WQ0002834_2020 Residual Annual Report_20210226

Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?* r Annual Report
r Residual Annual Report
r Additional Information
r Other
Annual Report Year* 2020
Permit Number (IR)* WQ0002834
Applicant/Permittee Town of Burnsville
Email Notifications
Does this need review by the hydrogeologist?* r Yes r No
Regional Office Asheville
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Rease provide inforration on the person to be contacted by N B Staff
Name * Paul Isenhour
Email Address*
[e-mail]
electronic subnittal, confirmation of receipt, and other correspondence.
Project Information
........ .................................................................................................................................................. .
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
8288986277
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* WQ0002834
Fbs Current Existing permt number
Applicant/Permittee Address* po box97, Burnsville, NC 28714
Facility Name * Town of Burnsville DCAR
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Specifications, Calculations, Rc.)
Water Quality Labs _20210226_181815.pdf 8.39MB
Upload only 1 FLFdocurrent (less than 250 MB). NLRiple documents rust be contained into one FDFfile unless file is larger than
upload limit.
* V By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
t
Submission Date 2/26/2021

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Burnsville WQ Permit Number: WQ0002834
WWTP Name: j Town of Burnsville
NPDES Number:
NCO020290
Monitoring Period: From 1/1/2020
To
12/31/2020
Pathogen Reduction 15A NCAC 02T .1106) - Please indicate level achieved and alternativeperformed:
Class A:
I Alt. A (time/temp) X
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑ Aerobic Digestion 11
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:.
Parameter
Allowable Level
in Sludge
Pathogen Density
Number of
Excee-
Frequency
of Analysis
Sample
Type
Analytical
Tech-nique
inimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
123
268
455
minn!hg
0
only pile
G
sm922le2
Salmonella bacteria
(in lieu of fecal
colifonn)
3 MPN per 4 grams
total solid (dry
weigh
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternativeperformed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) X
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector
attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector
attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
s eternunahon as een made under my direction and supervision in accordance wit t e system designed to
ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and
vector attraction reduction requirements have been met. I am aware that there are significant penalties for false
certification including fine and imprisonment."
Paul Isenhour, Lab Manager
Preparer Name and Title (type or
Land Applier Name and Title (if applicable)(type or print)
print)
ture of Prep Date Signature of Land Applier (if applicable)
Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0002834
FACILITY NAME: Town of Burnsville
�TYOIr - Jadd Brewer
FACILITY TYPE tpjeasetcheck n ur ace isposa comp e e art A (Scurce(s) an "Residual n Volume only) and Part
..one):
Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar ear? Yes No ❑ If No skip parts A, B, C and certify form below
Part A*
*-
Sources(s) (include NPDES # if
Volume (dry tons
Reci lent Information
Amendmentl
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
Month
applicable)
January
NCO020290POTW
42.27
21.14
63.41
STEVE TAYLOR
0.25
NONROOT/LEF CROP
February
Digester
SARA ALLEN
0.17
NONROOT/LEF CROP
March
DALE BOLE
0.34
MULCH
April
JASON GREGORY
4.08
MULCH
May
WILLIAM MEEHAN
1.03
MULCH
June
JOE GLAIDINA
0.26
LAND RECLAMATION
July
JACOB EHRISMAN
0.42
MULCH
August
WILLIAM THOMAS
0.08
POTTING SOIL
September
October
November
December
Total from FORM DMSDF (su)
0
0
0
0
Totals: Annual(dry tons):tons):1
42.27 1
21.14
63.41 1
7 1
6.63
Amendment(s) used: I I
Bulking Agent(s) used: woad chips
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)
_
Part C:
Facility was comp ant urtng tVe past ca eaad r wil—all conditions of the an application pernut X yes 1
_
(including but not limited to items 1-3 below) issued by the Division of Water Resources: ❑ No P- If No, Explain in Narritive
17 AII-monitoring was done in actor ante witN-the permit and reported tor the year as required tlire-e-(3) copies of ee t fled laboratory results are attar e
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization__ was received from the Division of Water Resources.
3. No contraventionon o�ou�Water Quality Standards occurred at a monitoring well.
_
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for.. mitt' _informa ' cluding-the_nossibiliri of fines orisonment10.�"7'nEv'0r1101`s`
—false
—�,
SIF,mtu fpermittee Date S gnature_ofPr�e arer** Date
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) 1 (if different from Perminee)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
W 0002834
Laboratory:
1
Envionmental Testing Solutions
Facility Name:
Town of Burnsville
2)
Water Quality Labs
Residual Source WQ # or
NPDES #:
WWTP Name:
NCO020290
3)
4)
Town of Burnsville
5)
Residual Analysis Data
_
Ceiling
Cone. Limit
m /k a
Sample or Composite Date
Parame er
(mg/kg)
6/11/20
Percent Solids (°/n)
NA
24
Arsenic
75
<3.95
Cadmium
85
<1.58
Copper
4,300
292
Chromium
NA
NA
Lead
840
24.2
Mercury
57
1.6
Molybdenum
75
5.33
Nickel
420
31.2
e emum
100
<7.9
Zinc
7,500
933
Total Phosphorus
NA
16200
TKN
1370
34300
Ammonia -Nitrogen
8.7
5400
Nitrate and Nitrite
30
<30
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals InniLs.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, including the
possib' ' of fines and imprisonment for knnq ine violations."
Si Lure of Preparer * Date
*Prepareris defined in YjrYand 1 SA NCAC 3'f .I 10- (I - -- -- -- - -

_ ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0002834 Laboratory: 1) Environmental Testing Solutions
Facility Name:.
Town of Burnsville
2)
Water Quality Labs
Residual Source
NPDES # or WQ#:
NCO020290
3)
4)
WWTP Name:
Town of Burnsville
5)
Narameter
(mg/kg)
Sample or Composite Date
6/11/20
PH
7.7
PAN
5620
Potasium
4960
Magnesium
4400
Calcium
20700
SAR
2.49
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties r submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature f reparer Date
*Pmw" is defined in 40 CFR Part 503.9(r) and I5A NCAC 2T .1102 (26)

L-- J-
vle,e 5 Pile Number
TOWN OF BURNSVILLE
Date
Initials
Tempt
Temp 2
Temp 3
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Sampling Date
Number of Samples Taken
Sampling Depth
Page of

soya
Number'
TOWN OF BU RNSVI LLE
Date
Initials
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Temp 2
Temp 3
Temp 4
Temp 5
Temp 6
Temp 7
Temp S
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Sampling Date
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Number of Samples Taken Page of

WATER QUALITY LAB & OPERATIONS, INC.
P.O. BOX 1167
BANNER ELK, NC 28604
[phone]
CLIENT: TOWN OF BURNSVILLE LOGIN TIME:
ADDRESS: SAMPLER:
CITY: RECEIVED DATE:
STATE: NC REPORTED DATE:
ID#: NCO020290
JOSH CAGLE
11-Jun-20
19-Jun-20
ANALY$1
LSll] #
ANALYSIS
MQL'.s
:::UN I TS
METHOD
SAMPLE:.
ANALYSE
INT.
RESULTS.
.. .....
.
LOCATION
DATE: .
TOTAL SOLIDS
37.3
%
BURN.
SLUDGE FECAL
1
455.0
1.00
MPN/G
SM9221E2
#2
11-Jun-20
PIIWPS
TOTAL SOLIDS
36.9
%
BURN.
SLUDGE FECAL
2
388.0
1.00
MPNIG
SM9221E2
#2
11-Jun-20
PI/WPS
TOTAL SOLIDS
37.5
%
BURN.
SLUDGE FECAL
3
266.0
1.00
MPNIG
SM9221E2
#2
11-Jun-20
PI/WPS
TOTAL SOLIDS
36.6
%
BURN.
SLUDGE FECAL
4
123.0
1.00
MPNIG
SM9221E2
#2
11-Jun-20
PIIWPS
TOTAL SOLIDS
37.1
%
BURN.
SLUDGE FECAL
5
150.0
1.00
MPNIG
SM9221 E2
#2
11-Jun-20
PI/WPS
TOTAL SOLIDS
36.9
%
BURN.
SLUDGE FECAL
6
450.0
1.00
MPNIG
SM9221 E2
#2
11-Jun-20
PI/WPS
TOTAL SOLIDS
37.1
%
BURN.
SLUDGE FECAL
7
258.0
1.00
MPNIG
SM9221E2
#2
11-Jun-20
PI/WPS
REPORTED BY: NC CERTIFIED LAB # 544
PAUL ISENHOUR, SUPERVISOR

Environmental Testing Solutions, Inc. Certificate of Analysis
Project name: Water Quality Labs
Collection date: 1 I-Jun-20
Date received: 11-Jun-20
Sample identification: 2020 Compost Pile 1 - Grab
PO Box 7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
Project number: 2006I1.503
Sample number: 200350
Parameter Method Result RL Units Date Analyst Footnotes
Analyzed
Reactive Cyanide
335.4
0.177
mg/kg
29•Jun-2o
ECHEM
2
Reactive Sulfide
SM 4500 S D
9.15
mg/kg
23-Jun-2o
ECHEM
2
[gnitability
SW 846 1030
<0.8
0.8
Inm/sec
7-1u1-2o
ECHEM
2
Paint Filter
SW 846 9095 B
<0.1
0.1
ml
I?-lun-20
KEK
Arsenic - TCLP
6010 D
<0.25
0.25
mg/L
23-Jun-20
MLR
I
Barium - TCLP
6010 D
<2.50
2.50
rng/L
23-Jnn-20
MLR
1
Cadmium -TCLP
6010 D
<0.05
0.05
mg/L
23-Jun.20
MLR
1
Chromium - TCLP
6010 D
<0.10
0.10
mg/L
234m-20
MLR
I
Lead - TCLP
6010 D
<0.25
0.25
mg/L
23-Jun-2o
MLR
1
Selenium - TCLP
6010 D
<0.25
0.25
mg/L
23-Jun-20
MLR
I
Silver - TCLP
6010 D
<0.10
0.10
mg/L
23-Jnn-20
MLR
1
Mercury - TCLP
6010 D
<0.0020
0.0020
mg/L
23-Jnn-20
TLT
I
Full Scan TCLP Organics
See attached
sheets
L 2
Arsenic
6010 D
<3.95
3.95
mg/kg
30-1un.20
MLR
I
Cadmium
6010 D
<1.58
1.58
mg/kg
30-Jun.20
MLR
I
Copper
6010 D
292
7.90
mg/kg
26.1un-20
MLR
1
Lead
6010 D
24.2
3.95
mg/kg
30-Jun-2o
MLR
[
Molybdenum
6010 D
5.33
3.95
mg/kg
30-Jun-20
MLR
I
Nickel
6010 D
31.2
7.90
mg/kg
26-Jun-2o
MLR
I
Selenium
6010 D
<7.90
7.90
mg/kg
3o-Jun-2o
MLR
I
Aluminium
6010 D
19600
998
mg/kg
26-Jnn.20
MLR
I
Calcium
6010 D
20700
1980
mg/kg
26-Jnn-20
MLR
I
Magnesium
6010 D
4400
98.8
mg/kg
26-Jun-20
MLR
I
Potassium
6010 D
4960
39.5
mg/kg
26-Nlar-20
MLR
1
Sodium
6010 D
279
39.5
mg/kg
26-Jon-20
MLR
1
Zinc
6010 D
933
19.8
mg/kg
26-Jun-20
MLR
Mercury
7471 B
1.6
0.15
mg/kg
27-lun-20
TLT
1
Total Kjeldahl Nitrogen
351.2
34300
657
mg/kg
I8-Jun-2o
LKH
I
Nitrate + Nitrate
300.0
<30.0
30.0
mg/kg
I6-Jnn-20
ANB
I
Total Nitrogen
Calculation
34300
39.5
mg/kg
is-Jun-2a
ANB
I
Total Phosphorus
200.7
16200
198
mg/kg
26-Jun-20
MLR
1
Total Solids
SM2540 G
25.3
0.100
%
15-Jun-2o
JND
l
pH in SOIL
SW 8469045D
7.7
0A0
S.U.
Iwun-20
MS
3
% Total Solid
SM 2540 G
24
0.10
%
I I-Jun-2o
KEK
Ammonia Nitrogen
EPA 350.3
5400
83
mg/kg
I9aun-20
KEK
Plant Avaliable Nitrogen
CALC
5620
mg/kg
6.Ju1-2o
KEK
Sodium Absorption Ration
CALC
2.49
mg/kg
6-Ju1-2o
KEK
This report should not be reproduced, exept in its entirely, without the written consent of Environmental Testing Solutions, Inc.
The results in this report relate only to the samples submitted For analysis,

r
4
PO Box 7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
Environmental Testing Solutions, Inc.
Certificate of Analysis
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
t, Sample analyzed by Rogers & Callcott Environmental.
2. Sample analzyed by Bnviro Chemists, [nc.
3. Sample analzyed outside hold time.
Date reviewed: R-L94. 2"o NC Certification Number: 600
Data reviewed by: Kelley E. Keenan SC Certification Number: 99053
NC Drinking Water Certification Number: 37786
Signature: l,/L--
This report should not be reproduced, exept in its entirety, without the written consent or Environmental Testing 5alutiuns, Inc.
The results in this report relate only to the samples submitted for analysis.

:CaRcott
ENV IRONNENTAL a
�y 9nxS°'
Laboratory Report
Client Environmental Testing Solutions Project:
Kelley C, Keenan Work Order:
351 Depot St.
Asheville, NC 23801-43 t0 Received:
Dear Client:
HumsviIle WWTP
0060723
06/12/2020 13:42
Rogers and Calico([ appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of
custody for samples that were received on ]line 12, 2020. Rogers and Callcott maintains a formal QAlQC program. Unless otherwise noted, all analyses
performed under NELAP certification have complied with all the requirements for the TNI standard The analyses met the QA/QC confidence interval
for each test melhod unless otherwise qualified. Estimated uncertainty is available upon request.
Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee, lfyou are not the addressee, or
the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. If you receive this message by
mistake, please notify Rogers and Callcott immediately.
We strive to provide excellent service to our clients. Please contact Lauren Hollister, your Project Manager, at Ihollis1erC4_Prcenviro.com,
(864)-232.1556 if you have any questions about this report.
Report Approved By:
Lauren Hollister
Project Manager
This rePorl nruv nul 8e wp,»duced, creep, MAY, withour arlueu permission from Rogers A Culfco!!, hwc
PO Box 5655 Greenville, SC 2%06 426 Fan -forest Nay Greenville, SC 29607 main 864.232.1556 h. 7 66-4_232.6140 rogersandealleott.com
an emt>lav'-e-oa„nvd rorrthany

} Rogers &. Cak®tt
FNVIR0NVF F ,! TA. I_
Certificate of Analysis
QBoagtQ�
South Carolina Greenville Labor alary Identification 23105
South CalvUrta Columbia Laboratory lderrlificafion 40572
Na7B Carolina Lahorator11 Certification Number27
North Carolina Drinking 6lratar Lab Number 45710
NELAP Utah Certificate Number SC000042014-1
Georgia Drinking Mater Lob !D 880
Client Environntenial Testing Solulions Project: Burnsville WWTP
Kelley E. Keenan Work Order: 0060723
351 Depot St,
Received, 05/12/2020 13:42
Asheville, NC 28901 -}310
Sample Number Sample Description Matrix Sampled 'type
0060723-01 Burnsville WW-rP2020 Composite Pile l -Grab Solid 06/11/20 08:05 Grab
0060723-02 Burnsville WWTP 2020 Composite Pile I - Grab Solid 06/11/20 08:05 Grab
Pd Box 5655 Grey ovule, SC 29606 426 Fairforesr Way Greenville, SC 29607 n:a n 964.232.1556 far 864.232.6140 rogersaf dcallcott.com
an empioyov-n:vned Company
07/06/2020 10..24 This report pray not be reproduced, accept irr frill, wirlroar written per prission from Rogers & Ca11co11, hrc. Page P d f z9

Rogers .. Cakott
#_tv1ViRDNMENTAL
Environmental Testing Solutions
351 Depot Sr.
Asheville, NC 28801-4310
Case Narrative
Revised Report
Project: Burnsville WWTP
Work Order: 0060723
Reported: 07/06/20 10:24
Revised to update the project description to Burnsville WWTP. This report replaces the one generated on 711120 at 16:52.
PO Box 5655 Greenville, SC 29606 426 Fahiloresc Way Greenville, SC 29607 .mnr 864.232.1556 fax [phone]l40 rogersandeafleott.com
an company
07/0612020 14-24 This repor-r rrrur nor 8c mprodrtced, ercepf in full. u-ifhroeh written permission frvnr Rogers & Cahhcoff, Gte, page 3 of 29

Rogers & CaUcott
ENV IRON M ENTAL
Environmental Testing Solutions
Project:
Marion WWTP
351 Depot St.
Work Order:
0060723
Asheville, NC 28801-4310
Reported:
07/01/20 16,52
Sample Data
Sample Number 0060723-01
Sample Description Burnsville W WTP 2020 Cornposite
Pile I - Grab
collected
on 06/11/20
08:05
Parameter
Result
Reporting
Unit
Units
DF
Analyzers
Method
plug Analyst
[Batch
TCLP Metals
Mercury
ND
0.0020
mglL
10.0
06/23/20 13:32
EPA 7470A
TLT
B01`0970
Arsenic
ND
0.25
mg/L
5.00
06/23/20 18:27
EPA 6010D
MLR
BOF0963
Barium
ND
2.50
mh1L
5.00
06/23/20 18:27
EPA 601OD
MLR
BOF0963
Cadmium
ND
0.05
mg/L
5.00
06/23/20 18:27
EPA 601OD
MLR
BOF0963
Chromium
ND
0.10
mg/L
' 5.00
06/23/20 18:27
EPA 60M
MLR
BOF0963
Lead
ND
0.25
mafL
5.00
06/23/20 18:27
EPA 60101)
MLR
BOF0963
Selenium
ND
0.25
mg/L
5.00
06/2320 18:27
CPA 601OD
MLR
BOF0963
Silver
ND
0.10
mg/L
5.00
06/23/20 18:27
EPA 6010D
MLR
BOF0961
TCLP Volatile Organics
Benzene
ND
0.100
mg/L
50.0
06/26/20 19:40
EPA B260D
LDM
130G0007
243ulanone (MEK)
ND
0.200
mg/L
50.0
06/26/20 19:40
CPA 9260D
LDM
BOG0007
Carbon tetrachloride
ND
0.100
mg/L
50.0
06/26/20 19:40
EPA 8260D
LDM
BOG0007
Chlorobenzene
ND
0.100
mg/L
5RD
06/26/20 19:40
EPA 8260D
LDM
BOG0007
C1tlOroform
ND
0.100
mFIL
50.0
06/26/20 19:40
EPA a260D
LDM
BOG0007
1,2-Dichloroethane
ND
O.t00
mg/L
50.0
06/26/20 19:40
EPA 8260D
LDM
BOG0007
1,4-Dichlorobenzene
ND
0.100
mg/L
50.0
0626/20 19:40
EPA 8260D
LDM
BOG0007
I,1-Dichloroetherte
ND
0.100
mg/L
50.0
06/26/20 19:40
EPA 8260D
LDM
BOG0007
Tetrachtoroethene
ND
0.100
mglL
50.0
06/26/20 19:40
EPA 8260D
LDM
BOG0007
Trichloroethene
ND
0.100
mg/L
50.0
0626/20 19:40
EPA8160D
LDM
BOG0007
Vinyl chloride
ND
0.100
mg/L
50.0
06/26/20 19�40
EPA 8260D
LDM
BOG0007
Surrogates
°/REC
%REC Limits
pips
1, 2-Dlrhloroolhane-Dd
89
70-130
Toluene-D&
109
70-130
a-Brmrroflvoraben:ene
98
70-130
TCLP Semi -Volatile Organics
2-Methylphenol (a -Cresol)
ND
0.100
mg/L
10.0
06/26/20 17:22
EPA 6270E
R1NI
BOF1096
3/4-Methylphenol (m,p-Cresol)
ND
0.100
mVL
1H
06/26/20 17722
EPA 8270E
R!M
BOF1096
total Cresol
ND
0.200
mg/L
10.0
06/26/20 17:22
EPA 8370E
RJM
BOF1096
2,4-Dinitrotoluene
ND
0.100
mg/L
10.0
06/26/20 17:22
EPA 8270E
RIM
BOF1096
Hexachlorobenzene
ND
0,100
mpJL
10.0
06/26/20 IT22
EPA 8270E
RIM
80F1096
Hexachlorobutadiene
ND
0.100
mg/L
10.0
06/26/20 17:22
EPAa270E
RIM
BOF1096
Hexachloroethane
ND
0.100
mg/L
IOX
0W2620 17:22
EPA 8270E
RIM
BOF1096
Nitrobenzcnc
ND
0.100
rnWL
10.0
06/26/20 17:22
EPA 8270E
RJM
BOF1096
PO Box 5655 Greenville, SC 29606 426 Fail forest
Way
Greenville, 5C 29607
main 86-1.232.656
fa� 864
232.6140 rogersandcaIJCOtt.00171
an ��mplayea-otia•netl company
16: SI This report may our be
reproduced,
ercept in frill, willroul urilleu
par•raissior+�uno Rogers &
Callcoll. hoc.
p�vde .3 Ol Z8

Rogers &Callcot
ENVIRONMENTAL
Environmental Testing Solutions Project: Marion W WTP
351 Depot St. Work Order: 0060723
Asheville, NC 2 8801-43 10 Reported: 07/01/20 16:52
Sample Number 0060723.01
Sample Description Burnsville WWTP2020 Composite
Pile 1 -Grab collected
on 06/1
112009:05
Parameter
Result
Reporting
Lhuit
Units
DF
Analyzed
M1lclhvd
Flag
Analyst
Batch
TCLPSemi-Volatile Organics
Penlachlorophenol
ND
0.100
mg1L
10.0
06/26/20 17:22
EPA 8270E
RIM
BOF1096
Pyridine
ND
0.100
mg/L
10.0
06/26120 17:22
EPA 8270E
RIM
BOF[096
214,5-Trichloropheno[
ND
0.100
mg/L
10.0
06/26/20 17:22
EPA 8270E
RIM
BOF1096
2,4,6-Trichlorophenol
ND
0.100
mg/L
10.0
06/26/20 17:22
EPA 8270E
RIM
BOF1096
Surrngates
%REC
%REC Limits
Flag
Ninrobenzene-D5
33
15-3I4
3-Plrrorobiphenyt
35
32.118
2-1-71110raphcrroi
24
20-110
phenol-D5
24
8-424
?,4.6-71ribromaphenol
54
39-130
Tvphen.0-D14
65
26-173
TCLP Pesticides
Gamma-BHC (Lindane)
ND
0.00050
mg/L
10.0
06/25/20 13:47
EPA 8081 B
RKH
BOF1084
Chlordane
ND
0.0050
mg/L
10.0
06/25/20 13:47
EPA 8081B
RKH
BOF1084
Endrin
ND
0.00050
mg/L
10.0
06/25/20 13:47
EPA 8081B
RKH
BOF1084
Heptachlor
ND
0.00054
mg(L
10.0
06/25/20 13:47
EPA 8081B
RKH
BOF1084
Heptachlor epoxide
N❑
0.00050
mg/L
10.0
06/25/20 13:47
EPA 8081 B
RKH
BOF1084
Toxaphene
ND
0.0050
mg/L
10.0
06f25/20 13:47
EPA808113
RKH
BOF1084
Methoxychlor
ND
0.00050
mg)L
10.0
06/25/20 13:47
EPA 80818
RKH
BOF1084
Surrogates
%REC
%REC Limits
Flag
2.4,5.6-Teo•acidarvan-rylene
80
60130
Decachlombiphenpl
61
30-150
PO Box 5655 Greenville, SC 29606 426 Fairforesc Way Greenville, SC 29607 main 864.232.1556 tar. 864.232.6140 rogersandcallcott.eom
Wn errrp10yae-0,Ancr1 company
0710112020 16; j 7 This -Pad neap nol he reproduced, except infrrll, +vlll+out urerten permission fiam Rogea:r & Cullcorr, Hie.
Page 4 Of 28

fs Rogers & Cakott
ENV IRON I1ENTAL
E
nmental Testing Solutions Project: Marion WWTP
pot St. Work Order: 0060723
lle, NC 28801-4310 Reported: 07/01/20 16:52
Sample Number 0060723-02
Sample Description Burnsville W WTP 2020 Composite Pile 1 - Grab collected on 06/1 U20 08:05
Reporting
Parameter Result Unde Units DF Analyzed Method
General Chemistry Parameters
Nitrate as N
Nitrite as N
Total Kjeldahl Nitrogen
Total Nitrogen (TKN+Nitra(e+Nitrile)
Total Solids
Total Metals
Mercury
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
sodium
Total Phosphorus as P
Zinc
Flag Analyst Batch
ND
25.0
mg/kgdry
5.00
116/18/20 15:58
EPA9056A
ANB
601--0884
ND
5.00
mg/kgdry
5,00
06/18/20 15:53
EPA9056A
ANB
BOF0884
34300
657
mglkg dry
5.00
06/18/20 10:21
EPA351.2
LKH
BOF0783
34300
39.5
mg/kg dry
1.00
06/18/20 15:5a
ANB
BOF0782
25.3
0.100
%
[.00
06/15/20 13:29
Dry Wcight
JNI1
BOF0719
1.6
0.15
mglkg dry
2.00
06/27/20 18:19
EPA 7471 B
TLT
BOF 1171
19600
988
mg/kgdry
500
06/26/20 16:35
EPA 601OD
MLR
BOF1II1
ND
3.95
mg/kg dry
2.00
06/30/20 18:50
EPA 6010D
x
MLR
BOF I. l l l
ND
1.58
mg/kg dry
2.00
06/30/20 18:50
EPA 6010❑
R
MLR
BOF I I 11
20700
1980
mg/kg dry
500
06/26/20 16:35
EPA 6010D
MLR
BOF 1 111
292
7.90
mg/kgdry
10.0
06/26/20 17:33
EPA 60100
MLR
B0F1111
24.2
3,95
ing/kg dry
2.00
06/30/20 [8:50
EPA 601 OD
S 1
MLR
BOF111 I
440D
98.8
mglkgdry
50.0
06/26/20 17:21
EPA 60tOD
MLR
BOF II11
5.33
3.95
mg/kgdry
2.00
06/30/20 18:50
EPA6010D
MLR
13OF1111
31.2
7.90
mg/kg dry
10.0
06/26/20 17:33
EPA 6010❑
s I
MLR
130171111
4960
39.5
mg/kgdry
10.0
06/26/20 17:33
EPA 601OD
INILR
BOFIIII
ND
7.90
mg/kg dry
2,00
06/30/20 19:50
EPA 6010D
MLR
60F l l i t
279
39,5
mglkgdry
10.0
06/26/20 17:33
EPA6010D
MLR
BOFllll
16200
198
mg/kg dry
100
06/26/20 W47
EPA 60IOD
MLR
BOFI 111
933
19.8
mg/kg dry
10.0
06/26/20 17:33
EPA 6010D
MLR
BOF l i 11
PO Box 5655 Greenville, SC 29606 426 Faieforesc Way Greenvi0e, SC 29607 mom B64.232.15S6 hx 86+232.6i40 rogersandcallcott.com
- - an employee -owned company
0IM112020 16:52 This repot/ may rml be rilnvdifeed, evicepl in full, Wilho+rt n'riNen permission from Rogers & Callcou, Inc.
Page 5 of 28

} Rogers & Cakott
ENVIRONMENTAL
Environmental Testing Solutions
351 Depot St,
Asheville, NC 28801-4310
Parameter
Batch BOF0783 - EPA 351.2-TKN
Blank (130170783-81LKI)
Total Kieldahl Nitrogen
LCS (BOF(1783-BSI)
r I
Project: Marion W WTP
Work Order: 0060723
Reported: 07/01 /20 16:52
General Chemistry Parameters
Quality Control Summary
Reporting Spike Source %REC RFD
Result Limit Units Level Result %REC Limits RPD Limit Flags
ND 8.76 mg/kgwcr
010 K}eldalll Nrtrogcn 248 8.73 tttg/kg wct 262 95 0-200
Duplicate (BOF0783-DUP1) Source: 0960723-02
Total Kjcldahl Nitrogen 34500 620 mg/kg dry 34300
Matrix Spike (BOF0783-MS I) Source: 0060723-02
Total Kjcldahl Nitrogen 37900 654 mglkg dry 3930 34300 91 65-130
Reference (BOF0783-SRM 1)
Total Kieldahl Nitrogen
Batch BOF0884 - IC Soil
Blank (BOF0884-BLKI)
Nitric as N
Nitrite as N
Blank (BOF0884-BLK2)
Nitrate as N
Nitritc as N
LCS (13OF0884-BSI)
N"
1100 32.2 mg/kg wet 1100
NO 5.00 mglkg dry
NO 1.00 mglkg dry
ND 5.00 mglkg dry
NO 1.00 -EA-g dry
10D 572-155.3
tsrale as,,
ND
5.00
mg/kg dry
2.50
too 90-110
Nitrite as N
NO
1.00
mglkg dry
0.500
99 90-1 t0
Duplicate (BOF0884-DUPI)
Source: 0060723-02
Nitrate as N
ND
25.0
mglkg dry
NO
Nitrite as N
NO
5.00
mg/kg dry
NO
Matrix Spike (BOF0884-MS1)
Source: 0060723-02
Nitrate as N
80.5
5.00
mg/kg dry
74.3 NO
99 65-130
Nirritc as N
14.7
1.00
mglkg dry
14.9 NO
99 65-130
0-6 30
30
30
PO Rnx 5655 Greenville, SC 29606 426 fairforasc Way Greenville, SC 2960; mam 864.232.1556 i,v, 86°1.232.6140 1'OgersandcaIICOtt-COfil
an empla/ee-oMned company
0710112020 16:52 This repuri ixgr not he reproduced, ercvl in frdl, wilhout written permission finin Rogers & Cullcoll, fort.
Page 6 of 28

Rogers &Callcott
ENVIRONMENTAL
Environmental Testing Solutions
351 Depot St,
Asheville, NC 28801-43 t0
[Parameter
Batch BOF0884 - IC Sail
Reference (I30P0884-SRb11)
Nitrite as N
Reference (BOF'0884-RN12)
Nitrate as N
Project: Marion WWTP
Work Order: 0060723
Reported: 07/01 /20 16:52
General Chemistry Parameters
Quality Control Summary
Reporting Spike Source % REC RPM
Resull Limit Units Level Result %REC Limits Rfi) [,unit Flags
4.40 1.00 ntglkg dry 4.55
355 5.00 mg/kg dry 400
97 0-200
69 66.2-109-5
PO Box 5655 Greenville, SC 29606 426 Fairforest Way Greenville, SC 29607 main 864.232J356 !ai 864.232.6140 rogersandcallcott-COfll
an ernployee-owned [rxnpany
07/01IM20 16.52 This repa l ntvy iral be rtprodrrced, ercept in fir!!, wilhont wrirren permission finny Rogers & Callcotl, ine, — Of 28

borers & Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Marion WWTP
35l Depot St. Work Order: 0060723
Asheville, NC 28801-43 10 Reported: 07/0 [ 120 16:52
Total Metals
Quality Control Summary
Reporting
Spike
Source
%REC RI10
Parameter
Result
Limit
Units
Level
Result % REC
Limits RPD Limil Flags
Batch BOF1111 - EPA 3050B
Blank (BOFII I1-BLKI)
Aluminum
ND
p,05
mg/kg we[
Arsenic
ND
0.05
mg/kg wel
Cadmium
ND
0.02
ntglkg we[
Calcium
ND
0.10
mg/kg wcl
Capper
ND
0.02
mg/ku wet
Lend
ND
0.05
mg/kg wet
Magnesium
ND
0.05
mg/kg wet
Molybdenum
N❑
0.05
mg/kg wcr
Nickel
ND
0.02
mg/kg wet
Potassium
ND
0.10
mg/kg wet
Selenium
ND
0.05
mg/kg wc[
Sodium
ND
0.10
mg/kgwcr
Total Phosphorus as P
ND
0.05
mg/kg wet
Zinc
ND
0,05
mg/kg we
LCS (BOFllll-BSI)
Aluminum
OS 1
D.05
mg/kg wet
0.500
102
80420
Arsenic
0.50
0.05
mg/kg wet
0.500
100
80-120
Cadmium
0.50
0.02
mgikg %vat
D.500
101
80-120
Calcium
0.54
0.i0
mg/kgwct
0.500
107
80-120
Coppet
0.52
0.02
mg/kg wet
0.500
104
80-120
Lead
0.50
0.05
rngft wcr
0.500
100
80-120
Magnesium
0.52
0.05
mglkg wet
0.500
105
80-120
Molybdenum
0.51
0.05
mglkg wet
0.500
103
80-120
Nickel
0.31
0.02
mg/kgwel
0.500
102
80-120
Potassium
4.76
0.10
mg/kg wc[
5.00
95
80-120
Selenium
OA8
0.05
tnykg wet
0,500
97
80-120
Sodium
0.32
0.10
mflkgwet
0.500
[04
80-120
Total Phosphorus as P
0.50
0.05
mg/kg wet
0.500
100
80-120
Zinc
0.51
0.05
mg/kgwcr
0.500
103
80-120
LCS Dup (BOFIIII-BSDI)
Aluminum
052
0.05 mg/kg wcl
0.500
- 103 80-120
2 20
Arsenic
0 51
0.05 mg/kg wct
0.500
101 80-120
0.8 20
Cadmium
0.50
0.02 mg/kg war
0.500
100 80-120
0.9 20
Calcium
0.54
0.10 mgikg wet
0.500
109 80.120
1 20
PO Box 5655
Greenville, SC 29606 426 Fairforest Way
Greenville, SC 29607
nt a t 864,231.1556
f,x 864.232.6140
f ogerSandcalICOtt.com
. _
an eutltlay�P-otvrted Company
0710112020 16:52
This repor-t oray not be repinduced, evicep l in fill!. wifhoul wrirfen permission firm Rogers & Crdleoll, hrc.
Page 8 of 28

+� Rogers& Cakott
ENWRONMENTAL
Environmental Testing Solutions Project:
351 Depot St, Work Order:
Asheville, NC 28801-4310 Reported:
Total Metals
Quality Control Summary
Marion W WTP
0060723
07/01/20 M52
Reporting
Spike
Source
"/REC
RI'D
Parameter
Result
Limit
Units
Level
Result
%REC
Limits
RPD
Limit
p[ags
Batch BOFIIII - EPA 3050B
LCS Dup (110r• ] II I-BSDI)
Copper
0.52
0.02
mg/kg wet
0.500
105
80-120
0.3
20
Lead
0.49
0.05
mg/kg wet
0.500
98
80-120
2
20
Magnesium
0,52
0.05
mg/kg wet
0500
103
80-120
I
20
Molybdenum
0.51
0.05
mg/kg wet
0.500
103
80-120
0.2
20
Nickel
0.50
0.02
mglkg wet
0.500
101
80-120
0.8
20
Potassium
4.83
0.10
mg/kg wet
5.00
97
80-120
2
20
Selenium
0.49
0.05
mg/kg wet
0.500
97
80-t20
0.6
2e
Sodium
0.54
0.10
inglkgwet
01500
toa
80-120
3
20
'rotor Phosphorus us f'
0.49
0.05
mg/kg wet
0.300
99
80-120
0.7
20
Zinc
0.51
0.05
mg/kg wet
0.500
102
80-120
0.8
20
Matrix Spike (BOFIIII-MS I)
Source: 0060723-02
Aluminum
ND
1.97
mglkg dry
19.7
19600
NR
75-125
S3
Arsenic
20.1
3.95
mg/kg dry
19.7
ND
86
75-125
Cadmium
18.2
1.58
mg/kgdry
19.7
N❑
88
75-125
Calcium
ND
3.95
mglkg dry
19.7
20700
NR
75-125
S3
Copper
252
1.5a
mg/kg dry
19.7
292
NR
75-125
S3
Load
36.7
3.95
mplkgdry
19.7
24.2
63
75-125
SI
Magnesium
ND
1.97
mgikg dry
M7
4400
NR
75-125
$3
Molybdenum
213
3.95
mglkgdry
19.7
5.33
81
75-125
Nickel
40.9
i.58
mg/kg dry
19.7
31.2
49
75-125
sl
Potassium
4270
7,90
mg/kg dry
07
4960
NR
75.125
S3
Selenium
7-1.7
7.90
mglkg dry
19.7
ND
87
75-125
Sodium
271
7.90
ing/kg dry
19.7
279
NR
75-125
SS
'total Phosphorus as P
ND
1.97
mgft dry
19.7
16200
NR
75-125
S3
Zinc
ND
1.97
mgfkgdry
19.7
933
NR
75-[25
S3
Matrix Spike Dup (130FIIII-MSDI)
Source: 0060723-02
Aluminum
ND
1.97
mglkg dry
19.7
19600
NR
75-125
30 S3
Arsenic
19.6
M5
mglkg dry
M7
ND
83
75-125
3 30
Cadmium
17.6
1.58
mg/kg dry
19.7
NO
85
75-125
3 30
Calcium
ND
3.95
tng/kgdry
19.7
20700
NR
75-125
30 S3
Copper
313
1.59
mgtkg dry
19.7
292
107
75-125
22 30 S3
Lend
41.9
3.95
mglkg dry
t9.7
24.2
90
75-125
13 30
Magnesium
ND
1.97
mglkgdry
19.7
4400
NR
75-125
30 S3
Molybdenum
21.2
3.95
mglkg dry
19.7
5.33
80
75-125
0.04 30
PO Box 5655 Greenville, SC 29606
426 FIirforest Way
Greenville, SC 29607
ma!n 864.232.1556
far 86'L232.6140
rogersandcallcott,eom
an employee -awned Company
0710112020 16.52 This report rnuy not Le repr»duced, ercepr infrdl. m1rlr0ar u-rh7un permission front Rogerr & callmn. Inc. Page 9 Of 28

Rogers S: aRcott
ENVIRONMENTAL
Environmental Testing Solutions
351 Depot St.
Asheville, NC 28801-4310
Parameter
Batch BOFllll - EPA 3050B
Project: Marion W WTP
Work Order: 0060723
Reported: 07/01 /20 16:5 2
Total Metals
Quality Control Summary
Reporting Spike Source °/,REC RPD
Result Limit tlnlis Level Result %REC Limits RPD Limit Fhg,
Matrix Spike Dup (BUI111-NISD1)
Source: 0060723-02
Nickel
46.2
Pmnssium
ND
Scicnium
0.9
Sodium
296
Total Phosphorus as P
ND
Zinc
ND
Post Spike (BOFIIII-PSI)
Source:0060123-02
Arsenic
38.7
Cadmium
35.6
Lead
57.9
Molybdenum
41.1
Selenium
40.1
Post Spike (BOFIIII-PS3)
Source:0060723-02
Copper
499
Nickel
227
Potassium
7230
Sodium
486
Zinc
1t10
PostSplke (BOTIIII-PS5)
Source: 0060723-02
Magnesium
5340
Post Spike (BOF111 I-PS7)
Source:U060723-02
Total Phosphorus as P
17900
Post Spike (BOF'IIII-PSS)
Source: 0060723-02
Aluminum
29100
Calcium
39500
Reference (BOFIII I-SRM1)
Atuminum
11400
Arsenic
89.2
Cadmium
97.3
Calcium
5180
Copper
91 1
1.58
mg/kg dry
19.7
31.2
76
75.125 12
30
3.95
mglkgdry
197
4960
NR
75-125
30 S3
7-90
mg/kgdry
19.7
ND
78
75-125 8
30
7.90
mglkg dry
19.7
279
87
75-125 9
30
1,97
mg/k; dry
19,7
16200
NR
75-125
30 S3
1.97
mg/kg dry
19.7
933
NR
75-125
30 S3
7.90
mg/kg dry
39.5
ND
90
75-125
3.16
ingllcg dry
39.5
ND
88
75-125
7.90
mglkg dry
39.5
24.2
85
75-125
7.90
mglkg dry
39,5
5.33
91
75-125
15.8
mg/kg dry
39.5
ND
90
75-125
7-90
mglkg dry
198
292
i05
75-125
7.90
Mgt;-. dry
198
31,2
99
75-125
39.3
mg/kg dry
1980
4960
115
75-125
39.5
mg/kg dry
198
279
105
75-115
19.8
mg/kgdry
198
933
90
75.125
98.8
mglkgdry
988
4400
95
75.125
198
mg)kg dry
1980
16200
90
75-125
988
mglkg dry
9880
19600
95
75425
1980
mg/kg dry
9880
20700
89
75-125
248
mglkg wet
8490
134
30.41-149.59
4.95
mg/k8 wet
97.6
91
59.98-130.12
1.98
mglkg wet
114
85
75-125.4
495
mog wet
4730
110
72,52-t27.3
1 98
mglk 1
97 7
g we 93 75.03-124.9
PO Box 5655 Greenville, SC 29006 426 Fsil-torest Way Greenville, SC 29607 mam 864,232.1556 (ar. 864.232,6 mo rogersandeallcott.com
ail employee oE:neel rornlz rrly
0710112020 16:52 This 1eporl ittr1v riol be lT.producad e'rceIH tofu/, 11gIll0!/f " IIflen hPt'lnssionfb7r) Rogej-s & t_rlllcafl, lllr.
Page 1 D of 28

Rogers & Galleon
`emu EINVIRONi"IENTEIL
Environmental Testing Solutions Project: Marion W WTP
351 Depot St. Work Order: 0060723
Asheville, NC 28801-4310 Reported: 07/01/20 16:52
Total Metals
Quality Control Summary
Reporting
Spike
Source
%REC RPD
Parameter
Result
Limit
Units
Level
Result
% REC
Limits RPD Limit Flags
Batch BOF1111 - EPA 3050B
Reference(BOFII1I-SRMI)
Lcad
94.0
4.95
mglkgtvct
105
90
70.48-128.6
Magucsium
2730
248
mg/kg wet
2310
Its
61.9.138.1
Molybdcoum
72.3
4,95
mglkgwct
78.8
92
69.54-130.7
Nickel
106
1.98
mVkg wet
119
89
69.92-130.2
Potassium
2180
9,91
mgAgwei
2040
107
S&I12-140.7
Selenium
78.9
4.95
mgikg wet
93.1
85
64.55-135.3
Sodium
169
9.91
mg/kg wct
154
109
39.68-161
Zinc
195
4.95
mg/kg wet
212
92
69.81-129.7
Reterence (BOF1111-SRMZ)
Total Phosphorus as P
672
24.9
mg/kg wet
597
113
18.76.180.9
Batch BOF1171 - EPA 7471B
Blank (BOF1171-BLKI)
Mercury
ND
0.00020
my'kgwct
Blank (BOF1171-BLK2)
Mercury
ND
0.020
mgiku wet
LCS (BOF3171-BS 1)
Mercury
0.0048
0.00020
mglkgtvet
0.00500
96
80-120
LCS (H0Ft17l-BS2)
Mercury
0.54
0.019
mulkgwet
0.481
113
80-120
Matrix Spike (130F1171-MSI)
Source: 0060723-02
Mercury
6.2
0-15
mglkg dry
3.79
1.6
120
8o-120
Matrix Spikc Dup (60FI171-NISDI)
Source: 0060723,02
—
Mercury
6.8
0.16
mglkg dry
3.90
1,6
133
80-120 10 20 51
Post Spike (BOF1171-PSI)
Source:0060723-02
Mercury
6.5
uglL
4.00
2.1
109
80-120
PO Bay 5655 Greenville, SC 29606 426 FarrforesL Way Greenville. SC 29607 mau, 864.2323556 by 864,232.614o rogersandeallcott.com
an employer-ovloed Corr piny
0710112020 16:52 This reporl may not be mpinduced. accept urfrdl, mithorrt svriffen pernrissiwl fanr Rugers & Callcoll, Lre. Page f f of Z8

} ogees Cakott
FNVIRONrIENTAi_
Environmental Testing Solutions Project: Marion WWTP
351 Depot St. Work Order: 0060723
Asheville, NC 29801-4310 Reported: 07/01/20 16:52
TCLP Metals
Quality Control Summary
Reporting
Spike
Source
% REC RPD
Parameter
Result
Limit
Units
Level
Result / RFC
Limits RPD Limit Flags
Batch BOF0963 - EPA 3005A
Blank (BOF0963•BLKl)
Arsenic
ND
O.Oi
mg/L
Barium
ND
0.50
mg/L
Cadmium
ND
0.01
mg/L
Chromium
ND
0.02
mg1L
Lead
ND
R05
mg/L
Scicnium
ND
0.05
mg/L
Silver
ND
0.02
mglL
Blank (BUr0963-BLK2)
Arsenic
ND
0125
mg1L
Barium
ND
2.50
mg/L
Cadmium
ND
0.05
mg/L
Chromium
ND
0.10
mg/L
Lead
ND
0.25
mg1L
Selenium
ND
0.25
mg1L
Silver
ND
0.10
mg1L
LCS (BOF0963-BSI)
Arsenic
0,46
0.05
mg1L
0.500
92
80-120
Barium
0.53
0.50
mg1L
0.500
105
80-120
Cadmium
0.52
0.01
mg/L
0.500
104
80-120
Chromium
0.50
0.02
mg/L
U00
10o
80-120
Lcad
0.47
0.05
mg1L
0.500
94
so-12o
Selenium
0,47
0.05
mg/L
0500
94
80-120
Silver
0.52
0.02
mg/L
0.500
105
80-120
LCS (80F0963-BS2)
Arsenic
2.22
0.05
mg/L
2.50
89
SO-[20
Barium
2.51
0.50
mg1L
2.50
100
80-120
Cadmium
2.49
0.01
mp�L
2.50
99
80-120
Chromium
2.38
0.02
mg/L
2,50
95
80-120
Lead
215
0.05
mg/L
2.50
90
80420
Selenium
31'?3
0.05
mg/L
2.50
89
80-120
PO Box 5655 Greenville, SC 29606 426 FairForesr Way Greenville, 5C 29607 mom 864-?3?-f556 nx 864.232.6140 rogersandeallcott.eom
.. 7n eml�loyeH-owned rornpany
0710112020 16r51 This ivpm-f may not 6e reproduced, ercepl in full, Willow n-o-juen permission from Rogers $ Cullcoll, Inc. Page 13 of �8

Rogers & Cako t
ENVIRONMENTAL
Environmental Testing Solutions Project: Marion WWTP
351 Depot St. Work Order: 0060723
Asheville, NC 28801-4310 Reported: 07/01/20 16:52
TCLP Metals
Quality Control Summary
Parameter
Result
Reporting
Limit
Units
Spike
Level
Source
Result
% REC
°/REC
Limits
RPD
RPD
Limit Flags
Batch BOF0963 - EPA 3005A
LCS Dup (B0FD963-BSDI)
Arsenic
0.44
0.03
mg/L
0.500
89
80-120
4
200
Bartum
0.51
Ma
mg/L
11500
102
80-120
3
200
Cadmium
0.50
0.01
mg/L
0.500
Imo
80.120
3
200
Chrom1un
0.48
0.02
mg/L
0.500
97
80-120
3
200
Lead
0.45
0.05
mglL
0.500
90
80-120
3
200
Selenium
0.45
0.05
mg/L
0500
90
30.120
4
200
Silver
0.51
0,02
mr/L
0.500
101
80.120
3
200
LCS Dup (ROF0963-BSD2)
Arsenic
2.15
0.05
mg/L
2.50
86
80.120
3
MU
Barium
2.45
0.50
mg1L
2.50
98
80.120
3
200
Cadmium
2-39
0.01
mg/L
2.50
96
80-120
4
200
Chromium
1- 31
0.02
mg/L
2.50
93
80-120
3
200
Lcad
2.t9
0.05
mg/L
2,50
87
80420
3
200
selenium
1.16
0.05
mg/L
2.50
87
80-120
3
200
Matrix Spike (B0F0963-NISB)
Source: 0060723-01
Arsenic
2.31
0.25
mg/L
2.50
ND
93
75-125
Barium
3.43
2.50
mg/L
2.50
NO
103
75-125
Cadmium
2.54
0.05
mg/L
2.50
NO
102
75-125
Chromium
7-45
0.10
mg/L
2.50
NO
98
75-125
Lead
2.26
0.25
mg/L
2.50
ND
90
75-125
Selenium
2.29
0.25
mg/L
2.50
ND
91
75-125
Silver
255
0.10
mg/L
2.50
NO
t02
75-t25
Batch BOF0970 - EPA 7470A
Blank (BOF0970-BLKI)
-Mc`cury
ND
0.0002
mg/L
Blank (BOF0970-13LK2)
Mercury
NO
0.0020
mg/L
PO Box 5655 Greenville, SC 29606 426 Fiirforest Way Greenville. SC 29607 rw:n 864.232.556 tar 564.232.6140 rogersandcallcott.com
an ernployee-owned ramlriny
07101/2020 15:51 This report mn3, not be repmdnced, ercept in fdl. wilhoul writhe), perwission fiwn Rogers & Collcotl. Inc. PSge j Q- Qf Z8

Rogers Cakott
ENVIRONMENTAL
Environmental Testing Solutions
351 Depot St.
Asheville, NC 28801-4310
Parameter
Batch BO1+0970 - EPA 7470A
LCS (BOF0970-BSI)
Mercury
LCS (BOF0970-BS2)
Mercury
Matrix Spikc (BOF0970-NI56)
Mercury
Project: Marion WWTP
Work Order: 0060723
Reported: 07/01/20 16:52
TCLP Metals
Quality Control Summary
Reporting Spike Scarce %REC RPp
Result Limit Units Level Result %REC Llmits RPM Limit flags
(1.0051 M002 mg/L 0.00500 102 85-115
0.0518 0.0020 mg1L 0.0500 104 85-lt5
Source;0060723-0t
0,0500 010020 mg/L 0.0500 NI) I00 75-135
PO Box 5655 Greenville, SC 29606 426 Fairforest V1+,y G-eenvUI,!, SC 29607 m ;in 864.232.t556 h. $64.232.6mo rogersandcalICOtt.corn
an employee -owned company
0710112020 16-92 This report way nor be reprndueed. cacepl irr firfl, "Whouf'wifreu Permission fawn Rogers & Culleog. lne.
Page 15 of 28

yL Ei',IVIIROnlM FINITAL
Environmental Testing Solutions
351 Depot St.
Asheville, NC 28801-43 W
Parameter
Batch BOG0007 - EPA 5030
Blank (BOG0007-BLKI)
Project: Marion WWTP
Work Order: 0060723
Reported: 07 /01 /20 16: S 2
TCLP Volatile Organics
Quality Control Summary
Reporting Spike Source ! RLC RPD
Result Limit Units Level Result %RFC Limits MID Limit Flags
Bcnzcnc
ND
0-00200
mg/L
2-6utanonc (MEK)
ND
0.00400
mg/L
Carbon tetrachloride
ND
0.00200
mg/L
Chlorobcnzcnc
ND
0.00200
mglL.
Chloroform
ND
0.00200
mFJL
1,2-Diclilorocthanc
ND
0.00200
mg/L
l.4-Dicldorobcnzcnc
ND
0.00200
n,g1L
1,1-Dichloracthcnc
ND
0.00200
mg/L
Tonichlorocthcnc
ND
0100200
mg/L
Trichlorocthenc
ND
0.00200
mg/L
Vinyl chloride
ND
0.00200
mg/L
Snrrvgole: 1, 2-Dick loroellrwrc-D4
Surmgore. Tnlreerre-D8
Suwr vgare: 4-9ro nrofl rro r aL m ecxe
Blank (BUG0007-BLK2)
Bcnzcnc
ND
0-100
mg/L
2-Bumnanc (MEK)
ND
0.200
mg/L
Carbon Ictrachloride
ND
0.I00
mg/L
Chlorobcnzcnc
ND
0.100
mWL
Chloroform
ND
0.100
mg/L
1,2-Dichlorocthanc
ND
0.100
mg/L
!,4-Dichlorobcnzcnc
ND
0.100
mg/L
I,t-Dichloracthcnc
ND
0.100
mg1L
Tctmchloroethcnc
ND
0.100
inglL
Trichloroed,enc
ND
0.100
mg/L
Vinyl chloride
ND
0.100
mg/L
Senrvgure: 1.2-Dichfor a ellronc-D4
Sunvgore: Tolxmte-D8
Sxrevgure: 4-8r'oniti luarohen_ene
Blank (BOG0007-BLK3)
Bcnzcnc
ND
0.100
mg/L
2-Sutananc (MEK)
ND
0.200
mg/L
Carbon tetrachloride
ND
U.100
mg/L
Chlorobcnzcnc
ND
D.100
mg/L
93 70-130
121 70-130
107 70-130
96 70-130
123 70-130
101 70-130
PO Bax 5655 Greenville, SC 29606 426 Fairforesr Way Gr Renville, SG 29607 main 864.232.1556 far. 864.232.6i4c rogersandcallcott.Corrl
- - an4n"ployt'-e-ownedurmp,Iny
0710112020 16:53 This repnii cony not be reprvelocad. ercepl in fIII, ividroor nWillen permission fivnr Rogers & Colleolr, Grc.
Page 16 ofi 28

Rogers & CaUcott
ENVIRONMENTAL
Environmental Testing Solutions
351 Depot St.
Asheville, NC 28801-4310
i'a ra meter
Result
Batch BOG0007 - EPA 5030
Blank (BOG0007-BLK3)
Chloroform
ND
1,2-Dichlorocthanc
ND
1.4-Dichlorobcnzcoe
ND
1,1-Dichlaroctltcnc
ND
Tctrachlorouthcne
ND
Trichlorocthcnc
ND
Vinyl chloride
ND
Sio rogure:
1,2-Dlchlor0e1lrane-D4
Surmgale:
Tohrcae-63
Sunngnle:
4-Branrofl uar obenzure
LCS (BOG0007-13SI)
Benzene
0.0208
2-Butanone (MEK)
0,0223
Carbon tclrachloridc
0.0214
Chlorobenzcnc
0.0224
Chloroform
0.0211
1,2-Dichlorocthanc
0.0201
1,4-Dichlorobcrimne
0.0215
1,1-Dichloroethene
0.0248
Tctrachloroclhcnc
0.0215
Trichloroctltcnc
0,0243
Vinyl chloride
0.0196
Surrogare: 1, 2-Diddor'oellrune-D4
Sorrogule: Toluene-DS
Snnngule.' 4-Bnomofllw'oberrerre
Matrix Spike (BOG0007-MSI)
Source: 0060723-01
Bcnzanc
0.968
2-Burnnone (MEK)
1.03
Carbon tetrachloride
1.08
Chturobenzcnc
1.03
Chloroform
0,994
t2-Dichlorocthanc
0.928
1,4-Dichlarobenzcne
0.990
1,1-Dichlomcthcne
1.29
Project: Marion W WTP
Work Order; 0060723
Reported: 07/01 /20 16:52
TCLP Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Limit Units Level Result % REC Limits RP'D Limit Flags
D.100
mg1L
0.100
mg/L
D.100
mg/L
0.100
mg/L
0.100
mg/L
0.100
mglL
0.100
mq/L
97
76-130
119
70-130
111
70-130
0.00200
mg/L
0.0200
104
70-130
0,00400
mg/L
0.0200
III
60-140
0.00200
mg/L
0.020D
107
70-130
0.00200
mglL
0.02o0
112
70-130
0,002oo
mg/L
0.0200
105
70.130
0.00200
mg/L
0.0200
100
70-130
0.00200
mg/L
010200
108
70.130
0.00200
mg/L
0,0200
124
70-130
D,00200
mg/L
0.0200
108
70.110
0.90200
m6/L
0.0200
122
70-130
0.00200
mg/L
0.D200
98
60.[40
102
70-130
109
70-130
103
70-130
0.100
mg/L
1.D0
ND
97
70-130
0.200
mglL
1.00
ND
03
60.140
11100
mg/L
1.00
ND
log
70-130
0.100
mg/L
t.00
ND
1D3
70-130
0.100
mg/L
1.00
ND
99
70-130
0.100
mg/L
1.00
ND
93
70-130
0](10
mg/L
L00
ND
99
70-130
0.100
mg/L
1.00
ND
129
70-130
PO Box 5655 Greenville, SC 29606 426 hirfares Way G'e--i)AIe. SC 29b07 main 864.232.1556 Erv. 864.232.6140 rogersandcallcott.com
r711 employee -owned company
0710112020 16.52 This reporrmay no! be reprndacM. erccp1 in fill. wlrhout mrilten permission fronr Rogers & Callcoll, Inc.
Page i 7 al 28

Rogers &Cakott
ENVIRONMENTAL
Environmental Testing Solutions
351 Depot St.
Asheville, NC 28801-4310
Parameter
Result
Batch BOG0007 - EPA 5030
Alatris Spike (BOG0007-MS1) Source: 0060723-0I
Telrach€orcethcnc
1.03
Trichlorocthene
I. t 3
Vinyl chloride
D,860
swogule: 1, 2-Dichloroeth,va-D4
Sift-mgale, Toluene-08
Surrogate; 4-111nmof trolubonrene
Matrix Spike Dup (BOG00074vISD1) Source: 0060723-01
Benzene
0.903
2-autanunc (MEK)
1.96
Carbon tclrachloridc
1.03
Chlarobcnzenc
0.978
Chloroform
0 936
1,2-Dichlorocthanc
0.874
t,4-Dichlorobcnzcnc
0.954
1,I-Dichloracthcnc
l 23
Totmchloroclhcne
0.983
Trichloroclitenc
1.08
Vinyl chloride
0.966
Sravnga re: 1.2-Dichlarnelhaim-D4
Srn"'ogafe: Toluene-D8
Surrogate: 4-Bturnofluorn benzene
Project: Marion WWTP
Work Order: 0060723
Reported: 07/01 /20 16:52
TCLP Volatile Organics
Quality Control Summary
Reporting Spike Source %REC ItI'D
Limit Units Level Result %REC Limits RPD Lhnil Flags
0.100
mg/L
i.0o
ND
103
70-130
0.100
mg/1,
1.00
ND
113
70-130
0.€130
mg/L
L00
ND
96
60-149
96
70-130
99
70-130
93
70-130
0.100
mg/L
LOU
ND
90
70-130
7
20
0100
mg/L
1.00
ND
106
60-140
3
20
0.100
mg/L
1.00
ND
103
70-130
5
20
0.100
mg/L
1,00
ND
98
70-130
5
20
0.100
mg1L
1.00
ND
94
70-130
6
20
0.100
mg/L
1.00
ND
87
70-130
6
20
0.100
mg/L
1.00
N ❑
95
70-130
4
20
0.100
mg/L
1.00
ND
123
70-130
5
20
0.100
mg/L
L00
ND
98
70-130
4
20
0.100
mg/L
1.00
ND
€08
70-130
4
20
0.100
mg/L
I.00
ND
87
60-[40
0.8
20
90
70-I30
95
70-)30
89
70-130
PO Box 5655 Greenville, SC 29606 426 Fairoresc Way GreLnVI(I®, SC 29607 main 864,232.656 fax 664.232.614o rogerSandcalleott.Com
an ernployev-owned company
0710112020 16: 52 This rmpoir nroy trot he rLppuduced, excepl in fall, without wriumi pernussion fine+ Rogers & Callcolr, Inc.
Page 18 of 28

Rogers & Galleon
Er1MOlvMEN r,aL
Environmental Testing Solutions
351 Depot St,
Asheville, NC 28801-4310
Parameter
Batch BOF1096 - EPA 3510C - GCMS
Blank(BOF1096-BLKl)
2-Mcthytphcnol (o-Cresol)
3/4-Mc1hylphcnol (m,)-Cresol)
total Cresol
2,4-Dinitrololuenc
Hcxachlombenzmc
Hcxachlorobuladienc
Hexachlarocthanc
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlwophona I
2.4,6-Trichlomphcno I
Blank (BOF1096-BLK2)
2-Mclttylphenal (o-Cresol)
3/4-htclhylphcnol(m,p-Cresol)
total Cresol
2,4-13initrotolucnc
Hexachlorobenzcnc
Hexachlorobutadicoc
Hcxachloracthanc
Nitrobenzene
Pentachloraphenol
Pyridine
2,4,5-Tric hlorophcnol
2A.6-Trichtoraphcnol
Project: Marion WWTP
Work Order: 0060723
Reported: 07/01/20 16:52
TCLP Semi -Volatile Organics
Quality Control Summary
Reporting Spike Source % REC RPt)
Result Limit Units Level Result %REC Limits RPD limit Fines
ND
ND
ND
N❑
ND
ND
ND
ND
ND
ND
ND
ND
Sunagale: Niwobe n-crrc-D5
Sm'ingate- 2-Fluoiobiphenyl
Srx ragrrle: 2-Fliraropher101
Sarrngale: Pbenal-D5
Sm i ngam: 2.4.6-Tribromophenol
Surmgale: Terphenyt-D14
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Strrmgale: Nihrrbenzene-D5
Sarvagare: 2-Fhrarobiphenyl
Sun rogule: 2-Fluompheno l
Sm,mgale: Phenol-05
0.0100
0.0 Wo
0.0200
0,0100
0.0100
0.0100
0.0100
0.9100
0.0100
0.0100
0.0100
0.0100
0.100
0.100
0.200
0.100
0.1110
0.100
0.100
0.100
O.t00
0.1110
0.100
0.I00
mg/L
mg/L
nrg/L
mg/L
mg1L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
rng/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg1L
mg/L
mg/L
mg/L
mg/L
mg/L
47
44
49
46
62
84
50
51
53
49
15-314
3 2-118
20-110
8-424
39-130
26-173
15-314
32-118
20-110
8-424
PO Box 5655 GrcanAiIL, SC 29606 426 F.fl aresc Way Greenvitle, SC 29607 mom 664,232.1556 nx 864.232.6140 rogersandcallcOtt.Com
an employee -owned company
07/O!/21120 16.'S2 This r�epw'l map nol be ruprodrrced, ercep! iu fidl, rvifhou! rvriNcu pernnrsion jmm Rogers cf Cullcarl, Inc.
Page 19 of 2$

o urs & Cakott
ENV IRONMENTAi-
Environmental Testing Solutions Project: Marion W WTP
351 Depot St. Work Order: 0060723
Asheville, NC 23801-4310 Reported: 07/01/20 16,52
TCLP Semi -Volatile Organics
Quality Control Summary
Reporting Spike Source %Mc tips]
['a ramrtcr Result Limit Units Level Result %RCC Limits RPD I,in€it Flag5
Batch BOF1096 - EPA 3510C - GCMS
Blank (B0F1096-BLK2)
Surrogate: 2,4,6-Tribranurpkenal 72 39-130
Stu-rogule: Terphenrl-D14 146 26-173
LCS (BOF1096-BSI)
2-Mcthylphenal (a -Cresol)
3/4-Mc1hylphcnol (m,p-Cresol)
2,4-Dinkmolucnc
Hexachlorohcnzcne
Hcxachlorohutadicnc
HOUClllarac[hane
Pcnlachlo raphena I
Pyridine
2,4.5-Tric13lorophenaI
2,4,6-Trichloropincnol
LCS (BBF1096-BS2)
Nitrohanzcnc
Matrix Spike (BOF1096-MS3)
2-F4tcthy1phcn0l (a -Cresol)
3/4-Mcthylphcnol (m,p-Cresol)
2,4-Dinilrotolucnc
Hcxachlorohcnzcnc
Hcxachlorabutadicnc
Flexachlomcthanc
0520
p,I00
mg/L
0.800
65
40-1[0
1.07
0,100
mg/L
1.60
67
40-110
0.529
0.100
mg/L
0.800
66
52.110
0 616
0,100
ra /L
0.800
77
52-121
D.262
0.100
mg/L
0.800
33
30-110
0.213
0.100
mglL
0.800
27
24-110
0,688
0.100
mg1L
0.800
86
43-125
0.339
0.100
mg/L
0.900
42
24-110
0.688
01100
mg/L
0.800
86
53-115
0.743
0.100
nlg/L
0.800
93
53-110
Srrrrugare: htitlobeu7ane-D5
30
15-314
Sunngole:?-Flntorobipben),i
36
32-118
Srrrmgale:2-Fhrnrnphenol
54
20-111)
Snringale: phenol-DS
53
8-424
Sor-rogote: 2,4,64-ribrnorophenot
79
39-130
Strrrvgare: Terphan)I-DN
lot
26-173
0.456
0.1011
mg/L
0.800
57
36-110
Snnungale: Ninnbenrerre-DS
52
)5-314
Surrngule:2-Flnmobiplrenpl
53
32-118
Surragale:2-Fluomphelrul
53
20-110
Surrogale: phenol-DS
52
8 4>4
Surmgare'2.4,6-Tribrom,phen°t
87
39-130
Snrrogurq: Terplrenyl-D14
115
26-173
Source; 0060723-91
0.242
0.100
mg/L
0.900
ND
30
30- [10
0.480
0.100
mg/L
L60
ND
30
26-I [0
0.412
0.I00
mg/L
0.800
ND
51
43-110
0,404
0.100
mg/L
0.800
ND
51
45-120
0,313
0,10o
mg/L
01800
ND
39
12-110
0.212
0.1DO
mglL
0.800
ND
26
15-110
PO Box 5655 Greenville, SC 29606 426 Fah -forest Way Greenville, SC 29607 n,a€n 864.232.IS56 tax B64.233.61•40 rogersandcallcott.Com
,an �mhlciyee o4mr'd carnpany
0710IJ2020 16-12 This report ilia)+aol be reproduced. except in fill!, without written perrrrissimr friar Rogers & Curicoll, htc.
Page 24 of 28

Rogers &Callcott
ENVIRONMENTAL
Environmental Testing Solutions
351 Depot St.
Asheville, NC 28801-4310
Parameter
Batch BOIL 1096 - EPA 3510C - GCMS
Project: Marion WWTP
Work Order: 0060723
Reported: 07/01 /20 l 6:52
TCLP Senii-Vola tile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Rugs
Matrix Spike (QOFt096-MS3)
Source: 0060723-01
Nitrobenzcac
0,278
0.100
mglL
0.800
ND
35
25-112
Pcntachlorophcnol
0.489
0.100
mg1L
01800
ND
61
30-140
Pyridine
0253
0.100
mg1L
0.800
ND
32
17-1t0
2,4,5-Trichlaraphenol
D.422
0.100
mg1L
0-800
ND
53
46-125
2,4,6-Trichlorophcnol
0.430
0.100
mg/L
0.800
ND
54
43-120
Surrngrrre: Nilrobeuzeue-W
34
15-314
Sur wgale, ?-Flumvbiphe» yl
37
32.118
Surrogate:2-Fhroropherrol
28
20-110
Surrogate.- Phercol-Di
28
8-424
Surrogate:2.3,6-Tribronropheunl
48
39-130
Surrogate.' 7erphem•1-D14
78
26-173
Po Box 5655 Greenville, SC 29606 426 Fiirforest Way Greenville, SC 29607 main 864.232.1556 F,a 864.732.6140 rogersandeallcott.com
- -- an rmi}}oyFe-oavned company
0710112020 16:52 This report may nor be rrpmduced, ercepl in fill. rvithoat wri7ten perxrissiou f+om Rogers & Cuticoll, bre,
Page 21 of 28

K®gers & Cakott
ENVIRONMENTAL
Environmenta[ Testing Solutions Project: Marion WWTP
351 Depot St. Work Order: 0060723
Asheville, NC 28 801-43 10 Reported: 07/01/20 16:52
TCLP Pesticides
Quality Control Summary
Reporting
Spike Source %REC RVD
Parameter Result
Limit
Units
Level Result %REC Limits RPD Limit Flags
Batch BOF1084 _ EPA 3510C - GC
Blank (BOFI084-BLKI)
Gamma-BHC fUndanc) NO
a.a000sa
mg/L
Chtordane N❑
0.0005o
mg/L
Endrin ND
0.000050
mg/L
Heptachlor ND
0.000fl50
mg/L
fieptachlorcpoxidc ND
0-000050
mg/L
Toxaplimc ND
0.00050
mg/L
Mcthoxychlor ND
0.000050
mg/L
Sunvgule:
83 69-130
Sru-rngalc: Decr+chlmvbiphen3d
43 30-150
Blank (R0F1084-BLK2)
Gamma-BHC(Lindanc)
ND
0.00050
mg/L
Chlurdanc
NO
U030
mg/L
Endrin
ND
0.00050
mg/L
Heptachlor
ND
0.00050
mg/L
Hcptachlarcpoxidc
HD
0.00050
mg/L
Toxaplieno
ND
0.0050
mg/L
ivlethoxychlor
NO
0.00050
mg/L
Surrogater2.4,5,6-Teouchlan-nr-rvlenc
82 60-130
Surrogate: Decachlorobiphenyl
85 317•150
LCS (BOF1084-BSI)
Gamma-DHC(Lindanc)
06034
0.00050
mg/L
0,00400
85
70-130
Endrin
0.0035
0.00050
mg/L
0.00400
87
70-130
Heptachlor
0.0033
00050
mg/L
0.00400
82
70-130
Hcpmchtorcpoxidc
U034
0,00050
mg/L
0.00400
85
70-130
Mchoxychlor
0.0034
0.001150
mg/L
0.00400
84
70-130
Surroguta:2,4,5.6-TeoacGlau-tn-.rylmre
85
60-130
Strrrngare; Decuehlarobiphenvl
89
30-150
Matrix Spike (BOF1084-MSI)
Source: 0060723-01
Gamma-BNC (Lindanc)
0.0032
0.00050
mglL
0.00400
NO
81
60-140
Endrin
0,0034
0.00050
mg/L
0.00401)
NO
84
60� 140
i-lcptachlor
0.0033
0.00050
mE/L
01)0400
ND
84
60-140
Hcptachlorcpoxidc
0.0032
0.00050
mg/L
0.00400
ND
so
60-140
Mcthoxychlor
0.0029
0.00050
mg1L
0.00400
ND
71
60-140
PO Box 5655 Greenville, SC 29606 426 hirloresr Way Greenville, SC 29607 ,r,au, 864,232.1556 hr. 86-4.73?.61,40 rogersandcalleott.com
- an emhloyse-awned company
0710112020 I6r52 This report mqv nor be repradueed, except in fill, ,villralrl wrirren permission front Rogers do Collcort, hic, �D 2S

Rogers &Cakott
ENV IRQN41IENTAL
Environmental Testing Solutions
351 Depot St.
Asheville, NC 28801-4310
Parameter
Project:
Work Order:
Reported:
TCLP Pesticides
Quality Control Summary
Reporting Spike Source
Result Limit Units Leyel Result
Batch BOF1084 - EPA 3510C - GC
Matrix Spike (li0f 1084-MS1) Source: 0060723-01
Marion WWTP
0060723
07/01/20 16:52
%REC RFD
%REC Limits RPD Limil hlags
Surrvgale: ?,d,5,6-Te/nncliiarn-ni ayienr
82
60-130
Surrvgale: Decachfombiphenyl
55
30-150
Matrix Spike Dup (BO PI 084-MSD
1) Source: 0060723-01
Gamma-1314C (Lindane)
0.003t
0.00050
mgIL
0.00400
ND
78
60-140
4
20
End6n
0.0034
0.00050
mgiL
D.00400
ND
84
60-140
D,6
20
Heptachlor
0,0034
D-00050
mg1L
0.00400
ND
84
60-140
0.6
20
Heptachlorcpoxide
0.003$
0.00050
mg1L
0.00400
ND
So
60-140
0.2
20
Mcthoxychlor
0.0027
0.00050
mpfL
0.00400
ND
67
60-140
6
20
Sr u•� vgure: 3. J.S, 6-Telrochlora-nr-.iylene
SfIrmgam: Decpdiloroblplrenyl
79 60-130
S9 30450
PO Box 5655 Greenville, SC 29606 426 Fairlorest Way Greenville, SC 29607 mam 864.232.1556 fay. 864.232.6l4c rogersandcallcott.com
- an ontpinyee-owned cnmp,, ny
0710112020 16:57 This report stay not be reprvdneed, eveepr ilr frill, "Whour n•rrllen permission f-onr Rogers & Callcorl, Inc. Page 23 of 28

-1; o ers & Cak®tt
ENVIRONMENTAL
Environmental Testing Solutions
351 Depot St,
Asheville, NC 28801-4310
Parameter
Batch BOF0918 - EPA 1311
Blank (130170918-BLKI)
TCLP Bottle Extraclion
Project: Marion WWTP
Work Order: 0060723
Reported: 07/01 /20 16:52
TCL V Bottle Extraction
Quality Control Summary
Reporling Spike Source %REC
Result Limit Units Level Result % REC Limits RPD
Complete
RPM
Limit Flags
PO Box 5655 Greenville, SC 29606 426 Fail -forest Way Greenville, 5C 2%07 roam 864,23?,i556 fa:: 864.237.6140 rogersandcalleott.com
-- - anamPlapee-ovrnerirornhaoy
0710112020 16:53 This repurl may not be reprodneed. c vvcpl in firll, wifhou! rw'itfurr permission finny Rogers & Caticolt, 1rre.
Page 24 0f 28

Rogers &CaRcott
ENVIRONMENTAL
Environmental Testing Solutions
351 Depot St.
Asheville, NC 28 801-43 10
Parameter
Batch BOF0894 - EPA 1311- ZHE
Blank (BOF0894-BLKI)
TCLPZI-IE Extraction
Project: Marion WWTP
Work Order: 0060723
Reported: 07/01 /20 16:52
TCLP ZHE Extraction
Quality Control Summary
Reporting Spike source %REC RPD
Result Limit Units Level Result % REC Limits RPD Limit Flags
Complete
Sample Preparation Data
Parameter
Batch
Sample ID
Prepared
Analyst
EPA 3005A ICP Digestion
EPA 3005A
BOF0963
0060723-01
06/22/2020 12:09
T€3H
EPA 3050E Metal Digestion
EPA3050B
BUI111
0060723-02
06/24/2020 08:20
MLR
EPA3510 Extraction
EPA351OC-GC
BOF1084
0060723-01
06/24/2020 08:15
DBB
EPA 3510 Extraction
CPA 351 OC - GCMS
BOF 1096
0060723-01
06/24/2020 10:30
DB 3
EPA 7470A Mercury Digestion
EPA 7470A
BOF0970
0060723-01
06/22/2020 13:56
TLT
EPA 74710 Mercury Digestion
EPA 7471E
B0F1171
0060723-02
06/26/2020 09:20
TLT
TCLP Extraction Data
Parameter
Extraction Initial
Batch Sample ID Started Finished Fluid # pH
Fina[
PEI
EPA 1311 - TCLP Extraction
CPA 1311
BOF0918 0060723-Oi 6/18/2020 at 1610 6/19/2020 at 1140 1 7.80
5, 11
EPA 1311- TCLP ZHE
CPA 1111 • ZHC
BOF0894 0060723-01 6117120 at [620 6118l20 at 0900 1 NIA
NIA
PO Bax 5655 Greenville, SC 29606 426 Fairforest VVay Greenville, SC 29607 main 864?32.1556 fix 864.232.6140 rogersandcalleott.com
All emhlum.-ovmed company
0711)112020 16:52 This rrport may not be reproduced, weep, in firll. ivithaul pa'irlen prrmis3ion fiom Rager3 & Callcort. arc. page 25 of 28

Rogers &, Callcott
ENVIRONMENTAL
Environmental Testing Solutions
351 Depot St,
Asheville, NC 28801-4310
Project:
Work Order:
Reported:
Data Qualifiers and Definitions
Marion W WTP
0060723
07/01/20 16:52
ND Analyze NOT DETECTED at or above the reporting limit
NR Not reported
RPD Relative percent Difference
s l The matrix spike and / or the matrix spike duplicate sample recovery was not within control limits due to matrix interfcrcucc. The
Laboratory Control Sample (LCS) was within control limits.
S3 Estimated value - the spike result cxceedcd the calibration range. The spike recovery was not evaluated against the control limits.
S5 The raw sample concentration was greater than four times the spike concentration. The spike recovery was not evaluated against the
control limits.
X Result subject to sample matrix interference. Reporting limit has been adjusted where applicable.
PO BON 5655 Greenville, SC 29606 426 nirfaresc Way Greenville, SC 29607 main 854.232.155E f,x 864.2.32 r 140 rogersandcalleott.com
an company
07101120247 16:52 This repol'I mqv not be lepiuduced, arcept trl llll, Ivllhow %wilt p permission from Rogers & Cullewt, Me. Page 26 of 28

Rogers & Cakott CHAIN OF CUSTODY RECORD
ENVIRONMENTAL
Mailing PO Box 5655 Shipping 426 Fairforest Way 215E Stoneridge Drive
Address: Greenvilie,5C296o6 Address: Greenville,5C291507 Cofum6ia,SC29210
Phone [phone] Fax [phone] Phone [phone]
Client Name
Address
y
ti
Report To:
.
Email Address
a
o
Telephone #
PO#
Project it
I;
zE,r--
B
R&C YR�
WORK ORDER DATE TIME
SAMPLE DESCRIPTION
o
a
TOt -oZ R;b S
b osF�,
OALER LINQUISHED BY: DATE/TIME: RECEIVED By:
f%1D BY: DATE/TIME. RECEID BY: 4. DATEMME: RECEIVED .D BY: 6
7 0ATEJTIME: RECE(VED BY:
8.
Passible Hazards associated with samples: Nan -Hazard OFIammable f-15kin Irritant r
unknown EDmher
4
DATE/TIME:
Ln(ell".
DATE/TIME.- illi/
DA7V
DATE/TIME-
WORK ORDER
Filtered (yes/N6-1
Container Type LlastifrGlass)
Container Volume (mQ
Sample Type (Grab omposlte)
Sample Source (WW, GW, DW, SW S, ther
Preservation Code(s)
A —None E—HC( I—ZnAcetate
B—HNOi F-•Na252o,3 J—H3P0,
C--142504 G—Boric Acid K-MCAA
D—NaOH H—AsmrblCAcid L-
COMMENTS
V f)b
Composite Start Date:
Composite Start Time:
Time or Flow (Circle one) Initials:
Temperature of blank or representative sample
At time of collection C
At time of lab receipt •C
Form Revised July, 2014 Page of
Pag2 27 of 28

Rogers, & Cattcott
ENVIRONMENTAL
Sample Receipt Verification
Date Work
Client: -is Received: SD 2.Zf) Order: OOLDPZZ
Carrier Name: Client edEx UPS US Mail Courier Field Services Other:
Tracking Number. Auu 3q i ! 35-32
Receipt Criteria
Y
N
Jo
N
Comments
A
Shipping container 1 cooler Intact?
Damaged Leaking Other:
Custody seals intact?
COC included with samples?
COC signed when relinquished and received?
X
Sample bottles intact?
Damaged Leaking Other:
Sample ID on COC agree with label on bottic(s)?
e on COC agree with label on bottle(s)?
FNumberf bottles on COC agrees with number of bottles received?eceived
within holding time?
Sample volume sufficient for analysis?
VOA vials free of headspace (<6mm bubble)?
t
Temp at receipt recorded on COC
Samples cooled?
Temp measured with IR thermometer- Sint: 97050067
x
Ice Cold Packs Dry Ice None
Samples requiring pH preservation at proper pH?
Nate; Samples for metals analysis may be preserved upon receipt in the lab.
�(
Note: Samples for O&G and VOA analysis — preservation checked at bench.
/1
Samples dechlorinated for parameters requiring chlorine removal at
the time of sample collection?
Note: Chlorine
�[
l�
checked at bench for samples requiring Bacteria!, VOA, and HAA
analysis,
If in-house preservation used — record Lot P
HCL H3PO4
H2SO4 NaOH
HNO3 Other
Comments: wG e -� V.o"c
Were non-conformance issues noted at samplceipt? Yes r No
samplereceipt?
Non -Conformance issue other than noted above:
Revised Febnmry2010 Completed by; ( QAJ
Page 28 of 28

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I OMA, _vlalltvo, NC 27 u51 9_j?_ �'73,5%4)2 Lclb%}'aY
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�55-A'VklFI-11ilt"Lill Ili I'll 4:'a_y. J7llak-St1jj-,4li@, NC 28710
ANALYTICAL N. GONS{)i_i )NIG CH_IJ4STS
rit10+t1.zMlvi l-e,lli!1 iGI1LEtl,::lt` Ill!SI�.C_itl
Environmental Testing Soll;tiorts,
inc. Date of Report: Jul 07, 2020
Post Office Box 7565
Customer PO #:
Asheville NC 28802
Customer ID: 08400055
Attention. Kelley Keenan (ETS)
Report #: 2020-09938
Project ID: Burnsville WWTP
Lab ID Sample ID
Collect I]atelTime'.,ra,z,.,�.��__ ��.�.....�.�..�...��,.�...w.�....�,.�.,.__,.._
Matrix Sampled by
20-24835 Site; Sludge
6/11/2020 8:05 AM Solid/Sludge C4ant
Test
_Method Results Date Analyzed
2,4,5-TP (TCLP)
SW846 Method 5151A <0 003 mg/L
06/24/2020
2,4-D (TCLP)
SW846 Method 5151A <0.003 mg/L
06/24/2020
RCI
Ignitability
EPA 1030 <0.8 mm/sec
07/07/2020
Cyanide
EPA 335.4 O. i 77 mg/kq
06/2912020
Sulfide
s1 4500 s o 9.15 mg/kg
06/23/2020
Cornm e n t:
f�
Reviewer! by:
ReportR- 2020.09936
r,a.,,,.. ....tip,., ........,..,...V-...:.......,_.o..-_,._.........�....._._.,,...�.�.,..,...a -___ _ _ _�--�+-.�..R,,... .�,:...a,,. ___ _....._. _ __ _ _
Faye 1 of I

nv�ir r:mer,ta! CherrlisT, inc., 1,N11FInington, I< Lab 494
6602 Windmill `dab
'Vilrnington, NC 2,94(35
:10.332.0223
( i
Date:; { 2,.
-- ��I W �eParY ,'1iui'nLer:
3eceipt of sample:
]elivered..x J
YES ❑ v0
14C3'
q WA JP5 ❑ FedEx �� Other C1
1. Nere custody
YES ❑ yo
seals present on the cooler? `�
❑ �/A 2. If custody seals
Original temwere present, were they intact/unbroken?
perature upon receipt JC
IHow temperature taken;
Corrected temperature upon receipt
i3fank
IR Gun ID: Thomas Traceable
5/,192511 57ture
.� against Bottles
i YES Cl© 40
Gun Correction Factor 'C. C3.0
3, If temperature of
i YES ❑ v©
cooler exceeded 6'C, was Project M r.
4. Were proper' custo B /QA notified?
dy
yFS i❑ �Q
procedures (relinquished/received) followed?
5. ''Mere sample ID's listed
YE5 ❑ NQ
on the CPC?
5. Were samples ID's listed
`(ES ❑ 4)
an sample containers?
7. Were collection
YES ❑ �f0
date and time li sted an the CDC?
3, Were
YES ClVp
tests to be performed listed on the CpC?
9.
ES '40
Did samples arrive inprop-
10. Did samples arrive in
_-�, YES __'❑ .VO
good condition forfor each test?
11. Was adequate
`J0
sarrsple volume available7' --- --
12. 'Nere
❑ ES ❑ �O
sam fee rzc
p eived within proper holding time or requested tests?
13. Were acid
I'❑ YES ❑ ua
pre served samples received at aH of e2?
I ;Nere cyanide
!F-I❑ YES ❑ O
samples received at a PH >12?
15. Were sulfide
YES ❑ �0
❑
sampfes received eta
16. Were NH3 at
received
YES C3 `JO
❑ YES
at a chlorine residual � n/L� Pm
17. Were Sulfide/Cyanide received
❑ y0
at a chlorine residual of cQ g
i 18. 'Nere orthophosphate sam l� m/L?
filtered
1
P s in the Field within 15 minutes?
° tQC/Volatiles are pH checked
at rime of analysis
ae Bacteria samples are checkad
and recorded an the berichsheet.
For Chlorine at tlrne o€
analysis and retarded on th�,eb hsh eecSample
Preservation:i
YTust be completed for
5amolefsl
any Sam le s
p I) incorrecterved
by addin $ (circle one):
or 'rnth headspace)
were received incorrectly preserved and Were adjusted
-4`50 -INO3
Time of preservation:
accordingly
10 VaOH
Vote' Wotrfy c�s[arner service m f more than one preservatfve is needed, notate in
meaiate[y for ncarrect[v oreserved comments below
sarnwe,. Obtain a ,.
rzat�f�r the state lab el directed tv analveeC b h w sample or
Y [ e customer 'Nho `vas no[}fied�'ate
Uolatifes 5amole(sj
and ume:
r2re received with headsoace
COMMENTS:
)OC. QA.002
,C

Anamly0cal RequesIll-.
if TM Nam:
Add"w
---- —.-- 7
EM4,-OMr;eAtai TeSting Kc-pol.f. �o-
W) 756.5. Ashevilif-,, NC 288W.). phone.. Fax:
Phone: [phone] Fax: JS28) 350068
roi L-0 Na mv.-
Rupcsttd Aoulyses
-7.7-7-
12�
"Y!
4j--
Temp.
)JAY) -.0 be
'411
IcL%
I Zi .......
Sainpiv-,* fniuc r:

}
Environmental Testing Solutions, Inc.
PO Box 7565, Asheville, NC 28802
Phone: [phone], Fax: [phone]
Project Name -
Project Number:
CHAIN -OF -CUSTODY l Analytical Request.-) I
r SV 1 _-
Client Name: ;~ � �y} (- I'1 , C_
Address:
Report to: c.-r
l
Phone: �W��.`���-�r� Fax:5�n
PO Number:
Preservatives
A Sample Identification
U o
z
-
on
U
z
c
z
x
o
o
..
c7
V) w
R
Temperature (°C)
Received on lee:
_Y) 1 N
Sealed Cooler:
Y 1 N
i
Samples Intact:
Y / N
Additional Comments:
uested Ana
Printed Name of Sampler: Y
DIG
Signature of Sampler: P
I Checked Upon
< 0 2 mgfl Upon
Field
Temp. (°C) Comments

Environmental Testing Solutions, Inc.
PO Box 7565, Asheville, NC 28802
Phone: [phone], Fax: [phone]
Project Name:
Project Nnmber-.
Sample Identification
Temperature
emperature (OC) 7
- c (OC
Received an Ice: Y N
Sealed Cooler: Y N
Samples Intact: Y N
Additional Comments;
CHAIN -OF -CUSTODY Analytical Request
Client Name: %
Address: I I
C'45A I,'
Report to:
Phone. Fax:
PO Number.
Preservatives
Z
E
7
Z
C6
+
0
r
p
L)
c
c?
C
z
Printed Name of Sampler:.
Signature of Sampler:
C1, < 0.2 mo Upon Rcccipt
Field
Temp. (OC) Comments
-�J