WI0500499_Other Correspondence_20140417

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LABORATORY 1572 Alcv Lane • Prates», MO (,S '33
Date of certificate: April 17, 2014
Client: ARCADIS-US
Project: Mallinckrodt ERD
Shipping address: 801 Corporate Center Drive, Suite 300
Raleigh, NC 27607
Project number: NC 107014.0008.00200
Contact people: [e-mail]
[e-mail]
117) 785-4289 • fax (t 17) 785-4290 • contact voAul,underl;rountll:tlr.cotn
Certificate of Analysis
Samples collected by:
Date samples shipped: April 3, 2014
Date samples rec'd at OUL: April 4, 2014
Date analyzed by OUL: April 14, 2014
Included with certificate of analysis: Table of
results, copy of sample collection data sheets
and discrepancy sheet
Results for water samples analyzed for the presence of fluorescein, eosine and rhodamine WT (RWT) dyes.
Peak wavelengths are reported in nanometers (nm); dye concentrations are reported in parts per billion (ppb).
OUL
Number
Sample Identification
Date/Time
Collected
Fluorescein
Eosine
RWT
Peak (nm)
Conc. (ppb)
Peak (nm)
Conc. (ppb)
Peak (nm)
Conc. (ppb)
X5350
DRW-1S
3/24/14 1540
ND
519.3 **
8.41
573.8
117
X5351
DRW-1D
3/24/14 1635
ND
520.1 **
1,190
ND
X5352
DRW-2S
3/26/141335
ND
515.0 **
45.8
574.0
76.2
X5353
DRW-2D
3/26/14 1430
ND
519.8 **
9.30
ND
X5354
TMW-1S
3/24/14 1330
ND
525.5 **
9.05
573.9
75.7
X5355
TMW-2D
3/27/14 1100
ND
517.5 **
105
ND
X5356
TMW-1BR
3/24/14 1430
ND
517.5 **
222
ND
X5357
TMW-2S
3/27/141005
508.1
101
ND
574.1
51.6
X5358
TMW-1D
3/24/14 1230
ND
516.1 **
286
ND
X5359
TMW-2BR
3/27/14 0855
ND
517.4 **
198
ND
X5360
Laboratory control water blank
X5361
B3a
3/26/14 1225
ND
523.9 **
8.02
574.1
32.6
X5362
Bla
3/28/141055
ND
ND
ND
X5363
IW-1S
3/26/141120
ND
ND
574.7
1,720
X5364
IW-1D
3/26/14 1030
ND
522.4 **
58.9
ND
X5365
IW-2S
3/24/141735
ND
ND
574.7
585
X5366
IW-2D
3/26/14 0850
ND
531.2 **
702
ND
X5367
IW-3S
3/26/141535
ND
ND
574.3
65,300
X5368
IW-3D
3/26/141645
ND
528.1 **
1,150
ND
X5369
IW-4S
3/27/14 1500
511.5 **
306
ND
574.2
9,970
X5370
IW-4D
3/27/14 1400
ND
532.0 **
3,100
ND
X5371
PP-1S
3/28/141220
507.4
0.464
ND
ND
X5372
PP-3S
3/28/141310
507.3
2.50
ND
ND
X5373
PP-8
4/3/14 1300
ND
529.4 **
0.424
ND
1 of2
F:\docs\COA\arcadis\ARCADIS_Mallinckrodt_NC_19

OUL
Number
Sample Identification
Date/Time
Collected
Fluorescein
Eosine
RWT
Peak (nm)
Conc. (ppb)
Peak (nm)
Conc. (ppb)
Peak (nm)
Conc. (ppb)
X5374
PP-16
3/28/14 1650
505.4 *
0.280
528.4 **
2.33
ND
X5375
PP-18D
3/26/141700
ND
ND
ND
X5376
FT-1S
3/26/141640
507.5
365
ND
ND
X5377
DUP-1
3/27/140000
ND
ND
ND
X5378
DUP-2
3/28/14 0000
ND
ND
ND
X5379
DUP-3
3/27/14 0000
508.0
101
ND
573.9
48.6
X5380
Laboratory control water blank
Note: Dye concentrations are based upon standards used at the OUL. The standard concentrations are based upon the as sold weight of the dye that the
OUL uses. If the client is not using OULdyes, the client should provide the OUL with a sample of the dye to compare to the OUL dyes.
Footnotes: ND = No dye detected
** = A fluorescence peak is present that does not meet all the criteria for this dye. However, it has been calculated as a positive dye result.
Thomas J. Aley, PHG and RG
2 of 2 F:\docs\COA\arcadis\ARCADIS Mallinckrodt NC 19

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DISCREPANCIES BETWEEN CHAIN -OF -CUSTODY SHEETS AND ACTUAL SAMPLES RECEIVED Page / of /
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rev. 12/28/99