WI0700012_Monitoring (Report)_20060509 (2)

keS-
PCS
Phosphate ' AURORA
PCS PHOSPHATE COMPANY, INC.
P.O. BOX 48, AURORA, NC U.S.A. 27806
May 9, 2006
Evan O. Kane
1636 Mail Service Center
Raleigh, North Carolina, 27626-1636
CERTIFIED MAIL
Subject: Underground Injection Control Program
Quarterly Groundwater Monitoring Report
February 2006 — April 2006
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Evan:
Please find the subject groundwater monitoring report attached. This includes the sampling and reporting
requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of
the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7 and
monitor_we1LMWTFICR,_b)Form_GW-59ioLeach_of_the_fourteen_wdthdrawal wells,_c)_piezometer level
monitoring field sheet, and d) the summary operational and maintenance report.
Please do. not hesitate to contact me at [phone] if you have any questions regarding this
information.
Sincerely,
A9.& ALI ?
D. Daniel Winstead III
Environmental Engineer
PCS Phosphate
Attachments

pc: Will Hart — Aquifer Protection DWQ, WaRO (w/ attachments)
R. M. Smith/12-07-02 (w/ attachments)
T. S. Ingra - Ardaman & Assoc. (w/attachments)
R. A. Allen (w/ attachments)
W. A. Schimming (w/ attachments)
Total Two Copies Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina, 27699
Attn: Information Management
E-Mail:
M. D. Johnson
Nubia Guzman
R. B. Lee
H:\Reports\2006\Quarterly\TFRAS Report Second Quarter 2006.doc
2

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Bnv AO
Contact Person:
Well Locations/t
Well Identificatior
Well Depth: _
Screened Interval.
Depth to Water Le
Measuring Point is
GALLONS of wat
Field Analysis: pH
Temp. 17.9
PARAMETERS: (Sa
COD
Coliform: MF Fecal _
Coliform: MF Total
(Note: Use MPN method for
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
444
7.1
5.5
19.0
N/A
N/A
N/A
<10.0
N/A
N/A
N/A
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/1
uMhos
mg/I
mg/I
E
2)322-8155
to be Sampled
—_ -a -
18Morn a,
For Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
rq
CLEAR
1 X Yes
)
`+- 1C1V I)
oral as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/15/08
Rotary Distributor
Other
Land Application of Stu*
7 1
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/5/06
Date sample analyzed: 4/5/06 to 4/27/06 0.'
Laboratory Name: PCS PHOSPHATE and ENV $ONMENT 1
Certification No(s) 330 10
—
(;(..rl
c J
No and field acidified X
N/A mg/I
N/A mg/I
0.022 mg/I
N/A mg/I
N/A ug/I
N/A ug/I
N/A ug/I
<0.001 ug/I
0.008 ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
0.017 ug/I
Yes No )
Ni - Nickel N/A
Pb - Lead N/A
Zn - Zinc N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride 0.56
MIBK N/A
Ag - Silver N/A
Se- Selenium N/A
Sodium N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
VOC : method#
method#
method#
ug/I
ug/I
ug/I
ug/I
mg/I
ug/I
ug/I
ug/l
ug/I
(2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Pe m
e- (ofAuthorized Agent) Name and Title - Please type or pr'
�M a -7 L
Signature of
ermittee (or Aut
orized Agent)
(D. e)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
MWTF1-CR
Well Depth: 42.00 ft. Well Diamter: 2 inch
Screened Interval: 38.70 ft. to 40.70 ft.
Depth to Water Level: 10.25 ft. below measuring point.
Measuring Point is 3.95 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
2100
Field Analysis: pH 7.2 , Specific Conductance 655 uMhos
Temp. 20.6 oC, Odor NONE Appearance:
CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
EXPIRATION DATE:
UIC X
01/15/08
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor
Other
Land Application of Slue
•'A
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/5/06
Date sample analyzed: 4/5/06 to 4/2
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 10
-rt -11
iY7
7/l
and BNS1RONMENT 1
--i
PARAMETERS: (Samples for metals were collected
COD
Coliform: MF Fecal
Coliform: MF Total
(Note:
Dissolved Solids: Total
pH (when analyzed)
TOC
N/A
N/A
<1.0
Use MPN method for highly turbid samples)
464
6.9
5.3
Chloride
Arsenic
mg/1
/100m1
/100m1
mg/1
units
mg/I
18.2 mg/I
Grease and Oils
Phenol
Sulfate
N/A mg/I
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
unfiltered X Yes
Nitrite (NO2 as N)
Nitrate (NO3 as N)
No and field acidified X Yes No )
N/A mg/I
N/A mg/1
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
0.635 mg/I
N/A mg/I
N/A ug/I
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I Fe - Iron
<10.0 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A ug/I
N/A ug/I
<0.001 ug/I
Ni - Nickel
Pb - Lead
Zn - Zinc
N/A
N/A
N/A
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
0.016 ug/I Se- Selenium
N/A ug/I Sodium
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
0.44
N/A
N/A
N/A
N/A
N/A ug/I VOC
0.058 ug/I
: method#
method#
method#
ug/I
ug/I
ug/I
ug/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Snpth - Manager, Environmental Affairs
(of Authorized Agent) a and Title - Please type or pri t
.v; ,�_ Na�.r� r/Z'1S 5�6 /ob
Signature of Permitte�Authortzed Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: 55.00 ft. Well Diamter:
CWW-1
4 inch
Screened Interval: 33.27 ft. to 52.68 ft.
Depth to Water Level: 5.11 ft. below measuring point.
Measuring Point is 2.25 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 2284
uMhos
Temp. 19.1 oC, Odor NONE Appearance: LT RUST
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
01 /15/08
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of SludER
,
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/4/06
Date sample analyzed: 4/4/06 to
Laboratory Name:
Certification No(s) 330 10
4/27/0f,-;
PCS PHOSPHATE
>0
rn�
A.1<
Mrri
c'tJ
and ENVIRONMENT '
w
PARAMETERS: (Samples for metals were collected unfiltered Yes
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
2024
6.3
9.2
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
73.0
N/A
N/A
N/A
733.4
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/1
mg/I
mg/I
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos
mg/I
mg/1
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A ug/I
n/a
No and field acidified
mg/1 Ni - Nickel
16.250 mg/I
Yes n/a No )
N/A N/A ug/I
N/A mg/1 Pb - Lead N/A ug/l
Zn - Zinc N/A ug/I
N/A mg/I Ammonia Nitrogen ug/I
N/A ug/I Other (Specify Compounds and Concentration Units)
N/A ug/I Fluoride 0.24 mg/I
N/A ug/I MIBK N/A ug/I
N/A ug/I Ag - Silver N/A ug/I
N/A ug/I Se- Selenium N/A ug/1
N/A ug/I Sodium N/A ug/I
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
N/A ug/I VOC method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
ermittee (of Authorized Agent) Name and Title - Please type or print
Signature of Permittee (or Au horized Agent)
O(p
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
prIpm per
Well Identification Number (from Permit):
Well Depth: 52.15 ft. Well Diamter:
CWW-2
Screened Interval: 30.57 ft. to 49.82 ft.
Depth to Water Level:
Measuring Point is
4 inch
5.04 ft. below measuring point.
3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.0 , Specific Conductance
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
2471 uMhos
Temp. 19.9 oC, Odor NONE Appearance:
CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
01/15/08
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/4/06
Date sample analyzed: 4/4/06 to
Laboratory Name:
Certification No(s) 330 10
Lagoon
Remediation: Infiltrations llery
Spray Field X Remediation : .�
Rotary Distributor Land Application of Sludgg
11:1
xl<
PCS PHOSPHATE and ENVIRONMENT
PARAMETERS: (Samples
COD
Coliform: MF Fecal
Coliform: MF Total
for metals were collected unfiltered Yes n/a
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
mg/I
/100m1
/100m1
2136 mg/I
6.3 units
11.5 mg/I
Chloride
Arsenic
76.3 mg/I
Grease and Oils
Phenol
Sulfate
N/A mg/I
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
Nitrite (NO2 as N)
Nitrate (NO3 as N)
No and field acidified Yes n/a No )
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I Fe - Iron
822.0 mg/I
Hg - Mercury
11.750 mg/I Zn - Zinc
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/I Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
0.20
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/I VOC method#
N/A ug/I
: method#
method#
ug/I
ug/I
ug/I
ug/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
1 certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee (of uthorized Agent) Name and Title - Please type or print
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
(I/Om w.,w,
Mail Original
to:
Well Identification Number (from Permit):
Well Depth: 53.00 ft. Well Diamter:
CWW-3
Screened Interval: 36.42 ft. to 50.67 ft.
Depth to Water Level:
Measuring Point is
4 inch
5.39 ft. below measuring point.
3.08 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINOUS
Field Analysis: pH 6.1 , Specific Conductance 2425 uMhos
Temp. 21.9 oC, Odor NONE
Appearance: CLEAR
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sluda
Ca
-t1
Note: Values should reflect dissolved and : e
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
4/4/06
4/4/06 to 4/27/0
PCS PHOSPHATE
330 10
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
mg/I
/100m1
/100m1
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
2120 mg/I Al - Aluminum
6.3 units Ba - Barium
9.9 mg/I Ca - Calcium
Chloride
Arsenic
70.5 mg/l Cd- Cadmium
Grease and Oils
Phenol
Sulfate
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
16.550 mg/I Zn - Zinc
Yes n/a No )
L7
r` s1
J
and El (IRONMENT 1
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A ug/I Other (Specify Compounds and Concentration Units)
N/A ug/I Fluoride
N/A ug/I MIBK
N/A ug/I Ag - Silver
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
N/A ug/I Se- Selenium
N/A ug/I Sodium
0.16
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
791.2 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A ug/I (Specify test method #. Attach lab report.)
ug/I
ug/I
ug/I
ug/I
mg/I
ug/I
ug/I
ug/I
ug/I
N/A ug/I Report attached? Yes (1) No X (2)
N/A ug/I VOC
N/A ug/I
: method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee-(of Authorized Agent) Name and Title - Please type or print
4�ir J /fr $ S//o ld 1,
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
�bom pmi)
Well Identification Number (from Permit):
Well Depth: 53.00 ft. Well Diamter:
CWW-4
4 inch
Screened Interval: 41.67 ft. to 50.92 ft.
Depth to Water Level: 4.27 ft. below measuring point.
Measuring Point is 2.75 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 2735 uMhos
Temp. 23.6 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/15/08
Other
Remediation: Infiltration Gallery
Rotary Distributor Land Application of Slurise
(73
-)
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/4/06
Date sample analyzed: 4/4/06
Laboratory Name:
Certification No(s)
to 4/27/0E
PCS PHOSPHATE i3ff11i
330 10
t't
YC)
i
LVIRONMENT 1
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 2348
pH (when analyzed) 6.3
TOC 8.4
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
90.3
N/A
N/A
N/A
896.6
N/A
N/A
N/A
mgll
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/1
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes nla No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
11.000 mg/I Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
N/A mg/1 Ammonia Nitrogen
N/A ug/I
N/A ug/I 0.12
N/A ug/I N/A
N/A ug/I N/A
N/A ug/l Se- Selenium N/A
N/A ug/I Sodium N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/l VOC method#
method#
method#
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
ug/I
ug/I
ug/I
ug/I
mg/I
ug/I
ug/I
ug/l
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please type or print
0 K,Qde r )/h S J/ 1 %(p
Signature o ermittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Im p
Well Identification Number (from Permit):
Well Depth: 53.17 ft. Well Diamter:
CWW-5
4 inch
Screened Interval: 41.75 ft. to 51.08 ft.
Depth to Water Level: 6.59 ft. below measuring point.
Measuring Point is 2.58 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 2385
uMhos
Temp. 28.2 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge UIC X
01/15/08
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
cD
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/4/06
Date sample analyzed: 4/4/06 to
Laboratory Name:
Certification No(s) 330 10
4/27/U
PCS PHOSPHATE
D0
rn
r'1
{
� r2
c_
and AVIRONMENT 1
--
PARAMETERS: (Samples for metals were collected unfiltered Yes
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1724
pH (when analyzed) 6.4
TOC 6.9
Chloride 77.6
Arsenic N/A
Grease and Oils N/A
Phenol N/A
Sulfate
Specific Conductance
Total Ammonia
TKN as N
625.6
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/1
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
n/a
No and field acidified
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
10.500 mg/I
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/l
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
K- Potassium
Mg - Magnesium
Mn - Manganese
0.15
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/I VOC : method#
: method#
: method#
N/A ug/I
ug/I
ug/I
ug/I
ug/i
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee
(of Authorized Agent) Name and Title - Please type or print
N�C`J W rzM.5 S/o / L
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
,nom pmmlj
Well Identification Number (from Permit): CWW-6
Well Depth: 53.00 ft. Well Diamter: 4 inch
Screened Interval: 36.62 ft. to 50.88 ft.
Depth to Water Level: 7.28 ft. below measuring point.
Measuring Point is 2.92 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 2272 uMhos
Temp. 30.2 oC, Odor NONE
Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Date sample analyzed:
Laboratory Name:
Certification No(s) 330 10
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/4/06
4/4/06 to
4/27/06 =
PCS PHOSPHATE
and E
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A mg/I Nitrite (NO2 as N)
N/A /100m1 Nitrate (NO3 as N)
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
1520 mg/I
6.4 units
10.0 mg/I
95.0 mg/I
N/A mg/I
N/A mg/I
Yes n/a
No and field acidified
N/A mg/1
N/A /100m1 Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I Fe - Iron
Sulfate 492.9 mg/I Hg - Mercury
Specific Conductance
Total Ammonia
TKN as N
N/A uMhos
N/A mg/I
N/A mg/I
15.750 mg/I
Ni - Nickel
N/A mg/1 Pb - Lead
Zn - Zinc
Yes n/a No )
Nr%A
Nf�l
N/A
N/A mg/1 Ammonia Nitrogen
N/A ug/I
N/A ug/l
N/A ug/I
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A ug/I
0.17
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/I VOC : method#
method#
: method#
ug/I
ug/I
ug/I
ug/I
mg/I
ug/l
ug/I
ug/I
ug/I
(2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE.
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Aut,prized Agent) Name and Title - Please t pe or print
L0611.4..4 SA. 0
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 53.00 ft. Well Diamter:
CWW-7
4 inch
Screened Interval: 36.58 ft. to 50.83 ft.
Depth to Water Level: 4.38 ft. below measuring p
Measuring Point is 1.25 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.5 , Specific Conductance
Temp. 23.2 oC, Odor NONE
oint.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
1182 uMhos
Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
01/15/08
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration allery
X Remediation :
Land Application ottIudg"e_;1
—1 pi
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/4/06
Date sample analyzed: 4/4/06 to 4/27/06
Laboratory Name:
Certification No(s) 330 10
►.)
az
alrq
s`- 0
r"
r--
PCS PHOSPHATE and ENVIRONMENT 1
PARAMETERS: (Samples for metals were collected u
COD
N/A mg/I
Coliform: MF Fecal
Coliform: MF Total
N/A /100m1
N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 852 mg/I
pH (when analyzed) 6.5 units
TOC 5.7 mg/I
Chloride 54.7 mg/I
Arsenic N/A mg/I
Grease and Oils N/A mg/I
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
188.8 mg/I
N/A uMhos
N/A mg/I
N/A mg/I
nfiltered Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
No and field acidified
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
5.300 mg/1
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/1
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/I Ag - Silver
N/A ug/I
N/A ug/I
K- Potassium
Mg - Magnesium
Mn - Manganese
Se- Selenium
Sodium
0.18
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/l
N/A ug/1
VOC
: method#
method#
: method#
ug/I
ug/I
ug/l
ug/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee (of uthorized Agent) Name and Title - Please type or print
print/
/0.4. .sn,.d.4� Q/�' co r l 5 s(` c 4 CD
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: 22.50 ft. Well Diamter:
SWW-1
Screened Interval: 18.30 ft. to 21.12 ft.
Depth to Water Level:
Measuring Point is
4 inch
7.07 ft. below measuring point.
1.52 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.0 , Specific Conductance
Temp. 18.6 oC, Odor NONE
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
CONTINUOUS
1440 uMhos
Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
Remediation: Infiltration Gallery
Rotary Distributor Land Application of Slue
Other
Note: Values should reflect dissolved and -- ---iy- I
colloidal concentrations
%t7..!
Date sample collected: 4/4/06 c-_,n/
Date sample analyzed: 4/4/06 to 4/21'6 �,
Laboratory Name: PCS PHOSPHATE andrENVIRONMENT 1
Certification No(s) 330 10 �;
PARAMETERS: (Samples for metals were collected unfiltered
COD
N/A mg/I
Coliform: MF Fecal
Coliform: MF Total
N/A /100m1
N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1124 mg/I
pH (when analyzed) 6.0 units
TOC
5.9 mg/1
Chloride 75.2 mg/I
Arsenic N/A mg/I
Grease and Oils N/A mg/1
Phenol
Sulfate 245.4 mg/1
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
N/A uMhos
N/A mg/I
N/A mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes n/a
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
125.500 mg/I Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/I Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
K- Potassium
Mg - Magnesium
Mn - Manganese
0.69
N/A
N/A
N/A
N/A
ug/I
ug/I
ug/I
ug/I
mg/I
ug/I
ug/I
ug/I
ug/I
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
: method#
N/A ug/I VOC
N/A ug/l
method#
: method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permit e (of Authorized Agent) Name and Title - Please type or print
Signature of Permittee (or Authorized Agent) Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well LocationslSite Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 23.00 ft. Well Diamter:
SWW-2
4 inch
Screened Interval: 18.80 ft. to 21.63 ft.
Depth to Water Level: 7.94 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 1859 uMhos
Temp. 19.6 oC, Odor NONE Appearance: CLEAR
Date sample analyzed:
Laboratory Name:
Certification No(s)
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
67)
Note: Values should reflect dissolved and
colloidal concentrations -- i�t
Date sample collected: 4/4/06 ,
4/4/06 to 4/2 cam:-- u
PCS PHOSPHATE an dr NVIRONMENT 1
330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total 1316
pH (when analyzed) 6.3
TOC 7.8
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
55.1
N/A
N/A
N/A
414.8
N/A
N/A
N/A
mg/I
/100m1
/100m1
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes
n/a No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mgll Cd- Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
80.000 mg/I Zn - Zinc
Yes nla No )
N/A
N/A
N/A
N/A mg/1 Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
0.18
N/A
N/A
N/A
N/A
N/A ug/I VOC
N/A ug/I
: method#
method#
: method#
ug/I
ug/I
ug/I
ug/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Perm tee (of uthppzed Agent) Name and Title - Please type or print
4.,c t ,r u etid,,rr lois S"/ooto
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-3
Well Depth: 24.50 ft. Well Diamter: 4 inch
Screened Interval: 20.17 ft. to 23.00 ft.
Depth to Water Level:
Measuring Point is
8.36 ft. below measuring point.
3.17 ft above land surface.
For Groundwater Treatment
Systems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 5.9 , Specific Conductance 1787 uMhos
Temp. 19.8
oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01 /15/08
Remediation: Infiltration Gallery
Rotary Distributor Land Application of Sludge
Other
tD
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
•
4/4/06 --t 2 t �7
4/4/06 to 4/27/0'6 - -3�
PCS PHOSPHATE and EtWIRONMENT 1
330 10
L 3
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
mg/I
/100m1
/100m1
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes n/a No and field acidified Yes n/a No )
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Phosphorus: Total as P
Orthophosphate
1376 mg/l Al - Aluminum
6.3 units Ba - Barium
7.0 mg/I Ca - Calcium
Chloride
Arsenic
37.2 mg/I Cd- Cadmium
Grease and Oils
Phenol
Sulfate
69.000 mg/I Zn - Zinc
/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/I Ag - Silver
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
485.0 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
0.10
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/I VOC
N/A ug/I
: method#
: method#
: method#
ug/I
ug/I
ug/I
ug/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Authored Agent) Name and Title - Please type or print
Signature of Permittee (or Authorized Agent)
o
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. -Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Forn ,,
Well Identification Number (from Permit): SWW-4
Well Depth: 25.00 ft. Well Diamter: 4 inch
Screened Interval: 20.50 ft. to 23.30 ft.
Depth to Water Level: 6.45 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 5.7 , Specific Conductance 2203 uMhos
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Temp. 27.3 oC, Odor NONE
Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
01 /15/08
Other
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge,
.110
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/4/06
Date sample analyzed: 4/4/06 to
Laboratory Name:
Certification No(s)
r,f
Ix
Try
4/27/M ( U
PCS PHOSPHATE and OIVIRONMENT 1
330 10 --r
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1680
pH (when analyzed) 5.9
TOC 7.9
Chloride
Arsenic
mg/I
Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
Yes n/a
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/1 Pb - Lead
/100m1 Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
34.2 mg/I Cd- Cadmium
Grease and Oils
Phenol
Sulfate
220.000 mg/I Zn - Zinc
Yes n/a No )
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A ug/I Other (Specify Compounds and Concentration Units)
N/A ug/I Fluoride
N/A ug/I MIBK
N/A ug/I Ag - Silver
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
590.7 mg/I Hg - Mercury
N/A uMhos K- Potassium
NIA ug/I Se- Selenium
N/A ug/l Sodium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
0.21
N/A
N/A
N/A
N/A
ug/I
ug/I
ug/I
ug/I
mg/I
ug/I
ug/I
ug/I
ug/I
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/l (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X (2)
N/A ug/I VOC
N/A ug/l
method#
method#
method#
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. 1 am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please type or print
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-5
Well Depth: 28.21 ft. Well Diamter:
Screened Interval:
Depth to Water Level:
Measuring Point is
24.83 ft. to 27.21 ft.
4 inch
7.87 ft. below measuring point.
2.96 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH
Temp. 27
6.0 , Specific Conductance
oC, Odor NONE
I=or Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
CONTINUOUS
2524 uMhos
Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
ra
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
4/4/06
4/4/06 to 4/27/06
PCS PHOSPHATE hJ ENVIRONMENT 1
330 10 .>
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform:
Coliform:
MF Fecal
MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
1568
6.2
11.3
40.0
N/A
N/A
N/A
739.9
N/A
N/A
N/A
Yes n/a
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
/100m1 Phosphorus: Total as P
mg/I
units
mg/I
mg/I
mg/1
mg/I
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos
mg/I
mg/I
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
51.000 mg/I Zn - Zinc
Yes n/a No )
_r
N/A
N/A
N/A
N/A mg/1 Ammonia Nitrogen
N/A ug/I
Cd- Cadmium
Chromium: Total
Cu - Copper
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A ug/I
N/A ug/I
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/I Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
0.41
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/I VOC : method#
: method#
: method#
ug/I
ug/I
ug/I
ug/I
mg/I
u g/I
ug/I
ug/I
ug/I
(2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
PA(of A thorized Agent) Name and Title - Please type or print
k. -4, 12M j 540).6
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled
18
,Irwn pemY,
Well Identification Number (from Permit):
Well Depth: 26.00 ft. Well Diamter:
Screened Interval:
Depth to Water Level:
Measuring Point is
SWW-6
4 inch
22.25 ft. to 24.62 ft.
7.16 ft. below measuring point.
2.58 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 3374 uMhos
Temp. 27.6 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
t.3
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/4106
Date sample analyzed: 4/4/06
Laboratory Name:
Certification No(s)
3310
5>t:i
—4rn
PCS PHOSPHATE and EBt/jtR(ONMENT 1
330 10 cz'
Q. 1>
to 4/27/06—
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
(Note:
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and
N/A
N/A
N/A
Use MPN method for highly turbid samples)
2440
6.2
14.5
76.5
N/A
Oils N/A
N/A
1194.0
N/A
N/A
N/A
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/1
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Yes n/a No )
29.000 mg/I Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
N/A ug/I
--t
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
0.08
N/A
N/A
N/A
Sodium N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
VOC : method#
method#
method#
ug/I
ug/I
ug/I
ug/I
mg/I
ug/I
ug/1
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Authori;ed Agent) Name and Title - Please type or print
2ft 3 6"-A/or0
Signatu of Permi ee (or Au horized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
County: Beaufort
Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-7
Well Depth: 29,50 ft. Well Diamter: 4 inch
Screened Interval: 25.17 ft. to 27.50 ft.
Depth to Water Level: 7.52 ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 5.7 , Specific Conductance 753 uMhos
Temp. 22.9 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC X
01/15/08
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
4/4/06 =c
4/4/06 to 4/27/06- y-i (-)
PCS PHOSPHATE and ONMENT 1
330 10 nry)
PARAMETERS: (Samples for metals were collected
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
unfiltered Yes nla
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
/100m1 Phosphorus: Total as P
Orthophosphate
572 mg/I Al - Aluminum
5.8 units Ba - Barium
7.0 mg/I Ca - Calcium
Chloride
Arsenic
45.4 mg/I Cd- Cadmium
Grease and Oils
Phenol
Sulfate
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
100.4 mg/I Hg - Mercury
N/A uMhos K- Potassium
44.750 mg/I
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/I Other (Specify Compounds and Concentration Units)
Yes n/a No )
N/A ug/I Fluoride
N/A ug/I MIBK
N/A ug/I Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
N/A ug/I
N/A ug/I
N/A mg/I Mg - Magnesium
N/A mg/l Mn - Manganese
r-
[V/A ug/I
N/A ug/I
N/A ug/I
ug/I
0.13
N/A
N/A
N/A
N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/I VOC
N/A ug/I
: method#
method#
method#
mg/I
ug/l
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true,
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory.
false information, including the possibility of fines and imprisonment for knowing violations.
accurate, and complete, and that the laboratory analytical data was produced
I am aware that there are significant penalties for submitting
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please type or print
A2 4) .(,4'', IZMS 6'/6/
Signature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
Contact Person: Jack H. Taylor, Jr.
Well Locations/Site Name: Tank Farm
County: Beaufort
Telephone: [phone]
No. of Wells to be Sampled 18
,from porn.
Well Identification Number (from Permit):
Well Depth: 6.40 ft. Well Diamter:
MWTF1-A
Screened Interval: 3.40 ft. to 5.40 ft.
Depth to Water Level:
Measuring Point is
2 inch
4.72 ft. below measuring point.
3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Systems Check One:
Influent (98)
Effluent (99)
2000
Field Analysis: pH 6.5 , Specific Conductance 660 uMhos
Temp. 18 oC, Odor NONE Appearance:
CLEAR
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note Use MPN method for highly turbid samples)
Dissolved Solids: Total 480
pH (when analyzed) 6.8
TOC 4.7
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
10.1
N/A
N/A
N/A
28.2
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I Ca - Calcium
mg/I
mg/I
mg/I
mg/I Fe - Iron
Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
mg/I Hg - Mercury
uMhos
mg/I
mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE:
01/15/08
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Note:
Lagoon
Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludgc
Other
Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
4/5/06
C73
4/5/06 to 4/27/0F
PCS PHOSPHATE and
330 10
CDFri
r—
ENVIRONMENT 1
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
0.248 mg/I
Yes n/a No )
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A ug/I Other (Specify Compounds and Concentration Units)
N/A ug/I Fluoride 1.62
N/A
N/A
N/A
N/A ug/I MIBK
N/A ug/I Ag - Silver
N/A ug/I
N/A ug/I
K- Potassium
Mg - Magnesium
Mn - Manganese
Se- Selenium
Sodium
N/A
N/A
N/A
N/A
N/A ug/l Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/I VOC
N/A ug/l
: method#
method#
method#
ug/I
ug/I
ug/I
ug/I
mg/I
ug/I
ug/I
ug/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please type or print
-ignature of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806
County: Beaufort
Contact Person: Jack H. Taylor, Jr. Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): MWTF1-B
Well Depth:
13.50 ft. Well Diamter:
Screened Interval: 10.60 ft. to 12.60 ft.
2 inch
Depth to Water Level: 4.88 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
MILILITERS of water pumped/bailed before sampling: 2100
Field Analysis: pH 5.6 , Specific Conductance 363 uMhos
Temp. 19.5 oC, Odor NONE
Appearance: LT YELLOW
Mail Original
to:
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
01/15/08
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/5/06
Date sample analyzed: 4/5/06 to 4/27/0E"
Laboratory Name: PCS PHOSPHATE gd !#y1 iRONMENT 1
Certification No(s) 330 10 cr. =� i
PARAMETERS: (Samples for
COD
Coliform: MF Fecal
Coliform: MF Total
metals were collected unfiltered
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
264
5.7
3.2
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
54.1
N/A
N/A
N/A
18.3
N/A
N/A
N/A
mg/I
/100mI
/100m1
mg/I
units
mg/I Ca - Calcium
mg/I
mg/I
mg/I
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos
mg/I
mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes n/a
No and field acidified
N/A mg/I Ni - Nickel
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
3.850 mg/I
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
Yes n/a No )
N/A ug/I
N/A ug/I
N/A ug/I
--4
1l/A
N/A
N/A
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A ug/I Ag - Silver
N/A ug/I Se- Selenium
N/A ug/I Sodium
K- Potassium
Mg - Magnesium
Mn - Manganese
0.21
N/A
N/A
N/A
N/A
N/A ug/I Organics: (GC, GC/MS, HPLC)
N/A ug/I (Specify test method #. Attach lab report.)
N/A ug/I Report attached? Yes (1) No X
N/A ug/l VOC : method#
method#
method#
N/A ug/I
ug/I
ug/I
ug/I
ug/I
mg/I
ug/I
ug/I
ug/I
ug/l
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the Laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 03/2000
Ross M. Smith - Manager, Environmental Affairs
Permittee (of Authorized Agent) Name and Title - Please type or print
Signature of Permittee (or Authorized Agent)
�Dto
(Date)

PCS Phosphate Co., Inc. - Tank Farm Remediation System Quarterly Monitoring
Date:
Time:
Tech:
W
System Gauge Pressures
SWW-1
A /pi/),.
/
;4'
<7!'re /.
SWW-7
CWw-1
''
CWW-7
DIY. OF WATER Q QUALITY
HAY 11200&
File: 12-07-02
pc: TLB
Rararanc.
Point MU.
Loral Rd
to MYL
Ditch
12.91
brl-
Barge Slip
Water Level
Control Tank
%=MSL
Sand Layer Pelzometers Level Indicators
Wet ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Spz-1
10.47
`�, y.:
, • l%
Cpz-1
10.51
/O. 0
. 4/6
Spz-2
11.21
-
Cpz-2
10.25
/ 2• 9
i
Spz-3
11.87
Z
j a 7
Cpz-3
11.12
, 7/
""65"
/ /
y
Spz-4
11.45
CO. %.
7,i 3
CPW
9.65
/O. /)
- e2 S/3
Spz-5
11.45
9�
0•/�
MWTF-1A*
14.35
-Y %�o'�
�/j.la�
%, 4/8
Spz-6
11.23
9. ,5-
/ 7/
MWTF-1B *
14.36
y. C7�
Spz-7
11.59
/
9, 7
/ 73
MWTF-1C •
14.44
/()-cRo
•y
Spz-8
11.57
''. 6
.J /
MWTF-2A
14.05
(j}, ,5-t)
7
Spz-9
11.01
A_`,
• (rho
MWTF-2B
14.02
// 9j?
•
e5 /0
Spz-10
12.16
. -- /G6'
C•7C.5
MWTF-2C
14.08
A/,' 1-'
. . 7'62
SPW
9.95
7 W.
c 7/
MWTF-3A
12.21//��
6p?
A5-9
MWTF-38
12.18
/C.)• /,,
cLi. n
MWTF-3C
12.19
/''• y�
- /L5/
10.69
Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Stc
Wtr
Level Ft.
Pump
Activation Depth
Rel MSL
Max Level
Relative To
MSL Ft.
Control
Point
MSL'
Is Well
Pumping?
(Y)es/(N)o
Comments
SWW-1
10.70
7 0 %
6'
/, 07
+1 'to+2'
X
CWW-1
10.60
..//
9'
._.�.,6„9
-2'to-1'
1C-s.
SWW-2
9.99
'/, 9Y
6'
/ 95/
+1'to+2'
'� f
CWW-2
10.23
..6-,C09
9'
- 3 96,
-2'to-1'
7/5
SW-3
W
9.97
LSD~
!i ..'
6'
_71 `6
+1'to+2'
i4e:
CWW-3
9.95
5.. 39
9'
-S,6/
-2'to-1'
iff•-S'
SWW-4
10.73
6�- Y `.'
6'
Z22��/`.�
+1 ' to +2'
L -
W
CW -4
10.73
% 's�r /
9'
47
-2'to-1'
SWW-5
10.80
7 Si
6'
/. 87
+1'to+2'
CWW-5
10.74
6,., 9
9'
--c- , //
-2'to_1'
/e
SWW-6
10.66
iz. Z"
6'
/�J6
+1'to+2'
f!i
CWW-6
9.92
9'
-/'a{
-2'to-1'
/ i
W SW-7
10.70
,7;G/er
/-5Gi
6'
/. ScJ�L
+1'to+2'
/ 9
CWW-7
9.95
`9�//. e�
9'
. -5 %
2'to-1'
Revised 7/29/02
* Riser length added to TOC elevation 1/24/97
D:\DatalForms\Well Fonn\Tank Farm Remed Wells.xls

SPZ
SPZ-1 '%
CPZr1
u
CO-1
cIW-1
OFFICE
CUT—OFF WALL
CP2-2 0 ASPHALT ROAD
CWW4
SPZ-E 0
S.P.A
PLANT
W. W-I
CWWR
VA1NORAWAL WELL
FLOW TOTALIZERS
AND CONTROL VALVES
CPZ-3 X
svz9 X
SPZ-6 SPZT
0
PIPERACK SPILL CONTAINMENT PAD
0
0
0
00
WATER LEVEL
CONTROL TANK
cRV. I9 01
e0-2(
•
044
IVI-6�
MWTP4
CLOSTUI
T
-0 \..
SPZ-10
002
004
Y,
Ai I' Yr
I I NI NI)
:{YMII11 OLRI /01'II1N
• M.,.!n....0
• , ..M. .M., ..,«....,. pmm11Awu w111
• ,n..:I..,,..nM.,.»,.,I,Y,tl.4Y WI I1
I..M WIII
t. ...,. ,..., .I„ .,,.I.. IN ..., , ,..M,.,,I
O .*,Is nvn
LOCATION PLAN FOR TANK FAIIM
AREA REMEDIAL ACTION SYSI1 M
WELLS AND PIEZOMETI Ill.
FIGURE 1

PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
February 2006 — April 2006
The Tank Farm Remediation System consists of a series of seven- (7) injection water wells located on the
south side of the Tank Farm Area and a series of fourteen,(14) withdrawal water wells located on the north
side of the Tank Farm Area.
Injection Water Well System
The injection water well system operated with the DPW Water - Ultraviolet Light Disinfection system
during the period.
Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs
Department. The total monthly and quarterly volumes of water injected as well as the month end water
level in the Water Level Control Tank are:
......m .v . . _
._ ._.._-...;
3 3a r
DPW WATER
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
Feb
950,629
0
950,629
23.6
15.0
March
888,890
0
888,890
19.9
15.0
April
466,368
0
466,368
10.8
15.0
TOTALS
2,305,887
0
2,305,887
H:\Reports\2006\Quarterly\TFRAS Report Second Quarter 2006.doc
3

Withdrawal Well System
The withdrawal water well pumps are monitored daily by the area Maintenance Department and
preventative maintenance work is performed as needed. The total monthly and quarterly withdrawal water
volumes for the period are:
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
Feb
297,820
92,635
390,455
9.7
March'
321,275
121,780
443,055
9.9
April
289,941
87,782
377,723
8.7
TOTALS
909,037
302,197
1,221,234
Some additional short periods of planned downtime for preventative maintenance, pipe header cleaning,
and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these
activities are:
Confined Sand Formation'Withdrawal Well (SWW) Pumps
On 279, 2/14, 2/23, 2728, 3/7, 3/15, 3721737317476,-4/12, 4720 and 4/25—flushed out pumps and -Imes on each
of the Confined Sand Formation Withdrawal Well (SSW) and the Croatan Formation Withdrawal Well
(CWW) Pumps. On 2/7 changed oil and filters in the system air compressor.
SWW-1: On 4/18 reset counter.
SWW-2: On 3/23 changed pump. On 3/28 reset pump. On 3/29 changed pump.
SWW-3:
SWW-4: On 2/22 shook pump. On 2/24 changed pump. On 4/25 reset pump. On 4/28 changed pump.
SWW-5: On 4/11 reset pump. On 4/25 reset pump.
SWW-6: On 2/1 changed counter.
SWW-7:
H:\Reports\2006\Quarterly\TFRAS Report Second Quarter 2006.doc
4

Croatan Formation Withdrawal Well (CWW) Pumps
CWW-1: On 3/1 reset pump head. On 3/16 changed pump.
CWW-2: On 2/22 reset pump head. On 3/9 changed pump.
CWW-3:
CWW-4: On 3/23 changed pump. On 4/17 changed counter.
CWW-5: On 2/6 changed pump.
CWW-6: On 4/17 reset pump.
CWW-7:
H:\Reports\2006\Quarterly\TFRAS Report Second Quarter 2006.doc
5