WI0700012_Monitoring (Report) Feb - April 2009_20090521

PotashCorp
Helping Nature Provide
May 21, 2009
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina, 27699
Attn: Information Management
CERTIFIED MAIL
Subject: Underground Injection Control Program
Quarterly Groundwater Monitoring Report
February 2009 — April 2009
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Qi:
Please find the subject groundwater monitoring report attached. This includes the sampling and reporting
requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of
the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7 and
monitor well MWTF1CR, b) Form GW-59 for each of the fourteen withdrawal wells, c) piezometer level
monitoring field sheet, and d) the summary operational and maintenance report.
Please do not hesitate to contact me at [phone] if you have any questions regarding this
information.
Sincerely,
/0 490(vtitia
D. Daniel Winstead III
Environmental Engineer
PCS Phosphate
Attachments
RECEIVED / DENR / DWQ
Aquifer Pmtectian Section
JUN 15 2009
1530 NC Hwy 306 South, Aurora, NC USA 27806 T [phone]
PCS Phosphate I www.potashcorp.com

pc: Will Hart — Aquifer Protection DWQ, WaRO (w/ attachments)
R. M. Smith/12-07-02 (w/ attachments)
T. S. Inga - Ardaman & Assoc. (w/attachments)
R. A. Allen (w/ attachments)
Mike Brom (w/ attachments)
Anthony Shrewsbury (w/ attachments)
R. B. Lee (w/ attachments)
Total Two Copies
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina, 27699
Attn: Information Management
H:\Reports\2009\Quarterly\TFRAS Report First Quarter 2009.doc
2

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor. Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone:
[phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 42.00 ft. Well Diamter:
MWTF1-CR
2 inch
Screened Interval: 38.70 ft. to 40.70 ft.
Depth to Water Level: 13.35 ft, below measuring point.
Measuring Point is 3.95 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
2000
Field Analysis: pH 6.7 , Specific Conductance 667 uMhos
Temp. 21.1 oC, Odor NONE
Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/31/13
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/21/2009
Date sample analyzed: 4/21/2009 to 5/1/2009
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total <1.0 /100m1
(Note:
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Use MPN method for highly turbid samples)
460
7.0
4.7
16.8
N/A
N/A
N/A
Specific Conductance
Total Ammonia
TKN as N
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
<10.0 mg/I
N/A uMhos
N/A mg/I
N/A mg/I
Yes n/a
No and field acidified
Nitrite (NO2 as N) N/A mg/I
Nitrate (NO3 as N) N/A mg/I
Phosphorus: Total as P 0.620 mg/I
Orthophosphate N/A mg/I
Al - Aluminum N/A ug/I
Ba - Barium N/A ug/I
Ca - Calcium N/A ug/I
Cd- Cadmium <0.001 ug/I
Chromium: Total 0.005 ug/I
Cu - Copper N/A ug/I
N/A ug/I
Hg - Mercury N/A ug/I
K- Potassium N/A ug/I
Mg - Magnesium N/A ug/I
Mn - Manganese 0.064 ug/I
Fe - Iron
Yes n/a No )
Ni - Nickel N/A ug/I
Pb - Lead N/A ug/I
Zn - Zinc N/A ug/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
Fluoride 0.46 mg/I
MIBK N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC . method#
Ag - Silver
Se- Selenium
Sodium
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE
GW-59 Rev 3/2000
REGEIVFO
MAY 2 8 2009
btiA, �, cis ICON
Information Processing Unit
ELC
JUN 92009
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please type or print
Signature of Permittee (or Authori ed Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Well Locations/Site Name: Tank Farm
Telephone: [phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 48.00 ft. Well Diamter:
CIW-7
Screened Interval: 31.00 ft. to 45.25 ft.
Depth to Water Level:
Measuring Point is
4 inch
N/A ft. below measuring point.
N/A ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.8 , Specific Conductance
Temp. 20.9 oC, Odor NONE
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
N/A
628 uMhos
Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH. NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
EXPIRATION DATE:
UIC X
01/31/13
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
Remediation: Infiltration Gallery
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/21/2009
Date sample analyzed: 4/21/2009 to 5/1/2009
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
<1.0
mg/I
/100m1
/100m1
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total 412 mg/I
pH (when analyzed) 7.3 units
TOC 5.0 mg/I
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
180 mg/I
N/A mg/1
N/A mg/1
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/1 Fe - Iron
<10.0 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
<0.010 ug/I
0.016 mg/I
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
Yes n/a No )
N/A ug/I
N/A ug/I
N/A ug/I
<0.001 ug/I
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
<0.005 ug/l Se- Selenium
N/A ug/I Sodium
0.57
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No
N/A ug/I VOC : method#
method#
method#
ug/l
ug/I
ug/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE: �- �/ Ross M. Smith - Manager, Environmental Affairs
GW-59 Rev 3/2000
MAY 2 8 2009
WAi L.. ;ON
Information Processing Unit
ELC
JUN 9 2009
P
Uitte (of Authprized Agent) Name and Title - Please type or print
/o
Signature of Permittee (or Authorized gent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-1
Well Depth: 22.50 ft. Well Diamter:
Screened Interval: 18.30 ft. to 21.12 ft.
Depth to Water Level:
Measuring Point is
4 inch
7.64 ft. below measuring point.
1.52 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 5.9 , Specific Conductance 1807 uMhos
Temp. 19.5 oC. Odor NONE
Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION. GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH. NC 27699-1636 Phone. [phone]
PERMIT #: WI0700012
Non -Discharge
EXPIRATION DATE:
UIC X
01/31/13
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
Remediation: Infiltration Gallery
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
4/21/2009
4/21/2009 to 5/1/2009
PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
mg/I
/100m1
/100m1
Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
1672 mg/I Al - Aluminum
5.9 units Ba - Barium
6.6 mg/I Ca - Calcium
86.8 mg/1 Cd- Cadmium
N/A mg/I Chromium: Total
N/A mg/1 Cu - Copper
N/A mg/1 Fe - Iron
232.0 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
No and field
acidified Yes n/a No )
N/A mg/I Ni - Nickel N/A ug/I
N/A mg/I Pb - Lead N/A ug/l
336.000 mg/I Zn - Zinc N/A ug/1
N/A mg/I Ammonia Nitrogen mg/I
N/A ugll Other (Specify Compounds and Concentration Units)
N/A ug/I Fluoride 0.49 mg/l
N/A ug/I MIBK N/A ug/I
N/A ug/I Ag - Silver N/A ug/I
N/A ug/I Se- Selenium N/A ug/I
N/A ug/I Sodium N/A ug/I
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/l (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
N/A ug/I VOC : method#
N/A ug/I
method#
method#
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. : Jr that there are significant penalties for submitting
false information, includin. the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
RECEi /ED
MAY 2 8 2009
;-C"ION
Wkt` Unit
Information Processing
JUN 9 2009 PP itt (of u orized Ag nt) Name and Titlle- Please type or print
f�%• -Cf
Signature of Permittee (or Authorized Agent) (Date)
Ross M. Smith - Manager Environmental Affairs

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 23.00 ft. Well Diamter:
SWW-2
4 inch
Screened Interval: 18.80 ft. to 21,63 ft.
Depth to Water Level: 6.45 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 5.4 , Specific Conductance 2592
uMhos
Temp. 20.3 oC, Odor NONE Appearance:
CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH. NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/31/13
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
UIC X
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/21/2009
Date sample analyzed: 4/21/2009 to 5/1/2009
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A
Coliform MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 3456
pH (when analyzed) 5.4
TOC 8.7
No and field acidified
mg/I Nitrite (NO2 as N) N/A mg/I
/100m1 Nitrate (NO3 as N) N/A mg/I
/100m1 Phosphorus: Total as P 747.500 mg/I
mg/I
units
mg/I
Chloride 58.3 mg/I
Arsenic N/A mg/I
Grease and Oils N/A mg/I
Phenol N/A mg/I
Sulfate
Specific Conductance
Total Ammonia
TKN as N
478.9 mg/l
N/A uMhos
N/A mg/I
Orthophosphate N/A mg/1
Al - Aluminum N/A ug/I
Ba - Barium N/A ug/I
Ca - Calcium N/A ug/I
Cd- Cadmium N/A ug/I
Chromium: Total N/A ug/I Se- Selenium
Cu - Copper N/A ug/I Sodium
Yes n/a No )
Ni - Nickel N/A ug/I
Pb - Lead N/A ug/I
Zn - Zinc N/A ug/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
Fluoride 0.23 mg/I
MIBK N/A ug/I
Ag - Silver N/A ug/I
N/A ug/I
N/A ug/I
Fe - Iron N/A ug/I Organics: (GC, GC/MS, HPLC)
Hg - Mercury N/A ug/I (Specify test method #. Attach lab report.)
K- Potassium N/A ug/I Report attached? Yes (1) No X (2)
Mg - Magnesium N/A ug/I VOC : method#
N/A mg/I Mn - Manganese N/A ug/I : method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE. Ross M. Smith - Manager, Environmental Affairs
a ..^t'a
MAY 2 8 2009
GW-59 Rev 3/2000
WATh . Y SECTION
Information Processing Unit
zoo
P mittej)(of JAuthh rized Agent) Name and Title - Please type or print
JUN �. �✓ , W f,t Q o ..� ,�, Pf is s /2 f /d
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Well Locations/Site Name: Tank Farm
Telephone: [phone]
No. of Wells to be Sampled 18
Mail Original
to:
Well Identification Number (from Permit): SWW-7
Well Depth: 29.50 ft. Well Diamter: 4 inch
Screened Interval: 25.17 ft. to 27.50 ft.
Depth to Water Level:
Measuring Point is
7.04 ft. below measuring point.
3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
N/A
Field Analysis: pH N/A , Specific Conductance N/A uMhos
Temp. N/A oC, Odor NONE
Appearance: CLEAR
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A /1
(Note. Use MPN method for highly turbid sample
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/
N/
N/
N/
N
N/
N/
N/
N
N
N/A
mg/l
/100m1
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as
sphorus: T
phosphat
luminum
arium _
alcium
admium
ium: To
opper
on
Mercury
Potassium
Mg - Magnesium
Mn - Manganese
Yes n/a No
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone. [phone]
PERMIT#: WI0700012 EXPIRATION DATE: 01/31/13
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X _ Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/21/2009
Date sample analyzed: 4/21/2009 to 4/21/2009
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
Organics: (GC, GC/MS. HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
VOC : method#
method#
method#
ug/l
N/A ug/I
ug/l
mg/I
N/A
N/A
N/A
N/A
N/A
mg/I
ug/l
ug/I
ug/l
ug/I
N/A ug/I
N/A ug/I
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
RECEIVED
VIF1`(, 2 8 2009
SaCTiON
Information ProcessingUnit
Ross M. Smith - Manager, Environmental Affairs
E L �e�mitte (of Auth rized Agent) Name r71d( Title - Please type or print /
(1*iJ, l�n �F-ar2/Y15 s//zr(c
opt
Signature of Permittee (or Authorized Agent) (Date)
JUN 92009

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
M1om Ga ra
Well Identification Number (from Permit): SWW-3
Well Depth: 24.50 ft. Well Diamter: 4 inch
Screened Interval: 20.17 ft. to 23.00 ft.
Depth to Water Level:
Measuring Point is
4.85 ft. below measuring point.
3.17 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
N/A
Field Analysis: pH N/A , Specific Conductance N/A uMhos
Temp. N/A oC. Odor NONE
Appearance: CLEAR
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal
N/A /100m1 Nitrate (NO3 a
Coliform: MF Total N/A /1llml
(Note. Use MPN method for highly turbid sam
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
mg/l
mg/I
osphorus:
hophosph
Aluminu
- Barium
Calcium
Cadmium
omium: T
Copper
Iron
Mercury
Potassium
Mg - Magnesium
Mn - Manganese
Yes n/a No
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
EXPIRATION DATE:
UIC X
01/31/13
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/21/2009
Date sample analyzed:
Laboratory Name:
Certification No(s)
and fi
4/21/2009 to 4/21/2009
PCS PHOSPHATE
330
d"Concentration Units)
Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
VOC method#
method#
method#
ug/I
N/A ug/I
ug/I
mg/I
mg/I
ug/I
ug/I
N/A ug/I
ug/I
N/A ug/I
N/A ug/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
RECEIVED
MAY 2 8 2009
JUN 9 2009
Ross M. Smith - Manager, Environmental Affairs
/P mitt (of Aut rized Agent) Name and Title - Please type or print
•I. "r.)r RMS 7'o?/
Signature of Permittee (or Authorized Agent) (Date)
'Mk t L...1� g; ON
Information Processing Unit

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Ofn If
Well Identification Number (from Permit):
Well Depth: 25.00 ft. Well Diamter:
SWW-4
Screened Interval: 20.50 ft. to 23.30 ft.
Depth to Water Level:
Measuring Point is
4 inch
6.47 ft. below measuring point.
3.42 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 5.3 , Specific Conductance 3960 uMhos
Temp. 32.3 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION. GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
01/31/13
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/21/2009
Date sample analyzed: 4/21/2009 to 5/1/2009
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /l00m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 4296 mg/I
pH (when analyzed) 5.2 units
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
9.0 mg/I
42.7 mg/I
N/A mg/I
N/A mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes n/a
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I Fe - Iron
655.1 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A ug/I
915.000 mg/I
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Yes n/a No )
N/A mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/I Ag - Silver
N/A ug/I
N/A ug/I
Se- Selenium
Sodium
mg/I
0.04 mg/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/l
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
N/A ug/I VOC : method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE: Ross M. Smith - Manager, Environmental Affairs
GW-59 Rev 3/2000
MAY 2 8 2009
I S .C'i tON
tnforrnation Processing Unit
JUN 9 2009
Peittee of Authorized Agent) Name and itle - Please type or print
LI J (ar 0115 s /2 0,
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Well Locations/Site Name: Tank Farm
Telephone: [phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-5
Well Depth: 28.21 ft. Well Diamter:
Screened Interval: 24.83 ft. to 27.21 ft.
Depth to Water Level:
Measuring Point is
4 inch
7.34 ft. below measuring point.
2.96 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 5.9 , Specific Conductance 2565 uMhos
Temp. 28.5 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone' [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/31/13
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/21/2009
Date sample analyzed: 4/21/2009 to 5/1/2009
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
1964 mg/I
6.0 units
8.3 mg/I
44.7 mg/I
N/A mg/l
N/A mg/I
Yes n!a No and field acidified
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I Fe - Iron
691.3 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A mg/l
N/A mg/I
212.000 mg/I
N/A mg/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I VOC
N/A ug/I
Yes nla No )
Ni - Nickel N/A ug/I
Pb - Lead N/A ug/I
Zn - Zinc N/A ug/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
Fluoride 0.23 mg/I
MIBK N/A ug/I
N/A ug/I
Se- Selenium N/A ug/I
Sodium N/A ug/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
method#
Ag - Silver
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
RECEIVED
MAY 2 8 2009
ELC
JUN 9 2009
Ross M. Smith - Manager, Environmental Affairs
Pe ittee f Authorized Agent) Name and Title - Please type or print
Signature of Permittee (or Authorized Agent) (Date)
tnforrnation Processing Unit

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit): SWW-6
Well Depth: 26.00 ft. Well Diamter: 4 inch
Screened Interval: 22.25 ft. to 24.62 ft.
Depth to Water Level:
Measuring Point is
5.75 ft. below measuring point.
2.58 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 7.2 , Specific Conductance 3514 uMhos
Temp. 28.7 oC, Odor NONE Appearance: CLEAR
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH. NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/31/13
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/21/2009
Date sample analyzed: 4/21/2009 to 5/1/2009
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 2396
pH (when analyzed) 7.2
TOC 14.2
Chloride 62.6
Arsenic N/A
Grease and Oils N/A
Phenol N/A
Sulfate 1132.4
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
mg/1 Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
/100m1 Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mg/1 Cd- Cadmium
mg/I Chromium: Total
mg/1 Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/l Mg - Magnesium
mg/I Mn - Manganese
No and field acidified
N/A
N/A
0.255
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/1 Ni - Nickel
mg/I
mg/I
mg/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
Yes n/a No )
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
N/A
N/A
N/A
0.06
N/A
N/A
N/A
N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No
VOC : method#
method#
method#
ug/I
ug/I
ug/l
mg/I
mg/1
ug/I
ug/I
ug/I
ugh
(2)
I certify thatto the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
RECEIVED
iviMT 2 8 2009
ELC
JUN 9 2009
Ross M. Smith - Manager, Environmental Affairs
P mittF (of Aut orized Agent) Name and Title - Please type or print
AC), (� s/e /o p
Signature o Permittee (or Authorized Agent) (Date)
tnfcr,•_..
, �cC;TION
;'rocessing Unit

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Mail Original
to:
Well Identification Number (from Permit): CWW-1
Well Depth: 55.00 ft. Well Diamter:
Screened Interval: 33.27 ft. to 52.68 ft.
Depth to Water Level:
Measuring Point is
4 inch
2.93 ft. below measuring point.
2.25 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
N/A
Field Analysis: pH NIA , Specific Conductance N/A uMhos
Temp. N/A oC, Odor NONE Appearance:
CLEAR
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
EXPIRATION DATE: 01/31/13
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/21/2009
Date sample analyzed:
Laboratory Name:
Certification No(s)
4/21/2009 to 4/21/2009
PCS PHOSPHATE
330
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
Note. Use MPN method for highly turbid samples
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
mg/I
/100m1
/100m1
Nitrite (NO2 as N)
Nitrate (NO3 as N
Phosphorus: T
hophosph
Aluminu
Barium
Calcium
Cadmium
omium: Total
Copper
Iron
- Mercury
Potassium
g - Magnesium
mg/I Mn - Manganese
Yes n/a
No and field acidified
N/A
ug/I
ug/I
ug/l
mg/1
mg/I
MIB N/A ug/I
Ag - N/A ug/I
ug/I
ug/I
Se-
Sodi
rganics: (GC, GC/MS, HPLC)
ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
N/A ug/I VOC method#
N/A ug/I
method#
method#
1 certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
J4'P i
Inforrna
RECE1A ED
MAY 2 $ 2009
c •; =rsrrscessing Unit
c
9 2009
Ross M. Smith - Manager, Environmental Affairs
Pe nitttee (of authorized Agent) Name and Title - Please type or print
�v % /Y15 f/2(
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 52.15 ft. Well Diamter:
CWW-2
Screened Interval: 30.57 ft. to 49.82 ft.
4 inch
Depth to Water Level: 2.43 ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH N/A , Specific Conductance N/A uMhos
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
X
N/A
Temp. N/A oC, Odor NONE Appearance:
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note Use MPN method for highly turbid sample
Dissolved Solids: Total N/
pH (when analyzed) N/
TOC N/
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/
N/
N/
N/
N/
N/
N/
N/A
mg/I
/100mI
/10
mg/I
CLEAR
Nitrite (NO2 as N)
Nitrate (NO3 as
sphorus: T
phosphat
uminum
arium _
alcium -
admium
ium: To
opper _
ro n
Mercury
otassium
Mg - Magnesium
Mn - Manganese
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/31/13
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/21/2009
Date sample analyzed:
Laboratory Name:
Certification No(s)
Yes n/a No and fie
4/21/2009 to 4/21/2009
PCS PHOSPHATE
330
ug/I
N/A ug/I
ug/I
mg/I
mg/I
MIBK N/A ug/I
Ag - S '} N/A ug/I
Se- S N/A ug/I
Sodiu NIA ug/I
/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
N/A ug/I
N/A ug/I
VOC : method#
method#
method#
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
RECEIVED
MAY 2 8 2009
EL
1 {-2nrtftl Signature of Permittee (or Authorized Agent)
Ross M. Smith - Manager, Environmental Affairs
C Pe`R ittee ( f A thorized Agent) Name and Title - Please type or print
,U6 .x-,,,r__,_ci C-f 1?,v)_s s-/..zr A 9
(Date)
WA-, t 'ION
Information Processing Unit

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): CWW-3
Well Depth: 53.00 ft. Well Diamter:
Screened Interval: 36.42 ft. to 50.67 ft.
Depth to Water Level:
Measuring Point is
4 inch
3.62 ft. below measuring point.
3.08 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
N/A
Field Analysis: pH N/A , Specific Conductance N/A uMhos
Temp. N/A oC, Odor NONE Appearance: CLEAR
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
(Note: Use MPN method for highly turbid sample
Dissolved Solids: Total N/
pH (when analyzed) N/
TOC Nl
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Nitrite (NO2 as N)
N/A /100m1 Nitrate (NO3 as
N/A /10lul •sphorus: T
phosphat
luminum
arium _
alcium -
admium
ium: To
opper
ron
Mercury
N/otassium
N/
N/A
Nl
N/
N/
N/
N/
g/I
mg/I
Mg - Magnesium
Mn - Manganese
Yes n/a
Mail Original
to:
N/A
N/A
N/A
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
EXPIRATION DATE:
UIC X
01/31/13
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
Remediation: Infiltration Gallery
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/21/2009
Date sample analyzed:
Laboratory Name:
4/21/2009 to 4/21/2009
PCS PHOSPHATE
Certification No(s) 330
and fie
/1
ug/I
ug/I
ug/I
ug/I
ug/I
N/A ug/I
ug/I
mg/I
uori. N/A mg/I
MIBK N/A ug/I
Ag - S 4 N/A ug/I
Se- S- N/A ug/I
Sodiu N/A ug/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC : method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
RE E VFD
Mir 2 8 2009
t�,•.•. IIQN
Inforr!,?: cr, Processing Unit
ELC
JUN 9 2009
Ross M. Smith - Manager. Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please type or print
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: 53.00 ft. Well Diamter:
CWW-4
4 inch
Screened Interval: 41.67 ft. to 50.92 ft.
Depth to Water Level: 3.07 ft. below measuring point.
Measuring Point is 2.75 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
NIA
Field Analysis: pH N/A , Specific Conductance N/A uMhos
Temp. N/A oC, Odor NONE
Appearance:
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note Use MPN method for highly turbid samp
Dissolved Solids: Total N/
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/
NI
N/
N/
N/
N/
N/
N/
N/
mg/1
/100m1
/100m1
N/A mg/I
CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION. GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/31/13
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/21/2009
Date sample analyzed:
Laboratory Name:
Certification No(s)
Yes n/a No and field acid
4/21/2009 to 4/21/2009
PCS PHOSPHATE
330
Nitrite (NO2 as N) o N/A ug/I
Nitrate (NO3 as :. N/A ug/I
osphorus: T ug/I
ophospha _ y gen mg/I
Iuminum
Barium _ r t Sri N/A mg/I
Calcium _ MIBK N/A ug/l
Cadmium Ag - ` N/A ug/I
mium: To - o Se- S N/A ug/I
Copper , Sodiu NIA ug/I
Iron . •rganics: (GC, GC/MS, HPLC)
Mercury . � •_ /A ug/I (Specify test method #. Attach lab report.)
otassium N/A ug/I Report attached? Yes (1) No X (2)
g - Magnesium N/A ug/I VOC • method#
Mn - Manganese N/A ug/I : method#
rnethod#
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
NL.,.\/ 'L
MAY 2 8 2009
vVA r_, �ci 2 iON
Information Processing Unit
Ross M. Smith - Manager, Environmental Affairs
Pefmittee (of uthorized Agent) Name and Title - Please type or print
S�ar�la�
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-5
Well Depth: 53.17 ft. Well Diamter: 4 inch
Screened Interval: 41.75 ft. to 51.08 ft.
Depth to Water Level: 5.04 ft. below measuring point.
Measuring Point is 2.58 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
N/A
Field Analysis: pH N/A , Specific Conductance N/A uMhos
Temp. N/A oC, Odor NONE Appearance:
CLEAR
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A Nitrite (NO2 as N)
Coliform: MF Fecal N/A Nitrate (NO3 as
Coliform: MF Total N/A osphorus: T
(Note: Use MPN method for highly turbid sampl ophospha
Dissolved Solids: Total N/ t/I .luminum
pH (when analyzed) N/ s :arium
TOC N/ t/1' alcium
NI /1 Cadmium
N/ /I ium: To
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia _
TKN as N
mg/I
/100m1
/100m1
opper
ro n
ercury _
otassium
g - Magnesium
N/A mg/I Mn - Manganese
Yes n/a
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/31/13
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/21/2009
Date sample analyzed:
Laboratory Name:
Certification No(s)
4/21/2009 to 4/21/2009
PCS PHOSPHATE
330
No and field aci �' Yes
ug/I
NIA ug/I
ug/I
mg/I
mg/I
MIBK N/A ug/I
Ag - ` N/A ug/I
Se- S N/A ug/I
Sodiu N/A ug/I
rganics: (GC, GC/MS, HPLC)
ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
N/A ug/I
N/A ug/I
VOC
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
RECEIVED
Mal 2 8 2009
t=°rocessingg Unit
info`, Ya.ti:%^
ELC
JUN 9 2009
Ross M. Smith - Manager, Environmental Affairs
P mittee (o Authorized Agent) Name and Title - Please type or print
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
mom o.omo,
Well Identification Number (from Permit): CWW-6
Well Depth: 53.00 ft. Well Diamter: 4 inch
Screened Interval: 36.62 ft. to 50.88 ft.
Depth to Water Level: 5.40 ft. below measuring point.
Measuring Point is 2.92 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
N/A
Field Analysis: pH N/A , Specific Conductance N/A uMhos
Temp. N/A oC, Odor NONE Appearance:
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note. Use MPN method for highly turbid samp
Dissolved Solids: Total N/
pH (when analyzed) N/
TOC NI
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
mg/I
/100m1
/100m1
CLEAR
Nitrite (NO2 as N)
Nitrate (NO3 as
osphorus: T
ophospha
luminum
Barium _
Calcium
Cadmium
um: To
Copper _
ron
ercury _
otassium
g - Magnesium
Mn - Manganese
Yes n/a
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: W10700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/31/13
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/21/2009
Date sample analyzed: 4/21/2009 to 4/21/2009
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
No and field acid' s
N/A
N/A
N/A
ug/I
ug/I
ug/I
ug/I
MIBK
Ag -
Se- S
Sodiu
rganics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC method#
ug/I
NIA ug/I
ug/l
mg/I
N/A mg/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete. and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
RECEIVED ELC
MAY 2 8 2009
_.,IION
Processing Unit
JUN 9 2009
Ross M. Smith - Manager, Environmental Affairs
Per ittee (of thorized Agent) Name and Title - Please type or print
.4J .r.,�t P 4 r) fl/ S / 6- z (///c�
Signature of Permittee (or Authorized gent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-7
Well Depth: 53.00 ft. Well Diamter:
Screened Interval: 36.58 ft. to 50.83 ft.
4 inch
Depth to Water Level: 4.12 ft. below measuring point.
Measuring Point is 1.25 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
N/A
Field Analysis: pH N/A , Specific Conductance N/A uMhos
Temp. N/A oC, Odor NONE Appearance:
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 ' •.sphorus: To
Coliform: MF Fecal
(Note Use MPN method for highly turbid sample
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
N/
N/
Nt
Nl.
N/
N/
N/
N/
N/
N/
N/A
Specific Conductance
Total Ammonia
TKN as N
phosphat
luminum
arium
alcium
admium
ium: Tot
opper
on
ercury
otassium
g - Magnesium
Mn - Manganese
CLEAR
Yes n/a
Mail Original
to:
N/A
N/A
N/A
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION. GROUNDWATER SECTION
1636 Mail Service Center
RALEIGH. NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
EXPIRATION DATE:
UIC X
01/31/13
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/21/2009
Date sample analyzed: 4/21/2009 to 4/21/2009
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
and field ac
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
mg/I
mg/I
MIB N/A ug/I
Ag - N/A ug/I
Se- ` _ s N/A ug/I
Sodi N/A ug/I
rganics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No
VOC • method#
method#
method#
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 3/2000
RFCED
MAY 2 8 2009
. W�Liti3N
Information Processing Unit
ELC
JUN 92009
Ross M. Smith - Manager, Environmental Affairs
P ,rmij(ee (of authorized Agent) Name and Title - Please type or print
(Date)
Signature of Permittee (or Authorized Agent)

PCS Phosphate Co., Inc. - Tank Farm Remediation System Quarterly Monitoring
Date:
Time:
Tech:
System Gauge Pressures
SW W-1
SW W-7
CW W-1
cww-7
177/J/9.
Flle: 12-07-02
pc: TLe
Reference
Point MSL
Level Rel
to MSL
Ditch
Barge Slip
12.91
10.59
n.5e9
D. 97
Water Level
Control Tank
MSL
Sand Layer Peizometers Level Indicators
Well ID
TOC
Ste Wtr
'
Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
TOC
Elevation
MSL'
Spz-1
10.47
'L/evel
/0
61,�-7
Cpz-1
10.51
/07, 9V
L/g
Spz-2
11.21
�41/.
.t.5-2
lgl/• �. t
Cpz-2
10.25
//a wl .5_
-a
07,t. W
Spz-3
11.87
©.4i7
// 7
Cpz-3
11.12
/02o 6
-/ 9B
Spz-4
11.45
/ L //
,coL/
CPW
9.65
/ .6d
pj, 97
Spz-5
11.45
95-
/n7
MWTF-1A• i
14.35
-5e/7
/D/19
Spz-6
11.23
/D, '/
6U'p/1
MWTF-1B•
14.36
I5;070
9 /0
Spz-7
11.59
/0. 95
Q.‘ V
MWTF-1C •
14.44
/i ij^
/ i0
Spz-8
11.57
-g
MWTF-2A
14.05
',as
,A00
Spz-9
11.01
p�-�/-
d.4y c5 6
. / 5-
MWTF-2B
14.02
/
/ 94
.9/0
Spz-10
12.16
/�/0'
�L7 p
MWTF-2C
14.08
/.. op/
-1, In
SPW
9.95
/%S
7 a 22
/ 4
MWTF-3A
12.21
, C-5-3
-/2c 7
8.641
/, 9,.J-
MWTF-38
12.1a_-
MWTF-3C
12.19
7 . te,
-6.7_ //
Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Stc
Wtr
Level Ft.
Pump
Activation Depth
Rel
Rel MSL
Max Level
Relative To
MSL '
Control
Point
MSL'
Is Well
Pumping?
(((111''')))jess//(N)o
Comments
SWW-,
10.70
/q' '
6'
/Ft.
�/
Y
+1' to+2'
CWW-1
10.60
01.95
9'
_/,
",97
-2'to-1'
/.�
Al
SWW-2
9.99
4 '• L/J`-
6'
-t
4 /$-
+1' to+2'
4/
CWW-2
10.23
9'
-lp,� 7
-2 ' to -1'
Al
SWW-3
9.97
".�213
c/, SS
6'
'7/6
+1 ' to+2'
11/
CWW-3
9.95
42 -
9'
-t 477.5
-2 ' to-1'
S1NW-4
10.73
,
6. 27 7
6'
/1). 4/7
+1' to+2'
CWW-4
10.73
p, 0'7/
9'
;5,9.-3
-2'to-1'
, p
///
SWW-5
10.80
/�'�y
/, j y
6'
Jd,4/ J
+1 'to+2'
V
CWW-5
10.74
-�Q4/
9'
nr'-96
-2 'to-1
SWW-6
10.66
,];7.�3
6'
-pas-+1'to+2'
CWW-6
9.92
S, y.o
9'
-,5, 0
-2 'to-1'
/1/
SWW-7
10.70
7do�y
6'
/04/
+1 'to+2'
/1/
CWW-7
9.95
4/ Lafh
9'
"17' V
-2 'to-1'
/11
Revised 7/29/02
• Riser length added to TOC elevation 1/24/97
D:DalaWorms\Well Form Tank Farm Romer] Wells.xls

PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
February 2009 — April 2009
The Tank Farm Remediation System consists of a series of seven- (7) injection water wells located on the
south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north
side of the Tank Farm Area.
Injection Water Well System
The injection water well system operated with the DPW Water - Ultraviolet Light Disinfection system
during the period.
Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs
Department. The total monthly and quarterly volumes of water injected as well as the month end water
level in the Water Level Control Tank are:
DPW WATER
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
February
657,320
0
657,320
16.3
15.0
March
1,084,754
0
1,084,754
24.3
15.0
April
1,034,108
0
1,034,108
23.9
15.0
TOTALS
2,776,182
0
2,776,182
H:\Reports\2009\Quarterly\TFRAS Report First Quarter 2009.doc
3

Withdrawal Well System
The withdrawal water well pumps are monitored daily by the area Maintenance Department and
preventative maintenance work is performed as needed. The total monthly and quarterly withdrawal water
volumes for the period are:
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
February
30,761
0
30,761
0.8
March
91,068
0
91,068
2.1
April
277,204
0
277,204
6.4
TOTALS
399,033
0
399,033
Some additional short periods of planned downtime for preventative maintenance, pipe header cleaning,
and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these
activities are:
Confined Sand Formation Withdrawal Well (SWW) Pumps
System operated on plant air from 12/29/2009 until the new compressor was received and installed on
4/6/2009.
SWW-1: On 2/17 acid washed well and replaced pump.
SWW-2: On 2/2 repaired pump. On 3/31 acid washed well and replaced pump.
SWW-3: On 2/24 replaced counter.
SWW-4: On 2/23 replaced pump. On 4/1 changed pump. On 4/21 pump discharge plugged. On 4/28
replaced pump.
SWW-5: On 2/19 changed pump.
SWW-6: On 2/19 changed pump.
SWW-7:
H:\Reports\2009\Quarterly\TFRAS Report First Quarter 2009.doc
4

Croatan Formation Withdrawal Well (CWW) Pumps
CWW-1:
CWW-2:
CWW-3:
CWW-4:
CWW-5:
CWW-6:
CWW-7:
H:\Reports\2009\Quarterly\TFRAS Report First Quarter 2009.doc
5