Recovery (Acceptance Limits)
Eurofins TestArnerica, Chicago,
Page 16 of 29 3/30/2020

QC Sample Results
Client: Blo-Nomics Services., inc.
Job ID: 500-179338-1
Project/Site: Greenville Utility Water Plant
Method: 8260D - Volatile Organic Cornpounds
by GC/MS
......... ...............
Lab Sample ID: MB, 500-535461/6
Client Sample ID. Method Blank
Matrix: Water
Prep Type: TotalINA
Analysis Batch: 535461
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
11,1-Dichloroethene
ND
1,00
ug/L
03126/20 10:20
1,2-Dichl!oroethane
ND
1.00
ug/L
03/26/20 1U0
2-Butanone (MEK)
ND
5.00
ug/L
03/26/20 10:20
Benzene
ND
1.00
uq/L
03/26/20 10:20 1
Carbon tetrachloride
ND
1.00
ug/L
03/26120 10:20 1
Ch:orobenzene
ND
1,00
ug/L
03/26/20 10:20 1
Chloroform
NI)
100
ug/L
03/26/20 10:20 1
Tetrachloroethene
ND
1
uq/L
03126/20 10:20 1
Trichloroethene
ND
1,00
ug/L
03126/20 10:20 1
Vinyl chloride
ND
1.00
ug/L
03126/20 10:20 1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1-,2--Dichforoelhane-d4 (Surr)
10 . 3
75-126
-5-3-1-2612010:20
4-Bromofluorobenzene (Surr)
96
72-124
03126120 10' -20 1
Dibromofluoromethane (Surr)
95
75-120
03/2820 10' -20 1
Toluene-d8 (Surr)
94
75-120
03126120 10:20 1
Lab Sample ID: LCS 500-535461/4
Client Sample ID-
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 535461
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
1—J-Dichl6roethene
50.0
41.89
ug/L
84
67-122
1,2-Dichloroethane
50.0
46.94
ug/L
94
68-127
2-Butanone (MEK)
50,0
47.50
ug/L
95
46-144
Benzene
50,10
44.22
ug/L
88
70-120
Carbon tetrachloride
50.0
48.11
uq/L
96
59-133
Chlorobenzene
Wo
44,02
ug/L
88
70-120
Chloroform
Wo
43.17
ug/L
8,6
70-120
Tetrachloroethene
50.0
48.77
ugIL
98
70-128
Trichloroethene
50.0
46,28
ug,/L
93
70-125
Vinyl chloride
50.0
40,62
ug/L
81
64-126
LCS LCS
Surrogate %Recovery Qualifier
Limits
1,2-Dichloroethane-d4 (Surr) 101 —
—7 - i25
4-Bromofluorobenzene (Surr)
91
72-124
Dibromofluoromethane (Surr)
96
75-120
Toluene -dB (Surr)
95
75-120
Lab Sample ID: LB 500-535216/1 -A
Client Sample
ID: Method Blank
Matrix: Water
Prep Type: TCLP
Analysis Batch: 535461
LB LB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
i""I-Dichloroethene
ND
20.0
ug/L
0312612010:47 20
1,2-Dichloroelhane
ND
20.0
ug/L
03126120 10:47 20
2-Butanone (MEK)
ND
100
ug/L
03/26/20 10:47 20
Benzene
ND
20.0
ug/L
03/26/20 10:47 20
Eurofins TestArnerica, Chicago
Page 17 of 29 3/30/2020

QC Sample Results
Client: Bio-Nomics Services., Inc. Job ID: 500-179338-1
Project/Site: Greenville Utility Water Plant
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
......... . -- - - ------- --- --------- —
Lab Sample ID: LB 500-535216/1-A
Client Sample ID: Method Blank
Matrix: Water Prep Type: TCLP
Analysis Batch: 535461
LB LB
Analyte
Result Qualifier
R L
MDL
Unit
D Prepared
Analyzed
Dil Fac
Carbon tetrachloride
—Nlj
—20.0
—UP
03/26/2-0 10:47
20
Chlorobenizene
ND
20.0
ug/L
03/26120 10:47
20
Chloroform
ND
40.0
ug/L
03126/20 10:47
20
Tetrachloroethene
ND
20.0
ug/L
03/26/20 10:47
20
Trichloroethene
ND
20,0
ug/L
03/26/20 10:47
20
Vinyl chloride
No
20.0
ugIL
03126/20 10:47
20
LB LB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
D11 Fac
1—,2-DiE-Roroethane-d4 —(Surr)
101
75-126
03-12-612010:47
20
4-Bromofluorobenzene (Surr)
93
72-124
03126120 10:47
20
Dibrornofluoromethane (Surr)
94
75-120
03126120 10:47
20
Toluene-0 (Surf)
94
75-120
03126120 10:47
20
Method: 8270E - Semivolat�ile Organic Compounds (GC/MS)
Lab Sample ID: MB 500-53513411-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 535155
Prep Batch: 535134
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
-1-,4--Dichlorob6nzene
ND
2,00
ug/L
03/24/20 08:12
03124/20 16:22
1
2,4,5-Trichlorophenol
ND
10.0
ug/L
03124120 08:12
03124/20 16:22
1
2,4,6-Trichlorophenot
ND
5.00
ug/L
03124/20 08:12
03/24/20 16:22
1
2,4-Dinitrotoluene
ND
1.00
ug/L
03124/20 08:12
03/24/20 16:22
1
HexaGhlorobenzene
ND
0,500
ug/L
03/24/20 08:12
03/24/20 16:22
1
Hexachlorobutadlienie
ND
5.00
ug/L
03124120 08:12'
03/24/20 16:22
1
Hexachloroethane
ND
5.00
ug[L
03/24120 0812
03124120 16:22
1
Cresols
ND
2.00
ug/L
03124/20 08:12
03/24/20 1622
1
Nitrobenzene
ND
1.00
ug/L
03/24120 08:12
03124/20 16:22
1
Pentachlorophenol!
ND
20.0
ug/L
03/24/20 08:12
03124120 16:22
1
Pyridine
ND
20,0
ug/L
03/24/20 08:12
03/24120 16:22
1
MB MB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2,4,6-Tribromophenol (Surr)
—Ti —
40-145
031-24120"d-8-42
03124-12016.22
I
2-Fluorobiphenyl
84
34-110
03124120 08:12
03124120 16:22
1
2-Fluorophenol (Surr)
63
27-110
03124120 08:12
03124120 16:22
1
Nitrobenzene-d5 (Surr)
75
36-120
03124120 06:1'2
03124120 16:22
1
Phenol-d5 (Surf)
33
20-100
03124120 08:12
03124120 16:22
1
Terphenyl-04 (Surr)
105
40-145
03124120 0812
03124120 16.,22
1
Lab Sample ID: LCS 500-53513412-A
Client Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA,
Analysis Batch: 535155
Prep Batch: 535134
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
14-Dichiorobenzene
40.0
32.05
ug/L
80
23-110
2,4,5-Trichlorophenol
40.0
37.70
ug/L
94
63-124
2,4,6-Trichlorophenol
40.0
37,20
ug/L
93
62-121
Eurofins TestAmerica, Chicago
Page 18 of 29 3/30/2020

QC Sample Results
Client: Bio-,Nomic,s Services., Inc. Job ID: 500-179338-1
Project/Site: Greenville Utility Water Plant
Method': 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
.1 . .. -.-- .... ... - --- -- ---- - ---- - --------- --- ----- - - ---- 11 .... ...... - -------- ---- ---- ...... .... ... -------------
Lab Sample ID: LCS 500-53513412-A
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 535155
Prep Batch: 535134
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
24--Dinitroto1u6n'—e
740—,0
—35.45 —
—ug/L
—89
—63.129
Hexachilorobenzene
40.0
41,44
ug/L
104
61-126
Hexachlorobutadiene
40.0
26,18
ug/L
65
20-100
Hexachloroethane
40.0
27.07
ug/L
-68
20-100
Cresols
80.0
64.74
ug/L
81
Nitrobenzene
40.0
38,46
ug/L
96
54-121
Pentachlorophenol
80.0
74.30
ug/L
93
42-148
Pyridine
80,0
39.42
ug/L
49
15-110
Surrogate
LCS LCS
%Recovery Qualifier
2,4—,6--TnbromophinW(—Surr)
—85- —
2-Fluorabiphenyl
98
2-Fluorophenot (Surr)
62
Nitrobenzene-d5 (Surr)
99
PhenoW5 (Surr)
41
TerphenyW14 (Surr)
98
Lab Sample ID: LB 50 0-53463711 -E
Matrix. Water
Analysis Batch: 535155
Analyte
LB LB
Result Qualifier
1,4-Dichloroben,zene
NO
2,4,5-Trlchlorophenol
NO
2,4,6-Trichlorophenol
NO
2,4-Dinitrotoluene
NO
l-lexachlorobenzene
NO
Hexachlorobutadiene
ND
Hexachloroethane
NO
Cresol's
NO
Nitrobenzene
NO
PentachJorophenol
ND
Pyridine
ND
Limits
40- 45
34-110
27-110
36-120
20-100
40-145
Client Sample ID: Method Blank
Prep Type: T'CLP
Prep Batch: 535134
RL
MDL Unit
D Prepared
Analyzed
Oil Fac
20.0
ug/L
03/24/20 08:12
03124120 15:22
1
100
ug/L
03/24/20 08:12
03124/20 15:22
1
50,0
ug/L
03124/20 08:12
03/24120 15:22
1
10.0
ug/L
03124/20 08:12
03124/20 15:22
1
5,00
uglL
03124/20 08:12
03/24120 15:22
1
50.0
ug/L
03/24120 08A2
03/24/20 15:22
1
50.0
ug/L
03/24120 08:1!2
03124/20 15:22
1
20,0
ug/L
03124/20 08:12
03/24/20 15,22
1
10.0
ug/L
03/24/20 08:12
03/24/20 15:22
1
200
ug/L
03/24/20 08:12
03124120 15:22
1
200
ug/L
03/24/20 0612
03/24/20 15:22
1
LS LB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
2,4,6- bromaphenol (Surr)
73 —
40-145
03-124120 08:12
63124-120 7'K,2-2 1
2-Fluorobiphenyl
66
34-110
03124120 08:12
03124120 15:22 1
2-Fluorophenof (Surr)
56
27-110
03124120 08:12
03124120 15:22 1
Nitrobenzene-d5 (Sort)
75
36-120
03124120 08:12
03124120 15:22 1
Phenol-d5 (Surr)
30
20-100,
03124120 08:12
03124120 15:22 1
Terphenyl-04 (Surr)
101
40-145
03124120 08:12
03124120 15:22 1
Lab Sample ID: 500-179338-E-2-F MS
Client Sample ID: 500-179338-E-2-F MS
Matrix: Sludge
Prep Type: TCLP
Analysis Batch, 535155
Prep Batch: 535134
Analyte
Sample Sample
Spike
Ms IVIS
%Rec.
Result Qualifier
Added
Result Qualifier Unit D %Rec
Limits
1,4-Dichlorobenzene
ND
—400. --274,5
— 6g-/L 69
23-110
Eurofins TestAmerica, Chicago
Page '19 of 29 3/30/2020

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville Utility Water Plant
Method: 8270E - Semivo...l. a.. t...i..le Organic Comp-o--u r nd -s GCIMS)-- Continued
o' ntinued
------ (.)
Job ID: 500-179338-1
Lab Sample ID: 500�-17'9338-E-2-F MS
Client Sample ID,: 500-179338-E-2-F MS
Matrix: Sludge
Prep Type: TCLP
Analysis Batch: 535155
Prep Batch: 535134
Sample Sample
Spike
MS MS
%Rec.
Analyte
Result Qualifier
Added
Result Qualifier
unit
D %Rec
Limits
2,4,5-Trichlorophenol
NO
400 -
—342,9
—ug/L
86
—
63-124
2,4,6-Trichlorophenol
NO
400
338.0
ug/L
85
62-121
2,4-Dinitrotoluene
NO
400
318.3
ug/L
80
63-129
Hexachlorobenzene
NO
400
356,6
ugIL
89
61-126
Hexachilorobutadiene
NO
400
238.8
ugIL
60
20- 1!00
Hexachloroethane
NO
400
23&2
ug/L
59
2!0 - 100
Cresols
NO
800
572A
ug/L
72
Nitrobenzene
NO
400
330.0
ug/L
83
54-121
Pentachlorophenol
NO
8010
639,1
ug/L
80
42-148
Pyridine
NO
800
341.2
ug/L
43
15-110
MS MS
Surrogate
%Recovery Qualifier
Limits
2,-4—,6-Tribromophenoi (,§trr—r)—
—86 —
4-0 - T4 —5
2-Fluorobiphenyl
85
34-110
2-Fluorophanol (Surr)
51
27-110
Nitrobenzene-dS (Surr)
66
36-120
Phenol-c(5 (Surr)
35
20-100
Terphenyl-dM (Surr)
88
40-145
Method: 8081B - OrganoChlorine Pesticides (GC)
Lab Sample ID: MB 500-535163/1-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 535231
Prep Batch: 535163
M8 MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Oil Fac
Chlordane (technical)
NO
0,100
ug/L
03124/20 09:29
03/24/20 20:!09 1
Endrin
NO
0.0500
ug/L
03124/20 09:29
03124/20 20:09 1
Heptachlor
NO
0.0400
ug/L
03/24/20 0929
03/24/20 20,09 1
Heptachlor epoxide
NO
0.0400
ugIL
03/24120 09:29
03124/20 20:09 1
gamma-BHC (Lindane)
NO
0,0500
uq/L
03/24120 09:29
03124120 20:09 1
Methoxychlor
NO
0,100
ug/1-
03/24/20 0929
03/24/20 20:09 1
Toxaphene
NO
0.500
ug/L
03/24120 09:29
03124120 20:09 1
ma MB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
DC6 Decachlorobipheny--1
—131 X
30-130
-63124120 0-9 29
63-12412-0 20--d§ 1
Tetrachloro-rn-xylene
106
30-120
03124120 09:29
03124120 20:09 1
Lab Sample ID. LCS 500.535163/2-A
Client
Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 535231
Prep Batch: 535163
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Endrin
—
0.0996
0.1150
ug/L
115
60-132
Heptachlor
0.0999
0.1024
ug/L
102
40-120,
Heptachlor epoxide
0.100
0,1107
ug/L
Ill
64-120
gamma-BHC (Undane)
0,0999 0.09340
ug/L
93
68-120
Methoxychlor
IM
1.086
ugIL
109
63-135
Eurofins TestAmerica, Chicago
Page 20 of 29 3/30/2020

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville Utility Water Plant
Method: 8081 B - Organochlorine Pesticides
Lab Sample ID: LCS 500-53516312-A
Matrix: Water
Analysis Batch: 535231
LCS LCS
Surrogate %Recovery Qualifier
DCB Decachlorobiphenyl 125
Tetrachloro-rn-xylene 103
Lab Sample ID: LCS 500-535163/3-A
Matrix: Water -
Analysis Batch: 535231
Analyte
Toxaphene
LCS LCS
Surrogate %Recovery Qualifier
DCB Decachlorobiphenyl 99
Tetrachloro-m-xylone 79
Lab Sample ID: LB 500-534637/1-F
Matrix: Water
Analysis Batch: 535231
Limits
30-130
30-120
Job ID: 500-179338-1
Continued)
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 535163
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 535163
Spike LCS LCS %Rec,
Added Result Qualifier Unit D %Roe Limits
100 8.363 50-150
Limits
30-130
30-120
Analyte
LB L13:
Result Qualifier
RL
15-10rdanj (techffical)
NO
-10,0
Endrin
NO
5,00
Heptachlor
NO
4,00
Heptachlor epoxide
NO
4,00
gamma-BHC (Lindane)
NO
5.00
Methoxychlor
NO,
10.0
Toxaphene
NO
50,0
LB LB
Surrogate
%Recovery Qualifier
Limits
DCB Decachlorobiphenyl
112
30-130
Tefrachloro-m-xyfene
92
30-120
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch: 535163
MDL Unit
D Prepared
Analyzed
Oil Fac
ug/L
03/24120 09:29
03/24120 2 1! 11
1
ug/L
03/24120 09:29
03/24120 2 1: 11
1
ug/L
03/24/20 09:29
03124120 21:11
1
ug/L
03124/20 09:29
03/24/20 21:11
1
ug/L
03124/20,09:29
03/24/20 21:11
1
ug/L
03124/20 09:29
03124120 21:11
1
ug/L
03/24120 09:29
03/24120 211:11
1
Prepared
Analyzed
Oil Fac
03124)20 09:29
03124120 21:11
1
03124120 09:29
03/24/20 21:11
1
Method: 8082A - Polychlorinated Biphenylls (PCBs) by Gas Chromatography
Lab Sample ID: MB 500-535414/1-A Client Sample 11); Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 535496 Prep Batch: 535414
MB MB
Analyte
Result Qualifier
RL
PCB-1016
NO
0.500
I PCB-1221
NO
0.500
PCB-1232
NO
0,500
PCB-1242
NO
0.500
PCB-1248
NO
0.500
PCB-1254
NO
OMO
PCB-1260
NO
0.500
MB MB
Surrogate
%Recovery Qualifier
Limits
Tetrachloro-m-xylene
68
30-120
MDL Unit
D Prepared
Analyzed
Oil Fac
ug/L
03/25120 18:08
03/26/20 08:44
1
uq/L
03125/20 18:08
03/26/20 08A4
1
ug/L
03125/20 18:08
03126120 08A4
1
ug/L
03/25120 18:08
03126120 08A4
1
ug/L
03125/20 16:08
03/26120 08A4
1
ug/L
03/25/20 18:08
03/26120 08:44
1
ug/L
03125/20 18:08
03/26120 08A4
1
Prepared
Analyzed
Oil Fac
6-3 �512 0 1 8, U8
03/26/20 -0 8 �4 4
1
Eurofins TestAmerica, Chicago
Page 21 of 29
3/30/2020

QC Sample Results
Client. Bio-Nomics Services., Inc.
Project/Site: Greenville Utility Water Plant
Job ID: 500-179338-1
.. . ........ -.-- I .-- I I
Method: 8082A - Polychlorinated Biphenvis (PCBs) by Gas Chromatography (Continued)
---------- -- - - ---- - ---- . . ... ................ ... .. .......... ---- - ---
Lab Sample ID: MB 500-53541411-A Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 535496 Prep Batch: 535414
MB MS
Surrogate %Recovery Qualifier Limits
DC8 Decachlorobiphenyl 95 30-140
Lab Sample ID: LCS 500-535414/2-A
Matrix: Water
Analysis Batch: 535496
Analyte
B-1016
PCB-1260
LCS LCS
Surrogate %Racovety Qualifier
Tetrachloro-m-.
—xyl�ne . .. 8.. 2
DCB Decachlorobiphenyl 100
Lab Sample ID. LCSD 500.53541413-A
1 Matrix: Water
Analysis Batch: 535496
Analyte
PCB-11016
PCB-1260
Spike LCS LCS
Added Result Qualifier
5.00 4.485
5.00 4.585
Limits
30-120
30-140
Prepared Analyzed Dil Fac
E3-125120 18 08 03+2F6-12008-44 —1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 535414
%Rec.
Unit D %Rec Limits
u-9—/L — — 9-0 56 - 120
ug/L 92 53-137
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 535414
Spike
LCSD LCSD
%Rec. RPD
Added
Result Qualifier Unit
0 %Rec Limits RPD Limit
5.00
3.488 u-g—/L
—70 --5�6---120 —'-fg —20
5,00
3.519 *1 ug/L
70 53-137 26 20
LCSD LCS'D
Surrogate %Reco,very Qualifier Limits
Te1rWch10rO-M-XY1ene 59 30-120
DC6 Decachlorobiphenyl 74 30-140
Method: 8151A - Herbicides
Lab Sample ID: MB 500-53496011-A
j Matrix: Water
, Analysis Batch: 53512�9
, Analyte
Silvex (2,4,5-TP)
MB MB
Result Qualifier RL
ND 0.00100
ND 0.00100
MB MB
Surrogate %Recovery Qualifier Limits
DCAA 70 —]25 - 1-30
Lab Sample ID: LCS 500-534960/2-A
Matrix: Water
Analysis Batch: 535129
Analyte
2,4-D
Silvex (2,4,5-TP)
MDL Unit
mg/L
rng/L
Spike LCS LCS
Added Result Qualifier
0 6TdT ---6.-0-07576
0.00250 0M1740
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 534960
D Prepared Analyzed Dil Fac
03/23120 09:51 03124120 08:58 1
03/23/20 09:51 03/24/20 08:58 1
Prepared Analyzed Dil Fac
03123120 09:5-1 ON �412O 08 �58 1
Client Sample ID: Lab Control Sample
Prep Type: TotalINA
Prep Batch. 534960
%Rec.
Unit D %Roe Limits
rnjj/--L 75 3-0 - i"i-5—
mg/L 70 32-115
Eurofins TestArnerica, Chicago,
Page 22 of 29 3/30/2020

QC Sample Results
Client: Rio-Nomics Services., Inc,
Project/Site: Greenville Utility Water Plant
. . ........
Method: 8151 A - Herbicides (GC)
tinu
Lab Sample ID: LCS 500-534960/2-A
Matrix: Water
Analysis Batch: 535129
LCS LCS
Surrogate %Recovety Qualifier Limits
DCAA 67 25-130
Lab Sample ID: LB 500-53463711-D
Matrix: Water
Analysis Batch: 535129
LB LB
Analyte Result Qualifier RL
�,4-D N .. D 0.100
Silvex (2,4,5-TP) ND 0,100
LB LB
Surrogate %Recovery Qualifier Limits
DCAA 65 25-130
Method: 6,010D Metals
-... - ....... ... .
Lab Sample ID: LCS 500-534857/2-A
Matrix: Water
Analysis Batch: 535002
Analyte
A-rienic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Job ID: 500-179338-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 534960
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch: 534960
MDL Unit D Prepared Analyzed Dil Fac
mg/L 03123120 09:51 03124120 10:16 1
mg/L 03123/20 09:51 03/24/20 10:16 1
Prepared Analyzed Dil Fac
03/23/20 09:51 03-124-12010-16 I
Spike
LCS LCS
Added
Result Qualifier
DOO
0.1138
0.500
0.4986 J
0.0500
0.05382
0.200
0,1921
0.100
0.09605
0.100
0.1053
0.0500
0.05532
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 534857
%Rec.
Unit D %Rec Limits
M9-1--
--11-4
80-120
mg/L
100
80-120
mg/L
108
80-120
mg1L
96
80.120
mg/L
96
80-120
mg/L
105
80-120
mg/L
111
80.120
Lab Sample ID: LB 500-534637/1-B
Client Sample ID: Method Blank
Matrix: Water
Prep Type: TCLP
Analysis Batch: 535002
Prep Batch: 534857
LB LB
Analyte
Result Qualifier
RL
MOL Unit
D Prepared
Analyzed Dil Fac
Arsenic
ND
0.0500
mg/L
03/22120 16:15
03/23120 08:53 1
Barium
ND
0.500
mg/L
03122/20 16:15
03/23/20 08:53 1
Cadmium
ND
0.00500
mg/L
03/22120 16:15
03/23120 08;53 1
Chromium
ND
0,0250
migiL
03122/20 16:15
03/23/2D 08:53 1
Lead
ND
0.0500
mg/L
03/22/20 16:15
03123/20 08:53 1
Selenium
ND
0.0500
mq1L
03/22/20 16:15
03/23120 013:53 1
Silver
ND
0.0250
mg/L
D3122120 16:15
03/23/20 08:53 1
Method, 7470A - Mercury (CVAA)
Lab Sample ID: MB 500-534911/12-A Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 53,4991 Prep Batch: 534911
MB me
Analyte Result Qualifier RL MOL Unit D Prepared Analyzed Dil Fac
Mercury ND 0.200 ug/L 03/23/20 07:50 03/23/20 11:27
Eurofins TestArnerica, Chicago
Page 23 of 29 3/30/2020

QC Sample Results
Client: Bic-Nomics Services., Inc.
ProjectlSite: Greenville Utility Water Plant
Method: 7470A - Mercury (CV
Lab Sample ID: LCS 500-534911/14-A
Matrix: Water
Analysis Batch: 534991
Analyte
WeTEdry
Lab Sample ID: LIB 500-53463711-C
Matrix: Water
Analysis Batch: 534991
Job ID: 500-179338-1
Continued
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 534911
Spike LCS LCS %Rec.
Addled Result Qualifier Unit D %Rec Limits
2.00 1,799 -90 _86__"1'2 . 0
L6 LB
Analyte Result Qualifier RL
Mercury NO 0.200
Method: 9014 - Cyanide
Lab Sample ID: MB 500-534916/1 -A
Matrix: Water
Analysis Batch: 535016
M13 MB
Analyte Result Qualifier RL
Cyanide, Total NO 0.01010
Lab Sample ID: LCS 500-53491612-A
Matrix: Water
Analysis Batch: 535016
Spike
Analyte Added
Cyanide, Total 0.100
Lab Sample ID: 500-179338-2 MS
Matrix: Sludge
Analysis Batch: 535016
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch: 534911
MDL Unit D Prepared Analyzed Oil Fac
ug/L 03/23/20 07:50 03/23120 11 A0 1
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 534916
MDL Unit 0 Prepared Analyzed Oil Fac
mg/L 03/23120 09:00 03/23/20 13:12 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 534916
LCS LCS %Rec.
Result Qualifier Unit D %Rec Limits
OA053 mg/L 105 85-115
Sample Sample Spike IVIS MS
Analyte Result Qualifier Added Result Qualifier Unit
Cyanide, Total ND 0.0400 0.03740 rl
Client Sample ID: Greenville Utility
Prep Type: Total/NA
Prep Batch: 534916
%Rec.
D %Rec Limits
94 75-125
Lab Sample ID; 500-179338-2 MSD Client Sample ID: Greenville Utility
Matrix: Sludge Prep Type., T'otal/NA
Analysis Batch: 53,5016 Prep Batch: 534916
Sample Sample Spike MSD MSD %Rec. RPD
Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit
Cyanide, Total . . . ....... _ lq_D 0-0400 0,0381 iii_g/L -95 ---- 1-5-125 __-__20
Method: 90-3-4 - -Sulfide, -Acid soluble and Insoluble (Titrimetric)
Lab Sample ID: MB, 500-534269/1 Client Sample ID: Method Blank
Matrix: Water Prep Type., Total/NA
Analysis Batch,: 534269
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fac
Sulfide NO 1.00 mg1L 03/17/20 11 : 19 1
Eurofins TestAmerica, Chicago
Page 24 of 29 3/30/2020

QC Sample Results
Client: Bio-Nomics Services., Inc. Job ID: 500-179338-1
Project/Site: Greenville Utility Water Plant
Method : 9034 - Sulfide, Acid soluble and Insoluble (Titrimetric) (Continued)
------- . .............. ... .... . ... . .....
.......... . ..
Lab Sample ID: LCS 500-53426912 Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 534269
Analyte
Sulfide
Method: 9 0-40"b" - pH'
Lab Sample ID: 500-179338-2 DU
Matrix: Sludge
Analysis Batch: 535938
Analyte
I pH
Sample Sample
Result Qualifier
5.56 H F
Spike LCS LCS %Rec.
Added Result Qualifier, Unit D %Rec Limits
395 362-3 ing/L— — —97 —80-120
Client Sample ID. Greenville Utility
Prep Type: Total/NA
DU DU RPD
Result Qualifier Unit D RPD Limit
5.550 SU 0,2
Eurofins TestAmerica, Chicago
Page 25 of 29
3/30/2020

Lab Chronicle
Client: Bic,-Nomics Services., Inc,
Project/Site: Greenville Utility
Water Plant
Client Sample
ID: Greenville Utility
Date Collected: 03/12/20 00:00
Date Received:
03114120 12:10
Batch
Batch
Prep Type
Type
Method Run
TCLP
Leach
131—I
TCLP
Analysis
8260D
TCLP
Leach
1311
TCLP
Prep
3510C
TCLP
Analysis
8270E
TCLP
Leach
1311
TCLP
Prep
3510C
TCLP
Analysis
80816
Total/NA
Prep
3510C
TotalINA
Analysis
8082A
TCLP
Leach
1311
TCLP
Prep
81511A
TCLP
Analysis
8151A
TCLP
Leach
1311
TCLP
Prep
301 OA
TCLP
Analysis
6010D
TCLP
Leach
1311
TCLP
Prep
7470A
TCLP
Analysis
7470A
TotaUNA
Analysis
1010A
Total/NA
Prep
9010B
Total/NA
Analysis
9014
Total/NA
Analysis
9034
Total/NA
Analysis
9040C
Job ID: 500-179338-1
Lab Sample ID: 500-1'79338-2
Matrix: Sludge
Dilution
Factor
Batch
Number
Prepared
or Analyzed
Analyst
Lab
535216
03124/20 12:23
BEG
TAL CHI
20
535461
03/26/20 17:09
PIVIF
TAL CHI
534637
03/19/20 12:22
BEC
TAL CHI
535134
03124120 08:12
DAK
TAL CHI
1
535155
03/24/20 17:21
AJD
TAIL CHI
534637
03119/20 12:22
BEG
TAL CHI
535163
03/24/20 09:29
DAK
TAL CHI
1
535231
03/24120 21 :31
PJ1
TAL CHI
535414
03/25/20 18:08
CIVC
TAL CHI
1
535496
03/26120 09:31
BJH
TAIL CHI
5,34637
03/19/20 12:22
SEC
TAL CHI
534960
03123/20 09:51
DAK
TAL CHI
1
535129
03/24/20 13:10
JBJ
TAIL CHI
534637
03119120 12:22
BEG
TAL CHI
534857
03122120 1615
BDE
TAL CHI
1
535002
03/23120 09:26
JEF
TAL CHI
534637
03/19120 1212
BEG
TAL CHI
534911
03/23120 07:50
MJG
TAIL CHI
1
534991
03/23120 12:04
MJG
TAL CHI
1
535749
INS
TAIL CHI
(Start)
03127120 08:27
(End)
03127/20 09:19
534916
03/23/20 09:00
MS
TAIL CHI
1
535016
03/23/20 1113
IVIS
TAL CHI
1
534269
CLS
TAL CHI
(Start)
03117120 12::37
(End)
03/17120 12:41
1
535938
JJB
TAIL CHI
(Start)
03/30/20 10:22
(End)
03130/20 10:25
Laboratory References•.
TAL CHI = Eurofins TestArnerica, Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534,5200
Eurofins TestArnerica, Chicago
Page 26 of 29
3/30/2020

Client: Bio-Nornics Services., Inc. Accreditation/Certification Summary Job ID: 500-179338-1
Project/Site: Greenville Utility Water Plant
Laboratory: Eurofins TestAmeri:ca, Chicago
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below,
............ . ...... ........ ....---
Authority Program Identification Number Expiration Date
North Carolina (WWI�W—) e 291 12-31-20
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer Certification.
Analysis Method
Prep Method
Matrix
Analyte
8270E
3510C
Sludge
2,4-Dinitrot—oluene
8270E
3510C
Sludge
Cresols
8270E
3510C
Sludge,
Pyridine
9040C
Sludge
pH
South Carolina
State
77001003 04-30-20
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer Certification,
Analysis Method
Prep Method'
Matrix
Analyte
B2600
Sludge ---
—1,1-Dichloroethene
8260D
Sludge
1.2-Dichloroethane
8260D
Sludge
2-Butanone (MEK)
8260D
Sludge
Benzene
8260D
Sludge
Carbon tetrachloride
8260D
Sludge
Chloroben:zene
8260D
Sludge
Chloroform
8260D
Sludge
Tetrach:loroethene
8260D
Sludge
Trichloroethene
82601)
Sludge
Vinyl chloride
8270E
3510C
Sludge
1,4-Dichlorobenzene
8270E
3510C
Sludge
2,4,5-Trichlorophenol
8270E
3510C
Sludge
2.4,6-Trichlorophenol
8270E
3510C
Sludge
2,4-Dinitrotoluene
8270E
3510C
Sludge
Cresols
8270E
3510C
Sludge
Hexachilorobenzene
6270E
3510C
Sludge
Hexachlorobutadiene
8270E
3510C
Sludge
Hexachloroethane
8270E
3510C
Sludge
Nitrobenzene
8270E
3510C
Sludge
Pentachlorophenol
8270E
3510C
Sludge
Pyridine
9034
Sludge
Sulfide
Eurofi'ns TestArnerica, Chicago
Page 27 of 29 3/3012020

w
I
rl milm
cl.
CM
cm
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Client: Bio-Nomics Services., Inc.
Login Number: 179338
List Number: 1
Creator: Buckley, Paula IMI
Question
Login Sample Receipt Checklist
Job Number: 500-,179338-1
List Source: Eurofins TestAmerica, Chicago
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
True
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with,.
Samples were received on ice.
True
Cooler Temperature is acceptable,
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information,
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC,
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled,
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
N/A
<6mm (1/4"').
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
1.8
Eurofins TestAmerica, Chicago
Page 29 of 29 3/30/2020

BIG-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: September 11, 2020
Greenville Utility Commision #4 Permit No. WQ0039053
16.30 %Solids
6.2 PH
Parameter
%
Mg/Kg Dry Weigh
(% x 110,000)
Pounds/Dry Ton
(Mg/Kg x O.00D
Nitrogen (TKN)
1.320
13,200.000
26.400
Phosphorus
0.326
3,260.000
6.520
Potassium
0.055
549.000
1.098
PAN (injected)*
0.292
2,92L700
5.843
PAN (surface)*
0.277
2,768.200
5.536
Ammonia Nitrogen
0,031
30T000
0.614
Calcium
0.187
1,870.000
3.740
Calcium Carbonate F9,
5200
52,000.000
104.000
Magnesium
0,065
650.00,0
1.300
Sodium
0.027
267.000
0,534
Sulfur
-
5,440.000
10,880
Nitrate N / Nitrite N
36.100
0V2
Barium
---
SAR
0.55
Chloride
---
---
---
Iron
---
32,800.00
65-600
Ceiling Concen.
Aluminum
152,000.00
304.000
(Mg/Kg)
Arsenic
---
16.10
0.032
75
Cadmium
---
0.,613
0.001
85
Chromium
50.100
0.100
---
Copper
---
319.00
0.638
4,300
Lead
---
23.10
0.046
840
Mercury
03130
0.001
57
Molybdenum
1.53
0.003
75
Nickel
13.60
0.027
420
Selenium
4.93
0.010
100
Zme
'
---
58.80
0.118
7,500
Waypoint Analytical 20-258-0003
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or< detection limits are listed as detection limits
for calculation purposes.
willcox&mabe
Prepared By: S O I L SOLUTIONS

0 (0
Waypoint
Art.&
9/22/2020
Bio-Nomic Servics Inc
Joel Coert
530 Wood'lawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 20-,258-0003
Project Description: GUC
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received'sample(s) on 9/14/2020 for the analyses presented in the following
report.
The above referenced project has been, analyzed per your instructions. The analyses were performed In
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-,NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved' oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance,
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
AA.
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page-1 of 6

Wayp nt(D
APYTICAL
Report Number: 20-258-0003
Client Project Description: GLIC
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
73629
GUC No 2
Solids
09/11/2020 11:22
09/14/2020
73629
GUC No 2
Solids
09/11/2020 11:22
09/14/2020
SM-2540G
WP MTN
73629
GUC No 2
Solids
09/11/2020 11:22
09/14/2020
SW-7471B
WP MTN
73629
GU'C No 2
Solids
09/11/2020 11:22
09/14/2020
SM-4500-NH3C-TKN
WP MTN
73629
GUC No 2
Solids
09/11/2020 11:22
09/14/2020
4500NO3F-2011
WP MTN
73629
GUC No 2
Solids
09/11/2020 11:22
09/14/2020
6010D
WP MTN
73629
GUC No 2
Solids
09/11/2020 11;22
09/14/2020
SM-4500-11113C
WP MTN
73629
GUC No 2
Solids
09/11/2020 11:22
0,9/14/2020
9045D
WP MTN
73629
GUC No2
Solids
09/11/2020 11:22
09/14/2020
AOAC 955.01
WP MTN
W'P MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 6

0
Waypo.
int
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 * Fax [phone]
ANALYTICAL
www.waypoiiltanalytical,com
45671
Blo-Nomic Servics Inc
Project
GUC
Joel Coert
Report Date 09/22/2020
530 Woodlawn St
Information
Received 09/14/2020
Belmont , NC 28012
kD WY
Report Number : 20-258-0003
REPORT OFANAL, YSIS Pa:uric Mc Groary Ph.D., CPA
Agronomist
Lab No 73629
Matrix: Solids
Sample ID: GUC No 2
Sampled: 9/11/2020 11:22
Test
Results
Units
MOL DF Date / Time By Analytical
Analyzed Method
Moisture
83.7
%
0.010 1 09/17/20 16:56 FMM SM-254OG
Calcium Carbonate Equivalent
5.2
% - dry
0.1 1 09/17/20 13,10 DXT AOAC 955.01
Test
Results
Units
MOL DF Date I Time By Analytical
Analyzed Method
Ammonia Nitrogen
307
mg/Kg - dry
153
1
09/20/20 13:30
JPJ
SM-4500-NH3C
Nitrate+ Nitrite-N
36.1
mg/Kg - dry
29.6
1
09/16/20 13:5�7
ZBD
4500NO3F-2011
Organic N
12900
mg/Kg - dry
1530
1
09/20/20 13:00
CALCULATION
pH
6.2
S.U.
1
09/16/20 15:50
ADM
9045D
Total Solids
16.3
%
0.010
1
09/17/20 16:56
FMM
SM-254OG
Total Volatile Solids
42.7
%
0.010
1
09/17/20 16:56
FMM
SM-2540G
Total Kjeldahl Nitrogen
13200
mg/Kg - dry
1530
1
09/20/20 13:00
JPJ ;M-4500-NH3C-TKr
Phosphorus
3260
mg/Kg - dry
30.7
1
09/18/20 03:09
]ADS
601013
Aluminum
152000
mg/Kg - dry
307
10
09/18/20 18:04
]ADS
6010D
Arsenic
16.1
mg/Kg - dry
3.07
1
09/18/20 03:09
JADS
6010D
Calcium
1870
mg/Kg - dry
307
1
09/18/20 03:09
JADS
6010D
Cadmium,
<0.613
mg/Kg - dry
0.613
1
09/18/20 03:09
JADS
6010D
Chromium
50.1
mg/Kg - dry
1.53
1
09/18/20 03:09
)ADS
6010D
Copper
319
mg/Kg - dry
3.07
1
09/18/20 03:09
]ADS
6010D
Iron
32800
mg/Kg - dry
61.3
1
09/18/20 03:09
]ADS
6010D
Lead
23.1
mg/Kg - dry
1.84
1
09/18/20 03.09
]ADS
6010D
Qualifiers/ DF
Dilution Factor
L
Urnit Exceeded
Definitions MQL
Method Quantitation Limit
Page 3 of 6

0
Waypoi,nt,
7621 Whitepine Road, Richmond,
VA 23237
Main 804-743-9401
O'Fax
804-271-6446
ANALYTICAL
www,waypointanalytical.com
45671
Bio-Nomic Servics Inc
Project
GUC
Joel Coert
Report
Date 09/22/2020
530, Woodlawn St
Information
Received 09/14/2020
Belmont, NC 28017
Report Number: 20-,258-0003
REPOR7'OFA'NAL YSIS
Pauric Vic Groary Ph.D., CPA
Agronomist
Lab No 73629
Matrix: Solids
Sample1D : GUC No 2
Sampled: 9/11/2020 11.2,2
Test
Results
Units
MOL
DF
Date I Time By
Analytical
Analyzed
Method
Magnesium
650
mg/Kg - dry
30.7
1
09/18/20 03:09 ]ADS
G,OIOD
Manganese
822
mg/Kg - dry
3.07
1
09/18/20 03:09 )ADS
6010D
Mercury
0.313
mg/Kg - dry
0,0858
1
09/17/20 12:00 DDB
SW-7471B
Molybdenum
<1.53
mg/Kg - dry
1.53
1
09/18/20 03:09 JADE
6010D
Nickel
13.6
mg/Kg - dry
1.53
1
09/18/20 03:09 ]ADS
6010D
Potassium
549
mg/Kg - dry
61.3
1
09/18/20 03:09 )ADS
6010D
Selenium
4.93
mg/Kg - dry
3.07
1
09/18/20 03:09 ]ADS
6010D
Sodium
267
mg/Kg - dry
153
1
09/IB/20 03:09 )ADS
6010D
Zinc
58.8
mg/Kg - dry
7.67
1
09/18/20 03:09 ]ADS
6010D
Sulfur
S440
mg/Kg - dry
61.3
1
09118/20 03:09 ]ADS
6010D
Qualifiers/ DF Dilution Factor L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 4 of 6

j
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-94010 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 20-258-0003
Shipping Method
I* Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample, label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vial's free of headspace
0 Yes
0 No
NI/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
High concentration, container (48 hr)
High concentration pre -weighed (methanol -14 d)
F Low concentration EnCore samplers (48 hr)
[_ Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments: I
Signature: lBrand'i Watson Date & Time: 09/14/2020 13
Page 5 oaf- 6

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IN

Willcox & Mahe Soil Solutions, PLLC
Surnmerfield, North Carolina
RESIDUAL PAN CALCULATION
Greenville Utilities WTP
TKN=
13,200
mg/kg
NH3=
307
mg/kg
NO3-NO2-N=
36
mg/kg
Min Rate=
0.20
PAN= [min.rate (TKN - NH3) + 0.5 (NH3) + NO3-NO21
0.20 12,893 154
PAN= 2768.20 mg/kg
36.10
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/ITT remaining,
2ND YEAR RESIDUAL PAN
PAN=: [min.rate (1st year org. - N 2nd year min. - NJ
0.10 12,893 2,579
PAN= 1031.44 mg/kg remaining from I st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - NJ
0.05 10,314 1,031
PAN= 495.09 mg/kg remaining from 1st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - NJ
0.03 9,283 495
PAN= 292.93 mg/kg remaining from I st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - NJ
0.02 8,788 293
PAN= 164.63 mg/kg remaining from I st year application
Residual PAN from years 2 thru 5 after the initial application = 1984.09 mg/kg
Application
Method
First Year PAN
(mg/kg)
Five Year Maximum
Adjusted PAN
Surface
2,768
4,752
Incorporation
2,922
4,906

WN
SAR Calculation
Na mg1I
Ca mg/I
Mg mg/I
43.521
304.81
105.95
Na
Ca
SAR
—1.992
15141
8.829
0.545
�aniii-i �q-
Ca mil �eq%­
mil e—q­
1,892
15.241
&829
Enter
Enter.% TS
16.3
Data
Nam /k
267
I.---
Ca mg/kg
1870
. ..... —�---Mg
mg/kg
650
Job Name:
Greenville Utilities
VV'TP
Page 2

F`
RESIDUALS SOURCE CERTIFICATION
APPLICATION FORM
CITY OF LENOIR WTP
(FORM: RSC 06- z 6)

State of North Carolina
DWR
Department of Environmental Quality Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
INSTRUCTIONS FOR FORM: RSC 06-16
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and
supporting documentation
For more information, visit the Water Quality. Permitting Section's Non-DischaLg_e Perinittiag Unit
General — This certification provides detailed information of residuals source generating facility and its residuals quality for land
application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without
a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Residuals Source Certification (FORM: RSC 11-15):
Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not
make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the
application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer.
For new or renewed permits, submit a separate certification for each source facility,
El For modified permits, submit a separate certification for only those: facilities that are affected by the proposed modification.
Z Complete the residuals source facility summary page. List all new, renewed, or modified facilities,
B. Residuals Source -Generating Facility Information:
Z For each source facility, attach the following:
Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Nlap Guidance for
RC8JL1L1,11,,Land Application
Process flow diagram and/or narrative: - A detailed narrative and/or process flow diagram that describes how the residuals
are to be generated, treated, processed, and stored at the facility.
Z Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item 1. 8.
Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of
the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed,
and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during
processing.
Z Sampling plan - A detailed sampling plan for the residuals source -generating facility, Ensure that the plan identifies
sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition,
ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and
vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as
they are to be land applied, distributed, and/or disposed,
C. Residuals Quality Information:
For each source facility, attach the following:
Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification.
Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector
attraction reduction requirements.
For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please
attach analytical results of residuals generated from a similar facility along with the description of similarities of the two
facilities.
INSTRUCTIONS FOR FORM: RSC 06-16 Page I of 1

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ccS
P�4

1. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.);
1. Facility Name: George L. Bernhardt, Sr. Lake Rhodhiss WTP
2. Facility pen -nit holder is: El Federal, El State, 0 Local Government or 0 Private.
Facility permit issued by: Div. of Water Resources, ❑ Div. of Environmental Health,
or ❑ Other (explain: -).
3. Facility contact person and title: Kevin Matheson, WTP Superintendent
Complete mailing address: 5474 Waterworks Road
City: Granite Falls State: NC Zip: 28630
Telephone number: [phone] E-mail address: [e-mail]
4. Facility physical address: 5474 Waterworks Road
City: Granite Falls State: NC Zip: 28630
Coordinates: Latitude: 35147' 8.38" Longitude: 81'28' 54.50"
Datum: NAD83 Level of accuracy: Nearest hundredths of second
Method of measurement: MAP
5. Purpose of the facility:
treatment of municipal wastewater, El treatment of 100% domestic wastewater,
treatment of potable water, El treatment of 100% industrial wastewater,
El treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: - % industrial and - % domestic)
other (explain:_).
6. Does the facility have an approved pretreatment program: F1 Yes ❑ No
7. Facility permitted/design flow: 12 MGD and facility average daily flow: 6.4 MGD
8. Average amount of residuals being generated at this facility 2000 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment. N/A
Type and volume of residuals storage (i,e., outside of residuals treatment units): 0.75 acres with an average depth of 8 feet.
11. RESIDUALS QUALITY INFORMATION (See Instruction C.):
L Specify if residuals are regulated under:
El 40 CFR Part 503 or Z 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals, are defined under 15A NCAC 02T. 1102(6) as:
n Biological E Non -Biological
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of'industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
FORM: RSC 06-16 Page 1 of 5

3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261,33: ❑ yes no.
If yes, list the number(s):
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21 -
261,24: ❑ yes Eil no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory- Eurofins Test America and Date of analysis: 5/22/20
Passed corrosivity test: 0 yes ❑ no. pH:: s:.u. (2 < pH < 12.5)
Passed ignitability test: [A yes ❑, no. Flashpoint: > 140 OF(> 140°F)
Passed reactivity test: Eyes [Ino.HCN:<0.435m,gikg(<250)&H2S.56mg/kg (<500)
TCLP Parameter
Limit
(mg/1)
Result
(Ing1l)
TCLP Parameter
Limit
(121gfi)
Result
(177gll)
Arsenic
5.0
<0.5
Hexachlorobenzene
0.13
<0.05
Barium
100,0
<2
Hexachloro-1,3-Butadiene
0.5
<0.05
Benzene
0.5
<0.2
Hexachloroethane
3.0
<0.05
Cadmium
1.0
<0.5
Lead
5.0
<0.5
Carbon Tetrachloride
0.5
<0.2
Lindane
0.4
<0.0005
Chlordane
0.03
<0.005
Mercury
0.2
<0.0002
Chlorobenzene
100.0
<0.2
Methoxychlor
10.0
<0.0005
Chloroform
6.0
<0.2
Methyl Ethyl Ketone
200.0
<0.2
Chromium
5.0
<0.5
Nitrobenzene
10
<0.05
m-Cresol
200.0
< 0.05
Pentachlorophenol
100,0
<0.2
o-Cresol
200.0
< 0.05
Pyridine
5.0
<0. I
p-,Cresol
200.0
< 0.05
Selenium
1.0
<0.5
Cresol
200.0
< 0.05
Silver
5.0
<0.5
2,4-D
10,0
<0,.04
Tetrachloroethylene
03
<0.2
1,4-Dichlorobenzene
T5
<0.2
Toxaphene
0.,5
<0.04
1,2-Dichloroethane
0,5
<0.2
Trichloroethylene
0.5
<0.2
1 , I -Dichloroethylene
03
<0.2
2,4,5-Trichlorophenol
400.0
<0,05
2,4-Dinitrotoluene
0.13
<0.05
2,4,6-Trichloroplienol
2.0
<0.05
Endrin
0.02
<0.0005
2,4,5-TP (Silvex),
1.0
<Ul
Heptachlor and its Hydroxide
0.008
<0.0005
Vinyl Chloride
02
<0.2
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T. 1105.
a. For DistributionlLandApplication: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Waypoint Analytical and Date of analysis: 8/17/20
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(niglkg)
Monthly Average
Concentration Limits
(Class A Only)
(niglkg)
Result
(nzglkg)
Arsenic
75
41
8,36
Cadmium
85
39
0303
Copper
4,300
1,500
373
Lead
840
300
34.,2
Mercury
57
17
0.0575
Molybdenum
75
n/a
1.89
Nickel
420
420
19.7
Selenium
100
100
1.52
Zinc
7,500
2,800
203
b. For Surface Disposal Unit (jaliffill ): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: _ and Date of analysis. .
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(nzg1kg)
Chromium
(mglkg)
Nickel
(Ing4g)
El > 0 but < 25
30
200
210
25 but < 50
........ . . .
34
220
240
El > 50 but< 75
19
260
270
El >75 but< 100
46
300
320
100 but < 125
53
360
390
125
62
450
420
Result (ing4g)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination. Complete the followin&
a. Total solids: 33.0 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Waypoint Analytical and Date of analysis: 8/17/20
Parameter
Result
(mg1kg)
Aluminum
11,200
Ammonia -Nitrogen
1,200
Calcium
1,420
Magnesium
2,110
Nitrate -Nitrite Nitrogen
40.6
PH (Standard Unit)
5.8
Phosphorus
1,890
Potassium
1,620
Sodium
75.8
Total Kjeldahl Nitrogen
. ..... . .... ... .....
6,640
c. Using the results listed in Item 11, 5b. above, calculate the sodium adsorption ration (SAR): 0.17
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsurn, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 20 %. This
rate is a (check one): Z default value, or El actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (V) Year PAN
Five -Year
Maximum Adjusted PAN
(tng1kg)
('rang/kg)
Surface
1,729
2,566
Injectionlincorporation
2,329
F 3,166
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses: N/A
FORM: RSC 06-16 Page 4 of 5

7. Patlio2en Reduction: Per 15A NCAC 02TJ 106, specify how residuals will meet the pathogen reduction requirements:
a. Foi-Distribittioiv'LandAyi2licationofClaris AorEoiiivaleiii,
Z A fecal coliforrn density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
❑ A salmonello sp. density that is demonstration to be less, than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
E] Alternative I [ 15A NCAC 02T. 1 106(b)(3)(A)] - Time/Temperature Compliance,
❑ Alternative 2 [15A NCAC 02T. I 106(b)(3)(B)] - Alkaline Treatment,
El Alternative 3 [15A NCAC 02T. I 106(b)(3)(C)] - Prior Testing for Enteric, Virus/Viable Helminth Ova.
n Alternative 4 [15A NCAC 02T. I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 5 [15A NCAC 02T. I 106(b)(3)(E)-(K)l - Process to Further Reduce Pathogens (PFRP).
Specify one: composting, ❑ heat drying, ❑ heat treatment,
thennophilic aerobic digestion, ❑ beta ray irradiation,
gamma ray irradiation, or pasteurization.
b. For Land Application of Class B.
❑ Alternative 1 [15A NCAC 02T. 1 106(c)(1)] - Fecal Coliforrn Density Demonstration.
El Alternative 2 [15A NCAC 02T. 1 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one. ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion,
composting, or ❑ lime stabilization.
c. For Surf geeDisposa
0 Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item 11, 7a. above.
F] Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item Il. 7b. above.
❑ Exempt - If Daily Cover Alternative is chosen in Item 11.8. below [15A NCAC 02T.1 106(a)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector, Attraction Reduction (VAR): Per 15A NCAC 02T. 1107, specify how residuals will meet the VAR requirements:
R Alternative 1 [15A NCAC 02T. I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion),
F1 Alternative 2 [15A NCAC 02T. I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion),
❑ Alternative 3 [15A NCAC 02T. I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 [15A NCAC 02T. I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion),
EJ Alternative 5 [15A NCAC 02T, I 107(a)(5)] - 14-Day Aerobic Processes.
El Alternative 6 [15A NCAC 02T. I 107(a)(6)] - Alkaline Stabilization,
Alternative 7 [15A NCAC 02T. I 107(a)(7)] - Drying of Stabilized Residuals,
Alternative 8 [15A NCAC 02T. I 107(a)(8)] - Drying of Unstabilized Residuals.
El Alternative 9 [15A NCAC 02T. I 107(a)(9)) - Injection.
❑ Alternative 10 [ 15A NCAC 02T, I 107(a)(I 0)] - Incorporation.
D Alternative for Surface Disposal Units Only - Soil/Other Material Cover [I 5A NCAC 02T. I 107(b)(2)].
N Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface,
FORM: RSC 06-16 Page 5 of 5

530 Woodlawn Street
Belmont, NC 28012
1110-HOMIC SERVICES
p: (704) 5290000
h [phone]
A Carylon Company
wwwbio-namic.corn
CITY OF LENIOR
GEORGE BERNHARDT LAKE RHODH'ISS WATER TREATMENT PLANT
Residuals Source- Generating Facility Information
- Process Flow Narrative
The City of Lenoir operates an existing water treatment plant at 5474 Waterworks Road, which
produces drinking water for the local community. The source of raw water originates from Lake
Rhodhiss, the second impoundment on the Catawba River.
The George Bernhardt Lake Rhodhiss Water Treatment Plant has been operational since 1956
and has a capacity of 12 MGD. The average daily flow is 6.5 million gallons per day.
Raw water from Lake Rhodhiss is pumped to a dual train Acti-flo mechanical pretreatment unit
capable of processing up to 9 MG on each side. Then the introduction of alum coagulant and an
anionic polymer causes particles to clump together allowing additional sedimentation to occur
with the aid of flocculators and a sedimentation basin.
Upon the completion of settled water, the treated water is gravity fed through 12 mixed media
filtration units. The filtrate is then disinfected using Sodium Hypochlorite, fluoridated, and finally
pH adjusted to produce clear, sediment free finished water. The finished water is then pumped
into clear wells and remote storage tanks ready for distribution. The collected alum sludge and
sediment from the treatment process is discharged into 2 holding tanks in series and
subsequently may be diverted into the original holding lagoon that is to be cleaned out.
The lagoon will hold the sediment until removal is necessary. A portable hydraulic dredge is
placed in the lagoon to pump the materials out of the basin. The floating hydraulic dredge is
advantageous as it allows the lagoon to remain in service during the process. The sediment is
pumped in slurry form to a 20,000-gallon receiving tank. The tank is fitted with mixers to,
homogenize the materials for mechanical dewatering.
The mechanical dewatering process is accomplished with a mobile belt filter press system. An
anionic or catanionic polymer is introduced to concentrate the slurry during the dewatering
process. The belt filter press further removes water by compressing the residuals between filter
belts generating a filter cake. The filtrate water resulting from the process can be returned to the
lagoon.
The filter cake, is now suitable for either onsite land application or for loading, into dump trucks
for transportation to a secondary application site as a soil amendment.
- Quantitative Justification for Residuals Production Rate
A minimum of 2,000; dry tons may be removed and land applied annually.
A Carylon Company

SAMPLING PLAN
Sampling Procedures
Accurate sampling is essential for valid laboratory test results. All samples collected at the respective
Water Treatment Plant's (WTP) are grab samples, which are samples taken at selected intervals to
represent conditions at a given location at a particular point in time.
Grab samples of residuals are stored in a manner that will not alter sample characteristics. Proper
preservatives are used for specific parameters. The samples are kept under refrigeration at 4* C until
delivered to laboratory for analysis.
Sampling Log
Sampling information is recorded on a chain of custody (COC) form by Bio-Nomic Services personnel
provided by the respective laboratory that is performing the required testing required by the permit. Log
book entries include, at a minimum:
• Purpose ' of sampling
• Location of sampling point
• Type of sample (grab or composite)
• Name of person collecting samples
• Type of residuals sampled (undigested, post -digestion, post -storage)
• Number and volume of sample(s) collected
• Description of sampling point
• Date and time of collection
The residual solids analysis will be conducted for, but not limited to, the following parameters, percent total
solids, phosphorus, lead, copper, cadmium, sodium, total Kjeldahl nitrogen, nitrate nitrogen, nitrite nitrogen,
magnesium, potassium, zinc, nickel, arsenic, mercury, selenium, molybdenum, calcium, ammonia nitrogen,
aluminum and pH on an Annual Basis, or as required by Permit Conditions based upon annual tons land
applied.

Lake Rhodhiss WTP
FIELD LOADINGS
DATESPD: 2019
FARM:
CAKE ACRES:
150.00
SITE:
Plant S46 RESIDUALS WET TONS
6,000.0
FIELD:
wl
WTIACRE
40.00
CROP:
Bermuda
% TS
31.30
Site Cond
G/D
DT/ACRE:
12.52
- -
. ) 50
101,coo b—r,:,eAe—,
willcox&mabe
Prepared By: SOIL SOLUTIONS

Environment Testing
America
W"W"Oni,
Eurofins TestAmerica, Pittsburgh
301 Alpha Drive
RIDC Park
Pittsburgh, PA 15238
Tel: [phone]
Laboratory Job ID: 180-106162-1
Client Project/Site: Lenoir WTP
For
Bio-Nomics Services., Inc.
530 Woodlawn Street
Belmont, North Carolina 28012
Attn: Mr. Joel Coert
�VA
Authorized for release by:
61412020 2.51:12 PM
Ken Hayes, Project Manager 11
[phone]
I<en,[e-mail]
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the, items tested and the sample(s) as received by the laboratory.
PA Lab ID: 02-00416

Client: Bio-Nornics services., Inc.
Project/Site: Lenoir WTP
Laboratory Job ID: 180-106162-1
Cover Page .............................................. 1
Table of Contents ......................... . . . .............
2
Case Narrative ...........................................
3
Definitions/Glossary ........................ . ..............
4
Certification Summary ......................................
5
Sample Summary ..... ......................................
6
Method Summary .............. . ..........................
7
Cab Chronicle ............................................
8
Client. Sample Results ......................................
1 o
CSC Sample Results ........................................
12
CSC Association Summary ....................................
24
Chain of Custody ..........................................
28
Receipt Checklists ................... . .....................
30
1, rr�iry 91
Page 2 of 30
Eurofins TestAmerica, Pittsburgh
614/2020

Case Narrative
Client: Bio-Nomics Services., Inc.
Project/Site: Lenoir WTP
J o b ID: 1 �6-' 1­0_ 61 2_-1
Laboratory: Eurofins TestArnerica, Pittsburgh
Narrative
Job ID: 180-106162-1
F
Job Narrative
180-106162-1
Receipt
The sample was received on 5/2312020 9:30 AM; the sample arrived in good condition, properly preserved, and where required, on ice.
The temperature of the cooler at receipt time was 2.8°C
Receipt Exceptions
The Field Sampler was not listed on the Chain of Custody.
GC/MS VOA
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Herbicides
Method 8151& Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate
(MS/MSD/DUP) associated with preparation batch 180-316683 and 180-316961.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
PCBs
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page,
Pesticides
Method 8081 B: Insufficient sample volume was available to perform a matrix spike/miatrix spike duplicatelsample duplicate
(MS/MSD/DUP) associated with preparation batch 180-316683 and'180-316951.
Method 8081 B: The Tetrachloro-m-xylene and/or DCB Deca,chlorobiphenyl (Surr) surrogate recovery for the following samples was
outside acceptance limits (high biased) on the primary or confirmation column due.: (LB 180-316683/1-E) and (LCS 180-31695112-A).
The recovery is within acceptance limits on the other column, indicating that the extraction process was in control. All associated samples
are ND.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page,
Metals
Method 601 0D-_ The low level initial calibration verification (ICVL) associated with prep batch 316941 recovered above the method 601 OD
upper control limit for arsenic. The sample associated with this ICVL was non -detect for the affected analyte; therefore, the data have been
reported. The associated sample is impacted: LENOIR VVTP (180-106162-1)-
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
General Chemistry
Method 9014: The following sample was found to contain Sulfide: LENOIR WTP (180-106162-1). The sulfide was treated and removed
prior to distillation. All samples assumed to have sulfide and were treated with 100 uL of bismuth nitrate solution.
Method 9034—Calc: The following sample(s) was received outside of holding time: <&commaMerge&>.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page,
Eurofins TestAmerica, Pittsbur h
Page 3 of 30 6/4/2090

Definitions/Glossary
Client: Bio-Nomics Services., Inc. Job IID; 180-106162-1
Project/Site: Lenoir WTP
Qualifiers
GC/MS Semi VIDA
Qualifier Qualifier Description
or LCSD is outside acceptance limits.
Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
GC Semi VOA
Qualifier Qualifier Description
p The %RPD between the primary and confirmation column/detector is >40%, The lower value has been reported,
X Surrogate recovery exceeds control limits
Metals
Qualifier Qualifier Description
ICV,CCV,ICB,CCB, ISA, ISB, CRI", CRA, DLCK or MRL standard: Instrument related QC is outside acceptance limits.
F1 MS and/or MSD recovery exceeds control limits.
F2 MSIMSD RPDexceads control limits
General Chemistry
Qualifier Qualifier Description
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request,
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
Listed under the "D"' column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNIF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL., RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoDIDOE)
LOCI Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MQL Method Quantitation Limit
INC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
Eurofins TestAmerica, Pittsburgh
Page 4 of 86 6/4/2020

Accreditation/Certification Summary
Client: Bio-Nomics Services., Inc. Job ID: 180-106162-1
Project/Site: Lenoir WTP
Laboratory: Eurofins TestAmerica, Pittsburgh
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority
Program
Identification Number
Expiration Date
North Carolina (WWISW)
State
434
01-01-21
The following analytes are included in this
report, but the laboratory is not certified by the governing authority.
This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method
Matrix
Analyte
EPA 1102013
Sludge
Ignitabilify----,
EPA 9014 9010C
Sludge
Cyanide, Total
South Carolina
State
89014
04-30-20
The following analytes are included in this
report, but the laboratory is not certified by the governing authority.
This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method
Matrix
Analyte
EPA 1020B
Sludge
Ignitability
EPA 8151A 8151A
Sludge
2,4-D
EPA 8151A 8151A
Sludge
Silvex (2,4,5-TP)
* Accreditation/Certification renewal pending - accreditation/cer-fification considered valid.
Eurcifins TestAmerica, Pittsburgh
Page 5 of 30 6/4/2020

Sample Summary
Client.- Bio-Nomics Services., Inc.
Project/Site: Lenoir WTP
Job ID: 1180-106162-1
Lab Sample ID Client Sample ID Matrix Collected Received Asset ID
180-106)62--1 LENOIR VVTP 81­udgE�­— 0-5/-221-2009W 6-5—/23126679-30
Eurofins TestAmerica, Pittsburgh
Page 6 of 30 6/4/2020

Method Summary
Client: Bio-Nornics Services., Inc. Job ID: 180-106162-1
Project/Site: Lenoir WTP
Method
Method Description
Protocol
Laboratory
EPA 62_60D
Volatile. Organic Compounds by _Gvms
9-w-846—
TAL PIT
EPA 8270E
Sernivolatile Organic Compounds (GC/MS)
SW846
TAL PIT
EPA 80816
Organochlorine Pesticides (GC)
SW846
TAL PIT
EPA 8082A
Polychlorinated Biphenyls (PCBs) by Gas Chromatography
SW846
TAL PIT
EPA 8151A
Herbicides (GC)
SW846
TAL PIT
EPA 601 OD
Metals (ICP)
SW846
TAL PIT
EPA 7470A
EPA 1020B
Mercury (CVAA)
Ignitability, Small Scale Closed -Cup Method
SW846
SW846
TAL PIT
TAL PIT
EPA 9014
Cyanide
SW846
TAL PIT
EPA 9034
Sulfide, Acid soluble and Insoluble (Titrimetric)
SW846
TAL PIT
EPA 9045D
pH
SW846
TAL PIT
3010A
Preparation, Total Metals
SW846
TAL PIT
3510C
Liquid -Liquid Extraction (Separatory Funnel)
SW846
TAL PIT
3541
Automated Soxhtet Extraction
SW846
TAIL PIT
5030C
Purge and Trap
SW846
TAIL PIT
7470A
Preparation, Mercury
SW846
TAL PIT
8151A
Extraction (Herbicides)
SW846
TAL PIT
9010C
Cyanide, Distillation
SW846
TAL PIT
9030B
Sulfide, Distillation (Acid Soluble and Insoluble)
SW846
TAL PIT
EPA 13111
TCLP Extraction
SW846
TAL PIT
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical! Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL PIT = Eurohns TestAmerica, Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
Eurofins TestArnerica, Pittsburgh
Page 7 of 30 6/4/2020

Lab Chronicle
Client: Bio-Nornics Services., Inc.
Job ID: 180-106162-1
Project/Site: Lenoir WTP
Client Sample ID: LENOIR WTP
Lab Sample ID: 180-106162"-1-
Date Collected: 05/22120 09.00
Matrix: Sludge
Date Received: 05/23/20 09:30
. .. . ....... —
Batch Batch
tail
Initial
Final
Batch
Prepared
Prop Type Type Method
Run Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
TCLP Leach EJPA131T---
—
25. 0-0 g,
—500mL
3-1-6691
05127120 22:00
JAS
TAL P-I—T--
TCLP Analysis EPA 8260D
1
0.125 mL
5ml-
316868
05129/20 11-125
KLG
TAL PIT
Instrument ID: CHHP9
TCLP Leach EPA 1311
100.00 g
2000 mL
316683
05/27/20 22:00
JAS
TAL PIT
TCLP Prep 3510C
200 mL
10.0 mL
316950
05/29120 15:00
CBY
TAL PIT
TCLP Analysis EPA 8270E
1
1 mL
1 mL
317153
06102120 12:23
MVP
TAL PIT
Instrument ID: CH732
TCLP Leach EPA 1311
100.00 g
2000 mL
316663
05127/20 22:00
JAS
TAL PIT
TCLP Prep 351 0C
101) mL
40.0 mL
316951
05/29120 15:00
CBY
TAL PIT
TCLP Analysis EPA 8081 B
1
317106
06101/20 19:39
DFE
TAL PIT
Instrument ID: CHGC15
Total/NA Prep, 3541
15A g
20.0 mL
316603
05127/20 lUl
GDH
TAL PIT
Total/NA Analysis EPA 8082A
1
316711
05128/20 16:59
JM:O
TAIL PIT
Instrument ID: CHGC8
TCLP Leach EPA 1311
100.00 g
2000 mL
316683
05/27120 22:00
JAS
TAL PIT
TCLP Prep 8151A
100 mL
10.0 mL
316961
05/29120 17:20
CBY
TAL PIT
TCLP Analysis EPA 8151A
20
317040
06101120 12:03
JMO
TAL PIT
Instrument ID: CGC1
TCLP Leach EPA 1311
100.00 g
2000 mL
316683
05/27120 22:00
JAS
TAIL PIT
TCLP Prep 301 OA
5mL
50 mL
316941
05/29/20 15:21
JL
TAL PIT
TCLP Analysis EPA 6010D
1
317142
06101/20 11:43
RJG
TAIL PIT
Instrument ID: C
TCLP Leach EPA 1311
100.009
2000 mL
316683
05127120 22:00
JAS
TAL PIT
TCLP Prep 7470A
50 mL
50 mL
316915
05/29/20 15:10
NAM
TAIL PIT
TCLP Analysis EPA 7470A
1
316982
05/29/20 18A0
NAM
TAL PIT
Instrument ID: HGZ
Total/NA Analysis EPA 1020E
1�
316583
05/27120 08:18
AVS
TAIL PIT
Instrument ID: NOEQUIP
Total/NA Prep 9010C
0.23 g
10 mL
317066
06101120 12:00
CMR
TAL PIT
Total/NA Analysis EPA 901:4
1
317144
06/01/20 14:05
CMR
TAL PIT
Instrument ID: SEAL2
Total/NA Prep 9030E
5.06 g
50 mL
316574
05127/20 09:00
CMR
TAL PIT
Total/NA Analysis EPA 9034
1
316625
05/27120 12:00
CMR
TAIL PIT
Instrument ID: NOEQUIP
Total/NA Analysis EPA 9045D
1
20.37 g
20 mL
316790
05129/20 15:30
PMH
TAL PIT
Instrument ID: NOEQUIP
Laboratory References-
TAL PIT = Eurofins TestAmerica, Pittsburgh, 301 Alpha
Drive, RIDC Park, Pittsburgh, PA
15238, TEL [phone]
Eurofins TestAmerica, Pittsburgh
Page 8 of 30 6/4/2020

Lab Chronicle
Client: Bio-Nornics Services., Inc. Job IU180-106162-1
Project/Site: Lenoir WTP
Analyst References:
Lab; TAL PIT
Batch Type:: Leach
JAS = Jeremy Stundon
Batch Type: Prep
GBY = Charles Yushinski
CDH = Christopher Hayburn
CMR = Carl Reagle
JL = James Lyu
NAM = Nicole Marfisi
Batch Type: Analysis
AVS = Abbey Smith
CMR Carl Reagte
DIE =David Eppinger
JMO = John Oravec
KLG = Kathy Gordon
NAM = Nicole Marfisi
PMH Paloma Hoelzle
RJG = Rob Good
VVP = Vincent Piccohno
Eurofins TestAmerica, Pittsburgh
All
Page 9 of 30 6/4/2020

Client Sample Results
Client: Bio-Nomics Services,, Inc.
Job ID: 180-106162-1
Project/Site: Lenoir WTP
Client Sample ID: LENOIR
WTP
Lab Sample
ID- 180-106162-1
Date Collected: 05/22/20 09:00
Matrix: Sludge
Date Received: 05/23120 09:,30
Method: EPA 8260D - Volatile Organic Compounds
by GC/MS - TCLP
Analyte
Result Qualifier
RL MDL
Unit
D Prepared
Analyzed
Oil Fac
Benzene ----- -
NO
—0,200
Wg—/L
1
2-Butanone (MEK)
NO
0.200
mg/L
05/29/20 11:25
1
Carbon tetrachloride
NO
0.200
mg/L
05/29/20 11: 25
1
Chlorobenzene
NO
0.200
mg/L
05/29/20 11:25
1
Chloroform
NO
0.200
mg/L
05/2912011:25
1
1,2-Dichloroethane
NO
0.200
mg/L
05129120 11;25
1
M-Dichloroethene
NO,
0.200
mg/L
05/29/20 11:25
1
Tetrachloroethene
NO
0100
mg/L
05/29120 11:25
I
Trichloroethene
NO
0.200
mg/L
05/29/20 11:25
1
Vinyl chloride
NO
0.200
mg/L
05/29/20 11:25
1
1,4-Dichlorobenzene
NO
0.2'00
mg/L
05129/20 11:25
1!
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
4-Bromofluorobenzene (SurrJ
73
54-125
W M
05/29/20 11:25
1
Dibromofluoromathane (Surr)
115
55-150
05129V20 11:25
1
1,2-13ichforoethane-& (Surf)
119
53-150
05/29/20 11:25
1
Toluene -dB (Surr)
85
63-127
05129120 11:25
1
Method: EPA 8270E - Sernivolatile Organic Compounds (GC/MS) - TCLP
I Analyte
Result Qualifier
RL MDL
Unit
D Prepared
Analyzed
Oil Fac
2,-4,5-Tiiichlorophenol
N b
—0.0500 — - -----
—mg/L
05/29/2-0 15:00
—06/0-2-12-0-1 -2—:23
1
2,4,6-Trichlorophe not
NO
0.0500
mg/L
05/29120 15:00
06102/20 12:23
1
2,4-Oinitrotoluene
NO
0.0500
mg/L
0512912015:00
06102/20 12:2!3
1
2-Methylphenol
NO
0,0500
mg/L
05/29/20,15:00
016102120 12:23
1
Methylphenol, 3 & 4
NO
0,0500
mg/L
05/29120 15:00
06102120 12:23
1
Hexachlorobenzene
NO
0.0500
mg/L
05/29/20 15:00
06102/20 12:23
1
Hexachlorobutadiene
NO
0.0500
mg/L
05129120 15:00
06102120 12:23
1
Hexachloroethane
NO
0.0500
mg/L
05/29/20 15M
06102120 12:23
1
Nitrobenzene
NO
0.0500
mg/L
05129/20 15:00
06102120 12:23
1
Pentachlorophe:nol
NO
0.250
mg/L
05129/20 15:00
06102/20 12:23
1
Pyridine
NO
01100
mg/L
05129/20 15M
06/02/20 12:23
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
i 2,4,6-Tfiro bmophenol (Surr)
- —
N
---1—
N -13
05/29/20 f,5-.--O0
2-Fluorobiphenyl
70
55-107
05/29/20 15:00
W'O2120 12:23
1
2-Fluorophenof (Surr)
69
60-108
05/29/20 15:00
06/02/20 1223
1
Nitrobenzene-d5 (Surr)
65
62-115
05a9120 15:00
06102120 12:23
1
Phenol-d5 (Surr)
57
52-107
05129120 15:00
06102120 12:23
1
Terphenyl-04 (Surr)
72
44-116
05129120 15:00
06/02/20 12:23
1
Method: EPA 8081 B - Organochlorine
Pesticides (GC)
- TC,LP
Analyte
Result Qualifier
RL MDL
Unit
D Prepared
Analyzed
Oil Fac
Chlordane (technical)
NO
0,00500
mg/L
05/29/20 15:00
06101120 19:39
1
Endrin
NO
0.000500
mg/L
05/29/20 15,00
06101120 19:39
1
gamma-BHC (Undane)
NO
0,000500
mg/L
05129/20 15:00
06101120 19:39
1
Heptachlor
NO
0.000500
mg/L
(15/29/20 15:00
06/01/20 19M
1
Heptachlor epoxide
NO
0.000500
mg/L
05/29/20 15:00
06101120 19:39
1
Methoxychlor
NO
0.000500
mg/L
05129/20 15,00
06/01/20 19M
1
Toxaphene
NO
0.0400
mg/L
05/29/20 1!5:00
06101/20 M39
1
Eurofins TestAmerica, Pittsburgh
Page 10 of 30 6/4/2020

Client Sample Results
Client! Bio-Nornics, Services., Inc.
Project/Site: Lenoir WTP
Client Sample ID: LENOIR WTP
Date Collected: 05/22/20 09:00
Date Received: 05123/20 09:30
Job ID: 180-106162-1
Lab Sample ID: 180-106162-1
Matrix: Sludge
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl (Surr)
114
58-115
0-0
b�6-10112019 Y§
— I
DCB Decachlorobiphenyl (Surr)
101
58-115
045,29120 15:00
06101120 19:39
1
Tetrachloro-m-xylena
100
43-118
05129120 15:00
06101120 19:39
1
Tetrachloro-m-xylene
114
43-118
05129120 15:00
06/01/20 19:39
1
Method: EPA 8082A - Polychlorinated
Biphenyls (PCBs) by Gas
Chromatography
Analyte
Result Qualifier
RL
MOIL Unit
D Prepared
Analyzed
Dil Fac
P—CB-101'6
NO
161
uq/Kg
05127120 *01
05128120 16;59
1
PCB-1221
NO
16.2
ug/Kg
05/27/20 10:01
05/28/20 1&59
1
PCB-1232
NO
16.2
ug/Kq
05/27/20 10:01
05128/20 16:59
1
PCB-1242
NO
16,2
ug/Kg
05/27/20 10:01
05128/20 M59
1
PCB-1248
NO
16.2
ug/Kg
05127/20 10:01
05128/20 16!59
1
PCB-1254
NO
16.2
ug/Kg
05/27/20 10:01
05128120 16:59
1
PCB-1260
NO
16.2
ug/Kg
05/27120 10:01
05128/20 16:59
1
Surrogate
%Recovery Qualifier
Tatrachloro-m-xyleneTS-u—fr)
86
Tetrachloro-m-xylene (Surr)
84
DCB Decachlorobiphenyl (Surr)
86
DCB Decachlorobiphenyl (Surr)
87
Method: EPA 8151A - Herbicides (GC) - TCLP
Analyte
Result Qualifier
NO
Silvex (2,4,5-TP)
N!D
Surrogate
%Recovery Qualifier
2,4-Dichlorophenylacetic acid
29
2,4-Dichlorophenylacetic acid
39
Method: EPA 601 OD - Metals (lCP) - TCLP
Analyte
Result Qualifier
Sliver
ND
Barium
ND
Cadmium
NO
Chromium
ND
Lead
ND
Selenium
ND
Arsenic
NO
Method: EPA 7470A - Mercury (CVAA) - TCLP
Analyte
Result Qualifier
Mercury
NO
General Chemistry
Analyte
Result Qualifier
Uiinide, Total
NO
Sulfide
56.0
Analyte Result Qualifier
Ignitability >140
pH 6,3 HF
Limits
Prepared
Analyzed
Dil Fac
51-112
05/27/20 10:01
05 �812O 16:09
1
51-112
05/27/20 10:01
05/28/20 16.-59
1
61-132
05/27/20 10:01
05126120 16:59
1
61-132
05127120 10.01
05126120 16:59
1
RL
MDL
Unit
D
Prepared
Analyzed
oil Fac
0.0400
mg/L
05129/20 17:20
6641&-12:03
20
0.0100
mg/L
05/29/20 1710
06/01/20 12:03
20
Limits
Prepared
Analyzed
Dif Fac
23-122
0529/20 17:20
06101120 12:03
20
23-122
05129120 17.20
06101120 12:03
20
RL
MOL
Unit
D
Prepared
Analyzed
Oil Fac
0.500
mg/L
05129/20 15:21
06/01/20 11:43
1
2.00
mg/L
05/29/20 15:21
06/01/20 11:43
1
0.500
mg/L
05129/20 15:21
06101120 11:43
1
0,500
mg/L
05/29120 15;21
06101120 11:43
1
0.500
mg/L
05/29/20 15:21
06/01120 11;43
1
0.500
mg/L
05/29120 15:21
06/01120 11:43
1
0.500
mg/L
05129/20 15:21
06101/20 11:43
1
RL
MDL
Unit
D
Prepared
Analyzed
Oil Fac
0.000200
mg/L
0,5129/20 15:10
05129/20 18:40
1
RL
MDL
Unit
D
Prepared
Analyzed
Oil Fac
0.435
mg/Kg
06101/20 12:00
06101120 14:05
1
29.6
mg/Kg
05/27/20 09':00
05/2,7120 112:00
1
RL
RL
Unit
D
Prepared
Analyzed
Oil Fac
. ........ . ... ..... .
Degrees F
65127120-08-18
1
0.1
SU
05/29/20 15,30
1
Eurofins TestAmerica, Pittsburgh
Page 11 of 30
6/4/2020

Client: Bio-Nomics, Services., Inc.
Project/Site: Lenoir VVTP
M'eth-od: EPA 8260D - Volatile I ..
- ---------- ---- - - ----- -- -1-1 - ------
Lab Sample ID: LCS 180�-316868/3
Matrix: Solid
Analysis Batch: 3168,68
Analyte
9-e—nzene
2-Butanone (MEK)
Carbon tetrachloride
ChJorobenzene
Chloroform
1,2-Oichloroethane
1,1-Dichloroethene
Tetrachtoroethene
Trichloroethene
Vinyl chloride
1,4-[Dichlorobenzene
QC Sample Results
anic Compounds by GC/MS
Spike
Added
LCS LCS
Result Qualifier
0.0106
0.01033
0.0100
0.01176
0,01100
0.009665
0,0100
0.01069
0.0100
0,009641
0.0100
0.01008
0.0100
0.008952
0.0100
0.01105
0.0100
0.009349,
0.0100
0-008684
0,0100
0.01133
LCS LCS
Surrogate %Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 103 54-125
Dibromofluoromethane (Surr), 93 55-150
1,2-Dichloroethane-& (Surr) 91 53-150
Toluene -dB (Surr) 93 63-127
Lab Sample ID: LB 180-316691/1-A
Matrix: Solid
Analysis Batch: 316868
Job ID: 180-106162-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Unit
D %Rec
%Rec.
Limits
W-9—IL
103
72-1'18
mg/L
118
33-133
mg/L
97
69-137
mg/L
107
77-122
mg/L
96
78-119
mg/L
101
62-129,
mg/L
90
60-131
mg/L
110
75-125
mg1L
93
76-120
mg/L
87
52-130
mg/L
113
76-1119
Client Sample ID: Method Blank
Prep Type: TCLP
LB LB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Oil Fac
Benzene
ND
mq/L
05129/20 08!55
1
2-Butanone (MEK)
NO
0.0500
mg/L
05129/20 08:55
1
Carbon tetrachloride
NO
0.0500
mg/L
05/29/20 08:55
1
Chl'orobenzene
NO
0.0500
mg1L
05/29/20 08:55
1
Chloroform
ND
0.0500
mg/L
05129120 08:55
1
1,2-Dichloroethane
NO,
0.0500
mg/L
05/29120 08:55
1
1,1-Dichloroethene
NO
0,0500
mg/L
05/29/20 08:55
1
Tetrachloroethene
NO
0.0500
mg/L
05129/20 08:55
1
Trichloroethene
NO
0.0500
mg/L
05/29/20 08:55
1
Vinyl chloride
ND
0.0500
mg/L
05/29/20 08:55
1
1,4-Dichlorobenzene
NO
0.0500
mg/L
05/29120 08:55
1
LE LB
Surrogate
1Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
4-Bromofluorobenzene (Surr)
61
54 - 12'5
Dibromofluoromethane (Surr)
111
55-150
05/29/20 06:55
1
1,2-Dichioroethane-& (Surr)
121
53-150
05/29/20 08:55
1
Toluene-d8 (Surr)
89
63-127
05129120 08:55
1
Lab Sample ID. 180-105839-A-13-B
MS
Client Sample ID: Matrix Spike
Matrix: Solid
Prep Type.
TCLP
Analysis Batch: 316968
Sample Sample
Spike
MS MS
%Rec,
Analyte
Result Qualifier
Added
Result Qualifier Unit
D %Rec
Limits
Benzene
NO
0A00
0.3556 mg/L
89
72-118
2-Butanone (MEK)
NO
0.400
0,3283 mg/L
82
33-133
Eurofins TestAmerica, Pittsburgh
Page 12 of 30 6/4/2020

QC Sample Results
Client: Bio-Nornics Services., Inc.
Project/Site'. Lenoir, WTP
Job ID: 180-106162-1
Method EPA 826 1 0 1 D - Volatile- Organic - Co I mp . oun ds - I by GC/MS (dointinued-)
.... ...... ... ......... - - ----- - . ...... --------- -- - - -
Lab Sample ID: 180-105839-A-13-B MS Client Sample ID. Matrix Spike
Matrix: Solid Prep Type: TCLP
Analysis Batch: 316868
Sample Sample
Spike
Ms MS
%Rec.
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
Carbon tetrachloride
Na
0A00
0.3682
mg/L
92
69-137
Chlorobenzene
ND
0.400
0.4116
mg/L
103
77-122
Chloroform
ND
0,400
0.4231
mg/L
106
78-119
1,2-Dichloroethane
ND
0.400
0,3949
mg/'L
99
62-129
I,I-Dichloroethene
ND
0.400
0.3457
mg/L
86
60.131
Tetrachloroethene
ND
0.400
0.41141
mg/L
104
75.125
Trichloroethene
ND
0.400
0.3306
mg/L
83
76-120
Vinyl chloride
ND
0.400
03336
mg1L
83
52-130
1,4-Dichloroberizene
ND
0.400
0A232
mg/L
106
76-119
MS MS
Surrogate
%Recovery Qualifier
Limits
4-8romofluorobenzene (Surr)
113
54-125
I Dibromolluoromethane (Surr)
88
55-150
1,2-Dichloroethane-& (Surr)
93
53-150
Toluene-d8 (Surr)
96
63-127
Lab Sample ID: 180-105839-A-13-C MSD
Client Sample ID: Matrix Spike Duplicate
Matrix: Solid
Prep
Type:
TCLP
Analysis Batch: 316868
Sample Sample
Spike
MSD MSD
%Rec.
RPD
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
RPD
Limit
Benzene
ND
0.400
0.3195
mg/L
80
72-118
11
20
2-Butanone (MEK)
ND
0A00
0.2914
mg1L
73
33-133
12
35
Carbon tetrachloride
ND
0,400
0,3254
mgIL
81
69-137
12
20
Chlorobenzene
ND
0.400
0.3943
mg/L
99
77-122
4
20
Chloroform
ND
0,400
0®3906
mg/L
98
78-119
8
20
1 2-Dichloroethane
NO
0.400
0.3303
mg/L
83
62-129
18
20
1,1-Dichloroethene
ND
0.400
0.2943
mg/L
74
60-131
16
35
Tetrachloroethene
ND
0.400
0.4046
mg/L
101
75-125
2
20
Trich,loroethene
ND
0.400
0,3630
mg/L
91
76 - 120
9
20
Vinyl chloride
NE)
0.400
0.2839
mg]L
71
52-130
16
21
1,4-Dichlorobenzene
ND
0,400
0.4107
mg/L
103
76-119
3
20
MSD MSD
Surrogate
%Recovery Qualifier
Limits
4-Bromofluorobenzene (Burr)
98
54-125
Dibromofluoromethane (Surr)
83
55-150
1,2-Dichloroethane-d4 (Surr)
82
53-150
Toluene-dS (Surr)
91
63-127
Method: EPA 8270E - Sernivolatile Organic Compounds (GC/MS)
Lab Sample ID: MB 180-31695011-A
Matrix: Solid
Analysis Batch: 317153 MB, MB
Analyte Result Qualifier RL
2-,4,5-Tnchi'o'r6p-henol ND 0.0500
2,4.6-Trichlorophenol ND OMOO
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 316950
MDL Unit D Prepared Analyzed Dil Fac
mg/L 05129/20 15M 06/02/20 08:55 1
mg/L 05/29/20 15:00 06102/20 08:55 1
Eurofins TestAmerica, Pittsburgh
Page 13 of 30 6/4/2020

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Lenoir WTP
Job ID: 180-106162-1
Method: EPA 827'OE - Semivolatile Organic Compounds (GC/MS) (Continued),
------------ . . . ............ ...... - - ----- --- - -- ............- - -- ------------- ---------- . .. . .......
Lab Sample ID: MB 180-316950/1 -A Client Sample ID: Method Blank
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 317153 Prep Batch: 316950
MB MB
An,alyte
Result Qualifier
2,4-Dinitrotoluene
ND
2-Methylphenol
ND
Methylphenol, 3 & 4
ND
Hexachlorobenzene
ND
Hexachlorobutadiene
ND
Hexachloroethane
ND
Nitrobenzene
ND
Pentachlorophenol
NO
Pyridine
ND
MB MB
Surrogate %Recovery Qualifier
2,4,6-Tfibromophenol (Surr)
68
2-Fluorobiphenyl
70
2-Fluorophenol (Surr)
73
Nitrobenzene-d5 (Surr)
65
Phenol,45 (Surr)
66
Terphenyl-dN (Surr)
73
Lab Sample ID: LCS 180-31695012-A
Matrix: Solid
Analysis Batch: 317153
RL
MDL Unit
D Prepared
Analyzed
ail Fac
0,0500
mg/L
05/29/20 15:00
06/02/20 08:55
1
0.0500
mg/L
05129120 15M
06/02120 08:55
1
0.0500
mglL
05/2�9120 15:00
06102/20 08:55
1
0,0500
mglL
05/29/20 15=
06102/20 08:55
1
0.0500
mg/L
05/29/20 15W
06/02/20 08:55
1
0.0500
mg/L
05/29120 15:00
06102/20 08:55
1
0.0500
mg/L
05/29f20 15:00
06/02120 08:55
1
0,250
mg/L
05/29120 15:00
06102120 08:55
1
0.100
mg/L
05129120 15:00
06/02/20 08:55
1
Limits
Prepared
Analyzed
Dil Fac
2�4 - 113
05129120 15:00
06102120
1
55-107
05129120 15:00
0610212008:55
1
60-108
05129120 15 * -00
06102120 08:55
1
62-115
05129120 15:00
06102120 08:55
1
52-107
05129120 15:00
06102120 08:55
1
44-116
05�9120 15:00
06/02/20 08:55
1
Spike
LCS LCS
Analyte
Added
Result Qualifier
2,4,5-Trichlorophenol
0.250
0.2139
2.4,6-Trichlorophenol
0.250
0.2709
2,4-Dinitrotoluene
0.250
0.2183
2-Methylphenol
0,250
0.2089
Methylphenol, 3 & 4
0.500
0,4550
Hexachlorobenzene
0,250
0,1838
Hexachlorobutadiene
0250
0M74
Hexachloroethane
0.250
0,2387
Nitrobenzene
0.250
0.2240
Pentachloro,phenol
0.250
0.1011 1
Pyridine
0,250
01791
LCS LCS
Surrogate
%Recovery Qualifier
Limits
2,4,6-Tribromophenol(Surr)'---"-
'- 106 -
------- ; 4 �-i 13
2-Fluarobiphenyl
102
55-107
2-Fluorophenol (Surr)
105
60-108
Nitrobenzene-d5 (Surr)
94
62-115
Phenol-d5 (Surr)
95
52-107
Terphenyl-04 (Surr)
110
44-116
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 316950
%Rec.
Unit
D %Rea
Limits
rnq1L
86
54 - 1 OO
mg/L
108
56-100
mglL
87
42-100
mg/L
84
60- 101
mg/L
91
62-106
mg/L
74
37-100
mg/L
123
50-103
mg/L
95
59-104
mg/L
90
5B - 1113
mg/L
40
18-100
rng/L
112
54-119
Eurofins TestAmerica, Pittsburgh
Page 14 of 30
6/4/2020

QC Sample Results
Client: Bio-Nornics Services., Inc, Job ID: 180-106162-1
Project/Site: Lenoir WTI"
Method: EPA 8270E - Sernivolatile Organic Compounds (GCIMS) ed) (Conti nui
- -- - ------------ - . ........
Lab Sample ID: LCSD 180-316950/3-A
Matrix: Solid
Analysis Batch: 317153
Analyte
4-45-Trichlorophenol
2,45-Trichlorophenol
2,4-Dinitratoluene
2-Methylphenol
Methylphenol, 3 & 4
Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
LCSD LCSD
Surrogate
%Recovery Qualifier
2,-4—,6-Td9Fomopheno1 (Surr)
- Y8
2-Fluorobiphanyl
95
2-Fluorophenot (Surr)
102
Nitrobenzene-d5 (Surr)
88
Phenol-0 (Surr)
92
Terphenyl-d14 (Surr)
102
Lab Sample ID: LB 180-316683/1-D
Matrix: Solid
Analysis Batch: 317153
Spike
Added
LCSD LCSD
Result Qualifier
0.2,56
0.2131
0,250
0.2507
0.250
0,2072
0.250
0.1843
0,500
0.4245
0.250
0.1782
0,250
0.2813
0.250
0,2245
0.250
0.2142
0.,250
0.09624 J
0.250
0,2758
Analyte
LB LB
Result Qualifier
2,4,5-Trichlorop,henol
ND
2,4,6-Trichlorophenol
KID
2,4-Dinitrotoluene
ND
2-Methylphenol
ND
Methylphenol, 3 & 4
NO
Hexachlorobenzene
ND
Hexachlorobutadiene
ND
Hexachloroethane
ND
Nitrobenzene
ND
Pentachlorophenol
ND
Pyridine
ND
LB LB
Surrogate
%Recovery Qualifier
Z 4,6- Tribro mophenol (Surr)
67
2-Fluorobiphenyl
69
2-Fluorophenol (5urr)
72
Nitrobenzano-d5 (Surr)
64
Phenobd5 (Surr)
65
Terphenyl-d14 (Surr)
70
Limits
24-113
55-107
60-108
62-115
52'- 107
44-116
Client Sample ID. Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 316950
%Rec, RPD
Unit
D %Rec
Limits RPD Limit
..... .....
mg/L
85
54-100 0 16
mq1L
100
56 - 100 a 15
mg/L
83
42-100 5 17
mg/L
74
60-101 13 15
mg1L
85
62- I06 7 15
mg/L
71
37-100 3 115
mg/L
113
50-103 9 15
mg/L
90
59-104 6 16
mg/L
86
5,8-113 4 15
mg/L
38
18-100 5 16
mg/L
110
54-119 1 16
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch: 316950
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
0.0500
mg/L
05129120 15:00
06102/20 10:06
1
0.0500
mg/L
05/29/20 15:00
06102120 10:06
1
0.0500
mg/L
05129/20 15:00
06102120 10:06
1
0.0500
mg/L
05/29120 15M
06/02/20 10:06
1
0.0500
mg/L
05/29/20 15:00
06/02/20 10:06
1
0.0500
mg/L
05/29120 15:00
06/02/20 10:06
1
0.0500
mg/L
05129120 15:00
06102/20 10:06
1
0.0500
rnglL
05129120 15:00,
06/02/20 10:06
1
0.0500
mg/L
05129/20 15:00
06/02/20 10:06
1
0.250
mq/L
05/29/20 15:00
06102/20 10:06
1
0.100
mg/L
05129120 15:00
06102120 10:06
1
Limits
Prepared
Analyzed
Dil Fac
24:- 113
05129-12016,U6
6610 2/2 110 06
1
55-107
05129120 15M
06102120 10:06
1
60-108
05129120 15:00
06/02'20 10:06
-06
1
62-115
05129120 15:00
06102/20 10:06
1
52-107
05/29120, 15:00
06/02/20 10:06
1
44-116
05129120 15:00
06102120 10:06
1
Eurofins TestArnerica, Pittsburgh
Page 15 of 30 6/4/2020

QC Sample Results
Client: Bic-Nornics Services., Inc. Job ID: 180-106162-1
Project/Site: Lenoir WTP
in M ww �N- I �---
nochlorine Pesticides (G
Lab Sample ID: MB 180-316951/1-A
Matrix: Solid
Analysis Batch: 317106
Analyte
MB MB
Result Qualifier
Chlordane (technicM)
ND
Endrin
ND
gamma-1314C (Lindane)
ND
Heptachlor
ND
Heptachlor epoxide
ND
Methoxychlor
ND
Toxaphene
ND
MS MB
Surrogate %Recovery Qualifier
DCB'DecachloroSiphenyl (Surr) 111
DCB Decachlorobiphenyl (Sun) 106
Tetrachldro-m-xylene 101
Tetrachloro-m-xylene 116
Lab Sample ID: LCS 180-31695112-A
Matrix: Solid
Analysis Batch: 317106
Analyte
E —nd r in
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
Methoxychlor
RL
0,00500
0.000500
0.000500
0,000500
0.000500
0,000500
0.0400
Limits
58-115
58-115
43-118
43'- 118
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 316951
MDL Unit
D Prepared
Analyzed
Dil Fac
iiig—/L
— b75i
06101120 18:06
—i
mg/L
05/29/20 15:00
06/01/20 18:06
1
mg/L
05129/20 15:00
06101/20 18:06
1
mg/L
05129120 1&00
06/01120 18,:06
1
mg1L
05/29120 15:00
06/01120 18:06
1
mg/L
05/29120 15:00
06/01/20 18:06
1
mg/L
05/29120 15:00
06/01/20 18:06
1
Spike
LCS LCS
Added'
Result Qualifier
0-0100
0.01056
0.0100
0.01113
0.0100
0.01099
0.0100
0.01155
0.0100
0.009171
LCS LCS
Surrogate
!Recovery Qualifier
Limits
DCB Decachlorobiphenyl (Surr)
119 X
58-115
DCB Decachlorobiphenyl (Surr)
109
58-115
Tetrachloro-m-xylene
104
43-118
Tetrachloro-m-xylena
121 X
43-118
Lab Sample ID: LCSD 180-31695113-A
Matrix: Solid
Analysis Batch: 317106
Spike
LCSD LCSD
Analyte
Added
Result Qualifier
Endrin
m 01.0100
0.01026
gamma-BHC (Lindane)
0,01100
0.01127
Heptachlor
0.0100
0.0,1117
Heptachlor epoxide
MIN
0,01157
Methoxychlor
0,0100
0.008714
LCSD LCSD
Surrogate
%Recovery Qualifier
Limits
DCB Decachlorobiphenyl (Surr)
110
58-115
DCB Decachlorobiphenyl (Surr)
102
58-115
Tetrachloro-m-xylene
104
43-118
Tetrachloro-m-xylene
116
43-118
Prepared Analyzed Dil Fac
J
05129120 15:00
06101120 18:06
1
05129120 15:00
06101120 18:06
1
05/29/20 15:00
06101120 IS.-06
1
05129120 15:00
06101120 18:06
1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 316951
%Rec.
Unit
D %Rec
Limits
i�-dT[ ----
— —106
37-150
mg/L
111
50-137
mg/L
110
49-135
mg/L
116
49-133
mg/L
92
45-150
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch,: 316951
%Rec. RPID
Unit
D %Rec
Limits RPD Limit
mg/L
103
37-150 3 15
mg/L
113
50-137 1 18
mg/L
112
49-135 2 22
mg/L
116
49-133 0 15
mg/L
87
45-150 5 17
Eurofins TestAmerica, Pittsburgh
Page 16 of 30 6/4/2020

QC Sample Results
Client: Blo-Nornics Services,, Inc.
Project/Site., Lenoir WTP
Method: EPA 8081 B - Organochlorine Pesticides (GC) (Continued)
- - - - --------- -- --
Lab Sample ID: LB 180-316683/1-E
Matrix: Solid
Analysis Batch: 317106
1-8 LB
Analyte
Result Qualifier
RL
Chlordane (technical)
NO
0.00500
E�ndrin
NO
0.000500
gamma-BHC (Linclane)
NO
0M0500
Heptachlor
NO
0.000500
Heptachlor epoxide
NO
0.000500
Methoxychlor
ND
0.000500
Toxaphene
NiO
0.0400
LB LS
Surrogate %Recovery Qualifier
Limits
DCB Decachlorobiphenyt (Surr)
jig
1-15
DCB Decachlorobiphenyl (Surr)
110
58-115
Tetrachloro-m-xylene
106
43-118
Tetrachloro-m-xylene
fis
43-118
Job ID: 180-106162-1
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch: 316951
MDL Unit
D Prepared
Analyzed
Oil Fac
mq1L
05129/20 15:00
06/01/20 1&52
1
mg/L
05129120 15:00
06101/20 1&52
1
mq/L
05129120 15:00
06/01/20'18:52
1
mg/L
05/29120 15M
06/01120 18:52
1
mgl/L
05/29120 15:00
06101/20 18:52
1
mg/L
05/29/20 15M
06/01/20 18:52
1
mg/L
05/29/20 15:00
06/01120 18:52
1
Prepared
Analyzed
flit Fac
b3; �912O 15, �OO
O(VO-1120M52
05129120 15:00
06101120 18:52
05129120 15:00
06101120 18:52
05129120 15:00
06101120 18:52
1
Method: EPA 8082A - Polychlorinated Biphenyls (PCBs) Gas Chromatography
- - — -- ------ . . . ............ . . ...... . . ... ..
Lab Sample ID: MIS 180-31660311-A Client Sample ID: Method Blank
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 316711 Prep Batch: 316603
MB MB
Analyte
Result Qualifier
PCB-1016
NO
PCB-1221
NO
PCB-1232
N'D
PCB-1242
NO
PCB-1248
NO
PCB-1 254
N D
PCB-1260
ND
MB MB
Surrogate %Recovery Qualifier
Tetrachloro-m-xylene (Surr) 100
Tetrachloro-m-xylene (Surr) 97
DCB Decachlorobiphenyl (Surr) 96
DC8 Decachlorobiphenyl (Surf) 94
Lab Sample ID: LCS 180-316603/2-A
Matrix: Solid
Analysis Batch: 316711
Analyte
PCB-1 0 16
PCB-1260
RL
MDL Unit
D Prepared
Analyzed
Oil Fac
16.7
ug/Kg
05127/20 10:01
05[28/20 16:22
-1
16.7
ug/Kg
05/27/20 10:01
05128/20 16:22
1
16.7
ug/Kg
05127/20 10,01
05/28/20 16:22
1
16.7
uglKg
05127120 10:01
05/28/20 16:22
1
16.7
uq/Kg
05/27120 10:01
05128120 16:22
1
163
ug/Kg
05/27120 10:01
05/28/20 1:6:22
1
16.7
tag/Kg
05/27120 10V
05128120 1612
1
Limits
Prepared
Analyzed
Dil Fac
51-112
05/27/20 10:01
b5/28)20 -16:22
-1
51-112
05127120 10:01
OWMO f6.,22
1
61-132
05127120 10:01
05/29/20 16:22
1
61-132
05127120 10:01
05128120 15:22
1
Spike LCS LCS
Added Result Qualifier
1330 1224
1330 1162
LCS LCS
Surrogate
%Recovery Qualifier
Limits
Tetrachloro-m-xylene (burr)
101
51-112
Tetrachloro-m-xylene (Surr)
96
51-112
DCB Decachlorobiphenyl (Surr)
98
61-132
DCB Decachlorobiphenyl (Surr)
97
61-132
Client Sample ID, Lab Control Sample
Prep Type: Total/NA
Prep Batch: 316603
%Rec.
Unit D %Rec Limits
4/1<9 92 48 -122
ug/Kg 87 47-127
Eurofins TestAmerica, Pittsburgh
Page 17 of 30
6/4/2020

QC Sample Results
Client:, Bio-Nornics Services., Inc,
Project/Site: Lenoir WTP
. ... ......
Method: EPA 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
.... . ....... . ..... .. . . ........... -
Job ID: 180-106162-1
Lab Sample ID: 180-106162-1 MS
Client Sample ID: LENOIR WTP
Matrix: Sludge
Prep Type: Total/NA
Analysis Batch: 316711
Prep Batch: 316603
Sample Sample
Spike
MS MS
%Rec.
Analyte Result Qualifier
Added
Result Qualifier Unit
D %Rec Limits
PCB -1016 mITm1320
1103 ug/Kg
84 48-122
PCB-1260 NO
1320
1017 ug/Kg
77 47-127
Surrogate,
MS MS
%Recovery Qualifier
Te-t—rwhl.-.-.y1.n.
85
Talrachloro-m-xylene (Surr)
83
DCB Decachlorobiphenyl (Surr)
79
DCB Decachlorobiphenyl (Surr)
80
Lab Sample ID: 180.106162-1 MSD
Matrix: Sludge
Analysis Batch: 316711
Sample Sample
Analyte
Result Qualifier
FYC B --10 1'6-
—NO
PCB-1260
NO
Limits
51-112
51-112
61-132
61-132
Spike
MSD MSD
Added
Result Qualifier
1310
1056
1310
1022
MSD MSD
Surrogate
%Recovery Qualifier
Limits
Tetrachloro-m-xylene (Surr)
82
51.112
Tatrachloro-m-xylene (Surr)
80
51-112
DCB Decachlorobiphenyl (Surr)
84
61-132
DCB Decachlorobiphenyl (Surr)
83
61-132
Method: EPA 8151A - Herbicides (GC)
Lab Sample ID: MB 180.316961111-A
Matrix: Solid
Analysis Batch: 317040
MB MB
Analyte Result Qualifier
2.4-D NO
Silvex (2,4,5-TP) NO
MB MB
Surrogate %Recovery Qualifier
2,4-Dichlorophenylacetic acid 75 p
2,4-Dichlorophenylacetic acid 114
Lab Sample ID: LCS 180-316961/2-A
Matrix: Solid
Analysis Batch: 317040
Client Sample ID. LENOIR WTP
Prep Type: Total/NA
Prep Batch: 316603
%Rec. RPD
Unit D %Rec Limits RPD Limit
ug/Kg 81 48-122 4 40
ug/Kg 78 47-127 0 40
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 316961
RL MD: L Unit D Prepared Analyzed oil Fac
0.0400 mg/L 0512!9/20 17:20 06/01/20 19:37 20
0.0100 mg/L 05129/20 1T20 06/01/20 19:37 20
Limits Prepared Analyzed Dil Fac
23 -T22 05129120 17,-20 06J011120 19:37 20
23-122 05129120 17:20 06101120 19,37 20
Analyte Spike LCS LCS
Added Result Qualifier
2,4-D 0.200 0.04237
SiNex (2,4,5-TP) 0.0500 0.01989
LCS LCS
Surrogate %Recovery Qualifier Limits
2,4-Dichlorophenylacefic acid 36 ­0 --12f
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch. 316961
%Rec.
Unit D %Roe Limits
mg/L 21 1 §-- 1"2-7
mg/L 40 24-128
Eurofins TestArnerica, Pittsburgh,
Page 18 of 30
6/4/2020

QC Sample Results
Client: Bio-Nomics Services., Inc,
Project/Site: Lenoir WTP
Job ID: 180-106162-1
Method: EPA 8151 A - Herbicides (GC) (Contin
Lab Sample ID: LCS 180-316961/2-A
Matrix: Solid
Analysis Batch, 317040
LCS LCS
Surrogate %Recovery Qualifier
2, 4-DlchlonmphenylaoRicacid -47
Lab Sample ID: LCSD 180-316961/3-A
Matrix: Solid
Analysis Batch: 317040
Analyte
T4--D-
Silvex (2,4,5-TP)
LCSD LCSD
Surrogate %Recovery Qualifier
2,4-Dichlorophenylacetic acid 37
2,4-Dichlorophenylacefic acid 48
Lab Sample ID: LB 180-316683/1-F
Matrix, Solid
Analysis Batch: 317040
Client Sample ID: Lab, Control Sample
Prep Type: Total/NA
Prep Batch: 316961
Limits
---2�3 - 1-22
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 316961
Spike LCSD LCSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
0166 0-04372 -- mg/L —22 —1-9 12-7 —3 —35
0.0500 0.02054 mg/L 41 24-128 3 35
Limits
23-122
23-122
LB LB
Analyte Result Qualifier RL
2,4-D NO 0.0400
i Silvex (2,4,5-TP) NO 0.0100
LB LS
Surrogate %Recovery Qualifier Limits
2,-4-Dichlorophenylacefic acid 25 23-122
2,4-Dichlorophenylacetic acid 33 23-122
Method: EPA 601 OD - Metals (IC
Lab Sample ID: MB 180-31694111-A
Matrix: Solid
Analysis Batch: 317142
MB MB
i Analyte Result Qualifier
Silver
NO
Barium
NO
Cadmium
ND
Chromium
NO
Lead
NO
Selenium
NO
Arsenic
NO A
Lab Sample ID,: LCS 180.316941/2-A
Matrix: Solid
Analysis Batch: 317142
Analyte
Silver
Barium
RL
0.0500
0.200
0.0500
0,0500
0.0500
0.0500
0.0500
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch: 316961
MDL Unit D Prepared Analyzed Oil Fac
mg/L 05/29120 17:20 06101/20 13:19
mg/L 05129120 17!20 06101/20 13:19 20
Prepared Analyzed Dil Fac
0&-912017:20 11CI0II-20 i3-79 20
05129120 17:20 06101120 13c19 20
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 316941
MDL Unit
D Prepared
Analyzed
Dil Fac
W9/L
,21
0-6-/01/2010,46
--Y
mg/L
05/29120 1521
06/01120 10:46
1
mg/L
05/29120 15:21
06/01120 10:46
1
mg/L
05/29120 15:21
05/01/20 10:46
1
mg/L
05/29120 15-21
06/01120 10:46
1
mg/L
05/29/20 15:21
06101/20 10:46
1
mq/L
05/29/20 M21
06101/20 10:46
1
Spike LCS LCS
Added Result Qualifier
0.250 0,2457
1.00 0.9948
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 316941
%Rec.
Unit D %Reo Limits
mg/L 99 80-120
Eurofins TestAmerica, Pittsburgh,
Page 19 of 30
6/4/2020

Client: Bio-Nornics Services., Inc.
Project/Site: Lenoir WTP
Method: EPA 6-010D -Mitalls HC
Lab Sample ID. LCS 180-316941/2-A
Matrix: Solid
Analysis Batch: 317142
Analyte
Cadmium
Chromium
Lead
Selenium
Arsenic
Lab Sample ID: LB 180-316683/1-C
Matrix: Solid
Analysis Batch: 317142
QC Sample Results
Continued)
Spike
Added
--6,500
0.500
0.500
IM
1.00
LB LB
Analyte
Result Qualifier
RL
Silver
NO
0.500
Barium
NO
2.00
i Cadmium
NO
0.500
Chromium
NO
0.500
Lead
NO
0.500
Selenium
NO
0.500
Arsenic
NO A
0.500
Job ID: 180-106162-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 316941
LCS LCS
%Rec.
Result Qualifier
unit
D %Roe
Limits
0.49131
iii—g/L
99
—80--f�o--
0.4918
mg/L
98
80-120
0,4933
mq1L
99
80-120
0,9703
mg/L
97
80-120
1.034 A
mg/L
103
80-120
Client Sample ID:,Method Blank
Prep Type: TCLP
Prep Batch: 316941
MDL Unit
D Prepared
Analyzed
Oil Fac
mg/L
05129/20 15:21
06/01120 10:56
1
mg/L
05129120 15:21
06/01/20 M56
1
mg/L
05129120 15:21
06/01/20 10:56
1
mg/L
05129/20 15:21
06101/20 10:56
1
mg/L
05/29120 15:211
06/01120 10:56
1
mg/L
05129120 15.21
06/01/20 10:56
1
mg]L
05129120 1521
06/01/20 10:56
1
Lai) Sample ID: 1180-106201 -A-1 -L MS
Client Sample ID: Matrix Spike
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 317142
Prep Batch: 316941
Sample Sample
Spike
MS MS
%Rec.
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
Silver
NO F1
1.00
NO F1
mg/L
25
75-125
Barium
3.03 F1 F2
50.0
27.10 F1
mg/L
48
75-125
Cadmium
ND
1.00
0.9592
mg/L
96
75-125
Chromium
ND
5,00
4.688
mg/L
94
75-125
Lead
ND F1 F2
5.00
3,606 F1
mg/L
72
75-125
Selenium
NO
1.00
0.8567
mg/L
82
75-125
Arsenic
NO A
5.00
4.920 A
mg/L
98
75-125
Lab Sample ID: 180-106201-A-1-M
MSD
Client Sample ID: Matrix Spike Duplicate
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 317142
Prep Batch: 316941
Sample Sample
Spike
MSD MSD
%Rec. RPD
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits RPD Limit
Silver
NO F1
1.00
NO F1
mg/L
28
75-125 10 20
Barium
3.03 F1 F2
50.0
18A0, F1 F2
mg/L
31
75-125 38 20
Cadmium
ND
1.00
0,9834
mg/L
98
75-125 2 20
Chromium
ND
5.00
4,836
mg1L
97
75-125 3 20
Lead
ND F1 F2
5.00
2.630 F1 F2
mg/L
53
75-125 31 20
Selenium
ND
1.00
0.8581
mg/L
82
75-125 0 20
Arsenic
NO A
5.00
5.053 A
mg/L
101
75-125 3 20
Eurofins TestArnerica, Pittsburgh
Page 20 of 30 6/4/2020

QC Sample Results
Client; Bier-Nomics Services., Inc. Job ID: 180-106162-1
Project/Site: Lenoir WTP
Method: EPA- 7470A_-_ Mercury (dV-' A A)
i Lab Sample ID. MB 180-316915/1-A
Matrix: Solid
Analysis Batch: 316982
ME ME
Analyte Result Qualifier RL
Mercury NO 0. 0 d �2 0-0
Lab Sample ID: LCS 180-31691512-A
Matrix: Solid
Analysis Batch: 316982
Client Sample ID; Method Blank
Prep Type: Total/NA
Prep Batch: 316915
MDL Unit D Prepared Analyzed Oil Fac
mg/L — b5l_29/201510 05/29/20 18:31 1 ..
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 316915
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec Limits
Mercury ----600250
6-.-002498
mg/L
too 0_120
Lab Sample ID. LB 180-316683t1-B
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 316982,
Prep Batch: 316915
LB LB
Analyte Result Qualifier
RL MDL Unit
0 Prepared Analyzed Dil'Fac
Mercury NO —
--6—,000200 mg/L
-6-5/2912015.-10 05129/2018:33 1
Lab Sample ID: 180-106201-A-1-1 M'S
Client Sample ID: Matrix Spike
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 316982
Prep Batch: 316915
Sample Sample,
Spike
IVIS MS
%Rec.
Analyte Result Qualifier
Added
Result Qualifier
Unit
D %Rec Limits
M—erMercuryNO —6-00500
0.004666
g_/L
m­
_93 75-125
Lab Sample ID: 180-106201-A-1-J MSD
Client
Sample ID: Matrix Spike Duplicate
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 316982
Prep Batch: 316915
Sample Sample
Spike
MSD MSD
%Rae. RPD
Analyte Result Qualifier
Added
Result Qualifier
Unit
D %Rec Limits RPD Limit
Mercury ND
0,0050
.004784
mg/L
96 75-125 2 20
Method: EPA 1020E - Ignitability, Small Scale Closed -Cup Method
Lab Sample ID: 680-181927-A-6 DU
Matrix: Solid
Analysis Batch: 316583
Sample Sample
Analyte Result Qualifier
fanitability > . 140
Method. EPA 9014 - Cyanide
Lab Sample ID: MB 180-317066/4-A
Matrix: Solid
Analysis Batch: 317144
ME ME
Analyte Result Qualifier RL
Cyanide, Total NO 0.506
Client Sample ID: Duplicate
Prep Type: Total/NA
DU DU RPD
Result Qualifier Unit D RPD Limit
ffe_qr,,, F NC-20
. . . . .........
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 317066
MDL Unit D Prepared Analyzed' Oil Fac
mg/Kg 06101120 12:00 06101/20 13AB 1
Eurofins TestAmerica, Pittsburgh
Page 21 of 30 6/4/2020

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Lenoir WTP
Method: EPA 9014 - Cvanide
ontinued
I Lab Sample ID: HLCS 180-317066/2-A
Matrix: Solid
Analysis Batch: 317144
Analyte
Cyanide, Total
Lab Sample ID: LCS 180-317066/3-A
Matrix: Solid
Analysis Batch: 317144
Analyte
t—yaKide-' --T-otal
I Lab Sample ID: LLCS 180-317066/1 -A
Matrix: Solid
Analysis Batch. 317144,
Analyte
Cyanide, Total
Lab Sample ID: 180-105925-B-1-W MS
Matrix: Solid
Analysis Batch: 317144
Job ID: 180-106162-1
Client Sample ID: Lab Control Sample
Prep Type: Total/N'A
Prep Batch: 317066
Spike HLCS HLCS %Rec.
Added Result Qualifier Unit D %Rec Limits
i�-g—/Kg —100 1-10
0.250 0,2504
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 317066
Spike
LCS LCS
%Rec.
Added
Result Qualifier
Unit D %Rec Limits
—
23
—2U 1-3 —
mg/Kg 25-150
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 317066
Spike
LLCS LLCS
%Rec.
Added
Result Qualifier
Unit D %Rec Limits
0.0500
0.05220
mg/Kg 104 90-110
Client Sample ID: Matrix Spike
Prep Type: Total/NA
Prep Batch. 317066
Sample Sample
Spike
MS MS
%Rec.
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
Cyanide, Total
ND
4.00
3.468
mg/Kg
87
75-125
Lab Sample ID: 180-105925-B-1
-X MSD
Client Sample ID: Matrix Spike Duplicate
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 317144
Prep Batch: 317066
Sample Sample
Spike
MSD MSD
%Rec. RPD
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits RPD Limit
Cyanide, Total
ND
3.92
3,206
mg/Kg
82
75-125 8 20
Method: EPA 9034 - Sulfide, Acid soluble and Insoluble (Titrimetric)
Lab Sample ID: MB 180-316574/1 -A Client Sample ID: Method Blank
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 316625 Prep Batch: 316574
MB M13
Analyte Result Qualifier
Sulfide ND
Lab Sample ID: LCS 180-316574/2-A
Matrix: Solid
Analysis Batch: 316625
Analyte
Sulfide
RL MDL Unit D Prepared Analyzed Dil Far
30.0 mg/Kg 05/27/20 09:00 05127/20 12:00 1
Client Sample ID,: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 316574,
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
f-612- — — ---- -­— — -- 172 mg/Kg — — 94 85-115
Eurofins, TestArnerica, Pittsburgh
Page 22 of 30
6/412020

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Lenoir WTP
Method: EPA 9034 - Sulfide, Acid soluble and Insoluble
-- — -- -------
Lab Sample ID: 180-105766-A-1-D MS
Matrix: Solid
Analysis Batch: 316625
Sample Sample
Analyte Result Qualiifier
Sulfide ND
Lab Sample ID: 180-105766-A-1-E MSD
Matrix: Solid
Analysis Batch: 316625
Sample Sample
Analyte Result Qualifier
Sulfide ND
Method' —EJA 9045D --pH------
I'Lab Sample ID: LCS 180-316790/1
Matrix: Solid
Analysis Batch., 316790
Analyte
pH
Lab Sample ID: 180-1 05906-A-1 DU
Matrix: Solid
Analysis Batch: 316790
Sample Sample
Analyte Result Qualifier
pH 8.6
Job 113: 180-106162-1
trimetric) (Continued)
..........
Client Sample ID,: Matrix Spike
Prep Type: Total,/NA
Prep Batch: 316574
Spike Ms MS %Rec,
Added Result Qualifier Unit D %Rec Limits
171 146.3 mg/Kg 85 75-125
Client Sample ID: Matrix Spike Duplicate
Prep Type: Total/NA
Prep Batch,. 316574
Spike MSD MSD %Ree. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
174 147.0 mg/Kg 85 75-125 1 20
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec,
Added Result Qualifier Unit D %Rec Limits
7.00 TO SU 100 99-101
Client Sample ID: Duplicate
Prep Type: Total/NA
DU DU RPD
Result Qualifier Unit 0 RPD Limit
-
8.6 -- §U— — — — —0."3 '---2
Eurofins TestAmerica, Pittsburgh
Page 23 of 30
6/4/2020

QC Association Summary
Client: Bio-Nordics Services,, Inc.
Project/Site: Lenoir WTP
dbM" S- V-O-A-
Leach Batch: 316691
Job ID: 180-106162-1
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
�F8-0.106162-1
LENOIR WTP
TCLP
Sludge
EPA 1311
LB 1180-31669111-A
Method Blank
TCLP
Solid
EPA 1311
180-105839-A-13-B MS
Matrix Spike
TCLP
Solid
EPA 1311
1180-105839-A-13-CMSD
Matrix Spike Duplicate
TCLP
Solid
EPA 1311
Analysis Batch: 316868
I Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
10,6162-1
LENOIR WTP
TCLP
Sludge
EPA 8260D
316691
LB, 180-31669111-A
Method Blank
TCLP
Solid
EPA 8260D
316691:
LCS 180-31686813
Lab Control Sample
Total/NA
Solid
EPA 82601)
180-105839-A-1 3-13 MS
Matrix Spike
TCLP
Solid
EPA 82600,
316691
180-105839-A-1 3-C MSD
Matrix Spike Duplicate
TCLP
Solid
EPA 8260D
316691
GCIMS Semi VOA
Leach Batch: 316683
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
1 180-106162-1
LENOIR WrP .
...... TCLP
Sludge
EPA 1311
LB 18D-316683/1-E)
Method Blank
TCLP
Solid
EPA 1311
Prep Batch: 316950
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
180-106162-1
LENOIR WTP
TCLP
Sludge
3510C 316683
LB 180-316683/1-D
Method Blank
TCLP
Solid
3510C 3166,83
MB 180-31695011 -A
Method Blank
Total/NA
Solid
3510C
LCS 180-31695012-A
Lab Control Sample
TotalINA
Solid
3510C
LCSD 180-316950/3-A
Lab Control Sample Dup
Total/NA
Solid
3510C
Analysis Batch: 317153
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-106162-1
LENOIR WTP
TCLP
Sludge
EPA 8270E
— —
316950
LB 180-316683/1-D
Method Blank
TCLP
Solid
EPA 8270E
316950
MB, 180-31695011-A
Method Blank
Total!/NA
Solid
EPA 8270E
316950
LCS 180-316950/2-A
Lab Control Sample
Total/NA
Solid
EPA 8270E
316950
LCSD 180-316950/3-A
Lab Control Sample Dup
Total/NA
Solid
EPA 8270E
316950
GC Semi VOA
Prep Batch: 316603
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
106162-1
LENOIR WTP
Total/NA
Sludge
3541
MB 180-316603/1-A
Method Blank
Total/NA
Solid
3541
LCS 180-316603/2-A
Lab Control Sample
Total/NA
Solid
3541
180-106162-1 MS
LENOIR WTP
Total/NA
Sludge
3541
180-106162-1 MSD
LENOIR WTP
Total/NA
Sludge
3541
Leach Batch: 316683
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
106162-1
[ENCIR WTP
TCLP
Sludge
— EPA 1-311
LB 180-316,68311-E
Method Blank
TCLP
Solid
EPA 1311
LB 180-31668311-F
Method Blank
TCLP
Solid
EPA 1311
Eurofins TestArnerica, Pittsburgh
Page 24 of 30 6/4/2020

QC Association Summary
Client: Bio-Nomics Services., Inc.
Project/Site: Lenoir WTP
GCSemi V6A
Job ID: 180-106162-1
Analysis Batch: 316711
Lab Sample ID
Client Sample ID
Prop Type
Matrix
Method
Prep Batch
-106162-1
E—ENOlR VVTP
Total/NA
Sludge
EPA 8082A
316603
MS 180-316603/1-A
Method Blank
Total/NA
Solid
EPA 8082A
316603
LCS 180-316603/2-A
Lab Control Sample
Total/NA
Solid
EPA 8082A
316603
180-106162-1 MS
LENOIR WTP
Total/NA
Sludge
EPA 8082A
316603
180-106162-1 MSD
LENOIR VVTP
TotalINA
Sludge
EPA 8082A
316603
Prep Batch: 316951
-Lab
Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prop Batch
106162-1
1 -E N-61 -1 —W—T P
TCLP
Sludge -—
3510C
316683
LB 180-316683/1-E
Method Blank
TCLP
Solid
3510C
316683
MB 180.31695111-A
Method Blank
TotaUNA
Solid
3510C
LCS 180-316951/2-A
Lab Control Sample
Total/NA
Solid'
3510C
LCSD 180-316951/3-A
Lab Control Sample Dup
Total/NA
Solid
3510C
Prep Batch: 316961
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180.106162-1
LENOIR WTP
TCLP
Sludge
-615 —1A
316683
LB 180-316683/1-F
Method Blank
TCLP
Solid
8151'A
3,16683
MB 180-316961/1-A
Method Blank
Total/NA
Solid
8151A
LCS 180-316961/2-A
Lab Control Sample
Total/NA
Solid
8151A
LCSD 180-316961/3-A
Lab Control Sample Duip
Total/NA
Solid
8151A
Analysis Batch: 317040
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch,
180-106162-1
LENOIR VVTP
TCLP
Sludge
EPA 8151A
316961
LB 180-31668311-F
Method Blank
TCLP
Solid
EPA 8151A
316961
MB 180-31696�1/1-A
Method Blank
Total/NA
Solid
EPA 8151A
316961
LCS 180-316961/2-A
Lab Control Sample
Total/NA
Solid
EPA 8151A
316961
LCSD 180-316961/3-A
Lab Control Sample Dup
Total/NA
Solid
EPA 8151A
316961
Analysis Batch: 317106
Lab Sample ID
-i-80-1061162-1
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
LENOIR P
TCLP
Sludge
— E—PA8081B
316951
LB 180-31668311-E
Method Blank
TCLP
Solid
EPA 80818
316951
MB 180-316951/1-A
Method Blank
Tota:I/NA
Solid
EPA 8081 B
316951
LCS 180-316951/2-A
Lab Control Sample
Total/NA
Solid
EPA 8081 B
316951
LCSD 180-3169,51/3-A
Lab Control Sample Dup
Total/NA
Solid
EPA 8081 B
316951
Metals
Leach Batch: 316683
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
106162-1
LENOIR WTP
TCLP
sludge
9PA1 311
LB 180-316683/1-B
Method Blank
TCLP
Solid
EPA 1311
LB 180-31668311-C
Method Blank
TCLP
Solid
EPA 1311
180-106201-A-1-1 MS
Matrix Spike
TCLP
Solid
EPA 1311
180-106201-A-1-J MSD
Matrix Spike Duplicate
TCLP
Solid
EPA 1311
180-10620 1 -A-1 -L MS
Matrix Spike
TCLP
Solid
EPA 1311
180-106201-A-1-M MSD
Matrix Spike Duplicate
TCLP
Solid
EPA 1311
Eurofins TestAmerica, Pittsburgh
Page 25 of 30 6/4/2020

QC Association Summary
Client: Bio-Nornics Services., Inc. Job ID: 180-106162-1
Proj:ect/Site: Lenoir WTP
Metals
Prep Batch: 316915
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
f R-1 06162-1
LENOIR WTP
TCLP
Sl—udge-
-7470A
316683
LB 180-31668311-B
Method Blank
TCLP
Solid
7470A
316683
MB 180-31691511-A
Method Blank
Total/NA
Solid
7470A
LCS 180-316915/2-A
Lab Control Sample
Total/NA
Solid
7470A
180-106201-A-1-1 MS
Matrix Spike
TCLP
Solid
7470A
316683
180-106201-A-1-J MSD
Matrix Spike Duplicate
TCLP
Solid
7470A
316683
Prep Batch: 31'6941
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-106162-1
LENOIR WTP
TCLP
Sludge
M I -OA
316683
LB 180-316683/1-C
Method Blank
TCLP
Solid
3010A
316683
MB 180-316941i1-A
Method Blank
Total/NA
Solid
3010A
LCS 180-316941/2-A
Lab Control Sample
Total/NA
Solid
3010A
1130-1 O6201 -A-1 -L MS
Matrix Spike
TCLP
Solid
3010A
316683
180-106201-A-1-M'MSD
Matrix Spike Duplicate
TCLP
Solid
301 DA
316683
Analysis Batch: 316982
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-106162-1
OIR WTP
TCLP
Sludge
EPA 7470-A
316915
LB 180-316683/1-B
Method Blank
TCLP
Solid
EPA 7470A
316915
MB 180-316915/1-A
Method Blank
Total/N'A
Solid
EPA 7470A
316915
LCS 180-316915/2-A
Lab Control Sample
Total/NA
Solid
EPA 7470A
316915
180-106201-A-1-1 MS
Matrix Spike
TCLP
Solid
EPA 7470A
316915
180-106201-A-1-J MSD
Matrix spike Duplicate
TCLP
Solid
EPA 7470A
316915
Analysis Batch: 317142
Lab Sample ID -
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-1106162-1
LENOIR WTP
TCLP
Sludge
EPA 601 OD
3169,41
LB 180-316683/1-C
Method Blank
TCLP
Solid
EPA 6010D
316941
MB 180-31694111-A
Method Blank
Total/NA
Solid
EPA 6010D
316941
LCS 180-316941/2-A
Lab Control Sample
TotaUNA
Solid
EPA 6010D
316941
180-106201-A-1-L MS
Matrix Spike
TCLP
Solid
EPA 6010D
316941
180-106201-A-1-M MSD
Matrix Spike Duplicate
TCLP
Solid
EPA 6010D
316941
General Che
Prep Batch:: 316574
Lab Sample ID
-1"80-106162-1
Client Sample ID
Prep Type
Matrix
Method Prep Batch
UE-NOIR WfP
Total/NA
Sludge
90308
MB 180-3165,7411-A
Method Blank
Total/NA
Solid
9030E
LCS 180-316574/2-A
Lab Control Sample
Total/NA
Solid
90308
180- 105766-A-1-D MS
Matrix Spike
Total/NA
Solid
9030E
180-105766-A-1-E MSD
Matrix Spike Duplicate
Total/NA
Solid
9030B
Analysis Batch; 316583
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
180-106162-1 -UE-N-0IR\AffP m Total/NA Sludge EPA 1020E
680-181927-A-6 DU Duplicate Total/NA Solid EPA 10206
Eurofins TestArnerica, Pittsburgh
Page 26 of 30 1 6/4/2020

QC Association Summary
Client: Bio-Nomics Services., Inc. Job ID: 180-106162-1
Project/Site: Lenoir WTP
General Chemist r ry ..... . .... - .. . .......
Analysis Batch: 316625
Lab Sample ID _
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-106162-1
CE—NO I R VVTP
Total/NA
Sludge
EPA 9034
316574
MB 180-31657411-A
Method Blank
Total/NA
Solid
EPA 9034
316574
LCS 180-31657412-A
Lab Control Sample
Total/NA
Solid
EPA 9034
316574
180-105766-A-1-D MS
Matrix Spike
TotalINA
Solid
EPA 9034
316574
180-105766-A-1-E MSD
Matrix Spike Duplicate
Total/NA
Solid
EPA 9034
316574
Analysis Batch: 316790
Lab Sample ID —
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-1061152-11
LENOtR WTP
Total/NA
Sludge
EPA 9045D
LCS 180-316790/1
Lab Control Sample
Total/NA
Solid
EPA 90451)
180-105906-A-1 DU
Duplicate
Total/NA
Solid
EPA 9045D
Prep Batch: 317066
Lab Sample 10
Client Sample ID
Prep Type
Matrix
Method Prep Batch
106162-1
UE-NOIR WtP
Total/NA
Sludge
9010C
MB 180-317066/4-A
Method Blank
Total/NA
Solid
9010C
HLCS 180-31706612-A
Lab Control Sample
TotalINA
Solid
9010C
LCS 180-31706613-A
Lab Control Sample
Total/NA
Solid
9010C
LLCS 180-317066/1-A
Lab Control Sample
Total/NA
Solid
9010C
1 60-105925-B-1 -W MS
Matrix Spike
Total/NA
Solid
9010C
180-105925-B-1-X MSD
Matrix Spike Duplicate
Total/NA
Solid
9010C
Analysis Batch: 317144
Lab Sample to
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
106162-1
E—E—NOJR WfO---
Total/NA
Sludge
EPA N 14
317066
MB 180-317066/4-A
Method Blank
Total/NA
Solid
EPA 9014
317066
HLCS 130-31706612-A
Lab Control Sample
Total/NA
Solid
EPA 9014
317066
LCS 180-317066/3-A
Lab Control Sample
Total/NA
Solid
EPA 9014
317066
LLCS, 180-31706611 -A
Lab Control Sample
Total/NA
Solid
EPA 9014
317065
180-1 05925-B-1-W MS
Matrix Spike
Total/NA
Solid
EPA 9014
317066
180-105925-B-1-X MSD
Matrix Spike Duplicate
Total/NA
Solid
EPA 9014
317066
Eurofins TestAmerica, Pittsburgh
Page 27 of 30 6/4/2020

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20

Client: Bio-N'omics Services., Inc.
Login Number: 106162
List Number: I
Creator: Watson, Debbie
Question
Login Sample Receipt Checklist
Job Number: 180-106162-1
List Source: Eurofins TestAmerica, Pittsburgh
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact,
True
The cooler or samples do not appear to have been compromised or
True
tampered with,
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible,
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
False
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection clateltimes are provided,
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MSIMSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
Eurofins TestAmerica, Pittsburgh
Page 30 of 30 6/4/2020

BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: August 17, 2020
Lake Rhodhiss WTP Permit No. WQ0039053
33-00 % Solids
SS PH
.Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry "Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
0.664
6,640,000
13.280
Phosphorus
0.189
1'890.000
1780
Potassium
0.162
1,620.000
3.240
PAN (injected)*
0,233
3,869.500
7.739
PAN (surface)*
0,173
3,77T000
7.554
Ammonia Nitrogen
0,120
1,200.000
2.400
Calcium
0.142
1,420.000
2.840
Calcium Carbonate Eq.
5A00
54,000.000
108,000
L
Magnesium,
0211
2,110.000
4.220
Sodium
0.008
75.800
0.152
Sulfur
---
3480.000
6.960
Nitrate N / Nitrite N
---
40.600
omi
Barium
SAR
0.17
Chloride
---
...
Iron
---
...
Ceiling Concen.
(Mg/Kg)
Aluminum
---
11,200,00
22,400
Arsenic
---
8,36
0.017
75
Cadmium
---
0.303
0.001
85
Chromium
82,.700
0,165
--
Copper
---
3730
0.075
4,300
Lead
34.20
0.068
840
Mercury
---
0.0575
0.000
57
Molybdenum
---
1.89
0.004
75
Nickel
---
19.70
0.039
420
Selenium
1.521
0.
Zinc
203.00 1
0.406
7,500::dl
Waypoint# 20-232-0006
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
willcox&mabe
Prepared By: SOIL SOLUTIONS

WayP)201nt,O
A ►
8/27/2020
Bio-Nomic Servics Ine
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 20-232,-0006
Project Description: Lencit-2
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-94010 Fax [phone]
wwwwaypointanalytical,com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 8/19/2020 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and N'ELAC uniless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This, report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 19

(0 7621 Whitepine Road, Richmond, VA 23237
Waypoint. Main 804-743-9401 1 Fax [phone]
ANALYTICAL www.waypoiiitanalytical.com
Sample Summary Table
Report Number: 20-232-0006
Client Project Description: Lencit-2
Lab No
Client Sample ID
Matrix
Date Collected
Date Received Method
Lab ID
73416
1
Solids
08117/2020 06:00
08/19/2020
73416
1
Solids
08/17/2020 06:00
08/19/2020
AOAC 955.01
WP MTN
73416
1
Solids
08117/2020 06:00
08/19/2020
450ONO3F-2011
WP MTN
73416
1
Solids
08117/2020 06:00
08/19/2020
9045D
WP MTN
73416
1
Solids
08/17/2020 06:00
08/19/2020
SM-254OG
WP MTN
73416
1
Solids
08/17/2020 06:00
08/19/2020
6010D
WP MTN
73416
1
Solids
08/17/2020 06:00
08/19/2020
SW-74718,
WP MTN
73416
1
Solids
08/17/2020 06:00
0811912020
SM-4500-NH3C
WP MTN
73416
1
Solids
08/17/2020 06:00
08/19/2020
SM-4500-NH3C-TKN
WP MTN
73417
2
Solids
08/17/2020 06:15
08119/2020
73417
2
Solids
08/17/2020 06:15
08/19/2020
SM-4500-NH3C-TKN
WP MTN
73417
2
Solids
08/17/2020 06:15
08/19/2020
SM-4500-NH3C
Will MTN
73417
2
Solids
08/17/2020 06:15
08/19/2020
SM-254OG
WP MTN
73417
2
Solids
08/17/2020 06:15
08/19/2020
450ONO3F-2011
WP MTN
73417
2
Solids
08/17/2020 06:15
08/19/2020
AOAC 955.0,1
WP MTN
73417
2
Solids
08/17/2020 06-15
08/19/2020
5W-7471B
WP MTN
73,417
2
Solids
08/17/2020 06:15
08/19/2020
9045D
WP MTN
73417
2
Solids
08/17/20,20 06:15
08/19/2020
6010D
WP MTN
73418
3
Solids
08/17/2020 06:30
08/19/2020
73418
3
Solids
08/17/2020 06:30
08/19/2020
6010D
WP MTN
73418
3
Solids
08/17/2020 06:30
08/19/2020
9045D
WP MTN
73418
3
Solids
08/17/2020 06:30
08/19/2020
4500NO3F-2011
WP MTN
73418
3
Solids
08/17/2020 06:30
08/19/2020
SM-4500-NH3C-TKN
WP MTN
73418
3
Solids
08/17/2020 06:30
08/19/2020
SM-2540G
WP MTN
73418
3
Solids
08/17/2020 06;30
08/19/2020
SW-7471B
WP MTN
73418
3
Solids
08/17/2020 06.30
08/19/2020
SM-4500-NH3C
W'P MTN
73418
3
Solids
08/17/2020 06;30
08/19/2020
AOAC 955.01
WP' MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 19

(D 7621 Whitepine Road, Richmond, VA 23237
Waypoint. Main 804-743-94011 Fox 804-271-6446
ANALYTICAL www.waypoi:iitanalytical.com
Sample Summary Table
Report Number: 20-232-0006
Client Project Description: Len,cit-2
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
73419
4
Solids
08/17/2020 06:40
08/19/2020
73419
4
Solids
08/17/2020 06:40
08/19/2020
SM-4500-NH3C
WP MTN
73419
4
Solids
08/17/2020 06:40
08/19/2020
SM-2540G
WP MTN
73419
4
Solids
08/17/2020 06,40
08/19/2020
AOAC 955.01
WP MTN
73419
4
Solids
08/17/2020 06.,40
08/19/2020
9045D
WP MTN
73419
4
Solids
08/17/2020 06:40
08/19/2020
SW-7471B
WP MTN
73419
4
Solids
08/17/2020 06:40
08/19/2020
6010D
WP MTN
73419
4
Solids
08/17/2020 06:40
08/19/2020
450ONO3F-2011
WP MTN
73419
4
Solids
08/1712020 06:40
08/19/2020
SM-4500-NH3C-TKN
WP MTN
73420
5
Solids
08117/2020 06:50
08/19/2020
73420
5
Solids
08/17/2020 06:50
08/19/2020
9045D
WP MTN
73420
5
Solids
08/17/2020 06:50
08/19/2020
SW-74718
WP MTN
73420
5
Solids
08/17/2020 0,6:50
08/19/2020
6010D
WP MTN
73420
5
Solids
08/17/2020 06:50
08/19/2020
4SOONO3F-2011
WP MTN
73420
5
Solids
08/17/2020 06:50
08/19/2020
SM-4500-NH3C-TKN
WP MTN
73420
5
Solids
08/17/2020 06:50
08/19/2020
SM-4500-NH3C
WP MTN
73420
5
Solids
08117/2020 06:50
08/19/2020
S,M-254OG
Wl? MTN
73420
5
Solids
08/17/2020 06:50
08/19/2020
AOAC 955.01
WP MTN
73421
6
Solids
08/17,12020 07:00
08/19/2020
73421
6
Solids
08/17/2020 07,00
08/19/2020
9045D
WP MTN
73421
6
solid's
08/17/2020 07:00
08/19/2020
SW-74718
WP MTN
73421
6
Solids
08/17/2020 07.00
08/19/2020
6010D
WP MTN
73421
6
Solids
08/17/2,020 07:00
08/19/2020
450ONO3F-2011
WP MTN
73421
6
Solids
08/17/2020 07:00
08/19/2020
SM-4500-NH3C-TKN
WP MTN
73421
6
Solids
08/17/2020 07:00
08/19/2020
SM-4500-NH3C
WP MTN
73421
6
Solids
O8/17/2020 07:00
08/19/2020
SM-2540G
WP MTN
WP MTN'- Memphis, TN: Waypoint AnalAcal - TN, Memphis, TN
,Page 3 of 19

(D 7621 Whitepine Road, Richmond, VA 23237
Waypoint (Main 804-743-94010 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number; 20-232-0006
Client Project Description: Lencit-2
Lab No Client Sample ID Matdx Date Collected Date Received Method Lab ID
73421 6 Solids 08/17/2020 07-00 08/19/2020 AOAC 955.01 WP MTN
WP MTN - Memphis, TN. Waypoint Analytical - TN, Memphis, TN
Page 4 of 19

a7621
Waypoeint,
W'hitepine Road, Richmond, VA 23237
Main 804-743-94010 Pax 804-271-6446
ANALYTICAL
www.waypointanalytical.com
45671
Bio-Nomic Servics Inc
Project
Lencit-2
Joel Coert
Report
Date 08/27/2020
530 Woodlawn St
Information
Received 08/19/2020
Belmont, NC 28012
Report Number: 20- 232-0006
REPORT OFANAL YSrS
Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No 73416
Matrix:
Solids
Sample ID: I
Sampled':
8/17/2020
6:00
Test
Results
Units
MUL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
67.0
%
0,010
1 08/24/20 14,00
FMM
SM-2540G
Calcium Carbonate Equivalent
5.4
% - dry
0.1
1
08126/20 09.44
DXT
AOAC 955.01
Test
Results
Units
MOL
DF
Date / Time
By
Analytical
Analyzed
Method
Ammonia Nitrogen
1200
mg/Kg - dry
179
1
06126/20 15:30
JP1
SM-4500-NH3C
Nitrate+ Nitrite-N
40.6
mg/Kg - dry
14.0
1
08/26/20 14:36
ZBD
4500NO3F-2011
Organic N
5420
mg/Kg - dry
758
1
08/26/20 11:00
CALCULATION
pH
5.8
slu.
1
08/24/20 12:57
ADM
9045D
Total Solids
33.0
%
0.010
1
08/24/20 14-00
FMM
SM-2540G
Total Volatile Solids
24.2
%
0.010
1
08/24120 14:00
FMM
SM-2540G
Total Kjeldahl Nitrogen
6640
mg/Kg - dry
758
1
08/26/20 11:00
JPJ ;M-4500-NH3C-TKP
Phosphorus
1890
mg/Kg - dry
15.2
1
08/24/20 22:45
TJS
6010D
Aluminum
11200
mg/Kg - dry
15.2
1
08/25/20 19:31
ADS
6010D
Arsenic
8.36
mg/Kg - dry
1.52
1
08/24/20 22:45
TJS
6010D
Calcium,
1420
mg/Kg - dry
152
1
08/25/20 19.26
DADS
6010D
Cadmium
<0.303
mg/Kg - dry
0,303
1
08/24/20 22:45
TJS
6010D
Chromium
82.7
mg/Kg - dry
0,757
1
08/24/2�0 22:45
TJS
6010D
Copper
37.3
mg/Kg - dry
1,52
1
08/24/20 22:45
TJS
6010D
Iron
30300
mg/Kg - dry
30.3
1
08/24/20 22:45
)ADS
6010D
Lead
34.2
mg/Kg - dry
0.909
1
08/24/20 22:45
TJS
6010D
Qualifiers/ DF Dilution Factor
L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 5 of 19.

Waypoint,
7621 Whitepine Road', Richmond,
VA 23237
Main 804-743-94010 Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
45671
Blo-Nomic Servics Inc
Project
Lencit-2
Joel Coert
Report Date 08/27/2020
530 Woodlawn St
Information
Received 08119/2020
Belmont , NC 28012
Report Number: 20-23 2-0006
REPoR r OF ANAL YSIS
Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No 73416
Matrix: Solids
Sample ID: I
Sampled: 8/17/2020 6:00
Test
Results
Units
MOL
DF
Date / Time By Analytical
Analyzed Method
Magnesium
2110
mg/Kg - dry
15.2
1
08/25/20 19:26 )ADS 6010D
Manganese
906
mg/Kg - dry
1.52
1
08/24/20 22:45 TJS 6010D
Mercury 0.0575
mg/Kg - dry
0.0454
1
08/24/20 13:48 DDB SW-7471B
Molybdenum
1.89
mg/Kg - dry
0.757
1
08/25/20 19:26 )ADS 6010D
Nickel
19.7
mg/Kg - dry
0.757
1
08/25/20 19:26 )ADS 6010D
Potassium
1620
mg/Kg - dry
30.3
1
08/24/20 22.45 TJS 6010D
Selenium
<1.52
mg/Kg - dry
1.,52
1
08/24/20 22:45 TJS 6010D
Sodium
<75.8
mg/Kg - dry
75.8
1
08/24/20 22:45 TJS 6010D
Zinc
203
mg/Kg - dry
3.79
1
08/24/20 22:45 TJS 6010D
Sulfur
3480
mg/Kg - dry
30.3
1
08/24120 22:45 TJS 6010D
Qualifiers/ DF Dilution Factor L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page G of 19

a7621
Waypoint,
Whitepine Road, Richmond, VA 23237
Main 804-743-94010 Fax [phone]
ANALYTICAL
www,waypointanalytkal.com
45671
Blo-Nomic Servics Inc
Project
Lencit-2
Joel Coert
Report Date 08/27/2020
530 Woodlawn St
Information
Received 08/19/2020
Belmont , NC 28012
Pauric Mc Groary Ph.D., CPA
Report Number: 20-232-0006
REPORT OFANAL YSIS
Agronomist
Lab No 73417
Matrix: Solids
Sample ID: 2
Sampled: 8/17/2020 6:15
Test
Results
Units
MOL DF Date / Time By Analytical
Analyzed Method
Moisture
64.8
%
0.010 1 08/24/20 14:00 FMM SM-2540G
Calcium Carbonate Equivalent
5.0
% - dry
0.1 1 08/26/20 09:44 DXT AOAC 955.01
Test
Results
Units
MOL DF Date t Time By Analytical
Analyzed Method
Ammonia Nitrogen
736
mg/Kg - dry
164
1
08/26/20 15:30
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
60.2
mg/Kg - dry
14.2
1
08/26/20 14:36
ZBD
4500NO3F-2011
Organic N
4860
mg/Kg - dry
710
1
08/26/20 11:00
CALCULATION
pH
5.8
S.U.
1
08/24120 12:57
ADM
9045D
Total Solids
35.2
%
0.010
1
08/24120 14:00
FMM
SM-254OG
Total Volatile Solids
23.0
%
0.010
1
08/24/20 14:00
FMM
SM-254OG
Total Kjeldahl Nitrogen
5600
mg/Kg - dry
710
1
08/26120 11:00
JP3 AM-4500-NH3C-TKl`
Phosphorus
1740
m9/Kg - dry
14.2
1
08/24/20 22:50
TIS
6010D
Aluminum
105000
mg/Kg - dry
142
10
08125/20 19:42
DADS
6010D
Arsenic
7.87
mg/Kg - dry
1.42
1
08/24/20 22.50
TIS
6010D
Calcium
1350
mg/Kg - dry
142
1
08/25/20 19:37
]ADS
6010D
Cadmium
0.327
mg/Kg - dry
0.284
1
08/24/20 22:50
TI'S
6010D
Chromium
75.6
mg/Kg - dry
0.710
1
08/24/20 22:50
TjS
6010D
Copper
35.2
mg/Kg - dry
1.42
1
08/24/20 22:50
TjS
6010D
Iron
36100
mg/Kg - dry
284
10
08/25/20 19:42
]ADS
6010D
Lead
35.8
mg/K9 - dry
0.,852
1
08/24/20 22:50
TIS
6010D
Qualifiers/ DF
Dilution Factor
L
Limit Exceeded
Definitions MQL
Method Quantitation Limit
Page 7 of 19

0
Waypoint.
7621 Whitepine Road, Richmond, VA, 23237
Main 804-743-94010 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
45671
Bio-Nomic SerAcs Inc
Project
Lencit-2
Joel Coert
Report Date : OB/27/2020
530 Woodlawn St
Information
Received: OB/19/2020
Belmont , NC 28012
kD ply
Report Number: 20-232-oOO6
REPORT OFANAL YSIS
Pauric Mc Groairy Ph.D., CPA
Agronomist
Lab No 73417
Matrix: Solids
Sample ID : 2
Sampled: 811712020 6:1,5
Test
Results
Units
MOL
DF Date / Time By Analytical
Analyzed Method
Magnesium
2200
mg/Kg - dry
14.2
1 08/25/20 19:37 ]ADS 6010D
Manganese
994
mg/Kg - dry
1.42
1 08/24/20 22:50 TJS 6010D
Mercury 0.0505
mg/Kg - dry
0.0420
1 08/24/20 13:49 DDB, SW-7471B
Molybdenum
1.66
mg/Kg - dry
0.710
1 08/25/20 19:37 DADS 6010D
Nickel
19.2
mg/Kg - dry
0.710
1 08/25/20 19:37 DADS 6010D
Potassium
1650
mg/Kg - dry
28.4
1 08/24/20 22:50 TJS 6010D
Selenium
<1.42
mg/Kg - dry
1.42
1 08/24/20 22:50 TJS 6010D
Sodium
<71.0
mg/Kg - dry
71.0
1 08/24/20 22:50 TJS 6010D
Zinc
272
mg/Kg - dry
3.55
1 08/24/20 22:50 TJS 6010D
Sulfur
37'50
mg/Kg - dry
28.4
1 08/24/20 22:50 TJS 6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Urnit Exceeded
Page 8 of 19

0
Waypoint
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-94010 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
45671
Blo-Nomic Servics Inc
Project
Lencit-2
Joel Coert
Report Date 08/'27/2020
530 Woodlawn St
Information
Received 08/19/2020
Belmont, NC 28012
Report Number : 20-232-0006
REPORT OFAIVAL YSIS Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No 73418
Matrix: Solids
Sample ID : 3
Sampled: 8/17/2020 6:30
Test
Results
Units
MQL DF Date I Time By Analytical
Analyzed Method
Moisture
67.5
%
0.010 1 08/24/20 14:00 FMM SM-254OG
Calcium Carbonate Equivalent
5.4,
% - dry
0.1 1 08/26/20 09,:44 DXT AOAC 955.01
Test
Results
Units
MQL DF Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen
892
mg/Kg - dry
181
1
08/26/20 15:30
JPJ
SM-4500-NH3C
Nitrate+ Nitrite-N
196
mg/Kg - dry
14.5
1
08/26/20 14:37
ZBD
4500110317-2011
Organic N
5970
mg/Kg - dry
769
1
08/26/20,11-.00
CALCULATION
pH
5.9
slu,
1
08/24/20 12:57
ADM
9045D
Total Solids
32.5
%
0,010
1
08/24/20 14:00
FMM
SM-254OG
Total Volatile Solids
23.8
%
0,010
1
08/24/20 14:00
F:MM
SM-254OG
Total Kjeldahl Nitrogen
68,60
mg/Kg - dry
769
1
08/26/20 11:00
JPJ ;M-4500-NH3C-TKr
Phosphorus
1780
mg/Kg - dry
15.4
1
08/24/20 22:56
TJS
6010D
Aluminum
104000
mg/Kg - dry
154
10
08/25/20 19:53
JADE
6010D
Arsenic
7.97
mg/Kg - dry
1.54
1
08/24/20 22:56
TIS
6010D
Calcium
1010
mg/Kg - dry
154
1
08/25/20 19:47
]ADS
6010D
Cadmium
0.326
mg/Kg - dry
0,308
1
08/24/20 22:56
TJS
6010D
Chromium
78.8
rng/Kg - dry
0.769
1
08/24/20 22:56
TJS
6010D
Copper
36.9
mg/Kg - dry
1,54
1
08/24/20 22:56
TJS
6010D
Iron
35100
mg/Kg - dry
308
10
08/25/20 19:53
]ADS
6010D
Lead
32.3
mg/Kg - dry
0,923
1
08/24/20 22:56
TJS
6010D
Qualifiers/ DF
Dilution Factor
L
Limit Exceeded
Definitions MQL
Method Quantitation Limit
Page 9 of 19

Waypoint.
7621 Whitepi'ne Road, Richmond, VA 23237
Main 804-743-94010 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
45671
Bio-Nomic Servics Inc
Project
Lencit-2
Joel Coert
Report Date 08/27/2020
530 Woodl'awn St
Information
Received 08/19/2020
Belmont , NC 28012
Report Number: 20-232-0006
REPOR T OF A NA L YSIS
Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No 73418
Matrix: Solids
Sample ID : 3
Sampled: 8117/2020 6:30
Test
Results
Units
MQL
DF
Dale I Time By Analytical
Analyzed Method
Magnesium
2040
mg/Kg - dry
15.4
1
08/25/20 19:47 ]ADS 6010D
Manganese
914
rng/Kg - dry
1.54
1
08/24/20 22:56 TJS 6010D
Mercury
0.418
mg/Kg .. dry
0.0470
1
08124/20 13:50 DDB SW-7471B
Molybdenum
1.70
mg/Kg - dry
0.769
1
08/25/20 19:47 JADE 6010D
Nickel
20.4
mg/Kg - dry
0,769
1
08/25/20 19:47 JADE 6010D
Potassium
1690
mg/Kg - dry
30.8
1
08/24/20 22:56 TJS 6010D
Selenium
<1.54
mg/Kg - dry
1.54
1
08/24/20 22:56 TJS 6010D
Sodium
<76.9
mg/Kg - dry
76.9
1
08/24/20 22:56 TJS 6010D
Zinc
256
mg'/Kg - dry
3.85
1
08/24/20 22:56 TJS 6010D
Sulfur
3170
mg/Kg - dry
30.8
1
08/24/20 22:56 TJS 6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Page 10 of 19

Report Number: 20-232-0006
Lab No : 73419
Sample ID : 4
762,1 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.corn
REPORT OFANAL YSIS
Report Date 08/27/2020
Received 08/1912020
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 8/17/2020 6:40
Test
Results
Units
MQL
DF Date / Time
By
Analytical
Analyzed
Method
Moisture
63.3
%
0.010
1 08/24/20 14:00
FMM
SM-2540G
Calcium Carbonate Equivalent
5.1
% - dry
0.1
1 08/26/20 09:44
DXT
AOAC 955.01
Test
Results
Units
MQL
DF Dale / Time
By
Analytical
Analyzed
Method
Ammonia Nitrogen
872
mg/Kg - dry
162
1
08/26/20 15:30
JPJ
SM-4500-NH3C
Nitrate+Njtrite-N
1830
mg/Kg: - dry
13.6
1
08/26/20 14:37
ZBD
4500NO3F-2011
Organic N
5500
mg/Kg - dry
681
1
08/26/20 11:00
CALCULATION
pH
6.1
SM.
1
08/24/20 12:57
ADM
9045D
Total Solids
36.7
%
0.010
1
08/24/20 14:00
FMM
S,M-254OG
Total Volatile Solids
22.9
%
0.010
1
08/24/20 14:00
FMM
SM-2540G
Total Kjeldahl Nitrogen
6380
mg/Kg - dry
681
1
08/26/20 11.00
JPJ ;M-4500-NH3C-TKP
Phosphorus
1600
mg/Kg - dry
13.6
1
08/24/20 23:01
TJS
6010D
Aluminum
91300
mg/Kg - dry
136
10
08/25120 20:14
]ADS
6010D
Arsenic
7.22
mg/Kg - dry
1.36
1
08/24/20 23:01
TJS
6010D
Calcium
1690
mg/Kg - dry
136
1
08/'25/20 20:08
JARS
6010D
Cadmium
0.313
mg/Kg - dry
0.272
1
08/24/20 23:01
TJS
6010D
Chromium
67.8
mg/Kg - dry
0.681
1
08/24/20 23:01
TJS
6010D
Copper
32.2
mg/Kg - dry
1.36
1
08/24/20 23:01
TIS
6010D
Iron
27200
mg/Kg - dry
27.2
1
08/24/20 23:01
DADS
6010D
Lead
31.9
mg/Kg - dry
0.817
1
08/24/20 23:01
TJS
6010D
Qualifiers/ DF
Dilution, Factor
L
Limit Exceeded
Definitions MQL
Method Quantitation Limit
Page 11 of 19

0
Waypoint,
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-941010 Fax [phone]
ANALYTICAL
www.waypointana:lytical.co,m
45671
Bio-Nomic Servics Inc
Project
Lencit-2
Joel Coert
Report Date 0,8/27/2020
530 Woodlawn St
Information
Received 08/19/2020
Belmont, NC 28012
Report Number: 20-232-,0006
REPO)?TOFANAL YSIS
Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No 73419
Matrix: Solids
Sample ID : 4
Sampled: 8/17/2020 6:40
Test
Results
Units
MOL
DF
Date I Time By Analytical
Analyzed' Method
Magnesium
2230
mg/Kg - dry
13.6
1
08/25/20 20:08 ]ADS 6010D
Manganese
812
mg/Kg - dry
1.36
1
08/24/20 23:01 TJS 6010D
Mercury
0.0509
mg/Kg - dry
0.0381
1
08124/20 13:52 DDB SW-7471B
Molybdenum
1.54
mg/Kg - dry
0.681
1
08/26/20 1731 )ADS 6010D
Nickel
19.8
mg/Kg - dry
0.681
1
08/25/20 20:08 ]ADS 6010D
Potassium
1540
mg/Kg - dry
27.2
1
08/24/20 23:01 TJS 6010D
Selenium
<136
mg/Kg - dry
1.36
1
08/24/20 2101 TJS; 6010D
Sodium
<68.1
mg/Kg - dry
68.1
1
08/24/20 23:01 TJS 6010D
Zinc
208
mg/Kg - dry
3.41
1
08/24/20 23:01 TJS 6010D
Sulfur
2940
mg/Kg - dry
27.2
1
08/24/20 23:01 TJS 6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Page 12 of 19

0 7621 Whitepine Road, Richmond, VA 23237
Waypoint. Main 804-743-9401 ' Fax [phone]
45671 ANALYTICAL www.waypoi ntanalytical com
Bio-Nomic Servics Inc Project Lendt-2
Joel Coert Report Date : 08/27/2020
530 Woodlawn St Information Received: 08/19/2020
Belmont, NC 28012
ko IVY
Report Number : 20-232-0006 REPoRrOFANALYSIS Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No: 73420 Matrix: Solids
Sample ID : 5 Sampled: 8117/2020 6:50
Test Results Units MOL DF Date / Time By Analytical
Analyzed Method
Moisture
Calcium Carbonate Equivalent
Test
62.4
4.5
Results
%
% - dry
Units
0.010
0.1
MQL
1
1
DF
08/24/20 14:00
08/26/20 09:44
Date / Time
Analyzed
FMM
DXT
By
SM-2540G
AOAC 955,01
Analytical
Method
Ammonia Nitrogen
973
mg/Kg - dry
155
1
08/26120 15:30
JPJ
SM-4500-NH3C
Nitrate+ Nitnte-N
107
mg/Kg - dry
12.7
1
08/26/20 14:38
ZBD
4500NO3F-2011
Organic N
4890
mg/Kg - dry
665
1
08/26/20 11:00
CALCULATION
pH
7.0
S.U.
1
08/24/20 12:57
ADM
9045D
Total Solids
37.6
%
0.010
1
08/24/20 14:00
FMM
SM-254OG
Total Volatile Solids
20.1
%
0.010
1
08/24/20 14:00
FMM
SM-2540G
Total Kjeldahl Nitrogen
5880
mg/Kg - dry
665
1
08/26/20 11:00
JPJ ;M-4500-NH3C-TKP
Phosphorus
1610
mg/Kg - dry
13.3
1
08/24/20 23:07
TJS
6010D
Aluminum
90400
mg/Kg - dry
133
10
08/25120 20:25
JADE
6010D
Arsenic
6.62
mg/Kg - dry
1.33
1
08/24/20 23:07
TJS
6010D
Calcium
2220
mg/Kg, - dry
133
1
08/25/20 20:19
)ADS
6010D
Cadmium
0.380
mg/Kg - dry
0.266
1
08/24/20 23:07
TJS
6010D
Chromium
67.3
mg/Kg - dry
0.664
1
08/24/20 23:07
TJS
6010D
Copper
33.0
mg/Kg - dry
1.33
1
08/24/20 23:07
TJS
6010D
Iron
26500
mg/Kg - dry
26.6
1
08/24/20 23:07
)ADS
6010D
Lead
44.1
mg/Kg - dry
0.797
1
08/24/20 23:07
TJS
6010D
Qualifiers/ DF
Dilution Factor
L
Limit Exceeded
Definitions MQL
Method Quantitation Limit
Page 13 of 19

a7621
Way it.
P
Whitepine Road, Richmond,
VA 23237
Main 804-743-94010 Fax
804-271-6446
A
www.waypointanalytical.com
45671
Bio-Nomic Servics Inc
Pr6ject
Lencit-2
Joel Coert
Report Date 08/2712020
530 Woodlawn St
Information
Received 08/19/2020
Belmont , NC 28012
Report Number : 20-232-0006
REPORT OFANAL YSrS
Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No 73420
Matrix: Solids
Sample ID: 5
Sampled: 8/17/2020 6:S0
Test
Results
Units
MOL
DF
Date I Time By Analytical
Analyzed Method
Magnesium
2330
mg/Kg - dry
13.3
1
08/25/20 20:19 ]ADS 6010D
Manganese
750
mg/Kg - dry
1.33
1
08/24/20 23:07 TJS 6010D
Mercury 0.0529
mg/Kg - dry
0.0401
1
08/24/20 13:56 DDB SW-7471B
Molybdenum
1.57
mg/Kg - dry
0.664
1
08/26/20 17:36 DADS 6010D
Nickel
17.7
mg/Kg - dry
0.664
1
08/25/20 20:19 ]ADS 6010D
Potassium
1520
mg/Kg - dry
26.6
1
08/24/20 23:07 TJS 6010D
Selenium
<133
mg/Kg - dry
1.33
1
08/24/20 23:07 TJS 6010D
Sodium
<66.5
mg/Kg - dry
66.5
1
08/24/20 23:07 TJS 6010D
Zinc
197
mg/Kg - dry
3.32
1
08/24/20 23:07 TJS 6010D
Sulfur
2740
mg/Kg - dry
26.6
1
08124/20 23:07 TIS 6010D
Qualifiers/ DF Dilution Factor L Limit Exceeded
Definitions MQL Method Quarititation Limit
Page 14 of 19

a762
Waypoint,
,1 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ' Fax [phone]
ANALYTICAL
www.waypointanalytical-com
45671
Bio-Nomic Servics Inc
Project
Lencit-2
Joel Coert
Report Date 08/27/2020
530 Woodlawn St
Information
Received 08/19/2020
Belmont, NC 28012
Report Number: 20-232-0006
REPORT OFANAL YSIS Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No 73421
Matrix: Solids
Sample ID : 6
Sampled: 8/17/2020 7:00
Test
Results
Units
MOIL DF Date / Time By Analytical
Analyzed Method
Moisture
64.,2
%
0.010 1 08124/20 14:00 FMM SM-2540G
Calcium Carbonate Equivalent
7.6
% - dry
0.1 1 08/26/20 09:44 DXT AOAC 955.01
Test
Results
Units
MQL OF Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen
520
rng/Kg - dry
166
1
08/26120 15:30
JP3
SM-4500-NH3C
Nitrate+Nitrite-N
21.7
mg/Kg - dry
12.8
1
08126/20 14:39
ZBD
4500NO317-2011
Organic N
4860
mg/Kg - dry
698
1
08/26/20 11:00
CALCULATION
PH
6.2
S. U.
1
08/24/20 12:57
ADM
9045D
Total' Solids
35.8
%
0.010
1
08/21/20 14:00
FMM
SM-2540G
Total Volatile Solids
21.9
0/0
0.010
1
08/24/20 14:00
FMM
5M-2540G
Total Kjeldahl Nitrogen
5390
mg/Kg - dry
698
1
08/26/20 11:00
JPJ iM-4500-NH3C-TKP
Phosphorus
1460
mg/Kg - dry
14.0
1
08/24120 23-12
TJS
6010D
Aluminum
84100
mg/Kg - dry
140
10
08125/20 20:35
)ADS
6010D
Arsenic
6.40
mg/Kg - dry
1.40
1
08/24/20 23:12
TJS
6010D
Calcium
1810
mg/Kg - dry
140
1
08/25/20 20:30
DADS
6010D
Cadmium
<0.279
mg/Kg - dry
0.279
1
08/24/20 23:12
TJS
6010D
Chromium
62.0
mg/Kg - dry
0.698
1
08/24/20 23:12
TJS
6010D
Copper
30.7
mg/Kg - dry
1.40
1
08/24/20 23:12
TJS
6010D
Iron
26300
mg/Kg - dry
27.9
1
08/24/20 23:12
]ADS
6010D
Lead
33.5
mg/Kg - dry,
0.837
1
08/24/20 23:12
TJS
6010D
Qualifiers/ DF
Dilution Factor
L
Limit Exceeded
Definitions MQL
Method Quantitation Limit
Page 15 of 19

Waypoeinte
ANALYTICIL
45671
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC 28012
Report Number -, 20�-232-0006
Lab No : 73421
Sample ID: 6
Project Lencit-2
Information :
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-94010 Fax [phone]
www.waypointanalytical.com
REPORT OFANAL YSIS
Report Date 08/27/2020
Received 08/19/2020
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 8,117/2020 7-00
Test
Results
Units
MQL
DF
Date I Time
Analyzed
By
Analytical
Method
Magnesium
2040
mg/Kg - dry
14.0
1
08/25/20 20:!30
]ADS
6010D
Manganese
1010
mg/Kg - dry
1.40
1
08/24/20 23:12
TJS
6010D
Mercury
0.0553
mg/Kg - dry
0.0418
1
08/24/20 13:57
DDB
SW-7471B
Molybdenum
1.57
mg/Kg - dry
0.698
1
08/26/20 17:42
DADS
6010D
Nickel
17.7
mg/Kg - dry
0.698
1
08/25/20 20:30
)ADS
6010D
Potassium
15001
mg/Kg - dry
27.9
1
08/24/20 23:12
TJS
6010D
Selenium
<1.40
mg/Kg - dry
1.40
1
08/24/20 23:12
TJS
6010D
Sodium
<69.8
mg/Kg - dry
69.8
1
08/24120 23:12
TJS
6010D
Zinc
213
mg/Kg - dry
3.49
1
08/24/20 23:12
TJS
6010D
Sulfur
2850
mg/Kg - dry
27.9
1
08/24/20 23:12
TJS
6010D
Qualifiers/ DF Dilution Factor L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 16 of 19

Wayp ARint(l
TICAL
7621 Whitepine Road, Richmand, VA 23237
Main 804-743-94010 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 20-232-0006
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
Yes
0 No
Number of coolers/boxes received
F 1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No►
Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
61 Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
High concentration container (48 hr) 7 Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -114 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments: I I
Signature: jBrandi Watson Date & Time: 8/i' 9J2020 11:04:1--9-1
Page 17 of 19

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Post Office Box 1056 • Granite Falls, North Carolina 28630
Phone [phone], EMAIL* [e-mail]
CITY OF LENOIR
P. O. BOX 958
LENOIR, NC 28645
SAMPLE I.D.: ALUM LAGOON SLUDGE (WATER TRT PLT)
COLLECTED: 10108/19 1420
COLLECTED BY: kEVIN MATHESON
FECAL COLIFORM BACTERIA
#1 13,2 MPN COLONIESIGRAM
#2 11.8
#3 10.8,
#4 9,.5
#5 13.2
#6 16.9
97 12.0
ANALYSIS BEGIN: 10/08/19 1630
ANALYSIS END: 10/09/19 1630
ANALYZED, AND REPORTED BY,
0 6NY GG

Willcox & Mabe Soil Solutions, PLLC
Summerfield, North Carolina
RESIDUAL PAN CALCULATION
George L. Bernhardt, Sr'. Lake Rhodhiss WTP
TKN= 6,640 mg/kg
NH3= 1,200 mg/kg
NO3-NO2-N= 41 mg/kg
Min Rate = 0.20
PAN= [min.rate (TKN - NH3) + 0.5 (NH3) + NO3-NO2]
0.20 5,440 600 40.60
PAN= 1728.60 mg/kg
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (Ist year org. - N 2nd year min. - NJ
0.10 5,440 1,088
PAN= 435-20 mg/kg remaining from I st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - NJ
0.05 4,352 435
PAN= 208.90 mg/kg remaining from 1st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - NJ
0.03 3,917 209
PAN= 123.60 mg/kg remaining from 1st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - Nj
0.02 3,708 124
PAN= 69.46 mg/kg remaining from 1st year application
Residual PAN from years 2 thru 5 after the initial application = 837.16
Application
Method
First Year PAN
(mg/kg)
Five Year Maximum
Adjusted PAN
Surface
1,729
2,566
Incorporation
2,329
3,166
mg/kg

m
SAR Calculation
Na mg/l -
Ca mg/i
Mg mg1l
-Mg
25.,014
_
468.6
696.3
Na
Ca
�AR
1.088
f�-.430
-8. 0 2-5
0.170
Na mil eq
Ca mil eq
Mg mil eq
1.088
23,430 mm
58.025
. ..... .. ..
Enter
Enter.% TS
33
Data
Na mg/'kg
75.8
Ca mg/kg
1420
Ma_mg/kg
2110
Job Name:
George L. Bernhardt, Sr. Lake Rhodhiss WTP