WI0700012_Monitoring (Report)_19970220

PCS
Phosphatie AURORA DIVISION
P.O. BOX 48, AURORA, NC 27806
February 20,1997
Underground Injection Control Program
Division of Water Quality, Groundwater Section
North Carolina DEHNR
P. O. Box 29578
Raleigh, North Carolina 27626-0578
Attention of Mark Milligan
Subject First Quarter 1997 - Monitoring Data
Injection Well Permit #WI0700012
PCS Phosphate Co., Inc.
Tank Farm Remedial Action System
Beaufort Co.
Dear Mark:
Please find enclosed, the Tank Farm Remedial Action System groundwater monitoring report for
the 1st quarter of 1997. The data were collected in January, per the requirements of the above
referenced permit. Note that the Injection Supply Well has been abandoned and will no longer be
included in these reports as the injectate supply now comes from the DPW & condensate water
sources.
Additional Compliance Monitoring Report Forms for well CIW-7 and the WLCT are included in
this report along with the monthly piezometer level monitoring field sheets and a summary
performance report of the individual wells.
• 'ected •
Withdrawn (; al)
January
December
November
722,050
795,660
835,370
587,488
572,210
608,028
Totals
2,353,080
1,767,726
Please contact me at [phone] if you have any questions regarding this information.
Sincerely,
Leon M. Montgomery
Environmental Engineer
Attachments
pc: Willie Hardison - DWQ WaRO (w/attch)

PhosphateW
memo
Date February 20, 1997
To L. M. Montgomery Location
From T. L. Baker Location
Subject TANK FARM REMEDIAL ACTION PLAN
QUARTERLY OPERATIONAL AND MAINTENANCE REPORT
FOR NOVEMBER 1996 - JANUARY 1997
The attached subject report, with required operational and
maintenance data, is provided for submittal to the Division of
Environmental Management, Ground Water Section. This report
should be submitted along with the laboratory sampling and water
level monitoring data.
If you have any questions concerning this information, please
contact me.
i'oY &AA,
T. L. Baker, Superintendent
Operations Environmental
Attachments
pc: W. K. Thornton
T. W. Davis/OE-00-01-00-07
C:\WTRMGMT\REPORTS\1997\OPDATA1.97

PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
OUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
NOVEMBER 1996 - JANUARY 1997
The Tank Farm Remediation System consists of a series of seven
injection water wells located on the south side of the Tank Farm
Area and a series of fourteen (14) water withdrawal wells
located on the north side of the Tank Farm Area.
Infection Water Well System
The injection water well system operated with the DPW Water -
Anthracite Sand Filter / Ultraviolet Light (ASF/UV) disinfection
system throughout the period. During November, some short
periods of planned downtime for preventative maintenance and
Programmable- Logic Controller (PLC) troubleshooting were
experienced. The PLC program cycle timers for alternating the
UV Sterilizers were revised to seven days for better performance
monitoring. On December 12 the system was down for
approximately 24 hours for valve replacement and filter
cleaning. On December 27 the flow was shutoff for approximately
6 hours to repair a leak in the DPW Water supply pipeline.
Daily operational data are collected by the Shipping Department
and reported to the -Operations —Environmental —Department. The
total volume of water injected this period was:
November
DPW Water 713,990
Condensate 8,060
Total Gallons 722,050
December
792,990
2,670
795,660
January
835,370
0
835,370
The water level in the control tank at the end
recorded in feet above MSL:
November
13.09
Withdrawal Well System
December January
13.93 13.93
Ortly Totals
2,342,350
10,730
2,353,080
of each month was
The Withdrawal Well System operated the entire period. Some
short periods of planned downtime for preventative maintenance,
pipe header cleaning, and troubleshooting on individual pumps in
the fourteen well system were experienced. The air dryer for
the system's air compressor malfunctioned on December 9
resulting in low system air pressure. The dryer was bypassed
while repair parts were ordered and the system pressure was
restored. The dryer was repaired and placed back in service on
December 19. On December 30 the discharge pipe headers on the

west legs of both the Sand and Croatan Formation wells were
partially plugged with 50-60 psig of pressure which normally is
5-10 psig. The headers were flushed and cleaned on December 31.
On January 1 all four discharge pipe headers were flushed and
cleaned with hot condensate and air.
There are some continuing problems with certain wells and pumps:
Confined Sand Formation Withdrawal Wells (SWW)
SWW-1; The well and pump scaled up during October and were out
of service through January 22 pending DEM approval of a cleaning
procedure. The well casing was cleaned with hydrochloric acid
solution on January 22-23 and was returned to service on January
23. The pump cycle counter started malfunctioning on January 27
only counting cycles part of the time.
SWW-2; The pump cycle counter malfunctioned and was replaced on
11/23. The pump scaled up in late November, was replaced with
a spare pump on December 3 and returned to service. The pump
stopped on December 9 and then returned to service on December
12 after the cam assembly air supply valve was repaired. The
pump stopped again on December 16-23 and was restarted on
December 23 by shaking. On January 24 the pump stopped, was
blowing air and had to be shaken to start it. The pump stopped
on January 25 and was removed for cleaning and inspection. The
problem was determined to -be -a -missing -snap ring on"the vent
valve. The cam assembly was replaced and the pump reinstalled
and started up.
SWW-3; The pump stopped on January 31. The discharge pipe to
the main header was found to be plugged.
SWW-4; The pump stopped and was blowing air on January 7. It
was cleaned and returned to service. On January 10 the pump
stopped and had to be shaken to start. On January 21 the pump
stopped, was blowing air and had to be shaken to start.
SWW-5; The pump stopped and was blowing air on December 30. The
snap ring was repaired on the cam assembly and the pump returned
to service.
SWW-6; The pump stopped and had to be shaken to start on
December 10 and 12. The pump stopped and was blowing air on
December 30. The pump was repaired and returned to service.
SWW-7; On January 23 the pump cycle counter malfunctioned only
counting cycles part of the time.
2

Croatan Formation Withdrawal Wells (CWW)
CWW-1; The pump stopped and had to be shaken to start on
December 23, 26 and 27. The cycle counter malfunctioned on
December 30. On January 10, 23, and 27-31 the pump cycle
counter malfunctioned only counting cycles part of the time. On
January 24 the pump stopped, was blowing air and had to be
shaken to start it.
CWW-2; The pump stopped on December 30 and the bottom ball check
valve was found to be plugged. The pump was repaired and
returned to service. On January 2 the pump stopped and had to
be shaken to start it.
CWW-3; The pump stopped and had to be shaken to start on
December 26. On January 10, 13-15, and 23 the pump cycle
counter malfunctioned only counting cycles part of the time. On
January 24 the pump stopped, was blowing air and had to be
shaken to start it.
CWW-4; The pump stopped and had to be shaken to start on
December 5 and 26. The pump stopped on December 30 and the pump
was found to be plugged. The pump was repaired and returned to
service.
CWW-5; The pump stopped and had to be shaken to start on
December 6-, 11, 19 and-20. On January 2, 3, and 6 the pump
cycle counter malfunctioned only counting cycles part of the
time. On January 7 the pump was removed and the counter parts
were cleaned. The pump was returned to service with counter
working. Note: The internal air chamber of this pump was found
to have a heavy oily film, possibly from the air compressor.
CWW-6; The pump stopped and had to be shaken to start on
December 11 and 23.
CWW-7; On January 28 the pump stopped and had to be shaken to
start it.
The withdrawal water well pumps are monitored daily by the area
Maintenance Department and preventative maintenance work is
performed is needed. The total withdrawal water volumes for the
period are:
Sand Formation
Croatan Formation
Total Gallons
November
378,235
209.253
587,488
December
375,516
196.694
January
413,624
194.404
572,210 608,028
Only Totals
1,167,375
600,351
1,767,726

COMPLIANCE', MONITORING,
GROUNDWATER QUALITY, MONITORING:
COMPLIANCE REPORT FORM
n DIVISION OF ENU,lRONMENTAL'IMANAGEMENT'
,, P:0. Box
RALEIGH,NC 2762670535
(919),733-3221.
Facility Name: PCS PHOSPHATE CO. - AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMITNO.: WI0700012
Non -Discharge Tank Farm Remedial System
_Lagoon Septic Tank/Drain Field
_Spray Field =Subsurface Low -Pressure
_Land Appl of Sludge
Well Location: Tank Farm
_Rotary Distributor _x_Ot
Well I.D. Number. INJ. SUPPLY Well Depth: 179.0 Well Depth:
Well Diameter 6" Sample (Screened) Interval N/A
Ft. to N/A Ft.
Depth to Water Level N/A Ft. below meas. pt.(before sampling) or N/A
FL (MSL)
Measuring Point is 1.00 Ft. above land surface or N/A
Ft. (MSL)
Gallons of water pumped/bailed before sampling CONTINUOUS
Field Analysis: pH Specific Conductance
uMhos Temp
oC Odor
Date Sample Collected Date Lab Sample Analyzed
Appearance:
Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No. 330
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
COD mg/1
NO2 as N
mg/1
Ni - Nickel
mg/I
Coliform: ME Fecal N /100m1
NO3 as N N
mg/1
Pb - Lead
N
mg/I
Coliform: MF Total 0 /100m1
Phosphorus: Total as P 0
I
mg/1
Zn - Zinc
0
mg/I
Dissolved Solids: Total T mg/I
AI - Aluminum T
mg/1
Pesticides/Herbicides (Specify)
T
pH (when analyzed) units
Ba - Barium
mg/1
ug/1
TOC A mg/I
Ca - Calcium A
mg/1
A
ug/I
Chloride P mg/1
Cd-Cadmium P
I mg/I
P
ug/1
Arsenic P mg/1
Chromium: Total P
mg/I
Other FLUORIDE
P
mg/1
Grease and Oils L mg/1
Cu - Copper L
mg/I
Other MIRK
L
ug/1
Hardness: Total I mg/I
Fe - Iron I
mg/1
Other Ag - Silver
I
mg/1
Phenol C mg/I
Hg - Mercury C
I mg/I
Other Se -Selenium
C
mg/1
Sulfate A mg/1
K -Potassium A
mg/1
A
ug/I
Specific Conductance B uMohs
Mg - Magnesium B
mg/1
B
. ug/1
Total Ammonia(NH4 + NH3) L mg/I
Mn - Manganese L
mg/I
L
TKN as E mg/I
Na- Sodium E
mg/I
E
Note:
I CERTIFY THAT TH REPORT IS TRUE AND ACCURATE
SIGNATURE OF PERMI EE (OR AUTHORIZED AGENT)
Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
477
DATE
er

CDl. I.ECT; .j AND -ANALYSIS OF GROUIvu'WATER SAMPLES
1 Sou+rIi ;t Should b9 analyzed a:; scroll :II possible alter collection. SAMPLES WHICH ARE ItOT'ANALYSED WITHIN 1HE HOLDING I IME SPECI-
FIED FOR THE METHOD USED (SEE 114. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
2. LIr ' i•::uedyses: 1h;o S1.3nrLurl Method 3030C lor sample preparation (mercury excluded). QQNQI FILTENLvtETALS SAL!PLES_IlI. 111 .i'IEl-I) !!1
h• ' im:d s:3ngd1s roust be I:i IIncred lor metals, then lield acidilied with 5 ml concentrated nitric acid per liter ol sample, and should be submitted to n1'•
Int :itlrin 21 her
`Iample prepandion in the laboratory (extraction and filtration) must be completed within 72 hours'01 collection.
3 AIIr.1.'rSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
GRC'1.IIIUWATER, NOT THOSEIIIAT ARE A BEI OE SEDIMENT ASSQCIAJED VIM WELL CONSTRUCJjON O)j SAME11NG EBQCEDUNES.
CIIECI< WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As I•'s I illy. I5. Hui Ili Carolina Administrative Code. Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of
Ibr I:dlrnvinrl publications, or by other methods approved belorehand by the Director, Division ol Environmental
Mar' (erne' it:
(a) Standard Melhods lor the Examination of Water and Wastewater, 16111 Edition, 1985 and 171h Edition, 1989, published joinlly by
American Public Health Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods lor Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number
EPA 600/4.79.020. as revised March 1983;
(c) Test Methods lor Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986. U.S. Environmental Protection Agency
publication number SW-846;
hi) Test Procedures for the Analysis of Polluanls Under the Clean Water Act, Federal Register Vol. 49. No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the deplli ol water in the well prior to pumping or bailing any water from the well.
6. At least 3 volumes of water in the well should be purnped or bailed prior to collecting a sarnple for analysis. II the well is purnped/bailed dry before 3 well
volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination for pH. Specific Conductance, temperature; odor and appearance must be made in the lield on unfiltered samples when the sample is
collected.
8. Field equipment must be calibrated in accordance with recommendations by the manufacturer.
9. Samples roust be filtered Through a 0.45 micron tiller immediately after collection when a dissolved analysis is required. (See #4. above)
10. The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected.
11.^Authorized agent" is any corporate ollicer or public ollicial authorized by the company, corporation, or governmental body to sign official documents.

COMPLIANCE 'MONITORING.wWi DIVISIONOFENVIRONMENTALIMANAGbMENT
GROUNDWATER QUALITY MONITORING;;,
COMPLIANCE REPORT FORM
POI BOX 2953i5
RALEIGH, NC 27626-0535
1(919) 733/3221
Facility Name: PCS PHOSPHATE CO. - AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: WI0700012
Non -Discharge Tank Fann Remedial System
_Lagoon Septic Tank/Drain Field
_Spray Field =Subsurface Low -Pressure
_Land Appl of Sludge
Well Location : Tank Farm
_Rotary Distributor _x_Ot
Well I.D. Number. CNNV-1 Well Depth: 55.0 Ft.
Well Diameter 4" Sample (Screened) Interval
33.27 Ft. to 52.68 Ft.
Depth to Water Level 7.45 Ft. below meas. pt.(before sampling) or
3.15 Ft. (MSL)
Measuring Point is 2.25 Ft. above land surface or
10.60 Ft. (MSL)
Gallons of water purged before sampling CONTINUOUS
Field Analysis: pH 6.1 Specific Conductance
2217 uMhos Temp 18.4 oC Odor
NONE
Date Sample Collected 01/08/97 Date Lab Sample Analyzed 01/08 - 01/14 1997 Appearance: CLEAR
Laboratory Name: PCS PHOSPHATE ENV. AFFAIRS LAB Certification No. 330 1
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
YES
NO
COD N/A mg/I
NO2 as N
N/A mg/l
Ni - Nickel
N/A mg/I
Coliform: MF Fecal N/A /10om1
NO3 as N
N/A mgA
Pb - Lead
N/A mg/1
Coliform: MF Total N/A /10om1
Phosphorus: Total as P
1.010 mg/I
Zn - Zinc
N/A mg/I
Dissolved Solids: Total 1976 mgA
AI - Aluminum
WA mgll
Pesticides/Herbicides (Specify)
pH (when analyzed) 6.1 units
Ba - Barium
N/A mg/I
-
ug/l
TOC 11.2 mgA
Ca - Calcium
N/A mg/I
ug/l
Chloride 78.6 mg/I
Cd - Cadmium
N/A mg/1
ug/I
Arsenic N/A mg/I
Chromium: Total
N/A mg/I
Other FLUORIDE
0.25 mg/I
Cu - Copper
N/A mgll
Other MIBK
N/A ugll
Grease and Oils N/A mgA
Hardness: Total N/A mg/I
Fe - Iran
N/A mg/I
Other Ag -Silver
N/A mgll
Phenol N/A mg/I
Hg - Mercury
N/A mgA
Other Se -Selenium
N/A mg/1
Sulfate 650.6 mg/1
K - Potassium
N/A mgll
ugA
Specific Conductance • N/A uMohs
Mg - Magnesium
N/A mg/I
ugA
Total Ammonia(NH4 + NH3) N/A mg/I
Mn - Manganese
N/A mg/I
TKN as N N/A mg
Na - Sodium
N/A mg/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
SIGNATURE OF P MITTEE (OR AUTHORIZED AGENT)
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
19(AtA
Date
er

COI.I.EC1L_:I AND ANALYSIS OF GROUI`t 4VATER SAMPLES
I Sou rlrt:t should be analyzed as coon al possible altar collection. SAMPLES WHICH ARE tIOT ANALYSED WITHIN 1HE HOLDING I IME SPECI-
FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED Al4D NEW SAMPLES COLLECTED.
2. far' 'I : l lutlysr:s: I lsn SI.imlard Method 3030C for sample preparation (mercury excluded). LQNQI FILTER_METALS.SAMPLES-lU!'lIl€.I°IELI! !!I
h • ' .: n:rl samples must bu r:,AfecIed for metals. then lield acidified with 5 rnl concentrated nitric acid per liter ol sample, and should be submitted lu nr»
lair •vitliiii 21 hour..
;aniiile preparation in the labor aka y (extraction and lillralion) must be completed within 72 hours of collection.
3 AIIPI.'fSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
GI1i'I.I11UWATETI, NOT THOU. THAT ARE A E EI Of SEDIMENT ASSOCIATED WIIU WELL CONSTFIUCTIQH OH SAMPLING ERQCEDIJUES.
CIIECIC WITH YOUR LABORATORY 014 PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As (•':i 1 illy, 15.110011 Carolina Administrative Code. Subchapter 2L, analytical procedures shall be in accordance with the methods described in one ol
Iht Itillowinq publications, or by other methods approved beforehand by the Director, Division ol Environmental
I•.Lni•ulement:
(al Standard tvlelhods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by
American Public Health Association, American Water Works Association and Water Pollution Control Federation;
Ib) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number
EPA 600/4-79-020, as revised March 1983;
(c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Piolcrtion Agency
publication number SW-846;
(cf) Test Procedures for the Analysis of Polluanls Under the Clean Water Act, Federal Register Vol. 49. No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well.
6. At least 3 volumes of water in the well should be purnped or bailed prior 10 collecting a sarnple for analysis. If the well is purnped/bailed dry before 3 well
volumes are removed. samples can be collected as soon as the well recovers to the point where enough wafer is available to collect your sample.
7. Determination for pH. Specific Conductance, lernperature, odor and appearance must be made in the field on unfiltered samples when the sample is
collected.
8. Field equipment roust be calibrated in accordance with recommendations by the manufacturer.
9. Samples roust be littered Through a 0.45 micron filler immediately alter collection when a dissolved analysis is required. (See 114. above)
I0.Tlie sample container should be labeled at the time ol collection with the facility name, well identification nurnber and dale and lime collected.
11."Authorized agent" is any corporate officer or public olficial authorized by the company, corporation, or governrnenlal body to sign ollicial documents.

COMPLIANCE MONITORING
GROUNDWATER QUALITY MONITORING;,
COMPLIANCE REPORT FORM
DIVISION OE ENVIiONMENTAL'MANAGEMEATI
PO::BOX 29535
RALEIGH, NC 27626-0535
[phone]'
Facility Name: PCS PHOSPHATE CO. - AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: WI0700012
Non -Discharge Tank Farm Remedial System
_Lagoon Septic Tank/Drain Field
_Spray Field =Subsurface Low -Pressure
_Land Appl of Sludge
Well Location: Tank Farm
_Rotary Distributor _x Ot
Well ID. Number. CWW-2 Well Depth: 52.15
Well Depth:
Well Diameter 4" Sample (Screened) Interval
30.57 Ft. to 49.82 Ft.
Depth to Water Level 7.32 Ft. below meas. pt.(before sampling) or
2.91 Ft. (MSL)
Measuring Point is 3.00 Ft. above land surface or
10.23 Ft. (MSL)
Gallons of water pumped/bailed before sampling CONTINUOUS
Field Analysis: pH 6.0 Specific Conductance
2432 ulvmos Temp 18.9
oC Odor
NONE
Date Sample Collected 01/08/97 Date Lab Sample Analyzed
01/08
- 01/14 1997 Appearance:
CLEAR
Laboratory Name: PCS PHOSPHATE ENV. AFFAIRS LAB Certification No.
330
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
I YES
NO
COD N/A mg/1
NO2 as N
N/A mg/1
Ni - Nickel
N/A
mg/I
Coliform: MF Fecal N/A /I00m1
NO3 as N
N/A mg/1
Pb - Lead
N/A
mg/1
Coliform: MF Total N/A /I00m1
Phosphorus: Total as P
35.750 mg/1
Zn - Zinc
N/A
mg/I
Dissolved Solids: Total 2012 mg/1
Al - Aluminum
N/A mg/1
Pesticides/Herbicides (Specify)
pH (when analyzed) 6.1 units
Ba - Barium
N/A mg/1
ug/I
TOC 13.5 mg/1
Ca - Calcium
N/A mg/1
ug/1
Chloride 98.2 mg/1
Cd-Cadmium
N/A mg/I
ug/1
Arsenic N/A mg/I
Chromium: Total
N/A mg/1 .
Other FLUORIDE
0.20
mg/1
Grease and Oils N/A mg/1
Cu - Copper
N/A mg/I
OtherMIBK
N/A
ug/1
Hardness: Total N/A mg/1
Fe - Iron
N/A mg/1
Other Ag -Silver
N/A
mg/1
Phenol N/A mg/1
Hg - Mercury
N/A mg/I
Other Se - Selenium
N/A
mg/1
Sulfate 715.5 mg/1
K- Potassium
N/A mg/1
ug/I
Specific Conductance N/A uMohs
Mg - Magnesium
N/A mg/I
ug/1
Total Ammonia(NH4 + NH3) N/A mg/I
Mn - Manganese
N/A mg/I
TKN as N N/A mg/1
Na - Sodium
N/A mg/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
SIGNATURE OF PERMITT (OR AUTHORIZED AGENT)
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
er

COL I.ECT ".J AND ANALYSIS OF GROUI' j jVATER SAMPLES
sluuld be analyzed as soorr a ; possible altar collecliun. SAMPLES WHICH ARE tIOT ANALYSED WITHIN 1HE HOLDIIIG I IME SPECI-
FIED FOR THE METHOD USED (SEE N4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
2. Llr •I•::'rn; lvsiz: I Mu !.3 Haul I.Ir;Ihod 3030C for sample preparation (eine ry excluded). pQNOT FILTEFILv1ETALS SAfv1P).ES Ijl 1fIE.I1EI-1! !it
'rr r •:n:d s3rrq,Ies must be cr.dlecled for metals. then field acidilied with 5 ml concentrated nilric acid per tiler of sample, and should be suburitted le nr••
!al) vitlrin 24 bees•.
;ample prepmation in the laboratory (extraction and lillralionl must be completed within 72 hours ol collection.
3 AlInl. 1SES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
GRC'I.II IDWATEFI, NOT TIiQSI II1AT Arm A pan' of SEDI SENT ASSQCIATED 7NLI1 WELL CONSTRUCS1QN Ojl SAMPLING PROCEDURES.
CIIECI( WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As (•ui line 15. Nor tl r Carolina Administrative Code. Subchapter 2L, analytical procedures shall be in accordance with the methods described in one ol
Ibc It 'Rowing publications, or by other methods approved beforehand by the Director, Division of Environmental
klnn•u)enrunC
(a) Standard klelhorls lor the Examination of Water and Wastewater, 16th Edition, 1985 and 171h Edition, 1989, published jointly by
American Public Heallh Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods lor Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number
EPA•60014.79.020. as revised March 1983;
(el Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Enviwnmenlal Protection Agency
publication number SW-846;
(d) Test Procedures for the Analysis ol Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the depth ol water in the well prior to pumping or bailing any water from the well.
6. At least 3 volumes of water in the well should be pumped or bailed prior to collectinga sample lor analysis. II the well is purnped/bailed dry before 3 well
volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination lor pH. Specific Conductance, ternperalure, odor and appearance must be made in the Iield on unfiltered samples when the sample is
collected.
8. Field equipment must be calibrated in accordance with recommendations by the manufacturer.
9. Samples must be Iiltered through a 0.45 micron lilter immediately after collection when a dissolved analysis is required. (See 114. above)
10.Tbe sample container should be labeled al the time of collection with the facility name, well identification number and dale and time collected.
11."Authorized agent' is any corporals ollicer or public ollicial authorized by the company, corporation, or governmental body to sign ollicial documents.

SIGNATURE OF PE
COMPLIANCE MONITORING
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
DIVISION OF ENVERONMENTAL MANAGEIvMENC'
P,Os�BOX7,9535,,,,
RALEIGH; NC 27626 0535 1,
[phone]
Facility Name: PCS PHOSPHATE CO. - AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMITNO.: WI0700012
Non -Discharge Tank Famr Remedial System
_Lagoon Septic Tank/Drain Field
_Spray Field =Subsurface Low -Pressure
_Land Appl of Sludge
Well Location: Tank Farm
_Rotary Distributor
_x_Otl
Well ID. Number. CW W-3 Well Depth: 53.00
Ft.
Well Diameter 4" Sample (Screened) Interval
36.42 Ft. to 50.67 Pt.
Depth to Water Level 7.24 Ft. below meas. pt.(before sampling) or
2.71 Ft. (MSL)
Measuring Point is 3.08 Ft. above land surface or
9.95 Ft. (MSL)
Gallons of water pumped/bailed before sampling CONTINUOUS
Field Analysis: pH 6.0 Specific Conductance
2768 uMhos Temp 24.7
oC Odor
NONE
Date Sample Collected 01/08/97 Date Lab Sample Analyzed
01/08
- 01/14 1997 Appearance:
CLEAR
Laboratory Name: PCS PHOSPHATE ENV. AFFAIRS LAB Certification No.
330
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
YES
NO
COD N/A mg/1
NO2 as N
N/A mg/I
Ni - Nickel
N/A
mg/I
Coliform: MF Fecal N/A /100m1
NO3 as N
N/A mg/1
Pb - Lead
N/A
mg/l
Coliform: MF Total N/A /100m1
Phosphorus: Total as P
7.850 mg/I
Zn - Zinc
N/A
mg/1
Dissolved Solids: Total 2156 mg/l
Al - Aluminum
N/A mg/I
Pesticides/Herbicides (Specify)
pH (when analyzed) 6.2 units
Ba - Barium
N/A mg/1
ug/1
TOC 11.7 mg/I
Ca - Calcium
N/A mg/1
ug/1
Chloride 99.6 mg/I
Cd-Cadmium
N/A mg/1
ug/1
Arsenic N/A mg/I
Chromium: Total
N/A mg/1
Other FLUORIDE
0.21
mg/I
Grease and Oils N/A mg/I
Cu - Copper
N/A mg/1
Other MIBK
N/A
ug/I
Hardness: Total N/A mg/1
Fe - Iron
N/A mg/I
Other Ag -Silver
N/A
mg/1
Phenol N/A mg/1
Hg-Mercury
N/A mg/I
Other Se -Selenium
N/A
mg/1
Sulfate 730.5 mg/1
K - Potassium
N/A mg/1
ug/I
Specific Conductance N/A uMohs
Mg - Magnesium
N/A mg/l
ug/1
Total Ammonia(NH4 + NH3) N/A mg/!
Mn - Manganese
N/A mg/l
TKN as N. N/A mg/I
Na-Sodium
N/A mg/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
®;r 1
-4 ITTEE (OR AUTHORIZED AGENT)
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
DATE
er

COI. I.ECT.r
,r:l AND ANALYSIS OF GROUietMATER SAMPLES
I S;un( Intl 511001 be analyzed a:; coon a n possible alter collection. SAMPLES WHICH ARE 110T ANALYSED WITHIN 1HE HOLDII IG 1IME SPECI-
FIED FOR THE METHOD USED (SEE /J4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
2. MO.*: Inlysr:s: t ):;u SLIM lnrd Method 3030C for sample preparation (mercury excluded). QQNQT FILT ELMETALs SAMEhEJIJINIE.I°IEI.I) !!I
14• r •a.:rl 5:3111p4es nu/Si be r: •1Incred for metals, then field acidilied with 5Int concentrated nitric acid per liter ol sample, and should be submitted Ire II
Inlr rillrin21 hems
!)ample preparation in the inbnralory (extraction and filtration) must be completed within 72 hours of collection.
3 All r'.I. •(SES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN TFIE
GM.1.11IUWATER, NOT THO$I I}IAT ARE A PART OE SEDIMENT ASSOCIATED wall WELL CONSTBUCJIQII OB SAMMaiNG PROCEDURES.
CIIECI( WITH YOUR LABORATORY 014 PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As (•is I illn 15. Nor III Carolina Administrative Code. Subchapter 2L, analytical procedures shall be in accordance with the methods described in one ol
Ilit Inlluwinq publications. or by other methods approved belorehand by the Director, Division ol Environmental
Mot ulernenC
(a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17111 Edition, 1989, published jointly by
American Public Health Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number
EPA 60014.79-020, as revised March 1983;
(c) Test Methods lor Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Prolec:lion Agency
publication number SW-846:
(d) Test Procedures for the Analysis ol Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the depth of wafer in the well prior to pumping or bailing any water Irom the well.
6. Al least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample lor analysis. 11 the well is purnped/bailed dry belore 3 well
volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination lor pH. Specilic Conductance, ternperature, odor and appearance must be made in the Iield on unlillered samples when the sample is
collected.
8. Field equipment must be calibrated In accordance with recommendations by the manufacturer.
9. Samples must be littered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See 114. above)
I0.The sample container should be labeled al the lime of collection with the facility name, well identification number and dale and lime collected.
11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governrnentat body to sign official documents.
1

COMPLIANCE', MONITORING'
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
,... :ONMENTACMANAGAMENT4
• P.0.1,130X29535„'�
RALEIGH; NC27626-0535
h mr,i
(919):733-322P
Facility Name: PCS PHOSPHATE CO. - AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: WI0700012
Non -Discharge Tank Farm Remedial System
_Lagoon Septic TanklDrain Field
_Spray Field =Subsurface Low -Pressure
_Land Appl of Sludge
Well Location: Tank Fann
1
_Rotary Distributor _x Ot
Well I.D. Number: CWW-4 Well Depth: 53.00
Ft.
Well Diameter 4" Sample (Screened) Interval
41.67 Ft. to 50.92 Ft.
Depth to Water Level 7.52 Ft. below meas. pt.(before sampling) or
3.21 Ft. (MSL)
Measuring Point is 2.75 Ft. above land surface or
10.73 Ft. (MSL)
Gallons of water pumped/bailed before sampling CONTINUOUS
Field Analysis: pH 6.1 Specific Conductance
2863 uMhos Temp 28.2
oC Odor
NONE
Date Sample Collected 01/08/97 Date Lab Sample Analyzed
01/08
- 01/14 1997 Appearance:
CLEAR
Laboratory Name: PCS PHOSPHATE ENV. AFFAIRS LAB Certification No.
330
AND FIELD ACIDIFIED
YES
NO
SAMPLES FOR METALS WERE COLLECTED UNFILTERED
COD N/A mg/I
NO2 as N
N/A mg/1
Ni - Nickel
N/A mg/1
Coliform: MF Fecal N/A /100m1
NO3 as N
N/A mg/1
Pb - Lead
N/A mg/I
Coliform: MF Total • N/A /100m1
Phosphorus: Total as P
5.550 mg/I
Zn - Zinc
N/A mg/1
Dissolved Solids: Total 2104 mg/I
AI - Aluminum
N/A mg/I
Pesticides/Herbicides (Specify)
pH (when analyzed) 6.3 units
Ba - Barium
N/A mg/I
ug/1
TOC 10.7 mg/1
Ca - Calcium
N/A mg/I
ug/1
Chloride 114.5 mg/I
Cd-Cadmium
N/A mg/1
ug/I
Arsenic N/A mg/l
Chromium: Total
N/A mg/1
Other FLUORIDE
0.15 mg/1
Grease and Oils N/A mg/I
Cu - Copper
N/A mg/l
Other MIBK
N/A ug/I
Hardness: Total N/A mg/1
Fe - Iron
N/A mg/I
Other Ag- Silver
N/A mg/1
Phenol N/A mg/1
Hg - Mercury
N/A mg/1
Other Se - Selenium
N/A mg/I
Sulfate 730.0 mg/1
K - Potassium
N/A mg/I
ug/I
Specific Conductance N/A uMohs
Mg - Magnesium
N/A mg/1
ugh
Total Ammonia(NH4 + NH3) N/A mg/l
Mn - Manganese
N/A mg/1
TKN as N N/A mg/I
Na - Sodium
N/A mg/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
11 �
r
a.
SIGNATURE OF PERMIT E (OR AUTHORIZED AGENT)
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
er

COI.L.EC1,�•;J AND ANALYSIS OF GROUt; WATER SAMPLES
I Saci:i be: slunrld he analyzed a:; soon as possible alter collection. SAMPLES WHICH ARE tIOT ANALYSED WITHIN THE HOLDING I IME SPECI-
FIED FOR THE METHOD USED (SEE 114. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
2. tar' -it.: Analysn:;: I ;so St.u;rfard t.lrahod 3030C for sample preparation pncrcury excluded). RQNOT FILTER r1ETALS SAh1Pl,ES IiINIE.FIELi) !!!
i h• ' .:n:d samples must be collected for metals, Then Iield acidified with 5 ml concentrated nitric acid per liter ol sarnple, and should be submitted to its••
late ••ritlrin 24 hcnrr.
rii )le preparation to the laboratory (extraction and Mallon) must be completed within 72 hours of collection.
:1 Al IN. 1SES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
GII.'I.IIMDWATER, NOT THOS&THAT ARR A EMI OE SEDIMENT ASSOC1ATED WIIU- WELL CONSTB_UCI1Qt4 Og SAMPUN{G EBVCEDUUES.
CIIECI< WITII YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As I•::; line 15. Nu; Ili Carolina Administrative Code. Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of
the I:dlowinrl publications, or by other methods approved belorehand by the Director, Division ol Environmental
kleingenicnt:
(a) Standard Methods for the Examination of Water and Wastewater, 161h Edition, 1985 and 17111 Edition, 1989, published jointly by
American Public Health Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods for Chemical Analysis el Water and Waste, 1979, U.S. Environmental Protection Agency publication number
EPA 600/4-79.020, as revised March 1983;
(c) Test Methods lor Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Ptolnction Agency
publication number SW-846;
(cl) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the depth ol water in the well prior to pumping or bailing any water from the well.
6. Al least 3 volumes of water in the well should be purnped or bailed. prior 10 collecting a sarnple for analysis. II the well is purnped/bailed dry before 3 well
volumes are removed, samples can be collecled as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination lor pH. Specific Conductance, ternperature, odor and appearance must be made in the field on unfiltered samples when the sample Is
collecled.
8. Field equipment must be calibrated in accordance with recommendations by the manufacturer.
9. Samples roust be littered Through a 0.45 micron litter immediately alter collection when a dissolved analysis is required. (See 114. above)
I0.The sample container should be labeled al the time of collection with the facility name, well identification number and dale and time collected.
11."Authorized agent" is any corporate ollicei or public otlicial authorized by the company, corporation, or governmental body to sign official documents.

COMPLIANCE' MONITORING'
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
DIVISION OFENVIRONMENTAL-MANAGEMENT
, P.O.,pOX 295331;.. r
RALEIGa NC 27626-0535
[phone]
Facility Name: PCS PHOSPHATE CO. - AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMITNO.: WI0700012
Non -Discharge Tank Farm Remedial System
_Lagoon Septic TankfOrain Field
_Spray Field =Subsurface Low -Pressure
_Land Appl of Sludge
Well Location: Tank Farm
_Rotary Distributor _x Ot
Well I.D. Number. CWW-5 Well Depth: 53.17
Ft.
Well Diameter 4" Sample (Screened) Interval
41.75 Ft. to 51.08 Ft.
Depth to Water Level 7.32 Ft. below meas. pt.(before sampling) or
3.42 Ft. (MSL)
Measuring Point is 2.58 Ft above land surface or
10.74 Ft (MSL)
Gallons of water pumped/bailed before sampling CONTINUOUS
Field Analysis: pH 6.0 Specific Conductance
2628 uMhos Temp 31.6
oC Odor
NONE
Date Sample Collected 01/08/97 Date Lab Sample Analyzed
01/08
- 01/14 1997 Appearance:
CLEAR
Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No.
330
FIELD ACIDIFIED
YES
NO
SAMPLES FOR METALS WERE COLLECIEU UNFILTERED AND
COD N/A mg/I
NO2 as N
, N/A mg/I
Ni - Nickel
N/A
mg/1
Coliform: MF Fecal N/A /100m1
NO3 as N
N/A mg/1
Pb - Lead
N/A
mg/I
Coliform: MF Total N/A /100m1
Phosphorus: Total as P
7.150 mg/1
Zn - Zinc
N/A
mg/I
Dissolved Solids: Total 1724 mg/I
Al - Aluminum
N/A mg/1
Pesticides/Herbicides (Specify)
pH (when analyzed) 6.5 units
Da - Barium
N/A mg/1
ug/1
TOC 9.9 mg/1
Ca - Calcium
N/A mg/1
ug/I
Chloride 110.4 mg/1
Cd-Cadmium
N/A mg/1
ug/I
Arsenic N/A mgil
Chromium: Total
N/A mg/I
Other FLUORIDE
0.15
mg/1
Grease and Oils N/A mg/I
Cu - Copper
N/A mg/I
Other MIRK
N/A
ug/1
Hardness: Total N/A mg/I
Fe - Iron
N/A mg/1
Other Ag - Silver
N/A
mg/1
Phenol N/A mg/I
Hg- Mercury
N/A mg/I
Other Se - Selenium
N/A
mg/1
Sulfate 559.1 mg/1
K-Potassium
N/A mg/1
ug/I
Specific Conductance N/A uMohs
Mg -Magnesium
N/A mg/1
ug/1
Total Ammonia(NH4 + NH3) N/A mg/I
Mn - Manganese
N/A mg/I
TKN as N N/A mg/1
Na - Sodium
N/A mg/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
SIGNATURE OF PERMITTEE (OR AUTHORIZED AGENT)
er

•
COI. I.ECT ,J AND ANALYSIS OF GROUN'iMATER SAMPLES
I S;url•Irc: slrcudcl be analyzed a:: soon as possible alter collcctiun. SAMPLES WHICH ARE 110T ANALYSED WITHIN THE HOLDING TIME SPECI-
FIED FOR TI-IE METHOD USED (SEE 114. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
2. t.lr' .1.: luralyses: !1st! St.Th:larcl Method 3030C for sample preparation (mercury excluded). LiQNOI FILTU_ ETAL$ SAL!PLES_I1LNIE.I°IELI) !!I
r 4• r'a':rl samples must be cr4fectucl for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be subedited to ar••
lab -.Milli 21 hoary.
;ample preparation in the laboratory (extraction and lillration) must be completed within 72 hours of collection.
:1 AtIr.l.'rSES ARE i0 BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
GRL'i1HDWATEl1, NOT THQSE IHAT ARE A !'ABI OE $EDIT 11LENT ASSOCIATED WITU WELL CONSTBIJC]'1QN OI3 SAMi ELIUG PROCEDURES.
CI IECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
I illy,. 15. Monty Carolina Administrative Code. Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of
II a rollowinq publications. or by other methods approved beforehand by the Director, Division of Environmental
Management:
(a) Standard Methods for the Examination of Water and Wastewater, 16111 Edition, 1985 and 17111 Edition, 1989, published jointly by
American Public Health Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number
EPA 60014-79-020. as revised March 1983;
(e) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmenlal Protu:lion Agency
publication number SW-846;
(d) Test Procedures for the Analysis of Polluanls Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Parl 136,
October 26, 1984;
5. Measure and record the depth of water in the well prior to pumping or bailing any wafer from the well.
6. AI least 3 volumes of water in the well should be purnped or bailed prior to collecting a sarnple lor analysis. II the well is purnped/bailed dry before 3 well
volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination lor pH. Specific Conductance, temperature, odor and appearance must be made in the Iield on unfiltered samples when the sample Is
collected.
8. Field equipment must be calibrated in accordance will, recommendations by the manufacturer.
9. Samples must be lillered Through a 0.45 micron litter immediately alter collection when a dissolved analysis is required. (See #4. above)
I0.The sample container should be labeled al the lime of collection with the facility name, well identification number and dale and time collected.
11."Authorized agent" is any corporate officer or public ollicial authorized by the company, corporation, or governmental body Io sign official documents.

COMPLIANCE.MONITORING
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
fT
DIVISION OF ENVIRONMENTAL MANAGEIMENT'
r 13:11. OX 29535'
R4LEIGH, NC 27626-0535'
( 19) 733-3221'
9
Facility Name: PCS PHOSPHATE CO. - AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMITNO.: WI0700012
Non -Discharge Tank Farm Remedial System
_Lagoon Septic Tank/Drain Field
Spray Field =Subsurface Low -Pressure
_Land Appl of Sludge
Well Location: Tank Farm
_Rotary Distributor
_x Ot
Well I.D. Number: CWW-6 Well Depth: 53.00
Ft
Well Diameter 4" Sample (Screened) Interval
36.62 Ft. to 50.88 Ft.
Depth to Water Level 7.42 Ft. below meas. pt.(before sampling) or
3.18 Ft (MSL)
Measuring Point is 2.92 Ft. above land surface or
9.92 FL (MSL)
Gallons of water pumped/bailed before sampling CONTINUOUS
Field Analysis: pH 6.3 Specific Conductance
1943 uMhos Temp 30.5
oC Odor
NONE
Date Sample Collected 01/08/97 Date Lab Sample Analyzed
01/08
- 01/14 1997 Appearance:
LT YELLOW
Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No.
330
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
YES
NO
COD N/A mg/l
NO2 as N
N/A mg/1
Ni - Nickel
N/A
mg/1
Coliform: MF Fecal N/A /100ml
NO3 as N
N/A mg/l
Pb - Lead
N/A
mg/1
Coliform: MF Total N/A /1o0m1
Phosphorus: Total as P
6.300 mg/1
Zn - Zinc
N/A
mg/1
Dissolved Solids: Total 1232 mg/1
AI - Aluminum
N/A mg/1
Pesticides/Herbicides (Specify)
pH(when analyzed) 6.7 units
Ba- Barium
N/A mg/I
ug/l
TOC 9.4 mg/1
Ca - Calcium
N/A mg/I
ug/1
Chloride 111.8 mg/1
Cd-Cadmium
N/A mg/1
ug/1
Arsenic N/A mg/1
Chromium: Total
N/A mg/1
Other FLUORIDE
0.18
mg/1
Grease and Oils N/A mg/1
Cu - Copper
N/A mg/I
Other MIBK
N/A
ug/1
Hardness: Total N/A mg/I
Fe - Iron
N/A mg/1
Other Ag- Silver
N/A
mg/1
Phenol N/A mg/I
Hg - Mercury
N/A mg/1
Other Se - Selenium
N/A
mg/1
Sulfate 299.9 mg/1
K - Potassium
N/A mg/I
ug/I
Specific Conductance N/A uMohs
Mg - Magnesium
N/A mg/1
ug/1
Total Ammonia(NH4 + NH3) N/A mg/l
Mn - Manganese
N/A mg/1
TKN as N/A mg/l
Na- Sodium
N/A mg/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
SIGNATURE OF PERMITT ' (OR AUTHORIZED AGENT)
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
V79.40
DATE
er

COI. I.ECT., _._I AND ANALYSIS OF GROUI.t. /ATER SAMPLES
Suuf in:: should he analyzer) a:; :;eon a ; possible alter collection. SAMPLES WHICH ARE 110T ANALYSED WITHIN 1HE HOLDING 'I IME SPECI-
FIED FOR THE METHOD IJSED (SEE 114. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
1:Ir•in1•: /'utlyscs: I;;u St.nr:lard!.lethod 3030C lor sample preparation (mercury excluded). IQ.N91 FILTERLdETALS SAMPLES-JJ1. I11E.FIEI_I) !!(
" • ':n:rl s:mq,fes must be adlecled for metals, then field acidified with 5 ml concontraled iritric acid per liter of sample, and should be submitted l' Or•
lali :ithin 21 Irr:un•.
S81111 to piepnr;rtion in the laboratory (extraction and filtration) must be completed within 72 hours of collection.
:1 Allr.l. 1SES ARE 10 BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN TFIE
GI11'UIIDWATER, NOT THOS1IHAT AREA BEI OE SEDIMERT ASSOCIATED WITH WEB CONSTfl C,TjQN OR 5AMPEB
L(NG OCEDULIES.
CI IECI( WITHYOUR LABORATORY OIJ PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As per I ill? 15. North Carolina Administrative Code. Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of
Ihr InIIowing publications. or by other methods approved beforehand by the Director, Division ol Environmental
Eloi Bement:
(a) Standard Methods for the Examination of Water and Wastewater, 16111 Edition, 1985 and 171h Edition, 1989, published jointly by
Arnerican Public Health Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number
EPA 60014.79.020. as revised March 1983;
(c) Test Methods lor Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986. U.S. Environmental Protection Agency
publication number SW-846;
(d) Test Procedures for the Analysis of Polluanls Under the Clean Water Act, Federal Register Vol. 49. No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the deptli ol water in the well prior to pumping or bailing any water born the well.
6. Al least 3 volumes of water in the well should be pumped or bailed prior to collecting a sarnple lor analysis. II the well is pumped/bailed dry before 3 well
volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination lor pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample Is
collected.
8. Field equipment must be calibrated in accordance with recommendations by the manulacturer.
9. Samples must be littered through a 0.45 micron filler immediately alter collection when a dissolved analysis is required. (See 114. above)
I0.The sample container should be labeled al the time ol collection with the facility name, well identification nurnber and date and lime collected.
11."Aulhorizod agent" is any corporate officer or public ollicial authorized by the company, corporation, or governmental body to sign official documents.

COMPLIANCE MONITORING'
GROUNDWATER QUALITY MONITORING;,,,
COMPLIANCE REPORT FORM
DIVISION OF ENVIRONMENTAL�MANAGEMIEN'YI?
29535„
RALEIOH, NC 27626-0535
[phone]'
Facility Name: PCS PHOSPHATE CO. - AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
dll
PERMIT NO.: W10700012
Non -Discharge Tank Farm Remedial System
_Lagoon Septic TankdDrain Field
_Spray Field =Subsurface Low -Pressure
_Land Appl of Sludge
Well Location: Tank Fann
_Rotary
Distributor _x Ot
Well ID. Number: CWW-7 Well Depth: 53.00
Ft.
Well Diameter 4" Sample (Screened) Interval
36.58 Ft. to 50.83 Ft.
Depth to Water Level 7.30 Ft. below meas. pt.(before sampling) or
2.65 Ft. (MSL)
Measuring Point is 1.25 Ft. above land surface or
9.95 Ft. (MSL)
Gallons of water pumped/bailed before sampling CONTINUOUS
Field Analysis: pH 6.4 Specific Conductance
1185 uMhos Temp 23.5
oC Odor
NONE
Date Sample Collected 01/08/97 Date Lab Sample Analyzed
01/08
- 01/14 1997 Appearance:
CLEAR
Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No.
330
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
YES
NO
COD N/A mg/I
NO2 as N
N/A mg/1
Ni - Nickel
N/A
mg/I
Coliform: MF Fecal N/A /100m1
NO3 as N
N/A mg/1
Pb - Lead
N/A
mg/I
Coliform: ME Total N/A /100m1
Phosphorus: Total as P
1.150 mg/I
Zn-Zinc
N/A
mg/1
Dissolved Solids: Total 782 mg/1
Al - Alumimmn
N/A mg/I
Pesticides/Herbicides (Specify)
pH (when analyzed) 6.6 units
Ba - Barium
N/A mg/I
ug/I
TOC 8.1 mg/I
Ca - Calcium
N/A mg/I
ug/I
Chloride 73.1 mg/I
Cd-Cadmium
N/A mg/I
ug/I
Arsenic N/A mg/1
Chromium: Total
N/A mg/1
Other FLUORIDE
0.18
mg/1
Grease and Oils N/A mg/I
Cu - Copper
N/A mg/I
Other MIRK
N/A
ug/I
Hardness: Total N/A mg/I
Fe - Iron
N/A mg/I
Other Ag - Silver
N/A
mg/I
Phenol N/A mg/1
Hg - Mercury
N/A mg/1
Other Se -Selenium
N/A
mg/1
Sulfate 153.9 mg/I
K - Potassium
N/A mg/1
ug/I
Specific Conductance N/A uMohs
Mg - Magnesium
N/A mg/I
ug/l
Total Ammonia(NH4 + NH3) N/A mg/1
Mn - Manganese
N/A mg/I
TKN as N N/A mg/1
Na - Sodium
N/A mg/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
SIGNATURE OF PERMITTEE +R AUTHORIZED AGENT)
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
DATE
er

�UL I.ECT 1 AND ANALYSIS OF GROUk.iWATER SAMPLES
I Far (lee:, 51ruuld he analyzed a:; :;non as possible alter collection. SAMPLES WHICH ARE IIOT ANALYSED WITHIN 1HE HOLDIIIG 'I IME SPECI-
FIED FOR THE METHOD IJSED (SEE Ili. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
2. 61r" '1•: A'ialcsi:s: Ilse SLiiIflartl 1.lelhod 3030C for sample preparation (mercury excluded). paNOT FILTER_METALS SAh1PLES-Ij!'iHE FIEI.I) !!!
' rr 1 ':n:rl samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter ol sample, and should be submitted lu rip.
Inle tl;in 2.1 Itcne::
Trento preparation in the laboratory (extraction and filtration) must be completed within 72 hours ol collection.
3 AlII'1 t'SES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
GIC1.II IIJWATER, NQT THOSI THAT ARC A j?ABI OE $EDIMEENT ASSQC AJED Vim WELL CONSTBUCSIQN on SAMajNG PROCEDURES.
CIIECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As per 1 illy. 15. Nor Ili Carolina Administrative Code. Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of
II t I:dlowinq publications, or by other methods approved beforehand by the Director, Division ol Environmental
Ll;nrulemenl:
(a) Standard Methods tor the Examination of Water and Wastewater, 161h Edition, 1985 and 171h Edition, 1989, published jointly by
American Public Health Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number
EPA 600/479-020, as revised March 1983;
(c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Proteclion Agency
publication number SW-846;
(d) Test Procedures Tor the Analysis ol Polluanls Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well.
6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sarnple for analysis. II the well is pumped/bailed dry before 3 well
volumes are removed, sarnples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination for pH. Specilic Conductance, temperature, odor and appearance must be made in the lield on unfiltered samples when the sample is
collected.
8. Field equipment must be calibrated In accordance with recommendations by the manufacturer.
9. Samples roust be littered through a 0.45 micron Tiller immediately alter collection when a dissolved analysis is required. (See 114. above)
10. The sample container should be labeled al the time ol collection with the facility name, well identification nurnber and dale and lime collected.
11."Authorizod agent" is any corporate ollicer or public ollicial authorized by the company, corporation, or governrnental body to sign ollicial documents.

COMPLIANCE, MONITORING
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
� s
DIVISION OFt` ��..
FNYBiONMENTAL:MANAGEIvff.NT.
P 01E0X 29535,
RALEIGH, NC 27626 0535.
[phone]
Facility Name: PCS PHOSPHATE CO. - AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMITNO.: WI0700012
Non -Discharge Tank Farm Remedial System
_Lagoon Septic Tank/Drain Field
_Spray Field =Subsurface Low -Pressure
_Land Appl of Sludge
Well Location: Tank Farm
Rotary Distributor
_x_Ot
Well ID. Number. SWW-1 Well Depth: 22.5
Well Depth:
Well Diameter 4" Sample (Screened) Interval
N/A
Ft. to N/A Ft.
Depth to Water Level N/A Ft. below meas. pt.(befare sampling) or
N/A
Ft. (MSL)
Measuring Point is 1.42 Ft. above land surface or
N/A
Ft. (MSL)
Gallons of water pumped/bailed before sampling CONTINUOUS
Field Analysis: pH Specific Conductance
uMhos Temp
oC Odor
Date Sample Collected Date Lab Sample Analyzed
Appearance:
Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No.
330
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
COD mg/1
NO2 as N
mg/1
Ni - Nickel
mg/I
Coliform: MF Fecal N /100ml
NO3 as N
N
mg/1
Pb - Lead
N
mg/I
Coliform: MF Total 0 /100m1
Phosphorus: Total as
D
mg/I
Zn - Zinc
0
mg/I
Dissolved Solids: Total T mg/1
Al - Aluminum
T
mg/1
Pesticides/Herbicides (Specify)
T
pH (when analyzed) units
Ba - Barium
mg/1
ug/l
TOC S mg/I
Ca - Calcium
S
mg/I
5
ug/1
Chloride A mg/I
Cd - Cadmium
A
mg/I
A
ug/I
Arsenic M mg/I
Chromium: Total
M
mg/1
Other FLUORIDE
M
mg/1
Grease and Oils P mg/1
Cu-Copper
P
mg/1
OtherMIBK
P
ugf
Hardness: Total L mg/1
Fe - Iran
L
mg/1
Other Ag -Silver
L
mg/I
Phenol E mg/1
Hg - Mercury
E
mg/I
Other Se -Selenium
E
mg/I
Sulfate D mg/1
K-Potassium
D
mg/I
D
ug/1
Specific Conductance uMohs
Mg - Magnesium
mg/I
ug/1
Total Ammonia(NH4 + NH3) mg/1
Mn - Manganese
mg/1
TKN as mg/I
Na-Sodium
mg/1
Note:
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
SIGNATURE OF PERMITTEE (OR AUTHORIZED AGENT)
Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
AAIA
DATE
er

COI. I.ECT•_,_1 AND ANALYSIS OF GROUII.•4VATER SAMPLES
I Sal in:: 5Iumid be analyzed a:; ;;crop a ; passible alter collection. SAMPLES WHICH ARE HOT ANALYSED WITHIN 1HE HOLDIIIG 'I IME SPECI-
FIED FOR TIIE METHOD USED (SEE N4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
2. 1.1r' 'r•: Arralysi: ,: 1h;o S!..urrlard Method 3030C for sample preparation (mercury excluded). QQ_NOI FIL1FEL 1ETAL5SAMPLES_IIt.1IIE.EIELI) Ill
h• ' 'a,:d sangdrs roust be cillnciecf for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be subu'inecf Lr nI'•
latI •:ithin 24 Irene:
''angle preparation to the laboratory 'extraction and filtration) roust be completed within 72 hours ol collection.
3 All"i. 1SES ARE 1'0 BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
GII.'I1I IDWATEtt, NOT TFIOSE THAT ARE A EALI Of SEDIMENT ASSOCIATED WITH WELL CONSTfiCSjQN OB SANEUNG PROCEDURES.
CIIECI( WITII YOUR LABORATORY 011 PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As I•'rr I ill! 15. I Irnllr Carolina Administrative Code. Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of
the I:,Ilnwinll publications, or by other methods approved belorehand by the Director, Division ol Environmental
I l;nr- gerrienL
(a) Standard Methods lor the Examination of Water and Wastewater, 16th Edition, 1985 and 17111 Edition, 1989, published jointly by
American Public Health Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods lor Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number
EPA 60014.79.020, as revised March 1983;
(c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmenlal Prolec:lion Agency
publication number SW-846;
(ci) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well.
6. At (east 3 volumes of water in the well should be purnped or bailed prior to collecting a sarnple lor analysis. II the well is purnped/bailed dry before 3 well
volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7., Determination lor pH. Specific Conductance, temperature, odor and appearance must be made in the lield on unfiltered samples when the sample is
collected.
8. Field equipment must be calibrated in accordance with recommendations by the manufacturer.
9. Samples must be littered Through a 0.45 micron liller immediately alter collection when a dissolved analysis is required. (See I14. above)
I0.Tho sample container should be labeled al the time ol collection with the facility name, well identification number and dale and lime collected.
11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governrnenlal body to sign official documents.

1'�• ( 1
COMPLIANCE 'MON ITORI N G Drvismii OF ENVIRONMENTAL MANAGENf6i7P
GROUNDWATER LeyALITY MONITORING: Po Boxz9s3s;
RALEIGH; NC27626' 0535)
(919)733'd3221 ,
COMPLIANCE REPORT 'FORM,
Facility Name: PCS PHOSPHATE CO. - AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMITNO.: WI0700012
Non -Discharge Tank Farm Remedial System
_Lagoon Septic Tank/Drain Field
_Spray Field =Subsurface Low -Pressure
_Land Appi of Sludge
Well Location: Tank Farm
Rotary
Distributor _x Ot
Well I.D. Number: SWW-2
Well Depth: 23 Ft.
Well Diameter 4"
Sample (Screened) Interval
18.80
Ft. to 21.63 Ft.
Depth to Water Level
8.36
Ft. below meas. pt.(before sampling) or
1.63
Ft. (MSL)
Measuring Point is
3.42
Ft. above land surface or
9.99
Ft. (MSL)
Gallons of water pumped/bailed before sampling
CONTINUOUS
Field Analysis: pH
5.9
Specific Conductance
2235
uMhos Temp 19.7 oC Odor
NONE
Date Sample Collected
01/08/97
Date Lab Sample Analyzed
01/08-01/14
1997 Appearance: CLEAR
Laboratory Name: PCS PHOSPHATE ENV. AFFAIRS LAB Certification No.
330
SAMPLES FOR METALS WERE COLLECTED
AND FIELD ACIDIFIED
YES
NO
UNFILTERED
COD
N/A
mg/l
NO2 as N
N/A
mg/1
Ni -Nickel
N/A
mg/I
Coliform: MF Fecal
N/A
/100ml
NO3 as N
N/A
mg/I
Pb - Lead
N/A
mg/1
Coliform: MF Total
N/A
/100m1
Phosphorus: Total as P
273.000
mg/1
Zn - Zinc
N/A
mg/1
Dissolved Solids: Total
1856
mg/I
Al - Aluminum
N/A
mg/1
Pesticides/Herbicides (Specify)
pH (when analyzed)
5.9
units
Ba - Barium
N/A
mg/1
ug/1
TOC
12.8
mg/I
Ca - Calcium
N/A
mg/l
ug/I
Chloride
83.9
mg/1
Cd-Cadmium
N/A
mg/1
ug/I
Arsenic
N/A
mg/I
Chromium: Total
N/A
mg/I
Other FLUORIDE
0.22
mg/1
Grease and Oils
N/A
mg/l
Cu - Copper
N/A
mg/1
Other MIBK
N/A
ug/l
Hardness: Total
N/A
mg/1
Fe - Iron
N/A
mg/1
Other Ag -Silver
N/A
mg/1
Phenol
N/A
mg/1
Hg - Mercury
N/A
mg/1
Other Se - Selenium
N/A
mg/I
Sulfate
545.1
mg/1
K - Potassium
N/A
mg/1
ug/I
Specific Conductance
N/A
uMohs
Mg - Magnesium
N/A
mg/I
ug/I
Total Ammonia(N114 + NH3)
N/A
mg/I
Mn - Manganese
N/A
mg/I
Note: Values should reflect total concentrations
TKN as N
N/A
mg/1
Na - Sodium
N/A
mg/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
SIGNATURE OF PERMITTEE (O AUTHORIZED AGENT)
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
019.2b
DAT
her

COI.I.ECT,::4 AND ANALYSIS OF GROUkLYGVATER SAMPLES
I Smiq•Ire: should be analyzed a:: soon ail possible aller collection. SAMPLES WHICH ARE IIOT ANALYSED WITHIN 1HE HOLDING IIME SPECI-
FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
Llr' 'I•::'rnnl} s ;: tau SL.ii u hint I.Irahod 3030C for sample preparation pncrcwy excluded). PQNQI FILTEFI METALS SAMPLES -If i I f IE. i!ELil !!!
h• 1 ':n:rl samples ems! be r:r..11rtcied for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be subnrilied Ir1 mr•
lalr •rilhin 21 Ileum
;amble preparation in the laboratory (exitaction and Iillralion) must be completed within 72 hours of collection.
:1 AtIP-I. •ISES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
GI1C'I.IIIDWATEft, NOT THOSI I)1AT ARE A I AEI OE $EDIT 1EENT ASSOCIATED WITU WELL CONST.BUCILQN OB SAMi ELING QRQCEDULIES.
CI IECK WITH YOUR LABORATORY 011 PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As NI I ill? 15. Ruth Carolina Administrative Code. Subcliapter 2L, analytical procedures shall be in accordance with the rnetlrods described in one of
II r 'Aiming publications, or by other methods approved beforehand by the Director, Division of Environmental
t.•nru)enront:
(a) Standard Methods for the Examination of Water and Wastewater, 161h Edition, 1985 and 171h Edition, 1989, published jointly by
American Public Health Association, American Water Works Association and Water Pollution Control Federalion;
(b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number
EPA 600/4.79•020, as revised March 1983;
(c) Test Methods for Evaluating Solid Wasles: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency
publication number SW-846;
(d) Test Procedures for the Analysis ol Polluants Under the Clean Water Act, Federal Register Vol. 49. No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the depth ol water in the well prior to pumping or bailing any water from the well.
6. Al least 3 volumes of water in Ilse well should be pumped or bailed prior to collecting a sarnple for analysis. If the well is pumped/bailed dry before 3 well
volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination for pH. Specilic Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample Is
collected.
8. Field equipment roust be calibrated in accordance with recommendations by the manufacturer.
9. Samples rrrusl be lillered through a 0.45 micron filler immediately eller collection when a dissolved analysis is required. (See 114. above)
I1.The sample container should be labeled al the time ol collection with the facility name, well identification number and date and time collected.
11."Arthorizod agent" is any corporate ollicer or public ollicial authorized by the company, corporation, or governrnenlal body to sign ollicial documents.

COMPLIANCE', MONITORING'
GROUNDWATER QUALITY MONITORING:
COMPLIANCE 'REPORT FORM
DIVISION OF ENVIRONMENTAL MANAGEMENT
P.OBOX 29535.
RALEIGH, NC 27626-0535.
. „ i(919) 733-323I
Facility Name: PCS PHOSPHATE CO. - AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMITNO.: WI0700012
Non -Discharge Tank Farm Remedial System
_Lagoon Septic Tank/Drain Field
_Spray Field =Subsurface Low -Pressure
Land Appl of Sludge
Well Location: Tank Farm
_Rotary Distributor _x_Ot
Well I.D. Number: SWW-3 Well Depth: 24.5 Ft.
Well Diameter 4" Sample (Screened) Interval
20.17
Ft. to 23.0 Ft.
Depth to Water Level 7.74 Ft. below meas. pt.(before sampling) or
2.23
Ft. (MSL)
Measuring Point is 3.17 Ft. above land surface or
9.97
Ft. (MSL)
Gallons of water pumped/bailed before sampling CONTINUOUS
Field Analysis: pH 5.9 Specific Conductance
1828
uMhos Temp 25.9
oC Odor
NONE
Date Sample Collected 01/08/97 Date Lab Sample Analyzed
01/08-01/14
1997 Appearance:
CLEAR
Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No.
330
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
YES
NO
COD N/A mg/I
NO2 as N
I N/A
mg/1
Ni - Nickel
N/A
mg/I
Coliform: MF Fecal N/A /100mt
NO3 as N
I N/A
mg/1
Pb - Lead
N/A
mg/I
Coliform: MF Total N/A /100m1
Phosphorus: Total as P
84.000
mg/1
Zn - Zinc
N/A
mg/1
Dissolved Solids: Total 1252 me
AI - Aluminum
N/A
mg/1
Pesticides/Herbicides (Specify)
pH (when analyzed) 6.0 units
Ba - Barium
N/A
mg/1
ug/1
TOC 13.1 mg/1
Ca - Calcium
N/A
mg/1
ug/1
Chloride 55.3 mg/1
Cd - Cadmium
N/A
mg/1
ug/1
Arsenic N/A mg/I
Chromium: Total
N/A
mg/1
Other FLUORIDE
0.11
mg/1
Grease and Oils N/A mg/1
Cu-Copper
N/A
mg/1
Other MIRK
N/A
ug/1
Hardness: Total N/A mg/1
Fe - Iron
N/A
mg/1
Other Ag - Silver
N/A
mg/l
Phenol N/A mg/1
Hg - Mercury
N/A
mg/1
Other Se -Selenium
N/A
mg/1
Sulfate 502.0 mg/1
K - Potassium
N/A
mg/1 -
ug/1
Specific Conductance N/A uMohs
Mg - Magnesium
I N/A
mg/I
ug/1
Total Ammonia(NH4 + NH3) N/A mg/1
Mn - Manganese
N/A
mg/1
TKN as N/A mg/1
Na- Sodium
N/A
mg/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
SIGNATURE OF PERMITTE (OR AUTHORIZED AGENT)
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
er

COI. I.ECTv .J AND ANALYSIS OF GROUP. VATER SAMPLES
slruuld be analyzed a:; soon al possible alter collection. SAMPLES WHICH ARE 110T ANALYSED WITHIN THE HOLDING I IME SPECI-
FIED FOR TIIE METHOD USED (SEE 114. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
2. ear' 4•:Ise SLuulnrd I.Iolhod 3030C for sample preparation (mercury excluded). fQNu FILTERJ1ETALS SAf,1PLE5J1I."1�IE.1°IELI) !!!
• ' ':e:d sarq,les must be erAlected for metals, then Iield acidified with 5 rnl concentrated nitric acid per liter of sample, and should be submitted Ikr a ••
lali ••:itliin 24 Ireurr.
;ample orepalarion in the laboratory (extraction and filtration) must be completed within 721rours ol collection.
3 AIIr!. 7SES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
GIIU.'I.IIIUWATER, NOT THOS& IIiAT ARE A BAB' OE SEDIf ILIEI,iT ASSOCIATED WIILI WELL CONSTRUCIIQN OB SAMELING ERPCEDURES.
CIIECI( WITH YOUR LABORATORY 011 PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As ref I itln 15. North Carolina Administrative Code. Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of
the I:dlowinrl publications, or by other methods approved beforehand by the Director, Division ol Environmental
klai lement:
(rl) Standard blethocls for the Examination of Water and Wastewater, 16111 Edition, 1985 and 171h Edition, 1989, published jointly by
Arnerican Public Health Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number
EPA"60014.79.020. as revised March 1983;
(c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency
publication number SW-846;
(d) Test Procedures for the Analysis ol Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the depth ol water in the well prior to pumping or bailing any water Irorn the well.
6. At least 3 volumes of water in the well should be pumped or bailed prior 10 collecting a sarnple for analysis. II the well is purnped/bailed dry before 3 well
volumes are removed, sarnples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination for pH. Specific Conductance, temperature, odor and appearance must be made in the Iield on unfiltered samples wlien the saiiiple Is
collected.
0. Field equipment must be calibrated in accordance will recommendations by the manufacturer.
9. Samples must be filtered through a 0.45 micron filter immediately alter collection when a dissolved analysis is required. (See #4. above)
I0. Tho sample container should be labeled at the lime of collection with the facility name, well identification number and dale and lime collected.
11."Aulhorized agent" is any corporate ollicer or public ollicial authorized by the company, corporation, or governmental body to sign otlicial documents.

COMPLIANCE, MONITORING DivisioNOPENVIRONMENTAL MANAGEMENT
GROUNDWATER QUALITY MONITORINGi
COMPLIANCE REPORT FORM
P,.O:BOX 295}Sa Ib
RALEIGH TjC 27626-OS35'
(919)7.133226
Facility Name: PCS PHOSPHATE CO. - AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMITNO.: WI0700012
Non -Discharge Tank Fenn Remedial System
_Lagoon _Septic Tank/Drain Feld
_Spray Field _Subsurface Low -Pressure
Land Appl of Sludge
Well Location: Tank Farm
Rotary Distributor :Other
Well LD. Number. SWW-4
Well Depth: 25 Ft.
Well Diameter 4"
Sample (Screened) Interval
20.50
Ft. to 23.3 Ft.
Depth to Water Level 7.37
Ft. below meas. pt.(before sampling) or
3.36
Ft. (MSL)
Measuring Point is 3.42
Ft. above land surface or
10.73
Ft. (MSL)
Gallons of water pumped/bailed before sampling
CONTINUOUS
Field Analysis: pH 5.7
Specific Conductance
2282
uMhos Temp 33.7 oC Odor
NONE
Date Sample Collected 01/08/97
Date Lab Sample Analyzed
01/08-01/14
1997 Appearance: CLEAR
Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No.
330
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
YES
NO
COD N/A
mg/1
NO2 as N
N/A
mg/1
Ni -Nickel
N/A
mg/1
Coliform: MF Fecal N/A
/100m1
NO3 as N
N/A
mg/1
Pb - Lead
N/A
mg/I
Coliform: MF Total N/A
/100m1
Phosphorus: Total as P
122.500
mg/1
Zn - Zinc
N/A
mg/I
Dissolved Solids: Total 1488
mg/1
Al - Aluminum
N/A
mg/I
Pesticides/Herbicides (Specify)
pH (when analyzed) 5.8
units
Ba-Barium
N/A
mg/I
ug/1
TOC 9.6
mg/1
Ca - Calcium
N/A
mg/1
ug/1
Chloride 61.4
mg/1
Cd-Cadmium
N/A
mg/1
ug/1
Arsenic N/A
mg/I
Chromium: Total
N/A
mg/1
Other FLUORIDE
0.07
mg/1
Grease and Oils N/A
mg/1
Cu-Copper
) N/A
mg/1
Other MIBK
N/A
ug/1
Hardness: Total N/A
mg/1
Fe - Iron
N/A
mg/1
Other Ag - Silver
N/A
mg/1
Phenol N/A
mg/1
Hg - Mercury
N/A
mgil
Other Se -Selenium
N/A
mg/I
Sulfate 544.8
mg/I
K- Potassium
N/A
mg/1
ug/1
Specific Conductance N/A
uMohs
Mg - Magnesium
N/A
mg/I
ug/1
Total Ammonia(NH4 + NH3) N/A
mg/1
Mn - Manganese
N/A
mg/I
Note: Values should reflect total concentrations
TKN as N N/A
mg/I
Na - Sodium
N/A
mg/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
SIGNATURE OF PERMITTED (OR AUTHORIZED AGENT)
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
DAT

2.
COI. I.ECT: -.1 AND ANALYSIS OF GROUt'hcMATER SAMPLES
Smith:: should be analyzed as soon al possible alter collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN 1HE HOLDING 'I IME SPECI-
FIED FOR THE METHOD USED (SEE tl4. BELOW) MUST BE DISCARDED AIID NEW SAMPLES COLLECTED.
tar-' 'I•::'rn;ilvsi:s: rise SIa;Ll;ruI Method 3030C for sample preparation (mercury excluded). QQNQI FILT I_METALS SAMPLES Jiang.FIEI.O !!!
h • ' ':n:rl s:3111,les Horst be collected Ior metals. then Iteld acidified with 5 ml concentrated nitric acid per liter ol sample, and should be submitted to nr.•
loll •.ilhin 21 Irer -
`rample preparation fir the Laboratory (extraction and filtration) must be completed within 72 hours of collection.
:1 AI II't'tSES ARE i0 BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
GII:'11NUWATER, NOT THQS&IHAT ARg A EABI0E SEDIMEtiT ASSOCIATED Wall WELL CONSTBUC.TI(_B Oj3 SM4EE NG PRQCEDULlES.
CIIECI( WITII YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As f•':r I itle 15. North Carolina Administrative Code. Subcliapter 2L, analytical procedures shall be in accordance with the methods described in one of
Ihr I:Mewing publications. or by other methods approved beforehand by the Director, Division of Environmental
El;ingenrenl:
(a) Standard Methods for the Examination of Water and Wastewater, lfith Edition, 1985 and 171h Edition, 1989, published jointly by
American Public Health Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number
EPA 600/4-79-020, as revised March 1983;
(c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986. U.S. Environmental Pro
tr:r:liorr Agency
publication number SW-846;
(d) Test Procedures lor the Analysis of Polluanls Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CPR Part 136,
October 26, 1984;
5. Measure and record the depth ol water in the well prior to pumping or bailing any water from the well.
6. At least 3 volumes of water in the well should be purnped or bailed prior to collecting a sarnple for analysis. II the well is purnped/bailed dry before 3 well
volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination for pH, Specific Conductance, lernperalure, odor and appearance must be made in the field on unfiltered samples when the sample is
collected.
8. Field equipment must be calibrated in accordance with recommendations by the manufacturer.
9. Samples must be littered through a 0.45 micron tiller immediately alter collection when a dissolved analysis is required. (See #4. above)
10.TIre sample container should be labeled al the time ol collection with the fa ility name, well identification nurnber and dale and time collected.
11."Aulliorizod agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign ollicial documents.
i

COMPLIANCEMONITORING � '} ntvi'sioi OFENvuioNLENTAi:!MwnGritazit
GROUNDWATER QUALITY MONITORING;: . I' P.g.B0X29535
COMPLIANCE, REPORT FORM
[phone]
Facility Name: PCS PHOSPHATE CO. - AURORA DIVISION County: BEAUFORT
Address P 0 BOX 48 AURORA, NC 27806
PERMIT NO.: WI0700012
Non -Discharge Tank Farm Remedial System
_Lagoon Septic Tank/Drain Field
Spray Field =Subsurface Low -Pressure
_Land Appl of Sludge
Well Location: Tank Fann
_Rotary Distributor _x_Ot
Well ID. Number: SWW-5 Well Depth: 28.21
Well Diameter 4" Sample (Screened) Interval
24.83
Ft. to 27.2 Ft.
Depth to Water Level 7.77 Ft. below meas. pt.(before sampling) or
3.03
Ft. (MSL)
Measuring Point is 2.96 Ft. above land surface or
10.80
Ft. (MSL)
Gallons of water pumped/bailed before sampling CONTINUOUS
Field Analysis: pH 5.8 Specific Conductance
2395
uMoos Temp 30.3
oC Odor
NONE
Date Sample Collected 01/08/97 Date Lab Sample Analyzed
01/08-01/,14
1997 Appearance:
CLEAR.
Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No.
330
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
YES
NO
COD N/A mg/I
NO2 as N
N/A
mg/I
Ni - Nickel
N/A mg/1
Coliform: MF Fecal N/A /100m1
NO3 as N
N/A
mg/I
Pb - Lead
N/A mg/I
Coliform: MF Total N/A /100m1
Phosphorus: Total as P
88.500
mg/1
Zn - Zinc
N/A mg/1
Dissolved Solids: Total 1452 mg/I
Al - Aluminum
N/A
mg/I
Pesticides/Herbicides (Specify)
pH (when analyzed) 6.0 units
Ba - Barium
N/A
mg/I
ug/I
TOC 11.8 mg/1
Ca - Calcium
N/A
mg/I
ug/I
Chloride 84.4 mg/I
Cd - Cadmium
N/A
mg/1
ug/I
Arsenic N/A mg/1
Chromium: Total
N/A
mgll
Other FLUORIDE
0.23 mg/I
Grease and Oils N/A mg/I
Cu - Copper
N/A
mg/1
Other MIBK
N/A ug/I
Hardness: Total N/A mg/1
Fe - Iron
N/A
mg/I
Other Ag -Silver
N/A mg/1
Phenol N/A mg/I
Hg - Mercury
N/A
mg/1
Other Se - Selenium
N/A mg/I
Sulfate 567.4 mg/I
IC - Potassium
N/A
mg/1
ug/1
Specific Conductance N/A uMohs
Mg - Magnesium
N/A
mg/1
ug/I
Total Ammonia(NH4 + N113) N/A mg/I
Mn - Manganese
N/A
mg/I
TKN as N/A mg/1
Na- Sodium
N/A
mg/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
SIGNATURE OF PERMITTEE R• R AUTHORIZED AGENT)
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
er

COL I.ECT. ,1 AND ANALYSIS OF GROUI•:.•vVATER SAMPLES
I Snug•lus sl torrid he analyzeda:; suon al possible alter collodiumSAMPLES WHICH ARE 110T ANALYSED WITHIN THE HOLDIIIG TIME SPECI-
FIED FOR TI-IE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
2. b(rh•ir•: 'uialvses: I: se t=1..uelard I.(rahod 3030C for sample preparation (mercury excluded). PQNQj FILTEHLIETALS SAMPI,ESIj1.1JIE.FIELU !!!
r q• 1 •:r .rl s:3mple;; mull bu rollecled lot metals, then field acidified with 5 ml concentrated liil(ic acid per lifer of sample, and should be submitted lir nr••
lal•;ilhin 24 Irene;.
`;ample preparation in the iabnrilmy (extraction and filtration) must be completed within 721rours ol collection.
3 Aill. YSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
GI1C'I•IIIDWATER, NOT MPS" IHAT ARE A PAEI Of SEDIMENT ASSQCIA[ED WITH WELL CONSTBDCIjQN OH MMELING ERQCEDUHES.
CI IECIC WITH YOUR LABORATORY 011 PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As pis I illy. I5. North Carolina Administrative Code. Subchapter 2L, analytical procedures shall be in accordance with the methods described in one o1
Ihr I;llluwinr) publications, or by other methods approved belorehand by the Director, Division ol Environmental
klnn-u)eroent:
(al Standard Mellrods for the Examination of Water and Wastewater, 16111 Edition, 1985 and 171h Edition, 1989, published jointly by
American Public Health Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number
EPA•600/4••79-020, as revised March 1983;
(c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency
publication number SW-846;
(d) Test Procedures for the Analysis of Poltuants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the depth ol water in the well prior to pumping or bailing any water from the well.
6. At least 3 volumes of water in the well should be purnped or bailed prior to collecting a sarnpie for analysis. II the well is purnped/bailed dry before 3 well
volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination for pH, Specilic Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample Is
collected.
8. Field equipment roust be calibrated in accordance with recommendations by the manufacturer.
9. Samples must be filtered through a 0.45 micron liller immediately alter collection when a dissolved analysis is required. (See #4. above)
I0.Tlre sample container should be labeled al the time ol collection with the facility name, well identification nurnber and date and lime collected.
11."Aulhorized agent" is arty corporate otlicer or public ollicial authorized by the company, corporation, or governmental body to sign official documents.
.z---

COMPLIANCE MONITORING
GROUNDWATER QUALITY MONITORING:,
COMPLIANCE. REPORT FORM
' DMSIONbOF ENVIRONMENTAL':MANAO]EPT'
P:o; BOX2953si
RALEIGII NC 27626-0535'
(919)13343221
Facility Name: PCS PHOSPHATE CO. - AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: WI0700012
Non -Discharge Tank Farm Remedial System
Lagoon _Septic Tank/Drain Field
_Spray Field _Subsurface Low -Pressure
_Laid Appl of Sludge
Well Location: Tank Farm
Rotav Distributor .Omer
Well I.D. Number: SWW-6
Well Depth: 26 Ft.
Well Diameter 4"
Sample (Screened) Interval
22.25
Ft. to 24.62 Ft.
Depth to Water Level 7.14
Ft. below meas. pt.(before sampling) or
3.52
Ft. (MSL)
Measuring Point is 2.58
Ft. above land surface or
10.66
Ft. (MSL)
Gallons of water pumped/bailed before sampling
CONTINUOUS
Field Analysis: pH 6.1
Specific Conductance
1943
uMhos Temp 30.8 oC Odor
NONE
Date Sample Collected 01/08/97
Date Lab Sample Analyzed
01/08-01/14
1997 Appearance: CLEAR
Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No.
330
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
YES
NO
COD N/A
mgil
NO2 as N
N/A
mg/1
Ni - Nickel
N/A
mg/I
Colifonn: MF Fecal N/A
/100m1
NO3 as N
N/A
mg/1
Pb - Lead
N/A
mg/1
Coliform: MF Total N/A
/100m1
Phosphorus: Total as P
14.500
mg/I
Zn - Zinc
N/A
mg/1
Dissolved Solids: Total 1156
mg/1
Al - Aluminum
WA
mg/1
Pesticides/Herbicides (Specify)
pH (when analyzed) 6.3
units
Ba-Barium
1 N/A
mg/1
ug/1
TOC 11.7
mg/1
Ca - Calcium
N/A
mg/I
ug/1
Chloride 111.9
mg/1
Cd - Cadmium
N/A
mg/1
ug/1
Arsenic N/A
mg/1
Chromium: Total
N/A
mg/I
Other FLUORIDE
0.09
mg/I
Grease and Oils N/A
mg/I
Cu-Copper
N/A
mg/I
Other MIBK
N/A
ug/1
Hardness: Total N/A
mg/1
Fe - Iran
N/A
mg/I
Other Ag -Silver
N/A
mg/1
Phenol N/A
mg/1
Hg - Mercury
N/A
mg/I
Other Se -Selenium
N/A
mg/1
Sulfate 291.4
mg/I
K-Potassium
N/A
mg/1
ug/1
Specific Conductance N/A
uMohs
Mg - Magnesium
N/A
mg/1
ug/1
Total Ammonia(NH4 + NH3) N/A
mg/1
Mn - Manganese
N/A
mg/1
Note: Values should reflect total concentrations
TKN as N N/A
mg/1
Na - Sodium
N/A
mg/1
Note:
I CERTIFY THAT THIS R PORT IS TRUE AND ACCURATE
SIGNATURE OF PERMITT E (OR AUTHORIZED AGENT)
Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
WC? -,
DATE

COI. I.ECT; _•_J AND ANALYSIS OF GROUT -"WATER SAMPLES
I Sanviii:: should be analyzed a:; soon ail possible: alter collection. SAMPLES WHICH ARE 110T ANALYSED WITHIN 1HE HOLDIIIG I IME SPECI-
FIED FOR TI-IE METHOD IJSED (SEE /M. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
2. I.Ir•' +I-: A'';rlysils: I Ino St.)nrlurcl Method 3030C !Or sample preparation (mercury excluded). NQNOI FILTER METALS SAMPLES_I)1.'1f IE.FIELD !!!
' h• ' .,n,l s:mrples must brr cc'llecled for metals, Then lield acidilied with 5 ml concentrated nitric acid per liter of sarnple, and should be submitted Iu sir••
Ialr •vithin 21 Iran::
Rangde preparation in the laboratory (extraction and filtration) must be cornploled within 721rours of collection.
AIIP I. iSES ARE 10 BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN TIIE
G11.'IJIiDWATER, NOT THOSE I)1AT AFiE A JQf1i OE SEDIMENZ ASSOCIATED WITH WELL CONSTBDCIj0JJj Ofl AWN PLING ERQCEDUBES.
CI IECIC WITH YOUR LABORATORY 014 PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As I•'n I ills 15. Nurllr Carolina Administrative Code. Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of
ll it lnllowinrl publications, or by other methods approved beforehand by the Director, Division ol Environmental
I•.1nn•ulemcnl:
(a) Standard Methods lor the Examination of Water and Wastewater, 161h Edition, 1985 and 171h Edition, 1989, published jointly by
American Public Health Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods tor Chemical Analysis ol Water and Waste, 1979, U.S. Environmental Protection Agency publication number
EPA 60014-79-020. as revised March 1983;
(c) Test Methods lor Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Proteclion Agency
publication number SW-846;
(d) Test Procedures for the Analysis of Polluanls Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the depth ol water in the well prior to pumping or bailing any water from the well.
6. At least 3 volumes of water in the well should be purnped or bailed prior to collecting a sarnple for analysis. If the well is purnped/bailed dry before 3 well
volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination lor pH. Specilic Conductance, ternperalure, odor and appearance must be made in the lield on unfiltered samples when the sample is
collected.
8. Field equipment must be calibrated in accordance with recommendations by the manufacturer.
9. Samples must be littered through a 0.45 micron liller immediately alter collection when a dissolved analysis is required. (See #4. above)
10. The sample container should be labeled at the lime ol collection with the facility name, well identification number and dale and time collected.
11. "Aulhorized agent" is any corporate ollicer or public ollicial authorized by the company, corporation, or governmental body to sign olliclal documents.

COMPLIANCE MONITORING
GROUNDWATER QUALITY MONITORING
COMPLIANCE REPORT FORM
DIVISION OF ENVIRONMENTALMANAGEMENT
ll i P,O.BOX 29535
RALEIGH NC 27626-0535
[phone]
Facility Name: PCS PHOSPHATE CO. - AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: WI0700012
Non -Discharge Tank Farm Remedial System
Lagoon _Septic Tank/Drain Feld
_Spray Field Subsurface Low -Pressure
Land Appl of Sludge
Well Location: Tank Fann
Roomy Distributor _ Other
Well I.D. Number. SWW-7
Well Depth: 29.5 Ft.
Well Diameter 4"
Sample (Screened) Interval
25.17
Ft. to 27.50 Ft.
Depth to Water Level 7.04
Ft. below meas. pt.(before sampling) or
3.66
Ft. (MSL)
Measuring Point is 3.00
Ft. above land surface or
10.70
Ft. (MSL)
Gallons of water pumped/bailed before sampling
CONTINUOUS
Field Analysis: pH 5.6
Specific Conductance
1322
uMhos Temp 25.7 oC Odor
NONE
Date Sample Collected 01/08/97
Date Lab Sample Analyzed
01/08-01/i14
1997 Appearance: CLEAR
Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No.
330
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
YES
NO
COD N/A
mg/I
NO2 as N
N/A
mg/1
Ni -Nickel
N/A
mg/I
Coliform: MF Fecal N/A
/100m1
NO3 as N
N/A
mg/I
Pb - Lead
N/A
mg/I
Coliform: ME Total N/A
/100m1
Phosphorus: Total as P
50.000
mg/1
Zn - Zinc
N/A
mg/1
Dissolved Solids: Total 904
mg/I
Al - Aluminum
N/A
mg/1
Pesticides/Herbicides (Specify)
pH (when analyzed) 5.8
units
Ba - Barium
N/A
mg/I
ug/I
TOC 15.3
mg/1
Ca - Calcium
N/A
mg/I
ug/I
Chloride 102.2
mg/I
Cd-Cadmium
N/A
mg/l
ug/1
Arsenic N/A
mg/I
Chromium: Total
N/A
mg/1
Other FLUORIDE
0.11
mg/I
Grease and Oils N/A
mg/1
Cu-Copper
N/A
mg/1
Other MB3K
N/A
ug/1
Hardness: Total N/A
mg/1
Fe - Iron
N/A
mg/1
Other Ag - Silver
N/A
mg/I
Phenol N/A
mg/1
Hg - Mercury
N/A
mg/1
Other Se -Selenium
N/A
mg/1
Sulfate 237.6
mg/1
K- Potassium
N/A
mg/I
ug/1
Specific Conductance N/A
uMohs
Mg - Magnesium
N/A
mg/1
ug/1
Total Ammonia(NH4 + NH3) N/A
mg/1
Mn - Manganese
N/A
mg/I
Note: Values should reflect total concentrations
TKN as N N/A
mg/I
Na - Sodium
N/A
mg/I
Note:
I CERTIFY THAT THIS REPT IS TRUE AND ACCURATE
SIGNATURE OF PE TTEE R AUTHORIZED AGENT)
Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
daz(n
DATE

COI.I.ECT_.1 AND ANALYSIS OF GROUP.°- DATER SAMPLES
I Siun! bat shu,kl be analyzed a:; SUen a l possible alter collection. SAMPLES WHICH ARE tIOT ANALYSED WITHIN 1HE HOLDING 1IME SPECI-
FIED FOR THE METHOD USED (SEE 114. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
2. t;lr I•: !uudvsrs: I ISO S!.i:Irl;utl I.Iulhod 3030C for sample preparation (mercury excluded). !QNQT FILTER_METALS SAMPI,ESJjt.NIE.11EI.0 !!(
r h" r ';n;rl samples must be collected Inc metals, Then field acidified wills 5 ml concentrated nitric acid per liter ol sample, and should be submitted to r h.•
I;dr :illrin 24 Item!:
Sample preparation in the Inbnrrkny (extraction and lillralion) must be completed within 72 hours ol collection.
:1 At IN. "rSES ARE i0 BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
GII:'1IIlUWATEtI, NQT THOSE D-1AT ARE A pABi OE SEDIMENT ASSOCIATED WITU WELL CONST 1lUCSjO 0E1 SAMPLING PROCEDURES.
CI IECIC WITII YOUR LABORATORY 014 PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As piu line 15. Neill' Carolina Administrative Code. Subchapter 2L, analytical procedures shall be in accordance with the methods described in one ol
Ihr It dkxvin!( puhlicalions, or by other methods approved beforehand by the Director, Division ol Environmental
P.l:rn•ulemenC
(al Standard Methods lor the Examination of Water and Wastewater, 161h Edition, 1985 and 17111 Edilion, 1989, published jointly by
American Public Health Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods tor Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number
EPA 60014.79-020, as revised March 1983;
(c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency
publication number SW-846;
(d) Test Procedures for the Analysis ol Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the depth ol water in the well prior to pumping or bailing any wafer from the well.
6. Al least 3 volumes of water in the well should be purnped or bailed prior to collecting a sarnple lor analysis. If the well is purnped/bailed dry before 3 well
volumes are removed, sarnples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination lor pH. Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is
collected.
8. Field equipment must be calibrated in accordance with recommendations by the manufacturer.
9. Samples must be filtered Through a 0.45 micron Titter immediately alter collection when a dissolved analysis is required. (See 114. above)
10. The sample container should be labeled al the ling of collection with the Iacitity name, well idenlilicalion number and dale and lime collected.
11."Authorized agent" is any corporate ollicer or public ollicial authorized by the company, corporation, or governmental body to sign ollicial documents.

COMPLIANCEMONITORING
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
' DIVISION OF ENVIRONMENTALMANAGEMENT'
P 0,43,9X 29533
RALEIGH, NC 2762610535,
(9193 733 3221
Facility Name: PCS PHOSPHATE CO. - AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: WI0700012
Non -Discharge Tank Farm Remedial System
_Lagoon Septic Tank/Drain Field
_Spray Field =Subsurface Low -Pressure
_Land Appl of Sludge
Well Location: Tank Fann
_Rotary Distributor _x Ot
Well I.D. Number. MWTF1-A Well Depth: 6.4
Ft
Well Diameter 2" Sample (Screened) Interval
3.40
Ft. to 5.40 Ft
Depth to Water Level • 0.00 Ft. below meas. pt.(before sampling) or
10.49
Ft. (MSL)
Measuring Point is 0.00 Ft. above land surface or
10.49
Ft. (MSL)
Gallons of water purged before sampling 5.6
Field Analysis: pH 6.8 Specific Conductance
563
uMhos Temp 14.6
oC Odor
NONE
Date Sample Collected 01/13/97 Date Lab Sample Analyzed
01/13-01/15
1997 Appearance:
CLEAR
Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No.
330
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
X YES
NO
COD N/A mg/I
NO2 as N
N/A
mg/1
Ni - Nickel
N/A
mg/1
Coliform: MF Fecal N/A /100m1
NO3 as N
N/A
mg/1
Pb - Lead
N/A
mg/1
Coliform: MF Total N/A /100m1
Phosphorus: Total as P
0.275
mg/I
Zn - Zinc
N/A
mg/1
Dissolved Solids: Total 516 mg/1
Al - Aluminum
N/A
mg/1
Pesticides/Herbicides (Specify)
pH (when analyzed) 7.1 units
Ba - Barium
N/A
mg/I
ug/1
TOC 5.0 mg/1
Ca - Calcium
N/A
mg/1
ug/I
Chloride 13.5 mg/1
Cd-Cadmium
N/A
mg/1
ug/1
Arsenic N/A mg/1
Chromium: Total
N/A
mg/1
Other FLUORIDE
2.53
mg/1
Grease and Oils N/A mg/1
Cu - Copper
N/A
mg/I
Other MBK
N/A
ug/1
Hardness: Total N/A mg/I
Fe - Iron
N/A
mg/1
Other Ag - Silver
N/A
mg/I
Phenol N/A mg/1
Hg - Mercury
N/A
mg/1
Other Se - Selenium
N/A
mg/1
Sulfate 44.8 mg/1
K - Potassium
N/A
mg/1
ug/1
Specific Conductance N/A uMohs
Mg - Magnesium
N/A
mg/1
ug/1
Total Ammonia(NH4 + NH3) N/A mg/1
Mn - Manganese
N/A
mg/1
TKN as N N/A mg/1
Na - Sodium
N/A
mg/I
Note: Purge Volume in Gallons for this sampling * Static level to Top of Casing
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
SIGNATURE OF PEA fITTEE (O-IAUTHORIZED AGENT)
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
i
er

COI.I.ECT;,;,1 AND ANALYSIS OF GROUlccivIATER SAMPLES
I Suuq•Ii::: should he analyzed a:; :;uon a; possible alter collection. SAMPLES WHICH ARE 110T ANALYSED WITHIN 1HE HOLDIIIG TIME SPECI-
FIED FOR TFIE METHOD USED (SEE 114. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
2. Lii.1 'I ::uralvscs: usu Stile ;l Method 3030C lor sample preparation Itncrcury excluded). QQ-NOT FILTEFILdETAL5 SAMP1:ES uill(E. FIELD !!)
rr• r ,i.:rl 53nrptes nursl bu r:r,Ileeted for metals, Then field acidified with 5 ml concentrated niuic acid per liter of sample, and should be subedited lu nr••
I;ilr fthfn 21 beer:
`sample preparation Mille laboratory (extraction and filtration) must be completed within 72 hours of collection.
AIIr I.1SES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
GIIL'I.IIIUWATER, NOT THOS1IHAT ARE A BEI OF SEDIMENT ASSOCIATED WITH WELL CONSTBLIC-TIQN 08 SAMEUNG ERQCEDUUES.
CIIECI< WITH YOUR LABORATORY 011 PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As t•i,r I file. 15. North Carolina Adminislralive Code. Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of
Ihr t;,lluwind publications, or by other methods approved beforehand by the Director, Division of Environmental
1.1;+n utenumrt:
(al Standard Methods for Ike Examination of Water and Wastewater, 161h Edition, 1985 and 171h Edition, 1989, published jointly by
Arnerican Public Health Association, American Water Works Association and Water Pollution Control Federalion;
(b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number
EPA 60014-79.020, as revised March 1983;
(c) Test Methods lor Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Ptotecliorn Agency
publication number SW-846;
(c1) 'Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the depth oI water in the well prior to pumping or bailing any wafer from The well.
6. At least 3 volumes of water in the well should be purnped or bailed prior 10 collecting a sample for analysis. If the well is purnped/hailed dry before 3 well
volumes are removed, sarnples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination for pH. Specific Conductance, temperature, odor and appearance must be made in the Iield on unfiltered samples when the sample Is
collected.
8. Field equipment must be calibrated in accordance with recommendations by the manulaclurer.
9. Samples must be filtered through a 0.45 micron litter immediately alter collection when a dissolved analysis is required. (See 114. above)
I0.The sample container should be labeled at the lime of collection with the facility name, well identification number and dale and time collected.
11."Authorized agent" is any corporate officer dr public ollicial authorized by the company, corporation, or governmental body to sign official documents.

it �n
COMPLIANCE MONITORING L I DIVISIONOF ENVI[tONMENTi1L"MANA4,MENT:
GROUNDWATER QUALITY MONITORING; �N r r.O.BOEY29535,
COMPLIANCE REPORT'FORM, RALEIGH,NC276260535
[phone]
Facility Name: PCS PHOSPHATE CO. - AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: WI0700012
Non -Discharge Tank Farm Remedial System
_Lagoon Septic Tank/Drain Field
Spray Field =Subsurface Low -Pressure
Land Appl of Sludge
Well Location: Tank Fann
Rotary
Distributor _x_Ot
Well I.D. Number: MWTF1-B Well Depth: 13.10
Ft.
Well Diameter 2" Sample (Screened) Interval
10.60
Ft to 12.60 Ft
Depth to Water Level 0.60 Ft. below meas. pt.(before sampling) or
9.90
Ft. (MSL)
Measuring Point is 0.00 Ft. above land surface or
10.50
Ft (MSL)
Gallons of water purged before sampling 11.4
Field Analysis: pH 6.0 Specific Conductance
831
uMhos Temp 20.1
oC Odor
NONE
Date Sample Collected 01/13/97 Date Lab Sample Analyzed
01/13-01/,15
1997 Appearance:
CLEAR.
Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No.
330
FIELD ACIDIFIED
X YES
NO
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND
COD N/A mg/1
NO2 as N
N/A
mg/1
Ni - Nickel
N/A
mg/1
Coliform: MF Fecal N/A /100m1
NO3 as N
N/A
mg/I
Pb - Lead
N/A
mg/1
Coliform: MF Total N/A /loom!
Phosphorus: Total as P
7.483
mg/I
Zn - Zinc
N/A
mg/I
Dissolved Solids: Total 740 mg/1
Al - Aluminum
N/A
mg/I
Pesticides/Herbicides (Specify)
pH (when analyzed) 6.5 units
Ba - Barium
N/A
mg/1
ug/I
TOC 4.4 mg/1
Ca - Calcium
N/A
mg/l
ug/1
Chloride 32.7 mg/I
Cd - Cadmium
N/A
mg/1
ug/1
Arsenic N/A mg/1
Chromium: Total
N/A
mg/I
Other FLUORIDE
1.76
mg/l
Grease and Oils N/A mg/I
Cu - Copper
N/A
mg/1
Other MIBK
N/A
ug/I
Hardness: Total N/A mg/I
Fe - Iron
N/A
mg/1
Other Ag - Silver
N/A
mg/l
Phenol N/A mg/1
Hg - Mercury
N/A
mg/1
Other Se - Selenium
N/A
mg/1
Sulfate 203.4 mg/1
K- Potassium
N/A
mg/I
ug/1
Specific Conductance N/A uMohs
Mg - Magnesium
N/A
mg/I
ug/I
Total Ammonia(NH4 + NH3) N/A mg/I
Mn - Manganese
N/A
mg/1
TKN as N N/A mg/1
Na - Sodium
N/A
mg/1
Note: Purge Volume in Gallons for this sampling * Static level to Top of Casing
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
1/
SIGNATURE OF ER ITTE
R,AUTHORIZED AGENT)
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
oathi
er

COL I.ECI = _1 AND ANALYSIS OF GROUk. JVATER SAMPLES
I S ui l b. Should be analyzed a:; tarorizil possible alter collection. SAMPLES WHICH ARE tIOT ANALYSED WITHIN THE HOLDIIIG TIME SPECI-
FIED FOR THE METHOD USED (SEE q4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
2. LIr r l•::'cnalysr;:;: use Stamlaid I.lolhod 3030C lor sample preparation (mercury excluded). QQNOT FILTERLv1ETALs SAMPLESJjlTJIE_11ELI) !!!
ur '':n:(l samples must bee r:oflected for metals, then field acidified with 5 rnl concentrated nitric acid per liter of sample. and should be submitted lu al
fah ithin 24 hem::
`)angrle preparation in the laboratory (extraction and filtration) must be completed within 72 hours ol collection.
AtlAi. 'SES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
GIt.'I.IHUWATEH, NOT TH05N jjiAT ARE A BEI OE SEDIMENT ASSQCIATED WITH WELL CONSjMJCJjQN ON SAMPLING PROCEDURES.
CIIECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As )•.a I illy. 15. hlortlr Carolina Administrative Code. Subchapter 2L, analytical procedures shall be in accordance with the methods described in one ol
Ill t:rllowinO puhlicalions, or by other methods approved belorehand by the Director, Division ol Environmental
1.In1•uiemumL•
(a) Standard Melliods lor the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by
American Public Health Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods lor Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number
EPA 60014.79-020, as revised March 1983;
(c) Test Methods lor Evaluating Solid Wasles: Physical/Chemical Methods, 3rd Edilion, 1986, U.S. Environmental Protu:tion Agency
publication number SW-846;
(c1) Test Procedures for the Analysis ol Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the deplli of water in the well prior to pumping or bailing any wafer from the well.
6. At least 3 volumes of water in the well should be purnped or bailed prior to collecting a sarnple lor analysis. If the well is purnped/bailed dry belore 3 well
volumes are removed, sarnples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination for pH. Specilic Conductance, temperature, odor and appearance must be made in the lield on unfiltered samples when the sample is
collected.
8. Field equipment must be calibrated in accordance with recommendalions by the manufacturer.
9. Samples roust be Iillered through a 0.45 micron tiller immediately alter collection when a dissolved analysis is required. (See #4. above)
10. The sample container should be labeled at the time of collection with the facility name, well identification number and dale and time collected.
11."Authorized agent" is any corporate ollicer or public ollictal authorized by the company, corporation, or governmental body to sign ollicial documents.

('i
COMPLIANCE, MONITORING
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
DIVISIONOF ENVIRONb1ENTAL MANAGEMENT
P.O. BOX 29535,
RALEIGH, NC 27626-0535,1
[phone]
Facility Name: PCS PHOSPHATE CO. - AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: WI0700012
Non Discharge Tank Farm Remedial System
_Lagoon Septic Tank/Drain Field
_Spray Field —Subsurface Low -Pressure
_Land Appl of Sludge
Well Location: Tank Faun
_Rotary Distributor
x_011
Well I.D. Number: MWTFI-C Well Depth: 41.20
Ft.
Well Diameter 2" Sample (Screened) Interval
38.70 Ft. to 40.70 Ft.
Depth to Water Level 3.16 Ft. below meas. pt.(before sampling) or
7.33 Ft. (MSL)
Measuring Point is 0.00 Ft. above land surface or
10.49 FL (MSL)
Gallons of water purged before sampling** 34.25
Field Analysis: pH 6.8 Specific Conductance
878 uMhos Temp 25.6
oC Odor
NONE
Date Sample Collected 01/13/97 Date Lab Sample Analyzed
01/13-01/30 1997 Appearance:
CLEAR
Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No.
330 (PCS Env Lab), 102 (Metals and Colifonn)
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
X YES
NO
COD N/A mg/1
NO2 as N
N/A ' mg/1
Ni - Nickel
N/A
mg/I
Colifonn: MF Fecal N/A /loom!
NO3 as N
N/A I mg/I
Pb - Lead
N/A
mg/1
Coliforrn: MF Total • POS/POS/NEG /100m1
Phosphorus: Total as P
0.150 1 mg/I
Zn-Zinc
N/A
mg/
Dissolved Solids: Total 668 mg/1
Al - Aluminum
N/A ' mg/I
Pesticides/Herbicides (Specify)
pH (when analyzed) 6.7 units
Ba - Barium
N/A mg/I
ug/I
TOC 4.7 mg/I
Ca - Calcium
N/A mg/I
ug/I
Chloride 13.1 mg/I
Cd-Cadmium
<0.5 ppb
ug/I
Arsenic N/A mg/1
Chromium: Total
<5.0 ppb
Other FLUORIDE
L41
mg/I
Grease and Oils N/A mg/I
Cu - Copper
N/A mg/1
Other MBK
N/A
ug/I
Hardness: Total N/A mg/1
Fe - Iron
N/A mg/1
Other Ag - Silver
N/A
mg/I
Phenol N/A mg/1
Hg- Mercury
N/A mg/1
Other Se -Selenium
N/A
mg/1
Sulfate 191.8 mg/I
K-Potassium
N/A mg/I
ug/I
Specific Conductance N/A uMohs
Mg - Magnesium
N/A mg/1
ug/I
Total Ammonia(NH4 + NH3) N/A mg/1
Mn - Manganese
0.03 ppm
TKN as N/A mg/1
Na- Sodium
N/A mg/I
Note: Micro -Purge System used for Samplit Initial Sample PositivelResample Negative ** Volume purged in gallons due to static water level.
Note: This well returned two (2) positive coliform results. After sample two (2), the well casing was raised 6" to alleviate any surface water intrusion.
A subsequent sample came back negative.
I CERTIFY THAT IS REM'
` TRUE AND ACCURATE
SIGNATURE OF PER T IT E (OR AIbTHORIZED AGENT)
Note: Values should reflect dissolved and
colloids cons ntrations. (see #3 on back)
DAT
er

CUI.i.EC11G.. AND ANALYSIS OF GROUN:,.•VATER SAMPLES
F' ;null: should he analyzed a:; scion as possible altar collection. SAMPLES WHICH ARE IIOT ANALYSED WITHIN 1HE HOLDING IME SPECI-
FIED FOR TIME METHOD IJSED (SEE 114. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
;+n;dc si:s: Ism Si..uelard Method 3030C lor sample preparation (mrrcury excludeilj. QQNOT FILTE_yLAETALs SAfv1PI,ES.IJI'IjIE.FIELII !!!
h r mans' samples nmsl be collected for metals, Then lield acidilied will' 5 rnl concentrated rrihic acid per liter ol sample, and should be subedited II: Iti•'
I ti ••rilhin 21 Irr:nr.-.
!I:1mph! preparation in the him:alory 104:action and filtration) roust be completed within 72 hours of collection.
3 AIIPI. 1SES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
Gl1C'I II IUWATER, NOT T110S& TAT Aqf A Mu OE SEDI EHI ASSQCIATED WITH WELL CONST&UCJIQN OH SAMPLING I'Ii)CFDUI1E$.
CI IECK WITII YOUR LABORATORY 014 PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As I•N:r I isle. 15. I ler III Carolina Administrative Code. Subchapter 2L, analytical procedures shall be in accordance with the methods described in one ol
Ihr It 'Rowing publications. or by other methods approved beforehand by the Director, Division ol Environmental
!.L+rrulemurrL
(al Standard Methods lot the Examination of Water and Wastewater, 16111Edilion, 1985 and 171h Edilion, 1989, published joinlly by
American Public Heallh Association, American Water Works Association and Water Pollution Conlrol Federalion;
(b) Methods lor Chemical Analysis of Water and Waste, 1979, U.S. Environmenlal Protection Agency publication number
EPA 600;4-79.020, as revised March 1983;
(cl Tesl Methods lor Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency
publication number SW-846;
Oil Test Procedures for the Analysis of Polluanls Under the Clean Water Act, Federal Register Vol. 49. No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the depth of water in the well prior to pumping or bailing any water Irorn the well.
6. AI least 3 volumes of water in the well should be pumped or bailed prior 10 collecting a sarnple for analysis. II the well is purnpedibailed dry before 3 well
volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Delerruinalion lor pH. Specilic Conductance, temperature, odor and appearance must be made in the lield on unlillered samples when the sample Is
collected.
8. Field equipment must be calibrated in accordance with recommendations by the manulaclurer.
9. Samples must be filtered through a 0.45 micron filler immediately alter collection when a dissolved analysis is required. (See #4. above)
I0. The sample container should be labeled at the tithe of collection with the Iacilily name, well iclentilicalion number and dale and lime collected.
11."Authorized agent' is any corporate officer or public ollicial authorized by the company, corporation, or governmental body to sign ollicial documents.

COMPLIANCE MONITORING
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
IDMSION OF ENVIRONMENTAL MANAGEMENT
,P.O. BOX 2955;
RALEIGN, NC 27626-0535.
[phone]
Facility Name: PCS PHOSPHATE CO. - AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMITNO.: WI0700012
Non -Discharge Tank Farm Remedial System
Lagoon Septic Tank/Drain Field
=Spray Field —Subsurface Low -Pressure
_Land Appl of Sludge
Well Location: Tank Farm
_Rotary Distributor _x_Ot
Well I.D. Number. WLCT Well Depth: n/a
Well Diameter n/a Sample (Screened) Interval
n/a Ft. to n/a Ft.
Depth to Water Level n/a Ft. below meas. pt.(before sampling) or
n/a Ft. (MSL)
Measuring Point is n/a FL above land surface or
n/a Ft. (MSL)
Gallons of water pumped/ailed before sampling CONTINUOUS
Field Analysis: pH 7.0 Specific Conductance
435 uMhos Temp 12.5
oC Odor
NONE
Date Sample Collected 01/13/97 Date Lab Sample Analyzed
1/13-1/30 1997 Appearance:
CLEAR
Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No.
330 (PCS Env. Lab) and 78 ( Colifonn & Metals)
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
X YES
NO
COD N/A mg/1
NO2 as N
N/A mg/I
Ni - Nickel
N/A
mg/I
Coliform: MF Fecal N/A /I00m1
NO3 as N
N/A
mg/I
Pb - Lead
N/A
mg/1
Colifonn: MF Total NEG /100m1
Phosphorus: Total as P
0.030 I
mg/1
Zn - Zinc
N/A
mg/1
Dissolved Solids: Total 508 mg/1
Al - Aluminum
N/A I
mg/1
Pesticides/Herbicides (Specify)
pH (when analyzed) 7.3 units
Ba - Barium
N/A
mg/I
ug/1
TOC 5.0 mg/1
Ca - Calcium
N/A
mg/1
ugf
Chloride 12.9 mg/I
Cd - Cadmium
<0.5
ppb
ug/1
Arsenic N/A mg/I
Chromium: Total
<5.0
ppb
Other FLUORIDE
0.68
mg/1
Grease and Oils N/A mg/l
Cu - Copper
N/A
mg/I
Other MBK
N/A
ug/l
Hardness: Total N/A mg/I
Fe - Iron
N/A
I mg/1
Other Ag - Silver
N/A
mg/1
Phenol N/A mg/I
Hg - Mercury
N/A
mg/1
Other Se - Selenium
N/A
mg/1
Sulfate <10 mg/1
K-Potassium
N/A mg/1
ug/1
Specific Conductance N/A uMohs
Mg -Magnesium
N/A mg/l
ug/I
Total Ammonia(NH4 + NIB) N/A mg/1
Mn - Manganese
<0.01 ' ppm
TKN as N N/A mg/I
Na - Sodium
N/A mg/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
SIGNATURE OF PERMITTIr'E (OR AUTHORIZED AGENT)
Note:
Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
alig"7
AT
er

COI.AND ANALYSIS OF GROUhc WATER SAMPLES
I Sauq•In:: should be analyzed a:; soon al possible alter collection. SAMPLES WHICH ARE 1IOT ANALYSED WITHIN 1HE HOLDIIIG'I IME SPECI-
FIED FOR TIIE METHOD USED (SEE f14. BELOW) MUST BE DISCARDED AIID NEW SAMPLES COLLECTED.
I:Ir i•: iuudvsi: ,: I Ise SI. If hid Method 3030C for sample preparation pncrcury excluded). PQNQT FILTER METAL5SAMPI,ES_Ij1.N(E.EIELI) 1!!
4• r 4r':rl samples must be r:nffecied for metals, then field acidified with 5 MI concentrated nitric acid per liter of sample, and should be submitted Irr nr..
tali •vithin 21 hymn
;augrle preparation in the Laboratory (extraction and filtration) must be completed within 72 hours of collection.
3 AlIN. 'rSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
G11.'IJNUWATER, NOT THOSgIFIAT ARE A EMI OE SEDI1INERT ASSOCIATED WITH WELL.CONSTRUCJjQy Og SAI PING PROCEDURES.
CI IECK WITII YOUR LABORATORY 014 PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As f»:r I illy. 15. florIIr Carolina Administr alive Code. Subchapter 2L, analytical procedures shall be in accordance with the rnelhods described in one ol
Ilu Iollowinc) publications, or by other methods approved beforehand by the Director. Division of Environmental
Morr•utement:
(a) Standard Methods for the Examination ol Water and Wastewater, 16111 Edition, 1985 and 17Ih Edition, 1989, published jointly by
American Public Health Association, American Water Works Association and Water Pollulion Control Federalion;
(b) Methods for Chemical Analysis ol Water and Waste, 1979, U.S. Environmental Proleclion Agency publication nunrbei
EPA 60014•79-020, as revised March 1983;
(c) Tesl Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Proleclion Agency
publication publication number SW-846;
(d) Test Procedures for the Analysis ol Polluants Under the Clean Water Act, Federal Register Vol. 49. No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the deplh of waler in the well prior to pumping or bailing any water Irom the well.
6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sarnple for analysis. If the well is pumped/bailed dry before 3 well
volumes are removed, sarnples can be collected as soon as the well recovers to the point where enough water is available 10 collect your sample.
7. Determination for pH. Specific Conductance, ternperature, odor and appearance must be made in the Iield on unliltered samples when the sample is
collected.
8. Field equipment must be calibrated in accordance with recommendations by the manufacturer.
9. Samples must be Iillered through a 0.45 micron filler immediately alter collection when a dissolved analysis is required. (See #4. above)
10. The sample container should be labeled at the lime of collection with the facility name, well identification number and dale and time collected.
11."Authorized agent" is any corporale ollicer or public ollicial authorized by the company, corporation, or governrnental body to sign ollicial documents.

COMPLIANCE MONITORING'
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
DIVISION1OF ENVIRONMENTAL MANAGEMENT
i„P.O. BOA{ 2935
RALEIGH, NC 27626=0535.
_ _.. 919) 733 3221
Facility Name: PCS PHOSPHATE CO. - AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMITNO.: WI0700012
Non Discharge Tank Farm Remedial System
_Lagoon Septic Tank/Drain Field
_Spray Field =Subsurface Low -Pressure
_Land Appl of Sludge
Well Location: Tank Farm
•
_Rotary Distributor x Otl
Well I.D. Number: CIW-7 Well Depth: 48.00
Well Depth:
Well Diameter 4" Sample (Screened) Interval
31.00 Ft. to 45.25 Ft.
Depth to Water Level n/a Ft. below meas. pL(before sampling) or
n/a Ft. (MSL)
Measuring Point is 3.33 Ft. above land surface or
13.13 Ft. (MSL)
Gallons of water pumped/bailed before sampling CONTINUOUS
Field Analysis: pH 7.0 Specific Conductance
446 uMhos Temp 13.7
oC Odor
NONE
Date Sample Collected 01/13/97 Date Lab Sample Analyzed
1/13-1/30 1997 Appearance:
CLEAR
Laboratory Name : PCS PHOSPHATE ENV. AFFAIRS LAB Certification No.
330 (PCS Env Lab) and 78 (Coliform & Metals)
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
,
X YES
NO
COD N/A mg/1
NO2 as
N/A
mg/1
Ni-Nickel
N/A mg/I
Coliform: MF Fecal N/A /100m1
NO3 as N
N/A I
mg/1
Pb - Lead
N/A mg/1
Coliform: MF Total NEGATIVE /100m1
Phosphorus: Total as P
0.027
mg/I
Zn - Zinc
N/A mg/I
Dissolved Solids: Total 352 mg/1
Al - Aluminum
N/A
mg/1
Pesticides/Herbicides (Specify)
pH (when analyzed) 7.4 units
Ba - Barium
N/A
mg/1
ug/1
TOC 5.6 mg/1
Ca - Calcium
N/A
mg/1
ug/I
Chloride 13.2 mg/1
Cd-Cadmium
<0.5
ppb
ug/I
Arsenic N/A mg/1
Chromium: Total
<5.0
ppb
Other FLUORIDE
0.69 mg/1
Grease and Oils N/A mg/1
Cu - Copper
N/A
me
Other MBK
N/A ug/I
Hardness: Total N/A mg/1
Fe - Iron
N/A
mg/I
Other Ag -Silver
N/A mg/1
Phenol N/A mg/I
Hg - Mercury
N/A
mg/1
Other Se -Selenium
N/A mg/I
Sulfate <10 mg/1
K-Potassium
N/A
I mg/I
ug/1
Specific Conductance N/A uMohs
Mg - Magnesium
N/A
mg/1
ug/1
Total Ammonia(NH4 + NH3) N/A mg/1
Mn - Manganese
<0.01
ppm
TKN as N N/A mg/1
Na - Sodium
N/A mg/1
Note:
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE
SIGNATURE OF PERMITTEE (ORAUT RIZED AGENT)
Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
47
DATE
er

COI. I.ECTIG.:'AND ANALYSIS OF GROUNL.JATER SAMPLES
1 soul 1!:: should be analyzed as :;eon al possible eller collection. SAMPLES WHICH ARE IIOT ANALYSED WITHIN THE HOLDING I IME SPECI-
FIED FOR THE METHOD USED (SEE 114. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
2. I.I(.' •I•: A'inlysr:s: I! .o Sl..urrland Ikrured 3030C lor sample preparation (ruacury excluded). QQNOI FILTEELN TALS SAh1PI:Es_I)I_jJ!g.I°IELI! n
h. r •:r•.r1 samples must lie crAler(rd for metals. then lield acidilied with 5 ml concentrated nitric acid per liter ol sample and should be suburilted lu II •
lul •vithin 21 le:nc•.
`'iarnlde preparation in tlrr) laboratory lexhaction and Nitration) must be completed within 72lrours ol collection.
3 Al iP 1. 7SES ARE 1O BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN TFIE
Gll1't1HDWATER, NOT MPS' I}IAT ARg A EABI OE SEDIM tJI ASSQCJAIED WiTI WELL CONSTBUCJIQN D)3 SAMELING ERQuDUHES.
CI IECI< WITII YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. Al; l'in I We 15. I for (l r Carolina Administrative Code. Subchapter 2L, analytical procedures shall be in accordance with the methods described in ono. ol
Ihr lidlowinr) publications, or by other methods approved belorehand by the Director, Division ol Environmental
hLnrulr:mertt:
(a) Standard Methods lor the Examination of Water and Wastewater, 16111 Edition, 1985 and 171h Edition, 1989, published jointly by
American Public health Association, American Water Works Associalion and Water Pollution Conlrol Federation;
(b) Methods tor Chemical Analysis ol Water and Waste, 1979, U.S. Environmental Protection Agency publication number -
EPA "60014"•79-020, as revised March 1983;
(c) Test Methods lor Evalualing Solid Wasles: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protr:clion Agency
publicalion number SW-846;
Id) •iesi Procedures lor the Analysis of Polluanls Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136,
Ocloher 26, 1984;
5. Measure and record Ilse deptli ol water in the well prior to pumping or bailing any water Irorn the well.
6. AI leas( 3 volumes of water in lite well should be pumped or bailed prior to collecting a sarnple for analysis. II the well is pumped/bailed dry before 3 well
volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination lor pH. Specific Conductance, temperature, odor and appearance must be made In the lield on unlillered samples when Ile sample is
collected.
8. Field equipment must be calibraled in accordance with recommendalions by the manufacturer.
9. Samples must be filtered through a 0.45 micron tiller immediately alter collection when a dissolved analysis is required. (See t14: above)
In.Tire sample container should be labeled at Ile lime ol collection with the lacilily name, well identification nurnber and dale and time collected.
11."Authorized agent" is any corporale ollicer or public ollicial aulhorized by the company, corporation, or governrnenlal body to sign ollicial documents.

PCS PHOSPHATE CO
Aurora Division
Tank Farm Remedianon System Monitoring
Sand Layer Peizometers Level Indicators
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
i e: L. `.0413-0 02 Revised 12/06/96
PCS095.XLS
Date ,/ 7- 97
Time
Tech . �dG
Spz-1
Spz-2
Spz-3
Spz-4
10.47
11.21
11.87
11.45
/v.,eo
e.ys
s9y
97
-C67
.Coo
Cpz-1
Cpz-2
Cpz-3
CPW
10.51
10.25
11.12
9.65
722
9. tz
7 93
877
Spz-5
11.45
9.020
MWTF-1A
10.49
0
L..29
D 63
3/9
0.136.
Jet'4/ b'lnwG
Spz-6
11.23
9zo
2.03
MWTF-1 B
10.50
99
566
Ditch Level
.5•W
System Gauge Pressures
SWW-1
SWW-7
0
O-8
CwW-1
CWW-7
9-/3
9-/-S
Spz-7
11.59
/O.
/ 1.s
MWTF-1 C
10.49
2 '0
7 89
Barge Slip
Level
Spz-8
Spz-9
Spz-10
11.57
11.01
12.16
/v.30
834/
.5; 22
so27
07-67
6.941
MWTF-2A
MWTF-2B
MWTF-2C
14.05
14.02
14.08
6.7?
//yy
/ .70
73/
-Zs8
0.,98
SPW
9.95
77+1
,2.2/
MWTF-3A
MWTF-3B
MWTF-3C
12.21
12.18
12.19
4!22
/0/0
/a./0
7 99
zoS
co. 09
9. %8
Flow GPM
SW W-E
Water Level
Control Tank
= MSL
eael$: /yos
sww-W
CWW-E
N/19
CW W-w
bona Layer Ana t..roatan
Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Stc
Wtr
Level Ft.
Max Level
Relative To
MSL Ft.
Control
Point
MSL'
Is Well
Pumping
(Y)es/(N o
Comments
SW W-1
10.70
/p.,229
/2I 8
+1 ' to +2'
. /y 1
Aim/2 ©a/ oA �e/'v •
CWW-1
10.60
21/5
-/.,S.S
-2'to-1'
Y
SWW-2
9.99
8..S
2 e
+1' to +2'
. y
CWW-2
10.23
712
-/ OS
-2'to-1'
SWW-3
9.97
7 7.
/ 7#
+1 .to+2'
v'
CVVW-3
9.95
729
-/76•
-2'to-1'
✓
SWW-4
10.73
797
/J7
+1'to+2'
v
CWW-4
10.73
752
-7 Al8
-2'to-1'
i
SW W-5
10.80
7. 72
G 77
+1 ' to +2'
1//
W CW-5
10.74
73�2
-/48
-2'to-1'
'
r
SW W-6
10.66
7j ./
7 /f
+1 ' to +2'
,✓
w CW-6
9.92
7y2
-/:5
-2'to-1'
SWw-7
10.70
70.,/
/ 07
+1 ' to +2'
Y
CWW-7
9.95
7, se
-/ 70
-2'to-1'
r
Is Injection
System Running?
(Y)es/(N)o
Fes

•si.r . r�

PCS PHOSPHATE CQ,
Aurora Division
Tank Farm Remediation System Monitoring
0
Sand Layer Peizometers Level Indicators
TOC
Elevation
Well ID MSL'
TOC
Stc UVIr
Level '
Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Spz-1
Spz-2
Spz-3
Spz-4
Spz-5
Spz-6
Spz-7
Spz-8
Spz-9
10.47
11.21
11.87
11.45
11.45
11.23
3.810
757
5SZ
560
8.54
8`y8
66/
1.55�
85-
a?-S/S
Cpz-1
Cpz-2
Cpz-3
cPW
MWTF-1A
MWTF-1 B
10.51
10.25
11.12
9.65
10.49
10.50
Levet
Relative To
MSC Ft
709 Sya
9 38 0.87
77.9 339
8a8 /.37
0 sr' 9.9'9
11.59
9. 98
/• 6/
MWTF-1C
10.49
a38
//
F1e 15 3.11034 Revised 12/06/96
PCS095.XLS
Date At 9-94'
Time 89-00
Tech ACl-
Ditch Level I System Gauge Pressures
Barge Slip
Level
11.57
S98
s
MWTF-2A
[14.05
660 7.y.5-
866
SWVV-1
SW W-7
ammo
/0
cW W-1
/5
C /-7
/0
Flow GPM
SW W-E
Sww-W
Spz-10
SPW
11.01
12.16
9.95
79.
.5/4
66.95
3.5re
7.00
S. 00
MWTF-28
MWTF-2C
MWTF-3A
MWTF-3B
MWTF-3C
14.02
14.08
12.21
12.18
12.19
/0.04) S. 9&
/a of/ /.oil
N.1B 2'98
9.S8 ago
Water Level
Control Tank
% = MSL
CW W-E
CWVV-W
Sand Layer Ana
Formation Withdrawal
t.roatan
Wells
Well ID
TOC
Elevation
MSL'
Max Stc
Wtr
Level Ft
Max Level
Relative To
MSL Ft.
Control
Point
MSL'
Is Well
Pumping
(Y)_es/(N)o
Comments
WV SV-1
10.70
6242
-0. 8
+1'to+2'
Y
Du// mz,4rlli c
CWW-1
10.60
7//9
-/•5/
-2'to-1'
Y 1
0/SWW-2
9.99
98et,
.3ay, •
+1'to+2
,
SmOn9 Si»//1sI/Cyele.
O('
CVVW-2
10.23
74/%/
" /. 56
-2'to-1'
SW W-3
9.97
83+,
a. ay
+1. to +2'
Y
Weetif 4404Wsxd
CWW-3
9.95
'/•56
-/•4/y'
-2'to-1'
I/
2
SW W-4
10.73
B.7/
o?. 7/
+1. to +2'
i / 1
'Weals 4Stne.r /
CVWV-4
10.73
720
- et, 80
-2'to-1'
Y '
Ok
SW W-5
10.80
8d3
y3
+1' to +2'
Y I
%i'4 icercr/Mw/
CW W-5
10.74
.73/
--/ 69
-2' to -1'
!/
at
SVVW-6
10.66
702
/ at
+1 ' to +2'
It I
04
CW W6
9:92
, 94/
-/ 06
-2' to -1'
Y '
Ot
SW W-7
10.70
r707
/, 07
+1 ' to +2'
Y 1
at
CWW-7
9.95
79/
-/59
-2'to-1'
Y
at
Is Injection
System Running?
(Y►esl(N)o

PCS PHOSPHATE CO
Aurora Division
I Hook FT9znn
MED.7Fl7JoM SySTEi
/-SLx c /O -v-.
Revised 06/06/96
PCS095.WK3
Sand Layer Peizometers Level Indicators
Date //-&5":-94c
Well ID
TOC
Elevation
MSL'
TOC
Ste Wtr
Level'
Level
Relative To.
MSL Ft.
Well ID
TOC
Elevation
MSL"
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Time
Tech A..BC-
Spz-1 .
10.47
.3Qg
(o,S9
Cpz-1
10.51
704
,3 s/S
Ditch Level
System Gauge
Pressures
Spz-2
11.21
7.4/8
.5'73
Cpz-2
10.25
aat
/ 29
5-./67
SWW-1
0
Spz-3
11.87
S. 6S
6. Ret
' Cpz-3
11.12
7. 75/
3.-.3f
w'1.4. } a,�, � �`
vA U' \� S i�a��'
�h � �,� . �
SWW-7
/0
Spz-4
11.45
S 6.2
S.49.3
CPW
9.65
7 9&
/ 49
CWW-1
S
Spz-5
11.45
f�ya
�?03
MWTF-1A
10.49
p. 60
zJ. B9
CWW-7
30
Spz-6
11.23
9767
a.4/5
MWTF-1B
10.50
/,.44'
9.64
Barge Slip
Level
Flow GPM
Spz-7
11.59
9•6V
/75-
MWTF-1C
10.49
a.?Ga
7.97
SWW-E
Spz-8
11.57
/6.0$
S.//9
MWTF-2A •
14.05
6•//6"--
7.4.0
9-az/
sww-w
.7V----
Spz-9
11.01
724
.Y7'S
MWTF-2B
14.02
97,
4'..24
0.53 i
Water Level
Control Tank
%= MSL
CWW-E
Spz-10
12.16
3/&,
7 oa
MWTF-2C
14.08
/3•SS
CWW-W
SPW
9.95
6.74/
3.a1
MWTF-3A
12.21
41,,20
g O/
Is Injection
System Running?
�`i / Y%b(/osc.rs-
(Y)es/(N)o
MWTF-3B
12.18
9o?0
a, 9Q
63/o. /a.9/
)7
W MTF-3C
12.19
//SF
D• 4"/
Sand Layer And Croatan
Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Stc
Wtr
Level Ft.
Max Level
Relative To
MSL Ft.
Control
Point
MSL'
Is Well
Pumping
(Y)es/(N)o
Comments
SWW-1
10.70
7?0
-O.B
+1'to+2'
A/
/ymp 4mo0ec
CWW-1
10.60
7158
-/ 4.2
-2'to -1'
-V
Jenl,'r7�9 ,7e Zic_.
SWW-2
9.99
g//S
al`/57
+1'to+2'
y
r✓J`i,
Weds t%ua/
CWW-2
10.23
/9J.S(o
/.S(,
-2'to-1'
1/
w(r')
7
SW W-3
9.97
eg..S Go
4,
075
+1 ' to +2'
I'
//,,
Weds 4d u97. o
CWW-3
9.95
7.4/
-/.39
-2'to-1'
it//
SWW-4
10.73
9.01
,.3,04,
+1'to+2'
;'
y/ceds %%sc 4J7
CWW-4
10.73
?,fat
'/.S5/
-2'to-1'
1-
SWW-5
10.80
8./3
Oq./3
+1'to+2'
K
CWW-5
10.74
Tin
-/ S%
-2'to-1'
Y
SWW-6
10.66
'7.34'
/• 34/
+1' to +2'
✓
CWW-6
9.92
/0.05/
/O4
-2'to-1'
y
,,,i, %ij'. jig
SWW-7
10.70
%DV
/•P9
+1'to+2'
Y
//
CWW-7
9.95
73/
- 64
-2'to-1'
Y
Nita
7.97
-/.0/ (4,0_1 �