WI0700012_Monitoring (Report)_20010821

r
PCS
Phosphatece AURORA
PCS PHOSPHATE COMPANY, INC.
P.O. BOX 48, AURORA, NC U.S.A. 27806
August 21, 2001
MARK MILLIGAN
GROUND WATER
DENR
1636 MAIL SERVICE CENTER
RALEIGH, NC 27626-1636
CERTIFIED MAIL
Subject: Underground Injection Control Program
Quarterly Groundwater Monitoring Report
May 2001— July 2001
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Mark:
Please find the subject groundwater monitoring report attached. This includes the sampling and reporting
requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of
the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7 and
monitor well MWTF1CR, b) Form GW-59 for each of the fourteen withdrawal wells, c) Form GW-59 for
monitor wells MWTF1A and MWTF1B, d) Form GW-59 for the WLCT, e) piezometer level monitoring
field sheet, and f) the summary operational and maintenance report.
Please do not hesitate to contact me at [phone] if you have any questions regarding this
information.
Sincerely,
k 0
D. Daniel Winstead III
Environmental Engineer
PCS Phosphate
Attachments
pc: Willie Hardison — DWQ- GWS, WaRO (w/attch)

Time:
Tech:
PCS Phosphate Co., Inc. - Tank Farm Remediation System Quarterly Monitoring
bate: 7A1 /p/
A/7
System Gauge Pressures
SWW-1
Neeos £/7/4rrrrven7 *
.r,/-ow g z-
SWW-7
CWW-1
/'
Q_ .J PSr1/9924eel,f-
0-// P�sr
cww-7
File: 15-03-003-02
pc: TLB
Level(msl)
Ditch Level
-5:-.527
Barge Slip
% 98'
Water Level
9,0
Control Tank
%=MSL
e / 6
/
Sand Layer Peizometers Level Indicators
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Spz-1
10.47
'L/evel'
4 y6
4.0/
Cpz-1
10.51
9.76
a %S
Spz-2
11.21
£tho
pf,/p/
Cpz-2
10.25
/6.42/
- 039
0. 7V
Spz-3
11.87
4.0V
3.53
Cpz-3
11.12
/OSt
Spz-4
11.45
/0.90
2i/.5,5
CPW
9.65
/0.S9
- 6.73
Spz-5
11.45
9,� Oo
/57
MWTF-1A•
14.35
4'<O7
/0.07
Spz-6
11.23
9-99
/e9
MWTF-1B •
14.36
9, 9aR
9. 1/4/
Spz-7
11.59
/a,aa�
/ 3'7
MWTF-1C •
14.44
/oQ.30
or.. /2/
Spz-8
11.57
7c?7/
4!33
MWTF-2A
14.05
6„s3/
76
Spz-9
11.01
8, 96
a5 3
MWTF-2B
14.02
// ,�',
a?. /70
Spz-10
12.16
6,/0
O.06
MWTF-2C
14.08
/
/9'66
p
- 0.3 p
SPW
9.95
7 90
c 0.$
MWTF-3A
12.21
lQ''OII
B..? /
W MTF-38
12.18
/t. z o
/ '7�
_
- - -MWTF-3C
12.19
-,t� ,_Od'
- D. 85
Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Stc
Wtr
Level Ft.
Max Level
Relative To
MSL Ft.
Control
Point
MSL'
Is Well
Pumping
(Y)es/(N)o
Comments
SW W-1
10.70
/. /a
/ /Z
+1 ' to +2'
%5
//np.ny 4 go/44
CWw-1
10.60
737
- / 6_5
-2'to-1'
Y� 5
a it,W
SW-2
9.99
799/
/ 72/
+1. to +2'
/E5
it n
CWW-2
10.23
4.40
l0'/, 7/0
-2'ta-1'
rP5
it n
SWW-3,
9.97
7e54
/ 510
+1. to+2'
✓eS
r' /r
CWW-3
9.95
7R7
- / 73
-2 ' to-1'
IP/�5
0 n
SWW-4
10.73
%
/36
/, 5
+1 .to+2'
re
rP5
rr n
CWW-4
10.73
(p. 2/0
-a 60
-2'to-1'
V5
n ii
SWW-5
10:80
16.89
089
+1'to+2'
"
0 ,/
CINW-5
10.74
6.4?
--tee
-2 ' to-1'
�5
SWW-6
10.66
Z
/ .39
+1' to +2'
re,
n q
CWW-6
9.92
/S�9
7,,67
-/3ij
-2' to-1'
'VSpy
,l //
SWW-7
10.70
7/-9
11,/5
+1'to+2'
VSSS
// .,
CWW-7
9.95
o.6o7
- ?33
-2'to-1'
7 e5
piping /B aiM
Revised 8/12/97
* Riser length added to TOC elevation 1/24/97
PCS095.XLS

PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
May 2001— July 2001
The Tank Farm Remediation System consists of a series of seven (7) injection water wells located on the
south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north
side of the Tank Farm Area.
Injection Water Well System
The injection water well system operated with the DPW Water - Anthracite Sand Filter / Ultraviolet Light
(ASF/UV) disinfection system throughout the period.
Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs
Department. The total monthly and quarterly volumes of water injected as well as the month end water
level in the Water Level Control Tank are:
DPW WATER
GALLONS
CONDENSATE
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
May
250,130
0
250,130
5.6
12.9
June
277,960
0
277,960
6.4
13.8
July
294,720
0
294,720
6.6
13.5
TOTALS
822,810
0
822,810
3

Withdrawal Well System
The system was down on 6-6-01 for 5 hours for preventive maintenance (replaced oil cooler, changed oil
and filters) on the air compressor. The system was down for 4 hours to change valves on the air dryer. The
withdrawal water well pumps are monitored daily by the area Maintenance Department and preventative
maintenance work is performed as needed. The total monthly and quarterly withdrawal water volumes for
the period are:
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
May
361,681
211,452
573,133
12.8
June
387,301
150,980
538,281
12.5
July
379,961
185,611
565,573
12.7
TOTALS
1,128,943
548,043
1,676,987
Some additional short periods of planned downtime for preventative maintenance, pipe header _cleaning,
and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these
activities are:
Confined Sand Formation Withdrawal Well (SWW) Pumps
SWW-1: On 5/1, 5/2 & 5/24 shook pump. On 5/10 & 7/11 acid washed the pump. On 5/14 acid washed
well downtime 24 hours. On 5/16 changed pump. On 5/30 repaired pump and changed valves.
SWW-2: On 5/9, 5/31, 6/1, 6/18, 6/25 & 7/10 shook pump. On 5/19, 7/11 & 7/23 acid washed pump. On
5/30 changed airline. On 7/12 changed pump.
SWW-3: On 5/10 & 7/11 acid washed pump.
SWW-4:
SWW-5: On 5/2 changed pump. On 6/4 rebuilt pump. On 6/5 cleaned counter.
S W W-6: On 7/13 changed airline. On 7/24 changed air regulator.
SWW-7: On 7/28 shook pump.
4

Croatan Formation Withdrawal Well (CWW) Pumps
CWW-1:
CWW-2: On 6/19 shook pump.
CWW-3: On 5/24 shook pump. On 5/29 changed pump. On 6/4 cleaned counter.
CW W-4: On 6/11 changed pump. On 7/25 acid washed pump.
CWW-5: On 5/10 replaced air filter and airline. On 7/25 acid washed pump.
CWW-6: On 5/24, 6/27 & 7/25 acid washed pump. On 5/24 changed airline. On 6/1 shook pump and
changed counter. On 6/27 changed totalizer.
CWW-7: On 5/2, 5/15& 6/26 shook pump On 7/11 & 7/25 acid washed pump.
5

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
,Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth:
Screened Interval:
Depth to Water Level:
Measuring Point is
55.00
33.27
7.37
2.25
CWW-1
ft. Well Diamter:
ft. to 52.68 ft.
ft. below measuring point.
ft above land surface.
4 inch
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH 6.9 , Specific Conductance
Temp. 20.2 oC, Odor NONE
For Groundwater Treatment
Sys ems Check One:
RInfluent (98)
Effluent (99)
CONTINUOUS
2170 uMhos
Appearance:
CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations �?
Date sample collected: 7/5/01 b.
Date sample analyzed: 7/5/01 to 7/31/01 V;j
Laboratory Name: PCS PHOSPHATE (V
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD
N/A
Coliform. MF Fecal N/A
Coliform: MF Total N/A
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total 2020
pH (when analyzed) 6.5
TOC 9.2
Chloride 79.6
Arsenic N/A
Grease and Oils N/A
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
696.2
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/1
mg/1
mg/I
mg/I
mg/I
uMhos
mg/1
m g/I
Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
No and field acidified
N/A mg/1
N/A mg/I
2.380 mg/l
KEYA
Ni - Nickel
Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
Yes n/a No
N/A mg/I
N/A mg/1
N/A mg/l
N/A mg/I
N/A mg/1
N/A mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/l
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/l
N N ug/I
NEI ug/I
CrlNit ug/I
mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
0.22
N/A
N/A
N/A
Sodium N/A
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC method#
method#
method#
mg/I
mg/I
mg/l
mg/I
ug/I
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
(of Authorized A
//L
Signatty2 ff.Perrmittee (or Authorized Agent)

01 ..�
s• re

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit): CWW-2
Well Depth:
Screened Interval:
Depth to Water Level:
Measuring Point is
52.15
ft. Well Diamter: 4 inch
30.57 ft. to 49.82 ft.
6.60 ft. below measuring point.
3.00 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH 7.0 , Specific Conductance
For Groundwater Treatment
Sys erns Check One:
Influent (98)
X Effluent (99;;
CONTINUOUS
2228 uMhos
Temp. 19.7 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/5/01
Date sample analyzed: 7/5/01 to
Laboratory Name:
PCS PHOSPHATE
Certification No(s) 330
r)
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform MF Fecal
Coliform: MF Total
(Note:
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
Use MPN method for highly turbid samples)
1980
6.8
10.2
104.7
N/A
N/A
N/A
753.5
N/A
N/A
N/A
mg/1
/100m1
/100m1
mg/I
units
mg/1
mg/l
mg/I
mg/l
mg/I
mg/l
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes n/a
No and field acidified
N/A mg/l Ni - Nickel
N/A mg/I Pb - Lead
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
22.700 mg/l Zn - Zinc
Yes n/a No
r<+
19 ug/I
4- ug/I
N/A mg/I Ammonia Nitrogen
N/A mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/1
N/A mg/l
K- Potassium
Mg - Magnesium
Mn - Manganese
f� ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
0.21
N/A
N/A
Se- Selenium N/A
Sodium N/A
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/l (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X
N/A mg/I VOC method#
method#
method#
N/A mgll
mg/I
mg/1
mg/I
mg/1
mg/1
ug/I
(2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per ittee (of Authorized A t) N e and Title - Please type or print
8�z4�
ee Authorized
Agent) Signatur�p-Permitt (org )
( te)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): CWW-3
Well Depth: 53.00 ft. Well Diamter:
4 inch
Screened Interval: 36.42 ft. to 50.67 ft.
Depth to Water Level: 7.27 ft. below measuring point.
Measuring Point is 3.08 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH 6.4 , Specific Conductance
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
2598 uMhos
Temp. 25.5 oC, Odor NONE Appearance: CLEAR
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1992
pH (when analyzed) 6.6
TOC 9.7
Chloride 226.3
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
533.4
N/A
N/A
N/A
mg/I
units
mg/I Ca - Calcium
mg/I
mg/I
mg/I
mg/1 Fe - Iron
mg/I Hg - Mercury
uMhos
mg/1
mg/1
Orthophosphate
Al - Aluminum
Ba - Barium
Cd- Cadmium
Chromium: Total
Cu - Copper
K- Potassium
Mg - Magnesium
Mn - Manganese
Yes n/a
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
w
a
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/5/01
Date sample analyzed: 7/5/01 to 7/31/0
Laboratory Name: PCS PHOSPHATE 63
Certification No(s) 330 r
No and field acidified
N/A
N/A
3.670
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/l
mg/I
mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes n/a No
PV
ug/I
ug/I
mg/I Ammonia Nitrogen
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/1
mg/I
19T14 ug/l
z mg/l
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC method#
method#
method#
0.19 mg/I
N/A mg/l
N/A mg/I
N/A mg/I
N/A ug/I
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Agent) N e and Title - Please type or print
7,1
St T1ature A(Permittee (or Authorized Agent)
(Dat

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GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): CWW-4
Well Depth: 53.00 ft. Well Diamter:
4 inch
Screened Interval: 41.67 ft. to 50.92 ft.
Depth to Water Level: 6.40 ft. below measuring point.
Measuring Point is 2.75 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
MILILITERS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.5 , Specific Conductance 2517 uMhos
Temp. 28.6 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
r.•
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/5/01
Date sample analyzed:
Laboratory Name:
7/5/01 to 7/31/01
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform MF Fecal
Coliform: MF Total
(Note:
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
Use MPN method for highly turbid samples)
1968
6.7
9.8
132.4
N/A
N/A
N/A
596.6
N/A
N/A
N/A
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
Yes n/a
No and field acidified
N/A mg/1 Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
/100m1 Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/1 Cu - Copper
mg/1 Fe - Iron
mg/1 Hg - Mercury
4.050 mg/I
Yes n/a No
t:t) N/// g/I
ug/I
N/A mg/1 Ammonia Nitrogen
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/1 Fluoride
N/A mg/1 MIBK
N/A mg/I Ag - Silver
N/A mg/I Se- Selenium
N/A mg/l
N/A mg/I
N/A mg/1
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
N/, ug/l
mg/I
0.14 mg/I
N/A mg/I
N/A mg/I
N/A mg/1
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes
N/A mg/1 VOC
N/A mg/I
N/A ug/I
(1) No X (2)
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Signatur
Terry L. Baker - Manager. Environmental Affairs
Peittee (of Authorized Age t Naand Title - Please type or print
L,pitlz5
te)
ermittee (or Aut onzed Agent) (D

Ct 5: is 1
• : •�

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH. NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth:
Screened Interval:
Depth to Water Level:
Measuring Point is
53.17
41.75
6.12
2.58
CWW-5
ft. Well Diamter: 4 inch
ft. to 51.08 ft.
ft. below measuring point.
ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 1958 uMhos
Temp. 30.2 oC, Odor NONE Appearance:
CLDY ORANGE
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
UIC X
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/5/01
Date sample analyzed:
Laboratory Name:
Certification No(s)
Ss
7/5/01 to 7/31/01 GI
PCS PHOSPHATE
330
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal
Coliform: MF Total
(Note. Use MPN method for highly
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
N/A
N/A
turbid samples)
1388
6.5
11.0
77.9
N/A
N/A
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
446.5
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/1
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
Yes n/a
No and field acidified
N/A mg/I
N/A mg/I
Ni - Nickel
Pb - Lead
49.250 mg/I Zn - Zinc
Yes n/a No
Nr"
N/� 55ug/I
N/71t ug/I
ug/I
N/A mg/I Ammonia Nitrogen mg/I
N/A mg/I
N/A mg/1
N/A mg/1
N/A mg/1
N/A mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
0.15
N/A
N/A
N/A
N/A mg/I Sodium N/A
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes
N/A mg/I VOC
N/A mg/I
(1) No
method#
method#
method#
mg/I
mg/I
mg/I
mg/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Pe mittee (of
Signaturff
Authorized Age am and Title - Please type or prin!
*Zr
ermittee (or Authorized Agent)
/t1
(Da

! t' 4

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH. NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): CWW-6
Well Depth: 53.00 ft. Well Diamter:
4 inch
Screened Interval: 36.62 ft. to 50.88 ft.
Depth to Water Level: 7.67 ft. below measuring point.
Measuring Point is 2.92 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH 6.4 , Specific Conductance
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
1906 uMhos
Temp. 31.6 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
09/03/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/5/01 _,
Date sample analyzed: 7/5/01 to 7/31/01 2
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330 -
PARAMETERS: (Samples for metals were collected unfiltered
COD
N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal
Coliform: MF Total
N/A /100m1 Nitrate (NO3 as N)
Yes n/a No and field acidified
N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1296
pH (when analyzed) 6.7
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
10.0
92.7
N/A
N/A
N/A
Specific Conductance
Total Ammonia
TKN as N
Orthophosphate
mg/1 Al - Aluminum
units Ba - Barium
mgll Ca - Calcium
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
372.8 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mgll Mg - Magnesium
N/A mg/I Mn - Manganese
N/A
N/A
4.625
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
m g/I
mg/l
mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes nla No
mgll Ammonia Nitrogen
mgll
mgll
mg/I
mgll
mgll
mg/I
mg/I
mg/I
mg/I
mg/I
mg/1
Organics: (GC, GC/MS,
(Specify test method #.
Report attached? Yes
VOC
N ug/I
t N/ ug/I
�1 NP4 ug/I
Other (Specify Compounds and Concentration Units)
mg/I
Fluoride 0.16 mgll
MIBK N/A mg/1
Ag - Silver N/A mgll
Se- Selenium N/A mg/I
Sodium N/A ug/I
HPLC)
Attach lab report.)
(1) No X (2)
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Age Na e and Title - Please type or rint
Signatur Af Permittee (or Authorized Agent) ( te)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. -Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit): CWW-7
Well Depth: 53.00 ft. Well Diamter: 4 inch
Screened Interval: 36.58 ft. to 50.83 ft.
Depth to Water Level: 6,67 ft. below measuring point.
Measuring Point is 1.25 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.7 , Specific Conductance 1022 uMhos
Temp. 23.7 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012
Non -Discharge
NPDES
EXPIRATION DATE:
UIC X
09/03/01
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field
Rotary Distributor
Other
N
w
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
ci
Ci
7/5/01 7art c' =
7/5/01 to 7/31/0' c�
PCS PHOSPHATE rn
N v;
330 rT
r-I
O
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 760
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
6.9
8.0
68.5
N/A
N/A
N/A
156.1
N/A
N/A
N/A
mg/1
units
mg/I Ca - Calcium
mgll
mg/I
mg/I
mg/1 Fe - Iron
mg/1 Hg - Mercury
uMhos
mgll
mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
K- Potassium
Mg - Magnesium
Mn - Manganese
Yes n/a No
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
N/A
N/A
5.480
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
and field acidified
mg/I
mg/I
Ni - Nickel
Pb - Lead
Yes n/a No
mg/I Zn - Zinc
mg/1 Ammonia Nitrogen
mg/1
mg/1
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/1
mg/1 VOC
mg/I
N fm ug/I
N� ug/I
.,� F ug/I
mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
0.17
N/A
N/A
N/A
N/A
method#
method#
method#
mg/I
mg/1
mg/1
mg/1
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per -- - Authorized Agent) e d Title - Please type or print
Signature e mittee (or Authorized Agent) (Date

'r';..:�

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): CIW-7
Well Depth: 48.00
Screened Interval: 31.00 ft. to 45.25 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is N/A ft above land surface.
ft. Well Diamter: 4 inch
For Groundwater Treatment
Sys ems Check One,
X Influent (98)
Effluent (99i
MILILITERS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.9 , Specific Conductance 671 uMhos
Temp. 22.1 oC. Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery r-,i
Spray Field X Remediation :
UIC X
09/30/01
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/3/01
Date sample analyzed:
Laboratory Name:
Certification No(s)
a
c�
r•.1
7/3/01 to 7/31/01 .4—
m
PCS PHOSPHATE and i` VIR?J 1ENT 1
330 10 r '
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N) N/A mg/l
<1.0 /100m1 Phosphorus: Total as P 0.025 mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate N/A mg/l
mg/I Al - Aluminum N/A mg/I
7.2 units Ba - Barium N/A mg/I
2-----, mg/I Ca - Calcium NIA mg/1
15.1 mg/I Cd- Cadmium <0.001 mg/1
Arsenic N/A mg/1 Chromium: Total <0.005 mg/l
Grease and Oils N/A mg/I Cu - Copper N/A mg/1
Phenol N/A mg/I Fe - Iron N/A mg/I
Sulfate <10 mg/1 Hg - Mercury N/A mg/I
N/A uMhos K- Potassium N/A mg/I
N/A mg/1 Mg - Magnesium N/A mg/I
N/A mg/l Mn - Manganese 0.013 mg/I
No and field acidified X Yes No
N/A mgil Ni - Nickel
Dissolved Solids: Total 452
pH (when analyzed)
TOC
Chloride
Specific Conductance
Total Ammonia
TKN as N
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
.c- C)
pt� N o ug/I
Nh ug/I
.. 3
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
mg/I
0.51 mgll
N/A mg/1
N/A mg/I
Se- Selenium N/A mg/I
Sodium N/A ug/l
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC : method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Pejttee (of Authorized ent Name and Title - Please type or print
(a'; S7/Z-/�O
Signatu.W f Permittee or Authorized Agent) (Date)

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GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: 42.00
MWTF1-CR
ft. Well Diamter: 2 inch
Screened Interval: 38.70 ft. to 40.70 ft.
Depth to Water Level: 12.30 ft. below measuring point.
Measuring Point is 3.95 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH 7.3 , Specific Conductance
For Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
2100
628 uMhos
Temp. 23.8 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation : c.J
Rotary Distributor Land Application of Sludge 0-1
09/30/01
Other
i
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
0
Zia
7/3/01
7/3/01 to 7/31/0
PCS PHOSPHATE and:ENVIWOJIMENT 1
330 10 '—'
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/1
Coliform: MF Fecal N/A /100m1
Coliform: MF Total <1.0 /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
418
7.5
5.6
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
11.9
N/A
N/A
N/A
49.4
N/A
N/A
N/A
mg/1
units
mg/l
mg/l
mg/l
mg/I
mg/I
mg/l
uMhos
mg/l
m g/I
X Yes
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
No and field acidified X
N/A
N/A
mg/1
mg/l
0.285 mg/l
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes No
N/A mg/I Ammonia Nitrogen
N/A mg/l
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/1
N/A mg/1
<0.001 mg/I
0.007 mg/l
N
OS
NRk ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
N/A mg/1 Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/l Report attached? Yes (1) No X
0.55
N/A
N/A
N/A
N/A
N/A mg/I
0.053 mg/I
VOC : method#
method#
method#
mg/1
mg/l
mg/I
mg/I
mg/1
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Si
Terry L. Baker - Manager, Environmental Affairs
Pe ittee (of Authorized A nt) me and Title - Please type or print
ez.o
e> ;
e or Authorized Agent) (�d'ate)
gnatu ermitte

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy
Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-1
Well Depth: 22.50 ft. Well Diamter: 4 inch
Screened Interval: 18.30 ft. to 21.12 ft.
Depth to Water Level: 7.12 ft. below measuring point.
Measuring Point is 1.52 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One
Influent (98;;
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.8 , Specific Conductance 2208 uMhos
Temp. 19.3 oC, Odor NONE
Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
09/30/01
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/5/01
Date sample analyzed: 7/5/01 to 7/31/02.0
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
D
c)r
i
mer
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Yes n/a No and field acidified
N/A mg/I Ni - Nickel
N/A mg/l Pb - Lead
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 1576 mg/1 Al - Aluminum
pH (when analyzed) 6.3 units Ba - Barium
TOC 10.4 mg/I Ca - Calcium
Chloride
Arsenic
Grease and Oils
85.4 mg/I Cd- Cadmium
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
129.500 mg/I Zn - Zinc
Yes n/a No
"d
N/A mg/I Ammonia Nitrogen
--tfri
ug/I
N I� ugll
4— ug/I
mg/I
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
N/A mg/I Fe - Iron
N/A mg/I Fluoride 0.65 mg/I
N/A mg/1 MIBK N/A mg/I
N/A mg/I Ag - Silver N/A mg/1
N/A mg/I Se- Selenium N/A mg/I
N/A mg/1 Sodium N/A ug/I
N/A mg/I Organics: (GC, GC/MS, HPLC)
554.1 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC
N/A mg/I
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Pe . itt2. (of Authorized Age Na e and Title - Please type or print
Signatur-s.' • ermittee (or Authorized Agent)
zI
(1 te)

U ! b S: PI

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
SWW-2
Well Depth: 23.00 ft. Well Diamter:
Screened Interval: 18.80 ft. to 21.63 ft.
Depth to Water Level:
Measuring Point is
4 inch
7.74 ft. below measuring point.
3.42 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH 6.9 , Specific Conductance
Temp. 18.9 oC, Odor NONE
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
2115 uMhos
Appearance: CLEAR
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
(Note:
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
Use MPN method for highly turbid samples)
1624
6.5
10.6
57.0
N/A
N/A
N/A
583.2
N/A
N/A
N/A
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
Yes n/a
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
UIC X
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/5/01 --
Date sample analyzed: 7/5/01 to 7131/0'
Laboratory Name: PCS PHOSPHATE G7
Certification No(s) 330 N
No and field acidified Yes n/a No
N/A mg/I Ni - Nickel
N!A mg/I Pb - Lead N
/100m1 Phosphorus: Total as P
Orthophosphate
mg/l Al - Aluminum
units Ba - Barium
mgll Ca - Calcium
61.500 mg/I
N/A mg/I
N/A mg/I
mg/1 Cd- Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
uMhos K- Potassium
mgil Mg - Magnesium
mg/I Mn - Manganese
N/A mg/I
N/A mg/I
N/A mg/I
Zn - Zinc
Ammonia Nitrogen
1 ugll
ug/I
mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
0.31 mg/I
N/A mg/1
N/A mg/I
Se- Selenium N!A mg/I
Sodium N/A ug/l
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per r ee1of Authorized Agent Nam and Title - Please type or print
CPA
mittee (or Authorized Agent) Da )
SignatureL�T g )

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: 24.50
Screened Interval: 20.17 ft. to 23.00 ft.
Depth to Water Level: 7.36 ft. below measuring point.
Measuring Point is 3.17 ft above land surface.
SWW-3
4 inch
ft. Well Diamter:
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH 6.6 , Specific Conductance
Temp. 21.3 oC, Odor NONE
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
1916 uMhos
Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
09/30/01
Rotary Distributor
Other
Land Application of Sludge tv
(,J
crN
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/5/01
Date sample analyzed:
Laboratory Name:
7/5/01 to 7/31 /01
PCS PHOSPHATE
Certification No(s) 330 -
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1472 mg/1
pH (when analyzed) 6.6 units
TOC 8.8 mg/I
Chloride 44.0 mg/I Cd- Cadmium
Arsenic N/A mg/1 Chromium: Total
N/A mg/l Cu - Copper
N/A mg/I Fe - Iron
570.6 mg/1 Hg - Mercury
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A uMhos
N/A mg/I
N/A mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Yes n/a No and field acidified Yes n/a No = z
N/A mg/1 Ni - Nickel N NM& ug/I
N/A mgll Pb - Lead rtr ug/I
30.750 mg/I Zn - Zinc r'\ ug/I
N/A mg/I Ammonia Nitrogen x mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/1
N/A mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
N/A mg/1 Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X
0.14
N/A
N/A
N/A
N/A
N/A mg/1
N/A mg/I
VOC : method#
method#
method#
mgll
mg/l
mg/I
mg/l
ugll
(2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per ee (of Authorized Ag nt) N e and Title - Please type or print
Signature ermittee (or Auth rized Agent) (Date)

d .� PI4 C '��'d i

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-4
Well Depth:
25.00 ft. Well Diamter:
Screened Interval: 20.50 ft. to 23.30 ft.
4 inch
Depth to Water Level: 7.36 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Fo Groundwater Treatment
Sys ems Check One:
Influent (98',
X Effluent (99)
CONTINUOUS
Field Analysis: pH 5.8 , Specific Conductance 2218 uMhos
Temp. 33.3 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
rY
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/5/01
CD
Date sample analyzed: 715/01 to 7/31/0
Laboratory Name: PCS PHOSPHATE r
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
Yes n/a
No and field acidified Yes n/a No
COD N/A mg/l Nitrite (NO2 as N) N/A
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A
Coliform: MF Total N/A /100m1 Phosphorus: Total as P 73.500
(Note: Use MPN method for highly turbid samples) Orthophosphate N/A
Dissolved Solids: Total 1512 mg/I Al - Aluminum N/A
pH (when analyzed) 6.2 units Ba - Barium N/A
TOC 7.2 mg/I Ca - Calcium N/A
Chloride 40.1 mg/I Cd- Cadmium N/A
N/A mg/I Chromium: Total N/A
N/A mg/1 Cu - Copper N/A
N/A mg/1 Fe - Iron
706.6 mgll Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
N/A
N/A
mg/I
mg/I
mg/1
Ni - Nickel
Pb - Lead
Zn - Zinc
mg/I Ammonia Nitrogen
mg/I
mg/I
mg/I
mg/I
mg/1
mg/I
mg/I
mg/1
mg/I
mg/I
mg/I
fy (n
ug/I
N ug/I
Nam, ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
mg/1
0.07 mg/I
N/A mg/I
N/A mg/I
Se- Selenium N/A mg/I
Sodium N/A ug/I
Organics: (GC, GC/MS. HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC method#
method#
method#
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per -- .f Authorized Agent) me nd Title - Please type or print
Signature of -rTittee (or Authorized Agent) (Dat
D%

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
SWW-5
Well Depth: 28.21 ft. Well Diamter: 4 inch
Screened Interval: 24.83 ft. to 27.21 ft.
Depth to Water Level: 6.89 ft. below measuring point.
Measuring Point is 2.96 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99;;
CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 2460 uMhos
Temp. 30.2 oC, Odor NONE
Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE:
09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
cp •
ram)
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations C
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
7/5/01
7/5/01 to 7/31/0
PCS PHOSPHATE ry
330
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1716
pH (when analyzed) 6.4
TOC 12.5
Chloride 53.9
Arsenic N/A
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
694.7
N/A
N/A
N/A
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
Yes nla No and field acidified
/100m1 Phosphorus: Total as P
Orthophosphate
mg/1 Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
mg/1 Chromium: Total
mg/1 Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
79.000 mg/I
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Yes n/a No
ug/I
r ug/I
Id 4 ug/I
N/A mg/I Ammonia Nitrogen
N/A mg/I
N/A mg/1
N/A mg/1
N/A mg/I
N/A mg/I
N/A mg/l
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
0.32
N/A
N/A
Se- Selenium N/A
Sodium N/A
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/1 (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes
N/A mg/I VOC
N/A mg/I
(1) No
method#
method#
method#
mg/I
mg/I
mg/1
mg/I
mg/I
ug/I
(2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per -e of Authorized Agent Nameeand Title - Please type or print
elmittee (or Authorized Agent) (D te)
Signature

r.�
t`.
tT,

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-6
Well Depth: 26.00
Screened Interval: 22,25 ft. to 24.62 ft.
Depth to Water Level: 7.39 ft. below measuring point.
ft. Well Diamter: 4 inch
Measuring Point is 2.58 ft above land surface.
Fo Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
MILILITERS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.3 , Specific Conductance 2360 uMhos
Temp. 30.5 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/30/01
Spray Field X Remediation :
h)
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
rD
7/5/01
7/5/01 to 7/31/01 N
PCS PHOSPHATE �o
m
Certification No(s) 330 —0
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A mg/I Nitrite (NO2 as N)
N/A /100m1 Nitrate (NO3 as N)
Yes n/a No and field acidified Yes nla No
rn�
N/A mg/I ug/I
N/A mg/I '`"1 N& ug/I
49.750 mg/l N1 i ug/I
N/A /100m1 Phosphorus: Total as P
(Note Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
1648 mg/I Al - Aluminum
6.7 units Ba - Barium
16.5 mg/I Ca - Calcium
92.3 mg/1 Cd- Cadmium
Arsenic
Grease and Oils
Phenol
Sulfate
Ni - Nickel
Pb - Lead
Zn - Zinc
N/A mg/l Ammonia Nitrogen
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/I Fluoride
N/A mg/I MIBK
N/A mg/I Ag - Silver
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
615.9 mg/1 Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/1 Mn - Manganese
N/A mg/1
0.07
N/A
N/A
Se- Selenium N/A
N/A mg/1 Sodium N/A
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X
N/A mg/I VOC method#
N/A mg/I
method#
method#
mg/1
mg/I
mg/I
mg/I
mg/1
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Signatu
Terry L. Baker - Manager, Environmental Affairs
Pee .ttee (of Authorized A ens) me and Title - Please type or print
Prt
ee (or Authorized Agent) (Date)
Permitt g )

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy
Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
o
Well Identification Number (from Permit): SWW-7
Well Depth: 29.50 ft. Well Diamter:
Screened Interval: 25.17 ft. to 27.50 ft.
4 inch
Depth to Water Level: 7.13 ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
MILILITERS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 1012 uMhos
Temp. 26.3 oC, Odor NONE Appearance: CLEAR
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
(Note:
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
Use MPN method for highly turbid samples)
752
6.0
10.9
65.8
N/A
N/A
N/A
178.9
N/A
N/A
N/A
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
Yes n/a No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
/100m1 Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mgll Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
46.750 mg/I
7/5/01
7/5/01 to 7/31 /041
PCS PHOSPHATE N
fi
330
Yes n/a No
N/A mg/I Ammonia Nitrogen
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/l Fluoride
N/A mg/I MIBK
N/A mg/I Ag - Silver
N/A mg/I Se- Selenium
N/A mg/1 Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X
0.11
N/A
N/A
N/A
N/A
N/A mg/I VOC : method#
method#
method#
N/A mg/1
ug/I
ug/I
ug/I
mg/l
m g/1
mg/I
mg/I
mg/l
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Agen Nam and Title - Please type or print
ignaturept efmittee (or Authorized Agent) (Date)

01 vn Si' 0,1 5-P1

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): MWTF1-A
Well Depth: 6.40 ft. Well Diamter: 2 inch
Screened Interval: 3.40 ft. to 5.40 ft.
Depth to Water Level: 4.28 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Fo Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
2100
Field Analysis: pH 7.3 , Specific Conductance 577 uMhos
Temp. 25.0 oC, Odor
NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
09/30/01
r..
Rotary Distributor Land Application of Sludge
Other
c: z
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 7/3/01 Mob
Date sample analyzed: 7/3/01 to 7/31/0'C
Laboratory Name: PCS PHOSPHATE fv
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a No and field acidified Yes n/a No
COD N/A mg/I Nitrite (NO2 as N) N/A mg/I Ni - Nickel fV NYAL ug/I
.
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A mg/I Pb - Lead Ng ug/I
Coliform: MF Total N/A /100m1 Phosphorus: Total as P 0.408 mg/I Zn - Zinc v Ng. ug/I
(Note: Use MPN method for highly turbid samples) Orthophosphate N/A mg/1 Ammonia Nitrogen mg/l
Dissolved Solids: Total 360 mg/I Al - Aluminum N/A mg/1 Other (Specify Compounds and Concentration Units)
pH (when analyzed) 7.2 units Ba - Barium N/A mg/I Fluoride 2.36 mg/I
TOC 4.2 mg/1 Ca - Calcium N/A mg/I MIBK N/A mg/I
Chloride 6.9 mg/I Cd- Cadmium N/A mg/1 Ag - Silver N/A mg/I
Arsenic N/A mg/1 Chromium: Total N/A mg/1 Se- Selenium N/A mg/I
N/A mg/I Cu - Copper N/A mgll Sodium N/A ugll
N/A mg/I Fe - Iron N/A mg/1 Organics: (GC, GC/MS, HPLC)
55.9 mg/l Hg - Mercury N/A mg/I (Specify test method #. Attach lab report.)
N/A uMhos K- Potassium N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I Mg - Magnesium N/A mg/1 VOC : method#
N/A mg/I Mn - Manganese N/A mg/I method#
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
method#
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per r ttee (of Authorized Age Nape and Title - Please type or print
g%z,//a
gnature
ermittee (or Authorized Agent)
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): MWTF1-B
Well Depth: 13.50 ft. Well Diamter:
2 inch
Screened Interval: 10.60 ft. to 12.60 ft.
Depth to Water Level: 4.92 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (991
MILILITERS of water pumped/bailed before sampling: 2100
Field Analysis: pH 5.9 , Specific Conductance 383 uMhos
Temp. 23.8 oC, Odor NONE Appearance: LT CLDY WHTE
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery.
Spray Field X Remediation : t\)
UIC X
09/30/01
Rotary Distributor Land Application of Sludge
Other
(,)
crt
GJ
Note: Values should reflect dissolved and In'"�
colloidal concentrations p
0
Date sample collected: 7/3/01 �— c",-,.,
Date sample analyzed: 7/3/01 to 7l311 Q'n
Laboratory Name: PCS PHOSPHATE 41 =rri
Certification No(s) 330 V
=! '
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Yes n/a No and field acidified Yes n/a No
N/A mg/I Ni - Nickel
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 268 mg/I Al - Aluminum
pH (when analyzed) 6.0 units Ba - Barium
TOC
4.0 mg/I Ca - Calcium
Chloride
Arsenic
Grease and Oils
42.6 mg/l Cd- Cadmium
N/A mg/1 Chromium: Total
N/A mg/I Cu - Copper
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
35.7 mg/I Hg - Mercury
N/A uMhos K- Potassium
NIA mg/I Pb - Lead
0.374 mg/I Zn - Zinc
;ha
rn t.,
+lifts_'
N/A mg/I Ammonia Nitrogen
J
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/I Fluoride
NIA mg/I MIBK
N/A mg/I Ag - Silver
N/A mg/I Se- Selenium
N/A mg/I Sodium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
0.34
N/A
N/A
N/A
N/A
N/A mg/1 Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/1 Report attached? Yes (1) No X
N/A mgll VOC
N/A mg/1
method#
method#
method#
ug/I
ug/I
ug/I
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Signature
Terry L. Baker - Manager, Environmental Affairs
Per ee of Authorized Agen am
and Title - Please type or print
'11" 6,4-1
(Date)
rmittee (or Authorized Agent)

:Sl Oa MA 10

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH. NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
WLCT
Well Depth: N/A ft. Well Diamter: NIA
Screened Interval: N/A ft. to N/A ft.
Depth to Water Level:
Measuring Point is
N/A
ft. below measuring point.
N/A ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH 6.9 , Specific Conductance
Temp. 19.8 oC; Odor NONE
For Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
CONTINUOUS
659 uMhos
Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
-
Land Application of Sludge
IV
W
C71
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 713/01 —' c-)_
Date sample analyzed: 7/3/01 to 7/31/0 0=r
Laboratory Name: PCS PHOSPHATE anii f NVOINMENT 1
Certification No(s) 330 10 N c:,-~
V
PARAMETERS: (Samples for metals were collected unfiltered
COD NIA mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total <1.0 /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 448
pH (when analyzed) 7.1
TOC 7.1
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
12.7
N/A
N/A
N/A
<10.0
N/A
N/A
N/A
mg/I
units
mg/I
mg/I
mg/I
m g/I
mg/I
mg/I
uMhos
mg/l
mg/I
X Yes
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
No and field acidified X
N/A mg/1 Ni - Nickel
N/A mg/1 Pb - Lead
0.028 mg/I Zn - Zinc
Yes No
N/A mg/I Ammonia Nitrogen
N N"' ug/l
J
N� ug/I
z mg/I
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/I
<0.001 mg/I
Fluoride 0.52 mg/I
N/A mg/I MIBK N/A mg/I
Ag - Silver N/A mg/I
N/A mg/I
N/A ug/I
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
0.015 mg/I
N/A mg/1
K- Potassium
Mg - Magnesium
Mn - Manganese
0.014 mg/I
Se- Selenium
Sodium
ug/I
N/A mg/I VOC method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Pe mi (of Authorized A t) N 'mee and Title - Please type or print
Signatur f'Permittee (or Authorized Agent) (Date)

yew -a/a00-DDT?v-76/6 s5 ry
PCS
Phosphate
AURORA
PCS PHOSPHATE COMPANY, INC.
P.O. BOX 48, AURORA, NC U.S.A. 27806
May 24, 2001
MARK MILLIGAN
GROUND WATER
DENR
1636 MAIL SERVICE CENTER
RALEIGH, NC 27626-1636
CERTIFIED MAIL
Subject: Underground Injection Control Program
First Quarter Groundwater Monitoring Report
February 2001 — April 2001
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Mark:
Please find the subject groundwater monitoring report attached. This includes the sampling and reporting
requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of
the overall Tank Farm Remedial Action Plan Enclosesi are• a). Form GW-59 for injection well CIW7 and
monitor well MWTF 1 CR, b) Dorm GW-59 for each of the fourteen withdrawal w t11s, c) Form GW-59 for
monitor wells MWTF1A and MWTF1B, d) Form GW-59 for the WLCT, e)-p ezometer level monitoring
field sheet, and f) the summary operational acid maintenance repoff.
Please do not hesitate to contact me at [phone] if you h. e any questions regarding this
information.
Sincerely,
2-00tAit:a —
111LA,L,49t�oQ �
D. Daniel Winstead III
Environmental Engineer
PCS Phosphate
Attachments
pc: Willie Hardison — DWQ- GWS, WaRO (w/attch)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-1
Well Depth:
22.50 ft. Well Diamter:
Screened Interval: 18.30 ft. to 21.12 ft.
4 inch
Depth to Water Level: 8.35 ft. below measuring point.
Measuring Point is 1.52 ft above land surface.
GALLONS of water pumped/bailed before sampling:
or Groundwater Treatment
ystems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 2730 uMhos
Temp. 19.1 oC, Odor NONE Appearance: CLEAR
PERMIT #: W10700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
EXPIRATION DATE:
UIC X
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/23/01
Date sample analyzed:
Laboratory Name:
4/23/01 to 5/15/01
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1376
6.1
11.4
81.5
Arsenic NIA
N/A
N/A
751.4
N/A
N/A
N/A
pH (when analyzed)
TOC
Chloride
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
No and field acidified Yes n/a
N/A mg/I
N/A mg/I
/100m1 Phosphorus: Total as P
Orthophosphate
mgll Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
mgll Chromium: Total
mgll Cu - Copper
mg/I Fe - Iron
mgll Hg - Mercury
50.500 mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
N/A mgll Ammonia Nitrogen
N/A mg!I
N/A mgll
N/A mg/I
N/A mgll
N/A mg/I
N/A mgll
N/A mg/I
N/A mg/I
uMhos K- Potassium
mg/I Mg - Magnesium
mgll Mn - Manganese
N/A mg/I
N/A mg/I
N/A mgll
No
N/A ug/I
N/A ug/l
N/A ugll
c.-4, mg/1
Other (Specify Compounds and Concentration UnitsP) c
Fluoride 0.34 mgll
MIBK 230 N/A mg/I
Ag - Silver
Se- Selenium
Sodium
N r,A mgll
N3� mg/I
Nt` ug/l
Organics: (GC, GC/MS, HPLC) 3 ti
m
(Specify test method #. Attach lab report.) «�'
Report attached? Yes (1) Nor...) DP (2)
VOC method o
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true,
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory.
false information, including the possibility of fines and imprisionment for knowing violations.
accurate, and complete, and that the laboratory analytical data was produced
I am aware that there are significant penalties for submitting
NOTE:
GW-59 Rev 4/98
Terry L. Baker- Manager, Environmental Affairs
Name and Title - Please type or print
Signatptf dfi Permittee (or Authorized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-2
Well Depth: 23.00
Screened Interval: 18.80
Depth to Water Level: 7.16
Measuring Point is 3.42
ft. Well Diamter:
4 inch
ft. to 21.63 ft.
ft. below measuring point.
ft above land surface.
or Groundwater Treatment
ystems Check One:
Influent (98)
X Effluent (99',
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 2010 uMhos
Temp. 18.6 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
UIC X
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/23/01
Date sample analyzed:
Laboratory Name:
4/23/01 to 5/15/01
PCS PHOSPHATE
CZ)
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/l
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note: Use MPN method for highly turbid samples)
1476
6.4
11.3
62.1
Arsenic N/A
Grease and Oils N/A
N/A
508.3
N/A
N/A
N/A
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
Yes nla
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/1 Ca - Calcium
mg/I Cd- Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/1 Mg - Magnesium
mg/I Mn - Manganese
No and field acidified Yes nla
137.250 mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Ammonia Nitrogen
No
N/A
N/A
N/A
Other (Specify Compounds and Concentration Units) CD
Fluoride
MIBK
Ag - Silver
N/A mg/I Se- Selenium
N/A mg/I Sodium
N/A mg/I Organics: (GC, GC/MS.
N/A mg/I (Specify test method #.
N/A mg/I Report attached? Yes
N/A mg/I VOC
N/A mg/I
HPLC)
Attach lab repo);
(1) No ;(2)
: methodk...) E
method . o
ug/l
ug/I
ug/I
mg/I
90.2 mg/I
WAG-) _mg/I
NAL) rr g/I
c. N/A~= ping/I
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized A nt) Name and Title - Please type or print
Signetof Permittee (or Authorized Agent)
(D

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-3
Well Depth: 24.50
ft. Well Diamter: 4 inch
Screened Interval: 20.17 ft. to 23.00 ft.
Depth to Water Level: 7.36 ft. below measuring point.
Measuring Point is 3.17 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.3 , Specific Conductance
or Groundwater Treatment
ystems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
2106 uMhos
Temp. 21.6 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
UIC X
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
4/23/01
4/23/01 to 5/15/01
PCS PHOSPHATE
330
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/l Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
1572
6.0
10.6
41.9
N/A
N/A
N/A
625.1
N/A
N/A
N/A
/100m1 Phosphorus: Total as
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
mg/I Cd- Cadmium
mg/l Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/l Mn - Manganese
Yes nla No and field acidified Yes nla
N/A mg/I Ni - Nickel N/A ug/I
N/A mg/I Pb - Lead N/A ug/I
P 39.000 mg/l Zn - Zinc N/A,_J _ ug/I
N/A mg/I Ammonia Nitrogen O z mg/l
4
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/I Fluoride a�.0.11 ,ng/I
N/A mg/I MIBK —cN/F ,-,:ttig/1
N/A mg/I Ag - Silver CA)N/rang/I
N/A mg/I Se- Selenium N/ omg/l
3 N/ ''mug/l
N/A mg/I Organics: (GC, GC/MS, HPLC) cn:;r
N/A mg/I (Specify test method #. Attach lab rep .) cj ""
N/A mg/I Report attached? Yes
N/A mg/I Sodium
(1) No.
N/A mg/l VOC : method#
N/A mg/I
method#
method#
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Signatu
Terry L. Baker - Manager, Environmental Affairs
P-rmitte e(of Authorized ent))) ame and Title - Please type or print
(Dat )
Permittee (or Authorized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-4
Well Depth: 25.00 ft. Well Diamter:
Screened Interval: 20.50 ft. to 23.30 ft.
Depth to Water Level:
Measuring Point is
GALLONS
4 inch
7.72 ft. below measuring point.
3.42 ft above land surface.
or Groundwater Treatment
ystems Check One:
Influent (98)
X Effluent (99)
of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 5.7 , Specific Conductance 2195 uMhos
Temp. 32.7 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
4/23/01
4/23/01 to 5/15/01
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered Yes nla
COD
Coliform: MF Fecal
Coliform: MF Total
N/A mg/I Nitrite (NO2 as N)
N/A /100m1 Nitrate (NO3 as N)
N/A /100m1 Phosphorus: Total as P
(Note Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total
pH (when analyzed)
TOC
1504 mg/I Al - Aluminum
6.3 units Ba - Barium
9.1 mg/I Ca - Calcium
Chloride
34.5 mg/I Cd- Cadmium
Arsenic
Grease and Oils
Phenol
Sulfate
No and field acidified Yes nla No
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
82.000 mg/I Zn - Zinc
N/A
N/A
N/A
N/A mg/I Ammonia Nitrogen
N/A mg/I Other (Specify Compounds and Concentration Units
N/A mg/I Fluoride
N/A mg/I
N/A mg/I
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
688.6 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
ug/I
ug/I
ug/I
mg/1
' 0.(7 mg/I
A N mg/I
--4 N -77.: mg/1
N/A mg/I Se- Selenium t� NUR:,-,-- mg/I
N/A mg/I Sodium N-c ug/I
NIA mg/I Organics: (GC, GC/MS. HPLC) 171
N/A mg/I (Specify test method #. Attach lab repplt.) cn;.:
N/A mg/I Report attached? Yes (1) No (2)
N/A mg/I VOC method#— t,
N/A mg/I
MIBK
Ag - Silver
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information. including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized
ignatur
Name and Title - Please type or ()Olt
v
ermittee (or Authorized Agent) (D te)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. -Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 28.21
SWW-5
ft. Well Diamter: 4 inch
Screened Interval: 24.83 ft. to 27.21 ft.
Depth to Water Level: 7.11 ft. below measuring point.
Measuring Point is 2.96 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 5.8 , Specific Conductance
or Groundwater Treatment
ys ems Check One:
Influent (98)
X Effluent (99',
CONTINUOUS
2580 uMhos
Temp. 29.9 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH. NC 27699.1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/23/01
Date sample analyzed:
Laboratory Name:
4/23/01 to 5/15/01
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total 1684
pH (when analyzed)
TOC
Yes n/a
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
/100m1 Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
5.7 units Ba - Barium
13.7 mg/I Ca - Calcium
Chloride
Arsenic
53.4 mg/I Cd- Cadmium
Grease and Oils
Phenol
Sulfate
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I
67.500 mg/1
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
N/A mg/I
N/A mg/I
Yes n/a No
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
N/A ug/I
N/A ug/I
NIA ug/I
o mg/I
Other (Specify Compounds and Concentration Units
G7
Fluoride —.c 0..^ mg/I
MIBK NY mg/I
��
Ag - Silver
Se- Selenium
Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
760.8 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/l
N/A mg/l Mg - Magnesium
N/A mg/I Mn - Manganese
N/A mg/I
N/A mg/l
N/A mg/I
^' NA`,;! mg/I
^a N',- mg/I
> ug/I
(Specify test method #. Attach lab re}t.)
Report attached? Yes (1) No
VOC : method#
method#
method#
(2)
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per (of Authorized Agen) Name and Title - Please type or print
/ zt)ttee (or Authorized Agent) (Da )
Signatur Perm g )

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH,NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: 26.00
Screened Interval: 22.25 ft. to 24.62 ft.
Depth to Water Level:
Measuring Point is
SWW-6
ft. Well Diamter: 4 inch
7.12 ft. below measuring point.
2.58 ft above land surface.
or Groundwater Treatment
ystems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 5.9 , Specific Conductance 2226 uMhos
Temp. 30.1 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/30/01
Spray Field X Remediation
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/23/01
Date sample analyzed:
Laboratory Name:
4/23/01 to 5/15/01
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note.
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
Use MPN method for highly turbid samples)
1532
5.8
14.5
92.5
N/A
N/A
N/A
529.3
N/A
N/A
N/A
Orthophosphate
mg/l Al - Aluminum
units Ba - Barium
mgll Ca - Calcium
Yes n/a No and field acidified
Yes nla No
Nitrite (NO2 as N) N/A mg/I Ni - Nickel N/A ug/I
Nitrate (NO3 as N) N/A mg/I Pb - Lead N/A ug/I
Phosphorus: Total as P 43.000 mg/I Zn - Zinc Ni ug/I
N/A mg/I Ammonia Nitrogen p - mg/I
u
N/A mg/l Other (Specify Compounds and Concentration Units
N/A mg/1 Fluoride I,. O., mg/I
N/A mg/l MIBK -< N/ mg/I
mg/I Cd- Cadmium N/A mg/1 Ag - Silver Ca _ NW< mg/I
mg/I Chromium: Total Ntiic mg/I
mg/I Cu - Copper 3 NSA-- ug/I
N/A mg/I Organics: (GC, GC/MS. HPLC) r�rr-'
N/A mg/1 (Specify test method #. Attach lab red t.) m "`'
N/A mg/I Report attached? Yes (1) No .- E (2)
N/A mg/I VOC method# z
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
N/A mg/I
N/A mg/I
N/A mg/I
Se- Selenium
Sodium
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager. Environmental Affairs
PertPe(of Authorized nt ame and Title - Please type or print
ee (or Authorized A ent (Da )
Signatty PermittAgent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Weil Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-7
Well Depth: 29.50 ft. Well Diamter:
4 inch
Screened Interval: 25.17 ft. to 27.50 ft.
Depth to Water Level: 6.67 ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 5.6 , Specific Conductance
or Groundwater Treatment
ys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
997 uMhos
Temp. 25.9 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/23/01
Date sample analyzed: 4/23/01 to 5/15/01
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Yes n/a No and field acidified Yes n/a No
N/A mg/I Ni - Nickel N/A ug/I
N/A mg/I Pb - Lead N/A ug/l
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 736 mg/I Al - Aluminum
pH (when analyzed) 6.2 units Ba - Barium
TOC 10.9 mg/I Ca - Calcium
Chloride 59.5 mg/I Cd- Cadmium
Arsenic N/A mg/I Chromium: Total
Grease and Oils
Phenol
Sulfate
N/A mg/1 Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
184.4 mg/I Hg - Mercury
52.000 mg/l Zn - Zinc N/A ug/I
N/A mg/I Ammonia Nitrogen p mg/I
N/A mg/I Other (Specify Compounds and Concentration Units) 1::
N/A m /I Fluoride �' g 06-..� Mtg/I
N/A mg/I MIBK <N/Ac4{tg/I
N/A mg/I Ag - Silver wN/A:Tng/I
N/A mg/1 Se- Selenium N/rng/I
N/mug/I
Organics: (GC, GC/MS, HPLC) {''
N/A mg/I Sodium
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A mg/1
cn_
N/A mg/1 (Specify test method #. Attach lab re .)
N/A mg/I Report attached'? Yes (1) Nor (2)
N/A mg/I VOC : method# 2
N/A mg/l
method#
method#
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
p
GW-59 Rev 4/98
Terry L. Baker - Manager. Environmental Affairs
Permittee (of Authorized 9e ) Name and Title - Please type or pri t
Signatur
Permittee (or Authorized Agent) (Da

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
I,OM rem.,
Well Identification Number (from Permit): MWTF1-A
Well Depth: 6.40 ft. Well Diamter:
Screened Interval:
3.40 ft. to 5.40 ft.
2 inch
Depth to Water Level: 4.44 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
or Groundwater Treatment
ys ems Check One:
Influent (98)
Effluent (99)
MILILITERS of water pumped/bailed before sampling: 2100
Field Analysis: pH 7.2 , Specific Conductance 499 uMhos
Temp. 19.6 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/24/01
Date sample analyzed:
Laboratory Name:
4/24/01 to 5/15/01
PCS PHOSPHATE
Certification No(s) 330
r—,
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A mg/l Nitrite (NO2 as N)
Coliform MF Fecal N/A /100m1 Nitrate (NO3 as N)
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 336 mg/I Al - Aluminum
pH (when analyzed) 8.2 units Ba - Barium
TOC 5.1 mg/I Ca - Calcium
Chloride
8.1 mg/I Cd- Cadmium
Arsenic
Grease and Oils
Phenol
Sulfate
0.494 mg/I
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
N/A mg/I Fe - Iron
<10.0 mg/l Hg - Mercury
Specific Conductance N/A uMhos K- Potassium
Total Ammonia
TKN as N
Yes n/a No W
N/A /l
r\t,6
r.,
Zn - Zinc — NA
N/A mg/l Ammonia Nitrogen _ r�,�=
N/A mg/I Other (Specify Compounds and Concentration Units'f< c:•'
CJ �_
N/A mg/I
N/A mg/I
N/A mg/I
ug/l
ug/l
mg/I
mg/I
N14:::-.% mg/1
N!' c~ mg/l
N/A mg/I Se- Selenium NtAr<-* mg/I
t.� N,a.v ug/I
-
.- o
(Specify test method #. Attach lab report.) z
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC method#
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/l Mg - Magnesium
N/A mg/I Mn - Manganese
N/A mg/I
Fluoride
MIBK
Ag - Silver
Sodium
Organics: (GC, GC/MS, HPLC)
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized en fy Name and Title - Please type or print
Signatur9f Permittee (or Authorized Agent)
(Daft=)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth:
13.50 ft. Well Diamter:
MWTF1-B
2 inch
Screened Interval: 10.60 ft. to 12.60 ft.
Depth to Water Level: 5.08 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
or Groundwater Treatment
ys ems Check One:
Influent (98)
Effluent (99)
MILILITERS of water pumped/bailed before sampling: 2100
Field Analysis: pH 6.0 , Specific Conductance 368 uMhos
Temp. 20.7 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/24/01
Date sample analyzed:
Laboratory Name:
4/24/01 to 5/15/01
PCS PHOSPHATE
czy
cry
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 276 mg/I Al - Aluminum
pH (when analyzed) 6.4 units Ba - Barium
TOC 6.1 mg/I Ca - Calcium
Chloride
39.7 mg/I
Arsenic
Grease and Oils
Phenol
Sulfate
N/A mg/I
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I Fe - Iron
46.0 mg/I Hg - Mercury
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/1 Pb - Lead
5.600 mg/I Zn - Zinc
Yes n/a No
N/A mg/I Ammonia Nitrogen
N/A ug/I
N/A ug/I
NIA ug/I
O t; mg/I
N/A mg/I Other (Specify Compounds and Concentration Units)a 2 _
N/A mg/I Fluoride 3:' 0.3 •mg/l
N/A mg/I MIBK Ga N/Xr'mg/I
N/A mg/I Ag - Silver N/X'r: mg/I
N/A mg/I Se- Selenium -0 NA mg/I
N/A mg/I Sodium NA ;T: ug/I
Organics: (GC, GC/MS, HPLC) Cn_-
(Specify test method #. Attach lab repot.) n
N/A mg/1 Report attached? Yes (1) No • 1G (2)
z
N/A mg/I VOC method#
N/A mg/I
N/A mg/I
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A mg/I
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are sign cant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Signaturg'6PPermittee (or Authorized Agent)
Terry L. Baker - Manager, Environmental Affairs
Petra (of Authorized Agent) theme and Title - Please type or print
/zi
(Dat )

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH. NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth:
Screened Interval:
Depth to Water Level:
Measuring Point is
WLCT
NIA ft. Well Diamter: N/A
N/A ft. to N/A ft.
N/A ft. below measuring point.
N/A ft above land surface.
or Groundwater Treatment
ys erns Check One:
X Influent (98)
Effluent (99;
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 7.7 , Specific Conductance 646 uMhos
Temp. 21.8 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation :
UIC X
09/30/01
Remediation: Infiltration Gallery
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
4/24/01
4/24/01 to 5/15/01
PCS PHOSPHATE and ENVIRONMENT 1
330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
<1.0
(Note: Use MPN method for highly turbid samples)
X Yes
No and field acidified X Yes No
mg/I Nitrite (NO2 as N) N/A mg/I
/100m1 Nitrate (NO3 as N) N/A mg/1
/100m1 Phosphorus: Total as P 0.043 mg/1
Orthophosphate N/A mg/I
Dissolved Solids: Total 452 mg/I
pH (when analyzed) 7.8 units
TOC 7.0 mg/I Ca - Calcium __
Chloride
Arsenic
Grease and Oils
12.1 mg/I Cd- Cadmium
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
19.3 mgll Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
Ni - Nickel
Pb - Lead
Zn - Inc
Ammonia Nitrogen
NIA ug/I
N/9k1 ug/l
CD NA ug/I
mg/I
Al - Aluminum N/A mg/I Other (Specify Compounds and Concentration Unit c'-'--.
Ba - Barium N/A mg/I Fluoride 0.acr" mg/I
N/A mg/I MIBK — NIAi;i mg/I
<0.001 mg/I Ag - Silver D Nt mg/I
<0.005 mg/I Se- Selenium 3 N mg/1
N/A mg/1 Sodium t,N ug/I
N/A mg/1 Organics: (GC, GC/MS, HPLC) CA)
N/A mg/I (Specify test method #. Attach lab reFbrt.) z
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC : method#
<0.010 mg/I : method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Pe ittee (of Authorizedent)�Name and Title - Please type or pn t
SignatujF6i Permittee (or Authorized Agent)
(Da e)

' PCS Ph'o'sphate��C/o., Inc. - Y {k ' Farm Remediation System Qr erly Monitoring
7 Date: , �/--,3-0/
Time: /`Y4/
Tech:
System Gauge Pressures
sWW-1
z9- 6 A5r
SWW-7
0 `/off Q3r
cWW-1
D - 5 Par
CWW-7
0-.5- P-1
File: 15-03-003-02
pc: TLB
Level (msl)
Ditch Level
J0-35' 7
Barge Slip
/0•-56 r
Water Level
0 0/
Control Tank
C
%=MSL
/y 1// 1
Sand Layer Peizometers Level Indicators
Well ID
TOC
Elevation
MSL'
TOC
Ste Wtr
LL,ee/vel'
Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level
Relative To
MSL Ft.
Spz-1
10.47
7. 60
Jam. 87
Cpz-1
10.51
�7Level'
9 «8
/ OS
Spz-2
11.21
/ . e V
o?. 67
Cpz-2
10.25
/ 0. 76,
^ 0, /
Spz-3
11.87
6. 6 8
.J . / !
Cpz-3
11.12
/0 , a 6,
0 8/O
Spz-4
11.45
6 .623
1/. 77
• CPW
9.65
9.99
-. a9
Spz-5
11.45
/
9. t 8
/, 77
MWTF-1A'
14.35
1/, 4/9
9- 9/
Spz-6
11.23 •
/O. 04
/. / /
MWTF-1B'
14.36
.J. 06
/,8
r7fq•4,
Spz-7
11.59
/0. t50
/•a!pp
MWTF-1C'
14.44
/a•00
Spz-8
11.57
'/, es
1//“R 9
MWTF-2A
14.05
6,5V
/�j
Spz-9
11.01
7r/7-
. 60
o7•��
MWTF-28
14.02
//.,/.f®
fit 4 J
of•74
-.0.5/
Spz-10
12.16
6 0 /p
6 . /0
MWTF-2C
14.08
SPW
9.95
.
,9 .0A
/. 93
MWTF-3A
12.21
y. o &
P. /J
MW TF-38
12.18
/ 0 . 1/8
/, 7/
MWTF-3C
12.19
/a, aS
-0.69
Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Sto
Wtr
Ft.
Max Level
Relative To
MSL Ft.
Control
Point
MSL'
Is Well
Pumping
(Y)es/(N)o
Comments
SWW-1
10.70
Level
1.3S
Q. 3r
+1 ' to+2'
X"
CWW-1
10.60
7.05
- /•95"
-2'to-1'
r/ff
SWW-2
9.99
7/6
/./4,
+1'to+2'
Ve5
CWW-2
10.23
a93
-X 0 7
-2'to-1'
yei •
SWW-3
9.97
7 a&
/ 64
+1, to+2'
ri
CWW-3
9.95
774)
-7a6
-2 ' to-1'
ye.6
SWWsi
10.73
7 902
/ 7.�
+1'to+2'
GYPS
CWW-4
10.73
_5e9/
-S. /,3
-2' to-1'
L/t3
SWW-5
10.80
7,//
///
+1'to+2'
y!i
CW
10.74
W
-e:)•.5(p
-2'to-1'
7083
a.W-5
SWW-6
10.66
7,/o
/.J0.t
+1 'to+2'
j cj
CW-6
W
9.92
4.a O
-cQ.7o
-2' to-1'
Ye.'
SWW-7
10.70
b. op
.0.67
. +1'to+2'
ye5
CWW-7
9.95
(p,//
'-o% Ur9
-2'to-1'
1.1ej
Revised 8/12/97
* Riser length added to TOC elevation 1/24/97
PCS095.XLS

PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
February 2001— April 2001
The Tank Farm Remediation System consists of a series of seven (7) injection water wells located on the
south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north
side of the Tank Farm Area:
Injection Water Well System
The injection water well system operated with the DPW Water - Anthracite Sand Filter / Ultraviolet Light
(ASF/UV) disinfection system throughout the period.
Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs
Department. The influent DPW totalizer was repaired during February. This required the DPW usage for
February to be derived from operating log sheets. On February 23, 2001 the Injection Well System was
down for 3 hours and 30 minutes to change the head tank control valve. The total monthly and quarterly
volumes of water injected as well as the month end water level in the Water Level Control Tank are:
REY-
DPW WATER
GALLONS
CONDENSATE
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
February
241,995
0
241,995
6.0
13.8
March
293,850
0
293,850
6.6
11.7
April
259,630
0
259,630
6.0
12.1
TOTALS
795,475
0
795,475
3

Withdrawal Well System
The system was down on 2-12-01 for 4 hours for preventive maintenance on the air compressor. The
system was down on 3-1-01 for 30 minutes for compressor maintenance. The withdrawal water well
pumps are monitored daily by the area Maintenance Department and preventative maintenance work is
performed as needed. The total monthly and quarterly withdrawal water volumes for the period are:
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
February
346,162
112,696
458,858
11.4
March
297,922
151,999
449,921
10.1
April
363,710
180,695
544,405
12.6
TOTALS
1,007,794
445,390
1,453,184
Some additional short periods of planned downtime for preventative maintenance, pipe header cleaning,
and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these
—activities-are.'
Confined Sand Formation Withdrawal Well (SWW) Pumps
SWW-1: On 2/5 cleaned the discharge line.
SWW-2: On 3/26 repaired the airline.
SWW-3: On 4/3 replaced the counter.
SWW-4: On 3/2 replaced the counter. On 3/8 replaced the pump. On 3/22 cleaned the pump. On 4/25
cleaned the discharge line.
SWW-5: On 2/14 replaced the totalizer. On 3/13 acid washed the well and replaced the pump.
SWW-6:
SWW-7: On 3/7 acid washed the pump. On 3/21 repaired the totalizer.
4

Croatan Formation Withdrawal Well (CWW) Pumps
CWW-1: On 2/19 replaced pump. On 3/1 repaired air line.
CWW-2: On 2/7 replaced airline to regulator. On 2/23 cleaned counter. On 4/10 replaced counter.
CWW-3: On 3/20 replaced inlet air supply.
CWW-4:
CWW-5: On 4/3 cleaned well. On 4/4 acid washed pump, well and replaced airline.
CWW-6:
CWW-7:
5

i
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
\low'
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit): CIW-7
Well Depth:
Screened Interval:
Depth to Water Level:
Measuring Point is
GALLONS
48.00 ft. Well Diamter:
31.00
N/A
N/A
4 inch
ft. to 45.25 ft.
ft. below measuring point.
ft above land surface.
or Groundwater Treatment
ys ems Check One:
X Influent (98',
Effluent (99)
of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 7.5 , Specific Conductance 596 uMhos
Temp. 18.7 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
UIC X
Lagoon
Spray Field x Remediation :
Rotary Distributor
Other
Remediation: Infiltration Gallery
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/24/01
Date sample analyzed: 4/24/01 to 5/16/01
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
(7)
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total <1.0
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
452
7.8
6.8
12.2
N/A
N/A
N/A
19.3
N/A
N/A
N/A
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
/100m1
mg/1
units
mg/I Ca - Calcium
mg/I
m g/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
No and field acidified X Yes
N/A mg/l Ni - Nickel
N/A mg/I Pb - Lead
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
0.029 mg/I Zn - Zinc
N/A mg/1 Ammonia Nitrogen
N/A mg/1
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
No
N/k ug/I
O N/ ug/I
- N/A;..ug/I
a�mg/I
Other (Specify Compounds and Concentration Unitsta 7 rr•
N/A mg/l Fluoride
N/A mg/I MIBK
<0.001 mg/1 Ag - Silver
<0.005 mg/I Se- Selenium
— O. mg/I
NP4 mg/I
NtA mg/I
mg/l
NYA
N/A mg/I Sodium c N/A ug/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
N/A mg/l Report attached? Yes (1) No X (2)
N/A mg/l VOC method#
method#
method#
N/A mg/I
N/A mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
<0.010 mg/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Pelee (of Authorized ygen
Signatur
Name and Title - Please type or print
7zSi
ermittee (or Authorized Agent)
(Data:)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
IFom pe
Well Identification Number (from Permit): MWTF1-CR
Well Depth: 42.00 ft. Well Diamter:
Screened Interval: 38.70 ft. to 40.70 ft.
Depth to Water Level:
Measuring Point is
2 inch
12.00 ft. below measuring point.
3.95 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH 7.5 , Specific Conductance
Temp. 21.8 oC, Odor NONE
or Groundwater Treatment
ystems Check One:
Influent (98)
Effluent (99)
2100
594 uMhos
Appearance: CLEAR
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
EXPIRATION DATE:
UIC
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
4/24/01
4/24/01 to 5/15/01
PCS PHOSPHATE and ENVIRONMENT 1
330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD
N/A mg/l
Coliform: MF Fecal
Coliform: MF Total
N/A /100m1
X Yes
Nitrite (NO2 as N)
Nitrate (NO3 as N)
No and field acidified X
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
<1.0 /100m1 Phosphorus: Total as P
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Orthophosphate
418 mg/l Al - Aluminum
7.6 units Ba - Barium
5.9 mg/I Ca - Calcium
Chloride
Arsenic
9.6 mg/I Cd- Cadmium
Grease and Oils
Phenol
Sulfate
<0.001 mg/I
N/A mg/I Chromium: Total
N/A mg/1 Cu - Copper
N/A mg/I Fe - Iron
45.0 mg/I Hg - Mercury
Specific Conductance
Total Ammonia
TKN as N
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
<0.005 mg/I
0.288 mg/I Zn - Zinc
Yes No
N/A mg/I Ammonia Nitrogen
N/A mg/l
N/A mg/I
Other (Specify Compounds and Concentration Units}
Fluoride W
N/A ug/I
N/tor, ug/I
Nt ug/I
= c,73 mg/1
0.1D mg/I
N/A mg/l MIBK — N =; mg/I
Ag - Silver --.a Nils' mg/1
Se- Selenium = l mgll
N/A mg/1 Sodium __ F P ug/I
N/A mg/1 Organics: (GC, GC/MS, HPLC) w
N/A mg/I (Specify test method #. Attach lab re rt.) E5
N/A mg/1 Report attached? Yes (1) No 3C (2)
N/A mg/1 VOC method#
0.056 mg/l
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Peuittee (of Authorized en Name and Title - Please type or print
Signat1 Permittee (or Authorized Agent) S D
u o

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. -Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): CWW-1
Well Depth:
55.00 ft. Well Diamter:
Screened Interval: 33.27 ft. to 52.68 ft.
4 inch
Depth to Water Level: 7.05 ft. below measuring point.
Measuring Point is 2.25 ft above land surface.
GALLONS of water pumped/bailed before sampling:
or Groundwater Treatment
ystems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 2171 uMhos
Temp. 20 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
09/30/01
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/23/01
Date sample analyzed: 4/23/01 to 5115/01
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
Cfl
PARAMETERS: (Samples for metals were collected unfiltered Yes nla No and field acidified Yes n/a No
COD N/A mg/I Nitrite (NO2 as N) N/A mg/I Ni - Nickel C, NI. ug/I
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A mg/I Pb - Lead -� N ug/l
Coliform: MF Total N/A /100m1 Phosphorus: Total as P 2.450 mg/I Zn - Zinc < N/A' ; , ug/I
(Note: Use MPN method for highly turbid samples) Orthophosphate N/A mg/I Ammonia Nitrogen r1 -==r'lmg/l
Dissolved Solids: Total 1972 mg/I Al - Aluminum N/A mg/I Other (Specify Compounds and Concentration Units? -
pH (when analyzed) 6.7 units Ba - Barium N/A mg/I Fluoride -R 0.2 ' mg/I
TOC 11.4 mg/I Ca - Calcium KEY N/A mg/I MIBK = Nli,n mg/I
Chloride 73.9 mg/I Cd- Cadmium N/A mg/I Ag - Silver Niki5 mg/I
Arsenic N/A mg/I Chromium: Total N/A mg/l Se- Selenium c..0 NE3 mg/1
N/A mg/l Cu - Copper N/A mg/I Sodium C..) NT, ug/I
N/A mg/I Fe Iron N/A mg/l Organics: (GC, GC/MS, HPLC)
694.6 mg/I Hg - Mercury KEY
N/A mg/l (Specify test method #. Attach lab report.)
N/A uMhos K- Potassium N/A mg/l Report attached? Yes (1) No X (2)
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/1 Mg - Magnesium N/A mg/I
N/A mg/I Mn - Manganese N/A mg/I
VOC method#
method#
method#
Le 1
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the Laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information. including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
P�tulittee (of Authorized gent Name and Title - Please type or pri t
Signatujiif Permittee (or Authorized Agent) (Dat

•
w
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
No. of Wells to be Sampled 113
Well Locations/Site Name: Tank Farm
Well Identification Number (from Permit): CWW-2
Well Depth: 52.15
ft. Well Diamter: 4 inch
Screened Interval: 30.57 ft. to 49.82 ft.
Depth to Water Level: 6.93 ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
or Groundwater Treatmeit
ys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 2189 uMhos
Temp. 20.2 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
EXPIRATION DATE:
UIC X
09/30/01
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/23/01
Date sample analyzed:
Laboratory Name:
4/23/01 to 5/15/01
PCS PHOSPHATE
C)
{
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
1972
6.6
11.8
93.6
N/A
N/A
N/A
678.7
N/A
N/A
N/A
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
No and field acidified
N/A mg/I Ni - Nickel
N/A mg/1 Pb - Lead
/100m1 Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
mg/1
units
mg/1
mg/I
mg/I
mg/I
mg/l
mg/I
uMhos
mg/I
mg/1
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
36.500 mg/l Zn - Zinc
Yes n/a No
N/A mg/I Ammonia Nitrogen
N/A mg/1
N/A mg/l
N/A mg/I
ug/l
p N11 ug/I
N
3 -
x. ,.:.�•:, mg/I
Other (Specify Compounds and Concentration Units
Fluoride
MIBK
N/A mg/I Ag - Silver
N/A mg/I
N/A mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
Se- Selenium
Sodium
ug/I
0.p< mg/I
mg/I
N mg/I
mg/I
_, ug/I
N/A mg/I Organics: (GC, GC/MS, HPLC) C..) (-;
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X
N/A mg/1 VOC method#
N/A mg/I
method#
method#
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
(of Authorized Agent) ame and Title - Please type or pri t
PI e;e/U�v�ys/e7 %
(Da ))
Signatof Permittee (or Authorized Agent)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): CWW-3
Well Depth: 53.00
Screened Interval: 36.42 ft. to 50.67 ft.
Depth to Water Level:
Measuring Point is
ft. Well Diamter: 4 inch
7.74 ft. below measuring point.
3.08 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.0 , Specific Conductance
Temp. 25.6 oC, Odor NONE
or Groundwater Treatment
ys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
2585 uMhos
Appearance: CLEAR
DIVISION OF WATER QUALITY
Mail Original GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
to: 1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT*: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/23/01
Date sample analyzed:
Laboratory Name:
4/23/01 to 5/15/01
PCS PHOSPHATE
Certification No(s) 330
f�
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
mg/I
/100m1
/100m1
Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
1932 mg/I Al - Aluminum
6.6 units Ba - Barium
10.9 mg/I Ca - Calcium
198.5 mg/I Cd- Cadmium
Arsenic
Grease and Oils
Phenol
Sulfate
No and field acidified Yes n/a No
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
3.900 mg/I Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A mg/I
N/A mg/I
N/A mg/I
N/A mgll
N/A mg/I Chromium: Total
N/A mgll Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
433.9 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A
N/A
C) NIA
c
Other (Specify Compounds and Concentrat
Fluoride
MIBK
Ag - Silver
N/A mg/I Se- Selenium
N/A mgll Mg - Magnesium
N/A mgll Mn - Manganese
N/A mg/1 Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab r
N/A mg/I Report attached? Yes
N/A mg/I VOC
N/A mg/I
f7
(1) No (2)
method#
ug/I
ug/I
ug/I
mg/I
mg/I
mg/I
mg/I
mg/I
ug/I
method#
method#
certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina OWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized A ent Name and Title - Please type or f nt
0
Go
ttee or Authorized Agent) ( te)
gnatur�;6fPermi ( g )

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
(from 7
Well Identification Number (from Permit): CWW-4
Well Depth:
Screened Interval:
Depth to Water Level:
Measuring Point is
53.00
41.67
5.87
2.75
ft. Well Diamter:
4 inch
ft. to 50.92 ft.
ft. below measuring point.
ft above land surface.
or Groundwater Treatment
ys ems Check One:
Influent (98)
X Effluent (99;
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 2450 uMhos
Temp. 28.1 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
UIC X
09/30/01
Spray Field X Remediation
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/23/01
Date sample analyzed:
Laboratory Name:
4/23/01 to 5/15/01
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
1816
6.8
9.3
124.0
N/A
N/A
N/A
501.9
N/A
N/A
N/A
mg/I Nitrite (NO2 as N)
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
No and field acidified Yes n/a No
N/A mg/I
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I
4.050 mg/I
N/A mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
N/A ug/I
N/11' ug/I
NIA: ug/I
mg/I
N/A mg/I Other (Specify Compounds and Concentration Unit r-
N/A mg/I Fluoride c 0.nE mg/I
N/A mg/I MIBK NEA mg/I
N/A mg/I Ag - Silver -0 Nik mg/I
N/A mg/I Se- Selenium "Z N(a; mg/I
N/A mg/I Sodium - 149tt ug/I
N/A mg/I Organics: (GC, GC/MS, HPLC) w 9
N/A mg/I (Specify test method #. Attach lab ret.) a
N/A mg/I Report attached? Yes (1) No X (2)
method#
N/A mg/I
N/A mg/I
VOC
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
r(of Authorize en Name and Title - Please type or print
ermittee (or Authorized Agent) (D e)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
ilparn
Well Identification Number (from Permit): CWW-5
Well Depth: 53.17
Screened Interval: 41.75 ft. to 51.08 ft.
Depth to Water Level:
Measuring Point is
ft. Well Diamter: 4 inch
8.44 ft. below measuring point.
2.58 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.0 , Specific Conductance
Temp. 29.9 oC, Odor NONE
or Groundwater Treatment
ystems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
1914 uMhos
Appearance:
CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
UIC X
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/23/01
Date sample analyzed:
Laboratory Name:
4/23/01 to 5/15/01
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
(Note:
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
Use MPN method for highly turbid samples)
1328
6.7
9.0
72.6
N/A
N/A
N/A
388.9
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/1
mg/I
mg/l
mg/I
mg/I
mg/I
uMhos
mg/I
mg/l
Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
No and field acidified
N/A mg/I
N/A mg/I
4.450 mg/I
N/A mg/l
N/A mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
N/A mg/l
N/A mg/I
N/A mg/I Ag - Silver
N/A mg/I Se- Selenium
N/A mg/I Sodium
N/A mg/I
N/A mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/l
N/A mg/1
N/A mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes n/a
No
CD
Ammonia Nitrogen c
Other (Specify Compounds and Concentration Unitsj7 .= T
Fluoride 0. '-= mg/I
MIBK Net-J mg/I
N47= mg/I
mg/I
t.) ug/l
Organics: (GC, GC/MS, HPLC) 41 o
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC : method#
N/4
NFA
method#
method#
ug/I
ug/I
ug/I
mg/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWO (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized A ent Name and Title - Please type or print
c
atur P
ign
ermittee (or Authorized Agent) (Dat
,.772:67(07

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: 53.00 ft. Well Diamter:
CWW-6
4 inch
Screened Interval: 36.62 ft. to 50.88 ft.
Depth to Water Level: 6.28 ft. below measuring point.
Measuring Point is 2.92 ft above land surface.
GALLONS of water pumped/bailed before sampling:
or Groundwater Treatment
ys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 1927 uMhos
Temp. 30.8 oC, Odor NONE
Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
09/03/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
1111
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/23/01
Date sample analyzed: 4/23/01 to 5/15/01
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
mg/1
/100m1
/100m1
1320 mg/I
5.9 units
11.1 mg/I
84.1 mg/I
Grease and Oils
Phenol
Sulfate
N/A mg/I
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
410.9 mg/I
N/A uMhos
N/A mg/I
N/A mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Yes n/a No and field acidified Yes n/a No
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
5.900 mg/I Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/l
N/PV ug/I
o Niio ug/I
:-f
Other (Specify Compounds and Concentration Units
Fluoride
MIBK
Ag - Silver
NO5 _., ug/I
cr; ,,,c mg/I
0.*z` mg/I
-oil N:-: mg/I
Z NtA4 , mg/I
Se- Selenium NW ~y mg/1
N/A mg/I Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #.
N/A mg/I Report attached? Yes
N/A mg/I VOC
N/A mg/I
GJ N ug/l
Attach lab report.)
(1) No X (2)
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Agent) Nfime and Title - Please type or print
ignature
ermittee (or Authorized Agent)
(Da )

•
w
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: 53.00 ft. Well Diamter:
CWW-7
Screened Interval: 36.58 ft. to 50.83 ft.
Depth to Water Level:
Measuring Point is
4 inch
6.11 ft. below measuring point.
1.25 ft above land surface.
or Groundwater Treatment
ystems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 1216 uMhos
Temp. 24.7 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/03/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 4/23/01
Date sample analyzed:
Laboratory Name:
4/23/01 to 5/15/01
PCS PHOSPHATE
Certification No(s) 330
CD
PARAMETERS: (Samples for metals were collected unfiltered
Yes n/a No and field acidified
COD N/A mg/1 Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
720
6.8
7.7 mg/1 Ca - Calcium
72.0
N/A
NIA
N/A
193.1
N/A
N/A
N/A
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Cd- Cadmium
mg/1 Chromium: Total
mg/1 Cu - Copper
mg/I Fe - Iron
mg/l Hg - Mercury
uMhos K- Potassium
mg/1 Mg - Magnesium
mg/1 Mn - Manganese
N/A
N/A
1.300
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
mg/I
mg/I
mg/l
mg/l
mg/1
mg/1
mg/I
mg/I
mg/I
mg/I
mg/I
mg/1
mg/1
mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes n/a No
N/A
N.
O
Ammonia Nitrogen
Other (Specify Compounds and Concentration Unit
Fluoride c..1
MIBK —
ug/I
ug/I
ug/I
c> mg/I
rJ,c�
c-`
mg/1
N`,;` mg/I
Ag - Silver
Se- Selenium
Sodium
mg/I
— t ug/I
Organics: (GC, GC/MS, HPLC) r—
(Specify test method #. Attach lab rep ?t.) o
Report attached? Yes (1) No
VOC : method#
method#
method#
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Age t) Ne and Title - Please type ri t
ignature
FTermittee (or Authorized Agent)
(Date)

PCS
Phosphate AURORA
PCS PHOSPHATE COMPANY, INC.
P.O. BOX 48, AURORA, NC U.S.A. 27806
February 23, 2001
MARK MILLIGAN
GROUND WATER
DENR
1636 MAIL SERVICE CENTER
RALEIGH, NC 27626-1636
Subject: Underground Injection Control Program
Fourth Quarter Groundwater Monitoring Report
November 2000 — January 2001
Injection Well Permit #WI0700012
Tank Farm Remedial Action System
Beaufort Co.
Dear Mark:
Please find the subject groundwater monitoring report attached. This includes the sampling and reporting
requirements of the above referenced permit, Part V, Section B 1 as well as the reporting requirements of
the overall Tank Farm Remedial Action Plan. Enclosed are: a) Form GW-59 for injection well CIW7 and
monitor well MWTF1CR, b) Form GW-59 for each of the fourteen withdrawal wells, c) Form GW-59 for
monitor wells MWTF1A and MWTF1B, d) Form GW-59 for the WLCT, e) piezometer level monitoring
field sheet, and f) the summary operational and maintenance report.
Please do not hesitate to contact me at [phone] if you have any questions regarding this
information.
Sincerely,
41„c,
D. Daniel Winstead HI
Environmental Engineer
PCS Phosphate
Attachments
pc: Willie Hardison — DWQ- GWS, WaRO (w/attch)
4

bpc: S. A. Beckel / K. C. West (w/attch)
T. L. Baker / 12-01-008-03-002 (w/ attch)
J. A. Hardy / RBL/T WD/SLD/JHT (w/ attch)
R. A. Allen / T. Lewis (w/attch)
D. D. Winstead / 00-24-000 (w/o attch)
W. A. Schinuning (w/o attch)
2

PCS PHOSPHATE - TANK FARM REMEDIAL ACTION PLAN
QUARTERLY OPERATIONAL AND MAINTENANCE REPORT FOR
THE INJECTION AND WITHDRAWAL WATER WELLS
November 2000 — January 2001
The Tank Farm Remediation System consists of a series of seven (7) injection water wells located on the
south side of the Tank Farm Area and a series of fourteen (14) withdrawal water wells located on the north
side of the Tank Farm Area.
Injection Water Well System
The injection water well system operated with the DPW Water - Anthracite Sand Filter / Ultraviolet Light
(ASF/UV) disinfection system throughout the period.
Daily operational data are collected by the Shipping Department and reported to the Environmental Affairs
Department. During the period the influent DPW totalizer failed. The DPW usage for January was derived
from operating log sheets. The total monthly and quarterly volumes of water injected as well as the month
end water level in the Water Level Control Tank are:
2000
DPW WATER
GALLONS
CONDENSATE
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
TANK
LEVEL
FEET, MSL
November
283,880
0
283,880
6.4
13.5
December
256,296
0
256,296
5.7
13.8
Jan-2001
292,224
0
292,224
6.5
13.8
TOTALS
832,400
0
832,400
3

Withdrawal Well System
The system was down on 11-16-00 to repair the air compressor. The withdrawal water well pumps are
monitored daily by the area Maintenance Department and preventative maintenance work is performed as
needed. The total monthly and quarterly withdrawal water volumes for the period are:
2000
SAND
FORMATION
GALLONS
CROATAN
FORMATION
GALLONS
TOTAL
GALLONS
AVERAGE
GPM
November
369,047
177,596
546,643
12.6
December
404,150
99,427
503,577
11.3
Jan - 2001
434,819
170,857
605,676
13.6
TOTALS
1,208,017
447,880
1,655,897
Some additional short periods of planned downtime for preventative maintenance, pipe header cleaning,
and troubleshooting on individual pumps in the fourteen well system were experienced. Details of these
activities are:
Confined -Sand -Formation -Withdrawal Well (SWW) Pumps
SWW-1: On 11/29 & 12/13 the pump was shaken to start. On 12/14 the pump was replaced.
SWW-2: Pump operated without incident.
SWW-3: On 11/8 the pump was shaken to start.
SWW-4: Pump operated without incident.
SWW-5: On 11/16 the counter was replaced. On 12/14, 12/27 & 12/28 the pump was shaken to start. On
1/9 the pump was replaced.
SWW-6: On 12/14 the flow meter and the counter were replaced.
SWW-7: Pump operated without incident.
4

Croatan Formation Withdrawal Well (CWW) Pumps
CWW-1: Pump operated without incident.
CWW-2: On 11/29, 12/26 & 1/4 the pump was shaken to start. On 12/4-5 the well was acid washed. On
12/5 the flow meter was changed.
CWW-3: On 11/21 the pump was shaken to start.
CWW-4: Pump operated without incident.
CWW-5: Pump operated without incident.
CWW-6: On 12/19 & 12/22 the pump was shaken to start. On 12/20 & 12/26 the pump was replaced.
CWW-7: On 12/27, 1/2 & 1/8 the pump was shaken to start. On 12/8, 1/9 & 1/16 the pump was changed.
5

PCS Phosphate Co., Inc.
Date: /-/O-O/
Time: Air/
Tech:
sank Farm Remediation System )arterly Monitoring
System Gauge Pressures
SW W-1
0-/.-p51
O:o?Sfar;
SWW-7
cww-1
D 6 Ai
CWW-7
O-// t2.5
File:1503-003-02
pc TLB
Level (msl
Ditch Level
-J. o(B
Barge Slip%
%Z
Water Leval
/eye%
Control Tank
e
%=MSL
/J /37
Sand Layer Pelzometers Level Indicators
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Well ID
TOC
Elevation
MSL'
TOC
Stc Wtr
Level'
Level
Relative To
MSL Ft.
Spz-1 '
10.47
icge
m tr
Cpz-1
10.51
/0./y
g.. 7
Spz-2
11.21
41$?70
.t S/
Cpz-2
10.25
/O• 449
- 0.23
/,Q,2
Spz-3
11.87
6,aF
5:6-9
Cpz-3
11.12
/0-/o
Spz-4
11.45
/- OB
97
CPW
9.65
/9.00
D- 36-
Spz-5
11.45
9 79
/ 7/
MWTF-1A•
14.35
1.. 59
/O.o/
Spz$
11.23
/4M9
/O.S
MWTF1B•
14.36
.S/a
9. 240
Spz-7
11.59
/0./O
/,'99
MWTF-1C•
14.44
Any
/, 6/
Spz-8
11.57
709
I SO
MWTF-2A
14.05
A 79
71/
Spz-9
11.01
S./p5
pl3e
MWTF-2B
14.02
//eg
a?.?5/
Spz-10
12.16
6./0
e . 06
MWTF-2C
14.08
/7 Z '
O. 70
SPW
9.95
Rao.
/. t9
MWTF-3A
12.21
/4sfj
z IS
MWTF-3B
12.18
/D.�ra
/44
MWTF-3C
12.19
/3 y0
--/.2/
Sand Layer And Croatan Formation Withdrawal Wells
Well ID
TOC
Elevation
MSL'
Max Ste
Wtr
Level Ft.
Max Level
Relative To
MSL Ft.
Control
Point
MSL'
Is Well
Pumping
(Y)es/(N)o
Comments
SWW-1
10.70
712
/ le.2
+1 'to+2'
ye'
cww-1
10.60
109
%. 43
2'to•1'
'~
ii Iiid/,It cy047e on o4
SWW-2
9.99
709
/D9
+1'to+r
fees
CWW-2
10.23
d. 96
p?.04/
-2'to -1'
yes
yei
A`[dG//47P ,e/i. ed
SW W-3
9.97
'7 O2
/ 02
+1. to +Y
CWW-3
9.95
77416
-/,,$-4/
-2'to -1'
ye4
SWW4
10.73
77/t%
/.17
+1'to +'
p.0
CWW-4
10.73
"0?. a
-2 ' to -1'
7li
/Q. .52
SWW-5
10.80
7 /5
/.a
+1'to+2'
ifei
t/G06/ /'ne /en.t/i,
CWW-5
10.74
7; if
- / • 62
-2'to-1'
/9
SW W-6
10.66
7 /3
/. / 9
+1 'to +2'
yes
)'l_
CWW-6
9.92
..94
- 29
-2'to-1'
�l
/to ///.1/Le e fa/a/pee/
.-
SWW-7
10.70
zee,
/. 06
+1 'to+2'
CWW-7
9.95
_ h. y/
o.19
-2' to -1'
/' qq
ree f/teeel Are4s. aaaoi 0/1
may,
tot/ e, seie Aim
Revised 8/12/97 '
' _' Rleer I `added to TOC elevation 124/97
PCSo95.XLS -t

-GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 48.00 ft. Well Diamter:
CIW-7
4 inch
Screened Interval: 31.00 ft. to 45.25 ft.
Depth to Water Level: N/A ft. below measuring point.
Measuring Point is N/A ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
X Influent (98)
Effluent (99)
CONTINUOUS
Field Analysis: pH 7.5 , Specific Conductance 522 uMhos
Temp. 12.6 oC, Odor NONE Appearance:
CLEAR
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
X Other
Note: Values should reflect dissolved and
colloidal concentrations
1/12/01 cr-�
1/12/01 to 1/24/01
PCS PHOSPHATE and EN1f/9IRONMENT 1
330 10
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
<1.0
(Note. Use MPN method for highly turbid samples)
mg/I
/100m1
/100m1
Dissolved Solids: Total 466 mg/I
pH (when analyzed) 7.8 units
TOC 6.4 mg/I
Chloride
11.1 mg/I
Arsenic
Grease and Oils
Phenol
Sulfate
N/A mg/I
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
28.4 mg/I
N/A uMhos
N/A mg/I
N/A mg/I
Yes n/a
No and field acidified
Nitrite (NO2 as N) N/A mg/I
Nitrate (NO3 as N) N/A mg/1
Phosphorus: Total as P 0.152 mg/I
Orthophosphate N/A mg/I
Al - Aluminum _ N/A mg/I
Ba - Barium N/A mg/I
Ca - Calcium N/A mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
<0.001 mg/I
<0.005 mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
0.043 mg/I
Yes n/a No 4-0
Ni - Nickel - N/A, .. sig/I
Cii Pb - Lead .' NIA i ug/I
Zn - Zinc NI ' ug/I
Ammonia Nitrogen Cnmg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC method#
method#
: method#
C=t
0.54 ; .mg/I
N/A .fng/l
N/A vg/I
N/A n99/I
N/A : ug/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
P rmittee (of Authod Pgent) Name and Title - Please type or print
L/i1/L
Signatyf€�of Permittee (or Authorized Agent)
�y-z-/>j
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): MWTF1-CR
Well Depth: 42.00 ft. Well Diamter:
Screened Interval: 38.70 ft. to 40.70 ft.
Depth to Water Level: 12.83 ft. below measuring point.
Measuring Point is 3.95 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH 7.3 , Specific Conductance 536
Temp. 18.1 oC, Odor NONE
2 inch
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
2100
uMhos
Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
UIC X
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/12/01
Date sample analyzed: 1/12/01 to 1/24/01 '
Laboratory Name: PCS PHOSPHATE and EpIVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected unfiltered X Yes
COD
Coliform:
Coliform:
(Note
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
N/A
MF Fecal N/A
MF Total <1.0
Use MPN method for highly turbid samples)
388
7.7
5.3
9.7
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
40.0
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
No
N/A mg/I
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
<0.001 mg/I
<0.005 mg/l
N/A mg/I
0.230 mg/I
N/A mg/I
N/A mg/I
N/A mg/I
and field acidified X Yes
Ni - Nickel
Pb - Lead
Zn - Zinc
No
'.o
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
N/A mg/I MIBK
Ag - Silver
Se- Selenium
N/A mg/I Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC : method#
IUD ug/I
NtPr' ug/l
(WAR ug/I
mg/1
0.5-i mg/I
N/A - mg/I
N/A Dmg/I
N/A mg/I
N/A ug/I
0.040 mg/I
method#
method#
I certify that. to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Pe ittee (of Authorized Age ) Name and Title - Please type or print
Signat / of Permittee (or Authorized Agent) (Date)

i
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): CWW-1
Well Depth: 55.00 ft. Well Diamter:
4 inch
Screened Interval: 33.27 ft. to 52.68 ft.
Depth to Water Level: 7.07 ft. below measuring point.
Measuring Point is 2.25 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6,0 , Specific Conductance 2201 uMhos
Temp. 18.8 oC, Odor NONE Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH. NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
UIC X
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/10/01
Date sample analyzed: 1/10/01 to 1/25/01
Laboratory Name:
PCS PHOSPHATE a7
Certification No(s) 330
_11
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note' Use MPN method for highly turbid samples)
Dissolved Solids: Total 1924
pH (when analyzed) 6.5
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
13.0
75.2
N/A
N/A
N/A
695.2
N/A
N/A
N/A
mg/I
units
mg/1 Ca - Calcium
mg/1
mg/I
mg/1
mg/I Fe - Iron
mg/I Hg - Mercury
uMhos
mg/I
mg/1
Al - Aluminum
Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total
Orthophosphateiti
No and field acidified Yes n/a No
N/A mg/I Ni - Nickel
2.920 mg/I
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A mg/I
Ba - Barium
Cd- Cadmium
Chromium: Total
Cu - Copper
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I
NIA ug/I
1.0
NA_ ug/I
Ul N c, ug/I
` 1-- mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
0.23- mg/I
N/A1g/I
N/A _ing/I
N/A wog/I
N/A ug/I
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/1 (Specify test method #. Attach lab report.)
N/A mg/1 Report attached? Yes (1) No X (2)
N/A mg/l VOC : method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager. Environmental Affairs
Permittee (of Authorized Agent) ame and Title - Please type�or print
�
Signat of Permittee (or Authorized Agent)
(Date)

'GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
Well Locations/Site Name: Tank Farm
[phone]
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 52.15 ft. Well Diamter:
CWW-2
4 inch
Screened Interval: 30.57 ft. to 49.82 ft.
Depth to Water Level: 6,96 ft. below measuring point.
Measuring Point is 3.00 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 2272 uMhos
Temp. 19.3 oC, Odor NONE Appearance:
CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/10/01
Date sample analyzed:
Laboratory Name:
Certification No(s) 330
CD
1/10/01 to 1/25/01 T
PCS PHOSPHATE
r..a
PARAMETERS: (Samples for metals were collected unfiltered Yes
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1956
pH (when analyzed) 6.6
TOC 12.5
Chloride 99.9
Arsenic N/A
Grease and Oils N/A
Phenol N/A
Sulfate 695.9
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
n/a No and field acidified Yes n/a No =
mg/I Ni - Nickel --. N/A- -ug/I
mg/I Pb - Lead Nl ug/I
8.900 mg/I Zn - Zinc 0}' N ug/l
N/A mg/I Ammonia Nitrogen { mg/I
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/I Fluoride 0.1P- mg/I
N/A mg/1 MIBK N/A - mg/I
N/A mg/I Ag - Silver N/A.1 mg/I
N/A mg/1 Se- Selenium N/A mg/I
N/A mg/I Sodium N/A - ug/I
N/A mg/I Organics: (GC, GC/MS, HPLC) —"
N/A mg/I (Specify test method #. Attach lab report.) I` )
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC : method#
N/A mg/I
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A
N/A
method#
method#
J
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Pe ittee (of Authorized Agen Name and Title - Please type or print
� I
Signatyf of Permittee (or Authorized Agent)
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: 53.00 ft. Well Diamter:
CWW-3
4 inch
Screened Interval: 36.42 ft. to 50.67 ft.
Depth to Water Level: 7.46 ft. below measuring point.
Measuring Point is 3.08 ft above land surface.
GALLONS of water pumped/bailed before sampling CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 2567 uMhos
Temp. 24.3 oC, Odor NONE Appearance: CLEAR
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
1110101
1/10/01 to 1/25/01
PCS PHOSPHATE
330
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1898
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
6.4
10.7
185.7
N/A
N/A
N/A
522.3
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Yes n/a
No and field acidified
N/A mg/I Ni - Nickel
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
N/A mg/I Pb - Lead
5.300 mg/I Zn - Zinc
Yes n/a No
N/A mg/I Ammonia Nitrogen
N/A mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
N/A mg/I
N/A mg/I
I N/A ug/I
NIA ug/I
N/A - ug/I
t� c; -mg/I
Other (Specify Compounds and Concentration Units ' 2_
Fluoride 0.4 mg/I
n (A, mg/I
N/A mg/I N/A c-mg/I
Se- Selenium N/A yng/I
Sodium N/A�g/I
N/A mg/I Organics: (GC, GC/MS, HPLC) r .)
N/A mg/I
N/A mg/I
K- Potassium
Mg - Magnesium
Mn - Manganese
MIBK
Ag - Silver
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached'? Yes (1) No X (2)
N/A mg/I VOC
N/A mg/I
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information. including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Agent) lame and Title - Please type or print
fX
Signature ejPermittee (or Authorized Agent)
(Date)

i
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1536 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: 53.00 ft. Well Diamter:
CWW-4
Screened Interval: 41.67 ft. to 50.92 ft.
Depth to Water Level:
Measuring Point is
4 inch
6.52 ft. below measuring point.
2.75 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 2463
uMhos
Temp. 27.1 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s) 330
1/10/01
1 /10/01 to 1 /25/0f"" :
PCS PHOSPHATE
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
mg/I
/100m1
/100m1
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total 1768 mg/1
pH (when analyzed) 6.6 units
TOC 11.8 mg/I
Chloride 131.5 mg/I
Arsenic N/A mg/1
Grease and Oils
Phenol
Sulfate 565.4 mg/I
N/A mg/I
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
N/A uMhos
N/A mg/1
N/A mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
No and field acidified Yes n/a
N/A mg/I Ni - Nickel
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
21.050 mg/I
N/A mg/I Pb - Lead
Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
N/A mg/I
N/A mg/I
C11
ILIA
NA-
RIAD
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A mg/I Ag - Silver
N/A mg/I Se- Selenium
N/A mg/I Sodium
K- Potassium
Mg - Magnesium
Mn - Manganese
CD
ug/I
ug/I
ug/I
mg/I
0.124- mg/I
N/A��mg/I
N/A .jng/I
N/A .-mg/1
N/A ug/I
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC : method#
: method#
method#
N/A mg/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete. and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Agent) ame and Title - Please type or print
Signat
Permittee (or Authorized Agent)
Date)

1
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mad Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled 18
Well Identification Number (from Permit): CWW-5
Well Depth: 53.17 ft. Well Diamter:
Screened Interval: 41.75 ft. to 51.08 ft.
Depth to Water Level:
Measuring Point is
4 inch
7.38 ft. below measuring point.
2.58 ft above land surface.
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 1956 uMhos
Temp. 28.7 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/10/01
Date sample analyzed:
Laboratory Name:
1/10/01 to 1/25/01
PCS PHOSPHATE
r-,
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note Use MPN method for highly turbid samples)
Dissolved Solids: Total
pH (when analyzed)
TOC
1284
6.7
8.8 mg/I Ca - Calcium
mg/I
/100m1
/100m1
Yes n/a
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
73.1
N/A
N/A
N/A
Specific Conductance
Total Ammonia
TKN as N
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Cd-• Cadmium
mg/I Chromium: Total
mg/I Cu - Copper
mg/I Fe - Iron
415.0 mg/I Hg - Mercury
N/A
N/A
N/A
uMhos K- Potassium
mg/I Mg - Magnesium
mg/I Mn - Manganese
No and field acidified Yes n/a No
N/A
N/A
6.600
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
_ram
l/A ug/I
/A u9/I
j7N/A �tlg/I
mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
0.11 omg/I
N/A o ' mg/I
Ag - Silver
Se- Selenium
Sodium
N/A r'mg/I
N/A ..3rtg/I
N/A Zig/I
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC : method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is trueaccurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information. including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized A nt) ame and Title - Please type or print j
Signaturegi Permittee (or Authorized Agent) (Date)

i
i
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
CWW-6
Well Depth: 53.00 ft. Well Diamter: 4 inch
Screened Interval: 36.62 ft. to 50.88 ft.
Depth to Water Level: 6.96 ft. below measuring point.
Measuring Point is 2.92 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 1880
uMhos
Temp. 31 oC, Odor NONE Appearance:
CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/03/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
1/10/01
1/10/01 to 1/25/01
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS:
COD
Coliform: MF Fecal
Coliform: MF Total
(Ncte
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
(Samples for metals were collected unfiltered
N/A
N/A
N/A
Use MPN method for highly turbid samples)
1252
6.8
10.0
89.4
N/A
N/A
N/A
347.5
N/A
N/A
N/A
mg/l
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
uMhos
mg/1
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes n/a
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
No and field acidified
N/A
N/A
6.750
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
mg/I
mg/1
mg/I
mg/I
mg/l
mg/I
mg/1
mg/I
mg/I
mg/I
mg/l
mg/I
mg/I
mg/I
mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Yes n/a
Ammonia Nitrogen
No
Other (Specify Compounds and Concentration Un
Fluoride
MIBK
Ag - Silver
Se- Selenium
Sodium
Organics: (GC, GC/MS. HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
• NIA rR-tIg71
`. 1/A
4'J/A ?t7g/I
VOC
_ mg/1
ts)
0.15®mg/I
N/A t7'mg/I
N/A mg/I
method#
method#
method#
N/A rhg/I
N/A ug/I
I certify that, to the best of my knowledge and belief. the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per ttee (of Authorized A nt) ame and Title - Piease type or print
c—.0
Signaturg if Permittee (or Authorized Agent)
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mal Service Center
RALEIGH. NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit):
Well Depth: 53.00 ft. Well Diamter:
Screened Interval: 36.58 ft. to 50.83 ft.
Depth to Water Level:
Measuring Point is
GALLONS
CWW-7
4 inch
6.41 ft. below measuring point.
1.25 ft above land surface.
of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.1 , Specific Conductance 1875 uMhos
Temp. 23.4 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
09/03/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations O
Date sample collected:
Date sample analyzed:
Laboratory Name:
Certification No(s)
1/10/01
1/10/01 to 1/25/01
PCS PHOSPHATE
n
C rrr
330 cn
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as
Yes n/a No and field acidified
N/A mg/I Ni - Nickel
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1212 mg/1
pH (when analyzed) 6.4 units
TOC 8.8 mg/I
Chloride 279.7 mg/I
Arsenic N/A mg/I
Grease and Oils N/A mg/I
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
194.7 mg/I
N/A uMhos
N/A mg/I
N/A mg/I
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
N/A mg/1
P 4.600 mg/1
N/A mg/l
N/A mg/1
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
N/A mg/I
N/A mg/1
N/A mg/1
Yes n/a No
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
0 N/(A ug/I
N/A... ug/I
Cn Nt}• ug/I
mg/I
2.29 j mg/1
N/A, __ mg/I
Ag - Silver N/A amg/I
N/A mg/1 Se- Selenium
N/A mg/I Sodium
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I
N/A ug/I
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC : method#
N/A mg/I
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true. accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Signa
of Permittee (or Aut
t) Name and Title - Please type or print
/zL
horized Agent) (I.te)

1
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-1
Well Depth: 22.50 ft. Well Diamter:
4 inch
Screened Interval: 18.30 ft. to 21.12 ft.
Depth to Water Level: 7.82 ft. below measuring point.
Measuring Point is 1.52 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.4 , Specific Conductance 2866 uMhos
Temp. 19.4 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
UIC X
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: infiltration Gallery
Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/10/01
Date sample analyzed:
Laboratory Name:
1/10/01 to 1/25/01
PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD mg/I
Coliform: /100m1
Coliform: /100m1
N/A
MF Fecal N/A
MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1692
pH (when analyzed) 6.6
TOC 12.1
Chloride 84.1
Arsenic N/A
Grease and Oils N/A
Phenol N/A
Sulfate 867.0
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
mg/1
units
mg/I
mg/I
mg/1
mg/1
mg/1
mg/I
uMhos
mg/I
mg/I
Yes
n/a
No and field acidified Yes n/a No
Nitrite (NO2 as N) N/A mg/I
Nitrate (NO3 as N) N/A mg/I
Phosphorus: Total as P 80.500 mg/I
Orthophosphate N/A mg/I
Al - Aluminum N/A mg/1
Ba - Barium N/A mg/1
Ca - Calcium N/A mg/I
Cd- Cadmium N/A mg/I
Chromium: Total N/A mg/1
Cu - Copper N/A mg/1
Fe - Iron N/A mg/1
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I
N/A mg/I
N/A mg/I
N/A mgll
Ni - Nickel
Pb - Lead
Zn - Zinc
La N/A
N/A
N/A
Ammonia Nitrogen kJ)
Other (Specify Compounds and Concentration Units
Fluoride 0A6
MIBK N/A
Ag - Silver
ug/I
ug/I
ug/I
mg/1
mg/I
mg/I
N/A mg/1
Se- Selenium NIA ) mg/I
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC
method#
method#
method#
N/A- ug/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Perittee (of Authorized Agent) ame and Title - Please type or print
�/z Z/4-,
Signatur
ermittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm
No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 23.00 ft. Well Diamter:
SWW-2
Screened Interval: 18.80 ft. to 21.63 ft.
Depth to Water Level:
Measuring Point is
4 inch
7.09 ft. below measuring point.
3.42 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 2288
Temp. 20.2 oC, Odor
uMhos
NONE Appearance:
CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected:
Date sample analyzed:
Laboratory Name:
1/10/01
1/10/01 to 1/25/01 Z
PCS PHOSPHATE =�
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A
Coliform: MF Fecal N/A
Coliform: MF Total N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1512
pH (when analyzed) 6.4
TOC 11.6
Chloride
Arsenic
64.4
Grease and Oils
Phenol
Sulfate
N/A
N/A
N/A
483.0
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
mg/I
/100m1
/100m1
mg/I
units
mg/I
mg/I
mg/I
mg/l
mg/I
mg/l
uMhos
mg/I
mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
No and field acidified
N/A mg/I
106.000 mg/I
Ni - Nickel
N/A mg/I Pb - Lead
Zn - Zinc
Yes n/a No
N/A mg/I Ammonia Nitrogen
N/A mg/1
N/A mg/I
N/A mg/I
N/A ug/I
t' A ug/I
N/A ug/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
N/A mg/I Ag - Silver
N/A mg/I
N/A mg/I
Se- Selenium
Sodium
mg/I
0.2tS , mg/I
N/A, _ mg/I
N/A -,mgll
N/A mg/1
N/A ug/I
N/A mg/1 Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #.
N/A mg/1 Report attached? Yes
N/A mg/I VOC
N/A mg/I
Attach lab report.)
(1) No X (2)
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete. and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per ee (of Authorized A ent)) Fame
and Title - Please type or print
Signatur,
Permittee (or Authorized Agent)
_y/Z y' /
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-3
Well Depth: 24.50 ft. Well Diamter: 4 inch
Screened Interval: 20.17 ft. to 23.00 ft.
Depth to Water Level: 7.02 ft. below measuring point.
Measuring Point is 3.17 ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 6.2 , Specific Conductance 1890
Temp. 22.8 oC, Odor NONE Appearance:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
uMhos
CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
UIC X
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/10/01 CD
Date sample analyzed: 1/10/01 to 1/25/01
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
PARAMETERS: (Samples for metals were collected
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total N/A /100m1
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total 1260
pH (when analyzed) 6.6
TOC 9.5
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
30.9
N/A
N/A
N/A
438.2
N/A
N/A
N/A
mg/I
units
mg/I
mg/l
mg/I
mg/I
mg/I
mg/I
uMhos
mg/I
mg/I
unfiltered
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd- Cadmium
Yes n/a
No and field
N/A mg/I
N/A mg/I
46.000 mg/1
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
N/A mg/I
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
acidified
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen
Yes n/a No
N/ it ug/I
t n NIA! ug/I
/4- ug/I
ILDr mg/I
Other (Specify Compounds and Concentration Units)
0.13 mg/I
N/A• mg/I
N/AP mg/I
N/A-° mg/I
N/A( Dug/I
•J
Fluoride
MIBK
Ag - Silver
N/A mg/I Se- Selenium
N/A mg/l Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.) CD
N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I VOC : method#
N/A mg/I
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager. Environmental Affairs
Perm ee (of Authorize Ager Na e and Title - Please type or print
1/1 tsi v✓� Z 7. e f
ignature o ermittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH. NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No, of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-4
Well Depth: 25.00 ft. Well Diamter:
4 inch
Screened Interval: 20.50 ft. to 23.30 ft.
Depth to Water Level: 7.17 ft. below measuring point.
Measuring Point is 3.42 ft above land surface.
GALLONSof water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 5.9 , Specific Conductance 2469 uMhos
Temp. 33.2 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and O
colloidal concentrations = C)
Date sample collected: 1/10/01 3::,'c4i'n
20 r-C'?
Date sample analyzed: 1/10/01 to 1/25/01 1 rry
Laboratory Name: PCS PHOSPHATE `'
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered Yes nla No and field acidified Yes n/a No t.,0 cr
r,
COD N/A mg/I Nitrite (NO2 as N) N/A mg/l Ni - Nickel cn N,fA ug/I
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N) N/A mg/l Pb - Lead =1 N/A ug/I
Coliform: MF Total N/A /100m1 Phosphorus: Total as P 96.000 mg/I Zn - Zinc N./A ug/I
(Note: Use MPN method for highly turbid samples) Orthophosphate N/A mg/I Ammonia Nitrogen mg/I
Dissolved Solids: Total 1420 mg/I Al - Aluminum N/A mg/l Other (Specify Compounds and Concentration Units) 0
pH (when analyzed) 6.3 units Ba - Barium N/A mg/l Fluoride 0.10'mg/I
TOC 9.3 mg/I Ca - Calcium N/A mg/I MIBK N/A mg/1
Chloride 43.8 mg/I Cd-- Cadmium N/A mg/I Ag - Silver N/A ''-•-?ng/I
Arsenic N/A mg/l Chromium: Total N/A mg/I Se- Selenium N/A 1i41g/1
Grease and Oils N/A mg/I Cu - Copper N/A mg/I Sodium N/A g/I
Phenol N/A mg/l Fe - Iron N/A mg/I Organics: (GC, GC/MS, HPLC)
Sulfate 592.7 mg/I Hg - Mercury N/A mg/I (Specify test method #. Attach lab report.)
N/A uMhos K- Potassium N/A mg/I Report attached? Yes (1) No X (2)
N/A mg/I Mg - Magnesium N/A mg/I VOC : method#
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Mn - Manganese N/A mg/I method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Peree (of Authorized t) t'me and Title - Please type or print
Signatuof Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-5
Well Depth: 28.21 ft. Well Diamter:
Screened Interval: 24.83 ft. to 27.21 ft.
4 inch
Depth to Water Level: 7.13 ft. below measuring point.
Measuring Point is 2.96 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatmen
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.0 , Specific Conductance 2618 uMhos
Temp. 30.4 oC, Odor NONE Appearance:
CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH. NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
U I C X
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/10/01
Date sample analyzed:
Laboratory Name:
1/10/01 to 1/25/01
PCS PHOSPHATE Cr1
G
Certification No(s) 330
ta.
PARAMETERS: (Samples for metals were collected unfiltered
COD N/A
Coliform: MF Fecal N/A
mg/I Nitrite (NO2 as N)
/100m1 Nitrate (NO3 as N)
Yes
n/a
No and field acidified Yes n/a No
N/A
N/A
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Ncte Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 1740 mg/l Al - Aluminum
pH (when analyzed)
TOC
Chloride
44.500
N/A
N/A
6.5 units Ba - Barium N/A
13.4 mg/I Ca - Calcium N/A
59.0 mg/I Cd- Cadmium N/A
Arsenic N/A mg/I Chromium: Total
Grease and Oils N/A mg/I Cu - Copper
Phenol N/A mg/I Fe - Iron
Sulfate 789.3 mg/I Hg - Mercury
Specific Conductance
Total Ammonia
TKN as N
N/A
N/A
N/A
N/A
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A
N/A
N/A
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/1
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
cal N/A ug/I
NJ ug/I
NMA ug/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
0.413 mg/I
N/Af' mg/I
Ag - Silver
Se- Selenium
Sodium
N/A mg/I
N/A .Drng/I
N/A t
Organics: (GC, GC/MS, HPLC) N
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC : method#
method#
method#
I certify that, to the best of my knowledge and beliefthe information submitted in this report is true, accurate, and complete. and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Pee (of Authorized Agent) me and Title - Please type or print
Signatur�j�t' Permittee or Authorized Agent)
ate)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): SWW-6
Well Depth: 26.00 ft. Well Diamter:
Screened Interval: 22.25 ft. to 24.62 ft.
Depth to Water Level:
Measuring Point is
4 inch
7.13 ft. below measuring point.
2.58 ft above land surface.
GALLONS of water pumped/bailed before sampling:
For Groundwater Treatment
Sys ems Check One:
Influent (98)
X Effluent (99)
CONTINUOUS
Field Analysis: pH 6.2 , Specific Conductance 2264 uMhos
Temp. 31.1 oC, Odor NONE
Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: z�.
Date sample analyzed: 1/10/01 to 1/25/011'3
Laboratory Name: PCS PHOSPHATE
L7
Certification No(s) 330
c-7
1/10/01
PARAMETERS: (Samples for metals were collected unfiltered Yes
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 1468
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
6.5
16.1
106.2
N/A
N/A
N/A
486.9
N/A
N/A
N/A
mg/1
/100m1
/100m1
mg/I
units
mg/1
mg/I
mg/l
mg/1
mg/1
mg/1
uMhos
mg/1
mg/1
n/a
No and field acidified Yes n/a No
Nitrite (NO2 as N) N/A
Nitrate (NO3 as N) N/A
Phosphorus: Total as P 73.000
Orthophosphate N/A
Al - Aluminum N/A
Ba - Barium N/A
Ca - Calcium N/A
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
N/A
N/A
N/A
N/A
N/A
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A
N/A
N/A
mg/1
mg/I
mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
mg/I Ammonia Nitrogen
mg/l
mg/I
mg/1
mg/I
mg/1
mg/I
mg/1
mg/I
mg/I
mg/1
mg/1
U1
N/A ug/I
N/A ug/l
&)A ug/l
mg/l
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
0.0b' mg/1
N/A ;r" mg/1
N/A mg/1
Se- Selenium N/A `44ng/I
Sodium N/A -.44g/1
Organics: (GC, GC/MS. HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X (2)
VOC : method#
method#
• method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true; accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per ttee (of Authorized Agent) N me and Title - Please type or print
ignature ermittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH, NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit): SWW-7
Well Depth: 29.50 ft. Well Diamter: 4 inch
Screened Interval: 25.17 ft. to 27.50 ft.
Depth to Water Level:
Measuring Point is
7.06 ft. below measuring point.
3.00 ft above land surface.
For Groundwater Treatme nt
Sys ems Check One:
Influent (98)
X Effluent (99)
GALLONS of water pumped/bailed before sampling: CONTINUOUS
Field Analysis: pH 5.7 , Specific Conductance 1040 uMhos
Temp. 25 oC, Odor NONE Appearance: CLEAR
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
09/30/01
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/10/01
Date sample analyzed: 1/10/01 to 1/25/0t
Laboratory Name: PCS PHOSPHATE
Certification No(s) 330
n
c—r
trf
PARAMETERS: (Samples for metals were collected unfiltered Yes n/a
COD N/A mg/I Nitrite (NO2 as N)
Coliform: MF Fecal N/A /100m1 Nitrate (NO3 as N)
Coliform: MF Total N/A /100m1 Phosphorus: Total as P
(Note. Use MPN method for highly turbid samples) Orthophosphate
Dissolved Solids: Total 744 mg/I Al - Aluminum
pH (when analyzed)
TOC
Chloride
6.1 units Ba - Barium
9.5 mg/I Ca - Calcium
64.3 mg/I Cd- Cadmium
Arsenic
Grease and Oils
Phenol
Sulfate
No and field acidified Yes n/a No PI
N/A mg/l Ni - Nickel IA.: ug/l
N/A mg/1 Pb - Lead c-n N{A ug/l
CI
53.000 mg/1 Zn - Zinc d17.A ug/I
N/A mg/l Ammonia Nitrogen O mg/I
N/A mg/1 Other (Specify Compounds and Concentration Units)
N/A mg/I Fluoride 0.10F:" mg/1
N/A mg/I MIBK N/A -'mg/I
N/A mg/I Ag - Silver N/A ~ mg/I
N/A mg/I Chromium: Total N/A mg/I Se- Selenium N/A ` ngll
N/A mg/I Cu - Copper
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I Fe - Iron
197.0 mg/l Hg - Mercury
N/A uMhos K- Potassium
N/A mg/1 Mg - Magnesium
N/A mg/I Mn - Manganese
N/A mg/I Sodium
N/A mg/l Organics: (GC, GC/MS, HPLC)
N/A mg/l (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
N/A ' Y.io/I
N/A mg/l VOC
N/A mg/I
method#
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized Agent Name and Title - Please type or print
ignat , ` of Permittee (or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH. NC 27699-1636 Phone [phone]
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
18
Well Identification Number (from Permit):
Well Depth: 6.40 ft. Well Diamter:
MWTF1-A
2 inch
Screened Interval: 3.40 ft. to 5.40 ft.
Depth to Water Level: 4.34 ft. below measuring point.
Measuring Point is 3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH 7.0 , Specific Conductance
Temp. 16.3 oC, Odor NONE
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
2100
411 uMhos
Appearance: CLEAR
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
mg/I
/100m1
/100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 276 mg/I
pH (when analyzed) 7.3 units
TOC 4.9 mg/I
Chloride 5.6 mg/I
Arsenic N/A mg/I
Grease and Oils N/A mg/I
Phenol N/A mg/I
Sulfate 11.0 mg/I
Specific Conductance
Total Ammonia
TKN as N
N/A uMhos
N/A mg/I
N/A mg/I
Nitrite (NO2 as N)
Nitrate (NO3 as N)
Yes
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
n/a
PERMIT #: WI0700012 EXPIRATION DATE:
UIC X
Non -Discharge
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
09/30/01
Lagoon
Spray Field
Rotary Distributor
Other
Remediation: Infiltration Gallery
X Remediation :
Land Application of Sludge
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/11/01
Date sample analyzed: 1/11/01 to 1/25/0'f:3
Laboratory Name: PCS PHOSPHATE c i
Certification No(s) 330
No and field acidified Yes n/a No
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
0.430 mg/l Zn - Zinc
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I Ammonia Nitrogen
t-O
NIA
}`/A
NIA
N/A mg/I Other (Specify Compounds and Concentration Units)
N/A mg/I Fluoride
N/A mg/I MIBK
N/A mg/I Ag - Silver
N/A mg/I Se- Selenium
N/A mg/I Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
ug/I
ug/I
ug/I
mg/I
N/A mg/I VOC : method#
method#
method#
N/A mg/I
2.28., mg/I
N/A — mg/I
N/A mg/l
N/A i-„irfg/1
N/A jqg/I
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurateand complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Per iittee (of Autho i ed AA nnt) Njme and Title - Please type or print
Signatu'oi Permittee (or Authorized Agent) ( ate)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone:
[phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH. NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012
EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon
Spray Field X Remediation
Remediation: Infiltration Gallery
18 Rotary Distributor Land Application of Sludge
Well Identification Number (from Permit):
Well Depth: 13.50 ft. Well Diamter:
Screened Interval:
Depth to Water Level:
Measuring Point is
MWTF1-B
2 inch
10.60 ft. to 12.60 ft.
5.16 ft. below measuring point.
3.86 ft above land surface.
MILILITERS of water pumped/bailed before sampling:
Field Analysis: pH 6.0 , Specific Conductance
Temp. 19.8 oC, Odor NONE
For Groundwater Treatment
Systems Check One:
Influent (98) 1 Note: Values should reflect dissolved and
X Other
Effluent (99) 1 colloidal concentrations
Date sample collected: 1/11/01
Q
2100 Date sample analyzed: 1/11/01 to 1/25/01 r
389 uMhos
Appearance: CLEAR
Laboratory Name: PCS PHOSPHATE ut
Certification No(s) 330
PARAMETERS: (Samples for metals were collected unfiltered
COD
Coliform: MF Fecal
Coliform: MF Total
N/A
N/A
N/A
(Note. Use MPN method for highly turbid samples)
Dissolved Solids: Total 280
pH (when analyzed) 6.4
TOC 5.1
Chloride
Arsenic
Grease and Oils
mg/I Nitrite (NO2 as N)
/100m1
/100m1
Yes nla No and field acidified
Nitrate (NO3 as N)
Phosphorus: Total as P
Orthophosphate
mg/I Al - Aluminum
units Ba - Barium
mg/I Ca - Calcium
29.0 mg/I Cd- Cadmium
N/A mg/I Chromium: Total
N/A mg/I Cu - Copper
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
Yes nla No
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
5.000 mg/1 Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A mg/I
N/A mg/1
N/A mg/I
N/A mg/1
NtA ug/I
NSA ug/I
N/A ug/I
mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
N/A mg/I Se- Selenium
N/A mg/I
N/A mg/1 Fe - Iron
49.8 mg/I Hg - Mercury
N/A uMhos K- Potassium
N/A mg/I Mg - Magnesium
N/A mg/I Mn - Manganese
N/A mg/I
N/A mg/1
N/A mg/1
N/A mg/I
N/A mg/I
Sodium
Organics: (GC, GC/MS, HPLC)
(Specify test method #. Attach lab report.)
Report attached? Yes (1) No X
0.54CNmg/I
N/A .'mg/1
N/A
N/A tlg/I
N/A — /1
VOC : method#
method#
method#
(2)
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false informationincluding the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
Permittee (of Authorized A.en Name and Title - Please type or print
Signatur /of Permittee (or Authorized Agent)
Zw Z Zi
(Date)

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORTING FORM
FACILITY INFORMATION
Facilty Name: PCS PHOSPHATE CO., INC. - Aurora Division
Permit Name (if different):
Facility Addresss: P.O. Box 48
Aurora, NC 27806 County: Beaufort
Contact Person: Jimmy Hardy Telephone: [phone]
Well Locations/Site Name: Tank Farm No. of Wells to be Sampled 18
Well Identification Number (from Permit): WLCT
Well Depth:
Screened Interval:
Depth to Water Level:
Measuring Point is
N/A ft. Well Diamter: N/A
N/A ft. to N/A ft.
N/A ft. below measuring point.
N/A ft above land surface.
GALLONS of water pumped/bailed before sampling:
Field Analysis: pH 7.5 , Specific Conductance
Temp. 11.1 oC, Odor NONE
For Groundwater Treatment
Sys ems Check One:
Influent (98)
Effluent (99)
X
CONTINUOUS
496 uMhos
Appearance: CLEAR
Mail Original
to:
DIVISION OF WATER QUALITY
GROUNDWATER SECTION -PERMITS AND COMPLIANCE UNIT
1636 Mail Service Center
RALEIGH. NC 27699-1636 Phone: [phone]
PERMIT #: WI0700012 EXPIRATION DATE: 09/30/01
Non -Discharge UIC X
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field X Remediation :
Rotary Distributor Land Application of Sludge
Other
Note: Values should reflect dissolved and
colloidal concentrations
Date sample collected: 1/12/01
Date sample analyzed: 1/12/01 to 1/24/01
Laboratory Name: PCS PHOSPHATE and ENVIRONMENT 1
Certification No(s) 330 10
PARAMETERS: (Samples for metals were collected
COD N/A mg/I
Coliform: MF Fecal N/A /100m1
Coliform: MF Total <1.0 /100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 460 mg/I
pH (when analyzed) 7.6 units
TOC 7.3 mg/I
Chloride 10.9 mg/I
Arsenic N/A mg/I
Grease and Oils N/A mg/I
Phenol
Sulfate
Specific Conductance
Total Ammonia
TKN as N
N/A mg/I
15.7 mg/I
N/A uMhos
N/A mg/I
N/A mg/I
unfiltered X Yes
Nitrite (NO2 as N)
Nitrate (NO3 as N)
No and field acidified X Yes No
N/A mg/I Ni - Nickel
N/A mg/I Pb - Lead
Phosphorus: Total as P
Orthophosphate
Al - Aluminum
Ba - Barium
Ca - Calcium
0.029 mg/I Zn - Zinc
N/A mg/I Ammonia Nitrogen
N/A mg/I
Cd- Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K- Potassium
Mg - Magnesium
Mn - Manganese
N/A mg/I
N/A mg/I
<0.001 mg/I
<0.005 mg/I
Lio
•N/ . ug/I
O N/ ug/I
mg/I
Other (Specify Compounds and Concentration Units)
Fluoride
MIBK
Ag - Silver
Se- Selenium
N/A mg/I Sodium
N/A mg/I Organics: (GC, GC/MS, HPLC)
N/A mg/I (Specify test method #. Attach lab report.)
N/A mg/I Report attached? Yes (1) No X (2)
method#
0.55�mg/I
N/A jng/I
N/A r�-tg/I
N/A mg/I
N/A ug/I
N/A mg/I VOC
<0.010 mg/I
method#
method#
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurateand complete, and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisionment for knowing violations.
NOTE:
GW-59 Rev 4/98
Terry L. Baker - Manager, Environmental Affairs
/Pe t� (of Aut`zed nt) ame and Title - Please type or print
� r�'� —4-/z 4/
SignatuPermittee (or Authorized Agent) (Date)