WQ0041666_2020 Residual Annual Report_20210216

Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?* r Annual Report
r Residual Annual Report
r Additional Information
r Other
Annual Report Year* 2020
Permit Number (IR)* W00041666
Applicant/Permittee EMA Resources, Inc.
Email Notifications
Does this need review by the hydrogeologist?* 0 Yes r No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Rease provide information on the person to be contacted by N B Staff
Name * Brent Collins
Email Address*
[e-mail]
electronic subnittal, confirmation of receipt, and other correspondence.
Project Information
........ ......... .......................................................................................................................
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
3367511441
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* WQ0041666
Fbs Current Existing permt number
Applicant/Permittee Address* 755 Yadkinville Rd, Mocksville, NC 27028
Facility Name * EMA Resources DCAR
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Specifications, Calculations, Rc.)
2020 EMA Resources Inc. Annual Report -
3.2MB
WQ0041666.pdf
Upload only 1 PCF docurrent (less than 250 M3). Maniple docurrents must be combined into one R7F file unless file is larger than
upload linit.
* W By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
o 0041, W
Submission Date 2/16/2021

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
VQ PERMIT #: WQ0041666 FACILITY NAME: Lear Corp.
PHONE: [phone] COUNTY: Davie OPERATOR: EMA Resources Inc.
FACILITY TYPE (please check one):
❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
® Distribution and Marketing (complete Parts A, B, and C)
'as the facility in operation during the past calendar ear? Yes El No ❑ --lo- If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tans)
Recipient Information
Amendment/
Bullring Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
inuar
:bruary
arch
pril
ay
Inc
i ly
ugust
ptember
ctober
)vember
member
Total from FORM DMSDF (sup)
U
138.8
138.8
138.8
rtals: I Annual (dry tons):
0
138.8
138.8 11
138.8
Amendments used:
1
Bulking Agent s used:
(supp)): Total Number of Form DMSDF (Supp) 0
If more space is required, attach additional information sheets (FORM DMSDF
in C:
icility was compliant during the past calendar year with all conditions of the land application permit 0 Yes
acluding but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No lo If No, Explain in Narritive
All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
No contravention of Ground Water Quality Standards occurred at a monitoring well.
certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
malties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2��4 R&rr�u-e �-LS21
gnature of Permittee I ate
"Preparer is defined in 40 CFR Part 503 9(r) and 15A NCAC 2T .1102 (26)
Signature of Preparer**
(if different from Permittee)
Date

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: WQ0041666 FACILITY NAME: Lear Corp.
PHONE: [phone] COUNTY: Davie OPERATOR: EMA Resources Inc.
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
❑ Distribution and Marketing (complete Parts A, and B)
Part A*:
Part B*:
Month
Sources(s) (include NPDES 1i if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
July
City of Reidsville WTP
72.27
72.27
Ronnie Marshall
72.27
Soil Amendment
November
City of Reidsville WTP
66.53
66.53
Ronnie Marshall
66.53
Soil Amendment
Totals:
Annual (dry tons):
0
138.8
138.8 138.8
Amendment(s) used: I Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)l I
DENR FORM DMSDF (Supp) (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0041666 Laboratory: 1) Waypoint Analytical
Facility Name: Lear Corp. 2)
Residual Source WQ # or NC0002305 3)
NPDES #: 4)
WWTP Name: Lear Corporation WWTP 5)
Residual Analysis Data
Parameter
Limit
Sample or Composite Date
Molybdenum
TotalConc.
• . •
' • 1
-----------
Nitrate and Nitrite
' For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Z-le 4;510 - 2/16/2021
Signature of Preparer *
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
WQ0041666
Facility Name: Lear Corp.
Residual Source
NPDES # or WQ#:
WWTP Name
Residual Analvsis Data
NC0002305
Lear Corporation WWTP
Laboratory: 1) Waypoint Analytical
2)
3)
4)
5)
Parameter
Sample or • •• - Date
------------
------------
------------
------------
------------
------------
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
2/16/2021
Date
DENR FORM RSSF - B (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
EMA Resources Inc. Total Dry Tons Applied (Annual):
WQ0041666 Cation Exchange Capacity (non 503 only):
Donnell Kornegay Owner: Donnell Kornegay Predominant Soil Series:
11.2 Acres Permitted: 11.2 Site #: NC-DU-08 Field #:
12.16
AuB
1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
_____________
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
1.09
Arsenic
0.035
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.035
Cadmium
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Copper
0.104
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.104
Chromiuni
0.016
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.016
Lead
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.012
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.028
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.028
denum
Nickel
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
Selenium
0.041
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.041
Zinc
0.090
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.090
Total
Phos-
28.888
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
28.888
horus
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/4/2021
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
EMA Resources Inc.
Donnell Komegay
Operator: Donnell Komegay
WQ Permit #: WQ0041666 Field #:
Annual Dry Tons Applied: 12.16 Site #:
Predominant Soil Series: AuB
Crop 1 Name: Bermuda - Pasture Crop 1 Max. PAN:
147
Crop 2 Name:
Acres Utilized: 11.2
NC-DU-08 Acres Permitted: 11.2
Cation Exchange Capacity (non 503): 0
Crop 2 Max. PAN:
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
F '5
w
*
o
o'
7�
* N
o
TKN
mg/kg
o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/29
110500
2.64
1.086
Guilford Mills
Dry
<.5"
S
0.5
0.3
30600
5350
192
22.683
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this
form):
TOTALS:
o
tto5oo
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
22.683
0.000
Lime Applied
Annuallbs/acre
0.035 0.004 0.104 0.016 0.012 0.000 0.028 0.014 0.041 0.090 28.888
0 0 0 0 0 0 0 0 0 0
0.035 0.004 0.104 0.016 0.012 0.000 0.028 0.014 0.041 0.090
1 36 34 1 1338 267 1 15 374 1 89 1 2498
1 147
Date
lbs/ac
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R. * * * *
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/4/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
EMA Resources Inc. Total Dry Tons Applied (Annual):
WQ0041666 Cation Exchange Capacity (non 503 only):
Donnell Kornegay Owner: Donnell Kornegay Predominant Soil Series:
23 Acres Permitted: 23 Site #: NC-DU-08 Field #:
14.31
AuB
2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
_____________
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
0.62
Arsenic
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.020
Cadmium
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Copper
0.060
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.060
Chromium
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Lead
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.016
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.016
denum
Nickel
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Selenium
0.023
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.023
Zinc
0.052
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.052
Total
Phos-
16.545
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
16.545
horus
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/4/2021
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
EMA Resources Inc.
Donnell Komegay
Operator: Donnell Komegay
WQ Permit #: WQ0041666 Field #:
Annual Dry Tons Applied: 14.31 Site #:
Predominant Soil Series: AuB
Crop 1 Name: Bermuda - Pasture Crop 1 Max. PAN:
147
Crop 2 Name:
Acres Utilized: 23
NC-DU-08 Acres Permitted: 23
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
F '5
w
*
o
o'
7�
* N
o
TKN
mg/kg
o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/30
130000
2.64
0.622
Guilford Mills
Dry
<.5"
S
0.5
0.3
30600
5350
192
12.995
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
o
t30000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
12.995
0.000
Lime Applied
Annuallbs/acre
0.020
0.002
0.060
0.009
0.007
0.000
0.016
0.008
0.023
0.052 16.545
0
0.052
1 2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.020
0.002
0.060
0.009
0.007
0.000
0.016
0.008
0.023
Permitted C. P. L. R. * * * *
1 36
34
1 1338
267
1 15
374
1 89
Permit PAN Limit 1 st/2nd Crop
1
1 147
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/4/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
EMA Resources Inc. Total Dry Tons Applied (Annual):
WQ0041666 Cation Exchange Capacity (non 503 only):
Donnell Kornegay Owner: Donnell Kornegay Predominant Soil Series:
87.73 Acres Permitted: 87.83 Site #: NC-DU-08 Field #:
46.50
AuB
4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
_____________
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
0.53
Arsenic
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Cadmium
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Copper
0.051
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.051
Chromiuni
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Lead
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
denum
Nickel
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Selenium
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.020
Zinc
0.044
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.044
Total
Phos-
14.098
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
14.098
horus
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/4/2021
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
EMA Resources Inc.
Donnell Komegay
Operator: Donnell Komegay
WQ Permit #: WQ0041666 Field #:
Annual Dry Tons Applied: 46.50 Site #:
Predominant Soil Series: AuB
Crop 1 Name: Bermuda - Pasture Crop 1 Max. PAN:
147
Crop 2 Name:
4 Acres Utilized: 87.73
NC-DU-08 Acres Permitted: 87.83
Cation Exchange Capacity (non 503): 0
Crop 2 Max. PAN:
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
F '5
w
*
o
o'
7�
* N
* w
o
TKN
mg/kg
o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
11/9
19500
2.64
0.024
Guilford Mills
Dry
<.5"
S
0.5
0.3
30600
5350
1 192
0.511
NA
Rye
11/10
71500
2.64
0.090
Guilford Mills
Dry
<.5"
S
0.5
0.3
30600
5350
192
1.874
NA
Rye
11/11
58500
2.64
0.073
Guilford Mills
Dry
<.5"
S
0.5
0.3
30600
5350
192
1.533
NA
Rye
11/21
45500
2.64
0.057
Guilford Mills
Dry
<.5"
S
0.5
0.3
30600
5350
192
1.192
NA
Rye
11/22
97500
2.64
0.122
Guilford Mills
Dry
<.5"
S
0.5
0.3
30600
5350
192
2.555
NA
Rye
11/23
130000
2.64
0.163
Guilford Mills
Dry
<.5"
S
0.5
0.3
30600
5350
192
3.407
NA
Rye
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
0
42250o
As
Cd
Cu
Cr
Pb
Hg,
Mo
Ni
Se
Zn P
11.072
0.000
Lime Applied
Annuallbs/acre
0.017
0.002
0.051
0.008
0.006
0.000
0.013
0.007
0.020
0.044 14.098 1
0
0.044
1 2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.017
0.002
0.051
0.008
0.006
0.000
0.013
0.007
0.020
Permitted C. P. L. R. * * * *
1 36
34
1 1338
267
15
374
89
Permit PAN Limit 1 st/2nd Crop
1
1 147
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/4/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
EMA Resources Inc. Total Dry Tons Applied (Annual):
WQ0041666 Cation Exchange Capacity (non 503 only):
Donnell Kornegay Owner: Donnell Kornegay Predominant Soil Series:
13 Acres Permitted: 13 Site #: NC-DU-08 Field #:
20.03
AuB
5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
_____________
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
1.54
Arsenic
0.050
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.050
Cadmium
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Copper
0.148
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.148
Chromiuni
0.023
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.023
Lead
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.039
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.039
denum
Nickel
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.020
Selenium
0.058
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.058
Zinc
0.128
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.128
Total
Phos-
40.991
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
40.991
horus
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/4/2021
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
EMA Resources Inc.
Donnell Komegay
Operator: Donnell Komegay
WQ Permit #: WQ0041666 Field #:
Annual Dry Tons Applied: 20.03 Site #:
Predominant Soil Series: AuB
Crop 1 Name: Bermuda - Pasture Crop 1 Max. PAN:
147
Crop 2 Name:
Acres Utilized: 13
NC-DU-08 Acres Permitted: 13
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
F '5
w
*
o
o'
7�
* N
* w
o
TKN
mg/kg
o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
11/24
104000
2.64
0.881
Guilford Mills
Dry
<.5"
S
0.5
0.3
30600
5350
1 192
18.393
NA
Rye
11/25
78000
2.64
0.661
Guilford Mills
Dry
<.5"
S
0.5
0.3
30600
5350
192
13.794
NA
Rye
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this
form):
TOTALS:
o
ts2000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
32.187
0.000
Lime Applied
Annuallbs/acre
0.050 0.006 0.148 0.023 0.018 0.000 0.039 0.020 0.058 0.128 40.991
0 0 0 0 0 0 0 0 0 0
0.050 0.006 0.148 0.023 0.018 0.000 0.039 0.020 0.058 0.128
1 36 34 1 1338 267 1 15 374 1 89 1 2498
1 147
Date
lbs/ac
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R. * * * *
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/4/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
EMA Resources Inc. Total Dry Tons Applied (Annual):
WQ0041666 Cation Exchange Capacity (non 503 only):
Donnell Kornegay Owner: Donnell Kornegay Predominant Soil Series:
34 Acres Permitted: 34 Site #: NC-DU-10 Field #:
45.80
AuB
1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
_____________
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
1.35
Arsenic
0.043
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.043
Cadmium
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Copper
0.130
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.130
Chromiuni
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.020
Lead
0.015
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.034
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.034
denum
Nickel
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Selenium
0.051
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.051
Zinc
0.112
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.112
Total
Phos-
35.830
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
35.830
horus
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/4/2021
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
EMA Resources Inc.
Donnell Komegay
Operator: Donnell Komegay
WQ Permit #: WQ0041666 Field #:
Annual Dry Tons Applied: 45.80 Site #:
Predominant Soil Series: AuB
Crop 1 Name: Bermuda - Hay Crop 1 Max. PAN:
196
Crop 2 Name:
Acres Utilized: 34
NC-DU-10 Acres Permitted: 34
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
F '5
w
*
o
o'
7�
* N
* w
o
TKN
mg/kg
o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/27
130000
2.64
0.421
Guilford Mills
Dry
<.5"
S
0.5
0.3
30600
5350
1 192
8.791
NA
Bermuda
7/28
208000
2.64
0.673
Guilford Mills
Dry
<.5"
S
0.5
0.3
30600
5350
192
14.065
NA
Bermuda
7/29
78000
2.64
0.253
Guilford Mills
Dry
<.5"
S
0.5
0.3
30600
5350
192
5.274
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
0
4t6000
As
Cd
Cu
Cr
Pb
Hg,
Mo
Ni
Se
Zn P
28.130
o.000
Lime Applied
Annuallbs/acre
0.043
0.005
0.130
0.020
0.015
0.000
0.034
0.017
0.051
0.112 35.830
0
0.112
1 2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.043
0.005
0.130
0.020
0.015
0.000
0.034
0.017
0.051
Permitted C. P. L. R. * * * *
36
34
1 1338
267
15
374
89
Permit PAN Limit 1 st/2nd Crop
1
1 196
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/4/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Waypointo
ANALYTICAL
1 /22/2020
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 20-010-0059
Client Project Description: Guilfield Miills
Kenansville, NC
2790 Whitten Road, Memphis, TIN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 1/10/2020 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015
Mississippi California #2904
Kentucky #90047 Tennessee #TN02027
VA NELAP #460181
NC #415
EPA #TN00012
Texas #T104704180 Arkansas #88-0650
Oklahoma #9311 SC #84002
Kentucky UST #80215 PA DEP #68-03195
Page 1 of 7

Waypoint
ANALYTICAL
Report Number: 20-010-0059
Client Project Description: Guilfield Miills
Kenansville, NC
Lab No Client Sample ID
92916 Guilford Mills WWTP
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Matrix Date Collected
Solids 01/09/2020 08:00
Date Received
O1/10/2020
Page 2 of 7

Waypoint
ANALYTICAL
Client: EMA Resources Inc
Project: Guilfield Miills
Lab Report Number: 20-010-0059
Date: 1 /22/2020
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 92916 (Guilford Mills WWTP)
Analyte: Aluminum
QC Batch No: 1-472729/1-472416
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 3 of 7

i
Wa2790 Whitten Road, Memphis, TN 38133
ypoint.Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Mr. Brent Collins Project Guilfield Miills Report Date : 01/22/2020
755 Yadkinville Rd Information : Kenansville, NC Received : 01/10/2020
Mocksville , NC 27028
Report Number : 20-010-0059 REPORT OFANALYSIS Danyale Love
Project Manager
Lab No : 92916
Matrix: Solids
Sample ID : Guilford Mills WWTP
Sampled:
1/9/2020
8:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
97.4
%
0.010
1
01/13/20 16:26
ADM
SW-DRYWT
Ammonia Nitrogen
5350
mg/Kg -
dry
962
1
01/21/20 14:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<192
mg/Kg -
dry
192
192
1
01/20/20 16:10
ZBD
4500NO3F-2011
Organic N
25230
mg/Kg -
dry
55.00
2754
1
01/14/20 16:16
CALCULATION
pH
6.8
S.U.
1
01/21/20 05:24
JSL
9045D
Total Solids
2.64
%
0.010
0.010
1
01/13/20 16:26
ADM
2540G-2011
Total Volatile Solids
69.5
%
0.010
0.010
1
01/13/20 16:26
ADM
2540G-2011
Total Kjeldahl Nitrogen
30600
mg/Kg -
dry
2750
1
01/14/20 16:16
CLP 4500NORGD-2011
Phosphorus
13300
mg/Kg -
dry
98.8
192
1
01/14/20 02:28
BKN
6010D
Aluminum
98500
mg/Kg -
dry
78.1
192
1
01/14/20 02:28
BKN
6010D
Arsenic
<16.1
mg/Kg -
dry
16.1
19.2
1
01/14/20 02:28
BKN
6010D
Cadmium
<1.90
mg/Kg -
dry
1.90
3.85
1
01/14/20 02:28
BKN
6010D
Calcium
7150
mg/Kg -
dry
646
962
1
01/14/20 02:28
BKN
6010D
Chromium
<7.31
mg/Kg -
dry
7.31
9.62
1
01/14/20 02:28
BKN
6010D
Copper
48.1
mg/Kg -
dry
5.58
9.62
1
01/14/20 02:28
BKN
6010D
Iron
361
mg/Kg -
dry
163
192
1
01/14/20 02:28
BKN
6010D
Lead
<5.73
mg/Kg -
dry
5.73
11.5
1
01/14/20 02:28
BKN
6010D
Magnesium
1540
mg/Kg -
dry
85.4
192
1
01/14/20 02:28
BKN
6010D
Manganese
36.9
mg/Kg -
dry
7.04
19.2
1
01/14/20 02:28
BKN
6010D
Mercury
<0.125
mg/Kg -
dry
0.125
0.565
1
01/15/20 16:22
TJS
7471A
Molybdenum
12.7
mg/Kg -
dry
5.00
9.62
1
01/14/20 02:28
BKN
6010D
Nickel
<6.35
mg/Kg -
dry
6.35
9.62
1
01/14/20 02:28
BKN
6010D
Potassium
2010
mg/Kg -
dry
115
192
1
01/14/20 02:28
BKN
6010D
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions L Limit Exceeded
MQL
Method Quantitation Limit
Page 4 of 7

i
Waypoint.
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 20-010-0059
Lab No : 92916
Sample ID : Guilford Mills WWTP
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Guilfield Miills
Information : Kenansville, NC
REPORT OFANALYSIS
Report Date : 01/22/2020
Received : 01/10/2020
Danyale Love
Project Manager
Matrix: Solids
Sampled: 1/9/2020 8:00
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
<18.8
mg/Kg -
dry
18.8
19.2
1
01/14/20 02:28
BKN
6010D
Sodium
2070
mg/Kg -
dry
297
962
1
01/14/20 02:28
BKN
6010D
Zinc
41.53
mg/Kg -
dry
41.5
48.1
1
01/14/20 02:28
BKN
6010D
Sulfur
14400
mg/Kg -
dry
188
192
1
01/14/20 02:28
BKN
6010D
Sodium Absorption Ratio
<2.22
Ratio
2.22
5.00
1
01/14/20 02:28
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 5 of 7

•
WayPAoi nt ..(2) 2790 Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 9fl1.213.2400 °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 20-010-0059
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
#70
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: rRory Phillips Date & Time: 01/10/2020 10:50:20
Page 6 of 7

Client Name/Address
Client Project Manager/Contact
Billing Information
For Laboratory Use Only
EMA Resources Inc
Brent Collins
ACCount #46245
755 Yadkinville Rd
Mocksville, INC 27028
Project Description
Project/Site Location (City/State]
RUSH -Additional charges apply
Me od of Shi nt
Matrix Key
Special Detection Limits}
Fed ExUPS �USPS
q
WW -Wastewater GW-Groundwater
vArd-cs
y'-N'1N5vzu_ AIC
❑ate Results Needed
CourierClient Drop Off
❑W - Drinking Water S - Soil /Solid 0 - Oil
P-Product M-Mist
'
Other
Project Number
Project Manager Phone p
Project Manager Email
Purchase Order Number
Site/Facility ID 4
336-399-3646
Brent-Collinsu@emaresourcescom
Z
(1)
A Cool r 10C Na25203 IMlcro Only)
G
CDq
a Coal t= 6C
Wa.�/Y r��' ��
d
'-
C H2504 pH<2
m
w
n
0
E
cu
Q
D None Required
ANALYTICAL
c
o
m
E
E
2
[n
E NaOH pH�10
2790 Whitler RoadV
Unless noted, all containers
p
Uj
[6
Q
Z
T
F HNO3 PH-2
U Het PH�z
Memphis, TN 38133
o
[phone]
per Table II of 40 CER Part
£
`
~
H H3PO4 pH�2
1 Cool <= 6C NA25203
136.
z
c?
Date
Time
s a Mp le Identification
Required
A alysis / Preservati
Comments/Notes
L
Metals.AI,As,Ca,Cd,Cr,Cu,Fe,Pb
Mn.Mg,Mo,Hg,Ni,Se, Na,P, S, K,Zn
1� 1i1111111111�1 lllllll�ll11111111111111111111 l�� 111111u1 lfq os ��° 0059
EMA Resources Inc 10:49:47
GuIlfield Millis
For Laboratory Use Only
Sampled by (Name -Print)
a 7 �-1��
Client Remarks/Comments
Sludge Samples - Report Dry Weight
Ice
Custody
Seals
Lab Comments
bp N
Relinqui d . SI A RE}
Time
Received by: (SIGN A RE}
Date Time
y
Blank ooler
Relinquish by: (SIG ATURE}
a e Time
/9
Receiv by: SIGNATURE)
Date Time
r 3=
Relinquished by: (SIGNATURE)
Date Time
Rere d ; {SIG URE}
Dje� TI e
01� ', US
Page 7 of 7

aceAnalytical a ANALYTICAL REPORT
National Center for Testing & Innovation January 21, 2020
EMA Resources
Sample Delivery Group: L1178358
Samples Received: 01/10/2020
Project Number: GUILFORD MILLS
Description: Sludge
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By: Jw C4V1--
Justin Carr
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources GUILFORD MILLS L1173353 01/21/20 15:50 1 of 22

TABLE OF CONTENTS
ONE LAB. NATIONWIDE. *
Cp: Cover Page
Tc: Table of Contents
Ss: Sample Summary
Cn: Case Narrative
Sr: Sample Results
GUILFORD MILLS L1178358-01
Qc: Quality Control Summary
Wet Chemistry by Method 9012 B
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9045D
Wet Chemistry by Method D93/1010A
Mercury by Method 7470A
Metals (ICP) by Method 6010D
Volatile Organic Compounds (GC/MS) by Method 8260D
Chlorinated Acid Herbicides (GC) by Method 8151A
Pesticides (GC) by Method 8081B
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
GI: Glossary of Terms
al: Accreditations & Locations
Sc: Sample Chain of Custody
1
2
3
4
5
5
7
7
8
9
10
11
12
14
16
17
18
20
21
22
ACCOUNT: PROJECT: SDG: DATE/TIME:
EMA Resources GUILFORD MILLS L1173353 01/21/20 15:50
PAGE:
2 of 22

SAMPLE SUMMARY ONE LAB. NATIONWIDE.
Collected by Collected date/time Received date/time
GUILFORD MILLS L1178358-01 Waste Roy Whittaker 01/09/2008:00 01/10/2009:00 t C
P
Method
Batch
Dilution Preparation
Analysis
Analyst
date/time
date/time
Preparation by Method 1311
WG1410079
1 01/13/20 09:07
01/13/20 09:07
IDW
Preparation by Method 1311
WG1410099
1 01/13/20 08:47
01/13/20 08:47
BAA
Wet Chemistry by Method 9012 B
WG1411287
1 01/15/20 09:07
01/15/2013:41
JER
Wet Chemistry by Method 9034-9030B
WG1411620
1 01/16/20 2106
01/16/20 2106
MJA
Wet Chemistry by Method 9045D
WG1412940
1 01/17/201100
01/17/2012:00
MSP
Wet Chemistry by Method D93/1010A
WG1413920
1 01/21/2012:25
01/21/2012:25
MJA
Mercury by Method 7470A
WG1410658
1 01/14/2010:46
01/14/20 20:49
TCT
Metals (ICP) by Method 6010D
WG1410815
1 01/15/20 07:28
01/15/2010:05
CCE
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1410537
1 01/14/2018:10
01/14/2018:10
BMB
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1412927
1 01/17/20 08:30
01/17/2019:54
MT-1
Pesticides (GC) by Method 8081B
WG1410888
1 01/15/20 06:59
01/15/2018:06
HMH
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG1412188
1 01/16/2010:44
01/16/20 20:59
JNJ
Location
FC
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fn
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fr
Mt. Juliet, TN
Mt. Juliet, TN
FC
Mt. Juliet, TN
Mt. Juliet, TN
�GI
SAI
RC
ACCOUNT: PROJECT: SDG: DATE/TIME:
EMA Resources GUILFORD MILLS L1173353 01/21/20 15:50
PAGE:
3 of 22

CASE NARRATIVE
ONE LAB. NATIONWIDE. *
All sample aliquots were received at the correct temperature, in the proper containers, with the FP
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data. 0
Fr
FC
GI
Justin Carr [Al
Project Manager
RC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources GUILFORD MILLS L1173353 01/21/20 15:50 4 of 22

GUILFORD MILLS
Collected date/time: 01/09/20 08:00
Preparation by Method 1311
SAMPLE RESULTS - 01
L1178358
Result Qualifier
Prep
Batch
Analyte
date / time
TCLP Extraction
1/13/2020 9:07:16 AM
WG1410079
TCLP ZHE Extraction -
1/13/2020 8:47:14 AM
WG1410099
Fluid 1
1/13/2020 9:07:16 AM
WG1410079
Initial pH 7.12
1/13/2020 9:07:16 AM
WG1410079
Final pH 5.00
1/13/2020 9:07:16 AM
WG1410079
Wet Chemistry by Method 9012 B
Result Qualifier
RDL Dilution
Analysis
Analyte mg/kg
mg/kg
date / time
Reactive Cyanide ND
0.250 1
01/15/202013:41
Wet Chemistry by Method 9034-9030B
Result Qualifier RDL
Analyte mg/kg mg/kg
Reactive Sulfide ND 25.0
Wet Chemistry by Method 9045D
Batch
WG1411287
Dilution Analysis Batch
date / time
1 01/16/2020 2106 WG1411620
Result Qualifier Dilution Analysis Batch
Analyte su date / time
Corrosivity by pH 7.13 T8 1 01/17/202012:00 WG1412940
Sample Narrative:
L1178358-01 WG1412940: 7.13 at 22.6C
Wet Chemistry by Method D93/1010A
ONE LAB. NATIONWIDE. *
Fp
Fc
FS
Fn
Fc
�GI
SAI
Rc
Result
Qualifier
Dilution
Analysis
Batch
Analyte Deg. F
date / time
Ignitability DNI at170
1
01/21/202012:25
WG1413920
Mercury by Method 7470A
Result
Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte mg/I
mg/I
mg/I
date/time
Mercury ND
0.0100
0.20
1 01/14/2020 20:49
WG1410658
Metals (ICP) by Method 6010D
Result
Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte mg/I
mg/I
mg/I
date/time
Arsenic ND
0.100
5
1 01/15/202010:05
WG1410815
Barium ND
0.100
100
1 01/15/202010:05
WG1410815
Cadmium ND
0.100
1
1 01/15/202010:05
WG1410815
Chromium ND
0.100
5
1 01/15/202010:05
WG1410815
Lead ND
0.100
5
1 01/15/202010:05
WG1410815
Selenium ND
0.100
1
1 01/15/202010:05
WG1410815
Silver ND
0.100
5
1 01/15/202010:05
WG1410815
Volatile Organic Compounds (GC/MS) by Method
8260D
Result
Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte mg/I
mg/I
mg/I
date/time
Benzene ND
0.0500
0.50
1 01/14/202018:10
WG1410537
Carbon tetrachloride ND
0.0500
0.50
1 01/14/202018:10
WG1410537
Chlorobenzene ND
0.0500
100
1 01/14/202018:10
WG1410537
Chloroform ND
0.250
6
1 01/14/202018:10
WG1410537
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
EMA Resources
GUILFORD
MILLS
L1173353
01/21/20 15:50 5 of 22

GUILFORD MILLS SAMPLE RESULTS
Collected date/time: 01/09/20 08:00 L1178358
Volatile Organic Compounds (GC/MS) by Method 8260D
- 01
Result
Qualifier RDL Limit Dilution
Analysis
Batch
Analyte
mg/I
mg/I mg/I
date/time
1,2-Dichloroethane
ND
0.0500 0.50 1
01/14/202018:10
WG1410537
1,1-Dichloroethene
ND
0.0500 0.70 1
01/14/202018:10
WG1410537
2-Butanone (MEK)
ND
J3 J4 0.500 200 1
01/14/202018:10
WG1410537
Tetrachloroethene
ND
0.0500 0.70 1
01/14/202018:10
WG1410537
Trichloroethene
ND
0.0500 0.50 1
01/14/202018:10
WG1410537
Vinyl chloride
ND
0.0500 0.20 1
01/14/202018:10
WG1410537
(S) Toluene-dH
104
80.0-120
0111412020 18.10
WG1410537
(S)4-Bromofluorobenzene
93.8
77.0-126
011141202018.10
WG1410537
(S) 1,2-Dichloroethane-d4
107
70.0-130
011141202018.10
WG1410537
Chlorinated Acid Herbicides (GC) by Method 8151A
Result
Analyte mg/I
2,4,5-TP (Silvex) ND
2,4-D ND
(S)2,4-DichlorophenylAcetic Acid 56.8
Pesticides (GC) by Method 8081B
Result
Analyte
mg/I
Chlordane
ND
Endrin
ND
Heptachlor
ND
Lindane
ND
Methoxychlor
ND
Toxaphene
ND
(S) Decochlorobiphenyl
74.6
(S) Tetrochloro-m-xylene
67.3
Qualifier RDL
Limit
Dilution Analysis
Batch
mg/I
mg/I
date / time
0.00200
1
1 01/17/202019:54
WG1412927
0.00200
10
1 01/17/202019:54
WG1412927
14.0-158
011171202019.54
WG1412927
Qualifier RDL Limit
mg/I mg/I
0.00500 0.03
0.00500 0.02
0.00500 0.0080
0.00500 0.40
0.00500 10
0.0100 0.50
10.0-128
10.0-127
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Dilution Analysis
date / time
01/15/202018:06
01/15/202018:06
01/15/202018:06
01/15/202018:06
01/15/202018:06
01/15/202018:06
0111512020 18.06
0111512020 18.06
Batch
WG1410888
WG1410888
WG1410888
WG1410888
WG1410888
WG1410888
WG1410888
WG1410888
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
1,4-Dichlorobenzene
ND
0.100
7.50
1 01/16/2020 20:59
WG1412188
2,4-Dinitrotoluene
ND
0.100
0.13
1 01/16/2020 20:59
WG1412188
Hexachlorobenzene
ND
0.100
0.13
1 01/16/2020 20:59
WG1412188
Hexachloro-1,3-butadiene
ND
0.100
0.50
1 01/16/2020 20:59
WG1412188
Hexachloroethane
ND
0.100
3
1 01/16/2020 20:59
WG1412188
Nitrobenzene
ND
0.100
2
1 01/16/2020 20:59
WG1412188
Pyridine
ND
0.100
5
1 01/16/2020 20:59
WG1412188
3&4-Methyl Phenol
ND
0.100
400
1 01/16/2020 20:59
WG1412188
2-Methylphenol
ND
0.100
200
1 01/16/2020 20:59
WG1412188
Pentachlorophenol
ND
0.100
100
1 01/16/2020 20:59
WG1412188
2,4,5-Trichlorophenol
ND
0.100
400
1 01/16/2020 20:59
WG1412188
2,4,6-Trichlorophenol
ND
0.100
2
1 01/16/2020 20:59
WG1412188
(S) 2-Fluorophenol
31.6
10.0-120
0111612020 20.59
WG1412188
(S) Phenol-d5
19.0
10.0-120
0111612020 20.59
WG1412188
(S) Nitrobenzene-d5
51.0
10.0-127
0111612020 20.59
WG1412188
(S) 2-Fluorobiphenyl
67.2
10.0-130
0111612020 20.59
WG1412188
(S) 2,4, 6-Tribromophenol
65.5
10.0-155
0111612020 20.59
WG1412188
(S) p-Terphenyl-d14
69.5
10.0-128
0111612020 20.59
WG1412188
ONE LAB. NATIONWIDE. *
Fp
Fc
FS
Fn
FA
Fc
�GI
SAI
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources GUILFORD MILLS L1173353 01/21/20 15:50 6 of 22

WG1411287 QUALITY CONTROL SUMMARY
ONE LAB. NATIONWIDE.
Wet Chemistry by Method 9012 B L1178358-01
Method Blank (MB)
C p
(MB) R3490983-1 01/15/201324
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TC
I
Reactive Cyanide -10.0390 0.250
FS
L1178358-01 Original Sample (OS) • Duplicate (DUP)
[�n]
(OS) L1173353-01 01/15/2013:41 • (DUP) R3490933-4 01/15/2013:42
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
5
Sr
Analyte mg/kg mg/kg
—
Reactive Cyanide ND 0.0962 1 0.000 20
Laboratory Control Sample (LCS)
GI
(LCS) R3490933-5 01/15/20 13:43
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
1711
Analyte mg/kg mg/kg
Reactive Cyanide 2.50 2.80 112 50.0-150
1—Sc
L1177905-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1177905-01 01/15/2013:33 • (MS) R3490933-2 01/15/2013:39 • (MSD) R3490933-3 01/15/2013:40
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 1.67 ND 1.08 1.16 65.0 69.8 1 75.0-125 J6 J6 7.12
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources GUILFORD MILLS L1173353 01/21/20 15:50 7 of 22

WG1411620
Wet Chemistry by Method 9034-9030B
Method Blank (MB)
(MB) R3491651-1 01/16/20 2106
MB Result
Analyte mg/kg
Reactive Sulfide U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
7.63 25.0
L1178358-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1178358-01
(OS) L1173353-01 01/16/20 21:06 • (DUP) R3491651-3 01/16/20 2106
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %_
Reactive Sulfide ND ND 1 0.000 20
L1178942-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1173942-01 01/16/20 21:06 • (DUP) R3491651-4 01/16/20 2106
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg
Reactive Sulfide ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3491651-2 01/16/20 2106
Spike Amount LCS Result
Analyte mg/kg mg/kg
Reactive Sulfide 100 95.6
LCS Rec. Rec. Limits LCS Qualifier
95.6 70.0-130
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources GUILFORD MILLS L1173353 01/21/20 15:50 3 of 22

WG1412940 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9045D L1178358-01
L1178942-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1173942-01 01/17/2012:00 • (DUP) R3491754-2 01/17/2012:00
Original Result DUP Result Dilution DUP RPD
Analyte su su
Corrosivity by pH 8.50 8.55 1 0.587
Sample Narrative:
OS: 8.5 at22C
DUP: 8.55 at21.8C
Laboratory Control Sample (LCS)
(LCS) R3491754-1 01/17/20 12:00
Spike Amount LCS Result
Analyte su su
Corrosivity by pH 10.0 9.95
Sample Narrative:
LCS: 9.95 at18.6C
DUP Qualifier DUP RPD
Limits
LCS Rec. Rec. Limits LCS Qualifier
99.5 99.0-101
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources GUILFORD MILLS L1173353 01/21/20 15:50 9 of 22

WG1413920 QUALITY CONTROL SUMMARY
Wet Chemistry by Method D93/1010A L1178358-01
L1178253-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1173253-02 01/21/2012:25 • (DUP) R3492610-2 01/21/2012:25
Original Result DUP Result Dilution DUP RPD
Analyte Deg. F Deg. F
Ignitability 110 107 1 2.77
L1179547-01 Original Sample (OS) • Duplicate (DUP)
DUP Qualifier DUP RPD
Limits
i
10
(OS) L1179547-01 01/21/20 12:25 • (DUP) R3492610-3 01/21/20 12:25
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte Deg. F Deg. F
Ignitability DNI at170 DNI at170 1 0.000 10
Laboratory Control Sample (LCS)
(LCS) R3492610-1 01/21/2012:25
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte Deg. F Deg. F
Ignitability 82.0 81.8 99.7 97.0-103
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources GUILFORD MILLS L1173353 01/21/20 15:50 10 of 22

WG1410658 QUALITY CONTROL SUMMARY
Mercury by Method 7470A L1178358-01
Method Blank (MB)
(MB) R3490773-1 01/14/20 20:00
MB Result MB Qualifier
MB MDL MB RDL
Analyte mg/I
mg/I mg/I
Mercury U
0.00330 0.0100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3490773-2 01/14/20 20:02 • (LCSD) R3490773-3 01/14/20 20:04
Spike Amount LCS Result
LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I
mg/I
Mercury 0.0300 0.0292
0.0294 97.2 98.1 80.0-120 0.919 20
L1178219-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1173219-02 01/14/20 20:06 • (MS) R3490773-4 01/14/20 20:03 • (MSD) R3490773-5 01/14/20 20:10
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Mercury 0.0300
ND
0.0286
0.0287 95.2 95.8 1 75.0-125 0.614 20
L1178302-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1173302-02 01/14/20 20:12 • (MS) R3490773-6 01/14/20 20:14 • (MSD) R3490773-7 01/14/20 20:22
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Mercury 0.0300
ND
0.0293
0.0296 97.5 98.8 1 75.0-125 1.28 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources GUILFORD MILLS L1173353 01/21/20 15:50 11 of 22

WG1410815
Metals (ICP) by Method 6010D
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1178358-01
(MB) R3490900-1 01/15/20 0931
MB Result
Analyte mg/I
MB Qualifier MB MDL
mg/I
MB RDL
mg/I
Arsenic U
0.0333
0.100
Barium U
0.0333
0.100
Cadmium U
0.0333
0.100
Chromium U
0.0333
0.100
Lead U
0.0333
0.100
Selenium U
0.0333
0.100
Silver U
0.0333
0.100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3490900-2 01/15/20 09:33 • (LCSD) R3490900-3 01/15/20 09:36
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
Arsenic
10.0
9.85
9.91
98.5
99.1
80.0-120
0.643
20
Barium
10.0
10.1
10.2
101
102
80.0-120
0.834
20
Cadmium
10.0
9.77
9.86
97.7
98.6
80.0-120
0.928
20
Chromium
10.0
9.76
9.75
97.6
97.5
80.0-120
0.113
20
Lead
10.0
9.82
9.92
98.2
99.2
80.0-120
1.03
20
Selenium
10.0
10.1
10.2
101
102
80.0-120
0.681
20
Silver
2.00
1.85
1.83
92.3
91.5
80.0-120
0.785
20
L1178499-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1173499-04 01/15/20 09:39 • (MS) R3490900-5 01/15/20 09:44 • (MSD) R3490900-6 01/15/20 09:46
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
Arsenic
10.0
U
9.57
9.54
95.7
95.4
Barium
10.0
U
10.3
10.2
102
101
Cadmium
10.0
U
9.69
9.65
96.9
96.5
Chromium
10.0
U
9.72
9.70
97.2
97.0
Lead
10.0
U
9.76
9.66
97.6
96.6
Selenium
10.0
U
9.74
9.64
97.4
96.4
Silver
2.00
U
1.82
1.82
91.1
91.0
ONE LAB. NATIONWIDE. *
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 75.0-125
0.237
20
1 75.0-125
0.845
20
1 75.0-125
0.454
20
1 75.0-125
0.148
20
1 75.0-125
1.09
20
1 75.0-125
1.04
20
1 75.0-125
0.0881
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources GUILFORD MILLS L1173353 01/21/20 15:50 12 of 22

WG1410815 QUALITY CONTROL SUMMARY
Metals (ICP) by Method 6010D L1178358-01
L1178878-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1173373-01 01/15/20 09:49 • (MS) R3490900-7 01/15/20 09:51 • (MSD) R3490900-8 01/15/20 09:54
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits MS Qualifier
Analyte
mg/I
mg/I
mg/I
mg/I
Arsenic
10.0
ND
9.97
9.95
99.7
99.5
1 75.0-125
Barium
10.0
0.388
10.4
10.5
100
101
1 75.0-125
Cadmium
10.0
ND
9.88
9.93
98.8
99.3
1 75.0-125
Chromium
10.0
ND
9.73
9.70
97.3
97.0
1 75.0-125
Lead
10.0
ND
9.84
9.91
98.4
99.1
1 75.0-125
Selenium
10.0
ND
10.2
10.2
101
102
1 75.0-125
Silver
2.00
ND
1.86
1.86
93.2
93.1
1 75.0-125
ONE LAB. NATIONWIDE. *
MSD Qualifier RPD
RPD Limits
0.200
20
0.544
20
0.525
20
0.329
20
0.701
20
0.498
20
0.0688
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources GUILFORD MILLS L1173353 01/21/20 15:50 13 of 22

WG1410537 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1178358-01
ONE LAB. NATIONWIDE. *
Method Blank (MB)
(MB) R3490638-8 01/14/201326
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Benzene
U
0.0167
0.0500
Carbon tetrachloride
U
0.0167
0.0500
Chlorobenzene
U
0.0167
0.0500
Chloroform
U
0.0833
0.250
1,2-Dichloroethane
U
0.0167
0.0500
1,1-Dichloroethene
U
0.0167
0.0500
2-Butanone (MEK)
U
0.167
0.500
Tetrachloroethene
U
0.0167
0.0500
Trichloroethene
U
0.0167
0.0500
Vinyl chloride
U
0.0167
0.0500
(S) Toluene-dH
103
80.0-120
(S) 4-Bromofluorobenzene
94.8
77.0-126
(S) 1,2-Dichloroethane-d4
104
70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3490638-1 01/14/20 09:04 • (LCSD) R3490638-3 01/14/201120
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/I
mg/I
mg/I
Benzene
0.250
0.277
0.287
111
115
70.0-123
Carbon tetrachloride
0.250
0.254
0.266
102
106
68.0-126
Chlorobenzene
0.250
0.244
0.267
97.6
107
80.0-121
Chloroform
0.250
0.276
0.288
110
115
73.0-120
1,2-Dichloroethane
0.250
0.267
0.288
107
115
70.0-128
1,1-Dichloroethene
0.250
0.278
0.279
ill
112
71.0-124
2-Butanone (MEK)
1.25
1.65
2.18
132
174
44.0-160
Tetrachloroethene
0.250
0.239
0.253
95.6
101
72.0-132
Trichloroethene
0.250
0.248
0.253
99.2
101
78.0-124
Vinyl chloride
0.250
0.259
0.291
104
116
67.0-131
(S) Toluene-dH
102
103
80.0-120
(S) 4-Bromofluorobenzene
95.6
96.6
77.0-126
(S) 1,2-Dichloroethane-d4
104
103
70.0-130
LCS Qualifier
LCSD Qualifier RPD
3.55
4.62
9.00
4.26
7.57
0.359
J3 J4 27.7
5.69
2.00
11.6
RPD Limits
20
20
20
20
20
20
20
20
20
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources GUILFORD MILLS L1173353 01/21/20 15:50 14 of 22

WG1410537 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1178358-01
ONE LAB. NATIONWIDE. *
L1178220-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1173220-02 01/14/20 14:03 • (MS) R3490633-4 01/14/20 11:45 • (MSD) R3490633-5 01/14/20 12:06
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
Benzene
0.250
ND
0.320
0.328
128
131
Carbon tetrachloride
0.250
ND
0.300
0.315
120
126
Chlorobenzene
0.250
ND
0.278
0.290
ill
116
Chloroform
0.250
ND
0.311
0.320
124
128
1,2-Dichloroethane
0.250
ND
0.297
0.305
119
122
1,1-Dichloroethene
0.250
ND
0.318
0.330
127
132
2-Butanone (MEK)
1.25
ND
1.95
2.02
156
162
Tetrachloroethene
0.250
ND
0.279
0.283
112
113
Trichloroethene
0.250
ND
0.280
0.286
112
114
Vinyl chloride
0.250
ND
0.320
0.324
128
130
(S) Toluene-dH
103
103
(S) 4-Bromofluorobenzene
95.4
97.7
(S) 1,2-Dichloroethane-d4
104
104
L1178556-04 Original Sample (OS) • Matrix Spike (MS)
(OS) L1173556-04 01/14/20 14:27 • (MS) R3490633-6 01/14/2012:26
Spike Amount
Original Result
MS Result
MS Rec. Dilution
Analyte
mg/I
mg/I
mg/I
Benzene
0.250
ND
0.311
124 1
Carbon tetrachloride
0.250
ND
0.299
120 1
Chlorobenzene
0.250
ND
0.280
112 1
Chloroform
0.250
ND
0.317
127 1
1,2-Dichloroethane
0.250
ND
0.295
118 1
1,1-Dichloroethene
0.250
ND
0.315
126 1
2-Butanone (MEK)
1.25
ND
1.81
145 1
Tetrachloroethene
0.250
ND
0.280
112 1
Trichloroethene
0.250
ND
0.275
110 1
Vinyl chloride
0.250
ND
0.314
126 1
(S) Toluene-dH
103
(S) 4-Bromofluorobenzene
95.8
(S) 1,2-Dichloroethane-d4
104
Rec. Limits
17.0-158
23.0-159
33.0-152
29.0-154
29.0-151
11.0-160
10.0-160
10.0-160
10.0-160
10.0-160
80. 0-120
77.0-126
70.0-130
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 17.0-158
2.47
27
1 23.0-159
4.88
28
1 33.0-152
4.23
27
1 29.0-154
2.85
28
1 29.0-151
2.66
27
1 11.0-160
3.70
29
1 10.0-160
J5 3.53
32
1 10.0-160
1.42
27
1 10.0-160
2.12
25
1 10.0-160
1.24
27
80.0-120
77.0-126
70.0-130
MS Qualifier
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources GUILFORD MILLS L1173353 01/21/20 15:50 15 of 22

WG1412927
Chlorinated Acid Herbicides (GC) by Method 8151A
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1178358-01
(MB) R3491837-1 01/17/201507
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
2,4-D U
0.000667
0.00200
2,4,5-TP (Silvex) U
0.000667
0.00200
(S) Z4-Dichlorophenyl Acetic 68.6
14.0-158
Acid
Laboratory Control Sample (LCS)
(LCS) R3491337-2 01/17/20 15:20
Spike Amount
LCS Result
LCS Rec.
Rec. Limits
Analyte mg/I
mg/I
2,4,5-TP (Silvex) 0.0500
0.0320
64.0
50.0-125
2,4-D 0.0500
0.0323
64.6
50.0-120
(S) Z4-Dichlorophenyl Acetic
60.6
14. 0-158
Acid
LCS Qualifier
L1178359-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1173359-01 01/17/20 20:03 • (MS) R3491337-3 01/17/20 20:22 • (MSD) R3491337-4 01/17/20 20:35
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
mg/I
2,4,5-TP (Silvex)
0.0500
ND
0.0323
0.0331
64.6
66.2
1 50.0-125
2.45
20
2,4-D
0.0500
ND
0.0316
0.0339
63.2
67.8
1 50.0-120
7.02
20
(S) Z4-Dichlorophenyl Acetic
54.8
56.6
14.0-158
Acid
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources GUILFORD MILLS L1173353 01/21/20 15:50 16 of 22

WG1410888
Pesticides (GC) by Method 8081B
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1178358-01
(MB) R3491227-1 01/15/201524
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Gamma BHC
U
0.00167
0.00500
Endrin
U
0.00167
0.00500
Heptachlor
U
0.00167
0.00500
Methoxychlor
U
0.00167
0.00500
Chlordane
U
0.00167
0.00500
Toxaphene
U
0.00333
0.0100
(S) Decachlorobiphenyl
85.8
10.0-128
(S) Tetrochloro-m-xylene
74.2
10.0-127
Laboratory Control Sample (LCS)
(LCS) R3491227-2 01/15/20 15:36
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
Gamma BHC
0.0100
0.00876
87.6
55.0-129
Endrin
0.0100
0.00926
92.6
57.0-134
Heptachlor
0.0100
0.00951
95.1
27.0-132
Methoxychlor
0.0100
0.0111
ill
54.0-155
(S) Decachlorobiphenyl
78.5
10.0-128
(S) Tetrochloro-m-xylene
68.4
10.0-127
L1177678-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1177673-01 01/15/201614 • (MS) R3491227-3 01/15/20 16:26 • (MSD) R3491227-4 01/15/20 16:39
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
Analyte
mg/I
mg/I
mg/I
mg/I
Gamma BHC
0.0100
ND
0.00873
0.00890
87.3
89.0
1 14.0-141
1.93
Endrin
0.0100
ND
0.00907
0.00929
90.7
92.9
1 10.0-160
2.40
Heptachlor
0.0100
ND
0.00946
0.00961
94.6
96.1
1 16.0-136
1.57
Methoxychlor
0.0100
ND
0.0102
0.0103
102
103
1 10.0-160
0.976
(S) Decachlorobiphenyl
71.9
75.0
10.0-128
(S) Tetrochloro-m-xylene
67.1
68.4
10.0-127
ONE LAB. NATIONWIDE. *
RPD Limits
40
39
40
34
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources GUILFORD MILLS L1173353 01/21/20 15:50 17 of 22

WG1412188 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1178358-01
Method Blank (MB)
(MB) R3491629-2 01/16/201752
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
U
0.0333
0.100
2,4-Dinitrotoluene
U
0.0333
0.100
Hexachlorobenzene
U
0.0333
0.100
Hexachloro-1,3-butadiene
U
0.0333
0.100
Hexachloroethane
U
0.0333
0.100
Nitrobenzene
U
0.0333
0.100
2-Methylphenol
U
0.0333
0.100
3&4-Methyl Phenol
U
0.0333
0.100
Pentachlorophenol
U
0.0333
0.100
2,4,5-Trichlorophenol
U
0.0333
0.100
2,4,6-Trichlorophenol
U
0.0333
0.100
Pyridine
U
0.0333
0.100
(S) 2-Fluorophenol
35.1
10.0-120
(S) Phenol-d5
20.5
10.0-120
(S) Nitrobenzene-d5
59.1
10.0-127
(S) 2-Fluorobiphenyl
72.4
10.0-130
(S) 2,4, 6-Tribromophenol
70.0
10. 0-155
(S) p-Terphenyl-d14
72.5
10.0-128
Laboratory Control Sample (LCS)
ONE LAB. NATIONWIDE. *
(LCS) R3491629-1 01/16/201731
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
1,4-Dichlorobenzene 0.500
0.336
67.2
18.0-120
2,4-Dinitrotoluene 0.500
0.403
80.6
49.0-124
Hexachlorobenzene 0.500
0.401
80.2
44.0-120
Hexachloro-1,3-butadiene 0.500
0.327
65.4
19.0-120
Hexachloroethane 0.500
0.321
64.2
15.0-120
Nitrobenzene 0.500
0.304
60.8
27.0-120
2-Methylphenol 0.500
0.277
55.4
28.0-120
3&4-Methyl Phenol 0.500
0.275
55.0
31.0-120
Pentachlorophenol 0.500
0.367
73.4
23.0-120
2,4,5-Trichlorophenol 0.500
0.427
85.4
44.0-120
2,4,6-Trichlorophenol 0.500
0.370
74.0
42.0-120
Pyridine 0.500
0.182
36.4
10.0-120
(S) 2-Fluorophenol
35.2
10.0-120
(S) Phenol-d5
21.8
10.0-120
(S) Nitrobenzene-d5
49.9
10.0-127
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
GUILFORD MILLS L1178358 01/21/20 15:50 18 of 22

WG1412188 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1178358-01
Laboratory Control Sample (LCS)
(LCS) R3491629-1 01/16/201731
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
(S) 2-Fluorobiphenyl 77.2 10.0-130
(S) 2,4, 6-Tribromophenol 86.5 10. 0-155
(S) p-Terphenyl-d14 77.3 10.0-128
L1178358-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1173353-01 01/16/20 20:59 • (MS) R3491629-3 01/16/20 21:20 • (MSD) R3491629-4 01/16/20 2141
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
0.500
ND
0.247
0.228
49.4
45.6
2,4-Dinitrotoluene
0.500
ND
0.359
0.338
71.8
67.6
Hexachlorobenzene
0.500
ND
0.356
0.333
71.2
66.6
Hexachloro-1,3-butadiene
0.500
ND
0.239
0.233
47.8
46.6
Hexachloroethane
0.500
ND
0.217
0.206
43.4
41.2
Nitrobenzene
0.500
ND
0.268
0.245
53.6
49.0
2-Methylphenol
0.500
ND
0.243
0.220
48.6
44.0
3&4-Methyl Phenol
0.500
ND
0.245
0.222
49.0
44.4
Pentachlorophenol
0.500
ND
0.319
0.282
63.8
56.4
2,4,5-Trichlorophenol
0.500
ND
0.379
0.332
75.8
66.4
2,4,6-Trichlorophenol
0.500
ND
0.325
0.284
65.0
56.8
Pyridine
0.500
ND
0.165
0.165
33.0
33.0
(S) 2-Fluorophenol
31.6
27.4
(S) Phenol-d5
19.1
16.8
(S) Nitrobenzene-d5
45.3
40.8
(S) 2-Fluorobiphenyl
70.2
62.0
(S)2,4,6-Tribromophenol
74.0
67.5
(S) p-Terphenyl-d14
68.8
64.9
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
1 17.0-120
8.00
1 39.0-125
6.03
1 35.0-122
6.68
1 12.0-120
2.54
1 10.0-120
5.20
1 12.0-120
8.97
1 10.0-120
9.94
1 10.0-120
9.85
1 10.0-128
12.3
1 33.0-120
13.2
1 26.0-120
13.5
1 10.0-120
0.000
10.0-120
10.0-120
10.0-127
10.0-130
10.0-155
10.0-128
ONE LAB. NATIONWIDE. *
RPD Limits
40
25
24
34
40
30
30
36
37
31
31
37
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources GUILFORD MILLS L1173353 01/21/20 15:50 19 of 22

GLOSSARY OF TERMS
ONE LAB. NATIONWIDE. *
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J3
The associated batch QC was outside the established quality control range for precision.
J4
The associated batch QC was outside the established quality control range for accuracy.
J5
The sample matrix interfered with the ability to make any accurate determination, spike value is high.
J6
The sample matrix interfered with the ability to make any accurate determination, spike value is low.
T8
Sample(s) received past/too close to holding time expiration.
Fp
Fc
FS
Fn
Fr
Fc
SAI
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources GUILFORD MILLS L1173353 01/21/20 15:50 20 of 22

ACCREDITATIONS
& LOCATIONS
ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide
from one location. One phone call, one point of contact,
one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our
single location laboratory is comparable to the collective
totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory
campus. The model is conducive to accelerated
productivity, decreasing
Cp
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium
quality and prompt service allows us to be YOUR
LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace
National.
Fc
State Accreditations
Alabama 40660
Nebraska
NE-OS-15-05
FS
Alaska 17-026
Nevada
TN-03-2002-34
Arizona AZ0612
New Hampshire
2975
Arkansas 88-0469
New Jersey—NELAP
TNO02
Fn
California 2932
New Mexico
n/a
Colorado TN00003
New York
11742
Connecticut PH-0197
North Carolina
Env375
Fr
Florida E87487
North Carolina'
DW21704
Georgia NELAP
North Carolina 3
41
Georgia' 923
North Dakota
R-140
Fc
Idaho TN00003
Ohio—VAP
CL0069
Illinois 200008
Oklahoma
9915
7G1
Indiana C-TN-01 f
Oregon
TN200002
Iowa 364
Pennsylvania
68-02979
Kansas E-10277
Rhode Island
LA000356
Kentucky' 6 90010
South Carolina
84004
Kentucky 2 16
South Dakota
n/a
Louisiana A130792
Tennessee'"
2006
Louisiana' LA180010
Texas
T104704245-18-15
Rc
Maine TN0002
Texas 5
LABO152
Maryland 324
Utah
TN00003
Massachusetts M-TNO03
Vermont
VT2006
Michigan 9958
Virginia
460132
Minnesota 047-999-395
Washington
C847
Mississippi TN00003
West Virginia
233
Missouri 340
Wisconsin
9980939910
Montana CERT0086
Wyoming
A2 LA
Third Party Federal Accreditations
A2LA— ISO17025 1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5 1461.02
DOD
1461.01
Canada 1461.01
USDA
P330-15-00234
EPA—Crypto TN00003
' Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
MT ND
OR
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VWY
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ACCOUNT: V PROJECT:
EMA Resources GUILFORD MILLS
ME
MN
WVI NY
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KY
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LA
FL
SDG: DATE/TIME: PAGE:
L1173353 01/21/20 15:50 21 of 22

Billing Information:
lv 1
Container
P
SPrva i
Chain of Custody Page of
EMA Resources
Mr, Brent Collins Pres
755 Yadkinville Road Chk
CBAa%t/cal•
755 Yadkinville Road
Mocksville, NC 27028
Mocksville, NC 27028
i
12065 Lebanon Rd
Mount Juliet, TIN 37122
Phone', 900-767 5859
Phone: 80o-767-5859 t1"'�:i
Fan615.758-5859
Report to:
Mr, Brent Collins
Email To:[e-mail]
Project
Description: Sludge
City/State
Collected: ,1�t15VT�CC-- ��
Please Circl
PT MT CT �
Phone:[phone]
Fax: [phone]
Client Project p
�yu��`�� W� �LC.S
Lab Project R
SQG q j
E1 99
a
Coll y { ri t).
Site/Facility ID p
P.O. N
B
L113`
0
?
Acctnum: EMARES
Template:T11413
Coe d at e):
Rush? (Lab MUST Be Notified} Quote #
Same Day _ Five Day
J
Prelogin: P748425
I me lately
Packed onlce N Y_
_ Next Day _ 5 nay > Rad only) Date Results Needed
Two Day 10 Day (Rad Only) No
_Three Day of
L1
_
t..1
J
LJ
PM: 807 - Tustin Carr
PB, '-3
Sample ID Comp/Grab Matrix' Depth Date Time
_.._..- ....... ................ -. ._.-.. _-- --- _
ntrs
Shipped via: Fel Standard
Remarks Sample z (lab onlvh
u Foa-r as
SS
.,�o ?Ok
2
x
x
1
* MatrixRemarks:
emp
COC Seal Present/intact; N
GW- Groundwater B- Bioassay
WW Waste Water
DW - Qrinking Water
OT - Other
Flow Other
_Y
COC Signed/Accurate: N
Bottles arrive intact: 7:N
Correct tattles Used: _Y _N
—
If Appliable
VOA Zero Headspa": ^V _Y _N
Preservation Correct/Checked: Y N
RAb Screen. <0.5 mR/hr:
Samples ret ed via:
—Uri Ier
14
Re4inquis b i natur
Date:
Time:
Received by {Signahirel
Trip Blartk Received: Yes /
HCL / MeoH
TBR
Relin uish d by : (Signature)
D te:
Time:
Received by: (Signature)
Temp, oc Bottles Received:
If preservation required by Login: Date/Time
M=
Relinquished by : (Signature)
Date:
Time:
Receive or la : (Signature)
Date: Time:
e0 , 1
Hold:
Condit'
NCF / OK

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Lear Corp. WQ Permit Number: WQ0041666
WWTP Name: Lear Corporation WWTP NPDES Number: NC0002305
Monitoring Period: From l/l/2020 To 12/31/2020
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ElAlt
B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
...................................................
Class B:
Alt. (1) Fecal Density p
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
I Air Drying ❑
I Composting ❑
jAerobic Digestion LI
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
um er of
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -pique
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
752
768
784
MPN/g
0
Annually
G
SM92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction)
❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. Oz uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑ I Alt. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed
LI
CERTIFICATION STATEMENT (please check the appropriate statement)
1 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Brent Collins - Director of Technical Services Brent Collins; Director of Technical Services
Preparer Name and Title ((tvbe or print) Land Applier Name and Title (if applicable)(type or print)
4�'�"' 2/5/2021Z4;2- 2/5/2021
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Analytical Results
EMA Resources, Inc.
755 Yadkinville Rd.
Mocksville, NC 27028
Receive Date:
01/09/2020
Reported:
01/10/2020
For:
Guliford Mills
Comments:
Geometric Mean= <764 MPN/g
STATESVILLE
C ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
200109-23-01
Fecal Coliforms
GM-1
<763
MPN/g
SM92210E-2006
01/09/2020
CL
200109-23-01
Percent Solids
GM-1
2.62
%
SM2540B-2011
01/09/2020
CL
200109-23-02
Fecal Coliforms
GM-2
<766
MPN/g
SM92210E-2006
01/09/2020
CL
200109-23-02
Percent Solids
GM-2
2.61
%
SM2540B-2011
01/09/2020
CL
200109-23-03
Fecal Coliforms
GM-3
<752
MPN/g
SM92210E-2006
01/09/2020
CL
200109-23-03
Percent Solids
GM-3
2.66
%
SM2540B-2011
01/09/2020
CL
200109-23-04
Fecal Coliforms
GM-4
<766
MPN/g
SM92210E-2006
01/09/2020
CL
200109-23-04
Percent Solids
GM-4
2.61
%
SM2540B-2011
01/09/2020
CL
200109-23-05
Fecal Coliforms
GM-5
<775
MPN/g
SM92210E-2006
01/09/2020
CL
200109-23-05
Percent Solids
GM-5
2.58
%
SM2540B-2011
01/09/2020
CL
200109-23-06
Fecal Coliforms
GM-6
<769
MPN/g
SM92210E-2006
01/09/2020
CL
200109-23-06
Percent Solids
GM-6
2.60
%
SM2540B-2011
01/09/2020
CL
200109-23-07
Fecal Coliforms
GM-7
<784
MPN/g
SM92210E-2006
01/09/2020
CL
200109-23-07
Percent Solids
GM-7
2.55
%
SM2540B-2011
01/09/2020
CL
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 200109-23-01 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 200109-23-02 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 200109-23-03 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 200109-23-04 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 200109-23-05 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 200109-23-06 Temp on Arrival:
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 200109-23-07 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Page 4 of 4