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WQ0001863_Residual Annual Report 2020_20210222
Initial Review Reviewer Thornburg, Nathaniel Is this submittal an application? (Excluding additional information.)* r Yes r No If not an application what is the submittal type?* r Annual Report r Residual Annual Report r Additional Information r Other Annual Report Year* 2020 Permit Number (IR)* W00001863 Applicant/Permittee City of Mount Holly Email Notifications Does this need review by the hydrogeologist?* r Yes r No Regional Office Mooresville CO Reviewer Admin Reviewer Submittal Form Project Contact Information Please provide inforration on the person to be contacted by N B Staff Name * Lysa Finnerty Email Address* Ifinnerty@synagro.com electronic subnittal, confirmation of receipt, and other correspondence. Project Information ........ ......... ....................................................................................................................................... . Application/Document Type* r New (Fee Req ui red) r Modification - Major (Fee Required) r Renewal with Major Modification (Fee Required) r Annual Report r Additional Information r Other Phone Number* 14105376150 O Modification - Minor C Renewal C GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 r Residual Annual Report r Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* r Wastewater Irrigation r High -Rate Infiltration r Other Wastewater r Reclaimed Water r Closed -Loop Recycle r Residuals r Single -Family Residence Wastewater r Other Irrigation Permit Number:* WQ0001863 Has Current Existing perrrit number Applicant/Permittee Address* 435 Williams Court, Suite 100, Baltimore, MD 21220 Facility Name * City of Mount Holly RLAP Please provide comments/notes on your current submittal below. 2020 Annual Report for City of Mount Holly NC At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form Engineering Fans, Specifications, Calculations, Bc.) Mt Folly NC 2020 Annual Report FINAL.pdf 22.36MB Upload only 1 FJF docurrent (less than 250 fvB). Miltiple documents rust be confined into one F7F file unless file is larger than upload lirrit. * V By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date 2/22/2021 435 Williams Court, Suite 100 Baltimore, MD 21220 www.synagro.com FEBRUARY 22, 2021 NCDEQ Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: 2020 Annual Report for Permit No. WQ0001863 Dear NCDEQ: SYNAGRO Synagro is submitting one electronic copy of the above referenced report on behalf of the City of Mount Holly, NC. If you have any questions or need additional information, please do not hesitate to contact Danny Jackson at (704) 827-4261 or Adam Brigman at (704) 650-4341. Sincerely, W�1 01_ I t Derrick Shivar Environmental Compliance Manager Enclosures cc: Danny Jackson, City of Mount Holly Adam Brigman, Synagro YOUR PARTNER FORA CLEANER, GREENERWORLD City of Mount Holly, NC RESIDUALS LAND APPLICATION PROGRAM Permit No. WQ0001863 2020 ANNUAL REPORT City of Mount Holly, NC Residuals Land Application Program 2020 Annual Report TABLE OF CONTENTS 1. Certification Form and Annual Operations Summary 2. Annual Residual Sampling Summary Forms and Residuals Analyses 3. Annual Land Application Field Summary Forms 4. TCLP Analysis 5. Pathogen Reduction/Vector Attraction Reduction 6. Soil pH & Lime Application Records 7. Soil Analyses SECTION 1 ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit #: W00001863 County Gaston Year 2020 Facility Name (as shown on pen -nit) Mount Holly WWTP & WTP NPDES No. NCO021156 & 01-36-020 Land Application Operator Synaero Phone# (336) 998-7150 Land application of residuals as allowed by the above permit occurred during the past calendar year? X YES NO. If NO, skip Part A, and PartEl and proceed to PartC. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A — Residuals Application Summary: Total number of application fields in the permit: 16 Total number of fields utilized for land application during the year: 11 Total amount of dry tons applied during the year for all application sites: 164.73 Total number of acres utilized for land application during the year: 144.6 Part B — Annual Compliance Statement: Facility was compliant during calendar year 2020 with all conditions of the land application pen -nit (including but not limited to items 1-13 below) issued by the Division of Water QualityX YES NO. If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All monitoring and reporting requirements in 15A NCAC 02T .1 I I I were complied with (applicable to 40 CFR Part 503 regulated facilities). 9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit. 12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13. All buffer requirements as specified on the permit were maintained during each application of residuals. Part C — Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false info nation, including the possibility of fines and imprisonment for knowing violations." T r, !/ Miles Braswell. Citv Manaeer Permittee Name and Title (type or print) �9 2� atur Af freparer* Date (if different from Permittee) Jl 2 2� of Pennittee Date signature of'L'and Applier Date (if different from Permittee and Preparer) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) - -n OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA ALL COUNTIES - ALL SITES DATE RANGE: 1/1/2020 - 12/31/2020 MOUNT HOLLY, NC MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID MONTH/YEAR February 2020 May 2020 July 2020 November 2020 TOTAL AMOUNT UNIT DRY TONS UNIT DRY METRIC TONS 316,200.00 G 23.47 D 21.29 384,400.00 G 24.20 D 21.95 1,109, 800.00 G 30.87 D 28.00 979,600.00 G 86.19 D 78.18 2.790.000.00 G 164.73 D 149.41 Report Date: 2/2/2021 11:48:22 AM SECTION 2 ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WO Permit Number: W00001863 Facility Name: MOUNT HOLLY, NC Residual Source WQ # or NPDES#: NCO021156 WWTP Name: MOUNT HOLLY WWTP Residual Analysis Data Laboratory: PACE ANALYTICAL; SHEALY ENVIRONMENTAL SERVICES INC. Product Type Sample or Composite Date AEDLIQ 01/16/20 AEDLIQ 04/29/20 AEDLIQ 07/27/20 AEDLIQ 10/08/20 Parameter (mg/kg dry weight) Ceiling Conc. Limit Percent Solids (°I°} NA 1.78 1.51 0.667 2.11 Arsenic 75 <4.6 <5.4 <12 11 Cadmium 85 1.6 2 <3.1 <0.97 Copper 4300 670 640 340 580 Chromium NA 230 200 96 180 Lead 840 11 13 <11 15 Mercury 57 <1 <1.3 <2.9 <0.86 Molybdenum 75 <9.2 <11 <25 <7.7 Nickel 420 17 18 <26 17 Selenium 100 <7.5 <8.8 <20 6.9 Zinc 7500 1000 1000 730 1200 Total Phosphorus NA 13000 19000 25000 18000 TKN NA 77000 73000 76000 54000 Ammonia -Nitrogen NA 6900 11000 23000 8500 Nitrate and Nitrite NA 806 340 276 122 For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer* Date *Preparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1102(26) DENR FORM RSSF-B (12/2006) Printed: 2/2/2021 12:19:55 PM For: 1701 01 ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: W00001863 Facility Name: MOUNT HOLLY, NC Residual Source NPDES # or WQ#: NCO021156 WWTP Name: MOUNT HOLLY WWTP Residual Analysis Data Laboratory: PACE ANALYTICAL; SHEALY ENVIRONMENTAL SERVICES INC. Product Type AEDLIQ AEDLIQ AEDLIQ AEDLIQ Sample or Composite Date 01/16/20 04/29/20 07,127120 10/08/20 Parameters (mgtkg dry weight) Aluminium 15000 22000 22000 26000 Calcium 12000 11000 7500 12000 Magnesium 3500 4200 2600 4600 PH (s.u.) 7.20 7.60 7.40 7.50 Potassium 4300 5000 6800 3600 Sodium 9200 10000 13000 6500 PAN 25286 24440 27676 18022 SAR (Ratio) 2.5275 2.5186 2.6838 1.8514 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there pre significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Z- 4� -2d Signature o Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1102(26) Printed: 2/2/2021 12:20:56 PM For: 1701 01 DENR FORM RSSF-B (12/2006) SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis Synagro 12701 Lancaster Hwy Pineville, NC 28134 Attention: Adam Brigman Project Name: Mt. Holly Project Number: 1701 Lot Number:VA16079 Date Completed:01/23/2020 01/24/2020 1:33 PM Approved and released by: Lab Director - Greenville: Lucas Odom Q pCcfto TNN acca� " Eoi B !1 BOo0o eLna The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 vwvw.shealylab.com Page 1 of 7 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative Synagro Lot Number: VA16079 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below. Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" qualifier If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. The pH analysis associated with the sample(s) in this report was/were performed after the method recommended 15 minute holding time. Metals by ICP The initial sample amount used for sample -001 deviated from the standard procedure. Due to low % solids, the initial amount of this sample was 3 times the standard procedure amount. The LOQ has been adjusted accordingly. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 vvww.shealylab.com Page 2 of 7 Client:Synagro Laboratory ID:VA16079-001 Description: 1 of 4 N+M Matrix: Solid Date Sampled:01/16/2020 0630 % Solids: 1.78 01/17/2020 0106 Date Received:01/16/2020 Inorganic non-metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (% Solids) SM 2540G 1 01/17/2020 0106 MDD 42119 1 350.1 (Ammonia - N ) 350.1 5 01/21/2020 1825 DRD 42312 1 (Nitrate - N ) 9056A 1 01/21/2020 1453 HKL 42577 1 (Nitrite - N ) 9056A 1 01/21/2020 1453 HKL 42578 1 (Phosphorus) 365.1 5 01/20/2020 1705 DMA 01/20/2020 1240 42313 1 (Soil pH meas) 9045D 1 01/20/2020 2034 HET 42404 1 351.4 (TKN) 351.2 1 01/17/2020 1655 DMA 01/17/2020 1153 42144 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run % Solids SM 254OG 1.78 % 1 Ammonia - N (gas diffusion) 350.1 6900 280 150 mg/kg 1 Nitrate - N (soluble) 9056A 780 28 1.4 mg/kg 1 Nitrite - N (soluble) 9056A 26 11 1.1 mg/kg 1 Phosphorus 7723-14-0 365.1 13000 1400 280 mg/kg 1 Soil pH measured in water @ 20 ° C 9045D 7.2 su 1 TKN 351.2 77000 1400 1400 mg/kg 1 CVAA Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7471B 7471B 1 01/23/2020 1139 KSH2 01/22/2020 1540 42153 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7471B ND 4.2 1.0 mg/kg 1 ICP-AES Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3050B 601OD 1 01/18/2020 1530 KSH2 01/17/2020 0939 42010 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Aluminum 7429-90-5 6010D 15000 370 140 mg/kg 1 Arsenic 7440-38-2 6010D ND 14 4.6 mg/kg 1 Cadmium 7440-43-9 6010D 1.6 J 4.6 1.2 mg/kg 1 Calcium 7440-70-2 6010D 12000 4600 570 mg/kg 1 Chromium 7440-47-3 6010D 230 9.2 2.3 mg/kg 1 Copper 7440-50-8 6010D 670 9.2 4.1 mg/kg 1 Iron 7439-89-6 6010D 9800 92 42 mg/kg 1 Lead 7439-92-1 6010D 11 9.2 4.1 mg/kg 1 Magnesium 7439-95-4 6010D 3500 J 4600 570 mg/kg 1 Manganese 7439-96-5 6010D 240 14 5.4 mg/kg 1 Molybdenum 7439-98-7 6010D ND 37 9.2 mg/kg 1 Nickel 7440-02-0 6010D 17 J 37 9.6 mg/kg 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 3 of 7 Client:Synagro Laboratory ID:VA16079-001 Description: 1 of 4 N+M Matrix: Solid Date Sampled:01/16/2020 0630 % Solids: 1.78 01/17/2020 0106 Date Received:01/16/2020 ICP-AES Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3050B 6010D 1 01/18/2020 1530 KSH2 01/17/2020 0939 42010 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Potassium 7440-09-7 6010D 4300 J 4600 570 mg/kg 1 Selenium 7782-49-2 6010D ND 18 7.5 mg/kg 1 Sodium 7440-23-5 6010D 9200 4600 570 nrl 1 Zinc 7440-66-6 6010D 1000 46 11 nrl 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 4 of 7 Chain of Custody and Miscellaneous Documents Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 5 of 7 SHEALY ENVIRONMENTAL SERVICES, INC. - � w ,T fiJ i I5 ,y oo R] + 4 m m gox Q- m '� av Wi n. C1 KU ; s 5�A pa 63 LU szf' LO 3 z i� ,•: z_ z � tk � o w i I� *r C ; �- c �_ } p E O Y � C k 1 yeyss ~ i rt' C ID3 a 9 E 6 p ` J r E r Cy �OE k�+ ,u a UP n ' .5 Y 5 F Cj 00 � c; fw 1 � * � G' �• � Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 6 of 7 SHEALY ENVIRONMENTAL SERVICES, INC. S6ca]yLm�imwr�Itl01S.x+•.r: I:... 1bp i on Udeumcnt Ni.nba: MUU t 14 t:t7etdtc Dale: 9/L�11 B Sample Receipt Checklist ( R(' Chant- SY11RgrO Cooler ]n. rctcd hy+datw' KWx ) 0l,'16,N20 Lot *: VA16079 hicans of rcwipt-. 0 SlW I-1 Clicuil UPS F-1 FedEx I-1 tklier L.1Yss Flo L. Wert; auswy seals prezent on the cooler's Yes; Nlo NA ?. Ifetrstody se4s wcro prcsmiwefa ilk:_y in6w't and unbroken? 51I Strip li]; NA C'hlarrnc Strip ID: NA Tcmtad byzNA �r�(ir�ginraly tpemperat+uu Iy l-O upon reecipt / Dcrivizd ry(Oxncted) tem�py erfm.+a�te upm rc :s ipl- 0/6 ohd Snap -Cup ID; 19L-2313 ae i vlathad: ier5speruF�im RIs�n]; �]lig s# l ottlos IR Gurr la: 6 IR Gun C'4reeUU Factor: d °C vTothnd ofcoatent- 0 wrr t.,= F F— 1>.,1I— ii r,— 1— F1 y— El — IftempeiLaure pf any Cooler eatCeeded fi.fl'°C`, W85 ProjeU Manugor Norifk& hex ©hl0 0NA I'M was NtAifiod + email l (oircle one). ❑ Yesi ❑ Ko 0 NA 4. 1,1 the vomtttefciai Couricr's packwg slip atiac hcd t0 this iskin? V&02 S- 1Vm proper custody pmceduucs (relic uizibmb'rccahrcd) followed? 6. were €:ample ms listed on tite cOC? 7. Were sample if-)s listed on ail s le centaijwn? 8, Was cplkction date & Bute hN1W m t e CoC? 9. 1h'aF1 caller=tian date & tiaw bsW on all le containers? ® Yes ❑ N0 10_ Did ull conUiaer label inform FLtion (ID, date, tirnc) agrec with the CDC? 0 Yea E] N0 11, Were tWS tv by per&nned hHtnd on the COC? m, yms ❑'N0 12. Did all spmpics arrive in dtie ilmprT containers for each tmt andlor in goad oonditiQu (Unbrok>en, lids 4ML, Yes ❑ Nn 13. Was aCl Numiz mmplc vole ne aveilttble? — Yes ❑ No 114. "ere ail ii"Ics recei�ved widiln'1a tho hold'holdin time car4A Furs, whickrevtr urmcs first? Y[ l+la is. V,'6re a<Yy sum leer acuatminem missirt 'c—CSS (circle urlel Namplas NQt listed ou COC; Yes 1:3 No O NA 16. For VOA and K K-175 "uplcb, were huhhles p,rccnk >1 pea -size" (A" sir 6tnm in diameter) in any of the V 0A vials' Yes0 No W1 NA 17, Were ell DRO+mcatls,+nUtrienL RmTks ro,-,aived flt a r.H of < 2? ❑ YaS ❑ No 0 NA I 18- Wffm a] I cyanide saint lei rweiverd 2L a pH -r 12 and su lfide s2m le- rcocived at t PH ? 9? ❑ Yes ❑ N4 7 0 NA 1. - Vdexe all alpplir,ab NH..i leyanic;ciphiano '625 (-< 0.53ng1sainples; frec of rr.4idua til>ll.lti llfrCry ❑ 10 NA 21), Were chenina l rolk5AequmiyG11 (t,, rcquested dilu6cros, US,, ^lM de-,�jn-AUons. Ctc.., j YES El Nocorrectly ttvtgorbad front the COC into Li1C comment tcaicn �n LIME? .LLYen l0 21. 4ias the quota ioumber listed rm the container I4#cl? If 5 s, Qu0tc # NA Mille Preservation (Must bti oompleWd for any saluple(a,) incarroody presefvctl or with lteadspw>tj tnple(s) wr:rc Nwived incorrcctly pfcserved and were adjusted 4CQtXding1y sat to rcrmving with NA tnL of circle cme: H2SO4, HNO3, HC 1, NaOli n:;J" 5R 4 NA me ref pTamrvad m NA if more than on-o preservative is nccdod. Please rlclte in the c-01M llel] 1. bulmu, mPle(g) NA _ +vest: =ived with huhblcs }( inni i11 +Jisimr. r. tnples(s) N A - were %-,'ith 'fR1C > a.$ mWL (ff 019 i.% un-) an d „'ore justxd accordingly in s;ampte reaaiving wWi Wdium thimulfate {KkS20,) with, Sheaf- I11); N-1 harcode lnhcla applied b±� DN4N Date. 01l1�, U20 Commeauz Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 7 of 7 Mille Preservation (Must bti oompleWd for any saluple(a,) incarroody presefvctl or with lteadspw>tj tnple(s) wr:rc Nwived incorrcctly pfcserved and were adjusted 4CQtXding1y sat to rcrmving with NA tnL of circle cme: H2SO4, HNO3, HC 1, NaOli n:;J" 5R 4 NA me ref pTamrvad m NA if more than on-o preservative is nccdod. Please rlclte in the c-01M llel] 1. bulmu, mPle(g) NA _ +vest: =ived with huhblcs }( inni i11 +Jisimr. r. tnples(s) N A - were %-,'ith 'fR1C > a.$ mWL (ff 019 i.% un-) an d „'ore justxd accordingly in s;ampte reaaiving wWi Wdium thimulfate {KkS20,) with, Sheaf- I11); N-1 harcode lnhcla applied b±� DN4N Date. 01l1�, U20 Commeauz Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 7 of 7 0p 0 PaceAnalyfical Report of Analysis Synagro 12701 Lancaster Hwy Pineville, NC 28134 Attention: Adam Brigman Project Name: Mt. Holly Project Number: 50-1-701 Lot Number:VD29083 Date Completed:05/07/2020 NIM�� Mr� 05/08/2020 10:24 AM Approved and released by: Lab Director - Greenville: Lucas Odom Q PCCRBp�� AAW 'ye I ANSI NdmlAccre00- Board eORft Al A C C R E D I T E D TESTING LABORATORY The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC. Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 Tel:803-791-9700 Fax:803-791-9111 www.pacelabs.com Page 1 of 7 PACE ANALYTICAL SERVICES, LLC SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative Synagro Lot Number: VD29083 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Pace policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below. Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' qualifier If you have any questions regarding this report please contact the Pace Project Manager listed on the cover page. The pH analysis associated with the sample(s) in this report was/were performed after the method recommended 15 minute holding time. Metals by ICP Due to low percent solids sample -001 was weighed out at 3 times the normal amount. The LOQ has been elevated to reflect the dilution. Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 vvvvvv.pacelabs.com Page 2 of 7 Client:Synagro Laboratory ID:VD29083-001 Description: Mt Holly 2 of 4 N+M Matrix: Solid Date Sampled:04/29/2020 0800 % Solids: 1.51 04/29/2020 2359 Date Received: 04/29/2020 Inorganic non-metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (% Solids) SM 2540G 1 04/29/2020 2359 HET 52469 1 350.1 (Ammonia - N ) 350.1 5 05/01/2020 1321 DRD 52545 1 (Nitrate - N ) 9056A 1 05/05/2020 1547 HKL 53002 1 (Nitrite - N ) 9056A 1 05/05/2020 1547 HKL 53003 1 (Phosphorus) 365.1 10 05/04/2020 1330 DMA 05/04/2020 0914 52789 1 (Soil pH meas) 9045D 1 04/30/2020 2036 SRB 52590 1 351.4 (TKN) 351.2 1 05/06/2020 1532 DMA 05/06/2020 0951 52983 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run % Solids SM 254OG 1.51 % 1 Ammonia - N (gas diffusion) 350.1 11000 330 170 mg/kg 1 Nitrate - N (soluble) 9056A 250 33 1.6 mg/kg 1 Nitrite - N (soluble) 9056A 90 13 1.3 mg/kg 1 Phosphorus 7723-14-0 365.1 19000 3300 660 mg/kg 1 Soil pH measured in water @ 19.6 ° C 9045D 7.6 su 1 TKN 351.2 73000 1700 1700 mg/kg 1 CVAA Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7471 B 7471 B 1 05/05/2020 0212 JMH 05/04/2020 0550 52784 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7471B ND 5.3 1.3 mg/kg 1 ICP-AES Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3050B 601OD 1 05/01/2020 1123 LLL 04/30/2020 1506 52486 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Aluminum 7429-90-5 6010D 22000 430 160 mg/kg 1 Arsenic 7440-38-2 6010D ND 16 5.4 mg/kg 1 Cadmium 7440-43-9 6010D 2.0 J 5.4 1.4 mg/kg 1 Calcium 7440-70-2 6010D 11000 5400 680 mg/kg 1 Chromium 7440-47-3 6010D 200 11 2.7 mg/kg 1 Copper 7440-50-8 6010D 640 11 4.9 mg/kg 1 Iron 7439-89-6 6010D 11000 110 49 mg/kg 1 Lead 7439-92-1 6010D 13 11 4.9 mg/kg 1 Magnesium 7439-95-4 6010D 4200 J 5400 680 mg/kg 1 Manganese 7439-96-5 6010D 260 16 6.4 mg/kg 1 Molybdenum 7439-98-7 6010D ND 43 11 mg/kg 1 Nickel 7440-02-0 6010D 18 J 43 11 mg/kg 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 3 of 7 Client:Synagro Laboratory ID:VD29083-001 Description: Mt Holly 2 of 4 N+M Matrix: Solid Date Sampled:04/29/2020 0800 % Solids: 1.51 04/29/2020 2359 Date Received:04/29/2020 ICP-AES Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3050B 6010D 1 05/01/2020 1123 LLL 04/30/2020 1506 52486 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Potassium 7440-09-7 6010D 5000 J 5400 680 mg/kg 1 Selenium 7782-49-2 6010D ND 22 8.8 mg/kg 1 Sodium 7440-23-5 6010D 10000 5400 680 mg/kg 1 Zinc 7440-66-6 6010D 1000 54 14 mg/kg 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 4 of 7 Chain of Custody and Miscellaneous Documents Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 5 of 7 PACE ANALYTICAL SERVICES. LLC T� t O di C Lk F 0. H p r [7 " � — E J7 d i I Li 4 F1 I ED �] a • 2 EL 4 w o4m .a �T—"I r7 a '� — {� O n.l-0v o o J J. I �a��ao ?C I � 7° ' L of (I7 Z z 1 E 4 r 3 x O 47 -u ~% 51 x 2 a 1 tirx vi t. _ & ..�. I EJ;13 5 i nr, h 42 w m E t N. vs :ZCL I I I m{{ii I CL d }� !] m] I QF " m X 'a ' i'c: }. j 'r, Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 6 of 7 PACE ANALYTICAL SERVICES, LLC tihrs'ly 4ari0m, ]IYC. rAge 1 orL I]wumerthlumtlr: i41Q]DIHC-I4 Erfeali4e �7,�9e, &21241s Sample Retwcip�' hccklist (S�tQ Client WMAG110 Cooler Inssueved la)-Alalr._ JSFI r 04 r9,'2020 JML �: vu.2909J ivJuar.s of re i;ai; Q Yes ® to YL s C L ID SESI ❑ Cller_t ❑ UPS ❑ Frju." C711L4r: - 1. werv. custody fc ]s msYrt On the eoolee? T�TAi ,_If CIrSU?ri Beals WE ent were Lh� ' intm:t and ULILJJ%0kan° - H Strip ID: WA _ Chlorinc Scrip ID_ NA � TUc Wd by_ N.4 pH ')Figin.l te arrilreraLxtrrec e Upon eipt 1' De.ivvd (Corrected) temperature urmn rcmuipi. i�Snlid 5t1ap Cup ID- 20-302 l 7 11.7 rC OVA JNA oC Nil {NA {C NA ,,NA °G Method= E]TemperaturC 9Wk ❑ ApIrrA Bottles lR GUTI EL)= _G iR Gun CALTecdion Radrr: 11 °C Me hod of euolaut: ® W VL Ice 13 let P'aLks ❑ Dr lcc ❑ NOtte ❑ Yes ❑ No ONA 3. Iftertperature of any ocuJerexrci,lfxl 6_DIC, was Prrrlect hiauager7dat: 1,50 PM was -Notified 'ay: phora:,' cmLdl f fauu-to-raoe (circle one), 4. Is the cmin rcial ru1mr1s:r's prr Ung slip aatached to this fbnu'k - -- ❑ Yes ❑ No ®NA Yc5 ❑ Nv 5. Wera proper eustcaly ae&u'os (re13nqui3aed1rcccivcd) CoLlrwed" r� I y_E ves ❑ NO 6- Wefe 3Luuple 1D. ll4#Pd orL fic COO W1 Ycf ❑ NO 7- Were sample Ills Itstcd on all sample nontainers r ® Yes Q No S- Was collection da:e & dmL: 119t:d vit (--ie COCF 9- Wn collection date & time Jistrd cn tell satnple COntainers7 LI Yes Z -Na ®_ Ye€ ❑ No 10. Did aLl milainer label infanination (:']), date, HmCl "ree WiLIN the CGO 'r' 8 0 rjp L ! . Were 'asts lobe perforlued ]htcd on tk COC? 12. Did all samples arrivc in the proper ronhiineF4 for each test widlor it good conditioa 1'imlunkcn, lidE Dn, c1c,)7 -- 21 Yes ❑ N ® ym �T L_.,LND 13, usbLIL-quutu wmipk vtOurnot awallable7 5ro5 ❑ No 14L Were sl] samFlesrtcdived9Althlp'l3 rhehnlcir_gt&e or49 hours, whiciv:vcrta€TICS =Ira? Yes! ONO I5. Wrrn env -samples containers Lnissin fixccss (airdo me) Sam Ics Not ]LSW on COC? 0 Ye4� [] No ® N Ain 16- For VDA and RSK-175 sarnplms, wrre Nihhles pregent >"pea -sin:' (1W or 63nm in &Uinclu) any of the VOA vials`? Q Yes No [, NA I7. Wem alI DRC?1rrimudsfnu-xiert samples received at a pLI oC< 2? �] Yes ❑ Na ® hlA L9. Were all ryunido aompLcs received at a pl-I > 12 and su:fide samples recciveyd at & H � 99 13Y ❑ NC, 0 KOL I99i�4'o1 a flat flpplica;rle N1.1vTKNicyanidelphe-ioll625 (-, 0.5mi1L) sample Fn�e J rL HL C11lerin ❑Yea; j No N' 8, SN15D dasigLations,vEc...) ' 20, Were client remarksfrNilmts (i,e. rtr)reS#ed di1Ur14hM correctly transw ed from the COC into the co�l:nant section in [ IM S? ❑ Yes Na 121. WaLs Lhe quote muter listed Liu the container label? If yc5, Qooe 9 NA ample Presemndm {Mat be oampletad for wy sPmplr.(5) in,cw=tly presen ed (rwith headspam) iSample(s) NA were received incorrectly prescrrcd and were adjustc3daCc�w4ingly in satnpla rec; iv'ng w:t]l NA mL of Cirelt ot1C: H SO4, FLM01, I ICI, NaCNI I using 5R # NA iiu� urpreseraaticrl �+�..__..r _.. ]f`ulOrL: t118i1 ATto pnC6CrYdCi� is nve[irxi, �Iea�e rLOLe iti CiC CDmLTiGltS l}Clow, Sanlplc(s) _ _ ., were -=Dived wilb b-UbbkI->61Ttn_ in ilia meLsr- Sar.Lplcs(3) N-1k _— were received with TRC- n 0.5 w20 , (ff gS 9 i s mu) and were adiustcd aC=dingly in sampla,receiving with sodium thiasulW-, (NL'S2Cia) Witb Sls�Wy ID: NA tilt barrade labeh applied by, ]SH rare: 0 L'_Ni' 02.11 Comments: Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 7 of 7 0p 0 PaceAnalyfical Report of Analysis Synagro 12701 Lancaster Hwy Pineville, NC 28134 Attention: Alex Fox Project Name: Mt. Holly Lot Number:VG27030 Date Completed:08/05/2020 NIM�� Mr� 08/06/2020 3:33 PM Approved and released by: Project Manager II: Lucas Odom Q PCCRBp�� AAW 'ye I ANSI NdmlAccre00- Board eORft Al A C C R E D I T E D TESTING LABORATORY The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC. Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 Tel:803-791-9700 Fax:803-791-9111 www.pacelabs.com Page 1 of 7 PACE ANALYTICAL SERVICES, LLC SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative Synagro Lot Number: VG27030 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Pace policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below. Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' qualifier If you have any questions regarding this report please contact the Pace Project Manager listed on the cover page. The pH analysis associated with the sample(s) in this report was/were performed after the method recommended 15 minute holding time. Metals by ICP Due to the low % solids value, sample -001 was weighed out 3 times the normal amount. The LOQ has been elevated to reflect the dilution. Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 vvvvvv.pacelabs.com Page 2 of 7 Client:Synagro Laboratory ID:VG27030-001 Description: Mnt Holly Matrix: Solid Date Sampled:07/27/2020 1015 % Solids: 0.667 07/29/2020 0155 Date Received:07/27/2020 Inorganic non-metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 (% Solids) SM 2540G 1 07/29/2020 0155 LSH 61560 1 350.1 (Ammonia - N ) 350.1 5 07/28/2020 1323 DMA 61436 1 (Nitrate - N ) 9056A 1 07/29/2020 1929 AMR 61679 1 (Nitrite - N ) 9056A 1 07/29/2020 1929 AMR 61744 1 (Phosphorus) 365.1 5 07/28/2020 1359 DMA 07/28/2020 0935 61432 1 (Soil pH meas) 9045D 1 08/04/2020 2226 SRB 62360 1 351.4 (TKN) 351.2 1 07/28/2020 1501 DMA 07/28/2020 1002 61429 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run % Solids SM 254OG 0.667 % 2 Ammonia - N (gas diffusion) 350.1 23000 750 390 mg/kg 1 Nitrate - N (soluble) 9056A 210 75 15 mg/kg 1 Nitrite - N (soluble) 9056A 66 30 15 mg/kg 1 Phosphorus 7723-14-0 365.1 25000 3700 750 mg/kg 1 Soil pH measured in water @ 21.5 ° C 9045D 7.4 su 1 TKN 351.2 76000 3700 3700 mg/kg 1 CVAA Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7471 B 7471 B 1 07/29/2020 1447 JAB2 07/29/2020 1025 61550 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7471B ND 12 2.9 mg/kg 1 ICP-AES Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3050B 601OD 1 07/30/2020 1411 KSH2 07/29/2020 1428 61551 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Aluminum 7429-90-5 6010D 22000 1000 370 mg/kg 1 Arsenic 7440-38-2 601OD ND 37 12 mg/kg 1 Cadmium 7440-43-9 601OD ND 12 3.1 mg/kg 1 Calcium 7440-70-2 6010D 7500 J 12000 1600 mg/kg 1 Chromium 7440-47-3 6010D 96 25 6.2 mg/kg 1 Copper 7440-50-8 6010D 340 25 11 mg/kg 1 Iron 7439-89-6 6010D 8100 250 110 mg/kg 1 Lead 7439-92-1 601OD ND 25 11 mg/kg 1 Magnesium 7439-95-4 6010D 2600 J 12000 1600 mg/kg 1 Manganese 7439-96-5 6010D 140 37 15 mg/kg 1 Molybdenum 7439-98-7 6010D ND 100 25 mg/kg 1 Nickel 7440-02-0 6010D ND 100 26 mg/kg 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 3 of 7 Client:Synagro Laboratory ID:VG27030-001 Description: Mnt Holly Matrix: Solid Date Sampled:07/27/2020 1015 % Solids: 0.667 07/29/2020 0155 Date Received:07/27/2020 ICP-AES Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3050B 6010D 1 07/30/2020 1411 KSH2 07/29/2020 1428 61551 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Potassium 7440-09-7 6010D 6800 J 12000 1600 mg/kg 1 Selenium 7782-49-2 6010D ND 50 20 mg/kg 1 Sodium 7440-23-5 6010D 13000 12000 1600 mg/kg 1 Zinc 7440-66-6 6010D 730 120 31 mg/kg 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 4 of 7 Chain of Custody and Miscellaneous Documents Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 5 of 7 PACE ANALYTICAL SERVICES, LLC C .s L 4 F— 1 £ ❑ m t i� S W n_ -TTo -Egq e o o ec' r E M �e ❑ D} � `m ii m U F [K DC ri L o _ C` m m Er J34'0 ill U iQ a �~} l al w Ci 9 G 3 yx x 2 m l 4j LL, Qi F - `- ❑ j1:3 1�J4 O " O Lj 0 C k C i O 41 10 'v, J2 o +� fl o � i ¢ r�4 i r. Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 6 of 7 PACE ANALYTICAL SERVICES, LLC Rhaly ervWmrwul 3urviax, dam. Cncaiw-iLNurnter; htW18C-Id PAgt '—ON Sample receipt Checidi t (SRQ :jkxif%k0UMLL%Ba e61S Client; S nagru C'aLl] r ins EC i}rl b}+date `�' a. T,''020 ' _ l o[ R. � ('r27030 �caass ofrccei t: 0 SGSI. ❑' CiiVnL ❑ UPS � FedHx � Of'! Al' - I_ i Yu%i Q N01 11. IV= custody seals 4rl.jcnt on thn cooler.? Yes X. o 1 A NA12. if cLastr►d• aeaLs wcra lresent, weae LFey intuc WW untwnkcn7 pH Strip ID: NA Cirlo!ine Stri I]]; NA - p Temed b; ; NA _ i ri inxl tervURL uporLreceipr,' Dri-i-ved{G417ecLetlltemperallime upon cupt 4asolid Snap-CL,p ID; 2Gt30 2.5 {2 lxra -5 =C 'N.4 INA DC NA {ETA "C NA {NA e*had: O'lcrrpei^Atur;e 13JiitLk []An dust JSouics rR Gran ID: 5 IR Crtir, C Lsry ctort pactar: 0 crlrod of ow lal. t- �, 114' et ]ce Jce Paum ❑ T3ry Ice ❑ NamC ❑ Y ❑ No NA 3. If temperii%re a rany ca0ler exceeded 6,0gC, QZ; I`mjecr Nf11na Cr N{a#if P1vf t4a s T�2otified by: phonu i email ,' faae .10- ea (Crrcic Oil Q Yes IJ Nn 91NA 4- is the rommemial caLrrier's mr'gin slip ant ed to [Isis formf 0 Yes { Ya Q NO 5- R�crc ousted)• prucedure_s (*.xrliriyuishe �cbived followed? s No rumple TDs listed an t1le COC7 YCs ❑No 7- V4'ere s�nple TD8 listed 4n all sample Con LLlinE T.37 r-, FTC S. Was cnll�c#ion daiL time iisDed im tha] CpG CJ Yes Z. T,Tu 9- W& c0110r.7na) [bate R. tine fisted or. rLJI sarrrp ooutoiucrs? - - '� ❑txJo IQ. Did All runtainer labe I infci7nati,m (1J], clr r, it a tegree with the COC? ® Ycx [J No J I. were Felts be performed listed art he Gp Yes ❑ No ' . D=d all samples arrive iir the pripjer ; cuttriine M fu!' eAtn rest andfor in goad eondil.iasn (unbrvlren, vn, 4tc.j? 1'es Na ]3, V4ras ad LIM s81nP r ral�ulle �vaiJahle;+ - Yes 'es ❑ fda 1:4L Wrra all samples reccivvd within !a thehaa•Jdi g lime or48 hrnin', wlliGhevu corners fiat? T�lo 1S, WPM an} sairtp[cs containers rsLiui�s excess irclr oraj saai lcs Tin:. r=stcd al; CQC? [� Yes QNo 1,fA �' FOE VC«?L and RS -l7 sLimples,�+erc hbbleipresea�# an an v _ "pea -;ice," (,°'uw Hamm in dixntexer) y o -P D;k vjals e � 7 NoFAI I':- Were ail Tj]��1ma�IyaLarJCrtt samprr.5 L-.ecei d at IL H of < 2? ❑ Ya., ❑ NuI & Were al l cyan ide santi les recwi vad at a pH > I and sulf de samples recei vLd at zL pP ;= 9 0 �L'cs ❑ hlo ® NA 1.9_ i� 're a]T 9Lpp icabl� A'llffKTLcyauidcr),henar < a �,rLg,2,j 5prnp cs frer of r esi�uu r aa:�� o �7,1A�20, i�WerC client rernFaka+'rssqucs-s (;,C rogLtes erl di oon=tly tranwhbcd from the OOC into the c:OIIuir 0 21. Was the quum numhnr Jisxxr ion the cctt#aiu�r ] ;ample YrCWrv;ltiaals (Must hn �;ompleLcd fa, any saQnple(sj ina<�rrectly arnpJe(g) A'.L were rfoeived inocin r sampl0L1•Eceiwing with NA _rnT, vfvircle orc: 11B(14, HNO3, JJC1, Na() itr1r-'0FprrserVtdii(3r, NA _ ifmOmthm,Dire prrsmrvaliw; is needed, E auLph*sj NA war,- ampre s) NA were rcacived with rusted Acccmdrmgl}' with radium tLiosrrrfate (N ,S,p3) v bmade labcb appli.�pd L15r; Crwi$2 Comman(s: Dale: 07 Lions, WWD designations, etc,.. j ,t sue-tion in LIMS? l? ] PyC5� QLteLn 4 NA :owed or wiFlt headspua) -- #ly pa:cs vcd and wer+: adjwgterr ucow-din,& Using SR # ETA .0 ; note in the cOJBL7LCnt3 be hw, ived with bubbl-es --6 mm in diZFnCtCL 4.5 nrg L (If#I 4 is tro) a,Id uCTZ 5heely ID. NA Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 7 of 7 0p 0 PaceAnalyfical Report of Analysis Synagro 12701 Lancaster Hwy Pineville, NC 28134 Attention: Alex Fox Project Name: Mt. Holly Lot Number:VJ09005 Date Completed:10/19/2020 NIM�� Mr� 10/20/2020 4:20 PM Approved and released by: Project Manager II: Lucas Odom Q PCCRBp�� AAW 'ye I ANSI NdmlAccre00- Board eORft Al A C C R E D I T E D TESTING LABORATORY The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC. Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 Tel:803-791-9700 Fax:803-791-9111 www.pacelabs.com Page 1 of 7 PACE ANALYTICAL SERVICES, LLC SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative Synagro Lot Number: VJ09005 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace") Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or discussed below. Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' qualifier If you have any questions regarding this report please contact the Pace Project Manager listed on the cover page. The pH analysis associated with the sample(s) in this report was/were performed after the method recommended 15 minute holding time. Metals by ICP Due to low percent solids, sample -001 were weighed out at 3 times the normal amount. The LOQ has been elevated to reflect the dilution. Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 vvvvvv.pacelabs.com Page 2 of 7 Client:Synagro Laboratory ID:VJ09005-001 Description: Mnt Holly Matrix: Solid Date Sampled:10/08/2020 1045 % Solids: 2.11 10/13/2020 0146 Date Received:10/08/2020 Inorganic non-metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (% Solids) SM 2540G 1 10/13/2020 0146 MOM 69633 1 350.1 (Ammonia - N ) 350.1 5 10/09/2020 1626 DRD 69087 1 (Nitrate - N ) 9056A 1 10/11/2020 1406 AMR 69684 1 (Nitrite - N ) 9056A 1 10/11/2020 1406 AMR 69689 1 (Phosphorus) 365.1 10 10/16/2020 1741 DMA 10/15/2020 1442 70039 1 (Soil pH meas) 9045D 1 10/15/2020 1547 AAB 70076 1 351.4 (TKN) 351.2 1 10/12/2020 1026 DMA 10/09/2020 1332 69306 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run % Solids SM 254OG 2.11 % 1 Ammonia - N (gas diffusion) 350.1 8500 240 120 mg/kg 1 Nitrate - N (soluble) 9056A 89 24 4.7 mg/kg 1 Nitrite - N (soluble) 9056A 33 9.5 4.7 mg/kg 1 Phosphorus 7723-14-0 365.1 18000 2400 470 mg/kg 1 Soil pH measured in water @ 21.5 ° C 9045D 7.5 su 1 TKN 351.2 54000 1200 1200 mg/kg 1 CVAA Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7471 B 7471 B 1 10/13/2020 1045 JAB2 10/13/2020 0742 69575 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7471B ND 3.6 0.86 mg/kg 1 ICP-AES Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3050B 601OD 1 10/15/2020 1830 KSH2 10/14/2020 1522 69435 2 3050B 601OD 1 10/16/2020 0555 KSH2 10/14/2020 1522 69435 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Aluminum 7429-90-5 6010D 26000 310 120 mg/kg 1 Arsenic 7440-38-2 6010D 11 J 12 3.9 mg/kg 1 Cadmium 7440-43-9 6010D ND 3.9 0.97 mg/kg 1 Calcium 7440-70-2 6010D 12000 3900 480 mg/kg 1 Chromium 7440-47-3 6010D 180 7.7 1.9 mg/kg 1 Copper 7440-50-8 6010D 580 7.7 3.5 mg/kg 1 Iron 7439-89-6 6010D 12000 77 35 mg/kg 1 Lead 7439-92-1 6010D 15 7.7 3.5 mg/kg 1 Magnesium 7439-95-4 6010D 4600 3900 480 mg/kg 1 Manganese 7439-96-5 6010D 190 12 4.6 mg/kg 1 Molybdenum 7439-98-7 6010D ND 31 7.7 mg/kg 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 3 of 7 Client:Synagro Laboratory ID:VJ09005-001 Description: Mnt Holly Matrix: Solid Date Sampled:10/08/2020 1045 % Solids: 2.11 10/13/2020 0146 Date Received:10/08/2020 ICP-AES Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3050B 6010D 1 10/15/2020 1830 KSH2 10/14/2020 1522 69435 2 3050B 6010D 1 10/16/2020 0555 KSH2 10/14/2020 1522 69435 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Nickel 7440-02-0 6010D 17 J 31 8.1 mg/kg 1 Potassium 7440-09-7 6010D 3600 J 3900 480 mg/kg 2 Selenium 7782-49-2 6010D 6.9 J 15 6.3 mg/kg 1 Sodium 7440-23-5 6010D 6500 3900 480 mg/kg 2 Zinc 7440-66-6 6010D 1200 39 9.7 mg/kg 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 4 of 7 Chain of Custody and Miscellaneous Documents Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 5 of 7 PACE ANALYTICAL SERVICES, LLC U p CD L L qJ t�n J kd' r B OIJ ad I Eq 1� .01103 qu k NKi- L 4WVL�j TILK Aj rrOON Utpl r2 r,!., 'flo lef) 1po IEV *pj - O"ON k f T 7 1 -XI 7, A L ku t a' i? TIC - - - =L — — — -------- k! 2. MT 2n I V 1.4% FrV-� Ock t R`i a! is 4fl 4 4 a V L) V JQ H. EU 7w -j E: Li IT L%l e Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803)791-9700 Fax (803) 791-9111 www.pacelabs.com Page 6 of 7 PACE ANALYTICAL SERVICES, LLC ,1W;Z1eArra4Pa--# Client- $Yraptn SamplesAlteelPit CNacklistIst IMEDQIRCIS) ar,,cuinb Autlioiity: race ENV - WCCL Sample Receipt Checklist ( ) �-Oolar InsprZied byMa-o: AUD ! 10flfli4ZU LOrt �'; VJM0003 112vised, IMJ202o Page � of 1 NICnrs Uf receipt' Yes ,I N01 Yes No Pace Client rj LtNS n FedEx Odier; Y I l- Were custody 5;ai.5 present or.Oc cualrO ; -gki-2. 1rvus-ixly scal3 vw'crc 5ent,wer6they insaetand unhmkcn? H Strip ID- 2'P-111-11 C.hIorihe Strip II): 20'223- Tcsted by. vID rigiTH11 t-Crripe ature upon w.niP1 1 Derived (Comcctcd) LAMPcraW* upon T*G&Pt %S61i d SnaP-Cup 1D: �-29sld l,] 11.1 aC NA J till o(,. NA +DNA cc IxA j'KA oc Mcttod_ E'f TttmperaPwe 131ank [D 105LSOaIeS IRGila ll� IR Ciuli ComecdoltFactor: c aC hluthaJ of r oulairr. ❑,� wct 100 Ice Paces 0 Dry Iv- 7 NertY ❑ Yes ©Na �t A 3, If 1ClnpC1a1Lre of aay CAo[or ra urtxled &OL5C:, 'has ling cCt [� wiupr Notified? PTA was Nutt led 'ap: ph4»es 1 t�rniail,' Face-to-facc (airolo unc), 4, Is the comet-orejat courier --a packing slip all, Cl,ed x'this fonin? — Yam; Tqo A UNO 5, G:-{: proNr custody pmeednr9S {I0Iir,Ci1115hrdirn:eiyEd'j FOE_Med7 1yes 71 Yes. Lj No 6- Were sample IN listed fin be C{3C? 7- Were saro pie ll3s [€5trd on al[ sample. ,-ontainers? V V,:4 ONo Yes LJNo, S- Was collection date &. time 16ted on the CO I Yes No 9- way cal:eotion d81a & tune listed on all sampler UTMirim? V Yt~ 77No 10. D d all cwtaincr [abel un:orrfl;WOn (ID, date, d ee) agree math d e CDC? -- Yes ND l L. Were uesrs to be pt~ifornird listed nn the COC? r2. Qj(1 a°l Gann }lbS al'rEYe [Ti tllo prcipar rontainers foreach test RFidlor in gES QC: [ MIdiliCM {unbroken. [ids on. 1 Ye:s ❑7du Yes I LJTtin 13. Wnb to unt= N-Wtple volnme av billblc? L] 1(csl LJ 14.W= all samples recoive: within Vi the ho[dingtimar ur 48 ho-jN: whichever comes first..' 15. wcFu env samples containers mis5ine-en ss {circle -one) sir'+ les Not listed on COO? t'CS - d l `Y`CS Tea �i*fA 16. For 1VOA x nd RSK-17 5 wnnplt- u�— I-Aibbles ese pr�i t •pea -size" f /4"or (mm.. in diatneter) ju ' ar Di the VOA via 141� 1-1. Wurc all DROYffietalshnatt'ielit S mptr.5 rec'-C' e 'VA a JIN of< 2? 18, %Vcre ull cyaniCle sa mples received at a pH > =3 and sulfide simple; recei red ar a pH -# 97 No J NA Et Nf) J N.4 Yes ONO ❑NA 9, Wcrc all applicable Nl.earrr Nlctiantdciphcnol!6rr�.11608.3 (< O.�tqsatrap-es free of esidual chlorine? © Y;es EINU MNA 20r Were b!mtremPrk5fTrgiu;Lds(i.e. rryieswddi_L[iUnS, MSWSE) deslguations, ctc...j wrrWdy �linscribed from the 00C 1no the, tmnent section in LIMS7 I Yes -2 No 21- Wvi G ie quote number listed on the ourazdntT €n'j�A? I r ,ps ante # Sample PresersaBnn (Must br compieled for any salnpla[s) inccmi-ectly 11p-eyvrvt-H or w hh hTencLspace-) Samplc(s) x" __WM rcraiw 6 1100ra-eot1;+ presenred aild -o-c ad.im-M ar t:{ Jin&ly in sarnplc rccciving with 4A mL efcjrcle ona; H2SO 1, HV03, 140, NPC H ufiing SR # NA Time Df preservation If uiui* thLi ono ?rescrvntive is needed. Is[ea-na nn -e in the cotr_m mts hc ow - ample($) N t were rCW6WX1 Wilk bubbitn;>6 irim iri diamater. Smple3(5) # .. wC:Te rt=lved with T11C ? QJ mg/L (lf #19 is utr) itnd wum tdjustrd arocordingly in sample receivi.ng, with sodium tF.iasulfAtc {A1F,).S2303) witll Sl;egly ID- SR barcodr, labels aipphed by. AHD I �. IOAII015 Comments; Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 7 of 7 SECTION 3 FACILITY NAME: MOUNT HOLLY, NC LAND OWNER: GREG SPRINGS OPERATOR: GREG SPRINGS CROP 1 NAME: FESCUE HAY (FSH) RESIDUAL SOURCE(S): * See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM WQ PERMIT #: W00001863 FIELD#: NC-GA-00041-0-0001- ANNUAL DRY TONS APPLIED: 2.76 SITE #: NC GA 00041 PREDOMINANT SOIL SERIES: MADISON CROP 1 MAX. PAN: 132 CROP 2 NAME: Page: 1 ACRES UTILIZED: 3.5 ACRES PERMITTED: 3.5 CATION EXCHANGE CAPACITY (NON-503): CROP 2 MAX. PAN: Gallons (G) Site Name of Crop Type or Cubic Yards (Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual Date or or Wet Tons (W) % Residual Dry, Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (lbs/acre) Application Month Solids DryTons/Ac Source Moist Inches Method* Rate** Rate*** mg/kg mg/kg mglkg Amount UOM Crop 1 Crop 2 Crop 1 Crop 2 2/18/2020 37,200.00 (G) 1.780 0.789 MHAEDL MOIST 0-<1/2'- SUR 0.5 0.30 77,000.00 6,900.00 806.00 39.897 FSH Feb-20 137,200.00 (G) Total 0.789 1.- MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID "I certify, under pen flaw, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there ar ' ficant pe ors mitting false information, including the possibility of fines and imprisonment for knowing violations." SIGNATURE OF LAND APPLIER DATE NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobicaliy digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report Printed: 2/1/2021 DENR FORM FSF (12/2006) FACILITY NAME: MOUNT HOLLY, NC LAND OWNER: GREG SPRINGS OPERATOR: GREG SPRINGS CROP 1 NAME: FESCUE HAY (FSH) RESIDUAL SOURCE(S): * See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM WQ PERMIT #: W00001863 FIELD#: NC-GA-00041-0-0006- ANNUAL DRY TONS APPLIED: 11.04 SITE M NC GA 00041 PREDOMINANT SOIL SERIES: CECIL CROP 1 MAX. PAN: 162 CROP 2 NAME: Page: 1 ACRES UTILIZED: 8.9 ACRES PERMITTED: 8.9 CATION EXCHANGE CAPACITY (NON-503): CROP 2 MAX. PAN: Gallons (G) Site Name of Crop Type or Cubic Yards (Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual Date or or Wet Tons (W) % Residual Dry, Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (Ibs/acre) Application Month Solids DryTons/Ac Source Moist Inches Method* Rate** Rate*** mg/kg mg/kg mg/kg Amount UOM Crop 1 Crop 2 Crop 1 Crop 2 2/5/2020 74,400.00 (G) 1.780 0.621 MHAEDL MOIST 110-<1/2" SUR 0.5 0.30 77,000.00 6,900.00 806.00 31.380 FSH 2/18/2020 74,400.00 (G) 1.780 0.621 MHAEDL MOIST 0-<1/2" SUR 0.5 0.30 77,000.D0 6,900.00 806.00 31.380 FSH Feb-20 148,800.00 (G) Total 1.242 '.- I.. AS CD CU CR PB HG MO NI SE ZN P L -- - - Annual Ibs/acre Applied 0.011 0.004 1.663 0.571 0.027 0.002 0.023 0.042 0.019 2.482 32.266 Date Cumulative Ibs/acre Applied 0.106 0.055 16.345 7.477 0.780 0.032 0.228 0.705 0.177 25.50D Permit PAN Limit (Ibs/acre) 1st Crop 162 Federal C.P.L.R. (Ibs/acre)**** 36.6 1 34.8 1 1,339.0 267.9 I 15.0 M ! 375.0 I 89.0 I 2,500.0 MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID "I certify, under penalty la that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are si a penalties-ferstt ing false information, including the possibility of fines and imprisonment for knowing violations." 2_ _ 2 SIGNATURE OF LAND APPLIER DATE NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report Printed: 2/1/2021 DENR FORM FSF (12/2006) FACILITY NAME: MOUNT HOLLY, NC LAND OWNER: GREG SPRINGS OPERATOR: GREG SPRINGS CROP 1 NAME: FESCUE HAY (FSH) RESIDUAL SOURCE(S): * See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM WQ PERMIT#: WQ0001863 FIELD#: NC-GA-00041-0-0014- ANNUAL DRY TONS APPLIED: 9.66 SITE M NC GA 00041 PREDOMINANT SOIL SERIES: CECIL CROP 1 MAX. PAN: 164 CROP 2 NAME: Page: 1 ACRES UTILIZED: 7.4 ACRES PERMITTED: 7.4 CATION EXCHANGE CAPACITY (NON-503): CROP 2 MAX. PAN: Gallons (G) Site Name of Crop Type or Cubic Yards (Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual Date or or Wet Tons (W) % Residual Dry, Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (Ibs/acre) Application Month Solids DryTons/Ac Source Moist Inches Method* Rate** Rate*** mg/kg mg/kg mg/kg Amount UOM Crop 1 Crop 2 Crop 1 Crop 2 2/4/2020 111,600.01) (G) 1.780 1.119 MHAEDL MOIST T<1/2- SUR 0.5 0.30 77,000.00 6,900.00 806.00 56.611 FSH 2/5/202D 12,400.00 (G) 1.780 0.124 MHAEDL MOIST "0-<1/2" SUR 0.5 0.30 77,000.00 6,900.00 806.00 6.290 FSH 2/18/2020 6,200.00 (G) 1.780 0.062 MHAEDL MOIST "0-<1/2" SUR 0.5 0.30 77,000.00 6,900.00 806.00 3.145 FSH Feb-20 130,200.00 (G) Total 1.305 1 Dian oo.Dyo u.Duu AS CD CU CR PB HG MO NI SE ZN P Lime Applied Annual Ibs/acre Applied 0.012 0.004 1.750 0.601 0.029 0.003 0.024 0.044 0.020 2.612 33.955 Date *s**c Cumulative Ibs/acre Applied 0.090 0.046 14.128 6.418 0.643 0.027 0.198 0.586 0.152 22.235 Permit PAN Limit (Ibs/acre) 1st Crop 164 Federal C.P.L.R. (Ibs/acre)**** 36.6 134.8 1 1,339.0 267.9 I 15.0 I ( 375.0 I 89.0 I 2,500.0 MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID "I certify, under penalty o la , that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are si penalties.�ting false information, including the possibility of fines and imprisonment for knowing violations." SIGNATURE OF LAND APPLIER DATE NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report Printed: 2/1/2021 DENR FORM FSF (12/2006) FACILITY NAME: MOUNT HOLLY, NC LANDOWNER: TONY JONES OPERATOR: TONY JONES CROP 1 NAME: FESCUE HAY (FSH) RESIDUAL SOURCE(S): * See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM WO PERMIT #: WQ0001863 FIELD#: NC-LT-00046-0-0001- ANNUAL DRY TONS APPLIED: 7.07 SITE #: NC LT 00046 PREDOMINANT SOIL SERIES: CECIL CROP 1 MAX. PAN: 188 CROP 2 NAME: Page: 1 ACRES UTILIZED: 11.8 ACRES PERMITTED: 11.8 CATION EXCHANGE CAPACITY (NON-503): CROP 2 MAX. PAN: Gallons (G) Site Name of Crop Type or Cubic Yards (Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual Date or or Wet Tons (W) % Residual Dry, Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (Ibs/acre) Application Month Solids Dry Tons/Ac Source Moist Inches Method* Rate** Rate*** mg/kg mg/kg mg/kg Amount UOM Crop 1 Crop 2 Crop 1 1 Crop 2 7/15/2020 37,200.00 (G) 0.667 0.088 MHAEDL DRY "0-<1/2" SUR 0.5 0.30 76,000.00 23,000.00 276.00 4.854 FSH 7/16/2020 105,400.00 (G) 0.667 0.248 MHAEDL DRY "0-<1/2" SUR 0.5 0.30 76,000.00 23,000.00 276.00 13.752 FSH - 7/17/2020 111,600.00 (G) 0.667 0.263 MHAEDL DRY "0-<1/2" SUR 0.5 0,30 76,000.00 23,000.00 276.00 14.561 FSH Jul-20 254,200.00 (G) Total 0.599 1 Dial AS CD Cu CR PB HG MO NI SE ZN P Lime Applied Annual Ibs/acre Applied 0.014 0.004 0.407 0.115 0.013 0.003 0.030 0.031 0.024 0.875 29.959 Date ILbs/Ac 0.091 10.602 1 5.552 1 0.669 1 0.025 1 0.153 1 0.496 1 0.143 1 16.951 Permit PAN Limit (Ibs/acre) 1st Crop, " Federal C.P.L.R. (Ibs/acre)**** 36.6 1 34.8 1 1,339.0 267.9 15.0 375.0 89.0 12,500.0 MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are signific t p alties fiW w r g false information, including the possibility of fines and imprisonment for knowing violations." �/ 2-9-z1 SIGNATURE OF LAND APPLIER DATE NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4 * Application Method: SUR - Surface, [NJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report Printed: 2/4/2021 DENR FORM FSF (12/2006) FACILITY NAME: MOUNT HOLLY, NC LAND OWNER: TONY JONES OPERATOR: TONY JONES CROP 1 NAME: FESCUE (FS) RESIDUAL SOURCE(S): * See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM WQ PERMIT #: WQ0001863 FIELD#: NC-LT-00046-0-OD02- ANNUAL DRY TONS APPLIED: 65.46 SITE M NC LT 00046 PREDOMINANT SOIL SERIES: CECIL CROP 1 MAX. PAN: 209 CROP 2 NAME: Page: 1 ACRES UTILIZED: 45.2 ACRES PERMITTED: 45.2 CATION EXCHANGE CAPACITY (NON-503): CROP 2 MAX. PAN: Date or Month Gallons (G) or Cubic Yards (Y) or Wet Tons (W) % Solids DryTons/Ac Residual Source Site Cond. Dry, Wet, Moist Precip Past 24 Hrs. Inches Application Method* Volati- lization Rate** Mineral- ization Rate*"* TKN mg/kg Ammonia Nitrogen mg/kg Nitrate and Nitrite mg/kg PAN Applied (Ibs/acre) Name of Crop Type Receiving Residual Application Amount UOM Crop 1 Crop 2 Crop 1 Crop 2 11/18/2020 148,800.00 (G) 2.110 0.290 MHAEDL DRY "0-<1/2" SUR 0.5 0.30 54,000.00 8,500.00 122.00 10.440 FS 11/19/2020 155,000.00 (G) 2.110 0.302 MHAEDL DRY "0-<1/2" SUR 0.5 0.30 54,000.00 8,500.00 122.00 10.875 FS 11/20/2020 173,6DO.OD (G) 2.110 D.338 MHAEDL DRY "O-<1/2" SUR 0.5 0.30 54,000.00 8,500.00 122.00 12.180 FS 11/23/2020 179,800.00 (G) 2.110 0.350 MHAEDL DRY "0-<1/2" SUR 0.5 0.30 54,000.00 8,500.00 122.00 12.615 FS 11/24/2020 86,800.00 (G) 2.110 0.169 MHAEDL DRY 110-<1/2" SUR 0.5 0.30 54,000.00 8,500.00 122.00 6.090 FS Nov-20 744,000.00 (G) Total 1.449 AS CD CU CR PB HG MO NI SE ZN P Lime Applied Annual Ibs/acre Applied 0.032 0.003 1.660 0.521 0.043 0.002 0.022 0.049 0.020 3.476 52.138 Date Lbs/Ac Cumulative Ibs/acre Applied 0.109 0.032 9.929 4.339 0.489 0.021 0.143 0.448 0.131 16.443 Permit PAN Limit (Ibs/acre) 1st Crop 209 Federal C.P.L.R. (Ibs/acre)**** 36.6 1 34.8 1 1,339.0 I I 267.9 I 15.0 I I 375.0 ( 89.0 1 2,500.0 MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID "I certify, under penalty f law, that thus document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there P. cant pen bmitting false information, including the possibility of fines and imprisonment for knowing violations." �o� SIGNATURE OF LAND APPLIER DATE NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4 * Application Method: SUR - Surface, [NJ - Injection, SURIN - Incorporation *"* C.P.L.R.: Cumulative Pollutant Loading Rate ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report Printed: 2/1/2021 DENR FORM FSF (12/2006) FACILITY NAME: MOUNT HOLLY, NC LAND OWNER: TONY JONES OPERATOR: TONY JONES CROP 1 NAME: FESCUE HAY (FSH) RESIDUAL SOURCE(S): * See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM WQ PERMIT #: WQ0001863 FIELD#: NC-LT-00046-0-0003- ANNUAL DRY TONS APPLIED: 7.24 SITE #: NC LT 00046 PREDOMINANT SOIL SERIES: CECIL CROP 1 MAX. PAN: 188 CROP 2 NAME: Page: 1 ACRES UTILIZED: 9.9 ACRES PERMITTED: 9.9 CATION EXCHANGE CAPACITY (NON-503): CROP 2 MAX. PAN: Gallons (G) Site Name of Crop Type or Cubic Yards (Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual Date or or Wet Tons (W) % Residual Dry, Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (lbs/acre) Application Month Solids Dry Tons/Ac Source Moist Inches Method* Rate** Rate- mg/kg mg/kg mg/kg Amount UOM Crop 1 Crop 2 Crop 1 Crop 2 7/14/2020 43,400.00 (G) 0.667 0.122 MHAEDL DRY "0-<1/2" SUR 0.5 0.30 76,000.00 23,000.00 276.00 6.749 FSH 7/15/2020 130,200.00 (G) 0.667 0.366 MHAEDL DRY "0-<1/2" SUR 0.5 0.30 76,ODO.00 23,000.00 276.00 20.247 FSH 7/16/2020 86,800.00 (G) 0.667 0.244 MHAEDL DRY 110-<1/2" SUR 0.5 0.30 76,OD0.00 23,000.00 276.00 13.498 FSH Jul-20 260,400.00 (G) Total 0.732 —.1 " "' MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID "I certify, under penalty o law that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are signi penalties fo ' ' false information, including the possibility of fines and imprisonment for knowing violations." 2--1�,- z/ SIGNATURE OF LAND APPLIER DATE NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report Printed: 2/4/2021 DENR FORM FSF (12/2006) FACILITY NAME: MOUNT HOLLY, NC LANDOWNER: TONY JONES OPERATOR: TONY JONES CROP 1 NAME: FESCUE (FS) RESIDUAL SOURCE(S): * See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM W Q PERMIT A W Q0001863 FIELD#: NC-LT-OOD46-0-0004- ANNUAL DRY TONS APPLIED: 20.73 SITE #: NC LT 00046 PREDOMINANT SOIL SERIES: CECIL CROP 1 MAX. PAN: 209 CROP 2 NAME: Page: 1 ACRES UTILIZED: 19.4 ACRES PERMITTED: 19.4 CATION EXCHANGE CAPACITY (NON-503): CROP 2 MAX. PAN: Gallons (G) Site Name of Crop Type or Cubic Yards (Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual Date or or Wet Tons (W) % Residual Dry, Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (Ibs/acre) Application Month Solids DryTons/Ac Source Moist Inches Method* Rate** Rate*** mg/kg mg/kg mg/kg Amount UOM Crop 1 Crop 2 Crop 1 Crop 2 11/24/2020 80,60D.00 (G) 2.110 0.366 MHAEDL DRY "0-<1/2" SUR 0.5 0.30 54,000.00 8,500.00 122.00 13.176 FS 11/25/2020 155,000.00 (G) 2.110 0.703 MHAEDL DRY 1.0-<1/2" SUR 0.5 0.30 54,000.00 8,500.00 122.00 25.339 FS Nov-20 235,600.00 (G) Total 1.069 1 orai sa.o i o v.uw AS CD CU CR PB HG MO NI SE ZN P Lime Applied - Annual Ibs/acre Applied 0.024 0.002 1.240 0.385 0.032 0.002 0.016 0.036 0.015 2.565 38.468 Date Ls c Cumulative Ibs/acre AcDlied 0.074 1 0.024 7,784 3.456 0.392 0.016 0.113 0.367 0.093 13.056 Permit PAN Limit (Ibs/acre) 1st Crop ` Federal C.P.L.R. (Ibs/acre)**** 36.6 1 34.8 1 1,339.0 267.9 15.0 375.0 1 89.0 1 2,500.0 MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID "I certify, under penalty of 1 w, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are signifi t nalties fo ' g false information, including the possibility of fines and imprisonment for knowing violations." zi SIGNATURE OF LAND APPLIER DATE NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report Printed: 2/1/2021 DENR FORM FSF (12/2006) FACILITY NAME: MOUNT HOLLY, NC LAND OWNER: TONY JONES OPERATOR: TONY JONES CROP 1 NAME: FESCUE HAY (FSH) RESIDUAL SOURCE(S): * See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM WQ PERMIT #: WQ0001863 FIELD#: NC-LT-00046-0-0005- ANNUAL DRY TONS APPLIED: 6.04 SITE #: NC LT 00046 PREDOMINANT SOIL SERIES: LLOYD CROP 1 MAX. PAN: 200 CROP 2 NAME: Page: 1 ACRES UTILIZED: 6.6 ACRES PERMITTED: 7.9 CATION EXCHANGE CAPACITY (NON-503): CROP 2 MAX. PAN: Gallons (G) Site Name of Crop Type or Cubic Yards (Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual Date or or Wet Tons (W) % Residual Dry, Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (Ibs/acre) Application Month Solids Dry Tons/Ac Source Moist Inches Method* Rate** Rate*** mg/kg mg/kg mg/kg Amount UOM Crop 1 Crop 2 Crop 1 Crop 2 7/10/2020 99,200.00 (G) 0.667 0.418 MHAEDL DRY "0-<1/2" SUR 0.5 0.30 76,000.00 23,000.00 276.00 23.140 FSH 7/13/2020 117,800.00 (G) 0.667 0.496 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 76,000,00 23,000.00 276.00 27.479 FSH Jul-20 217,000.00 (G) Total 0.914 1.- AS CD CU CR PB HG MO NI SE ZN P Lime Applied Annual Ibs/acre Applied 0.022 0.006 0.622 0.176 0.020 0.005 0.046 ! 0.048 0.037 1.335 45.724 Date Lbs/Ac +++++ +++++ Cumulative Ibs/acre Applied 0.078 1 0.029 6.608 3.218 0.340 0.015 0.113 0.301 0.105 10.484 Permit PAN Limit (Ibs/acre) 1st Crop " Federal C.P.L.R. (Ibs/acre)**** 36.6 34.8 1,339.0 267.9 15.0 375.0 89.0 2,500.0 MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID "I certify, under penalty of law, tb t this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant p alf s for submittin false i formation, including the possibility of fines and imprisonment for knowing violations." 7=,(?—z/ GNATURE OF LAND APPLIER DATE NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***+* See Site pH & Lime Application Records Section of Report Printed: 2/4/2021 DENR FORM FSF (12/2006) FACILITY NAME: MOUNT HOLLY, NC LAND OWNER: TONY JONES OPERATOR: TONY JONES CROP 1 NAME: FESCUE HAY (FSH) RESIDUAL SOURCE(S): * See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM WQ PERMIT* W00001863 FIELD#: NC-LT-00046-0-0007- ANNUAL DRY TONS APPLIED: 5.52 SITE #: NC LT 00046 PREDOMINANT SOIL SERIES: PACOLET CROP 1 MAX. PAN: 208 CROP 2 NAME: Page: 1 ACRES UTILIZED: 7.0 ACRES PERMITTED: 7.0 CATION EXCHANGE CAPACITY (NON-503): CROP 2 MAX. PAN: Gallons (G) Site Name of Crop Type or Cubic Yards (Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual Date or or Wet Tons (W) % Residual Dry, Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (Ibs/acre) Application Month Solids Dry Tons/Ac Source Moist Inches Method* Rate** Rate— mg/kg mg/kg mg/kg Amount UOM Crop 1 Crop 2 Crop 1 Crop 2 7/9/2020 142,600.00 (G) 0.667 0.567 MHAEDL DRY 110-<1/2" SUR 0.5 0.30 76,000.00 23,000.00 276.00 31.363 FSH 7/10/2020 55,800.00 (G) 0.667 0.222 MHAEDL DRY "0-11/2" SUR 0.5 0.30 76,000.00 23,000.00 276.00 12.272 FSH Jul-20 1 198,400.00 (G) Annual Ibs/acre Applied Cumulative Ibs/acre Apl 1st Crop Total 0.789 AS CD CU 0.019 0.005 0.536 0.064 0.028 1 6.364 CR PB HG MO NI SE ZN 0.151 0.017 0.005 0.039 0.041 0.032 1.151 3.096 i 0.356 0.015 0.105 0.318 0.097 9.720 P Lime 39.416 Date 208 Lbs/Ac Federal C.P.L.R. (Ibs/acre)**** 36.6 1 34.8 1 1,339.0 I I 267.9 I 15.0 I I 375.0 I 89.0 I 2,500.0 MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID "I certify, under penalty of la , t t this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significa p alties for else information, including the possibility of fines and imprisomnent for knowing violations." SIGNATURE OF LAND APPLIER DATE NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4 * Application Method: SUR - Surface, [NJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report Printed: 2/4/2021 DENR FORM FSF (1212006) FACILITY NAME: MOUNT HOLLY, NC LANDOWNER: TONY JONES OPERATOR: TONY JONES CROP 1 NAME: FESCUE HAY (FSH) RESIDUAL SOURCE(S): * See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM WQ PERMIT #: WQ0001863 FIELD#: NC-LT-00046-0-0008- ANNUAL DRY TONS APPLIED: 5.00 SITE #: NC LT 00046 PREDOMINANT SOIL SERIES: CECIL CROP 1 MAX. PAN: 182 CROP 2 NAME: Page: 1 ACRES UTILIZED: 6.6 ACRES PERMITTED: 6.6 CATION EXCHANGE CAPACITY (NON-503): CROP 2 MAX. PAN: Gallons (G) Site Name of Crop Type or Cubic Yards (Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual Date or or Wet Tons (W) % Residual Dry, Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (lbs/acre) Application Month Solids DryTons/Ac Source Moist Inches Method* Rate** Rate*** mg/kg mg/kg mg/kg _Amount_ATount UOM Crop 1 Crop 2 Crop 1 Crop 2 7/13/2020 43,400.00 (G) 0.667 0.183 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 76,000.00 23,000.00 276.00 10.124 FSH 7/14/2020 136,400.D0 (G) 0.667 0.575 MHAEDL DRY "0-<1!2" SUR 0.5 0.30 76,000.00 23,000.00 276.00 31.817 FSH Jul-20 179,800.00 (G) Total 0.758 —.1 " " 1 """ MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significantp al s for su� information, including the possibility of fines and imprisonment for knowing violations." SIGNATURE OF LAND APPLIER DATE NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4 * Application Method: SUR - Surface, ]NJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report Printed: 2/4/2021 DENR FORM FSF (12/2006) FACILITY NAME: MOUNT HOLLY, NC LAND OWNER: DEAN & DALE CONNELL OPERATOR: DEAN & DALE CONNELL CROP 1 NAME: FESCUE PASTURE (FSP) RESIDUAL SOURCE(S): * See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM WQ PERMIT#: WQ0001863 FIELD#: NC-MG-00037-0-0001- ANNUAL DRY TONS APPLIED: 24.20 SITE #: NC MG 00037 PREDOMINANT SOIL SERIES: CECIL CROP 1 MAX. PAN: 139 CROP 2 NAME: Page: 1 ACRES UTILIZED: 18.3 ACRES PERMITTED: 18.3 CATION EXCHANGE CAPACITY (NON-503): CROP 2 MAX. PAN: Gallons (G) Site Name of Crop Type or Cubic Yards (Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual Date or or Wet Tons (W) % Residual Dry, Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (Ibs/acre) Application Crop 1 Crop 2 Crop 1 Crop 2 Month Solids DryTons/Ac Source Moist Inches Method* Rate** Rate*** mg/kg mg/kg mg/kg Amount UOM 5/7/2020 130,200.00 (G) 1.510 0.448 MHAEDL DRY "0-<1/2" SUR 0.5 0.30 73,000.00 11,000.00 340.00 21.898 FSP 5/8/2020 264,200.00 (G) 1.510 0.875 MHAEDL DRY "0-<1/2" SUR 0.5 0.30 73,000.00 11,000.00 340.00 42.753 FSP May-20 384,400.00 (G) Total 1.323----- AS CD Cu CR PB HG MO NI SE ZN P Lime Applied .. __ . Annual Ibs/acre Applied 0.014 0.005 1.693 0.529 0.034 0.003 0.029 0.048 0.023 2.645 50.261 Date Lbs Ac Cumulative Ibs/acre Applied 0.21 0.052 1 12.112 1 5.878 1 0.621 1 0.024 0.531 I 0. Permit PAN Limit (Ibs/acre) 1st Crop 139 Federal C P L R (Ibs/acre)**** 36.6 34.8 1,339.0 267.9 15.G 375.0 89.0 2,500.0 MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID "I certify, under penalty of law, that thi document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant pen ti for sub e information, including the possibility of fines and imprisonment for knowing violations" SIGNATURE OF LAND APPLIER DATE NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report Printed: 2/4/2021 DENR FORM FSF (12/2006) SECTION 4 SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis Synagro 12701 Lancaster Hwy Pineville, NC 28134 Attention: Adam Brigman Project Name: Mt. Holly Project Number: 1701 Lot Number:VA16082 Date Completed:01/28/2020 01/29/2020 9:54 AM Approved and released by: Lab Director - Greenville: Lucas Odom Q pCCRFO TNN acca� " Eoi B !1 BOo0o eLna The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 vwvw.shealylab.com Page 1 of 11 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative Synagro Lot Number: VA16082 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below. Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" qualifier If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. The pH analysis associated with the sample(s) in this report was/were performed after the method recommended 15 minute holding time. Paint Filter Sample -001 has been qualified with an "H", however, paint filter analysis does not have a method defined hold time. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 vvww.shealylab.com Page 2 of 11 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary Synagro Lot Number: VA16082 Sample Number Sample ID Matrix Date Sampled Date Received 001 2020 Mt. Holly TCLP Solid 01/16/2020 0640 01/16/2020 (1 sample) Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 3of11 SHEALY ENVIRONMENTAL SERVICES, INC. Detection Summary Synagro Lot Number: VA16082 Sample Sample ID Matrix Parameter Method Result Q Units Page 001 2020 Mt. Holly TCLP Solid Ignitability (Pensky-Martens 1010A >140 ° F 5 001 2020 Mt. Holly TCLP Solid Paint Filter Test 9095B Fail H' pass/fail 5 (2 detections) Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 4 of 11 Client:Synagro Laboratory ID:VA16082-001 Description: 2020 Mt. Holly TCLP Matrix: Solid Date Sampled:01/16/2020 0640 % Solids: 1.24 01/17/2020 0106 Date Received:01/16/2020 Inorganic non-metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Ignitability) 1010A 1 01/22/2020 1406 SLC 42609 1 (Paint Filter) 9095B 1 01/28/2020 1408 HET 1 (Reactive Cya) 7.3.3 1 01/27/2020 1835 MSG 01/23/2020 1057 1 (Reactive Sul) 7.3.4 1 01/27/2020 1544 HET 01/23/2020 1057 1 (Soil pH meas) 9045D 1 01/20/2020 2053 HET 42404 CAS Analytical Parameter Number Method Result Q LOQ Units Run Ignitability (Pensky-Martens Closed -Cup) 1010A >140 140 o F 1 Paint Filter Test 9095B Fail H" pass/fail 1 Reactive Cyanide 7.3.3 ND 50 mg/kg 1 Reactive Sulfide 7.3.4 ND 50 mg/kg 1 Soil pH measured in water @ 19.5 ° C 9045D 7.1 su 1 TCLP Volatiles Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/5030B 8260D 10 01/25/2020 0128 JTH 42876 01/22/2020 2342 CAS Analytical Parameter Number Method Result Q LOQ Units Run Benzene 71-43-2 8260D ND 0.050 mg/L 1 2-Butanone (MEK) 78-93-3 8260D ND 0.10 mg/L 1 Carbon tetrachloride 56-23-5 8260D ND 0.050 mg/L 1 Chlorobenzene 108-90-7 8260D ND 0.050 mg/L 1 Chloroform 67-66-3 8260D ND 0.050 mg/L 1 1,2-Dichloroethane 107-06-2 8260D ND 0.050 mg/L 1 1,1-Dichloroethene 75-35-4 8260D ND 0.050 mg/L 1 Tetrachloroethene 127-18-4 8260D ND 0.050 mg/L 1 Trichloroethene 79-01-6 8260D ND 0.050 mg/L 1 Vinyl chloride 75-01-4 8260D ND 0.010 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 104 70-130 1,2-Dichloroethane-d4 100 70-130 Toluene-d8 103 70-130 TCLP Semivolatiles Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8270E 1 01/28/2020 1505 SCD 01/22/2020 1642 42622 01/20/2020 2316 CAS Analytical Parameter Number Method Result Q LOQ Units Run 1,4-Dichlorobenzene 106-46-7 8270E ND 0.040 mg/L 1 2,4-Dinitrotoluene 121-14-2 8270E ND 0.080 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 5 of 11 Client:Synagro Laboratory ID:VA16082-001 Description: 2020 Mt. Holly TCLP Matrix: Solid Date Sampled:01/16/2020 0640 % Solids: 1.24 01/17/2020 0106 Date Received:01/16/2020 TCLP Semivolatiles Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8270E 1 01/28/2020 1505 SCD 01/22/2020 1642 42622 01/20/2020 2316 CAS Analytical Parameter Number Method Result Q LOQ Units Run Hexachlorobenzene 118-74-1 8270E ND 0.040 mg/L 1 Hexachlorobutadiene 87-68-3 8270E ND 0.040 mg/L 1 Hexachloroethane 67-72-1 8270E ND 0.040 mg/L 1 2-Methylphenol 95-48-7 8270E ND 0.040 mg/L 1 3+4-Methylphenol 106-44-5 8270E ND 0.040 mg/L 1 Nitrobenzene 98-95-3 8270E ND 0.040 mg/L 1 Pentachlorophenol 87-86-5 8270E ND 0.20 mg/L 1 Pyridine 110-86-1 8270E ND 0.040 mg/L 1 2,4,5-Trichlorophenol 95-95-4 8270E ND 0.040 mg/L 1 2,4,6-Trichlorophenol 88-06-2 8270E ND 0.040 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 92 37-129 2-Fluorophenol 55 24-127 Nitrobenzene-d5 100 38-127 Phenol-d5 69 28-128 Terphenyl-d14 118 10-148 2,4,6-Tribromophenol 110 41-144 TCLP Herbicides Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/8151A 8151A 1 01/27/2020 1250 DAL1 01/23/2020 1207 42707 01/20/2020 2316 CAS Analytical Parameter Number Method Result Q LOQ Units Run 2,4-D 94-75-7 8151A ND 0.020 mg/L 1 2,4,5-TP (Silvex) 93-72-1 8151A ND 0.0050 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits DCAA 58 50-112 PCBs by GC Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3550C 366013/3665A 8082A 1 01/28/2020 1312 CHG 01/27/2020 2245 43002 CAS Analytical Parameter Number Method Result Q LOQ Units Run Aroclor 1016 12674-11-2 8082A ND 1300 ug/kg 1 Aroclor 1221 11104-28-2 8082A ND 1300 ug/kg 1 Aroclor 1232 11141-16-5 8082A ND 1300 ug/kg 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 6 of 11 Client:Synagro Laboratory ID:VA16082-001 Description: 2020 Mt. Holly TCLP Matrix: Solid Date Sampled:01/16/2020 0640 % Solids: 1.24 01/17/2020 0106 Date Received:01/16/2020 PCBs by GC Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3550C 3660B/3665A 8082A 1 01/28/2020 1312 CHG 01/27/2020 2245 43002 CAS Analytical Parameter Number Method Result Q LOQ Units Run Aroclor 1242 53469-21-9 8082A ND 1300 ug/kg 1 Aroclor 1248 12672-29-6 8082A ND 1300 ug/kg 1 Aroclor 1254 11097-69-1 8082A ND 1300 ug/kg 1 Aroclor 1260 11096-82-5 8082A ND 1300 ug/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits Decachlorobiphenyl 86 41-132 Tetrachloro-m-xylene 75 35-106 TCLP Pesticides Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8081B 1 01/24/20201854 DAL1 01/23/20201511 42724 01/20/2020 2316 CAS Analytical Parameter Number Method Result Q LOQ Units Run gamma-BHC (Lindane) 58-89-9 8081B ND 0.00040 mg/L 1 Chlordane 57-74-9 8081B ND 0.0040 mg/L 1 Endrin 72-20-8 8081B ND 0.00040 mg/L 1 Heptachlor 76-44-8 8081B ND 0.00040 mg/L 1 Heptachlor epoxide 1024-57-3 8081 B ND 0.00040 mg/L 1 Methoxychlor 72-43-5 8081B ND 0.0016 mg/L 1 Toxaphene 8001-35-2 8081B ND 0.0080 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Decachlorobiphenyl 88 20-131 Tetrachloro-m-xylene 95 26-132 TCLP Metals Run Prep Method 1 1311/3010A 1 1311/7470A Analytical Method Dilution Analysis Date Analyst 6010D 1 01/23/2020 2000 KSH2 7470A 1 01/22/2020 1603 KSH2 Prep Date Batch Leachate Date 01/22/2020 0955 42552 01/20/2020 2316 01/22/2020 1155 42553 01/20/2020 2316 CAS Analytical Parameter Number Method Result Q LOQ Units Run Arsenic 7440-38-2 6010D ND 0.15 mg/L 1 Barium 7440-39-3 6010D ND 0.25 mg/L 1 Cadmium 7440-43-9 6010D ND 0.050 mg/L 1 Chromium 7440-47-3 6010D ND 0.10 mg/L 1 Lead 7439-92-1 6010D ND 0.10 mg/L 1 Mercury 7439-97-6 7470A ND 0.0020 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 7 of 11 Client:Synagro Laboratory ID:VA16082-001 Description: 2020 Mt. Holly TCLP Matrix: Solid Date Sampled:01/16/2020 0640 % Solids: 1.24 01/17/2020 0106 Date Received:01/16/2020 TCLP Metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3010A 6010D 1 01/23/2020 2000 KSH2 01/22/2020 0955 42552 01/20/2020 2316 1 1311/7470A 7470A 1 01/22/2020 1603 KSH2 01/22/2020 1155 42553 01/20/2020 2316 CAS Analytical Parameter Number Method Result Q LOQ Units Run Selenium 7782-49-2 6010D ND 0.20 mg/L 1 Silver 7440-22-4 6010D ND 0.10 mg/L 1 Footnote(s): 'Paint Filter: 53mL collected; LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 8 of 11 Chain of Custody and Miscellaneous Documents Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 9 of 11 SHEALY ENVIRONMENTAL SERVICES, INC. ,13 J._ E I— F " m Elm r m a r C] M L � co S F � k3 co a qy m v p m 29 cc - � L I a o s�SAmCE�r � S ]7 yp �i x ro � 4V L3 E > m m � 6 $ ID Lp� rr E L 4 E v I� Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 10 of 11 SHEALY ENVIRONMENTAL SERVICES, INC. shrilly Bwimmmimal $ClViuee., rn... nccmnt t3,haduMLE!WI$G].d .Sample Receipt Checklist (SRC) Pf6mieeng9e_a12/1�r��[ GliarD S}na r Gooier ins ecl.rdb 'date,�N UIl1G,2020 140. VA16092 ean$e of receipt: j Sf Client ❑ hill FcdFxEJ Other; WL-JiC _ No I. V1'ere o 6Wd - se'IS greseu( on the caoleo I1�> rda NA 2_ it C1L%qVtr =TF Wel'C 1►rM�sen(, were lh it '2= a.lIJ unbroken? H %ipID; TKA C'Wvrinc Stop 1G' NA Original teFgXrature uPM receipt 1 Derived (ConT tedd) tcrn Pmt1 Lte — Tcs�cd >� NA P upon re ipt °(.' o2id8xwpC�r�II7; l�}-�323 NA I��IA 'G NA INN a Method; �Tert�perature Blank QAgaitl�t 1#Dtll ]R Ga;n FD= 6 alb Gwi Cun=rjon uactor 0 °C ed+s+d afcoalattz R'ctiu'd Paolcs ❑ Diry ice Q Nont — — 0 Yes ❑ No 21 NA 3, !f te"iperaittre of any cooler e_kc"dad 6_i) C3 wEN Pboj eot i�l3rtog�- N obfied? ❑ 'fez FM was Notified by,, phone r' &uail I face-to-face (circle one). No O NA 4. 1s the odnn A-ditT courier's parlaug slip attacked to [his fDinx? Yen ❑ Yes ❑ No 5. Wrll;p pr r Q1w[cjdy prucVdUref (rel uished+rcccived) follou�orl? No 5. L4'� saMp]e CDs llstcd W the COC_? ]fee ❑Tea 7, v4'erc saukPlo 1Dt listed cut al FAmple cDntahwrb? Yes ❑ No R_ Wwr ooflecd m darn &. time ]]sted Yes 0 Y$s Zia on ttLe C 9. Was collactic,n date 8c time ] isted Dn al! sample + um("en:? ❑ Ycs ❑ T'T0 ❑ No 10, Did all mfitainer iahcl uZormatinn (II}_ chat time) agrKc v ith the OOC 1 ] . Vfr'ere Icxtx en berfurrned listed ore the COC' � Tula 12_ Did all ga y arrive in the proper utintailters for each rest and+Dr in gousl oamditiDn (uubrukcn. Inds; oil, ew,)7 ® 1'c9 ❑ No 13. Was adtqwte sample %noluJAe txva a1r1 7 Yes 3Crx ND No 14. Were all samples ret,N-ed within V. the Mlding l Fuv or 49 Tjcurs, whtchever camex first? 15. 4YCr rr sa emplca o0rttsiuer4 ces4 (circle one) sNmplts NQC listed can COC? ❑ Yes ❑ No DNA 16. For VOA ant.[ Fiti.l{-175 samples, Voerc bubbles pi*!AmL �ta-size" (;;°•C, 6UMN ]n dialmetcr) ❑ Yea m any of the VOA vials? -yes 1 o ❑ N NA 1 i_ Wft,c all i' R{1rmcolls,'nutrfent attmples rtceivt:d at a pa of < Z? NA 1$, yVerc 411 ❑ YM4 Q No ide se lei received a t a H > 12 19_ cdle all it 43 + 1'1 7+1 a +p r $nd sulfdo s, Ics � Ec M!d at a p1FI :> 0' 0 1 }„teol 2S ( {t,Stn sa,rarrleR tom., „ae„��i C7 Yes ❑ Nn ETA 2P. Were client femarkg.+requcstx 0^ re Li sted dihitlow, MS!kf&D t1,�;ignatir"5. e(c_.) anrrcfidy h'a]]acrtbcd frown the COC into the crmrnant section in LIMO,? ❑ yer, V" 21, V s the ucrte number ]istcd ort the container IEakael2 !i' Lmw # 1 'A ample hv!wrvatiun (MMt be NNUPleI.Cd for any x3m0a(5) ift4;mT .ctly preserved or With heidspaee.) Swtep]ti(a) NA wee ro�ived incorreotiy�snved and uerG ad]ufitcd acC�rdtn�i+r in 6ample Teceiving with Y, mL of cfkle c,o,G, 112 504, 11NM KC1. NaOR using Sh" # NA Timc of preservahan NA � li'more, than one prLsmative i5 needed, pjmw njDte in the tumntients > tclov._ tllple(s} NA _were received with tar hbles . mm in diattie4cr. Swnples(s) NA Wen receivcd withTRC f 0.5 mg/L(If#19 is Hu}and+�'erc djitbted amordingly in sample recLiviug -nitih sodium thiosW f4lt_ (1fa}S,Da} with srttaly ID; NASTtbQrccFdc]abelsapplicdhy; D]�iN Data Qlr']�r202Q Gar��ocnt�; Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 11 of 11 SECTION 5 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Mount Holly WQ Permit Number: W00001863 WWTP Name: Mt Holly WWTP NPDES Number: NCO021156 Monitoring Period: From 01/01/2020 To 03/31/2020 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Theimophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If an H—hla to alternative nerfarmed !Gins- A nr Class Rl cmmnlete the following monitoring data: yParameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 6a' MPN Coliform power per gram MPN/g Quarterly Grab SM9221C of total solids CFU 58,865 363,788 1,604,887 CFU/g 0 Quarterly Grab SM9222D 1000 MPN per gram of total solids (diy weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) X (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (All- Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 (Injection) Option/Alt. 10 (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification ' 1 ding fine and imprisonment." Doug Shoudt Division Manager Wastewater Z / �7/taS /V Zr •ame and Title (type or print) Lan plier Nle (if applicable) (type or print) ture Pr Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis Synagro 12701 Lancaster Hwy Pineville, NC 28134 Attention: Adam Brigman Project Name: Mt. Holly Biosolids Project Number: 1701 Lot Number:VA16073 Date Completed:01/22/2020 01/23/2020 1:41 PM Approved and released by: Lab Director - Greenville: Lucas Odom Q pCcfto TNN acca� " Eoi B !1 BOo0o eLna The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 vwvw.shealylab.com Page 1 of 13 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative Synagro Lot Number: VA16073 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below. Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" qualifier If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. Fecal Coliform Samples -001 through -007 were pulled out late from the incubator, the results may be biased high even though the plate count for the highest filtration mass is less than 20. Geometric Mean 363,788 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 vvww.shealylab.com Page 2 of 13 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary Synagro Lot Number: VA16073 Sample Number Sample ID Matrix Date Sampled Date Received 001 1 of Fecal Solid 01/16/2020 0646 01/16/2020 002 1 of Fecal Solid 01/16/2020 0646 01/16/2020 003 1 of Fecal Solid 01/16/2020 0646 01/16/2020 004 1 of Fecal Solid 01/16/2020 0646 01/16/2020 005 1 of Fecal Solid 01/16/2020 0646 01/16/2020 006 1 of Fecal Solid 01/16/2020 0646 01/16/2020 007 1 of Fecal Solid 01/16/2020 0646 01/16/2020 (7 samples) Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 3of13 Inorganic non-metals Client:Synagro Laboratory ID:VA16073-001 Description: 1 of 4 Fecal Matrix: Solid Date Sampled:01/16/2020 0646 % Solids: 1.70 01/17/2020 0106 Date Received:01/16/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Fecal Colifo) SM 9222 D-2006 1 01/18/2020 1250 MDD 01/16/2020 2046 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Fecal Coliform-MF SM 9222 D- 131149 20 col/g 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 4of13 Inorganic non-metals Client:Synagro Laboratory ID:VA16073-002 Description: 1 of 4 Fecal Matrix: Solid Date Sampled:01/16/2020 0646 % Solids: 1.81 01/20/2020 2323 Date Received:01/16/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Fecal Colifo) SM 9222 D-2006 1 01/18/2020 1250 MDD 01/16/2020 2023 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Fecal Coliform-MF SM 9222 D- 1019789 20 col/g 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 5of13 Inorganic non-metals Client:Synagro Laboratory ID:VA16073-003 Description: 1 of 4 Fecal Matrix: Solid Date Sampled:01/16/2020 0646 % Solids: 1.93 01/20/2020 2323 Date Received:01/16/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Fecal Colifo) SM 9222 D-2006 1 01/18/2020 1250 MDD 01/16/2020 2023 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Fecal Coliform-MF SM 9222 D- 1604887 20 col/g 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 6of13 Inorganic non-metals Client:Synagro Laboratory ID:VA16073-004 Description: 1 of 4 Fecal Matrix: Solid Date Sampled:01/16/2020 0646 % Solids: 1.87 01/20/2020 2323 Date Received:01/16/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Fecal Colifo) SM 9222 D-2006 1 01/18/2020 1250 MDD 01/16/2020 2023 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Fecal Coliform-MF SM 9222 D- 1014524 20 col/g 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 7of13 Inorganic non-metals Client:Synagro Laboratory ID:VA16073-005 Description: 1 of 4 Fecal Matrix: Solid Date Sampled:01/16/2020 0646 % Solids: 1.84 01/20/2020 2323 Date Received:01/16/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Fecal Colifo) SM 9222 D-2006 1 01/18/2020 1250 MDD 01/16/2020 2023 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Fecal Coliform-MF SM 9222 D- 381181 20 col/g 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 8of13 Inorganic non-metals Client:Synagro Laboratory ID:VA16073-006 Description: 1 of 4 Fecal Matrix: Solid Date Sampled:01/16/2020 0646 % Solids: 2.00 01/17/2020 0106 Date Received:01/16/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Fecal Colifo) SM 9222 D-2006 1 01/18/2020 1250 MDD 01/16/2020 2046 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Fecal Coliform-MF SM 9222 D- 172570 20 col/g 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 9of13 Inorganic non-metals Client:Synagro Laboratory ID:VA16073-007 Description: 1 of 4 Fecal Matrix: Solid Date Sampled:01/16/2020 0646 % Solids: 1.95 01/17/2020 0106 Date Received:01/16/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Fecal Colifo) SM 9222 D-2006 1 01/18/2020 1250 MDD 01/16/2020 2046 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Fecal Coliform-MF SM 9222 D- 58865 20 col/g 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 10 of 13 Chain of Custody and Miscellaneous Documents Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 11 of 13 SHEALY ENVIRONMENTAL SERVICES, INC - - - -------- n Pik D3 � Tli di E CP R05 E8: L,u U L "D -E zM r'- 9 2N' L' .1 Pua4 -W L L �. X Z 9 5 p Z. K3 22 ti A X z ri q 06 > nn -t'-T .L3 FL3 *02ty 73 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 12 of 13 IF 11 13 p se Lr < 6. U 13 a ❑ 0 2 M ir SHEALY ENVIRONMENTAL SERVICES, INC. Shea1yEnvi=fl)Mr I3cr.iems,11Ls D0%;LuiiLaL \vmher M E0018C=14 client: Syn deans of re 2-S W=- Sample Receipt Checklist (SRQ C661-cr impaefind .+date' an the Uhler LotP. VA1{i073 Er.,1 of L E IA.;iuc Dear vmo I � XC%F I IN01h1,4'�'i ^stetl saals were PTWtLt, wee intact and unbirocerp? Strip ID. KA Chlorine Strip ID: LTA Tested by~ A[A Onal terrLp tore uprm receipt f Derived (Carro.tM) tempmture upon moeipt %Solid Snap -Cup ID: 19-3313 `,'2.t LC TEA N-A u�[ KA INA °C NA }NA °C. hod: ®TernPcralure Blank �A inst $oulea fR (;iue 11): 1R (fun Corrmtion Factor- Q o aoet li olarlt W e ❑ ke Packs ❑ © T Dry ke Qmr, ❑ Yea ❑ No Z NA ITf tatnpereluxc of any rc ler excecLW 6,4°C, wan ProjeL=t R4aTL3gcr Noti£ed? I'M was NotiCbd by-- Ii Wt -..+ email ? face -to -fare {pirr,le aete Oy. ❑ Yes © -No NA 4- Is the cominercia! c;rurier's kntg slip atr8w bexl la tl�L� k�tII" Yes Q N n 5- Y4fM proper V43sb]d v proccdtuieLc (TrJi Yes NO IS. W" sample lD5 listed {m the COC? Ycx NO 7. l�r' rz gam }e TDs f isted on all sample OoLitaitiem? yer, No S. Was collection date & time lisocd on the CO ? 19. Yes No Was col l=iolr ddLc & time lixttd OffLill wmpk cantainmPA Yes ❑ No to- Dial ail contai,w label irLCUTMtion QD, date, limn) agree with the CO-? YCs L1 N, 11. v4'ere tests to be prrfarmexl lifted ou t}LC COC! ID Yts ON"I i 12r Did ellmtmpJe& srri4n thT ie propercontainers foreach rest and•'ar in g �,nIitifm uubmlM1k, &14 vn, et4;-)3 h[J )Ies LI No 13- Was adcy¢atc mmpic Volume uvailabl4e'! —Yes No 14. Ware all Sam tes =Cived Within flee hvldkg rime or 48 how's, whichever c:otnes fust7 Y'cs Na 1-5, Wam any aemples corAtaiaers miHLrilig'ea€ceSg circle one naui111es �'Tu4 ]i ttid an C f1C Yes 1b, For VOA and R ialsr? ramples, w bubbles PweLwOT>``n*1Iize'' ('/,"Or 6inm ur dimncter) ❑ ❑ 1'�To ®i�TA in any of d7a ��OA vial�� U 'Yes No ATE, T x. Were all DRO.?Me[aTs?nutrient -,amplcs received at a off of < Z., 0—ye; —CFN-01 60 NAj IS. Wem a]1 c3wicle samples received at a 4i'• T? L-1-.1111- Saft-k lei JtL:C ved '9t a pia ? ❑ Yes 0 o VA 19: Were ILI 4PPICZ1131CNHj !'iC-�Tlcy�n: ?1alLcnp] _5 {� 0-Smg;i l samples flee of rtat aa[ ❑ Yes 0 Na 1'1r1 20. WETC c]ient reMarkalraTI&3 s (i.e. reyur tc€i dilutint, i5'lti1SD de , s�latiinus. etc-..] corre�.tly tiarns"ibcd from the COC ini-0 the comment section in TIMS? _ 4'cs bfa 21. Was die unto number listed ao the aominer labc!? if 21ore # N A :an1pIt Preket-vatf4ii (Must be coropiauxi fur suy samples} in OMCtly przry or wiLh hcadsfaae.) ---plc(s) NA _were r!Mved aricorrcc(1ypmwrved W)dwereadjusbxi accol4jugly� t satv}r1e rcxciv g 7th NA mis of circle Er,c; H- 2SO4, FTN03, HCI, MROH using SR ti AA 'role of pnmserywion NA Tfmom than Ono pmervati�,e is LeedW, please ttolc in IJ,c cxrmments helovr- 9mple(s) ETA +. raeciv�cT u-ith l�ubblcs = 6 men it d;�meter. amRies(a) NAwere rcccivail i !' D.5 mg+'L {Tf #T J is uo ) and were Jjusted accordingly in sawplc Teoeiving with sodium Thiosu[ a[c (Na,52O3) wid, 5llcaly ll]; NA barcode labels applied by- DMN -CammerL : ]bate- 411I0p2G Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 13 of 13 PAF;Z PROMPT•ACCURAT E• RELIABLE LABORATORIES, INC W W W.PARLABS.COM REPORT OF ANALYSES Attn: ADAM BRIGMAN SYNAGRO 12701 LANCASTER HWY PINEVILLE, NC 28134- PROJECT NAME: JAN 20 DATE: 03/03/20 SAMPLE NUMBER- 138175 SAMPLE ID- MT HOLLY 1 OF 4 SAMPLE MATRIX- SO DATE SAMPLED- 01/28/20 TIME SAMPLED- 1000 DATE RECEIVED- 01/29/20 SAMPLER- AB RECEIVED BY- DJ TIME RECEIVED- 1030 DELIVERED BY- AB TYPE SAMPLE- Grab Page 1 of 1 ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS 30 DAY BENCH SCALE TEST VAR 01/29/20 1600 RE 2.18 % LABORATORY DIRECTOR" 2217 Graham Park Drive • Charlotte, NC 28273 Phone: (704) 588-8333 • Fax: (704) 588-8335 PI 1� R PROM PT• A CCU RATE -RE LIABLE LABORATORIES, INC WWW.PARLASS.COM 30 Day Bench Scale Extended Aeration Test Percent Volatile Solids Reduction SYNAGRO • MT HOLLY • 138175 01 /29/20 02/27/20 Start: End: TS () 0.1885 0.1947 TS% 1.92% 1.90% VS () 0.1517 0.1545 VS% 80.48% 79.35% y Mass Fraction of Volatile Solids in Liquid Sludge 0.0154142 0.0150745 x Mass Fraction of Fixed Solids in Liquid Sludge 0.0037392 0.0039223 FSVR (Mass Balance) 2.22% FSVR (Van Kleeck) 2.18% FSVR (Mass Balance) <15% YES FSVR (Van Kleeck) <15% YES P.O. Box 411483 • Charlotte, NC 28241-1483 Phone: (704) 588-8333 • Fax: (704) 588-8335 PLLR PROM PT•ACCU RATE -RE LIABLE LABORATORIES, INC WWW.PARLABS.COM 30 Day Bench Scale Extended Aeration Test VAR Ootion 3. Percent Volatile Solids Reduction CLIENT NAME: Iffa' • SAMPLE ID: • SAMPLE #: START DATE: END DATE: As Received Day 0 Day 7 Day 14 Day 21 Day 28 Collected 01/29/20 01/29/20 02/06/20 02/13/20 02/20/20 02/27/20 D.O. Crucible Tare Wt (g) Sample Wt + Tare Wt (g) Liquid Sludge W1 (g) Oven Temp 'C Date/Time In Date/Time Out Dried Sample W + Tare Wt (g) Dried Sludge Wt (g; Fixed Solids Wt (g Furnace Temp C Date/Time In Date/Time Out Burned Sample Wt + Tare Wt (g Volatile Solids Wt (g) TS% VS% 2.38 3.09 4.11 4.84 5.02 X12 X12 X31 X17 X30 X33 19.3066 19.3066 22.1023 16.9922 18.3469 17.4893 29.1482 29.1482 32.1418 27.3980 28.3652 27.7384 9.8416 9.8416 10.0395 10.4058 10.0183 10.2491 106 106 106 106 106 106 01/29/20 16:00 01/29/20 16:00 02/06/20 09:00 02/13/20 10:05 02/20/20 08:50 02/27/20 09:15 01 /30/20 16:05 01 /30/20 16:05 02/07/20 09:10 02/14/20 09:55 02/21 /20 09:00 02/28/20 09:20 19.4951 19.4951 22.2941 17.1941 18.5393 17.6840 0.1885 0.1885 0.1918 0.2019 0.1924 0.1947 0.0368 0.0378 0.0407 0.0396 0.0402 it 550 550 550 550 550 '� �ii�',��i 02/03/20 08:50 02/07/20 15:15 02/14/20 14:45 02/21/20 15:30 02/28/20 15:45 ��,f„����,�,,� 02/03/20 10:00 02/07/20 15:20 02/14/20 16:00 02/21/20 16:35 02/28/20 16:50 19.3434 22.1401 17.0329 18.3865 17.5295 0.1517 0.1540 0.1612 0.1528 0.1545 1.92% 1.92% 1.91% 1.94% 1.92% 1.90% 80.48% 80.29% 79.84% 79.42% 79.35% yf Mass Fraction of Volatile Solids in Liquid (Feed) Yb Mass Fraction of Volatile Solids in Liquid (Bottom) Sludge at Start of Test 0.0154142 Sludge at End of Test 0.0150745 xf Mass Fraction of Fixed Solids in Liquid (Feed) Sludge xb Mass Fraction of Fixed Solids in Liquid (Bottom) at Start of Test 0.0037392 Sludge at End of Test 0.0039223 TS W1 0.1885 TS 0.1947 VS 0.1517 VS 0.1545 Volatile Fraction In: 1 0.41917 Volatile Fraction Out: 1 0.41763 P.O. Box 411483 • Charlotte, NC 28241.1483 Phone: (704) 588-8333 9 Fax: (704) 588-8335 AR CHAIN OF CUSTODY 480RATORIES. INC. r PAR Laboratories, Inc Phone (704)588-8333 www.parlabs.com Fax (704)-588-8335 Shipping: Mailing: 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28273 Charlotte, NC 28241-1483 It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories. Inc. and the North Carolina Deoadment of Environmental and Natural Resnurces Company Name (billing) Comments/ Special Instructions Clarifier Effluent provided in the event that SYNAGRO CENTRAL Address the sample needs to be reduced to below 12701 LANCASTER HWY 2% solids. City, State Et zip code PINEVILLE NC 28134 Point of Contact Ft Telephone Number ADAM BRIGMAN 704-650-4341 Sample Taken By: SIGNATURE PRINTED NAME 4M a c< rn�r ARE SAMPLES FOR STATE or EPA REPORTING? YES NO *Sample Type: DW WW GWMW HW soil other (. Sample Temp at time of sampling: o C Sample Temp upon receipt: ° C **Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes No n/a Residual Chlorine checked at time of sampling (Y/N): Dechlorination Necessary (Y/N): Client Sample I.D. Sample Location / Number) Comp Grab Preserv. Set Up Date/Time Collection DaterTime Analyses Requested l j i NG'��! 10, q 3C !/G� V" )128�?d/0'o 50 volz 4, h „� 61 Reiinquisneci by i ua ei I t e Received by: uatel l ime I 2 '� G' l C ie 0-% -r 60✓ G� l 't �j - %0 ��O 3 J Relinquished by: v v datedime Received by: Date/Time C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Mount Holly WQ Permit Number: WQ0001863 WWTP Name: Mt Holly WWTP NPDES Number: NCO021156 Monitoring Period: From 04/01/2020 To 06/30/2020 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Theimophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion rf an 1—hle to alternative nPrfarmed !Class A nr Qnss Rl cmmnlete the fnllowing monitoring data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 61h MPN Coliform power per gram MPN/g Quarterly Grab SM9221C of total solids CFU 4560 15,564 110,629 CFU/g 0 Quarterly Grab SM9222D 1000 MPN per gram of total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) X (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 (Injection) Option/Alt. 10 (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the athogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification ' ing fine andd ii 1prisonment." Doug Shoudt Division Manager Wastewater -e OC hap Preparer me and Title (type or print) Land�ppli Name and Ti e (if applicable) (type or print) 2� zi Kio&e o reparer* Date SignaK e of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) 0p 0 PaceAnalyfical Report of Analysis Synagro 12701 Lancaster Hwy Pineville, NC 28134 Attention: Adam Brigman Project Name: Mt. Holly Biosolids Lot Number:VD29011 Date Completed:05/04/2020 NIM�� Mr� 05/06/2020 2:04 PM Approved and released by: Lab Director - Greenville: Lucas Odom Q PCCRBp�� AAW 'ye I ANSI NdmlAccre00- Board eORft Al A C C R E D I T E D TESTING LABORATORY The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC. Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 Tel:803-791-9700 Fax:803-791-9111 www.pacelabs.com Page 1 of 13 PACE ANALYTICAL SERVICES, LLC SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative Synagro Lot Number: VD29011 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Pace policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below. Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' qualifier If you have any questions regarding this report please contact the Pace Project Manager listed on the cover page. Geometric Mean 15,564 Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 vvvvvv.pacelabs.com Page 2 of 13 PACE ANALYTICAL SERVICES, LLC Sample Summary Synagro Lot Number: VD29011 Sample Number Sample ID Matrix Date Sampled Date Received 001 Mt. Holly 2 of 4 Fecal Solid 04/29/2020 0815 04/29/2020 002 Mt. Holly 2 of 4 Fecal Solid 04/29/2020 0815 04/29/2020 003 Mt. Holly 2 of 4 Fecal Solid 04/29/2020 0815 04/29/2020 004 Mt. Holly 2 of 4 Fecal Solid 04/29/2020 0815 04/29/2020 005 Mt. Holly 2 of 4 Fecal Solid 04/29/2020 0815 04/29/2020 006 Mt. Holly 2 of 4 Fecal Solid 04/29/2020 0815 04/29/2020 007 Mt. Holly 2 of 4 Fecal Solid 04/29/2020 0815 04/29/2020 (7 samples) Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 3of13 Inorganic non-metals Client:Synagro Laboratory ID:VD29011-001 Description: Mt. Holly 2 of 4 Fecal Matrix: Solid Date Sampled:04/29/2020 0815 % Solids: 1.66 04/29/2020 2359 Date Received: 04/29/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Fecal Colifo) SM 9222 D-2006 1 04/30/2020 2229 MDD 04/29/2020 2049 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Fecal Coliform-MF SM 9222 D- <4905 20 col/g 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 4of13 Inorganic non-metals Client:Synagro Laboratory ID:VD29011-002 Description: Mt. Holly 2 of 4 Fecal Matrix: Solid Date Sampled:04/29/2020 0815 % Solids: 1.62 04/29/2020 2359 Date Received: 04/29/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Fecal Colifo) SM 9222 D-2006 1 04/30/2020 2229 MDD 04/29/2020 2049 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Fecal Coliform-MF SM 9222 D- 66433 20 col/g 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 5of13 Inorganic non-metals Client:Synagro Laboratory ID:VD29011-003 Description: Mt. Holly 2 of 4 Fecal Matrix: Solid Date Sampled:04/29/2020 0815 % Solids: 1.58 04/29/2020 2359 Date Received: 04/29/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Fecal Colifo) SM 9222 D-2006 1 04/30/2020 2229 MDD 04/29/2020 2049 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Fecal Coliform-MF SM 9222 D- <4695 20 col/g 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 6of13 Inorganic non-metals Client:Synagro Laboratory ID:VD29011-004 Description: Mt. Holly 2 of 4 Fecal Matrix: Solid Date Sampled:04/29/2020 0815 % Solids: 1.55 04/29/2020 2359 Date Received: 04/29/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Fecal Colifo) SM 9222 D-2006 1 04/30/2020 2229 MDD 04/29/2020 2049 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Fecal Coliform-MF SM 9222 D- 19019 20 col/g 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 7of13 Inorganic non-metals Client:Synagro Laboratory ID:VD29011-005 Description: Mt. Holly 2 of 4 Fecal Matrix: Solid Date Sampled:04/29/2020 0815 % Solids: 1.55 04/29/2020 2359 Date Received: 04/29/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Fecal Colifo) SM 9222 D-2006 1 04/30/2020 2229 MDD 04/29/2020 2049 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Fecal Coliform-MF SM 9222 D- 15072 20 col/g 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 8of13 Inorganic non-metals Client:Synagro Laboratory ID:VD29011-006 Description: Mt. Holly 2 of 4 Fecal Matrix: Solid Date Sampled:04/29/2020 0815 % Solids: 1.53 04/29/2020 2359 Date Received: 04/29/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Fecal Colifo) SM 9222 D-2006 1 04/30/2020 2229 MDD 04/29/2020 2049 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Fecal Coliform-MF SM 9222 D- 4560 20 col/g 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 9of13 Inorganic non-metals Client:Synagro Laboratory ID:VD29011-007 Description: Mt. Holly 2 of 4 Fecal Matrix: Solid Date Sampled:04/29/2020 0815 % Solids: 1.60 04/29/2020 2359 Date Received: 04/29/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Fecal Colifo) SM 9222 D-2006 1 04/30/2020 2229 MDD 04/29/2020 2049 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Fecal Coliform-MF SM 9222 D- 110629 20 col/g 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 10 of 13 Chain of Custody and Miscellaneous Documents Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 11 of 13 PACE ANALYTICAL SERVICES, LLC — — �'� ~'�—T—��xx-uhs-.'."•T. it -- 4 o I — I jj sdsAjG/ JaLnn : W {J F , d 7 qlvr't .�. + of dl �� I ; C5 zLdhaZA p It u Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 12 of 13 h 0 R o' a 5 U I 's N ED eq m E � ti x +n S IS c ry � M Nj Er PACE ANALYTICAL SERVICES, LLC bftMlV Envimnm ml Serer. 1� dRtiiw-[rLNuin�„j.�[yjQl3lr'A r�� Inl'I ample Receipt C:1 ecklislt (SRQ bl:Lud'oL' Ante. s'-1�a18 Sample Receipt Checklist �+ Clicnr; S 1rLC RC1 Cooler lu; +ec1.ud 3v{daln. BF1 f (14+'29f2020 :.got 4 VD2901 1 Means it roceipt: [yQ SFST Clicnf UPS ❑ FcdLx Other: n Yr_� ltirl 1_ furc custoev seJ5 Drrgcnt orL ibe coole-7 Yes ira 1 M N A 11, Tf,Lq Ody s—J% -ere prewnt. vrern they+ intact mid u,y,roken? pH Strip Tip: 7tlA Chlorine Strip ID: NA Ter.Nx 6y, NA r rigirEa I ton3}:era41Atc LIPM rrcei ( { 1L)Crived rnrer c -- 1� ( lallj teatplerr�r,+-e upon ncpt °�65[olid &nap -Culp !b; 20-302 1.7 QC 11.7 NA r NA aC NA /NA "C LNA ,+NA L 44 thod; "f nperplture I31mk C]A 'nst 13r7[#!es Ia Gun ID: -6 1R Gun a -i-e.;tiun Fsctor: 0 °C Cti7etF,4d afcruilatllt wet Ice LI IOU Backe n [fir I ❑ ] ane Q Yn �] NO � NA �j� L 3, 1`" [rauporature of a r1oller exceeded d,VC, was Project h1 nager Nolifiad7 PM w as Nod feed by- giant 1 emfi 1 } fac&_1A1.Fkce {c [role Dole). ❑ " s Q No LB NA 4. Is tftie CD}r?tm rcia(caueier's p it l:in�=slip ai.wrhod to thin fora? Y.5; QNu 5, CiUI}CuFerGGSluElyprocedures1l%e1ihruish8dlrECGLY4�d)foliDweO Yrs Flo b. Werc €:ampte JJDs 1is-&don the COC7 `r'eg Q fit* 7. 1Nr+ra sampJa MS listed on all samlrin eonwillurs2 Ysai NO S, Was CnllUtbEI dHtY3& tlrru listed m the COC? Yes ❑ N+l 9, Was r:ul lcw-riail &M &. time listed on aA Fay,pie coaEtuinm? Ye_y 0 No L0, Did all contain" label ;r, r e-ion (11). dj;, time) 8gree 1viLh the CDC? Yes No 11, li are tests to bL: perro"_ed !isle] cL1 the OOC� Yes ❑ N, 12 Did all sample�.arrive in tllc prAprr collininers for each test und; or ih goad >1mi1iri.an '— (trnhrCken, lids on, eat.)? _ 'efE:s ❑off I=_ asadCqu�sam l�volumeat^�11AbJa? .. .� ye No 14. Werea]I 4ALIJPIOx rcce3ved widliW4, the fL[EldingticLc or44 h-Durs,whichever caL:Ies f-jrtir? Yes Na 15. 14 Mo aqy swnple L Co itairre missing+excess (circJa one) sam3lss NuE l islcd ant C ❑ Y-s 0 No ® N' 16. For VOA and RSK•17.9 .4ampie9. ware bubbles Present>`E ra-si "C/,por GrnLtt in iiamete-}-} in any of I h,7 VGA viaJs7 Q Yes No NA, 17_ veers au kb?j el;Lls{nut:ient sarnplcs reoeiw4d at a nH afr �? Yes �] ]�To NA [$. el'e �][ rya�ide sam 11. rcCivrd at a [a�j ?2 871d sulfic[t sam les r�CBitcEl ar a H } 97 4, Vk`L1d �If.app �cpblc NIIa1T _ {cyHni{{e7phYaa 2S( 0.1nigf _ sarnpics fief ofresid"isI ❑ Yes Frio �R' chla�riofe? ❑ Yes ONo 0 NA Llrt clrerf r nrarks{_NIts 0, 0. r_questcddilur ions, h1S,'Mi=D cJcsi�l ti k1ts, eic,,,) rotrec[ly lrarrucrtb from tf c C:W into the+:o111L'11Liierden in 1_1[4TS:1 ❑ "E'es i`Ja 1. Was t11C uVi nlunber listed on tEtie cp�1#ai:ae,' Isba1,' If s uole NA ample Preyervat'eun {Must be uurnpieted 1'or any' s; tnpJeW insorreclfy' }uesarv:•d or With hepLispace_ i sw _were recelvod inch-rectly preseL ed and xcrc� adiufils i accnrawly sa7nplc receivirl wish 1A nil.ofpircla One: H2SO4, HNO3, HOJ,1N'aOH using SR NA -nc afprewcrvatio,E NA If mare Aran MG preservatirc is needed, plea6u RODE in [he. cE�rurnerttx Jlrlaw. .npJe(4) NA _w2r&mo&ivrxl witfl Nibbles 7�-6 ram ;r dim neu, -np[eb(s) NA ~ � —were raxivad -witli ,5 nld'L ;[f # 14 is ►ro) And vE wir 11%W acuvrdingly [in sFanpin roceiving with sodium thiosulfa+x mith SJleaJy ID: NA Ltaratxdc lahrls applied iav_ JSf[ Dar&, 04+2W0 Comments, Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 13 of 13 AM PACI R PROM PT•ACCU RATE -RE LIABLE LABORATORIES, INC WWW.PARLABS.COM REPORT OF ANALYSES Attn: ADAM BRIGMAN SYNAGRO 12701 LANCASTER HWY PINEVILLE, NC 28134- PROJECT NAME: APR 20 DATE: 06/19/20 SAMPLE NUMBER- 138849 SAMPLE ID- MT HOLLY 2 OF 4 SAMPLE MATRIX- SO DATE SAMPLED- 04/29/20 TIME SAMPLED- 1000 DATE RECEIVED- 04/30/20 SAMPLER- AB RECEIVED BY- DJ TIME RECEIVED- 0824 DELIVERED BY- AB TYPE SAMPLE- Grab Page 1 of 1 ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS 30 DAY BENCH SCALE TEST VAR 04/30/20 1630 RE 3.79 % LABORATORY DIRECTOR 2217 Graham Park Drive • Charlotte, NC 28273 Phone: (704) 588-8333 • Fax: (704) 588-8335 RbLF;Z PROMPT•ACCURA-rE• RELIABLE LABORATORIES INC WWW.PARLABS.COM 30 Day Bench Scale Extended Aeration Test Percent Volatile Solids Reduction SYNAGRO • MT HOLLY 2 OF 4 138849 04/30/20 06/04/20 Start: End: TS () 0.0890 0.1094 TS% 0.90% 0.91 % VS () 0.0696 0.0814 VS% 78.20% 74.41 % y Mass Fraction of Volatile Solids in Liquid Sludge 0,0070374 0.0067706 x Mass Fraction of Fixed Solids in Liquid Sludge 0.0019616 0.0023289 FSVR (Mass Balance) 3.78% FSVR (Van Kleeck) 3.79% FSVR (Mass Balance) <15% YES FSVR (Van Kleeck) <15% YES P.O. Box 411483 Charlotte, NC 28241-1483 Phone: (704) 588-8333 • Fax: (704) 588-8335 PLLR PROM PT•ACCU RATE RELIABLE LABORATORIES, INC W W W. PARLABS.COM Collected D.O. Crucible Tare Wt (g) Sample Wt + Tare Wt (g) Liquid Sludge WI (g) Oven Temp °C Date/Time In Date/Time Out Dried Sample Wl + Tare Wt (g) Dried Sludge Wt (g) Fixed Solids Wt (g) Furnace Temp °C Date/Time In Date/Time Out Burned Sample Wt + Tare Wt (g) Volatile Solids Wt (g) TS% VS% 30 Day Bench Scale Extended Aeration Test VAR Ontion 3 Percent Volatile Solids Reduction SYNAGRO MT HOLLY 2 OF 4 138849 04/30/20 06/04/20 As Received Day 0 Day 7 Day 14 Day 21 Day 28 nd/3n/2n nF/n7/2n nF/14i2n n5/2v2n n5/2wn n6/n412n 3.60 4.11 4.80 4.86 5.32 X8 X35 X6 X15 X32 X19 24.7161 18.7316 16.2948 23.1836 24.4290 22.6254 32.3113 28.6216 26.5265 33.4343 34.6692 34.6480 7.5952 9.8900 10.2317 10.2507 10.2402 12.0226 105 106 106 106 105 106 04/30/20 16:30 05/07/20 08:45 05/14/20 09:20 05/21/20 09:30 05/28/20 08:55 06/04/20 09:00 05/01/20 16:30 05/08/20 09:00 05/15/20 09:15 05/22/20 10:00 05/29/20 09.40 06/05/20 09:10 24.9267 18.8206 16.3869 23.2769 24.5222 22.7348 0.2106 0.0890 0.0921 0.0933 0.0932 0.1094 0.0194 0.0213 0.0222 0.0228 0.0280 550 550 550 550 550 05/08/20 15:50 05/15/20 15:10 05/22/20 14:55 05/29/20 16:05 06/05/20 15:00 05/08/20 17:00 05/15/20 16:05 05/22/20 16:00 05/29/20 17:15 06/05/20 16:10 18.7510 16.3161 23.2058 24.4518 22.6534 0.0696 0.0708 0.0711 0.0704 0.0814 0.90% 0.90% 0.91% 0.91% 0.91% 62.77% 78.20% 76.87% 76.21% 75.54% 74.410/. yf Mass Fraction of Volatile Solids in Liquid (Feed) yb Mass Fraction of Volatile Solids in Liquid (Bottom) Sludge at Start of Test 0.0070374 Sludge at End of Test 0.0067706 Xf Mass Fraction of Fixed Solids in Liquid (Feed) Sludge Xb Mass Fraction of Fixed Solids in Liquid (Bottom) at Start of Test 0.0019616 Sludge at End of Test 0.0023289 TS 0.089 TS 0.1094 VS ) 1 0.0696 VS 0.0814 Volatile Fraction In: 1 0.86889 Volatile Fraction Out: 1 0.81769 P.O. Box 411483 • Charlotte, NC 28241-1483 Phone; (704) 588-8333 • Fax; (704) 588-8335 LLAR CHAIN OF CUSTODY 480PATORIES.INC. PAR Laboratories, Inc _ Phone (704) 588-8333 www.pariabs.com Fax (704)-588-8335 Shipping: Mailing: 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28273 Charlotte, NC 28241-1483 It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc. and the North Carolina Department of Environmental and Natural Resources. Company Name (billing) Comments/ Special Instructions SYNAGRO CENTRAL Clarifier Effluent provided in the event that Address the sample needs to be reduced to below 12701 LANCASTER HWY 2% solids. City, State Ix zip code PINEVILLE NC 28134 Point of Contact 8 Telephone Number ADAM BRIGMAN 704-650-4341 Sample Taken By: SIGNATURE PRINTED NAME 1fdo it & r'i(mo l ARE SAMPLES FOR STATE or EPA REPORTING? YES NO *Sample Type: DW WW GWMW HW soil other ✓ Sample Temp at time of sampling: ° C Sample Temp upon receipt: ° C **Field Preserved: Yes I/No _Teflon Liner/Zero Headspace: Yes No n/a Residual Chlorine checked at time of sampling (YIN): Dechlorination Necessary (YIN): Client Sample I.D. Sample Location / Number) Comp Grab Present. Set Up Date/Time Collection Date/Time, Analyses Requested NL Ho (I 2d q 30 A ✓ �/Za � ;o:� �0 �, 13���i ��� err mulnigwaneu uate I rme rc Ive y-. vale I Ime A;zY ��=3o-�v l Relinqui Datemme Received by: Date rime * C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Mount Holly WQ Permit Number: WQ0001863 WWTP Name: Mt Holly WWTP NPDES Number: NCO021156 Monitoring Period: From 07/01/2020 To 09/30/2020 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. l/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If annlicable to alternative nerformed Class A or Class B complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 6th MPN Coliform power per gram MPN/g Quarterly Grab SM9221 C of total solids CFU 5,755 7,644 9,032 CFU/g 0 Quarterly Grab SM9222D 1000 MPN per gram of total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) X (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 (Injection) Option/Alt. 10 (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certificatioXot, ing fine and imprisonment�Yy Doug Shoudt Division Manager Wastewater A, SV Preparer Name and Title (type or print) Land A�l�ame and Title (if applicable) (hype or print) �Signnature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Analytical Results Synagro 284 Boger Rd. Mocksville, NC 27028 Receive Date: 07/16/2020 Reported: 07/20/2020 For: Mt Holly Comments: STATESVI LLE ANALYTICAL 4i Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 200716-30-01 Fecal Coliforms 1 9032 MPNIg SM92210E-2008 07/17/2020 WC 200716-30-01 Percent Solids 1 1.55 % SM25408-2011 07/17/2020 WC 200716-30-02 Fecal Coliforms 2 7965 MPNIg SM92210E-2006 07/17/2020 WC 200716-30-02 Percent Solids 2 1.13 % SM254OB-2011 07/17/2020 WC 200716-30-03 Fecal Coliforms 3 6000 MPNIg SM92210E-2006 07/17/2020 WC 200716-30-03 Percent Solids 3 1.50 % sM2546B-2011 07/17/2020 WC 200716-30-04 Fecal Coliforms 4 6164 MPNIg SM92210E-2006 07/17/2020 WC 200716-30-04 Percent Solids 4 1.46 % SM254OB-2011 07/17/2020 WC 200716-30-05 Fecal Coliforms 5 8462 MPNIg SM92210E-2006 07/17/2020 WC 200716-30-05 Percent Solids 5 1.30 % SM25403-2011 07/17/2020 WC 200716-30-06 Fecal Coliforms 6 8824 MPNIg SM92210E-2006 07/17/2020 WC 200716-30-06 Percent Solids 6 1.36 % SM254OB-2011 07/17/2020 WC 200716-30-07 Fecal Coliforms 7 5755 MPNIg SM92210E-20M 07/17/2020 WC 200716-30-07 Percent Solids 7 1.39 % SM2540B-2011 07/17/2020 WC Respectfully submitted, rOP,.-vt/% J'")t Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 Condition of Receipt Sample Number 200716-30-01 Temp on Arrival: 3.2 Parameter Schedule: Percent Solids Received on ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on ice Sample Number 200716-30-02 Temp on Arrival: 3.2 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 200716-30-03 Temp on Arrival: 3.2 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 200716-30-04 Temp on Arrival: 3.2 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 200716-30-05 Temp on Arrival: 3.2 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 200716-30-06 Temp on Arrival: 3.2 PO Sox 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 4 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 200716-30-07 Temp on Arrival: 3.2 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 4 Client 4'r PIV I L ; F AN,-UYliCAL 122C0UrTStrW - P.0_Nx228 '77 Address: 4 L Statesville, NC 29697 (704) 872-4697 Contact Person: Phone # FAX# x IILI-I Chain of Custody Record PO # Requisitioned by: J (rin-ra Dale) Customer Sample IDN Lab-IDIt Time mpled (Graol(anly) Date (Grab Only) ED Malrix Parnmcrers mqueqM foran.T36i, SWO. I1 Vd I W, "7 7 022 1 Pyl� 7 t-IM 0 Relinquished by; Time am, pm Date Sampled by: Received by: Tme am, ODatO Transported by Relinquished by: Time am, pm Date __j_L_ Holding times met: Received by: Time am, pm Date ry Compliance work: Composite Sampling #11: Time begin -am, pm Date Non-compliance work:_ Time end am, pm Date Lab CzrnrnenI& Samples Transported on ice: Composite Sampling 42. Time begin -am, pinn Date _j_,__I_ Time end am, pm Date __j --- Inifials: r- 00 k.0 00 rI4 U Analytical Results Synagro 284 Boger Rd. Mocksville, NC 27028 Receive Date: 07/16/2020 Reported: 08/27/2020 For: Mt Holly Comments: STATESVILLE ANALYTICAL f Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 200716-31-01 30 Day Benchscale Mt Holly Respectfully submitted, u Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 32 EPA625-R-92/0 07/16/2020 WC PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 Condition of Receipt Sample Number 200716-31-01 Temp on Arrival: 3.2 Parameter Schedule: Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 4 Client: IRA "TATFSVIt# if ANALYTICAL 122 Court Street • PA. Box 228 Address: ( �. 1 l_ _. +� Statesville, NC 28687 #b (704) 872 d6g7 Chain Contact Person: Phone # •' FAX# 94 /- —�j�: s � .: � of Custody Record PO # Requisitioned by: j' (nme Date) Customer Sample ID# Lab-lD Time Sampled (Grab Only) Date Sampled (Grab Only) Matrix Parameters requested For analysis sew9e w wvu Pill o-2- VV — Fn� t i1 , P Relinquished by: ? Time am, pm Date /!_ Sampled by: Received by: _ ��� Time f '(ram am„aate _7f1 161Z? Transported by: Relinquished by: Time am, pm Date, /_/_ Holding times met: Received by: Time am, pm Date I 1 - -__ Compliance work: Composite Sampling_#1: Time begin am, pm Date!__. / Non-compliance work: Time end am, pm Date -- Lab Comments: Samples Transported On Ica: Composite Sampling #2: Time begin am, pm Date Time end am, pm Date Initials: rn Q0 N O M 00 N O a- n n 00 t.O 00 N U Ln tv ro U0 00 N N X O m O a 30 Day Bench Worksheet WEEK 1 Sample 1D # MCI { U - J I.01 Samples Total Solids Volatile Solids % Volatile Fraction 10--7115 2 0-51 0 - -;5r� 0. (003 3 7 Average: t WEEK 2 OKOa.L12Mw IOM 0 Fol 9 / :i ffi%� WEEK 3 Samples Total Solids Volatile Solids % Volatile Fraction 1 2 -1 (076 3 i 7 Average: 2% WEEK 4 Samples Total Solids Volatile Solids % Volatile Fraction 1 z 2 . 57 Average: 0.35 0.2 2 WEEK 5 Samples Total Solids Volatile Solids % Volatile Fraction 1 7 0 -1 2 0 1 215 0,1-7 3 2 i .-T YO Average; Q• 1'1 WEEK 6 Samples Total Solids Volatile Solids % Volatile Fraction 1 -27 Q. 1-7 2 3 0.7 Avera e: 0 - 17Cr 0 - I b. +WVI 3 c). -1 I SU - 6. V213 I t00 0. W3 Van Kleeck Reduction: Initial % Vol. Frac. - Final % Vol. Frac. X 100 = % Initial % Vol. Frac. — ( Initial % Vol. Fr(aap X Final % Vol. Frac.) 2 FINAL RESULT 32 % PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 4 %VS R (older, more conservative method) %VS in 0.7126 Enter in VS out t 0.6273 decimal form %VSR= (%VS in - %VS out) ((%VS in - (%VS in x %VS out)) %VSR= 32.12 (method from p.132 of WH manual) %VSR= (%VS in - %VS out) %VS in ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Mount Holly WQ Permit Number: WQ0001863 WWTP Name: Mt Holly WWTP NPDES Number: NCO021156 Monitoring Period: From 010/01/2020 To 12/31/2020 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If nnnlicable to alternative performed (Class A or Class B) comnlete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 61h MPN Coliform power per gram MPN/g Quarterly Grab SM9221 C of total solids CFU 29,590 81,619 308640 CFU/g 0 Quarterly Grab SM9222D 1000 MPN per gram of total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) X (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying —Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification in ng fine an, lLimprisonment. A'/ems Doug Shoudt Division Manager Wastewater Preparer Name and Title (type or print) Lan plier Name and Title (if applicable) (type or print) SiWaturel& Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Analytical Results Synagro 284 Boger Rd. Mocksville, NC 27028 Receive Date: 10/08/2020 Reported: 10/09/2020 For: Mt Holly Comments: GEOMETRIC MEAN: 81619 MPN/g STATESVILLE ANALYTICAL „ Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 201008-21-01 Fecal Coliforms 1 94970 MPN/g SM92210E-2006 10/08/2020 WC 201008-21-01 Percent Solids 1 1.79 % SM2540B-2011 10/08/2020 WC 201008-21-02 Fecal Coliforms 2 78650 MPN/g SM92210E-2006 10/08/2020 WC 201008-21-02 Percent Solids 2 1.78 % SM2540B-2011 10/08/2020 WC 201008-21-03 Fecal Coliforms 3 29590 MPN/g SM92210E-2006 10/08/2020 WC 201008-21-03 Percent Solids 3 1.69 % SM2540B-2011 10/08/2020 WC 201008-21-04 Fecal Coliforms 4 46510 MPN/g SM92210E-2006 10/08/2020 WC 201008-21-04 Percent Solids 4 1.72 % SM2540B-2011 10/08/2020 WC 201008-21-05 Fecal Coliforms 5 101800 MPN/g SM92210E-2006 10/08/2020 WC 201008-21-05 Percent Solids 5 1.67 % SM2540B-2011 10/08/2020 WC 201008-21-06 Fecal Coliforms 6 308640 MPN/g SM92210E-2006 10/08/2020 WC 201008-21-06 Percent Solids 6 1.62 % SM2540B-2011 10/08/2020 WC 201008-21-07 Fecal Coliforms 7 74710 MPN/g SM92210E-2006 10/08/2020 WC 201008-21-07 Percent Solids 7 1.74 % SM2540B-2011 10/08/2020 WC 201008-21-08 30 Day Benchscale Mt. Holly % EPA625-R-92/0 Respectfully submitted, vojz n- �M� ') Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 Condition of Receipt Sample Number 201008-21-01 Temp on Arrival: Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 201008-21-02 Temp on Arrival: Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 201008-21-03 Temp on Arrival: Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 201008-21-04 Temp on Arrival: Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 201008-21-05 Temp on Arrival: Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 201008-21-06 Temp on Arrival: PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 4 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 201008-21-07 Temp on Arrival: Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 201008-21-08 Temp on Arrival: Parameter Schedule: Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 4 N N �cU.. �:• .� U 3 N J a w E C) a o` wn W C 'O C E on CL p Z n. U .Y. CQ.. N n Ge� C E C m U Z F N �" $ � AI I c R! Y 0 0 �.. u C1 CL C1 X lQL E E E E m m m R7 c * !\ v Q) (D m E c E E � H F J a m 00 - ... O E c 90 Q o 0' .0 a 4) I az . j- � N , E F 1� m cc 00 o E E E E Q Q LC c Nyr IE 2'C a > -D m -0 mwE C N N m £. d 4) N T3 a C Q E DJ v Q) E '� Q E E c� U IL ¢ i= P c� i= P- PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 4 Analytical Results Synagro 284 Boger Rd. Mocksville, NC 27028 Receive Date: 10/08/2020 Reported: 11 /30/2020 For: Mt Holly Comments: GEOMETRIC MEAN: 81619 MPN/g STATESVILLE ANALYTICAL „ Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 201008-21-01 Fecal Coliforms 1 94970 MPN/g SM92210E-2006 10/08/2020 WC 201008-21-01 Percent Solids 1 1.79 % SM2540B-2011 10/08/2020 WC 201008-21-02 Fecal Coliforms 2 78650 MPN/g SM92210E-2006 10/08/2020 WC 201008-21-02 Percent Solids 2 1.78 % SM2540B-2011 10/08/2020 WC 201008-21-03 Fecal Coliforms 3 29590 MPN/g SM92210E-2006 10/08/2020 WC 201008-21-03 Percent Solids 3 1.69 % SM2540B-2011 10/08/2020 WC 201008-21-04 Fecal Coliforms 4 46510 MPN/g SM92210E-2006 10/08/2020 WC 201008-21-04 Percent Solids 4 1.72 % SM2540B-2011 10/08/2020 WC 201008-21-05 Fecal Coliforms 5 101800 MPN/g SM92210E-2006 10/08/2020 WC 201008-21-05 Percent Solids 5 1.67 % SM2540B-2011 10/08/2020 WC 201008-21-06 Fecal Coliforms 6 308640 MPN/g SM92210E-2006 10/08/2020 WC 201008-21-06 Percent Solids 6 1.62 % SM2540B-2011 10/08/2020 WC 201008-21-07 Fecal Coliforms 7 74710 MPN/g SM92210E-2006 10/08/2020 WC 201008-21-07 Percent Solids 7 1.74 % SM2540B-2011 10/08/2020 WC 201008-21-08 30 Day Benchscale Mt. Holly 5.2 % EPA625-R-92/0 10/08/2020 WC Respectfully submitted, vojz n- �M� ') Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 5 Condition of Receipt Sample Number 201008-21-01 Temp on Arrival: 5.0 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 201008-21-02 Temp on Arrival: 5.0 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 201008-21-03 Temp on Arrival: 5.0 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 201008-21-04 Temp on Arrival: 5.0 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 201008-21-05 Temp on Arrival: 5.0 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 201008-21-06 Temp on Arrival: 5.0 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 5 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 201008-21-07 Temp on Arrival: 5.0 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 201008-21-08 Temp on Arrival: 5.0 Parameter Schedule: Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 5 v O W 0 x N N 00 arti Z n N 00 Ol 00 Client: A N A LY1 Y »- AL AT 122 Cnurt Street P.O.228 opts \r Statesville, NC 28687 87 (704) Chain of Custody Record Address: c7� / - - DG SY, _ �(� Contact Person: �x Phone # zy G� _ FAX# 7VT-I" PO # Requisitioned by: (Tlme _ Dale) Customer Semple ID# Lab -ID 0 Time Sampled (Grab Only) Date sampled (Grab Only) Matrix Udge iro vnru Yammetm. requested for analysis /17 r t 02 � t1 S 03 �1 �( 05 a4 Relinquished by: l Time �% , fS am, pm Dater_ Sampled by: Received by: !A Timelf� am, pm Date Transported by: Relinquished by: Time _ am, pm Date �hl— Holding times met: Received by: Time am, pm Date ! 1 Compliance work: Composite Sam link a #1: - Time begin am, pm Date Ii Non-compliance work: Time end am, pm Date / /_ - Lab Comments: Samples Transported on Ice: Composite Sampling #2: Time begin am, pm Date tI_ Time end am, pm Date / __ Inttlals: 30 Day Bench Worksheet WEEK I Sample ID #� i �;�• 2I ��� Samples I Total Solids Volatil Solids % Volatile Fraction 1 0..Uu C. 2 1 0.4110 3 LJ. -Average: WEEK 2 Samples i Total Solids Volatile Solids % Volatile Fr ction 1 C.� ? 0. ocl to If 2 . 15 . __�7 3 . 15 3 1 Average:(06151 WEEK 3 Samples I Total Solids Volatile Solids % Volatile Fraction 1 i ) 2 [j 3. Avera e: 6 WEEK 4 Samples I Total Solids Volatil Solids % Volatile lFraction .— 1 -� 2 I 3 �i _ -Average: �C� WEEK 5 Samples I Total Solids Volatile Solids % Volatile Fraction 1 W 5 ' 2 3 0. 5 1_0. 3_1 5 -Average: f I , WEEK 6 Samples Total Solids Volatile Solids % Volatile Fraction 1 () . 2 p_ 3' 3 S��E 1 �. -Average: ( i Van Kleeck Reduction: Initial % Vol. Frac. - Final % Vol. Frac. X 100 = % Initial % Vol. Frac. — ( Initial % Vol. Frac. X Final %!VaoJl. Frac.) FINAL RESULT 5.2 % 0- 7-2-Iq ',5"2 01 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 5 SECTION 6 Agricultural Lime Application Log Year: 2020 Project: MT Holly Field (state -county -site -field) Soil pH Lime Requirement (from soil analysis) Tons/Acre Applied(CCE Eq.) Date Applied GA-41-1 6.5 0.0 T/Ac. LT-46-1 6.2 0.0 T/Ac. LT-46-2 6.9 0.0 T/Ac. LT-46-3 6.1 0.0 T/Ac. LT-46-4 6.0 0.0 T/Ac. LT-46-5 6.1 0.0 T/Ac. LT-46-7 5.8 0.4 T/Ac. LT-46-8 6.1 0.0 T/Ac. MG-37-1 5.8 0.4 T/Ac. GA-41-6 GA-41-14 6.3 6.0 0.0 T/Ac. 0.0 T/Ac. * Lime is ordered and be spread soon SECTION 7 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY21-SL005771 Client: Greg Springs Advisor: Alex Fox vo- Predictive 410 West Catawba Ave Synagro Mount Holly, NC 28120 284 Boger Rd .'..,$' Soil Report Mehlich-3 Extraction Mocksville, NC27028 _ Sampled County: Gaston Links to Helpful Information Client ID: 452256 Advisor ID: 501947 Sampled: 09/22/2020 Received: 09/24/2020 Completed: 10/02/2020 Farm: GA-1 Sample ID: 1 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 0 90 0 0 pH$ 0 0 0 Note: 12 Note: 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.41 1.02 12.1 93 0.8 6.5 101 25 65 27 86 155 102 521 521 494 0.2 2 Sample ID: 6 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 90 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.56 0.96 12.3 92 1.0 6.3 127 26 65 26 84 132 91 621 621 532 0.2 2 Sample ID: 14 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 80 100 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.46 1.02 7.6 83 1.3 6.0 25 21 61 20 58 963 595 174 174 283 0.2 3 North Carolina r Tobww Trust FwW C47mmisslan Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Aqriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY21-SL005771 Greg Springs Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn- mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htn*fsfind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index Zn-1 zinc index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwncagr.gov/agronomi/uvrst.htm NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY21-SL005776 Client: Alex Fox Advisor: Alex Fox vo- Predictive Synagro Synagro 284 Boger Rd 284 Boger Rd :...,$� Soil Report Mehlich-3 Extraction Mocksville, NC27028 Mocksville, NC27028 Links to Helpful Information Sampled County: Lincoln Client ID: 501947 Advisor ID: 501947 Sampled: 09/22/2020 Received: 09/24/2020 Completed: 10/08/2020 Farm: Lt-46( Tony Jones) Sample ID: 1 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 120 60 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.18 1.05 6.1 87 0.8 6.2 10 37 56 28 110 101 75 37 37 77 0.1 2 Sample ID: 7 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.3 120-200 90 90 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.18 0.94 7.7 84 1.2 5.8 20 23 62 21 138 557 351 108 108 217 0.2 3 Sample ID: 3 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 110 60 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.22 1.01 8.6 88 1.0 6.1 12 37 61 25 50 678 422 116 116 143 0.1 1 North Carolina r Tobww Trust Fw►d C47mmisslan Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Aqriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY21-SL005776 Alex Fox Page 2 of 3 Sample ID: 8 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 120 90 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.36 1.05 5.7 87 0.7 6.4 10 26 58 27 72 216 141 45 45 68 0.1 2 Sample ID: 5 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 90 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.46 1.01 8.7 85 1.3 6.1 89 24 68 15 59 323 210 325 325 419 0.2 2 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY21-SL005776 Alex Fox Page 3 of 3 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn- mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htn*fsfind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index Zn-1 zinc index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwncagr.gov/agronomi/uvrst.htm NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY21-SL011137 �5{i �141..tiL Client: Tony Jones Advisor: Synagro Predictive 1418 Nature Preserve Trl. Synagro ;• Denver, NC 28037 284 Boger Rd. +_ Soil Report Mehlich-3 Extraction Mocksville, NC 27028 Sampled County: Lincoln Links to Helpful Information Client ID: 272840 Advisor ID: 503079 Sampled: 10/23/2020 Received: 10/28/2020 Completed: 11/12/2020 Farm: LT-46 Sample ID: 2 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 20 0 0 0 pH$ 0 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.51 0.99 10.0 96 0.4 6.9 52 129 65 24 74 689 417 429 429 397 0.1 1 Noah Carolina Futaw frum Fund Ciwn1nl55km Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Aqriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY21-SLO11137 Tony Jones Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn- mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htn*fsfind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index Zn-1 zinc index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwncagr.gov/agronomi/uvrst.htm Page 1 of 1 Report No: 21-004-0510 Account No: 12259 Advisor: Synagro/Columbus NC Mary Brewer 284 Boger Rd Mocksville NC 27028 Waypoint'(D ANALYTICAL Client: Tony Jones 2020 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Farm: U-46 Date Received:01/04/2021 Date of Report: 01/05/2021 Lab No Field ID Sample ID Soil Class HM% W/V pH Ac P-1 K-1 S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 CEC BS% Ca% Mg% ESP Na 109898 4 MIN 1.2 6.0 0.7 13 16 27 88 70 0 130 130 30 4.4 84 51 30 1.2 0.1 Crop Recommendations: Rec Uom Lime (Vacre) N P205 K20 S Mn Zn Cu B Mg Last Crop 1- Fescue Hay Ib/acre 0.5 150 111 109 20 0 0 0 0 0 Comment: Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/V in g/cm3 North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc. NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY21-SL005773 �5{i �141..tiL Client: Nathan Thomsen Advisor: Alex Fox Predictive 111 Heart Wood ct Synagro ;• Clayton, NC 27527 284 Boger Rd Soil Report Mehlich-3 Extraction Mocksville, NC 27028 Sampled County: Mecklenburg Links to Helpful Information Client ID: 482907 Advisor ID: 501947 Sampled: 09/22/2020 Received: 09/24/2020 Completed: 10/02/2020 Farm: MG-37 Sample ID: 1 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.4 120-200 50 10 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.41 0.98 8.4 84 1.4 5.8 37 72 53 27 71 353 229 312 312 265 0.1 1 Noah Carolina fdtaw frum Fund Ciwn1nl55km Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Aqriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY21-SL005773 Nathan Thomsen Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn- mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htn*fsfind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index Zn-1 zinc index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwncagr.gov/agronomi/uvrst.htm