WI0700012_Monitoring (Report)_20011128

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
CIW-7
Well Depth: 48.00 ft. Well Diamter:
Screened Interval: 31.00 ft. to 45.25 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is N/A ft above land surface.
GALLONS of water pumped/bailed before sampling:
4 inch
For Groundwater Treatment
Sys ems Check One:
(X 'Influent (98)
1Effluent(99)
N/A
Field Analysis: pH 7.1 , Specific Conductance 606 uMhos
Temp. 20.2 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations CD
Date sample collected: 10/9/01 CD
Date sample analyzed: 10/9/01 to 11/6/01 n
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
X Yes
COD N/A mg/I Nitrite (NO2 as N)
Coliform. MF Fecal N/A /100m1 Nitrate (NO3 as N)
No and field acidified X Yes No
N/A mg/I Ni - Nickel
N/A mgil Pb - Lead
Coliform: MF Total 13* /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 392 mg/I Al - Aluminum
pH (when analyzed) 7.8 units Ba - Barium
TOC 8.5 mg/1 Ca - Calcium
Chloride 14.0 mg/I Cd- Cadmium
Arsenic
Grease and Oils
Phenol
Sulfate
0.024 mg/I Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A mg/I
N/A mg/1
N/A mg/I
N/A ug/I
N7\ ug/I
d N.A ug/I
c? -- mg/I
Other (Specify Compounds and Concentration Unii
Fluoride
MIBK
<0.001 mg/I Ag - Silver
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
N/A mg/I Fe - Iron
<10.0 mg/I Hg - Mercury
Specific Conductance N/A uMhos K- Potassium
Total Ammonia
TKN as N
<0.005 mg/I Se- Selenium
N/A mg/I Sodium
N/A mg/1 Mg - Magnesium
N/A mg/I Mn - Manganese
NiA=
W
mg/I
mg/I
mg/1
mg/I
ug/I
N/A mg/I Organics: (GC, GC/MS, HPLC) W -
N/A mg/I (Specify test method #. Attach lab reHrt.) O
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC • method#
<0.010 mg/I
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
* RESAMPLED = <1.0
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Pe iiteeof Authoriz d Agpgt) N e and Title -Please typeor q�i e/P `
Permittee (or Authorized Agent)
te)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): MWTF1-CR
Well Depth: 42.00 ft. Well Diamter: 2 inch
Screened Interval: 38.70 ft. to 40.70 ft.
Depth to Water Level: 12.86 ft. below measuring point.
Measuring Point is 3.95 ft above land surface.
MILILITERS of water pumped/bailed before sampling: 2600
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
Field Analysis: pH 7.4 , Specific Conductance 627 uMhos
Temp. 23.6 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
U I C
Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor
Other
Land Application of Sludge W
W
—.t
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/9/01
Date sample analyzed:
Laboratory Name:
Certification No(s)
10/9/01 to 11/6/01
PCS PHOSPHATE and ENVIRONMENT 1
330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
X Yes
N/A mg/I Nitrite (NO2 as N)
N/A /100m1 Nitrate (NO3 as N)
No and field acidified X Yes No
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
<1.0 /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Orthophosphate
404 mg/I Al - Aluminum
8.0 units Ba - Barium
5.9 mg/l Ca - Calcium
Chloride
13.7 mg/1 Cd- Cadmium
Arsenic
Grease and Oils
Phenol
Sulfate
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
45.3 mg/I Hg - Mercury
N/A uMhos K- Potassium
0.391 mg/I Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/I Fluoride
N/A mg/I MIBK
<0.001 mg/I Ag - Silver
0.01 mg/1 Se- Selenium
N/A mg/I
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A mg/1
N/A mg/I
N/A mg/l
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
N/A mg/I VOC : method#
0.052 mg/I : method#
method#
N/A o ug/I
SI/A ug/I
( /A E' /1
rc"^) Ing/I
t o
c't.49:'. rAg/I
-10\I/AR,�g/I
l/A .erng/I
.z
t.':/J/A cn:mg/I
C/A o ug/l
(2)
I certify that. to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Perraittee
ignature
of Authorized Age
�l y'
Na and Title - Please type or pri t
/j
rmittee (or Authorized Agent)
(Dat )

1
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-1
Well Depth: 22.50 ft. Well Diamter: 4 inch
Screened Interval: 18.30 ft. to 21.12 ft.
Depth to Water Level: 7.32 ft. below measuring point.
Measuring Point is 1.52 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 2253 uMhos
Temp. 20.9 oC, Odor NONE
Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/10/01
Date sample analyzed: 10/10/01 to 11/6/01
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes n/a No and field acidified
N/A mg/I Ni - Nickel
N/A mg/l Pb - Lead
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1352
pH (when analyzed) 6.7
TOC 10.8
Chloride 85.3
Arsenic N/A
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
530.2
N/A
N/A
N/A
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/1 Cu - Copper
mg/1 Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/l Mg - Magnesium
mg/I Mn - Manganese
119.000 mg/I Zn - Zinc
Yes n/a No
G N
N/A mg/I Ammonia Nitrogen
t-47
c7
N/A mg/I Other (Specify Compounds and Concentration Unit,
N/A mg/I Fluoride
N/A mg/I MIBK
N/A mg/1 Ag - Silver
N/A mg/I
N/A mg/I
Se- Selenium
Sodium GwJl N7�1
N/A mg/1 Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
0.
Witk
;ern
ug/I
ug/I
ug/I
mg/I
C.J
N/A mg/I VOC : method#
N/A mg/I method#
method#
mg/1
mg/I
mg/I
mg/I
ug/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
.7 at '
�gnatur Permittee (or Authorized Agent)
Terry L. Baker - Manager, Environmental Affairs
Per yi4Eeesof Authorize Ag- N- e and Title - Please type or pdnt
11/2 70)
(Da

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled 18
ohumare
Well Identification Number (from Permit): SWW-2
Well Depth: 23.00
Screened Interval: 18.80 ft. to 21.63 ft.
Depth to Water Level: 6.86
Measuring Point is
ft. Well Diamter: 4 inch
ft. below measuring point.
3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.4 , Specific Conductance 2244 uMhos
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Temp. 20.2 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
UIC X
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/10/01
Date sample analyzed: 10/10/01 to 11/6/01
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Yes n/a No and field acidified Yes n/a No
N/A mg/I
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 1504 mg/I Al - Aluminum
pH (when analyzed) 6.8 units Ba - Barium
TOC
Chloride
Arsenic
11.5 mg/I Ca - Calcium
Grease and Oils
52.9 mg/I Cd- Cadmium
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
601.1 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/1 Mg - Magnesium
N/A mg/I Mn - Manganese
N/A mg/I
69.000 mg/I
Ni - Nickel N/A ug/I
Pb - Lead N/f7 ug/I
Zn - Zinc Nf$; ug/I
N/A mg/I Ammonia Nitrogen c-) , mg/1
N/A mg/I Other (Specify Compounds and Concentration Unit c'
c_
N/A mg/I Fluoride t 0.2 i L mg/l
N/A mg/I MIBK -) NtAr; mg/I
N/A mg/I Ag - Silver __ —0 NIA., ^ mg/I
N/A mg/I Se- Selenium NAA.-„ mg/I
N/A mg/1 Sodium C.ti N: ug/l
N/A mg/1 Organics: (GC, GC/MS, HPLC) W
N/A mg/I (Specify test method #. Attach lab refit.)
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC method#
N/A mg/I
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per
gnature
(of Authorized Age p Naryfe and Title - Please type or pr nt
ermittee (or Authorized Agent)
(Dat
d /

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 24.50
Screened Interval:
Depth to Water Level:
Measuring Point is
ft. Well Diamter:
SWW-3
20.17 ft. to 23.00 ft.
4 inch
6.86 ft. below measuring point.
3.17 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.3 , Specific Conductance
Temp. 22.6 oC, Odor NONE
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
1480 uMhos
Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/10/01
Date sample analyzed:
Laboratory Name:
10/10/01 to 11/6/01
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfilt
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
1016
5.6
8.6
54.4
N/A
N/A
N/A
397.8
N/A
N/A
N/A
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
mg/1
/100m1
/100m1
mg/I
units
mg/I
mg/l
mg/1
mg/I
mg/1
mg/1
uMhos
mgll
mg/I
ered Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
No and field acidified
N/A mg/1 Ni - Nickel
N/A mg/1 Pb - Lead
58.750 mg/1 Zn - Zinc
Yes nla
N/A mg/1 Ammonia Nitrogen
N/A mg/l
Cd- Cadmium
Chromium. Total
Cu - Copper
Fe - Iron
Hg - Mercury
N/A mg/I
N/A mg/I
N/A mg/l
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I
N/A mg/I
N/A mg/1
No
N/A
N/A
N/A
t:
Other (Specify Compounds and Concentration Units}— C)
0 0§3
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
ug/I
ug/1
ug/I
mg/I
mg/1
C7 Ng•mg/1
t NF23` mg/1
N-s mg/I
NTi , ug/l
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab repkt.) rc14=-u
Report attached? Yes (1) No avt
VOC method# CD
method#
method#
<n:r_
(2)
1 certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee Authorized A en m nd Title - Please type or print
(Date)
ignature
mittee (or Authorized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
(from pe.n.I
Well Identification Number (from Permit):
SWW-4
Well Depth: 25.00 ft. Well Diamter: 4 inch
Screened Interval: 20.50 ft. to 23.30 ft.
Depth to Water Level: 7.44 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 2327 uMhos
Temp. 32.7 oC, Odor NONE
Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
U I C X
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/10/01
Date sample analyzed:
Laboratory Name:
10/10/01 to 11/6/01
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I
Nitrite (NO2 as N)
Yes n/a No and field acidified Yes n/a No
N/A mg/I Ni - Nickel
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 1404 mg/I Al - Aluminum
pH (when analyzed) 6.7 units Ba - Barium
TOC 8.2 mg/I
Chloride 43.7 mg/l
Arsenic N/A mg/I
Grease and Oils
N/A mg/1
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
673.3 mg/l
N/A uMhos
N/A mg/1
N/A mg/I
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
N/A ug/1
N/A mg/I Pb - Lead N/A ug/I
67.500 mg/I Zn - Zinc NIPc ug/I
N/A mg/I Ammonia Nitrogen O G mg/1
N/A mg/I Other (Specify Compounds and Concentration Units) c7 c7.a
N/A mg/1 1 10.0�i ng/I
N/PED ng/I
W N/A7;!:ing/1
—v N/f g/I
_i N// .1g/I
N/A mg/I Organics: (GC, GC/MS, HPLC) W
N/A mg/I (Specify test method #. Attach lab repgr) y
N/A mg/I Report attached? Yes (1) No N7 Xc-7 (2)
N/A mg/I VOC : method#
N/A mg/1
N/A mg/I
N/A mg/I
N/A mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Pe tee (of Authorized Agoyt) Nte and Title - Please type or print
Signature/f'Permittee (or Authorized Agent)
i7/ZRAV
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth:
Screened Interval:
Depth to Water Level:
Measuring Point is
28.21
24.83
7.08
2.96
ft. Well Diamter:
SWW-5
4 inch
ft. to 27.21 ft.
ft. below measuring point.
ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.2 , Specific Conductance
Temp. 29.5 oC, Odor NONE
Fo Groundwater Treatment
Sys ems Check Or.e:
Influent (98)
X Effluent (99)
CONTINUOUS
2546 uMhos
Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
UIC X
09/30/01
Spray Field X Remediation : ,
Rotary Distributor Land Application of Sludge 43
W
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
10/10/01
10/10/01 to 11/6/01
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unf
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
mg/I
/100m1
/100m1
Dissolved Solids: Total 1592 mg/I
pH (when analyzed) 5.4 units
TOC 12.2 mg/I
Chloride 60.6 mg/I
Arsenic N/A mg/I
Grease and Oils N/A mg/I
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
679.5 mg/I
N/A uMhos
N/A mg/I
N/A mg/1
iltered Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
No and field acidified Yes n/a No
N/A mg/I Ni - Nickel N/A ug/I
N/A mg/I Pb - Lead N/A ug/l
83.000 mg/I Zn - Zinc NI€ ug/I
Ammonia Nitrogen a - . mg/I
T_+
Other (Specify Compounds and Concentration Units)" c., --,
Fluoride e7' 0.3V-r ning/I
MIBK t7 N/! =ngll
Ag - Silver r , N/ '_ Ong/I
Se- Selenium N/A;t ng/I
-73 N/fig/I
(A) L
(Specify test method #. Attach lab repo ri
N/A mg/I Report attached? Yes (1) No (.13X (2)
N/A mgll VOC method# z
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/1
N/A mg/I
N/A mg/I
Sodium
Organics: (GC, GC/MS, HPLC)
method#
method#
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per 'tee (of Authorized Agen m and Title - Please type or print
/1
Z,, 0J
igiiature 9fjPermite (or ' u horized Agent)
(Dat

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 26.00 ft. Well Diamter:
SWW-6
4 inch
Screened Interval: 22.25 ft. to 24.62 ft.
Depth to Water Level: 7.36 ft. below measuring point.
Measuring Point is 2.58 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.4 , Specific Conductance
Temp. 29.9 oC, Odor NONE
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
2489 uMhos
Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/10/01
Date sample analyzed:
Laboratory Name:
10/10/01 to 11/6/01
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform. MF Fecal N/A /100m1 Nitrate (NO3 as N)
Yes n/a No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 1720 mg/I Al - Aluminum
pH (when analyzed) 7.0 units Ba - Barium
TOC 15.6 mg/I Ca - Calcium
Chloride 102.6 mg/I Cd- Cadmium
39.750 mg/I Zn - Zinc
Arsenic N/A mg/I Chromium: Total
Grease and Oils
Phenol
Sulfate
N/A mg/l Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/1 Fe - Iron
654.0 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I
N/A mg/I
Yes n/a No
G7
O
rrt
(')
Ammonia Nitrogen r co <
c.i -e ri
Other (Specify Compounds and Concentration Units)
N/A mg/I Fluoride 3 0.V7c:
N/A mg/I MIBK NIA
N/A mg/I Ag - Silver Nba,
N/A mg/I Se- Selenium c.n, NA
N/A mg/l Sodium
N/A mg/1 Mg - Magnesium
N/A mg/I Mn - Manganese
N/A mg/l
N1-4
ug/I
ug/I
ug/I
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
N/A mg/l Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per r ittee (of Authorized Aged Nayne and Title - Please type or pri t
(D 4'!
(Da )
Signature Permittee (or Authorized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. -Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: 29.50
Screened Interval: 25.17 ft. to 27.50 ft.
Depth to Water Level:
Measuring Point is
GALLONS
SWW-7
ft. Well Diamter: 4 inch
7.14 ft. below measuring point.
3.00 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance
944 uMhos
Temp. 25.6 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/10/01
Date sample analyzed:
Laboratory Name:
10/10/01 to 11/6/01
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note: Use MPN method for highly turbid samples)
628
6.4
9.2
67.0
N/A
N/A
N/A
155.0
N/A
N/A
N/A
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
Yes n/a No and field acidified Yes n/a No
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
mg/1 Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
mg/1 Chromium: Total
mg/1 Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
41.250 mg/I Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A mg/I
N/A mg/1
N/A mg/I
N/A mg/1
N/A mg/I
N/A mg/I
uMhos K- Potassium
mgll Mg - Magnesium
mg/I Mn - Manganese
N/A ug/I
N ugll
O NIA ug/I
Other (Specify Compounds and Concentration Unit
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
c m mg/I
0
C (S�
0. A mg/I
W N/Z5mg/I
-p N/g; 3mg/I
3 N/R:I ^img/I
C- N/ir nug/I
N/A mg/I Organics: (GC, GC/MS, HPLC) c�J
N/A mg/I (Specify test method #. Attach lab repel)
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC
N/A mg/I
method#
method#
method#
certify that. to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
f Authorized Agent N me/and Title - Please type or pri
itegio
�
ture o e ittee (or Authorized Agent)
z e
(Dat
i

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled 18
Pom
Well Identification Number (from Permit): MWTF1-A
Well Depth: 6.40 ft. Well Diamter:
2 inch
Screened Interval: 3.40 ft. to 5.40 ft.
Depth to Water Level: 4.49 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
2100
Field Analysis: pH 7.1 , Specific Conductance 565 uMhos
Temp. 23.5 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
UIC X
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/9/01
Date sample analyzed:
Laboratory Name:
10/9/01 to 11/6/01
PCS PHOSPHATE
N
cn
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
Yes n/a
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note:
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
Use MPN method for highly turbid samples)
328
7.5
5.4
10.3
N/A
N/A
N/A
<10.0
N/A
N/A
N/A
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/1 Ca - Calcium
No and field acidified
N/A mg/I
N/A mg/1
0.306 mg/1
N/A mg/I
N/A mg/I
mg/I Cd- Cadmium
mg/1 Chromium: Total
mg/1 Cu - Copper
mg/1 Fe - Iron
mg/I Hg - Mercury
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/1
N/A mg/I
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes n/a No
Other (Specify Compounds and Concentration UnitCf
Fluoride
MIBK
Ammonia Nitrogen 0
zr •
2.. <
N3Ar�
Ag - Silver s NIt
Nam;,
Se- Selenium
Sodium
ctt o
(Specify test method #. Attach lab report.) z
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC method#
ug/I
ug/I
ug/I
mg/I
mg/I
mg/l
mg/I
mg/I
ug/I
N/A mg/I
Organics: (GC, GC/MS, HPLC)
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager. Environmental Affairs
Per
Signature
e, e (oj Authorized Agent) - �e • d Title - Please type or print
�� .9► /,/ 794l
(Date
rr iitte(or Authorized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit): MWTF1-B
Well Depth: 13.50 ft. Well Diamter: 2 inch
Screened Interval: 10.60 ft. to 12.60 ft.
Depth to Water Level: 5.38 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
2100
Field Analysis: pH 5.8 , Specific Conductance 368 uMhos
Temp. 23.9 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
UIC X
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/9/01
Date sample analyzed:
Laboratory Name:
10/9/01 to 11/6/01
PCS PHOSPHATE
IN)
Certification No(s) 330
cD
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD NIA mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note. Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total
pH (when analyzed)
TOC
248 mg/l Al - Aluminum
6.1 units Ba - Barium
4.4 mg/I Ca - Calcium
Chloride
44.3 mg/I Cd- Cadmium
Arsenic
Grease and Oils
Phenol
Sulfate
No and field acidified Yes n/a No 0
N/A mg/I Ni - Nickel n
N/A mg/I Pb - Lead 1
Loa
4.775 mg/I Zn - Zinc
N/A mg/I Ammonia Nitrogen 'v r;�
N/A mg/I
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
34.2 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/1 Mg - Magnesium
N/A mg/I Mn - Manganese
N/A mg/I
N/A mg/l
Other (Specify Compounds and Concentration Units
Fluoride 9
MIBK
N47
N <
N/A mg/I Ag - Silver
N/A mg/l Se- Selenium
N/A mg/I Sodium
N/A mg/I Organics (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
N
N/A
N/A
ugll
ug/I
ug/I
mg/l
N/A mg/I VOC method#
method#
method#
N/A mg/1
mg/I
mg/l
mg/l
mg/I
ug/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per rxtii>;6e (of Authorize Age Ne and Title - Please type or pri t
v SLICE
Signature rmittee (or Authorized Agent)
(Da e)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled 18
OM pelynet
Well Identification Number (from Permit): WLCT
Well Depth: NIA ft. Well Diamter: N/A
Screened Interval: N/A ft. to NIA ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is N/A ft above land surface.
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 7.0 , Specific Conductance 581 uMhos
Temp. 17.9 oC, Odor NONE Appearance: CLEAR
Fo Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 10/9/01
Date sample analyzed: 10/9/01 to 11/6/01
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered X
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Yes
Coliform: MF Total <1.0 /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 432 mg/I Al - Aluminum
pH (when analyzed) 7.7 units Ba - Barium
TOC 8.5 mg/I Ca - Calcium
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
14.4
N/A
N/A
N/A
<10.0
N/A
N/A
N/A
No and field acidified X Yes No c),
N/A mgil Ni - Nickel p, fi f sa r;;1 ug/I
N/A mg/1 Pb - Lead C N r- ug/I
0.024 mg/I Zn - Zinc I I ug/I
ca
Ammonia Nitrogen r ;c ; mg/I
Other (Specify Compounds and Concentration Unit rn C-1
N/A mg/1 Fluoride t� 0,427:t mg/I
N/A mg/I MIBK •• N09, ' mg/l
<0.001 mg/I Ag - Silver tw11 Ng mg/l
0.026 mg/1 Se- Selenium NA mg/I
N/A mg/1 Sodium N/A ug/1
N/A mg/l Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/1 Report attached? Yes (1) No X (2)
method#
N/A mg/I
N/A mg/I
mg/1 Cd- Cadmium
mg/1 Chromium: Total
mg/1 Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
N/A mg/I VOC
<0.010 mg/I
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate. and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
rr?iittee (or Authorized Agent)