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HomeMy WebLinkAboutWQ0035049_Monitoring - 03-2021_20210421 (2)Monitoring Report Submittal ............................................................................................................................................ Permit Number #* WQ0035049 Name of Facility:* Maple Hill WWTF Month:* March Year:* 2021 Report Information Type* Upload Document* NDMR, NDAR-1, NDAR-2, NDMLR March2021 NDMR NDAR1.... 1.25MB FDF Only GW-59 March2021 GroundwaterRe... 1.61 MB FDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Confirmation Email Address:* kkeel@pendercountync.gov Name of Submitter:* Kenny Keel Signature: Date of submittal: 4/21/2021 This will be filled in autocratically Initial Review Reviewer: Williams, Kendall Is the project number correct?* WQ0035049 Is the monitoring report Yes r No accepted?* Regional Office* Wilmington Accepted Date: 4/21/2021 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER ALI- Q U QUALITY MONITORING: DEPARTMENT C Co MP L COMPLIANCE OMPLIANCE FORM REPORT Fri., • •DIVISION O-FIEN I MENTA NATURAL RESOURCES OF WATER QUALITY -INFORMATION FACILITY TY FACILITY INFORMATION ILI Please Print Clearly or Type � PROCESSING UNIT 17 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 (9-19) 733-3M mPhOnO: Facility MpillWWT Facility Name: Maple Hill WWTF - Wastewater Irrigation System PERMIT Number: WQ0035049 Expiration Date: March 31, 2026 Permit Name (if different): Non -Discharge W00035049 ---------- UIC Facility Address: 306 Maple Hill School Rd NPDES Other Maple Hill 1­110 NC 612 28454-7 County Pander TYPE OF PERMITTED OPERATION ION BEING MONITORED 7 Contact -7, —r) 11 Lagoon 11 Remediation: Infiltration Gallery Person: James Proctor Telephone#: 910-259-1570 9 Spray Field El Remediation: Well Location/Site Name: MW-1 No. E3❑Rotary Distributor El Land Application of Sludge SAMPLING INF0_RMA_T1 11ON of wells to be sampled: 4 Permit ❑Water Source Heat Pump 0 Other: WELL ID NUMBER (from Permit): MW-1 Well Depth: 20 ft. Date sample collected: 3/18/21 If WELL FIELD ANALYSES: Depth to Water Level 82546: 7 .2 ft. below measuring Well Diameter: 2 in. point Screened Interval: 3 S pH 00400: 6.8 units Temp. 000lo: 16.8 WAS 1) C DRY at 7� Measuring Point is 3 ft. above land surface Volume of water — ft. Relative M.P. Elevation: 33 to 20 — ft. m Spec. Cond. 00094: gMhos time of Odor pumped/baited before sampling: 10 gallons — 00086: Non mpl sampling, §amples for metals were collected unfiltered: ❑YE �sl] NO Appearance Clear check LABORATORY INFORMATION and fiplri ne-it4if'-4. r-1 xfn^ 1:3 NO --------------- here: F1 Date sample analyzed: March 1 - March 1812021 —±fdl Laboratory Inc. PARAMETERS NOTE: Nam: Environmental Chemists uati' 5"OUld reflect dissolved an; colloidal concentration*eCertification No. 94 COD 00335 mg/L Coliform: MF Fecal 31616 -<-I -------- . Nitrite (NO2) as N 00615 <0.02 mg/L Pb m Lead clo5i /100mL Coliform: MF Total 31504 Nitrate (NO3) as N 00620 0,02 mg/L ug/L Zn -Zinc 01092 (Note: Use mPN Method for highly turbid 'samples) /100mL Phosphorus: Total as P00665 mg/L mg/L issolved Solids:Total 70300 189 mg/L Orthophosphate 70507 ---- mg/L Other (Specify Compounds and Concentration pH (Lab) 00403 6.8 Al -Alurninum ol jo5 mg/L Units): TOC 00680 5.8 — units Ba -Barium 01007 ug/L ------ -------- mg/L Chloride oog4o 1 Ca - Calcium 00916 mg/L Arsenic 01002 ----------- mg/L Cd - Cadmium 01027 ug/L ug/L Grease and Oils 00552 Chromium: Total 01034 ug/L mg/L Phenol 32730 ug/L Cu - Copper 01042 ------ Fe mg/L ORGANICS: (by GC, GC/MS, HPLC) ------ Sulfate oog45 mg/L �pecific - Iron 01046 Hg -Mercury 71900 ug/L (Specify test and method #. ATTACH LAB REPORT.) Conductance 000gs pMhos K - Potassium 00937 ug/L Lab Report Attached? ❑ Yes (1) El No (0) Total Ammonia o0610 <0.2 mg/L (Ammonia Nitrogen; NH3ae 14, Ammonia Mg - Magnesium 00927 mg/L VOC 78732: method # Nitrogen, Total) TKN as N 00625 Mn - Manganese 01055 - mg/L ug/L ----------- method # mg/L Ni - Nickel 01067 ug/L method # ---------- For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: method # mg/L Effluent Total VOC s: -Fd= mg1L VOC Removal% James Proctor/Superintendent Perm! e (or Authorized Aycjjj) n4arne and Title -Please print or type GW-59 Rev. 212010 �. �ature of SUBMIT FORM ON YELLOW PAPER ONLY ROUNDWATER QUALITY MONITORING: CIMPLIANCE REPORT FORM or Facility Name: Maple Hill WWTF - Wastewater Irrigation System Permit Name (if different): Facility Address: 306 Maple Hill School Rd Maple Hill NC 28454-7612 County Pender contact Person: James Proctor Telephone#: 910-259-1570 Nell Location/Site Name: MW-2 No. of wells to be sampled: 4 001cm I UP FNVIRONMENT & NATURAL RMS_0_UWC_E_S_­� DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT 1617 - MAIL SERVICE CENTER,, RALEIGH, NC 27699.1617 Phone: 4919)73. .21 PERMIT Number: WQ0035049 Expiration Date: March 31, 2026 Non -Discharge WQ0035049 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MITORIED E] Lagoon C1 Remediation: Infiltration Gallery WE Spray Field ❑ Remediation: E] Rotary Distributor n Land Application of Sludge El Water Source Heat Pump 0 Other: WELL ID NUMBER (from Permit): MW-2 Well Depth: 12 Date sample collected: 3/18 /21 FIELD ANALYSES: If WELL Depth to Water Level 82546:4.0 ft. below measuring point Well Diameter: 2 in. Screened Interval: 3 PH 00400: 6.1 units Temp. 000lo: 15.o 0C WAS DRY at Measuring Point is 3 ft. above land surface ft. to 12 ft. Relative M.P. Elevation: 31.5 Spec. Cond. 00094: pMhos time of Volume of water Pumped/bailed before sampling: 10 - ft. Odor 000n: Slight Sulfur- sampling, gallons Samples for metals were cnil­+acl unfiltered- M VI=4' , M NO ) LABORATORY _IN.FORMATION and field acidified: ❑El YES ❑. 1:1 NO Appearance Clear/Tan check here: F Date sample analyzed: March 1 - March /18 /2021 Laboratory Name: Environmental Chemists Inc. PARAMETERS NOTE: Values sfiould reflect dissolved iolved Ce Certification No. 94 COD 00335 and colloidal concentrations. Coliform: MF Fecal 31616 j mg/L Nitrite (NO2) as N oor,15 <0.02 mg/L Pb - Lead o1o51 Coliform: MF Total 31504 /100mL Nitrate (NO3) as N 00620 0.10 mg/L ug/L Zn - Zinc 01092 mg/L (Note: Use MPN method for highly turbid -samples) /100ML Phosphorus: Total as P 00665 mg/L )issolved Solids:Total 703oo 333 mg/L Orthophosphate 70507 - Al mg/L Other (Specify Compounds and Concentration Units): PH (Lab) 00403 6.1 -Aluminum ol jo5 mg/Lunits TOG 00680 13.2 mg/L Be - Barium 01007 ug/L Chloride 0094o 24 Ca - Calcium 00916 mg/L Arsenic 01002 mg/L Cd - Cadmium 01027 ug/L Grease and Oils 00552 ug/L Chromium: Total 01034 ug/L Phenol 32730 mg/L ug/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Sulfate 00945 mg/L Fe -Iron 01045 Hg ug/L (Specify test and method #. ATTACH LAB REPORT.) Specific Conductance 00095 gMhos - Mercury 71900 K - Potassium 00937 ug/L Lab Report Attached? ❑F� Yes (1) ❑E3 No (0) Total Ammonia 00610 0.5 �Nftgw mg, /L Mg - Magnesium 00927 mg/L VOC 78732: method # (Ammonia Nitrogen-, NH3aS N; Ammonia Total) Mn - Manganese c1os5 mg/L method # TKN as N 00625 mgiL Ni - Nickel 01067 ug/L method # ;or Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: ug/L method # . mg/L Effluent Total VOCS: mg/L VOC Removal% James Proctor /Superintendent Permitt a (or Authorized lie -Please print or type GW-59 Rev. 21201107'". d1ju 1 life W,,n t.r. of Permrttee (or Author zed Agent) SUBMIT FORM owYELLOW PAPER ONLY OUNDWATER QUALITY MONITORING: MPLIANCE REPORT FORM Facility Name: Maple Hill WWTF - Wastewater Irrigation System Permit Name (if different): Facility Address: 306 Maple Hill School Rd Maple Hill Wjty� NC 28454-7612 County Pander octPerson: James Proctor Telephone# 910ee91570 No. of wells to be 5ampled: 4 DIVISION OF WATER QUALITY-INFORMA71ON PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-161 PERMIT Number- WQ0035049 Expiration Date: March 31, 2021 NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED El Lagoon Remedlation: Infiltration Gallery ME Spray Field Remediation: El Rotary Distributor Land Application of Sludge El Water Source Heat Pump El Other: LLIDNUMBER �p,ww� m Permit): mW-u Da�somp�cn/�u���m1omou1 |Dop�: un � �--------' � Well Diameter: o in mk`Water Level 82546:4a fLbelow measuring point Screened Interval: ----ML �u on � ouhngPo��ia » ft. above �ndou�a� Re|��aM.P.E�vo�on'---- --- meofwater pumped/bailed before sampling: 10 gallons -------'` YES ONO FIELD ANALYSES: WAS pHo04ou6.a unite Tmmp.mmiu 17o "C DRY at Spec. Cond,nu094: gNhos---' time of Odu,nooxo. Sulfur sampling, Appearance un Clear check |hena:0 3temomple analyzed: March ---' Laboratory Name: enwmnmon�/c�o �� mc kRAMETERS «wQo�a concentrations. '--- Chemists, � Ce�5caUonNo�o4 Coliform: MF Fecalmmo ~, ^V^ �=km��mc�m�� mg/L �_L�m� ���— �OOmL N����«], as o�u ~uuu mg/L ��-�]n�meo ��� � Cd��m��FTu�|o�aw /1VomL Phosphorus: mg/L �---- — � mg/L mnhed8o1ido:Tu�!r0000 347 0rthoph»ophatem«m m Other (8PodfyCompoundeand Concentration Units): mB/LPH(Leb)owuo Al"'-~"""oxvmm�»o mg/L _- units Bo'Barium o1onr mA8- TOCmmxvo.2 mg/L Ca-Ca(dumooum mg/L Chloride oo9womo --------'--' mg/i Cd-Codmiumo`our ------ u�� Amenico1o02 wq/L Chromium: �------- — »�L Grease and Ooaooanu Phenol oz/uo mU/� Cu�u Cnpparo1cwo mg/L ORGANICS: (oYuc.008NG.HPLC) 8u0a»mooswo uu/ u�L (Specify mmtandm�hpd #.ATTvwCHLAB REPORT.) *:ifinConductance »»«»s m@/L 11Nhos Hg_�emuryr�uon wg/� Lab Repr�/u±ouhed? [] yes (1) [] No<0> Tu�|Ammonia »»m» mg/L K_po�aeaiumooezr Mg_�oQneoiumommr mg/L method mmm"/awxmv.";wx,a° mg/L methou# k�n-Manganeawoioso u�/� ' TKNaeNnmms mg/L NiNicke|n�osr ��--------' ug/L method# ' ~~^k.A° For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/T James Proctor / Superintendent Permitt a (or Authorized A ant) Na � and Titi Pleas print or pe Effluent Tota|\xoCu: mg/L VOC Remmvm[& �---- SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM or Facility Name: Maple Hill WWTF - Wastewater Irrigation System Permit Name (if different): Facility Address: 306 Maple Hill School Rd Maple Hill 3¢rcaePt NC 28454-7612 County Fender (134i , 74-,, act Person: James Proctor Location/Site Name: MW-4 Telephone#: 910-259-1570 No. Of wells to be sampled: 4 QrAr% 1 Mr.FJ I VIP- ENVIRONMENT & NATURAL RESOURCES ------ DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 .... Phone: (91191) 733-3221 PERMIT Number. WQ0035049 Expiration Date: March 31, 2021 Non -Discharge WQ0035049 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED El Lagoon El Remediation: Infiltration Gallery Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: L ID NUMBER (from Permit): MW-4 Date sample collected: 3/18 /2021 Depth: 20 ft. Well Diameter: 2 in. I to Water Level 82546: 6.0 ft. below measuring point Screened Interval: 3 ft. to 20 ft, uring Point is 3 -ft. above land surface Relative M.P. Elevation: 35.5 ne of water pumped/bailed before sampling: 10 gallons ft )Ies for Metals were collected unfiltered: El YES [I NO and field acidified: M YES )RATORY INFnR IRATInM 13 NO ate sample analyzed: March 1s _12091 Laboratory Name: Environmental Chemists, Inc. kRAMETERS NOIr_; values should reflect dissolved COD 00335 and colloidal concentrations. Coliform: MF Fecal 31616 _mg/L Nitrite (NO2) as N 00616 <0,02 mg/L /100mL Nitrate (NO3) as N 00620 <0.04 mg/L Coliform: MF Total 31504 (Note: Use MPN method for highly turbT-_-MP1.-) /100mL W. Phosphorus: Total as P orj,,-(j& rrig/L solved Solids:Total 70300 385 Orthophosphate 70507 mg/l, PH (Lab) 00403 6.4 mg1l_ Al - Aluminum 01105 mg/L TOC oo68o 20.4 units Ba - Bariurn 01007 uq11L Chloride 00940 49 mg/l. Ca - Calcium oo916- rng/L Arsenic 01002 mg/L Cd - Cadmium 01027 unit. Grease and Oils 00552 uq/L Chromium: Total 01034 - uci/L Phenol 32730-- '--- rrig/L Cu - Copper 01042 mg/t. Sulfate 00945 ug/L Fe - Iron 01045 ugiL Icific Conductance 00095Vk molt. Hg - Mercury 71900- ug/L Total Ammonia owo 0.3 K - Potassium UU937 mg/L (Ammonia Nitrogen; NH, as N, Ammonia Nitrogen, Total) mg1L Mg - Magnesium 00927 mg/L TKN as N 00625 Mn - Manganese o1o55 ug& mg/L Ni - Nickel 01067 uQ1L For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L FIELD ANALYSES: If WELL WAS PH 00400: 6.4 units Temp. 000lo: 16.0 Oc DRY at Spec. Cond. 00094: gMhos time of Odor 00085: Slight Sulfur sampling, Appearance Clear/Tan check here:f--1 Certification No. 94 Pb - Lead o1o51 ugJL Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (sr,erify test and method #. ATTACH LAB REPORT.) Lab Report Attached? 0 yes (1) D No (0) VOC 78732: method # method # method # method # Effluent Total VOCs: Environment-aL Chemists, Inc. L envirochem 7 6602 Windmill Way, Wilmington, NC 28405 • 910,392.0223 Lab * 910.392.4424 Fax L 71013owsertown Road, Manteo, NC 27954 o 252.473.5702 Lab; Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists,com Pender County Utility Operations Date of Report: Mar 26, 2021 Post Office Box 995 Customer PO #: Burgaw NC 28425 Customer ID: 08100095 Attention: Chris Pickett Report #: 2021-04588 Project ID: Maple Hill WWTF (Monitoring Wells) Lab ID 21-11307 Test Sample ID: Collect Date/Time - Matrix Sampled by Site: MW-1 3/18/2021 10:10AM Water Jay Baker Method Results Date Analvzod Color Color Depth to water, ft. Depth to Water, Ft, Ammonia Nitrogen EPA 3501 Gallons bailed before sampling Gallons Bailed before sampling Odor Qualitative Total Dissolved Solids (TDS) SM 2540 C Temperature SM 2550 8 Chloride SM 4500 Cl E pH SM 4500 H B Total Organic Carbon (TOC) SM 5310 B Fecal Coliform SM 9222D MF Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353 2 Nitrate+Nitrite-Nitrogen EPA 353.2 Nitrate Nitrogen Subtraction Method Clear 03/18/2021 7.2 feet 03/18/2021 < 0.2 mg/L 03/22/2021 10gallons 03/18/2021 None 03/18/2021 189 mg/L 03/19/2021 16.8 C 03/18/2021 17 mg/L 03119/2021 6.8 units 03/18/2021 5.8 mg/L 03/22/2021 <1 Colonies/100ml 03/18/2021 * 0.02 mg/L * 0.02 mg/L <0. 02 mg/L 03/18/2021 03/2212021 03/24/2021 Report # 2021-04588 rage i or 4 Environmental Chemists, Inc, envirochem 6602 Windmill Way, Wilmington, NC 28405 1 910.392.0223 Lab . 910.392.4424 Fax sra 710 Bowsertown Road, Manteo, NC 27954 , 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com environmentalchemists.com Pender County Utility Operations Date of Report: Mar 26, 2021 Post Office Box 995 Customer PO #: Burgaw NC 28425 Customer ID: 08100095 Attention: Chris Pickett Report#: 2021-04588 Project ID: Maple Hill WWTF (Monitoring Wells) Lab ID Sample ID: Collect Date/Time Matrix Sampled by 21-11308 Site: MW-2 3/18/2021 10:35 AM Water Jay Baker Test Method Results Date Analyzed Color Color Clear/Tan 03/18/2021 Depth to water, ft. Depth to water, Ft. 4.0 feet 03/18/2021 Ammonia Nitrogen EPA 350.1 0.5 mg/L 03/22/2021 Gallons bailed before sampling Gallons Baited before sampling 10 gallons 03/18/2021 Odor Qualitative Slight Sulfur 03/18/2021 Total Dissolved Solids (TDS) SM 2540 C 333 mg/L 03/19/2021 Temperature SM 2550 B 15.0 C 03/18/2021 Chloride SM 4500 Cl E 24 mg/L 03/19/2021 pH SM 4500 H B 6.1 units 03/18/2021 Total Organic Carbon (TOC) SM 5310 B 13.2 mg/L 03/22/2021 Fecal Coliform SM 9222D MF <1 Colonies/100mi 03/18/2021 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353 2 < 0.02 mg/L 03/18/2021 Nitrate+Nitrite-Nitrogen EPA 353 2 0.10 mg/L 03/22/2021 Nitrate Nitrogen Subtraction Method 0.10 mg/L 03/24/2021 Report# 2021-04588 Page 2 of 4 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab a 910.392.4424 Fax L sw 710 Bowsertown Road, Manteo, NC 27954 252.473.5702 Lab/Fax --.MA 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info c@environmentalchemists.com Pender County Utility Operations Date of Report: Mar 26, 2021 Post Office Box 995 Customer PO #: Burgaw NC 28425 Customer ID: 08100095 Attention: Chris Pickett Report #: 2021-04588 Project ID: Maple Hill WWTF (Monitoring Wells) Lab ID Sample ID: Collect Date/Time Matrix Sampled by 21-11309 Site: MW-3 3/18/2021 10:55 AM Water Jay Baker Test Method Results Date Analyzed Color Color ClearrTan 03/18/2021 Depth to water, ft. Depth to Water, Ft 4.9 feet 03/1812021 Ammonia Nitrogen EPA 350,1 < 0.2 mg/L 03/22/2021 Gallons bailed before sampling Gallons Bailed before sampling 10 gallons 03/18/2021 Odor Qualitative Sulfur 03/18/2021 Total Dissolved Solids (TDS) SM 2540 C 347 mg/L 03/19/2021 Temperature SM 2550 8 17.0C 03/18/2021 Chloride SM 4500 Cl E 55 mg/L 03/19/2021 pH SM 4500 H 8 6.3 units 03/18/2021 Total Organic Carbon (TOC) SM 5310 8 6.2 mg/L 03/24/2021 Fecal Coliform SM 9222D MF <1 Colonies/100ml 0311812021 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353 2 < 0.02 mg/L 03/18/2021 Nitrate+Nitrite-Nitrogen EPA 3532 < 0.02 mg/L 03/22/2021 Nitrate Nitrogen Subtraction Method <0.02 mg/L 03/24/2021 sport #' 2021-04588 Page 3 of 4 -71 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 + 910.392.0223 Lab • 910.392.4424 Fax sM 710 Bowsertown Road, Manteo, NC 27954 a 252.473,5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 , 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info a environmentalchemists.com Pender County Utility Operations Date of Report: Mar 26, 2021 Post Office Box 995 Customer PO #: Burgaw NC 28425 Customer ID: 08100095 Attention: Chris Pickett Report #: 2021-04588 Project ID: Maple Hill WWTF (Monitoring Wells) Lab ID Sample ID: Collect Date/Time Matrix Sampled by 21-11310 Site: MW-4 3/18/2021 11:10 AM Water .lay Baker Test Method Results Data Anahr70ei Color Color Clear/Tan 03/18/2021 Depth to water, ft. Depth to Water, Ft 6.0 feet 03/18/2021 Ammonia Nitrogen EPA 350 1 0.3 mg/L 03/22/2021 Gallons bailed before sampling Gallons Bailed before sampling 10 gallons 03/18/2021 Odor Qualitative Slight Sulfur 03/18/2021 Total Dissolved Solids (TDS) SM 2540 c 385 mg/L 03/19/2021 Temperature SM 2550 B 16.0 C 03/18/2021 Chloride SM 4500 Cl E 49 mg/L 03/19/2021 pH SM 4500 H B 6.4 units 03/18/2021 Total Organic Carbon (TOG) SM 5310 B 20.4 mg/L 03/24/2021 Fecal Coliform SM 9222D MF <1 Colonies/100ml 03/18/2021 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353 2 < 0.02 mg/L 03/18/2021 Nitrate+Nitrite-Nitrogen EPA 353 2 0.04 mg/L 03/22/2021 Nitrate Nitrogen subtraction Method 0.04 mg/L 03/24/2021 Comment: Reviewed by: Report# 2021-04588 Page 4 of 4 Date: .Analyst: t�1� PH Certification # 94 Pacility Name: Permit #: % Reference Method SM4500 H-B -201 I Instrument ID wf Calibration Time Cat Buffer 4 0 s u Cat Buffer 10 0 s u Check Buffer 7 0 s u Comments A "pH check buffer must read within ±0 1 pH units of the buffers true value 4 su buffer Lot#/: Ricca 2001 B20 Ezo 1 /2022 7 su buffer Lot= .-Ricca 2009993 Exp. 7/7022 10 su buffer Lot-4 Ricca 1001791 7 2021 Sample location Sample Collection Sample Anaysis pH Result ►post -analysis Buffer Times Timt ♦ s u Check value s u Comments Data Qualifiers ! + f I it } /.of,`+` sf 4-70. l(t� tttt G•�'� ► Post analysis buffer check is required when performing analyses at multiple sampling locations and must be within = 0 I units of the buffer's true value All plf values in pH units (i.e, s u ) Record all data to the nearest 0 01 s u and report to the nearest 0.1 s u Total Residual Chlorine (TRC) Reference [Method: SM 450" C1•132011: Hach 8167 HR: I Please circle applicable Method Instrument ID Daily Check Post -analysis Time check Check Sid Sample Sample Sample TRt' Result Standard Result Standard Collection Analysis C mmentsData Qualifiers (when analyzing Analyzed Location Time Ttme µ_ Q µg9_ or mgL e I, or meL ai multinle sites) TRC Daily' Check Standard true value µg/L or mg/L acceptance range µg I or mg 1. Check standards must recut er w ithin s 10° o of the check standard's true value Annual Calibration Curve Verification Date: LOT #i _ Exp. Date: Reagent Blank Value __ (When applicable. Analyze and document a reagent blank %then standards, sample dilution; or PT Samples are prepared) Dissolved Oxygen (DO) Reference hfethod:Sltt 4500 0 G,-2 1 ` Instrument ID Calibration` Calibration variable Meter reading •Post -analysis calibration Verification o, - Verification -when or ,a efficiency Comments Time Barometric after calibration Theoretical Calculated Temperature pressure Value mg L Value mtt'L I I i I I I ( Use this ro%% when performine a %cri6cation instead of I Sample Location f Sample Collection `Sample Analysis ' DO reading Comments Data Qualifiers When performing analyses at multiple locations, the meter must be recalibrated at each site before analysis or a post -analysis calibration verification must be performed Ifsampie is measured directly in the stream and or onsite, only time analyzed would be recorded with a note that they are measured in situ or immediatey Temperature Reference ivfethod SM 255 + B-2010 Instrument ID Sample 1 'Sample Temperature L I Sample Location Collection Anal%sts oC Comments Data Qualifiers Time Time C t If I t A'L ' If sample is measured directiv in the stream and or on site, only time analyzed would be recorded, with a note Annual Verification Date Field Personnel Note: are measured in situ or immediately QA.00I Environmental Chemist, Inc., Wilmington, NC Lab #94 Sample Receipt Checklist Clien Date: 31, 00 J- 2 � ij- Report Number: 6602 Windmill Way Wilmington, NC 2840 910.392.0223 Receipt of sample: ECHEM Pickup IX -nt Delivery 0 JuPS 0 0 YES 0 113 NO N/A 1. Were custody seals present on the cooler? 0 YES - NO IR resent, were they intact/unbroken? Original temperature upon - %-.If oc Corrected temperature upon receipt How temperature taken: 0 Temperature Blank I �ainst Bottles IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor *C: 0.0 0 YES 113 NO 13. if temperature of cooler exceeded 6*C, was Project Mgr./QA notified? YES JEJ NO 14. Were proper custody procedures (relinquished/received) followed? 1P YES 10 NO S. Were sample ID's listed on the COC? I Ep YES E3 N 0 6. Were samples ID's listed on sample containers? ES- 113 N 0 7. Were collection date and time listed on the COC? YES -J 0 NO 8. Were tests to be performed listed on the COC? 10 NO 19. Did samples arrive in proper containers for each test? VYES YES 10 NO 110. Did samples arrive in good condition for each test? YES 10 NO Ill. Was adequate sample volume availableT YES 0 NO J12. Were samples received within proper holding time for requested tests? YES 10 NO 113. Were acid preserved samples received at a pH of <2? YES 113 NO [-1-4. Were cyanide samples received at a pH >12? YES 10 NO 115 Were sulfide samples received at a pH >9? YE Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? 0 YES 0 NO 117. Were Sulfide/Cyanide received at a chlorine residual of <0,5 m/L? 0 YES 10 No 118. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Vobdlesare pHchecked attime cfanalysis and recorded onthe benchsheeC ** Bacteria samples are checked for Chlorine at time ofanalysis and recorded unthe benchsheet. [S Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2SO4 HNO3 HCl NaOH Time of preservation: — If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain anewsample or 0C 4= 1 Analytical & Consulting Chemists CLIENT: Pender County Utilities Sample Identification Well: f pth to water, 9 � Ions bailed: 10 IfiPiril- 6 •Vr) '1 .4 f- of 4 wolfs: due In March, July, November. 1. — 2. Temperature when Delivered By: ENVIRONMENTAL CHEMISTS, INC OFFICE: 910-392-06602 Windmill Way , NC 28406 223 FWilmingtonAX 910-392-4424 NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 lnfo@environmentalchemists.com COLLECTION — AND CHAIN OF CUSTODY NAME: Maple Hill WWTP Monitoring Wells REPORT NO: CONTACT NAME: PO NO: REPORT TO: Chris Pickett, ORC PHONE/FAX: COPY TO: lemail:: 15 SAMPLE 0 TYPE: 0 I = Influent, E E ©W :E z = Effluent, PRESERVATION W-= Well, ST = Stream, SO = Soil, SL = Sludge, Other: ANALYSIS REQUESTED Alection Time Temp 0 z U 0 7 0 z —z a 41 are C P x TDS, Cl, NO2 G G C P r _x NO3, NH3 G G C P x Fecal Coliform G C —G P x Total Or anic Carbon G G C P G ---G— C P G G I L—C P G—F—G--1 By; Time: I 4w Analytical & onsulting Chemists CLIENT: Pender County Utilities .... r.-- —Y ........ m=� Sample Identification Pth to water di 0 Ions balled: %x (field): )r (field): cA, 416-e of 4 wells: due in March, July, November. 6 602 WindmiWy , NC 28406 ENVIRONMENTAL CHEMISTS, INC OFFICE: 910-ll 392-a0223 FWilmingtonAX 910-392-4424 NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 infog nvironmental— I em 513.com COLLECTION AND CHAIN OF CUSTODY PROJECT NAME Maple Hill WWTp Monitoring Wells REPORT NO: Cp- CONTACT NAME: PO NO: REPORT TO: Chris Pickett, ORC PHONEIFAX: ICOPY TO: lemail:: 4, SAMPLE $1 'A jo & I LV TYPE: 0 C V. U I = Influent, a C ro 2 ? E G w a 5 = z = Effluent, PRESERVATION W — = Well, ST = Stream, So = soil, s � L Sludq Other - ANALYSIS REQUESTED )Ilectio;, Time Temp w z 2 d . I . x § nc * — 2 F 0 = C —P x --- TDS, Cl, NO2 G G C G G x NO3, NH3 C P G G x Fecal Coliform C P G C G P x Total Organic Carbon G G C P G G C P G G 1. nuGelvea OV: 2. :1 Temperature when Received-- Accepted: Re* ct d:— Resample Delivered By: Received By: Comments: Date:- T : Time: ENVIRONMENTAL CHEMISTSINC 6602 Windmill Way Wilmington, NC 28405 4M , 910-392-0223 F910-392- Analytical & Consulting Chemists NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 OFFICE: info@environmentachemists .com 4424 COLLECTION AND CHAIN OF CUSTODY CLIENT: Pender County Utilities PROJECT NAME: Maple Hill WWTP Monitoring.Aells REPORT NO: 62- ADDRESS: CONTACT NAME: PO NO: REPORT TO: Chris Pickett, ORC PHONEIFAX: COPSampled By:— Y TO: email:: SAMPLE TYPE: uent, E = Effluent, W = Well, ST =Stream So = Soil Qi Sample Identification Date ell: ,pth to water: llons bailed: ja I (field): C - 3-> odor (field): total of 4 Wells: due In March, July, November. 1. — 2. Temperature when Delivered BY: Comments: Mew" PRESERVATION er. ANALYSIS REQUESTED Uj z 0 8 z 0 2 5 0 x TDS. Cl, NO2 x NO3, NH3 x Fecal Coliform X.. Total Orqanic Carbon ......... . ..... Received By: Daterrime By: Lbd—L-L—Time: TURNAROUND: ` INC B502WindmillWayWilmington,NC28405 ENVIRONMENTAL CHEMISTS, Analytical &Consulting Chemists910- NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 OF ni o@envir3onmenta chemists cam 24 COLLECTION AND CHAIN OF CUSTODY CLIENT: Pender County Utilities PROJECT NAME: Maple Hill WWTp Monitorin Wells REPORT NO: ADDRESS: CONTACT NAME: PO NO: REPORT TO: Chris Pickett, ORC PHONE/FAX: Sam Ied B COPY TO: email:: Collection Sample Identifflication --- ate Time Temp Well: q `' ll Depth to water: 41 y gallons bailed: / 0 PH (field): ador Field): t hri 1»14* 4,z —6- el otal of 4 wags: due In March, Jury, November. SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Sol[. SL = Sludge, Other: n ii = a ° . W c c� q . c g ur PRESERVATION a°i }� c° o a r E u z o z 0 cc o ANALYSIS REQUESTED 0 C P �p G G X TDs, Cl, NO2 x� G G C P NO3, NH3 G C G P x Fecal Coliform G C G p X Total Organic Carbon G G C p G G CI P G G 1. - - received By: Date/Time 2. Temperature when Received: —Accept,d: Delivered By: �; Rejec Resampl ted: Comments: Received By: Date: Time: TURNAROUND: