WQ0006946_Monitoring - 11-2020_20210129 (3)

(AV-59 A ('0NIPLI.ANCE REPORT FORM Permit # WQ0006946 p
('Suhmit am each monitoring period with G1V 59 f)rm%.)
I
Enter date monitoring results were due. (1 vsv?mn ) Will this monitoring report (GW-59 and GW-59A)
NO
be submitted after the established due date?
2
Was any required information missing on the GW-59 report forms?
1'ES
IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
TFS
identification plate, area overgrown, etc.)? 1J'the answer is 1es", contact the Regional Qfice far guidance.
4
Are any monitored constituents equal to or above the established standards?
NO
If the answer to question 4 is "NO", skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below.
Well # 2: TDS 788mg/L 11/04/2020
Well # 3 :TOC 26.2 11/04/2020
S
For the constituents identified in question 4 above, have standards been exceeded previously for the
NO
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO", skip to section S.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding
standards, concentrations) reported, and sample collection date for each occurrence (for the last two years).
Monitoring Well # 2 TDS 812 Date 07/2020 Monitoring well # 2TDS 868 Date 03/2019
Monitoring well # 2 TDS 736 Date: 03/2020 Monitoring well # 2 TDS 792 Date 11/2018
Monitoring well # 2 TDS 816 Date 11/2019 Monitoring well # 2 TDS 828 Date 07/2018
Monitoring well # 2 TDS 794 Date 07/2019 Monitoring Well # 3 TDS 862; Date 03/2018
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
1EB
NO
If the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells maybe improperly
located; contact the Regional Office.
7
Is the pennittee implementing previously approved actions required by the Division involving this
NO
groundwater quality problem?
ff the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO" contact the Regional Office within 90 days; an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility, Failure to do so may subiect theoerin fte to a Notice of Violation
frees, and/or penalties. U:1
O
o
8
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this
form with G W-59 forms for required wells to the address provided at the top of the current G W-59 form.
hereby acknowledge that the above information was evaluated and the information submitted in this
report (Compliance Report -58A rue nd complete to the best of my knowledge.
ignat o PeAnittAbrAuth7,741 Agent) 13e
GA\-59 % 12/$/2003

NDWATER QUALITY MONITORING:
LIANCE REPORT FORM
TY INFORMATION grease Phrif Clearly or
Name: Reed Gold Mine State Historic Site
Name (if different):
Address: 9621 Reed Mine Rd.
Midland
act Person: Robert L. Garner
Location/Site Name:
NC 28107
Reed Gold Mine State Historic Site
WELL ID NUMBER (from Permit): MW # 1
Well Depth: 60 ft.
Depth to Water Level 82546: 11.4 ft. below measuring point
Measuring Point is • 3 ft. above land surface
Volume of water pumped/bailed before sampling: 26
Samples for metals were collected unfiltered: ❑ YES ❑
t AGAOA7rinV r�r C/1n�awYr�ar
SUBMIT FORM ON VFl I nw GADCD nr.lt v
County Cabarrus
Telephone#: [phone]
No. of wells to be sampled: 3
oEPARTMENT OF EWRONMENTAL QUALITY - DIV. OF WATER RESOURCES
INFORMATION PROCESSING UNIT
116117 MAIL SERVICE CENTER, RALEIGH, NC 276994617 Phone: [phone]
PERMIT Number: WQ0006946 Expiration Date: 01/31/2022
Non -Discharge UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon ❑ Remediation: Infiltration Gallery
>Woc Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
Date sample collected: 11 /04/2020
Well Diameter: 2 in.
Screened Interval: 50 ft. to 60 ft.
Relative M.P. Elevation: 544 ft,
gallons
NO and field
M
Date sample analyzed: 11 / 4-19 / 2020
Laboratory Name:
K & W Laboratory
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 0061E
mg/L
Coliform: MF Fecal 31616 7
1100mL
Nitrate (NO3) as N oo620
<0.05 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 0o665
<0.05 mg/L
(Note: Use MPN mathod for highly turbid samples)
Orthophosphate 70507
mg/L
issolved Solids:Total 70300 330
mg/L
AI -Aluminum o1105
mglL
pH (Lab) 00403
units
Ba - Barium oio07
uglL
TOC oasso 1.1
mg/L
Ca - Calcium oo916
mg/L
Chloride 00940 62
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug1L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Specific Conductance oao95
µMhos
K - Potassium 00937
mg/L
Total Ammonia 00610 <0.1
mg/L
Mg - Magnesium 00927
mg/L
(Ammonia Nitrogen: NH3 as N; Ammonia Nitrogen, Total)
-
Mn -Manganese p1o55
ug/L
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
1 _•_••••• ,...,.� t.�......... r.aw r.cyan oar. 1114luclit Juidl vu%lb.
Larry K. Neal , Historic Site Manger III
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.3-1.2016
FIELD ANALYSES:
pH 00400: 7.57 units Temp. 000iov 16.2 °C
Spec. Cond. 00094: µMhos
Odor 000ss: slight
Appearance Clear
Certification No. 559
Pb - Lead o1os1 ug1L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units):
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes (1) ❑ No (0)
VOC 7673 method #
method #
method #
method #
mglL trluent Iotal VOGs:
mg/L VOC Removal%
l
WAS
DRY at
time of
IN

SUBMIT FORM ON YFI I nW aaaGo nkn v
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION Please Print Clearfy or Type —
Facility Name: Reed Gold Mine State Historic Site
Permit Name (if different):
Facility Address: 9621 Reed Mine Rd.
Midland NC 28107 County Cabarrus
(Contact Person: Robert L. Garner Telephone#: [phone]
Well Location/Site Name: Reed Gold Mine State Historic Site No. of wells to be sampled: 3
DEPARTMENT OF ENVIRONMENTAL QUALITY- DIV. OF WATER RESOURCES
INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1017 Phone: 919-S07-6308
PERMIT Number: t/1/(Q0006946 Expiration Date: 01/31/2022
Non -Discharge UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
XLagoon ElRemediation: Infiltration Gallery
[Kpray Field ❑' Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
SAMPLING INFORMATION
WELL ID NUMBER {from Permit): MW # 2 Date sample collected: 11 / 04 / 2020
Well Depth: 60 ft. Well Diameter: 2 in.
Depth to Water Level 82546: 13.0 ft. below measuring point Screened Interval: 50 ft. t060 ft.
Measuring Point is 3 ft. above land surface Relative M.P. Elevation: 540 ft.
Volume of water pumped/bailed before sampling: 7 gallons
for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: El YES NO
FIELD ANALYSES:
pH 00400: 6.97units Temp. 000lo: 15.7 eC
Spec. Cond. 00094: µMhos
Odor 00085: None
Appearance clear
If WELL
WAS
DRY at
time of
sampling,
check
here:
❑Samples
LABORATORY INFORMATION
Date sample analyzed: 11 / 04 - 19 / /2020
Laboratory Name:
K & W Laboratory
Certification No. 559
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L
Pb - Lead o1os1 u fL
Coliform: MF Fecal 31616 16
I100mL
Nitrate (NO3)N0as N 00620
<0.05
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
<0.05
mg/L
(Note: Use MPN method for highly turbid samples)
-
Orthophosphate 70507
mg1L
Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 788
mg1L
Al - Aluminum oilo5
pH (Lab) 00403
units
Ba - Barium 01007
_mg/L
ug/L
TOG oo68o 5.2
mg/L
Ca - Calcium oom
mg/L
Chloride 00940 93
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance o0095
µMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia oo6lo 0.16
Mg - Magnesium 00927
mg/L
method #
(Ammonia
(amnia Nitrogen: NH3 as N; ammonia Nitrogen. rotaq
Mn - Manganese o1o55
ug/L
, method #
TKN as N 00525
mg/L
Ni- Nickel 01067
ug/L
method #
--•--•—.. ..J....,. v" y traaaaaa.aI a.aav INUPVI Lai: lllliuent iota] vVl,s
Larry K. Neal, Historic Site Manger III
Permittee (or Authorized Agent) Name and Title - Please print or type
OW-59 Rev.3-1-2016
mg/L Effluent 1 f1 •
tnd that the laboratory analytical +'ata was producee using approved methods of analysis by a
,11ty of fir .s and Iand Imprisci, men, h r knowlnr vitdP%ens,
re -j O.

UNDWATER QUALITY MONITORING:
PLIANCE REPORT FORM
Name: Reed Gold Mine State Historic Site
Name (if different):
Address: 9621 Reed Mine Rd.
Midland NC
act Person: Robert L. Garner
Location/Site Name:
SUBMIT FnRM r]N YFl I nW aeocra nntt v
Clearly or
28107 County Cabarrus
Reed Gold Mine State Historic Site
Telephone#: [phone]
No. of wells to be sampled: 3
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
INFORMATION PROCESSING UNIT
11617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1817 Phone: [phone]
PERMIT Number: WQ0006946 Expiration Date: 01/31/2022
Non -Discharge UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
tcs. Lagoon ❑ Remedlation: Infiltration Gallery
Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
WELL ID NUMBER (from Permit): MW # 3
Date sample collected: 11 / 04 / 2020
FIELD ANALYSES:
If WELL
WAS
Well Depth: 60 ft.
Well Diameter: 2 in.
pH 00400: 7.6 units Temp, 000lo: 15.7 eC
DRY at
Depth to Water Level 82546: 14.3 ft. below measuring point
Screened Interval: 50 ft. to 60 ft.
Spec. Cond. 00094: µMhos
time of
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: 538 ft.
Odor o0oas: None
sampling,
Volume of water pumped/bailed before sampling: 14.0 gallons
Appearance Clear
check
here:
for metals were collected unfiltered: ❑ YES ❑ NO
and field acidified: ❑ YES El NO
❑Samples
Date sample analyzed: 11 / 04-19 / 2020
Laboratory Name:
K & W Laboratory
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 0o335
mg/L
Nitrite (NO2,) as N 00615
mg/L
Coliform: MF Fecal 31616 11
/100mL
Nitrate (NO3) as N 00620
<0.05 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
<0.05 mg/L
(Note: use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
issolved Solids:Total 70300 326
mg/L
Ai - Aluminum o1lo5
mg/L
PH (Lab) 00403
units
Ba - Barium 01007
ug/L
TO 00680 26.2
mg/L
Ca - Calcium oo916
mg/L
Chloride 00940 42
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total wom
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Specific Conductance oao95
µMhos
K - Potassium 00937
mg/L
Total Ammonia ooslo <0.1
mg/L
Mg - Magnesium 00927
mg/L
(Ammonia N;trogsr: NHyas N: Ammonia Nitrogen, Total)
Mn - Manganese o1055
ug/L
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
Certification No. 559
Pb - Lead o1o5l ug/L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units):
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes (1) ❑ No (0)
VOC 7873 method #
method #
method #
method #
a.an r%upulLkip uutueni total vvcs: mg1L Effluent Total VOCs: mg/L VOC Removal%
Larry K. Neal, Historic Site Manger III
Permittee (or Authorized Agent) Name and Title - Please print or type A—ur.
GW-59 Rev.3-1-2016
1.�

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trw paealaba.com
ANALYTICAL RESULTS
Project: GW Sampling
Pace Project No.: 92504583
Pace Analytical Services, LLC
9800 lOncey Ave. Suite 100
Huntersvi;le, NC 28078
[phone]
Sample: 20110406-RGM
Parameters
Lab ID: 92504583003 Collected: 11/04/20 11:03
Results Units Report Limit DF
Received: 11/06/20 08:00 Matrix: Water
Prepared Analyzed CAS No.
Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Tetrachloroethene
ND ug/L
2.5
2.5
11/23/20 21:26
127-18-4
H1
Toluene
ND ug/L
2.5
2.5
11/23/20 21:26
108-88-3
H1
1,2,3-Trichlorobenzene
ND ug/L
2.5
2.5
11/23/20 21:26
87-61-6
H1
1,2,4-Trichlorobenzene
ND ug/L
2.5
2.5
11/23/20 21:26
120-82-1
H1
1,1,1-Trichloroethane
ND ug/L
2.5
2.5
11123/20 21:26
71-55-6
H1
1,1,2-Trichloroethane
ND ug/L
2.5
2.5
11/23/20 21:26
79-00-5
H1
Trichloroethene
ND ug/L
2.5
2.5
11/23/20 21:26
79-01-6
H1
Tdchlorofluoromethane
NO ug/L
2.5
2.5
11123/20 21:26
75-69-4
H1
1,2,3-Trichloropropane
ND ug/L
2.5
2.5
11/23/20 21:26
96-18-4
H1
Vinyl acetate
ND ug/L
5.0
2.5
11/23/20 21:26
108-05-4
H1
Vinyl chloride
ND ug/L
2.5
2.5
11/23/20 21:26
75-01-4
H1
Xylene (Total)
ND ug/L
2.5
2.6
11/23/20 21:26
1330-20-7
m&p-Xylene
ND ug/L
5.0
2.5
11123/2021:26
179601-23-1
H1
o-Xylene
ND ug/L
2.5
2.5
11/23/20 21:26
95-47-6
H1
Surrogates
4-Bromofluorobenzene (S)
95 %
70-130
2.5
11/23/20 21:26
460-00-4
1,2-Dichloroethane-d4 (S)
99 %
70-130
2.5
11/23/20 21:26
17060-07-0
Toluene-d8 (S)
102 %
70-130
2.5
11/23/20 21:26
2037-26-5
5310E TOC
Analytical Method: SM 531OB-2011
Pace Analytical Services - Asheville
Total Organic Carbon
- 26.2 mg/L
1.0
1
11/19/20 13:19
7440-44-0
Date: 11/24/2020 05:38 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, U.C.
Page 7 or 18

�aceAna"ical
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I
ANALYTICAL RESULTS
Project: GW Sampling
Pace Project No.: 92504583
Pace Analytical Services, LLC
gaoo Kncey Ave. Suite 100
Huntersville, NC 28078
(704)B75-9092
Sample: 20110406-RGM
Parameters
Lab ID: 92504583003 Collected: 11/04/20 11:03 Received:
Results Units Report Limit OF Prepared
11/06/20 08:00 Matrix: Water
Analyzed CAS No.
Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
858
ug/L
62.5
2.5
11,123/20 21:26
67-64-1
H1
Benzene
NO
ug/L
2.5
2.5
11/23i20 21:26
71-43-2
H1
Bromobenzene
NO
ug/L
2.5
2.5
11/23/20 21:26
108-86-1
H1
Bromochloromethane
NO
ug/L
2.5
2.5
11/23/20 21:26
74-97-5
H1
Bromodichloromethane
NO
ug/L
2.5
2.5
11/23/20 21:26
75-27-4
H1
Bromoform
NO
ug/L
2.5
2.5
11/23/20 21:26
75-25-2
H1
Bromomethane
NO
ug/L
5.0
2.5
11/23/20 21:26
74-83-9
H1
2-Butanone (MEK)
NO
ug/L
12.5
2.5
11/23/20 21:26
78-93-3
H1
Carbon tetrachloride
NO
ug/L
2.5
2.5
11123/20 21:26
56-23-5
H1
Chlorobenzene
NO
ug/L
2.5
2.5
11/23/20 21:26
108-90-7
H1
Chloroethane
NO
ug/L
2.5
2.5
11/23/20 21:26
75-00-3
H1
Chloroform
NO
ug/L
12.5
2.5
11/23/20 21:26
67-66-3
H1
Chloromethane
NO
ug/L
2.5
2.5
11/23/20 21:26
74-87-3
H1,v2
2-Chlorotoluene
NO
ug/L
2.5
2.5
11123/20 21:26
95-49-8
H1
4-Chlorotoluene
NO
ug/L
2.5
2.5
11/23/20 21:26
106-43-4
H1
1,2-Dibromo-3-chloropropane
NO
ug/L
12.5
2.5
11/23/20 21:26
96-12-8
H1
Dibromochloromethane
NO
ug/L
2.5
2.5
11/23/20 21:26
12448-1
H1
1,2-Dibromoethane (EDB)
NO
ug/L
2.5
2.5
11/23/20 21:26
106-93-4
H1
Dibromomethane
NO
ug/L
2.5
2.5
11/23/20 21:26
74-95-3
H1
1,2-Dichlorobenzene
NO
ug/L
2.5
2.5
11/23/20 21:26
95-50-1
H1
1,3-Dichlorobenzene
NO
ug/L
2.5
2.5
11/23/20 21:26
541-73-1
H1
1,4-Dichlorobenzene
NO
ug/L
2.5
2.5
11/23/20 21:26
106-46-7
H1
Dichlorodifluoromethane
NO
ug/L
2.5
2.5
11/23/20 21:26
75-71-8
H1
1,1-Dichloroethane
NO
uglL
2.5
2.5
11/23/20 21:26
75-34-3
H1
1,2-Dichloroethane
NO
uglL
2.5
2.5
11/23/20 21:26
107-06-2
H1
1,1-Dichloroethene
NO
ug/L
2.5
2.5
11/23/20 21:26
75-35-4
H1
cis-1,2-Dichioroethene
NO
ug/L
2.5
2.5
11/2312021:26
156-59-2
H1
Vans-1,2-Dichloroethene
NO
ug/L
2.5
2.5
11/23/20 21:26
156-60-5
H1
1,2-Dichloropropene
NO
ug/L
2.5
2.5
11123/20 21:26
78-87-5
H1
1,3-Dichloropropane
NO
ug/L
2.5
2.5
11123/20 21:26
142-28-9
H1
2,2-Dichloropropane
NO
ug/L
2.5
2.5
11/23/20 21:26
594-20-7
H1
1,1-Dichloropropene
NO
ug/L
2.5
2.5
11/23/20 21:26
563-58-6
H1
cis-1,3-Dichloropropene
NO
ug/L
2.5
2.5
11/23/20 21:26
10061-01-5
H1
trans-1,3-Dichloropropene
NO
ug/L
2.5
2.5
11/23/20 21:26
10061-02-6
H1
Dilsopropyl ether
NO
ug/L
2.5
2.5
11/23/20 21:26
108-20-3
H1
Ethylbenzene
NO
ug/L
2.5
2.5
11/23/20 21:26
100-41-4
H1
Hexachloro-1,3-butadiene
NO
ug/L
2.5
2.5
11/23/20 21:26
87-68-3
H1
2-Hexanone
NO
ug/L
12.5
2.5
11/23/20 21:26
591-78-6
H1
p-Isopropyltoluene
NO
ug/L
2.5
2.5
11/2312021:26
99-87-6
H1
Methylene Chloride
NO
ug/L
12.5
2.5
11/23/20 21:26
75-09-2
H1
4-Methyl-2-pentanone (MIBK)
NO
ug/L
12.5
2.5
11/23/20 21:26
108-10-1
H1
Methyl-tert-butyl ether
NO
ug/L
2.5
2.5
11/23/20 21:26
1634-04-4
H1
Naphthalene
NO
ug/L
2.5
2.5
11/23/20 21:26
91-20-3
H1
Styrene
NO
ug/L
2.5
2.5
11/23/20 21:26
100-42-5
H1
1,1,1,2-Tetrachioroethane
NO
ug/L
2.5
2.5
11/23/20 21:26
630-20-6
H1
1,1,2,2-Tetrachioroethane
NO
ug/L
2.5
2.5
11/123/20 21:26
79-34-5
H1
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced,
except In full,
Date: 11/24/2020 05:38 PM
without the written consent of Face Analytical Services, LLC.
Page 6 of 18

aceAnalj6cal
tvwkliaealab c m
ANALYTICAL RESULTS
Project: TOC & VOC T5827-RGM
Pace Project No.: 92513089
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: T5827-RGM
Lab ID: 92513089001 Collected:
12/18/20 10:25
Received: 12/21/20 12:00 Matrix: Water
Parameters
Results
Units Report Limit
OF
Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Tetrachloroethene
NO
ug/L
1.0
1
12/23/20 23:33 127-18-4
Toluene
ND
ug/L
1.0
1
12/23/20 23:33 108-88-3
1,2,3-Tdchlorobenzene
NO
ug/L
1.0
1
12123/2023:33 87-61-6
12,4-Trichlorobenzene
ND
ug/L
1.0
1
12/23/20 23:33 120-82-1
1,1.1-Tdchloroethane
ND
ug/L
1.0
1
12123/2023:33 71-55-6
1,1,2-Tdchloroethane
ND
ug/L
1.0
1
12/23/20 23:33 79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/23/20 23:33 79-01-6
Trichlorofluoromethane
NO
ug/L
1.0
1
12/23/20 23:33 75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/23/20 23:33 96-18-4
Vinyl acetate
NO
ug/L
2.0
1
12/23/20 23:33 108-05-4
Vinyl chloride
NO
ug/L
1.0
1
12/23/20 23:33 75-01-4
Xylene (Total)
NO
ug/L
1.0
1
12/23/20 23:33 1330-20-7
m&p-Xylene
NO
ug/L
2.0
1
12/23/20 23:33 179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/23/20 23:33 95-47-6
Surrogates
4-Bromofluorabenzene(S)
98 %
70-130
1
12/23/20 23:33 460-00-4
1,2-Dichloroethane-d4 (S)
101 %
70-130
1
12/23/20 23:33 17060-07-0
Toluene-d8 (S)
100 %
70-130
1
12/23/20 23:33 2037-26-5
5310E TOC
Analytical Method: SM 531OB-2011
Pace Analytical Services -Asheville
Total Organic Carbon
1.9 mg/L
1.0
1
12/30/20 08:08 7440 44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/30/2020 04:21 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 16

Pace Analytical Services, LAC
® Kincey Ave. Suite 100
aceAnallah& l 9800 Huntersville, NC 28078
towq.paeNaha.eora
[phone]
ANALYTICAL RESULTS
Project: TOC & VOC T5827-RGM
Pace Project No.: 92513089
Sample: T5827-RGM Lab lD: 92513089001 Collected: 12/18/20 10:25 Received: 12/21/20 12:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
33.0
ug/L
25.0
1
12/23/20 23:33 67-64-1
Benzene
ND
ug/L
1.0
1
12123/20 23:33 71-43-2
Bromobenzene
ND
ug/L
1.0
1
12/23/20 23:33 108-86-1
Bromochloromethane
ND
ug/L
1.0
1
12/23/20 23:33 74-97-5
Bromodichloromethane
NO
ug/L
1.0
1
12/23/20 23:33 75-27-4
Bromoform
NO
ug/L
1.0
1
12/23/20 23:33 75-25-2
Bromomethane
NO
ug/L
2.0
1
12/23/20 23:33 74-83-9
2-Butanone (MEK)
ND
ug/L
6.0
1
12/23/20 23:33 78-93-3
Carbon tetrachloride
ND
ug/L
1.0
1
12123/20 23:33 56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/23/20 23:33 108-90-7
Chloroethane
ND
ug/L
1.0
1
12/23/20 23:33 75-00-3
Chloroform
ND
ug/L
5.0
1
12/23/20 23:33 67-66-3
Chloromethane
ND
ug/L
1.0
1
12/23/20 23:33 74-87-3
2-Chlorotoluene
ND
ug/L
1.0
1
12/23/20 23:33 9549-8
4-Chlorotoluene
NO
ug/L
1.0
1
12/23/20 23:33 106-43-4
1,2-Dibromo-3-chloropropane
NO
ug/L
5.0
1
12/23/20 23:33 96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/23/20 23:33 124-48-1
1,2-Dibromoethane (EOB)
ND
ug/L
1.0
1
12/23/20 23:33 106-93-4
Dibromomethane
ND
ug/L
1.0
1
023/20 23:33 74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/23/20 23:33 95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.0
1
12/23/20 23:33 541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/23/2023:33 106-46-7
Dichlorodifluoromethane
ND
ug/L
1.0
1
12/23/20 23:33 75-71-8
1,1-Dichloroethane
ND
ug/L
1.0
1
12/23/20 23:33 75-34-3
1,2-Dichloroethane
NO
ug/L
1.0
1
12/23/20 23:33 107-06-2
1,1-Dichloroethane
NO
ug/L
1.0
1
12/23/20 23:33 75-35-4
cis-1,2-Dichloroethene
NO
ug/L
1.0
1
12/23/20 23:33 156-59-2
trans-1,2-Dichloroethene
NO
ug/L
1.0
1
12/23/20 23:33 156-60-5
1,2-Dichloropropane
NO
ug/L
1.0
1
12/23/20 23:33 78-87-5
1,3-Dlchloropropane
ND
ug/L
1.0
1
12/23/20 23:33 142-28-9
2,2-Dichloropropane
NO
ug/L
1.0
1
12/23/20 23:33 594-20-7
1,1-Dichioropropene
ND
ug/L
1.0
1
12/23/20 23:33 563-58-6
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/23/2023:33 10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
1.0
1
12/23/20 23:33 10061-02-6
Diisopropyl ether
ND
ug/L
1.0
1
12/23/20 23:33 108-20-3
Ethylbenzene
ND
ug/L
1.0
1
12/23/20 23:33 100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
1.0
1
12/23/20 23:33 87-68-3
2-Hexanone
NO
ug/L
5.0
1
12/23/20 23:33 591-78-6
p-lsopropyltoluene
ND
ug/L
1.0
1
12/23/20 23:33 99-87-6
Methylene Chloride
ND
ug/L
5.0
1
12123/20 23:33 75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/23/20 23:33 108-10-1
Methyl-tert-butyl ether
ND
ug/L
1.0
1
12123/20 23:33 1634-04-4
Naphthalene
ND
ug/L
1.0
1
12/23/20 23:33 91-20-3
Styrene
ND
ug/L
1.0
1
12/23/20 23:33 100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12123/20 23:33 630-20-6
1,1,2,2-Tetrachloroethane
NO
ug/L
1.0
1
12/23/20 23:33 79-34-5
REPORT OF LABORATORY ANALYSIS
v2
IL
v2
This report shall not be reproduced, except In full,
Date: 12/30/2020 04:21 PM without the written consent of Pace Analytical Services, LLC, Page 4 of 16