WQ0036561_Residual Annual Report 2020_20210228

Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?*
Annual Report Year*
Permit Number (IR)*
Applicant/Permittee
Email Notifications
Does this need review by the hydrogeologist?*
Regional Office
CO Reviewer
Admin Reviewer
Annual Report
r Residual Annual Report
r Additional Information
r Other
2020
WQ0036561
City of Danville
r Yes c No

Submittal Form
Project Contact Information
Rease provide inforration on the person to be contacted by N B Staff
Name * Brent Collins
Email Address*
[e-mail]
electronic subnittal, confirmation of receipt, and other correspondence.
Project Information
........ ......... .......................................................................................................................
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
3367511441
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* W00036561
Fbs Current Existing permt number
Applicant/Permittee Address* 279 Park Avenue, Danville, VA24541
Facility Name * City of Danville RLAP
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Specifications, Calculations, Bc.)
2020 Danville Annual Report - WQ0036561.pdf 19.25MB
Upload only 1 FLFdocurrent (less than 250 NB). NLRiple docurrents rust be contained into one FDFfile unless file is larger than
upload limit.
* V By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
ff &kgw
Submission Date 2/28/2021

February 8, 2021
DENR/Water Quality Section
Non -Discharge Compliance Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2020 Annual Report — City of Danville, VA
Treatment and Land Application of Residuals
Permit No. WQ0036561
Dear Sir or Madam:
Enclosed is one copy of the 2020 Annual Report for the above referenced land
application permit
During 2020 EMA Resources, Inc. land applied 816.73 dry tons of wastewater residuals
to 228.17 acres of private farmland. Lime was ordered to be applied to the fields that had
a pH under 6.0. Site conditions have been too wet to apply the lime. Please contact Brent
Collins - Director of Technical Services if you have any further questions regarding this
report.
Sincerely,
Brent Collins
Director of Technical Services
brent.collins2emaresourcesinc.com
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

,EMA
---Resources, Inc.
City of Danville
2020 Annual Report
Residuals Land Application
Permit No. WQ0036561
Prepared By:
EMA Resources, Inc.
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: W00036561 County: Pittsylvania County, VA Year:
2020
Facility Name (as shown on permit):
City of Danville, Northside WWTP
Land Application Operator: EMA Resources inc. Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
❑ Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in thepermit:
33
Total number of fields utilized for land application during the year:
7
Total amount of dry tons applied during the year for all application sites:
F 816.73
Total number of acres utilizes for land application during the year:
1 228.17
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2020 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. 0 Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T. 1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the possibility
of fines and imprisonment for knowing violations."
Alan Johnson - Division Director of Water & Wastewater Treatment
Permittee Nam Title t c or print Signature of irer rii�
j�1_" �j� Date
/
0 /C/ / d90.) 1 �94;:; "' 1/20/2021
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
WQ0036561
Facility Name: City of Danville
Residual Source WQ # or
NPDES #:
VA0060593
WWTP Name: Northside WWTP
Residual Analysis Data
Laboratory;
1)
2)
3)
4)
5)
Waypoint Analytical
Parameter
(mg/kg)
Cone.
Limit
(mg/kg)
Sample or Composite Date
4/21/20
5/5/20
5/18/20
612/20
Average
Percent Solids (%)
NA
5.24
6.47
7.12
6.5
6.33
Arsenic
75
9.62
7.83
7.04
7.69
8.05
Cadmium
85
1.92
1.54
1.41
1.54
1.60
Copper
4,300
313
369
332
326
335.00
Chromium
NA
48.7
55.7
51.4
51.4
51.80
Lead
840
44.6
49.1
44.8
48.2
46.68
Mercury
57
0.944
1.21
1.42
1 1.01
1.15
Molybdenum
75
8.4
10.4
8.77
9.02
9.15
Nickel
420
59.8
66.9
62.8
63.2
63.18
Selenium
100
9.62
7.69
7.04
7.69
8.01
Zinc
7,500
2190
2220
2170
2250
2207.5
Total Phosphorus
NA
18900
20600
20100
20900
20125
TKN
NA
34800
41500
36500
43400
39050
Ammonia -Nitrogen
NA
11000
7820
4820
9110
8188
Nitrate and Nitrite
NA 1
235
71.8
83.1
366
188.98
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for snbmitti Ise information, including the possibility of fines and imprisonment for knowing violations."
Signature of
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
l 6` f /)0,)
Date
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
Facility Name:
Residual Source
NPDES # or WQ#:
WWTP Name:
Residual Analvsis Data
WQ0036561
City of Danville
VA0060593
Northside WWTP
Laboratory: 1) Waypoint Analytical
2)
3)
4)
5)
Sample or Composite Date
Parameter
(mg/kg)
4/21/20
5/5120
5/18/20
6/2/20
Average
Aluminum
30400
43100
34100
38000
36400
Calcium
11800
11600
11100
11600
11525
Magnesium
3310
3550
3230
3370
3365
pH
7.1
7.1
7
7.8
7.25
Potassium
3020
3340
2860
2850
3017.5
Sodium
13100
10500
9580
10600
10945
PAN
12875
14086
11997
15208
13541
SAR
6.27
5.55
5.48
5.66
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26)
lo/ %ao0"'1
Date
DENR FORM RSSF - B (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Danville Total Dry Tons Applied (Annual):
Permit #: WQ0036561 Cation Exchange Capacity (non 503 only):
Operator: James Blackwell Owner: James Blackwell Predominant Soil Series:
Acres Used: 26.6 Acres Permitted: 26.6 Site #: CS06 Field #:
90.68
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 1
Summer
Average
2
Unifi
4/9/20
3
4
5
6
7
8
9
10 J
11
12
% Solids
6.33
3.84
Arsenic
8.05
11
Cadmium
1.6
1.3
Copper
335
175
Chromium
51.8
54.7
Lead
46.68
64.7
Mercury
1.15
0.811
Molyb-
denum
9.15
3.42
Nickel
63.18
16.2
Selenium
8.01
12.9
Zinc
2207.5
716
Total
Phos-
horns
20125
4320
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1 1
2
3
4
5
6
7
8
9
10 J
11
12
DT/Ac./
App.
Event
3.10
0.31
Arsenic
1 0.050
0.007
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.057
Cadmium
0.010
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Copper
2.074
0.110
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.184
Chromium
0.321
0.034
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.355
Lead
0.289
0.041
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.330
Mercury
0.007
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Molyb-
0.057
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.059
denum
Nickel
0.391
0.010
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.000
0.401
Selenium
0.050
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.058
Zinc
13.669
0.448
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
14.117
Total
Phos-
124.614
2.704
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
127.318
horns
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 1/28/2021
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Danville
James Blackwell
Operator: James Blackwell
WQ Permit #: WQ0036561 Field #:
Annual Dry Tons Applied: 90.68 Site #:
Predominant Soil Series: FbB2
Crop 1 Name: Bermuda -Hay Crop 1 Max. PAN:
146
Crop 2 Name:
Acres Utilized: 26.6
CS06 Acres Permitted: 26.6
Cation Exchange Capacity (non 503): 0
Crop 2 Max. PAN:
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
F '5
w
*
o
o'
7�
* N
* w
o
TKN
mg/kg
o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
8/12
65000
6.33
0.645
Northside WWTP
Dry
<.5"
S
0.5
0.3
39050
8187.5
1 188.98
17.469
NA
Fescue
8/13
247000
6.33
2.451
Northside WWTP
Dry
<.5"
S
0.5
0.3
39050
8187.5
188.98
66.382
NA
Fescue
0.000
0.000
0.000
4/10
52000
3.84
0.313
Unifi, Inc.
Dry
<.5"
S
0.5
0.3
18700
8470
132
4.655
NA
Fescue
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
0
36400o
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
88.507
0.000
Lime Applied
Annuallbs/acre
0.057
0.011
2.184
0.355
0.330
0.008
0.059
0.401
0.058
14.117 177.3181
21.321
35.438
1 2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.172
0.044
25.448
1.864
1.103
0.027
0.207
0.866
0.072
2000
Current Cumulative lbs/ac
0.229
0.055
27.632
2.219
1.433
0.035
0.266
1.267
0.130
Permitted C. P. L. R. * * * *
1 36
34
1 1338
267
1 15
374
1 89
Permit PAN Limit 1 st/2nd Crop
1
1 146
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/28/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Danville Total Dry Tons Applied (Annual): 72.06
Permit #: WQ0036561 Cation Exchange Capacity (non 503 only):
Operator: James Blackwell Owner: James Blackwell Predominant Soil Series: FaB3
Acres Used: 20.7 Acres Permitted: 20.7 Site #: CS06 Field #: 3
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
3.48
Arsenic
0.056
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.056
Cadmium
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Copper
2.332
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.332
Chromiuni
0.361
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.361
Lead
0.325
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.325
Mercury
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Molyb-
0.064
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.064
denum
Nickel
0.440
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.440
Selenium
0.056
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.056
Zinc
15.369
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
15.369
Total
Phos-
140.110
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
140.110
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 1/20/2021
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Danville
James Blackwell
Operator: James Blackwell
WQ Permit #: WQ0036561 Field #:
Annual Dry Tons Applied: 72.06 Site #:
Predominant Soil Series: FaB3
Crop 1 Name: Fescue -Hay Crop 1 Max. PAN:
194
Crop 2 Name:
Acres Utilized: 20.7
CS06 Acres Permitted: 20.7
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
F '5
w
*
o
o'
7�
* N
* w
o
TKN
mg/kg
o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/19
52000
6.33
0.663
Northside WWTP
Dry
<.5"
S
0.5
0.3
39050
8187.5
1 188.98
17.958
NA
Fescue
7/20
221000
6.33
2.818
Northside WWTP
Dry
<.5"
S
0.5
0.3
39050
8187.5
188.98
76.323
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
0
27300o
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
94.282
0.000
Lime Applied
Annuallbs/acre
0.056
0.011
2.332
0.361
0.325
0.008
0.064
0.440
0.056
15.369 110.1101
55.602
70.971
1 2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.477
0.116
61.135
3.931
2.512
0.053
0.567
2.138
0.157
2000
Current Cumulative lbs/ac
0.533
0.127
63.467
4.292
2.837
0.061
0.631
2.578
0.213
Permitted C. P. L. R. * * * *
1 36
34
1 1338
267
1 15
374
1 89
Permit PAN Limit 1 st/2nd Crop
1
1 194
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/20/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Danville Total Dry Tons Applied (Annual):
Permit #: WQ0036561 Cation Exchange Capacity (non 503 only):
Operator: James Blackwell Owner: James Blackwell Predominant Soil Series:
Acres Used: 25.67 Acres Permitted: 25.67 Site #: CS06 Field #:
89.23
0
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
3.48
Arsenic
0.056
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.056
Cadmium
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Copper
2.329
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.329
Chromiuni
0.360
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.360
Lead
0.325
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.325
Mercury
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Molyb-
0.064
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.064
denum
Nickel
0.439
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.439
Selenium
0.056
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.056
Zinc
15.347
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
15.347
Total
Phos-
139.909
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
139.909
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 1/20/2021
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Danville WQ Permit #: WQ0036561 Field #: 4 Acres Utilized:
James Blackwell Annual Dry Tons Applied: 89.23 Site #: CS06 Acres Permitted:
James Blackwell
Crop 1 Name: Fescue -Pasture
Predominant Soil Series:
Crop 1 Max. PAN: 157
Z
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
25.67
25.67
0
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
11rs.
inches
a
F '5
w
*
o
o'
7�
* N
* w
o
TKN
mg/kg
o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/18
214500
6.33
2.206
Northside WWTP
Dry
<.5"
S
0.5
0.3
39050
8187.5
188.98
59.736
NA
Fescue
7/19
123500
6.33
1.270
Northside WWTP
Dry
<.5"
S
0.5
0.3
39050
8187.5
188.98
34.394
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
94.130
o.000
Lime Applied
Annuallbs/acre
0.056
0.011
2.329
0.360
0.325
0.008
0.064
0.439
0.056
15.347 139.909
44.011
59.358
1 2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.366
0.082
40.509
2.779
1.776
0.036
0.436
1.656
0.13
2000
Current Cumulative lbs/ac
0.422
0.093
42.838
3.139
2.101
0.044
0.500
2.095
0.186
Permitted C. P. L. R. * * * *
36
34
1 1338
267
15
374
1 89
Permit PAN Limit 1 st/2nd Crop
1 157
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/20/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Danville Total Dry Tons Applied (Annual): 70.34
Permit #: WQ0036561 Cation Exchange Capacity (non 503 only):
Operator: James Blackwell Owner: James Blackwell Predominant Soil Series: CgB2
Acres Used: 19.6 Acres Permitted: 19.6 Site #: CS07 Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
3.59
Arsenic
0.058
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.058
Cadmium
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Copper
2.405
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.405
Chromiuni
0.372
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.372
Lead
0.335
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.335
Mercury
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Molyb-
0.066
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.066
denum
Nickel
0.454
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.454
Selenium
0.057
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.057
Zinc
15.845
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
15.845
Total
Phos-
144.457
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
144.457
horus
1
1
1
1
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fZ4;��_
Signature of Land Applier
1/20/2021
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Danville
James Blackwell
Operator: James Blackwell
Crop 1 Name:
Fescue -Pasture
WQ Permit #: WQ0036561 Field #:
Annual Dry Tons Applied: 70.34 Site #:
Predominant Soil Series: C:;B2
Crop 1 Max. PAN:
156 Crop 2 Name:
Acres Utilized: 19.6
CS07 Acres Permitted: 19.6
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
0
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
11rs.
inches
F '5
w
*
o
o'
7�
* N
* w
o
TKN
mg/kg
o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/14
175500
6.33
2.364
Northside WWTP
Dry
<.5"
S
0.5
0.3
39050
8187.5
188.98
64.011
NA
Fescue
7/15
91000
6.33
1.226
Northside WWTP
Dry
<.5"
S
0.5
0.3
39050
8187.5
188.98
33.191
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
As
Cd
Cu
Cr
Pb
Hg,
Mo
Ni
Se
Zn P
97.202
o.000
Lime Applied
Annuallbs/acre
0.058
0.011
2.405
0.372
0.335
0.008
0.066
0.454
0.057
15.845 144.457
104.179
120.024
1 2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.659
0.215
106.92
6.188
4.622
0.083
0.874
3.81
0.305
Current Cumulative lbs/ac
0.717
0.226
109.325
6.560
4.957
0.091
0.940
4.264
0.362
Permitted C. P. L. R. * * * *
1 36
34
1 1338
267
15
374
89
Permit PAN Limit 1 st/2nd Crop
1
1 156
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/20/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Danville Total Dry Tons Applied (Annual):
WQ0036561 Cation Exchange Capacity (non 503 only):
James Blackwell Owner: James Blackwell Predominant Soil Series:
33.6 Acres Permitted: 33.6 Site #: CS07 Field #:
175.02
FpD
2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
5.21
Arsenic
0.084
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.084
Cadmium
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Copper
3.490
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.490
Chromiuni
0.540
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.540
Lead
0.486
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.486
Mercury
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.012
Molyb-
0.095
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.095
denum
Nickel
0.658
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.658
Selenium
0.083
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.083
Zinc
22.998
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
22.998
Total
Phos-
209.662
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
209.662
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fZ4;��_
Signature of Land Applier
1/20/2021
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Danville
James Blackwell
Operator: James Blackwell
Crop 1 Name: Fescue -Hay
WQ Permit #: WQ0036561 Field #:
Annual Dry Tons Applied: 175.02 Site #:
Predominant Soil Series: FpD
Crop 1 Max. PAN:
158 Crop 2 Name:
Acres Utilized: 33.6
CS07 Acres Permitted: 33.6
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
0
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
F '5
w
*
o
o'
7�
* N
* w
o
TKN
mg/kg
o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/15
117000
6.33
0.919
Northside WWTP
Dry
<.5"
S
0.5
1 0.3
39050
8187.5
188.98
24.893
NA
Fescue
7/16
214500
6.33
1.685
Northside WWTP
Dry
<.5"
S
0.5
0.3
39050
8187.5
188.98
45.638
NA
Fescue
7/17
214500
6.33
1.685
Northside WWTP
Dry
<.5"
S
0.5
0.3
39050
8187.5
188.98
45.638
NA
Fescue
8/14
117000
6.33
0.919
Northside WWTP
Dry
<.5"
S
0.5
0.3
39050
8187.5
188.98
24.893
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this
form):
TOTALS:
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
141.0621
0.000
Lime Applied
Annuallbs/acre
0.084 0.017 3.490 0.540 0.486 0.012 0.095 0.658 0.083 22.998 209.662
0.648 0.183 108.87 5.739 4.263 0.077 0.73 3.314 0.264 99.133
0.732 0.200 112.360 6.279 4.749 0.089 0.825 3.972 0.347 122.131
1 36 34 1 1338 267 1 15 374 1 89 1 2498
1 158
Date
lbs/ac
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R. * * * *
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/20/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Danville Total Dry Tons Applied (Annual): 87.06
Permit #: WQ0036561 Cation Exchange Capacity (non 503 only):
Operator: Glenn Hodges Owner: Glenn Hodges Predominant Soil Series: CgB2
Acres Used: 37 Acres Permitted: 37 Site #: CS09 Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
Summer
Average
2
Unifi
4/9/20
3
4
5
6
7
8
9
10 J
11
12
% Solids
6.33
3.84
Arsenic
8.05
11
Cadmium
1.6
1.3
Copper
335
175
Chromium
51.8
54.7
Lead
46.68
64.7
Mercury
1.15
0.811
Molyb-
denum
9.15
3.42
Nickel
63.18
16.2
Selenium
8.01
12.9
Zinc
2207.5
716
Total
Phos-
horns
20125
4320
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1 1
2
3
4
5
6
7
8
9
10
11
12
DT/Ac./
App.
Event
1.76
0.59
Arsenic
1 0.028
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.041
Cadmium
0.006
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
1.181
0.207
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.387
Chromium0.183
0.065
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.247
Lead
0.165
0.076
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.241
Mercury
0.004
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Molyb-
0.032
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.036
denum
Nickel
0.223
0.019
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.242
Selenium
0.028
0.015
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.043
Zinc
7.779
0.846
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
8.626
Total
Phos-
70.921
5.106
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
76.027
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fZ4;��_
Signature of Land Applier
1/28/2021
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Danville
Glenn Hodges
Operator: Glenn Hodges
Crop 1 Name:
Fescue -Pasture
WQ Permit #: WQ0036561 Field #:
Annual Dry Tons Applied: 87.06 Site #:
Predominant Soil Series: C:;B2
Crop 1 Max. PAN:
156 Crop 2 Name:
Acres Utilized: 37
CS09 Acres Permitted: 37
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
F '5
w
*
o
o'
7�
* N
* w
o
TKN
mg/kg
o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/21
195000
6.33
1.391
Northside WWTP
Dry
<.5"
S
0.5
0.3
39050
8187.5
188.98
37.676
NA
Fescue
7/22
52000
6.33
0.371
Northside WWTP
Dry
<.5"
S
0.5
0.3
39050
8187.5
188.98
10.047
NA
Fescue
0.000
0.000
0.000
4/8
136500
3.84
0.591
Unifi, Inc.
Dry
<.5"
S
0.5
0.3
18700
8470
132
8.786
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this
form):
TOTALS:
0
3s35oo
As
Cd
Cu
Cr
Pb
Hg,
Mo
Ni
Se
Zn
P
56.509
o.000
Lime Applied
Annuallbs/acre
0.041 0.007 1.387 0.247 0.241 0.005 0.036 0.242 0.043 8.626 76.027
0.101 0.032 5.446 0.889 0.7 0.015 0.17 0.846 0.063 23.565
0.142 0.039 6.833 1.136 0.941 0.020 0.206 1.088 0.106 32.191
1 36 34 1 1338 267 15 374 89 1 2498
1 156
Date
lbs/ac
Prior Years Cumulative lbs/ac
2000
Current Cumulative lbs/ac
Permitted C. P. L. R. * * * *
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/28/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Danville Total Dry Tons Applied (Annual):
Permit #: WQ0036561 Cation Exchange Capacity (non 503 only):
Operator: Glenn Hodges Owner: Glenn Hodges Predominant Soil Series:
Acres Used: 65 Acres Permitted: 65 Site #: CS09 Field #:
262.54
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
4.04
Arsenic
0.065
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.065
Cadmium
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
Copper
2.706
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.706
Chromiuni
0.418
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.418
Lead
0.377
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.377
Mercury
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Molyb-
0.074
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.074
denum
Nickel
0.510
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.510
Selenium
0.065
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.065
Zinc
17.832
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
17.832
Total
Phos-
162.570
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
162.570
horus
1
1
1
1
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fZ4;��_
Signature of Land Applier
1/20/2021
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Danville WQ Permit #: WQ0036561 Field #: 3 Acres Utilized:
Glenn Hodges Annual Dry Tons Applied: 262.54 Site #: CS09 Acres Permitted:
Glenn Hodges
Crop 1 Name: Fescue -Pasture
Predominant Soil Series:
Crop 1 Max. PAN: 125
I'
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
65
65
0
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
a
F '5
w
*
o
o'
7�
* N
* w
o
TKN
mg/kg
o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/22
162500
6.33
0.660
Northside WWTP
Dry
<.5"
S
0.5
0.3
39050
8187.5
188.98
17.872
NA
Fescue
7/23
104000
6.33
0.422
Northside WWTP
Dry
<.5"
S
0.5
0.3
39050
8187.5
188.98
11.438
NA
Fescue
8/5
136500
6.33
0.554
Northside WWTP
Dry
<.5"
S
0.5
0.3
39050
8187.5
188.98
15.013
NA
Fescue
8/10
188500
6.33
0.765
Northside WWTP
Dry
<.5"
S
0.5
0.3
39050
8187.5
188.98
20.732
NA
Fescue
8/11
1
240500
6.33
0.977
Northside WWTP
Dry
<.5"
S
1 0.5
0.3
39050
8187.5
188.98
26.451
NA
Fescue
8/12
162500
6.33
0.660
Northside WWTP
Dry
<.5"
S
0.5
0.3
39050
8187.5
188.98
17.872
NA
Fescue
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this
form):
TOTALS:
0
99450o
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
109.377
0. 000
Lime Applied
Annuallbs/acre
0.065 0.013 2.706 0.418 0.377 0.009 0.074 0.510 0.065 17.832 162.570 1
0.101 0.032 5.446 0.889 0.7 0.015 0.17 0.846 0.063 23.565
0.166 0.045 8.152 1.307 1.077 0.024 0.244 1.356 0.128 41.397
1 36 34 1 1338 1 267 1 15 374 1 89 1 2498
1 1 125
Date
lbs/ac
Prior Years Cumulative lbs/ac
2000
Current Cumulative lbs/ac
Permitted C. P. L. R. * * * *
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/20/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Waypointo
ANALYTICAL
5/7/2020
Inframark
A/P
Northside WWTP
229 Northside Drive
Danville, VA, 24540
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Ref: Analytical Testing
Report Number: 20-115-0001
Project Description: WASTEWATER TREAT PLANT
VPDES PERMIT# VA0060593
Dear A/P:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/24/2020 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pam« mar,--
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 14

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 20-115-0001
Client Project Description: WASTEWATER TREAT PLANT
VPDES PERMIT# VAOO6O593
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
71153
LTS B-Basin 20-1262A
Solids
04/21/2020 09:00
04/24/2020
71153
LTS B-Basin 20-1262A
Solids
04/21/2020 09:00
04/24/2020
9045D
WP MTN
71153
LTS B-Basin 20-1262A
Solids
04/21/2020 09:00
04/24/2020
SM-2320 B
WP MTN
71153
LTS B-Basin 20-1262A
Solids
04/21/2020 09:00
04/24/2020
6010D
WP MTN
71153
LTS B-Basin 20-1262A
Solids
04/21/2020 09:00
04/24/2020
4500NO3F-2011
WP MTN
71153
LTS B-Basin 20-1262A
Solids
04/21/2020 09:00
04/24/2020
SW-7471B
WP MTN
71153
LTS B-Basin 20-1262A
Solids
04/21/2020 09:00
04/24/2020
SM-4500-NH3C
WP MTN
71153
LTS B-Basin 20-1262A
Solids
04/21/2020 09:00
04/24/2020
SM-4500-NH3C-TKN
WP MTN
71153
LTS B-Basin 20-1262A
Solids
04/21/2020 09:00
04/24/2020
SM-2540G
WP MTN
71154
LTS B-Basin 20-1262C
Solids
04/21/2020 09:00
04/24/2020
SW-9045C
WP MTN
71154
LTS B-Basin 20-1262C
Solids
04/21/2020 09:00
04/24/2020
SW-7.3.4
WP MTN
71154
LTS B-Basin 20-1262C
Solids
04/21/2020 09:00
04/24/2020
SW-7.3.3
WP MTN
71154
LTS B-Basin 20-1262C
Solids
04/21/2020 09:00
04/24/2020
ASTM D93-80
WP MTN
71155
LTS B-Basin 20-1262B
TCLP
04/21/2020 09:00
04/24/2020
SW-1311 (ZHE)
WP MTN
71155
LTS B-Basin 20-1262B
TCLP
04/21/2020 09:00
04/24/2020
SW-1311
WP MTN
71155
LTS B-Basin 20-1262B
TCLP
04/21/2020 09:00
04/24/2020
8270C
WP MTN
71155
LTS B-Basin 20-1262B
TCLP
04/21/2020 09:00
04/24/2020
8260B
WP MTN
71155
LTS B-Basin 20-1262B
TCLP
04/21/2020 09:00
04/24/2020
8151A
WP MTN
71155
LTS B-Basin 20-1262B
TCLP
04/21/2020 09:00
04/24/2020
8081A
WP MTN
71155
LTS B-Basin 20-1262B
TCLP
04/21/2020 09:00
04/24/2020
7470A
WP MTN
71155
LTS B-Basin 20-1262B
TCLP
04/21/2020 09:00
04/24/2020
6010D
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 14

�'
WayP
7621 Whitepine Road, Richmond,
VA 23237
Main 804-743-9401 Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
79434
Inframark
Robert
Clifton/Kim Wickemeyer
A/P
Project
WASTEWATER TREAT PLANT
Report Date : 05/07/2020
Northside WWTP
Information : VPDES
PERMIT# VA0060593
Received : 04/24/2020
229 Northside Drive
Danville VA 24540
Pr�c mL G
,
Submitted By : Robert Clifton/Kim Wickemeyer
Pauric McGroary
Report Number : 20-115-0001
REPORT OFANALYSIS
Agronomist
Lab No : 71153
Matrix:
Solids
Sample ID : LTS B-Basin 20-1262A
Sampled:
4/21/2020 9:00
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Moisture
94.8
%
0.010
1
04/27/20 16:38
CJR SM-2540G
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Alkalinity (as CaCO3)
36500
mg/Kg -
dry
1920
1
04/29/20 10:40
CMF SM-2320 B
Ammonia Nitrogen
11000
mg/Kg -
dry
1920
1
05/06/20 14:00
JPJ SM-4500-NH3C
Nitrate+Nitrite-N
235
mg/Kg -
dry
96.2
1
04/30/20 14:44
ZBD 4500NO3F-2011
Organic N
23800
mg/Kg -
dry
4810
1
05/06/20 10:00
CALCULATION
pH
7.1
S.U.
1
05/05/20 06:32
JSL 9045D
Total Solids
5.24
%
0.010
1
04/27/20 16:38
CJR SM-2540G
Total Volatile Solids
44.7
%
0.010
1
04/27/20 16:38
CJR SM-2540G
Total Kjeldahl Nitrogen
34800
mg/Kg -
dry
4810
1
05/06/20 10:00
JPJ ;M-4500-NH3C-TKI`
Phosphorus
18900
mg/Kg -
dry
96.2
1
04/28/20 23:24
KKM 6010D
Aluminum
30400
mg/Kg -
dry
96.2
1
04/29/20 17:41
TJS 6010D
Arsenic
<9.62
mg/Kg -
dry
9.62
1
04/28/20 23:24
KKM 6010D
Calcium
11800
mg/Kg -
dry
962
1
04/28/20 23:24
KKM 6010D
Cadmium
<1.92
mg/Kg -
dry
1.92
1
04/28/20 23:24
KKM 6010D
Chromium
48.7
mg/Kg -
dry
4.81
1
04/28/20 23:24
KKM 6010D
Copper
313
mg/Kg -
dry
9.62
1
04/28/20 23:24
KKM 6010D
Iron
32900
mg/Kg -
dry
192
1
04/28/20 23:24
KKM 6010D
Lead
44.6
mg/Kg -
dry
5.77
1
04/28/20 23:24
KKM 6010D
Qualifiers/ DF Dilution Factor
L
Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 3 of 14

�'
WayP
7621 Whitepine Road, Richmond,
VA 23237
Main 804-743-9401 Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
79434
Inframark
Robert
Clifton/Kim Wickemeyer
A/P
Project
WASTEWATER TREAT PLANT
Report Date : 05/07/2020
Northside WWTP
Information :
VPDES
PERMIT# VA0060593
Received
: 04/24/2020
229 Northside Drive
Danville VA 24540
Pr�c
mL G
,
Submitted By : Robert Clifton/Kim Wickemeyer
Pauric McGroary
Report Number : 20-115-0001
REPORT OFANALYSIS
Agronomist
Lab No : 71153
Matrix:
Solids
Sample ID : LTS B-Basin 20-1262A
Sampled:
4/21/2020 9:00
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Magnesium
3310
mg/Kg
- dry
96.2
1
04/28/20 23:24
KKM
6010D
Manganese
1020
mg/Kg
- dry
9.62
1
04/28/20 23:24
KKM
6010D
Mercury
0.944
mg/Kg
- dry
0.283
1
04/30/20 16:42
DDB
SW-7471B
Molybdenum
8.40
mg/Kg
- dry
4.81
1
04/28/20 23:24
KKM
6010D
Nickel
59.8
mg/Kg
- dry
4.81
1
04/28/20 23:24
KKM
6010D
Potassium
3020
mg/Kg
- dry
192
1
04/28/20 23:24
KKM
6010D
Selenium
<9.62
mg/Kg
- dry
9.62
1
04/28/20 23:24
KKM
6010D
Sodium
13100
mg/Kg
- dry
481
1
04/28/20 23:24
KKM
6010D
Zinc
2190
mg/Kg
- dry
24.0
1
04/28/20 23:24
KKM
6010D
Sulfur
9370
mg/Kg
- dry
192
1
04/28/20 23:24
KKM
6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Page 4 of 14

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 79434
Customer Name: Inframark
Report Number: 20-115-0001
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
® UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: lBrandi Watson Date & Time: 04/24/2020 10:03:36
Page 11 of 14

`)Ll6--% t
Client Name/Address
Client Project Manager/Contact
Billing Information
2a115-0007
IIi`IIJII
Dan�lie vvvra
Robert Clifton - Loh Mgr.
Inframar
IIIIIIIIIII III IlI1fI1IIIIIIII1I
79434Inframark
229 Northside Dr,
Kim Wlckerneyer - Sr. Lab Tech.
229 Nvrthside Dr.
04.24-2020
ntramdrk D9:59 32
Data Ale, VA 24540
Danville. VA 24540
method
WASTEWATER TREAT PLANT
Project Description
Project/Site Location lCity/State)
RUSE+-Addinonal charges apply
VPDES Permit #:
Danville, VA
special Detection Umitlsj
❑ I-ed L ,
Date ResuitsNeeded
Courier ❑CliensD
El
port ow - DrinicingWater S- Soil/Solid 0-0I
VA0060593
Wastewater Treatment Plant
O - Product M - Mrsc
0511512020
orh�r
project Number
"*a Manager Phone ■
Project Manases Email
Purchase order Number
Site/Facility ID R
waypoint Acct. 79434
434-799-5137
robert.d1fton c@inframaric-com
101352
VPQES #- VA0060593
A Cool < MC Nan ZO3 (Mk to Qnh)
�y �j;
GWay
8 Coto c= K
C
point
K
;e
None equ
0 None Rputred
ANALYTICAL
.t,
E
t N20H PH>L4
2a40 Whitten Read
Unless rested, ail containers
a
T
x
o
`o
J
_ J
Lf.YL
F HM03 VOQ
G � �
'AcWhis TN 38133
TaVe n of 4a CFFt Part
H K3PO4
(901) 213-240D
Per
E
t
toot — K MAM203
136.
Date
Time Sample Identity ation
Required Analysis / Preservative
Comments/Notts
o.rttrx�
LTS B-Basin 20-1262A
I
S
G
1 4/
1
1
O.5 L plastic, preservative = B
LTS B-Basin 20-1262B
I
Is
C
1 L amber glass; preservative = B
LTS B-Basin 20-1262C 1
S C ll✓
1 L amber glass; preservative = 9
Lab# E 71153-1
LTS B-Basin 20-1252A
Cust: 79434 Inframark
CIA: 04/21/2020 04:00
20 115-040{
ReC: 04/24/2020 00:Do
Preservation: r = 6 degrees C
Lab# E 71155-1
LTS B-Basin
20-12626
Cult: 79434 Inframark
ME
Lab# E 71154-1
Cal: 04/21/202009:00 Rec: 04/ 24/ 2020 00:00
20-115-0001
LTS B-Basin 20-1262C
Preservatlon: HNO3,PH
< 2
Cust: 79434 Inframark
CDI: 04/21/2020 09.00 Rec: 04/24/2020 00:00
20-115.0001
Preservatron;
I L
led by (Name - Print)
Client Remarks/Comments
Ice Ga
tabCarnmGntY
F<Dbei Clifton
All Analyses must be performed by a certified lab
sears
Sek
C)/ H
l L
Tirm
Received by: (SIGNATURE) Date Time
Y
R
uisheQ by' {SIGNATURE}
C
Date
��Jz.o res�Z
BlankIr ler emP
Relinquish (SIGNATURE)
Date Time
Received by. (SIGNATURE) Rate lime
c��''
Relinquished by: (SIGNATURE)
Date Time
Received by: (SIGNATURE) Date Time

L: S
12)
� a - LaUa.�► w
Required Tests for inframark-Danville, VA WWTP (Waypoint VA Account 79434)
✓%Ts
ViATVS
./p H
./Alkalinity
,4N
,/Ammonia -Nitrogen
.Nitrate + Nitrite as Nitrogen
-#/Organic Nitrogen (calculation)
Phosphorus
_4P0ta5siurn
."/5uIfur
'/Calcium
./Magnesium
./Sodium
/Iron
./A/luminum
•/Manganese
Copper
� f
m
Zi
..f nc
m
n
%/Cadmium
Chromium
z
t%Nickel
Aead
— Arsenic
Lh NA [[Onnnn
W N��
,Mercury
Selenium
J
..IGiolybdenum
Page 13 of 14

Purchase Order
1NFRAMARK
Date: 4/20/2020
PO#: 101352
Bill To Buyer Name: Anjelina Munoz
229 Northside Drive Buyer Email: anjelina.muriozC(_Lnfrarnark.corrr
Danville Virginia 24540 End User Name: Kimberly Wickemeyer
United States End User Email: kim erly__,wickemeyer5inframark.corn
Vendor: Ship To:
Waypoint Analytical Inc 229 Northside Drive
Danville Virginia 24540
United States
Item
Description
Qty
units
EDD
Rate
Amount Memo
SIP00017
SL2 Biosolids Test pack
1
Ea
5129/2020
$79 80
$79.80
SIP00017
503E Metals
1
Ea
5/29/2020
5249.90
$249.90
SIP00017
Nitrogen Series
1
Ea
5/29/2020
$42 00
$42.00
SIP00017
Total Volatile Solids
1
Ea
5129/2020
$17 85
$17 B5
SIP0001 7
Total Alkanity
1
Ea
512W2020
$16 80
$16.80
SJP00017
pH
1
Ea
512g12020
S15 75
$15.75
SIP00017
TCLP
1
Ea
5/29/2020
51,075.00
$1.07500
SIP00017
ICIR
1
Ea
5/29/2020
$160 00
$160 00
Vendor Acceptance.
Date
Total $1,65710
Inframark, LLC General Conditions of Purchase, a copy of which is available at https 11www.inframark.com/contact-usldoi
with -us) , and any specific conditions or other terms not inctuded in these General Conditions of Purchase that are mul
upon in writing (herein after "Specific Conditions") shall govern this Purchase Order, In the event of a conflict between
Conditions noted in the Purchase Order and the General Conditions of Purchase. the Specific Conditions shall control
conditions inctuded in any Supplier documentation are specifically rejected by Purchaser and shall be of no effect on 9
Order
Page 14 of 14

Waypointo
ANALYTICAL
5/15/2020
Inframark
A/P
Northside WWTP
229 Northside Drive
Danville, VA, 24540
Ref: Analytical Testing
Report Number: 20-128-0010
Project Description: VPDES #VA0060593
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear A/P:
Waypoint Analytical Virginia, Inc. received sample(s) on 5/7/2020 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pam« mar,--
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 20-128-0010
Client Project Description: VPDES #VAOO6O593
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
71292
LTS B
Basin
20-1299
Solids
05/05/2020
08:00
05/07/2020
71292
LTS B
Basin
20-1299
Solids
05/05/2020
08:00
05/07/2020
71292
LTS B
Basin
20-1299
Solids
05/05/2020
08:00
05/07/2020
71292
LTS B
Basin
20-1299
Solids
05/05/2020
08:00
05/07/2020
71292
LTS B
Basin
20-1299
Solids
05/05/2020
08:00
05/07/2020
71292
LTS B
Basin
20-1299
Solids
05/05/2020
08:00
05/07/2020
71292
LTS B
Basin
20-1299
Solids
05/05/2020
08:00
05/07/2020
71292
LTS B
Basin
20-1299
Solids
05/05/2020
08:00
05/07/2020
71292
LTS B
Basin
20-1299
Solids
05/05/2020
08:00
05/07/2020
SM-2540G
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SM-4500-NH3C
WP MTN
9045D
WP MTN
SM-2320 B
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 7

�'
WayP
7621 Whitepine
Road, Richmond,
VA 23237
Main 804-743-9401 Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
79434
Inframark
A/P
Project
VPDES
#VA0060593
Report Date : 05/15/2020
Northside WWTP
Information :
Received : 05/07/2020
229 Northside Drive
Danville VA 24540
Pr�c mL G
,
Pauric McGroary
Report Number : 20-128-0010
REPORT OFANALYSIS
Agronomist
Lab No : 71292
Matrix:
Solids
Sample ID : LTS B Basin 20-1299
Sampled:
5/5/2020 8:00
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Moisture
93.5
%
0.010
1
05/11/20 15:35
CJR SM-2540G
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Alkalinity (as CaCO3)
36600
mg/Kg -
dry
1540
1
05/12/20 11:09
CMF SM-2320 B
Ammonia Nitrogen
7820
mg/Kg -
dry
1540
1
05/14/20 13:00
JPJ SM-4500-NH3C
Nitrate+Nitrite-N
<71.8
mg/Kg -
dry
71.8
1
05/11/20 13:41
ZBD 4500NO3F-2011
Organic N
33700
mg/Kg -
dry
3850
1
05/14/20 10:00
CALCULATION
pH
7.1
S.U.
1
05/12/20 06:40
JSL 9045D
Total Solids
6.47
%
0.010
1
05/11/20 15:35
CJR SM-2540G
Total Volatile Solids
44.9
%
0.010
1
05/11/20 15:35
CJR SM-2540G
Total Kjeldahl Nitrogen
41500
mg/Kg -
dry
3850
1
05/14/20 10:00
JPJ ;M-4500-NH3C-TKI`
Phosphorus
20600
mg/Kg -
dry
76.9
1
05/08/20 17:18
KKM 6010D
Aluminum
43100
mg/Kg -
dry
76.9
1
05/08/20 17:18
KKM 6010D
Arsenic
7.83
mg/Kg -
dry
7.69
1
05/08/20 17:18
KKM 6010D
Calcium
11600
mg/Kg -
dry
769
1
05/08/20 17:18
KKM 6010D
Cadmium
<1.54
mg/Kg -
dry
1.54
1
05/08/20 17:18
KKM 6010D
Chromium
55.7
mg/Kg -
dry
3.85
1
05/08/20 17:18
KKM 6010D
Copper
369
mg/Kg -
dry
7.69
1
05/12/20 15:32
TJS 6010D
Iron
35800
mg/Kg -
dry
154
1
05/08/20 17:18
KKM 6010D
Lead
49.1
mg/Kg -
dry
4.62
1
05/08/20 17:18
KKM 6010D
Qualifiers/ DF Dilution Factor
L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 3 of 7

waypANALYTICAL
79434
Inframark
A/P
Northside WWTP
229 Northside Drive
Danville , VA 24540
Report Number : 20-128-0010
Lab No : 71292
Sample ID : LTS B Basin 20-1299
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Project VPDES #VA0060593
Information :
REPORT OFANALYSIS
Report Date : 05/15/2020
Received : 05/07/2020
Psi' mL (fever
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 5/5/2020 8:00
Test
Results
Units
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Magnesium
3550
mg/Kg
- dry
76.9
1
05/08/20 17:18
KKM
6010D
Manganese
1160
mg/Kg
- dry
7.69
1
05/08/20 17:18
KKM
6010D
Mercury
1.21
mg/Kg
- dry
0.243
1
05/11/20 12:21
DDB
SW-7471B
Molybdenum
10.4
mg/Kg
- dry
3.85
1
05/08/20 17:18
KKM
6010D
Nickel
66.9
mg/Kg
- dry
3.85
1
05/08/20 17:18
KKM
6010D
Potassium
3340
mg/Kg
- dry
154
1
05/08/20 17:18
KKM
6010D
Selenium
<7.69
mg/Kg
- dry
7.69
1
05/08/20 17:18
KKM
6010D
Sodium
10500
mg/Kg
- dry
385
1
05/11/20 12:58
TJS
6010D
Zinc
2220
mg/Kg
- dry
19.2
1
05/08/20 17:18
KKM
6010D
Sulfur
9510
mg/Kg
- dry
154
1
05/08/20 17:18
KKM
6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Page 4 of 7

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 79434
Customer Name: Inframark
Report Number: 20-128-0010
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
® UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: lBrandi Watson Date & Time: 05/07/2020 15:26:45
Page 5 of 7

Billing information Illlll III IIII IIIII IIIII I Ill ICIIIII III ! IUII III I IIII III
Client NameJAddress
L}Iertt Project ManagerlConran
Inframark - Danville WVVTP
Robert Clifton - Lab Mgf.
079434
5-07 2020
Infrafnark nftamalk 152549
229 Northlside Or.
Kim Wlckernepx - Sr- Lab Tech-
229 Northside Dr VPDES #VQDD50593
Danville. VA 24540
{7anville, VA 24540
RUSS - Acid iIionai charges aPoly -- -- - ----- •--.
special Detection [] Fed Ex � ✓ jUPS C3USPS WW - Wastewater GW - Groundwater
Project Descrtotion
Project/Site Uocatlon fChy/StateI
VPDES Permit #:
Danville, VA
omit(s)
Date Results Needed Courier �ClienIompO f llW- D rin king Wa ter 5-5WIJSolid 0-Oil
Vldl� UrJ��
Wastewater Treatment Plant
P-Product M-Mlst
05/30/2020 C3ttler
Project Number
Project Manager Phone x
Project Manager Email
Purchase Order Number�y
Site/Facility 10 Of
Waypoint Acct. 79434
434-799-51 37
robertclifton@inframark -com
! D
VPDES #: VA0060593
A Coal < 10C Na2S2Q3 {Micro 6nry]
w�y�o�nt
s `0°'`.�
C H2SD4 pHti
ANALY7lCAl
x
n
0 None Requlrad
E
a
z
7790 Whitten Rand
�
u
u
Fp�pK30
HM03 Pi 1
HCLp
Mcmphis. TN 38133
[finless rested, all amitainers
it:
`a
�
(901 ) 213 2400
per Ta We It of 40 CFR Pan
$
£
T
w
g
P Ha
Cad — &C NAIS103
136
�
x
n
�
Date
irme
sample Identification
Required
Analysis j Preservative
CarnmentsJNotes
"�.�
° o
LTS B-Basin 20- �,�a
S
C
0.5 L plastic-, preservative = B
Lab# E 71292-1 LTS B Brim 20-1299
{
Cust: 79434 Inframark
Col: 05/05/2020 08:00 ReC: 05/07/2020 00:00
-
20-128-01)ta PreSerVatlon: < = 5 degrees C
For Laboratory Use Only
Sampled by [Name - Print)
Robert Clifton
L71ent Remar"tComments
All Analyses must be b a certified lab
C
Lab COryMl9ents
N
Seal
Seats
performed
Reli he by: !SIGNATURE]
Date
Received 6y: (SIGNATURE)
Date Time
LJ
�nTim�e}
Blank ooler mp
Relinquished by: tSiGNA E]
Date Time
Recehred 4y. (SIGNATURT)
Date Time
d[r
Relinquished by: (51GNATURE)
Date Time
eh VV: t51GNA }
Date Time
L

�/%T5
%TVs
PH
Alkalinity
J TKN
Ammonia -Nitrogen
Nitrate t Nitrite as Nitrogen
Organic Nitrogen (calculation)
/Phosphorus
,/ Potasslum
.,,/Sulfur
,Aalcium
✓MMagnesium
"Sodium
,Aron
.!Aluminum
./Aanganese
../Copper
,47"inc
.Cadmium
16romium
LAickel
,/Lead
Arsenic
,/(Aercury
'''Selenium
LMolyhdenum
Required Biosolids Tests for Inframark Danville, VA 14WTP
o'-nP°� sty 3�n
zo -1z99
Page 7 of 7

Waypointo
ANALYTICAL
6/2/2020
Inframark
A/P
Northside WWTP
229 Northside Drive
Danville, VA, 24540
Ref: Analytical Testing
Report Number: 20-143-0003
Project Description: Wastewater Treatment Plant
VPDES Permit# VA0060593
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear A/P:
Waypoint Analytical Virginia, Inc. received sample(s) on 5/22/2020 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pam« mar,--
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 20-143-0003
Client Project Description: Wastewater Treatment Plant
VPDES Permit# VAOO6O593
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
71772
LTS B-Basin
20-1327
Solids
05/18/2020
09:00
05/22/2020
71772
LTS B-Basin
20-1327
Solids
05/18/2020
09:00
05/22/2020
71772
LTS B-Basin
20-1327
Solids
05/18/2020
09:00
05/22/2020
71772
LTS B-Basin
20-1327
Solids
05/18/2020
09:00
05/22/2020
71772
LTS B-Basin
20-1327
Solids
05/18/2020
09:00
05/22/2020
71772
LTS B-Basin
20-1327
Solids
05/18/2020
09:00
05/22/2020
71772
LTS B-Basin
20-1327
Solids
05/18/2020
09:00
05/22/2020
71772
LTS B-Basin
20-1327
Solids
05/18/2020
09:00
05/22/2020
71772
LTS B-Basin
20-1327
Solids
05/18/2020
09:00
05/22/2020
SM-2540G
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SM-4500-NH3C
WP MTN
9045D
WP MTN
SM-2320 B
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 7

�'
WayP
7621 Whitepine Road, Richmond,
VA 23237
Main 804-743-9401 Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
79434
Inframark
A/P
Project
Wastewater Treatment Plant
Report Date : 06/02/2020
Northside WWTP
Information : VPDES
Permit# VA0060593
Received : 05/22/2020
229 Northside Drive
Danville VA 24540
Pr�c mL G
,
Pauric McGroary
Report Number : 20-143-0003
REPORT OFANALYSIS
Agronomist
Lab No : 71772
Matrix: Solids
Sample ID : LTS B-Basin 20-1327
Sampled: 5/18/2020 9:00
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Moisture
92.9 H
%
0.010
1
05/26/20 18:11
ADM SM-2540G
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Alkalinity (as CaCO3)
26800
mg/Kg -
dry
1410
1
05/28/20 11:30
CJD SM-2320 B
Ammonia Nitrogen
4820
mg/Kg -
dry
352
1
06/01/20 14:00
JPJ SM-4500-NH3C
Nitrate+Nitrite-N
83.1
mg/Kg -
dry
69.3
1
05/26/20 15:42
ZBD 4500NO3F-2011
Organic N
31700
mg/Kg -
dry
3520
1
06/01/20 10:00
CALCULATION
pH
7.0
S.U.
1
06/01/20 06:42
JSL 9045D
Total Solids
7.12 H
%
0.010
1
05/26/20 18:11
ADM SM-2540G
Total Volatile Solids
45.0 H
%
0.010
1
05/26/20 18:11
ADM SM-2540G
Total Kjeldahl Nitrogen
36500
mg/Kg -
dry
3520
1
06/01/20 10:00
JPJ ;M-4500-NH3C-TKl`
Phosphorus
20100
mg/Kg -
dry
70.4
1
05/27/20 20:54
TJS 6010D
Aluminum
34100
mg/Kg -
dry
70.4
1
05/27/20 20:54
TJS 6010D
Arsenic
<7.04
mg/Kg -
dry
7.04
1
05/27/20 20:54
TJS 6010D
Calcium
11100
mg/Kg -
dry
704
1
05/27/20 20:54
TJS 6010D
Cadmium
<1.41
mg/Kg -
dry
1.41
1
05/27/20 20:54
TJS 6010D
Chromium
51.4
mg/Kg -
dry
3.52
1
05/27/20 20:54
TJS 6010D
Copper
332
mg/Kg -
dry
7.04
1
05/27/20 20:54
TJS 6010D
Iron
36200
mg/Kg -
dry
141
1
05/27/20 20:54
TJS 6010D
Lead
44.8
mg/Kg -
dry
4.23
1
05/27/20 20:54
TJS 6010D
Qualifiers/ DF Dilution Factor
H
Beyond holding time
Definitions L Limit Exceeded
MQL
Method Quantitation
Limit
Page 3 of 7

WayPANALYTICAL
79434
Inframark
A/P
Northside WWTP
229 Northside Drive
Danville , VA 24540
Report Number : 20-143-0003
Lab No : 71772
Sample ID : LTS B-Basin 20-1327
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Project Wastewater Treatment Plant
Information : VPDES Permit# VA0060593
REPORT OFANALYSIS
Report Date : 06/02/2020
Received : 05/22/2020
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 5/18/2020 9:00
Test
Results
Units
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Magnesium
3230
mg/Kg
- dry
70.4
1
05/27/20 20:54
TJS
6010D
Manganese
1120
mg/Kg
- dry
7.04
1
05/27/20 20:54
TJS
6010D
Mercury
1.42
mg/Kg
- dry
0.192
1
05/28/20 12:12
DDB
SW-7471B
Molybdenum
8.77
mg/Kg
- dry
3.52
1
05/27/20 20:54
TJS
6010D
Nickel
62.8
mg/Kg
- dry
3.52
1
05/27/20 20:54
TJS
6010D
Potassium
2860
mg/Kg
- dry
141
1
05/27/20 20:54
TJS
6010D
Selenium
<7.04
mg/Kg
- dry
7.04
1
05/27/20 20:54
TJS
6010D
Sodium
9580
mg/Kg
- dry
352
1
05/27/20 20:54
TJS
6010D
Zinc
2170
mg/Kg
- dry
17.6
1
05/27/20 20:54
TJS
6010D
Sulfur
9480
mg/Kg
- dry
141
1
05/27/20 20:54
TJS
6010D
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
H Beyond holding time
MQL Method Quantitation Limit
Page 4 of 7

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 79434
Customer Name: Inframark
Report Number: 20-143-0003
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
® UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: lBrandi Watson Date & Time: 05/22/2020 13:47:07
Page 5 of 7

3
111111111111111111 IN IIII IIII I oil IIIII I1111 III IIII o��
Client Name/Address Client Project Manager/Contact Ruling information
Inrretevvanak
Inframark • Danville VVWTP Robert Clifton - Lab Mgr- Inframark 122452
Wastewater Trealmenl Plarl!
229 Northside Dr. Kim Wlckerneyer- Sr. Lab Tech. 229 Northside Dr.
Danville, VA 24540 Danville, VA 24540
Project Description Project/Site Location (City/State) RUSH - Addr;iom, I charges apply Method ed Shipment Matrix Key
Fed Ex UPS LISPS WW -Wastewater GW -Groundwater
❑
VP❑ES Permit Danville, VA Sprfclal DeteMton Umit(sl
#� �
Date Results Needed Courier e Client Drop Off DWV - Drinxing Water S - Soil /Solid O - Oil
VA0060593 Wastewater Treatment Plant , Product M . Misc
46/30/2020 arnP-
Pralect Number
Project Manager Phone P
Project Manager Email
Purchase Order Number
Site/Facility 10 N
Waypoint Acct. 79434
434-799-5137
robert.ctifton@infra mark. corn
102817
VPDES #: VA0060593
.1 Cool c 10( Na2S2U3 tMicra Only)
����j■.wy
_
T
u
6 Coal <= bC
Hwy ■V��
■ ■S.i �i/�■ ■t
k
N
a
„
1 Nine Required
t7 None flequirr!d
ANALYTEtAL
o
3
c
e N=dH PH10
:-.. SRO Whittca Road
s,r
v
"
c
F HNO3 per<1
'Temphis, TN 39133
unless noted, ail containers
d
G HCL pH<2
�Cli] Yt3.2800
per Table it of 40 CFR Part
u
,p
w
`
y H3aoa H<x
P
i tool —6C NAISIO3
r
l7
is^�•t:f-caovn
Required
Ana ly%iS / Preservative
Comments/Notes
LTS B-Basin 20-1327
1
S
C
✓
0.5 L plastic, preservative = B
Lab# E 71772-1 L75 B-Basin 20-1327
Cust; 79434 Inframark
Cal: 05/18/2020 09:00 Re[: 05/22/2020 00:00
`
20-143-0003 Preservation. < = 6 degrees C
For Laboratory Use Oniv
Sampled by {Name - Print]
Robert Clifton
Client Remarks/Cort+ments
All Analyses must be performed by a certified lab
Fce
Custody
4ahCOminents
N
Seals
R�frquished b
Date Time
Received by: (SIGNATURF)
Date Time
r
Y N I
jw y: (SIGNATURE)
�
511ec{CMG
f
9 a -
Relinquished by7 l5lGNATU I
Date Time
Recei by tC,NATURE)
Date Time
r �
Q -
Rellriquished by: ;SIGNATURE)
Uale Time
ReC rd : (SI TUREjT
Dare Time
/U'UU
v
r�
a

Required Biosolids Tests for Inframark Danville, VA WWTP
%TS --
%TVs
PH ---
Alkalinity—
TKN
Ammonia -Nitrogen —
Nitrate + Nitrite as Nitrogen --
Organic Nitrogen (calculation)
Phosphorus --
Potassium
Sutfur
Calcium
Magnesium
Sodium —
Iron —
Aluminum
Manganese —
Copper
—Zinc
r Cadmium
-- Chromium
Nickel
---Lead
,Arsenic
--- Mercury
'Selenium
---Molybdenum
4111_���_
QC -7q 3�{
-oq 0C)
po �oabi`1
Page 7 of 7

Waypointo
ANALYTICAL
6/16/2020
Inframark
A/P
Northside WWTP
229 Northside Drive
Danville, VA, 24540
Ref: Analytical Testing
Report Number: 20-160-0010
Project Description: Danville VA-WWTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear A/P:
Waypoint Analytical Virginia, Inc. received sample(s) on 6/8/2020 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pam« mar,--
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 20-160-0010
Client Project Description: Danville VA-WWTP
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
72597
LTS-B-Basin
20-1369
Solids
06/02/2020
08:25
06/08/2020
72597
LTS-B-Basin
20-1369
Solids
06/02/2020
08:25
06/08/2020
72597
LTS-B-Basin
20-1369
Solids
06/02/2020
08:25
06/08/2020
72597
LTS-B-Basin
20-1369
Solids
06/02/2020
08:25
06/08/2020
72597
LTS-B-Basin
20-1369
Solids
06/02/2020
08:25
06/08/2020
72597
LTS-B-Basin
20-1369
Solids
06/02/2020
08:25
06/08/2020
72597
LTS-B-Basin
20-1369
Solids
06/02/2020
08:25
06/08/2020
72597
LTS-B-Basin
20-1369
Solids
06/02/2020
08:25
06/08/2020
72597
LTS-B-Basin
20-1369
Solids
06/02/2020
08:25
06/08/2020
SM-2540G
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SM-4500-NH3C
WP MTN
9045D
WP MTN
SM-2320 B
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 7

•
0
Waypoint
7621 Whitepine
Road, Richmond,
VA 23237
Main 804-743-9401 0 Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
79434
Inframark
Project
Danville VA-WWTP
A/P
Report Date : 06/16/2020
Northside WWTP
Information :
Received : 06/08/2020
229 Northside Drive
Danville VA 24540
Pr�c mL G
,
Pauric McGroary
Report Number : 20-160-0010
REPORT OFANALYSIS
Agronomist
Lab No : 72597
Matrix:
Solids
Sample ID : LTS-B-Basin 20-1369
Sampled:
6/2/2020 8:25
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Moisture
93.5
%
0.010
1
06/09/20 16:57
FMM SM-2540G
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Alkalinity (as CaCO3)
24000
mg/Kg -
dry
1540
1
06/10/20 11:00
CMF SM-2320 B
Ammonia Nitrogen
9110
mg/Kg -
dry
385
1
06/15/20 14:37
JPJ SM-4500-NH3C
Nitrate+Nitrite-N
366
mg/Kg -
dry
76.5
1
06/09/20 15:32
ZBD 4500NO3F-2011
Organic N
34300
mg/Kg -
dry
3850
1
06/15/20 10:00
CALCULATION
pH
7.8
S.U.
1
06/15/20 05:45
JSL 9045D
Total Solids
6.50
%
0.010
1
06/09/20 16:57
FMM SM-2540G
Total Volatile Solids
45.3
%
0.010
1
06/09/20 16:57
FMM SM-2540G
Total Kjeldahl Nitrogen
43400
mg/Kg -
dry
3850
1
06/15/20 10:00
JPJ ;M-4500-NH3C-TKI`
Phosphorus
20900
mg/Kg -
dry
76.9
1
06/10/20 22:49
TJS 6010D
Aluminum
38000
mg/Kg -
dry
76.9
1
06/11/20 18:00
TJS 6010D
Arsenic
<7.69
mg/Kg -
dry
7.69
1
06/10/20 22:49
KKM 6010D
Calcium
11600
mg/Kg -
dry
769
1
06/10/20 22:49
KKM 6010D
Cadmium
<1.54
mg/Kg -
dry
1.54
1
06/10/20 22:49
KKM 6010D
Chromium
51.4
mg/Kg -
dry
3.85
1
06/10/20 22:49
KKM 6010D
Copper
326
mg/Kg -
dry
7.69
1
06/10/20 22:49
KKM 6010D
Iron
36300
mg/Kg -
dry
154
1
06/10/20 22:49
KKM 6010D
Lead
48.2
mg/Kg -
dry
4.62
1
06/10/20 22:49
KKM 6010D
Qualifiers/ DF Dilution Factor
L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 3 of 7

•
0
Waypoint
7621 Whitepine
Road, Richmond,
VA 23237
Main 804-743-9401 0 Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
79434
Inframark
Project
Danville VA-WWTP
A/P
Report Date : 06/16/2020
Northside WWTP
Information :
Received : 06/08/2020
229 Northside Drive
Danville VA 24540
Pr�c mL G
,
Pauric McGroary
Report Number : 20-160-0010
REPORT OFANALYSIS
Agronomist
Lab No : 72597
Matrix:
Solids
Sample ID : LTS-B-Basin 20-1369
Sampled:
6/2/2020 8:25
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Magnesium
3370
mg/Kg
- dry
76.9
1
06/10/20 22:49
KKM 6010D
Manganese
1110
mg/Kg
- dry
7.69
1
06/10/20 22:49
TJS 6010D
Mercury
1.01
mg/Kg
- dry
0.218
1
06/12/20 11:57
DDB SW-7471B
Molybdenum
9.02
mg/Kg
- dry
3.85
1
06/10/20 22:49
KKM 6010D
Nickel
63.2
mg/Kg
- dry
3.85
1
06/10/20 22:49
KKM 6010D
Potassium
2850
mg/Kg
- dry
154
1
06/10/20 22:49
KKM 6010D
Selenium
<7.69
mg/Kg
- dry
7.69
1
06/10/20 22:49
KKM 6010D
Sodium
10600
mg/Kg
- dry
385
1
06/11/20 18:00
TJS 6010D
Zinc
2250
mg/Kg
- dry
19.2
1
06/10/20 22:49
KKM 6010D
Sulfur
10300
mg/Kg
- dry
154
1
06/10/20 22:49
KKM 6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Page 4 of 7

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 79434
Customer Name: Inframark
Report Number: 20-160-0010
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
® UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
® No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
® No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: lBrandi Watson Date & Time: 06/08/2020 10:10:30
Page 5 of 7

�!I
"`I+20-160-001(3
rim Nam['IAddrrsi Client Prol"t 811kng information79434
{
l:=iramark i�anvrllr_ ':v^.'Y T Robert Clifton - LaL Mgt lniramark nframark 106-0&2020
Danville VA-WWTP 09:48,22
.129 Norttlside Dr Kim Wckemeyer Sr Lab Tech 229 Nortfl!We ❑r
0arwille. VA 24540 Danville, VA 24540
fair•[[ Of-w-Pe+on Pr of ectls it lot -it Pon ICa V15tateI Fe U',rr - As:dttiundl Charges apr:Method of 5hipmv,-1 Pne.e Pw ncV
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Proirtt Number
Project Manager Phone s
Prujecl Manager Email
P uIChase Order Number
site/Facihty ID
Waypoint Acct. 79434
434--799-5137
robert chfton@infrar-nark curl
103507
VPDES #: VA0060593
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Cust: 79434 Infra mark
C01: 0610212020 08:25 ReC: 06/0812020 00:00
20-160-0010 PreservatiOn: < = 6 degrees C
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P .�.IlPiI. PrR
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For Labaralory Use Oniv
Sampled by (Name -- P•irtt j
Robert Clifton
Client RemarkslComrnents
All Analyses must be performed by a certified lab
rye
Custody
LahCommenis
Sealq
1
Y J N
YIN
.. � Y�
Rnlinquishe�y ISIGNATtJRil1
/ J
Bate Time
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Relinquished by: ISIGNATUf f )
Date 1ime
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Date Time
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Date TPme
Rec (wad - {SIGNArURLI
Datq ime
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VvDe s VA U a �, Lsc�3
Required Biosolids Tests for Inframark Danville, VA WWTP
%TS `/ �
%TVs
pH
Alkalinity
TKN
Ammonia -Nitrogen
�C �c
T ryllct
Nitrate + Nitrite as !Nitrogen
Organic Nitrogen (calculation) ]O� 1 G-35D 1
Phosphorus./
Potassium J
Sulfur t/
f
Caicium f
,, 7 z
+ �IIIl��l z
,J"'.«k rfl���f11111� sr
Magnesium
09 m 31
Sodium ./
Iron
Aluminum./
Ma nga nese-/
Copper -/
J�
W
Zinc
Cadmium k/
Cnromium
J vx�
Nickel ✓
MOM -
Lead I
r
Arsenic
Mercury J
Selenium
g`�g4
Molybdenum/ � N
o a
Page 7 of 7

Waypointo
ANALYTICAL
5/7/2020
Inframark
A/P
Northside WWTP
229 Northside Drive
Danville, VA, 24540
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Ref: Analytical Testing
Report Number: 20-115-0001
Project Description: WASTEWATER TREAT PLANT
VPDES PERMIT# VA0060593
Dear A/P:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/24/2020 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pam« mar,--
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 14

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 20-115-0001
Client Project Description: WASTEWATER TREAT PLANT
VPDES PERMIT# VAOO6O593
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
71153
LTS B-Basin 20-1262A
Solids
04/21/2020 09:00
04/24/2020
71153
LTS B-Basin 20-1262A
Solids
04/21/2020 09:00
04/24/2020
9045D
WP MTN
71153
LTS B-Basin 20-1262A
Solids
04/21/2020 09:00
04/24/2020
SM-2320 B
WP MTN
71153
LTS B-Basin 20-1262A
Solids
04/21/2020 09:00
04/24/2020
6010D
WP MTN
71153
LTS B-Basin 20-1262A
Solids
04/21/2020 09:00
04/24/2020
4500NO3F-2011
WP MTN
71153
LTS B-Basin 20-1262A
Solids
04/21/2020 09:00
04/24/2020
SW-7471B
WP MTN
71153
LTS B-Basin 20-1262A
Solids
04/21/2020 09:00
04/24/2020
SM-4500-NH3C
WP MTN
71153
LTS B-Basin 20-1262A
Solids
04/21/2020 09:00
04/24/2020
SM-4500-NH3C-TKN
WP MTN
71153
LTS B-Basin 20-1262A
Solids
04/21/2020 09:00
04/24/2020
SM-2540G
WP MTN
71154
LTS B-Basin 20-1262C
Solids
04/21/2020 09:00
04/24/2020
SW-9045C
WP MTN
71154
LTS B-Basin 20-1262C
Solids
04/21/2020 09:00
04/24/2020
SW-7.3.4
WP MTN
71154
LTS B-Basin 20-1262C
Solids
04/21/2020 09:00
04/24/2020
SW-7.3.3
WP MTN
71154
LTS B-Basin 20-1262C
Solids
04/21/2020 09:00
04/24/2020
ASTM D93-80
WP MTN
71155
LTS B-Basin 20-1262B
TCLP
04/21/2020 09:00
04/24/2020
SW-1311 (ZHE)
WP MTN
71155
LTS B-Basin 20-1262B
TCLP
04/21/2020 09:00
04/24/2020
SW-1311
WP MTN
71155
LTS B-Basin 20-1262B
TCLP
04/21/2020 09:00
04/24/2020
8270C
WP MTN
71155
LTS B-Basin 20-1262B
TCLP
04/21/2020 09:00
04/24/2020
8260B
WP MTN
71155
LTS B-Basin 20-1262B
TCLP
04/21/2020 09:00
04/24/2020
8151A
WP MTN
71155
LTS B-Basin 20-1262B
TCLP
04/21/2020 09:00
04/24/2020
8081A
WP MTN
71155
LTS B-Basin 20-1262B
TCLP
04/21/2020 09:00
04/24/2020
7470A
WP MTN
71155
LTS B-Basin 20-1262B
TCLP
04/21/2020 09:00
04/24/2020
6010D
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 14

WayP
�' 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL www.waypointanalytical.com
79434
Inframark
A/P
Northside WWTP
229 Northside Drive
Danville , VA 24540
Submitted By : Robert Clifton/Kim Wickemeyer
Report Number : 20-115-0001
Lab No : 71154
Sample ID : LTS B-Basin 20-1262C
Robert Clifton/Kim Wickemeyer
Project WASTEWATER TREAT PLANT Report Date : 05/07/2020
Information : VPDES PERMIT# VA0060593 Received : 04/24/2020
REPORT OFANALYSIS
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 4/21/2020 9:00
Test
Results
Units MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Cyanide (Reactivity)
<0.125
mg/Kg 0.125
1
04/28/20 10:55
FMM
SW-7.3.3
Ignitability
>96
degrees C
1
04/27/20 08:30
JDT
ASTM D93-80
pH
7.1
S.U.
1
05/05/20 06:32
JSL
SW-9045C
Sulfide (Reactivity)
<25.0
mg/Kg 25.0
1
04/28/20 10:00
FMM
SW-7.3.4
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Page 5 of 14

WayP
�' 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL www.waypointanalytical.com
79434
Inframark Robert Clifton/Kim Wickemeyer
A/P Project WASTEWATER TREAT PLANT Report Date : 05/07/2020
Northside WWTP Information : VPDES PERMIT# VA0060593 Received : 04/24/2020
229 Northside Drive
Danville , VA 24540 p�c m` Rr1�01'
Submitted By : Robert Clifton/Kim Wickemeyer
Pauric McGroary
Report Number : 20-115-0001 REPORT OFANALYSIS Agronomist
Lab No : 71155 Matrix: TCLP
Sample ID : LTS B-Basin 20-1262B Sampled: 4/21/2020 9:00
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
TCLP Herbicide Extraction
Combined
1
04/29/20 13:20
SAJ
SW-1311
TCLP Metals Extraction
Combined
1
04/29/20 13:20
SAJ
SW-1311
TCLP Pesticide Extraction
Combined
1
04/29/20 13:20
SAJ
SW-1311
TCLP SVOC Extraction
Combined
1
04/29/20 13:20
SAJ
SW-1311
TCLP VOC ZHE Extraction
Combined
1
04/29/20 13:20
SAJ
SW-1311 (ZHE)
Analytical Method: 6010D
Prep Batch(es):
L489666
05/01/20 11:42
Prep Method: 3015A
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
TCLP Arsenic
<0.250
mg/L
0.250
1
05/01/20 17:21
KKM
L489952
TCLP Barium
<0.250
mg/L
0.250
1
05/01/20 17:21
KKM
L489952
TCLP Cadmium
<0.0500
mg/L
0.0500
1
05/01/20 17:21
KKM
L489952
TCLP Chromium
<0.100
mg/L
0.100
1
05/01/20 17:21
KKM
L489952
TCLP Lead
<0.100
mg/L
0.100
1
05/01/20 17:21
KKM
L489952
TCLP Selenium
<0.500
mg/L
0.500
1
05/01/20 17:21
KKM
L489952
TCLP Silver
<0.0500
mg/L
0.0500
1
05/01/20 17:21
KKM
L489952
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 6 of 14

�'
WayP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
79434
Inframark
Robert
Clifton/Kim Wickemeyer
A/P
Project WASTEWATER TREAT PLANT
Report Date : 05/07/2020
Northside WWTP
Information : VPDES
PERMIT# VA0060593
Received
: 04/24/2020
229 Northside Drive
Danville VA 24540
Pr�c
mL G
,
Submitted By : Robert Clifton/Kim Wickemeyer
Pauric McGroary
Report Number : 20-115-0001
REPORT OFANALYSIS
Agronomist
Lab No : 71155
Matrix: TCLP
Sample ID : LTS B-Basin 20-1262B
Sampled: 4/21/2020 9:00
Analytical Method: 7470A
Prep Batch(es):
L489527 04/30/20 09:50
Prep Method: 7470A
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
TCLP Mercury
<0.0200
mg/L
0.0200
1 04/30/20 14:59 DDB
L489587
Analytical Method: 8081A
Prep Batch(es):
L489520 04/30/20 13:00
Prep Method: 3510C
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
TCLP Endrin
<0.001600
mg/L
0.001600
10 05/01/20 04:11 VIC
L489741
TCLP gamma-BHC
<0.001600
mg/L
0.001600
10 05/01/20 04:11 VIC
L489741
TCLP Methoxychlor
<0.001600
mg/L
0.001600
10 05/01/20 04:11 VIC
L489741
TCLP Toxaphene
<0.01200
mg/L
0.01200
10 05/01/20 04:11 VIC
L489741
TCLP Chlordane
<0.008000
mg/L
0.008000
10 05/01/20 04:11 VIC
L489741
TCLP Heptachlor Epoxide
<0.001600
mg/L
0.001600
10 05/01/20 04:11 VIC
L489741
TCLP Heptachlor
<0.001600
mg/L
0.001600
10 05/01/20 04:11 VIC
L489741
Surrogate: Decachlorobiphenyl
50.00
Limits: 36-116%
10 05/01/20 04:11 VIC
L489741
Surrogate: Tetrachloro-m-xylene
63.71
Limits: 25-123%
10 05/01/20 04:11 VIC
L489741
Analytical Method: 8151A
Prep Batch(es):
L489613 04/30/20 16:30
Prep Method: 8151A
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
TCLP 2,4-D
<0.0200
mg/L
0.0200
1 05/01/20 19:49 VIC
L489962
TCLP 2,4,5-TP (Silvex)
<0.0020
mg/L
0.0020
1 05/01/20 19:49 VIC
L489962
Surrogate: DCAA
73.80
Limits: 20-120%
1 05/01/20 19:49 VIC
L489962
Qualifiers/ DF Dilution Factor
MQL
Method Quantitation Limit
Definitions
Page 7 of 14

�'
WayP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
79434
Inframark
Robert
Clifton/Kim Wickemeyer
A/P
Project WASTEWATER TREAT PLANT
Report Date : 05/07/2020
Northside WWTP
Information : VPDES
PERMIT# VA0060593
Received
: 04/24/2020
229 Northside Drive
Danville VA 24540
Pr�c
mL G
,
Submitted By : Robert Clifton/Kim Wickemeyer
Pauric McGroary
Report Number : 20-115-0001
REPORT OFANALYSIS
Agronomist
Lab No : 71155
Matrix: TCLP
Sample ID : LTS B-Basin 20-1262B
Sampled: 4/21/2020 9:00
Analytical Method: 8260B
Prep Batch(es):
L489902 05/01/20 08:01
Prep Method: 5030B
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
TCLP Benzene
<0.0100
mg/L
0.0100
1
05/01/20 16:15 ELM
L489904
TCLP Carbon Tetrachloride
<0.0100
mg/L
0.0100
1
05/01/20 16:15 ELM
L489904
TCLP Chlorobenzene
<0.0100
mg/L
0.0100
1
05/01/20 16:15 ELM
L489904
TCLP Chloroform
<0.0100
mg/L
0.0100
1
05/01/20 16:15 ELM
L489904
TCLP 1,4-Dichlorobenzene
<0.0100
mg/L
0.0100
1
05/01/20 16:15 ELM
L489904
TCLP 1,2-Dichloroethane
<0.0100
mg/L
0.0100
1
05/01/20 16:15 ELM
L489904
TCLP 1,1-Dichloroethene
<0.0100
mg/L
0.0100
1
05/01/20 16:15 ELM
L489904
TCLP Methyl Ethyl Ketone (MEK)
<0.200
mg/L
0.200
1
05/01/20 16:15 ELM
L489904
TCLP Tetrachloroethene
<0.0100
mg/L
0.0100
1
05/01/20 16:15 ELM
L489904
TCLP Trichloroethene
<0.0100
mg/L
0.0100
1
05/01/20 16:15 ELM
L489904
TCLP Vinyl Chloride
<0.0100
mg/L
0.0100
1
05/01/20 16:15 ELM
L489904
Surrogate:4-Bromofluorobenzene
109
Limits:71-137%
1 05/01/20 16:15 ELM
L489904
Surrogate: Dibromofluoromethane
115
Limits: 70-128%
1 05/01/20 16:15 ELM
L489904
Surrogate: 1,2-Dichloroethane - d4
109
Limits: 63-136%
1 05/01/20 16:15 ELM
L489904
Surrogate: Toluene-d8
103
Limits: 70-130%
1 05/01/20 16:15 ELM
L489904
Analytical Method: 8270C
Prep Batch(es):
L490127 05/05/20 10:15
Prep Method: 3510C
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
TCLP 2-Methylphenol
<0.0200
mg/L
0.0200
1
05/05/20 15:51 DCM
L490278
TCLP 3&4 Methylphenol
<0.0400
mg/L
0.0400
1
05/05/20 15:51 DCM
L490278
TCLP 2,4-Dinitrotoluene
<0.0200
mg/L
0.0200
1
05/05/20 15:51 DCM
L490278
Qualifiers/ DF Dilution Factor
MQL
Method Quantitation Limit
Definitions
Page 8 of 14

WayP
�' 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL www.waypointanalytical.com
79434
Inframark Robert Clifton/Kim Wickemeyer
A/P Project WASTEWATER TREAT PLANT Report Date : 05/07/2020
Northside WWTP Information : VPDES PERMIT# VA0060593 Received : 04/24/2020
229 Northside Drive
Danville , VA 24540
Submitted By : Robert Clifton/Kim Wickemeyer
Pauric McGroary
Report Number : 20-115-0001 REPORT OFANALYSIS Agronomist
Lab No : 71155
Sample ID : LTS B-Basin 20-1262B
Matrix: TCLP
Sampled: 4/21/2020 9:00
Analytical Method: 8270C
Prep Batch(es):
L490127 05/05/20 10:15
Prep Method: 3510C
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
TCLP Hexachlorobenzene
<0.0200
mg/L
0.0200
1
05/05/20 15:51 DCM
L490278
TCLP Hexachlorobutadiene
<0.0200
mg/L
0.0200
1
05/05/20 15:51 DCM
L490278
TCLP Hexachloroethane
<0.0200
mg/L
0.0200
1
05/05/20 15:51 DCM
L490278
TCLP Nitrobenzene
<0.0200
mg/L
0.0200
1
05/05/20 15:51 DCM
L490278
TCLP Pentachlorophenol
<0.0400
mg/L
0.0400
1
05/05/20 15:51 DCM
L490278
TCLP Pyridine
<0.0200
mg/L
0.0200
1
05/05/20 15:51 DCM
L490278
TCLP 2,4,5-Trichlorophenol
<0.0200
mg/L
0.0200
1
05/05/20 15:51 DCM
L490278
TCLP 2,4,6-Trichlorophenol
<0.0200
mg/L
0.0200
1
05/05/20 15:51 DCM
L490278
Surrogate: TCLP 2,4,6-Tribromophenol
65.0
Limits: 42-102%
1 05/05/20 15:51 DCM
L490278
Surrogate: TCLP 2-Fluorobiphenyl
48.5
Limits: 24-86%
1 05/05/20 15:51 DCM
L490278
Surrogate: TCLP 2-Fluorophenol
20.5
Limits: 13-37%
1 05/05/20 15:51 DCM
L490278
Surrogate: TCLP 4-Terphenyl-d14
61.5
Limits: 30-122%
1 05/05/20 15:51 DCM
L490278
Surrogate: TCLP Nitrobenzene-d5
45.3
Limits: 25-78%
1 05/05/20 15:51 DCM
L490278
Surrogate: TCLP Phenol-d6
14.3
Limits: 9-27%
1 05/05/20 15:51 DCM
L490278
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 9 of 14

Waypointo
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Client: Inframark CASE NARRATIVE
Project: WASTEWATER TREAT PLANT
Lab Report Number: 20-115-0001
Date: 5/6/2020
Total Aqueous Mercury Analysis - CVAA (TCLP) Method 7470A
Sample 71155 (LTS B-Basin 20-1262B)
Analyte: Mercury
QC Batch No: 1-489587/1-489527
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 10 of 14

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 79434
Customer Name: Inframark
Report Number: 20-115-0001
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
® UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: lBrandi Watson Date & Time: 04/24/2020 10:03:36
Page 11 of 14

`)Ll6--% t
Client Name/Address
Client Project Manager/Contact
Billing Information
2a115-0007
IIi`IIJII
Dan�lie vvvra
Robert Clifton - Loh Mgr.
Inframar
IIIIIIIIIII III IlI1fI1IIIIIIII1I
79434Inframark
229 Northside Dr,
Kim Wlckerneyer - Sr. Lab Tech.
229 Nvrthside Dr.
04.24-2020
ntramdrk D9:59 32
Data Ale, VA 24540
Danville. VA 24540
method
WASTEWATER TREAT PLANT
Project Description
Project/Site Location lCity/State)
RUSE+-Addinonal charges apply
VPDES Permit #:
Danville, VA
special Detection Umitlsj
❑ I-ed L ,
Date ResuitsNeeded
Courier ❑CliensD
El
port ow - DrinicingWater S- Soil/Solid 0-0I
VA0060593
Wastewater Treatment Plant
O - Product M - Mrsc
0511512020
orh�r
project Number
"*a Manager Phone ■
Project Manases Email
Purchase order Number
Site/Facility ID R
waypoint Acct. 79434
434-799-5137
robert.d1fton c@inframaric-com
101352
VPQES #- VA0060593
A Cool < MC Nan ZO3 (Mk to Qnh)
�y �j;
GWay
8 Coto c= K
C
point
K
;e
None equ
0 None Rputred
ANALYTICAL
.t,
E
t N20H PH>L4
2a40 Whitten Read
Unless rested, ail containers
a
T
x
o
`o
J
_ J
Lf.YL
F HM03 VOQ
G � �
'AcWhis TN 38133
TaVe n of 4a CFFt Part
H K3PO4
(901) 213-240D
Per
E
t
toot — K MAM203
136.
Date
Time Sample Identity ation
Required Analysis / Preservative
Comments/Notts
o.rttrx�
LTS B-Basin 20-1262A
I
S
G
1 4/
1
1
O.5 L plastic, preservative = B
LTS B-Basin 20-1262B
I
Is
C
1 L amber glass; preservative = B
LTS B-Basin 20-1262C 1
S C ll✓
1 L amber glass; preservative = 9
Lab# E 71153-1
LTS B-Basin 20-1252A
Cust: 79434 Inframark
CIA: 04/21/2020 04:00
20 115-040{
ReC: 04/24/2020 00:Do
Preservation: r = 6 degrees C
Lab# E 71155-1
LTS B-Basin
20-12626
Cult: 79434 Inframark
ME
Lab# E 71154-1
Cal: 04/21/202009:00 Rec: 04/ 24/ 2020 00:00
20-115-0001
LTS B-Basin 20-1262C
Preservatlon: HNO3,PH
< 2
Cust: 79434 Inframark
CDI: 04/21/2020 09.00 Rec: 04/24/2020 00:00
20-115.0001
Preservatron;
I L
led by (Name - Print)
Client Remarks/Comments
Ice Ga
tabCarnmGntY
F<Dbei Clifton
All Analyses must be performed by a certified lab
sears
Sek
C)/ H
l L
Tirm
Received by: (SIGNATURE) Date Time
Y
R
uisheQ by' {SIGNATURE}
C
Date
��Jz.o res�Z
BlankIr ler emP
Relinquish (SIGNATURE)
Date Time
Received by. (SIGNATURE) Rate lime
c��''
Relinquished by: (SIGNATURE)
Date Time
Received by: (SIGNATURE) Date Time

L: S
12)
� a - LaUa.�► w
Required Tests for inframark-Danville, VA WWTP (Waypoint VA Account 79434)
✓%Ts
ViATVS
./p H
./Alkalinity
,4N
,/Ammonia -Nitrogen
.Nitrate + Nitrite as Nitrogen
-#/Organic Nitrogen (calculation)
Phosphorus
_4P0ta5siurn
."/5uIfur
'/Calcium
./Magnesium
./Sodium
/Iron
./A/luminum
•/Manganese
Copper
� f
m
Zi
..f nc
m
n
%/Cadmium
Chromium
z
t%Nickel
Aead
— Arsenic
Lh NA [[Onnnn
W N��
,Mercury
Selenium
J
..IGiolybdenum
Page 13 of 14

Purchase Order
1NFRAMARK
Date: 4/20/2020
PO#: 101352
Bill To Buyer Name: Anjelina Munoz
229 Northside Drive Buyer Email: anjelina.muriozC(_Lnfrarnark.corrr
Danville Virginia 24540 End User Name: Kimberly Wickemeyer
United States End User Email: kim erly__,wickemeyer5inframark.corn
Vendor: Ship To:
Waypoint Analytical Inc 229 Northside Drive
Danville Virginia 24540
United States
Item
Description
Qty
units
EDD
Rate
Amount Memo
SIP00017
SL2 Biosolids Test pack
1
Ea
5129/2020
$79 80
$79.80
SIP00017
503E Metals
1
Ea
5/29/2020
5249.90
$249.90
SIP00017
Nitrogen Series
1
Ea
5/29/2020
$42 00
$42.00
SIP00017
Total Volatile Solids
1
Ea
5129/2020
$17 85
$17 B5
SIP0001 7
Total Alkanity
1
Ea
512W2020
$16 80
$16.80
SJP00017
pH
1
Ea
512g12020
S15 75
$15.75
SIP00017
TCLP
1
Ea
5/29/2020
51,075.00
$1.07500
SIP00017
ICIR
1
Ea
5/29/2020
$160 00
$160 00
Vendor Acceptance.
Date
Total $1,65710
Inframark, LLC General Conditions of Purchase, a copy of which is available at https 11www.inframark.com/contact-usldoi
with -us) , and any specific conditions or other terms not inctuded in these General Conditions of Purchase that are mul
upon in writing (herein after "Specific Conditions") shall govern this Purchase Order, In the event of a conflict between
Conditions noted in the Purchase Order and the General Conditions of Purchase. the Specific Conditions shall control
conditions inctuded in any Supplier documentation are specifically rejected by Purchaser and shall be of no effect on 9
Order
Page 14 of 14

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Danville WQ Permit Number: W00036561
WWTP Name: Northside WWTP NPDES Number: VA0060593
Monitoring Period: From l/l/2020 To 12/31/2020
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) El
Alt. C (Prior Testing)❑
AIt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
ThermopElic ❑
Beta Ray
Gamma Ray ❑
1 Pasteurization ❑
Class B:
Alt. (1) Fecal Density r❑
I Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
f Air Drying ❑
r Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring
data:
Parameter
Allowable Level
in Sludge
en Pathog Density
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech-nique
Minimum
Geo. Mean
Maximum
nits
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000
1000
1000
col/g
0
Quarterly
G
SM9222D
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
I weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed -
Alt. I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) RI
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAIL 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
21 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
William Shreve - Area Manager Brent Collins; Director of Technical Services
Preparer Name and Title (type or print) ---------Land Applier Name and Title (if applicable)(type or print)
E / a f 1 /20/2021
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (1212006)

(�Ia'ne Analytical
www.pacelabs.com
April 29, 2020
Mr. Robert Clifton
INFRAMARK
229 NORTHSIDE DR
Danville, VA 24540
RE: Project: INFRAMARK-DANVILLE #92-618203
Pace Project No.: 7324866
Dear Mr. Clifton:
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, vW 25813
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on April 21, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - WestVirginia
• Pace Analytical Services - Lexington
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Stacy Heasley
[e-mail]
800-999-0105
Project Manager
Enclosures
cc: Ms. Kimberly Wickemeyer, INFRAMARK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, WV 25813
[phone]
Project: INFRAMARK-DANVILLE #92-618203
Pace Project No.: 7324866
Pace Analytical Services Beaver
225 Industrial Park Drive, Beaver, WV 25813
Virginia VELAP 460148
Virginia DCLS 00281
West Virginia DEP 060
Pace Analytical Services Lexington
782 North Lee Highway, Lexington, VA24450
CERTIFICATIONS
West Virginia DHHR 00412CM
North Carolina DEQ 466
Kentucky Wastewater Certification KY90039
Pennsylvania DEP 68-00839
Virginia VELAP 460150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, WV 25813
[phone]
Project:
Pace Project No.:
INFRAMARK-DANVILLE #92-618203
7324866
Lab ID
Sample ID
7324866001
CATWALK 131 #1
7324866002
CATWALK 132 #2
7324866003
CATWALK 133 #3
7324866004
CATWALK 134 #4
7324866005
CATWALK 135 #5
7324866006
CATWALK 136 #6
7324866007
CATWALK 131 #7
SAMPLE SUMMARY
Matrix
Date Collected
Date Received
Solid
04/21/20 08:25
04/21/20 13:14
Solid
04/21/20 09:00
04/21/20 13:14
Solid
04/21/20 08:35
04/21/20 13:14
Solid
04/21/20 08:55
04/21/20 13:14
Solid
04/21/20 08:40
04/21/20 13:14
Solid
04/21/20 08:50
04/21/20 13:14
Solid
04/21/20 08:30
04/21/20 13:14
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, WV 25813
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
INFRAMARK-DANVILLE #92-618203
7324866
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
7324866001
CATWALK 131 #1
SM 9222D - 2006
MJV
1
PASI-LX
SM 2540G-11
MRP
1
PASI-BVWV
7324866002
CATWALK 132 #2
SM 9222D - 2006
MJV
1
PASI-LX
SM 2540G-11
MRP
1
PASI-BVWV
7324866003
CATWALK 133 #3
SM 9222D - 2006
MJV
1
PASI-LX
SM 2540G-11
MRP
1
PASI-BVWV
7324866004
CATWALK 134 #4
SM 9222D - 2006
MJV
1
PASI-LX
SM 2540G-11
MRP
1
PASI-BVWV
7324866005
CATWALK 135 #5
SM 9222D - 2006
MJV
1
PASI-LX
SM 2540G-11
MRP
1
PASI-BVWV
7324866006
CATWALK 136 #6
SM 9222D - 2006
MJV
1
PASI-LX
SM 2540G-11
MRP
1
PASI-BVWV
7324866007
CATWALK 131 #7
SM 9222D - 2006
MJV
1
PASI-LX
SM 2540G-11
MRP
1
PASI-BVWV
PASI-BVWV = Pace Analytical Services - WestVirginia
PASI-LX = Pace Analytical Services - Lexington
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 10

aceAnalytical
www.paeelabs.eom
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, VW 25813
[phone]
ANALYTICAL RESULTS
Project: INFRAMARK-DANVILLE #92-618203
Pace Project No.: 7324866
Sample: CATWALK 131 #1 Lab ID: 7324866001 Collected: 04/21/20 08:25 Received: 04/21/20 13:14 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <1000 CFU/g 1000 1 04/21/20 15:13 04/22/20 14:50
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 95.1 % 0.10 1 04/24/20 14:36
Sample: CATWALK 132 #2 Lab ID: 7324866002 Collected: 04/21/20 09:00 Received: 04/21/20 13:14 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <1000 CFU/g 1000 1 04/21/20 15:13 04/22/20 14:50
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 95.8 % 0.10 1 04/24/20 14:38
Sample: CATWALK 133 #3 Lab ID: 7324866003 Collected: 04/21/20 08:35 Received: 04/21/20 13:14 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <1000 CFU/g 1000 1 04/21/20 15:13 04/22/20 14:50
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 94.5 % 0.10 1 04/24/20 14:39
Sample: CATWALK 134 #4 Lab ID: 7324866004 Collected: 04/21/20 08:55 Received: 04/21/20 13:14 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <1000 CFU/g 1000 1 04/21/20 15:13 04/22/20 14:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/29/2020 03:56 PM without the written consent of Pace Analytical Services, LLC.
Page 5 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, VW 25813
[phone]
ANALYTICAL RESULTS
Project: INFRAMARK-DANVILLE #92-618203
Pace Project No.: 7324866
Sample: CATWALK 134 #4 Lab ID: 7324866004 Collected: 04/21/20 08:55 Received: 04/21/20 13:14 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 95.7 % 0.10 1 04/24/20 14:40
Sample: CATWALK 135 #5 Lab ID: 7324866005 Collected: 04/21/20 08:40 Received: 04/21/20 13:14 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <1000 CFU/g 1000 1 04/21/20 15:13 04/22/20 14:50
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 93.7 % 0.10 1 04/24/20 14:41
Sample: CATWALK 136 #6 Lab ID: 7324866006 Collected: 04/21/20 08:50 Received: 04/21/20 13:14 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <1000 CFU/g 1000 1 04/21/20 15:13 04/22/20 14:50
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 93.0 % 0.10 1 04/24/20 14:42
Sample: CATWALK 131 #7 Lab ID: 7324866007 Collected: 04/21/20 08:30 Received: 04/21/20 13:14 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <1000 CFU/g 1000 1 04/21/20 15:13 04/22/20 14:50
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 95.5 % 0.10 1 04/24/20 14:44
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/29/2020 03:56 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, WV 25813
[phone]
QUALIFIERS
Project: INFRAMARK-DANVILLE #92-618203
Pace Project No.: 7324866
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/29/2020 03:56 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, VW 25813
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: INFRAMARK-DANVILLE #92-618203
Pace Project No.: 7324866
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
7324866001
CATWALK B1 #1
SM 9222D - 2006
24267
SM 9222D - 2006
24278
7324866002
CATWALK B2 #2
SM 9222D - 2006
24267
SM 9222D - 2006
24278
7324866003
CATWALK B3 #3
SM 9222D - 2006
24267
SM 9222D - 2006
24278
7324866004
CATWALK B4 #4
SM 9222D - 2006
24267
SM 9222D - 2006
24278
7324866005
CATWALK B5 #5
SM 9222D - 2006
24267
SM 9222D - 2006
24278
7324866006
CATWALK B6 #6
SM 9222D - 2006
24267
SM 9222D - 2006
24278
7324866007
CATWALK B1 #7
SM 9222D - 2006
24267
SM 9222D - 2006
24278
7324866001
CATWALK B1 #1
SM 2540G-11
24449
7324866002
CATWALK B2 #2
SM 2540G-11
24449
7324866003
CATWALK B3 #3
SM 2540G-11
24449
7324866004
CATWALK B4 #4
SM 2540G-11
24449
7324866005
CATWALK B5 #5
SM 2540G-11
24449
7324866006
CATWALK B6 #6
SM 2540G-11
24449
7324866007
CATWALK B1 #7
SM 2540G-11
24449
Date: 04/29/2020 03:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 10

ed
LAB USE ONLY- Affix Workorder/Login Label Here or List Pace Workorder Number or
CHAIN -OF -CUSTODY Analytical Request DOCUment
7�I1T11 II-:-n�... ---- -
aceAnalytical`'
Chain -of -Custody is a LEGAL DOCUMENT -Complete all relevent fields ,
WO# : 7324866
Company: Billing Information:
Inframark-Danville Infrarna-k-Danville
N LY
-� 229 Northside Drive
II I I II II I'I I IIII II I II I III
Address: 229 Northside Dr., Danville, VA 24540Danville, VA24540
^�
2 2 2
7324866 de,
Report To: Email To: [e-mail]
Robert.Cfifton@ [ lfrai ?rk•�^^ hanieMOSk p - `'inframarkeom
"' .
Preservative (6) methanol, (7) souwm
(s) zinc acetate,
Distillate, Iti) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (B) ammonium sulfate,
(C) ammonium hydroxide,
(D) TSP, (U) Unpreserved, (0) Other
Site Collection Info/Address:
COPY To:
[e-mail] Danville VA WWTP 229 Northside, Dr., Danville, VA 24540
Analyses Lab Profile/Line:
—
lab sample Receipt checklist:
Customer Project Name/Number. State: County/City: Time Zone Collected:
Inframark-Danville (client #: 92-618203) VA /Danville [ ] PT [ ] MT [ ] CT VET
Custody Seals Present/Intact Y N
Site/Facility ID #: Compliance Monitoring?
Z I
1 i
I
Custody Si9uaLures PresenL Y N 4W
Collector Signature Present. ®N NA
Phone: [phone]
Danville, VA WWiP permit VA0060593 [�YeS [ ]NO
N
O
Bottles Intact �N NA
Email: kimberywiCke"X,yer@Wd9n1Erx.0M
DW PWS ID #:CoilectedBy(print):
} Z (
Correct Bottles N NA
�N NA
Purchase Order#: 101350
Sufficient Volume
Robert Clifton Quote Ilk OW74511 DW Location Code:
! +
I
Z j
1
Samples Received on Ice ®N NA
VOA - Headspace Acceptable Y N NA
USDA Regulated Soils N NA
II (si a )'
TUmaround Date Required:
Immediately ac on ce:
Co Y
(Yes [ )NO
Sample Disposal: Rusfi: Field Filtered (if applicable}
No
(wj Dispose as appropriate ( ]Return [ ]Same Day ( ]Next Day [ ]Yes [✓)
[ I Archive; [ ) 2 Day [ ] 3 Day [ ) 4 Day [ ] 5 Day Analysis:
[ J Hold: (Expedite Charges Apply)
• Matrix Codes (insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (."JW),
Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT)
Comp / Collected (or Composite End
Customer Sample ID Matrix' Grab Composite Start)
Date Time Date Time
Catwalk B1 #1 SL* Grab 04/21/20 0825 - - - - - - - - N
Res
a
Catwalk B2 #2 SL* Grab 04/21/20 0900 - - - - - - - No
Catwalk B3 #3 SL* Grab 0835 - - - - - - - - NO
Catwalk 134 #4 SL* Grab 04121 20 0855 - - - - - - - - No
*
Grab 04/21/20 0& - - - - - - - - No
#ofIZ
Ctns
1
1
1
Catwalk B5 #5 SL 1
Catwalk B8 #6 SL* -Grab 04/21/20 0850
__-- __-- No 1
Catwalk B1 #7 SL* Grab 04121QD 0830 - - - - - - - - No 1
Customer Remarks / Special Conditions / Possible Hazards:
'Biosolids for Fecal Coliform
Bottles: 120 mL Sterile for microbiology
O
M
Z Z
Z f I
I
'L
E } i-
(a
Q Z
Type of Ice Used: We Blue Dry None SHORT HOLDS PRESENT (<72 hours): N N/A
Packing Material Used: Lab Tracking #:
Samples received via:
Samples in Holding Time
(Y)N NA
Residual Chlorine Present
N NA
Cl Strips:
Sample pH Acceptable
Y N NA
pH Strips:
Sulfide Present
Y N NA
Lead Acetate Strips:
LAB USE ONLY:
Lab Sample # / Comments:
Radchem sample(s) screened (<500 cpm): Y N NA FEDEX UPS en Courier Pace Courier
MTJL LAB USE ONLY
Date rime: Received by/Company: (Signature) n Date/Time:
v-'7 G �l/ `� �� O�" 1 Table #:
Acctnum:
Date/Time: Received by/Company: (Signature) Date/Time: Template:
Preiogin:
Date/Time: Received by/Company: (Signature) Date/Time: PM:
PB:
Lab Sample Temperature Info:
Temp Blank Received: Y N NA
Therm ID#: n
Cooler 1 Temp Upon Receipt _'__l_oc
Cooler 1 Therm Corr. Factor: a oC
Cooler 1 Corrected Temp: —oC
Comments:
Trip Blank Received: Y N NA
HCL McOH TSP Other
.
Non Conform ance(s): PAW•9,of 10
YES / NO of: I

LIMS73 Lab Sample Condition Upon Receipt (West Virginia)
ace 4+�tyai
Client Name:
WO#:7324866
PM: SDH Due Date: 05/01/20
CLIENT: INFRAMARK
Courier: ❑ Fed Ex ❑ UPS ❑ USPS L ?Client ❑ Commercial ❑ Pace ❑ Other:
Tracking #:
Custody Seal on Cooler/Box/Containers Present: ❑ yes no Seals intact: ❑ yes ❑ no
Thermometer UsedUVX_6��^ Type of Ice: Wet Blue None C Jet
o'�t \ Correction Factory: V•� - Final Tem
Cooler Temperature Observed Temp p•
pH paper Lot# Date and Initials of person exa i g
Comments:�I�r� ,!1�
contents:
Chain of Custody Present:
1 •
Chain of Custody Filled Out.
2.
Chain of Custody Relinquished:
E4.
3.
Sampler Name & Signature on COC:
Sample Labels match COC:-Includes date/time/ID Matrix
Samples Arrived within Hold Time:
C/
6.
Short Hold Time Analysis (<72hr remaining):
7.
Rush Turn Around Time Requested:
8.
Sufficient Volume:
9.
Correct Containers Used:
-Pace Containers Used:
t
V
10.
Containers Intact:
11.
Orthophosphate field filtered:
12.
Hex Cr Aqueous sample field filtered:
-pH adjusted within 24 hours? (If yes, indicate acid lot #
13.
Filtered volume received for Dissolved tests:
14.
I
All containers have been checked for preservation:
exceptions: VOA, coliform, O&G, LLMercury, Non -aqueous matrix
All containers meet method preservation requirements:
Initial when
completed '
Date/time sample_ti 1
provided to lab .,
Tests not preserved:
Headspace in VOA Vials:
16•
Trip Blank Present:
Trip Blank Custody Seals Present:
17•
rn4a en
completed:
Date:
Client Notification/ Resolution:
Person Contacted:
Comments/ Resolution:
Date/Time:
Contacted By:
❑ A check in this box indicates that additional information has been stored in ereports.
'PM review is documented electronically in LIMS, when the Project Manager closes the SRF Review schedule in LIMS. The status may be reviewed in the Status section
of the Workorder Edit Screen.
SCUR WV -rev. 1`10Of10

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contact: Brent Collins Report Date: 6/5/2020
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028 Date Sample Rcvd: 5/6/2020
Vector Attraction Reduction / Aerobically Digested Sludge 30 Day Test
Meritech Work Order # 05062010 Sample: Danville Composite 5/6/20
Total Solids Volatile Solids % Volatile Solids
Week 1 0.640 0.300 0.466
Week 2 0.710
Week 3 0.670
Week 4 0.850
Week 5 0.800
Van Kleek Reduction (%): 11.82
0.320 0.453
0.330 0.492
0.370 0.434
0.350 0.435
Pass or Fail
Pass
I hereby certify that I have reviewed and approve these data. \'
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

..M� mm� Now NM
PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS
SM 2540 B-2011
B - A x 100 = % TOTAL SOLIDS
C
4�l
LAIill
TIME
ANALYST
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 30 minutes)
(initial ignition 550°C for I hour)
(repeat iginition 550°C for 30 minutes)
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 30 minutes)
13=D x 100 = % VOLATILE SOLIDS
C
(initial ignition 550°C for 1 hour Ignite Wt Diff
REPORTED BY: ) Ignition Wt (g) Tinal Ignite�Wt(g) (final -initial °
(repeat iginition 550°C for 30 min) 5 q 9) /° VOL SOLIDS
k Acceptance criteria for constant dry/ignition weight: Dry/Ignite, cool and weigh and repeat dry/ignite cycle, weight must not change >4% or>SOmg (O.OSOOg), whichever is less.
WB476

PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS
SM 2540 B-2011
B - A x 100 = % TOTAL SOLIDS
B - D x 100 = % VOLATILE SOLIDS
C
%
"" C
✓ A
C
B
DATE
, 94fll7 �J /Z
SAMPLE
U/SED
DISH #
TARE
1st Dr Wt
Dr Wt
Dry Wt Diff
final -initial
% TOT SOLIDS
TIME
�Z •Z
dfe� O U o7/ i�// Q
,{
�J• ��(0
/'
lW//T.
�/ U�7(0
2
✓
2 gFinal
J /,IIII Z
0,
ANALYST
D
REPC
(initial ignition 550°C for 1 hour)
RTED BY: (repeat iginition 550°C for 30 minutes)
DATE
SAMPLE
USED
DISH #
TARE WOT
TIME
//
ANALYST
(initial ignition 550°C for 1 hour)
RTED BY: (repeat iginition 550°C for 30 minutes)
REP
DATE
SAMPLE
USEDD)ISH
#
TAREaWT
TIME
�^
�J • P
ANALYST
(initial ignition 550°C for 1 hour)
RTED BY: (repeat iginition 550°C for 30 minutes)
REP
DATE
SAMPLE
USED
DISH #
TAREQIWT
TIME
�
13r/'11Y
�•5
�73f 1j
ANALYST I .li
(initial ignition 550°C for 1 hour)
REPORTED BY: (repeat iginition 550°C for 30 min)
1st Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
3
9.
Dry Wt Diff *
(final -initial) I % TOT SOLIDS
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
Lll, I
1. 9
ry
Dry Wt (0 1 Final
SOLIDS
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
I q02
VIV2
0
0,U
Dry Wt Diff *
(final-inil I % TOT SOLIDS
Ignite Wt Diff *
Ignition Wt (g) Final Ignite Wt (g) (final -initial) % VOL SOLIDS
* Acceptance criteria for constant dry/ignition weight: Dry/Ignite, cool and weigh and repeat dry/ignite cycle, weight must not change >4% or >50mg (0.0500g), whichever is less.
WB476

PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS
SM 2540 B-2011
B - A x 100 = % TOTAL SOLIDS B=D x 100 = % VOLATILE SOLIDS
C / C
REP RTED BY:
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 30 minutes)
1st Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
2
Z
DATE
TIME
SAMPLE
g USED
. 989
DISH #
TARE WT.
Dr Wt
Final Dr Wt
Dry Wt Diff final -initial
% TOT SOLIDS
ANALYST
.3
(initial ignition 550°C for 1 hour)
BY: (repeat iginition 550°C for 30 minutes)
DATE SAMPLE gUSED DISH # TARE
TIME / � 2 7 .
ANALYST I/
(initial ignition 550°C for 1 hour)
TED BY: (repeat iginition 550°C for 30 minutes)
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
00 y
.3
D
TOT
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
q. I
y.974
DATE
TIME
SAMPLE
USED
DISH #
TARE WT.
Dr Wt
Final Dry Wt
Dry Wt Diff*
linal-initial
%TOT SOLIDS
ANALYST
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff
(final -initial)
I % VOL SOLIDS
(initial ignition 550°C for 1 hour)
REPORTED BY: (repeat iginition 550°C for 30 min)
* Acceptance criteria for constant dry/ignition weight: Dry/Ignite, cool and weigh and repeat dry/ignite cycle, weight must not change >4% or >SOmg (O.OSOOg), whichever is less.
►OO •

••.+c �r �wr �� �� Io�1 �� I��l � � Ill � � {� !�! t� � f� t�! I
PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS'
SM 2540 B-2011
B - A x 100 = % TOTAL SOLIDS BB=D x 100 = % VOLATILE SOLIDS
C � C
C A B
df/ G Dry Wt Diff
DATE
IO/I SAMPLE g USED DISH # uTARE WT. 1st Dr Wt Final Dr Wt final -initial % TOT SOLIDS
TIME 9 ��� Of�� ZO�� 07/7✓/ (1 �5• ��O / 0 7 �L . L
ANALYST
D
(initial ignition 550°C for 1 hour)
REP TED BY: (repeat iginition 550oC for 30 minutes)
1st Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
. 62
DATE
SAMPLE
USED
DISH #
TARE WT.
Dr Wt
Final Dr Wt
Dry Wt Diff
final -initial
%TOT SOLIDS
TIME
1 9�
37. U y58Z
ANALYST
(initial ignition 550°C for 1 hour)
REP RTED BY: (repeat iginition 550°C for 30 minutes)
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
�
9
DATE
TIME
SAMPLE
USED
/J_ N 7
DISH #
e
TARE WT.
y/.
Dr Wt
/, Z
Final Dry Wt
1
Dry Wt Diff
final -initial
% TOT SOLIDS
19
ANALYST
Ignite Wt Diff
DATE
TIME
SAMPLE
// U(S�ED
IS !0 9d
DISH #
TARE WT.
. M
Dr Wt
Final Dr Wt
Dry Wt Diff
final -initial
% TOT SOLIDS
ANALYST
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
(initial ignition 550°C for 1 hour)
REPORTED BY: (repeat iginition 550°C for 30 min)
* Acceptance criteria for constant dry/ignition weight: Dry/Ignite, cool and weigh and repeat dry/ignite cycle, weight must not change >4% or >50mg (0.0500g), whichever is less.
WB476

�c mil nw,
PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS
SM 2540 B-2011
B -A x 100 = % TOTAL SOLIDS
C
TIME
1NALYST
(initial ignition 550°C for i hour)
(repeat iginition 550°C for 30 minutes)
(initial ignition 550°C for I hour)
(repeat iginition 550°C for 30 minutes)
(initial ignition 5500C for 1 hour)
(repeat iginition 550°C for 30 minutes)
B=D x 100 = % VOLATILE SOLIDS
C
(initial ignition 550°C for 1 hour) I
REPORTED BY: g (g) Final Ignite
peat iginilcceptance criteria for constant dry/ignition: Dry/Ignite, cool and ee gion minfqounition Wt
wh andtrepeat dry%ignite550T for s cycle,)
weight must not change . or>SOm
�7
g (0.0500g), whichever is less.
WB476

8/9/18 Chain of Custody Record (COC)
NPDES#:
Client: Phone:
M E RITECH, INC.
Address: 75.E Yod lzmv+ to QV Fax:
`+ ENVIRONMENTAL LABORATORIES
NG 27a7w Email:
i 642 Tamco Rd. Phone: [phone]
Project:
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
G/,)�1
Attention: r'{^ r Turn Around Time*
*RUSH work needs prior approval,
How would you like your report sent?
www.meritechiabs.com
Char es Ann1v
Circle all that apply: mai referred), Fax, Mail Stcl 10 days) 3 5 Da�rs 24O48 Hrs
��
Sampling Dates &Times
p g
Person Taking Sample(Sign/Print):
Lab Use Only
Sample Location and/or ID # Start End
comp? #of On Ice? pH OK?
Test(s) Required
Date Time Date Time
Grab? Cont. yes / No Cl OK?
IJGAv�)�>✓
Slr!i
9+yseM
C
I
30 b eA cA 1
Temperature Upon
Receipt: ) li
Method of *** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to reservation. *** '`' l
Comments: .r Compositor #
Shipment: �%6r� SP�� �4,�,�.,�,,� S�i>!��s w�`! rr_
❑ UPS Jug #
❑ Fed Ex Are these results for regulatory purposes? Yes 0' No ❑ Report results in: mg/L ❑ mg/kg 0' ug/L ❑
❑ Relinquished by: D�g
Hand Delivery �/G/2D Time: /-0. /` Received by: Date: Time:
Other
Relinquished by: Date: Time:
Received by: Date: Time:
Relinquished by: Date: Time:
Received by Lab:r Time:+'

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name:
WWTP Name:
City of Danville
Northside WWTP
Monitoring Period: From l/1/2020 To
WQ Permit Number: WQ0036561
NPDES Number: VA0060593
12/31/2020
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑ 1 Alt B (Alk Treatment) ❑
Alt. C (Prior Testing)❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs E3
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
JAK (1) Fecal Density p
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion U
Anaerobic Digestion ❑
.. . ..........
If applicable to alternative performed (Class A or Class B) complete the following
monitoring
data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g ty
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech-nique
MinimurdGeo.
Mean
Maximurr
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000
1000
1000
col/g
0
Quarterly
G
SM9222D
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
jAlt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Ait. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation)
INe vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met,"
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
William Shreve - Area Manager Brent Collins; Director of Technical Services
Preparer Name and T (type or print) ---------Land Applier Name and Title(if(if applicable)(type or print)
0 a00 1 /6/2020
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

(�Ia'ne Analytical
www.pacolahs.com
May 13, 2020
Mr. Robert Clifton
INFRAMARK
229 NORTHSIDE DR
Danville, VA 24540
RE: Project: CLIENT# 92-618203
Pace Project No.: 7326258
Dear Mr. Clifton:
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, vW 25813
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on May 05, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - WestVirginia
• Pace Analytical Services - Lexington
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Stacy Heasley
[e-mail]
800-999-0105
Project Manager
Enclosures
cc: Ms. Kimberly Wickemeyer, INFRAMARK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, WV 25813
[phone]
Project: CLIENT# 92-618203
Pace Project No.: 7326258
Pace Analytical Services Beaver
225 Industrial Park Drive, Beaver, WV 25813
Virginia VELAP 460148
Virginia DCLS 00281
West Virginia DEP 060
Pace Analytical Services Lexington
782 North Lee Highway, Lexington, VA24450
CERTIFICATIONS
West Virginia DHHR 00412CM
North Carolina DEQ 466
Kentucky Wastewater Certification KY90039
Pennsylvania DEP 68-00839
Virginia VELAP 460150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, WV 25813
[phone]
SAMPLE SUMMARY
Project:
Pace Project No.:
CLIENT# 92-618203
7326258
Lab ID
Sample ID
Matrix
Date Collected
Date Received
7326258001
CATWALK 131 #1
Solid
05/05/20 07:25
05/05/20 11:57
7326258002
CATWALK 132 #2
Solid
05/05/20 08:00
05/05/20 11:57
7326258003
CATWALK 133 #3
Solid
05/05/20 07:35
05/05/20 11:57
7326258004
CATWALK 134 #4
Solid
05/05/20 07:55
05/05/20 11:57
7326258005
CATWALK 135 #5
Solid
05/05/20 07:40
05/05/20 11:57
7326258006
CATWALK 136 #6
Solid
05/05/20 07:50
05/05/20 11:57
7326258007
CATWALK 131 #7
Solid
05/05/20 07:30
05/05/20 11:57
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, WV 25813
[phone]
SAMPLE ANALYTE COUNT
Project: CLIENT# 92-618203
Pace Project No.: 7326258
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
7326258001
CATWALK 131 #1
SM 9222D - 2006
HADR
1
PASI-LX
SM 2540G-11
JPH
1
PASI-BVWV
7326258002
CATWALK 132 #2
SM 9222D - 2006
HADR
1
PASI-LX
SM 2540G-11
JPH
1
PASI-BVWV
7326258003
CATWALK 133 #3
SM 9222D - 2006
HADR
1
PASI-LX
SM 2540G-11
JPH
1
PASI-BVWV
7326258004
CATWALK 134 #4
SM 9222D - 2006
HADR
1
PASI-LX
SM 2540G-11
JPH
1
PASI-BVWV
7326258005
CATWALK 135 #5
SM 9222D - 2006
HADR
1
PASI-LX
SM 2540G-11
JPH
1
PASI-BVWV
7326258006
CATWALK 136 #6
SM 9222D - 2006
HADR
1
PASI-LX
SM 2540G-11
JPH
1
PASI-BVWV
7326258007
CATWALK 131 #7
SM 9222D - 2006
HADR
1
PASI-LX
SM 2540G-11
JPH
1
PASI-BVWV
PASI-BVWV = Pace Analytical Services - WestVirginia
PASI-LX = Pace Analytical Services - Lexington
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 10

aceAnalytical
www.paeelabs.eom
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, WV 25813
[phone]
ANALYTICAL RESULTS
Project: CLIENT# 92-618203
Pace Project No.: 7326258
Sample: CATWALK 131 #1 Lab ID: 7326258001 Collected: 05/05/20 07:25 Received: 05/05/20 11:57 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <1000 CFU/g 1000 1 05/05/20 14:47 05/06/20 16:02
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 90.4 % 0.10 1 05/06/20 15:47
Sample: CATWALK 132 #2 Lab ID: 7326258002 Collected: 05/05/20 08:00 Received: 05/05/20 11:57 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <1000 CFU/g 1000 1 05/05/20 14:47 05/06/20 16:02
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 93.7 % 0.10 1 05/06/20 15:50
Sample: CATWALK 133 #3 Lab ID: 7326258003 Collected: 05/05/20 07:35 Received: 05/05/20 11:57 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <1000 CFU/g 1000 1 05/05/20 14:47 05/06/20 16:02
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 90.6 % 0.10 1 05/06/20 15:54
Sample: CATWALK 134 #4 Lab ID: 7326258004 Collected: 05/05/20 07:55 Received: 05/05/20 11:57 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <1000 CFU/g 1000 1 05/05/20 14:47 05/06/20 16:02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/13/2020 01:50 PM without the written consent of Pace Analytical Services, LLC.
Page 5 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, WV 25813
[phone]
ANALYTICAL RESULTS
Project: CLIENT# 92-618203
Pace Project No.: 7326258
Sample: CATWALK 134 #4 Lab ID: 7326258004 Collected: 05/05/20 07:55 Received: 05/05/20 11:57 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 93.7 % 0.10 1 05/06/20 15:56
Sample: CATWALK 135 #5 Lab ID: 7326258005 Collected: 05/05/20 07:40 Received: 05/05/20 11:57 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <1000 CFU/g 1000 1 05/05/20 14:47 05/06/20 16:02
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 91.9 % 0.10 1 05/06/20 15:58
Sample: CATWALK 136 #6 Lab ID: 7326258006 Collected: 05/05/20 07:50 Received: 05/05/20 11:57 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <1000 CFU/g 1000 1 05/05/20 14:47 05/06/20 16:02
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 92.5 % 0.10 1 05/06/20 16:00
Sample: CATWALK 131 #7 Lab ID: 7326258007 Collected: 05/05/20 07:30 Received: 05/05/20 11:57 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <1000 CFU/g 1000 1 05/05/20 14:47 05/06/20 16:02
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 92.1 % 0.10 1 05/06/20 16:02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/13/2020 01:50 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, WV 25813
[phone]
QUALIFIERS
Project: CLIENT# 92-618203
Pace Project No.: 7326258
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/13/2020 01:50 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, WV 25813
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: CLIENT# 92-618203
Pace Project No.: 7326258
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
7326258001
CATWALK B1 #1
SM 9222D - 2006
26178
SM 9222D - 2006
26179
7326258002
CATWALK B2 #2
SM 9222D - 2006
26178
SM 9222D - 2006
26179
7326258003
CATWALK B3 #3
SM 9222D - 2006
26178
SM 9222D - 2006
26179
7326258004
CATWALK B4 #4
SM 9222D - 2006
26178
SM 9222D - 2006
26179
7326258005
CATWALK B5 #5
SM 9222D - 2006
26178
SM 9222D - 2006
26179
7326258006
CATWALK B6 #6
SM 9222D - 2006
26178
SM 9222D - 2006
26179
7326258007
CATWALK B1 #7
SM 9222D - 2006
26178
SM 9222D - 2006
26179
7326258001
CATWALK B1 #1
SM 2540G-11
25693
7326258002
CATWALK B2 #2
SM 2540G-11
25693
7326258003
CATWALK B3 #3
SM 2540G-11
25693
7326258004
CATWALK B4 #4
SM 2540G-11
25693
7326258005
CATWALK B5 #5
SM 2540G-11
25693
7326258006
CATWALK B6 #6
SM 2540G-11
25693
7326258007
CATWALK B1 #7
SM 2540G-11
25693
Date: 05/13/2020 01:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 10

CHAIN -OF -CUSTODY Analytical Request Document
LAB USE( WUN ' [ JZ0Z0 $ mberor
aceAnalytical II I I I I I I II II I'll? I I II I I I I
Chain -of -Custody is a LEGAL DOCUMENT -Complete all relevent fields �2
Company: Billing Information: o
Inframark-Danville Inframark-Danville WWTP 7326258 0,
229 Northiside Drive Preservative * L rn
Address: 229 Northside Dr., Danville, VA 24540 Container. rsarvative Type * Lab Project Manager. m
Danville, VA 24540 2._, 2 2 2 U U 8 3 2 U d—
Report To: Robert. [e-mail] Email To: [e-mail] " Preservative Types: (1) nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) zinc acetate,
(6) methanol, (7) sodium bisulfate, (8) sodium thiosulfate,19) hexane, (A) ascorbic acid, (B) ammonium sulfate,
Copy To: Site Collection Info/Address: (C) ammonium hydroxide, (0) TSP, (U) Unpreserved, (0) Other
[e-mail] Danville VA WWTP 229 Northside, Dr., Danville, VA 24540
_ Ana ses Lab Profile/Line:
Customer Project Name/Number: State: County/City: Time Zone Collected: Lab sample Receipt Checklist:
Inframark-Danville (client #: 92-618203) VA /Danville [ J PT [ I MT [ J CT VET
Custody Seals Present/intact Y N
Phone: [phone] Site/Facility ID #: Compliance Monitoring? I , custody Siyuatures Preseut Y N
Danville, VA V4 :hfTP ^^ nit VA�080593 ' t l cs [ ] No t1) col l error Si gnature Present'. N NA
Email: kimberly.wickemeyerCdinframark.com per f O I Bottles Intact N NA
Collected By (print): Purchase Order#: ,/a0 DWPWSID#: i Z
Correct Bottles N NA
Robert Clifton Quote #: 00074511 DW Location Code + Sufficient volume g� N NA
_ Samples Received on Ice ®N NA
Coiley�d By (ignatur j: Turnaround Date Required: Imm fate y ac on Ice: Z VOA - Headspace Acceptable Y N NA
/Ll [�y� t l No O USDA Regulated Soils Y N NA
+ - Samples in Holding Time Y N NA
Sample Disposal: Rush: Field Filtered (if applicable): Z Residual Chlorine Present Y N NA
[� Dispose as appropriate [ ] Return [ ] Same Day [ j Next Day [ ) Yes P1 No th Z i I Cl Strips:
[ ] Archive: [ ] 2 Day [ 13 Day [ j 4 Day [ ] 5 Day = o ) Sample pH Acceptable Y N NA
Analysis: +� �) i I pH Strips:
[ Hold: (Expedite Charges Apply) Z Sl= I O Sulfide Present Y N NA
-' s Wastewater 1 ,� O Lead Acetate Strips:
Matrix Codes (nse, t ,n Matrix box below): Drinking Water (DW), Ground Water (GW), astewater (WW), ( CU L � i qj !
Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT) O + _ Ur .! V LAB USE ONLY:
1 Comp / Collected (or Res j # of Q o Q �p Lab Sample Comments:
TComposite End Z s_ (n U (�
Customer Sample ID Matrix i Grab Composite Start) G Ctnsy- y, v 06 (i
06
Date Time Date Time F— Q Z F— CO F— W O U U- .
Catwalk B 1 #1 SL* Grab ; owwo v72.5 - - - - - - - - No 1
Catwalk 62 #2 SL* Grab 05/05/20 10000 - - - - - - No 1 X
Catwalk 133 #3 SL* I Grab 05!05/20 ' b735 - - - - - - No 1
Catwalk R4 #4 SL* 1 Grab 05/05/20 5rj _ _ _ _ _ _ No
—__
Catwalk B5 #5 SL* j Grab 05/05rto ��C7 - - - - - - No 1 1 x
---- - -- —t
Catwalk B6 #6 SL* I Grab 05/05!20 ' 6 75D - - - -_- - - - NO 1 X
Catwalk B1 #i SL* Grab 05/05/20 07 - - - - - - - - No 144
x
i
Customer Remarks /Special Conditions / Possible Hazards: Type of Ice Used: Blue Dry None i� SHORT HOLDS PRESENT (<72 hours):D N N/A Lab Sample Temperature Info:
Packing Material Used: Lab Tracking #: Temp Blank Rece Therm ID#: /� ed: Y N NA
'Biosolids for Fecal Coliform Cooler 1 Temp Upon Receipt:h&OC
Bottles: 120 mL Sterile for microbiology Samples received via: _ Cooler 1 Therm Corr. Factor:— , oC
Radchem sampie(s) screened (<SUU cpm): Y N NA FEDEX UPS lent Courier Pace Courier Cooler 1 Corrected Temp: , oC
Relinquished by/Compan : (Signature) Date/Time: Re v d by/Company: (Signature) Date/Time: MT1L LAB USE ONLY Comments:
0 ��'sr Table #:
_ _ .--pAcctnum: _ _�
Relinquished y/Co ny: (Signature) Date/Ti Received by/Company: (Signature) Date%Time:
f Template: Trio Rlank Received: v N NA
I I HCL McOH TSP Other
Preiogin:
Relinquished by/Company: (Signature) Date/rime: Received by/Company: (Signature) Date/Time: PM; Non Conformance(s): Page:
I f (PB: YES / NO of:

�LIMS73 Lab Sample Condition Upon Receipt (West Virgir"i0# : 7326256
.. Face,4nayibsar. WW
Client Name: ✓) CJ74tM4 rL PM: SDH Due Date: 05/ 15/20
� CLIENT: INFRAMARK
Courier: ❑ Fed Ex ❑ UPS ElUSPS V Client ❑ Commercial ❑ Pace F
Tracking #:
Custody Seal on Cooler/Box/Containers Present: ❑ yes 46 no Seals intact: ❑ yes ❑ no
Thermometer Used %X (&� Z cl Type of Ice: Ce ) Blue None
q �1,
Cooler Temperature Observed Temp U C Correction Factor: C Final Temp: V ' -C
Comments: pH paper Lot# Date and Initials of person examining
contents:
Ye
No
N/A
Chain of Custody Present:
1.
Chain of Custody Filled Out:
2.
Chain of Custody Relinquished:
3.
Sampler Name & Signature on COC:
z
4.
Sample Labels match COC: V
-Includes datettime/ID Matrix:
5.
Samples Arrived within Hold Time:
6.
Short Hold Time Analysis (<72hr remaining):
7.
Rush Turn Around Time Requested:
8.
Sufficient Volume:
9.
Correct Containers Used:
-Pace Containers Used:
10.
Containers Intact:
11.
Orthophosphate field filtered:
12.
Hex Cr Aqueous sample field filtered:
-pH adjusted within 24 hours? (If yes, indicate acid lot #)
13.
Filtered volume received for Dissolved tests:
14.
All containers have been checked for preservation:
exceptions: VOA, coliform, O&G, LLMercury, Non -aqueous matrix
All containers meet method preservation requirements:
15.
Initial when
when
Datettime samples S% g
provided to lab
Tests not preserved:
Heads ace in VOA Vials:
116.
Trip Blank Present:
Trip Blank Custody Seals Present:
17.
Initial when
completed:
r^ !1 1� ,
Date: —J J V O)-o
Client Notification/ Resolution:
Person Contacted: Date/Time: Contacted By:
Comments/ Resolution:
❑ A check in this box indicates that additional information has been stored in ereports.
'PM review is documented electronically in LIMS, when the Project Manager closes the SRF Review schedule in LIMS. The status may be reviewed in the Status section
of the Workorder Edit Screen.
Pa
SCUR WV - reaK2299 f 10

Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Report Date: 6/12/2020
Date Sample Rcvd: 5/12/2020
Vector Attraction Reduction / Aerobically Digested Sludge (30 Day Test
Meritech Work Order # 05122007 Sample: Danville Composite 5/12/20
Total Solids Volatile Solids % Volatile Solids
Week 1 0.460 0.190 0.409
Week 2
0.510
0.230
0.444
Week 3
0.500
0.230
0.456
Week 4
0.450
0.200
0.444
Week 5
0.480
0.220
0.458
Van Kleek Reduction (%): -22.42
I hereby certify that I have reviewed and approve these data.
Pass or Fail
Pass
Laboratory Represe tative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

DATE
TIME /l a
ANALYST
rDATE
TIME
NALYST
PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS
SM 2540 B-2011
B - A x 100 = % TOTAL SOLIDS B=D x 100 = % VOLATILE SOLIDS
C
C
C A B
Dry Wt I
USED DISH # TARE WT. 1st Dry Wt 9 Final DEX Wt final-ini
D yy. 2 1 qq-blol
D
(initial ignition 5500C for 1 hour)
BY: (repeat iginition 5500C for 30 minutes)
TOT
1st Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
Dry Wt Diff
]VIPLE L USED DISH # TARE WT. Dr Wt Final Dr Wt (final -initial) % TOT SOLIDS
(initial ignition 5500C for 1 hour)
REP TED BY: (repeat iginition 550oC for 30 minutes)
DATE SAMPLE USED DISH # I TARE WT
TIME /J! 59 / 9/2
ANALYST
M
(initial ignition 550°C for 1 hour)
(repeat iginition 5500C for 30 minutes)
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
I
Wt (g) 1 Final
SOLIDS
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
D
DATE
Dry Wt Diff
SAMPLE USED DISH # ////TARE WT, Dr Wt Final DryWt final -initial
7/-
�f / l __y/-'3z52 41,5252
% TOT SOLIDS
TIME
ANALYST
(initial ignition 550°C for 1 hour)
REPORTED BY: (repeat iginition 5500C for 30 min)
* Acceptance criteria for constant dry/i nition wei ht D /I 't I
WB476
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
ll''
D-
2
J. /
g g ry gm e, coo and weigh and repeat dry/ignite cycle, weight must not change >4% or >50mg (0.0500g), whichever is less.

TIME
ANALYST
TIME
ANALYST
TIME
ANALYST
PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS
SM 2540 B-2011
B - A x 100 = % TOTAL SOLIDS BD x 100 = % VOLATILE SOLIDS
C C
% C VV A B
Dry Wt Difl
SAMPLE g USED DISH # i TARE WT. 1st Dry Wt Final Dry Wt final-initia
122 0 7 1..,5 259. 3 9. 33 55D
i D
I.=
(initial ignition 5500C for 1 hour)
(repeat iginition 550°C for 30 minutes)
(initial ignition 550°C for 1 hour)
BY: (repeat iginition 550°C for 30 minutes)
MPLE e USED DISH # I TARE
TED BY:
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 30 minutes)
1st Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
29. 218 1
13.1
Dry Wt Diff *
Dry Wt Final Dry Wt
1.213qgl.207q
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
/.
Wt Final Dry Wt final-initia
319 I 3 9.13 3
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
.D
.22
Dry Wt Diff
DATE I I I SAMPLE t USED I DISH # I TARE WT. (a) Dry Wt (2) Final Dry Wt (e) 1 (final -initial) I % TOT SOLIDS
TIME 0 J . 171L 't Z I
ANALYST
(initial ignition 550°C for 1 hour)
REPORTED BY: (repeat iginition 550°C for 30 min)
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
* Acceptance criteria for constant dry/ignition weight: Dry/Ignite, cool and weigh and repeat dry/ignite cycle, weight must not change >4% or>50mg (0.0500g), whichever is less.
WB476

PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS
SM 2540 B-2011
B -A x 100 = % TOTAL SOLIDS B=D x 100 = % VOLATILE SOLIDS
C / C
_
u
DATE
%f S
SAMPLE
jz USED
DISH #
WT.
1st Dr Wt
Final Dry Wt(final-initial)
Dry Wt Diff
% TOT SOLIDS
TIME
l/T/AR/E
1,
ANALYST
r,
(initial ignition 550°C for 1 hour)
BY: (repeat iginition 550°C for 30 minutes)
DATE
SAMPLE
a USED
DISH #
I TARE
TIME
ANALYST
(initial ignition 550°C for 1 hour)
BY: (repeat iginition 550°C for 30 minutes)
Ist Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
&
Dry Wt Di
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
DATE
TIME
SAMPLE
USED
�� 1 l/
DISH #
Z.
TARE WT.
. 1. yff
Dr Wt
Final Dr Wt
Dry Wt Diff
final -initial
% TOT SOLIDS
ANALYST
RE ORTED BY:
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 30 minutes)
Ignite Wt Diff *
Ignition Wt (g) Final Ignite Wt (g) (final -initial) % VOL SOLIDS
DATE
TIME
SAMPLE
g UUSpED
�� �a / J
DISH #
J • �
TARE WT.
� �f�
Dr Wt
Final Dr Wt
Dry Wt Diff
final -initial
% TOT SOLIDS
ANALYST
(initial ignition 550°C for 1 hour)
REPORTED BY: (repeat iginition 550°C for 30 min)
* Acce tance criteria for co t t d
i
WB476

PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS
SM 2540 B-2011
B - A x 100 = % TOTAL SOLIDS B_D x 100 = % VOLATILE SOLIDS
C V C
7711jrS 4 L4
DATE
Q
SAMPLE
USED
DISH #
TARE WT.
Ist Dry Wt
Final Dry Wt
Dry Wt Diff
final -initial
% TOT SOLIDS
TIME
: y�
_122,00
5•
3 . y
/
y�
ANALYST
' n
DATE
TIME
ANALYST
DATE
TIME
ANALYST
(initial ignition 5500C for I hour)
BY: (repeat iginition 5500C for 30 minutes)
AMPLEg USED DISH # I TARE
(initial ignition 550°C for 1 hour)
BY: (repeat iginition S50°C for 30 minutes)
SAMPLE g USED DISH # I TARE
TED BY:
(initial ignition 550"C for 1 hour)
(repeat iginition 550°C for 30 minutes)
1st Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
3 .q
.2
Dry Wt Diff *
Wt (g) I Final
SOLIDS
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
q•q
LI y 9
kWt Final
1-initia
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
'(final -initial)
% VOL SOLIDS
3 11rlv
RIM•2
DATE
SAMPLE
9 USED
#
TARE/WT.
Dr Wt
Dr Wt
Dry Wt Diff
final -initial
% TOT SOLIDS
TIME
I �-JD
QDISH
3•
• !
/Final
�(/• 2.72
ANALYST
(initial ignition 550°C for I hour)
REPORTED BY: (repeat iginition 5500C for 30 min)
* Acceptance criteria for constant dry/ignition weight: Dry/Ignite, cool and weigh and repeat dry/ignite cycle, weight must not change >4% or >50mg (0.0500g), whichever is less.
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
WB476

MUNW-1. MMWi 1.i nwx
DATE
TIME ry:Z
ANALYST R }
DATE
TIME
ANALYST
DATE
TIME
ANALYST
DATE
TIME
ANALYST
PERCENT TOTAL SOLIDS / PERCENT VOLATILE
SOLIDS
SM 2540 B-2011
B - A x 100 = % TOTAL SOLIDS
C
B=D x 100 = % VOLATILE
SOLIDS
�5
gs
C
A
B
SAMPLE
IZ USED
52p
DISH #
MTAREW�.Istl)r
Wt
Final Dr Wt
DryWtDiff*o/2 final -initial
/o TOT SOLIDS
I
(initial ignition 5500C for 1 hour)
BY: (repeat iginition 5500C for 30 minutes)
SAMPLE g USED DISH
(initial ignition 550°C for 1 hour)
BY: (repeat iginition 550°C for 30 minutes)
SAMPLE g USED DISH
(initial ignition 550°C for 1 hour)
TED BY: (repeat iginition 550oC for 30 minutes)
SAMPLE g USED DISH # TARE'
ly 9?yfi I I-
Ignite Wt Diff *
1st Ignition Wt (g)
Final Ignite Wt (g)
(final -initial)
% VOL SOLIDS
Dry Wt Diff
Final Dt'y W (g) final-inftial
TOT
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
-
79. d Z
a
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
0
.ZZ
Dry Wt
Final Dr Wt (g)
final-i.
0I
�
Ignite Wt Diff *
Ignition Wt (g)
Final Ignite Wt (g)
(final -initial)
% VOL SOLIDS
� r. afjz
a
�z 0�
. �z
(initial ignition 5500C for 1 hour)
REPORTED BY: (repeat iginition 550°C for 30 min)
* Acceptance criteria for constant dry/ignition weight: Dry/Ignite, cool and weigh and repeat dry/ignite cycle, weight must not change >4 /o or >50mg (0.0500g), whichever is less.
WB476

5-9-2016 Chain of Custody Record (COC)
NPDES#:
ME R I TE C H INC.
Client: EMA Resources Inc. Phone:_ 336-751-1441
1
ENVIRONMENTAL LABORATORIES
Address:_ 755 Yadkinville Rd Fax: [phone]
Mocksville NC 27028 Email: Brent. collins (cDemaresourcesinc.com
642 Tamco Rd. Phone: [phone]
Project:
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention:_ Brent Collins Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
WWW.CIIerltechlabS.COm
Circle all that appl Email( eferrecl), Fax, Mail Std soda s) 3-s Days zs
.
Sampling Dates &Times
p g
Person Taking Sample (Sign/Print):
��n f �j/,;,5
Lab Use Only
Sample Location and/or ID #
Start
End
Comp?
#of
Test(s) Required
on Ice?
pH OK?
Date
Time
Date
Time
Grab?
Cont.
Yes / No
CI OK?
\
UoAII; I L
s�71
g y%.�
C
I
30 Q a ,r i elj �J
Temperature Upon
Receipt:
Method of *** Dechlorination (<0.5 m) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. ***
,
Comments: �%�r� ������ S�=� fs Compositor#
Shipment: ,.c,/c�/�.b�
❑ UPS
Jug #
❑ Fed Ex Are these results for regulatory purposes? Yes � No ❑ Report results in: mg/L ❑ mg/kg Rr ug/L ❑
❑ Relinquished by: Date: / Time: Received by: Date: Time:
Hand Delivery 6/Z R�faw
❑ Other
Relinquished by: Date: Time:
Received by, Date: Time:
Relinquished by: Date: Time:
R ived 2!b:... v Ti 3�

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Danville WQ Permit Number:
WWTP Name: Northside WWTP NPDES Number:
Monitoring Period: From l/l/2020 To 12/31/2020
WQ0036561
VA0060593
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)❑
Alt. C (Prior Testing)❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
[_Heat
Gamma Ray ❑
Pasteurization ❑
Class B:
1Alt. (1) Fecal Density 21
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
F Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring
data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g tY
Number o
Excee-
dens
Frequency
of Analysis
Sample
Type
Analytical
Tech-nique
inimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
113
130
183
col/ g
0
Quarterly
Q Y
G
SM9222D
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform) I
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
It, 2 (40-day bench) ❑
Alt. 3 (30-day bench) 0
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
INo vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
William Shreve - Area Manager
Pre�rcr]NgAp and Tit type or print)
Signature of
Brent Collins; Director of Technical Services
-------Land Applier Name and Tw�ittl/lee (if applicable)(type or print)
4�24- 1/20/2021
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

(�Ia'ne Analytical
www.pacolahs.com
May 29, 2020
Mr. Robert Clifton
INFRAMARK
229 NORTHSIDE DR
Danville, VA 24540
RE: Project: INFRAMARK- DANVILLE 92-618203
Pace Project No.: 7328055
Dear Mr. Clifton:
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, vW 25813
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on May 18, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - WestVirginia
• Pace Analytical Services - Lexington
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Stacy Heasley
[e-mail]
800-999-0105
Project Manager
Enclosures
cc: Ms. Kimberly Wickemeyer, INFRAMARK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, WV 25813
[phone]
Project: INFRAMARK- DANVILLE 92-618203
Pace Project No.: 7328055
Pace Analytical Services Beaver
225 Industrial Park Drive, Beaver, WV 25813
Virginia VELAP 460148
Virginia DCLS 00281
West Virginia DEP 060
Pace Analytical Services Lexington
782 North Lee Highway, Lexington, VA24450
CERTIFICATIONS
West Virginia DHHR 00412CM
North Carolina DEQ 466
Kentucky Wastewater Certification KY90039
Pennsylvania DEP 68-00839
Virginia VELAP 460150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, WV 25813
[phone]
Project:
Pace Project No.:
INFRAMARK- DANVILLE 92-618203
7328055
Lab ID
Sample ID
7328055001
CATWALK 131 #1
7328055002
CATWALK 132 #2
7328055003
CATWALK 133 #3
7328055004
CATWALK 134 #4
7328055005
CATWALK 135 #5
7328055006
CATWALK 136 #6
7328055007
CATWALK 137 #7
SAMPLE SUMMARY
Matrix
Date Collected
Date Received
Solid
05/18/20 08:25
05/18/20 13:10
Solid
05/18/20 09:00
05/18/20 13:10
Solid
05/18/20 08:35
05/18/20 13:10
Solid
05/18/20 08:55
05/18/20 13:10
Solid
05/18/20 08:40
05/18/20 13:10
Solid
05/18/20 08:50
05/18/20 13:10
Solid
05/18/20 08:30
05/18/20 13:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, WV 25813
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
INFRAMARK- DANVILLE 92-618203
7328055
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
7328055001
CATWALK 131 #1
SM 9222D - 2006
HADR
1
PASI-LX
SM 2540G-11
NEM
1
PASI-BVWV
7328055002
CATWALK 132 #2
SM 9222D - 2006
HADR
1
PASI-LX
SM 2540G-11
NEM
1
PASI-BVWV
7328055003
CATWALK 133 #3
SM 9222D - 2006
HADR
1
PASI-LX
SM 2540G-11
NEM
1
PASI-BVWV
7328055004
CATWALK 134 #4
SM 9222D - 2006
HADR
1
PASI-LX
SM 2540G-11
NEM
1
PASI-BVWV
7328055005
CATWALK 135 #5
SM 9222D - 2006
HADR
1
PASI-LX
SM 2540G-11
NEM
1
PASI-BVWV
7328055006
CATWALK 136 #6
SM 9222D - 2006
HADR
1
PASI-LX
SM 2540G-11
NEM
1
PASI-BVWV
7328055007
CATWALK 137 #7
SM 9222D - 2006
HADR
1
PASI-LX
SM 2540G-11
NEM
1
PASI-BVWV
PASI-BVWV = Pace Analytical Services - WestVirginia
PASI-LX = Pace Analytical Services - Lexington
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, VW 25813
[phone]
ANALYTICAL RESULTS
Project: INFRAMARK- DANVILLE 92-618203
Pace Project No.: 7328055
Sample: CATWALK 131 #1 Lab ID: 7328055001 Collected: 05/18/20 08:25 Received: 05/18/20 13:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <123 CFU/g 123 0.123 05/18/20 17:38 05/19/20 15:38
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 91.8 % 0.10 1 05/20/20 16:28
Sample: CATWALK 132 #2 Lab ID: 7328055002 Collected: 05/18/20 09:00 Received: 05/18/20 13:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <183 CFU/g 184 0.184 05/18/20 17:38 05/19/20 15:38
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 94.5 % 0.10 1 05/20/20 16:29
Sample: CATWALK 133 #3 Lab ID: 7328055003 Collected: 05/18/20 08:35 Received: 05/18/20 13:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <120 CFU/g 121 0.121 05/18/20 17:38 05/19/20 15:38
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 91.7 % 0.10 1 05/20/20 16:32
Sample: CATWALK 134 #4 Lab ID: 7328055004 Collected: 05/18/20 08:55 Received: 05/18/20 13:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <141 CFU/g 142 0.142 05/18/20 17:38 05/19/20 15:38
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/29/2020 01:46 PM without the written consent of Pace Analytical Services, LLC.
Page 5 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, VW 25813
[phone]
ANALYTICAL RESULTS
Project: INFRAMARK- DANVILLE 92-618203
Pace Project No.: 7328055
Sample: CATWALK 134 #4 Lab ID: 7328055004 Collected: 05/18/20 08:55 Received: 05/18/20 13:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 92.9 % 0.10 1 05/20/20 16:33
Sample: CATWALK 135 #5 Lab ID: 7328055005 Collected: 05/18/20 08:40 Received: 05/18/20 13:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <113 CFU/g 114 0.114 05/18/20 17:38 05/19/20 15:38
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 91.2 % 0.10 1 05/20/20 16:34
Sample: CATWALK 136 #6 Lab ID: 7328055006 Collected: 05/18/20 08:50 Received: 05/18/20 13:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <120 CFU/g 121 0.121 05/18/20 17:38 05/19/20 15:38
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 91.7 % 0.10 1 05/20/20 16:37
Sample: CATWALK 137 #7 Lab ID: 7328055007 Collected: 05/18/20 08:30 Received: 05/18/20 13:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <119 CFU/g 119 0.119 05/18/20 17:38 05/19/20 15:38
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 91.6 % 0.10 1 05/20/20 16:39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/29/2020 01:46 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, WV 25813
[phone]
QUALIFIERS
Project: INFRAMARK- DANVILLE 92-618203
Pace Project No.: 7328055
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/29/2020 01:46 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, VW 25813
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: INFRAMARK- DANVILLE 92-618203
Pace Project No.: 7328055
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
7328055001
CATWALK B1 #1
SM 9222D - 2006
27176
SM 9222D - 2006
27194
7328055002
CATWALK B2 #2
SM 9222D - 2006
27176
SM 9222D - 2006
27194
7328055003
CATWALK B3 #3
SM 9222D - 2006
27176
SM 9222D - 2006
27194
7328055004
CATWALK B4 #4
SM 9222D - 2006
27176
SM 9222D - 2006
27194
7328055005
CATWALK B5 #5
SM 9222D - 2006
27176
SM 9222D - 2006
27194
7328055006
CATWALK B6 #6
SM 9222D - 2006
27176
SM 9222D - 2006
27194
7328055007
CATWALK B7 #7
SM 9222D - 2006
27176
SM 9222D - 2006
27194
7328055001
CATWALK B1 #1
SM 2540G-11
27460
7328055002
CATWALK B2 #2
SM 2540G-11
27460
7328055003
CATWALK B3 #3
SM 2540G-11
27460
7328055004
CATWALK B4 #4
SM 2540G-11
27460
7328055005
CATWALK B5 #5
SM 2540G-11
27460
7328055006
CATWALK B6 #6
SM 2540G-11
27460
7328055007
CATWALK B7 #7
SM 2540G-11
27460
Date: 05/29/2020 01:46 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 10

CHAIN -OF -CUSTODY Analytical Request Document LABU, WO# ; 7323®55
Number or
�,ir ac.c.rv.uyuvu.
--- Chain -of -Custody is a LEGAL DOCUMENT -Complete all relevent fields
.�
! ��I
Company:
Billing Information:
7328055
-'
Inframark-Danville
Inframark-Danville WWTP
229 Northside Drive
Container Preservative Type * Project Manager:
Address: 229 Northside Dr., Danville, VA 24540
Danville, VA 24540
�11-ab
2 2 U U 8 3 2 U
�
a
* Preservative Types: (1) nitric acid, (2) sulfuric acid (3) hydrochloric acid, (4) sodium hydroxide, (5) zinc acetate,
(6) methanol, (7) sodium bisulfate, (8) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (8) ammonium sulfate,
�.
Report To: [e-mail]
@
Email To: [e-mail]
Site Collection Info/Address:
(C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (0) Other
Copy To: [e-mail] er Inframark.com
y y
Danville VA WWTP 229 Northside, Dr., Danville, VA 24540
Analyses Lab Profile/Line:
n
Customer Project Name/Number:
State: County/City: Time Zone Collected:
Lab sample Rece'Pt cnee ci tt:
Inframark-Danville (client #: 92-618203)
VA /Danville [ ] PT [ ] MT [ ] CT [yrET
.._ i5 a15 t es n Si
F
`I
Y
Phone: [phone]
Site/Facility ID #:
Compliance Monitoring?
t s vdy iq a sties -sent
r
N e for ..ynat_r:re Ureeant
Email: [e-mail]
Danville, VA WWTP permit VA0060593
[ /Yes [ ] No
g ,
0
e ttlf
m NA
Collected By (print):
Purchase Order #: I 0 a>3 9
DW PWS ID #:
Z i _Fn v< - :ram
d NA
Robert Clifton
Quote #: 00074511
DW Location Code:
+ s r R i reo. e Ice
•,•. N NA
Col t By e)
Turnaround Date Required:
Imme late y Pace on Ice:
Z I riea �5L v �e h� e tables
r 3 .�eq - ' ed .:K-.
t N NA
N NA
(� a [KYes [] No 3 3 F x I c T Te r NA
Sample Disposal: Rush: Field Filtered (if applicable): Z c �c c .er _� :f NA
Same Da Next Da Yes No i3
[� Dispose as appropriate [ ]Return [ ] Y [ ] Y [ ] lid M O sa r aclr. N NA
[ ]Archive: [ ] 2 Day [ ] 3 Day [ ] 4 Day [ ] 5 Day Z O �
[ ]Hold: (Expedite Charges Apply) Analysis: Z i Q V) O esl �' '! N NA
'� r'a .7 ACe .1 �' or.I' �._
* Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW), a M z O
Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT) + -C C) LAB USE, ONLY.,,,
Comp / Collected (or Res # of l O ? od a Lab said le ems:
Customer Sample ID Matrix * Grab Composite Start) Composite End Cl Ctns v E = O 0 U) U
Date Time DaterTime 1-: Q Z � m < [—ALL! 0 .. -�.
Catwalk 61 #1 SL* Grab o5n8no2o O� - - - - No 1CatwalkB2 #2 SL* Grab o5n8no2o C)d ---- No 1Catwalk B3 #3 SL* Grab o5n8no2o 5 ----No 1
Catwalk B4 #4 SL* Grab 05n8n020 p$ - - - - - - - - No 1
Catwalk B5 #5 SL* Grab 05n8n020 ll - - - - - - - - No 1 s l t
o5/18no20 - - - - - - - - No 1
Catwalk B6 #6 SL* Grab
Catwalk B1 #7 SL* Grab 05n8n020 n$ - - - - - - - - INo 1
f �
Customer Remarks / Special Conditions / Possible Hazards: Type of tee Used: e lue Dry None SHORT HOLDS PRESENT (<72 hours)(N N/A Lab Sample Temperature Info:
Lab Temp Blank R ceived: NA
Packing Material Used: Therm ID#: /
"Biosolids for Fecal Coliform �._aP. Cooler 1 Temp Upon Receipt: oC
]
Sterile for microbiology Samples received via: Cooler 1 Therm Corr. Factor: _ , oC
Bottles: 120 me
Radchem sample(s]cre�ned (<500 cpm): Y N NA
FEDEX UP5 Courier Pace Courier Cooler 1 Corrected Temp:_-oC
EDate�/Ti MT1L LAB USE ONLY Comments:
Reli ui hed by/Company: (Sign re) Date/Time: Received by/Com (Signatur�^?j
C� Q Table#:
lIt/(L l d ��/X'/�' jn� r (� 1 Acctnum:
Relinquished by/Co pang: ( ignature) Date/Time: ------------------
ived by/Company: (Signature) Date/Time: Template: Trip Blank Received: Y N NA
HCL McOH TSP Other
Prelogin: _
Relinquished by/Company: (Signature) Date/Time: Received by/Company: (Signature) Date/Time: PM: Non Conformance(s): Page:
oa• YES / NO $of:

WO#:7328055
LIMB/3 Lab Sample Condition Upon Receipt (West Virginia)
Client Name:
PM: SDH Due Date: 05/29/20
Courier: ❑ Fed Ex [I UPS ❑ USPS lent ❑ Commercial ❑ Pace ❑ Ot CLIENT: INFRAMARK
Tracking #:
Custody Seal on Cooler/Box/Containers�re nt: ❑ yesO Seals intact: ❑yes ❑ no
Thermometer Used t\i\�f \`(n"A� Type of Ice:o
Blue None--�(�
Cooler Temperature Observed Temp ° C Correction Factor: `� ° fO�° C Final Temp: 3 �i ° C
Comments: pH paper Lot# Date and G� / initials off person exa ini
contents)c`AT•
Yes
No
N/A
1
Chain of Custody Present:
V
Chain of Custody Filled Out:
2
Chain of Custody Relinquished:
7:73
Sampler Name & Signature on COC:
4
Sample Labels match COC: V
-Includes date/time/ID Matrix:
5.
6
Samples Arrived within Hold Time:
Short Hold Time Analysis (<72hr remaining):
7.
Rush Turn Around Time Requested:
g
Sufficient Volume:
9
Correct Containers Used:
-Pace Containers Used:
10.
Containers Intact:
11
Orthophosphate field filtered:
12
Hex Cr Aqueous sample field filtered:
-pH adjusted within 24 hours? (If yes, indicate acid lot #)
g
�i`_
Filtered volume received for Dissolved tests:
U14.
All containers have been checked for preservation:
exceptions: VOA, coliform, O&G, LLMercury, Non -aqueous matrix
All containers meet method preservation requirements:
Initial when
complet
Dateftime sa 1
provided to I
Tests not preserved:
Headspace in VOA Vials:
16.
Trip Blank Present:
Trip Blank Custody Seals Present:
17
Initial when
completed:
Date:
Client Notification/ Resolution:
Person Contacted:
Comments/ Resolution:
Date/Time:
Contacted By:
❑ A check in this box indicates that additional information has been stored in ereports.
'PM review is documented electronically in LIMS, when the Project Manager closes the SRF Review schedule in LIMS. The status may be reviewed in the Status section
of the Workorder Edit Screen.
Page 10 of 10
SCUR_M - rev.082219

Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Report Date: 6/29/2020
Date Sample Rcvd: 5/26/2020
Vector Attraction Reduction
/ Aerobically Digested Sludge
(30 Day Test)
Meritech Work Order # OS262019
Sample: Danville Composite
5/26/20
Total Solids
Volatile Solids
% Volatile Solids
Week 1
1.52
0.740
0.485
Week 2
1.32
0.700
0.530
Week 3
1.41
0.750
0.532
Week 4
1.57
0.750
0.481
Week 5
1.08
0.540
0.498
Van Kleek Reduction (%): -5.69
I hereby certify that I have reviewed and approve these data.
Pass or Fail
Pass
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

DATE
TIME
ANALYST
1
3.
H
SAMPLE USED DISH # TARE WT. Ist Dr Wt
5 2I / 9 / D . Z . 59 y
�
B
Final Dr Wt
Dry Wt Diff
final -initial
% TOT SOLIDS
9. 2
/..52
(initial ignition 5500C for 1 hour)
REPO TED BY: (repeat iginition 550°C for 30 minutes)
DATE
MPLE
USED
DISH #
TARE'
TIME
/ i
/� 2
ANALYST
(initial ignition 550°C for 1 hour)
REP rRTEDBY: (repeat iginition 550°C for 30 minutes)
DATE
AMPLE
USED
DISH #
TARE
TIME
O
Z.
T.5�
T
ANALYST
(initial ignition 5500C for I hour)
RE ORTED BY: (repeat iginition 550°C for 30 minutes)
Ignite Wt Diff *
Ist Ignition Wt (g)
Final Ignite Wt (g)
(final -initial)
% VOL SOLIDS
9.7/! y
i9, 7
0
� 7
Wt Final
3 W.3_1
Dry WtDiff *
final -initial) I % TOT
Ignite Wt Diff *
Ignition Wt (g)
Final Ignite Wt (g)
(final -initial)
% VOL SOLIDS
lw
_77
wtWt (g) Final
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
DATE SAMPLE USED DISH # TARE WT. I 2 Final Dr W
TIME /�. _58.9 2 J
WJ
ANALYST
(initial ignition 5500C for 1 hour)
REPORTED BY: (repeat iginition 550°C for 30 min)
* Acceptance criteria for constant dry/ignition weight Dry/Ignite cool and wei h and t d /'
Dry Wt Diff
final -initial % TOOT
"7 L
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
�9 a74
p
g repea ry ignite cycle, weight must not change >4% or >50mg (0.0500g), whichever is less.
WB476

PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS
SM 2540 B-2011
B - A x 100 = % TOTAL SOLIDS
C l
B=D x 100 = % VOLATILE SOLIDS
C
DATE
Gi 3 D
Dry Wt Diff
SAMPLE 2 USED DISH # TARE WT. Ist Dr Wt Final Dr Wt final -initial % TOT SOLIDS
TIME
3 Z ZZ
ANALYST
F
n
TIME
ANALYST
DATE
TIME
ANALYST
(initial ignition 550°C for 1 hour)
BY: (repeat iginition 550°C for 30 minutes)
SAMPLE g USED DISH # TARE
(initial ignition 550°C for I hour)
BY: (repeat iginition 550°C for 30 minutes)
SAMPLE g USED DISH # I TARE
TED BY:
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 30 minutes)
1st Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
.y6
Dry Wt
Final Dry Wt
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
Final
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
l.3
.
DATE
�ANEALYST
SAMPLE
9 USED
DISH #
5.
TARE WT.
3C� • l
Dr Wt
I
f
Final Dr Wt
Dry Wt Diff
final -initial
% TOT SOLIDS
(initial ignition 550°C for 1 hour)
REPORTED BY: (repeat iginition 5500C for 30 min)
* Acceptance criteria for constant dry/ignition wei ht D /I nite c 1 d : 1 d
WB476
Ignite Wt Diff
Ignition Wt (g) Final Ignite Wt (g) (final -initial) % VOL SOLIDS
g ry g , oo an we i an repeat dryhgmte cycle, weight must not change >4 /° or >50mg (0.0500g), whichever is less.

PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS
SM 2540 B-2011
B - A x 100 = % TOTAL SOLIDS
C
(repeat iginition 5500C for 30 minutes)
(repeat iginition 5500C for 30 minutes)
BB=D x 100 = % VOLATILE SOLIDS
C
1st Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
1 y
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
Ignite Wt Diff *
Ignition Wt (g)
y
Final Ignite Wt (g)
(final -initial)
% VOL SOLIDS
.17
(initial ignition 5500C for 1 hour)
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
REPORTED BY: (repeat iginition 5500C for 30 min)
* Acceptance criteria for constant dry/ignition weight: Dry/Ignite, cool and weigh and repeat dry/ignite cycle, weight must not change >4% or>50mg (0.0500g), whichever is less. 7
WB476

PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS
SM 2540 B-2011
DATE 6 • r SAMPLE USED DISH #
TIME ds 2 q �f
ANALYST R F 1 L
(initial ignition 550°C for 1 liour)
REPO TED BY: (repeat iginition 5500C for 30 minutes)
DATE
SAMPLE
USED
DISH #
TARE
TIME
14.12_
, y
ANALYST
(initial ignition 5500C for 1 liour)
RE RTED BY: (repeat iginition 550°C for 30 minutes)
DATE
SAMPLE
g USED
DISH #
TARE
TIME
ANALYST
5.
. 2
(initial ignition 5500C for 1 hour)
ZTED BY: (repeat iginition 550°C for 30 minutes)
Wt
n
nal-initial) I % TOT
1st Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
D. 9 7
W 3_?77
Dry Wt Diff
Final Dry Wt (g) (final -initial)
Ignite Wt Diff *
Ignition Wt (g)
Final Ignite Wt (g)
(final -initial)
% VOL SOLIDS
TT I7
Tel
r
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
. l3
DATE
SAMPLE
g USED
DISH #
TARE WT.
DryWt
Dr W
TIME
1. O
Q
�/ �/
gFinaol
ANALYST
(initial ignition 5500C for 1 ]tour)
REPORTED BY: (repeat iginition 550°C for 30 min)
* Acceptance criteria for constant dry/ignition weight: Dry/Ignite cool and wei h and re t d /' :
Dry Wt Diff
5
t (g)
7wti
Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
77gqFinal
g pea ry ignite cycle, weight must not change >4% or>50mg (0.0500g), whichever is less.
W B476

PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS
SM 2540 B-2011
B - A x 100 = % TOTAL SOLIDS B=D x 100 = % VOLATILE SOLIDS
C C
W tf �
��""
Dry Wt Diff
DATE
(y Z�//Z�//��
SAMPLE
ii USED
DISH #
TARE WT.
1st Wt
Fin7al Dr Wt
final -initial
% TOT SOLIDS
TIME
• �19f i
/
/ 5 22
l% /D'r
7�7
/'
`V 1
r
.
• /
ANALYST
46F
I D
TIME
ANALYST
rANALYST
ATE
ME
(initial ignition 550°C for 1 hour)
BY: (repeat iginition 550°C for 30 minutes)
SAMPLE USED DISH # TARE WT.
I Il)I I /.A qI AN
(initial ignition 550°C for 1 hour)
TED BY: (repeat iginition 550°C for 30 minutes)
SAMPLE e USED DISH # I TARE
TED BY:
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 30 minutes)
1st Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
07 1/0
�ydf
Wt Diff *
al -initial)
W
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
�7 073 7
117 0
I
al Dry Wt
% TOT
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
9 If6
/
DATE
SAMPLE
USED
DISH #
TARE WT.
Dr Wt
Final Dr Wt
Dry Wt Diff
final -initial
% TOT SOLIDS
TIME
15. 9
3
.3J- � 4 T
1 A W 7
D9
ANALYST
Ignite Wt Diff
(initial ignition 550°C for 1 hour) Ignition Wt (g) Final Ignite Wt (g) (final -initial) % VOL SOLIDS
REPORTED BY: (repeat iginition 550°C for 30 min) , S35 f3� Q f
* Acceptance criteria for constant dry/ignition weight: Dry/Ignite, cool and weigh and repeat dry/ignite cycle, weight must not change >4% or>50mg (0.0500g), whichever is less.

5-9-2016 Chain of Custody Record (COC)
NPDES#:
Client: EMA Resources Inc. Phone:_336-751-1441
Address:_ 755 Yadkinville Rd Fax: [phone]
Mocksville NC 27028 Email:[e-mail]
Project:
P.O.#:
Attention:_ Brent Collins Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply mail referred) , Fax, Mail St d to da s) 3 - 5 Days 2s
Person Taking Sample (Sign/Print):
,ar„�t C,�;, f Lab Use Only
MERITECH INC.
1
J \
\\ ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritechlabs.com
Sampling Dates & Times
p g
Sample Location and/or ID # Start End
Date Time Date Time
comp?
Grab?
#of
Cont.
Test(s) Required
On Ice?
Yes / No
pH K?
Cl OK?
7),Ilc
A�:
p G..'J', e�•C �,
�'
�/
i
-F
Temperature Upon
Receipt:
Method of
Shipment:
*** Dechlorination
<0.5 m of Ammonia, Cyanide, Phenol and TKN
samples must be done in the field prior to preservation. ***
Comments:
f�s�-.� daf� s�.�f a-/r�5�l�k
Compositor #
❑ UPS
Jug #
❑ Fed Ex
❑
Hand Delivery
Are these results for regulatory purposes? Yes [i�r No ❑
Relinquished by: Date: Time:
Report results in: mg/L ❑ mg/kg E�i' ug/L ❑
Received by: Date: Time:
❑ Other
Relinquished by: Date: Time:
Received b Y: Date: Time:
Relinquished by: Date: Time:
eiv y
at
: , Tits% 1
v

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Danville WQ Permit Number:
WWTP Name: Northside WWTP NPDES Number:
Monitoring Period: From 1/1/2020 To 12/31/2020
WQ0036561
VA0060593
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)[]
Alt. C (Prior Testing%S0
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogen g
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 111
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
JAK (1) Fecal Density p
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑ F Composting ❑
jAerob1c Digestion ❑
Anaerobic Digestion ❑
...
If applicable to alternative performed (Class A or Class B) complete the following
monitoring
data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
Number oFrequency
Excee-
dent
of Analysis
Y
Sample
Type
Analytical
Tech-ni ue
q
inimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
120
135
159
col/g
0
Quarterly
Y
G
SM9222D
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
colifonn)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt. I (VS reduction) ❑
1Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) r❑
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
jAlt. 6 (Alk. Stabilization ❑
jAlt 7 (Drying - Stable) ❑
1 Alt. 8 (Drying -Unstable) ❑
Alt. 9 (Injection) ❑
jAlt. 10 (Incorporation) ❑
INo vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
William Shreve - Area Manager Brent Collins; Director of Technical Services
Preparer Name Title (type or print Land Applier Name and Title (if applicable)(type or print)
�6 1/20/2021
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

(�Ia'ne Analytical
www.pacelabs.com
June 12, 2020
Mr. Robert Clifton
INFRAMARK
229 NORTHSIDE DR
Danville, VA 24540
RE: Project: DANVILLE VA0060593
Pace Project No.: 7329775
Dear Mr. Clifton:
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, vW 25813
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on June 02, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - WestVirginia
• Pace Analytical Services - Lexington
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Stacy Heasley
[e-mail]
800-999-0105
Project Manager
Enclosures
cc: Ms. Kimberly Wickemeyer, INFRAMARK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, WV 25813
[phone]
Project: DANVILLE VA0060593
Pace Project No.: 7329775
Pace Analytical Services Beaver
225 Industrial Park Drive, Beaver, WV 25813
Virginia VELAP 460148
Virginia DCLS 00281
West Virginia DEP 060
Pace Analytical Services Lexington
782 North Lee Highway, Lexington, VA24450
CERTIFICATIONS
West Virginia DHHR 00412CM
North Carolina DEQ 466
Kentucky Wastewater Certification KY90039
Pennsylvania DEP 68-00839
Virginia VELAP 460150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, WV 25813
[phone]
Project:
Pace Project No.:
DANVILLE VA0060593
7329775
Lab ID
Sample ID
7329775001
CATWALK 131 #1
7329775002
CATWALK 132 #2
7329775003
CATWALK 133 #3
7329775004
CATWALK 134 #4
7329775005
CATWALK 135 #5
7329775006
CATWALK 136 #6
7329775007
CATWALK 131 #7
SAMPLE SUMMARY
Matrix
Date Collected
Date Received
Solid
06/02/20 07:50
06/02/20 12:34
Solid
06/02/20 08:25
06/02/20 12:34
Solid
06/02/20 08:00
06/02/20 12:34
Solid
06/02/20 08:20
06/02/20 12:34
Solid
06/02/20 08:05
06/02/20 12:34
Solid
06/02/20 08:15
06/02/20 12:34
Solid
06/02/20 07:55
06/02/20 12:34
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, VW 25813
[phone]
SAMPLE ANALYTE COUNT
Project: DANVILLE VA0060593
Pace Project No.: 7329775
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
7329775001
CATWALK 131 #1
SM 9222D - 2006
HADR
1
PASI-LX
SM 2540G-11
NEM
1
PASI-BVWV
7329775002
CATWALK 132 #2
SM 9222D - 2006
HADR
1
PASI-LX
SM 2540G-11
NEM
1
PASI-BVWV
7329775003
CATWALK 133 #3
SM 9222D - 2006
HADR
1
PASI-LX
SM 2540G-11
NEM
1
PASI-BVWV
7329775004
CATWALK 134 #4
SM 9222D - 2006
HADR
1
PASI-LX
SM 2540G-11
NEM
1
PASI-BVWV
7329775005
CATWALK 135 #5
SM 9222D - 2006
HADR
1
PASI-LX
SM 2540G-11
NEM
1
PASI-BVWV
7329775006
CATWALK 136 #6
SM 9222D - 2006
HADR
1
PASI-LX
SM 2540G-11
NEM
1
PASI-BVWV
7329775007
CATWALK 131 #7
SM 9222D - 2006
HADR
1
PASI-LX
SM 2540G-11
NEM
1
PASI-BVWV
PASI-BVWV = Pace Analytical Services - WestVirginia
PASI-LX = Pace Analytical Services - Lexington
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, VW 25813
[phone]
ANALYTICAL RESULTS
Project: DANVILLE VA0060593
Pace Project No.: 7329775
Sample: CATWALK 131 #1 Lab ID: 7329775001 Collected: 06/02/20 07:50 Received: 06/02/20 12:34 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <120 CFU/g 1000 1 06/02/20 16:52 06/03/20 16:23
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 91.7 % 0.10 1 06/04/20 17:03
Sample: CATWALK 132 #2 Lab ID: 7329775002 Collected: 06/02/20 08:25 Received: 06/02/20 12:34 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <145 CFU/g 1000 1 06/02/20 16:52 06/03/20 16:23
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 93.1 % 0.10 1 06/04/20 17:06
Sample: CATWALK 133 #3 Lab ID: 7329775003 Collected: 06/02/20 08:00 Received: 06/02/20 12:34 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <130 CFU/g 1000 1 06/02/20 16:52 06/03/20 16:23
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 92.3 % 0.10 1 06/04/20 17:07
Sample: CATWALK 134 #4 Lab ID: 7329775004 Collected: 06/02/20 08:20 Received: 06/02/20 12:34 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <159 CFU/g 1000 1 06/02/20 16:52 06/03/20 16:23
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/12/2020 02:59 PM without the written consent of Pace Analytical Services, LLC.
Page 5 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, VW 25813
[phone]
ANALYTICAL RESULTS
Project: DANVILLE VA0060593
Pace Project No.: 7329775
Sample: CATWALK 134 #4 Lab ID: 7329775004 Collected: 06/02/20 08:20 Received: 06/02/20 12:34 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 93.7 % 0.10 1 06/04/20 17:09
Sample: CATWALK 135 #5 Lab ID: 7329775005 Collected: 06/02/20 08:05 Received: 06/02/20 12:34 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <127 CFU/g 1000 1 06/02/20 16:52 06/03/20 16:23
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 92.1 % 0.10 1 06/04/20 17:11
Sample: CATWALK 136 #6 Lab ID: 7329775006 Collected: 06/02/20 08:15 Received: 06/02/20 12:34 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <132 CFU/g 1000 1 06/02/20 16:52 06/03/20 16:23
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 92.4 % 0.10 1 06/04/20 17:12
Sample: CATWALK 131 #7 Lab ID: 7329775007 Collected: 06/02/20 07:55 Received: 06/02/20 12:34 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LEX Fecal Coliform (MF) Analytical Method: SM 9222D - 2006 Preparation Method: SM 9222D - 2006
Pace Analytical Services - Lexington
Fecal Coliforms <137 CFU/g 1000 1 06/02/20 16:52 06/03/20 16:23
Percent Moisture Analytical Method: SM 2540G-11
Pace Analytical Services - WestVirginia
Percent Moisture 92.7 % 0.10 1 06/04/20 17:14
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/12/2020 02:59 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, WV 25813
[phone]
QUALIFIERS
Project: DANVILLE VA0060593
Pace Project No.: 7329775
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/12/2020 02:59 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
225 Industrial Park RD
Beaver, VW 25813
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: DANVILLE VA0060593
Pace Project No.: 7329775
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
7329775001
CATWALK B1 #1
SM 9222D - 2006
29097
SM 9222D - 2006
29098
7329775002
CATWALK B2 #2
SM 9222D - 2006
29097
SM 9222D - 2006
29098
7329775003
CATWALK B3 #3
SM 9222D - 2006
29097
SM 9222D - 2006
29098
7329775004
CATWALK B4 #4
SM 9222D - 2006
29097
SM 9222D - 2006
29098
7329775005
CATWALK B5 #5
SM 9222D - 2006
29097
SM 9222D - 2006
29098
7329775006
CATWALK B6 #6
SM 9222D - 2006
29097
SM 9222D - 2006
29098
7329775007
CATWALK B1 #7
SM 9222D - 2006
29097
SM 9222D - 2006
29098
7329775001
CATWALK B1 #1
SM 2540G-11
29221
7329775002
CATWALK B2 #2
SM 2540G-11
29221
7329775003
CATWALK B3 #3
SM 2540G-11
29221
7329775004
CATWALK B4 #4
SM 2540G-11
29221
7329775005
CATWALK B5 #5
SM 2540G-11
29221
7329775006
CATWALK B6 #6
SM 2540G-11
29221
7329775007
CATWALK B1 #7
SM 2540G-11
29221
Date: 06/12/2020 02:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 10

1 R6 USE ONLY- A4i Y u+ ,r ce Workorder Number or
r
11�
CHAIN-OF-CUSTODY Analytical Request Document . � �����
aceAnalytical ® WO#
Chain -of -Custody is a LEGAL DOCUMENT -Complete all relevent fields
16
Company: Billing Information: III JSE ONLY rn
Inframark-Danville Inframark-Danville WWTP II
229 Northside Drive IIIIIIIIIIIIIIIII
anager:
Address: a_229 Northside Dr., Danville, VA 24540 Danville, VA 24540 2 7329775
Report To: [e-mail] Email To: [e-mail] " Pres ..__.._ . yi, °. kii nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) zinc acetate,
(6) methanol, (7) sodium bisulfate, (S) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (B) ammonium sulfate,
Copy To: Kimberl .Wickeme er Inframark.com Site Collection Info/Address: (C) ammonium hydroxide (D) TSP, (U) Unpreserved, (0) Other _
y y Danville VA WWTP 229 Northside, Dr., Danville, VA 24540 Analyses Lab Profile/Line:
Customer Project Name/Number: State: County/City: Time Zone Collected: ab �a t P xet:e ipt che< k --
Inframark-Danville (client M 92-618203) VA /Danville [ ] PT [ ] MT[ ] CT VET
Z
Phone:[phone] Site/Facility ID #: Compliance Monitoring? r ay 7r . ur ;Ge r A
Y
Danville, VA WWTP permit VA0060593 [ QVYes ( ] No lector ?``` `e
Email: [e-mail] :Q
DW PWS ID #: t d9
Collected By (print): Purchase Order #: 103506 ��350 to Z i ] yr a
Robert Clifton
Quote #: 00074511 DW Location Code: } es Re zca N NA
F
Collyd y (s'g at re): Turnaround Date Req fired: Immediately Pace on Ice: ' g� a - p acre
WC 5-�Ce r kWA �._P- s I N'l
[i�Yes [ ] No " .-. � � i � � , T... s r
Sample Disposal: Field Filtered if applicable): Z Z
Rush: ( PP ):
[� Dispose as appropriate [ ]Return [ ] Same Day [ ] Next Day [ ] Yes �/] No Cr) L
[ ] Archive: [ ] 2 Day [ ] 3 Day [ ] 4 Day [ ] 5 Day Z N € _
Analysis: '
[ 1Hold: (Expedite Charges Apply) Z �` �: (n -_ „e
* Matrix Codes Cn
(Insert
liAbDrinking
Water (DW), Ground Water ( Wastewater T? � (0
Product (), Soil/Sod (, Oil (OL)Wipe (WP),Ai(R), Tissue (TSB Bioassay (B)Vapor(V)Other(0) C O (D
Comp / Collected (or Res # of a _ a O (73
Composite End € U) ] U U
Customer Sample ID Matrix ` Grab Composite Start) CI Ctns
�-+
Date7 Time Date Time Q Z F— m I— l WILL
Catwalk 61 #1 SL* Grab 06/02/20 0715C) - - - - - - - - No 1 ,•
Catwalk B2 #2 SL* Grab 06/02120 O :Facj - - - - - - - - No 1 '
Catwalk 63 #3 SL* Grab 06/02/20 p a - - - - - - - - No 1 = m
Catwalk 134 #4 SL* Grab 06/02/20 o8a - - - - - - - - No 1
Catwalk 135 #5 SL* Grab o6i02120 pgD - - - - - - - - No 1 ] ,
Catwalk 136 #6 SL* Grab 06/02/20 t)'?[. - - - - - - - - No 1
Catwalk 131 #7 SL* Grab 06/02/20 i - - - - - - - - No 1 I
I
1
Customer Remarks Special Conditions Possible Hazards: %Type of ice Used eta Blue Dry None SHORT HOLDS PRESENT {<72 hours) l Y N N/A l Lab Sample Temperature Info
Temp Blank Received Y. fV NA j
Packing Material Used: Lab Tracking #.
Therm ID#: i
Cooler 1 Temp Upon Receipt oC
`Biosolids for Fecal Coliform
Bottles: 120 mL Sterile for microbiology a
'<Samples received via: — - i Cooler 1 Therm Corr. Factor J oC
Radchem samplers) screened (<S00 cpm). Y N NA 3 FEDEX UPS _ LitIent , Courier Pace Courier Cooler 2 Corrected Temp: a oC
C
MTJL LAB USE ONLY omment s: i
Relinquished by/Company: (Signature) Date/Time Receive ompany (`Signature - Cate/Time:
a, Table #:
SIZ L Acctnum: m.
Relinquished / ompany: (Signature) Date/Time: Received by/Company: (Signature) Date/Time: :Template: Trip Blank Received: Y N NA
iPretogin: 1 HCL McOH TSP Other
Relinquished by/Company: (Signature) Date/Time: Received by/Company: (Signature) Date/Time:nM: I Non Conformance(s): Page:
.r._..._.....�.,_._.—...... �........_, f ..._.....�.-- ........_.�.r.._.,_��,_,F— ,.�..._. F�.,._�.._-.. �._._,a�6..,�� .a .YES /.NO ...__,..w,0' ��.a,

LIMS73 Lab Sample Condition Upon Receipt (West Virginia) WO# : 7329775
b'" •'' PM : SDH J _FaoeanatytW Due Date; 05/12/20
Client Name: CLIENT: INFRAMARK
Courier: ❑ Fed Ex ❑ UPS ❑ USPS Client ❑ Commercial I—PPace ❑ Other:
Tracking #:
Custody Seal on Cooler/Box/Containers Present: ❑ yes Ehln. Seals intact: ❑ yes ❑ no
Thermometer Used a M L�j'1r.t( Type of Ice: l0 Blue None ?
Cooler Temperature �Obbssterrved Temp ° C Correction Factor: �'� ° C Final Temp: J ° C
Comments: pH paper Lot# Date and Initials of person examining
contents:
Yes
No
N/A
Chain of Custody Present:
1.
Chain of Custody Filled Out:
2.
Chain of Custody Relinquished:
3.
Sampler Name & Signature on COC:
4.
Sample Labels match COC:
-Includes date/time/ID Matrix:
5.
/r
✓0�
Samples Arrived within Hold Time:
6.
Short Hold Time Analysis (<72hr remaining):
7,
Rush Turn Around Time Requested:
g.
Sufficient Volume:
g.
Correct Containers Used:
-Pace Containers Used:
10.
Containers Intact:
11.
Orthophosphate field filtered:
12.
Hex Cr Aqueous sample field filtered:
-pH adjusted within 24 hours? (If yes, indicate acid lot #)
13.
Filtered volume received for Dissolved tests:
/
14.
All containers have been checked for preservation:
exceptions: VOA, coliform, O&G, LLMercury, Non -aqueous matrix
All containers meet method preservation requirements:
15.
Initial when
completed
Date/time samples
provided to lab
Tests not preserved:
Headspace in VOA Vials:
16.
Trip Blank Present:
Trip Blank Custody Seals Present:
17.
initial when
completed:
Date:
Client Notification/ Resolution:
Person Contacted:
Comments/ Resolution:
Date/Time:
Contacted By:
❑ A check in this box indicates that additional information has been stored in ereports.
*PM review is documented electronically in LIMS, when the Project Manager closes the SRF Review schedule in LIMS. The status may be reviewed in the Status section
of the Workorder Edit Screen.
Y
SCUR_WV - rev.0022jt9 10 of 10

Contact: Brent Collins
CIient: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Report Date. 7/24/2020
Date Sample Rcvd: 6/22/2020
Vector Attraction Reduction
I Aerobically Digested Sludge
30 Day Test
Meritech Work Order # 06222014
Sample: Danville Composite
6/22/20
Total Solids
Volatile Solids
o Volatile Solids
Week 1
1.50
0.720
0.480
Week 2
1.36
0.660
0.487
Week 3
1.23
0.630
0.512
Week 4
1.13
0.590
0.518
Week 5
1.27
0.630
0.497
Van Kleek Reduction (%): -7.20
I hereby certify that I have reviewed and approve these data.
Pass or Fail
Pass
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS
SM 2540 13-2011
13 - A x 100 = % TOTAL SOLIDS B=D x 100 � % VOLATILE
SOLIDS
C
C
/
W
C �/ A B
DATE
SAMPLE,
a USED
1.)LSII #
TARE WT.
1st Dr Wt
Finul Dry Wt
Dry WI
final-i
TIME
�.�
IR
D
a
ANALYST
AE
D
(initial ignition 550°C for 1 hour)
REPO TED BY: (repeat iginition 550°C for 30 minutes)
1st Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
19.17�
i7�
D
DATE
AMPLE;
USED
DISH # TARE WT.
Dr Wt
Dry Wt Diff
Final Dr Wt fnal-initial
TIME
1
� �.
7� �� D
//
7 • T
ANALYST
(inithd ignition 550°C for I hour)
REP RTED BY: (repeat iginition 550°C for 30 minutes)
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
�1
"
L
DATE
SAMPLE
USED
DISH #
TARE WT,
Dry Wt
Dry WtDiff*
final Dry Wt(final-initial) % TOT SOLIDS
Trn1E
Y.
ANALYST
(initial ignition 550°C for 1 hour)
RE RTED BY: (repeat iginition 550°C for 30 minutes)
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
y4 7 V
Ald
DATE_
SAMPLEUSED
DISH #
TARE tiVT.
Dr Wt
Dry Wt Diff
Final br Wt Enal-initial
TIME
ANALYST
(initial ignition 550°C for I hour)
REPORTED BY: (repeat iginition 550'C for 30 min)
Acceptance criteria for constant d I' ht D
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
f7IMM
f7 679
O
ry �gni ion we�g ryllgntte, cool and weigh and repeat dry/ignite cycle, weight must not change >4% or>50mg (0.0500g), whichever is less.
WB476
.1I

PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS
SM 2540 B-2011
R - A x 100 = % TOTAL SOLIDS
C
(initial ignition 550°C for I hour)
(repent iginition 5500C for 30 minutes)
(initial ignition 550°C for I hour)
(repeat iginition 5500C for 30 minutes)
(initial ignition 550°C for I hour)
(repeat iginition 5500C for 30 minutes)
B=D x 100 = % VOLATILE, SOLIDS
C
1st Ignition Wt (g)
Ignite Wt Diff *
Final Ignite Wt (g) (Final -initial)
% VOL SOLIDS
7
7
Ignition Wt (g)
Ignite Wt Diff
Final Ignite Wt (g) (final -initial)
% VOL SOLIDS
F
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
y
Ignite Wt Diff
(initial ignition 550°C for 1 hour)
Ignition Wt (g)
Final Ignite Wt (g)
(final -initial)
% VOL SOLIDS
REPORTED BY: (repeat iginition 550°C for 30 min)
, 2177
J - Z
tJ
* Acceptance criteria for constant drylignition weight: Dry/Ignite, cool and weigh and repeat dry/ignite cycle, weight must not change >4% or >50mg (0.0500g), whichever is less.

PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS
SM 2540 113-2011
B - A x 100 = % TOTAL SOLIDS BHD x 100 = % VOLATILE SOLIDS
C
,.1
wrd#3 C A C
B
DATE /8/10 SAMPLE USED DISH # TARE WT. I
TINY %'
ANALYST / 9• p l
Is
DATE
TINIE
ANALYST
DATE
TINY
ANALYST
DATE
TIME
ANALYST
Dry Wt Diff *
! D
(initial ignition 5500C for I hour)
TED BY: (repeat iginition 550°(: for 30 minutes)
SAMPLE iz USED DISH # I TARE WT
(initial ignition 550°C for I hour)
TF,D BY: (repeat iginition 550°C for 30 minutes)
SAMPLE g USE, D DISH # TARE
Ignite Wt Diff
Ist Ignition Wt (g)
Final Ignite Wt (g)
(final --initial)
% VOL SOLIDS
9/
Dry Wt Diff I
br IVt Final Dry Wt final -initial) I %TOTSOLIDS
Ignitian Wt (g)
Final Ignite Wt (g)
Ignite WI Diff *
(final -initial)
9/6 VOL SOLIDS
(initial ignition 550°C for I hour) Ignition Wt (g)
TED BY: (repeat iginition 550°C for 30 minutes)
SAMPLE USED DISPI # TARE WT. (g)_ Dry Wt (0
Finial Dr Wt
Dry Wt Diff
final -initial
% TOOT SOLIDS
Ignite Wt Diff*
Final Ignite Wt (g) (final-fittial) p/ VOL SOLIDS
+. (l
Dry Wt Diff
Final Dry Wt (g) (final -initial) % TOT SOIJt)S
(initial ignition 5500C for I hour) Ignition Wt (g) Final Ignite Wt
REPORTED BY: (repeat iginition 550°C for 30 min) 3
* Acceptance criteria for constant dry/ignition weight: Dry/Ignite, cool and weigh and repeat dry/ignite cycle, weight must not change>4% or>50mg (0.0500g), whichever is less.
(final -initial) I % VOL SOLIDS
W 84 76

PERCENT TOTAL SOLIDS / PERCENT VOLATILE
SOLIDS
SM 2540 B-2011
D - A x 100
C
= % TOTAL SOLIDS
Ii - D x 100 = % VOLATILE SOLIDS
C
V � �'l
C A
Q
Dry Wt Dil'f *
DATE
15
SA LE
USED
DISH 4 TARE WT. {
1st Dr Wt
final Dr Wt
D
final -initial
%TOT SOLIDS
I
TIME
.-NI
ANALYST
Ignite Wt Diff
(initial ignition 550°C for I hour)
Ist Ignition Wt {g)
g
final Ignite Wt (g)
(finai -initial)
% VOL SOLIDS
REPO
TED BY:
(repast iginition 550°C for 30 minutes)
38.1 Egg
Dry Wt Diff *
DATE
S 14IPLE
USED
DISH
TARE WT.
Dr Wt
Final Dr 1Vt
Ago
final -initial
%TOT SOLIDS
I•'
TIME
ANALYST
(Initial ignition 550°C for I hour}
Ignition Wt (g)
g
Final Ignite Wt (g)
Ignite Wt Diff*
(final -initial)
% VOL SOLIDS
REPORTED
BY:
(repeat iginition 550°C for 30 minutes)
Dry Wt Diff
DATE
AMPLE USED
DISH i# TARE 1VT,
Dr Wt
.
Final DryWt
final -initial)
%TOT SOLIDS
TIME
ANALYST
(initial ignition 550°C for I hour)
Ignition Wt (g)
Final Ignite Wt (g)
Ignite tDifr*
(final -initial)
% VOL SOLIDS
REl
ORTED BY:
(repeat iginition 550°C for 30 minutes)
Dry Wt Diff
DATE
SAMPLE
USED
DISH # TARE WT. )
Dry Wt )
q .
Final Dr Wt
�1�. 8
final -initial
% TOT SOLIDS
`-
TIME
ANALYST
Ignite Wt Diff *
(initial ignition 550°C for I hour)
Ignition Wt (g) Final Ignite Wt (g)
(final -initial}
% VOL SOLIDS
(repeat iginition 550°C for 30 min)
�' L
REPORTED 13Y.
* Acceptance criteria for constant dry/ignition weight: Dry/Ignite, cool and weigh and repeat dry/ignite cycle, weight most not change >4% or >50mg (0.05009), whichever is less.
ft— P-w

TIME
ANALYST
DATE
'TIME
ANALYST
DATE
'rimy;
ANALYST
PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS
SM 2540 B-2411
B=D x 100 = % VOLATILE SOLIDS
B -A x 100 = % TOTAL SOLIDS
C
_�✓
C
A
B
C
Dry Wt Dill
L L
SAMPLE
g USED
DISH #
1 TARE WT.
1st Dr Wt
Final Dr Wt
final-initlal
% TOT
z
q 1
�.2
..
n
(initial ignition 5500C for 1 hour)
TED BY: (repeat iginition 550,C for 30 minutes)
annr r a rt.Rrn I DISH # 1 TARE
(initial ignition 550°C for I hour)
By. (repeat iginition 550°C for 30 minutes)
AMPI.r e USED DISI-1 # I TARE..
(initial ignition 550°C for 1 hour)
BY: (repeat iginition 550°C for 30 minutes)
1st Ignition Wt (g)
Final Ignite Wt (g)
ignite Wt Diff *
(final -initial)
% VOL SOLIDS
'79. �
1 Dry WtDiff*
Final Dry Wt (g) final -initial % TOT
Ignition Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
J'
Dry Wti
Dry Wt (a) I (final-ini
IDS
Wt (g)
Final Ignite Wt (g)
Ignite Wt Diff
(flfinal-initial)
% VOL SOLIDS
7Ignition
r D
1
DATE SAMPLE g USED DISH # 1 TARE WT. Dr Wt Final Dry W
TIME K q 1317/7Z11
ANALYST
(initial ignition 550°C for 1 hour)
REPORTED BY- (repeat iginition 550°C for 30 min)
Dry Wt Diff
(final -initial) F.I. OT SOLIDS
Ignition Wt (g)
Final Ignite! Wt (g)
Ignite Wt Diff *
(final -initial)
% VOL SOLIDS
9•L
9(Z7
* Acceptance criteria for constant drylignition weight: Dry/Ignite, cool and weigh and repeat dry/ignite cycle, weight must not change >4% or >50mg (0,05009), whichever is less.

Chain of Custody Record (COC)
NPDES#:
ME R I T E C H INC.
client: �r��- ��5°"r`� �i1-�. Phone:
Address: 75S Fax:
ENVIRONMENTAL LABORATORIES
G�CSv,`I� L 7i-70Z Email:
i 642 Tamco Rd. Phone: [phone]
Project:
f Reidsville NC 27320 Fax: [phone]
Email: info@ meritechlabs.com
Attention: � rtr►•�-�'l/r +i Turn Around Tlme*
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Sampling Dates & Times
Person Takin Sample (Sign/Print):
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Lab Use Only
Sample Location
and/or ID # Start End
Comp? Hof TestsRequired
Date Time Date Time }
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*** Dechlorination (<0.5 p m) of Ammonia, Cyanide, Phenol and TKN samples must be done In the field prior to reservation. ***
Receipt: I G r
Shipment:
Comments:
Compositor #
❑ UPS
Fed Ex
Are these results for regulatory purposes? Yes
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NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY21-SL005467
�5{i �141..tiL
Client: James Y Blackwell
Advisor: Brent Collins
Predictive
7402 NC Hwy 158 W
EMA Resources Inc
;•
Yanceyville, NC 27379
755 Yadkinville Rd
f'. Soil Report Mehlich-3 Extraction
+_
Mocksville, NC27028
Sampled County : Caswell
Links to Helpful Information
Client ID: 242509
Advisor ID: 405413
Sampled: 09/11/2020 Received: 09/22/2020 Completed: 10/01/2020 Farm: C506
Sample ID: 00002
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O Mg S Mn Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.4 120-200 0
70 0 0 0 0
0 0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.51 1.16 5.2 75 1.3 5.7 89 33 51 21
32 228 154 100 100
267 0.1 2
Noah 0, olina
i
I Awl'
fotciW frum fuWCurnml5skm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY21-SL002215
�5{i �141..tiL
Client:
James Y Blackwell
Advisor: Brent Collins
Predictive
7402 NC Hwy 158 W
EMA Resources Inc
;•
Yanceyville, NC 27379
755 Yadkinville Rd
f'. Soil Report Mehlich-3 Extraction
+_
Mocksville, NC27028
Sampled County : Caswell
Links to Helpful Information
Client ID: 242509
Advisor ID: 405413
Sampled: Received: 08/11/2020 Completed: 08/19/2020
Farm: CS06
Sample ID: 00003
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.6
120-200 120
0
0 0
0
0
0 0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.22 1.08 7.2 79 1.5 5.6 11 108
45 26
56
353
229
76
76
103 0.1 1
Sample ID: 00004
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 1.1
120-200 0
0
0 0
0
0
0 0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.66 1.02 16.6 84 2.7 5.6 447 278
52 23
83
352
228
753
753
251 0.1 1
Noah 0, olina
i
I Awl'
Futacii frum fuWCurnml5skm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY21-SL002214
�5{i �141..tiL
Client:
James Y Blackwell
Advisor: Brent Collins
Predictive
7402 NC Hwy 158 W
EMA Resources Inc
;•
Yanceyville, NC 27379
755 Yadkinville Rd
f'. Soil Report Mehlich-3 Extraction
+_
Mocksville, NC27028
Sampled County : Caswell
Links to Helpful Information
Client ID: 242509
Advisor ID: 405413
Sampled: Received: 08/11/2020 Completed: 08/19/2020
Farm: cs07
Sample ID: 00001
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1 -Fescue/OGrass/Tim, M 0.0
120-200 0
40
0 0
pH$
0
0 0
Note: 12 Note:
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.36 1.11 10.6 99 0.1 7.1 112 51
88 9
49
400
240
383
383
929 0.1 1
Sample ID: 00002
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0
120-200 0
0
0 0
pH$
0
0 0
Note: 12 Note:
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.22 1.20 11.8 98 0.3 7.1 170 105
72 21
46
524
315
635
635
935 0.1 1
Noah 0, olina
i
I Awl'
Futacii frum fuWCurnml5skm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY21-SL002216
Client:
Glenn (Jr) Hodges
Advisor: Brent Collins
Predictive
2388 Allison Rd
EMA Resources Inc
Pelham, NC 27311
755 Yadkinville Rd
~$ Soil Report Mehlich-3 Extraction
+_
Mocksville, NC 27028
Sampled County : Caswell
Links to Helpful Information
Client ID: 309118
Advisor ID: 405413
Sampled: Received: 08/11/2020 Completed: 08/19/2020
Farm: CS09
Sample ID: 00001
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 1.0
120-200 0
0
0 0
0
0
0 0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.36 1.09 7.3 73 2.0 5.4 255 79
49 18
70
243
163
1112
1112
836 0.1 1
Sample ID: 00003
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.7
120-200 0
90
0 0
0
0
0 0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.36 1.20 5.2 68 1.6 5.5 149 26
51 15
50
315
206
173
173
616 0.1 2
Noah 0' olina
i
I Awl'
Futacii frum fuWCixrlml5skm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture