WI0700012_Monitoring (Report)_20071115 (2)

PCS
Phosphate
AURORA
PCS PHOSPHATE COMPANY, INC.
P.O. BOX 48, AURORA, NC U.S.A. 27806
November 15, 2007
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina, 27699
Attn: Information Management
CERTIFIED MAIL
Subject: Underground Injection Control Program
Quarterly Groundwater Monitoring Report
August 2007 — October 2007
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Qi:
Please find the subject groundwater monitoring report attached. This includes the sampling and reporting
requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of
the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7 and
monitor well MWTFICR, b) Form GW-59 for each of the fourteen withdrawal wells, c) piezometer level
monitoring field sheet, and d) the summary operational and maintenance report.
Please do not hesitate to contact me at [phone] if you have any questions regarding this
information.
Sincerely,
10.AinAa �1 2
D. Daniel Winstead III
Environmental Engineer
PCS Phosphate
Attachments
RECEIVED
NOV 2 7 2007
Information Processing Unit
DWQ/BOG

pc: Will Hart — Aquifer Protection DWQ, WaRO (w/ attaclunents)
R. M. Smith/12-07-02 (w/ attachments)
T. S. Ingra - Ardaman & Assoc. (w/attachments)
R. A. Allen (w/ attachments)
W. A. Schimming (w/ attachments)
Anthony Shrewsbury (w/ attachments)
R. B. Lee (w/ attachments)
Total Two Copies
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina, 27699
Attn: Information Management
\\aurdata2\users\AUR1DDW\Reports\2007\Quarterly\TFRAS Report Third Quarter 2007.doc
2

mg/l
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit):
Well Depth: 48.00 ft. Well Diamter:
CIW-7
Screened Interval: 31.00 ft. to 45.25 ft.
Depth to Water Level:
Measuring Point is
4 inch
N/A ft. below measuring point.
N/A ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
N/A
Field Analysis: pH 7.1 , Specific Conductance 652 uMhos
Temp. 22.6 oC, Odor NONE Appearance: CLEAR
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
EXPIRATION DATE: 01/15/08
UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
Rotary Distributor
Other
Remediation: Infiltration Gallery
Land Application of Sludge
RECEIVED
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
10/16/2007
10/16/2007 to
PCS PHOSPHATE
NOV 2 7 2007
11/lo tion PP�r��oggceessing Unit
and ENVIRONMT 1
330 10
PARAMETERS:
COD
(Samples for metals were collected unfiltered X Yes
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
<1.0
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol Organics: (GC, GC/MS, HPLC)
<10.0 mg/1 Hg - Mercury N/A mg/I (Specify test method #. Attach lab report.)
N/A uMhos K- Potassium N/A mg/I Report attached? Yes (1) No X
N/A mg/1 Mg - Magnesium N/A mg/1 VOC : method#
N/A mg/I Mn - Manganese <0.010 mg/I method#
method#
No and field acidified X Yes No )
Nitrite (NO2 as N) N/A mg/I
Nitrate (NO3 as N) N/A mg/I
Phosphorus: Total as P 0.015 mg/l
Orthophosphate N/A mg/I
411 mg/I Al - Aluminum N/A mg/I
6.9 units Ba - Barium N/A mg/1
4.4 mg/I Ca - Calcium N/A mg/1
mg/I
/100m1
/100m1
18.0 mg/I Cd- Cadmium <0.001 mg/1
N/A mg/I Chromium: Total <0.005 mg/1
Ni - Nickel
Pb - Lead
Zn - Zinc
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
0.54
N/A
N/A
N/A
N/A
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/1 Cu - Copper N/A mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/l
(2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
Perrn riz Aegent) me Title -Please type or print/
Signature of Permittee (or Authorited Agent) (Date)
N/A mg/1 Fe - Iron N/A mg/I

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit): MWTF1-CR
Well Depth: 42.00 ft. Well Diamter: 2 inch
Screened Interval: 38.70 ft. to 40.70 ft.
Depth to Water Level:
Measuring Point is
15.02 ft. below measuring point.
3.95 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
MILILITERS of water pumped/bailed before sampling: 2100
Field Analysis: pH 7.1 , Specific Conductance 684 uMhos
Temp. 23.5 oC, Odor NONE Appearance: CLEAR
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
10/16/2007
10/16/2007 to 11/1/2007
PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered X Yes
No and field acidified X Yes No )
COD N/A mg/I Nitrite (NO2 as N) N/A mg/I
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A mg/I
Coliform: MF Total <1.0 /100m1 Phosphorus: Total as P 0.480 mg/I
(Note. Use MPN method for highly turbid samples) Orthophosphate N/A mg/I
Dissolved Solids: Total 424 mg/I Al - Aluminum N/A mg/1
pH (when analyzed) 6.8 units Ba - Barium N/A mg/I
TOC 6.3 mg/I Ca - Calcium N/A mg/I
Chloride 16.7 mg/I Cd- Cadmium <0.001 mg/I
Arsenic N/A mg/I Chromium: Total <0.005 mg/I
Grease and Oils N/A mg/I Cu - Copper N/A mg/I
N/A mg/I Fe - Iron N/A mg/I
<10.0 mg/I Hg - Mercury N/A mg/I
N/A uMhos K- Potassium N/A mg/I
N/A mg/I Mg - Magnesium N/A mg/I
N/A mg/I Mn - Manganese 0.055 mg/I
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
N/A mg/I
N/A mg/I
N/A mg/I
mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC • method#
method#
method#
0.43 mg/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
Signature of Permittee (or
ame, cl Title - Please type orr rint
/C%
! %� �z!/ 1—/ V 7
horized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No- of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-1
Well Depth: 22.50 ft. Well Diamter: 4 inch
Screened Interval: 18.30 ft. to 21.12 ft.
Depth to Water Level: 8.18 ft. below measuring point.
Measuring Point is 1.52 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
Field Analysis: pH 6.0 , Specific Conductance 1498 uMhos
Temp. 22.9 oC. Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION. GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01 /15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
10/15/2007
10/15/2007 to 11/1/2007
PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a No
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
1132
6.0
8.8
82.5
N/A
N/A
N/A
244.1
N/A
N/A
N/A
Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos
mg/l
mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
and field acidified Yes n/a No )
N/A mg/I Ni - Nickel
N/A mg/1 Pb - Lead
158.500 mg/I
N/A mg/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/l
Zn - Zinc N/A ug/I
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A ug/l Organics: (GC. GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
N/A ug/I VOC method#
method#
method#
mg/I
N/A ugll
0.70 mg/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee (pt Aushori ed Agen a and Title - Please type or print
, 1s� l77--/7
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-2
Well Depth: 23.00 ft. Well Diamter: 4 inch
Screened Interval: 18.80 ft. to 21.63 ft.
Depth to Water Level: 8.17 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
Field Analysis: pH 5.6 , Specific Conductance 2876 uMhos
Temp. 22.1 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH. NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01 /15/08
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
10/15/2007
10/15/2007 to 11/1/2007
PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note:
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
Use MPN method for highly turbid samples)
3612
5.5
10.2
44.7
N/A
N/A
N/A
572.6
N/A
N/A
N/A
mg/I
/100m1
/100m1
Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/1 Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
No and field acidified
N/A mg/1
N/A mg/I
655.000 mg/I
N/A mg/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
Ni - Nickel
Pb - Lead
Yes n/a No )
N/A ug/I
N/A ug/I
Zn - Zinc _ N/A ug/I
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A ug/I Organics: (GC, GC/MS,
N/A ug/I (Specify test method #.
N/A ug/I Report attached? Yes
N/A ug/I VOC
N/A ug/I
mg/I
0.21 mg/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
HPLC)
Attach lab report.)
(1) No X (2)
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross
Perm
Smith - Manager, Environmental Affairs
Aytho ed Ag^t) me and Title - Please typ9..or print
Signature of Permittee (or AFfthorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-3
Well Depth: 24.50 ft. Well Diamter: 4 inch
Screened Interval: 20.17 ft. to 23.00 ft.
Depth to Water Level:
Measuring Point is
N/A ft. below measuring point.
3.17 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH N/A , Specific Conductance N/A uMh
Temp. NIA oC. Odor NONE Appearan
PARAMETERS: (Samples for m
COD
Coliform: MF Fecal
Coliform: MF Total
(Note: Use MPN method for highly turbid s
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
mg/I
mg/I Hg - Mercury
uMhos
mg/I
mg/I
filtered
itrite (NO
itrate (NO
hosphorus:
rthophos
I - Alumi
a - Bariu
a - Calciu
Cd- Cadmium
Chromium: Total
Cu - Copper
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
N/A
Fe - Iron
K- Potassium
Mg - Magnesium
Mn - Manganese
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH. NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE: 01/15/08
UIC X
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentra
Dat- s • • ' Ile 2007
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
2007 to 11/1/2007
OSPHATE
ug/I
Pb - N/A ug/I
Zn - . c N/A ug/I
Amm mg/I
Other ( . csmouns and Concentration Units)
Fluoride N/A mg/I
MIBK N/A ug/I
Ag - Silver N/A ug/I
N/A ug/I
N/A ug/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC method#
Se- Selenium
Sodium
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
WQ\l "ipi'
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
Per t ittee (of Authorized Name and Title -Please type r print
Signature of Permittee
� /5 id /3 / ,
Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Well Locations/Site Name: Tank Farm
Telephone: [phone]
No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit):
Well Depth: 25.00 ft. Well Diamter:
Screened Interval:
Depth to Water Level:
Measuring Point is
SWW-4
20.50 ft. to 23.30 ft.
4 inch
N/A ft. below measuring point.
3.42 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH N/A , Specific Conductance N/A uMh
Temp. N/A oC, Odor NONE Appearan
PARAMETERS: (Samples for m
COD
Coliform: MF Fecal
Coliform: MF Total
(Note: Use MPN method for highly turbid s
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
mg
mg/I
N/A mg/1
N/A mg/I
N/A uMhos
N/A mg/I
N/A mg/I
Itered
itrite (NO
itrate (NO
hosphorus:
rthophos
I - Alumin
a - Bariu
a - Calciu
Cd- Cadmium
Chromium: Total
Cu - Copper
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
N/A
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
Dat s
colloidal concentra
Ile
Pb-1
Zn -
Amm
Other (
Fluoride
fi)/A ug/I MIBK
2017
/2017 to 11/1/2007
,HOSPHATE
ompounds and Concentration Units)
N/A ug/I Ag - Silver
N/A
N/A
N/A
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A ug/l
N/A ug/I
N/A ug/I
N/A
N/A
Organics: (GC, GC/MS,
(Specify test method #.
Report attached? Yes
N/A ug/I VOC
N/A ug/I
HPLC)
Attach lab report.)
(1) No X
: method#
method#
method#
ug/I
ug/I
ug/I
mg/l
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
W eLl_ bR'
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
Per ee f A_uthgr it)) ame and Title - type or nt
Signature of Permittee (or
horized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 28.21 ft. Well Diamter: 4 inch
Screened Interval: 24.83 ft. to 27.21 ft.
Depth to Water Level: 7.44 ft. below measuring point.
Measuring Point is 2.96 ft above land surface.
GALLONS of water pumped/bailed before sampling:
SWW-5
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 2227 uMhos
Temp. 28.3 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone' [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
10/15/2007
10/15/2007 to 11 /1 /2007
PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS:
COD
Coliform: MF Fecal
Coliform: MF Total
(Note.
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
(Samples for metals were collected
N/A mg/I
N/A /100m1
N/A /100m1
Use MPN method for highly turbid samples)
1484
6.3
8.9
49.5
N/A
N/A
N/A
618.4
N/A
N/A
N/A
mg/I
units
unfiltered
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes n/a No and field acidified
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/1 Cu - Copper
mg/l Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
N/A mg/I Ni - Nickel
N/A mg/I
113.750 mg/I
N/A mg/I
N/A ug/I
N/A ug/I
N/A ug/l
N/A ug/I
Yes n/a No )
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No
N/A ug/I
N/A ug/I
VOC
method#
method#
method#
0.37
N/A
N/A
N/A
N/A
ug/I
ug/I
ug/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete. and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Mpnaqer, Environmental Affairs
Permit t (of Authori d Agent a and Ttle - Please type or print
Signature of Permittee (or Authckized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-6
Well Depth: 26.00 ft. Well Diamter: 4 inch
Screened Interval: 22.25 ft. to 24.62 ft.
Depth to Water Level: 7.18 ft. below measuring point.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
Measuring Point is 2.58 ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 3323 uMhos
Temp. 28.6 oC, Odor NONE Appearance: LT RUST
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone [phone]
PERMIT #: WI0700012
Non -Discharge
EXPIRATION DATE:
UIC X
01/15/08
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
Remediation: Infiltration Gallery
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
10/15/2007
10/15/2007 to 11/1/2007
PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Nitrite (NO2 as N)
N/A /100m1 Nitrate (NO3 as N)
N/A /100m1 Phosphorus: Total
Orthophosphate
2336 mg/1 Al - Aluminum
6.3 units Ba - Barium
14.2 mg/1 Ca - Calcium
87.7 mg/I Cd- Cadmium
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
N/A mg/1 Fe - Iron
1004.2 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
No and field
N/A mg/1
N/A mg/I
as P 50.250 mg/I
N/A mg/I
N/A ug/l
N/A ug/I Fluoride
N/A ug/I MIBK
N/A ug/I Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A ug/I Organics: (GC, GC/MS
N/A ug/I (Specify test method #
N/A ug/I Report attached? Yes
N/A ug/I VOC
N/A ug/I
acidified Yes n/a No )
Ni - Nickel N/A ug/I
Pb - Lead N/A ug/I
Zn - Zinc N/A ug/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
•
0.07 mg/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
HPLC)
Attach lab report.)
(1) No X (2)
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
Pert�ttee offAuth�rized A nt) ame and Title - Please type or print'
(tart 1lV4 %
Signature of Permittee (or Af thorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone:
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
[phone]
18
Mail Original
to:
Well Identification Number (from Permit):
Well Depth: 29.50 ft. Well Diamter:
SWW-7
Screened Interval: 25.17 ft. to 27.50 ft.
4 inch
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
MILILITERS of water pumped/bailed before sampling: N/A
Field Analysis: pH N/A , Specific Conductance N/A uMhos
Temp. N/A oC, Odor NONE Appearance: CLEAR
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
PARAMETERS: (Samples for metals were collec
COD
Coliform: MF Fecal
Coliform: MF Total
(Note: Use MPN method for highly turbid
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
mg/I
uMhos
mg/I
mg/I
unfiltered
Nitrite (N
Nitrate (N
Phosphor
Orthophos
Al - Aluminu
Ba - Barium
Ca - Calci
Cd- Cad
Chromium
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636
Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/16/2007
Date sample analyzed: 1 /2007 to 11/1/2007
LaboratSPHATE
ug/I
N/A ug/I
N/A ug/I
Ag - Silver
No)
N/A
N/A
N/A
Se- Selenium
Sodium
N/A
N/A
Organics: (GC, GC/MS,
N/A ug/I (Specify test method #.
N/A ug/I Report attached? Yes
N/A ug/I VOC
N/A ug/I
HPLC)
Attach lab report.)
(1) No X
: method#
method#
method#
ug/I
ug/I
ug/I
mg/1
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and beliefthe information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
tiJ EL,L. bit;
GW-59 Rev 3/2000
Ross M. Smith - Manager, Environmental Affairs
Permitt (off ut oriz Agent) m nd Titl Please type or print
Signature of Permitte
thortfed Agent) (Date)