WQ0034688_Renewal Application_20210617

Non -Discharge Branch Upload/Submittal Form
Initial Review
Reviewer
Thornburg, Nathaniel D
Is this submittal an application? (Excluding additional information.)*
a Yes r No
Permit Number (IR)* WQ0034688
Applicant/Permittee Neuse Regional Water and Sewer Authority
Applicant/Permittee Address 2811 Barrus Rd, La Grange, NC 28551
Is the owner in BIMS? a Yes r No Is the facility in BIMS? r Yes r No
Owner Type County
Facility Name Neuse Regional Water and Sewer Authority DCAR
County Lenoir
Fee Category Minor Fee Amount $0
Is this a complete
application? *
a Yes r No
Signature Authority
Signature Authority Title
Signature Authority Email
Document Type (if non -application)
Email Notifications
Does this need review by the hydrogeologist?* r Yes NO
Regional Office
CO Reviewer
Admin Reviewer
Complete App Date 06/17/2021
Below list any additional email address that need notification about a new project.
Email Address
Comments to be added to email notfication
Comments for Admin
Comments for RO

Comments for Reviewer
Comments for Applicant

Submittal Form
Project Contact Information
Rease provide information on the person to be contacted by NEB Staff regarding electronic subnittal, confirmation of receipt, and other correspondence.
Name* Chris Wynne
Email Address*
[e-mail]
Project Information
Application/Document Type *
✓ New (Fee Required)
✓ Modification - Major (Fee Required)
✓ Renewal with Major Modification (Fee
Required)
✓ Annual Report
✓ Additional Information
✓ Other
Phone Number*
3369098627
O Modification - Minor
G Renewal
O GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
✓ Residual Annual Report
✓ Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
✓ Wastewater Irrigation
✓ Other Wastewater
✓ Closed -Loop Recycle
✓ Single -Family Residence Wastewater
Irrigation
✓ High -Rate Infiltration
✓ Reclaimed Water
t: Residuals
✓ Other
Permit Number:* WO0034688
Has Qirrent Existing permit number
Applicant/Permittee *
Neuse Regional Water and Sewer Authority
Applicant/Permittee Address* 2811 Barrus Rd, La Grange, NC 28551
Facility Name *
Neuse Regional Water and Sewer Authority DCAR
Please provide comments/notes on your current submittal below.
Find attached all supporting documentation for the renewal of NRWASA's land application
permit (WQ0034688). Let me know if you have any questions or concerns. Thanks.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Flans, Specifications, Calculations, Etc.)
NRWASA renewal_2021.pdf 54.95MB
Upload only 1 REFdo;urn:nt (less than 2501vt3). NLftiple documents must be corrbined into one FIT file unless file is larger than
upload lint.
* fJ By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature

Submission Date 6/17/2021

DWR
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS
INSTRUCTIONS FOR FORM: DCAR 06-16 & SUPPORTING DOCUMENTATION
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted, the Applieant shall submit one original and two copies of the application and
supporting documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit website
General — This application is for treatment, storage, transport, distribution, land application, and/or marketing of Class A (or Equivalent)
residuals under 15A NCAC 02T .1100.
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Distribution of Class A Residuals (FORM: DCAR 06-16):
® Submit the completed and appropriately executed Distribution of Class A Residuals (FORM: DCAR 06-16) form. Please do
not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to
the application may be made, as long as the attachments are numbered to correspond to the section and item to which they
refer.
E The project name should be consistent on the plans, specifications, etc.
El The Applicant's Certification on Page 3 of this form shall be signed in accordance with 15A NCAC 02T .0106(b). An alternate
person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A
NCAC 02T .0106(b).
❑ If this project is for a modification of an existing permit, submit one copy of the existing permit.
® Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to
operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units.
B. Application Fee (New and Major Modification Application Packages)
❑ Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental
Quality (NCDEQ).
Facility Classification
[—New Permit Major Modification
Major (residuals permitted for distribution > 3,000 dry tons/year)
$1,310
$395
Minor (residuals permitted for distribution < 3,000 dry tons/year)
$810 $245
' - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage;
adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted.
There is no fee for minor permit modifications_
C. Cover Letter (All Application Packages)
Z List all items included in the application package, as well as a brief description of the requested permitting action.
INSTRUCTIONS FOR FORM: DCAR 06-16 Page 1 of 3

D. Program Information (All Application Packages)
® Provide a narrative explaining the following:
® How the materials will be handled and transported from where the residuals were produced to where it will be treated.
® How the residuals will be processed/treated (attach process flow diagram).
❑ How leachate collection will be handled.
® Where the residuals will be stored until processed.
IZI How the fmal product will be distributed (packaging, bulk, etc.)
EWhat nutrients or other constituents (Le. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the
limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause
contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality.
® Attach a marketability statement detailing destinations and approximate amounts of the fmal product to be distributed.
® Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the
person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following
information:
® Name and address of the person who prepared the residual that is sold or given away.
® A statement that application of the residuals to the land shall be in accordance with the instructions on the label or
information sheet.
Ej A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered.
A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored
residuals into any surface waters.
® Information on all applicable setbacks in accordance with 15A NCAC 02T .1108(b).
® A statement that the residuals shall be applied at agronomic or recommended rates for intended uses.
E. Detailed Plans and Specifications (Application Involving New or Changes to Treatment or Storage Units)
❑ Submit detailed plans and specifications that have been signed, sealed, and dated by a NC Professional Engineer per 15A
NCAC 02T .1104(a). Specifications for standard equipment may only be omitted for municipalities with approved standard
specifications, but use of the standard specifications must be noted on each sheet of the plans.
❑ Plans must include the following minimum items: a general location map, a topographic map, plan and profile view of the
residuals treatment and storage units as well as the proximity of the residuals treatment and storage units to other utilities and
natural features within 500 feet of all treatment and storage facilities, and detail drawings of all items pertinent to the residuals
treatment and storage units. Depict minimum separations required in 15A NCAC 02T .1108(a) on the plans.
❑ Specifications must include, at a minimum, the following for all items pertinent to residuals treatment and storage units:
description of materials to be used, methods of construction, quality of construction testing procedures to ensure the integrity
of the fmal product in accordance with 15A NCAC 02T .1 I04(a)(2)(B), including leakage and pressure testing as appropriate.
❑ Plans and specifications must not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR
CONSTRUCTION, etc.) that indicate that they are anything other than final plans and specifications. However, the plans and
specifications may be labeled with the phrase: FINAL DESIGN — NOT RELEASED FOR CONSTRUCTION.
F. Engineering Calculations (Application Involving New or Changes to Treatment or Storage Units)
❑ Submit all design calculations that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T
.1104(a).
G. Environmental Assessments (May be Required — See 15A NCAC IC .0300)
❑ Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include
information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals
treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for
the construction of the subject facilities.
INSTRUCTIONS FOR FORM: DCAR 06-16 Page 2 of 3

H. Operation and Maintenance Plan (New and Renewal Application Packages)
® For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan.
® Submit the O&M Plan in accordance with 15A NCAC 02T .1110 and include at a minimum:
El Operational functions; describe the operation of the program to show what operations are necessary for the program to function
and by whom the functions are to be conducted.
El Maintenance schedules; may include equipments calibration, maintenance of signs, etc.
• Safety measures; may include safety training program, manuals, signs, etc.
® Spill response plan; including control, containment, remediation, emergency contact information, etc.
El Inspection plan including the following information;
Names and titles of personnel responsible for conducting the inspections.
® Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected
location(s) and inspection frequency are representative of the residuals management program.
® Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event
that noncompliance is observed.
® Sampling and monitoring plan including the following information;
• Names and titles of personnel responsible for conducting the sampling and monitoring.
• Detailed description of monitoring procedures including parameters to be monitored.
® Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow,
and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling
plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet
pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual
sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected
by cold temperatures.
ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL
SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS:
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF WATER RESOURCES
WATER QUALITY PERMITTING SECTION
NON -DISCHARGE PERMITTING UNIT
By U.S. Postal Service:
1617 MAIL SERVICE CENTER
RALEIGH, NORTH CAROLINA 27699-1617
TELEPHONE NUMBER: [phone]
By Courier/Special Delivery:
512 N. SALISBURY STREET
RALEIGH, NORTH CAROLINA 27604
FAX NUMBER: [phone]
INSTRUCTIONS FOR FORM: DCAR 06-16
Page 3 of 3

DWR
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS
FORM: DCAR 06-16
I. APPLICANT INFORMATION:
1. Applicant's name: Neuse Regional WASA
Applicant type: ❑ Individual ❑ Corporation ❑ General Partnership ►1 Privately -Owned Public Utility
❑ Federal ❑ State 0 Municipal 0 County
Signature authority's name per 15A NCAC 02T .0106: Harold Herring Title: Executive Director
Applicant's mailing address: 2811 Barrus Rd
City: La Grange State: NC Zip: 28551-
Telephone number: [phone] Email Address: harold.herringna,nrwasa.org
2. Consultant's name: License Number (for P.E.):
Affiliation: ❑ On Staff ❑ Retained (Firm: )
Consultant's mailing address:
City: State: Zip:
Telephone number: ( ) - Email Address:
3. Fee submitted: $0 (See Instruction B)
II. PERMIT INFORMATION:
1. Application is for (check all that apply): ❑ new, ❑ modified, renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: WQ0034688
Date of most -recently issued permit: 8/2/2016
Date of most -recently certified Attachment A (if different than the permit):
III. FACILITY INFORMATION:
1. Name of residuals processing facility: Neuse Regional Water Treatment Plant
City: La Grange State: NC Zip: 28551-
Coordinates: Latitude: 35° 15' 01" Longitude: 77° 42' 36"
Datum: Map Level of accuracy: Second
Method of measurement: Map
County where facility is located: Lenoir
2. Facility contact (person familiar with residuals preparation):
Name: Charlie Colie Title: Plant ORC
Mailing address: 2811 Barrus Rd
City: La Grange State: NC Zip: 28511-
Telephone number: [phone] E-mail address: charlie.colie@a,nrwasa.org
FORM: DCAR 06-16
Page 1 of 3

3. Is the residual process facility also the generator? ® Yes; ID No
If No, please specify delivery frequency and quantity of residual to be processed:
4. Length of residuals storage at facility: 365 days (Note: the Division requires minimum 30 days storage in units that are
separate from treatment system, i.e. not in clarifiers, aeration basins, etc.)
IV. RESIDUALS QUALITY INFORMATION:
1. Specify how these residuals will be distributed:
❑ sold or given away in bags or other containers; 0 lawn (bulk); ❑ home garden (bulk);
El other (explain); Synagro will perform land application of the bulk water treatment plant residuals
Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a
load capacity of one metric ton or less.
2. Complete the following if residuals are to be mixed with other materials:
Type of Materials
Amounts to be added
per 1.0 dry ton of residuals (dry ton)
3. Approximate amounts of the residuals received and processed at the facility: 834 dry tons per year.
4. Approximate amounts of the final product (processed residuals) to be distributed: 834 dry tons per year.
5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and
maximum storage times prior to distribution):
application begins.
Water treatment plant residuals will be stored in lined lagoons until land
6. Does the facility have a stormwater management plan? ® Yes; Q No
Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled: The water treatment
plant residuals are stored in lined lagoons that are not under roof.
V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and submit the attached Residuals Source Certification and all associated documentation.
RSC 06-16.doc
FORM: DCAR 06-16
Page 2 of 3

Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units)
1, , attest that this application for
has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge
the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package
may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed
this material and have judged it to be consistent with the proposed design.
North Carolina Professional Engineer's Seal, Signature, and Date:
Applicant's Certification:
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
® Yes
I,
0 No, Explain; J�
phi , '"72/ Z4" Executive Director
(Signature Authority's Name — PLEASE PRINT) (Title)
attest that this application for
Neuse Regional Water Treatment Plant
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water
Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed
and that if all required supporting information and attachments are not included, this application package will be returned to me as
incomplete.
Note: In accordance with North Carolina General Statutes §143-215.6A and §143-215.6B, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil penalties up to $25,000 per violation.
Signature:
Date:
6//7/2/
FORM: DCAR 06-16
Page 3 of 3

DCAR Statement
Neuse Regional WASA (WQ0034688)
D. Land application narrative
Water treatment residuals will be pumped from the treatment plant to the line lagoons on -site.
The residuals will be collected and stored in the basins until land application begins. The residuals will be
land applied in bulk using the appropriate spreading equipment that achieve a uniform spread pattern.
Land application rates are based on soil series, realistic yield expectation, and limited to the nitrogen
requirements for the intended crop.
Chris Wynne
Technical Services Specialist

Neuse Regional WTP
Land Application Permit WQ0034688
Label for Land Application
The residuals that are land applied form Neuse Regional WTP are produced at 2811 Barret Road in La
Grange, NC 28551. Mr. Harold Herring, Executive Director is the preparer of the residuals and
responsible for the plant operations.
The residuals from Neuse Regional WTP will be applied to agricultural fields at agronomic rates based
on the RYE rate for the fields and crops to be grown. The WTP residuals will not be applied to frozen,
snow covered or flooded fields. The fields will be flagged with the following buffers to help prevent
runoff from the applied fields:
Setback Description
Setback by residual type (feet)
Liquid
Cake*
Private or public water supply
100
100
Surface waters (streams — intermittent and perennial,
perennial waterbodies, and wetlands)
100
25
Surface water diversions (ephemeral streams,
waterways, ditches)
25
0
Groundwater lowering ditches (where the bottom of
the ditch intersects the SHWT)
25
0
Wells with exception to monitoring wells
100
100
Bedrock outcrops
25
0
Residuals produced by Neuse Regional WTP will be applied to agricultural fields in bulk and will be
applied according this label as well as following all permit conditions as listed in the the land application
permit WQ0034688.

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OPERATIONS AND MAINTENANCE PLAN
SYNAGRO RESIDUALS LAND APPLICATION FOR WQ0034688 (Neuse Regional Water & Sewer Authority)
Inspection Plan
Inspections for the land application of residuals will be conducted on a weekly basis at the land application site during the land
application activities of this project. The inspection frequency is based on the time frame that it is going to take to complete the
project and the amount of dry tons to be land applied from this facility. The inspections will consist of inspecting a current field that
is being applied as well as inspecting random fields that have been completed. These inspections will consist of:
1. Verifying that the Pre -Operations Check List has been completed and signed by both Operations and Technical staff.
2. Checking the calculated loads to ensure the correct amount of residuals are being land applied.
3. Ensure that all manned equipment has a copy of the spill control plan, the permit, and the operations and maintenance
plan.
4. Ensure that the field has been flagged properly and that all buffers are being adhered to.
5. Ensure that the Crop and Landowner Verification form has been filled out.
6. Verifying that the correct number of samples of the residuals has been taken and that it meets the criteria for land
application.
7. The records will be kept in the project files in the respective office for the project.
8. The Permittee or Inspector shall report by telephone to the Washington Regional Office by telephone at 252-948-3939 as
soon as possible but no later than 24 hours after or the next working day following the occurrence or the first knowledge of
the occurrence of the following.
• Any occurrence with the distribution program resulting in the land application of significant amounts of material
that is abnormal in quantity or characteristics.
• Any failure of the distribution system that results in the release to surface waters.
• Any time that self -monitoring indicates that the facility has gone out of compliance with the permit.
• Any process failure that results in the system not adequately treating the residuals.
• Any spill or discharge from a vehicle or piping system during residuals transportation.
• Any release that requires immediate reporting outside of normal business hours shall be called in to DENR at 1-
800-662-7956, 1-800-858-0368, or 1-919-733-3300. These numbers are to be called in the event of a release to
surface waters, imminent failure of a storage system when the event occurs outside of normal business hours.
« Within 5 days of the first notice of on occurrence a written response in the form of a letter shall be sent to DENR
outlining the actions taken or purposed actions taken to ensure that the problem does not recur. Persons
responsible for inspections on this project are as follows:
Chris Wynne, Technical Services Specialist or his designee

OPERATIONS AND MAINTENANCE PLAN
SYNAGRO RESIDUALS LAND APPLICATION FOR WQ0034688
Sampling Plan
Sampling for this project consists of sampling the residuals prior to or during the time that land application is
occurring. This will result in one round of sampling to occur before land application commences to ensure that the
residuals are suitable for land application. Based on the dry tonnage of this plant this will be four samples for all
parameters per year except for the TCLP.
The residuals shall be sampled annually
Arsenic (5.0)
Barium (100.0)
Benzene (0.5)
Cadmium (1.0)
Carbon tetrachloride (0.5)
Chlordane (0.03)
Chlorobenzene (100.0)
Chloroform (6.0)
Chromium (5.0)
M-Cresol (200.0)
o-Cresol (200.0)
p-Cresol (200.0)
Cresol (200.0)
2,4-D (10.0)
for the following: (Regulatory level in
1, 4-Dichlorobenzene (7.5 )
1, 2-Dichloroethane (0.5)
1, 1-Dichloroethylene (0.7)
2, 4-Dinitrotoluene (0.13)
Endrin (0.02)
Hexachlorobenzene (0.13
Heptachlor (and its hydroxide) (0.008)
Hexachloro-1,3-butadiene (0.5)
Hexachlorethane (3.0)
Lead (5.0)
Lindane (0.4)
Mercury (0.2)
Methoxychlor (10.0)
Methyl ethyl ketone (200.0)
milligrams per liter in parentheses.)
Nitrobenzene (2.0)
Pentachlorophenol (100.0)
Pyridine (5.0)
Selenium (1.0)
Silver (5.0)
Tetrachloroethylene (0.7)
Toxaphene (0.5)
Trichloroethylene (0.5)
2,4,5-Trichlorophenol (400.0)
2,4,6-Trichlorophenol (2.0)
2,4,5 TP (Silvex) (1.0)
Vinyl Chloride (0.2)
The residuals will also be sampled based on the chart below for the following constituents:
Dry Tons Generated
(short tons per year)
Monitoring Frequency
(Established in 40 CFR 503 and 15A NCAC 02T.1111)
<319
1 time per year
=>319-<1,650
1 per Quarter (4 times per year)
=>1,650-<16,500
1 every 60 days (6 times per year)
=>16,500
1 every month (12 times per year)
Aluminum
Ammonia -Nitrogen
Arsenic
Cadmium
Calcium
Copper
Lead
Sodium Adsorption Ratio (SAR)
Magnesium
Mercury
Molybdenum
Nickel
Nitrate -Nitrite Nitrogen
Phosphorous
Potassium
pH
Plant Available Nitrogen (calculation)
Selenium
Sodium
Total Solids
Total Kjeldahl Nitrogen
Zinc
Samples that will be pulled are a TCLP and a nutrient and metals sample to prove that the material is suitable for land application.
The nutrient and metal and TCLP sample will be collected randomly and consist of at least 10 individual samples mixed to get the
composite sample for these parameters.
The following people are responsible for sampling:
Chris Wynne Technical Services Specialist or his designee.

OPERATIONS AND MAINTENANCE PLAN
SYNAGRO RESIDUALS LAND APPLICATION FOR WQ0034688 (Neuse Regional Water & Sewer Authority)
Operational Functions
The operation function of this project is going to involve mixing the lagoon up with a tractor powered Houle pump to
achieve a well mixed and consistent material that is suitable for land application. It is going to be spread at agronomic
rates that are determined by the nutrient and metal sample that is current for that monitoring period. It is going to be
spread with a liquid applicator that will use pressure to spread the material in such a way to achieve a consistent spread
pattern. The material is going to be land applied on fields that are in normal agricultural row crop production.
SAFETY MEASURES
Synagro believes in operating in a safety conscious manner and has all employees participate in quarterly online safety
course that are designed to help its employees recognize safety issues and take steps to prevent accidents from
occurring. In addition, all Synagro employees have the authority to stop operations if they think any aspect of the
operation is going to cause environmental or personal harm.
Maintenance Schedule
Synagro will follow the maintenance schedule as recommended by the Synagro fleet manager for the equipment
necessary to complete the job.

SPILL RESPONSE PLAN
PROJECT: Neuse Regional Water & Sewer Authority W00034688
IN THE UNLIKELY EVENT OF A SPILL, THE FOLLOWING ACTIONS SHALL BE TAKEN
IMMEDIATELY:
1. MANAGEMENT OF SPILL CLEAN-UP ACTIVITIES:
The Operations Manager shall take immediate charge and initiate clean-up activities. Synagro labor and equipment is to
be utilized. In the event additional labor and equipment is required, assistance may be requested from the Neuse Regional
Water & Sewer Authority, the NC Department of Transportation, and other private contractors as necessary.
2. HALT THE SOURCE OF THE SPILL:
Such as a ruptured container or damaged transport unit.
3. CONTAIN THE SPILL:
Form a barrier. Sufficient quantities of straw shall be used for such purposes. Earthen barriers may be constructed to
augment the straw bale containment area of the spill. The Operations Manager or the person in charge on the spill site
will advise the clean-up personnel where to get the straw, lime, and other items necessary to complete the clean-up
operation, i.e., local farmers, farm supply centers, nurseries, etc.
4. CLEAN-UP:
Employ front-end loaders, vacuum equipment, sludge application vehicles, and/or local septic tank service to remove as
much of the spilled material as possible. Straw and/or sand should be scattered in the spill area to soak up the remaining
material. The straw- and sand -soaked material will be collected and removed to a disposal area approved by
representatives of the state regulatory agency.
5. FINAL CLEAN-UP:
Employ rotary brush sweeper if needed, and apply lime to the spill area upon the approval of the clean-up efforts by the
state regulatory representative. If the event occurs on private property, the clean-up will be completed to the satisfaction
of the property owner and state regulatory representatives. The ultimate goal will be to restore the spill area to its original
condition if possible.
6. NOTIFICATION:
As soon as possible after the spill occurs, the Synagro Operations Manager or assistant will notify the Synagro Central
office, and they will then be responsible for notifying other key Synagro personnel.
7. REPORTING:
Synagro Central personnel will notify the Washington Regional Office of the NCDENR by telephone [phone]) as
soon as possible, but not more than 24 hours after, or on the next working day following the occurrence. The Operations
Manager shall provide a written report within 48 hours of the spill to the Technical Services Director. The report shall list
all relative information and actions taken. Synagro Central personnel will file a written report to the Wilmington Regional
office of the NCDENR within 5 days of the occurrence. For after hours reporting the Division's emergency number shall
be called to report all incidences (800-662-7956 or 800-858-0368 or 919-733-3300)

DWR
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
INSTRUCTIONS FOR FORM: RSC 06-16
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and
supporting documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit
General — This certification provides detailed information of residuals source generating facility and its residuals quality for land
application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without
a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Residuals Source Certification (FORM: RSC 11-15):
® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not
make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the
application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer.
® For new or renewed permits, submit a separate certification for each source facility.
❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification.
® Complete the residuals source facility summary page. List all new, renewed, or modified facilities.
B. Residuals Source -Generating Facility Information:
® For each source facility, attach the following:
® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for
Residuals Land Application Permits".
® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals
are to be generated, treated, processed, and stored at the facility.
® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8.
Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of
the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed,
and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during
processing.
® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies
sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition,
ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and
vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as
they are to be land applied, distributed, and/or disposed.
C. Residuals Quality Information:
® For each source facility, attach the following:
® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification.
® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector
attraction reduction requirements.
❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please
attach analytical results of residuals generated from a similar facility along with the description of similarities of the two
facilities.
INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1

91-90 DS21
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Neuse Regional WASA
Facility Permit Holder
Neuse Regional Water
Treatment Plant
Facility Name
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Applicant's name: Neuse Regional WASA
RESIDUALS SOURCE FACILITY SUMMARY

DWR
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Neuse Regional Water Treatment Plant
2. Facility permit holder is: ❑ Federal, fl State, ❑ Local Government, or i1, Private.
Facility issued permitby:12 Div. of Water Resources, 0 Div. of Environmental Health,
or ❑ Other (explain:
).
3. Facility contact person and title: Charlie Colie, Plant ORC
Complete mailing address: 2811 Barrus Rd
City: La Grange State: NC
Zip: 28511-
Telephone number: [phone] E-mail address: charlie.coliena,nrwasa.org
4. Facility physical address: 2811 Barrus Rd
City: La Grange State: NC Zip: 28511-
Coordinates: Latitude: 35° 15' 00" Longitude: 77° 42' 36"
Datum: Map Level of accuracy: Second
Method of measurement: Map
5. Purpose of the facility:
treatment of municipal wastewater, 0 treatment of 100% domestic wastewater,
treatment of potable water, ❑ treatment of 100% industrial wastewater,
0 treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: % industrial and % domestic)
other (explain: ).
6. Does the facility have an approved pretreatment program: D Yes El, No
7. Facility permitted/design flow: 15 MGD and facility average daily flow: 7.5 MGD
8. Average amount of residuals being generated at this facility 224.63 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment:
Type and volume of residuals storage (i.e., outside of residuals treatment units): Water treatment plant liquid, 3 2 million
gallon lagoons
H. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or El 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
Biological t Non -Biological
FORM: RSC 06-16
Page 1 of 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes El no.
If yes, list the number(s):
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: f yes ® no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Summit Environmental Technologies, Inc. and Date of analysis: 9/9/2020
Passed corrosivity test:
Passed ignitability test:
Passed reactivity test:
yes ❑ no. pH: s.u. (2 <pH < 12.5)
yes ❑ no. Flashpoint: >140 °F (> 140°F)
yes Ono. HCN: ND mg/kg (<250) & H2S: 70 mg/kg (<500)
TCLP Parameter
Limit
Result
(mg/1)
TCLP Parameter
Limit
(mg/1)
Result
(mg/1)
Arsenic
5.0
ND
Hexachlorobenzene
0.13
ND
Barium
100.0
ND
Hexachloro-1,3-Butadiene
0.5
ND
Benzene
0.5
ND
Hexachloroethane
3.0
ND
Cadmium
1.0
ND
Lead
5.0
ND
Carbon Tetrachloride
0.5
ND
Lindane
0.4
ND
Chlordane
0.03
ND
Mercury
0.2
ND
Chlorobenzene
100.0
ND
Methoxychlor
10.0
ND
Chloroform
6.0
ND
Methyl Ethyl Ketone
200.0
ND
Chromium
5.0
ND
Nitrobenzene
2.0
ND
m-Cresol
200.0
ND
Pentachlorophenol
100.0
ND
o-Cresol
200.0
ND
Pyridine
5.0
ND
p-Cresol
200.0
ND
Selenium
1.0
ND
Cresol
200.0
ND
Silver
5.0
ND
2,4-D
10.0
ND
Tetrachloroethylene
0.7
ND
1,4-Dichlorobenzene
7.5
ND
Toxaphene
0.5
ND
1,2-Dichloroethane
0.5
ND
Trichloroethylene
0.5
ND
1,1-Dichloroethylene
0.7
ND
2,4,5-Trichlorophenol
400.0
ND
2,4-Dinitrotoluene
0.13
ND
2,4,6-Trichlorophenol
2.0
ND
Endrin
0.02
ND
2,4,5-TP (Silvex)
1.0
ND
Heptachlor and its Hydroxide
0.008
ND
Vinyl Chloride
0.2
ND
FORM: RSC 06-16
Page 2 of S

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 9110/2020
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mg/kg)
Monthly Average
Concentration Limits
(Class A Only)
(mg/kg)
Result
(mg/kg)
Arsenic
75
41
10
Cadmium
85
39
ND
Copper
4,300
1,500
180
Lead
840
300
19
Mercury
57
17
ND
Molybdenum
75
n/a
ND
Nickel
420
420
ND
Selenium
100
100
ND
Zinc
7,500
2,800
100
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: and Date of analysis:
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
0 > 0 but < 25
30
200
210
Q > 25 but < 50
34
220
240
Q > 50 but < 75
39
260
270
> 75 but < 100
46
300
320
> 100 but < 125
53
360
390
> 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16
Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 2.19 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Pace Analytical Services, LLC " and Date of analysis: 9/10/2020
Parameter
Result
(mg/kg)
Aluminum
180000
Ammonia -Nitrogen
940
Calcium
2400
Magnesium
ND
Nitrate -Nitrite Nitrogen
33.4
pH (Standard Unit)
6.2
Phosphorus
2800
Potassium
2100
Sodium
1900
Total Kjeldahl Nitrogen
13000
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 1.58
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 24 %. This
rate is a (check one): 1i default value, or [] actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (Pt) Year PAN
(mg/kg)
Five -Year
Maximum Adjusted PAN
(mg/kg)
Surface
2915
4771
Injection/Incorporation
3385
5241
Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:
FORM: RSC 06-16
Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
0 A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
0 Alternative 1 [15A NCAC 02T.1106(b)(3)(A)] - Time/Temperature Compliance.
• Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment.
O Alternative 3 [15A NCAC 02T.1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
0Alternative 4 [15A NCAC 02T.1106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
❑' Alternative 5 [15A NCAC 02T.1106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, ❑ heat drying, 0', heat treatment,
❑' thermophilic aerobic digestion, 0 beta ray irradiation,
0 gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
0 Alternative 1 [15A NCAC 02T.1106(c)(1)] - Fecal Coliform Density Demonstration.
D Alternative 2 [15A NCAC 02T.1106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑' aerobic digestion, 0 air drying, 0' anaerobic digestion,
composting, or []! lime stabilization.
c. For Surface Disposal:
❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
❑I Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
O Exempt - If Daily Cover Alternative is chosen in Item 11.8. below [15A NCAC 02T.1106(a)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
• Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
O Alternative 2 [15A NCAC 02T.1107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
Alternative 3 [15A NCAC 02T.1107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
0 Alternative 4 [15A NCAC 02T.1107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
• Alternative 5 [15A NCAC 02T.1107(a)(5)] - 14-Day Aerobic Processes.
❑ Alternative 6 [15A NCAC 02T.1107(a)(6)] - Alkaline Stabilization.
0 Alternative 7 [15A NCAC 02T.1107(a)(7)] - Drying of Stabilized Residuals.
• Alternative 8 [15A NCAC 02T.1107(a)(8)] - Drying of Unstabilized Residuals.
O Alternative 9 [15A NCAC 02T.1107(a)(9)] - Injection.
Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation.
Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.1107(b)(2)].
I Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

VICINITY MAP
SYNAGRO
5
E60-3j
I 1318
1)3091
70
1 24
15201
Fields
c5..Harvey Pkwy
9Lenoir County Landfill CR
UNC Leno
1622
Falling Creek
goNeuse Regional WASA
Kinston Public Services
COUNTY: Lenoir OWNER(S): Neuse Regional WASA

Q 4 4 Q
o-
o-
8
0-1
a
o-
0-
1
V
6
I, I
'KNV.V.V \ Niiu
2
8
INNYKI „D
b
0
4
NEUSE REGIONAL WATER TREATMENT PLANT
2
a
a
H
in

Quantitative Justification for Residuals Production
Neuse Regional WASA (WQ0034688)
Based on the average of the past 4 years dry tonnage land applied, there is no request to
change the current permitted dry tonnage of 834 dry tons/year.
2020: 281.91 dry tons
2019: 291.56 dry tons
2018: 0 dry tons
2017: 325.04 dry tons
Average: 224.63 dry tons
Chris Wynne
Technical Services Specialist

Residual Sampling Plan
Neuse Regional Water and Sewer Authority
Neuse Regional Water Treatment Plant
Nutrient -Metal Concentration Analysis
Sampling point:
Sampling frequency:
Sample type:
Laboratory:
Reclamation ponds
Based on dry tonnage
Composite
Pace Analytical Services, Inc.
TCLP & RCI
Sampling point:
Sampling frequency:
Sample type:
Laboratory:
Reclamation ponds
Annually
Composite
Summit Environmental Technologies, Inc.
Pathogen and Vector Attraction Reduction Monitoring
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution

Summ
E1 111RONMEUTAL tECHNOLO( S, ;Nr
AnNytical f ,shprgiorMB
September 09, 2020
Chris Wynne
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: NRWASA
Dear Chris Wynne:
Summit Environmental Technologies, Inc. received 1 sample(s) on 8/27/2020 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
Website: http://www.settek.com
Order No.: 20081630
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
)77.4064•41010-
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 2943, Colorado, Connecticut PH-0108, Florida NELAC E87688, Idaho OH00923, Illinois 200061, Indiana C-OH-13, Kansas
E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988, Minnesota 1780279, Nevada OH009232020-1, New
Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP CL0052, Oklahoma
2019-155, Oregon 01-1200001, Pennsylvania 011, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-19-16, Utah OH009232020-12,
Virginia VELAP 10381, West Virginia 9957C
Page 1 of 32

■ l
SUMMI
ENVIRONMENTAL 1ECNNOton«.s, '.
A natytical t. s twolones
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
Website: http://www.settek.com
Case Narrative
WO#: 20081630
Date: 9/9/2020
CLIENT: Synagro
Project: NRWASA
WorkOrder Narrative:
20081630: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
20081630-001A Ignitability_S(1030): does not propagate
Analytical Sequence QC Notes:
20081630-001ADUP Ignitability S(1030): does not propagate
20081630-001AMS TCLP-SVOC_8270E: High RPD due to suspected sample inhomogeneity.
20081630-001AMSD TCLP-SVOC_8270E: High RPD due to suspected sample inhomogeneity.
Original
Page 2 of 32

il
SUMMI
Summit Environmental Technologies, In
3310 Win
ENVIRONMENTAL T£CNMC)f o ,+rs. ,. r Cuyahoga Falls, Ohio 442.;
4natyricat Laboratom • TEL: [phone] FAX- (330) 253-446
Website: http://www.settek.co
Qualifiers and Acronyms
WO#: 20081630
Date:
9/9/2020
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC -I+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-ft The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
QC
MB
LCS
LCSD
QCS
DUP
MS
MSD
RPD
ICV
ICB
CCV
CCB
RLC
DF
Not Detected
Quality Control
Method Blank
Laboratory Control Sample
Laboratory Control Sample Duplicate
Quality Control Sample
Duplicate
Matrix Spike
Matrix Spike Duplicate
Relative Percent Different
Initial Calibration Verification
Initial Calibration Blank
Continuing Calibration Verification
Continuing Calibration Blank
Reporting Limit Check
Dilution Factor
RL
MDL
LOD
LOQ
PQL
CRQL
PL
RegLvl
MCL
MinCL
RA
RE
TIC
RT
CF
RF
Reporting Limit
Method Detection Limit
Level of Detection
Level of Quantitation
Practical Quantitation Limit
Contract Required Quantitation Limit
Permit Limit
Regulatory Limit
Maximum Contamination Limit
Minimum Compound Limit
Reanalysis
Reextraction
Tentatively Identified Compound
Retention Time
Calibration Factor
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 32

SUMMI
ENVIRONMENTAL TEC 1NOL.OG:ES, Ok
Anafytteal tab�Farcrias
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
Website: httpJ/www.settek.com
Workorder
Sample Summary
WO#: 20081630
09-Sep-20
CLIENT:
Project:
Synagro
NRWASA
Lab SampleID Client Sample ID
20081630-001 NRWASA
Tag No Date Collected
8/26/2020 11:00:00 AM
Date Received
8/28/2020 11:55:00 AM
Matrix
Sludge
Page 4 of 32

Analysis Date
Leachate Date
Collection Date
Client Sample ID
§
�
J
8/31/2020 2:00:00 PM
itability of Solids (SW-846: 1030)
8/26/2020 11:00:00 AM
20081630-OOIA
9/3/2020 4:50:00 PM
0
§
/
Percent Solids
8/28/2020 12:37:32 PM
pH (SW9045D)
9/2/2020 12:54:00 PM
Reactive Cyanide (9014/7.3.3.2)-Solid
9/3/2020 12:54:00 PM
Reactive Sulfide (9034)/7.3.4.2
9/3/2020 10:39:00 PM
9/2/2020 5:00:00 PM
TCLP Herbicides by EPA 8321B
9/4/2020 2:09:00 PM
TCLP Metals Analysis (SW I311/6010;9/2/2020 5:00:00 PM
9/4/2020 11:38:00 PM
9/3/2020 9:03:00 PM
9/4/2020 11:16:00 AM
9/2/2020 5:00:00 PM

SuMMI
EPiVIifONMENTAL TECHNOLOGIES, IN
Anistrfcal Laborrtortas
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
Website: http://www.settek.com
Analytical Report
(base report)
WO#: 20081630
Date Reported: 9/9/2020
CLIENT:
Matrix:
Lab ID:
Project:
Synagro
SLUDGE
20081630-001A
NRWASA
Client Sample ID NRWASA
Tag Number:
Collection Date: 8/26/2020 11:00:00 AM
Analyses Result
RL Qual Units
DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW7470A
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury
ND 0.00200 mg/L
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
TCLP Barium(Ba)
TCLP Cadmium(Cd)
TCLP Chromium(Cr)
TCLP Lead(Pb)
TCLP Selenium(Se)
TCLP Silver(Ag)
ND
ND
ND
ND
ND
ND
ND
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
2,4, 5-Trichlorophenol
2,4, 6-Trichlo rophenol
2,4-Dinitrotoluene
Cresols, Total
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
Surr: 2-Fluorophenol
Sun': Phenol-d6
Surr: Nitrobenzene-d5
Surr: 2,4,6-Tribromophenol
Surr: 2-Fluorobiphenyl
Surr: p-Terphenyl-d14
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
56.9
65.2
65.5
72.5
65.6
86.6
0.500
5.00
0.100
0.200
0.500
0.0500
0.500
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
1
SW7470A Analyst: MJM
9/4/2020 2:09:00 PM
SW6010D SW3010A Analyst: EAM
9/4/2020 11:19:01 AM
9/4/2020 11:19:01 AM
9/4/2020 11:19:01 AM
9/4/2020 11:19:01 AM
9/4/2020 11:19:01 AM
9/4/2020 11:19:01 AM
9/4/2020 11:19:01 AM
SW8270 SW3510C Analyst: SFG
0.200 mg/L
0.500 mg/L
0.500 mg/L
0.100 mg/L
10.0 mg/L
0.0400 mg/L
0.100 mg/L
0.200 mg/L
0.200 mg/L
0.500 mg/L
0.500 mg/L
10 - 157 %Rec
10 - 169 %Rec
32.1 - 130 %Rec
45.4 - 166 %Rec
35.7 - 130 %Rec
74.7 - 145 %Rec
2 9/3/2020 9:03:00 PM
2 9/3/2020 9:03:00 PM
2 9/3/2020 9:03:00 PM
2 9/3/2020 9:03:00 PM
2 9/3/2020 9:03:00 PM
2 9/3/2020 9:03:00 PM
2 9/3/2020 9:03:00 PM
2 9/3/2020 9:03:00 PM
2 9/3/2020 9:03:00 PM
2 9/3/2020 9:03:00 PM
2 9/3/2020 9:03:00 PM
2 9/3/2020 9:03:00 PM
2 9/3/2020 9:03:00 PM
2 9/3/2020 9:03:00 PM
2 9/3/2020 9:03:00 PM
2 9/3/2020 9:03:00 PM
2 9/3/2020 9:03:00 PM
Qualifiers:
B
H
MC
ND
PL
RL
Analyte detected in the associated Method Blank
Holding times for preparation or analysis exceeded
Value is below Minimum Compound Limit.
Not Detected
Permit Limit
Reporting Detection Limit
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits
U Samples with Ca1cVal < MDL
Original
Page 6 of 32

SUMMI
£NVIRONMENTCL TECHNOL©GiFS, ii:
An. y kal Labwieorlrs
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
Website: http://www.settek.com
Analytical Report
(base report)
WO#: 20081630
Date Reported: 9/9/2020
CLIENT:
Matrix:
Lab ID:
Project:
Synagro
SLUDGE
20081630-001A
NRWASA
Client Sample ID NRWASA
Tag Number:
Collection Date: 8/26/2020 11:00:00 AM
Analyses Result
RL Qual Units
DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8081
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total
Toxaphene
Endrin
gamma-BHC
Heptachlor
Heptachlor epoxide
Methoxychlor
Surr: TCMX
Surr: DCB
TCLP HERBICIDES BY EPA 8321E
2,4-D
2,4,5-TP
Surr: 2,4-Dichlorophenylacetic aci
ND
ND
ND
ND
ND
ND
ND
73.7
82.1
ND
ND
105
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
1,2-Dichloroethane
MEK
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
93.0
90.3
98.2
0.125 mg/L
0.250 mg/L
0.0125 mg/L
0.0125 mg/L
0.0125 mg/L
0.0125 mg/L
0.0125 mg/L
10 - 119 %Rec
10 - 119 %Rec
0.500
0.500
70 - 130
SW3510C Analyst: MES
5 9/4/2020 11:38:00 PM
5 9/4/2020 11:38:00 PM
5 9/4/2020 11:38:00 PM
5 9/4/2020 11:38:00 PM
5 9/4/2020 11:38:00 PM
5 9/4/2020 11:38:00 PM
5 9/4/2020 11:38:00 PM
5 9/4/2020 11:38:00 PM
5 9/4/2020 11:38:00 PM
SW8321A SW1311M Analyst: BJH
mg/L
mg/L
%Rec
50 9/3/2020 10:39:00 PM
50 9/3/2020 10:39:00 PM
50 9/3/2020 10:39:00 PM
SW8260 SW1311 M Analyst: RMT
0.250 mg/L
0.250 mg/L
5.00 mg/L
0.250 mg/L
0.250 mg/L
2.50 mg/L
0.250 mg/L
0.250 mg/L
0.250 mg/L
0.100 mg/L
70 - 130 %Rec
70 - 130 %Rec
70 - 130 %Rec
50 9/4/2020 11:16:00 AM
50 9/4/2020 11:16:00 AM
50 9/4/2020 11:16:00 AM
50 9/4/2020 11:16:00 AM
50 9/4/2020 11:16:00 AM
50 9/4/2020 11:16:00 AM
50 9/4/2020 11:16:00 AM
50 9/4/2020 11:16:00 AM
50 9/4/2020 11:16:00 AM
50 9/4/2020 11:16:00 AM
50 9/4/2020 11:16:00 AM
50 9/4/2020 11:16:00 AM
50 9/4/2020 11:16:00 AM
Qualifiers:
B
H
MC
ND
PL
RL
Analyte detected in the associated Method Blank
Holding times for preparation or analysis exceeded
Value is below Minimum Compound Limit.
Not Detected
Permit Limit
Reporting Detection Limit
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits
U Samples with CalcVal < MDL
Original
Page 7 of 32

SuMMI
ENVIRONMENTAL TECHNOLOGIES, th.t'
AnalyNCat L abofaoofMs
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
Website: http://www.settek.com
Analytical Report
(base report)
WO#: 20081630
Date Reported: 9/9/2020
CLIENT: Synagro
Matrix: SLUDGE
Lab ID: 20081630-001A
Project: NRWASA
Client Sample ID NRWASA
Tag Number:
Collection Date: 8/26/2020 11:00:00 AM
Analyses
Result RL Qual Units
DF Date Analyzed
RCI
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive
IGNITABILITY OF SOLIDS (SW-846: 1030)
SW9014
ND 0.490 mg/Kg
SW1030
Ignitability <2.2 mm/sec
NOTES:
does not propagate
PERCENT SOLIDS BY SM2540MOD
Percent Solids
RCI
PH (SW9045D)
pH
RCI
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive
1
1
Analyst: MS
9/2/2020 12:54:00 PM
Analyst: AJT
8/31/2020 2:00:00 PM
A2540B Analyst: DHC
3.12 % 1 9/3/2020 4:50:00 PM
SW9045D Analyst: VVK
6.6
s.u.@20.6C 1 8/28/2020 12:37:32 PM
SW9034 Analyst: MS
70.0 25.0 mg/Kg 1 9/3/2020 12:54:00 PM
Qualifiers:
B
H
MC
ND
PL
RL
Analyte detected in the associated Method Blank
Holding times for preparation or analysis exceeded
Value is below Minimum Compound Limit.
Not Detected
Permit Limit
Reporting Detection Limit
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits
U Samples with CalcVal < MDL
Original
Page 8 of 32

i,
SuMMI1
ENVIRONMENTAL TECHNOL0c ES, +N
Analytical Laboratarlrc
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
Website: http://www.settek.com
Accreditation Program
Analytes Report
WO#: 20081630
09-Sep-20
Client: Synagro
Project: NRWASA
State: NW
Program Name: NC WW SCM
Sample ID
Matrix
Test Name
Analyte Status
20081630-001A
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Ignitability of Solids (SW-846: 1030)
Percent Solids by SM2540Mod
pH (SW9045D)
Reactive Cyanide (9014/7.3.3.21-Solid
Reactive Sulfide (9034)/7.3.4.2
TCLP Herbicides by EPA 8321B
TCLP Herbicides by EPA 8321B
TCLP Mercury Analysis (SW1311/7470)
TCLP Metals Analysis (SW1311/6010)
TCLP Metals Analysis (SW1311/6010)
TCLP Metals Analysis (SW1311/6010)
TCLP Metals Analysis (SW1311/6010)
TCLP Metals Analysis (SW1311/6010)
TCLP Metals Analysis (SW1311/6010)
TCLP Metals Analysis (SW1311/6010)
TCLP Pesticides Analysis (SW1311/8081)
TCLP Pesticides Analysis (SW1311/8081)
TCLP Pesticides Analysis (SW1311/8081)
TCLP Pesticides Analysis (SW1311/8081)
TCLP Pesticides Analysis (SW13I1/8081)
TCLP Pesticides Analysis (SW1311/8081)
TCLP Pesticides Analysis (SW1311/8081)
TCLP Semi-Volatiles Analysis (SW1311/8270)
TCLP Semi-Volatiles Analysis (SW1311/8270)
TCLP Semi-Volatiles Analysis (SW1311/8270)
TCLP Semi-Volatiles Analysis (SW1311/8270)
TCLP Semi-Volatiles Analysis (SW1311/8270)
TCLP Semi-Volatiles Analysis (SW1311/8270)
TCLP Semi-Volatiles Analysis (SW1311/8270)
TCLP Semi-Volatiles Analysis (SW1311/8270)
TCLP Semi-Volatiles Analysis (SW1311/8270)
TCLP Semi-Volatiles Analysis (SW1311/8270)
Ignitability
Percent Solids
Hydrogen Ion (pH)
Cyanide, Reactive
Sulfide, Reactive
2,4,5-TP
2,4-D
Mercury
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Chlordane, total
Endrin
gamma-BHC
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
1,4-Dichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dinitrotoluene
Cresols, Total
Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
A
A
Key
NC WW SCM A Accredited
Key
NC WW SCM N Not Accredited
Key
NC WW SCM U Unavailabl
Original #1
Page 9 of 32

Summit Environmental Technologies, Inc.
3310 Win St.
ENVIROHMENTAI. TECHNOLOGIE$, attC Cuyahoga Falls, Ohio 44223
Analytical( Laboraro•res TEL: [phone] FAX: [phone]
Website: http://www.settek.com
SUMMI
Accreditation Program
Analytes Report
WO#: 20081630
09-Sep-20
Client: Synagro
Project: NRWASA
State: NW
Program Name: NC_WW_SCM
Sample ID
Matrix
Test Name
Analyte Status
20081630-001A
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
TCLP Volatiles Analysis
TCLP Volatiles Analysis
TCLP Volatiles Analysis
TCLP Volatiles Analysis
TCLP Volatiles Analysis
TCLP Volatiles Analysis
TCLP Volatiles Analysis
TCLP Volatiles Analysis
TCLP Volatiles Analysis
TCLP Volatiles Analysis
Pyridine
1,1-Dichloroethene
1,2-Dichloroethane
2-Butanone
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chloride
A
A
A
A
A
A
A
A
A
A
A
Key
NC_WW_SCM A Accredited
Key
NC WW SCM N Not Accredited
Key
NC_WW_SCM U Unavailabl
Original #1
Page 10 of 32

Summit Environmental Technologies, Inc.
0
E
Nf o
in 10• 00
e.• CTS
N 0
cc
Z
cc cn
TCLP-VOC-M
SampType: MBLK
Sample ID: MB-45155
Ana
Batch ID: 45155
RPD Ref Val
SPK Ref Val
I)
76
0
c
J
0
a
m
CC
CO CO m
o o o
d' V N
tl) 0) 0)
0) w rn
0 0 O
0 0 0 0 0 0 0 0 0 0
0 0 0 0 0 0 0 0 0 0
0 0' 0 0 0 111 0 0 0 0
0 0 0 0 0 0 0 0 0 0
O O O O 0 O 0 0
O D O 0 0 0 0 0 0 0 t� co
Z Z Z Z Z Z Z Z Z Z t et et oi
1,1-Dichloroethene
1,2-Dichloroethane
c
N
m
Carbon tetrachloride
Chlorobenzene
0
O
O
0
Tetrachloroethene
Trichloroethene
a)
a
c
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
z
•
W � w
a
Spike Recovery outside accepted reco
Reporting Detection Limit
RPD outside accepted recovery limits
Page 11 of 32

0
W
CY
Summit Environmental Technologies, Inc.
\1I
CO
Q:
"
v a;
m
0
E
J
0
d
a.
RPD Ref Val
N N E
0) ▪ 4.
asL
o)
ca
O 0
o. to E
a)) .N
a
0
J
TestCode: TCLP-SVOC_ Units: mg/L
Ana
TestNo: SW8270
Batch ID: 45168
U
w
SPK Ref Val
J
0
a
N
CL
co
re
0 a)
CIS
C
U Q
2
a
E
• N O N N CO N r LC) V N CO 0 CO CO CO V'
N lf) CC) et CO C,) CC) et CO C*7 M a' CO U) CO in N
...... r r r r !- r r r r r r
N co Co IX) 6) CO M M (V et M n r` 0) (M et Co
Lci O r- (fl N. in et N r. o ^ O r et
coN N N Cf) r et7 o) N N N LO
CO. Tr. of O co. O N COO O N r, CT O Cn r` Caof o er CO (D r - o r` co r• (o Lci .= o
to co C%) 0) N r` (O CC) N CA et (o (o (o co N
0 0 0 0 O 0 0 0 0 0 CO 0
000000000000000000
0 0 0 0 0 0 0 0 0 O O O O 0 0 O 0 O
0 0 0 0 0 (0 0 O O 0 O O O O O O O O
N cc:O O (o M CD co. a0 M of r-
O o 0 o O O O O O o
O 0 0 0 O O 0 0 O O CDO
N • to CC) Or i0 et 0 N N ) Lt.)0 0 0 0 0 0 o O O o 0
et ▪ N Co NLC) Z d- co .cr. CO N. Z CO O CD CO On
O 0 0 0 O O o o O 0 o 0 0
1,4-Dichlorobenzene
La)
c
0 0
0 0
U U
co
Cb 0
Nr v Q
N N (V o
Cresols, Total
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
Nitrobenzene
x
Value above quantitation range
•
01)
U
� a
Manual Integration used to determine area response
Second column confirmation exceeds
w � a
Vi
w
d
Spike Recovery outside accepted reco
(n
Reporting Detection Limit
RPD outside accepted recovery limits
Page 12 of 32

co co
m
rti
d,
N p0
Summit Environmental Technologies, Inc.
3310 Win St.
Rt
RunNo: 117450
TestCode: TCLP-SVOC Units: mg/L
Sample ID: 20081630-001AMSD SampType: MSD
SeqNo: 2958628
Analysis Date:
TestNo: SW8270
Batch ID: 45168
To
0
J
0
a
0
a
HighLimit RPD Ref Val
E
J
0
SPK value SPK Ref Val
J
0
0
CD 0 0 0 0 0 0 0 0 0 0 0
C') c') CO C•) M C+) 0) 0) 0) 0) 0) 0)
O ti CNO 0, N 0 c0 Co CA co 0 0 0 0 0 0 0
c4 r cfl r ri cNi ui
0
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✓ - cco N. L v 0 v m ti
0 o o 0 0 0 o o O o
N 0 7N N CO N C() N CO O CD CO CO V'
N O Cn M C'0) CC) eh C0) M C0 d. �h CO Lt) CO Cn CA
N CD CO CO 6) CO CO CO N d' (") t` O) (+) V CO
ui oo N O CO N cri in 7 N V co N- N N
LO
C() N- N O 0 00 0 �t O ti N N Co O CO O Co 00
co Cn I� O V' d o-i O to O O O M CO O o
co co CO r` ti O Ls) co N Co CO CO co ti
O 0 0 0 O 0 0 O O 0 0 0
O 0 0 0 0 0 0 0 0 O 0 0 0 0 0 0 0 0
0 o O 0 0 O 0 O O O 0 0 0 0 O O O 0
O O 0 0 O O 0 0 0 0 0 0 0 0 0 0 0 O
CO CO CO CO CO ' CO CO CO CO CO CO
O O O O O 0 O o 0 0 0
O 0 0 0 0 0 0 0 0 0 0 0
0 0 O O O 0 0 0 O O O O
N Cn LO Cn .7 N N Cn CC)
O 0 0 0 0 0 0 0 0 0
0
CO f` M 0) 0 •cr N O CO Co 0 CD 0 CO 0 CO 00
"tY COO 0 co z CLO c LD Z CMO. COO, COO, CO
o 0 0 0 0 O O O O O O O O O O
1,4-Dichlorobenzene
Cresols, Total
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
Nitrobenzene
Holding times for preparation
•
0
0
0
0
,a0
Permit Limit
Second column confirmation exceeds
w � a
y
a
d
Spike Recovery outside accepted reco
Reporting Detection Limit
x
Page 13 of 32

CZ ttb
EN en
g &
0I 00
AN O
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c4
c)
a
Summit Environmental Technologies, Inc.
0
3-4
0
Z
0
CC
c3
0 0
a U E
2 3
O.o
SeqNo: 2955952
0
E
J
0
0
C.
RPD Ref Val
TestCode: SVOC-BNA T Units: mg/L
SampType: MBLK
Sample ID: MB-45168
Ana
0
1
TestNo: SW8270
Batch ID: 45168
U
W
SPK value SPK Ref Val
J
0
0) 0) O 0 N. (0
O O N N
O O 0) 0) N
co O O co N
� co co 0) n
O 0 0 O 0 0
O 0 O 0 O 0
O O O O O O
O 0 0 0 O O 0 O O 0 O O
0 LO LO 0 U) 0 0 0 0 0 L0 L()
N N (0 N N( N N
0 0 co 0 0 0 0 0 0 0 0
0 cl0 0 0 0 0 0 0 0 0 0 M O O) M N
ZZZZZZZZZZZZ
6.000.
1,4-Dichlorobenzene
2,4-Dinitrotoluene
0
0
Cresols, Total
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachtoroethane
Nitrobenzene
0
c
0
t
0_
O
0
Lr
N
t
)
Surr: Phenol-d6
Surr: Nitrobenzene-d5
Surr: 2,4,6-Tribromophenol
Surr: 2-Fluorobiphenyl
Surr: p-Terphenyl-d14
0
0
0
0
0.
5
C
0
0
en
0
Spike Recovery outside accepted reco
Reporting Detection Limit
RPD outside accepted recovery limits
Page 14 of 32

00
cro
Summit Environmental Technologies, Inc.
co
h
O
TestCode: SVOC-BNA T Units: mg/L
SampType: LCS
Sample ID: LCS-45168
SeqNo: 2955953
Analysis Date:
TestNo: SW8270
Batch ID: 45168
76
0
E
J
0
a
a.
cC
0
cc
0
SPK Ref Val
d
76
a
CO
CD
MMMMM CO 0MCOCO 0M 0 CD MCO M M CO CO CO CO 00 CO CO
Cr r` .- co co n It .- Cc) Cn Cr 0 — O CO CO W et;
M c
M M M V-M M M V M M ' M
co co N- O U) .- ti N '0 CC) Cr h (A r` N N CD '0
N M h: r` M tf) r` M O O c O to N w' l() c0
c co co rn O CO c CO c 10 co CO c u) c CO u) h
0 0 0 0 0 0 0 0 0 0 0 0
O O O O 0 O (0 O O 0 O O 0 0 0 0 0 0
0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
O O O O O CO O 0 0 0 0 0 0 0 0 0 0 0
CO CO CO CO CO 00 CO CO CO CO CO
O 0 0 0 0 0 0 0 0 o
O o 0 0 0 0 0 0 0 0 0 0
NN M N O O O O O O N N
O O O O O O O O O O
c0 0) CO CO 0 N u) N N '0 O) 0) h N (0 Cp t!)
M CO O I� O z 00 CO r` '0 h 0 '0 N [D CO In CO
M CO h n t[) M (O M Cr O M Cf In CY O to
O O C7 O O O C C O C O O O O O O O
1,4-Dichlorobenzene
2,4-Dinitrotoluene
y
0
Cresols, Total
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
Nitrobenzene
0
xpy
a
Value above quantitation range
a
Second column confirmation exceeds
Spike Recovery outside accepted reco
Reporting Detection Limit
Page 15 of 32

i4l
o
Ai N p
F
Summit Environrnental Technologies, Inc.
0 0
N N
N N
M d'
O) O)
SampType: MBLK
Sample ID: MB-45175
Analysis Date:
Batch ID: 45175
Client ID: PBS
RPD Ref Val
E
J
2
E
- J
U
z
SPK value SPK Ref Val
'�5,
[ti
Q
O 0 0 0 0 0 0
t0000000 () L
N tC)
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O
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✓ N
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00
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N
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❑
N
d
TestCode: MtI-TCLP-7(6 Units: mg/L
SampType: LCS
Sample ID: LCS-45175
Analysis Date:
TestNo: SW6010D
Batch ID: 45175
0
J
HighLimit RPD Ref Val
E
0
cc
SPK Ref Val
O O 0 0 0 0 0
N'- N- NNN
r N
O O 0 0 0 0 0
CO OD CO CO CO CO CO
0 0 0 0 0 0 0
o 0 0 0 0 0 0
O O O O O O O
O O O o O O o
N N N N N N
0 0 0 0 0 0 0
o O 0r N 0 0 t0
O O O O O°
O
O ❑ co co O coO
N Z N N N N N
0
44
B Analyte detected in the associated Method Blank
a)
a
ND Not Detected
Spike Recovery outside accepted reco
Reporting Detection Limit
RPD outside accepted recovery limits
c4
Page 16 of 32

Summit Environmental Technologies, Inc.
0
fl(U
.01
ea
RunNo: 117398
TestCode: Mtl-TCLP-7(6
SampType: MS
Sample ID: 20081710-001AMS
SegNo: 2956656
Analysis Date:
TestNo: SW6010D
Batch ID: 45175
0
E
J
O
a
cC
a
HighLimit RPD Ref Val
E
J
0
J
0
SPK Ref Val
C)
Trs
d
J
0
3-
0000000
M r r CO r a)r r r
0 0 0 O O O O
h r N- r n
cp I-- M r CV
1- a) d• O tf)
ca co a) a) 0
CO0 CO m CO CO
7 0 0 0 0
O O O O
O O 0
O O O O O O O
0 0 0 0 0 O 0
O O O O O 0 O
N N N N N N
0000000
0 0 o 0u07, 0 Lt.)O id O o O O o
O
a) Z CO CO 0 r O
r r r r CV cV
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c▪ o
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a a a a a 3- a
J J J J J J J
I-'- F- I- I- F- F- F-
RunNo: 117398
SegNo: 2956659
O 0
M d'
CA O)
ai
❑
J
E
TestCode: MtI-TCLP-7(6
Analysis Date:
O
M
y
TestNo: SW6010D
Batch ID: 45175
0
E
J
d
a
atz
SPK Ref Val
d
3)
J
0
a
O 000000
NNNNNNN
CNI 0 COO 0 7r CO LOO
I- Ca CO r rl ti
0 0 0 0 0
O 0) Nr to Co al
O W 00 O O ON
r r r r (V cV
0 0 0 0 0 0 0
CO M CO CO CO CO CO
0000000
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O Co co a) to O
0) co a) Co Co
O M - ( 0 c- 00)
a! a) 0_ r
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O O O
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00 0 0 0 0 0
0000000
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0
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r r r r CV N
TCLP Silver(Ag)
Value above quantitation range
0'
00
Manual Integration used to determine area response
Second column confirmation exceeds
ND Not Detected
Spike Recovery outside accepted reco
Reporting Detection Limit
RPD outside accepted recovery limits
Page 17 of 32

er
AtA
d
o
6.0
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0 N
N N
M et
a)
c0
0
N
TestCode: Mtl-TCLP-7(6
Sample ID: TCLP BLANK 9-3-20 SameType: MBLK
Analysis Date:
TestNo: SW6010D
Batch ID: 45175
HighLimit RPD Ref Val
E
J
O
J
0
W
SPK value SPK Ref Val
J
0
d
CC
O 00 O O 0 0
10 O N 1 10 Lg.
C 0 0 0 � 0
O
0 0 0 0 0 0 0
ZZZZZZZ
TCLP Arsenic(As)
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
0
Permit Limit
ND Not Detected
Spike Recovery outside accepted reco
Reporting Detection Limit
R RPD outside accepted recovery limits
Page 18 of 32

Summit Environmental Technologies, Inc.
0 0
N N
0) 0)
m
a7
0
N
0
Units: PPM
ti
a
J
co
2
0
0
0
F a
Analysis Date:
m
0
LowLimit HighLimit RPD Ref Val
U
w
cc
SampType: MBLK
Sample ID: MB-45177
Batch ID: 45177
SPK value SPK Ref Val
0)
cc
a
a)
00i 0
U Q
0
O
0
O
0
z
TCLP Mercury
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0
O O~f CC
n CO
a
z z o
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Cn
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N N
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a)
CO
0
n
0
TestCode: HG_TCLP(74
SampType: LCS
Sample ID: LCS-45177
Analysis Date:
TestNo: SW7470A
Batch ID: 45177
LowLimit HighLimit RPD Ref Val
SPK value SPK Ref Val
J
0
d
7
0)
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O
O
Ci
O
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f0
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d
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Sample ID: TCLP BLANK 9-3-20 SampType: MBLK
Analysis Date:
TestNo: SW7470A
Batch ID: 45177
0
%RPD RPDLimit
LowLimit HighLimit RPD Ref Val
U
w
Et
SPK Ref Val
7
[0
a
a
a
O
O
O
0
0
z
TCLP Mercury
RunNo: 117406
TestCode: HG_TCLP(74
SampType: MS
Sample ID: 20081640-001AMS
W
0
en
0
z
0
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TestNo: SW7470A
Batch ID: 45177
%RPD RPDLimit
RPD Ref Val
0
w
cc
SPK value SPK Ref Val
J
0
a
2
0
co
1
0
N
O
O
O
0
0
0
O
0
0
0
0
z
TCLP Mercury
B Analyte detected in the associated Method Blank
w
J Analyte detected below quantitation limits
0
Permit Limit
Second column confirmation exceeds
ND Not Detected
Spike Recovery outside accepted reco
Reporting Detection Limit
R RPD outside accepted recovery limits
Page 19 of 32

A/ M N
CIO) F0
00
tol
AA O
F�1 N O
N O
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N
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0
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0 0
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N N
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aa_
01 61 L
o
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hi i 4) N
O.o
SampType: MS
Sample ID: 20081640-001AMS
Ana
TestNo: SW7470A
Batch ID: 45177
RPD Ref Val
0
W
SPK Ref Val
d
J
a
a
U
TO
0
E
J
0
co a'
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a
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0 •y 3
a T
0
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TestCode: HG_TCLP(74 Units: PPM
Ana
TestNo: SW7470A
Batch ID: 45177
RPD Ref Val
U
W
SPK Ref Val
N
7
>
a
J
Cr
0-
a)
CC
Cn
CC
O
N
O
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0
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O
O
O
O
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0
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TCLP Mercury
7
0
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toco CO CL
0
eh 0
N d
Z Z
N N
N N
0
TestCode: HG_TCLP(74 Units: PPM
SampType: MBLK
Sample ID: MB2-45177
Analysis Date:
TestNo: SW7470A
Batch ID: 45177
HighLimit RPD Ref Val
E
0 0
J
U
SPK value SPK Ref Val
J
0
a
N
d)
Cr
0
N
O
O
O
0
TCLP Mercury
a
0
xUa
Second column confirmation exceeds
w
0)
a
a
ND Not Detected
Spike Recovery outside accepted reco
Reporting Detection Limit
RPD outside accepted recovery limits
a
Page 20 of 32

0
A4
C4
TestCode: pH_OiI(9045D Units: s.u.@21.0C
0
0 _
N
N
CO
as
❑ ❑
Q
3
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U
w
CC
Ana
TestNo: SW9045D
Batch ID: R117088
0
a
V
m
RPD Ref Val
SPK value SPK Ref Val
J
ci
N
CC
0
co
_
m
0
E
J
c ❑
or. o
e.
N 0
CL
z z
cr
CC co
TestCode: pH_Oil(9045D Units: s.u.@21.3C
Ana
TestNo: SW9045D
Batch ID: R117088
RPD Ref Val
SPK value SPK Ref Val
-J
0
a
0
Co
csi
_
n
0
Second column confirmation exceeds
W P,
B Analyte detected in the associated Method Blank
sue',
0
a
ND Not Detected
Spike Recovery outside accepted reco
Cel
Reporting Detection Limit
Ri
RPD outside accepted recovery limits
c4
Page 21 of 32

N
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tal Technologies, Inc.
coo
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a.
d
TestCode: pH_NPW(450 Units: s.u.@21.3C
SampType: LCS
Sample ID: LCS-R117088
Analysis Date: 8/28/2020
TestNo: SW9045D
Batch ID: R117088
RPD Ref Val
E
0)
2
E
J
0
w
SPK value SPK Ref Val
J
0
a
co
0)
0
0
a
O
_
0
0
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f N
z z
• 0-
cn
d)
N
❑
a
TestCode: pH_NPW(450 Units: s.u.@21.8C
SampType: LCS
Sample ID: CHECK 7
Analysis Date: 8/28/2020
TestNo: SW9045D
Batch ID: R117088
m
a
cb
J
a
0
CC
RPD Ref Val
E
J
2
E
J
0
J
0
w
SPK value SPK Ref Val
0)
0
a
0
a
E
0
coo o CC
a)
• N d
w
z z o
a cr
0
a
a
m
a
N
TestCode: pH_NPW(450 Unit
SampType: LCS
Sample ID: CHECK 7
0
0
CO
CO
CO
Analysis Date:
TestNo: SW9045D
Batch ID: R117088
HighLimit RPD Ref Val
E
3
J
0
w
SPK value SPK Ref Val
y
G)
0)
2
a
0)
.5
0
0
0
0
0
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ati
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ation exceeds
Second column
ND Not Detected
Spike Recovery outside accepted reco
Reporting Detection Limit
R RPD outside accepted recovery limits
Page 22 of 32

0
Vl
Summit Environmental Technologies, Inc.
RIM
GO
r
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C4
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CO
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e- N
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E
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TestCode: Ignitability_S Units:
SampType: LCS
Sample ID: LCS-R117185
TestNo: SW1030
Batch ID: R117185
Tp
0
E
J
0
a
0
CL
HighLimit RPD Ref Val
0
W
SPK Ref Val
a)
J
cc
0
O
N
O
N
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r
N
N
z Q
w
a)
0
TestCode: Ignitability_S Units: mm/sec
Sample ID: 20081572A01ADUP SampType: DUP
M
CO
Analysis Date:
TestNo: SW1030
Batch ID: R117185
0
V
is
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E
J
0
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0
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W
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0
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O
V
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Cn
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V
N
E
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CO
Analysis Date:
TestNo: SW1030
Batch ID: R117185
0
W
SPK value SPK Ref Val
J
0
a
0
a
ro
N
U ▪ <
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O
Csi
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0
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Second column
Spike Recovery outside accepted reco
O
Reporting Dete
Page 23 of 32

TestCode: IgnitabilityS Units: mm/sec
SeqNo: 2944142
Analysis Date: 8/31/2020
TestNo: SW1030
Batch ID: R117185
0
E
J
0
a
RPD Ref Val
SPKRef Val
d)
a
V)
J
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O
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O
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VI
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x
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Page 24 of 32

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SampType: MBLK
Sample ID: Blank
Analysis Date: 9/2/2020
TestNo: SW9014
Batch ID: R117333
To
0
HighLimit RPD Ref Val
E
3
0
J
0
W
SPK Ref Val
N
Tr
d
J
0
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RunNo: 117333
E
C
TestCode: Cyanide,Rea
SampType: LCS
Sample ID: LCS
SeqNo: 2952983
N
Analysis Date:
TestNo: SW9014
Batch ID: R117333
cTs
0
E
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LowLimit HighLimit RPD Ref Val
U
ce
SPK Ref Val
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0
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SampType: RLC
Sample ID: RLCheck
Analysis Date: 9/2/2020
TestNo: SW9014
Batch ID: R117333
HighLimit RPD Ref Val
E
J
U
W
SPK Ref Val
O
O
O
O
N
0
Cyanide, Reactive
3
0
E
0
co co 11
M N
r 0
a
z z
cc 5
TestCode: Cyanide,Rea
SampType: MS
Sample ID: 20081541-001AMS
Analysis Date: 9/2/2020
TestNo: SW9014
Batch ID: R117333
HighLimit RPD Ref Val
E
0
-J
0
W
SPK Ref Val
a)
To
0_
-J
a
O
O
O
Cyanide, Reactive
O
0
0
0
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0
ation exceeds
Second column con
ND Not Detected
Spike Recovery outside accepted reco
Reporting Detection Limit
R RPD outside accepted recovery limits
Page 25 of 32

\ 1
k k
d
TestCode: Cyanide,Rea
SampType: MS
Sample ID: 20081541-001AMS
TestNo: SW9014
Batch ID: R117333
HighLimit RPD Ref Val
SPK Ref Val
\
\
/
k
■
\
TestCode: Cyanide,Rea
Analysis Date: 9/2/2020
TestNo: SW9014
RPD Ref Val
SPK Ref Val
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j
%
§
a.
0
\
§
0
0
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N.
a
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\
Ot
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P
Spike Recovery outside accepted reco
Reporting Detection Limit
RPD outside accepted recovery limits
Page 26 of 32

it Environmental Technologies, Inc.
r-
at
as
Z
TestCode: Sulfide,React Units: mg/Kg
SampType: MBLK
Sample ID: MB-R117334
Analysis Date:
TestNo: SW9034
0
W
0
52
SPK Ref Val
7,3
a
J
0
d
0
Z
Sulfide, Reactive
a
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J
nr 0
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N
0
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TestCode: Sulfide,React Units:
SampType: LCS
Sample ID: LCS-R117334
Analysis Date:
TestNo: SW9034
Batch ID: R117334
LowLimit HighLimit RPD Ref Val
0
ce
SPK Ref Val
N
N
co
W
0
b
M
0
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N
Sulfide, Reactive
(6
0
0.
a
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TestCode: Sulfide,React Units:
0
N
N
Of
Analysis Date:
TestNo: SW9034
3
0
E
J
0
CC
0
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HighLimit RPD Ref Val
E
0
J
0
W
SPK Ref Val
0
N
O
N
M
Sulfide, Reactive
0_
0
SampType: MSD
Sample ID: 20081541-001AMSD
Analysis Date: 9/3/2020
HighLimit RPD Ref Val
E
3
0
W
SPK value SPK Ref Val
O
M
0
CO
O
0
M
Sulfide, Reactive
7
a
z
0
Permit Limit
Spike Recovery outside accepted reco
Reporting Detection Limit
Page 27 of 32

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ation exceeds
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Page 28 of 32

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TestCode: PctSoiid_S(2 Units: %
Sample ID: MB-R117416
SeqNo: 2957316
0
01
Analysis Date:
TestNo: A2540B
Batch ID: R117416
0
0
J
d
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❑
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SPK Ref Val
En
CC
❑
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ca
a
TestCode: PctSolid_S(2 Units:
SeqNo: 2957319
0
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Analysis Date:
TestNo: A2540B
Batch ID: R117416
m
E
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LowLimit Highlimit RPD Ref Val
U
W
SPK Ref Val
7
cc
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m
v
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Percent Solids
B Analyte detected in the associated Method Blank
0
a
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ro
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Reporting Detection Limit
Page 29 of 32

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Page 30 of 32

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SUMMI
EM intNMENTAL TECHNOLOGIES.
Analytical Laboratories
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX• [phone]
Website: http://www.settek.com
Sample Log -In Check List
Client Name: SYN-NC-27028
Work Order Number: 20081630
RcptNo: 1
Logged by: Jennifer C. Richards 8/27/2020
Completed By: Jennifer C. Richards 8128/2020 12:12:51 PM
Reviewed By: Sara E. Kidd 8/28/2020 2:29:02 PM
Chain of Custody
1, Is Chain of Custody complete? Yes El
2. How was the sample delivered? FedEx
No ❑ Not Present ❑
Log In
3. Coolers are present? Yes No ❑ NA ❑
4. Shipping container/cooler in good condition? Yes
Custody seals intact on shipping container/cooler? Yes ❑
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes 0
6. Were all samples received at a temperature of >0° C to 6.0°C
No ❑
No ❑
No ❑
Yes ❑J No ❑
7. Sample(s) in proper container(s)? Yes 0 No ❑
8. Sufficient sample volume for indicated test(s)? Yes No ❑
9. Are samples (except VOA and ONG) properly preserved? Yes 0 No ❑
10. Was preservative added to bottles? Yes ❑ No ❑d
Not Present 0
NA ❑
NA ❑
NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm? Yes ❑ No ❑ No VOA Vials 0
12. Were any sample containers received broken? Yes ❑ No 0
13. Does paperwork match bottle labels? Yes ❑d No ❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody? Yes El No ❑
15. Is it clear what analyses were requested? Yes 0 No ❑
16. Were all holding times able to be met? Yes 0 No ❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes ❑
No ❑ NA 0
Person Notified:
By Whom:
Regarding:
Client Instructions:
Date: I -
Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
18, Additional remarks:
Cooler Information
Cooler No
Temp °C
Condition
Seal Intact
Seal No
Seal Date
Signed By
1
1.4
Good
Not Present
Page 32 of 32

aceAnalytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Chris Wynne
Project Name: NRWASA
Lot Number:VH27084
Date Completed:09/10/2020
09/10/2020 2:16 PM
Approved and released by:
Project Manager II: Lucas Odom
NUB
ANSI NaBanal Accreditation Board
ACCREDITED
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: VH27084
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance
Management Plan (QAMP), standard operating procedures (SOPs), and Pace policies. Any exceptions to
the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 2 of 7

Client: Synagro
Description: NRWASA
Date Sampled:08/26/2020 1100
Date Received:08/27/2020
Laboratory ID: VH27084-001
Matrix: Solid
% Solids: 2.19 08/28/2020 0132
Inorganic non-metals
Run
1
1
1
1
1
1
1
Prep Method
350.1
351.4
Analytical Method
(% Solids) SM 2540G
(Ammonia - N ) 350.1
(Nitrate - N ) 9056A
(Nitrite - N ) 9056A
(Phosphorus) 365.1
(Soil pH meas) 9045D
(TKN) 351.2
Dilution
1
1
1
1
2
1
1
Analysis Date Analyst
08/28/2020 0132 MOM
09/01/20201146 DMA
09/02/20201703 AMR
09/02/20201703 AMR
09/02/20201306 DMA
09/02/2020 2316 SRB
09/02/20201614 DMA
Prep Date Batch
64970
65272
65639
65640
09/02/2020 0857 65438
65557
09/02/2020 1023 65445
Parameter
Solids
Ammonia - N (gas diffusion)
Nitrate - N (soluble)
Nitrite - N (soluble)
Phosphorus
Soil pH measured in water @ 22.2 ° C
TKN
CAS
Number
Analytical
Method Result Q LOQ DL
SM 2540G 2.19
350.1 940 46 24
9056A 28 23 4.6
9056A 5.4 J 9.2 4.6
7723-14-0 365.1 2800 460 92
9045D 6.2
351.2 13000 1100 1100
CVAA
Units Run
1
mg/kg 1
mg/kg 1
mg/kg 1
mg/kg 1
su 1
mg/kg 1
Run Prep Method
1 7471B
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
7471B 1 09/04/2020 1608 JAB2 09/04/2020 0655 65431
Parameter
Mercury
CAS
Number
7439-97-6
Analytical
Method
7471B
ICP-AES
Result Q LOQ DL
ND 3.5 0.85
Units Run
mg/kg 1
Run Prep Method
1 3050B
2 3050B
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
6010D 1 09/04/2020 0509 KSH2 09/02/2020 1621 65429
6010D 1 09/10/2020 0334 KSH2 09/02/2020 1621 65429
Parameter
CAS
Number
Analytical
Method Result Q LOQ DL Units Run
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
7429-90-5
7440-38-2
7440-43-9
7440-70-2
7440-47-3
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-98-7
6010D 180000 810 300 mg/kg 1
6010D 10 J 30 10 mg/kg 1
6010D ND 10 2.5 mg/kg 1
6010D 2400 J 10000 1300 mg/kg 1
6010D 30 20 5.1 mg/kg 1
6010D 180 20 9.1 mg/kg 1
6010D 49000 200 92 mg/kg 2
6010D 19 J 20 9.1 mg/kg 1
6010D ND 10000 1300 mg/kg 2
6010D 1400 30 12 mg/kg 1
6010D ND 81 20 mg/kg 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40°% J = Estimated result < LOO and > DL
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client: Synagro Laboratory ID: VH27084-001
Description: NRWASA Matrix: Solid
Date Sampled:08/26/2020 1100 % Solids: 2.19 08/28/2020 0132
Date Received:08/27/2020
ICP-AES
Run Prep Method
1 3050B
2 3050B
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
6010D 1 09/04/2020 0509 KSH2 09/02/2020 1621 65429
6010D 1 09/10/2020 0334 KSH2 09/02/2020 1621 65429
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Nickel
Potassium
Selenium
Sodium
Zinc
7440-02-0 6010D ND 81 21 mg/kg 1
7440-09-7 6010D 2100 J 10000 1300 mg/kg 2
7782-49-2 6010D ND 40 16 mg/kg 1
7440-23-5 6010D 1900 J 10000 1300 mg/kg 1
7440-66-6 6010D 100 100 25 mg/kg 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40"/ J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
irs
Chain of CUS
EinP14.1a1.4
e lat. liP.1
e
4
a
tO
t"g
DEitz 06-27-2012
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
Strad} F.nvirrememi scviccs. tnc.
Uucuncrt Number:14ZODAC-I4
Iteett_ Syaugro
Yes No
Yes ■ Nu
D: NA Chlorine Strip ID_ N Tested try. INA
Sample Receipt Checklist (SRC)
Cooler Inspected hyi:lare: rs,1t; 1 Ot;e27r2OryfJ Lot;l: vr.errog4
CI I e
Q
c 'sear Pere resent, were the r itl t yye ar,d unbroken?
b rat temperature upon receipt .+ Derived (Correace) temperature upon tuceip %Solid Strap -Cup
r � I
4.ti r 4_1) c NA tNA 'C NA /NA cC NA ;NA oc
thod: VITemperntuie Blank DAgainst Bottles IR Gun ID: 5
of coolant: PI Wet Ice 0 Ice Packs ❑ Dry Ice [] None
0 Yes
Ycs
R3 Ye
D No
't, i art
Efro lien l;)ce: r; 32013
(RGor. Currnct nn FaC.oe: 4 `C
;. if temperature of any cooler exec teed 6.0°C, was Pi»iect Msnegt:r Notified"
was Notitied riv: one/ email/face-to-face (circle one).
corm/went' o' crier's packing slip attached to this form?
Were proper t:ustudy procedures (relinquished/received) ±'o;lowed?
�] No 1Z1 NA PM
No [j NA 4_ Is the
ho 6- ere sample tT)s listed on the COC?
ample lea listed an alI sample colic ncrs?
[l_ Nd all container k b
p
on the COC'?
:d on all sample
istcd on the COC?
2. Did all samples urrive in the proper cor_taErten iur each test and/or in good condition
en, lids on, etc.)?
ID No 13. Wa,, adequate sample volume avai'able'7
4, tot re at, samples received within f_• the holdinit time or 48 Iiuu, whichr comes first?
ND .5. Were any sample:, containers missing/excess (;;:rcic eti
16_ For VOA and RRK-175 samples, were Ix.ihblcs prese,a
l®• No
L.iNo
❑ Nu
DNo
iy ENo
in NA to any of the VOA vials?
NA 17. Were all Dx0?uterahlnutricnt samples re
'--'.pea-size" ('W or 6,nm in dirmeter)
d sit a pH of e: 2?
WO NA Ib. Were al! cyanideslamped ata p14:• 12 en
Were all atrp}ie cola iriT t, iTI. cy iiid
chlorine"
INA su
co
*e
L) sarrmDh s
Heat retnarkurequests (i.e. requested dilutions, MS/MSD de4igial
sed from the COC izOn the comment section in LIMS?
Ycs �No ?1. 1Vrs rite qurne mar trl3er listexl on ,he container label?
Pre9ei vatiun (Ibtast be completed for any nplo(3)cor'rectly prceeived or with heads( ce, j
Vo3x mote tr NA
umplc(s) NA were received IJlcorrcr:Ily preserved and were adjusted acconiin ,ly
in.yample receiving with NA mLofcircle one: 1-12SC)4, I•INO3, HCI, NaOH using SR li NA
Time of preservation NA Tr mom titan one preservative: is needed, please note in the comment; below_
Sartmpic(s): NA
Samples(s) NA
were received with bubbles >6 mm in d ame er.
were received anal TRC - O. nr/L Oft 19 b no) and were
cljusted ac ordingly in sample receiving with soma-n this>sul6ur (NaiS ) with Shealy ID: NA
SR. barcode lapels applied hv; BI
0So26.r2(121)
gamma
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7