WQ0001759_Regional Office Historical File Pre 2018 (3)

State of North Carolina
Department of Environment,
Health and Natural Resources
Mooresville Regional Office
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary IDEIHNFR
Division of Waste Management
Hazardous Waste Section
May 30,1997
To- Rex Gleason, Supervisor
Division of Water Quality/Water Quality Section
Throu& Keith Masters
Compliance Unit Supervisor
Hazardous Waste Section
From- Jesse W, Wel]14UA�
Waste Management Specialist
Hazardous Waste Section
RE: City of Statesville 1,J a-0 0 U f 7 "1
Fourth Creek Monofill
Sampling and Analysis Report
Statesville, Iredell County, NC
Attached is information regarding the subject facility. The facility has completed sampling
activities required by the HWS, After review, it has been detertnined that at this time, the
hazardous waste regulations (RCRA) do not apply to this site Our review of the assessment
report did indicate that site conditions exist which may warrant a review by your office.
Consequently, we respectfully refer this site to your section for consideration. Please advise
should you have any questions.
attachment
cc- Doug Holyfield
Central Files
919 North Main Street,
Mooresville, North Ccarotin 28115
Voice 704-663-1699
FAX 704k&3��6040
An Eclud 01*6r"ty/AffirmdtIVe Adflon �mployer
ros�w/l 0,% post -cons r

Sampling and Analysis Report
Fourth Creek Mono ill
City oStatesville
Statesville, North Carolina
sv " s ° , "
May , 1997
prepared for
City of Statesville
Statesville, North Carolina
for submittal to
North Carolina Department of Environment,
Health and Natural Resources
es
Division of Wa to Management
Hazardous ante Section
prepared by
+uaterra, Inc.
Greensboro, North, Carolina

Terra0 ENRONMLCO V�ENTANSULTANTS:
P.,,,i 0-tu BOX 49532 - NC 27419 - (9M852 5003 - F A 9M,
A GREAT LAKES CHEMICAL CORPORATtON COMPANY
May 22,1997
Ms. Renee Parkman
Assistant Director
City of Statesville Water/Wastewater Treatuient
Post Office Box 1111
Statesville, North Carolina 28687-1 Ill
Subject: Sampling and Analysis Report
Fourth Creek Nionofill
City of Statesville
Statesville, North Carolina
Aquaterra job Pilo. 7302301
Dear Ms. ParkiiTan:
Aquaterra, Inc. (AqUaterra) is pleased to provide this Sawp,�n , g and Ania4,szs Repon for the sampling
activities conducted at the Fourth Creek Monofdl located outside the city fit -nits of Statesville, North
Carolina. This report was prepared in response to a March 3, 1997 request by the North Carolina
Department of Encironfrient, Healdi and Natural Resources (NCDEHNR), Division of Waste
Management PWNI), Hazardous Vlaste Section q-1XVS), Mooresville Regional Office (kth'(D),Tlrr
field activities and laboratorvanalvses discussed in this report were conducted in accordance wifli the
,�amp&zg andAna#jis Plan (,SXP) prepared by Aquateria dated April 3, 1997, 'll'a's, SAP was approved
by die -AV in a letter dated April 11, 1997.
Aquaterra appreciates the opportunity to provide environmental consulting services to the City of
Statesville. If you have any questions or require additional information, please do not hesitate to
contact us at 910, 52.500 .
Sincerely,
AQUATERR,A, INC.
Edward M. Kuhn, P.G.
Project Manager
Susan Kite, P-G,
Senior Project Manager
pc: Mr. Jesse Wells - NCDEHNF, DW7NI, FIWS, MooresEffle Regional Office
GR70341EMKISKIjo
CORPORATE HEAD QUART ERR; 49111 NC 27606 - 919, 859 9987 - Fex o917 1 8599930

Fourth Creek MonofilI
City of Statesville
Stattsvi*i North Car4na
May 22, IM
PINEENEURN=
The City of Statesville (the City) operates Fourth Creek Wastewater Treatment Plant (%'W7P) arid
Moncifill located cast of the city limits of Statesville, North Carolina (see Figure 1), The site operates
under an NPDES permit (Permit No. NCO031836) and a nondischarge permit (lie it No.
WQ0001759). On February 24,1997, the City became aware that, sludge from the Statesville Water
Treatment Plant and the Third Creek VAVIT exceeding the ceiling concentration for chromium had
been disposed of in three trenches at the Fourth Creek Monofill (see Figure 2). The chrornium
concentration of the sludge analyzed from the Statesville Water Treatment Plant on July 30, 1996
was reported to be 425 rng/kg, The chrorniurn concentration of the sludge analyzed from the Third
Creek W%V1-P on July 30, 1996 was reported to be 393 mg/kg- The concentrations in these sludges
are in violation of the ceiling concentration for chromiurn of 260 mg/ k-g (Pennit No. WQ0001759,
Permit Condition, Part 11 (2)),
Based on a March 3. 1997 request from the North Carolina Department of Environinerit, Health,
and Natural Resources (NCDFMNR), Division of Waste Management PWIM), Hazardous Waste
Section (FRKS), the City elected to characterize die sludge contained in the three trenches at the
Monoffil to deternime whether the sludge is a hazardous waste (40 CFR 262,11). Aquaterra, Inc.
(Acluaterra) prepared a SampYng avd 4nabsif Plan (SAP) dated April 3, 1997 that described the
-re. 7ntis SAP was approved in
activities and methodologies to be used to characterize the waste stud g
a Apra 11, 1997 letter from Mr. Jesse Wells of the HWS. The sludges were analyzed by the Toxicity
Characteristic Leaching Procedure (TCLP) to determine the concentration of the eight RCRA metals,
In addition, one sample from each trench was also analyzed for volatile and semi -volatile orb is
compounds (VOC-s and SVOCs) according to theTCLP method.
2 Scope of Service
1"his Sam 'ping and Ana_4sis Itoott describes the approach that was used to characterize waste sludge in
the monofill trenches at the Fourth Creek Monofi]l (see Figure 2). The sludges were sampled and
analyzed for chromium said the other RC: RA metals by the `CLP method. In addition, one sample
from each trench was also analyzed for VC Cs and SVOCs. Tlie objective for characterizing the
sludge was to determine whether it was hazardous waste based on the concentration of chromium
contained in the sludge.
Aquaterra has prepared this Sa,-np#n ,g and AnaAjis Report based on the recommendations received
from the DSW, and it into rates accepted methods and procedures published in US EPA
guidance documents that Aquaterra has employed on sintilar projects under NCDF--.T-LNR,
FIVIS review.
PAGE 1, OF 9

QWWA,
GR7034
May 22, 1 "7
3 Project Organization
'fhe pto*ffi
t organization was designed to ecienfly complete the samplin& analysis and data
reporting to characterize the sludge at the City of Stateville's Fourth Creek Morrofill- The
responsibility for sample collection, management; coordination, and reporting was assigned to Nfs.
Susan Kite, the Project Manager. Duties of the Project Manager included the following-
• Direct on -site operations
• Ensure safe operation of on -site activities
• Work closely with the Assistant Director of Water/Wastewater for the City of Statesville
• Control project schedule and budget
• Chrersee miy subcontractor operations assigned to this project
Trained sample collection technicians collected all samlrs. The s,,unple team for the monofill
trenches utilized a direct push smi4)ler to advance the borings. The sample collection team collected
samples, documented and labeled the samples, packaged the samples, and transferred the samples to
die analytical laboratory.
Ile Project Manager tracked all samples from the time they were collected in the field through the
analysis process, All field and analytical data obtained during this project was reviewed by the
Project Manager to ensure that the requirements of the Sampkng and Ana#,ds Plan dated April 3, 1997
have been met.
4 Monoritl Trench Sludge Sample Locations
Four composite samples were collected for laboratory analysis from each individual monofill trench.
flie sampling be by dividing each trench into four sections of approximately equal lengths. Two
soil borings Nvere located withiri each section of a trench (see Figure 3). A core sample representing
the ftill depth of each boring was collected; then the two core samples were!nrixed together to create
a composite sample of the sludge in the first quarter of the moncifill trench. The same sampling
procedures were repeated in each of the other three sections of the manofill trench. Each of the
three trenches were sampled this same way. This sampling Procedure produced four separate
composite samples from each monofill trench, for a total of twelve composite sarriples, 'I'liese
samples were collected for analysis for the eight RCRA metals from die monofill area. In addition,
one grab sample from each trench was analyzed for VC)Cs and SVOCs.
5 Mormfill Trench Sample Collection Procedures
Two direct push operators and a swnple collection technician sampled the sludge material in the
monofill trenches. 'Ilie operators were responsible for advancing the borings from which the sludge,
samples were collected. Each boring in the monofill trenches was advanced through the soil
overburden to the tipper surface of the sludge material. At that time:, a 4-foot long, I -inch interior
diameter continuous sampler was connected to sample the sludge material. After the sampler had
been advanced up to 4 feet, the continuous sampler was removed to recover the sample. The
continuous sampler was opened to retrieve the sample, The recovered sample was removed and
PAGE 2 OF 9

Fourth Creek Monofill
GR7034
May 22, 1997
hornogenized to represent the sludge material over the 4-foot interval penetrated by the continuous
sampler, he continuous sampler was re-inserted and -additional sludge material was collected until
reaching the interface between the sludge material and the native soils at the bottom of the trench,
All samples from the boring were then homogenized to form a composite of the full length of the
boring. The mixing was performed manually to obtain a thoroughly mixed composite sample.
After the two borings in each trench quarter section were sampled arid thoroughly tnixed over this
total depth, a composite sample for each trench quarter was fonned using approximately equal
aliquots from each of the two borings in each section. If a composite sample was to be split into
duplicate samples, the procedure discussed in Section 7.3 was followed.
The sample collection technician was responsible for overseeing the sampling and compositing
procedures, and completing all required documentation. The sampling technician also assisted with
decontairrinating the sampling equipment. The direct push team was responsible for
decontaminating the probe and sampling equipment.
Decontamination procedures were performed as described in Section 9.0
5.2 Manual Sample AExing and Composidng Procedures
Composite sludge samples were thoroughly mixed on -site. Manual rnixing and compositing were
accomplished by first placing the individual subsamples that were, to comprise a composite sample
into a stainless steel mixing bowl. Free water was carefully drained from any wet saniples. Debris
such as small rocks and vegetation were then removed, Next, die samples were folixed together and
split into four, equal portions, Each quarter was individually rnixed by hand within the mixing bowl
and then recombined into one sample. The sample was split into quarters again, and the, process of
rnixing each quarter and combining repeated. A representative sample for analysis was then
collected out of the irtixing bowl by removing an approximately equal aliquot from each qu,.u-ter of
the mixing pan and combining them into as clean, labeled sample container. If a duplicate sample
was to be, prepared, a second container was filled in the same manner as the original sample by
taking approxisnately equal aliquots from each quarter of the rttixing pan. Tee samples were then
properly identified as described in Section 6.0 and handled and shipped as described in Section 11 O
61 Sample Container Labels
All samples were properly labeled,%vith a tag fastened to the sample bottle. Sample container labels
were completed with waterproof black ink and included the following info nation at a mu-iinium
8 Sample number
Date and time of sample collection
Location of sample collection
Analysis required
Preservative added, if any
Name/initials of the collector
Designation of "grab" or "composite" sample

Fourth Creek Montifill
GR7034
May 22, 1997
Sample labels were completed for each sample container as the samples were collected. The labels
were attached to each container before it was filled. After filling, each conniner was sealed, wiped
clean, and placed into a plastic resealable bag.
6.2 Chain-of-Costody Record
A Chain-of-Custorly Record (C.O(.) was maintained for all samples collected and shipped off -site,
during this project. This record desigriated the location of samples shipped off site, 'Ihe Project,
Manager subsequently tracked all samples. A COC was completed for every group of samples to be
shipped off -site, and the CO was sealed in a rescalable bag and taped to the inside of the lid of the
cooler.
When transferring the possession of samples, the individuals relinquishing mid receiving the samples
signed, dated, and noted the time on the COC.
Possession of samples collected in the field was dm-urriented from the time the sample was collected
until it is disposed of. Chain -of -custody records are used to -attest to samples being in a person's
custody under the following criteria:
• The samples were in physical possession.
• 'Me samples were m=,itained in view after being in possession.
® '11e samples were in physical possession and then transferred to a designated secure
area or forwarded to an express delivery firm,
7 Field Quality Control Samples
To ensure the reliability and validity of the field and analytical data compiled in this sampling and
analysis program, the folloNving sections descrit.)e quality control (QC) field samples that were
collected.
ZI TWp Blank Samples
No aqueous samples were collected for volatile compound analysis'; therefore, no trip blank samples
were collected.
Z2 Equipment Rinsate Samples
Equipment rinsate samples were taken during the sampling effort and were analyzed only for total
chromium. They were taken at a rate of one, for every five composite samples, Equipment rinsates
were collected after the final decontarrunation rinse of the sampling equipment (see Section 9,0 for
decontainination procedure). 1-he rinsate sample was collected by rinsing deirinized water over and
through the sample equipment (e.g,, core sampler) and recovering it in the sample-nrixing pan. The
rinse water was they transferred from the bowl to an appropriately labeled bottle and submitted to
the laboratory for too, chromium analysis. The purpose of the equipment rinsate was to confirm
that the decontamination procedures were adequate and to check for potential contamination
residues on the sampling equipment.
PAcis 4 oF 9

Fourth Creek Monofill
GR7034
May 22, 1997
Field duplicate samples were collected at a rate of one duplicate sample for every five composite
samples. the field duplicate samples consisted of a second sarnple that is a split of the original
composite sample. The duplicate samples were analyzed for TCLP metals. oa collect the duplicate
sample, approximately equal aliquots were taken from the compositing bowl and were placed into
two identical sample containers. The original and duplicate samples were then identified with
unique sarnple numbers and documented as required in Section 6,0. 'nie purpose of field duplicates
was to provide a quality control indicator concerning the variabaity associated with the field
sampling and analytical procedures.
Matrix spike samples &,ere prepared during analysis of the sample s to evaluate the accuracy of the
laboratory methods and to determine if the recovery of the spiked materials was affected by the
sample matrix. Matrix spike samples were prepared for this project in the laboratory by spiking die
'I'C-I,P extract prior to analyzing the extract, 'I'lle matrix spike results obtained allowed the laboratory
method to be evaluated by measuring recovery of the spike. The puqose of analyzing a matrix spike
duplicate sample with a marrix spike, sample was to evaluate the variance U'l the applied andyncal
method,
8 Sample Collection Equipment
All sampling equipment was constructed of stainless steel or Teflon when feasible to avoid any
interference with the target analytes. Wieri possible, disposable sampling materials and equipment
were utilized to reduce decontarturiation <efforts and the potential for cross-cont inating samples.
Equipment rinsate samples discussed in Section 7.2 were collected to verify cleaidiness of the
sampling equipment.
9: Sample Equipment Decontamination
All samplirig equipment was properly cleaned before, its initial use and between distinct sample
locations that were not co posited together. These procedures were necessary to prevent or
imnimize the introduction of potential contamination between distinct sample points,
Decontamination took place at a decontamination station designed to contain waste decontamination
solutions. 'fhe decontarnination -area was located close to the area under investigation, All
equiprnern decontamination solutions were containerized on -site in 55-gallon steel drarms.
hidividual sampling equipment that contacted the sarnple matrix was not cleaned between fraction
takes of the same composite sample-, however, the equipment was decontarninated before collecting
a different composite sample. 'Ihe continuous samplers were decontaminated before boring in each
of the four sections of a monofdl trench, Decontamination was not required between borings, in the
same section.

Fourth Creek Mon
GR7034
May 22, 1997
9.1 Decontamination Procedures
Decontamination procedures for the sampling equipment were as follows',
• Wash sampling equipment thoroughly with non phosphate laboratoq detergent and potable
tap water, using plastic or metal brushes to remove any particulate trutier or surface Film.
• Rinse equipment with potable tap water.
Rinse equipment with isopropyl, alcohol.
lZinse equipment thoroughly with deionized water.
■ Wtap equipment with clean plastic wrap or aluminum foil.
92 Disposal ofDccontaminadon Liqzdds
All liquids generated during equipment decontamination were collected and appropriately labeled for
disposal All waste liquids %vere stored on -site icy 55-gallon drurns, and will be returned to the waste
water treatment plant facility for final disposal.
10 Sample Containers
Sample containers and caps were new, precleaned containers made of material(s) recommended by
EPA in 40 CF`R 136 and S\V-846. Sample containers were provided by die analytical laboratory, and
were previously cleaned according to EPA guidelines and included a 10% rutnic acid solution rinse,
followed by a distilled water rinse, followed by an isopropyl -alcohol rinse.
11 Sample Preservation, Packaging, and Shipping
Samples were collected in appropriate containers and preienred according to the analytical method
requirements. Sample holding tines stated in the approved analytical methods were met.
Samples were packed in accordance with the U,S. Department of Transportation POI)
reqUircruClItS, Samples were placed on ice immediately and chilled to a temperature of
approximately VC and maintained at that temperature by means of refrigeration or ice until fliey
were received at die laboratory. preservatives, if required, were added to the samples at die time,
they were collected.
,AJI sample coolers were transferred directly to laboratory personnel.
12 Sample Handling and Tracking
12.1 Sample Handling
When samples were received at the contract laboratory, the laboratory signed the appropriate section
on the' OC to acknowlerig ,,e receipt of the samples,

GR7034
M# 22,1997
E99012MIZ=
Sample tracking was accomplished by using the contract laboratory savpk and Analysis Data Entg
Form -.Nrex, Samp ks form and the COC form.
12.3 Sample Disposal
Samples collected at this site and transferred to die analytical laboratory will remain at the laboratory,
until it is determined that no forther analysis will be required. Once no further analysis is required,
the method of disposal will be derennined. Samples will be disposed of by the laboratory.
13 Health and Safety Requirements
All on -site activities were conducted in a safeatid healthful manner. Prior to the comniencernent of
the on -site activities, a site specific Fleakh and Safety Plan (14ASP) was prepared and provided to all
contractor and subcontractor personnel assigned to the project, The HASP prescribed the,
procedures that were to be followed by all personnel while working on -site to perform the 'activities
described in this report. The method and procedures in the TIASP were consistent with 0SI-Lk
regulations and comply with federal, state, and local regulations.
A safety meeting was conducted by the site supervisor for personnel assigned to the project prior to
the start of the project. Items covered in the meeting were activities to be Performed, potential
chemical and physical job hazards, and health and safety procedures to he followed. No person was
aya in meral, e
allowed near any site operation without first being given a site h , rd briefing: In ge th
briefing consisted of a review of the safety meeting.
14 Iabnratory AnAytical Methods
The composite samples were analyzed for the eight RCRA metals including chrormurn, according to
the TCIT IMethod 1311 as set foith in 40 CFR, 261 Appendix 11. The leachate was analyzed for the
eight RCF—,'i metals utilizing EPA Method 6010, or an equivalent method as set forth in SVI-846,
The equipment rinsate sr pies were analyzed for chroanuin utilizing EPA %lethod 6010 only, The
TCLP extraction is not necessary for water samples. In addition, the grab samples collected from
the site were analyzed using the TCLP for VC Cs according to SIXT-846 Alethod 8240 and for
SVOCs according to S%XL846 &lethod 8270.
15 Investigation Results
The depth of the soil overburden in Trench #1 ranged from one to three feet below land surface.
The sludge depth in Trench # 1 ranged from 11 to 13 feet below farad surface, One grab sample was
collected from this trench at a depth of eight feet below land surface for analysis of V 0 Cs and
SVOCs using the TCLP- The depth of the soil overburden in Trench #2 ranged from six inches to
three feet below land surface, The sludg depth iii Trench #2 was approximately 12 feet below land
surface. One duplicate sample was collected from the first quadrant of this trench for TCLP Metals
analysis, The depth of the soil overburden in Trench #3 ranged from six inches to four feet below
land surface. The sludge depth in Trench #3 ranged from nine to ten feet below land surface, One
PAc,E 7 oF 9

Fourth Creek Manofill
GR7034
May 22,1997
grab sample for analysis of VOCs and SVOCs using the TCLP and one duplicate sample for TCLP
Metals analysis were collected from the third quadrant of this trench. Figure 3 shows the locations
of the borings advanced in each trench. Boring log-, for each trench are contained in Appendix A.
mnnlzz���
The analytical results for all samples collected from the Fourth Creek Nionofdl site are SUfflularized
inTable l. The complete wialytical reports for A samples are contairled in Appendix B.
I&I Trench #1
"I"he sample collected from Trench # 1, Quadrant # 1 (I'l -Q 1) indicated detectable concentrations of
mm-)
arsenic (0,068 mg/L), barium (0-21 rng/L)miu , chrom (0-076 1rig/L), ercury (0.00073 g/l,grad
selenium (0,006 mg/L). The conceritrations of the other RCRA metals in this sample were below
the method detection limu�-
The sample collected from Trench #1, Quadrant #2 (1'1,-Q2) contained detectable concentrations of
arsenic (0,026 mg/L), barium (0.48 m /L), chrornium, (0.022 mg/T,.,), mercury (0,00021 mg/l,), and
9
selenium (0,012 /1)® The COLICentrationS of the other RCPZ-A metals in this sample were below
the method detection limit,
The sam, ple collected front Trench # 1, Quadrant #3 (rl-Q i) contained detectable concen trations of
arsenic (0.012 mg/L), barium, (1.4 mg/l,), and chromium (0.041 mg/L), The concentrations of the
other RC R.A metals iti this sarriple, were below the method detection lirnit.
The sample collected from Trench #1, Quadrant #4 (ri-Q4) contained detectable concentrations of
barium (0,47 mg/L), The concentration,.; of the other RCRA metals in this sample were, below the
method detection limit.
16.2 Trench #2
The sample collected fromTrerich #2, Quadrant #1 (172-Q1) contained detectable concentrations of
barium (1-1 rng/L)- 'nie held duplicate sample collected from this quadrant Cf2-QlD) contained 1.3
mg/L of barium and 0.011 mg/L of cadmium. The concentrations of the, other RCRA metals in
these samples were below the method detection limit.
The sample collected from Trench #2, Quadrant #2 (I'2-Q-1) contained detectable concentrations of
barium (1,5 mg/L)� Die concentrations of the other RCRN metals in this sample were below the:
method detection limit.
The sample collected from Trench #2, Quadrant #3 (T-?-Q3) contained detectable concentrations of
barium (1.7 mg/L). The concentrations of die other RCRA metals In this sample were, below, the
method detection Iii-nit.
The sample collected from Trench #2, Quadrant #4 (T2-( 4) contained detectable concentrations of
barium (1.8mg/L) and cadium (0.023 mg/L). The concentrations of the other RCRA metals in
this sample were below the method detection limit.
PAGE 8 OF 9

Fourth Creek Monofill
GR7034
May 22, 1997
The sample collected ftom Trench #3, Quadrant #1 (f3-Ql) contained detectable concentrations of
arsenic (0.070 mg/L) and barium (0.52 nig/L). 'I"he concentrations of the other RCRA metals in this
sample,ivere below the method detection limit.
The sarnple collected frorn Trench #3, Quadrant #2 (1'3-Q2) contained detect -able concentrations, of
arsenic (0.010 mg/L) and barium (1,2 nig/l.). The concentrations of the other RCRA metals in this
sample were below the method detection limit,
T'he sample collected fromfeench #3, C,)uadrant #3 (F3-Q3) contained detectable concentrations of
arsenic (0.009 nig/1) and barium, (1.3 trig/1). The field duplicate sample collected from this
quadrant (r3-Q3D) contained 0,99 mg/L of iurn. The concentrations of the other RCIL,\ metals
in these samples were below the method detection limit.
The sample collected from Trench #3, Quadrant #4 (1'3-Q4) contained detectable concentrations of
barium (L2 mg/L) and cadiniurn (0.014 rng/l,). The concentrations of die other RCRA metals -ill
this sample were below the method detection limit-
16 4 Other Analytical Results
'Flee grab samples collected frorn'rrench #I Trench #2 (r2-G) and Trench #3 (1'3-G) did
not cont;iici VOCs or SV0- Cs in concentrations that exceeded the method detection linut. The two
rinsate samples collected from the site (E-D-I and ED-22) did not contain total chromium in
concentrations that exceeded the method detection limit,
17 Conclusions and Recommendations
None of the samples collected from the Fourth Creek IMoncifill facility contained concentrations of
the eight RCRA metals that exceed the federal TCLP regulatory limits (40 CF1Z 261.24), For
comparative purposes, 'Fable 1 lists the respective TCLP regulatory limit for each of the eight RC JA
metals along with the concentrations of the metals detected in samples collected during this
investigation. In addition, VOCs mid SVC Cs were not present in concentrations above the
laboratory method detection limits.
Based upon these analytical results, the material disposed of in the three trenches at the facility
should not be considered hazardous waste. A copy of this report should tie submitted to I'Vir. Jesse
Wells the NCDFJ-IN'R, DARN4, HVIS Mooresville Regional Office,

w
Trcmh #1
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04
03
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Legend
Gwprobe Sample Uxation
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1-ayers Data Title
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Statesville, i-,brthCa-oEna

Table t , Analytical Results, Fourth Creek Monofill Facility, Statesville, North Carolina
Notes:•:
A& units in tqglL
NA = Not zod
TCLP AqaljsesA Methods 8240 and 8270 were below rnethad dete an &miisfor all compounds,
An tic . tbaratog.- t tical Smices, ins, Flunteraille, North Cam&na and Haorstanr Texas.
G

Boring /Well Construction Log
Well Construction Permit Number Aquaterra, Ina
Project Name Fourth Creek rlt Contractor Geologic Exploration
Project N. 02301 _ registration No. trig
Geologist ynes Driller Nelson
Start Date Complete Date &W7 Equipment Geoprobe
quaterra r of

iConstruction
1 I
I lipip
Riser 7�pe
M
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, III I II�IIIIIII I I
VariesV n depth.
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lip
Aquaterra, Inc.
Aquaierra Dm-BAmWog, Pagei

Boring AVell Construction Log
Well Construction Permit Number Aquaterra, Its
1. D. Number T -Q 1, Q r Q3, Q4 Purpose -Charactefization _
Project Name Fourth Creek norill Contractor Geologic Exploration
Project No. 7302301 --Registration No. N
Geologist THeynes Driller Nelson
Start Date , 7 Complete Date r' 7 Equipment Geoprobe
Drilling thod Direct push Geoprobe,
o—Mments `drench T3 approx. 100' long", with lest " underwater,
D,lP D
ell ont coon Tlepth '-Blow Count ppm
Information From To 6" o,r it 6" Soil d bock Description Comments Depth (ft.)
ore role I: ia. ` - 1 - sehll w area of sludge a 5-6
Miser v°pe Push to 1 ` in 1 st point of Q 1. 2nd
Diameter point sludge at 4 r 10'
oreerl Type
Diameter
Riser terval
Aquaterra Doc-BlanUeg, Pagel

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Cal Huntersville, NC 28078
Tel: [phone]
Fax, 704-875-9091
May 21, 1997
Ms. Susan to
Aquaterra Environmental Consultants
4600 Dundas St.
Suite 105
Greensboro, NC 27407
RE: PACE Project No. 670506.520
Client Reference: 7302301/4,th Creek Monofill
Dear Ms. Kite:
Enclosed is the report of laboratory analyses for samples received
May 06, 1997.
Footnotes are given at the end of the report.
If you have any questions concerning this report, please feel free
to contact us.
Sincerely,
Felicia C Grogan
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical sere s, Inc,

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NG 28078
Tel: [phone]
Fax: [phone]
Aquaterra Environmental Consultants May 21, 1997
4600 Dundas St. PACE Project Number: 670506520
Suite 105
Greensboro, NC 27407
Attn: Ms. Susan Kite
Client Reference: 7302301/4th Creek Mono ill
PACE Sample Number: 92 0090780
Date Collected: 05/05/97
Date Received: 05/06/97
TI-G
Parameter Units PRE Leachate METHOD DATE ANALYZED
TCLP BASE/NEUTRAL & ACID EXTRACTABLES
8270
Pyridine
mg/L
0.50
NO
05/12/97
1,4-Dichlorobenzene
mg/L
0.75
NO
05/12/97
1,2-Cresol
mg/L
20
NO
05/12/97
Hexachloroethane
mg/L
0.30
NO
05/12/97
1,3 & 1,4-Cresol
mg/L
20
ND
05/12/97
Nitrobenzene
mg/L
0.20
ND
05/12/97
Hexachlorobutadiene
mg/L
N.
NO
05/12/97
2,4,,6-Trichlorophenol
mg/L
0.20
NO
05/12/97
2,4,5-Trichlorophenol
mg/L
40
NO
05/12/97
2,4-Dinitrotoluene
mg/L
0.013
ND
05/12/97
Hexachlorobenzene
mg/L
0.013
NO
05/12/97
Pentachlorophenol
mg/L
10
NO
05/12/97
Surrogate - 2-Fluorophenol
%
46
05/12/97
Surrogate - Phenol-dS
%
34
05/12/97
Surrogate - Nigro benzene-d5
%
69
05/12/97
Surrogate - 2-Fluorobiphenyl
%
48
05/12/97
Surrogate - 2,4,6-Tribromophenol
%
67
05/12/97
Surrogate - Terphenyl-d14
%
28
05/12/97
Date Extracted
Date
050797
05/07/97
REPORT OF
LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace
analytical services, Inc.

Pace Analytical Services, Inc,
9800 Kincey Avenue, Suitt! 100
ja Analy. =*I
Huntersville, NG 28078
Tel; 704-875-9092
Fax: [phone]
Ms. Susan Kite
May 21,
1997
Page 2
PACE Project Number: 670506520
Client Reference: 7302301/4th
Creek Monofill
PACE Sample Number:
92 0090837
Date Collected:
05/05/97
Date Received:
05/06/97
Client Sample ID:
T1-QI
Parameter
Units
PRL
Leachate
METHOD DATE ANALYZED
INORGANIC ANALYSIS
'TCLP RCRA TOXICITY METALS
1311
Arsenic
mg/L
0.01
0.068
05/12/99
Barium
mg/L
0.010
0.21
05!08/97
Cadmium
mg/L
0.010
NO
05/08/97
Chromium
mg/L
0.010
0.076
05/08/97
Lead
mg/L
0.10
NO
05/08/977
Mercury
mg/L
0.0002
0.00073
0502/97
Selenium
mg/L
0.005
0.006
05/08/97
Silver
mg/L
0.050
ND
05/08/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services,
Inc,

Pace Analytical Services, Inc,
9999
Kincey Avenue, Suite 10
Hunters ille, NG 28078
Tel: 70 - 7 -999
Fax: [phone]
s. Susan Kite
May 21,
:1997
Page 3
PACE Project r: 670506520
Client Reference: 71/4th
Creek !`lnrrnfill
PACE Sample umber:
92 0090845
Date Collected:
05/ 5/ T'
Date Received,
U /U5/97
Client Sample ID:
1-Q
Parameter
Units
P L
Leachate
METHOD DATE ANALYZED
INORGANIC ANALYSIS
TCLP RCRA TOXICITY METALS
1311
Arsenic
mg/L
0.005
0.026
05/ 9/97
Barium
9/L
0.010
0.48
05/08/97
Cadmium
rng/L
0.01'0
NO
05/0 /97`
Chromium
rig/L
0.010
0.022
05/08/97
Lead
erg/L
0.1
ND
5/ , 97
Mercury
g/L
0.0002
0.00021
5/1 /97
Selenium
/L
0.5
0.012
0/97
Silver
Ira /L
0.050
ND
05/ /97
WWW
6

Pace Analytical Services, Inc.
.
9800 Kinceyr Avenue„ Suite 189
Huntersvilie, NC 28078
TO', 704-875-9982
Fax- 704.875-9091
Ms. Susan Kite
May 21,
1997
Page 4
PAGE Project Number: 57050552
Client Reference: 7 02 01`/4th
Creek Mono i 11`
PACE Sample Number:
92 009085 `
Date Collected:
5/0597
Date Received.
5/06/97
Client Sample ID:
T1-
Paraleter
Units
PRE
Leachate
METHOD DATE ANALYZED
INORGANIC ANALYSIS
TLLP'RRA TOXICITY METALS
111
Arsenic
mg/L,
0.005
0.012;
05/ 9/97`
Barium
mg/L
0.010
1.4
05/ 8/97
Cadmium
mg/L
0.010
NO
05/0 /97
Chromium
/L
0.010
0.041
05/ 8/97
Lead
mg/L
0.10
NO
05/ /97
Mercury
mg/L
0.0002
ND
05/12/97
Selenium
g/L
0.005
ND
05/ /97
Silver
mg/L
0.050
ND
05/ /97REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full;
without the written consent of Pace Analytical Services, Inc,

Race Analytical services, Inc
9500 Klncey Avenue, Suite 100
Huntersyslle, NC 28078
TO 704-75-909
Fax: 704m975-9091
Ms. Susan Kite
May 21,
1997
Page 5
PACE Project Number: 670506520
Client Reference: 7
0 01/4th Creek .Mene ill
PACE Sample Number
92 0090861
Date Collected:
05/05/9
Date Received:
0/06/97
Client Sample ID:
T1-Q4
Parameter
Units
PRL
Leachate
METHOD DATE ANALYZED
1
INORGANIC ANALYSIS
TCLP RCRA TOXICITY METALS
111
Arsenic
g/L
0.005
NO
05/09/97
Barium
g/L
0t01
0.47 ,
05/0 /97
Cadmium
g/L
0.050
NO EQ
05/1 /97
Chromium
g/L
0.050
NO EQ
05/13/97
Lead
/L
0.50
NO EQ
05/1/97
Mercury
/L"
0.0002
NO
05/1 /97
Selenium
rig/L
0.005
NO
05/08/97
Salver
lrlg/L
0.5
NO EQ
05/1/97
These data have been
reviewed and are approved
for release.
Margaret S. Harding
_.w
Manager, Laboratory
Operations
REPORT OF LABORATORY
This report shall not he reproduced, except In fuil;
without the written consent of Pace Analytical Services, Inc::

Pace Analytical Services, Inc.
800 Kincey Avenue, Suite 100
Hilntersvill IN0 28078
Tel: [phone]
Fax.[phone]
Ms. Susan Kite, FOOTNOTES May 1 1997
Page 6 for pages l through 5 PACE Project Number: 670506520
Client Reference: 0 01J th Creek Monafill
EQ Elevated quantitation limits resulting from matrix interference
NO Not detected at or above the PLA
PRL PACE Reporting Limit'
1 All analysis performed on Toxic Characteristic- Lea ate
REPORT OF LABORATORY ANALYSIS
This report shad not be reproduced, except in full,
without the written consent of Face Analytical Services, Inc.

Pace Analytical Services, Inc.
*cal
9800 Kincey Avenue, Suite 100
P.j-=.,AnaJ1
Huntersville, NC 28078
TO 704-875-9092
Faxl704-875-9091
Ms. Susan Kite
QUALITY CONTROL DATA May 21, 1997
Page 7
PACE Project
Number: 670506520
Client Reference: 7302301/4th Creek Monofill
Arsenic
Batch: 92 59284
Samples: 92 0090837, 92
0090845, 92 0090853, 92 0090861
METHOD BLANK AND SAMPLE
DUPLICATE:
Duplicate
Method
of
Parameter
Units PRL Blank
930381340
93 0381340
RPD
Arsenic
lag/ f— U—.005 -N-[Y--
—ND—
NO
SPIKE AND SPIKE DUPLICATE:
Spike
Spike Dup]
Parameter
Units PRL 930381340 Spike
Recv Recv
RPD
Arsenic
mg/L 0.005 NO
0.020
—9'2—% —0%
LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE:
Reference
Du
Parameter
Units PRL
Value
Recv Recv
RPD
Arsenic
iiFg —/E 0.005
0.020
1-05%
—2S-%-
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Face Analytical Services, Inc,
9800 Kincey Avenue, Suite 19
Huntersville, NC 2807
TO- 79-575-999
Fax. 70-S75-9091
. Susan Kite
QUALITY CONTROL
DATA
May 21, 1997
Page 8
PACE Project Number: 605850
Client Reference: 08014th Creek
Monofill
Mercury
Batch: 92 59304
Samples: 92 0090845, 92 0090861
METHOD BLANK AND SAMPLE DUPLICATE.'
920090861 Duplicate
Hatred TI-4 of
Parameter
Units
PPL
Blank Leachate 92 00 861 PPU
SPIKE.
920090861
T-4 Spike
Parameter
Units
PPL
Leachate §Rike Pear
Re—rcury8.
UU
U.UU I04
LABORATORY CONTROL SAMPLE;
Reference
Parameter
Units
PRL
Value Rc
W rcu _
L
B.CCC
T 00-2 104

s. Susan Kite QUALITY CONTROL DATA
Page
Client Reference: 1P4th Creek Monofill
Mercury
Batch: 92 59353
Pace Analytical Services, Inc.
9800 incey Avenue,, Suite 19
Huntersville, NG 28078
Tel: 704-875@9992
Fax- 79-975-9991
May 21, 1997
PACE Project Number: 670506520
METHOD BLANK AND SAMPLEDUPLICATE:
920090853 Duplicate
Method T-
Parameter Units PRL Runk Leachate 92 0090853 R
e ry .CC - - Il _ C
SPINE.
CS
Tl-03-
Spike
Parameter
Units PRL Lea hate
Spi e
Ree
LABORATORY
CONTROL SAMPLE;'
Reference
Parameter
Units PRL
Valle
Recv
erc r
F C . CCC
. C �
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced, except in full,
without the written consent of Pace Analytical SeMces, Inc:

Pace Analytical Services, Inc.
9800 KinceyAvenge, Suite 10
Hun ersville, NC 28078
Tel: [phone]
Fax:[phone]"
Ms. Susan Kite
QUALITY CONTROL DATA May
21, 1997
Page 10
PACE
Project
Number: 670506520
Client Reference: 7 02 01/4th Creek M000fill
Selenium
Batch: 92 59242 ;
Samples: 92 0090837, 92
0090845, 92 0090853, 92 0090861
METHOD BLANK AND SAMPLE
DUPLICATE.
Duplicate
Method
of
Parameter
Units ` PRL .bl ank
920089413
92 00 941
RPD
e en i u 1
f L 0.005 ND
RID—
N - __®ND
SPIKE AND SPIKE DUPLICATE:
Spike
Spike Dul
Parameter
Units PRL 920089413
§pjke
Recy Recy
RPD
Se ei m
li1g/ L . 05 ND `
0.020
104° 102
LABORATORY CONTROL. SAMPLE AND CONTROL SAMPLE DUPLICATE.
Reference
Dull
Parameter
UnitsPRL
value
Recv Recv
RPD
S —eFe—n a u m
1ttg / L 0.005
0.020
104 1 D
1 `
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced,except in full,
without the written consent of nice Analytical Services, Inc,

Pace Analytical services, Inc.
Kincey Avenue, suite 100
Hu tersvtlie; NC 28078
Tel; 704-875-9092
fax: [phone]
e
. Susan Kite QUALITY CONTROL
DATA
May 21,997
Page 11
PACE Project Number: 670506520
Client Reference: 7302301/4th Creak
Monofill
ICP QUALITY CONTROL
Rat. 92 59255
Samples: 92 009037 92 0090845, 92
0090g3, 92 0090C1
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method
T
Parameter
Units
PRL
Blank
920090381 92 0090381 RPU
INDIVIDUAL PARAMETERS
Cadmium
mg/L
0.010
NO NO NC
1CP QUALITY CONTROL
Barium
mg/L
0.010
1.2 1.2 U
Aluminum
mgL
0.10-
NO
Antimony
g/L
U. U,
NO
Arsenic
mg/L
0.50
NO
Barium
mg/L
0®010
NO
Beryllium
mg/L
0.010
NO
Boron
tag/L,
0.10
NO
Cadmium
mg/L
0.010
NO
Calcium
mg/L
0.10
NO
Chromium
mg/L
0.019
NO
Cobalt
g/L
0.010
NO
Copper
mg/L_
0.010
NO
Iron
mg/L
0.050
NU
Lead
mg L
01.10
NU
Magnesium
g/L
Uk 9
N[1
Manganesemg/L
0.010
NO
Molybdenum
/L
9.05
NO
Nickel
mg/L
0.05
NO
Potassium
gL
1.0
N
Selenium'
mg/L -
0.50
NU
;Silver
mg/L
0.050
NO
Sodium
mg/L
0.20
NO
Thallium
mg/L
0.50
NO
Tin
mg/L
U.0
NO
Titanium
mg/L
C®CC
NO
Vanadium
mg/L,
0*01
NO
7n
mg/L
0.10`
NO
�r ar w y •® y �i t �
Thisfewpoortetra I not be reproduced, except in full,
without the written consent of iytioa) S�ervioes, [ft.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Hunter vllle, N0 28078
Tel: [phone]
Fax: [phone]
s. Susan Kite, QUALITY CONTROL DATA May 21, 1997
Page 12 PACE Project Number: 670506520
Client Reference; 7302301/4th 'Creek Monofil
ICP QUALITY CONTROL
Batch: 92 59255
Samples: 92 009037, 92 00904,
92 009053, 92
009051
SPIKE AND SPIKE DUPLICATE.
Parameter
Units
PRL-
920090381
S i
A uminum
m L
0.10
1:6
50
Antimony
mg/L.
0.20
NO:
5.0
Arsenic
mg/L
0.50
NO
5.0
Barium
mg/L
0.010
1.2
5.0
Beryllium
mg/L
0.010
NO
1.0
Boron
mg/L
0.10
0.16
1.0
Cadmium
mg/L
0.010
NO
1.0
Calcium
mg/L
0.10
1.4
100
Chromium
mg/L
0.010
NO
1.0
Cobalt
mg/L
0.010
0.014
1.0
Copper
mg/L
0.010
0.10
1.0
Iron
mg/L
0.050
NO
50
Lead,
mg/L
0.10
NO
5.0
Magnesium
mg/L
0.20
1.7
50
Manganese
g/L
0.010
0.45
1.0
Molybdenum
mg/L
0.05
NO
1.
Nickel
mg/L
0.05
NO
1.0
Potassium
mg/L
1.0
2.1
100
Selenium
mg/L
0.50
NO
5.0
Silver
mg/L
O.050
NO
5.0
Thallium
leg/L
0.50
NO
5.0
Tin
mg/L
0.20
NO
1.0
Titanium
mg/L
0.010
NO
1.0
Vanadium
mg/L
0.010>
NO
1.0
Zinc
mg/L
0.010
0.19
5.0
REPORT OF LABORATORY1
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
Spi ke
Spike
Oupl
Recv
Recv
RP
97
9
91 %
93
2
9
97
1`
92`
94
2
100
100`
0
93
94
1
95
95
1°
92
92
0
93
93%
0
92`
92
0
95
95
1
91
91
0
92
92%
0°
95
96
0
91
92
1
90
90
0
92Y.
91
I'r
90
101
3
10
109
1
91
91
0
91
91
0`
00
3
4
93`
94
1
94
95
1
95
95
0

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
TO 704-875-9092
Fax: [phone]
Ms. Susan Kite
QUALITY CONTROL DATA
May 21, 1997
Page 13
PACE Project
Number: 670506520
Client Reference: 7302301/4th
Creek Monofill
1CP QUALITY CONTROL
Batch: 92 59255
Samples: 92 0090837, 92 0090845, 92 0090853, 92
0090861
LABORATORY CONTROL SAMPLE AND
CONTROL SAMPLE DUPLICATE:
Reference
Dupl
Parameter
Units
PRL
Value
Recv Recv
RPD
Al _u _mfin_u m—
M—g /T—
0.10
5_0_
--9T%— —92—%
—I %
Barium
mg/L
0.010
5.0
89% 90%
1%
Beryllium
mg/L
0.010
1®0
92% 93%
1%
Cadmium
mg/L
0.010
1.0
90% 91%
1%
Chromium
mg/L
0.010
1.0
89% 90%
1%
Lead
mg/L
0.10
5.0
89% 90%
1%
Magnesium
mg/L
0.20
50
92% 93%
1%,
Manganese
mg/L
0.010
1.0
90% 91%
1%
Potassium
mg/L
1.0
100
93% 94%
1%
Selenium
mg/L
0.50
5.0
90% 91%
1%
Silver
mg/L
0.050
5.0
90% 90%
0%
Sodium
mg/L
0.20
50
90% 91%
1%
Titanium
mg/L
0.010
1.0
90% 91%
1%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite too
Cal
Huntersvitle. NC 28078
Tel: [phone]
Pax. 704.7-909
Ms. _Susan Kite
QUALITY CONTROL
DATA
May
21 1997
Page 14
PACE
Project
Number: 670506520
Client Reference: 7 02 01/4th Creek Monnfill"
TCLP BASE/NEUTRAL & ACID ETRLTABLES
Batch: 92 5928
Samples: 92 0090780
METHOD BLANK.
Method
Parameter
Units
PRL
Blank
Pyri ine
mg/
1,4- ichlnrnbenzene
L
0.75
N
1,2-Cresol
rig/L
20
N;
He achlnr ethan
g/L
0.30
NO
1, 1,4-Cresol
mg/L
20
NO
Nitrobenzene
mg/L_
0.20
N
He achlor butadiene
mg/L
0.05
ND
2,4,5-Trichlor phenol
mg/L
0.20
N
2,4,5-Trichlorophenb
mg/L
40
N
2,4- initrotoluene
g/L,
0.013
N
He achlor bent n
mg/L
0.013
N
Pentachl orophenol
mg/L_
10
N
Surrogate - 2-Fl uorphenl
54
Surrogate - Phenol-5
5
Surrogate - Nitrobenzene-d5
91`
Surrogate d 2-Fluordbiphenyl
85
Surrogate - 2,,5-Tribro ophendl
B;
Surrogate - Terphenl-d14
112
LABORATORY CONTROL SAMPLE;
Reference
Parameter
Units
PRL
Value
Rec
Pyridine
Ing/
C.
1,4- 7chld n enzend
mg/L
0.75
0.50
78
1,2-Cresol
mg/L
20
0.50
82
He achloroethane
mg L
0.30;
0a50
72
1, 1,4Cresol
mg/L
20
1.0
77
Nitrobenzene
m9/L
0.2
0.5
92
e a hlorobutadiene
mg/L
0.05
0.50
5
2,4,5-Trichlorophenol
mg/L
0.20
0.50
185
2,4,5-Trichlerophen l
mg/L
40
0.50
1 4
2,4- initrotolu ne
mg/L
0.013
0.50
112
He achlorobenzene
mg/L
0.013
0.50
140
This rep rt shall not be produced, except in fUll,
'rs a.

Pace Analytical Services, Inc
9800 Kincey Avenue, Site 19
Ntrritersvik NC 28078
Tel: [phone]
Fax. [phone]
. Susan Kite QUALITY CONTROL DATA May 21, 1997
Page 15 PACE Project Number: 670506520
Client Reference: 7302301/4th CreekMonnfill'
TLP BASE/NEUTRAL & ACID EXTRACTABLES
Rater
Samples:
LABORATORY CONTROLSAMPLE:
Reference
Parameter Units PRL Value Recv
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full
without the written consent of Face Analytical Services, Irks

Pace Analytical Services, Inc.
A 9800 Kinney Avenue, Suite 100
Hunter villa, NC 28078
Tel: [phone]
Fax. [phone]
Ms. Susan Kite FOOTNOTES May 21, 1997
Page 16 for pages 7 through 15 PACE Project Number: 670506520
Client Reference: 7302301/4th Creek Monofill
NC No calculation due to value below detection limit.
NO Not detected at or above the PR.
PRL PACE Reporting Limit
RPD Relative Percent Difference
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in Nit,
without the written consent of Pace Analytical Services, Inc,

CHAIN -OF -CUSTODY RECORD
Analytical Request
Merit � . ,r t�
i r C
Re r To; �.
Face Client No,
Address
Bill To: __.
Rre eat tw1n er
F .O. #t ; Bitiir Referent
Face Project No
Phone
lame ! �rct
*Re ue D to
Sampled By (PRINT)
� .
PRESERVATIVES ANALYSESw
�
LU
REQUEST
LU
Dampier Signature
Date Sampled
0
u r"
Y
a
„ v
0.
y+�,
..
Co 4 J
Additional Comments

Face Analytical Services, Inc;
8 0 ince Avenue, Suite 188
untersville, NC 28078
TO 70-875-80
Fax: [phone]
May 20, 1997
Ms. Susan Kite
q aterra Environmental Consultants
4600 Dundas St.
Suite 105
Greensboro, NC 27407
RE: PACE Project e. 670507.51
Client Reference, 70014th Greed Moncifill
Dear Ms. Kite:
Enclosed is the report of laboratory analyses for samples
received
May 07, 1997.
Footnotes are given at the end of the report.
If you have any questions concerning this report, please
feel free
to contact us.
Sincerely,
..
Felicia E Grogan
Project Manager
Enclosure
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Puce Analyucal Services, Int,

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Cal Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Aquaterra Environmental Consultants May 20, 1997
4600 Dand St. PACE Project Number: 670507512
Suite 105
Greensboro, NC 27407
Attn: Ms. Susan Kite
Client Reference: 7302301/4th Creek Monofill
PACE Sample Number: 92 0091493
Date Collected: 05/06/97
Date Received: 05/07/97
ED-1
Parameter Units PRL METHOD DATE ANALYZED
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chromium mg/L 0.010 ND 200.7 05/10/97
10 woo

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
-'Ar-Ask "W Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Ms. Susan Kite May 20, 1997
Page 2 PACE Project Number: 670507512
Client Reference: 7302301/4th Creek Monofill
PACE Sample Number: 92 0091590
Date Collected: 05/07/97
Date Received: 05/07/97
Client Sample ID: ED-2
Parameter Units PRL METHOD DATE ANALYZED
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chromium mg/L 0.010 ND 200.7 05/10/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
+ Huntersville, NC 28078
N-4111111111 A&
Tel: [phone]
Fax- 704-875-9091
Ms. Susan Kite May 20, 1997
Page 3 PACE Project Number: 670507512
Client Reference: 7302301/4th Creek Monofill
PACE Sample Number: 92 0091604
Date Collected: 05/06/97
Date Received: 05/07/97
Client Sample ID: T2-Q1
Composite
Parameter Units PRL Leachate METHOD DATE ANALYZED
-0-
INORGANIC ANALYSIS
TCLP RCRA TOXICITY METALS
1311
Arsenic
mg/L
0.005
ND
05/12/97
Barium
mg/L
0.010
1.1
05/08/97
Cadmium
mg/L
0.010
ND
05/08/97
Chromium
mg/L
0.010
ND
05/08/97
Lead
mg/L
0.10
ND
05/08/97
Mercury
mg/L
0.0002
ND
05/12/97
Selenium
mg/L
0.005
ND
05/08/97
Silver
mg/L
0.050
ND
05/08/97

Pace Analytical Services, Inc.
900 Kincey Avenue Suite 100
untereviile; NC 28078
Tel: 7C4-878-9 9
Fax: [phone]`
Ms, Swart kits
May 20,
1997'
Page 4
PACE Project Number: 67050751
Client Reference: 730 3Q1/4th
Creek Monofill
PACESample Numbers
92 0091612
Date Collected:
5/06/97
Date Received:
05/07/97
Client Sample Igo
-1
Composite
Parameter
Units
PRL
Leach to
METHOD DATE ANALYZED
INORGANIC ANALYSIS
TCLP RCRA TOXICITY METALS
1311
Arsenic
g/L
0.005
ND
05/09/97
Bari
m /L
0.010
1.3
05/08/97
Cadmium
mg/L
0.010
0.011
05/08/97
Chromium
leg/L
0.010
Ng
05/08/97
Lead
g/L
0.10
ND
05/08/97
Mercury
mg/L
0.0002
NO
05/1 /97
Selenium
mg/L
0.005
ND
05/08/97
Silver
mg/L
0.050
ND
05/08/97

Pa Analy
tical lytca Services,
ice, Inc.
9800
KIncey Avenue; Suite 100
untersvtllea NC 28078
Tel: 79-9m999
Fax: 04- 7 -99 1
M. Susan Kits
May 20,
1997
Page 5
PACE Project umbe • 670507512
Client Reference: 7302301/4th
Creek M nti it
PACE Sample Number:
92 0091620
Nate Collected:
/ /97
Hate :.Rirr
/7/97
Client ent Sample I
T -
Composite
Parameter
Units
PRL
Leachate
METHOD DATE ANALYZED
TTY-
INORGANIC; ANALYSIS
T LP RCRA TOXICITY
METALS
1311
Arsenic
mg/L
0.005N
/ 9/97
Barium
m /L
0.010
1..
S/ /97
Cadmium
m /L
0.010
N;
S/ 8 /97
Chromium
mg/L
0.010/
/97
Leah;
m /L
0.10
ND
/ /97
Mercury
mg/L
0.0002
ND
/1 /97
" Selenium
m /L
0.005
N
5/ /9 t
Silver
m /L
0.050
NCB
5/ /97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fall,
without the wd ten consent of Pace analytical Services Inc.

Pace An lytical Services, Inc,
9 00 Kinsey Avenue, ufte 190
ea AkHunter vi0e, NC 28078
Tet 704-879-909
Fax: [phone]
. Susan Kite May 20, 1997
Page 6 PACE Project umber: 670507512
Client Reference: 7 02 01/4th Creek Monofill
PACE Sample Number: 92 0091639
Date Collected: 05/06/97
DateReceived: 05/07/97
Client Sample I T2-0
Grab
Parameter Units PPL Leaehate METHOD DATE ANALYZED
,
TCLP BASE/NEUTRAL & ACID EXTRACTABLES
8270
Pyridine
mg/L
0.50
NO
05/2/97
1, - 1ehl r be zene
rg/L
0.75
N0-
05/12/97;
1,2-Cresol
mg/L
20
NO
05/12/97
He a hlnruethane
erg/L
0.30
NO
05/12/97<,
1, 1,4-Cresol
lag/L
20
NO
05/12/97
Nitrobenzene
mg/L
0.20
NO,
05/12/97
e a hl rubutadlene
mg/L
0.05
NO
05/12/97
2,4,5 Tri hlor phen l
mg/L
0.20
NO
05/12/97
2,4,5-Trhlnraphendl
mg/L
40
NO
05/12/97
2,4-Oinitroteldene
mg/L.
0.013
NO
05/12/97`
e a hlurnbenz ne
mg/L
0.01
05/12/97
Penta hlurephen l
mg/L
10
NO
05/12/9
Surrogate - 2-Fluerophenbl_
50
05/12/97
Surrogate Phenol- 5
4
05/12/97
Surrogate - Nitrobenzene-d5
95
05/12/97
Surrogate - 2-Fluoroiphel
1
05/12/97
Surrogate _ 2,4,5-Tribromphenl
4
05/12/97
Surrogate - Terphenl-d14
90
05/12/97
Date , Extracted
Late
050897
05/08/97
TCLP VOLATILES
8240
Benzene
mg/L
0.05
NO
05/15/97
2-5utanon (E)
mg/L
20
NO
05/15/97
Carbon Tetrachloride
mg/L
0.05
NO
05/15/97`
Chlorobenzen
mg/L
10
NO
05/15/97
Chloroform
mg/L
0.60
NO
05/15/97
1,2- ichldroethane
mg/L
0.05
NO
05/15/97
I,I-Oichloroe hene
g/L
0.07
NO
05/15/97
Tetrachlordethene
mg/L
0.07
NO
05/15/97
Tr chlo oethen
/L
0.05
ND
05/15/97
Chloroethee (Vinyl chloride)
mg/L
0.02
NO
05/15/9
7t'rep:; $h;I not be reproduced, exceWo to,

Pace Analytical Services, Inc,
A
9800 Kincey Avenue, Suite 100
kc
Eac
Huntersville, NC 28079
Tel: [phone]
Fax: [phone]
Ms. Susan Kite
May 20,
1997
Page 7
PACE Project Number: 670507512
Client Reference:
7302301/4th Creek Monofill
PACE Sample Number:
92 0091647
Date Collected:
05/06/97
Date Received:
05/07/97
Client Sample ID:
T2-Q3
Composite
Parameter
Units
PRL—
Leachate
METHOD DATE ANALYZED
INORGANIC ANALYSIS
(rF-
TCLP RCPA TOXICITY
METALS
1311
Arsenic
mg/L
0.005
NO
05/09/97
Barium
mg/L
0.010
1.7
05/08/97
Cadmium
mg/L
0.010
NO
05/08/97
Chromium
mg/L
0.010
Ni
05/08/97
Lead
mg/L
0.10
NO
05/08/97
Mercury
mg/L
0.0002
ND
05/12/97
Selenium
mg/L
0.005
ND
05/08/97
Silver
mg/L
0.050
NO
05/08/97
REPORT OF LABORATORY ANALYSIS
This report shelf not be reproduced, except in full,
without the written consent of Pace
Analytical Services, Inc,

Pace Analytical Services, Inc.
9899 Kincey Avenue, Suite 190
Huntersville;, NC 289 8'`
Tel: [phone]
Fax: [phone]'
M. Susan Kite
May 20,
1997
Page 8
PACE ProjectNumber: 670507512
Client Reference: 7302301/4th
Creak Monofill
PACE Sample Number:
92 0091655
Date Collected:
05/06/97'
Date`Received:
5/07/9
Client Sample ID
T2- 4
Composite
Parameter
Units
PRL
Leachate
METHOD DATE ANALYZED
PT -
INORGANIC ANALYSIS
TCLP RCRA TOXICITY METALS
1311
Arai
m/L
0.005
NO
05/09/97
Barium
m /L
0.010
1.8
05/08/97
Cadmium
m0/L
0.010
0.023
05/08/97
Chromium
m /L
0.010
ND
05/08/97
Lead
m /L
0.10
ND
05/08/97
Mercury
m9/L
0.0002
ND
05/12/97
Selenium
m9/L
0.005
NO
05/08/97
Silver
m /L
0,050
ND
05/08/97
REPORT OF LABORATORY
This report shall not be reproduced, except in full, p
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 Klncey Avenue, Suite 100
Wall
Huntersvllle, NG 28078
Tel; 794- 7 -909
Pax; 7 4-97 -909
s* Susan Kite
May
20, 1997
Page 9
PACE
Project Number: 67050751
Client Reference: 7 C C1/4tF`
Creek Monofill
PACE Sample Aber
0055
Date Collected:
0/0/7
Date Received:
0/07/7
Client Sample ID:
T -1
Composite
Parameter
Units
PRL
Leachate
TT -
METHOD DATE ANALYZED:
INORGANIC ANALYSIS
TCLP'RCRA TOXICITY METALS
111
Arsenic
/L
0.01
U�07
05/0/7
Barium
/L
0.010
0.52
05/0/ 7
Cadmium
m/L
0.010
ND
05/0/7
Chromium
m /L
0.01
C1
05/0/ 7`
Lead
rat /L
0.10
U
05/0/ 7
Mercury
m/L
C.CCC
U
05/1/7"
Selenium
/L
C. 05
NO
05/1 /57
Silver
mU/L`
0.50
NO
05/0/7

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
AM A—
Huntersville, NC 28078
Tel: [phone]
Fax., 704-875-9091
Ms. Susan Kite
May 20,
1997
Page 10
PACE Project Number: 670507512
Client Reference: 7302301/4th
Creek Monofill
PACE Sample Number:
92 0091671
Date Collected:
05/06/97
Date Received:
05/07/97
Client Sample ID:
T3-Q2
Composite
Parameter
Units
PRL
Leachate
METHOD DATE ANALYZED
INORGANIC ANALYSIS
TCLP RCRA TOXICITY
METALS
1311
Arsenic
mg/L
0.005
0.010
05/09/97
Barium
mg/L
0.010
1.2
05/08/97
Cadmium
mg/L
0.010
NO
05/08/97
Chromium
mg/L
0.010
NO
05/08/97
Lead
mg/L
0.10
NO
05/08/97
Mercury
mg/L
0.0002
NO
05/12/97
Selenium
mg/L
0.005
NO
05/13/97
Silver
mg/L
0,050
NO
05/08/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace
Analytical Services, Inc:

Pace Anatyfical Services, Inc.
9800 Kinsey Avenue, Suite 100
alyt* al
Huntersvilte, NC 28078
TO: 704-876-9092
Fax: [phone]
Ms. Susan Kite
May 20,
1997
Page 11
PACE Project Number: 670507512
Client Reference: 7302301/4th
Creek Monofill
PACE Sample Number:
92 0091680
Date Collected:
05/07/97
Date Received:
05/07/97
Client Sample ID:
T3-Q3
Composite
Parameter
Units
PRL
Leachate
METHOD DATE ANALYZED
09-
INORGANIC ANALYSIS
TCLP RCRA TOXICITY METALS
1311
Arsenic
mg/L
0.005
0.009
05/09/97
Barium
mg/L
0.010
1.3
05/08/97
Cadmium
mg/L
0.010
ND
05/08/97
Chromium
mg/L
0.010
NO
05/08/97
Lead
mg/L
0.10
NO
05/08/97
Mercury
mq/L
0.0002
ND
05/12/97
Selenium
mg/L
0.005
NO
05/13/97
Silver
mg/L
0.050
NO
05/08/97
............

Pace Analytical Ser*es, Inc.
A
9800 Kincey Avenue, Suite 100
CaL
Huntersville, NC 28078
Tel, 7G4-875-9092
Fax: [phone]
Ms. Susan Kite
May 20,
1997
Page 12
PACE Project Number: 670507512
Client Reference: 7302301/4th
Creek Monofill
PACE Sample Number:
92 0091698
Date Collected:
05/07/97
Date Received:
05/07/97
Client Sample ID:
T3-Q4
Composite
Parameter
Units
PRL
Leachate
METHOD DATE ANALYZED
(IT
INORGANIC ANALYSIS
TCLP RCRA TOXICITY METALS
1311
Arsenic
mg/L
0.005
ND
05/019/97
Barium
mg/L
0.010
1.2
05/08/97
Cadmium
mg
0.010
0.014
05/08/97
Chromium
mg/L
0.010
NO
05/08/97
Lead
mg/L
0.10
NO
05/08/97
Mercury
mg
0.0002
ND
05/12/97
Selenium
mg/L
0.005
ND
05/08/97
Silver
mg/L
0.050
ND
05/08/97
I MINE

Pace Analytical Services, Inc.
900 Kincey Avenue„ Suite 100
Huntersville; NC 28078
`el. 704- 79-9092
Fax. 70 - 7 -9091
N. Susan Kite
May 20,
1997
Page 13
PACE Project umber. 670507512
Client Reference, 7302341/4th Creek Menefill
PACE Sample Number.
92 0091701
Date Collected.
05/07/97
Date Received:
05/07/97
Client Sample 14t
T3-0
Grab
Parameter
Units
PRL
Leachate
METHOD DATE ANALYZED
RGA 1C ANALYSIS
TCLP BASE/NEUTRAL & ACID E TRACTABLES
827
Pyridine
mg/L
0.50
NO
05/12/97
1,4- lehlnrebenzene
mg/L
0.75
NO
05/12/97
1,2-Cresol
mg/L
20
NO
05/12/97
Nexachloreethane
mg/L
0.30
NO
05/12/97
1,3 & 1,4-Cresol
mg/L',
20
NO
05/12197
Nitrobenzene
mg/L
0.20
NO
05/12/97
Ne achlor beta lene
mg/L
0.05
NO
05/12/97
2,4,-Trichlorphenol
mg/L,
0.20
NO
05/12/97
2,4,5-Tri hlorophen l'
9 L
40
NO
05/12/97
2,4-initrotoluene'.
g/L
0.013
NU
05/12/97
Neaehlorebenzene
mg/L,
0.013
N0
05/12/97
Pentaehlorophenol
mg/L
10
NO
05/12/97
Surrogate - 2-Fluorophenol
44
05/12/97
Surrogate - Phenol-d
30
05/12/97
SurrogateNitrobenzene-d5
5
05/12/97
Surrogate - 2-Fluord ipheoyl
%
77
05/12/97
Surrogate - 2,4,5-Tribromophenol
79
05/12/97'
Surrogate - Terphenyl-d14
88
05/12/9
Date Extracted
Date
050897
05/ 8/97'
TCLP VOLATILES
8240
Benzene
mg/L_
0.05
NO
05/15/97
2-Butanon(NEK)
mg/L
20
ND
05/15/97
Carbon Tetrachloride
mg/L
0.05
NO
05/15/97
Chlorobenzene
mg/L
10
NO
05/15/97
Chloroform
"
mg/L-
0.60
NO
05/15/97
1,2-ichloroethane
m9/L
0.05
NO
05/15/97
l,l-ichloroethene
mg/L
' 0.07
NO
05/15/97'
Tetrachlorethene
m/L
0.07
NO
05/1/97
Trichloroethene,
mg/L
0.05
0.02
NO
NO
05/1 /0
05/15/
Chlor~oethene ('vinyl chloride)
mg/L
REPORT OF
LABORATORY ANALYSIS
This report shall not be reproduced, except'in full,
(..
PRIMMMAIMMMETITaror,"71=1

Pace Analytical Services, Inc,
800 Kincey Avenue, Suite 100
Hunteraville, NC 2 078
Tel; 704-875-9092
Fax:74-7-C1
. Susan Kite
May -0,
1997
Page 14
PACE Project Number: 670507512
Client Reference: 7 0 01/4t Creek
enofill
R 0.
PACE Sample umber
00 171
Date Collected: :
0/07/7
g y
Date Received.
0/07/7
Client Sample ID:
T3-Q30
Composite
Parameter
Omits
PRL
Leaeitate
METHOD DATE ANALYZED
INORGANIC ANALYSIS
T LP RCRA TOXICITY METALS
1311
Arsenic
r0/L
0.005
NO
0 /0 / 7
Barium
m0/L;
0.010
0.99
0 /0 / 7
Cadmium
/L
0.010
ND
0/0/7
Chromium
ring/L
0.010
NO
0 /0 / 7
Lead
In/L
0.10
R0
0/00/7
Mercury
a1 /L
0.0002
NO
0 /1 / 7
Selenium
m0/L
0.005
ND
05/p8/97
Silver
mg/L
0.050
ND
0 /0 7
These data have been reviewed and are approved
for release.
a '
Margaret S. Harding
Manager, Laboratory Operations
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,-
without the written consent of pace Analytical Services, Inc,

Pace Analytical Services, tnc.
9590 Oicey Avenue, Suite 10,
li
calHunter ville, IBC 897 .
iet 794-875-999
Fax: [phone]
. Susan Kits FOOTNOTES May 20, 1997
Page 15 for pages 1 through 14 PACE Project Number: 670507512
Client Reference: 7302301/4th Creek Monofill
NO Not detected at or above the PL.
PPL PACE Reporting Limit
1 A11 analysis performed on Toxic Characteristic Le ch te.
LABORATORYREPORT OF L
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, rho:

Pace Analytical Services, Inc,
9800 Kincey Avenue, Suite 100
Huntersville, NO 28079
Tel- 704-875-9092
Fax, 704-875-9091
Ms. Susan Kite QUALITY CONTROL DATA
May 20, 1997
Page 16
PACE Project Number: 670507512
Client Reference: 7302301/4th Creek
Mono ill
Arsenic
Batch: 92 59284
Samples: 92 0091604, 92 0091612, 92
0091620, 92
0091647,
92 0091655
92 0091663, 92 0091671, 92
0091680, 92
0091698,
92 0091710
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method of
Parameter
Units
PRL
Blank 930381340 93 0381340
RPD
A—rsenic
-m—g/U-
0—.005
Wb-- RF— NO
N—C
SPIKE AND SPIKE DUPLICATE:
Spike
Spike Dupl
Parameter
Units
PRL
930381340 Spike Recv Rev
RPD
A—rsenic
mg —/L
U-005
WDT — U 020
LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE:
Reference Oupl
Parameter
Units
PRL
Value
Recv Rev
RPD
A—rsenic
mg/L
0.005
--0 —.U-0 1-03% -il-2%
_M5%
gaidow

Pace Analytical 5rvisx Inc,
9859 Kincey Avenue, wife 189
Ical
HuntersvOl ; NC 28078
Tel: [phone]
m 794-875-9891
Ms. Susan Kits QUALITY CONTROL DATA
May 20, 1997
Page 17
PACE Project
Number: 670507512
Client Reference: 7302301/4th Creek
Mnnnt`i11
Mercury
Batch; 92 5934
Samples: 92 60 16 4 92 0091612, 92
0091620, 92
BU 1647,
92 0091655
92 0091663, 92 0091671, 92
0091680, 92
0091698,
92 009171
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method
of
Parameter
Units,
PRL
Blank 990661
9 6990661 RFD
rr r -
Fg /L
- 0
NUNU
NU NL
SPIKE:
Spike
Parameter
Units
PRL
920090861 Spike
Re v
Mercury
/L
0.0002
NO 0.005
194'
LABORATORY CONTROL SAMPLE:
Reference
Parameter
Units
PRL
Value
R cv
rc
Mercury
mg 6'
O. O
_ O.00 —
reportThis

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
+1 rd
Huntersville, NG 28078
Tel -I 704-875-9092
Fax, 704-875-9091
Ms. Susan Kite
QUALITY CONTROL DATA May
20, 1997
Page 18
PACE
Project
Number: 670507512
Client Reference: 7302301/4th Creek Monofill
Selenium
Batch: 92 59242
Samples: 92 0091604, 92
0091612, 92 0091620, 92 0091647, 92 0091655
92 0091698, 92
0091710
METHOD BLANK AND SAMPLE
DUPLICATE*
Duplicate
Method
of
Parameter
Units PRL Blank 920089413
92 0089413
RPD
SeTe—nium
N-9— O
mg/L 0.005 N
ff-D—
N—C
SPIKE AND SPIKE DUPLICATE:
Spike
Spike Dupl
Parameter
Units PRL 920089413
§pJke
Recy Recy
RPO
S-eTe—nium
mg —/L 0—.005 N-D
0 - F2-0
WO 4-% 1-02-%
LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE:
Reference
Dupl
Parameter
Units PRL
Value
Recv Recv
RPD
_751-H
TO e n —iu—L
07-005
--6—.020
TORK 1—I9Y.
30.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of use Anatytical Services, Inc,

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 10
in A
Huntersville, NC 28078
Tel, 704-875-9092
Fax;704-875-8091
. Susan Kite QUALITY CONTROL
DATA
May 20, 1997
Page 19
PACE Project
Number: 670507512
Client Reference. 733014th Creek
Mcui11
Selenium
Batch: 92 59347
Samples: 92 0091663, 92 0091671, 92
0091680
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
gq
Method
of
Parameter
Units
PRL.
Blank 920089405
92 0089405
RPD
Se erlrul
/L
.005
NO
NL
SPIKE AND SPIKE DUPLICATE.:
Spike
Spike Uupl
Parameter
Units
PRL
99406 S 1ke
Recv Recy
RPU
Se -'Fe n i u m
ar/L
0.005
N U.0
S
S
LEI MI
LABORATORY CONTROL SAMPLE AND CONTROL SAMPLEDUPLICATE:
Reference
Oul
Parameter
Units
PRL
Value
Recv Recv
RPLI
Se enru
"9/L
0.005
O.Q O
9 101
404
..sir! � •. ^.s r •.

Pace Analytical Services, Inc.
950Kincey Avenge, suite t@
Hunterswille, NG 28078
TO 70-875-9092
Fax° 79 - 75-99 t
Ms. Susan Kite
QUALITY CONTROL DATA
May 20, 1997
Page 20
PACE Project
umber. 670507 12
Client Reference: 7 2 g1/4th Creek Monofill
ICP QUALITY CONTROL
-
Batch: 92 6925
Samples: 92 0091604, 92
0091612, 92 009162 , 92
00916 7
92 0091655
92 009166 92
0091671, 92 00916 , 92
0091698,
92 0091710
CNCD BLANK AND SAMPLE
PLICATE.
Duplicate
Method
of
Parameter
Units
PRL
Blank 920090381
92 0090381 RPO
INDIVIDUAL PARAMETERS
Cadmium
mg/L
0.010
NO
ND NC-
I P QUALITY CONTROL
Barium
mg/L
6.010
1.2
1.2 C
Aluminum
mg/L
0.10
N
Antimony
mg/L
0.20
NO
Arsenic
mg/L
0.50
NO
Barium
mg/L
0.010
NO
Beryllium
mg/L
0.010
NO
Boron
mg/L
0w10
N
Cadmium
tog/L
0.010
NO
Calcium-
tg/L
0#10
NO
Chromium
mg/L
0.010
N
Cobalt
g/L
0.010
ND
Copper
erg/L
0.010
NO
Iron
mg/L
0.06
NO
Lead
mg/L
0.10
N
Magnesium
mg/L
0#2
Ng -
Mangan s
m / L
0.010
N
Molybdenum
/L
0.05
N
Nickel
mg/L
0.05
NO
Potassium
mg L
1.0
N
Selenium
mg/L
0.50
NO
Silver
mg/L
0.050
N
Sodium
mg/L
0.20
N
Thallium
/L
0»60
N
Tin
mg/L
0.20-
NO
Titanium aniu
erg/L.'
0.010
NO
Vanadium
I g/L
0,010
ND
LABORATORYREPORT OF ANALYSIS
This report shall not be reproduced, except in hail,;
4
without the written consent of Pace
Analytical Services Inc:

Fax.7 - 75- 091
. Susan Kite QUALITY CONTROL DATA May 20, 199
Page 21 PACE Project Number: 670507512
Client Reference: 221/ih Creek Nnnnfill
ICP QUALITY CONTROL
Rah: 92 59255
Samples: 92 0091604, 92 0091612, 92 0091620, 92 0091647, 92 0091655,
92 0091663, 92 0091671, 92 0091680, 92 0091698, 92 0091710
METHOD BLANK AND SAMPLE PLICATE:
Duplicate
Method
Parameter Units PRL Bland 920090381 92 0090381 RP
Inm9/ 1 N
SPIKE AND SPIKE DUPLICATE:
Anam
Silver
Thal I i um
Tin
Titanium
Vanadium
Zinc
E
Units
PRL
920090381
Spike
g/L
0-.10
1,
mg/L,
0w2
ND
5.,
mg/L,
0.50
ND
5.
mg/L
0.010
1.2
5:0
mgL
0.010
ND
1.
mg/L
0.1
0.15
1.
mg/L
0.010
NO
1.0
mg/L
0.10
1.4
10
g/L
0.010
0.014
1.0
9/L
0.010
0.10
1.
mg/L
O.050
NO
5
g/L
0.10
NO
5.
mg/L
0.20
1.7
5
mg/L
0,010
0.461.0'
tag/L
0.05
ND
1.
tag/L
0.59
ND
5,
g/L
0.050
NO
5.0
mg/L
0.50
NO
5.
g/L
O.20
NO
1.
lag/L
0.010
ND
1.0
fg/L
0.010
NO
1.
9/L
0.010
0.19
5.0
LABORATORYREPORT OF ANALYSIS
This report rt h ll not be reproduced, except un full,
without the written consent of Pace Analytical Services, Inc,
:1
s
94
95 95

Pace Analytical Services, trip,
9800 in Avenue,1 quite Cll
Huntersville, NC 5Q
Tel: [phone]
Fax: [phone],91
. Susan Kite
QUALITY CONTROL DATA
May
20, 1997
Page 22
PACE
Project
umber:
5 050 51
Client Reference: 7302301/4th Creek Monofill
ICP QUALITY CONTROL
Rah: 92 5955
Samples: 92 0091604, 92 0091612,
92 0091620,
92 0091647,
92 0091655
92 0091663, 92 0091671,
92 0091680,
92 0091698,
92 0091710
LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE
DUPLICATE:
Reference_
Oul
Parameter
Units
PRL
Value
Recv
Recv
RP
AT—uminummg
L
0
91
9 °
1
Barium
m L
0.010
5.0
09
9
1%
Beryllium
g L
0.010
1.0
9
9
1
Cadmium
l g/L
0.010
1.0
90
91
1
Chromium
mg/L
0.010
1.0
09
90
1
Lead
g/L
0.10
5.0
9
90
1
Magnesium
m L
0.20
50
9
9
1
Manganese
fg/L
0.010
1.0
90
91
1
Potassium
mg/L
1.0
100
9
9
1
Selenium
mg L
0.50
5.0
90%
91
1
Silver
- /L
0.050
5.0
90
90
0
Sodium
tg L
0.20
50
90
91
1
Titanium
lg/L
0.010
1.0
90
91`
1
REPORT OF LABORATORY ANALYSIS
This report stall not be reproduced, except in full;
4hout the rritt n consent of Pace Analytical Services. Inc;

Pace Analytical Services, Inc,
0 Kincey Avenue, Suite 100
Huntervifle, NC 28078
Tel: 704-8Fax 75-9042
s. Susan Kits
QUALITY CONTROL
DATA
May
20, 1997
Page 23
PACE
Project Number: 670507512
Client Reference: 7331/4th Crk_Mnrrfi11
1CP QUALITY CONTROL
Batch: 92 59308
Samples: 92 0091493, 92 0091590
MPTBCg BLANK AND SAMPLE DUPLICATE
Duplicate
Method
of
Parameter
units
PPL
Blank
930387217 93 0387217 BP
'A urnnual
g/L
C, C
CBg
Antimony
g/L
0.20
NO
Arsenic
mg/L
0.50
N
Bari
mg/L
0.010
N
Beryllium llium
g/
0.010
N
Boron
g/L
0.10
N
Cadmium
rig/L
0.010
N
Calcium
mg/L
0.10
N ,
Chromium
mg/L
0.010
N
Cobalt
mg/L
0.010'
N
Capper
mg/L
0.010
N
Iron
mgL
0.050
N
Luau'
mg/L
0.10
N
Magnesium
mg/L
0.20
N
Manganese
/L
0.01
N
Molybdenum
mg/L
C.0 '
N
Nickel
g/L
0.05
NO
Potassium
mg/L
1.0
NO`
Selenium
g/L
0.50
NO ;
Silver
mg/L
0.050'NO
Sodium;mg/L
0.20
Thallium
Ong/L
0.50
NO
Tin
mg/L
0.20
NO
Titanium
mg/L
0.010
N
Vanadium
mg/L
0.010
N
Zinc
1g/L
0,010
N
report shallw .

Pace Analytical Services, Inc,
9800 Kinsey Avenue, Suite 100
untersville, NC 28078
Tel. [phone]
w 704-875- 0 1
. Susan Kite
QUALITY CONTROL
DATA ,
May 20, '1997
Page 24
PACE Project
umber*
67050751
Client Reference: 7 01/ th
Creek Monofill
ICP QUALITY CONTROL
Batch: 92 59308
Samples: 92 0091493, 92 0091590
SPIKE. AND SPIKE DUPLICATE:
Spike
Spike
gul
Parameter
Unity
PRL
930387217
S ike
Rec
Rec
RP
umin-um
mg/L
9.1017
Arsenic
mg/L
9.50
ND
5.0
99
101
Barium
mg/L
0.010
0.040
5.0
9
95
Beryllium
mg/L
0.919
ND
1.0
99
100'
1
Boron
mg/L
0.10
1.3
1.0
5
Cadmium
g/L
9,01
NO
1.0
95
97
1
Calcium
g/L
0.1
12
100
95
9
Chromium
mg/L
0.910
NU
1.0
9
95
1
Cobalt
r g/L
0.010'
ND
1.0
92
93`
1
Copper
mg/L
0.010
9.071
1.0
9
93
Iron
mg/L
0.050
1.2
50
9
9
1
Lead'
g/L
0.10
ND
5.0
9
95
1°
Magnesium
mg/L
0.20
9.5
59
9
95
P
Manganese
m9/ L
0.010`
0.097
1.0
9
96
Nickel
/
m9 L
ffUS-
NU
1
9
9
C
Selenium
mg/L
0.59
NU
5.0
9
99
1
Thallium
g/L
0.50
NU
5.0
90
9I
Vanadium
g/L
0.010`
. 035.
110
9
95
1`
Zinc
mg/L
0.010
O.18
5.0
96
9 "
LABORATORY CONTROL SAMPLE AND
CONTROL SAMPLE DUPLICATE:'
Reference
Nul
Parameter
Units
PRL,
Value
Recv
Recv
RPU'
A umiu
mgL
0.1
5
95
95
9
Antimony
g/L
0.20
5.0
9
1
Arsenic
mg/L
0.50
5.0
9 "
99
1
Barium
mg/L
0,010
5.9
96
5
Beryllium
mg/L
0.01
1.0
9
99
1
Rerun
m/L
0.10
1.0
95
97
1
Cadmium
m /L
0.010
1.0
97
9
1
Calcium
m/L
0.10
109
95
95
1

Pace Analytical Services, Inc.
9800 Kincey Avenue,„ Suite 100
H nler vide, NC 2868
Tel: [phone]
Fax. [phone]
s. Susan Kite
QUALITY CONTROL
DATA May
70, 1997
Rage 75
PACE Project
Number:
670507512
Client Reference: 7302301/4th Creek` Monofill
ICR QUALITY CONTROL
Oat: 92 590
Samples: 97 0091493,
97 0091590
-
LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE:
Reference
Ou l
Parameter
Units
RRL
Value
Recv
Rev
RRU
romi u
m /
. 010
..
9
1
Cobalt
m /L
0.010
1.0>
94
94
0 ;
Copper'
1/L
0.010
1.0'
96
9
0
Ire
9L
0.050
90
94%
95
f%
Lead
m/L
0.10
5.0
9
97
Magnesium
m /L
0.20
50
97`
9
1'
Manganese
t /L ;
0.010
1.0
97
90
1
Molybdenum
leg/L
0.05
1.0
97'
97
0%
Mickel
m/L
0.05
1.0
97
94`
7'
Potassium
/L
1.0
100
97
97
0"
Selenium
m /L
0.50
5.0
9
98`
7
Silver
m/L
0.050
5.0
97
97
0
Sodium
m /L
0.70
50;
0
80
0
Thallium
leg/L
0.50
5.0
95
95'
0`
Tin
m9/L
0.70
1.0
104
102
7
Titanium
m9/L
0.010
1.0
9
97
1
Vanadium
m /L
0.010
1.0
9
97
1
Tin
m /L
0.010
5.0
97
9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except;ln full,
without the written consent of Pate Analytical Services, Inc.

Pace Analytical Services, Inc.
9889 Kincey Avenue, Suite 198
Hun eraville„ NC 28Q78-
Tel: [phone]
Fax: [phone]
M. Susan Kite
QUALITY CONTROL
DATA
May 20,
1557
Page 26
PACE
Project
Number: 57 50751
Client Reference: 73031/4th Creek Monofill
TLLP BASE/NEUTRAL & ACID EXTRACTABLES
Batch: 92 59329
Samples: 92 0091639,92 0091701
METHOD BLANK
Method
Parameter
Units
PPL
Blab
Fy rl;ne
mg/L
" 5U
U _�
1,4-U1c lernben ene
mg/L
0.75
NU
1,-Cresol
leg/L
20
NO
Hexachloroethane
g/L
0.30
NO
1,3 & 1,-Cresol
mg/L
20
NO
Nitrobenzene
mg/L
0.20
NU
Neachlurnbutadene
mg/L
0.05
NO
,4,5-Trichlnrnphene
g/L
0.20
N
;,4,5-Trihlrnphennl
mg/L
40
NU
2,4-Uinitr toluene
leg/L
0.013
NU
He achlernben e e
mg/L
0.013
NO
Pentac leruphene
mgL
10
NU'
Serrate --Plunrnphennl
45
Surrogate - Phenol-d5
Surrogate - it're engine-d5
7
Surrogate - - luurupiphen l
75
Surrogate - ,45-Trbrmphenl
1
Surrogate - Terphen l-d14
109
SPIKE
920091701
T3-5
Grab
Spike
Parameter
Units
PPL
Leahate
e
Pec
Pri ine
mg/L
0.50
U
. U
U
1,4-Uichln ben ene
mg/L
0.75
NU
0.5
5 %
1, -Cresol
g/L
20
NO
0.50
95
Ne achlure thane
m /L
0,3
NO
0.50
50
113 & 1,4-Cresol
mg/L
20
NC1-
0.50
1
Nitrobenzene
mg/L
0.20
NO
0.50
7
Neachlorobutadene
m/L
0.05
ND
0.5
4
,4,5-Trich orophenol'
mg/L
Ba g
NO
0.5
,4,5-Tri hlerephene
rig/L
40
NO
0.50
4

Pace Analytical Services, "Inc.
9899 Kince7 Avenue, Suite 100
l-luntersville, SIG 28078
Tel: [phone]
Fax: [phone]
. Susan Kite
QUALITY CONTROL
DATA
May
201997
Page 27
PACE
Project Number: 670507512
Client Reference:
7 2 01/ th Creek Monofill
TLP BASE/NEUTRAL _ AL
_ ACID LTA L5
Batch: 92 59329
Samples: 92 0091639,
92 0091701
SPIKE:
920091701
T^
Grab
Spike
Parameter
Units
PL
Lahat
5 k ev
2, - 1nitrtoln
tg/
l
Hexachlorobenzene
tng/L
0.013
U
0.50
P nt hlornphn» l
mg/L
10
NO
0.50 72
R

Pace Analytical Services, inc.
9800 Kinsey Avenue, Suite 100
.ace.. Icai Huntersville, NC 28070
Tel: [phone]
Fax: [phone]
Ms. Susan Kite FOOTNOTES May 20, 1997
Page 28 for pages 16 through 27 PACE Project Number: 670507512
Client Reference: 7302301/4th Creek Monofill
ail Matrix interference.
NC No calculation due to value below detection limit.
NO Not detected at or above the PRL.
PRL PACE Reporting Limit
PP D Relative Percent Difference
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9888 Kinsey Avenge, Suite 100
Huritersville, NG 28078,
Tel: [phone]
�x`1 8 5-99 1
May 2
Report No.: 00061441'
Section C Page 1
TEST'
ACCEPTANCE'
COME
DETERMINATION RECOVERY
RECOVERY LIMITS RPt3
BATCH NO:
74395
SAMPLE NO: H386844
OVZHE
VoLatl €es - HE/Part
261
1,1-tlichtorcethyte
89'
1,2®Cichtorcetha -
99
enzen
Carbon tetrachloride
114-
hLorobenzene
98
ShLorofor i
11
Methyl ethyl ketone
101
etrachtcrcethylene
68
Trichtorcethyl ne
9
w
Vinyl, chloride
32
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full;,
without the written consent of pace AnMytical services, Inc:

Pace Analytical Services, Inc.
9800 Kincey Avenue Suite 100
Hulltersville, IBC 28078
TO 704-875-9092
May 1'1-9091
Report No. 000141
Section E Page 1"
Trt � DATA:`
--- --------------------------------
TEST
CODE DETERMINATION RESULT UNIT
BATCH NO: 74395 SAMPLE O- W386845
OVZHE Votatiles H /Part 261
1,3-Dichl roethylen 0.005 mg/L
1, -Di htorcetiane < 0.00 mg'
Benzene < 0.005 mg/L
Carbon tetrachloride < 0.005 mg/L
Chtarobenxene c 0�005 /C
Chloroform < 0.005 mg/L
Methyl ethyl ketone < 0.010 mg/
Tetrachloroethytene < 0.005 mall
Trichtor°oethyl ne < 0,00 /G
vinyl chloride s 0.010 mg/L
i
REPORT
OF LABORATORY ANALYSIS
This report shell not be reproduced, except In full„
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
0 Kinsey Avenue, Suite 100
Ca
1 unterSville; NC 28078
Tel. [phone]
Fax: 704- 7 - 0 1
May 20, 1997
Report No.: 00EE1441
Section H Page 1
TEST
Ms MSD
M -T m,_-_____v__.
MS PDT MSD PCT
CODE
DETERMINATION RESULT RESULT UNITS
RP RCVRY RCVRY
8 iCH NC
74395
SAMPLE- NO: H 50864
OV7HE
Votatit a n 7HE/Part
261
1,1-DichLoroethytene''
0,043 0.035 /L
20.4 108 88
Benzene
0.046 Quo mg7L
22.0 116 93
htoroben ene
0.046 0.038 /L
18.0 115 96
Trichtereethyt ne
0.042 0.035 mg7L
16.7 104 88
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fWt,
without the written consent of Face Analytical Services, Inc.

x
t h ffil,>
il
einjeu6ts joldwPS
f,.
83S38d11
cn
�` '' �'(Mljd} M-AdWUS
: jec] ano pills nk oU.
'Opp uM t)ad
'.
0—N 1n ,tia
w
nee } ujlls
3
sSOJppV
juallo
isenball looliAleuV,
S31VOlVUOM IVIUMNOUIAR3
,1 .: i
� r*w

■
kiff-MA ALI a
Clint
Address F
Phone �
Sampled By (PRINT),
Additional Comments
q ... ?; tl
. .—
Analytical Request
CHAIN -OF -CUSTODY RECORD
Report To: Mace Client No.
Rill TO Pace Prco-' t a
PeQ, , l Rillin teteren _ i r Pace Pro"act Na. , '
Prt�' t Narxre �` No. � '� � „o. ,��: � �°� r ,� `� � � i�
1 Requested Clue Date:

Pace Analytical Services, Inc.
0 Gemini Avenue
teal
Houston, TX 77058
Tel:[phone]
Fx:21-485-4651
May 21, 1997
Report No.: 00061525
Section A Page 1'
LABORATORY ANALYSIS REPORT
CLIENT NAME: PACE ANALYTICAL -CHARLOTTE
LIMS CLIENT:
0719 0631
ADDRESS: 9800 K NCEY AVENUE, SMITE 100
PACE PROJECT:
670506520
HUNTERSVILLE, NO 28078-
PACE CLIENT:
621231`
ATTENTION: FELECIA GROGAN
P.O.- NO:
VERBAL,
SAMPLE ID: 90.21/90280/ T1 -G
DATE SAMPLED:
05-M;'AY-97 151
SAMPLE NO:: H450267
DATE RECEIVED:
07-MAY-47
SAMPLE MATRIX: SOLID PROJECT MANAGER:
Debbie Proctor
TEST
DILUTION
LNCODE' DETERMINATION
FACTOR
RESULT UNITS
1 OVZHE VoLati les - ZHE/Part 261
1,1-Dichloroethylene
1
< 0.005 mg/L
1,2-Dichlcoethan
1
< 0.005 mg/t
Benzene
1
< 0.05 mg/L
Carbon tetrachloride'
1
< 0.00 /L
Chtorobenzene
1'
< 0.005 mg/L
Ch l oroforl
1 "
< 0.005 mg/L
Methyl ethyl ketone
1
< 0.010 mg/L,
Tetrachloroethylene
1
< 0.00 mg/L
Trichloroethylene
1
< 0.005 mg/L
Viyt chloride-
1
< 0.010 g/L
$904 TCLP ZHE leaching Procedure
Done
COMMENTS: Analysis performed at Pace Analyticat Services, Houston Latratory.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc:
f

Pace AnWival Services, Inc.
900 Gemini Avenue
hical Houston, TX 77658
Tel. [phone]
Fax; 281-488-4661
May 21, 1997
Report No.: 0006152
Section S page 1;
SUPPLEMENTAL INFOR14ATION
LCSR IrUP/MS------------- SAMPLE PREPARATION -- -------------- SAMPLE ANALYSIS ---------------
TEST SLNK MS714S0
LN CODE BATCH BATCH LR-METHOD EATEITIME ANALYST L -METHOD DATE/TIME ANALYST INSTRUMENT
SAMPLE I 907"7r21/90780/ T1-G SAMPLE NO: H4502 7
1 OVZHE 74459 7 459 NA 19-82405 15-MAY-97 1857 JSP CCMS
S904 74176 74176 NA 19-1311 12- Y-97 1500 JLJ 005EPE
LR Method Literature Reference
19 EPA -Test Methods for Evatuating Sand taste, 3rd ed, Nov. 1986 and updates
REPORT OF LABORATORYANALYSIS
This report .shad not be reproduced, except in full,
without the wvntten consent of Pace Analytical Services, Inc.

Pace Analytical services, Inc.
■
900 Gemini Avenue
Houston, TX 7 088
Tel: [phone]
Fay. 81-488-4661
May 21, 1997
Report No.: OOO6152
Section C Page 1
SURROGATE STANDARD RECOVERY
TEST PERCENT ACCEPTANCE
LN CODESURROGATE COMPOUND RECOVERY LIMITS REF LN
-------
SAMPLE to: "9077. 1/90 T1-C SAMPLE NO: M450 67
MAW GUNS Votatites Surrogates 1
4-8romoftuorobenzene
107
Oibromfluoromethene 107
Totu -
REPORT F LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
lthout the written consent of Pace An ly4lcel SeMces, Inc:

Pace Analytical Services, Inc.
900 Gemini ,Avenue
Houston, TX 7705
Tel: 61-458M1 1
Fax, 81-488-4661
May 21, 17
Report No.: 00061525
SectionD Page 1
LABORATORY CONTROL SAMPLE RECOVERY
TEST
LCS X
LCSO ACCEPTANCE
CODE
DETERMINATION RECOVERY
RECOVERY LIMITS RPu
BATCH NO
74459
SAMPLE NO: H386952"
OVZHE"
vctatlte - 7HE/Part 261
1,1-D1chtr thyten6 64
Henze
68
ChLor z
72 '
ToLuene
69
-
TrichLoroethytene
6
m.
ANALYSISREPORT OF LABORATORY
This report shall not he reproduced', except in full, ,
y
t
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services. Inc.
900 Gemini Avenue
ca
Houston TIC 77058
Tel., 281-88-1810
Fax: [phone]
May 21, 17'
Report No.: 000 1525
Section E Page 1
METHgQ BLANK DATA
TEST
COOS
DETER141H T10N
RESULT
UNIT
BATCH NO:
74459
SAMPLE NO: H386953
ZHE
Votatites, ZHE/Part 261
1,1-Olchtor' thyterie
0.00
IL
1,2-0lchlor etha
0.00
/L
Benzene
< 0.005
E
Carbon tetrachloride
< 0.005
/t
Chtar
< 0.005
/
Chtorof om
< 0.005
7t
Methyt ethyt, ketone
< 0.010
g/L
Tetr nhler d hytene
,
< 0.005
iL
Trich for thylene '
< M05
r f
Vinyt chloride,
< 0.010
OWL
LABORATORYREPORT OF L
This report shall not be reproduced, except in full;
without the written consent of pace Analytical Services, Inc.

Pane Analytical Services, Inc.
tt Gemini Avenue
Houston, TX 7705
Tel: - 1 l0
Fax: 2S1-4 -4 61
May 21, 1997
Report No.; 00061525
Section R Page I
MATRIX SPIKE AND HATRIX,,SPIKE DUPLICATE DATA
TEST
MS MSD
MS P T MSO PI
CODE
DETERMINATION RESULT RESULT UNITS
RPD
RCVRY" RGVRY
BATCH NO:
74459
SAMPLE NO: H450267
OV HE
Votatites 2HEI art 261
1,1-Otchloruethytene 0.034 0.035 L
5.2
85 as
Benzene 0.036 0.036 /L
0.0
90 90
chtorobenzene 0.035 0.036 7i.
2.8
88 9 ,
Tot0.900 0.754 /l.
1.6
191 * 1545
TrichloroethyLene 0.033 0.034 L
0.0
82 H
* The concentration of the analyte, prevented accurate determination of the<
matrix spike recovery.
REPORT OF LABORATORY ANALYSIS
This report shad not be reproduced, except in full
without the written consent of Pace Analy icai Services, Inc,

* M
NORTH CAROLINA DEPARTMENT O
ENVIRONMENT AND NATuRAL REsouRcEs
MOORESVILLE REGIONAL OFFICE
DrVISION OF WATER QUALUY
JNovember 3 2000
�� HUNT' Fz,
ovr R NO
Mr, L.F, Ire Hudson, Jr., Director of r°ater"5 caste titer Treatment
Cite of Statesville
P.C. Box 1 1.1 l
SILL fi-1ciLMAN Statesville, North Carolina 28687
Subject.- Permit No, WQ000175
City of Statesville
Fourth Creels WP Morrofill Facility
Iredell County, NC
Dear. i r. Hudson
-records show that Pernut No, WQ0001759 was issues on October 16, 2000 for the
slud,e monofrll located at your wastewater treatment facility The purpose of this letter is to
advise you of the importance of the Permit said the liabilities in the event of failure to comply with
the terns and conditions oft e Permit. If you have not already drone sir, it is requested that you
and other appropriate persons thoroughly read the Permit.
The Permit sets forth specific performance standards. operation and maintenance
requirements, monitoring requirements, plus general conditions applicable to non -discharge
permits, failure to comply with the terms and conditions ofthe Permit subject the Perruittee to
enforcement action pursuant to Section, 1 -215,6 of the North Carolina General Statutes in the,
form of civil or criminal penalties,
Please note that the subject Permit expires onSeptember 30:2005. Part V1, No. 6 of the
Permit require that a renewal request he submitted at leash sifa months prior to -expiration,
Also, the Permit is non -transferable until such time that the Permittee has requested a name
charure to the now Permittee.
s mentioned previously,the purpose of this lenter is to advise y it f the impo t ce of
your Permit, please read the permit and contact this Office at 704/6 —1699 in 1v ooresvdle if
you have any questions or need clarification. We look forward to providing any assistance;
Sincerely,
4 D. Rex Gleason, P. E,
'eater Quality Regional Supervisor
19 NORTR MAIN STREET, 1R1C ORVSl+tLLt, NORTH ARC LtNA 281 1
HONE :SCR - ,6 -160R FAX 04- - oAO
AM EQUAL...:OPPORTUNITY /..AF'FBRMATWE ACTION EMPL YtRd 0 RECYCLE d10 POST -CONSUMER PAPER

NoRTH CAROUNA DEPARTMENT OF
ENVRONMENT AND NA-r'URAL RE:souRcEs
October 16, 2000
MR, LF. "JOE" HUDSON, JR,, DIRECTOR OF WATER/WASTEWATER TREA,rNtFNT
CITY OF STATESVILLE
POST OFFICE BOX I I I I
"S
STATESVILLS, NORTH CAROLINA 28687
"1",x 10
�ubjeet: Permit No. WQ0001759
NOV City of Statesville
Fourth Creek WWTP Monofill Facility
Surface Disposal of Wastewater Residuals
,' Iredell County
Dear Mr. Hudson:
In accordance with your application received on May 31, 2000 as well as the additional information
received on September 20, 2000, we are forwarding herewith Permit No. WQ0001 759, dated October 16, 2000, to
the City of Statesville for the continued operation of a wastewater residuals surface disposal unit at its Fourth Creek
Wastewater Treatment Plant for the purposes of groundwater monitoring only.
This permit shall be effective from the date of issuance until September 30, 2005; shall void Peraut No.
'GHQ 0001759, issued July 17, 1996; and shall be sulaject to the conditions and limitations as specified therein.
Please take time to review this permit thoroughly. Of special interest are the following new and/or amended
provisions-
* Condition 1. 1...: This condition requires that a formal closure plan and a post -closure care management
program along with applicable implementation schedules be submitted to the Division of Water Quality
within 360 days of permit issuance.
* Condition 11, 2.: This condition has been modified to clarify that no residuals are. permitted for disposal
in the surface disposal unit, as it is now inactive,
+ Condition 11. 1: This condition has been amended to require that public access to the surface disposal
unit site, be controlled throughout this entire permit cycle (i.e., as opposed to only 36 months following
closure).
+ Condition Ill. 4.: Written reports for events of non-compliance Must now be filed within five days (i.e.,
reduced from 15 days) following first knowledge of the event's occurrence.
Z:�
+ Condition 1V 1As requested by the Permittee. groundwater monitoring events are now firnited to the
month of December only. In addition, anurionia-nitrogen and zinc have been dropped from the list of
parameters fix which groundwater samples must be analyzed. Please note that new guidance is
provided in this condition regarding acceptable methods for the analysis of volatile organic compounds
in the groundwater samples. Finally, this condition has also been amended to reflect the new mailing
address to be used when submitting all groundwater monitoring and reporting information.
1617 Mail Service Center, Raleigh, North Carolina 27699-1617
An Equal Opportunity Affirmative Action Employer
Telephone [phone] Fax [phone]
50% recycled/I 0% post -consumer paper

Please dray particular attention to the monitoring and reporting requirements contained in this permit.
4
Failure to establish an adequate system for collecting and maintaining the required operational information will
result in future compliance problems
f any parts, requirements, or limitations contained in this permit are unacceptable, you have the right to
request an adjudicatory hearing upon written request within 30 days following receipt of this pen -nit. This request
must be in the form of a written petition, conforming to Chapter 150B of North Carolina General Statutes, and filed;
with the Office of Administrative Hearings, 6714 Mail Service Center, Raleigh, NC 7 p -671 . Unless such
demands are made. this permit shall be final and binding.
If you need additional information concerning this matter, please coact Mir. Shannon Mohr Thornburg at
i91 7 -CIS , extension ,
`din ' r 'y, r r
Kerr T. Steven
cc., Iredell County Health De'partmen
Mooresville Regional' Office, Water Quality Section
Mooresville Regional Office, Groundwater Section
Central Office, Groundwater Section
Technical assistance and Certification Unit
Non -Discharge Compliance and Enforcement Unit

NORTH IT CAROLINA
ENVIRONMENTAL MANAGEMENT MENT O ISSI N
DEPARTMENT OF ENVIRONMENTAND NATURAL RESOURCES
RALEIGH
SURFACE DISPOSAL UNIT PERMIT
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, and
ether applicable Laws, Rules and Regulations
PERMISSION IS HEREBY GRANTED TO
City of Statesville,
Iredell County
FOR THE
continued operation of a surface disposal unit for groundwater monitoring purposes only. The surface disposal
unit, which was originally constructed in 1983, has been inactive since 1996, is no longer permitted to receive
residuals, and consists of eight areas comprising 9.4 acres total. Area No. I was utilized during 1983, Area No. ?
was utilized during 195 , Area No. '3 was utilizes in 1985, Area No. 4 was utilized in 1985 and 1986, Area No. 5
was utilized in 1986, Area No. 6 was utilized from 1987 through 1994, and area Nos. r and 8 were utilized from
1995 through 1996. All eight areas were filled in with trenches that were approximately 80 to 100 feet in length
and 10 feet in depth- All residuals disposed in the surface disposal unit were generated by the. City of Statesville's
Fourth Creek Wastewater Treatment plant`tl'v`PDES Permit No, Iv1'f:O 31 3 ?, Third Creek Wastewater water Treatment
Plant ( PDES Permit No. t 020591), as well as the Statesville rater Treatment Plant. The above -described
operational activities shall not result in a discharge of wastes to the surface waters; shall be pursuant to the
application received on May 31, 2000 as well as the additional information received on September 20, 9000; and
shall be in conformity with the project plans, specifications, and other supporting data: subsequently filed and
approved by the Department of Environment and Natural resources and considered a part of this permit.
This permit shall be effective from the date of issuance until September 30, 3005 shall void Permit No.
' 0001759, issued July 17, 1996, and shall be su lest to the following specified conditions and limitations-.
1. PERFORMANCE STANDARDS
1. Within 360 days of this permit's issuance a formal closure plan and afrost-closure management care "
program shall be submitted to the Division of Water ter Quality (Division). This information shall be
specific to the subject surface disposal unit site as well as relate to the Pe vittee.s future plans for the
land.. A schedule for implementing both the closure plats and the post -closure management care
program shall be provided as well. The Division will accept a submittal that Has been prepared in
accordance with the document entitled "Process Design Manual: Surface Disposal of Sewage Sludge
and Domestic Septafe ( P.AJ35-95f{102)," published by the United States Environmental :Protection
Agency's Office: Of research and l evelopnsent. Submit three copies of all i;nfortnation to the Non-
Discharpe: Permitting Unit, 161.7 Mail Service Center, Raleigh, NC ? 699-161 ,
1

16
1 Each surface disposal unit shall be effectively maintained and operated as a non -discharge system to
prevent the discharge of any wastes resulting from the operation of this program,
3. The issuance of this permit shall not relieve the Permittee of the responsibility for damages to surface
waters or groundwater resulting from the operation of this surface disposal unit,
4. A copy of this permit shall be maintained at the surface disposal unit site during the life of this permit.
11. OPERATION AND MAINTENANCE REQUIREMENTS
L The surface disposal unit shall be properly maintained and operated at all times,
2. No residuals shall be approved for disposal in the surface disposal unit,
3. Appropriate measures shall be taken to control public access to the surface disposal unit during active
use and following closure of the surface disposal unit. Such controls may include> fencing and the
posting of signs indicating the activities being conducted at each site.
4. Adequate provisions shall be taken to prevent any surface runoff from occurring from any active
surface disposal unit. If runoff cannot be preventad, a collection system shall be installed with the
capacity to handle runoff from a 24-bour, 25-year storm event, All collected runoff shall be disposed
in a manner approved by the Division of Water Quality (Division).
5. Adequate provisions shall be taken to prevent wind erosion from conveying pollutants or residuals
from the Surface disposal unit onto the adjacent property or into any surface waters.
111. MONITORING AND REPORTING REQUIRENIENTS
I. Any monitoring (i.e,, including groundwater, surface water, residuals, soil, or plant tissue analyses)
deemed necessary by the Division to ensure protection of the environment shall be established and an
acceptable sampling and reporting schedule shall be followed.
2. Noncompliance Notirication:
The Permittee shall report by telephone to the Mooresville Regional Office. telephone number (704)
663-1699, as soon as possible, but in no case more than 24 hours or on the next working day following
the occurrence or first knowledge of the occurrence of any of the following:
a. Any occurrence with surface disposal activities that results in the disposal of significant amounts of
wastes that are abnormal in quantity or characteristic,
K Any failure of the surface disposal activities resulting in a release of material to receiving waters.
c. Any time that self -monitoring information indicates that the surface disposal unit has gone out of
compliance with the conditions and limitations of this permit or the parameters on which the
system was designed.
d. Any process unit failure, due to known or unknown reasons, that renders the surface disposal unit
incapable of adequate residual treatment,
e. Any spillage or discharge from a vehicle or piping system transporting residuals to the surface
disposal unit.
Persons reporting such occurrences by telephone shall also file a written report in letterform within five
days following first knowledge, of the occurrence. This report must outline the actions taken or
proposed to be taken to ensure that the problem does not recur.
2

IV. GROUNDWATER 9hQL!REMEN:LS
I Existing groundwater monitoring wells MW-1, M -2, and MW-3 shall be sampled every December
for the following parameters: ,
Cadmium (C"d) Eat
Copper (Cu) Total Dissolved Solids (TICS)
Chlorides Total Organic arbc n (TOC
Fecal + olifortxa eater Level
Nitrate -Nitrogen (NO,- )
Volatile Organic Compounds ( OCs), using one of the following methods;
(A) Standard Method o 3 (PQL at 0.5 ltt;/L or less),
(l3) Standard Method 6210D (PQL at 0.5 ftg/k, or less),
(C") EPA Method 8021(Low Concentration, PQL at 0.5 Fag/L or less),
( PA Method 8260 (Low Concentration, PQL at 0.5 li /L or less), or
( °) Another method with prior approval by the Groundwater Section Chief
Any method used shall meet the following qualifications-
(1) The laboratory shall be Division certified to run any method used.
(2) The method used shall, at a minimum, include all the constituents listed in Table
' 111 of Standard Method 6230D.
(3) The -method used shall provided a PQL at 0.5 Rg/L or less which shall be
supported by laboratory proficiency studies as required by the Division's
Laboratory Certification Unit. Any constituents detected above the N DL, but
below the PQL at 0.5 4,p shall be qualified'(estimated) and reported.
If any V Cs are detected by the methods listed, then the Mooresville Regional Office Groundwater
Supervisor, telephone number `/ ) 663-1699, shall be contacted immediately for further instructions
regarding any additional follow-up analyses required. The results of all initial and follow -tip analyses
shall be submitted simultaneously:
If TC C concentrations gretiter than 10 milligrams per liter are detected in any downgradient
groundwater monitoring well, additional sampling and analysis shall be conducted to identify the
individual constituents cornpriSing this TOC concentration. If the TC C7 concentration as measured in
the background groundwater monitoring well exceeds 10 irullrgrasns per liter, this concentration shall
be taken to represent the naturally -occurring T"CFCs concentration. Any e ceedances of this naturally -
occurring TCIC concentration in the downgradient groundwater monitoring well shall be subject to
additional sampling and analysis as described above.
The measurement of water levels shrill be made prior to sampling the groundwater for the remaining
parameters. The depth to water in each monitoring well shall be measured frorn the sure°eyed point on
the top of the casing.
The results of the sampling and analysis shalt be received can the Groundwater Quality Monitoring
Compliance Deport po (i.e.. Forrii W-59) can or before the last working days of the month follovwin
the sampling month at the f olloxvin address:
Groundwater Section
Permits and Compliance 1.1n t
136 ]Nail Service Center
Raleigh. North Carolina 7699- 63Ci

2. The COMPLIANCE BOUNDARY for the surface disposal unit shall be specified by regulations in
15A NCAC 2L (i.e., Groundwater Classifications and Standards). The Compliance Boundary for
surface disposal units constructed after December 31, 1983 shall be established at either (1) 250 feet
from the surface disposal unit -or (2) 50 feet within the property boundary, whichever is closest to the
surface disposal unit. An exceedance of Groundwater Quality Standards at or beyond the Compliance
Boundary shall be subject to immediate remediation action in addition to the penalty provisions
applicable under NCGS § 143-215.6A(a)(1).
In accordance with 15A NCAC 2L, a RE'IE V BOUNDARY shall be established around the surface
disposal unit midway between the Compliance Boundary and the perimeter of the surface disposal unit.
Any exceedance of Groundwater Quality Standards at the Review Boundary shall require remediation
action on the part of the Permittee.
1 Any groundwater quality monitoring, as deemed necessary by the Division, shall be provided.
V. INSPECTIONS
L The7 Permittee or his designee shall inspect the surface disposal unit to prevent malfunctions and
deterioration, operator errors and discharges that may cause or lead to the release of wastes to the
environment, a threat to human health, or a nuisance. The Permittee shall maintain an inspection log or
summary including at least the date and time of inspection; observations made; and any maintenance,
repairs, or corrective actions taken, by the Permittee. This log of inspections shall be maintained by the
Permittee for a period of five years from the date of the inspection and shall be made available to the
Division or other permitting authority, upon request.
2. Any duly authorized officer, employee, or representative of the Division may, upon presentation of
credentials, enter and inspect any property, premises, or place on or related to the surface disposal unit
at any reasonable time for the purpose of detennining compliance with this permit-, inspect or copy any
records that must be kept under the terms and conditions (if this pen-tral- and obtain samples of
groundwater, surface water, or leachate.
V1. GENERAL CONDLTIONS
1, This permit shall become voidable unless the surface disposal unit activities are carried out in
accordance with the Conditions of this permit, the supporting materials, and in the manner approved by
this Division,
2, This permit shall not be automatically transferable. In the event that there is a desire for the surface
disposal unit to change ownership or a name change of the Permittee, a fon-nal permit request shall be
submitted to the Division accompanied by an application fee, documentation from the parties involved,
and other supporting materials as may be appropriate, The approval of this request shall be considered
on its merits and may or may not be approved,
Failure to abide by the conditions and limitations contained in this permit may subject the Permittee to
an enforcement action by the Division in accordance with NCGS §143-215,6A through §143-215.6C.
4. The annual administering and compliance fee shall be paid by the Permittee within 30 days after being
Z"
billed by the Division, Failure to pay the fee accordingly stray cause the Division to initiate action to
revoke this permit as specified by 15 NCAC 211,0205 (c)(4),
5The issuance of this permit shall not preclude the Pernlinee from complying with any and all statutes,
rules, regulations, or ordinances that may be. imposed by other govemment aaencies (i,e,, local, state,
and federal) that havejuriWictian.
4

. The Permittee, at least sip months prior to the expiration of this perout, shall request its extensions
Upon receipt of the request,the Division shall review the adequacy of the surface disposal unit
described therein and, if warranted, shall extend the permit for such period of time and tender such
conditions and limitations as it ay deem appropriate.
.. This permit may be modified, or revoked and/or reissued to incorporate any conditions, limitations„ and
monitoring requirements the Division deems necessary in order to protect the `environment and public
health adequately.
Permit issued this day of Ctder,tt
NORTH OLINA ENV E TAL MANAGEMENT COMMISSION
Derr T. Stevens, Director
Division of Water Quality
y Authority of the Environmental Management ement Commission
Permit Number ''N Q0003 75

t to 0 I;
r
m��v aw

+�,: '" "..,.•`',,,✓r' `"�_, ,"r' €'ON, WELL
40 ` a
HOT ITOnIHr, WELL ��-u 4 �'`4iASTEWATER TREATMENT !�L -NIT
a °
�63 3i 3ti"'} 4 dro r d I
AI
r rrr�
xdSTlNt;drrrdr d
FILL
rr )'?' A it f ddOTT
NG
dF'a�7".lr 'r*'`,e }"
k
drd* rrt SILL dd "'
�t 4� FX. CLEVAIE0 fiA drdr rr k
''",,t3 "44,'•s3 - 764.'Si" f"t, CAt a� " .rd'r ✓r ✓ r r L.t i �„""�.:- ` "" » --�.-- . ,�
rr*r { FILL rrr`
fioNI7QFaSra WELL :!-Ci` e
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'�""` •_„.. „�, �"*" w '"`"" , w . `"_` . "-" d ✓ ddr rrd ✓ rd rdr rrr rrr drr}
„. �,«- ..• C., , >.,., - �" y`••4. rr dd rd rd rr rr rd rd rr r rr drr co T.
rr}'i dr Mrdl rrd ddd drd�rrr �i
4
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e
_ �- to .� 11 5"��` srrrdddrrd ✓ r rr rd r ddr r a }
�—� ' ...y ``,v`/�yv..� Jrr °".+r v"r'Fdr �, rl rr �"'./d / �, �"" ✓ �. d Z'
,� x"`cr '„ '"r rdr r'° d ✓ rr d d r r { dr _ ' d d o rr
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. _ t.. tr
y
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NO WELL 41-0
`
FIGUI +E
_ 100 20off CITY OIL STATESILL - FOURTH CRE EK T► WTIY
SURFACE DISPOSAL OF RE, I UAL SOLIDS
IREDELL COUNTY
SITE L. L AILd MA

September 18, 2000
ina 28687
x:r
„A10
v
1*
Ms, Shannon Thornburg
,
G
Non -Discharge Permitting Unit �
Division of Water Quality
,.4
1617 Mail Service Center
Raleigh, NC 27699-1617
Re:, Additional Information
Jed Np. 17 >
Fourth Creek WWTP Monofill
Dear Ms. Thornburg:
e have received your August 21, 2000 utter requesting additional information and appreciate
the opportunity to comment. Please accept the following additional information and comments:
General lnforrmtion:
1. Please find enclosed a letter from Mr. Rob Hites authorizing L.F. "Joe" Hudson, Jr. to
sign permit documents.
Surface Disposal Unit:
m A. formal closure plan has not been developed, We have not been given sufficient
guidance at this time to be able to draw up a formal closure plan.. We would
appreciate any information or guidance as to minimum requirements for closure.
While in operation, daily cover was used with each finished trench receiving three t
four feet of cover. Natural vegetation is maintained year-round.
, Since the unit is inactive and has not received any residuals since 1996, we do not
utilize the provision for temporary storage of residuals.
Public access to the monotill is controlled by a barbed wire fence that surrounds the
plant sites 'rhe plant's fence is adjacent to the monofill on two sides with the
remainder being encompassed within the plant site's fence. The gate is kept shut and
padlocked. Appropriate signage is frosted....
Methane monitoring is conducted once a reek by checking the methane level with a
handheld gas monitor at the nmnofill fence line; The reading is recorded in our
operating log. In addition, the attached management practices are utilized.

Nor
Draft Permit:
1$ The cover sheet of the deaf permit references six fill areas. There were actually
eight fill areas as shown on the rno rrofill reap, Figure 2.. areas seven and eight were
used between 1995 and 1996,
. Condition III. 2. requires continuous methane monitoring in structures within the
rnonoafill and at the property lime. As stated above, we conduct methane monitoring
once per week with a handheld monitor at the property line. The result is lugged in
our operating log and is always noon -detectable. Since the site in general has been
inactive for four years, and longer in other areas ofthe unit(refer to Figure , we
request that the methane monitoring requirement be completely removed from the
permit,
`here is a dilapidated shed within the rnono fill boundary that is no longer used, We
have plans to demolish it during the winter months. `his shed is located in an area
that has been inactive since 19(between areas #1 and . Periodic checks for
methane within the shed indicate that there is no urethane present.
3. We are pleased in the reduction of well monitoring and appreciate the consideration
given.
If you need any additional information or need to discuss these items, please contact me
at -.
inco�rei ,
L.F. "Joe" Hudson, Jr., Director
Water'Resources
enclosure

ppi L
t
C. 1 1 t jai 1.0 t v of
art retina 28607
September-, 2000
lbs. Shannon Thornburg
Non -Discharge Permitting Unit
Division of Water Quality
1617 flail Service Center
Raleigh, NC 2 9-1 1
Re: Signatory Signatory uth ri ati n
Third Creep WWTP, App, No, W 00 4 40
Fourth Creep WWTP, App. No. " Q0001 9
Dear Ms. Tho burg:
By this letters Mr. L.F. "Joe" Hudson, Jr., Director of Water Resources, is authorized to sign all
documents and correspondence pertaining to the referenced permit applications for the City of
Statesville:
Sincerely,
Robert W. Hires, Jr.
City Manager

Management Practices Description
Furth Creek WWTP Sludge Monorill
NPDES Permit No. NCO031,836
Non -Discharge Permit No. WQ0001759
40 CFR 503.24
a Threatened or Endangered Species: No known threatened or endangered species occupy or
frequent ent the disposal site.
(b) Base Flood Flow R stricti m The monofill does not restrict the flow of a base flood.
c) Not Applicable-
d Not applicable
e The monofill is located in a stable area:.
The monofill is not located in a wetland area:
g lunofolletion: Trenches were constructed so as to prevent disposed material from
exiting as a part ofany runoff:- Berms and swales were constructed to contain erosion. Finished
trenches were domed with clean earth to allow shedding of water out and away from Tilled
trenches, dative vegetation is maintained and encouraged to grow around the entire area.
h The monofill does not have a liner:
i The monofill does not have a liner or leachate collection.
The monofill has been inactive for four years:
Crops are not grown on this site,.
lAnimals are not grazed on this site.
m Public access to the site is prohibited by a barbed-wire, padlocked fence.
n groundwater monitoring; system is in place.: Results from well sampling indicate that there
is no groundwater contamination.

State of North Carolina
N,,k.,,, 1A,*
Department of Environment q
and Natural Resources
Division of Water Quality AUG 124
IMAP"'410F
James B. Hunt, Jr,, Governor , "" ";0", 4" OW g,4-
g
Bill Holman, Secretary WIM 11
4fftli'41111",41 "A,",
Kerr T. Stevens, Director NoRTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
Atioust 21, 2000
MR. LF. "J(,)F-" HUDSON, JR., DIRECTOR OF WATERAVASTF-WATER, TREATMENT
CITY OF STATESVILLE
POST OFFicF, Box I I I I
STATESVILLE, NORTH CAROLINA 28687
Subject-, Application No, WQ0001759
Additional Information Request
City of Statesville
Fourth Creek W')NIFP Monofill Facility
Surface Disposal of Residual Solids
Iredell County
Dear Mr. Hudson:
The Non -Discharge Permitting Unit has completed a preliminary, engineering review of the
1:
subject application, Additional information is required before we can continue our review, Please
address the following items no later than September 21, 2000-
General Information:
1) As requested in Item 1. 2. on Page I of 9 of the submitted application form, Mr. L.F.
"Joe" Hudson, Jr., Director of Water/Wastewater Treatment is listed as the permit
signing official's name and title. Please note that Regulation 15A NCAC 2H .0206 (b)
(4) requires that municipal permit applications must be signed by a principal executive
officer., ranking elected official, or other duly -authorized employee. Please provide a
letter that authorizes Mr. Hudson to sign such documents for the City of Statesville.
L_
Surface Dist)osal Unit:
1) Please clarify whether or not a formal closure, plan has been submitted to the Division
of Water Quality (Division), as was required by Condition V1. 9. of the existing
permit, issued July 17, 1996.
2) The existing permit for this surface disposal unit makes several references to the
approval of temporary storage of residuals. Specifically, Condition I. 7. states that
residuals generated at times other than normalbusiness hours may be temporarily
stockpiled in the vicinity, of the surface disposal unit site. Please clarify whether or not
this is still practiced and, therefore, provisions for this activity should be included in
the renewed/modified pemut when issued,
1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Telephone [phone] FAX[phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

"'qq
Surface Disposal Unit, (continued):
,3) Please clarify whether or not public access to the surface disposal unit is currently
Being actively controlled. Describe what measures are beingused to accomplish this
goal, and detail face long these measures "rill continue to be implemented.
4 Please clarify whether or not methane gas monitoring in structures within and at the
property lime of the surface disposal site is presently being performed. Note that this is
required by Condition 111, 7. of the existing permit; however, this type of monitoring is
typically only required when daily cover was used when the surface disposal unit was
acti pie;
Draft Permit:
I) Please find a copy of the draft permit, as currently proposed for issuance, attached to
this correspondence. Reo!iew this draft thoroughly, and provide any comments,
clarifications, and/or questions accordingly, In particular, r, note the following with
respect to your requested modifications, in the required groundwater monitoring
pros, amn
+ The Groundwater Section has concurred with the proposal to reduce the
frequency of groundwater monitoring to one per year i;e,, in December).
.
♦ The Groundwater Section has agreed to eliminate the requirement to analyze
groundwater samples for ammonia -nitrogen and zinc. Other parameters are t
remain in the groundwater monitoring program because of the potential for
continued leaching of the constituents from the surface disposal unit into the
groundwater.
Please reference the subject pen -nit application number when providing the requested
information, Five copies of all response information should be submitted to my attention at the
address on this first page of this correspondence. Note that failure to provide this additional'
information ation on or before the above requested date can result in your application package being
returned as incomplete:
If you have any questions regarding this request, please call nee at qlq 73_5 fir. extension
353. Thank you in advance for your cooperation and timely response.
c.c: Ms. Ellen Huffman, Mooresville
Mr. David Goodrich, Central Ofl
Permit pile 1759
NA..L�_
rncer,y,
Shannon Mohr Thornburg
Environmental Engineer
on -Discharge Permitting tting Unit

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
A�
James B. Hunt, Jr., Governor
Bill Holman, Secretary NCDENR
Kerr T. Stevens, Director NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
Au-ust/SeptoTaber XX, 2000
MR. L.F. "JoE7HUDSON, JR., DIRECTOR OF WATER/WASTEWATER TREATMENT
CITY OF STATESVILLE DRAFT
POST OFFICE Box I I I I
S'TAT ESVILLE, NORTH CAROLINA 28687
Subject: Permit No. WQ0001759
City of Statesville
Fourth Creek WWTP Morrofill Facility
Surface Disposal of Wastewater Residuals
Iredell County
Dear Mr, Hudson:
In accordance with your application received on May 31, 2000 as well as the additional information
received on August/September XX, 2000, we are forwarding herewith Permit No, WQ0001759, dated
AugustISeptember XX, 2000, to the, City of Statesville for the continued operation of a wastewater residuals surface
disposal unit at its Fourth Creek Wastewater Treatment Plant for the purposes of groundwater monitoring only.
This permit shall be effective from the date of issuance until July/August 31. 2005; shall void Permit No.
WQ0001759, issued July 17, 1996-1 and shall be subject to the conditions and limitations as specified therein.
Please take time to review this permit thoroughly. Of special interest are the following new and/or amended
provisions:
* Condition 11. 2.: This condition has been modified to clarify that no residuals are permitted for disposal
in the surface disposal unit, as it is now inactive.
+ Condition 11. 3.: This condition has been amended to require that public access to the surface disposal
unit site be controlled throughout this entire permit cycle (i.e., as opposed to only 36 months following
closure).
* Condition 11.1. 3.: This condition requires that methane gas monitoring 'results be submitted on an
annual basis.
* Condition 111. 4.: Written reports for events of non-compliance must now be filed within five days (i.e,,
reduced from 15 days) following first knowledge of the event's occurrence.
* Condition IV, 2.: As requested by the Permittee, groundwater monitoring events are now limited to the
month of December only. In addition, ammonia-rutrogen and zinc have been dropped from the list of
parameters for which groundwater samples must be analyzed. Please note that new guidance is
provided in this condition regarding acceptable methods for the analysis of volatile organic compounds
in the groundwater samples. Finally, this condition has also been amended to reflect the new mailing
address to be used when submitting all groundwater monitoring and reporting information.
Please pay particular attention to the monitoring and reporting requirements contained in this pen -nit.
Failure to establish an adequate system for collecting and maintaining the required operational information will
result in future compliance problems,
1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Telephone [phone] Fax [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

If any parts, requirements, or limitations contained in this permit are unacceptable, you have the right to
request an adjudicatory hearing upon written request within 30 days fallowing receipt of this permit. This request
must be in the form of a written petition, conforming to Chapter 150E of North Carolina General Statutes, and filed
with the Office of Administrative clearings, 6714 Mail Service Center, Raleigh, NC 27 -6714. Unless such
demands are made, this permit shall be final and binding.
If you need additional information concerning this matter, phase contact Ms. Shannon Mohr Thornburg at
(1) 7 3- 08 3, extension 353.
Sincerely; DRAFT
Kerr T. Stevens
cc: fredell County Health Department
Mooresville Regional Office, Water Quality Section
MooresvilleRegional Office, Groundwater Section
Central Office, Groundwater Section
Technical Assistance and Certification Unit
Non -Discharge ComplianceandEnforcement Unit

Nn 'TTTCAD T INIA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF ENVIRONMENTAND NATURAL RESOURCES
RALEIGH
SURFACE DISPOSAL UNIT PERMIT
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, and
other applicable Laws, Rules, and Regulations
PERMISSION IS HEREBY GRANTED TO
City of Statesville 'RAFT
Iredell Countypb
FOR THE
continued operation of a surface disposal unit for groundwater monitoring purposes only. The, surface disposal
unit, which was originally constructed in 1983, has been inactive since 1996, is no longer permitted to receive
residuals, and consists of six areas comprising 9.4 acres total. Area No. I was utilized during 1993, Area Flo® 2 was
utilized during 1984, Area No. 3 was utilized in 1985, Area No. 4 was utilized in 1985 and 19,86,Area No. 5 was
utilized in 1,986, and Area No. 6 was utilized from 1987 through 1994. All six areas were filled in with trenches
that were approximately 80 to 100 feet in length and 10 feet in depth, All residuals disposed in the surface disposal
unit were generated by the City of Statesville's Foruth Creek Wastewater Treatment Plant (NPDES Permit No.
NC0031836), Third Creek Wastewater Treatment Plant (NPDES Permit No. NC00220591), as well as the Statesville
Water Treatment Plant. The above -described operational activities shall not result in a discharge of wastes to the
surface waters; shall be pursuant to the application received on May 31, 2000 as well as the additional information
received on August/Septernber XX. 2(KX); and shall be in conformity with the project plans, specifications, and
other supporting data subsequently filed and approved by the Department of Environment and Natural Resources
and considered a part of this peritnt.
This perritit shall be effective from the date of issuance until July/August 31, 2005; shall void Permit No.
WQ0001 759, issued July 17, 1996-1 and shall be subject to the following specified conditions and lit nitations:
1. PERFORMANCE STANDARDS
1. Each surface disposal unit shall be effectively maintained and operated as a non -discharge system to
prevent the discharge of any wastes resulting from the operation of this program,
2. The issuance of this permit shall not relieve the Perm tree of the responsibility for damages to surface
waters or groundwater resulting from the operation of this surface disposal unit.
3. - A copy of this permit shall be maintained at the surface disposal unit site, during the life of this permit.

11. OPEIZA'DTI ON AND MAJIN�TENA�NCE �REU�IREINI�ENTS�
L The surface disposal unit shall be properly maintained and operated at, all times.
1 No residuals shall be approved for disposal in the surface disposal unit.
3, Appropriate measures shall be taken to control public access to the surface disposal unit during active,
use and following closure of the surface: disposal unit. Such controls may include fencing and the
posting of signs indicating the activifie-s being conducted at each site.
4, Adequate provisions shall be taken to prevent any surface runoff from occurring from any active
surface disposal unit, If runoff cannot be prevented, a collection system shall be installed with the
capacity to handle runoff from a 24-hour, 25-year storm event. All collected runoff shall be disposed
in a manner approved by the Division of Water Quality (Division).
5Adequate, provisions shall be taken to prevent wind erosion from conveying pollutants or residuals
from the surface disposal unit onto the adjacent property or into any surface water&
111. MONITORING AND REPORTING REQUIREMENTS
L Any monitoring (i.e., including groundwater, surface water, residuals, sail, or plant tissue analyses)
deemed necessary by the Division to ensure protection of the environment shall be, established and an
acceptable sampling and reporting schedule shall be followed.
1 The air in all structures within the surface disposal unit site and the air at the property line shall be
continuously monitored for the presence of methane gas. The following`criteria shall be met-
a. In structures, the concentration of methane gas in the air shall not exceed 25 percent of the lower
explosive limit (LEL) for inethane gas.
bt the propero, line, the concentration of methane gas in the air shall not exceed the LEL for
methane gas.
3. Three copies of the required monitoring and reporting requirements as specified in Condition HL 2_
shall be submitted annually on or before March 1st of each calendar year
NCDENR-DWQ
Water Quality Section
NOD -Discharge Compliance/Enforcement Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
4. Noncompliance Notification -
The Permittee shall report by telephone to the Mooresville Regional Office. telephone number (704)
663-1699, as soon as possible, but in no case more than 24 hours or on the next working day following
the occurrence or first knowledge of the occurrence of any of the following:
a. Any occurrence with surface disposal activities that results in the disposal of significant amounts of
wastes that are abnon-nal in quantity or characteristic.
K Any failure of the surface disposal activities resulting in a release of material to receiving waters.
c. Any time that self- monitoring information indicates that the surface disposal unit has gone out of
compliance with the conditions and limitations of this permit or the parameters on which the
system was designed.
2

d.. Any process unit failure, due to known or unknown reasons, that renders the surface disposal unit
incapable of adequate residual treatment:
e. Any spillage or discharge from a vehicle or piping system transporting residuals to the surface'
disposal unit:
Persons reporting such occurrences by telephone shall also file a written report in letterforni, within five
days following first knowledge of the occurrence. This report must outline the actions taken or
proposed to be taken to unsure that the problem does not recur.
IV. GROUNDWATER REQUIREMENTS
1. Existing groundwater mr onitor ng wells l W-L - , and MW-3 shall be sampled every December
for the following parameters,
Cadmium (C'd) p
Cropper (Cu) Total Dissolved Solids (Tl )
Chlorides Total Organic Carbon (TOC)
Fecal Coliform Water Level
Nitrate -Nitrogen (NO,-N
Volatile Organic Compounds (VOC's), wing one of the following methods:
( ,Standard Method 6230D Pt L at 0.3 l tg/L, or less),
( ) ,Standard Method 6210D (Pfi L at 0.3 pg/"L or less),
(C) EPA Method 8021 (Low Concentration'. PC L. at 0.5 p /L. or less)
(D) EPA:: Method 8260 (Low Concentration P L at 0,5 pg1L or less), o
(E) Another method with prig approval by the Groundwater section Chief
Any method used shall meet the fallowing qualifications
(1) The laboratory shall be Division certified to run any method used
() The method used shall, at a minimum, include all the constituents listed in Table
VIR of standard Method a 30D,
(3) The method used shall provided a Pm L at 0.5 gga"L or less which shall be
supported by laboratory proficiency studies as required by the Division's
Laboratory Certification Unit. any constituents detected above. the M.DL, but
below the PQL at 0.5 lrg/1.., shall be qualified (estimated) and reported:
If any VOCts are detected by the methods listed., therm the Mooresville regional Office Groundwater
Supervisor, telephone number (70) 663-169, shall be contacted immediately for further instructions
regarding any additional follow-up analyses required. The results of all initial and follow-up analyses
shall be submitted simultaneously.
If "IOC concentrations greater than 10 milligrams per liter are detected in any downgradient
groundwater monitoring well:, additional sampling and analysis shall be conducted to identify time
individual constituents comprising this TOC° concentration. 1f the TOC~ concentration as measured in,
the back -ground groundwater monitoring well exceeds 10 milligrams per liter, this concentration shall
be taken to represent the naturally -occurring TOC concentration. Any e ceedances of this naturally -
occurring TCIC3 concentration in the downgrad ient groundwater monitoring well shall be sulaject to
additional sampling and analysis as described above:
The: measurement of water levels shall be made prior to sampling the groundwater for the remaining;
parameters. The depth to water in each monitoring well shall be measured from time surveyed point on
the top of time casing:

The results of the sampling and analysis shall be received on the Groundwater Quality Monitoring
Compliance Report Form (i.e., Form GW-59) on or before the last working day of the month following
the sampling month at the following address;
NCDENR-DWQ
Groundwater Section
Porn -tits and Compliance Unit
1636 Mail Service Center
Raleigh, North Carolina 27699-1636
2. The COMPLIANCE BOUNDARY for the surface disposal unit shall be specified by regulations in
15A NCAC 2L (i.e., Groundwater Classifications and Standards). The Compliance Boundary for
surface disposal units constructed after December 31, 1983 shall be established at either (1) 250 feet
from the surface disposal unit or (2) 50 feet within the property boundary, whichever is closest to the
surface disposal unit. An exceedance of Groundwater Quality Standards at or beyond the Compliance
Boundary shall be sulbject to immediate remediation action in addition to the penalty provisions
applicable under NCGS § 143-215.6A(a)(1).
In accordance with 15A NCAC 2L, a REVIEW BOUNDARY shall be established around the surface
disposal unit midway between the Compliance Boundary and the perimeter of the surface disposal unit.
Any exceedance of Groundwater Quality Standards at the Review Boundary shall require remediation
action on the part of the Permittee.
1 Any groundwater quality monitoring, as deemed necessary by the Division, shall be provided.
V. INSPECTIONS
1. The Pen-nittee or his designee shall inspect the surface disposal unit to prevent malfunctions and
deterioration, operator errors and discharges that may cause or lead to the release of wastes to the
environment, a threat to human health, or a nuisance. The Permittee shall maintain an inspection log or
summary including at least the date and time of inspection; observations made, and any maintenance,
repairs, or corrective actions taken by the Pertnittee. This log of inspections shall be maintained by the
Permittee for a period of five years from the date of the inspection and shall be made available to the
D i v i sion or other permitting authority, upon request.
2, Any duly authorized officer, employee, or representative of the Division may, upon presentation of
credentials, enter and inspect any property, premises, or place on or related to the surface disposal unit
at any reasonable time for the purpose of deternnning compliance with this permit; inspect or copy any
records that must be kept under the terms and conditions of this permit; and obtain samples of
groundwater, surface water, or leachate.
VI. GENERAL CONDITIONS
I. This permit shall become voidable unless the surface disposal unit activities are carried out in
accordance with the conditions of this pernrit, the supporting materials, and in the manner approved by
this Division.
2, This permit shall not he automatically transferable. In the event that there is a desire for the surface
disposal unit to change ownership or a name change of the Permittee, a formal permit request shall be
subrintted. to the Division accompanied by an application fee, documentation from the parties involved,
and other supporting materials as may be appropriate. The approval of this request shall be considered
,on its merits and may or may not be approved.
4

3. Failure to abide by the conditions and limitations contained in this permit may subject the Permittee to
an enforcement action by the Division in accordance with NCGS §143-215.6A through §143-215.6C.
4, The annual administering and compliance fee shall be paid by the Permittee within 30 days after being
billed by the Division. Failure to pay the fee accordingly may cause the Division to initiate action to
revoke this permit as specified by 15 NCAC 2H .020,5 (c)(4).
5. The issuance of this permit shall not preclude the Permittee from complying with any and all statutes,
rules, regulations, or ordinances that -may be imposed by other government agencies (i.e., local, state,
and federal) that have jurisdiction.
C. The Permittee, at least six months prior to the expiration of this permit, shall request its extension.
Upon receipt of the request, the Division shall review the adequacy of the surface disposal unit
described therein and, if warranted, shall extend the permit for such period of time and under such
conditions and limitations as it may deem appropriate.
7, This permit may be modified, or revoked and/or reissued to incorporate any conditions, limitations, and
monitoring requirements the Division deems necessary in order to protect the environment and public
health adequately.
Permit issued this theXXX day of August/September, 20(,X)
NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION
Kerr T. Stevens, Director DRAFT
ivision of Water Quality
By Authority of the, Environmental Management Commission
Permit Number WQ0001 759

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SURFACE DISPOSAL OF'RESIDUAL O
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IRE ELL COUNTY
' t- L 1 N II

C C PRIORITY PROJECT:Yes—No
If Yes, SOC No, -
To: Permits and Engineering Unit
Water Quality Section
Attention: Ms. Shannon Thornburg
Mooresville sville 00-6
Date. July: 24, 2000
NON -DISCHARGE STAFF RE PORT AND RECOMMENDATION
COUNTY: Iredell
Permit No. NVQ000I7 P
Renewal for rnonofrll (fourth Creek WW I`P
Groundwater monitoring only
PART I - GENERAL INFORMATION
I,.
Facility and address. City of Statesville
Fourth Creek {F'
Post Office Boas I 1 . l
Statesville, NC 28687
`'.
Vats of Investigation, June 26, 2000
..
Report Prepared y, Ellen Huffman
.
Person(s) Contacted and Telephone Number: L.F. "Joe", Hudson, Jr.
704/878-3438
5.
Directions to it s . From the intersection of I- 7 and, Hwy 70, travel east on Irwy 70
(towardSalisbury) abort d aeries to Bell Farm Road. Turn left onto Dell Farm Road and
travel about I mile. Lank for sign and en , ice to Plant on right,.
d.
Type of permit: Renewal of non -discharge sludge rrronofll permit.
,
Size (land permitted for application). 9.4 acres
This is an inactive m nofill (since 1' Permit is for CAW`monitoring only.
. _
Topography (relationship to 1 0CI-y°ear flood plain included): Monolll is not in or near a I00
year flood plain. USGS map showing monofil is included in the permit package.

. Buffer conflicts with location of nearest dwelling and water supply well: Yes_ No
10. Watershed Stream Basin Information for"land application sites:
a. Watershed Classification: Mass
b. River Basin and Subbasin No.: Catawba, 03-07- d
C. Distance to surface grater from disposal system. n/a
FART 11 - DESCRIPTION OF WASTES AND TREATMENT `WORKS
I : a. Residuals Volume: 300 dry tons per year, wastewater treatment plant residuals
b. Types and quantities of wastewater: % Industrial % domestic
C. Volume of wastewater residual stor --e. n/a
d. Estimated days of storage._ days n/a
e; Volume of water treatment residuals. n
2. Wastewater Treatment Facilities
a. Current permitted capacity of the)V�kT facility" 6,0 I GI
b. Average daily floe of the WWT facility,: 4.0 MGM
c, Description of existing wastewater treatment facilities: n/
d. Description of proposed wastewater treatment facilities. n/a
3. Residuals handling and utilization/disposal sche e: The sludge mono ] has been inactive
since 1996 and the groundwater monitoring for this site continues to reflect compliance with
groundwater standards.
4. Treatment plant classification: Grade IV Biological Water Pollution Control ygstemtV ' P
.. _ SIC C'ode(s)
Wastewater Codes) 01
Primary: Secondary -
Main Treatment Unit Code:
FART" III - OTHER PERTINENT INFORMATION
I is this facility being constructed with Construction Grant Funds(municipals only) n/a
Special monitoring requests: Groundwater monitoring can be reduced to annual sampling (in
December) for pH, water level, cadmium, VOC and NO3. Also perform the usual field
2
Page

measurements and procedures listed on the cproundwater monitoring form.
3. Important SOC, JOC or Compliance Schedule dates: n./a
Other Special Items: /a
PART IV - EVALUAT O :AND RECOMMENDATIONS
The application is a request for renewal of an existing, monofil (inactive) pe it
monitoring only). This renewal also regues:,s a reduction in the groundwater monitoring
frequency, Peggy Finley, GW-MRO, agrees that the monitoring frequency can he reduced;
to annually in December) for pH, water ;level, cadmium, , i d NO3. Permittee must
continue to perform the usual field measurements and follo-w the sampling procedures listed
on the groundwater monitoring form. This office has no objection to the request for reduction
of GW monitoring frequency. MRO GW report is attached..
The. Cite of Statesville currently handles residuals produced by its Third Creep and Fourth
Creep WWTPs by two permitted methods l rf a class A residual lime product (permit
Qu a ), and 2) land application pe=it 4WQOO 16247).
This office recommends issuing the e , ii with the above mentioned groundwater
monitoring changes
Signature of Deport Pied' er
Water Quality regional Supervisor
Date-
r

RECORD OF WASTE DISPOSAL. PERMIT APPL)CATION REVIEW
4IEW _ y D A TE FIELD INVESTIGATION? 'r/N)
OUN d '
0_ S'SP SAL SYSTEM, ILAG100N, E- T ) � DESIGN GP(u D
E PI s IOCN F :FAa IL€ T
SSE OF IMP LIIVDME T ^, l R S2E OF APPLISA T ION AREA -
v,>"my�xl. tvv,"wry: -PRIMARY-SECONDARY a i
IND. SLUD',"SE INN. WELL WATER NTH IRS:
ANC'=_ FROIM WASTE SOURCE TO NEAKST. STREAM -FT., WELL _F7
F:CR WELL: TYPE OF USE DEPTH _ PUMP RATE (EST.
V;7i,4,7 DESIIGN CONDITIONS IL! REEDUCE4SRE;ASE CHANCE OF WCON A INA ION:
`� —14,.T NATURAL € i E CONDIT6ONS WILL REDU EA1~ ORE SE CHANCE OF G'ri1" CONTAMINATION.- -
= R T : EEDR I r- l ., SEASONAL HIGH t� J, F ANNUAL W T, FLUX s.
SURxFISIALAOIJIFER SEDR SI /ARTESIAN AQUIFER
,.EEN, Lf (RDL GY
I<3E .S IrREi I MEASURE
"E. ND. __ r JDA�r
==
" -S T ImATEC7 ."EAY E T IMATE
�"'I K y
N ', OF EONI1E:P Vpla LLS UDOWN � ; EXISTING- Up WN
D%i W0RI=;SiYl-:- T : Sl TE ?r'�"svl vA': D Ew10,T 10Il.� m
T I 2 3Lis
E D , , ; . S T U,A T 0 N
HH IVE HER_ BEEN ANY EXCEEDANCES OF THE GR UNIDWATR S TANDARDS'� YES NO �
a
rAS ANY ENFORKEIvlENT rA`-� T IONI SEEN TA E_N?YES _alb DATE OF AIS T ID I;
u IEF S!,?IMMARY OF EIFDRT.EMEt I T AS T I°D TAAEM
IONS (Continue on ravetse, Id necessary):

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality JON13
iL
James B. Hunt, Jr., Go'inn ^" -%ENR
sfs
Bill Holman, Secretary lu I y
t'42:7 iT1111 �m N C
Kerr T. Stevens, lrt J NORTH CAROB INA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
June 2, 2000
L. E "JOE" HUI)SON, JR
CITY OF STA,rESVILLE
POST OFFICE BOX I I I I
STATESVILLE. NORTH CAROLINA 28687
SubJect: Acknowledgement of, pplicat on No.
WQ0001759
City of Statesville
SluqV- ',an ;�q
Sludgy_- I )­e/_1/-
Iredell County
Dear Mr.. Hudson:
The Non -Discharge Pernritting Unit of the Division of Water Quality acknowledges receipt of your
Z
permit application and supporting materials on May 31, 2000
Your application package has been assigned to Shannon Thornburg, for a detailed review. Tile reviewer
will contact you with a request for additional information if there are, arry questions concerning your
submittal.
If you have any questions, please contact Shannon Thornburg at 919-733-5083 extension 353. Ti the
,reviewer is unavailable, you may leave a message on their voice mail, and they will respond promptly.
PLEASE REFER TO THE ABOVE APPLICATION NUMBER WHEN MAKING INQUIRIES
AVI Ir"14Z PDA11110'r
'j, ,
harge Pe thing Unit
1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled / 10% post -consumer paper

TON F3PDES FACILITY NND PERMIT DATA 0 /TI/00 10_a 59:3
ATE OPTION TRXID 5OU KEY W 001759
_-—
PERSONAL DATA FACILITY APPLYING FOR PERMIT APP/PE I'T FEE- ,00 REGION
FACILITY NAME> S`T'ATESVILLE, CITY —A SLU E/FOO COT .TY> IREUELL 0
ADDRESS: MAILING (REQUIRED) ENGINEER:
STREET- P , 0 , ECE 1,111 STREET
CITY: STATESV LLE ST NC ZIP 28687 CITY ;ST LIP C
TELEPHONE 704 87E 3438 TELEPHONE:
STATE CONTACT> THORNBURG FACILITY CONTACT L . . JOE HUDSON JR
TYPE OF PROJECT> SLUDGE —SURFACE DISPOSAL LAT: 354625 LONG: 0804715
DATE APR RCS 05/31/00 N=NEW,M=MODIFICATION,R=REISSUE> E
DATE ACKNOWLEDGED 0 / 0 / G 0 DATE REVIEWED RETURN DATE
REG COMMREQE / l DATE DENIED / iPDE S
R G COMM RCVD " DATE RETURNED / ! TRIP, Q __ 0000 MG
ADD INFO REQS AT AC COM RE S TRIR DATE
—
ADD INFO RCVD CT AC COO 'RCVD
END STA'T= ATOP P 0 /29/ 0 DATE ISSUED I LATE EXPIRE
FEE CODE( 5 )1=(>IMGD),2-(>I0KGD), =(>IKGD),4=(<TKGD+SF),=(S>300A),=(S<=300A)a
7= (SENIDEL) , = (SEDEL) , 9= (CLREC) , O= (NO FEE) DISC CODES ASN/C CT PART
ENG CERT DATE 00/00/00 LAST NOVDATE 00/00/00 CONBILL
COMMENTS:
MESSAGE: * * * DATA MODIFIED SUCCESSFULLY �

of
eS 's t tr
ij(1). Nwx 1111 - 4,ltatmoillc. North Tarohna 218687
May 26, 2000
Mr, Kim Colson
NC Division of Water Quality
Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: Surface Disposal of Residual Solids
Permit Renewali'Modification Request
Fourth Creek WWTP — WQ0001759
Dear Mr, Colson:
The City of Statesville requests the renewal of Permit No. WQOOO 1759 for the Fourth
Creek W'WTP monofill. Although this site is currently inactive and has not received
residuals since 1996, we understand that we must maintain the permit for monitoring of
the groundwater monitoring wells, All residuals produced from Fourth Creek NkVTP,
Third Creek WWTP and the Water Plant are now processed either through our lime
stabilization process under Permit WQ0006245 or through our contracted land
application program under Permit WQOO 16247,
Recently, staff discussed this permit renewal with Peggy Findley of the Mooresville
Regional Office, Groundwater Section to determine feasible reduction of monitoring, and
analysis. She indicated that a brief history of the monofill would be helpful. The history
of the monofill is such that it has been in operation since approximately 1983 and is
basically full, Area Ir4rI was filled with trenches during 1983, Area 42 was filled during
1984, Area #3 during 1985, Area 44 during 1985-86, Area #5 in 1986, Area #6 during
1987 — 1994 with additional trenches as indicated by the attached map. Since required by
permit all sludge has passed the annual TCLP and metals tests, Groundwater monitoring
results continue to indicate that there is no contamination or adverse impact to the area.
Due to the site inactivity for four years and the relatively clean history, of the monitoring
well results, we request reduced monitoring and a reduction in the parameters to be

May 26, 2000
Page
Kim ColsoniNCDWQ
Fourth Cr. Permit Renewal
ill 75
analyzed. We propose to monitor annually in December with reduction of the following
parameters: nitrate, total dissolved solids, Natal organic carbon, ammonia nitrogen,
chloride, fecal coliform cadmium, copper, zinc and volatile organic compounds.
We trust that you will find the application complete. Because the site is inactive, there i
no data to be presented for Sections I - III, If you have any questions or need to discuss
this request, please contact Renee Par man at 70 7 - 4 ,
-Sin
L P. " oe" Hudson, Jr., Director
Water/Wastewater Treatment
I.,FR,s
Enclosure
Filc colson penrz t renewal
i

State of North Carolina
Department of Environment, Health and Natural Resources
Division of, Environmental Management
Non -Discharge Permit Applicafion Form Rrcel,
(THIS FORM MAY BE PHOTOCOPIED FOR USE AS AN ORIG)WEj,3JjlV VED
7ysp("
SURFACE DISPOSAL OF RESIDUAL SOLVO$4 _7101V
This application is intended for facilities which are to be un�" regulated Q Cu�
b CFR , jk 3
This application shall be completed for residuals that are placed on an area of lana4ft4j) P;
moI disposal such as
a
monofills, surface impoundments, lagoons, piles or rounds. Reclamation shall be addre199 n the Lnd
Application of Residuals application form. An activity is not considered Surface Disposal if residuals are
placed on the land for 2 years or less for the purpose of storage.
L GENERAL VSFORMAT[W
I. Applicant's name (please specify the name of the municipality, corporation, individual, etc.):
2. Print Owners or Signing Official's name and title (the person who is legally responsible for the facility and its compiance)
3. Malling, address: &Y I I I I
City: Il State:_�! zip:
Telephone Number:
N
4, Application Date: 4 �:� I ()
5. Fee Submitted: S ,�_ [The permit processing fee should be as specified in 15A NC AC 2H .0205(c (5).1
6. Specify whether these residuals will be placed in: --morrofill, --surface cuipoundment or lagoon.,
piles or mounds,, -Other. If Other, please explain:
7. County(ies) were surface disposal unit(s) are located:
11. PERMIT INFORMATION:
I. Application No. (will be completed by DEM):
2. Specify whether project is: new- t,'_ renewal*;_ modification
For renewals, complete all sections included in the application.
3: If this application is'being submitted as a result of a renewal or modification to existing permit, list the existing -_,ermit
number and its issue date
FORM: SDRS 06/94 Page 1 of 9

111. FACILITY 1INFO1INIATION (attach additional pages for additional sources of residuals):,'
1, Name of facility where residuals are generated orprepared-, Ow
2, Facility permit number:
Facility permit holder:
3. Specify whether facility in III, I is owned by: federal; private; s tLa c; t--- local 17overnment,
_
4. Specify facility design flow: a L) m g, d
Facility average dadly flow: ------ I-L and
Type of residual storage:
Volume of residual storage: Zk A­o of
Length of residuals storage at facility: days (the Division requires a minimum 30 days storage in units tl�
are separate from treatment system, i.e, not in clarifiers, aeration basins, etc,)-,
Estimated volume of residuals: (dry tons/yr.);
5. Facility contact (person farruiliar with residuals preparation),-
6, Facility contact's telephone number:
T Location of treatment facility: � �10 �n State-, County
8. Mailitiv, address:
0 LLLL—
zi,
9, Latitude: Pd 35 Yl - S Longitude: Aa,_1� ��, 5_�
10, Specify the source of the residuals: L­ treatment of domestic wastewater; treatment of industrial wastewater
other (explain):
Please attach an explanation of either the treatment process, manufacturing process, or how the waste is generated. Provid,
full and complete details of the entire process.
11. Does the facility which generates the residuals have anapproved pretreatinent pro - ram! Yes; No,
This includes facilities which are classified as a "Class I" facility (any publicly owned treatment works required, under 4(
CFR 403.8, to have an approved pretreatment program or any facility treating domestic sewage that is classified as '"Class
I" by the appropriate federal or State authority)
IV. RESIDUALS INFORMATION (attach additional pages for additional sources of residuals):
'ktio Qtsl(u-, CU's?0,T_Ct of — jk_
1. Information for Hazardous Waste (RCRA) Determination. The, information requested on the limitations specified belo%
pertain only to those residuals that are generated from a municipal wastewater treatment facility with Lndustrial contributic
or active pretreatment program and from any other treatment facility with wastewater sources that include industrial sources
a. Are any of the residuals covered by this application listed in 40 CFI 261.31-26133? — Yes-, _ZNo. If Yes,
list the number(s):
b , Do the residuals exhibit any of the four characteristics defined by 40 CFR 261.21-261.24? — Yes; No,
Attach laboratory results for the Toxicity Characteristic Leactrinla Procedure Analyses, Reactivity, Ignitability, an,-
Corrosivity for each residual.
FORM: SDRS 06/94 Page 2 of 9

N-ift-c if the followint constituent levels ..rs determined by die Toxicity Characteristic Leachan� procedure Ana.
exceeded in the residuals or if tb . pl-1 of the residual
,
is not within (lie range listed below,
the residua,
definition a Hazardous waste, Chemical artalyses InUSL be made to Minimum Detection Levels.,
1' —PM
PE
Arsenic 5,0
Barium
100,0
Benzene 0,5
Cadmium
Lo
Carbon tetrachloride: 0.5
Chlordane
0,03
Chloroben ene Iflf O
chloroform
6.O
Chromium 5.
o-Cresol
200.
rn-tw resol 200,0
p®Cresol
200,0
Cresol 20 .
2„4_pD
if o
1,4-Dichlorobenzene 7,5
1,-Diclalor t e
0,5
1„1-Dic loroetbylene 0,7
2,4-i tnitrotoluene
0,13
Endrin & 2.
Heptachlor d its hydroxide)
0,008
;~ltlorobenzene il_1
He chloro-l.5-butadiene
.5
gape
Lindane 0A
Mercury
0.2.
Methoxychlor 10,0
Methyl ethyl ketone
200,0
Nitrobenzene 2,
Pentach orophenol
100,0
Pyiidine 5.f1
Selenium
1,0
Silver 5,O
Tetrachloroethylene
03
Tom pheue 015
Trichloroethylene
0,5
2,4,5-Trichlorophenol 400.0
2,4, _Trtchlorophenol
10
2,4,5-'TP (Silvex); Lo
Vinyl chloride
0,2
pH (2:1 vol./wt.): >2.0 s.u. - , 2.5 s.u.
NOTE: IF ANY OF THE RESIDUALS ?MEET
THE DEFINITIONS OF A
HAZARDOUS WASTE-,
AS NOTED IN EITHER "A" OR "B"
ABOVE, A PERMIT CANNOT BE ISSUED FOR
THAT RESIDUAL AND IT SHOULD
NOT BE INCLUDED
AS PART OF THIS
APPLICATION.
1 .For each residual, please attach a cbemical analysts of the material
that includes at a minimum the following:
Arsenic Chromium Mickel
5. The pollutant ceiling concentration for Arsenic, Chromium and Nickel will be determined in accordance with 40 CFR Pa
505_ In the table below, please state the act..a.l distance from the active sewage sludge unit boundary to the property line o
the surface disposal site in meters I meter _ 3.281 feet)
and the pollutant concentrations for Arsenic, Chromium anu.
Nickel in the table below (attach lab alysz�,).
RM: SDRS06/94
Page 3 of 9

V. PATHOGEN AND VECTOR ATTRACTION REDUCTION INFORIMATION (attach additional pa-.qes
additional sources of residuals),
1. For a residual to be disposed in a Surface Disposal Unit, one of the following options for pathogen reduction and vecLo,
attraction reduction must be met, Please specify which of the following options will be met: *
Sewage sludge, placed tan an active sewage sludge unit shall be covered with soil or other mterial at the end of each
0 C,
operating day. If this option is act, skip number 2 and number 3 and continue on to Section VI,
Class B pathogen reduction, in accordance with the Pathogen requirements in 40 CFR 503.32(b). If Class B, please,
continue on to number 2 and number 3.,
2. In order for Lhe residuals to be Class 3, with respect to pathogens, one of the folloxing criteria must be achieved,
— Please specify a, bl, K, b3, b4, by or c from below (submit all lab analysis, test results and calculations):
a, at least seven residuals samples should be collected at the time of use and analyzed for Fecal coliforms durinla each
monitoring period. The geometric mean of the densities of these samples will be calculated and should be less than
0
2,000,000 most probable number per grant of total dry solids, or less than 2,000,000 Colony Forming its per Sr- rn
of total dry solids.
W'
I. & �jDi �eti IRn - residuals arer agitated with air or oxygen to maintain aerobic conditions for a mean cell
residence time and temperature between 40 days at 200 C and 60 days at 150 C.
1 AiLD Ly,mg - residuals are dried on sand beds or on paved or basins for a minimum of three months. During two of
the three months, the ambient average daily temperature is above 00 C.
0
3. Anaunbic—DigiaLm - residuals are treated in the absence of air for a mean cell residence time and temperatwe
between 15 days at 3513 C to 50 C and 60 clays at 200 C
4. C2mrj �_�a - using either the within -vessel, static aerated pile, or windrow composting methods, the temperature
of the residuals are raised to 400 C or hicber for five days. For four hours during the five days, the temperature in
0 y
the compost pile exceeds, 550 C.
5. Lime Stabilia =j _n - sufficient lime is added to the residuals to raise the pH of the residuals to 12 after two hours
of contact.
c. The residuals shall be treated by a process that is equivalent to a "Process to Significantly Reduce Pathogens" (PSRP),
as determined by the perrnitting authority, based on an evaluation of the recommendations provided by the Pathogen
Equivale.?cy Committee,
3. When residuals are disp osed in a surface disposal unit, at least one of the following vector attraction reduction requirements
(a, b, c, d, e, I, g, It, i, or j) described below must be met.
Specify the letter(s) of the vector attraction reduction requirement that has been met (submit lab results, test results
and calculations), Any variation of the below must be described in full detail and attached.
a, A_ejahlc_2r,anaerobic DigeLtQT Digestion - The mass of volatile solids are reduced by at least 38%. Volatile solids reduction is
_
measured between the residuals, prior to stabilization, and the residuals ready for use or disposal. This criterion should
be readily met by properly designed and operated anaerobic digesters, but not as readily met by aerobic digestors.
Treatment facilities with aerobic digestors may need to meu the vector attraction reduction requirement through 18c or
IBd
h. AnaerobiQigt��n - If 3 38% volatile solids reduction cannot be achieved, vector attraction reduction can be c
demonstrated by further digesting a portion of the previously digested residuals in a bench scale unit for an additional
40 days at 300 C to 370 C. If, at the end of the 40 days, the volatile solids are reduced by less than 1717c, vector
attraction reduction is achieved.
c. A��JD�igti rt Af 38% volatile solids reduction cannot be achieved, vector attraction reduction can be demonstrated
by further digesting a portion of the previously digested residuals that have a solids content of 2% or less in a bench
scale unit for an additional 30 days at 200 C. If, at the end Of [he 30 days, the volatile solids are reduced by less than
15%, vector attraction reduction is achieved -
FORM: SDRS 06/94 Page 4 of 9

The specific oxvoen uptake rate (SOUR) shall be equal to or less than
, :> L5 milligrams of oxygen
per hour per grant of total dry solids at 20' C.
c. The temperature of the residuals for at least 14 days shall be greater than 400 C. During this time
the average temperature shall be greater than 450 C.
L The pH of the residuals is raised to 12 or higher by alkali addition and, without the, addition of
more alkali, remains at 12 or big -her for 2 hours and then at 11.5 or hicC,her for an additional 2hours.
g rvnn f 3i d stalidsi - The total solids of residuals that do not contain unstabilized solids, and which are generated
in a primary wastewater treatment process, -shall be equal to 'or greater than 75%. Blending with other materials is not,
allowed to achieve the total solids percentage,
h . Irvin cr fun to ili7ed5DIi - The total solids of residuals that contains unstabilized solids, aud which are generated in z
primary wastewater treatment process, shall be equal to or greater than 90%. Blending with other materials is not
allowed to achieve the total solids percentage.
Z�
i InjUji" - Liquid residuals are injected below the land surface, with no significant amount of residuals present on the
land surface after I hour, unless the residuals are Class A for pathogen reduction. In this case, the residuals shall be
injected within 8 hours after being discharged from the pathogen treatment process.
j JacQZKm1iron - Residuals that are surface land applied shall be incorporated into the soil within 6 hours of application,
unless the residuals are Class A for pathogen reduction. In this case, the residuals shall be incorporated within 8 hours
after discharge from the pathogen treatment process,
VI. LINER AND GROUNDWkTER INFORMATION:
L Describe the liner for the proposed or existing sewage sludge unit. The liner should be of natural material at least one too
in thickness, compacted to 95% proctor standard dry density and installed and compacted in layers no thicker than sil
inches, with a hydraulic conductivity of no greater than 1 x 10-7 centimeters per second or a or a synthetic material tha
covers the bottom of a sewage sludge unit with a hydraulic conductivity of no greater than I x 10-7 centimeters per second
Verification of the liner's compliance with hydraulic conductivity and thickness specifications must be provided. Al
construction and design specifications shall be attached.
2. Describe the leachate collection system for the proposed or existing sewage sludge unit. The leachate collection system is,
system or device installed mimednrtely*above a liner that collects and removes leachate, (liquid waste, from rainfall that szep,
through the contents of the disposal site). All construction and design specifications shall be attached.
3. Vertical distance between bottorn- of the sewage sludge unit to the seasonal high water table.
4. Depth to the seasonal high water table:
0
VIL RESIDUALS TRANSPORT AND APPLICATION:
1. How will the residuals be delivered to the active sewage sludge unit (pumps, leak proof trucks, etc.)?
2. What type of equipment will be utilized for the distribution of residuals in an active sewage sludge unit?
3. Will the surface disposal operation utilize a contractor who specializes in Residuals Management or will the permitte,
manage the program? - Contractor; - Pertirittee, If a contractor is utilized, provide the name of the firm,
contact, address, and telephone number-,
FORM: SDR S 06/94 Page 5 of 9

VHL SITE EVALUATION:
1, For each active sewage sludge unit, please submit the following:
a. A vicinity map. This map must show the location of each site in relation to at least two geographical 9 . references and
major intersection (numbered roads, named streams/rivers, etc.).
b. A detailed site location map, This map must be drawn to scale with topographical contour intervals not exceeding ren,
feet or 25% of total siege relief (whichever is more descripti ' ve) and showing
g the property lipes; all existing wells, a
surface waters and drainage ways- 100-year flood zone; all dwellings within 500 feet of the active sewage sludge unit.-
and include all buffers.
Note: At a minimum the following buffers must be maintaine_-d�
I. 400 feet from any habitable residence,
1 100 feet between the active sewage sludge unit and any public or private water supply source, all streams classiflieC
as WS or B, waters classified as SA or SJ3 and any Class I or Class 11 impounded reservoir used as a source
drinking water,t
3, 100 feet between the active sewage sludge unit and any stream, lake, river, or natural drainage way,t
450 feet between the active sewage sludge unit and property lines (if the original permit was issued with the buffo,
distance to property line as 10O feet, updated maps must I-- submitted and new acreage delineated for the buffer t�,
be reduced), 1_�
5 a 10 feet between the active sewage sludge unit and any interceptor drains or surface water diversions (upslope),
6. 25 feet between the active sewage sludge unit and any inter( ptor drains or surface water diversions (downslope),
7. 25 feet between the active sewage sludge it and any groundwater lowering and surface drainage ditches,
SPECIFY THE NAME OF ANDT CLASSIFICATION OF THE CLOSEST DOWNSLOPE, SURFACE WATERS
(as established by the Environmental Management Commission) TO T14E LAND APPLICATION SITE(S). US --
THE ATTACHED INFORMATION SHEET (PAGE 8 OF 9) TO OBTAIN THIS INFORMATION,
2, For each active sewage sludge unit, attach a soil evaluation by a soils scientist (the evaluation must be signed by the sci!
scientist) which addresses soil color, the depth, thickness and typeof restrictive horizons-, the presence gar absence, of 2
seasonal high water table or bedrockVithin thme vertical feet of the deepest point of residual application; pH and catio,-,
exchange capacity. If the depth to either groundwater or bedrock- is less than three feet, please also attach a demonstratior'. .
using predictive calculations or modeling methods acceptable to the Director of the Division of Environmenta' '
Management, that the use of this site will net result in the contravention of classified groundwater standards as contained in
N , CAC 2L .0200. one . 'This report must be signed by the soil
scientist and submitted with application,
3. Explain how access to the active sewage sludge unit, by both people and animals, will be controlled:
4. Describe how runoff will be collected and disposed. The runoff collection system of an active sewage sludge unit must
have the capacity to handle runoff from a 2-hour, 25-year storm event -
IX. GENERAL LNFORMATION:
I. Five (5) complete copies of the permit application and five (5) copies of all required supporting information, including
cover letters must be submitted or the application package will be returned as incomplete.
2. The attached Watershed Classification Form must be submitted to the appropriate Regional Office prior to the submittal of
the application package to the address below.
3, If more than one active sewage sludge unit will be included in this permit, each active sewage sludge unit must be assigner.,'
an identification number. in
FORM: SDRS 06/94 Page 6 of 9

..........--_ ._
c and tw ortrplete Address of Engineering Finn:
ity:State; tom•
Telephone Number: � ;d
Professional Engineer's Certification:
I, }-attest that this application for
has been reviewed by me and is accurate and complete to the best of my ktnowFletlge. I further attest that to the Hest of testy kcnourledtt<w
the proposed design has been prepared in accordance withthe applicable regulations, Although certain portions of this subniitta'
package may have been developed by other professionals, inclusion of these materials under my saanature and seal signifies that I hay, r
reviewed this rxtaienal and have judged It to be consistent with tare proposed design. V
North Cartshna, Professional Engineer's Seal, Signature., and" am:
Applicant's Certification:
I attest that this application for _.
has been reviewed by me and is accurate and complete to the hest of my knowledge, e, i understand that if all required harts of this;
application are not completed and that if all required ,supporting inforttration and attachments are not included, this application vack;a c
THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTING I R-MA1 ION MkTERIALS,
SHOULD BE SENT TO THE Pt LL ING . D SS.
NORTH ALI DIVISION O I N T L °t: 1 G-EMENT
WATER QUALITY SECTION
PERMITS AND ENGINEERING UNIT
POST OFFICE BOX 29535
,LEI S, NORTH LI =27626-0535
TELEPHONE UMBER: (1. 733-5083
FAX NUM 1.9 733-9919
` ; SDRS 06/ `
Page 7 of

APR 13 20W "144
Ice This form insist be completed by the appropriate Reojona Ofr rind includd wit
Submission of the application pacl;a,_,e.
INSTRUCTION'S TO APPLICANT
In order to dermine ihe classil"Ication of Lhc watershed in which these active sl%Va': slud2- units will
located, vou at,. r,,jUircd to sus)-mit this fo.-In, with itCrns 'I through 8 completed, to the, appropriate Div worm
Environmerv,ak1anazc-m_-nL Reuional Wa_,r Quality Supci­N,isor (see attached listing). At,a minimum., V011
lm­,ludc, an 8.5" 1,y 11" copy of tic ,ion of a T5 n1mute USG S Topographic Map which shows m�- subjz_"
P
surface waters. You must identify the locai*',on of the facility and the closest downslope surface waters lkkaters
which vou are J-S"iJ2 the classification) on thesubmitted map copy. The application may not
submitted until this form is completed and included with the submittal.
inlean specyhnmyotherApplleeap,po,nvidualor
-Le Address of Applicant:
Z' Namc arid Comple
CiLy. StatcZip,- ___28LZ3
Telcr,,hone Number:
3. Project.,,-ame.,
4. Volume of residuals to be disposed: dry tons, per year
5. Name of closest surface waters:
inactive
6. County(ics) where a__sewalaelsludce unit is located- 1 1
z -
7. Map name and date: Statesville East 1993
8 Applicant Signature:
TO: REGIONAL WATER QUALITY SUPERVISOR
Pleasa provida rne'�vith the clessification of -Lhel w2tcrshe.d where these active sewac4e. slud2e, units are. locate,
as identified on the attached map segment:
Narne of surfacCl lxaL.-rs:
Chassification (as -established by the Environirriental Management Commission):
Proposed Classification, if applicable:
Sianature, of reaional office personnel- Date: Z7 _4
FORM: SDRS (16/94 Page 8 of 9

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State of North Carolina
Department of Environment,
Health and Natural Resources
Division of Environmental Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
A., Preston Howard, Jr., P.E., Director
Mr. Jack King, City Manager
C�
City of Statesville
P,O, Box 1111
Statesville, NC 28687-1111
Dear Mr, King:
III
July 17, 1996
Subject: PernritNo.WQ0001759
City of Statesville, Fourth Creek Monofill
Surface Disposal of Wastewater Residuals
Iredell County
I In accordance with the request dated January 18, 1996, a draft permit and the subsequent
acceptance of this draft by the City of Statesville by letter dated June 24, 1996, we are forwarding
herewith Permit No. WQ0001759, dated July 17. 1996, to the City of Statesville for continuing operation
of a surface disposal site for the purpose of the disposal of wastewater residuals with temporary storage of
dewatered residuals allowed at the surface disposal site on recognized holidays, weekends and after
normal business hours. The facility must comply with federal and state requirements for the collection of
all runoff from the surface disposal site (as outlined in 40 CFR Part 503.24 (g) (1) and (2)).
This permit shall be effective from the date of issuance until November 30, 2000 shall void Permit
No. WQ0001759 issued December 20, 1995, and shall be subject to the conditions and limitations as
specified therein. Please pay particular attention to the monitoring and reporting requirements contained in
this permit, Failure to establish an adequate system for collecting and mwntaining the required operational
information will result in future compliance problems.
The City of Statesville has reviewed and accepted a draft of this pen -nit, therefore, this permit is
final and binding,
PD, Box 29535, Raleigh, North Carolina 27626-0535 Teleph6ne 919-733-7015 FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycledJ 10% post -consumer paper

if you need additional information concerning this matter, please contact Ms. Carolyn McCaskill atN
[phone] ext. 540 or Mr. Matt Williams at ext. 509.
Sincerely,
cc'� Iredell County Health Department A. Presto�jHoward, Jr., P.E.
Mooresville Regional Office, Water Quality Section
Mooresville Regional Office, Groundwater Section
Bob Cheek, Groundwater Section, Central Office
Training and Certification Unit no revised rating)
Facilities Assessment Unit

NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES
RALEIGH
SURFACE DISPOSAL PERMIT
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as
amended, and other applicable Laws, Rules, and Regulations
PERMISSION IS HEREBY GRANTED TO THE
Clily of Statesville
Iredell County
W-41AW0
d a part of this permit.
This permit shall be effective from the date of issuance until November 30, 2000, shall void Permit
No. WQ0001759 issued December 20, 1995, and shall be subject to the following specified conditions
and limitations:
I I. PERFORMANCE STANDARDS
3. In the event that any sewage sludge unit is not operated satisfactorily, including the creation
of nuisance conditions, the pertnittee shall cease disposing of the wastewater residuals to
the, sewage sludge unit and take any irmnediate corrective actions as may be required by the
Division.

The following buffer zones shill be maintained:
r
Some of the buffers specified above may not have been included in previous permits for
this surface disposal site. These buffers are not intended to prohibit or prevent
modifications, which are required and approved by the Division, to improve performance
of the existing disposal facility. These buffers- do apply, however, to any expansion or
modification of the surface disposal site and apply in instances in which the sale of
property would cause any of the buffers now complied with, for the disposal facilities, to
be violated. The applicant is advised that;any modifications to the existing facilities will
require a permit modification,
copy of this permit shall be maintainedat the surface disposal site when residuals are
being disposed during the life of this pernut. A spill prevention and control plan shall be
maintained in all residuals transport and application vehicles.
8. Disposal (or any application) Of residuals W"test, or are classified, as hazardous or
toxic waste as defined in 40 CFR Part 261 is expressly prohibited at this site.
OPERATION A- MAINTENANCE RE EIREMEI TT
1. The facilities and sewage sludge sites shall be properly maintained and operated at all times.
I9

o residuals other than the following e hereby approved for disposal in the sewage
sludge units in accordance with this pe it
Perrin t Estimated
dour e rin �urn r �' ltrrrr� d n��e
Fourth Creek WWTP lredcll NCO031836 1,200
ThirdCreek WWTP bedeh NCO020591 930
Statesville WIP Iredell 160
The pollutant concentrations in the residuals which will be disposed in sewage sludge unit
shall not exceed the following Ceiling Concentrations"((Dry 'Weight Basis):
41
Parameters rrra
Arsenic 39
Chromium 260
Nickel 270
. An active sewage sludge unit shall not restrict the flow of a base flood.
m An active sewage sludge unit ,shall not be. located in an unstable area.
Appropriate measures must be taken to control public access to the surface dispo, al site
during active site use and for the -months following closure of the sewage sludge unit.,
Such controls may include fencing and the posting of signs indicating the activities being
conducted at each site,..
9. Adequate provisions shall be taken to prevent rind erosion from conveying pollutants from
the surface disposal site onto the adjacent property or into any surface eaters
10. Application rates to this surface disposal siteshallnot exceed 1,000 cubic feet per year.
IL Food crops, feed crops and fiber crops shall not be grown on an active sewage sludge unit;
unless approval has been requested and received from the Division of Environmental
Management.
12. Animals shall not be grazed on an active sewage sludge unit unless approval has been
requested and received from the Division of Environmental Management.
3

Ill. 7qq
1. Any monitoring (including groundwater, surface water, residuals, soil, or plant tissue
analyses) deemed necessary by the Division of Environmental Management to insure
protection of the environment will be established and an acceptable sampling and reporting
schedule shall be followed.
2. Proper records shall be maintained by the Permittee tracking all application activities.
Theserecords shall include, but are not necessarily limited to the, following info rmation-
a. source of residuals
b. volume of residuals disposed in gallons/year, dry tons/year, or kilograms/year
3. A residuals analysis shall be conducted quarterly from the date of permit issuance for the
residuals from the Third Creek and Fourth Creek wastewater treatment facilities, and
annually for the residuals from the water treatment plant. The analyses shall be the
responsibility of the Perritittee and the results shall be maintained on file by the, Pe tree
fora minimum of five years. If disposal of residuals from either of these facilities at the
subject site occurs at a frequency less than quarterly, a residuals analysis will be required
for each instance of land application for the applicable facility.
The residuals analysis shall include, but is not necessarily limited to the following
parameters -
Arsenic % Total Solids
Chromium pH
Nickel
After the residuals have been monitored for two years at the above frequency, the Perrnittee
may submit a request to the Division for a permit modification for the reduction of the
frequency of monitoring for pollutant concentrations and for the pathogen density
requirements, but in no case, shall the frequency of monitoring be less than once per year
when residuals are, applied to the land.
4 A Toxicity Characteristics Leaching Procedure (TCLP) analysis shall be conducted by the
Pernuttee annually for the residuals from each of the wastewater treatment facilities. This
requirement does not apply to the residuals from the water treatment, plant. The TCLP
analysis shall include the following parameters (please note the regulatory level in mg/L in
parentheses). -
Arsenic (5.0) Barium (100. 0)
Benzene (0.5) Cadmium (1.0)
Carbon tetrachloride (0.5) Chlordane (0.03)
Chlorobenzene (100.0) Chloroform (6.0)
Chromium (5.0) o-Cresol (200.0)
in -Cresol (200.0) p-Cresol (200.0)
Cresol (200.0) 2,4-D (10.0)
1,4-Dichlorobenzene (7.5) 1,2-Dichloroethane (0.5)
1,1-Dichloroethylene (0.7) 2,4-Dinitrotoluene (0,13)
Endrin (0.02) Heptachlor (and its hydroxide) (0.008)
Hexachlorobenzene (0.13) Hexachloro-1,3-butadiene (0.5)
Hexachloroethane (3.0) Lead (5,0)
Lind (0-4) Mercury (0.2)
Methoxychlor (10-0) Methyl ethyl ketone (200.0)
Nitrobenzene (2.0) Pentachlorophenol (100,0)
Pyridine (5.0) Selenium (1.
Silver (5.0) Tetrachloroethylene (0.7)
Toxaphene (0.5) Trichloroethylene (0.5)
2,4,5-Trichlorophenol (400.0) 2,4,6-Trichlorophenol (10)
2,4,5-TP (Silvex) (1.0) Vinyl chloride (0.2)
4

i. The EPA certification statements concerning compliance with pathogen requirements,
vector attraction reduction requirements and management practices must be completed
quarterly by the proper authority or authorities if more than one is involved, either the
person who prepares the residuals, the person who derives the material, or the person who
applies the residuals.
r
rThr&b copies of all required monitoring and reporting
conditions 1111, 1112, 1113, 1114, and 1115 shall be s mi ed n ally on or before March
NC Division of Environmental Management
`dater Quality Section
Facility Assessment Unit
PO Box 29535
Raleigh, NC 27626-0535
.7 : The air in all structures within the surface disposal site and the air at the property line shall
be continuously monitored for methane gas. The following criteria shall be met.
• In .structures the concentration of methane gas in the air shall not exceed 5% of
the lower explosive limit f L L,l for methane gas.
• At the property lane: the concentration of methane gas in the air shall not exceed the
lower explosive limit (f, L) for methane gas.
8. Noncompliance Notification:
The Permittee shall report by telephone to the Mooresville Regional Office, telephone
number [phone], as soon as passible, but in no case more than hours or on the
next working day following the occurrence or first knowledge of the occurrence of any of
the following:
a. Any occurrence with the surface disposal program which results in the disposal of
significant amounts of wastes which are abnormal in quantity or characteristic.
b . Any failure of the surface disposal program resulting in a release of material to
receiving waters;
ce Any time that self -Monitoring information indicates that the facility has gone out of
compliance with the conditions and limitations of this permit or the parameters on
which the system was designed.
d. Any process unit failure, due to known or unknown reasons, that render the facility
incapable of adequate residual treatment.
e. Any spillage or discharge from a vehicle or piping system transporting residuals to the
disposal site,
Persons reporting such occurrences by telephone shall also file a written report in letter
form within 15 days following first knowledge of the occurrence. This report must outline
the actions taken or proposed to be taken to ensure that the problem does not recur.
E

IV.
GROUNDLNVLA-TER REQUIREMENIS
1. The three ) existing monitor wells (numbers l ,'2 and shown on the attached site reap,
roust be sampled every March, July and November for the following; parameters:,
NO3 'IDS
TOC p
Ammonia Nitrogen Chloride
"Water Level Fecal Coliforms,
Cadmium
Copper
Volatile OrganicCompounds-In November only (ley Method l or Method 2, low)
MethodMethod 1- Methods
Examination of Water and Wastewater". 17th ed.I1089
Method 2: Method Q2.2 "Methods For The Determination Of Organic Compounds
In Drinking dater", U.S. EPA-600/4-88/039
The measurement of water levels must be made prior to sampling for the remaining
parameters. The depth to water in each well shall he measured from the surveyed point on
the top of the casing.
The measuring paints (top of well casing) of all monitoring wells shall be surveyed to
provide the relative elevation of the measuring print for each monitoring well.
« «
« «
«
« « « «
«
GroundwaterThe results of the sampling ad analysis shall besent to the o
Complianceand «
Report[Compliance Monitoring ;
• � a
M

In accordance with 15A NCAC 2L, a MMY-MINLAn is established around the
disposal systems midway between the Compliance Boundary and the perimeter of the
waste disposal area. Any exceedance of standards at the Review Boundary shall require
rernediation action on the part of the Permittee.
1 Any additional groundwater quality monitoring, as deemed necessary by the Division, shall
be provided.
V !NSEECT—I-Q N S
I The Permittee or his designee shall inspect the residuals storage, transport, and disposal
facilities to prevent malfunctions and deterioration, operator errors and discharges which
may cause or lead to the release of w&,,tes to the environment, a threat to human health, or a
nuisance. The Permittee shall maintain an inspection log or summary including at least the
date and time. of inspection, obsentations made, and any maintenance, repairs, or corrective
actions taken by the Permittee. This log of inspections shall be maintained by the Permittee
for a period of five years from the date of the inspection and shall be made available to the
Division of Environmental Management or other permitting authority, upon request.
Any duly authorized officer, employee, or representative of the Division of Environmental
Management may, upon presentation of credentials, enter and inspect any property,
premises or place on or related to the surface disposal site or facility at any reasonable time
for the purpose of determining compliance with this permit, may inspect or copy any
records that must be kept under the terms and conditions of this permit; and may obtain
samples of groundwater, surface water,, or leachate.
VL GENERAL CONDITLQ.�N .LS
1. This permit shall become voidable unless the surface disposal activities are carried out in
accordance with the conditions of this permit, the supporting materials, and in the manner
approved by this Division.
This permit is effective only with respect to the nature and volume of wastes described in,
the application and other supporting data.
C�
3r This permit is not automatically transferable. In the event that there is a desire for the
facilities to change ownership or a name change of the Pertittee, a formal permit request
must be submitted to the Division of Environmental Management accompanied by an
application fee, documentation from the parties involved, and other supporting materials as
may be appropriate. The approval of this request will be considered on its merits and may
or may not be approved,,
4. Failure to abide by the conditions and limitations contained in this permit may subject the
Permittee to an enforcement action by the Division of Environmental Management in
accordance with North Carolina General Statute 143-215.6(a) to 143-215,6(c).
5 The annual administering and compliance fee must be paid by the Permittee within thirty
(30) days after being billed by, the Division. Failure to pay the fee accordingly may cause
the Division to initiate action to revoke this per miras specified by 15 NCAC 2H D205
6. The issuance of this permit does not preclude the Pernrittee from complying with any and
all statutes, rules, regulations, or ordinances which may be imposed by other government
agencies (local, state, and federal) which have jurisdiction.
7

7. The Pe tree, at least six ) months prior to the expiration of this permit, shall request its
extension. Upon receipt of the request, the Commission will review the adequacy of the
facilities described therein, and if warranted, will extend the permit for such period of time
and under such conditions and limitations as it may deem appropriate.
. This permit may be modified, or revolved and reissued too incorporate any conditions,
limitations and monitoring requirements the Division of Environmental Management deems
necessary in order to adequately protect the environment and public health.
9. The Division must notified in writing at least 180 days prior to closing of the surface
disposal site. A forinal closure plan shall be required to be submitted at that time,
Permit issued this the 17th day of July, 1996
NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION
e -
w
'" :
A. Presto o °a d, Ir., ,, Director
Division 4IEnvironrnent l Management,
y authority of the Environmental Management Commission
Permit Number NNIQ0001759

SOC PRJORITY PROJECT- Yes No X
If Yes, SOC No.
To: Permits and Engineering Unit
Z!�
wo.t"V- fAvaalrrvtia
Attention: Ms. Shannon Thornburg
Mooresville
Date- July 24, 2000
NON -DISCHARGE STAFF REPORT AND RECOMMENDATION
COUNTY: Iredell
Permit No. WQ000 175 9
Renewal for monofill (fourth Creek W)VTP)
Groundwater monitoring only
PART I - GENERAL INFORMATION
I Facility and Address-, City of Statesville
Fourth Creek W',N'7.--P
Post Office Box I I I I
Statesville, NC 286977
1 Date ol'Investigation: June 26, 2000
1 Report Prepared By: Ellen Huffman
4; Person(s) Contacted and Telephone Numb-_,r: L.F. "Joe" Hudson, Jr.
704/878-3438
5Directions to Site(s): From the intersection of 1-77 and H)Ny 70, travel east on hwy 70
(toward Salisbury) about 6 miles to Bell Farm Road. Turn left onto Bell Farm Road and
travel about I mile, Look, for sign and entrance to plant on right.
6Type of permit: Renewal of a non-dischargle sludge monofil permit.
7. Size (land permitted for application): 9.4 acres
This is an inactive monofill (since 1996). Ilermit is for GW monitoring only,
8. Topography (relationship to I 00-year tlooCf plain included): Monofil is not in or near a 100-
year flood plain. USGS map showing monofil is included in the permit package.
1
Page

i ; Buffer conflicts with location of nearest dwelling and water supply well: Yes No
10. Watershed Stream Basin Information for land application sites:
a. Watershed Classification. Class
baver Basin and Subbasin No.: Catawba 03-07-06
. Distance to surface water from disposal system; n1a
P - DESCRIPTION OF WASTES TREATMENT W
l , a. residuals Volume: 300 drys tons per year, wastewater treatment plant residuals
b. Types and quantities of wastewater: % Industrial % domestic
Volume e of wastewater residual sto pep n/
d. Estimated days of storage: days n/a
e, Volume of water treatment; residuals: n a
Wastewater Treatment Facilities
a; Current permitted capacity of the 'WWT facility - 6.0 MG
1 . average daily flow of the WWT facihiy� 4,0 MGD
Description of existing wastewater treatment facilities: n/a
Description of proposed wastewater treatment facilities: a
3. _ residuals handling and utilization/disposal scheme: The sludge rnonofil has been inactive
since 1996 and the groundwater monitoring for this site continues to reflect compliance with
groundwater standards;
4, 'Treatment plant classification: Grade IV Biolo2ical Water Pollution Control SystemONTWT, P
SIC Code(s;
Wastewater Code(s) i
Primary.- Secondary -
Main Treatment Unit Code:
PART III - OTHER PERTINENT INFORMATION
l: Is this facility 'being constructed with ons Lruotion Grant Funds (municipals only)? n/a
W Special monitoring requests': Groundwater monitoring can be reduced to annual sampling it
December) for ply, water level, cadmium, 70d NO3. Also perforni the usual field
2
Pig

measurements and procedures listed on the groundwater monitoring form.
1 Important SOC, JOC or Compliance Scheduie dates: n/a
4. Other Special Items: n-la
PART IV - EVALUATION AND RECOMMEND ATIONS
The application is a request for renewal of an existing monofil (inactive) permit (GW
monitoring only). This renewal also requests, a reduction in the groundwater monitoring
frequency. Peggy Finley, GW-MRO, agrees that the monitoring frequency can be reduced
to annually (in December) for PH, water leve-1, cad mium,'VOC, and NO3- Permittee MUSt
continue to perforrn the usual field measurements and follow the sampling procedures listed
on the groundwater monitoring form. This office has no objection to the request for reduction
of GW monitoring frequency. I GW report is attached.
The City of Statesville currently handles residuals produced by its Third Creek and Fourth
Creek \k'WTPs by two permitted methods 1) a class A residual lime product (permit
4'WQ0006245), and 2) land application (perntit 4WQOO 16247).
This office recommends issuing the permit with the above mentioned groundwater
monitoring changes,
Signature of Report Pr ,eparer
Water QuTt-7,Regional Supervisor
Date
3

-'Yzv A
r1orth C',-,arohna, Depairtrnent of Et*,ronment and 1,,Ialturad Resaurces
11�
D'Vsicn of "'Q'U"'311[y
DRevedy vi-s Pe,,-,1"ue challes 'V*Va""'IkHd1 P
r�overnor Director e, c to r Y
Augtist 22, 20 1'-
NIR, L.F. I I IAY,30N.JR., DIRF'ICTCaIAOF' A'fl",,R RESOURCES
CITY 01" STA "T PS,, V 11, L 1 -1
f`0S"F0FFK1't,,., Box I I l I
STATJ1"",V11A-.E, NC 28687
SLAJect: Rescission of Surl'ace Disposal of Residuals Permit
Perinit No, WQ0001759
Fourth Creek Wastewater Treatment Plant
tredell County
AU")
BY:
Dear Mr. Hudson:
Reference is made to your reqtiest for rescission ofthe subject Surface Disposal of ResidUals Permit, Staff
from the Mooresville Recrional office:has confirined that permit conditions for post closure have (recta
met and this Pertuit is no longer required. Therefore, in accordance with your re(lucst, Permit No
WQ0001759 will be rescinded upon completion of tire monitoring well abandonment requirements as
Specified beltm
Monitoring wells MW-1, IAW-2, an(] MW-3 shall be permanently abandoned. Within 30 &-iys of
abandonment, a Well Abandonment Record (Form GW-30) listing this pernut nuniber and Lhe
appropriate monitoring well identification number, shall be cornpleted for each well abandoned
and mailed to (lie Division of Water Quality, Aquifer Protection Section, 1636 Mall Service
Center, Raleigh, NC 27699-1636, A North Carolina Certified Well Contractor shall abandom the
monitoring wells according to tire North Carolina Well Construction Standards (I 5A NNSAC` 0`2C
.O t 13) and local county rides.
Please submit as copy of this letter along with the Well Abandonment Record (Fonn GW-30),
If it would be helpful to discuss this nv'irter further, please do not hesitate to contact Clionticha k1clianict
at telephone [phone], or the Mooresville Regional Office, Aquifer Protection Section,
in cerely,
C,,,'Charles Wakild, P. E,
cc: fredell County Health Department
Mooresville- Aquifer Protection Regional Supo""IECEIVEDIDENRIDWO
Permit File WQ0001759
F E B if 5
A QU IF ER PR(11,7t E-CTiCN!S�CT ION
1636 t-Aiasl Cr er Rile,,,',h, troth
Ilxatimr 512 -N S�, Raletgh, North P50, 4 Aquifer Protection Secoon ai,
Phone: 9,19-807-64W, FAX, 919 807-64% N O.FfkC iarol i i io,
ki qu,'i!

F
�� � , a � � rrtkCa t.`ttt'd'3lirara 1+~tiatritat�tai tat I aa�•°ardattaaactNl astarT fvatrrarat Et°s<.kaarces- I„Tfvi,�alti�:rT'f,)$iaTlity-
1! WELL CONTRACT R—
DANNY SUMMERS
Well Contractor (Incte.,Kdtaal) Nsmo
GEOLOGIC L"XJ`1 R TTCII1, ILTC
Well CtsacfNr 10f Cotalprany Name
176 COMMERCE CaLVD 6.
lieut iyflriress
ST A I ESVIL..LE" NC 28625
City or Town state Zip Cote
t....,, ..�...) _ ._.
704 tI7;�-7ttt
a r cStl PhOrle number
r
2. WELL INFORMATION:
SITE WELL 10 # (if appati pble), MW 1 IL
STATE WELL PERM T e (it a piacratal )_ .
COUNTY WELL PERMIT V (it appaficalale) .
DING Or OTHER PERMIT # (if rapplacaUo)
WELL USE (Check afaplicabhi use),use)Fj Monitoring r Residential
arrrtclpa"Ptab is Ir®tdetstri,'altCorrarraerc i I n, Atfricultural
Reccrverlr 0 Injection Li Irrigation
Li Other (1sl ante)
MMMIMMM
a, Total Depth . 38 fT
Water Level (Bdea EleL4suhrr(I
Pkanl): � ,..._ it
fAQa','waar'9 {k0711 Ia....^..._ ...
.. Lt. ataove"`4atao Surface
As
t ongtft D arrxrte,r
NIA
..,._._._...Idle,
It. Casing Rtyrortve&
3otdr3 fl if)
DISINFECTION: N/A
(Arnt"Aint of 51*7 aka' jcarrhj tryprichiodle used)
SEALING MATERIAL:
Neaticalwat
C'erritlit rtl.
wpter.
Bron mile 1b,
Iyper: V Slurry `' peftept,
_-gal
Littler
s e Ttt
Ce not _ In,
1'Vpe, milirmai F't" RT ATE D BEN'TT KITE SLURRY
3, WELL LOCATION
#0rtttf$ataf 6255 GALLONS
d'OUN rY IRE.00_t.QUADRANGIE NAME
f lF 1CTII:: ti7 roism STATESVILLE
. EXPLAIN METHOD OF EMPLACIEMENT OF MAI-ERIAL,
TPT BELL TiiL2T1 ROAD 28626
.,_._. _..,,.� ..m.,.. _....___
IA LRU1LL CTE . LT(tMlir
1 _ .
. (;trraedIROad Name, Number, urnfmiluty, Subaivrasion UM No_ ParcRl, Zip t,odC)
.. .. J"""' ..`__ .-�°...�.;_ ._ _ mTM�-
fCaPrirTRAVI fl, I aANU SE T'dT Gi
a) Sf;a(aaY l.i iTafley VFl,,t ! i TTIrStlei:.J 0tttrr
(4 faed:k apTri'rprlalaselling)
ILL WELL DIAGRAM ' Drawn dfaortfro ketM of ll .Bs on Ill! ttac
g y v 1� A VV^^�� ,� ��yy
torn silo wng tnial depth, tdepth and diarrieter tat tj,,e (a8 star; icnsaiNaiifCq
_m CxTa
i CIN IT UD 80 � "''f T i90' I.t�'QS
ra tl rva ff Edra l interval„ inter¢ ais of Casing$eTkaratlt ss, and adepYhs and
T
OR
_ .._ _.. _.._. f l>
Gi aas of fill rn telial eaj
I_alitttoeipong fade stautce 4PS of opoUraphie rn aTs
(lrarzathm sat rtett most be sholftza rar) a USGS traps map affeeItec:iaert Ici
11. DATE WELL ARANLSC3PTEL5 10112112
this form it not uqklg GpSj�
4a. FACILITY -'The v arraP,'Of tin ttelskirass wherry tree well is located Corrtpxfete 4$a
Id,01fER'"ByCERTfr'YTHAT THIS Lr- WAS Alt,$aPt`ON 'rirk�a,,COR[,a rCE
f ', Tt T t � �af't 47i
rOy�v�iDE
,
(if caa r identi al well, skip 4a" Cra�FPole 4h, weil ari9 onr dn(I3"k3ts[,¢E ready.)
I R �n HAJF-EN To=LLh3E�
FAG IL1TY ID # (if appltr.afalr }yBWAME
OF FA liil t � TT# CPEFV tiuLM1tf
�iC tir S EL i
STRFF-I AI�tDRESSs 0.Af f.f_ !'#iISCVf R
C5 a"rE........
STATESVIP LE NC28625
fp5
_�.._......._
on St
,.._M
_ . aL
C�sNtTE WEL
T6LFCtygtT�A�rLi�T..E_iC_
tdo i e
"3
(The aaauarn well nWre' must be arredralWltsr*tatq)abandns
,-NsIber $esidentk if Weil
41a. CONTACT PERSON ELL OWNER:
NERr
In rcccurta c av Lr 9 ah'tJi ids 2C ; sa 13 i
NAME CITY OF ST"ATES"ViLLELITf CREEK tWT F
a�Afitf lf` SUMMERSLd,A
v_
EE0
6NA,-
t €R iEtA tI t7F F li tiN ABANDONING THE L i
STREET . DRESS 403 BELL FARM L' AD STATT SI,R f_E. F�SSd a6 i
Submit a GOPY to itle owner area the C.IrI 3It ( o- Division of Water Quality - Information Processing,
Form CAN 3p
1617 rlai) SOrvice Center, Raleigh, INCr SS -1617, Phorre : �919) 7-630
Evf.'.V. `�Lff

p "qp $ �" '(�� �p.� '$'] ��''y.'q �'}
XY:1TY"d.\.7.�a9'§Al,.+RP$.,[.f..
w!f y+i
onh Imam iar.t llrltatat4t ent ofl: n iratnmem and Natural Resources- Division €rt Water `{ unlit
2579
1, WELL CONTRACTORWELL DETAILS'.
lANNY SUMMERS s Total 1h 36.0 f#. CJiasY€ #t.r:,' 1 0 ill
R
D
LAD I# t rarttraci {Ind'sv tltral} tta as a Dater Level (Setr v frletvalring hoot): u at,
GEOLOGIC EXPLORATION, IN � MeasuOrig Point is ft above land Sufact.,
Weis C rintr§actor Coil slimy Name
176 COMMERCE BLV0 CASING: Lr€ratllh Diameter
A Address
STATESVILLE NC 28625 a Casing Deplh(it Srromt)
Cityor Tom __ t Casing Removed ILIA
,E°ta8rr Ts#? Ct�I� � �# I1. laa.
"T04 f .a72 686 _ _. �
Tarr a rT,—d t Phtaint illarriber 7. DISINFECTION: NIA
WELL ihtFti12A1ATl41N (Tatraarunt taf 6551,67 % mltturn hypochlotite )
SITE WELL ID # (if app icable).._._ VV'S m IL SEALING MATERIAL:
g
STATE, WELL 1wLR#T # (if rr(1#icats#q
Cement _ w u,- th Gerrtent If):
COUNTY WELL PERMIT # of applicaTbk)), trUater ,_.:,:. m,_._., rlaI; widerylt i.
[DWO or OTHER PERMIT #(if a ,#ic attlr �3s rsttattlta
WELL USE {t'.#tech; applic atDte rs caaMonitoring _; Residential tic nteartit th
Tye V Slurry I 1 Pellets
ursicipalllruuhlic a I Industrial/Commarabil Agricultural 1Aiatt s
r
l'.i Reria cry i1 Iej*ction E brig titaia
Other
R Olfaat (list umt€) n ... _ = tyT x rnaater€a# PORT LAND CENT NITS SLUR
1 WELL LOCATION Ara ril 6.CI GALLONS
S
COUNTY IRE DELL „ CTiwI,LI�ITAhJC;#[: �tAItTF:I
NF+S.I='ESI TtlWN, rATtm trlLLt 8. EXPLAIN E'tlw OD OF EMPLACEMENT OF MATERIAL:
49BELL. FARM ROAD BgTaaf11LrRy
fk?kCiE
(Stfe ,Vfload Name, Nuf nimar, Community, Subdtvi5km I'M No, P amet, Zip Gode)
't_>I'alC `=I2AF'I #E J L aLt,Ii t SF # f INC
(C tatac6 api t >t#atn Setting) 11h WELL DIAGRAM : Draw ,a detailed sk,-Idl Of #I ' *#I nn the back of Ibis
farm shovi4ip iota$ rclepttt, s9el tin arad €I#aarntjbcsr of srr n5 {¢t any) reraartirc ei�
LATITUDL T;r 4a lil4400 "#DN45 OR W # Dd':D in the av lS gravy I interval, intervals Of casia PO(fofa:time, amyl depths and
lmiiNGsIUD Fail Ir 51 '1t3I10" DIMS CC
_. ......� ,.. DD types of fist InatWfio�rd pro
L atitudellC,ttrlitrrcle scicrree.; ° PS L._lt`opo latatwtt" rr»ap
00catian Of well must be showktr earn a LISCS francs am all andaataaa-' ed to 11L DATE WELL ABANDONED °I`CDC't -Di
this form it not araaarrCr
100 HERFCDY ti:Ftl1 W Y° TlroT TMS LL Lrat ; AaLANDONED IN ACCORDANCE
4a, FACILITY, � 1 H ISA N AA: 2C;, E'?#€Lt C`Ot4ST R CTIO TANDARD ;, AND HAT A COPY OF I The nrxrntt Of Ittr� I�risrrwa%+�tfivam I11e well r. Irre al�tk Ctswi� lkxt€, 4r3 . Thl$� Plot) HAS L3EE � `w'tLt�t�'r�a "I"k ELLOWNER (Ft a rc i#entiat �w6t skim A4a, cx n giete 4ti well Owner inkirrmton oralp )
FACILITY IQ # (if apptsTalc) #ikfaATt#EF CERTIFIED WELL CON csL / tla"l
NAME OF FAC:hLlyr' 4TH C REUf WlAi1"t'
STREET ADDRESS SIC 3 BELL FARM ROAD
ST 4TE511ILI.F NI 28625 t ra T6 €� Vl XiE -WEE�.OiW4ER &Ei INU .. f WL,-LL _... C
Ity f r TitwYia ICrta i}a La1 t ft tote web owner must bean ier Nid sat ers;a bang r � t ufae€ rr L, xa # w ell
_.. m.
in
4Ir.CTC}AtTaLCTPE SCJ#f VELf i�fP3Eft:' ar orian with 1SAlolt°AC2C,011a.y
NAME CI iY CIF 8TATESL LLE14TH CREEK V`!WTF CDAhiPtY � tlh9tv&F'f�Ss
I.------ w _._ ..�... _ n .. : PRINTED NAME OF PEfT to R ABANDONING THEY E C L
STREET ADDRESS 493 SELL FARM ROAD S iAI ESVILLL, NC: 28625
Submit a COPY to the OWn r and the original to, Division f Water Quality- 1111INFtrlation Processing, Form C,;W-3T
1617 Mail Service Center, I p h, SIC 7699-1617„ Phone: 15 tt7-Suitt
F?nw. Vista

i
a t ;, "�:�pnh Carolina Depastcotr t ro-J` nvir,�rnoeo-rl land Natural Resources- Divi iota lrf Water' V ualiiy .
1. WELL CONTRACTORt 6. yELI. DETAILS:
DAtNNY Si1MME S T.Total Depth 390 ff. Diameter, 2,0 7.
Well C crnlraCttar (ieaitvi iur:l) Narlaa la. Water Level (Dalrrvv MeasudnrT Point): ft,
GEOLt GlG EXPLORATION, IN Measuring yacaa'iI Is ft. above landcarfaa^
w .. .. _ �.
VVeH C ontsasralcat C;raaaa iany t^t'ranie
176 COMMERCE t3l VD 6. CASING: Length t3ssTmeter
Slreet Address
STATE VILLE Nr 28625 a. Casing Def0 (If knovdn): NIA fl e;
_��,. . �..�..... _. — _
d:aha+easTtav4m �alaalr. radptRiatla t Ls. <.sirgT-Ieri'leWm NIA _....."..tt. in,
672-7686
7. DISINFECTION: NIA
Ateaa code Phorw nursattrar
WELL INFORMATION:fAa Tt}untl Of ta5" ?5% c�alr.ststn fotgv lea~iie lasecip
SITE WELL Ili # (if applicable)_ IL SEALING MATERIAL:
Pt t it ttltlt
STATE WELL PERMIT # (It �pplaeaRak)__.
Cement
l lbCement _ to.
OUNTR'WEl L PEgIorr ... Water—,_m . Jail. Water �a�8
DWQ or OTHER PERMIT # (if appal al)tc,).._ eetsaaTltay
I ntenile Ib.
WELL USE (GLie #c appIlcaNe use}y Monitonisa F) TleskleiWal
rule: V Slurry Pellets
Municipal/Public (J IndestridallC:aaaacraerclaal L" AAgr#easltur i later
Recovery F) Injection I-1 Irrigation Q#Ch
U t"Ither (fist eases) Type material P:"ORTLA,ND BENTONITE SLURRY
Y`
5 GALLONS
3,. aL L LexCAT#Tttu
COLINTT;, IE!.EDELIL .. _ OUAClRAN IE NAMF
NEARESTTOWCL S,TATESViLt E _.. t" EXPLAIN IIMET OO OF EM PLACEMENT OFMATERIAL-.
tES SELL I FARM RCTALf t"f#t? } A-UI -PIR
t.atreeilhaaaei N"tixaa:, P9rerlalaer, Conanunity, subdivision lot No, Paw", Zip Coiled ....,.�....�.�,_._...,_.�._._ .......�,...,�.�..........__...... T.......,._,�...�_..� N.. .......,..:� _
_ ..., _..
T'k.a#'O(:,lla'16'°l-If; ! LAND SETT INC,:
"Slope Iw_l Tilley '' I i:al ) RkkLeU Cato r
(Chprk aprapraata s ttirc#)TCt. WELL DIAGRAM ° Oraw a ctietailed skelrl'i of II —:I ore llte read of this
form shomAract total depth, depttl and efi amene of sefex".rls (if any) rt rrraaialfarf
Lr "fli aIC,L 35 l r ttt 4400 " %dt #" ORI)#t in It* well, gravel interval, intervals of Casing peLrfcaraallclras, and depths and
l i:iNRAI Tt1T)t: Tli .. t t E . tfaClt) ° ltf i`a OR l
l ac s at fall rarrslariais ;ed
Lalitudellailelihaete source WiPS restate
tvtraaatxrarl Of welt foust be shot-vo care ra I I SGS lrs Mtip acaaia"ttacheae`i Ic 11, RATE WELL ABANDONED I D/1 2112
this Ps'arrra i+`not aastrr SPSj
i K) HEiER) CCRTIFY TROT THUS WELL WAS t4DONED TN ACCORDANCE
lWs H 75A NCAC 2G, WELT. GON TI'dUCTIs� .�xTt'§ t3,ttiFirl . AtatT tHAI A COPY Of
rk. FACILITY = Thena nv rat rb e kaetty sc a}iree Ih roes8} #s 4r aced, fr Ts .ie 4 I'I #I?i ft *CSttla atAS SEC tilliEti TTT Tt 4N# t ti.4�a l 62
(If a rmidersiai wall Skip 4 s; C'Nup,"ete 4 b, weft awn n rE Mgov s tion any.)
FACIt_ITY ID # i4 appC .aLa#e) 1if r"if}f 1
T#-I CREEll W TE _
NAME {)I FAt;kL#TI _ aPd# fTEC IECtELLi C9tiTF7if4.. _. ___. CAA....._,_
STREE T C7DRFS,a 4 3 BELL FARM ROAE
STAiESVILLE ND 2862 �� ..,".
Catya tclvra Ste#a _ _._.. _ __
yija L to (Pie private well owner mist be sat, indfo ual ;I ?saxlltal ar dons Nalti t resa lent_M ann
4b. CONTACTPERS Ir ELL OWNER:
acxrrsarac�wthi Alv"�C �.tttra.)
DANNY SUMMERS
NAME CITY" OF S`I ATES'ttILLFJ4T REEK` TF .
PRINTER NAME OF PERSON ABArND014ING THE WE LL
STREET AT1CiRE5S 3 BELL FARM ROAD ST.ATESVIt LE, NC: 2E62I°
Submit a eopy to the yawner and the original to: Division of Water Duality « Inflar#ltation Processing,
1 1`T frail ServiceCenter, Raleigh, N7'Fa -1 17, Phone . (1) B07-6300 Ferree 4At43

GENERAL INFORMATION
BIOSOLIDS REPORT
FOURTH CREEK MO
PERMIT NO. WQ0001759
,.1
I-'AC'ILITY NAME: E: Fourth Creek WWTTP NPDES NCO03..M
LOCATION: 693 Bell Fann Read urv,
MAILING ADDRESS P.O.13o l l II �
St to ille, NC 28 i87-1111 �; s'
(7 4) 878-3 38
d°U U
RESPONSIBLE OFFICIAL- IF.E "Joe" Hudson Jr., Director
Water Resources
P.O, Box 1111
Statesville, SIC 8 a87-1111 .w
I704 878-3 38
I' C~ILI T Y OPERATOR: Andy Smith
Plant Supervisor
P.O, Bc)x III1
Statesville, NC 28 87-1:11 ].
(704) 878- 3 3
RESIDUALS CIRCA: Andy Smith
Residuals Supervisor
P.O. Box 1111-
Statesville, NC 8 87-111l
APPLICATION- Surface Disposal Unit
This tJnit Was Not Used For Disposal In 2007
Ir
1 9!j
$r
~ E
7
3

Management Practices Description
Fourth Creek WWTP Sludge Morrofill (Surface Disposal Unit)
NPDES No. NCOO' ) 1836
40 CFR 503,24
Non -Discharge Permit apt OOO 1759
THREATENED OR ENDANGERED SPECIES� No known threatened or endangered species
occupy or frequent the disposal site.
BASE FLOOD FLOW RESTRICTION: The site is located above the flood plan).
LOCATION OF GEOLOGICAL STABLE AREA.- Soil consists of tight red clay on high ground
and the site has had no history of movernent or shifting due tosaturation with rainwater or
seismic conditions. No known faults exist in the area,
WETLANDS LOCAJION: Not a wetland location,
RUNOFF COLLECTION -, Trenches are constructed as to prevent disposed material from exiting
as a part of any runoff. Berating and swales are constructed to contain erosion. Finished trenches
are domed with clean earth to all(-,)w shedding of water out and away from filled trenches. A
,,green belt" is maintained and encouraged to grow around the entire area.
LEACHATE COLLECTION.- As a liner is not used, leachate collection is not required,
METHANE GAS MEASUREMENTS: Periodic checks of air with electronic air monitors reveal
that methane is not escaping the surface dispoW area.
CROP PROHIBITION: Crops are nor grown on the site
GRAZING PROHIBITION: Grazing is not permitted on the site.
PUBLIC ACCESS RESTRICTED: Chain link fencing encloses the site property. NO
TRESPASSING signs are posted,
AQUIFER CONTAMINATION: Monitoring well samples for this calendar year show no danger
of aquifer contamination.
No disposal activities occurred in 2007.

ANNUAL RESIDUAL SAMPLING L.IN SUMMARY
Attach this form to the corresponding laboratory analysis.
Please note that your permit may contain additional parameters to be anatyzed than threw r qu�rad to be summarized on this form
P rmit N umb r W00001759 Laboratory
Facility array Fourth Creek Mon fii
NPDES # NCO031836 ff3)
or
WVVTP Name Fourth Crack f' on fiN
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I aura aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
DEM FORM S F (1 W)

FV
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
A
U.
Facility Name Fourth Creek VVWTP Moncifill Permit Number WQ0001769 W
to
WWTP Name Fourth Creek WWTP NPDES # NCO031836
Monitoring Period: From I 11 / 07 To 12131107 0
Class A — Alternative 1 Alternative 2 Alternative 3
Alternative Alternative 5 Alternative 6
Class B Alternative 1 Alternative 2 Alternative 3
If applicable to alternative performed (class B only) indicate "Process to Significantly Reduce Pathogens"
Aerobia. Digestion _ Air Drying _ Anaerobic Digestion — Composting — Lime Stabilization
if applicable to alternative performed (Class A or Class B) complete the following monitoring data-,
Aflowaide Level Pathogen Density
- Number of Frequency of sampte Analylicai
Parameter In Sludge Minimum F-Ge.Mean Maximum Units Exceedences Analysis Type
!F --- Terrinique
Fecal ah Crm 2,x 106 WIN
per gram of totaIi
sohris pr 2 x 106
CFU per gram
of totaIt salids
1000 MPN
Per gram of
total Solo!
(dry weight)
7;a-fmonella 3 MPN per 4
bacteria (in grams total
lieu of fecal scud (dry
Figure I
Vector Attraction Reduction (40 CFR 603.33) - Please indicate option performed
Option 1 Option 2 — Option 3 Option 4 Option 5
Option 6 Option 7 _ Option 8 Option 9 Option 10
No vector attraction reduction options were performed _
CERTIFICATION STATEMENT (please check the appropriate statement)
I'l certify, under penalty of law, that the pathogen requirements in 40 CFP 503,32 and the vector
attraction reduction requirement in 40 CFR 503,33 have been met."
1 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFI 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
ling fine and imptisonment."
2011111INSMA110HI!
Nte Signature of Land Applier (if applicable) Date E
DEM FORM RF (10194)

11 1 � 14 Via 1111 ;11
FACILITY NAME Fourth Creek Monofill Permit # WQ0001759 County Iredell
FACILITY TYPE (please check one)- [3Surface Disposal (complete Part A (Source(s) and "Residual IN" Volume only) and Part C) PHONE [phone]`i
C]Distribution and Marketing (complete Parts A, 8, and C)
WAS THE FACILITY IN OPERATION DURING THE PAST CALENDAR YEAR? _ YES _X_ NO. If NO, skip Parts A, 8, and C and certify form below.
Part A*
Sources(s) Volume (dry tons) Recipient Information
onth (indude PDES 4 applica1cfe) A nd
Name(s) Volume Intended use
sulkingAgent t/Ij Z�dualfN Product OUT dry tons
MNme
January
February
March
April
May
June
July
August
September
October
ovember
Decemb r
TotaW Annual (dry tons)
lAdmendment(s) used: Bulking Agent(s) used:
if more space is required than given, please use the comment space provided below or attach additional sheet(s), Check box if additional sheet(s) are attached.
Comments:
Part 0
Facility was compliant during calendar year 2007 with all conditions of the permit (including but not limited to items 1-3 below) issued by the
Division of Water Quality —YES — - . If NO, please provide a written description why the facility was not compliant.
1, All monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached.
Z All operations and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality,
3, No contravention of Ground Water Quality Standards occurred at a monitoring well,
"I CERTIFY, UNDER PENALTY OF LAW, THAT THE ABOVE INFORMATION IS, TO THE BEST OF MY NOWLEDGE AND BELIEF, TRUE, ACCURATE AND COMPLETE, I AM AWARE Tj
THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING TH 0 IBILITY 00 FIN AND IMPRISONMENT FOR KNOWING VIOLATIONS."
SIGNAidgE OF PERMITTEE DATE SIGNAT RE OF PREPARER* DATE
(if diffe nt from Permittee) "Preparer is defined in 40 CFR Part 503,!

FV
GENERAL INFORMATION
I S LI S REPORT
CALENDER YEAR 2006
PERMIT NO. WQ0001759
FACILITY YNAME:
Fourth Creep WWrP NPDES NCO031836
LOCATION.-
693 Bell Farm Road
MAILING ADDRESS;
P.O. Box 1111
Statesville, NC 2 7-111
(704878-3438
RESPONSIBLEOFFICIAL:
L.F. "Joe" Hudson Jr., Director
Water Resources
P.O. Box 1111
Statesville, NC 2 r 7-1111
[phone]
FACILITY OPERATOR O
Andy Smith
Plant Supervisor
P.O. Box 1111
Statesville, NC 28 7-1111
(7 0 4) 7 - 4 5
RESIDUAL RC:
Andy Smith,
Residuals Supervisor
P.O. Box 1111
Statesville, NC 2 6 7-1111
APPLICATION:
Surface Disposal Unit
This Unit Was Not Used For Disposal In 2006

Management Practices Description
Fourth Creek WWTP Sludge Monofill `ace Disposal f `t
PDES No. NCO031836
40 CFR 503.24
Non-Dischar o Pen -nit WQOOO 17
THREATENED OR ENDANGERED SPECIES: No known threatened or endangered species
occupy or frequent the disposal site.
BASE itl.,OOD FLOW RESTRICTION: The site is located above the flood plain.
LOCATION OF GEOLOGICAL STABLE AREA: Soil consists of tight red clay on high ground
and the site has had no history of movement or shifting due to saturation with rainwater or
seismic conditions. No known faults exist in the area.
WETLANDS LOCATION: ATION: Not a wetland location,.
RUNOFF COLLECTION: Trenches are constructed as to prevent disposed material from exiting
as a part of any rruno f, Berming and swales are constructed to contain erosion. Finished trenches
are domed with clean earth to allow shedding ofwater out and away from filled trenches. A
"green belt" is maintained and encouraged to grow around the entire area,
LEACHATE COLLECTION. TION. As a Hirer is not used, leachaate collection is not required
METHANE GAS MEASUREMENTS: TS: Periodic checks of air with electronic air monitors; reveal
that methane is not escaping the surface disposal area.:
CROP PROHIBITION: Crops are of grown on the site,
GRAZING PROHIBITION: Grazing is not permitted can the site;
PUBLIC ACCESS RESTRICTED: C'TED: Chain link fencing encloses the site property, .
TRESPASSING signs are posted.
AQUIFER CONTAMINATION, ]Monitoring well samples for this calendar year show no danger
of aquifer contamination,
No disposal activities occurred in 2006.

E 11
0
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form,
Permit Number WQ0001759 Laboratory
Facility Name Fourth Creek Monofil L)
NPDES# NCO031836 3)
orWQ#
WVVTP Name Fourth Creek Monofil
IGNATU
SI

R ii� All 1 111
Facility Name Fourth Creek WWTP Monofill Permit Number W00001769
WVVTP Name Fourth Creek WWTP NPDES # NC00311836
Monitoring Period: From 111 106 To 12131106
Pathogen Reduction (40 CFR 603.32) - Please indicate level achieved and alternative performed
Class A Alternative I Alternative 2 Alternative 3
Alternative Alternative 5 Alternative 6
Class B Alternative I Alternative 2 Alternative 3
If applicable to alternative performed (class B only) indicate "Process, to Significantly Reduce Pathogens":
Aerobic Digestion __Air Drying _ Anaerobic Digestion — Composting — Lime Stabilization
if applicable to alternative performed (Class A or Class B) complete the following monitoring data'.
FAllowable Level Pathogen Density Number of Frequency of Sample Analytical Paranneter in Sludge Mimmum Geo. Mean Maximum Units Exceectences Analysis Type Tech"
FecM Coliforn) 2 x 106 MPN
per gram of tool
solids gL 2 x 106
CFU per gram
1000 MPN
per gram of
total solid
(dry vanght)
Salmonella 3 MPN per 4
bacteria (In grams total
lieu of fecal solid (dry
L coliform)
Figure I
Vector Attraction Reduction (40 CFR 603.33) - Please indicate option performed
Option 1 Option 2 — Option 3 Option 4 Option 5
Option 6 Option 7 Option 8 Option 9 Option 10
No vector attraction reduction options were performed _
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503,32 and the vector
attraction reduction requirement in 40 CFR 503,33 have not been met." (Ptease not if you check
this statement attach an explanation why you have not met one or both of the requiremen ts.r
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel property gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met, I am aware that there are
si ifl ant nalt- S f�alno�rtification including fine and imprisonment," fall
Ck
re re Name and Title (type or print)Land Applier Name and This (if applicable)(type or print)
Signature of eparer Date Signature of Land Applier (if applicable) Date
OEM FORM RF (10194)

FACILITY NAME Fourth Creek Monofill Permit # WQ0001759 County Iredell "
r-111
FACILITY TYPE (please check one): El Surface Disposal (complete Part A (Source(s) and "Residual IN" Volume only) and Part C) PHONEAY- 8/6.3Y-213
7 Distribution and Marketing (complete Parts A, B, and C)
WAS THE FACILITY IN OPERATION DURING THE PAST CALENDAR YEAR? _ YES NO. If NO, skip Parts A, B, and C and certify form below;
N
Recipient Information
tiIII Volume (dry tons oIIIIIIIIIII� 4
Intended usetsj
See Attached Tables I and 2
y.
i $eptMber
Bulkin�t(s)_Used:
ii�gp 1111 11 � glill
Comments:
Part C
Facility was compliant during calendar year 200_ with all conditions of the permit (including but not limited to Items 1-3 below) issued by the
Division of Water Quality - YES NO. If NO, please provide a written description why the facility was not compliant.
1. All monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached.
2. All operations and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water' Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I CERTIFY, UNDER PENALTY OF LAW, THAT THE ABOVE INFORMATION IS, TO THE BEST OF MY K I W1,EDGE AND BELIEF, TRUE, ACCURATE AND COMPLETE. I AM AWARE THAT
THERE AR SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING THE P St 0Ty OE�FMES ANC IMM PR ONENT FO KNOWING VIOLATIOlI
"0
UROF PERMITTEE SIGNA 'R F PREPARER' ATE
G TE
(if differen from Permittee) *Preparer is defined in 40 CFR Part 503.9(r)

GENERAL INFORMATION
BIOSOLIDS REPORT
FOURTH CREEK MONOFIL
PERMIT NO. WQ0001759
FACILITY 4 Fourth Creek WWTP NPDES NCO031836
LOCATION: 3 Bell Farm Road
P.O.MAILING ADDRE SS: 1111
Statesville, NC 28687-1111
Q -3 3
RESPONSIBLE OFFICIAL: L.F. "Joe" Hudson Jr., Director
Water Resources
P.O. Box, 1111
Statesville, NC 28687-1111
-3 3 '
FACILITY TIke Evans
Plant Supervisor
P.O. Box 1111
Statesville, NC 28687-1111
4 -33
RESIDUALS ORC: Andy Smith
Residuals Supervisor
P.O.1111
Statesville, a -1111
APPLICATION: Surface Disposal Unit
This Unit Was Not UsedFor Disposal In

Management Practices Description
FourthCreek P Sludge Monotill ace Disposal Unit)
PIES No. NCO031836
0 CFR 503.24
Non -Discharge Permit WQ0001759
T14REATENED OR ENDANGERED SPECIES: No known threatened or endangered species
occupy or t"re cent the disposal site,
BASE FLOOD FLOW RESTRICTION: The site is located above the flood plain.
LOCATION OF GEOLOGICAL STABLE L . Soil consists oftight red clay on high ground
and the site has had no history of movement or shifting due to saturation with rainwater or
seismic conditions. No known faults exist in the area.
WETLANDS LOCATION: Not a wetland location.
RUNOFF COLLECTION: Trenches are constructed as to prevent disposed material from exiting
as a part of any runoff. Be ink and swwral s are constructed to contain erosion. Finished trenches
are domed with clean earth to allow shedding of water out and away from filled trenches.
"green belt" is maintained and encouraged to grow around the entire area.
LEACHATE COLLECTION: As a liner is not used, leachate collection is not required.
METHANE GAS ME SU AR TS: periodic cheeps of air with electronic air monitors reveal
that methane is not escaping the surface disposal area.
CROP PROHIBITION: Crops .are riot grown can the site.
GRAZING PROHIBITION: Grazing is not pernfitted on the site:
PUBLIC ACCESS REST ,rED Chain link fencing encloses the site property. 14+
TRESPASSING signs are posted.
AQUIFER CONTAMINATION: Monitoring well samples for this calendar show no danger
ofaquifer contamination.
No disposal activities occur in 2002.

RESIDUALANNUAL
Attach this form to the corresponding tab•
Please note that your dt _ additional Parameters
P ..I.unte
"I certify, under penalty of law, that this drw urraerat was prepared under tray direction or supervison In accordance with a system
designed to assure that qualified Personnel properly gathered andevaluated the Information sUtatraltted. I arts a , re that there are
significant penalties for submitting false Information, including the possibility of fines and Imprisonment for knovving vlolati ns."

FaI Name Fourth Creek WWTO Mondfili Permit Number WQOM169
WWTP Name NPDES#
Monitoring Period: From I I I / 01 To 12131102
Patho n 96&IIIm':
Class A Altennative I —
Alternative 2
Alternative 3
Alternative 4
- Alternative 5 -
Alternative 6
Class B Alternative 1 —
Alternative 2 -
Alternative 3
if applicable to afternative performed (class B onlY) i"cate "ProciaSs to Significantly RedUde Pathogens
.AercibicDigestion —AirDryinq _AnaerdbicOlgestion Composting _LimeStabilization I
Option 1 Option 2 Option 3 Option 4 Option 5 _
Option 6 Option 7 Option 8 Option 9 Option 10
No vector attraction reduction options were performed
"I certify, under penalty of law, that the pathogI requirorrients in 40 GFR 50332 And the wctor
altraction reduction reouirothent in 40 CFR 503.33 have been met."

ANNUAL DISTRIBUTION AND M A R K FTING/SUR FACE DISPOSAL CERTIFICATION AND SUMMARY FORM
FACILITY NAME Iourth Creek WwTI,
FACILITY TYPE (Pleas t check o"tt:
WAS THE FACILITY IN OPFRATION DURING 1-1
PART A*
2233MEMEB=
Admi5ndment(s) used, -
I f more space is required
Comments
PERMIT#_WQ0001759COUNTY— Iredell —
Sorlice Disposal (cotholete Part Orrd, 11pp? eirl"0k
Distribution and Marketing (complete Parts A, R. and C)
-Bulking Agebt(s) used,
M1
zzaal=
Em
ElCheck box if additional sheet ) are attaclied,
Port C
FlIcility was compliant during calendar year j with all conditions of the permit (including but not limited to items 1-3 below) issued by the
Division of Water Quality X YES NO. If NO, please provide a written description why the facility was not compliant.
L All monitoring was per Forrnd_in accWr_1i_ncc with the pertnit and reported during the year as required and three (3) copies of certified laboralory results are ittiched,
2All operations and maintenance reqUiretirents were con iplied with or, in the case of a deviation, prior authorization was received from the Division cif "water (�uality.
1 No contravention of GrOUnd Water Quality Standards occurred at is monitoring well,
I CERTIFY, UNDER PENALTY OF LAW, TITAT TTIE ABOVE INFORMATION IS, TO TJIV REST OF MY KNOWLEDGE AND BELIEF, TRUE, ACCI IRATF, AND
COMPLETE I AM AWARE TliAT TIIERF ARE SIGNIFICANT PENALTIFS FOR Stin ITTING' FALSE INFORMATION, INCLUDING TI I E POSSI III LITY OF FIN ES
A,ND IMPRISONMENT FOR KNOWING VIOLATIONS.- R
4 61 C
P
'OF PRE
/4:11G��NTUR`EF I,' Mifi:FF, DATE SIG NATtJ E PAPER* DATF
(Irdifrerent from hermit ce) *Prepater is defined in 40 (TR Pnd 501 9(r)

-........ .
At
GENERAL INFORMATION
SLUDGE REPORT
CALENDAR YEAR 1996
i
1997
i
FACILITY N
kvl
Fourth Creek WWTP-NPDES NCO031836
LOCATION,
93 Bell Farm Pad
MAILING ADDRESS:
P. 0, Box 1111
Statesville, NC 28687-1111
7 4- 78-3435
RESPONSIBLE OFFICIAL:
L. F. "Joe" Hudson, Jr., Director
Water/Wastewater Treatment
P. 0. Bic 1111
Statesville, NC 28687-11.11
74-878-343
FACILITY OPERATOR,
Harold Anderson
Plant Manage
P. 0. Box 1111
Statesville, NC 28687-1111
74-57-343 S
PLI ATION:
Surface Disposal Unit
����� ., ��ti
t

ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FOR
FACILITYNAMEcr I � r �.t k 11�� I
b w� p , a
PERMIT iI COUNTY FACILITY TYPE please hen one): surface �
ue Disposal (complete part A_(Srsurce(s) and "Residual IN" Volume only) and fart C
Ej Distribution and Marketing (Complete farts Ar B, and C
WAS THE FACILITY IN OPERATION DURING THE PAST CALENDAR YEAR
_ ,..m.r.— YES. �..� NO. If NO, ship Marta A, 8, and C and certify frarrrw below,
Fart A*
s
Sources art
� .� Volume dry trans
13*
Recipient InforrationM nth tindvde NPOES td r arkicobf } ndme�r
Name(s) Vrsiunae
Jarmary dry town
February
March s ,
_M. tado r"ij,I
April�
May
June pa
a
rt rrac,rr SPaCe is required Irian given, please, LISP the crair ment space Provided blowy or attrarla additional sla t(s)' Check box If additional ssr ewl(;s) are allached,
d,
Comments:
Part C
Facility was Compliant during calendar year 199E with all conditions of the permit (including but not limited to items 1-3 below) issued by the
Division of Environmental Management _______,_YES, _. . If NO, please provide a written desription why the facility was not corraptiani
I All monitoring was performed in accordance with the permit and reported during the year as regUired and three (3) nri( ies of certified laboratory
2. All operations and rnaintera�ance requirements were c raapiled witty or, lie the case of a deviation, prior authoti a i an asio results are ent,l1 M
3 No Contravention of round Water Quality landard ,occurred at a monitr ung well, t ran was recialwett Irrarta 9lae fJiviisirarr ral I nwirraiarr7erat it Management,
`I CERTIFY, UNDER PENALTY OF LAW, THAT THE A13OVE INFORMATION IS, TO THE BEST OF MY KNOWLEDGE AND BELIEF, TRUE, ACCURATE AND COMPLETE. I AM AWARE THAT
THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING THE POSSIBILITY OF FINES AND IMPRISONMENT FOR KNOWING VIOLATIONS."
�7 1
SIC`sN+'4t.IRE OF PERMIT TEE
SIGNATURE OF PnEPAREff* DATE
(if different from PerrnRtee) `Preparer is defined in 40 CFR Part 503, t(r)

February 26, 1997
Rex Gleason, P.E.
Water Quality Supervisor
Mooresville Regional Office
919 North Main St.
Mooresville, NC 28115
e: Notice of Violation Response 2/ 1 g197
Fourth Creek ionoll
Permit No. WQOOO 1759
Iredell County
Dear 'fir, Gleason:
We are in receipt of the referenced Notice of Violation for the subject facility, After
careful review of the self monitoring data, we offer the following explanation:
Sludge from the "water Treatment Plant and the Third Creek'WWTP which contained
chromium in concentrations greater than the permit limit of 260 mglkg was disposed of in the
subject monofill during 1996, Since we had had no prior problems meeting the pollutant
concentrations contained is the permit, the long-standing practice had. been 1,hat self -monitoring
samples were taken quarterly as a mixture of all permitted sludges. However, during 1996, our
residuals program changed such that Fourth Creek WWTP sludge was not disposed of in the
monofill and the disposal of Water Plant and Third Creek sludge was not done on a regular basis,
Therefore, individual self -monitoring sludge samples were taken at the timc ofdisposal.
In addition, we have found that the employee who was responsible for all residuals
monitoring did not complete the monitoring activities as is required by the permit. This person is
no longer employed by the City.
Further, T I P analyses for both Third Creek and Water Plant sludges were completed
during the same months as the samples which were non -compliant, August 5, 1996 and July 30,
1996 respectively: Leachable chromium for both sludges was reported as less than the detectable
limit: Please refer to the attached TLP analyses.

k
Since the discovery of the non -compliant results on February 18, 1996, we have changed
our sampling practices, We will sample sludges to be disposed of in the rr. nofill prior to
disposal. Ifthe results are not within the permit limits, the sludge will not be disposed of the
rnonofill.
Thus far, we are compliant, for 1997 and plan to pursue closure rc of the mo o ll during
1997, Should you require any additional information, please contact me at 878-3438.
Sincerely,
� C9 tus em
ReneeParkman, Asst Director
Water/Wastewater Treatment
attachment
cc. W, Jesse Wells, Hazardous Waste Section, MRO

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding laboratory analysis.
Please mite that ycrur permit may contain additional parameters to be analyzed than those required to be surnmarized on this form..
Permit Number� 2
Laboratory
Facility Name f � � „. � ..
NPD5S# 2} r
or WO tt faastdusar only fildllttesj � �
iiVWTP Name
-------------
IEI NATt. RE OF PAE'ARE ij DATE
"°t certify, under penalty of lase, that this documant was prepared sander my direction or supervision In accordance wine e system
designed to assure trial qualified personnel property gathered and evaluated the information submitted, t am aware trial there are
_ srtgnfticant penalties for submitting Parse Information, including the possibility or Rises and Imprisonment for knowing violations.-
DEM Fortm SSF (1019 )

ANNUAL PATHOGENAND VECTOR ATTRACTION I Ti
ON FORM
Facility Name
WWTP Name
Monitoring Period: From Tot l /
Permit Number
Pathogen Reduction 0 CFR 503-32)- Please indicate level achieved and alternative performed
Class A
Alternative 1 Alternative 2 Alternative
,Alternative 4 alternative 5 Altermative
Clasp
Alternative 1 altermative 2 alternative
If applicable to altemative performed (Class l3 only) indicate "Process to Significantly Reduce Pathogens":
-,Aerobic Digestion Air Drying Anaerobic Digestion Composting , Lime Stabilization
If applicable to alternative performed (Class A or Class ) complete the following monitoring data:
Alowaole Level a Oerwyf tas rsf Frequency f l
Parameter in minimum is .'� M frnum Units `" vs r Analytical
w niqu
Fecal li#orrrt 2x 100 MPfvl �
FU pergrant
of total solkis 5-9 Cr
1000 MP
totalper gram of
(dry weight)
Salmonella 3 MPN m
w
_ # R - "` _ � _ .. '* • • � ,• .. � .,. _ rya � ,i# _ ,.... �.....
_
r�" y
Prepar r Name and Ttle (type or print)
. .,
Signature of Prepares Date
Land .Applier Marna and Ttl (if applicable) (type or print)

DATA REPORT
City of Statesville
Fourth Creek WWTP
Post Office Box 1.11 I
Statesville, North Carolina 28687
Received 3-28-96
Reported 4-15-96
Work Order # 05-03-18
S,-'%i\,I,PLE ID: Third Creek SlUdge Cake
SANIPLE 4 PARAMETER
AS RECEIVED
DRY WF-IGHT
05-0328-1 Fecal Coliform
39X0 CFU/g
I ,l 61,826 CFU/g
% Solids
') 4, 1 %
05-0328-2 Fecal Coliforrn
200,000 CFU,/g
775,194 CTU/c
05-0328-2 % Solids
25,8%
05-0328-3 Fecal CoUbrm
90,000 CFU/g
376,569 CFU/�g
05-0328-3 % Solids
23,9 %
05-0328-4 Fecal Coliform
65X0 CFU/g
474,S36 CFtJ/g
05-0328-4 % Solids
13.7%
05-0328-5 Fecal Crah form
210,000 CFU/g
1.468,531 CFU/g
05-0328-5 % Solids
14, `3 % -
05-0328-6 Fecal Colifibrin
190,000 CFU/g
1,366,906 NFU/g
05-0328-6 % Solids
13.9 , %
05-0328-7 Fecal Coliform
230,000 CFU/g
I, 3, 3 CFU/g
05-0328-7 % Solids
18,5%
Geometric Mean
665,054 ,FUG'g
Respectfully Submitted,
011f
Dena Myers
NC Cert. 4 440
P.O. Box 228 - Statesville, North Carolina 28687 7041872/4697

Client:
Address:
J i
Contact Person.-
Phono #
PO # Requisitioned by.
Customer
Ramnla in If Lab ID Preservative
FAX #
('rme D;
Par —am eter—sr—eque—s—tedfor a—na—lys—is'
- r5l z"
M
9MCOU, EANAMICAL
IIZ2Couttstfrd - R413oxMX
StRiesville, NC186V
") 8,72-4697
ClIviln of
CuStody Record
EmaryalLye
12.
920&s.
Relinquished by:
— ----------
---------
Sampled
1
HNO3
HCI
Received by.,
'rime/Date
Transported via;
I
NaOH
--LI
4.
H 2SO4
Relinquished by
Holding times met:,
5,
6,
Other chemical
Chemicals in containers, lab,
Received in lab:
L 3
IVY--
Compliance work:
7.
Chemicals in containers, client
8.
Chemicals added upon receipt
Non-compliance work:
9. Received chilled
'M Samples delivered as soon as pulled
I I . . Samples chilled upon receipt
'12. Other

DATA REPORT
City of Statesville
fourth .'reek WWTP
Post Office Box 1 I 1 1
Statesville. North Carolina 28687
Received 5- 3,l - 6
Reported -1 - t
Work Order # 02-053 1
SAMPLE , Monofil 4th Creek
SAMPLE PARAIMFTER
AS RECEIVED
DRY'�MGHT
02- 531-1 Fecal Coliform
26 CFLT/gm
71 U/gm
-05")1- % Solids
3 .5 %
- 5 l-2 Fecal Coliform
21 CFUIgm
` U/gam
- 5')1-3 Fecal Coliform
29 CFULgm
67 CFULqm
-0531-) ',10 Solids
3.3 %
02-05311-4 Fecal Chl a
5 Fla. /gm
93 'Fly/ tit
- 5314 % Solids
2
2-53) 1-5 Fecal Coliform
'18CF /gig
.
54 CFU/gni
02-0531-5 % Salida
3 A %
2-0531-6 Fecal Coliform
24 CFU/gm
101 CFULgm,
- 531 _ % Salts
,, '
2- 0 5 1-7 Fecal Colifortri
28 CFU/gni
1 I S t FULgm,
02-05 31- % Solids
3, °r
02- 5 -3 1- I ChrortiJium
15 5 �
49.7 mg/Kg Kg
0- 5 3 l k l Nickel
11. 0 nig/
)2 1
3.97 mg/Kg
R speed ally° Submitted,
A
SA.x
Dena Myers
NC C rt, 9 440
F. t Box 228 * Statesville; I"3Farth Carolina 28687 104`, 4697,

Client:
Address:
J\J C Z4 4
7-
Contact Person:
Z
Phone #
FAX #
PO #
Customer
Requisitioned by:
Ime
Sam e ID
Lab ID
Sam led preservative
Time Date
1� matrix
0
Param,eters
requested for analysis
M-0 3
'0 -31
'> 'i #') A - r
9MIESVILLE XNAIYP!CXL
122CourtSuttt 4 pO,Bbx228
Statcs*dlc�NCMV
(704) VZ460
Chain of
Custody Record
Arrival
Relinquished by:
E)/Date
Sampled b
1.
HNO 3
2.
HCJ
Received by,
Transported via: i e'n +
3
NaOH
4,
H2SO` 4
Relinquished by:
Date
Holding times met:
5.
Other chemical
Received in
6.
Chemicals in containers, lab,
lab:
Time/ a
QaL t) -9 t'p
Compliance work-
7.
Chemicals in containers, client
&
Chemicals added upon receipt
Non-compliance work:
9.
Received chilled
Lab Comments:
II.
. Samples delivered as soon as pulled
Samples chilled upon receipt
-Other

AWE ID,
4th Mon fil Sludge
SAMPLE
PAR-AMETER
AS RECEIVED
RESULTS
03 - 619-1 B
pH
1
03-0619-113
03-06l9�-1 l
Fecal Clifo rm
%
.1
f 1 1
1 CFU/
03-0619-2B
Solids
Fecal Coliforn,
.
30 FU/
03-0619.2
% Solids
16.7
1911 FUG
03-0619-313
3-0619-313
Fecal Coliforrn
�
400 C$FU/
1146 CFUf
3-fi619-4
% Salads
Fecal C" l form
34.9 r`�
2500 CFU/g
7418
03-06194B
% Solids
33.7 "
CU/
133-0619-513
3 ® 619- 3
Fecal Coliform
% Solids
1000 CFU/g
2994 /
03-0619-613
3- 619-6B
Fecal Coliform
33 A
1000 CF'U/
2933 C� f T/
93a�i6I 9-7
% Solids
Fecal C` lifo�
4.1 .�
400 FU/
92
03.0619-
% Solids
43.1 e
Ll
3-0619-2
03-0619-2
Arsenic
Chromium
4.96mg/Kg
�i3�Ct619;�2
Nickel
17,4
4C�.4 rug/Kg
10.
23.2
R spcct%illy Submitted,
'e-
Dena Myers'
ETC" C"rt:`# 441

Client:
Address:
contact Person:
PO
Lab iD
EM22E .. radry a;
I. HNO3
2, HCI
3, NaOH
4. H 2SO4
5. Other chemical
6Chemicals in containers, lab,
7Chemicals in containers, client
& Chemicals added upon receipt
9. Received chilled
101 Samples delivered as soon as pulled
11. sample t upo receipt
12�7 Other`
FAX #
by. (Time D
�tnx Parameters requested for WWWY—si�
--, - T—'; 'e
Relinquished byawe le
-
Received by:
Relinquished by- Time/Date
Received in lab: Tme/Date
$�WV�VHIIKANAINWAI.
P01"228
stwtviot, Nit 1mv
(704) 8724W
Chttirt of
Custody Wcord
Data
Sampled
Transported via:
Holding times met:
ri
Compliance work:
Non-compliance work-,

Page 1 of 7
DATA REPORT
ORT
City Of Statesville
Fourth Creek ` INITP
Post Office Box 1 j 1 1
States-•ille, NC 28687
ATTN- - Carpal Rogers
Received 7/ II 6
Reported 8/26/96
Work Order 04-0731
SAMPLE : Water Plant Sludgy
SAMPLE
PARAMETER
SULTS
04-0731-1
Aluminum
822,180
04-0731.1
Calcium,
7218 ,
04-0731-1
Magnesium
30,687 mg/Kg,
04-0731-1
Nitrate
< 1,.0 mg/Kg
04-0731-1
Nitrite
<I.0 mg/Kg
04-0731-1
pH
6.00
04-07 1-1
T.Phosphorus
3 5 71
04-0731-1
Potassium
6, 48
O4-0731-1;
Sodium
7971 m
04-07 31-1
T. field hl Nitrogen
40,916 mg/Kg
04-O731-1
% Solids
51.7%
04-0731-1
N 3-1 I
324 mg/Kg
4-0731-1
Arsenic eni
8.4 mg/Kg
04-0731-1
Chromium
425 mg/Kg
0-0731-1
Cadmium
0,212 mg/Kg
04-07 31-1
Cropper
1750 m °I
04-0731-1
Lead
27.8 mg/Kg
04-073 l -1
Mercury
0;1 mg/Kg
0 -0731' -1
Molybdenum
< 1, 0 mg/Kg
P,Oi, Box
Statesville, North Carolina 28687 70ej/87214697

Fags 2 of
04- 7 1- I
Nickel
27.4 mg/Kg
04-07 1-I
Selenium
< I mg/Kg
04-07 1- I
Zinc
479 mg/Kg
4- 7 1- l
Reactive tive Cyanide
<7 m gXg
04-0731-1
Reactive Sulfide
2,0 mg/Kg
4-07 I-1
Corr sivity
Not Corrosive
4-0731- I
Ignitability
Not Ignitable up t
4-07 I - I
PAN
243lbs. /dry ton
Respectfully Submitted,
�4
Dena Myers
C Crt. # 44

Client, r -.F A, i
# I Lab ID #
1. HNO3
2HCI
1 NaOH
4. H 2SO4
5Other chemical
6, Chemicals in containers, tab.
7Chemicals In containers, client
& Chemicals added upon receipt
9- Received chilled
Wamples delivered as soon as pulled
I il. Samples chilled upon receipt
12.- Other
FAX #
(T�IMOR
Parameters requested for analysis
M
Relinquished by:
MUSVILUANAt"CAL
12!60�insmua * POB<*228
Suut�'NC28W
(704) MAW
Chaitt of
Custody Record
Received by:
T ate
Transpoilod via:
Relinquished by: 3irrreJDate
Holding times met: 1'n I
n
Received in lab: Time/Date 01-
Compliance work:
4-ap
Non-compliance work-
FLab mments-

PF IA l IZETl ASSAYS, INC.
2960 Foster Creighton Dr:
NashviHe., IN 37204,-i' 566
a
STATESVILLE ANALYTICAL 6445
TT : DENA MYERS
122 COURT STREET Lab 1 um 1- a 6-AO4 '9
Samole ID: ()4-0731-1 Date Collected:
Project: Time Collected.
Pi-ojLect Name: Date Received: / /
mpl rm HARRY MYERS Time Received: ; 0
State Certification: 367 mple Typeg Soil
Site »%.
Report Ruan Nil
Analyte Result knits Lust' Limit factor pate iise' Analyst Method Rats=h
Aluminum 48600 eg/kg 49.3 1.0 5 81 6/96 7s86 R.Street 6010A 6866
Arsenic 5.1 op/kg 110 1.8 t 81 6/96 706' R.Street 6418A 6866
Calcium 374{ mg/kg 1.8 1.0 1 81 619 7:06 R.Street 6 18A 6966
Magnesium 15" a f g 9.8 1.8 1 8/ 6/96 7s86 R.Street 6810A 6866
Mercury ND eg,/kg 0.1 0.1 1 8/ 5/ 6 18s56 B.Haoilton 7471 7888
Molybdenum R8 mg/kg 1.8 1.0 1 81 6/96 7:06 R.Street 6810A 6866
Potassium 360 A/kg 9.8 1.0 1 81 6/46' 706' R.Street 6010A 6866
Selenium N8' a/kg 0.98 1.8 1 8/ 6/96 7.86 R.Street 6010A 6666
Sodium 413.. solkg 9.8 1.0 1 81 6/96 7:06 R.Street 6810A 6866
Reactive Cyanide NO mg/kg 2.0 8.8 1 8/ 6/96' 17i833 B. Hoover S-84 7346
Reactive Sulfide N3 to/kg 8.8 8.8 1 81 6196 17s83 B. Hoover SN-846 7346
Corrosivity NOT CORROSIVE 81 3196 18.89' B. Hoover 1110 696
Ignitptility Not ignitable up to ROO F 8118/96 9$45; M.Dunn IDIOM 8598
Nitri e-N N8 a/kg; 1.8 8.1 1 8/ 6196 111.39 B.Buey 9056 7498'
Nitrate-R' NB /k' 1.8 0.1 1 81 6/96 11s37 B.Bucy 9856 748
Rleldahl Nitrogen 2120 ag1kg 1.0 1.00 1 8/ 9196 16.45 B.By 351.4 8556
NB z Not detected at the report limit.,
Report Approveda"X_t��rt Date: /1 /9
Theodore J. hu llo, Ph.D.
Michael H. Dunn, M.S.
_Danny B. Hale,, M.S.
COPS"

,
DATA REPORT
i, WM�N4 uMM11W U1
Page I of
City of Statesville
Furth Creek WWIT
,
Post Office Box I I I
I
Statesville, NC 28687
'Received 8/9/9
Reported /9/9
'Fork Order # t - 809
SAMPLE ID.- Third Creek: Monralill Sludge
SAMPLESAMPLE#
PARAIMETER
DRY WEIGHT
03 -08 I9- I A
Fecal Coliform
8 , 1 `F /
03-08 9-I
% Solids
.'
03-0809-IB
Fecal Coliform
l 11,1 I I /
9-0899-1 E
% Salads
l 8. 0 �
- 819-1 C
Fecal Coliform
I98,89 FI ,/
- 809-I
% Salads
18A
03-0809-ID
Final Coliform
68,702 'CF /
0 -08 9- I
° Solids
262 %
- 8 9-IE
Fecal Coliform
93,923 CFU/S
03-08 8-IE
% Salads
18.1
9 µ 8 9-1 F
Feat Coliform
1 I,86FU/
- 809- I F
% Salads
18.
3-0809- I G
Feral Coliform
1667667 F1...`/
-0809- I i
% Solids
18 q,10
03-08 9- I
Geometric Mean
114,438 `FUT/
03-0809-1
relce I
�,�`
19 2 m03
} I
Chromium 7tI133i
� ? m
03-0809-I
Arsenic
<1 0 mg/Kg
03-08 9-1
III
684
0. Box 228 0 Statesville, North Carolina 28687 8; '4897

Page 2of
S. i LE IFourth
Creek Monofill Sludge
SAMPLE 4
PARAMETER
ESULTS
03-0809-2A
Fecal Coliform
72,797 CFU/
3-0809-
'N
� Solids
26A %
03-0809-2B
Fecal Coliform
27,223 C 'C/
3- 809- <
% Solids
55A %
03- 809- C
Fecal Coliform
64,706 CFTC/
03-08 9,_ C
% Solids
3
14 0°
03-0809-2113
Fecal Coliform
67,251 C'FU/
03- 8 9_ 1
% Solids
3 a °
03-0809-2E
Fecal Coliform
78,313 CF /
3-08 9-2
% Souris
33, %
03-0809-2F
Fecal Coliform
63,604CCU/
3-08 9-
% Solids
283
3- 8 9- G
Fecal Coliform
57,348 C Lr/
03- 809-2G
% Solids
27.9 ,
03- 8 9- a
Geometric Mean
58,691 C U/
03,- 8 9-2
Nickel
81.9mg/Kg
03- 8 9.2
Chromium
108
03-0809-1
Arsenicmg/Kg
03-0809-2
pf 1,
7,43
Respectfully Submitted,
Dena y rs
NC Cert

70�
e�Iielig:+�i
LAddress:
STATES % AL ICAO
122 Court Surer a RO. Box 228
Statesville, NC 28687
04 872-4697
Contact Person: -,,„
.d
Phone m FAX
in o
P
Requisitioned by; (Time Date)
Custody Record
Customer bti8r
arrt la 91 i
arrt ! PreservativeMatrix
T e DateDaiwa
praretersrttquetadlcraalysistrr"l
d x'
�+ /
T
# t
y/(
e s
�res4ratl - .
Relinquished by.
Titrt tC�ata t�
1 a O
4s... ,..
Sampled
P
Received by.
5y
firm tC� tTransported
ragyrt v ia-
I NaOH
H 2 so
Relinquished by; TirtaaiDate
oiiYdtimes
Holding met:
Other chemical
Received in lab:.
Chemicals in turtitairtace; lab:. _.
rm dCJttts i
Compliance works
7, Chemicals in containers, client
Chemicals added upon receipt"
Non-compliancework:
Received chill
4 Lab Comments:
10. Samples delivered as soon as
Gaulle
11. Samples chilled upon receipt
1. Other

SPECIALIZED , INC.
2960 Foster Creighton Dr.
R 0. Box 40566
Naafi all f 37 0 4 t56
Phan 1-615-7 17'7
STATESVILLE ANALN"'TICAL
6445
2 COURT STREET
Lab Number: 96—AO48106
TAT SVILL E, NC 28677
a n°Ile ID.* 01-0605
Dare Collected:
Time Collected;
ProjectProject-.
Na
Date Received: /7/96
Time Received.- 12:00
Statesamoler:
1. ion : 387
S k 1 1 Type: Solid waste
Site I.D. z
TCLR Results
Matrix Spike
Analyte Result;
Units
Reg Limit Recovery (I)
pate Method
S,41 f 5.0
1
10.0 lib
8/15196 8150
Cndrtn t 0.010_
e9/1
0.02 97
8/15196 0080
Reotacbl r T 0.0050
49/1
0.008 95
8/15/96 0000
Lin ane f 0.20
e9/1
0.4 to
8/15/96 Soso
Retiozyc l r' 1.0
4911
10.0 99
0/15116 8080
ToraAen /0.25
e0/1
0.50 64
9J15/96 SSS
Silvea 0«5
rgl
1.0 15,
S/15196 S15p
Heptachlor epoxide t .0050
$911
p.pllld
8/15196 SRS
ND = Not detected at the apart limit.
TCLR preparation follows method 1311 SW-846 as
revised November 24, 19gR
57 C R 551141.
as
RIALITI' CONTROL DATA if
Surrogate Recoveries
Surrogate % Recovery
Target Range
9CA Surrogate, 1,2-5 cbloroethane, 0
100.
S - 124
VOA Surrogate, Toluene 49
10.
86 - 1S'
VOA Surrogate,-Brorofloorobanzene
95.0
77 - 118
RNA Surrogate, Nitrobenzene
90.0
35 - 115
COPY

SPECIALIZED ASSAYS, INC.
2960 Foster Creighton Dr.
P 0, BOX 40566
Nashville, TN 37'20"566
Pfrone 1-615-726-0177
#0*M0NL_V_r X
STATESVILLE ANALYTICAL 6445
AT7: DENA MYERS
122 COURT STREET
Lab Number: 96-AO48106
STATESVILLE, NC 28677
Samole ID: 01-0505-1
Date Collected.-
Projectl
Time Collected:
Project, Name.-
Date Received: e/ 7/96
Sampler:
Time Received: lezoo
State Certificationt. 387
Samclle Type: Solid waste
Site I.D.*.
DUALITY CONTROL DATA #4
--------------- - ------------ ------------- - -----------------------------------
- --------- - ---------
Surrogate Recoveries
Surrogate I Recovery
------------- ------- —_
Target Range
---------- -
DNA Surrogate, 241uorobiphenyl 130.
43 - 116
DNA Surrogate, Terphenyl 414 85.0
20 - 130
DNA Surrogate, Phenol ds 30.0
10 -110
DNA Surrogate, 9-Fluorophenol 25.0
20 - 110
10 Surrogitet 2,416-Tribrosoohenol 120.
to - 122
Post/PCI Surrogate, TCAX 67.0
22 - 135
Pest/ PC8 Surrogate, ORC 36.0
22 - 135
Report Approved By:
Peoort Datei 8/19/96
Theodore
J. DUello, Ph.D.
Michael H. Dttnn, M.S.
Dartnv B.
Hale, M.S.
COPY 3

Phone
T T SV I LLE ANALYTICAL 6443
AT' DENA MYERS
'SPTATESVILLE, NC 28677
samole ID; 01-0805-1 Date Collected,: Time Collectedt
r.4r meDate Baca°ward: lei 7/96
Samol r : Time Received.; .1 :00
State r- l t ion: 387 SamoleTySolid waste
' i 1: e I . D. r
TChR 'Result
Natrix Spike
nol9te
Result
Units
Reg Limit
Recovery W
pate
Method
Chromium
5.50
0911
5.
?a
R 101%
60104
Led
0.5
191
5.
810196`6510
Mercury
5.01
69 1
. 11
106
8t 8116
' 7471
leniue
0.10
0411
1.5
120
9 1 /96
6010
Silver
5.1
/1
5.5
1
1196
61
Benzene
0.1
eg t
0.5
100
8115i 6
0240
Carbon tetrachloride
0.1
#111
0.5
96
15M
8240
Chleroben ene
< 0.1
a /1
too
98
0115/96
8240
Chloroform
t 0.1
egyl
6.0
96
8115M
8240
1.-5rchlo ceth n
9.1
0971
9.5
96
8/15/96
8240
1.1-5zchloroetheoe
t 0.1
6911
0.7
15
RJ"15J96
BZ40
Why lethylketone
t 1.0
/1
200
156
R 15196
8240
Te richloroethene
6.1
43/1
0.7
96
R 151 6
8240
Trick oroethene
5.1
49/1
015
98
8115/96
8240
Vinyl Chloride
t 0.1
6,111
0.2
98
8/15f96
82,40
Cresols
r owl
mgll
200
60
116 96
0270
•1.4-Dichloro enzene
5.1
mga"1
7.5
75
R116196
8270
R, -broitrot.oluene
t 0.10
mgdl
0.13
95
R 16196
8270
he chlorobenzene
t 0.10
sq/1
0.13
Ito
W 16/96
R 76
exchlor-1,6-botadzen
t 0.1
4g/1
0.5
too
9116196
8275
Hexechloroethene
5.1
mgdl
3.0
75
16/96
8270
Nitrobenzene
1 0.1
9/1
2.5
85
/16196
R 7
ent chloroo enol
1 0.1
eg/1
100
96
8/161%
8870
pyridine
t 0.1
eg 1
5.0
10
0/16196
0270
C,4.5 Trrchloroghenol
.1
mg 1
400
to
8/16/96
RRTS
, ,6-Trichloroohenol
5.1
eg11
2.0
75
/16176,
8,270
Chlordane
t 0®01
my/l
0.030
107
8t15/96
RCRo
COPY

SPECIALIZED ASSAYS, INC.
29W Faster Creighton Tit
Box 40566
iaa6ya1, TN 37204-0566
Phone 1-61 - 2 17
STATESVILLE ANALYTICAL
6445
AT-: i l�
122 COURT STREET
Lab NQmbei- t96-AO48106
Via )- O j t
Time `'
I I t
Pi-oject Name;
DateReceived;
/ '
/1;1 a
samoler:Time
w
i ci
12:00
.t. E-Ilia:
387
Sample
T Solid
Site I.
Report
Wen
Oil
Anal to
Result
Units
Limit
Limit
Factor
Date
Time
Analyst
Method
Batch
Alumnus
1400
# 1kg
0.7
1.0
1
81 IM6
1608
R.Street
6010A
0130
Arsenic
RO
' 1kg
1.0
1.0
1
R 9196
IWO
R.Street
6010A
0131
Calcium
1600`
lkg
1.0
1.0
1
/ 919
IWO
R.Street
6010A
81
Magnesium
?30.
#914
9.7
1.0
1
/ gJ 6
16119
R.Street
6010A
81
mercury
RO
*q1k9
0.10
0.10
1,
0112176
121
R.Street
7671
O
Molybdenum
2.1 "
mO1kg
1.0
1.0
1
/ i
16s1O
R.Street
6010A
8139
Potassium
531.
#O kg
9.7
1.0
1
176
1608
R.Street
4010A
0139
Selenium
NO
9/kg
0.07
0.97
1
R1 W96
16118
R.Street
6010A
' OIOg
Sodius
1630
#q1kq
0.7
1.0
1
61 9154
I6 1O
R.Street
6010A
8137
Reactive Cyanide
RO'
lkg
2.0
2.0
1
R1 /%
20:55
D. Hoover -RR-R
6
8014
Reactive Sulfide
5.8
Ag
2.0
2.0
1
81 8/16
2005D.
Hoover
RR-0 6
8094
Corraoivity
ROT CORRO6Ig
'
811 IR6
16s3
D. Hoover
1110
1356
lgnitaW i ty
ROT IGNITABLE TO 200 F
81141g6
16:30
K.Witte
10109
7241;
nitrite-R
RO
ulkg
1.0
0.1
1
8117176
10»2
K.9itte
106
7771
Nitrate-R
R0
oglkg
1.0
0.1
1
2116/%
1704
k.Ritte
1006
7770
rlelda6l Nitrogen
7760
uglkg
1.0
1.0
1
Oi 9116
16:4
Macy
351.E
8556
TCLR Results
Natrix
Soike
Analyte
Result
Unite
Reg Limit
Recovery
1 ?
Date
Retnod
TCLR 'Extraction
COMPLETES
R1 81R6
1311;
Zero Readaoace Extraction
CSRLI,TRO
21 0176
1311
Arsenic
� 0.10
I911
5.0
110
allot%
6010
Barium
1 1.00
gll
100
85
81101 6
6010A
Cadman
ti
0.10
09t1
1®0
7 ,
RMOl76
6010A
COPY

Relinquished by Tre Date Received In Lab by Time Date Remarks-
na Ate; AW pb,)nI
w
Sampled y Time Date Preservation:

Lap ReRpq
r om: 'er tification No. 402
L SC Certification No. 99012
KC Drinking Water Cert. No.
FL Certification No. E87519
37735
'JAN 10 W7
January 7, 1997
To: City of Statesville
Attn: Hammer Anderson
P.O. Box 1111
Statesville, NO 28687
The following analytical results have beet-, obtained for the
indicated sample which was submitted to this laboratory:
SanPle I.D. AA61323 Customer Code- STATESVI
Ls gin Group #: 997681 Customer Refer'ence: 4THCREEK
Phone Number: [phone]/Fax[phone]
Customer Sample I.D#: 4TH CK SLUDGE
Sample collection date: 12/20/96 Tim : 13:00
Lab submittal date; 12/20/96 Time: 18:26
Received by: CP Validated by: ADO
Parameter: TCLP EXTRACTION (METALS ONLY)
Method reference: 1311 Unit:
Result; Completed MDL or sensitivity.
Date started: 12/30/96 Date finished: 12/1/96
Time started: 14i3O Analyst: LAS
198UNW,
Method reference; EPA 3010
Unit:
Result: Completed
MDL or sensitivity:
Date started: 12/31/96
Date finished: 12/31/96
Time started: 10:oo
Analyst: LAB'
Parameter: ARSENIC, LEACHABLE
Method reference: 6010
Unit: mg/L
Result: Less than
Date started; 01/02/97
MDL or sensitivityj o.50
Time started: 09:00
Date finished: 01/02/97
Analyst: LAM
Parameter: SELENIUM,, LEACHABLE
Method referencei 6010 Unit: mg/L
Results Less than MDL or sensitivity: 0,10
Date started: 01/02/97 Date finished: 01/02/97
Time started: 09:00 Analyst: LAM
Parameter: CADMIUM, LEACHABLE
Method reference: 6010 Unit: mg/L
Result: Less than MDL or sensitivity: 0.10
Date started: 01/02/97 Date finished: 01/02/97
Time started: 09100 Analyst: LAM
449 Springbrook Road At. P,O. Box 240543 & Charloue. NC 28224-0543
Phone: [phone] &, Toll Free Number: 1-8001529-6364 A, FaX: [phone]

Parameter: CHROMIUM, LEACHABLE
Method reference: 6010
Result: 3.2 mg/L MDL or sensitivity: 0.50
Date started: 01/02/97 Date finished: 01/02/97
Time started: 09:00 Analyst: LAM
Parameter: LEAD, LEACHABLE
Method r0!0t6hciB­ 6010
Result.- Less 'than
Date startedt 01)02�/�j'7
Time started: 09.-00
Parameter: SILVER, LEACHABLE
Method reference: 6010
Result-. Less than
Date started: 01/02/97
Time started.- 09:00
P6�rameter: MERCUkYo LEACHABLE
Unit: mg/L
MDL or sensitivity: 0.50
Date finished: 01/02/97
Analyst: LAM
Unit: mg/L
MDL or sensitivity; 0.50
Date finished: 01/02/97
Analyst: LAM
Method reference: 7471
Unit mg/L
Result: Less than
MDL or sensitivity: 0.02
Date started: 12/31/96
Date finished: 12/31/96
Time started: 13:15
Analyst.* LAS
Parameter: BARIUM, LEACHABLE
Method reference: 6010
Unit: mg/L
Result.- Less than
MDL or sensitivity: 10.0o
Date started: 01/02/97
Date finished: 01/02/97
Time started: 09-00
Analyst: LAM
Parameter: MERCURY DIGESTION
Method reference: 7471
Unit:
Result: Completed
MDL or sensitivity:
Date started: 12/31/96
Date finished: 12/31/96
Time started: 09:00
Analyst: LAB"
Parameter: TCLP EXTRACTION (VOLATILES
ONLY)
Method reference: 1311
Unit:
Result: Completed
MDL or sensitivity:
Date started: 12/30/96
Date finished: 12/31/96
Time started: 14:30
Analyst: DRY,
Parameter: TCLP EXTRACTION ( SEMI- VOLATILES)
Method reference: 1311
Unit:
Result: Completed
MDL or sensitivity*
Date started: 12/30/96
Date finished: 12/3*1/96
Time startedt 14:30
Analyst: DRY
Parameter: PREP. METHOD 3510
Method reference: 3510
Unit:
Result: Completed
MDL or sensitivity:
Date started: 12/31/96
Date finished: 12/31/96
Time started: 09:00
Analyst: DRR
449 Springbrook Road -a. P.O. Box 240543 A, Charlotte, NC 28224-0543
Phone: [phone] *,. Toll Free Number, 1-800/529-6364 .*. FaX; 704/525-0409

Par meter: PREP. METHOD 3510 WITH EXCHANGE
Method reference: 3510 Unit:
Result: Completed MDL or sensitivity:
Date started: 01/03/96 Date finished: 01/03/96
Time started: Analyst: VOA
Parameter: PREP. METHOD 3510 WITH
EXCHANGE
Method reference: 3510
Unit:
Result: Completed
MDL or sensitivity:
Date started: 01/03/96
Date finished:
01/03/96
Time started:
Analyst: VOC
Parameter: TCLP VOLATILES BY 8240
Method reference: SW846-8240
Unit: mg/L
Result: see below
Date started- 12/31/96
Date finished.-
12/31/96
Time started: 18:37
Analyst: MP
Parameter: TCLP SEMI-VOL,ATILES BY
8270
Method reference: 8270
Unit: mg/L
Result: see below
Date started: 12/31/96
Date finished:
12/31/96
Time started: 13:37
Analyst: MP
Parameter: TCLP PESTICIDES
Method reference:
Unit: mg/L
Result: see below
Date started: 01/06/97
Date finished-.
01/06/97
Time started:
Analyst: VOC
Parameter: TCLP HERBICIDES
Method referencez
Result: see below
Date started: 01/06/97
Time started:
Data for TCLP VOLATILES BY 8240 mg/L:
Component Name
BENZENE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROFORM
1,4-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,1-DICHLOROETHENE
METHYL ETHYL KETONE
TETRACHLOROETHEN
E
TRICHLOROETHENE
VINYL CHLORIDE
Date linighedt. 01/06/97
Anal"t. VOC
Result
Component MLPL
Not
detected
0.01
Not
detected
0.01
Not
detected
0.01
Not
detected
0.01
Not
detected
0.014
Not
detected
0.01
Not
detected
0.01
Not
detected
O.04
Not
detected
0.012
Not
detected
0.01
Not
detected
0.02
449 Springbrook Road *. P.O. Box 240543 *, Charlotte, NC 28224-054,3
Phone: [phone] ,,*. Toll Free Number: 1-800/529-6364 Fax. [phone]

ort
`pity+ f Statesville Sample L D. AA6132 (continued)
`age: 4
Januarys 7, 1997.��.,.:
Fu€I
Service Analytical $ Environmental Solutions
Data for T LP" SEMI-VOLATIL mg/La
Component ame
Result
Component MDL
CRESOLS
Not
detected
0.050
1,4-DICHLOROBENZENE
Not
detected
0.050
, 4-DINITR T LU NE
Not
detected
0.012
HEXACHLORDBENZENE
Not
detected
0.010
HEXACHLOROBUTADIENE
Not
detected
0.050
BBXA NL RQ THANB
Not
detected
0.050
NITROBENZENE
Not
detected
0.050
P NTA BLOROPHB CIL
Not
detected
0.25
PYRIDINE
Not
detected
0.25
, 4, -TNI NLOROPH NOL
Not
detected
0.25
2,4,6-TRIGHLOROPHENOL
Not
detected
0.10
Data for TCLP PESTICIDES mg/L
Component Name
Result
Component MDL
CHLORDANE
Not
detected
0.015
ENDRIN
Not
detected
0.010
HEPTACHLOR
Not
detected
01005
HEPTACHLOR EPDXIDE
Not
detected
0.005
LINDANE
Not
detected
0.2
METHOXYCHLOR
Not
detected
1.
TOXAPHENE
Not
detected
0.25
Data for T" LPHERBICIDES mg/
Component Name
Result
Component MDL
, 4-D
Not
detected
5.0
SILVEX
Not
detected
0.5
Sample comments:
T LP pesticides and herbicides subcontracted
to NG certified lab #
444.
If there are any questions regarding
this data, please
call.
Angela D,
rca h
tY
ctcLaboraoDer
449 Springbrook Road K0. Brix 240543 h rlotW, NC 224-0543
Phone; 704/ 2 . 364 Toll Free Numben 1-8/ 29-5364 A, F : 7041525-0409

'J
IES, INC
17A Service AnalVfical & Environmental Solutions
C I i�o hmt
Address_
Mohe
449 *tiqgbt66k Road Chilf!Otte, NC 28217
char
plime: 704/529-6364
FAX 104J�!�-040�
U6 Location Requested
fo(Certt�dAh*sis NCL/Sc.--�Oths,�
Water Chlorinated Yes —.- No �NA -
Sa(*e "d Ppon Collection yes No
Report
Bill To
P-0-Milling Reference
Project Narne
Sc Sc "%'— DRINKINGWATER: NC_ THESOLIDWASTE.-
ER NC
SC
OR 0-I'HOTHERSC
— SC
OTHER_
*CONTAINER TYPE CODES. A . Amber C = Clear G , Glass P w Plastc; TL - Teflon-Uned Cap VOA w Volatile organic$ Analysis (Zero Head Space)
OTHtFi� kC
sc
OTHER-
9;3m��

port
m. NC Certification No. ; 40
SC Certification No. 99012
C Drinking dater Cert. No. 37735�+���� �
FL Certification No. 1 No » EnOmmental Soulons
July 5, 1996 J
City of Statesville
Attn. Ms. Carol Rogers
P.O. Box1111
Statesville, NC 28687
The following analytical results have been obtained for the
indicated sample :which was submitted to this laboratory:
Sample I.D. AA51884 Customer Code: STATESVI
Login Group . 6108BI CustomerReference: 7" -1
Phone Number.- [phone]/Fax[phone]
Customer Sample 1. DadSLUDGE CAKE
Sample collection date. 6/1 / 6 Time: 1
Lab submittal date. /1/ Time. 13.E
Received by CP Validated by MM
Method reference: 1311
Unit.
Result: Completed
MDL or sensitivity:
Date started. // 8
Date finished: /8
Time started. 14.-30
Analyst; LA
Parameter: TCLP EXTRACTION
(VOLATILE ONLY
Method reference: 1311
Unit:
Result: Completed
MDL orsensitivity:
Date started: 06/25/96
Datefinished:06/26/96
Time started.- 18:45
Analyst: DRY
Parameter.- TCLP EXTRACTION
(IiI-VOLATIL )
Method reference: 1311
Unit:
Result: Completed
MDL or sensitivity:
Date started. 06/20/96
Date'finished"» / 1/ C
Time started. 0.0
Analyst: UR
Method reference: EPA 3010
Unit
Result: Completed
MDL or sensitivity:
Date started, 7/01/ C
Datefinished.-07/01/96
Time started: 10:15
Analyst: LAS
Parameter PREP. METHOD 3510
Method reference: 3510
Unit,
Result: Completed
MDL or sensitivity:
Date ;started: 06/24/96
Date ,finished 06/24/96,
Time started: 09:00
Analyst. DRR
449 Sprin brook Bond A6, P.O. Box 240543 Charlotte, NC 28224-0543
Phone: 04/ 9-63 4 A, Toll Free Nurnben t- 1 9µ6364 , past: 704/ 5_Ci40

wdpotl
117�y of Statesville N
779age:
July 51 .«
method Seto
Result.
Uoitt ■
MDL or 0.50
Parameter: SELENIUM, LEACHABLE
Method reference: 6010 Uni.t. m /L
Result: Lees than MDL or sensitivity: 0.10
Date started: 07/02/96 Este inishe07/02/96
Time started: 08:00 Analyst: H
Parameter: CADMIUM, LEACHABLE
Method reference: 1 nit: gag
Result: Less than; MDL or sensitivity: 0.10
Date started: 07/02/96 Date finished07/02/96
Time tarted: 08:00 Analyst: DH
Method reference: 1 Unit: mgl/L
Result: Les than NDL or sensitivity: 0.50
Date started: 7/0 / Date finished:07//96
Time started: 08:00 Analyst: DHJ
Parameter.* LVAD,� LEACHABLE
Method rederencot 6010
*es
ultt Less that
D- 07102/96
Time started*. 08.00
Method
Parameter.- 9ILVZ9, LEACHABLE
referohoet 601,o
Result-. Less than
9i W «07/02/96
Time ■ +i0
1 r
.50
Date finished-.r
Analyst*. DRI
Unit /L
MDL orsensitivity:
Date finished:07/02/96
Analyst
Parameter: MERCURY, LEACHABLE
Method reference: 7471: Unit mg/L.
Result: mess than MDL or sensitivity: 0.02
Datestarted: 7/ / Date finished: 7/ /
Time started: 1 Analyst: DHJ
Method reference: 6010 Unit: /L
Result: Less than MDL orsensitivity: 10.00
Date started:: 07/02/96 Date finished: 7 /
Time started.- :00 Analyst: DHJ
Method reference: W - 740 Unit: m /
Result: see below
Date started i 06/28/96 mate finished:07/01/96
Time started 18:09 Analyst
449 Springbrook Road A. P,O. Box 240543 Charlorre, NC 28224-0543
Phone. [phone] A. Tall Free Numben 1-80t 29-6364 Fax: [phone]()9

Parameter: T L ' EMI- ' LATILEE BY a270
Method reference: 8270
Unit.
/L
Result: see below
Date tarts 0
Datefinished;
27/
Time started: 15:57
Analyst:
Parameter: MERCURY DIGESTION
Method reference: 7471
Unit'.
Result.- Completed
MDL orsensitivity:
Date started: 06/28/96
Date finished:06/28/96
Time started 11
Analyst: LAE
Data for TELE V LATIL E BY
8240 mg/L:
Component a
eSUlt
Component MDL
BENZENE
Not
detected
0.01
CARBON TETRACHLORIDE
Not
detected
0.01
CHLOROBENZENE
Not
detected
0.01
CHLOROFORM
40.01
1,4-DICHLOROBENZENE
Not
detected
0.01
1,2-DICHLOROETHARE
Not
detected
0.01
1,1-DICHLOROETHENE
Not
detected
0.01
METHYL ETHYL KETONE
Not
detected
0.02
TETRACHLOROETHENE
Not
detected
0.01
TRICHLOROETHENE
Not
detected
0.01
VINYL CHLORIDE
Not
detected
0.02
Data for TCLP SEMI -VOLATILE BY 8270 mg/L
Component
e ul
Component MDL
CRESOLS
Not
detected
0.05
1,4-DICHLOROBENZENE
Not
detected
0.05
2,4-DINITROTOLUENE
Not
detected
0.05
HEXACHLOROBENZENE
Not
detected
0.05
HEXACHLOROBUTADIENE
Not
detected
0.05
HEXACHLOROETHANE
Not
detected
0.05
NITROBENZENE
Not
detected
0.05
PENTACHLOROPHENOL
Not
detected ted0.25
PYRIDINE
of
detected
0.25
2,4,5-TRICHLOROPHENOL
Not
detected
0.25
2,4,6-TRICHLOROPHENOL
Not
detected
0.25
If there are any questions
regarding this da
a, please
call
An Overcash
Laboratory Director
449 a rin br' k Road
P. e Box 240543 Charlotte, NC
2 224-0 4
Phone: 7 4t52 -6364 . Toll free Number: f - /52 -6364
Fa ; 704/5 5- 4
9

ftu
tea i8ax 1111 # tNatestfille, North Cfarofina 28687
February 27, 1995
. Lou Polletta
Division of Environmental Management
DEHNR
P.O. Box 29535
Raleigh, NC 27626-0535
Rey Non -Discharge Permit WQ0001759
Fourth CreekSludge Landfill
Fourth Creek WWTP NCO031836
Dear . plle
Attached is the annual repot on our surface disposal: unit (sludge landfill) located at the
Fourth Creek WWTP, Bell Farm Rd., Statesville, fredell, NC. Information pertaining to the
activities daring the calendar year 1994 are as follows:
Groundwater monitoring indicated exceedances mostly in Fecal Coliform, TDS, and T C
parameters. The November, 1994 samples still indicated this. However subsequent resarn lin
of e offending monitoring wells now indicate full compliance. ce. We have submitted maps and
data to the Mooresville Regional Office to aid in their efforts to insure further compliance.
s this is a surface disposal unit, Options tender 40 CFR 503 allow for vector and'
pathogen concerns to be addressed by daily cower or bacteriological examination® We have
performed bacterial analysis and maintained daily cover.

Mr. Lou Pfilletta
Division of Environmental Management
WQ0001759 Fourth Creek Sludge Landfill
Page 2
Mr. Steven Lambert expresses his great appreciation the help your office and Permits and
Engineering have provided in the successful completion of these reports. Should you have any
questions you may contact Mr. Lambert or Mr. Harold Anderson at 704-878-3438.
Sincerely,
L.F. "Joe" Hudson, Yr., Director,
Water/Waste-Water Treatment
LFH/slI

ppp-
ppppp� ANNUAL LA"Dr-ILL/COMP'OST/STABILIZATION CERTIMA'"ON AND SUMMARY FORM
Iredell
rArJLITi tIAME Cth Creek SIpd pp-tmlt # -W-Q COUNTY
FAMI I Y I YP E (ploase 011ock one), (OLondfill ( tomplots Pott A (Sourc#(#) and "nosidust IW Vol"mo only) sod Port C
E]Cojopost/ StabIlIzollop Foollity ( tomplet* Potim A, 8, and C)
VI A$ TIME MILITY m or-r=nAnbN uulollE PAST CALIENDAR YF-An? _-&-- YES NO, R "0, sklp Poito A, 0, md C and owrify form bolow.
Part A*
Volw {drys 1 8)
7— ndtd us#(*)
IN nowum dry flons
Water Plant 1.8
rAqr�Tl water Plant 7.0
wtl Water Plant 12.2
rimy water Plat 12.4
-------------------------------------
- - - - - - - - - - - - - - - - -

C"1
•. w .V Vr C`w'd C
y
NIcnitcringrxrcr 1 � r`?f
rt Reductolcn ( 2 -P!ease indicate !seal achieved and alternativeperformed
I � rrt tier ', f t rr is i rr ti,) 4
Alternative 4 alternative 5 A t rrs tt
Cass
Alternative t Afternative, 2 , It rr at
It iic i to altemativep rfcr 3 (C'.ass a Davy) indicate ' ,.c s tic Significartty Reducstnc rs"'
Aerctic Cigesticm rc lc i cm c r-.lime t lli c
f it able tc aiternative p rc rsd ( .'ass A or .ass ) c i t ': t l INirg mcnitc n data.
4woq90 I:Srwv ,4u=er d premwvy Ct Samms Anamww
Pararreter Mintmum Avft—aqe I M=,MjM 'JUVS I S=wm= AnWyMs T -1 YPO 7===S
C�dcrm 2 x 10 .MPN �
C; i c ° qmmI I
V
FORM RIF (1 1 )

.4 k
DATA REPORT
City of Statesville
Fourth Creek WWTP
Rost Office Box 1111
Statesville, North Craolina
Received 9- 9
Reported -9-9
Work Order # 06-0907
SAMPLEPARAMETER RECEIVED DRY WEIGHT
- 99 h Crk. Press Fecal Coliform, 160, 9 Q f 9
9 - 907-1 4th Crk.PressSolids .9"
Respectfully Submitted,
Dena e
Statesville Analytical
NC Cent.
SC Cent. # 99010
NC TAW e.
. , Box2,28 * Statesvffle, North Carolina 9 i 71 9"

DATA REPORT
City of Statesville
Fourth Creek WWTP
Post Office Sax 1111
Statesville, North Carolina 28687
Receive: 118-
Reported 12-20-94
Work Order 1118
SAMPLE # CUST ID
PARA.
AS RECEIVED
DRY WEIGHT
04-1118-1 4th Crk. Mono.
SEE, ATTACHED
1 - 8-1 4th Crk. mono.
Cadmium
.5 5ppm
1.12ppm
1118-1 4th Crk. Mono.
Nickel
3.97ppm
12, ppr
-1118-1 4th Srk. Mono.
Lead
, 15 pp a
. 51° ppm
04-1118-2 4th Crk. Mono.
Mercury'
.250ppm
.81 p a
04-1118-1 4th Crk. Mono.
Chromium
5.3 0ppm
1 . ppm
-1 18 t;h Crk. Mono.
Arsenic
2. ppm
6.49ppm
04-1118-3 4th Crk. Mono.
ply
6.12
04-1118-4 4th Crk. Mono.Solids
8 .8
Respectfully ,Submitted
Dena Myer
NC Cert.
P.O. Box 228 * Statesville, North
Carolina 28687 704/87W4697

...............
Blue Ridge Labs
A0. BOX 2W * fte momuw Road
Lemir, NMIh CAtOUM 2644$
WePhOnt (704p 72"M
CLIENT-
Statesville Analytical
P.O. Box 228
Statesville, NC 28687
Attention: Ms. D. Myers
DATE RECEIVED:
November 22, 1994
DATE REPORTED:
December 15, 1994
DATE REISSUED:
January 06, 1995
aAMEPIE NUMM
5AMLU DESCRIPTION
411-2568
Solid; 04-1118-1 for TCLP Metals, TCLP
VOC,
TCLP Serni-Voc,
TCLP Herbicides, TCLP Pesticides, % Solids.
PARAMETER
"T
M
DAR EARM
411-2568 - TCLP
Metals
As
2.00
mg/l
11/29/94
Ba,
1.00
mg/l
11/29/94,
Cd
0.25
mg/I
11/29/94
Cr
0.50
mg/1
11/29/94
Pb
2.00
mg/l
11/29/94
Hg
0.004
0.001
mg/I
12/14/94
Se
1.00
mg/l
11/29/94
Ag
2.00
mg/1
11/29/94
Concentrations are below Minimum Quantification Limit except where noted
NC Laboratory Certificate No. 275.

EARAM w
SAT
411-2568 i
Benzene
M
12/02/94
CarbonTetrachloride
.
12/02/94
Chlorobenzene
0.050
rng1l12/02/94
Chloroform[
12/02/94
r
12/02/94
1,2-Dichloroethane
0.050
mg/I
12/02/94
Methyl Ether Ketone (MEK)
0.050
mg/I
12/02/94
Tetrachloroethene
0.050
mg/I12/02/94
Trichloroethene
Vinyl Chloride
0.050
mg/l
12/02/94
Solids.111/29/94
L iattached)
TCLP Herbicides (th8150)
,
12/15/94
-P i
112/15/94
TCLP Pesticides (Method
Chlordane1
112/15/94
r
1
l
1 �" 1
Heptachlor
ffi
l
12/15/94
Undane
0.1
1 '1 4
Concentrations are below minimum Quantification Limit except where noted,
NC Laboratory Certificate No.
275.
-

9
I
EARAMETER RESULTS
1 - - TCLP Pesticides(Method
Methoxychlor 1. 12/15/94
Toxaphene "l 12/15/94
a Customer requested lower detectionlimits.
***NOTE: o r hN al error
REPORTED BY:: �.---
ID.. Ire r General Manager
Concentrations are below Minimum Quantification Limit except where rooted.
NC Laboratory Certifi to No. 275.

1 a 'Ran 1 u, -6-9 ^i
Date Extracted 11 w]9
g/l
" I
,Pyricine
TCL /8270
1
o-Cresof
T LP/827
1
p-Cresol
TCLPle,"8270
1
Hexachicroethane
TCLP/82701
rn-Cresol
TCLP,18270
1
Nitrobenzene
�°
f L / 0
1
Hexachlorobutadiene
TCLP/8270
1
4, -Tri binroph n l
TCLP,18270
1
, ,-Trinhinr ph nol
T LP/827
1
, _ initrdtoluen
TCLP/8270
1
Hexachlorobenzene
TCLP/8270
1
Pentachlorophenol
TCLP/8270
1
Concentrations below ntit .tinn lirni" n pt where noted
Reported By.m.
D. in r - General Manager
N,C. Wastewater Cert 275

OL(� 15 '94 IS: 30
p 5
ANALYTICAL MUSTRIAL RESEARCH LABORATORIES, INC.
4295 CROMWELL RD.,
STE 611
CHATTANOOGAt TN 37421-2177
AIRL SAMPLE I.D.
19150
TCLP
METHOD 1311
BLUE RIDGE LASS
SAMPLE DATER'
11 J28/94
SAMPLE'* 411-2568
IPA MW CONSTITUENT
REGULATORY MOL,
RESULT
DATE
METHOD
NUMBER
LML(MCVL)
(Mg/L)
Q"QlL)
ANALYZED
(SW446)
TCLp PESTICIDES
0020 CHLORDANE
0.03
0.01
NO
121151$4
m
D012 FENSIN0.03
0101
NO
1,2115/94
BOW
0031 HEPTACHLOR
01008
0Z6
NO
12(15/94
$060
-SPDXIDE
0.008
0=3
NO
12118/94
wao
0013 UNDANS
O.4
al
NO
12/10194
am
0014 METHOXYCHLOR
10
I.0
NO
12JIS/$4
8080
0016 TOXAPHENE
0.6
0.1
NO
12(1"4
Soso
T-OLP HER131CIOP-9
0016 2+0
I=
0Z
NO
12115/94
$150
0017 2,4,5;TP (SILVE)Q
1.0
015
NO
1211w"
$150
Porlormod In accordance w#h 40 CFR 261(06/29/90)
------------------ ------------ -------------------------

10 TVA 4:R4 A;T4100 461
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Analytical nConsulting Chemists
OMRD DATE REDEIVED 11-23-94 1316 South Fifth Street
DATE REPORTED 12- -i t n , N.C. 28401
r 3 R 3 91 3-9 `93
nc. 91)343-9688
PAGE 1 Off°
STATESVILLE ANALYTICAL P.O.
P.
STATESVILLE, NC 28687
SAMPLE R P' N:` 2 SAMPLES 3-
. R-
RESULTS
z
Mercury, as Hg, PPS .2504
Arsenic, as As, PPM 2.00
ROGER C. OXFORD, CHEMIST

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We# Lomtion 0 Subswface LOW -PM -A"
Wei kfentificaton, Number ---We# Depth �Ft, S" Reld POM (LPP)
Wetj DiarM*r___2.n_Sarrple (Scrmied) Interval-- Ft -TO_ft L�nd AWra*n of SW90
Doh to WaW Lem --Z2..Z4t below measuring poh, pefore sampling) notary OisuhAor __X_ Othor r, a rl (I f i I I
Wasuring point Is __Z,J 5____ ft. *me land surtaw
,allons of WOW purnpedimled before S,,Impling C Oder _, Appearance
pH_spedric Conductance __ Ming Temp.
COIL._-W 3 / 1 QL9 4__DAb Lab SwTOO An*zed cedtfication No_JAI3
Laborattsy, Name ....... H ydEq Aq4lyticll
I CEMIIFY PW THIS WPM tS TRtjF MD
Signabxe of PeMiftee (or hithorized Ager)
GW,59 FIEV. "21
NickeL—.—
MqA
mgA
Ztl - 7jnc
rngl
Pesticides/Herbicides
(Speafy compounds)
Ug/l
ugA
ugA
Mer (Spe(* compounds and
Concentration units)
NqW VWOq OiWd m4*d dls� OT)d
(se6 42 oh bodK)
see bw* for k"ftw 10 06*0"
Dat wvl Okyw wp;" Onty e L
I
7ij

A 41 1 .
w
w w
w
�
w
w
Specificn
Total i k MgA Na -:
I CERTIFY T THIS REPORT IS TRUE AW ACCURATE.
QIQ,, Values, w
dissolved- and,

Facility Name Fourti-t creek WWIP
Address Blll Fang Road
statesville, NC__County__jredglj___
PERMIT NUMBER: (REQUIRED) V 169
Non -Discharge
Pi C 3
NES
rl�p��� OPERATION iEINGWONITORED,
(REQUIRED) __ Lagoon - septic Tani E)rain Field
Well Location
r mmwell, #1 ----Well D pth Ft. Spray Field
be
Coliform, MF Fec 1 20
Mg/I
/1 00ml
Colitorm: MF Total
/I 00ml
(Note: Use MPN method (or highly turbid Samples)
2052
Dissolved Solids: Total
pH (wtien anal�
s
mung/I
TOC -- 117
Chloride .
Mg/I
Arsenic
mg/l
mg/I
Grease and Oils —
mg/I
Hardness , Total
mg/I
Phenol
mg/l
Sulfate
uctan—
Specific Condce---
umh os
Total Ammonia 4, 10
mg/I
mg/I
TKN as N
Nitrite (NO2) as N
mgA
Nitrate (NO3) as N 41.5
TgA
Phosphorus: Total as P
mg/I
mg/I
Al - Aluminum
Mg/I
Ba - Barium
mg/I
lci
Ca - Caum
Cd - Cadmium
m9l'
Chromium' Total
Mg/I
mgA
Cu - Copper .327
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/1
Mn - Manganese
mg/I
Na - Sodium
ate
Subsurface Low-PressUre
Piping (LPP)
Land koicatidn of Sludge otrert,
®w
Ni - NickeL---- M9"
Pb - Lead mgA
Zn -Zinc Mg/I
Pesficides/Herbir-ides
(Specify Compounds) Ug/l
UO/I
Ug/I
Other (Specify Compounds and
concentration units)
nfl•
ack tor
ohly to amross
xgj� coolesi

�ON IALITYVI
Type or Use a ball -pent pen and press firmly.
PERMIT NUMBER, (REQUIRED)
a1
Non -Discharge
NPDES
Address ---_-
a,
JyREDLUJ&DL;OPERATION BEING MONITORED
Well Location 4 �� LL .., � �.,..
__
Lagoon SepticTank/Draft FkAo
Well Identification Number t ._
Well Depth ®, F .
T splay Fuld Subsurface Lair-Pfrx°::�ut&
Well Diameter Sample (Screened) Interval
Ft. To --Ft.
Piping ILPPI
Depth to Water Level I ft. below measuring point (before Sampling)
Land Application of Sludgeti 1, a� �
other
Measuring point i _ ft. above land surface
RotaryDistributor
Rotary Distributor
Gallons of water pumped/bailed before sampling _
a
Field Analysis: pH —Specific Conductance
_ uMhoa `fern . C�
Odor _ Appearance --
Date Sample Collected Date Lab Sample ,analyzed
Laboratory Marne
Certification No,
SAMPLES FOR METALSE COLLECTED UNFILTEREDD FIELD ACIDIFIED -A—YES
COD m /I
Nitrite as __
/l Ni i eI__ _ c x _ nir /l
oliform. MF Focal ... _ /10 mi
Nitrate (I C as N
__ g/l Pb - Lead—_______-,_ ._ M g/I
Colifo= MF Total A 00ml
Phosphorus: Total as ..
l Zn - Zinc rfl/l
(Net Use MPN method for highly turbid samples)
AI - Aluminum �
/I Pesticides/Herbicides
Dissolved Solids: Total 1 m /l
Ba - Barium
mgA (Specify Compounds)
pH (when analyzed - _ _---units
Ca - Calcium
m_ rt-mg/I � — /1
O _.._ _ m /l
Cad - Cadmium �
'
_ /i � _ �. ,. /l
Chloride � _ � ` _� ._ _ mg,A
Chromium: Total
mgA Ug/I
Arsenic ___- - _- _.w: _ .... mg/1
Cu - Copper ; ____..
_ ...._ . m /I Other (Specify Compounds and
Grease and Oils Mr /l
Fe - Iron
mgA Concentration unit >
Hardness: Total m /l
H - Mercury.
nag/i
Phenol mil
K - Potassium
m i
Sulfate m /l
Mg - Magnesium
mgA
Specific Conductance �� tr hesMn
- Manganese ,� �_ _
mgA
Total Ammonia _ . tri ll
_�--�
No - Sodium
mgA
TKN as N lit/l
I CERTIFY THAT THIS C IS TRUE AND ACCURATE.
NDIgi Values should reflect dissolved
colloidal concentrations. (see #3 on back)
�.e. �
�w
< n
Sep
for In tructioyI�
nature of ermIttee (or 'Rti)
at
bbg r„ and only t address above.
copies
allow
:b:ack
GW-59 REV.6/93

Iwo
a
K_ glasig-jug"Wol 4 MI
r
�
y
i�
M
TKN as N_ .A .. _ g
1 CERTIFY THAT THIS REPORT T IS TRUE AND ACCURATE.
n
Signature f P rmitt (r Authorized Agent*)fit
See 4ack for inWualons.
GW-59 REV.6/93

� ti a ' . . �-.� .. < „., �, r ,:. ,,: •., Y,na ,-,. n ,.v� ...... ..: . ....:
Wx
., .' ... ':: ... ,.. .., ....:.:.. . 5.*.r � 31, *, tit:. • i�i'' . `�.. .�`�,> yea..: �.
.„ :,....., _ , • •-.. ..�... . -. „,. ,.� ,<...x „ ..� ,. .,..-„,q ... ,,.� � m:'... y..n.` .c.. . �. �., ..ax � � a .�r "» ham• � y�o� � �..
Type or Use s ball-point err and pre firmly. .
° PERMIT Ilt�t: ��NFn� R.
Facility Name ° ion- isch r o - - _ , . .
Address _--gell Fast Road NPDESTy
____�qt_ate@_vi119A NC 28677 County Iredell ly DjWDB& OPERATION BEING MONITORED
ICI [ thin radiant (f IRED
Lagoon Septic Tarp rain Pieta
Well Identification NufnWr 1 Well Depth F=t:
oa , . fit %a�rtee t.s�-�'€esc�re
Well Diameter sample (Screened) Interval Ft. To Ft. . ` °
Depthto Water t«sol - � f 1
ttR below measuring point tors sampling) � . is trr f sty
Measuring point is 1- � ft, at�o o Ian�l srrrfao Omer Lan 111
Gallons of water pumped/balled before sampling . f r ar di r�i r l
Flnf n lyl is: p Specific Conductance a hos Temp. r Appearance.
Dante Sample Coll -ICate Lab Sample Analyzed
Labor,itory'Name U Certification No, t
SANIPLES FOR METALSCOLLECTED UNFILTERED AND FIELD ACIDIFIED yE
mgA Nitrite s N I t' i 94
lit rm: MF Fecal t 00ml Nitrate (NO3) as N 2.51 gA' b -tea rng,1l
nl l rm: I t t1 I t pl pt t l ' n- Il.099
{Note. Uri MPH triethod for highly turbid tam Al - Aluminum mgAPesticides/Hetblcides
Dissolved Slid :Total g - Barium MgA(Specify potln
t (wharf analyze . —unit - Calcite _ g/I
TOc.___ __ g - Cadmium less to rt . il' ug/
ArsenicmCu - Copper .296 mgA Other (Specify drra unds and
Grease and Oilsrng l Fe - Iron << MgA Concentration units) t
Phenol _ Potassium g
Cult lr, mgA Mg, - Magnesium mg/l.;
Specific Conductance uMhoe Mn - Manganese mgA'
Total x nl Less thLaq,-. rn /l Na - Sodium r tg
TKN as
colloidalI CERTIFY THAT THIS REPONT­1� TRUE AND ACCURATE.
NM9, Values should ro
J.
Sae back tor InstructlorrA.
Aign 6re k---ttec r catty rl Agents Date Submit blue, green, and y
GIN-Y' REV. 6/93

Fc
°iit Name .
. .
W W
a
aM
♦ '. �. i W i :' i :M M m N . '...
L 1.:
�
� M a b �, p� e
y:
�y i®',�. .y y
SignattireofPermftee Authorized
h ri c Agent*
.- 3 REV.
N
M i
» W w oow: W

r
Older
.. .. ...........
Dissolved id: Total
- Barium
MgA
(Specify d)
l"1 hen analyzed) _
units
Ca - Calcium
—
ug/l
T - "mg/l
Cd - Cadmium
.001 mg/l
ugll
thl ri" le
mgA
Chromium: Total
.. g
g
Arsenic
rrrg
- Copper
mg/l
Other (Specify Compoundso
Grease and OilsA
Fe - Iron
mgfi:'Concentration
units)
Hardness: Total
ri
Hgm Mercury
g
Marro€ �m�
g
- t
Sulfatew
mg/l
Mg - Magnesium
nng
.
Specific Conductance
has
Mn - Manganese
mgA
Total Ammonia Leas than .
- Sodium
g
1 CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE.
NDje,
Values should reflect dissolved and
iSee back for 41*001

HYDRO ANALYTICAL LABORATORIES
CERTIFICATE OIL ANALYSIS
Fri Lee 16, 1994
Page 1
CLIENT NAME :
4TH CREEK WWTP
CLIENT
NUMBER :
800149
REFERENCECITY
OF STATES ILLE
PO 94953
SAMPLE NUMBER
66483
66484
66485
66486
RECEIVED DATE g
11/16/
11/1.6/
11/16/
11/16/9
COLLECTED DATE
11/16/'
11/16/ 4
11/16/9
1.1/16_/9
METHOD
DESCRIPTION!
WELLI
WELL2
WELL3
COMMENT
*TEST NAME
UNIT
RESULTS
RESULTS
RESULTS
RESULTS
--------------------------------------------------------------------------------
62ST
AMMONIA NITROGEN
m 11
< 1
< .16
. 16
< .16
CADMIUM
m /l
. 001
.00
.001
.002
CHLORIDE
mg/l
<16
<10
21.3
11.5
COPPER
mg/1
.296
.61
.235
.6`18
DISSOLVED SOLIDS
mg1l
125
110
243
163
FECAL COLIFORM
4/1001
84
2
1
LAB pH
SI
5.2
6.6
6.4
6.
NITRATE-N3
mg /l
2.51
1.34
17.48
1.29
TOC
mg1l
3
0.66 _-
1.41
31.2
IN
m /l
.69
.036
3
.62
'IFIED BY �

HYDRO ANALYTICAL LABORATORIES
CERTIFICATE OF ANALYSIS
Fri Dec 16 1994
Page
CLIENT NAME TH CREEK WWTP CLIENT NUMBER 80014
REFERENCE CITY OF STATESVILLE PC 94953
6637 663
SAMPLE NUMBER 11 / 16 / 11/16/94
RECEIVED BATE F 11/16/ 11,/16/9
COLLECTED B SATE G
METHOD D
DESCRIPTION
COMMENT
TEST NAME NIT RESULTS RESULTS
6 30D /1 .10 .1
AMMONIA I 'RO E T / .City 1 .001
CADMIUM 24.8 24.8
CHLORIDE' /, I .006
COPPER 143 143
FECAL COLIFORM #/100 6.6 6®6
LAB PH U 1.14 0.72
ZINC /1
o "Y' d
CERTIFIED BY

Analytical and Consulting Chemists
"(DXFORD 1316 South Fifth Street
Wilmington, N.C. 28401
bowtorles DATE RECZ17ED 11-13-94 [phone]
2-0-
nc. DATE REP1794 ORTED Pax [phone]
94W2755
PAGE I OF 5
HYDRO ANALYTICAL LABORATORIES
6300 RAMADA DRIVE BOX C-2
CLEMMONS, NC Z7012
ATTENTION: TERESA PERRY IC94 it
SAMPLE DESCRIPTION: 6 6230D
1. 66483
2. 66484
3. 66485
4. 66486
5. 66487
6. 66488
RESULTS
3
3 4 5 6
230D COMPOUNDS
ATE ANALYZED 11-22 11-22 11-22 11-22 11-22 11-22
ichloradifluoromethane, "PR <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
hloromethane, PPB <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
in Chloride, PP B <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
romp ethane, PP B <0.5 <0.5 .5 <0.5 <0.5 <0.5
hloroethane, PP B <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
luorotrichloromethane, PPS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
.1-Dichloroethylene, PPS '<0.5 <0.5 <O.S <0.5 <0.5 <0.5
ichloromethane, PPB <0.5 'C0.5 <0.5 <0.5 .5 <0.5
rans-1.2-Dichloroethylene, PPS <0.5 <0.5 <0.5 <0.5 <0.5 .5
,1-Dichloroethan e, PP B <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
,2-Dichloropropane, PP B <0.5 <0.5 <05 <0.5 <0.5 <0.5

'(Dj(FORD
Analytical and
Consulting Chemists
1316 South Fifth
Street
Wflmington,
N.C.
28401
bwatorles DATE
RECEIVED 11-18-94
[phone]
DATE
REPORTED 12-07-94
Fax (910) 343-
.9688
nc
94W2755
PAGE 2 OF
5
HYDRO ANALYTICAL LABORATORIES
INC P.O.
#
L94527
6300 RAMADA DRIVE BOX C-2
CLEMMOHS, NC 27012
ATTENTION: TERESA PERRY
SAMPLE DESCRIPTION: 6 6230D
1. 66483
2. 66484
3. 66485
4. 66486
5. 66487
6. 66488
RESULTS
1
2
3
4
5
6
is-1.2-Dichloroethylene, PPP
<0.5
<0.5
<0.5
<0.5
<0.5
<0-5
h1oroform, PPB
14.9
0.59
15.8
0.61
13.9
19.3
romochloromethare e, PPB
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
,1,1-Trichloroetha,ne, PPB
'<0.5
<0.5
'<0.5
<0.5
<0.5
<0.5
I-Dichloropropen e, PPS
<0.5
<0.5
'<0.5
<0.5
<0.5
<0.5
Tetrachloride, PP B
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
enzene, PPB
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
.2-Dichloroethane, PPS
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
4
.richloroethylene, PPB
<0.5
<0.5
<0.5
40.5
<0.5
<0.9
1, 2-81chloropropane, PPS
<0.5
40.5
<0.5
<0.5
<0.5
<0.5
romodichloromethane, PPB
(0.31)
<0.5
1.55
<0.5
2.35
8.30
ibromamethane, PPB
-0.5
<0.5
<0.5
<0.5
<0.5
<0.5
1,3-Dichlaropropene, PPB
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5

Analytical and
Consulting Chemists'(S)XFORD $
15 South Fifth
WUraing,ton, N.C.
28401
� DATE
I 1113-54
0
DATE
REPORTED 1--
Fax
94W2755
PAGE 3 Off°
HYDRO ANALYTICAL LABORATORIES
INC.
.
L94527
CLEMMONS, NO 27012
ATTENTION: TERESA PERRY
SAMPLE DESCRIPTION: 6 6230
1. 6643
2. 6644
3. 66485
4. 66486
5. 66487
. 6648
RESULTS
1
2
3
4
5
6
oluene, PPB
<0.5
<0.5
<0.5
0.66
<0.5
<0.5
,1,2-Trichloroethane, PPB
<0.5
<0.5
<9.5
<0.
<0.5
<6.5
trachl `oethen, PPB
<0.5
<0.5
9.5
<0.5
<0.5
<0.5
1., 3- 10 .o o o ane , PPB
<0.5
<0.5
<0.5
<0.5
<9
<0.5
ibramochloromethane, PPS
(0.26)
<0.5
1. 33
<0.5
(0.44) 4.26
�hlorobenzene, PPS
<0.5
<0.5
<0.5
<0.5
'<0.5
0.5
'thylbenzene, PPB
<0.5
<0.5
.
<6 a 5
<0.5
'<0.5
1,1,1,2 t o to oe a , PPB
<0.5
<0.5
6,
<0.5
'<0.5
.5
a - .rye PPB
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
I-Xylene, PPB
<0.5
<0.5
<0.5
<0.5
. 5
a-Xylene, PPB
<0.5
<0.5
6.5
<0.5
<0.5
.5
Styrene, PPB
<0.5
<
9.5
<0.5
40.5
<0.5
I op ova . n, PPS
< .5
<0.
<0.5
<0.5
<0.5
'<0.5

Analytical and
Consulting Chemists
�FORD
1316 South Fifth
Street
'18401
NUmington,
N.C.
bc,1110des DATE
RECEIVED 11-18-94
[phone]
DATE
REPORTED 12-07-94
Fax [phone]
nc.
94W2755
P.NGE 4 OF
5
HYDRO ANALYTICAL LABORATORIES
INC
P.O. #
L94527
6300 RAMADA DRIVE aOX C-2
CLEMMONS, NC 27012
ATTENTION: TERESA PERRY
SAMPLE DESCRIPTION: 6 62505
1. 66483
2. 66484
3. 66485
4. 66486
5. 66487
6. 66488
REASULTS
1
2
3
4
5
6
romotorm, PPB
<0.5
<0.5
1.0
<0.5
<0.5
<0.5
PPB
<O.S
<0.5
<0.5
<0.5
<0.5
<0.5
,2,3-Trichloroprop ane, PPB
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
-Pr opylbenzene, PPB
<0.5
<0.5
<0.5
<0.5
-0-5
<0.5
romobenzane, PPB
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
1,3,S-Trimethylbenzene, PPB
<0.5
<0.5
<0.5
.5
<0.5
-Chlorotoluene, PPB
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
"-Chlorotoluene, FPS
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
",.ert-Butylbenzene, PPS
<0.5
<0.5
<0.5
-0.5
<0.5
<0.5
1,2,4-Trimethylbenzene, PPB
<0.5
<0.5
<0.5
<0,.S
<0.5
<0.5
sec-Butylbenzene, PPS
<0.5
<0.5
.0-5
<0.5
<o-S
moo.5
9-Isopropyltaluene, PPS
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
1,3-Oichlorohen zene. PPB
<0.5
<0.5
<6.5
<6.5
<0.5
<0.5

'(E)XFORD
Analydcal and
Consulting Chemists
1316 South FifthStreet
Wilmington, N.C. 28401
DATE
RECEIVED1-18 - 4
1 763-97 3
DATE
REPORTED 1 -
Pax 1 343- 33
94W275S
AGE
HYDRO ANALYTICAL LABORATORIES
INC . O. # L94527
6300 RAMADA DRIVE
CLEMMONS, NC 27012
ATTENTION: TERESA PERRY
SAMPLE DESCRIPTION: 6 62300
. 6648
. 66484
3. 66485
4. 66486
S. 66487
6. 66485'
RESULTS
1
2
3
4 6 6
,4-Dichlorobenzene, PPB
.5
. 6
6. 6
0. 6 0. 6
-SY1hz, PPB
<6.6
<a
.5
<,6 <.6 .6
i h1 bn;z n , PP
< . S
< .
. 6-
< , 6 .6 .
., , 4 i h or z ne, PPS
< .
< .
. 6
<0. 5 < , <0 . 6
eahi u.°n, PPB
< . S
< . 6
< . < . 6 . S
aph h leas PPB
< -
< .
.S
< . <0.5 .6
PPB
<.
<0,6
.5
<. <.6 .S
ETHOD 64 COMPOUNDS
ATE ANALYZED
11 3
11- 3
11 3
1.1 3 11- 3 11-23
thylene dibromide(L ) PPB
< ,
<0.
< . < :1 .1
, 2 -Dhz -3- hl pr e , ?PB
< .
< . 0
< .
< , 3 < . 1 <0. 1
ANN MCMILLAN, ANALYST

I
Consulting
Analytical and
11 South FifthStreet
(DX.FORD
nc.# i LATE L 1 - ) b
DATE REPORTS 12-07-94
ADDITIONAL T
LAB ID#CLIENT'S L ALSO DETECTED
°BLANK LAB L .
BROMODICHLOROMETHANE @ 1.10
94WZ755.5 66487 ACETONE @ 761PPS
METHYL ISOBUTYL KETONE @ 0.53

.�or Laboratories, Inc.
NORTH CAROLINA OEM SAMPLE SUBMISSION FORM
LABORATORY N. P. . S S. ID # 75
Analytical and Consulting Chemists m
6 Scut Mh Street
Wilmingtori, N.C. 28401
763-9793
Fax [phone]
CLIENT: COUNTY:
CCLLSC `S PURCHASE CR CR
SOURCE OF SAMPLE CCMTAINER ( ) c _ OXFORD LAB OTHER
TYPE OF SAMPLS (S) s PLEASE INDICATE
SOIL WASTEWAONITORFN_G_WELL
OTHER-
130TTLE SAMPLE LOCATION TIME DATA ANALYSIS
LOCATION CCCS COLLECTED COLLECTED REQUESTED
vz-
MA IMUM HOLDING TIME AND LAB SCHEDULE FOR THE FOLLOWING:
S_ HRS BODS (TUE AND TMURS : s 4 s 0) (WED AND 1 s S
48 HRS FOR MBAS , C . PC4—P (THURS 5 . : 3 (P S b - 13 : C
S FOR T. CCLIPCRMO TF RS S :
. MRS FOR P . COLD" MCA — TM R S F
UNLESS OTHERWISE SPECIFIED REGULAR TIME PC : SAMPLES MON - FRI S a _— : 3
LAC iTCRY USE L
CLI LAB IDS
CONDITION CPC A
PROPER PRESERVATION ( ACID, BASE, CHEMICAL): "DES M
IF NO, PLEASE EXPLAIN:
RECEIVED WIT SIN REQUIRED HOLDING TIME;YES, N
IF 90, PLEASE LAIN
RECEIVED IN WATER ITT ICE OR CHILLED C 4 YES NO
IF NO, PLEASE PLXIN
EATS RECEIVED: Zl— TIME RECEIVED- / a'
ACCEPTED- REJECTED: BY
RN —SAMPLE REQUESTED: YES No
SPECIAL COMMENTS:
V. 3-31-5

FORM
ANNUAL LANDFILLICOMPOST/STABILIZTION CERTIFICATIONY
FACILITY NAMFourth Creek'Sludqe Monofill PERMIT III -Wf)1Mj2-9 „ — COUNTY -i rat
FACILITY TYPE (please check a): Landfill complete Parts A and
Compost/ Stabilization Facility I complete Parts A, 8, and
Source($) ICU
reWduat/ sill
MM
Intend use
Part
Facility was compliant during calendar year 1993 with all conditions of the permit (including but not limitedto Items 1-3 below) Issued by the
Division of Environmental Management _ Yp __NO. If NO, please provide a written deartptlon why the facility was not compliant.
t: All monitoring was perforated In accordance with the permit and reported during the year as required and three () copies of certified laboratory results are attached,
All operations and maintenance requirements were compiled with or, In the case of a deviation, prior authorization was received from the Division of Environmental Management..
No contravention of Ground Water Quality Standards occurred at a monitoring well.
i CERTIFY THAT THE ABOVE INFORMATION IS ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE, AND ALL THE INFORMATION IN THE
SUCCEEDING FAMES IS ACCURATE AND COMPLETE.
P`RMIT E SIGNATURE DATE OPERATOR OR AGENT SIGNATURE DDT ;
:.

FACILITY NAME Fourth Creek lur_ede Mortqf illPERMIT # QQ_QU"1.i 5 1 ml I
r;
FACILITY IMF (please check one): Landfill ( complete Farts A and C
Compost Stabilization Facility ( complete Darts A, B, and
4S THE FACILITY IN OPERATION DURING THE PAST CALENDAR YEAR , —, YES ___ NO. It NO, skip Farts A, 8, and C and certify form below.
1 1111 ill "Ill
go
Annual (dq to")
M
Em
Part
Facility was compliant during calendar year 1993 with all conditions of the permit (Including but not limited to Items 1-3 below) Issued by the
Division of Environmental Management tf:: YES NO. If NO, please provide as written dosription why the facilitywas not compliant
1, All monitoring was performed In accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached.
All operations and maintenance requirements were compiled with or, In the case of a deviation prior authorization was received from the Division of Environmental Management
3, No contravention of Ground Water Quality :standards occurred at a monitoring well.
I CERTIFY THAT THE ABOVE INFORMATION 1S ACCURATE AND pL TO THE BEST OF MY KNOWLEDGE, AND ALL THE INFORMATION IN THE
SUCCEEDING PAGES ISACCURATE AND COMPLETE.
CDATE OPERATOR CS AGENT SIGNATURE IiMtrPR

HYDRO ANALYTICAL LABORATORIES
CERTIFICATE OF ANALYSIS.
Tue, Nov 30, 1993 Pa
Client Name. 4 h
CREEK
WW7F ClientNumber: 800149
Re-ference CITY OF STATESVILLE
Sampte Number;
49175
ReceivedDate:
11/09/93
Collected
L/0 /
Method:
Description;
Comment;
SLUDGE
Test Name
InL
exults
% I _
4 .
CADMIUMmg/kg
CHROMIUM
4.
COPPER
mg/kg
444
mg/kgLEAD
METAL PREP
YES
NICKEL
mg/kg
41. ,
ILVER
mg/kg
45.4
TCLP METALS
ZINC
k
CERTIFIED :

SAVANNAH LJ ORATORIES
S L & ENVIRONMENTAL SERVICES- INC-
Lakeside Drive * Mobile, Alabama 3 3-5118 • (0 666-6633*Fax (5 -6696
LO O: 3--15199
Received: 11 NOV 93
A Teresa Perry
0 ANALYTICAL
HYDR6300
Purchase Order;L93-031
Ramada Drive
Clemons, NC 27012
Project: Statesville
Sampled S Client
PORT OF RESULTS
Page 1
LOG NO SAMPLE DESCRIPTION SOLID OR SEMISOLID ISOLI
P S
DATE SAMPLED
15199-1 49175 Sludge
11-09-93
15199- 2 49180 Sludge
11-0 - 3
P R
15199_1
15199-
V lati.le in " LP Extract (8240)
Benzene (T L.P) , mg/1
0.010
. 1
Carbon tetrachloride (T LP), g11
0.010
0.010
for n en (T LP) ,
0 ®010
<0.010
Chloroform ('LP) 1
0,010
.010
1, 3°Ol lretane (TLP) , t11
0.010
0.010
1,1Oi lre °lene (TLP), m&1
0.010
0#010
Methyl ethyl ketone (T LP), 11
0.10
0;10
Tetra l r e lene (T LP), mg/1
0.010
0.010
Tric l r e lene (T LP), mg1l.
<0.010
0.010
Vinyl chloride (T LP), 1
0.0 0
<0a020
Semivolatiles in T LP Extract (5 70)
Cresol o,m,p (T L ), mg11
<0.013
0.013
1,4-Oic lcrc en ene (T LP) 11
0.013
0.01
3; ®Oin.itrot luene (TOLP), 11
0,013
<0.013
eacl:rcbenene (TLP), ;1
<0.013
0.013
ie achlarOb ta,die e (T LP) 11
<0.013
<0.01
dexac lcr e ane (T LP) , z 1
-013
0.013
Nitrobenzene (TOLP), l
0.013
0.013
Penta loop encl (T P) , mg11
0, 0
<0.062
3, ,5-Trio l r en l (T LP), mg11
0.0
0.0 3
, , Trichl r tend (TOT"?), mg11
<0.01
0.01
Pyridine (TLP) 1l
0.35
0,3
Wbit0i Alt)

SAVANNAH b ORATORIES
S L & ENVIRONMENTAL SERVICES. INC.
900 Lakeside Drive - Mobile, Alabama 36693-5118 # [phone] # Fax [phone]
LOG NO: M3-15199
Received: 11 NOV 93
Ms. Teresa Perry
HYDRO ANALYTICAL
Purchase Order: L93-631
6300 Ramada Drive
Clemons, NC 27012
Project: Statesville
Sampled By: Client
REPORT OF RESULTS
Page 2
LOG NO SAMPLE DESCRIPTION SOLID OR SEMISOLID
— --- — ------
SAMPLES
---------
DATE SAMPLED
— --- — — - — -----------
— --------- -------- — ------------------
15199-1 49175 Sludge
11-09-93
15199-2 49180 Sludge
11-09-93
-----------------------
-- — ------ ------------- — -----------------------------------
PARAMETER
— ------ ----- — --- ----------
15199-1
----------
15199-2
---------- — ----- --
---------------------
Pesticides in TCLP Extract (8080)
Chlordane (TCLP), mg/l
<0.,0030
<0.0030
Endrin (TCLP), ing/l
<0.0020
<0.0020
Heptachlor (TCLP), mg1l
<0.00080
<0.00080
Heptachlor epoxide (TCLP), mg1l
<0.00080
<0.00080
Lindane (g-BHC) (TCLP), mg11
<0.040
<0.040
Methoxychlor (TCLP) , mg/1
<1.0
<1.0
Toxaphene (TCLP), mg/l
<0.050
<0.050
Herbicides in TLCP Extract (8150)
(TCLP), mgll
<0.025
<0.025
2,4,5-TP Silvex (TCLP), mg1l
<0.021
<0.021
Metals in TCLP Extract (6010)
Arsenic (TCLP), mg/1
<0-20
Barium (TCLP), mgJ1
<11. 0
1.2
Cadmium (TCLP), mgJ1
<0.10
4.0
Chromium (TCL2), mg/l
<0.20
<0.20
Lead (TCLP), mg/l
<0.20
<0.20
Selenium (TCLP), mg/l
<0.10
<0.10
Silver (TCLP), mg13
<0-10
<0.10
Mercur7 (TCire) , mgJ1
---------- ----------
<0.010
-- — --- —
<0.010
------ — -- ---------
— — ----- -----------------
RE'rEU,110E: EPA SW-346 3rd Edition, 1986
Savannah Laboratories North Carolina Certification
No. 39.14.
woor4toty Imadons in Savannah, GA * TWMO;40� FL - *04 AL 040rOeM 804�ihf PL q

SAVANNAH U -'ORATORIES
S L & ENWRONMENTAL SERVICES. INC.
900 Lakeside Drive Mile; Alabarna 36693-51`15 * [phone] * Fax [phone]
LOG NO: 3-15 99
Mt4 Teresa Perry
HnRO ANALYTICAL
6300 Ramada Drive
Clemmta.
Project. Statesville
Sampled By: Client
REPORT CP RESULTS Page
LOG NO SAMPLE DESCRIPTION , QC REPORT FOR. SOLID/SEMISOLI
9 Laboratory,
.. a ,.
PARAMETER
151993
15199-
15199-5
-------
------Volatile
Volatiles in TCLP Extract (82 0)
Benzene (TCLP), 11
<0. 10
93
Z
5.
Carbon tetrachloride (TCLP), g,11
< . 91
lren e (TCLP), m&11
97
Z
2.1_
Chloroform (TCLP), mgll
< , 1
---
1,2-i lre ane (TCLP), mgJ1
<.1
-
--_
1,-i lre ylene (TCLP), m11
<0.010
85
Z
2.4
z
Methyl ethyl ketone (TCLP), l
< .19
..
Tetra l roe ylene (TCLP), mg/1
<0.910
--
T is lore ylene (TCLP).
<C. 91C
86
1.2
Vinyl chloride (TCLP), m 1l
< . 2
_
-
---
Semivolatiles in °CP Extract (827)
Cresol o, ., (TCLP), ll
< .959
86
Z
12
1, -Czchl r Len ene (TCLP), mg1l
<0.050
74
Z
8.1
2, - initr t l .ene (TCI,P) , 1l
<0195
108
8.3
exachl ro6en ene (TCLP), mgJ1
<0.95
98
«
17'
e achl rob tadiene (TCLP), 11
<0.95
56
.9
e achl roe pane (TCLP), 11
< .35C
6
7.8
b
Nitrobenzene, (TCLP), mg1l
<.85
11
21
P ntachlor hen l (TCLP), mg1l
<0.25
76
22
, ,5 Tric l r henol (T ), mg1l
< .25
--
--
2, , 6-Trichl r hen l (TCI. ) , 11
<0.050
94
Z
113
Pyr-, dine (TCLP) , rig J l
<1.0
42
«
----------
21
Laboratory locations In Savannah, GA . Tallahassee, FL code, AL , Deerfield Beach, AFL Tampa, FL

IN
a
Received: 11 NOV 93
Teresa Perry
HYDROANALYTICAL
Order:-631
6300 RamadaDrive
Clemons, 271
Project: Statev l
Sampled 3 Client
REPORT, OF SUL"J'S Page
LOG NO SAMPLEDESCRIPTION , QC REPORT FOR SOLIDISEEMISOLID
Accuracy R.
Precision
PARAMETER
1513
1.51-4
151--5
Pesticides in TLP E.rct, (SS)
Chlordane (T ), 11
. 3
-
rin (T LP),
<0.0020
94
Z
4.3
Heptachlor (T , mgJ1
<0.00080
96
Z
5.1
Heptachlor epoxide (T LP) , M911
<0.00080
91
z
4.5
L . d ne -3 ) ('T LP) , 11
<0.040
86
Z
4.3
e c for L ). mg11
<1.0
1006.8"Z
Toxaphene (T LP), 11
---
Herbicides ide i P Extract (8150)
2, 4-(' LP) , mg1l
r. 25
35
ZI,
18
2,4,6-TP Sil e ('TLLP), mg11
. 25
66
3
Metals in T LP Extract (6 13 )
Arsenic (TLP), 511
<0.20
108
5.6
Bari (T LP') , mg11
<.0
84
1.2
Z
Cadmium (TLL), 11
<0.10
92
Z
2'.2
ZF
Chromium (TLP), mgJl
<0.20
93
Z
2.2
Lead (T LP) , mg /
. 2
S
4.1
Selenium (T LP)N 11
.23
SS
2.3
Silver (T LP), mgJ1
<0.20
84
terzr , (TL , mg,11
<01010
13
Laboratory fccattcn, in Savannah, A � i n , AL Deerfield Beach, FL Tampa, FL

704-078-3438
Of
It
. ram-;.. •� .. �.
t t t 1 tattsuille. W (Carolina 29677
April 27, 1993
Environmental Management Division
Groundwater Section
P. t. Box 27687
Raleigh, NC 27611-7687
Subject: Fourth Creek WWTP Landfill Wells Analyses
Permit WQ0001759
Dear Sirs
Enclosed salts of ourlandfill wells, sampled March 23, 1993, at
Fourth Creek WWTP, NCO031836.
The Fourth Creek WWTP Lab, 1 1, ran the ors -site measurements. Our "water Plant
b, #37-620, ran the Total Coliform.. .11 other parameters were contracted out to Hydra
Analytical Lab in Clernmons.
VO 's were ;ly d chloroform levels remain high. The laboratory believes this
s due to using chlorox solution as a disinfectant for the bailer; they sent a copy of an alternate
rinsing method, which we will incorporate. Results of the VOC analyses are attached.
1f 1 can be of further assistance, please call at 7
Sincerely,
Lk F. "Joe" Hudson, Jr., Director
Water/Wastewater Treatment
LFH1sg
Enclosure

Environmental Management Division
Groundwater Section
27687
Subject: Fourth Creek WWTP Landwell Wells
Permiti7
Dear Sirs.
Please find enclosedthe results of our three
.ill malls, sampled July i, 1993 9 our Fourth Creek
WWTP, NCO031836.
Our Fourth Creek WWTPi %, ran the -sits measurements.
All other parameters were contracted out to Hydro Analytical
Lab in Clemmons.
resampling for 'non -compliant pare e s i scheduled.
If I can be of further assistance, please call 7 4)
878-3438.
Sincerely,
Z:��J_
L. F. "Joey Hudson, Jr., Director
Water/Wastewater Treatment
Enclosures;

FRIt
%
r
I CERTIFY THAT THIST I'll
Signature, of `a
a e (or AuMorized Agent*)
REV, 9W.,
�• M � . r �A � a •�" • wN
as i et

Milt
# 1. S ",� # # ## • # :; #
* a
pg
w+
CAM �
Odor.Appearance
'Pertfrca-
fc a ? fy
u w
R #F

w
*
« . «
..
Appearance
y � a
r0ficabon No.
I CERTIFY THAT THIS REPORT IS °T '`
Signatre
GW-59 REV.
«VAlues shoWd «
coWdal ooncefibufioftrt2 on «o

Water/Wastewater Treatment Plants
704-878-3438
tat
III I t t ill. -Nud4 Taratina 28577
October 5, 1993
Environmental ement Division
Groundwater Section
P. . Box 27687
Raleigh, NC 27611-7687
Subject: Resample ;for Third Creek & Fourth Creek`
Landfill Wells
Dear Sirs:
In our letter of August 20, 1993, we stated at re Ales would be taken for non-
compliant t parameters. Attached the results from these samples.
Hydro l ys initially Creekb, Certificate
1 1, ran the resample for Fecal Coliform.
If you have y questions, please call at 7 4) 878-3438.
lueerly,
Hudson, Jr., Director
'
Water/WastewaterTreatment

�9
^
CERTIFICATE ANALYSIS
y
P
ded Sep 8, 1993
5
,
CLIENT NAME ,
4TH CREEK WWTP
CLIENT NUMBER 800149
4S S :
CITY OF STATES " LL
°
SAMPLE NUMBER
45843
45844
DATE
8319
SSSS
�SEES
LLECT SATE
S S 1 SS
SS 1 S
:.
SSA T I J
3
;
p
TH
H
iEST PRAMS
UNTII RESULTS
— ww« ww «+as+ .—.®..---w.—,-----
RESULTS
mwr :--------- ------ um ..----
m ----- ran..: ..----......, .—,.—.—.
ISS L "S SOLIDS
— ,.gymm-----:wrr
MG/1 204
SS

A a
CERTIFICATE OF ANALYSIS
ed Sep 9, 1993
Page
LIENT NAMET
9
WWTP
CLIENTNUMBER
800149
ITT OF STATESVILLE
AMPLE NUMBER
45839
45840
45841
45842
ECEIVSD DATE :
08/31/930
/ 1 /93
/1 /9
/ 1 /9 �
OLLSCTED DATE
08/ 1 /9
/31 /9
/ 1 /93
9/91 /"99
iM
1
W2
W2
U
MMEN1`
4TH
�a
'SST NAME
UNIT
RESULT'S
RESULTS
—ay..ww.,---- Rwa
RESULTS
-- ----, .m—..mm--si.,
RESULTS
---
awwv w ---errs..-----.cmtansewni
HISS L" SOLIDS
«oProP------
g/1
—iw+rr---- Y.----- -----
100
116
1
R k
EARAC-N,pry {{ yN�p�q! ®ryry�
Wgg Sasr L I F O M
�{g
/ 0
99
yy yyµ���awr±.w
I� k B`
•"erg!
yg �ryp
6.
pq9 Y.YS
0 O V
pdp
G
r
4
r.
m
a
G l
S
w

CERTIFICATE AT P ANALYSIS
led Sep 8, 1993
Page
;LIEN T1 NAME E r
4TH CREEKWW` P
CLIENT
NUMBER
F
800149
CITY OF STATESV ,LLE
a �kPLE NUMSER
4583E
45a36
45837
45838
E E:VEE DATE
/ 1/
/ 1
/ 1/08/31/93
, LLE TE DATE :
/ 1 /912
6E/ 1 /
/ 1 /
08/31/93
E 7 HCD
IESgCR.ghdaP T . N
W#�1
WRD
W
w
{gyp
}ply
"E'EN` NA M E
LINK RESULTS
RESULTS
RESULTS
RESULTS
e assr.------------
)_ SLVED SOL110S
-- s.vasp--auw
E/1 <4
104
148
6
CERT,T-F'-1E0 BY

FE�Lf,�CLJF�CRM �ANAL�YSIS
�Wo R �KS H E E T
aa
M
0
[E
M
RM
7�-7—
MMMMMWAW
(cc
AnalySt
Date Set UP
Time
-r-
Read Byv ---------------
Date—
Time
C..ecked
JQ u a I t 'Ill
-T
0
B 1k
Sam, pled by
sample type
/vol
0 F E-H,
'TCR _7

"ady Nw*--IRMjfth Creek►; ! a
Address
M'
s «:..: FW a .,
Nowl:
..
_
_.
Rotary
,.y
-.
i •
� � w"
Fli:
� "�.: ill, t $r:.
y
�yg
4' m i 'r a -._ �« � � � t^
* � � � � *
�
4, f': :. t S, M '� & '; t t • a `,: t M S

a
.. t. s
Oxford Labor Analyfical and tin he
C.
DATE RECEIVED 11-11 3 1316 trek
ATE REPORTED 12-07-93 Wilmington, .. 28401
1311in'T'W" Fax [phone]
' t 3 PAGE 1 OF 5
HYDRO ANALYT TOPS S INC
6300 RAMADA DRIVE SO C`-3
CLEMMONS, NC 27012
ATTENTION: SA PERRY
SAMPLE DESCRIPTION: 4'TH CREEX (6 30
1.. #1
.
3. #
. #
5 #5
6{ #6
6230D COMPOUNDS
DATE ANALYZED
Dichlorodifluoramethane, PP
Chloromethane, PP
Vinyl Chloride, PPB
Bromomethane. PPS
Chloroethane. PP; ,
Pl r ri hl r me hane, PPS
I,I-Dichloroethylene, PPS
Dichloromethane, PPS
r ns-1 -Oichl r e h le e, PPB
1, 1 ichl roe ha e, PPS
3, `-Oi hl r 'Pr pane PP
RESULTS
1
h:�
LDEC 0 9 1993
l U lu L=3
4 56
11-1
1-1
1-1
1-1
11-1
11-12
0.5
1,0
0.
0.
0.5
0.5
0.5
1®
0.5
0.5
.5
0.5
.5
1<.
0.
0.5
0.5
0.5
0.5
1;0
0.5
0e5
0,5
0.5
.5
1,0
0.
0.5`
0.5
`0.
1, 0
0. 5
0.
5
0.5
.5
1.0
0.5
0.5
0.5;
0.5
0.5
1,.
0.5
0.5
0,5
0.5
0.
1.0
0.5
0.5
.5
0.
0.5
1.0
0.5
0.5`
.5
0.5
0.5
1..0
0.5
0.5'
0.5
0.5`

Oxford Laboratonies, Inc. Analytical and Consulting Chemwits
ATE RECEIVED 11-11 93 1316 South FMh Street
DATE REPORTED 1 -07 Wilmington,N.C. 1
W 91l
Fax [phone]
P
HYDRO ANALYTICAL LABaRATORIES INC
4300 RAMADA DRIVE
SAMPLE DESCRIPTION: 4TH CREEK (5 'S id
1 1
.
. #4
5.
5.
Chloroform, PP
Bromochloromethane, PPB
1,1,1-Trichloroethane, PPS
1, 1-Si hl r Pr pone, PP
Carbon Tetrachloride, PPP
Benzene, PP
1,2-Dichloroethane, PPS
Trichloroethylene, PPB
Bromodichlaromethane, PPP
RESULTS
1
2
S
-5
92.3
15.5
.5
<0.5
2.55
.5
1.
.5
.5
.
.
.5
<1.
.5
.5
<0.5
.5
.5
.
.5
.5
.5
.5
.5
1.
.5
.5
.5
.5
.5
1<..
.5
.5
.5
0.5
.5
1
.5
.5
5
.5
.5
1.
0.5
.5
.5
.5
.5
1.0
.5
.5
.5
0.5
.5
2.65
0.5
.S
_.5
0.5`
.5
.5
.5
5
.5
0.5
1.
.5
0.5
.5'
.5

Oxford r ,es, Inc.
Analytical
and Consulting gists'
:DATE
RECEIVED11-11-93
1316 South
Fifth
Street
ATE
REPORTED
1 -Wilmington,
MC.
28401
9 5 917
(916) 76 -979
Fax (916) -9666
PAGE 3 Or 5
HYDRO ANALYTICAL LABORATORIES
INC
P.O. #
L93630
6300 R M,ADA DRIVE BOX C-I
CLPCN , NC 27012
ATTENTION: TERESA PERRY
SAMPLE DESCRIPTION: 4TH CREEK
( D
w
.
.
4,
5.
6. #6
;;.
RESULTS
1
2
3
4
5
Toluene,
1.0
•c -5
0.5
0.79
0.5
1, , -T i h n ne h n , PPS
. 5
1. 0
<.
C w 5
O. 5
. 5
Tet a hloro hen , PPS
1.
.5
.5
0.5
.5
, -Dl hl rn n a.n PP
9.5
1-0
0.5
.5
.5
.5
Cih n n hl o ha.n , PP
C. 5
.
. 5
. 5
C, 5
. 5'
Chl roben , PP
9. 5
1
. 5
. 5
Q . 5
. 5
hylhnan:, PP
. 5
1,
. 5
-. 5
. 5
Total Xylenes, PPS
.5
1..
.5
.5
_.5
.5
Styrene, PPP
.5
1.
.5
0.5
.5
0.5
Isopropylbenzene, PPS
. 5
1
0. 5
i. 5
:. 5
Q. 5
oo, PPS
. 5
1.
5
. 5
5
,. 5
1, , , -i..a hloroetha , PPS
. 5
1:... W:
.
. 5
0. 5.
< . 5

Oxford Laboratories, Inc.
Analytical and Consulting Chemists
DATE
RECEIVED
11-11 3
1316South
Fifth Street
DATA
REPORTED
12-53
Wilmington, .. 28401
Fax ()343-9688
PAGE 4 CP
HYDRO ANALYTICAL BC C 3
INC
P.O. L93620
6300 RAMADA DRIVE BOX C-2
CLEMMONS, NC 27012
ATTENTION: TERESA PERRY
SAMPLE DESCRIPTION: 4TH CREEK
(62
1.
2.
3.
4
.
6.` 6
RESULTS
I
2
3
4
5 6
1, 2, r , PPB
< . 5
<I .. 0
< . 5
< . 5
n-Propyl. , PPB
< . 5
<1..
<0.
< - 5 < .5
Bromoberizene:. PPS
<.5
<1._
.5
.5
<.5 <.5
1,3,5-Tri ethyl nzen , PPB
< ..5
<1.
.5
.5
< .5 < .5
C lo, lu n , PPS
< .5
<1
<0.
< .5
<0.5 < .
P-Chlorotoluene, PPB
< .5
<1.
.5
< .
< .5 < .5
tert-Butylbenzene, PPS
< , 5
<1._
. 5
.0. 5
<0,5 < .
1. 2 - Trimet i 1. na, P
. 5
1.
C. 5
. 5
5 . 5'
sec Butyl ben , PPB
< . 5
<1
. 5
< . 5
0.80 <0 . 5
p-Isopropyltoluene, PPS
< .5
<1.
< .5
< .5
0.62 < .5
1. -O u l nzen , PPS
( . 42
), <1.
<0. 5
< . 5
< .. 5 < . 5
n - utylbe zen , PPP
< . 5
<1
< . 5
< . 5
3.27 <0 . 5

Water/Wastewater Treatment Plants
tt 704-878-3438
t a t Its t1i I te
M. i5ax tatesuille. Xvrt4 (tarolma 2flfi77 w. c. nm-r. 07 NATTItA4.
RESGUIRCEIi !'\�)
co-pvqt,�Nrry DEN r RECEIVE
January 19, 1993 FEB 0 1 1993 JAN 25 1993 D
OM W syKWUM4 1ADURtS AY_,�UWVArit
N.C. Division of Environmental Managemen4t moubmAl t WWW1 REWU 90
Water Quality Section
Facility Assessment Unit
P.O. Box 27687
Raleigh, NC 27611-7687
Re: Permit Number WQ0001759
Fourth Creek WWTP Sludge LandfiR
Sludge Applied from December 1, 1991
Through November 30, 1992
Dear Sirs:
Complying with Section 21, Chapter 143 of the statutes of the State of North Carolina,
we submit the following:
Dry Tons Applied
Statesville Water Purification Plant
156.6 Dry Tons Applied
Fourth Creek WWTP
1201.3 Dry Tons Applied
Total Dry Tons Applied 1,347.9

WQ0001759 Annual Report
Page 2
Cubic Footage Applied
Statesville Water Purification Plant
8,400 Cubic Feet Applied
Fourth Creek WWTP
144,360 Cubic Feet Applied
Total Cubic Feet Applied 152,760
It should be not that the amount of Cubic Feet reported exceeds the annual application
to of 95,000 Cubic Feet per Year specified in the permit. This did not overfill the permitted
site.
The Fourth Creek WWTP has always been over -loaded with solids. With the acceptance
of the plant expansion in 1990, solids handling gained until the accelerated wasting schedule
loaded the digester to the point that reducing volume through supernating of liquid after
settling the solids in the digester became impossible. This virtually eliminated our ability to
cope with rising MLSS in the aerators.
Had this condition continued, allparameters on the NPDES Permit would be in danger
of violation, particularly Total Suspended Residue and F:oliform. It was becoming
extremely difficult to maintain compliance, and a distinct possibility existed that the conditions
before the plant expansion would return.
Beginning in May, 1992 we he an accelerated - dewatering schedule with 224 hour
operation of the der Grin equipment to remove excess solids from the digester and allow for
further loading the digester from Waste Activated Sludge (WAS). This resulted in an
accelerated use of the Landfill. Mechanical breakdowns often took days to repair, indicating on
the surface lost capacity instead of a gain in output.
The result was a reduction in MISS from a peak of 10,000 mg/L. to a low of 3,000
mg/L. (from July, 1992 to October, 1992). Our goal is to maintain 3,000 to 4,000 mg/L. during
winter months, and somewhat less during the warm months, to maintain effective treatment and
control MLSS.

Page WQ0001759 Annual Report
Phasing Out Monofill Operations
The -Viro Compost Facility is under construction and is designed to pr u
marketable liming -fertilizing agnot, eliminating the need for disposal of sludge in landfill.
However, with this recent incidenceof high a of the landfill the is a riotpossibilityat
a small ire the permitted may be :n ore city owned land is available
adjacent to the Permitted space. We do not presently see the need for an increase in the
application volume Breit, but this will require study also. The main reason for this possibility
is the extremely wet weather that has hampered s' coon.
Once facility testing and product compliance is assured the operations at the Fourth Creek
Sludge Landfill will be completely phased out and the permit retired.
Should you have any questions about this report, contact Steven Lambert or myself at
7-7-337.
Sincerely,
L.F. "Joe" Hudson, Jr., Director,,
Water Wastewater Treatment
. Mooresville RegionalOffice
Steven Lambert
l_ /sl

P a
cl
HYDRO ANALYTICAL
LABORATORIES
CERTIFICATE F ANALYSIS
CLIENTT L F t
CITY OF
CLIENT NUMBER 1 800149
CITY OF STATESVILLE
NUMBERSAMPLE
RECEIVEDDATE
COLLECTEDm1/04/93
'. roly
DESCRIPTION
SLUDGE
,COMMENT
4TH
NAME
UNIT
RESULTSTEST
------a---.n.. ---ra w.mw. aw.w aw am:-----------w -..a..
a
UN
COPPED
4
NICKEL
mg/kg
.I
LEAD
mg/kg
39.9
ZINC
mg/kg
SOLIDS
stilt/
ro
:

ITord Laboraton'es,Analytical and Consulting Chemists
DATE RECEIVED 11-12-92 13,16 South Fifth Street
DATE REPORTED 12-04-92 Wilmington, NX. 28401
92W2572 [phone]
PAGE 1 OF 4
HYDRO ANALYTICAL LABORATORIES INC P.O. # L92143
6300 RAMADA DRIVE BOX C-2 DEC 0 IJ-432
CLEMMONS, NC 27012 b,
L�Tn _QW-2-1 0. -U�
ATTENTION: TERESA PERRY ......................... rZA
SAMPLE DESCRIPTION: 33466 (TCLP)
1. RESULTS FOR THIS SAMPLE
2. OXFORD LABORATORIES ROUTINE DETECTION LIMIT
3. NORTH CAROLINA LANDFILL MAXIMUM
4. EPA MAXIMUM CONTAMINANT LEVEL
RESULTS
1 2 3 4
RESULTS ON TCLP BA AT
pH @ 5% Sample
Extraction Fluid Used
Arsenic, as As. mg/1
Barium, as Ba, mg/1
Cadmium, as Cd, mg/1
Chromium, as Cr, mg/1
Lead, as Pb, mg/11"
Mercury. as Hq. mg/1
Selenium, as Se, mq/1
Silver. as Ag, mg/1
9 . 2
#1
�BDL
0.005
0.5
5.0
.460
0.020
10.0
100.0
. 028
0.005
0.1
1.0
.020
0.010
0.5
5.0
BB L
0.010
0.5
5.0
BDL
0.0005
0.02
0.2
BDL
0.005
0.10
1.0
SOL
0.010
0.50
5.0

mr
ord Laboratories, 111C.
F
Analytical and
Consulting Chemists
P
1316 South FIfth Street
DATE
RECEIVED
11-12-92
Wilinington, N.C763-9793. 28401
DATE
REPORTED
12-04-92
92W2572
(91)
9
PAGE 2 OF
4
HYDRO ANALYTICAL LABORATORIES
INC
P.O. #
L92143
6300 RAMADA DRIVE BOX C-2
CLEMMONS, NO 27012
ATTENTION: TERESA PERRY
SAMPLE DESCRIPTION: TCLP)
1. RESULTS FOR THIS SAMPLE
2. OXFORD LABORATORIES ROUTINE DETECTION LIMIT
3. NORTH CAROLINA LANDFILL MAXIMUM
4. EPA MAXIMUM CONTAMINANT LEVEL
RESULTS
1
2
3
4
RESULTS ON TCLP LEACHATE
Vinyl Chloride, mg/1
BDL
0.020
0.02
0.2
1,1-Dichloroethylene, mg/1
BDL
0.020
0.07
0.7
Chloroform, mg /l
BDL
0.020
0.60
6.0
1,2-Dichloroethane, mg/1
BDL
0.020
0.05
0.5
Carbon Tetrachloride, mg/l
BDL
0.020
0.05
0.5
Methyl Ethyl Ketone, mg
BEL
0.50
20.0
200.0
Trichloroethylene, mg/1
BDL
0.020
0.05
0.5
Benzene, mg/1
BDL
0.020
0.,05
0.5
Tetrachloroe thylene, mg/l
BDL
0.020
0.07
0.7
Chlorobenzene, mg/1
BDL
0.020
10.0
100.0
1.4-Dichlorobenzene, mg/1
BDL
0.020
0.75
7.5
Hexachloroethane, mg/1
BDL
0.001
0.30
3�0

F'ord Laboratories, Inc. Analytical and Consulting Chemists
DATE RECEIVED 11-12-92 1316 South Fifth Stivet
DATE REPORTED 12-04-92 Wilmington, N.C. 28401
92W2572 [phone]
PAGE 3 OF 4
HYDRO ANALYTICAL LABORATORIES INC P.O. # L92143
6300 RAMADA DRIVE BOX C-2
CLEMMONE, NO 27012
ATTENTION: TERESA PERRY
SAMPLE DESCRIPTION: 33466 (TCLP)
1. RESULTS FOR THIS SAMPLE
2. OXFORD LABORATORIES ROUTINE DETECTION LIMIT
3. NORTH CAROLINA LANDFILL MAXIMUM
4. EPA MAXIMUM CONTAMINANT LEVEL
RESULTS
1 2 3 4
RESULTS ON TCLP LEA 'HAT
Nitrobenzene, mg/1
Hexachlorob titadiene, mg/1
2.4-Dinitrotoluene, mg/1
Hexachlorobenzene, mg/1
Lin dane, mg/1
Heptachlor, mg/1
Heptachlor Epoxide. mg/1
Chlordane, mg/1
Endrin, mg/1
Methoxychlor, mg/1
Toxaphene, mg/1
2,4-D, mg/1
BUD
0.010
0.20
2.0
BDL
0.001
0.05
0.5
BDL
0.003
0.013
0.13
BDL
0.0002
0.013
0.13
BDL
0.0002
0.04
O40
BDL
0.0002
0.0008
0.008
BDL
0.0002
0.0008
0.008
BDL
0.0007
0.003
0.03
BDL
0.0004
0.002
0.02
BDL
0.004
10
10.0
BDL
0.01
0.05
0.5
EDL
0.10
1.0
10.0

JoFrdL—abora—tornies,
lyti and Consulting Chemists
q�q 1316 South Fifth Street
CRATE RECEIVED 11-12-92
HYDRO ANALYTICAL LABORATORIES INC P.O. # L92143
6300 RAMADA DRIVE BOX -2
CLEMMONS. NC 21
ATTENTION: TERESA PERRY
SAMPLE DESCRIPTION: 33466 (T LP
1. RESULTS FOR THIS SAMPLE
2. OXFORD LABORATORIES ROUTINE DETECTION LIMIT
3. NORTH CAROLINA LANDFILL MAXIMUM
4. EPA MAXIMUM CONTAMINANT LEVEL
RESULTS
1 2 3 4
RESULTS ON TCLP LEACHATE
2,4,5-T' 1 iI 1> /1
Pentachlorophenol, mg/1
, 4, T it h nol, /
2,4, -T i I ° enol, /1
0-cresol, /
m-Cresol, /
P-Cresol, /
Pyridine, /
"BDL = BELOW DETECTION LIMIT'
DL
0.02
0.10
1.0
PCAI,
0.05 5
10.0
. 0 9 .
L
0.05
40.0
. 0
DL
0.05
0.202.
BDL
1.0
29
200.0
L
1
20
2 9.
L
0.50
.
':�e xfC1-'Z0';"
BRUCE A. BABSON, CHEMIST

Tt-tv laf
704-078-3430
n
RECEIVED
UNjj
N.C. Division of Environmental Management
Water Quality Section
Facility Ass+ ssm nt Unit
P.O. Box 22687
RAL
Raleigh, C 7611-77 vsn
r° t rn
u
Permit Number WQ0001759
Fourth Crash W WWTP Sludge Landfill
Sludge Applied from December 1, 1990 "1" 11 'Ai
Through November 31, 1991 tt iR11 REGIF J l Olt U
Dear Sirs;
Complying with Section 21, Chapter 143 of the statutes of the State of North Carolina
and conditions set forth in this permit, we submit the following:
Sludge from City of Statesville
Alum Sludge Facility
,
161.3 Dry Ton
,7 Cubic Feet
Sludge from City of Statesville
Fourth Creep WWTP
784.5 Dry Tons
67,560 Cubic Feet
Total Sludge Applied
945.8 Dry Tons
7777 Cubic Feet

ppppppp
Annual Sludge Report Page
Should you require further information contact t rp Steven Lambert or Myself at
-7-7
Sincerely,
L.F. "Joe," Hudson, Jr., Director,
Water/Wastewater Treatment

9 j'
ry w . �,
ACA `, . t ,
N. C. Division of Environmental ManagementWater
Quality Section
Facility Assessment Unit
Box 22687
.
�ok,KAt
Raleigh, NC 27 6 11 17`
Dear 3i.s's
In accordance with Section 21, Chapter 143 andPermit
o. WQ0001759, we submit thisat for 11 d Municipal
Sludge at the FourthCreek . .' . .
This is for the' twelve month permed from December
1
19819, through November 30, 1990.
Sludge Volume and Weight
39,512 Cubic Feet
76.7 Dry Tons
Should h information required please
contact
us at 704-878-3438.
Sincerely,
s
L. F. "Joe" uds , Jr., i recto
Water/Wastewater Treatment
LFli

N.C. Div. fEnvironmental Managewent
,,
NATO
Water Quality Section
A,
Facility As e stri ni Unit
,f19
Raleigh, N.C. 27 1. L-7 87
Subject. F "urth Creek Municipal Sludge Landfill
�
Permit No. WQ0001759
DearSirs:
Please e findenclosed two copies f the TCLP
and Heavy
Metal Analyses for the Fourth Creek Sludge Landfill,
Permit
No.WQ0001759. This is for the one year period
ending
Dec. :3I, Its._
Our hater Plant's alum sludge is buried at
this landfill.
The approximate ratio is 1. part alum sludge to 2
parts
Fourth Creek Sludge. Therefore, sludge analyses
are conducted
n a sludae cake f this ratio.
If T can be of further assistance, please call
at
704-878-3438.
inc.erely,
,
L.F. "Joe" Hudson, Jr., Director
Water/Wastewater Treatment
FF1/ .f
yL
cc: Carol Rogers

n
ANALYTICAL TESTING & CONSULTING SERVICES
PD. BOX 3148# CHARLOTTE, No NIT * TREPKAE (70) 5 7-4153 i F [phone]
City of Statesville Ion
Attn: Carol Waunh
P.O. Box 1111
Statesville, NC 28677
Dear, MS. KJAUG10.
Below are results of analysis of I sample received r examination
r1 November . I LA
Customer sa ITYST T
Phone Number: : [phone]
LAB I.D. 4Bold ID
Number 247`1 Bold
Customer Number
604
Submittal Date: 11/06/90
Submittal Time;
1 r. 1
-------------------------------------------------------------------------
TE T
UNITS
TEST
DETECTION
PARAMETER
RESULT
LIMIT
------------------------------------------------------------------------
SEN I C, LEACHABLE
mTr /L
& 01 x.
.005
BARIUM. LEACHABLE
ma/L
& 3
..a.
CADMIUM, LEACHABLE
mq/L
0.09
CHROMIUM, LEACHABLE
mQ/L
0.06
UEPO, LEACHABLE
Tarn
0.08
21
.021
MERCURY. RY. LEACHABLE
mo/L
{ off. o v a
SELENIUM, LEACHABLE
r L.
t. o
.005
ZINC, LEnCHPBLE
malL
1.63
. 0
NICKEL. LEACHABLE
30 / L
1.92
.02
TCLP EXTRACTION
don
Lu1 a. om000 ent araa1 v s w :
LEACHABLE VOLATILE
ORGANICS
IC
CARBON TETRACHLORIDE
un/L
Not Det
t.
HL OROB NZEN
un/L
Not Lear
CHLOROFORM
,fir1/L.:
Not Det
t
1, , DIC.. LOROBE° ZE N
un/L
Not Det
I
1,2—ICO LC FtOETHANE
ua/L
Not D t
t:
1, 1-DI HMETHYL L��RO HE
un/L.,�
Not De
1
^CI
TETRACHLORDETHENE
aTt L .
Not De
t,
T IC HL_OPOET ° ENE
Not Ix C:
I
VINYL CHLORIDE Of IE
u n L
1
t.
Multicamponent analysis: LEACHABLE ACID E` TRe" C TABLE
O—CRESOL u n / L Not Let L e"1

f "' 0 r ;'4 1'
ANALYTICAL TESTING CONSULTING SERVICES
City of St ate i�P4%bkxuw - cHARLoTrE, Nc MI TELEPHONE [phone] *FAX: [phone]"
Pa q e : 2'
December 2(�:'. 1990
LEACHABLE ACID EXTRACT ABLES (continued)a
M-CRESOL
un/L
Not
Det
1
F—CRESOL,
u rl / L".
r"l 0 t
D e t
I �Zl
PENT ACHLOROPHEN01-
url/L
Not
Det
its,
2, 4, 5-TR I CHLOROPHENOL
u, q / L
N ot
Deb
I
R4. 6-TRICHLOROPHENOL
un /L
t-4 o t
P, (.t
Ml-kltiCOMPOTient analvCis-
LEAC[if-ISLE BnSE'-- NEUTR()L-S
2.4-DINITROTOLUENE
ijn/l-
Not
Det
HEXACHLOROPENZENE
urcl/L
Not
Dot
10
HEXACHUOROBUTADIENE
ttn/L
Not
Det
I-
HEXACHLOROETHnNE
u q L
Not
Det
10
NITROBENZENE
Not
Det
10
PYRIDINE
u n L
Not
Det
I
Multicomn-onent anzil,)sis:
LEf"ICHABLE PESTICIDES
CHLORDANE
uq/L
Not
Det
10
ENDRIN
I.( a / L
Not
1) c' t
I 14"j
HEPTOCHLOR
tk q / L
Not
Det
I
HEPITOCHLOR EPDXIDE
u a / I-
Not
Drt
I
LINDANE
uq/L
Not
Det
10
METHOXYCHLOR
u a / L
N in- t
1) et
II ZI
TOXAPHENE
s-t n / L
Not
ID
I Till
MulticompoTaft ent analv`iis:
LEACHABLE IdERBICIDES
2,4-1)
u. rl / L
Not
Det
1
2. 4, 5-TP (SILVEX)
utn/L
N o t
D c' t
1
ARSENIC, TOTAL
til rl / k 11
G'. 190
Q). 011711
SELENIUM. TOTnL
M n / k t3
Q1.
I'll 0 1
BARIUM, TOTAL
MCI I k q
12.5
LEAD, TOTAL
m u/ k ri
4.45
�21. i:'1t2
MERCURY, TOTAL
In q / kri
0. 167
(111. t?)OLI--"
SILVER. TOTAL
ir u / ka
17,1. 25
11). Q) 2
CADMIUM, TOTAL
M rl / kn
8. 25
Cf. 02,
CHROMIUM. TOTAL
M u / ka
31.25
Q). I'll-12
Comm nt
ALREADY BILLEn FOR TCLV1
AND L-EnCHABI-E [YIETALS
INVOICE # 1006/6634
VAL; KCR
VA,L:(3WB
449 SPRINGBROOK
ROAD CHAf3LOTTE, NO 28217

. .,,mum,
Oil Lab
ANALYTICAL TESTING CONSULTING SERVICES
City Of St ate : CHARLOTTE, *TELEPHONE (7 ) 5274183 *FAX, �704)525-0409
Please advioie should You have questions nc rninQ these dat,,%
Respectfull,v skjbmjtte(j.
Grady W. Burnin
Laboratory Manamer
449 SPRINGSPRINGBROOK ROADo CHARLOTTE, NC 28217

,Bold Research Lais',,,
I
ANALYTICAL TESTING & CONSULTING SERVICES
PC, BOX 31486 - CHARLOTTE, NC 28231 * TELEPHONE [phone] * FAX: [phone]
December 26. 1990
City of Statesville
10
Attna Carol Waunh
P.O. Box 1111
Statesville, NEC 28677
Dear MS. WAUGH:
Below are results of analysis
of I samDle received for examination
on November 6. 1990:
Customer Code: CITYSTAT
Phone Number:
[phone]
LAB I.D. PA02044 Bold ID
Number 247F1
Bold Customer Number
60811-
Submittal Date; 11/06/90
Submittal Timet 10:19
Customer Samole I.D#: 4TH
SLUDGE
-------------------------------------------------------------------------
TEST
UNITS
TEST
ESE TECTIO19
PARAMETER
-------------------------------------------------------------------------
RESULT
LIMIT'
ARSENIC, LEACHABLE
mn/L
0.017
.005
BARIUM. LEACHABLE
ma/L
0.3
CADMIUM. LEACHABLE
mp/L
0.09
CHROMIUM, LEACHABLE
M&L
0.06
.02
LEAD, UEACHABLE
mq/L
0.08
.02
MERCURY. LEACHABLE
ma/L
< 0.002
0.0027C'
SELENIUM, LEACHABLE
mq/L
< .005
.005
SILVER. LEACHABLE
mn/L
0.02
.021
ZINC, LEACHABLE
mq/L
1.63
.02
NICKEL, LEACHABUE
ma/L
1.92
TCLP EXTRACTION
on
Multicomponent analvsis:
LEACHABLE VOLATILE ORGANICS
BENZENE
Un/L
2
CARBON TETRACHLORTDr---
un/L
Not Det
CHLORODER ZENE
un/L
Not Detti
CHLOROFORM
un/L
Not BetE.
1,4-DICHLOROBENZENE
uQ/L
Not Det1.
1,2-DICHLOPOE1 HANE
ua/L
Not Drys
1,1-DICHLOROETHENE
up/L
Not Det
I
METHYL ETHYL KETONE,
un/L.
24
1
TETRACHLOROETHENE
ua/L
Mot Det
I
TRICHLOROETHENE
un/L
Not Dot
1,
t)INYL CHLORIDE
un/L
17
1
Multicomponent analysis:
LEACHABLE ACID EXTRACTABLES
O-CRESOL
Un/L
Not Det
449 SPRINGBROOK
ROAD *
CHARLOTTE, NC 28217

Labs
I
ANALYTICAL TESTING & CONSULTING SERVIOES
CitV Of St ate TP,0jBbA 34486 -CHARLOTTE, NO blil m TELEPHONE J7041527-41a3 #FAX (70425-0"
Paqe: 2
December 26, 1990
LEACHABLE ACID EXTRACTABLES (CMITItinued)
M—GRESOL
Ij L'I I.w
Not
Det
1
P—CRESOL
Not
Det
1
PENTACHLOROPHENOL
L
N o t
Det
I
2, 4, 5—TRICHL.0R0r-',llEN0I_
uQ/L
Not
I,,) e t
10
2, 4. 6—TRICHLOROPFIENOL
1,i ii /L
N n t
Dot
1, %.yj
Mull: a` analysis.,
LEFICVAF-�LE BA,- E NEUTRALS
J_ 4—D I N I T ROTOLUENE-
u L
Not
Det
HEXRCHLOROBENZENE
url/L
Not
Dot
HE X ACHLOROBUTAD T ENF".
s_t rl / I".
N o, t
D t
HEXRCIALOROETHANE
u q L
Not
Det
NITROBENZENE
Not
D e t..
PYRIDINE
Not
Det
M u I t i r o m n- a n e n t a n a I v s i s
L EACI 4,0, S LE F" E 5 T I C T U, E E'
CHLORDANE
k,ArITL
Not
Det
CAI
ENDRIN
u rt / L_
riot
Det
HEPTOCHLOR
up/L
Not
Det
HEPTOCHLOR EPDXIDE
un/L
Not
Det
LINDANE
tk Q / L
Not
Det
10
METHOXYCHLOR
un/L
Not
Det
10
TOXAPHENE
u q / L
Not
De t
1
M"Iticomponent aTlc,11.VliS.'
L.Ef-)ICIABLE HERBICIDES
2,4—D
uq/L
Not
Det
I
2. 4, 5—TP (S I L Q E X 1.
u n / L
Not
Det
1
ARSENIC, TOTAL,
PI cI / ka
cl I 19 171
c1l. C1121 I
�ELENIUII. TOTAL.
mu/ku
0 0 1
10ri rll.10„711'
BARIUM, TOTAL
mri/krl
12.5
0. 1
LEAD� TOTAL
m ri / kn
4. 45
0. o2l'
MERCURY, TOTAL.
M Ll / k rl
1. I G 7
0. 01"I'llf-ill
SILVER. TOTAL
ir, a / k n
0.25
(A. 02
CADMIUM, TOTAL
MCl/lin
8.25
Q1. 1712
CHROMIUM. TOTAL
Mn/ku
3 1. ,...5
Q). 02
Comments:
------------------
ALREADY BTL.LED FOR TCLP
AND LEAf.,Hs',llL1LE METAL.S
I VOICT EE 1006/6684
VAL-P',CR
VAL:GWB
449 SPRINGBROOK ROAD * CHARLOTTE, NC 28217

t ,.z
ANALYTICAL TESTING k Ci NSU TWI ERVt
v of St at e t *CHARLOTTE, NO 2M * T LEPF ONE (7 ) 527- 183 » rAX €704) 525=0409
Pane: ,,
Please advise should you have auestions concerninq these data
Respectfullv submitted,
Grady R Burnin
Laboratory Mananer
9 SP
RINGBROOK ROAD CHARLOTTE:, NC 28217

m
�r
Waterigastmattr 01 rtatturnt Plants
704-878-3430
etattsuffit
December 14, 1988
r. J. Wells
Mooresville Regional~ Office
D.E.M.
P. 0. Box g`
Mooresville_, NC 28115
Subject: Fourth Creek Municipal Sludge Landfill. g -R2
Dear Sir:
In accordance with Section No. 21, Chapter I., please find
attached the required sludge analyses including EP Toxicity
and Heavy Metal concentrations for the Fourth: Creek ;Mudge
Landfill., Permit -R2. This is for a one year period ending
Dece be° 31, 1988.
Also, please note, that our alum sludge from our Water Plate
was discharged into our sewer system and treated at the Fourth
Creep WWTP, with the subsequent mixed sludge cake being permitted
to be buried at this landfill:. we have a new Alum Sludge Facility
at our Water Plant that now treats the alum sludge with a palate
press. The resulting sludge cakes are being transported to
and buried at this same landfill The approximate ratio is I
part glum Sludge Cake to 2 parts "Fourth Creek Sludge Cake being
buried..
Please find attached the analyses for the Alum Sludge Cake..
If i can be of further assistance, please call me at 78-3 .
Sincerely,
,
Dennis Crowson Crab Supervisor
Water/Wastewater Treatment
Enclosure

C E R
PCOR
T I F I C A T E 0 F A N A L S
t�
O ------------
.-------- .---____—._-------- _—_TM—____--
SAMPLE ----------
EMS Laboratories, IncN.C.
baste Lab C rtb No. 00
EIS SAMPLE m 012011
4132 Pompano Street
N.C. Water Lab Cert. No. 37727
REPORT DATE , I2/08DS
Charlotte, N. Carolina 28216
S.C. Lab Cert. No. OOO 1
DATE RECEIVED * 11/'30/88
3 3-1R53
U.S. EPA id 11011E
DATE COMPLETE : 12/077EE
----------_-- REPORT TO ---_
____-___--____--___----- :,.-------
SILL TO ___-_--_--____-_--
DENNIS CRO SON
DENNIS CROWSON
CITY OF STATESVILLE
CITY OF STATESVILLE
S 70 EAST
P. 0. BOX 1111
P. D. BOX 1111r
STATESVILLE
NC 2E57
STATESVILLE NC
2377,
�3,
DESCRIPTIONW
_
4TN CREEK SLUDGE CAKE
DATE
ADDITIONAL ANALYSIS ON
SAMPLE R12310
TIME
P.O. NUMBER VERBAL
- -
_ w
TEST DESCRIPTION
METHOD
DATE ANAL
ANALYTE
RESULT
DET. LIMIT UNITS
ARSENIC, TOTAL ........... ....*,*.:
... ...'«m},.SU3 Ea- CEO
1 J`01/88 LE
ARSENIC, TOTAL ........M:.....
. 0.25
0.25 MC KC
INSTRUMENT ........
.*.m m.... : PE Z3030
BARIUM, TOTAL ..........................
BARIUM, TOTAL ...............
.**..*.*54046-7000
07«9
12`02/00 LC
1 m MG KC
INSTRUMENT ..........mm,,....,,
PE 3030
CADMIUM, TOTAL .m.#**W.. .m.
p,�4'7130
........e... ... �"t.m
12/ 5/D R
CADMIUM, TOTAL ..
......— : 1.49
0.25 MG/KG
INSTRUMENT «m.......
......... : PE 3030
CHROMIUM, TOTAL .. .......m..
— .................. SW846-71 0
12/05/88 LPS
CHROMIUM, TOTAL ...
— .*.>*... ; 23.1
0.75 MG/KG
INSTRUMENT ......*,............
PL 3030
COPPER, TOTAL*....tl***._b.*****
....... ***#wo*** , S 45-721D
12/01/88 LRS
COPPER, TOTAL ................
. 45*8
0.75 MC/ KG
INSTRUMENT m ..... « m ... r *". .. , *.* k PE 303O
LEAD, TOTAL ............ ......... ....m .* p 7p [{@
2/01/E
LEAD, TOTAL ..................
. 21.4
2.5 MG/KG
INSTRUMENT .............,........
, PE 3030
MERCURY, TOTAL IN LIQUID WASTE ... ..........— ..SUE40-7470
12/06/88 L3S
MERCURY,TOTAL ..mm.m...........
ND
O.25 MG/KG
INSTRUMENT e s Am *
k i t k 8 C R i....P a♦ t f d x E CO
Page 1of 2

EMS SAMPLE
i
TEST DESCRIPTIONMETHODCATS
ANALYSE
ANAL" TRESULT
-------------------------------------------------------------------------------------
CDFT. LIMIT
UNITS
E NICKEL, TOTAL . — , ...
NICKEL, TOTAL
_
.�. N55 5
12/06/88
L5
................
INSTRUMENT .........
I.
: 52,E
: PE SC C
0.25
icy KG
SELENIUM, TOTAL ..................... ..
SELENIUM, TOTAL:
; 1
/
.... .. � ®.. ,
INSTRUMENT ....................
.
: PE Z3030
0.25
MG/KG
SILVER TOTAL ..
SILVER, TOTAL
.
.... ... ...
INSTRUMENT ... ...............
7.26
: PE 3030
1.25
LAC
ZINC, TOTAL ..:.......... ..-. — ..............
ZINC, TOTAL
SW846-7950
12/06/88
LP
.. a ..... ,.. , .......
INSTRUMENT .... ...... ........
- 25.8
g : PE 3030
0.75
MIG/K
ACID DIGESTION IN S 'S, S FOR ANALYSIS BY
FAA OR ICPS1 5-SC5
11/30/88
MR
METALS, DIGEST .......... ....
INITIAL
COMPLETE
NA
N
WT OR VOL .. .... .....
2.01
FINAL WT OR VOL ...��..,......
50
ACID DIGESTION IN S'S/S FOR ANALYSIS BY
CFAA .. a..SN - C5C
11/30/88
MR
METALS DIGEST ................
INITIAL
COMPLETE'
NA
NA
NT OR VOL .. .... ....`.
2.0I
FINAL WT OR VOL ' ........ . . ...
t 5
NO - Not Detected
NA - Not 'Applicable
Sample was accompanied by chain of custody
papers
r
a
Approved by
�v
Page 2 of 2
.w

CERTIFICATE
OF ANALYSIS
--w--w CORRESPOND TO; ---------------____--w.-_-w_-_-------___-w-----_w__-
SAMPLE ----------
EMS Laboratories, Inc N.C.
Masts Lab Cert. No. 98
EMS .SAMPLE
P1331
4132 Pompano Street N.C.
Water Lab Cert. No. 37727
REPORT DATE
11/" 3/ 8
Charlotte, N. Carolina 28216 S.C.
Lat Cara. No. 99011
DATE RECEIVED
11/0/63
703 3-1653 U.S.
EPI id 0011I
DATE COMPLETE
11/22/83
--w..*---- -----w REPORT T ww-w_w__w_-__wwwww-ww-____-_wwan-____-www
BILL TO ------------------
DENNIS CRUNSON
TENNIS CROWSON
CITY UE STATESILLE
CITY OF STATESILLE
U S 70 EAST
P. U. BOX 1111
P. UW BOX 1111
STATSVILLE
NC 1`E677
x
STATESILLE NC, 28677
DESCRIPTION _
TH CREEK SLUDGE CAFE
[ATE . 11/8/88
_
1 iE W.
P.U. NUMBER w DC-4 SC
a�
--------------�.-.�w w, �w_w_
TEST DESCRIPTION
,� �____-.�ww--_
MEP1UU
DATE ANALYST
A ALYTE
--------------------------------------------------------------------------------------------
RESULT
UET. LIMIT
UNITS
ARSENIC, EXTRACT..W...t..........................SW8
ARSENIC, EXTRACT
6-7060
... . . ND
11/14/88
0.01._
Lt1S
MG/l
.. ....
4 INSTRUMENT ..................
. RE 23030
BARIUM, ,..,.. ..*aw wwW.
a s WW,..wS i�N6-7UEC
11/16f6
LES
.EXTRACT
BARIUM, EXTRACT
1.4
0W6
ttC/L
a,. ....
INSTRUMENT.... .................
PE 303
CAUMIUMt EXTRACT ............ .................
..SU646-713C
11/17/88
L11S
CADMIUM, EXTRACT
W 0.06
CWC1
MC/L
.............
INSTRUMENT ........ .........
. W PE 3030
CHROMIUM, EXTRACT ...ttw.... ........
.t.#Wt.*#...S 46-7190
I1/15/8
LCS
CHROMIUM, EXTRACT t ... W t ..
W t a
6.C3
MC I_
INSTRUMENT• a+. a a w a y a a a a a e
�g.1.3
�Py }
a r o.. x C 6� u�#; w l
CPPER,. EXTRACT eastern#6tt•s Wtt ea moresrta
ra.tu W W t .. SW 4C-1C
11/18
j
LR
S(
MC
COPPER, EXTRACT .... wertrrnr
t W 0.31
4J raJ'
4w
t
INSTRUMENT .. > ...........
� PE 3030
LEAD, EXTRACT ...tnrtnt.........erttrw.......—..S
46- 4 C
II 6
L S
LEAD, EXTRACT ....... ........
NC
0.1
MC/L
INSTRUMENT
PE 3030
.............>.......
1ERCUR" EXTRACT ............ SNC46— 470
11/16/88
MR
eret..re..e-tnr......*
MERCURY, EXTRACT ♦t.._nrn.tnr . NC
0.0005
MC/L
INSTRUMENT.....
PE SCC
......... W r
Page I of 2

EMS SAMPLE B12318
DESCRIPTION
METHOD DATE ANALYST
RESULT / ——__ _ —_ —_ �_� � _ NET. LIMIT UNIT
NICKEL, EXTRACT
• ................
NICKEL EXTRACT .
,,
...�...S 846-75
11'14R
LES
.. .:
INSTRUMENT .....r
PE GG
,
.G1
MG'L
SELENIUM, EXTRACT ..........
SELENIUM, EXTRACT
:'ND
PE GGSG
0.01INSTRUMENT...........
iG L
SILVER, EXTRACT r .•,.•µ. ___,--­­SW846-7760
SILVER,
II � GG
LGS
,EXTRACT ....r........r
INSTRUMENT•....•..•. r...,•.
m NN
R FE SGG
G.GS°GAL
ZING EXTRACT
................ •...
EXTRACT
k r ..:..SW €46-51
11 I/GG;
LGSINU,
INSTRUMENT ......
1.
PE GGG
. GG
r IG/L
EP TOXICITY EXTRACTION, WITHOUT ORGANICS
EP TOX E T,
........ -•S 84 —1 1G
1/1 88
MR
,G .. ..... .•...
TOT SAMPLE WEIGHT, G..........
aCOMPLETE
80,00
NA
N
SOLID PORTION, G ............
80.00
LIQUID PORTION, ML ...........
NA
.S MM SIEVE TEST .... ...... •_a
PASSED
INITIAL DI ADDED, ML. ...... , ..
1280
FINAL DI ACHED, ML • . , . .. , .:
• 320 ,
INITIAL PH
FINAL PM
PSI ADJUSTMENTS
.
. » ..
TOTAL ACID ACE, L.r .�...•
: NONE'
L EXTRACT FILTH ML... ..•.
1600
�
TOT VOL FILTRATE,EIS....<,......
; 1600
VOL EXTRACT ANAL, ML ..........
* 1
SPIKE SOLUTION', ML .r........
: I
ACID DIGESTION OF LEAGNATE FOR FAA OR ICP
METALS DIGESTION
— ..... S 846- G1G
11/10/88
MR
..W_.N# _ .
INITIAL VOL, ML ..............
COMPLETE
1600
NA
NA
FINAL VOL, ML ........ •
16,00
ACID DIGESTION OF LEAGIIATE FOR GFAA ......•..r.r•.SUG4G-
METALS DIGESTION
G G
11/10/88
MR
.• .•......... r
INITIAL VOL, ML — ........... ,
COMPLETE
1600
NA
FINAL VOL, 1L ,...•.......... .
1600
N - Not Detected
N - NotApplicable
m #.
Sample was accompanied by chain of custody Ar
Approved by t)
Page
I

L
RO BOX 31486 CHARLOTTE, NC 28231 m TEI.EPHONE ,[704) 342-3496
LAB A S
7 MPLENO,(# 401A-1 DATE OF REPORT: 12/12/88
P.O. DATE RECEIVED- 12/09/88
RECEIVED FROM: CUSTOMER NO,: 6084
NAI ; Dennis Crowson TELEPHONE NO.: [phone]
ORG. CitY Of Statesville
ADD: U.S. 70 East Off Bell Road
P.O. Box 1111
Statesville, NC 28677
SAMPLEN Ot Filter Cake Alum Sludge
A-,
MARKED: A: E.P. Toxicity B,
C: D:
SAMPLE/TEST NO, A A-1 C: D:
ANALYSIS UNITS
J
TOTAL RESIDUE
TOTAL VOLATILE RESIDUE
TOTAL NONFILT RESIDUE
TOTAL DISSOLVED RESIDUE
COD
AMMONLA AS N
TOTAL _KJELDAHL NITROGEN
_�r�T4A_S _N _JT9 LW
TOTAL PHOSPHATE AS P
CHLORDE AS CI ir
61L & GREASE
..q�YANITOTAL
METALS UNIT'
ARSENIC
SELENIUM
P_
CA6MIU
(rng+ L
COPPER (M91)
tp
DEL
ZINC
MEACUSY
-BAD M
APPROVED BY: Jeffrey K. THam, Manager
' 303 NIFACHIAM ST, CHARLOTTE, NC 28203

abs
O BOX 3 486 # 04A LlT7E, NC 28231 0 TELEPHONE 17� 342•34--
EBoLlResearch Labs
i SAMPLE .(s): L 1 A— I DATE REPORT: I i 2� S
P.O. CEO.: DATE RECEIVED: 1 1% 15� S
RECEIVED FROM.UST C NO,: 6084
NAME-' E® DENNIS G. CROWSON TELEPHONE NO.: 7 - 3 4 38
ORG, CITY OF ` AT LLE/FO RTI CPS
ADD: U.S. 70 EAST OFF 13ELL ROAD. Y �
P.O. BOX 1111
SAMPLE(s) of. FILTER CAKE
E.P. TOXICITY
MARKED, A -ALUM SLUDGE PRESS CAKE B:
cr
co
SAMPLEJEST NO, 1 ;
__...
ANALYSIS UNITS
TOTAL AL RESIDUE
TOTAL 0. OLATILP RESIDUE
LEAD �mg!Q
33 m 'L
w. _
10—
MERCURYBARIUM
§-i —LV

�(IT
tt t t r Cat 'elan
704-078-3438
41,
*tUtCoUffir
00, Nax I I I I -t tr-quint. Dhirt4 Q'arohna7
February 1 1988
Mr... Jessie Wells
Mooresville Regional Office
Dept. of Environmental Management
P. 0. Box 950
Mooresville, 811
Dear, w ells
In compliance with Sec. 21, Chaster 143, we submit the following
data on sludge applied to the Third and Fourth Creek WWTP,
Sludge Landfills. This data is for: the period ending December
1_ , 1988.
1.. "third Creek Sludge Landfill_
Permit #13849;
1.81 . I Dry Tons
9,950 Cubic Tons
2. Fourth Creek Sludge Landfill'
Permit #8884P
{
211.5 -r ns
44,277 Cubic: Feet
If you have any questions, please call us.
Sincerel
,.' F. "' eit ud on, Director
Water Wastewater Treatment
s

r
�qy
aw
704-070-3430
40,
20677
Y
=s
t
Mr. J. Wells
Mooresville Regic,,tnal Office
DEM
Mooresville, NC 28115
15
Subjeett Fourth Creek Municipal Sludge Landfill
Deal", Mr. Wells:
ThaaH enclosed copies, ware sent .o F'al °igh 1.rs FrrAa°or'°. We have ce.,.a,;-e aed
our- a'° c u �� a�� d s . $„F., cc,,, r d i ri g l y to prevevA this %.". p.<.:.� m h af,.: p e rA. A nq ea g a i. n ..
*S r r°e4:°»ant jl
" r ini S G. Crcroson, Lab Supervisor
Watev-/Wastewater Treatment
y�
t,';' C/
&r°'a a

m Ifuttrignatexuater 01 reatnunt Plants
Tt'**t1j of
µ794-070-3430
t t t te
t m t t t t teat uilt . TNTarttl Crarolitut
January 12, 1988
Division of_ Health Services
State Laboratory of Public Heald
P. 0. Box 28047
Raleigh, NC 27611-8047
DearSir:
In accordance with Section No. 21, Chapter No. 143, please find
attached the required sludge analysis of E.P. Toxicity and Heavy
Metals for the Fourth Creek Municipal Sludge Landfill, Fermat
o. 6934-RZ, for the period ending December er 31, 1987.
If 1 can be of any assistance, please call rye at 70 876-3 37.
Sincerely,
}
Dennis Crowsoh,
ab Supervisor
Water/Wastewater"treatment
`a
Enclosure

DIRECT INQUIRIES TO :
FINAL REPORT
ON SAMPLE
86506 00
EMS LABORATORIES, INC.
DATE RECEIVED
: 12/02/87
DATE COMPLETE M
01/06/88
4132 POMPANO STREET
CHARLOTTE, N. CAROLINA 28216
DESCRIPTION 1
: 4TH
CREEK
SLUDGE CAKE
[phone]
DESCRIPTION 2
:
Q 1 n
DATE SAMPLED
TIME SAMPLED
N.,C. WASTE LAB CERT. O.
98
N.C. WATER LAB CERT. NO.
37727
/*
S.C. LAB CERT. NO. 99011
U.S. EPA 10 00118
BILL
TO
REPORT TO
c-
DENNIS CROWSON
DENNIS
CROWSON
c
CITY OF STATESVILLE
CITY
OF STATESVILLE
U S 70 EAST
P. 0.
BOX 1111
P. O. BOX lill
STATES
ILLS NC
28677
STATESVILLE NC
28677
TEST DESCRIPTION
RESULT
GET.
LIMIT UNITS
METHOD
ANALYST
DATE
ARSENIC, TOTAL .............................
0.70
0.25
MG/KG
EPA
206.2
MR
12/29/87
INSTRUMENT .........
PE 3030
GFAA
BARIUM, TOTAL ..................
62
12.5
MG/KG
EPA
208.1
MR
12/14/87
INSTRUMENT
PE 560
FAA
CADMIUM, TOTAL ....... .............
.........
1.5
0.25
MG/KG
EPA
213.1
MR
12/08/87
INSTRUMENT ....
-- PE 560
FAA
CHROMIUM, TOTAL .................
-- .......
11
0:25
MG/KG
EPA
218.1
MR
12/17/87
INSTRUMENT .........
: PE 560
FAA
LEAD, TOTAL,
...........
32
1.25
MG/KG
EPA
239.1
MR
12/07/87
INSTRUMENT
: PE 560
FAA
MERCURY, TOTAL . .....
.........
ND
0.25
MG/KG
EPA
245.1
MR
12/22/87
INSTRUMENT
: PE 360
CVAA
PAGE 1 OF 3

FINAL REPORT
ON SAMPLE NO.
: B6506
00
TEST DESCRIPTION
RESULT
DET. LIMIT
UNITS
METHOD
ANALYST
DATE
SELENIUM, TOTAL ... ....................
.........
0.84
0.25
MG/KG
EPA 270.2
MR
12/29/87
INSTRUMENT .........
: ZSG GFAA
SILVER, TOTAL .... .................
.......... —
30
0.25
MG/KG
EPA 272.1
MR
12/17/87
INSTRUMENT . ........
: RE 560 FAA
ARSENIC, EP EXTRACT ................
--- ......
ND
0.01
MG/L
SW846-7060
MR
01/05/88
BARIUM, EP EXTRACT ..........
................
ND
0.01
MG/L
SW846-7080
CG
12/18/87
CADMIUM, EP EXTRACT .............
............ ...
NO
0.01
MG/L
SW846-7130
MR
12/08/87
CHROMIUM, EP EXTRACT
...... ..... —
NO
0.01
MG/L
SW846-7190
MR
12/17/87
LEAD, EP EXTRACT
............
ND
0.05
MG/L
SW846-7420
MR
12/07/87
MERCURY, EP EXTRACT ..............
-- ...........
NO
0.0005
MG/L
SW846-7470
MR
12/22/87
SELENIUM, EP EXTRACT
ND
0.01
MG/L
SW846-7740
MR
12/29/87
SILVER, EP EXTRACT . .........................
— ...
NO
0.01
MG/L
SW846-7760
MR
12/17/87
EP TOXICITY EXTRACTION,
WITHOUT ORGANICS ..........
COMPLETE
NA
NA
SW846 1310
DH
12/03/87
TOT SAMPLE WEIGHT, G
100
SOLID PORTION, G —
a NA
LIQUID PORTION, ME
NA
9.5 mm SIEVE TEST
PASSED
INITIAL DI ADDED, ML
NA
FINAL DI ADDED, ML
NA
INITIAL PH
176
FINAL PH — ........
3.16
PH ADJUSTMENTS .....
ATTACHED
TOTAL ACID ADDED, ML
NA
VOL EXTRACT FILT, ML
TOT VOL FILTRATES,ML
VOL EXTRACT ANAL, ML
19
SPIKE SOLUTION, ML
1
METALS DIGESTION ........
COMPLETE
NA
NA
EPA 200pO
DH
12/03/87
INITIAL WT OR VOL
2.03 9
FINAL WT OR VOL ...
50
PAGE
2 OF
3
EMS

Ms. Tana Fryer
and �.�. Dept. of Natural Resources :,�&,
Community Development
P. 0.. Box .ram:+a,.
Mooresville, NC 28115-0950
Dear Tana;
In rrrspsa}"8se to your y,-rarequr..s."ts for additional information on sludge
di,ap,wx.,at. tonnage at the Fourth Creek WWTP, the following information K
submitted f o r your consideration; Annual Tonnage 1987 (actual): 753 tons
Average per cent solids: 22%
Annual Tonnage ge Dry Weight Equivalent; 166 tons
We have adios:"@ the laboratory oftheir failure to report all tha
parameters t er s in the analysis of sludge sc:$ta'aples for 19BE, a:r7'"8a: thmse will be
reported in the 19B7 analysis.
I. r any further information is required please let us know.
Sincerely, ;.
i�
Harold L.'Fulpl'-Kreator
s w��
Water/Wastewater Treatment
F .F .ar A rai an
�. (. Nox 1111 • %datitty Narf Carolina U677 • 7114- 7 -2121

{ M x
OfceP
y mo
a'
V�
Division of Health Set -vices
State Laboratory oPublic Health
Raleigh, NC 27611-8047
ar~ S L
In accordance with Section No. 21, ..i mi t No. 694""'R2,enclosed eta"e
the required sludge analysis for the Fourth Creek Municipal Sludge
Landfill for the period endingDecember 31 1986.
.
If arty furth r information is required please let rrr kn--_$ .
Sincerely,
el
Harold of L: l=c't1 4*1rCz t0 r•5
Water/Wastewater Treatment
ent
HLF/pds
n
cc; Mr. Richard Bridgertian, Mooresville
878-3438

EMS Laboratories, Inc.
REPORT DATE
12/w/db
DATE RECEIVED
413 POMPANO DRIVE
a
CHARLOTTE, NORTH CAROLINA 28216
EMS AMPLE #
1826
REPORT
(704) 3 2-627
NC Cart. #37727
P.C. #
DC 120386
SAMPLE TYPE
GRA
NUMBER
NC Cert. 49
____COMPOSITE
AMPLE SOURCES
WASTEWATER
DATE SAMPLE[)
12/03/86
4th Creek Drying Bed
SLUDGE __.COLLECTED
BY
ILL TO: City of Statesville„
OIL
REMARKS
4th Creek
Cake
P. C. Box 1111
No. 1904
Statesville, N. C. 28677
LEA HATE
ATTN: Mr. Dennis Crowson
B not r�
TEFL
X
this copy
PARAMETER
RESULTS
DATE ANALYZED
ANALYST
METHOD OF ANALYSIS CHARGE
Total Metals: (results reported
in rig/kg,
dry weight
Arsenic, As
18.1
12/8
DP
206.2
Cadmium, Cd
6.5
12/5
DM
213.1
Chromium, Cr
165..
12/5
DM
21.1
Lead,, Pb
235
12/5
DM
239.1
Selenium, Se
2.1
12/8
DM
270.
Mercury, Hg
1.1
12/8
DB
245.1
14 ��
Barium, Be
406.
12/8
DM
208.
°.
Silver, Ag
3.4
12/5
DM
272.1
B P Tox Metals: results reported
in mg/1 )
Arsenic, As
<D.DB
12/8
D'P
206.2
Cadmium, Cd
<0.01
12/4
DM
213.1
Chromium, ;Cr
0.05
12/4
DM
218.1
,P
Lead, Ph
<0.0512/5
DM
239.1
Selenium, Se
0.01
12/8
D
270.1
Mercury, ur°y, g
0.007
12/8
DB
245.1
Barium, Ba
0.08
12/8
DIM
208.2
Silver, Ag
<0.01
12/4
DM
272.1
$424.00
t
WED BY:
REPORT COPY
k