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Home My WebLink AboutNCG120045_2021 DMR_20210712NCDEQ Division of Energy, Mineral and Land Resources Stormwater Discharge Monitoring Report (DMR) Form for NCG120000 Landfills Click here for instructions Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office. Certificate of Coverage No. NCG120045 Person Collecting Samples: Hoggard Facility Name: East Carolina Environmental Laboratory Name: ENCO Facility County: Bertie Laboratory Cert. No.: 591 Discharge during this period:✓ Yes 0 No (if no, skip to signature and date) Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? Yes ❑✓ No If so, which Tier (I, II, or III)? A copy of this DMR has been uploaded electronically via https://edocs.deg.nc.gov/Forms/SW-DMR Eyes ❑ No Date Uploaded:July 12, 2021 Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red) Parameter Parameter Outfall 1 Outfall 2 Outfall H-1 Outfall Outfall Code N/A Receiving Stream Class C, SW C, SW C, SW N/A Date Sample Collected MM/DD/YYYY 06/30/2021 06/30/2021 06/30/2021 46529 24-Hour Rainfall in inches Trace Trace Trace C0530 TSS in mg/L (100 or 50*) 3.2 3.2 <2.5 00400 pH in standard units (6.0-9.0 FW, 8.3 8.3 8.2 6.8 — 8.5 SW) Chemical Oxygen Demand in mg/L 00340 (120) 13 11 31616 Fecal Coliform in # per 100 ml (1000) 22 7.5 Additional parameters for outfalls in drainage areas that use >55 gallons per month of new hydraulic oil on average 00552 Non -Polar Oil & Grease in mg/L (15) <2.70 NCOIL Estimated New Motor/Hydraulic Oil >55 Usage in gal/month * Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA) have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 mg/L. FW (Freshwater) SW (Saltwater) Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 07/12/2021 Signature of Permittee or Delegated Authorized Individual Date meinsmann@republicservices.com Email Address 919-672-2837 Phone Number ENCO Laboratories 9g Accurate, Timely. Responsive. Iuuovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Thursday, July 8, 2021 Republic Services of NC (RE016) Attn: Matt Einsmann East Carolina Environemntal, 1922 Republican Road Aulander, NC 27805 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater ENCO Workorder(s): CE09431 Dear Matt Einsmann, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Wednesday, June 30, 2021. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Amanda L. Gaines Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 1 of 9 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Outfall H-1 Lab ID: CE09431-01 Sampled: 06/30/21 06:40 Received: 06/30/21 16:00 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664B EPA 1664B 07/28/21 07/06/21 15:30 07/07/21 10:47 SM 254OD-2011 NO PREP 07/07/21 07/02/21 11:30 07/02/21 11:30 Client ID: Outfall 1 Lab ID: CE09431-02 Sampled: 06/30/21 07:03 Received: 06/30/21 16:00 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) Colilert 18 NO PREP 06/30/21 14:58 07/01/21 14:47 06/30/21 16:43 07/01/21 11:04 SM 254OD-2011 NO PREP 07/07/21 07/02/21 11:30 07/02/21 11:30 SM 4500H +B-2011 Same 06/30/21 07:17 07/01/21 09:08 07/01/21 09:08 SM 5220D-2011 Same 07/28/21 07/01/21 08:58 07/01/21 11:48 Client ID: Outfall 2 Lab ID: CE09431-03 Sampled: 06/30/21 07:23 Received: 06/30/21 16:00 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) Colilert 18 NO PREP 06/30/21 15:18 07/01/21 14:47 06/30/21 16:43 07/01/21 11:04 SM 254OD-2011 NO PREP 07/07/21 07/02/21 11:30 07/02/21 11:30 SM 4500H+B-2011 Same 06/30/21 07:37 07/01/21 09:08 07/01/21 09:08 SM 5220D-2011 Same 07/28/21 07/01/21 08:58 07/01/21 11:48 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 2 Of 9 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Outfall 1 Lab ID: CE09431-02 Anala Results Flag MDL POLL Units Method Notes Chemical Oxygen Demand 13 10 10 mg/L SM 5220D-2011 Coliform, Fecal 22 1.0 1.0 MPN/100 mL Colilert 18 Q-02 pH 8.3 1.0 1.0 pH SM 4500H+B-2011 Q-01 Temperature for pH (deg. C) 23 pH SM 4500H+B-2011 Q-01 Total Suspended Solids 3.2 2.5 2.5 mg/L SM 254OD-2011 Client ID: Outfall 2 Lab ID: CE09431-03 Anala Results Flag MDL POLL Units Method Notes Chemical Oxygen Demand 11 10 10 mg/L SM 5220D-2011 Coliform, Fecal 7.5 1.0 1.0 MPN/100 mL Colilert 18 Q-02 pH 8.3 1.0 1.0 pH SM 4500H+B-2011 Q-01 Temperature for pH (deg. C) 23 pH SM 4500H+B-2011 Q-01 Total Suspended Solids 3.2 2.5 2.5 mg/L SM 254OD-2011 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 3 Of 9 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: Outfall H-1 Lab Sample ID: CE09431-01 Received: 06/30/21 16:00 Matrix: Surface Water Sampled: 06/30/2106:40 Work Order: CE09431 Project: Stormwater Sampled By: Mitch Hoggard Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL 2 Batch Method Analyzed By Notes Total Suspended Solids^ 2.5 U mg/L 1 2.5 2.5 1G02006 SM 254OD-2011 07/02/21 11:30 DMJ Classical Chemistry Parameters ^ - ENCO Jackson ville certified analyte [NC 442] Analyte rCAS Numberl Results Flag Units DF MDL 2 Batch Method Analyzed By Notes Oil & Grease (HEM-SGT) Non -Polar 2.70 U mg/L 1 2.70 5.00 1G06004 EPA 1664B 07/07/21 10:47 LTS Material^ Description: Outfall 1 Lab Sample ID: CE09431-02 Received: 06/30/21 16:00 Matrix: Surface Water Sampled: 06/30/2107:03 Work Order: CE09431 Project: Stormwater Sampled By: Mitch Hoggard Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL 2 Batch Method Analyzed By Notes Chemical Oxygen Demand' 13 mg/L 1 10 10 1GO1005 SM 5220D-2011 07/01/21 11:48 JOC pH^ 8.3 pH 1 1.0 1.0 1GO1002 SM 4500H+B-2011 07/01/21 09:08 ZGW Q-01 Temperature for pH (deg. C) 23 pH 1 1GO1002 SM 4500H+B-2011 07/01/21 09:08 ZGW Q-01 Total Suspended Solids^ 3.2 mg/L 1 2.5 2.5 1G02006 SM 254OD-2011 07/02/21 11:30 DMJ Microbiological Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF 2 Batch Method Analyzed _By Notes Coliform, Fecal^ 22 MPN/100 mL 1 1.0 1F30023 Colilert 18 07/01/21 11:04 MSE Q-02 Description: Outfall 2 Lab Sample ID: CE09431-03 Received: 06/30/21 16:00 Matrix: Surface Water Sampled: 06/30/2107:23 Work Order: CE09431 Project: Stormwater Sampled By: Mitch Hoggard Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL 2 Batch Method Analyzed By Notes Chemical Oxygen Demand^ 11 mg/L 1 10 10 1GO1005 SM 5220D-2011 07/01/21 11:48 JOC pH^ 8.3 pH 1 1.0 1.0 1GO1002 SM 4500H+B-2011 07/01/21 09:08 ZGW Q-01 Temperature for pH (deg. C) 23 pH 1 1GO1002 SM 4500H+B-2011 07/01/21 09:08 ZGW Q-01 Total Suspended Solids^ 3.2 mg/L 1 2.5 2.5 1G02006 SM 254OD-2011 07/02/21 11:30 DMJ Microbiological Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF POLL Batch Method Analyzed _By Notes Coliform, Fecal^ 7.5 MPN/100 mL 1 1.0 1F30023 Colilert 18 07/01/21 11:04 VISE Q-02 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 4 Of 9 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch IG01002 - Same LCS (1G01002-BSI) Prepared & Analyzed: 07/01/2021 09:08 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes pH 7.0 1.0 pH 7.00 100 99-101 Duplicate (1G03002-DUP1) Prepared & Analyzed: 07/01/2021 09:08 Source: CD06970-01 Spike Source %REC RPD Analvte Result Flao Q Units Level Result %REC Limits RPD Limit Notes pH 6.5 1.0 pH 6.5 0 25 Batch 1GO1005 - Same Blank (1G01005-BLK1) Prepared: 07/01/2021 08:58 Analyzed: 07/01/2021 11:48 Spike Source %REC RPD Analyte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (1G03005-BS1) Prepared: 07/01/2021 08:58 Analyzed: 07/01/2021 11:48 Spike Source %REC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 510 10 mg/L 500 103 90-110 Matrix Spike (11301005-MSI) Prepared: 07/01/2021 08:58 Analyzed: 07/01/2021 11:48 Source: CD21054-01 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 570 10 mg/L 526 35 101 90-110 Matrix Spike Dup (1G01005-MSD1) Prepared: 07/01/2021 08:58 Analyzed: 07/01/2021 11:48 Source: CD21054-01 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 570 10 mg/L 526 35 102 90-110 0.8 5 Batch 1G02006 - NO PREP Blank (1G02006-BLKI) Prepared & Analyzed: 07/02/2021 11:30 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (1G02006-BSI) Prepared & Analyzed: 07/02/2021 11:30 Spike Source %REC RPD Analvte Result Flao Q Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 98 2.5 mg/L 100 98 80-120 Duplicate (1G02006-DUPI) Prepared & Analyzed: 07/02/2021 11:30 Source: CE03363-01 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 620 170 mg/L 600 3 20 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 5 Of 9 QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch IG02006 - NO PREP - Continued (� �Eo www.encolabs.com Duplicate (1G02006-DUP2) Prepared & Analyzed: 07/02/2021 11:30 Source: CE09675-01 Spike Source %REC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 34 25 mg/L 37 8 20 Microbiological Parameters - Quality Control Batch IF30023 - NO PREP Blank (1F30023-BLK3) Prepared: 06/30/2021 15:27 Analyzed: 07/01/2021 11:04 Spike Source %REC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Coliform, Fecal 1.0 U 1.0 MPN/100 mL Duplicate (1F30023-DUP3) Prepared: 06/30/2021 14:05 Analyzed: 07/01/2021 11:04 Source: CE09256-02 Spike Source %REC RPD Analvte Result FFF`lau Q Units Level Result %REC Limits RPD Limit Notes Coliform, Fecal 1.0 U 1.0 MPN/100 mL 1.0 U 25 Classical Chemistry Parameters - Quality Control Batch IG06004 - EPA 1664E Blank (1G06004-BLKI) Prepared: 07/06/2021 15:30 Analyzed: 07/07/2021 10:47 Spike Source %REC RPD Analvte Result FFF`lau Q Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 2.70 U 5.00 mg/L LCS (1G06004-BSI) Prepared: 07/06/2021 15:30 Analyzed: 07/07/2021 10:47 Spike Source %REC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 90.7 5.00 mg/L 80.6 112 64-132 LCS Dup (1G06004-BSDI) Prepared: 07/06/2021 15:30 Analyzed: 07/07/2021 10:47 Spike Source %REC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 80.7 5.00 mg/L 82.3 98 64-132 12 34 Matrix Spike (1G06004-MS3) Prepared: 07/06/2021 15:30 Analyzed: 07/07/2021 10:47 Source: CE09431-01 Spike Source %REC RPD Analvte Result FFF`lau Q Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM-SGT) Non -Polar Material 78.1 5.00 mg/L 74.3 2.70 U 105 64-132 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 6 Of 9 (� �Eo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. Q-01 Analysis performed outside of method - specified holding time. Q-02 Sample received outside of method - specified holding time. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 7 of 9 F --r _0 E v CO _ W 0. - E c N m ro Z) o � 0 m GJ 3 a C a � C O N " V W � v m a r .c m 7+ Q U) " QOiWS SSl x x x LL N 8 H-OOSVWS Hd x x 0 U a IDS Gv%9 DWO a x IiO-A x x cn Na ncLU p oom WS O00 x x O� o p� N O J 7 �J] C R� m �a�LL Z > � S r •-4 _ a Q � m cr uj a f m z c o It ° - W E �. C u E G w W z O J O Z fl N a` a d EE m m C LL Ln O a \ W � v a � a � a m � � t3 n N Sti! {� i � a T 0 H E N r O O n N ro v Y co r m m m t w 1 Q C 9 a U Page 8of9 Sample Preservation Verification ENCO Cary Work Order: CE09431 Project: Stormwater Client: Republic Services of NC (RE016) Project #: [none] Lagged In: 30-Jun-21 16:16 Logged By: Rachel Ann Y nish bi 1 �� Preservation Check Performed By:LAi DatelTime: W 6 CE09431-01 Cont Type Pres (pH) Requirement pH Checked / In Control pH Adjusted DatelTirne Adjusted Reagent Used/Cornments B 250mLA+H2SO4 <2 Y/ N I Y/ N VA, C 250mLA+H2SO4 <2 Y/ N NA Y/ N NA CE09431-02 Cott Type Pres (pH) Requirement pH Checked / -In Control pH Adjusted Date/Time Adjusted Reagent Used/Comments C 250mLP+H2SO4 <2 f Y/ N I NA Y (.N)'/ NA D 250mLA+H2SO4 <2 Y/ N/ Y/ N 1 E 250mLA+H2SO4 <2 Y/ N A Y/ N NA CE09431-03 Cont Type Pres (pH) Requirement pH Checked / in Control pH Adjusted DatefT'irne Adjusted Reagent UsedlComments C 250mLP+H2SO4 <2 Y N/ NA Y N NA D 250mLA+H2504 <2 Y/ N/ Y/ N E 250mLA+H2504 <2 Y/ N NA Y/ N N Rea ent Name ID 1 2 Rea ent Name ID 3 4 Rea ent Name ID 5 6 pH Strip ID: pH Strips C0F0555 C:Ielmnt\Pril..,.. ,�_rreservationCheck. rpt Page 9 of 9 age I o 1