NC0006521_Regional Office Historical File Pre 2018

r
Michael F, Easley„ Governor
'i[iiern G Floss Jr,, Secretary
North Carolina Department of Environment and Natural Resources
Gregory J, Thorpe, Ph,D,
Acting Director
Drvision of Water Quality
GROUNDWATER SECTION
December 17, 2001
Mr. Rick Kilpatrick
Corporate III f EH S Manager
136 Patterson Road
P.O. Box 609
Kings Mountain, NC 28086
Reference: Non -Discharge Permit Number21181-0005
Dear Mr. Kilpatrick:
I have just received your letter of august 20, 2001 regarding your request to
discontinue semi-annual monitoring at the two equalization basin monitor wells i - I
and MW- located at Spectrum's facility in Belmont, North Carolina. We believe that
this permit is associated with NPDES Permit Number NCO006512 1, issued to the facility's
wastev,rater treatment plant. It is our understanding that the equalization basin which has
been monitored by these wells for more than ten years is no longer being used and that
there are no plans to use it in the future. The most recent monitoring data has shown no
concentrations of concern for the constituents reported.
In view of these conditions, the Groundwater Section re onluiends that
monitoring be discontinued at both wells, and that monitor well M'4 -1 be abandoned
using the procedures and requirements outlined under 15A NCAC 2C .0113. Monitor
well MW-2 should be temporarily abandoned by securing the wellhead to prevent access
by hand.
If you have any questions, please contact ire at 1) 715-6160,
Sincerely,
Debra J. Watts
Supervisor, Pe its & Compliance Unit
"c. Matt Feller, MRO
Peggy Finley, MR
Kim Colson, DWG
X XN*
I MN
Customer Service Division of Water Quality t Groundwater Section 1
1 800 23-7748 1636 Mail Service Center Raleigh, NC 27699.1 36
Phone (919) 73:3.3221 Fax: (919) 71"33 Internet: httpJ/gw,ehnr,state,nc.us

F-
Spectrum Dyed Yams
Subject: Spectrum Dyed Yarns
Date.- Thu, 13 Dec 2001 11.-41:03 -0500
From: Peggy Finley <Peggy Finley@ncmail,net>
Organization: NC DENR - Mooresville Regional Office
To- [e-mail]
Dave:
Spectrum submitted gw-59s for MW-1 and MVO- 2 for sampling conducted on
July 28 of this year, The results looked ON based on my review. This
disposal system is a stabilization lagoon and is under the Town of
Belmont's pretreatment program (hence the odd "permit" number). The
reason for the request to discontinue monitoring is that reportedly the
dyehouse is no longer used and the flow to the lagoon has been blocked
off.
The Gw incident relates to solvent contamination (TCH, PCB. They have a
natural attenuation CAP. I checked with Chuck Pippin about use of
these wells for that issue. MW-2 should not be abandoned. It may be
needed in the future for sampling but he does not foresee a need for
MW-1 so it could be abandoned.
Peggy Finley - [e-mail]
North Carolina Dept. of Environment & Natural Resources
Div. of Water Quality - Ground Water Section
919 N. Main St.
Mooresville, NC 28115
Ph- [phone] Fax: ('704) 663-6040
off 12/13/0111-.,41 AN1

MOORESVILLE REGIONAL OFFICE
GROUNDWATER SECTION
September 19, 2001
MEMOILANDUM
TO Debra Watts
FROM: Peggy Finley
THROUGH: Hiatt Heller � � � , rr 1�r
SUBJECT: Spectrum Dyed Yams
Pretreatment Facility
I1 1-000
Gaston Co.
As a follow-up to et ms request, this office has no objection to discontinuing the
groundwater monitoring for the pretreatment lagoon, Should you have any questions, please
contact nee,
')
MA F/watts.merxr

Re: Infomiation Request
Subject: Re: Information Request
Date: Fri, 20 Jul 2}Ell 09:30:32 -0400
From: Peggy Finley <[e-mail]>
Organization: NC DENR - Mooresville Regional Office
To: Rick Kilpatrick <[e-mail]>
Mr. Kilpatrick:
I would request that you sample one more time. In reviewing our file, I noticed
that the method used to test most recently for volatile organic compounds was
not an acceptable method. The following methods are acceptable provided that
the practical quantitation limit (PQL) is 0.5 micrograms per liter or less:
1. Standard method 6230D
2. Standard method 6210D
3. EPA Method 8021, Low Concentration
4EPA Method 8260, Low Concentration
When you submit all the sampling results, you should attach a formal request to
discontinue groundwater monitoring and send it to:
Debra Watts, Supervisor
Groundwater Permits & Compliance Unit
1636 Mail Service Center
Raleigh, NC 27699-1636
It you have additional questions, please contact me.
Peggy Finley
Rick Kilpatrick wrote:
> Ms. Finley,
> Spectrum Dyed Yarns is currently scaling back activities at our plant in
> Belmont, C. Spectrum purchased', and began operating this facility in March
> 1993. The previous owner of the facility was Piedmont Processing Company, a
> division of Dixie Yarns, Inc.
* This facility received an "Authorization to Construct" a 7,000,000 gallon
* flow equalization basin in November 1987 - the basin was completed soon
* after authorization was granted and has been in operation since.
* one of the requirements listed in the Authorization to Construct was the
* installation and sampling of two monitor wells. Since our purchase of the
* facility, we have completed sampling in March, July and November as
* required. Results of all sampling should be on file at the following
* address:
> NCDENR - DWQ
> Attn: Groundwater Section - Permits and Compliance Unit
> 1628 Mail Service Center
> Raleigh, NC 27699-1628
* Since the dye -house at the facility is no longer being operated and all flow
* through the basin is permanently suspended, do we need to continue the
* sampling of the two groundwater wells ? Since sampling is required in July,
* your response to this matter would be greatly appreciated.
• If you have any additional questions, please reply to this e-mail or contact
• me at 704 739-7401 e) 302.
of T120101 9:30 AM

Re: lafonuation Request
> Your assistance with this matter is greatly appreciated,
> Regards,
• Rick Kilpatrick
• Corporate HR / BH&S Manager
Peggy Finley - [e-mail]
North Carolina Dept. of Environment & Natural Resources
Div. of Water Quality - Ground Water Section
919 N, Main St.
Mooresville, NC 28115
Ph. [phone] Fax- [phone]
- ---------
----------
� inte � <re"—yT F �inl �,ncnia�ilnet>
NC TEE - Mooresville
Div. of Water Quality - Ground Water Section
2 of 2 7/20/019:30 AM

STATt
r
State of North Carolina
Department of Environment, Health, and Natural Resources
Mooresville Regional Office
James G. Martin, Govemor Albert F. Hilton, Regional Manager
William W Cobe54 Jr., Secretary
DIVISION OF ENVIRONMENTAL MANAGEMENT
December 5, 1991
Mr. William Burch
Dixie Yarns, Inc.
Post Office Box 1006
Belmont, North Carolina 28012
RE.* TOX Sampling
Piedmont Processing
Gaston County, NC
Dear M. Burch:
On December 3, 1991, the Groundwater Section of the
Mooresville Regional Office received the compliance monitoring
reports for the subject site. Please not the following analysis
changes:
Volatile organic compound analysis requires test method 6230D
"Standard methods for the Examination of Water and Wastewater"
or Method 502.2 "Methods for the Determination of Organic
compounds in Drinking Water". TOX is no longer acceptable.
If you have any questions regarding this matter, I may be
reached at 704/663-1699.
Sincerely,
V
Tony McManus
Hydrogel logical Technician
TLM/ds
919 North Main Street, Moorewille, N.C. 28115 0 Telephone [phone] & FAX 3®
An Equal Opportunity Affirmative, Action Employer

r .
r.
State of North Carolina
Department of a l Resources and CommunityeC e t
Division of Environmental Management
512 NorthSalisbury i , North Carolina 27611
Jantem G Martin, Covernor R. Paul Wilms
Thornas Rhodes, Secretary November 16 1987 Director
,k
Mr. Buddy Burch �
Piedmont Processing Company � �:. �,
44
P.O. Box 1006
Belmont, N.C. 28102
�
,
SUBJECT: Permit No. 1181-000-
Authorization to Coast'
Piedmont Processing Comp;rary
Pretreatment Par i lit ir,
Gaston County
Dear Mr. Burch:
letter of request for an Authorization to Construct was rocr�ived May 26, 1987,
by the Division and final plans and specifications for the. subbed project t have been
reviewed and found to be satisfactory. Authori art.ion is hor oby ra ntrrd for the
construction of ai tt. 90 MOP, wastewater pretreatment f€acility ad-dia ion ronsisting Of
1,000, 00-gallon flaw - equalization basin containing as mixer, n rate rs, fill sensors, and
temperature sensors; ar duplex pumping station with appro imatoly 420 linear feet of
1 -inch force main, an effluent measuring structure, piping, :,ind appurtenances to
serve Piedmont Processing in Gaston County.
This Authorization to Construct is is ued err acr0rcl3uC(' wit.l) tlae City of Belmont
Permit No. NCO00issued November 15, 1986, and shall be sobjoct to revocation unless
the wastewater treatment facilities are constructed in ~aCc0raEaauC(1 With the conditions
and limitations specified in Permit No. Ntv005.
e sludge generated from these treatment facilities must ho disposed of in
accordance with G. S. 143-215.1 and in a manner aPProvabl e by ill- North Carolina
ina
Division of Environmental Management.
The Mooresville Regional Office, telephone number 704/661- lA9 , shall be, notified
twenty-four 4 hours in advance of operation of the installod a;ys,t>nm so that an
in -place inspection can be tirade;. Such notificnt ;on.t the Re ionn] Supervisor %hall be
grade during normal office hours:,
In event the facilities fail to perform satisfactorily in mrrtin,g its permit
effluent limits, the pe.rmittee small take such immediate corrective act -ion as may be
required by this Division, including the construction of nddit ionnJ wnstewater
treatment and disposal facilities,
lak llut rr hr"hon Pays
PO Rm 27North Ca"ina 27611,7697 TSlwMw S
An Equal Oppwtunfry Affirmative Faye

FFPF-
Upon completion of construction out] prlo'l- t,0 OP01-11t i0t) Of t hi'' pQrM I L ted far-! I ity
a certificatiou must be received from a proross, iollal 011)"ifirr'l I ('I I i ry in thnt tit(-',
permitted facility has been installed in with It- -wil-1voll plans And
specifications.
Prior to beginning waste disposal operat, tons, two m(,Ill i t (it, wfI 1�
q caner 1
upgradient and one (1) downgradient, must be instAll0d 60 trreatr i t rrtgroundwater
quality. The location and construction details for these wo-Ils mlist be by approval of
the Mooresville Regional Office, from which a wel I coast ruci jor, pr,rmit. must be
obtained.
The monitor wells must be sampled Ini tin't ly ,after ccni.st rm-,i ion (and prior to
waste disposal operations) and thereafter evory Mni-ch, Jnly, nittl Novembor for the
following parameters:
COD P11
TDS TOC ,
Water Levels Chloride
TOX (In November Only) SO4
The measurement of water level must be, made prior If) Nnmpl htp, for the remaining
parameters.
The analytical methods used for TOX must be c-npnblr of (folocf in the, total of all,
halogenated organic compounds present at a concentrAtion of '1.0 parts per billion
(pleb} or greater. Any individual halogenated organic compoul)(i preqellt at a
concentration at or above the method detection limit flltl l mti,-,t bf, identified,
quantified and reported with the sampling results, All reslilt,; �hnll be sent to the
NX. Division of Environmental Management on Form GW-59 Womplitricl- Monitoring Report
Forml.
Any additional groundwater quality monitoring, n,,4 deemed twcossnry by tile
Division, shall be provided,
The wastewater equalization basin shall be fully lined witi, ,I In, mil hypalon
liner.
The elevation of the bottom of the basin shall not I I
measured from bench mark indicated op n approved ,lans). jo I ql,�q- tit, u 105 f t . has
The effluent from these facilities shall be adequntoly trant fd !it the City of
Belmontts treatment plant prior to discharge.
If you have any questions or need additional infortlint iowt, contact Mr, Gil
Vinzani, telephone number 919/733-5083, extension 178
Sincer ely,
R. Paul, Wilms
cc Gaston County Health Department
Mooresville Regional Supervisor
Frank B. Hicks & Associates

n in erls (qf!rqfication
as a duty registered Professional Engineer in
the State of Northaline, hereby certifythat construction of these permitted
facilities been completed in accordance with the approved plans d
specifications.
Signature RegistrationNumber_
Date

James 8, Hunt, Jr., Governor
Jonathan B. Rogues, Secretary
DIVISION OF ENVIRONMENTAL MANAGEMENT
October 31, 1995
Spectrum Dyed Yatri$o IfICOrporated
Pbst Office Boxr
NorthKings Mountain,
Attention:
a Rick
Kilpatrick
SubjectNotice of Regulatory Requirements
Piedmont Plant-
Incident W 9957'
Gaston County, N.C.
Dear Mr. Kilpatrick:
The Groundwater Section of the Mooresville Regional Office
( received your response to the Notice of Regulatory
Requirements ( on October 20, 1995, In particular, you
stated that Spectrum Dyed Yarns, Inc.does not use any of the
contaminants detected in 1 and MW-2 and that Dixie Yarns is
responsible or the cleanup of this site. At this time, your
response sufficiently Beets the requirements of the NORR dated
October 11, 1995. Karen Connell, of the MRO, will he provided
copy of your response and monitoring data: to facilitate the
cleanup of this site.
Should you have any questions, please call me at 7) 5
1, ext. 241.
Sincerely,
Steven Bogr7ad
Hydrogeological Technician
919 Garth Main Street, Moor oore llle, North Carolina 28115 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmanve Action Employer 5016 rec yde:jr" iT,. p eat -consumer paper

DIVISION OF ENVIRONMENTAL MANAGEMENT
GROUNDWATER SECTION
October 20, 1987
MEMORANDUM
TO: Arthur Mouberry
C";
THROUGH: Bob Cheek
FROM: Bill Reid
SUBJECT: Piedmont processing Company
Wastewater Equalization Basin
Gaston County
AC0006521/GW87125
(Gil Vinzani: DEM SERG Review Engineer)
The Groundwater Section has reviewed the subject permit
application and recommends issuance of the permit with the
following conditions:
(1) Prior to beginning waste disposal operations,
t.,Wn monitor wells, one (1) upgradient and
one (1) downgradient, must be installed to monitor
groundwater quality. The location and construction
details for these wells must be by approval of the
Mooresville Regional Office, from which a well
construction permit must be obtained.
(2) The monitor wells must be sampled initially after
construction (and prior to waste disposal operations)
and thereafter every March, July, and November for
the following parameters:
COD pH
TDB T.
Water Levels Chloride
TOX(In November only) so 4
The measurement of water level must be made prior to
sampling for the remaining parameters.
The analytical methods used for TO X must be
capable of detecting the total of all halogenated
organic compounds present at a concentration of
5.0 parts per billion (ppb) or greater. Any
individual halogenated organic compound present at
a concentration at or above the method detection
limit (MDL) must be identified, quantified and
reported with the sampling results.

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Aueust 20. 2001
Debra Watts, Supervisor
Groundwater Permits and Compliance Unit
16' )6 Mail Service Center
Raleigh, NC 27699-1636
Non-Dischar ge Permit # - 2.II 81-0005
GIs:. Warts:
Attached are the sample results fi-ora two equalization basin monitoring wells located at
Spectrum's facility in Belmont, NC. These results are being sear to you at the request of Peggy
Finley also with NCDENR,
Spectrum is no longer operating, the dyehouse at this plant and therefore the lagoon is no longer
being used, Based on this, we would like to discontinue the sari -annual monitorinc, of the two
wells, Ms. Finley stated you should review the data before a decision is made.
When, you review the results, please be aware that this faciliq, is currently operating under a
Corrective Action Plan and is listed as Groundwater Incident No, 09957 (Dixie Yarns / Piedmont
Facility)- °rlus contamination was identified in 19,83 following an Environmefltal Site
Ass essnietit ,
If you have any questions or need clarification of any data, please feet free to contact nre. I can
Inc reached at [phone] e. 302,
Regards,
/Rich Kilpat ck-
Corporate HR / EH&S Manager
enclosures
FL
-8TJH 2 0OR
CUSTOMER SERE J-
136 PATTERSON RD
11460 BROADWAY
800 828,2078 tSPIJM
P.0. Box 609
#4 EW YOHK, NY 10GIS
Fx, 704 739,4754
KINGS NITIN., INN 28086
212 391-8181
800 831-9343 (FILAMENT)
704 739, 740 a
Fa- 212 921.9139
FIJIM -104.322,1668
Fax: [phone]
:;rr rn
M --
CB
M
E5 (A --r,
M X
422 15m ST 541
161 PIEDMONT 37
30 SARNES RO,
P.0, BOX 1308
P.Q Box 1006
P,0, BOX IM
HICKORY NC 28603
BELNION"r. NC 280!12
NIAMON, NC 28752
828 322,1663
704 H 2 5,1614
8218 659-1904
Pax 828 322-166B
Fav 704 826,4477
Fare: 828 6559 2337

Pace -knaly-fical
Field Data Sheet
well samplina
otio. r0t ec
Client., S j Lcan85
L-J?Q kQ S1
well Inforinauon:
Wt-11 ID:
Locked- no
J Ge)
Well Diameter
Stec! Stainless st-.el
Total Wtll Deuth:
fc ct Mu2ti Factor*: _ 0, 'Radius '12)-' x 3.14 x 7,18]
jj�j[
Stauc ',,Vatt-7 Le-vel: t
fe I- t Caslnqy Volume! gr a 1,
He i gin T of ''a t er C c I 1�t- 5f
feet Call. 3 Volume:
Pur-e Information:
late Pmrged: -7 f2,5-10 t Tune
Purc_­.d: 13 -1 Purs-re Rate: IJ14
Purzinz Mediod.
Ted 3 A,', Touad Volwne Purged.- 2al,
Sampling, Information:
Date am,' le CollecTIL-d: -71,2,,�7i
1 Tie Sanzple CoH.ected. Q
SaintilingffiEquipment Used.
"',�ield �J--asuremtints
Time (hr) Field Mensurements Time (1-ir)
Sample Temp. ("C):
T bidiry (nru)-
i or
san"Pie 7-H (SU* I
gj D.
Spc�ci,fiac Cond.. (uS)
5 ResC1 (mg/L),
ReDox--.
Other.
Odor:
.upper ranct:
Bottle Type
Preservation .4aialysis Required
_XU 04
-5 L
/0' C&L('
Name & Affiliation ol'Samnlcrs-
T'J'U
Name & Affiliation of lnspector,
Weather Conditions,
C( w e, )-4q t -75
0bsen,ations-___...__111
Stabilization Test:
Soc"
";Ic
' e�
Time P'xrg'-d PH Conducmnce, Tempe ranire. Volume Renloved Other
(us,) CC) (L-allons)
3'. �2.

Spectrum Dyed Yarns
P.O, Box 1006
Belmont, NC 28012"
Attn: Ms. Sherry Mayhew
Phone: 1704T825-1514
Pace Analytical Services, Inc.
,98-00 N'inc y A untie, Suits 160
lfuntersvrtlu. trrC 28078
i
Lary Project Number: 9224785
Client. Project 1D: Monitoring Wells
Lao Sample No: 921731253 Project Sample Number: 9224785.001 Date Collected; 07/25/01 14:00
Client Sample 1D: MW-1 Matrix. Water Date Received: 07/25/01 15:20
Parameters Results Units Report Limit Dilutii n Artalvzed CAS No. mote ReI Limit
Field Services
Monitoring Well Data
Method:
Collected By
Jt
Collected Date
07/25/01
Collected Time
14:00
Field pfi
6.18
Std. Units
Field Specific Conductance
255,-
umhos/cm
Field Temperature
21.6
deg C
Static Water Level
12JI
feet,
Total Well Depth
26.65
feet
Odor
None
No units
Field Appearance:
Clear
No units
Well Volume Purged
2.5Dry
No units
Wet Chemistry
Total Dissolved Solids
Total Dissolved Solids
Ion Chromatography
Chloride
Sulfate
Chemical Oxygen Demand
Chemical Oxygen Demand
C Volati es
CC VOCs in Water
Dictlorodifluoromethane
Date: 08108/01
Wastewater 12
Drinkrng theater 3770
99036
Prep/Method: EPA 160.1 / EPA 160.1
190 mg/1 10,
Prep/Method: EPA 300.0 / EPA 300.0
15. mg/l 1.0
16. mg/l 1,0
Prep/Method: EPA 410.4 / EPA 410.4-
0D rngfl 25.
Prep/Method: SM 6230D / SM 62300
NO ug/l0.50
1.0
07/25/01
SNH
1.0
07/25/01
SNH
1.0
07/25/01
SNIT
1.0
07125/01
SNH
1.0
07/25/01
SNH'
1-0
07/25101
SNH
1.0
07/25/01
SNH
1,0
07/25/01
SNH
1.0
07125/01
SNH
1.0
07/25/01
SNH
1.0
07125101
SNH
1.0 07126/01 CD[.
1.0 07/26101 YMH 16887.00-6
1.0 07/26101 YMH
1.0 07/26/01 YMH
1.0 07131 O1 KST 75.71-.8
REPORT OF USOR"'Ilr MAIM
TM report shal� hot be reproduced, except in UL
Without the Wfitf0b Content of Pace Analytical Serkes, Inc;
Ll C4tcrry Lery-Eu trn r0-5
KY DrIruking Water 00000
VA Drinking Witer 213
FL NELAP 887627

c 1 "'
www.p celabs cone
Lab Sample No: 921731253
Client Sample ID: MW-1
Parameters
Chl ororrrethane
Vinyl chloride-
Bromomethane
Chloroethane
Triehlorofluoromethane
1,1-Dichloroethene
Methylene chloride
trans-1,2-Dichloroethen
1.. • Di chlcroethane
cis-1,2.Dithloroethene
Bromochloromethane
Chloroform
2.2-Dichloropropane
1,2-Dichloroethane
1,1,1-Tr°ichloroethane
1,1-Dichloropropene
Carbon tetrachloride
Di bromomethane
1,2-Dichloropropane,
Trichloroethene
Bromodichloromethane
cis•1.3,Di hloropropene
trams-1,3-Dichloropropene
1.1„2•Tricloroethane
1,3-Dichloropropane
Dibromochloromethane
1.2-Dibromoethane (LDB)
Tetrachloroethene
1,1,1,2-Tetrwachloroethane
Chlorobenzene
Bromo€orm
1,1„2,2-Tetrachloroethane
1.2.3-Trichloroproparie
Bromobenzene
2•Chlorotoloene
4•Chlorotol"uene
1,3-Dic:hlorobenzene
Data: 08108/01
Paco Analytical Setvices, Inc,
Hunter vil4e„ NIC 78078
Fax [phone]J91
Lab Project Number: 9224785
Client Project ID: Monitoring Wells
Project Sample Number: 9224785.001 date Collected: 07/25/01 14:00
Matrix: Water Date Received: 07/25/01 1520
Results Units
NO
ug/l
N0
ugll
ND
ug/l
ND
ug/I
1.5
ug/1'
N0
ug/1'
ND
ug/l
ND
ug/l
ND
ug/l
ND
ug/l
ND
ug/l
ND
ugl)
ND
ug/l
L
ug/1'
ND
ugll
ND
ug/l
Nor
ug/ l
ND
ugly
ND
ug/l
N,
ug'/l
ND
ug'/l
Nil
ug11
ND
ug/l
ND
ug/l
ND
ug/l
ND
ug/l
ND
ug/l
NO
ug/l
NO
ug/I
NO
ug/I
ND
ugtl
N0
ug/l
ND
ug/l
NO
ug/l
ND
ug/l
ND
ug/l
ND
ugly
4teport Limit
Dilution Anal zed
C5 No:
0,50
1.0
07/31/01
KST
74.87-3
0.50"
1.0
07/31/01
KST
75.0.4
0.50
1.0
07/31/01
KST
74-83-9
0.50
1:0
07/31/01
KST
75-00-3
0.50
1.0
07/31/01
KST
75-69.4
0,50
1.0
07/31/01
KST
75-35.4
0.50
1.0
07/31/01
KST
75.09.2
0.50
1.0
07131101
KST
156-0-5
0.50
1.0
07/31/01
KST
75.34.3
0.50
1.0
07/31/01
KST
156.59-2
g.50
1.0
07/31/01
KST
74.975
0,50
1.0
07/31/01
KS,T
67.66-3
.50
1.0
07/31/01
KST
594.20.7
0.50
1.0
07/31/01
KST
107-06-2
0.50
1.0
07/31/01
KST
71.55-6
0,50
1,0
07/31/01
KST
563-58.6
0,50
1.0
07/31/01
KST
56-23-5
0,50
1.0
07131101
KST
74.95.3
0.50
1.0
07/31/01
KST
78.877-
0.50
1.0
07/31/01
KST
79.01-6
0,50
1.0
07/31/01
KST
75.27-4
0,50
1.0'
07/31/01
KST
10061-01.-5
0.50
1,0
07/31/01
KST
10061-02.6
.50
1.0
07/31/01
KST
79-00.5
0.50
1.0
07/31/01
KST
142-28-9
0.50
1,0
07/31/01
KST
124.4 -1
0,50
1,0
07/31/01
KST
106.93-4
0,50
1�0
07/31/01
KST
127.18.4
0.50
1.0
07/31/01
KST
630.20-6
0.50
1.0;
07/31/01
KST
108-90®7
0.50
1.0
07/31/01
KST
75-25-2
0,50
1.0
07/31101
KST
79-3-5
0,50
1.0
07131101
KST
96.18-4
0,50
1.0
07131101
KST
108.86.1
0.50
1.0
07/31/01
KST
95-49.8
0.50
1.0
07131,/01
KST
106.43.4
1.0
1,0'
07/31./01
KS"
541.73.1
Uab-c rat- I it Is
NC Wastewater 12 REPORT
i LABORATORY
NG Drinking Water 37706 Thi's report shall not be reprodoced, except 'M U,
SC 99006 Without the written consent of Pace Aua�yfical Services, Inc,
Ftnote Reg Limit
Y Chinking Water
VA Drinking Water
EL NELAP

I
Pace Anal,ylieal Services, Inc.
wwtcpacelabscom
Lab Project Number. 9224785
Client Project ID- Monitoring Wells
Lain Sample o: 921731253 Project Sample Humber: 9224785.001 Date Collected; 07/25/01 A AR
Cl�ert Sample 1t1: MW-1 Matrix; Water Date Received: 07/25/01 15.20
Pa.rameters:
Results
units_
gprg Limit
Dilution Analyzed
CAS No, Ftnote R !_sm2 t
1,4-Dichlorobenzene
Nt1_
ug/1
1..0
1,0
07/31/01
KST
1011-46.7
1.2-Dichlorobenzene
N9
u /l
1.0
1A
07./31/01
KST
95-5 -1
1:2-Di bromo-3-chloroprogane
ND
ug/l
2.0
1.0
07/31/01
KST
95.12-0
1.2,4-Tridhlorobenzene
ND
Ugll
2.O
1.0
07/31/01
KST
120t02.1
Hexachlor �1,3-butadiene
ND
ug/l
2.0
IA
07/31/01
KST
87w50.3
I,2.3-Trichlorobenzene
Nil
ugll
2.0
IA
07/31/01
KST
87- 1.5
Methyl -teat -butyl ether.
ND
ugll
0.50
1.0
07/31101
PST
1634-04.4
0ilsopropyl ether
N0
ug/l
0,50
1.0
07/31/01
PST
108•20.3
Benzene
ND
ug/1
0.50
1.0
07/31/01
KST
71.43.2
toluaend
ND
ug/1
0.50
1.0
07/31/01
KST
109-118-3
Fthylbenzene
ND
ug/l
0.50
1.0
07/31/01
KST
100.41.4
ru p-Xylene
ND
ug/l
0.50
1.0
07/31/01
KST
Styrene
N?
ug/l
0.50
1A
07/31/01
KST
100.42
o,Xylene
ND
a Jl
0.50
IA
07/31/01
KST
95.47.6
ltopropylbenzene (Cumene)'
ND
ugtl
0.50
1.0
07/31/01
KST
93®02.8
n,Propylbenzene
1'1
ug/l
0.50
1.0
07/31101
KST
103-55-1,
1,3',5•Trimethylbenzene
ND
ug/1
0,50
1.0
07/31/01
KST
108.57.0
ter``°t-llutylbenzene
ND
ug/l
0r50
1.0
07/31/01
KST
98-06.6
1,2,4-Trimethylbenzene
ND
u ll
0,50
1.0
07/31/01
KST
95-63.5
set-Butylbenzene
ND
ug/l
0.50
1.0
0713 101
KST
135-93,0
p�lsopropyltelruene
ND
ug/l
1A
1.0
07/31/0
KST
99.87-6
n,0'uty^lbenzene
ND
ug/l
1.0
1.0
07/31/01
KST
104,51.8
Naphthalene
ND
urJ/l
2A
1.0
07/31/01
KST
91.20-
1-Chloro-3-tluorcbenzene 4S1
105
t
1,0
07/31/01
KST
525-98-9
Lab Sample No. 921731261
Project Sample
Number: 9224785-002
Date Collected: 07/25/01 13:45
Client Sample 10. Mt1-2
Matrix. Water
Crate Received:
07/25/01 15:20
Parameters
Results
Units
e22LLinrit
Dilution
Anal
zed
SAS No. Ftnote Reg Limit
Field Services;
Monitoring Well data
Collected By
Collected Date
Collected Time
mate: 08/08101
Wastewaler 12
llrariking hater 37706
99006
Method;
JJtI' 1.0 07/25101 SNH
07/25/01 1,0 07/25/01 SNN
13;45 1,0 07125/01 SNN
REPORT w " !r
Page:
��br�t0�.l�0rtsfr rill r� 5
KY prinking dilate` 90090
VA Drinking Water 21
FL NELAP 03762'

Pace Analytical , ervi
Fax. 28,;
PAST Inc. Charlottu Lab Project Number: 9322230
9800 Kincey Ave. Went Project ln® PECTRUM-9224785
Suite 100
Huntersv "s t l e, Nr.:
PARAMETER r,
r41;11
alC
Phone: L 7Cdi 3C 5 -' 0Q,,s
Lab Sarrxple Nox. ,3125i Prroject 5ampLe Number: 9322230-001 hate Collected: 07/25/01 14:00
Client Sample 1v: 's..Matrix: Water Cate Received: 07/25/01 15:2
Parameters Results Units Report l.Wt Analyzed CAS No. rtnote Reg Limit
Wet Chemist...,
Total CrRan ;..° =tx Prep/Method.;SM 5310C t SM 5310
Total Orgar,: ,,, 2.0 m9Pt 2.0 08106/01 ASS 74 0-44-
t C�tr F'r't:it,Ji:1
LaboratQr
atr�atar Ct 1
REPORT OF LABORATORY ANALYSIS
NC War p except in full, TN Chinking
NC Drinking Water 71 This report shall rlat b� reproduced, p
C Drip without the written consent at Pace Analytical Services, Inc: C Envirnnr

Pace Analyfical
Field Data Sheet
Well Sampling
Client:��JLocation
Pmject 4
Cl 1'� C? b
Well Information:
'Well IDt
Locked: Es
yes no
Well Diameter
steel sminleas steel
To,ml Well Depth- q&, 3 3 feet MWti Factor*: -(Radius 12):1 x 3,14 N 7,48
Static Water Level: � I - 53 feet Casing Volume: gal.
I ;)_110 feet Lei of dater Col,: Cal. 31 Vol,,)jn-.: gal
Purge Information. -
Date Purzcd: Hj -)-5W TimePurged.
Purge Rate. -
Purging Method*
3,,, Ct,—_ Total Volume Purged: gal.
Samplina Information:
Date Sample Collected: Tim ne Sarrmlt Collected)
Sannoling Eqiilipment Used:
A I
'r7ield Measuremeale
ffir) Field Measurements T lac ter
Sample Temp. ('C)-
Turbidity (ntu)-
Sample pH (s.u.)-
j3+3 D.0. (M_).,
Specific Cond. (uS)., _j J!5�
4 3 Res. Cl (mz/L),
R-.Dox.:
Other:
Odor:
Appe2ranc.-,
Bottle Type
Prtservauon AnJaysis Required
-y-yo-4 wA
H CQ b
I-qo.A vo4
Pasov 71DC�
2 S-0 ,g
i4a S q_y C06
—
laA6 r) C44 S
Name & Affiliarion of Samplers -
Name & Aff1harion of Inspector:
AJ/A
Weather Conditions-
h 5
Observations:
Stabilization Test:
if
I
The Puryed H
P
CoSr)ecc
tan an -
cTemp.-Mture Volume Resac v-d Other
(us) CC) (gallons)
C)

00
cv
�a
�D
CD
CN :J
4 a
t
a.a
00

Pace Analytical Services, 1
n 800 x"r 7re'y Avenue, quite 1
t/untrrs P rlle, NC 280
Phone 704,875.9t1,92
r r r. acela .cnrn Fax: 704N5.91121
Lab Project Number."9224785
Client Project IQ Monitoring Wells
Lab Sample No. 921731261
Project Sample
plumber: 9224785.002
Date Collected: 07125/01
13,45
Client Sample ID: MW-2
Matrix, plater
Date Received, 07/25/01
15:20
Parameters
Results
Units
Repart t m t
Dilution Analyzed
CA3 No, Ftnote Reg limit
Field pH
6.05
Std. Units
1.0
07/25/01
SNH
Field Specific Conductance
185
umhos/cm
1.0
07/25/01
SNH
Field Temperature
19,0
deg C
1.0
07/25/01
SNH
Static hater level
21.53
feet
1,.0
07125101
SNH
Total Well Depth"
4633
feet
1.0
07/25/01
SNH
Odor
None
No unite:
1.0
07/25/01
SNH
Field Appearance
Turbid
No units
1.0
07/25/01
SNH
Well Volume Purged
27.06t1ry
No units
1.0
07/25/01
SNH
Wet Chemistry
Total dissolved Solids
Prep/Method:
EPA 160.1 /
EPA_160,1
Total dissolved Solids
190
mg/l
40.
4.0
07126101
CDE
Ion Chromatography
Prep/Method:
EPA 300.0 /
EPA 300.0
Chloride
2.6
mg/l
1.0
1.0
07/26101
YMH
1688 -00-
Sul'ate'
14.
m /l
1,0
1.0
07/26/01
YMH
Chemical Oxygen Demand
Prep/Method:
EPA 410.4 /
EPA 410.
Chemical Oxygen Remand
ND
mil
25,
1.0
07/26/01
YMl1
GC Volatiles
6C Vl1Cs in dater
Prep/Method;
SM 6230C / SM 62300
Dichlorodifluoromethane
ND
ug/1
0.50
1,0
07/31 01 09:23
KST
75,71-6
Chloromethane
0.94
ug/l
0,50
1.0
07/31/01 09:23
KST
74-8 .3
Vinyl chloride
N0
u0/l
0.50
1,0
07/31/01 09:23
KST
75-01 4
8romometharre
NU
ug/I
0.50
1.0
07/31101 09:23
KST
7 -83.
Chloroethane
NO
ug/l
0.50
1.0
07/31`01 09,23
KST
75.00.
Trichiorofluoromethane
Na
ug/1
0,50
1.0
07/31/01 09:23
KST
75-69
1„1-Dichloroethene
N0
ugll
0.50
1,0
07/31/01 09:23
KST
75-35�4,
Methylene chloride
N0
a /1
0.50
1,0
07/31/01 09.23
KST
75.09-2'
trans•1,2-Dichloroethene
NO
ug/l
0.50`
1.0
07131/01 09:23
KST
156.60.5
1.1-Dichloroethane
ND
a /l
0,50
1.0
07/31/01 04:23
KST
75-34 3
cis-1,2-Uichloroethene
NO
Ug/l
0.50
1,0
07/31/01 09.23
KST
156.59-2
5romochloromethane
ND
ugll
0.50
1.0
07/31/01 09:23
KST
74-97 5
Chloroform
NO
ug/l
0 50
1.0
07/31/01 09,23
KST
67-6 .3
2,2-Dichloropropane
NO
ug/l
0,50
1.0
07/31/01 09:23
KST
594-20.7
1,2•Dichlofoethane
ND
u /l
0.50
1,0
07/31/01 09:23
KST
107.06-2
Date: 08IrPtil01
Page: d
UIoP 0r ification Qs
NC Wastewater 12REPORT
OF
grr,t r �1itspri Yl
NC Drinking water 37706
This report
shall hot be reproduced,
except in full,
KY Drinking Water
VA Drinking Water.
90090
213
SC 99006
without the written consent
of Pace Analytical Services,
inc,
FL NEIAP
E87627

;a'ceAnalyticaf"'
l r rviracela scorn
Pace Analytical ServicesIfn
80 K"r�cgAr rive, ir tr,rtjrsoila IVY' Phrine 704, 70T" r 704 0'd
Lab Project Number: 9224785
Client
Project
1D: Monitoring Well
Cab Sample No-. 921731261
Project Sample
Number: 9224785-002
Date Collected: 07125/01 13:45
Client Sample M HW-2
Matrix: Water
Date Received: 07/25101 15:20
Parameters
Results
_ Units
Rgp2E Limit
Dilution
ilnalyzed
CAS No Ftnute 5.ea tiriJt
1,1,1•Trichl€rroethane
ND
ug/1
0,50
1..0
07/31/01
09:23
KST
71.55-6
1 1-Dichloroprrrpene
NO
ugrl
q,SR
1.0
D7/31/01
09:23
KST
56 -58-6
Carbon tetrachloride
ND
ug/l
0,50
1.0
07131101
09:23
KST
56.23-5
Dibromomettane,
NO
ug/l
0,50
1.0
07/31/01
09:23
KST
74.95.0
3 2rDichloropropane
ND
ug/l
0.50
1,0
07/31/01
09:23
KST
78.87.5
Triehluroethene
NO
u /l
0.50
1,0
07/31/01
09:23
KST
7 .01-6
Bromodichloromethane
ND
uq)l
0,50
1.0
07/31/01
09.23
KST
75-27-4
cisw1,3•Dic'hlorcprdpene
NO
u 1
0,50
1.0
07/31101
09:23
KST
10061-01-5
trans-1,3.Dichloropropene
ND
a /li
MO
1.0
07/31/01
09:23
KST
10061.02-6
1.1,2-Trichloroethane
NO
u9/1
0,50
1,0
07/31/01
M 23
KST
79-00-5
1 3-Dichloropropane
NO
ug11'
0,50
1.0
07/31/01
09:23
KST
142-28-9
Dibromochloromethane
NO
ug/l
0.50
1,0
07/31i01
09:23
KST
124.48.1
1,2,Di bro ethane (EDB)
NO
ug/1
0,50
1.0
07/31101
09:23
KST
106.93.4
Tetrachloruethene
ND
ug/l
0.50
1.0
07/31/01
09:23
KST
1.27.18.4
1,1_,1.2-Tetrachloroethane
NO
ug/l
0.50
1.0
07131/01.
09.23
KST
630-20-6
Chlorobenzpne
NO
ug/l
0,50
1.0
07/31`01
09:23
KST
108.90.7
Bromoform
ND
Ugtl
0.50
1.0
07131/01
09:23
KST
75-25.2
1,1,2,2•Tetrachlorcoethane
ND
U9/l
0,50"'
1.0
07/31101
09:23
KST
79-3 -5
1,2,8-Trichloropropane
NO
ug/l
O1 50
1a0
07/31/01
09:23
KST'
96-18.4
Bromobenzene
NO
ug/l
0.50
1.0
07/31/01
09:23
KST
108.86.1
2-Chlorotoluene
ND
u /1
0.50
1,0
07/31/01
09:23
KST
95.49-8
4-Chlorotoluere
ND
ug11
0,50
1.0
07/31/01
09:23
KST
106-43.4
1,3-Dichlorubenzene
ND
ug/1
1.0
1.0
07/31101
09:23
KST
541-73-1
1.4.Dichlnrobenzene
ND
ug/l
1,0
1.0
07/31/01
09:23
KST
1.06.46•7
1,2.Dichlorobenzene
NO
ug/l
1.0
1.0
07/31/01.
09:23
KST
95-50-1
1,2-Dibromo-3-chloropropare
NO
ug/l
2,0
1,0
07/31101.
09:23
KST
96.12 8
1.2„4-Trichlor,obenzene
ND
u l
2.0
1.0'
07131/01
09,23
KST
120-82.1
Hexachloro-1,3-b€stadiene
NO
ug/I
2,0
1,0
07/31d01
09:23
KST
87.68-3
1.2.3-Trichlorobenzene
ND
a 11
2.0
1.0
07/31/01
09:23
KST
87-61-6
Methyl -tent -butyl ether
ND
ug/l
0,50
1.0
07/31/01
M 23
KST
1634.04-4
Diisopropyl ether
ND
ug/l
0,50
1,0
07/31/01
09:23
KST
108.20.3
Benzene
ND
ug/1
0,50
1,0
07/31/01
09:23
KST
71.43-
Tcluene
ND
ug/l
Mo
1,0
07/31/01
09.23
KST
108.88-3
Ethylbenzene
NO
ug/l
0,50
1,0
07/31/01
09:23
KST
100.41-
,p-Xylene
ND
ug/l
0,50
1.0
07/31/01
09:23
KST
Styrene
ND
ugly
MO
1.0
07131/01
09:23
KST
100-42-6
o-Xylene
NO
ug/l
0,50
1.0
07/31/01
09:23
KST
95�47-6
Lgbaraigr e.ififi a iQ-r IQi
NC Wastewater 12,
NC'tlfting Water 37706
SC 99006
This report �hall not be reproduced, except '�n Nil,
without t�he written congobt of Nee Aha[yficA Services, Inc,
LLIQu rU� i ri.%
KY Dhnking Water 90090
VA Drinking Water 213
EL NELA9 E87627

Pace Analyti al Services, l
$
�71106 Kr?pceyy Avenfje, 45tjtte It,
III
�., pp��yy,,ggpp�xew�yg ggyy
PP'i�NYx 4x �} +spy �tr p�.:gg �gp
Sa lLd $/.Tr C!VPNB
1`Fr rrG. f'LM Y.7j,:iC1MC�`y,,`1..
Fax t'04 8575 r 09t
Lab Project Number, 9224785
j
Client Project
10 Monitoring' ells
Lab Sample No: 9211731261
Project Sample
Number: 9224785.002
azm�
DateCollected: 07/25/01 1
Client Sample ID- tW, 2
Matrix: stater
,:4
Date deceived: 07/25/01 15:20x''
Parameters
gestalts !bits
de rt L m?t Dilution Anal zed
6/rS No, 1 nub d� i.lr�lt
1sopropylbenzene Itrarenel
ND ug/l
0,50 1,0 07/31/01
09:23 KSl,.
99-02.6
rr-Prupylbenzene
ND ug/l
0.50 1.0 07/31/01
09:23 KST
103®65.1
1.3,5-Trimethylbenzene
ND ug/7
0.50 1,0 07/31/01
09:23 KST
108- 67.5
tert�Butylbenzene
NO ug/l
0.50 1.0 07/31/01
09:23 KST
90-06-6
1,2,4-Trimet'6ylbenzene
NO ug/l
0.50 1.0 07/31I01
09:23 KST
95-63.6
sec-Butylbenzene
N0 U9/1
0,50 1A 07/31/01
09:23 KST
135-98.6
-1s
tr oprupyltOluenn
N0 u /1
9
1.0 1.,0 07/31`01
09:23 KST
99-57-6
n Butylbenzene
NO u9/1
1.0 1.0 07/31/01
09:23 KST
104-51-6
Naphthalene
ND ug/l
2.0 1.0 07/31/01
09°23 KST
91.20m3
l Otrloro-.3-tlararubenzene (S)
117 t
1.0 07/31/01
09:23 CST
625.98•9
I
Date: 08/08/01
Paget
- ,-&,1tC -r,e— tGf muoupa
NG Wastewater 12
REPORT OF LABORATORY ANALYSIS
t l` itd Icc tt 1-
INC Drinking Water 37706
This report small riot be reproduced, except an tuH,
KY Drinking Water 90090'
SC 99006
without the written consent of Pace nal7fical Services, eric,
VA C7rtnKirr t'WOter 213
FL N6t.P la8e627

Pace Analytical Services,
/7U 9800 Kincey A veaue, Suite I
aneAnalytica
www.pacefahs'com ftne:,704 875,9092
Fax, 704,87,15,9,091
Lab Project Number: 9224785
Client Project ID: Monitoring Wells
PARAMETER FOOTNOTES
NO Not Detected
NC Not Calculable
(S) Surrogate
Date: 08108/01
rage: 7
La pQ-F='L-Q-Qqd —1c 6PA Ills La-b—QratgryS211jt 10�
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drng Water 90090
NC Drinking VVIter 37706 This report shall not be reproduced, except in full, VA Dri*ng Water 213
SC 99006 without the written consent of Pace Analytical Services, Inc, FL NELAP E87627

Pace Analytical, Services, Inc.
54 Rol eraserI Drive
aneAnalyficafo
I#ashevi#6, NC 28801
Phone; . al. 17
ecsf a.cn
Fed 828.254,4618'
Lab Project Number: 9322230
client Project ICI: SPECTRUM_92247 5
Lab Sample NO:
92!731261 Project Sample
Number: 322230-002 DateCollected; t 7125/01 13:45
Client Sampte
ID: !,,W-2
Matrix, hater
Date Received. 07/25/01 15:20
Parameters
Results Units
Report Limit
Analyzed GAS No: Ftnote Reg Limit
Pet Chemistry
Total Organic
Carbcin Prep/Method: 'SM 5310 I
SM 5310
Tatal Organic
C:rcr,r 6.0 mgll
2.0
08/06/01 AAIS 7440.44-0
Date: UB/Oulol Page. 2
brlratnry rtifia#inn i Da REPORT OF LABORATORY ANALYSIS U nrf"fit" I�
NC Wastewater 40 This report shall rent be reproducedTN Drinkin Water 02980
N DrinkingWater 3771 R , e eflt In foil, Environmental 99030
without the written consent nt Pane Analytical Services„ Inc. SC
t

7--
/,,,�Pa'ceAnalylical
Sirwttacelati .cot Fte were
rr art T4
Required Client hitormation" Section A
Company Copy to,
ddraza 3n_valce T
r
Prolact N
F.. Project N
�
C14
Section D Required O�onf Information: �SAM
PLE ID
ft
2 One character per box,
w (A-Z, 0­9 / -)
t Sample I MUST BE UNIQUE
......... [ -------
Additional Comments:
*.a A a 0 _� a w V 11 6 1 r%* I" i Y &I%,, LAS I aam4 %A
The Chain -of -Custody is a LEGAL DOCUMENT. Ali relevant fields must be completed accurately.
Information: Sect I ion B Page: Of 6303075
To Be Cornpreted by Paco AnaMwfcal and C4irml Section C
rliAnt Information fcheck quoteloontractIL
Requested Doe Date: TAM Prooct Manager.
Turn around times less than 14 days subject to Project C_
taboratory and contractual Wilfgabons and may result in a
Rush Turnaround Surcharge. Profile C
Tom Around Tyne (TAT) in calendar days.
Requested AaaIysIs7-T
TI� COP —
�Isi A Preee servatives
_"—k w Y
WATER wf w UJ UJ -In
SOIL SL LU UJ
0 : -I _JJ fir
OIL OL 9
"y
we X 0 WIPE
AIR AR
0 0
IISSUE T rnZ Q at
2 iffm drift I yy h1v M a/P r Z Z 2 RemarksI Lab ID
,7
Y
4— —
fl
SAMPLE CONDITION
Sealed Center Y tN

Instructions for comollotin g Chain of Custody (COCA
1. Complete all Client Information at top of sheet: name, address, phone, contact (person to whom
report will be sent and contact can be made if questions arise), billing information if different from
client, PO#, Project Name and/or Project Number as it will appear on the report.
2. Quote Reference, Project Manager, Project No. and Profile No. will be completed by Pace.
3, A separate COCR must be filled out for each day of sample collection.
4. Sampler should print their name in the space provided and sign their name followed by the date of
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5. Complete Sample Description as it will appear on the laboratory report', include, time of sampling,
sample matrix, no. of containers and preservative Used,
6. Analysis Requested: Complete analysis on the lines provided and place a check in the column for
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7. Submission of samples to laboratory., Indicate Item Number of those samples being transferred;
sign relinquished by, and include your affiliation.
* IMPORTANT NOTE:
Standard Turnaround Time is 2 weeks, If this does not satisfy your requirements, arrangernents
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5peci-al-Project RKe(LLyrqLnen-ts such as Lov Level Detection Limits or level of QC reported Must
be indicated on the chain Of CUstody. (Use, Additional Comments Section.)

w
m
F"My Flamm—
Paunit Name (11 differeal);
Fa res
Co
PI C•
t Person., —
SUM T FORM ON -YE L.L-QW. PAPER ONLY
111111 MI!
Caunly UUr 11,
Telephone #;
No. of Wells to bo Sample&
Check 0118'.
Ej ItAlluent too)
0 Effluen
DIVISION OF WAI E11 QUALITY
GROMIDWATIEFf SECIjohl, PERM114 ATU) COMPLIALICE 11111T
U1 13
, ,'
RAI-00111 14C 21826-057 8 1'110;lil ig 21
EX 1111A "6
PERMIT M, EX�')IFIM ION DATE.
Non-Uschar oe--� UIC__
NPDES---,
IIJ.LI20i'EtIA'lIONBEIN(03M()Nl'IOIIE-ID
to 3L
Lagoon —Remadiallon: InlHirallon Gallig mc:�
n L 11, r�
Spray Field Aarivdhillon:
'I
1, 'j tic,
fininry Clistribill r —1-andApplicaConal, lUdgir
CAI
em
sef__ 01--
Values should relloct dissolved and
cotioldal conceritta I Ions.
Date sample cofleclerjm 115--Of Date Mamp�o
E�pnqlyzed ,41
ni
PI -IQ
0�
Laboratory Name:
Cerillicallon No, — kR -
TOO-
Chlorlde
--------------
W"/ 4110 /
--- YES — NO)
NI - Nicket----
Ing/I
Pb - Lead
Ing/1
Z11 - Zinc
mg/1
Ammonia Nitrogen---
rylg/1
Other (Specify Compounds anci Concentration
Nulls)
01-IGANICS: (GC,GCIMS,I,IPLC)
ISTroelly last and method #. Attach tab report,)
Repott Altache(17 Yes —,—(I) No
voc method If
mehiod it
mathod 11

1

www. adela s'com
Spectrum Textured Yarns
P.O. Box 1389
Marion„ NC 28752
Attn: Mr. Rick Kilpatrick
Phone;:
Pace Analytical Services, Inc.
9800 KinceyAverrrre, Smile 10
Hantorsvrlle, NC 2 078
Fax. 704. 8,75 9091
Lab Project Number: 9221685
Client Project 1D: Monitoring Wells
Lab Sample No; 921533600
Project Sample Numbera 9221685.001
Date Collected: 03/28/01 16:35
Client Sample 1Dr MW-1
Matrix: Water
Date Received; 03/28/01 17:32
Parameters
Results Units PRL
Dilution
Analyzed
Analyst CAS# Ftnote Limit
Field Services
Monitoring Well Data
Method.
Collected By
3aQ
1.0
04/03/01
SNH
Collected Date
03/28/01
1.0
04/03/01
SNH
Collected Time
16:35
1.0
04/03 01
SNH
Field pal
6.47 Std. Units
1.0
04/03/01
SNH
Field Specific Conductance
264 umhos/'cm
1.0
04103/01
SNH
Field Temperature
18.0 deg C
1,0
04I03/01
SNH
Static Water Level
1032 feet
1.0
04/03/01
SNH
Total Well Depth
26,65 feet
0
1.0
04/03/01
SNH'
Odor
None No units
0
1,0
04103/01,
SNH
Field Appearance
Clear No units
0
1.0
04/"03/01
SNH
Well Volume Purged
3,0&dry No units
B
1.0
04/03/01
SNH
Wet Chemistry
Total Dissolved Solids
Method; EPA 160,1
Prep Method:
EPA 160,1
Total Dissolved Solids
190 mg/l
1
1.0
04/06/01
CDE
Ion Chromatography
Method. EPA 300.O
Prep Method:
EPA 300.0
Chloride
17. mg/l
1,0
1.0
03/29/01
YMH 16887-00-6
Sulfate
18, mg/l
1.0
1.0
03/29/01
YM
Chemical Oxygen Demand
Method: EPA 410,4
Prep Method;
EPA 410.4
Chemical Oxygen Demand
NO mg/l
25.
1.0
03130/01
YMFI
Laboratory Certifi ationn ID
NC Wastewater 12
NC Drinking Water 3770
SC 9900
ANALYSISREPORT OF LABORATORY
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services,; Inc.
Imm
KY Drinking fter 90090

Pace Analytical Services, Jars.
9800 Kincey Arerrtae, Su ile 100
aceAnalyfical' Huntersville, NC 28078
Phone: 704,875 909
wwwr a ela sacdart Fax. [phone]
Lab Project Humber: 9221685
Client Project ID: Monitoring Wells
Lab Sample No., 921533618 Project Sample Number. 9221685-002 Gate Collected. 03/28/01 16-:25
Client Sample ID: MW-2 Matrix: stater Gate Received,. 03/28/01 17 32
Parameters Results Units P L Dilution Analyzed Analyst CAS# Ftnote Limit
Field Services
Monitoring Well Data
Method:
Collected By
JJQ
1.0
04/03/01
SNH
Collected Date
03/28/01:
1.0
04/03/01
SNH
Collected Time
16:25
1.0
04/03/01
SNH
Field pH
6.34 Std. Units
1.0
04/03/01
SNH
Field Specific Conductance
188 umhos/cm
1.0
04/03/01
SNH
Field Temperature
17.4 deg C
1.0
04/03/01
SNH
Static hater Level
18,25 feet
1.0
04/03/01
SNH
Total Well Depth
46.08 feet
0
1.0
04/0301
SNH
Odor
None No units
0
1.0
04/0301
SNH
Field Appearance
Turbid No units
1
1.0
04/03/01
SNH
Well Volume Purged
31.0 dr~y No units
0
1.0
04/03/01
SNH
Wet Chemistry
Total Dissolved Solids
Method: EPA 160.1
Prep Method:
EPA 160.1
Total Dissolved Solids
90. mg/l
10.
1,0
04/06/01
CDE
Ion Chromatography
Method: EPA 300.0
Prep Method:
EPA 300.0
Chloride
1,9 mg/l
1.0
1.0
03/29101
YMH 16887.00.6
Sulfate
9.1 mg/I
1.0
1,0
03/ 9/01
YMH
Chemical Oxygen Demand
Method: EPA 410.4
Prep Method:
EPA 410.4
Chemical oxygen Demand
ND mgf'l
1.0
03/30/01
YMH
Date: 04/11/01 Page. 2
Laboratory Certification Ds REPORT OF LABORATORY ANALYSIS
NC Wastewater 12
NG Drinking Water 37706 This report shall not be reproduced, except in full;
SC 99006 without the written consent of Pace Analytical Services; Inc:
Laboratory Certific i n iC
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E876 7

Pace Analytical Services, Inc.
,9800 Kincey{ Avenue, ,Sure 100
aceAnalXicaTM Hunters NC 28078
Phone: [phone]
rw. acetahsceaa Fax: [phone]
Lab Project Plumber: 9221685
Client Project ID: Monitoring Wells
PARAMETER FOOTNOTE
NO Not Detected
NC Not Calculable
PRE Pace Reporting Limit
Date. 04/11/01
Page:'
I
Laotogfinn IREPORT
OF LABORATORY
t
Laboralf'
tllD
NC Wastewater 12
CDrinking
Ddater
90090
E Drinking hater 37706
This report shall not be reproduced„ except in full,
VA Drinking Water
21
Sc 99006
without the written consent of Pace Analytical Services, Inc.
FL NELAP
E87627

Pace Analytical "ervi es, Inc.
64 Ravensc°roft Drive
Asheville, NC 28801
Phone[phone]
www pacelabs, errs Fax 6 6.216 . 61R
PA 1 Inc, Charlotte Lab Project Number: 9319272
9800 Kincey Ave Client Project ID: SPECTRUM-92216 5
Suite 100
nuntersvitle, NC 28070
Attn: Project Management
Phone: [phone]
Lab Sample No; 921533 00 Project Sample Number: 9319272a001 Date Collected. 03/28101 16:35
Client Sample ID: MW-1 Matrix: Water bate Received: 03 28/01 17:32
Parameters, Results Units PRL Analyzed Analyst CAS# Ftno'te Limit
I
Wet Chemistry
total Organic Carbon Method„ SM 5310C Peep Method, SM 53100
Total Organic Carbon 7 0 1t 2.0 04/10/01 AAS 7440-44-0
Date: 0110/01 Page: I
U r 1aut-1 0i l iREPORT OF LABORATORY ANALYSIS law-ratkaLff2fisaki n 1 5
NC Wastewater 40 TN Drinking Water 02 0
N Drinking Water77i This reporthaii not be reproduced, except Sri full, C Environmental ��
without the written consent of Pace Analytical Services, me,

Pace Analytical Services, Inc.
4shevilia, NC ,� 1
Phone: 828..N,7176
www.p celab . o ax: 828252 461
Lab Project r: 931972
Client Project ID SPECTRUM-92 16 5
Lab Sample No: 921533618 Project Sample NLffnber. 9319272-002 Date Collected: 03 /01 16: 5
Client Sample to MW-2 Matrix. Water Date Received; 03/28/01 17:3
Parameters Results units PRL Analyzed Analyst CAS# ftnote Limit
Wet Chemistry
Total Organic Carbon Method. SM 5:310C Prep Method: SM 5310C
Total Organic Carbon 4.0 mg t 2.0 D4/10J01 AAS 7440-4440
Date. 04/10T01 Page: 7
uWnwr
U'U-r'a—t9-ry&M1fiU� Qnl REPORT OF LABORATORY ANALYSIS
NC Wastewater r 40 T DrinkingWater 02980
NC DrinkingWater 771 This report shill not be reproduced, �n NO, nw�r�rirn�ntal ACC
Mthout the written consent t Pace .Anal tica� Services, Inc,

��a'i 54 Ravenscroft Drive
Pace Analytical Services, Inc,
Asheville, NC 28801
ceAnalyfical"' Phone. [phone]
w. eeeta .corgi fax ;828.2 2,46i
Lair Project N re 9319272
client Project 1D: SPECTRUM-9 1685
PARAMETER FOOTNOTES
ND Not Detected
ND Not Calculable
PRL Pace Reporting Limit
Date: 0/1 ID Page: 3
h ratnry — i n lQ REPORT OF LABORATORY ANALYSIS
L r ray rtit° atirsn i s
C Wastewater A Drinking
enter 0
2980
NG Grater 771 This report shaIi not be reproduced, except in full, 030
i �r�nin Water
itrsnit�n without the written consent of Pace Analytical Services, Inc

P 4m ^6 A -OF-CUSTODY /Analytical Request Document,
ate-AnaWftal CHAIN
The fthi Chemisny, The fthtSohition­ Tice Chain-of-Clast ody is a LEGAL DOCUMENT All relevant fields must be completed accurately,
512357
Required Client Informatiom Section A Required Client Information, Section B of j Ill Be Completed by Pace Analytical and Client Section C
RePDO TO: Wadi Referenoe'
ClipInfirm stint fCheck quotelcontrac
ar
/1
Address Involine Tw m Requested Drie Date: `TAT. Prefect Manager
L
RO, Turn around l4nes toss than 14 nayrSUbjest Is
6e /, 6 IVtxres tit
/2-. laboratory and contractual obtillawns anti may result in a -s'
Proj;�Namc!j� Rush Turnaround Surcharge. Profile tsje ItS -rum Around Time (TAT) gn "endar days,
_1_Fax 'Prqect Number: Requested Analysis.,
Section D Required Client utforonnion: Valid Mains Codes Preservatives
M411" w — — — — — —
WATF,R WT LU Lu e! l'-
a
soiL SL !R w w
SAMPLE I D 0 _j N, '� 10 �Q x
OIL Obi. O:j _j 0
_W WPE Wild x 0 0
One character per nox. 0 E_ 6 0 0. R� /Vy
AIR AR 0
w (A-Z, 0-9 TMSUE TS 0 10 z
ra
Sample Me MUST BE UNIQUE !1TIKE _ car man I dd I yy W Turn alp =t z: z z Remarks Lab ID
A/�;
—
+ 3 1'2 9/01 jb2 S
0c:
f e'-f
�SIGNAT lto�IPL DATE Signed: T�
SEE REVERSE SIDE FOR INSTR JCT�, NS nalytical Services, Inc. FonnG0001.XLS12

Analytical 'lfi
Spectrum Dyed Yarns
P .0 Box. 1000
Belmont. NC 28012
Attn: Mr. Terry Ward
Phone: t7049825-1514
eported on a dry weight basis
e iJ0
Pace Analytical Services, Inc.
IV
DATE: 12/06/00
PAGE: 1
Pace Project Number: 9218715
Client Project ID: November 2000
Pate Sample No: 921334959
Gate
Collected:
11/17/00
Matrix, Water~
Client Sample ID MW-1
Date
Received:
11/17/00
Parameters
Results
Units:
PPF
Apo,
DF Analyzed Analyst
CAS# Footnotes
Field Services
Monitoring Well Data
Method.
Prep Method:
Collected By
JJQ
1.00
11/27/00 SNH
Collected Date
11/17/00
1.00
11/27/00 SNFI
Collected Time
1015
1.00
11/27/00 SNft
Field pH
0.43
Std. Units
1.00
11127100 SNIP
Field Specific Conductance
263
umhos/cm
1.00
11127100 SNff
Rteld'Temperature
19.6
deg C
1,00
11127100 SNtt
Static Water Revel
11,114
meet
1.00
11127100 SNFi
Total Well Depth
20.64
feet
0
1.00
I1/27/00 SNN
Odor
none
No units
0
1,00
11/27/00 SNIT
Field Appearance
clear
No units
0
1.00
11127100 SNt1
Well Volume Purged
2.4&dry
No units
0
1.00
11127100 SNH
Wet Chemistry`
Total Dissolved Solids
Method:
EPA 160.1
Prep Method; EPA.
160,1
TotalDissolved Solids
170
mg/1
10
1.00
11/27/00 YNH
lore Chromatography
Method:
EPA 300.0
Prep Method; EPA
300.0
Chloride
16
mg/1'
1.
1.00
11121/00 CB;)
Sulfate
1.7
Mg/l
1
1,00
11121100 CBJ
Chemical; Oxygen Demand
Method:
EPA 410.4
Prep Method: EPA
410.4
Chemical Oxygen Demand
NO
mp/1
25
1.00
11121100 YrJ'
Cr���pr:�1c.1°_.�rtiir ,alit€l @[1s
C Wastewater 12
NC Drinking Water 3770
SC 99006
REPORT OF LABORATORY ANALYSIS
Tins report shrill not he reproduced, except in frill„
without the written consent of Pace Analyticoi Services, 4)c,
Labilratrr y-Qa of atio l r
KY Dfinking Water 90090
ild LIST List,
VA DrinirirarJ'Water 21

4
a. i„ S. ., d4. U
Pace ,Analytical Services, Inc,.,
a
aceAnaly
5 arernrraftCurve
•&.Rev Kier P 41 7880
YA Y9X0�tle RVRc tahs.cnrn
��tone 828,2547175
,p
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p
ARTS:
11l2 /I1C
PAGE:
1
PA I Inc. Charrratte
Pace Project Number.
9316732
9800 Kincey Ave,,
Client Project ID:
SPECTRUM
- 921 715
Suite 100
NUntersvil er NC 28073
Attnt Project Management'
Phone: (704) 75- C92
oHd resu£ts are reported on a wet weight basis
Pare SampLe No: 921334959
Date CoLl ecte ; 11/17/00
Matrix;
Water
Client Sample ID: M 1
Date Received: 11/17/00
` Parameters Resaatts units
PRL AnaLyzed Ana[yst CAS4
Footnotes
f1 Wet Chemistry
Total Organic Carbon Method: SM 5 10C
Prep Method: SM
5 10C
Total Organic Carbon 18 rug/t
2 11128106 AAN 7440-44-
�r7I3Car2? r � ert9fl`"it9 nREPORT OF LABORATORY ANALYSIS
NC ew W
l�ite�v�ater 40
NEB s Water 977i This report shall not 9e reproduced, except in full,.
WithOLst the i cuter Consent of Pace Anafytresl Services., Eric:
TN Drinking ing Water 02980
SC Environmental 99030

BE I
Pace Analytical Services, lrrc
u
fvo slo,oTX 770,5
Lab Project Number: 8518556
Client Project ID: TOO/9218715/Spectvu€r
PARAMETER FOOTNOTES
ND Not Detected
NC Not Calculable
PRL Pace Reporting Limit
A
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, Inc,
Page;

Pace Servicn, Inc,.
` a ran
{An;Wytical
ut tdY rtit �a4 Avenue !.cle f(t!9
17 tntec; 1i',,. NC 2801",8
www.pacelahs,com
Rhone,, 704 875, 90 2 /
m.,.,")
7
DATE:
0
12/0li6/6D
PAGE.
Pace Project Nraaaher.' 9216715
Client Project, 1D. November
2000
Pale Sample No ,.�... 213467
..__.._.____.
.�,...
Date
Colleted:
11117100 Matrix:
Water
Client Sample ID: MW-2
Gate
Received:
11/17/00
Parameters
Results,
units
PPR
App,
DE Analyzed Analyst CAS#
Footnotes
Field Services
Monitoring Well Data
Plethad:
Prep Method:
Collected By
Jeff
a,00
11127100 SNH
Collected pate
11/17/00
1.00
11127100 SNH
Collected Time
1046
1.011
11/27100 SNH
Field PH
6:24
Std. units
1.00
11127100 SNH
Field Specific Conductance
184
ramhos/cm
1.05
11/27/00 SNH
Field Temperature
17.5
deg C
1.00
11/27/00 SNH
Static Water Level
21.80
feet
1.00
11127100 SNH
Total Well Depth
4530
feet
0
1,0
11/27/00 SNH
Odor
roue
No snits
0
1.00
11/27/00 5N11
Field Appearance
salty
No units
it
1,00
11127/00 SNH
Well Volume Purged
25.0&dr,y
No units
C
1.00
1.1/27t110 SNH
Wet Chemistry
Total Dissolved Solids
Method:
EPA 160,1
Prep Method: EPA 160.1
Total Dissolved Solids
150
Mg/1
10
1.Cd1
11127100 YFdtl
Ion Chromatography
Method:
EPA 200.D
Prep Method: EPA 300.dl
Chloride
2.0
mg/l
1
1,00
11/21/00 CBJ
Sulfate
11
mg11
1
1,00
11121100 C6,1
Chemical Oxygen Demand
Method:
EPA 410,4
Prep Metho& EPA 410.4
Chemical Oxygen Demand
ND
g/1
25
1,00
11121100 i"E.1'
ado .t r a t6i taori RG
NC Wastewater 12
NC Drinking Dilater 3770
C 99006
REPORT OF LABORATORY ANAMIS
This report shall not be reproduced, except 41 full
without 016 Written consent of Pace Analftal Serviom loo,
a .prat Cell kdtion IDs
KY Drinking' trater 90090
TN UST fist
VA Drinking Water 213

Pace Analytical Services, Inc.
54 Ralensciott Orive
shevilte. NC 28801
DATE:
11 /29/trig
PAGE:
Pace Project Nu rc
9316732
Client Project 1C:
SPECTRUM -
921 715
Pace Sample No 921334967
elate Coiiected: 11/17/00
Matrix.
Water
Client Sample ic; M -2
Gate Received: 11/ 7/0
Parameters results Units
PRr Analyzed Analyst' CAS#
Footnotes
Wet Chemistry
lotal Organic Carbon Method: GM 5 a1CC
Prep Method: 5M
5 14C
Total Organic Carbon No malt
2 11/2 /CQ AA5 7440-44-0
L rater -QertificaNQ Dhs
NC Wastewater 40
NC Drinking Later` 3771
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except Ir1 full,
mrri hoot the written consent of Pace Analytical Services, Inc,
L r MP.r'i ' tr r I
TN Drinkft Water 02980
SC Environmental 99030

r
;aceAnalyficafm A,06144(e, NC 28801
Pace Analytical Services, Inc
54 Ravenscfoft Drive
www.pacelabs.com
Phan 82, 541 1 6
DATE: 11/28/00 Fax: 8�82524618
PACE: 3
Paco Project N` r:-931673
Client Project ID: SPECTRUM - 9218715
PARAMETER FOOTNOTES
NO Not Detected
NC Not CatcutabL
PRt Pace Reporting Limit
6 t r " Nlifi auotN s: 3 rat r °_ St�fl t# i31_ t
NC Wastewater 40 TTin rinking Water 02980
tt Drinking Water 37712 This report shalt not �� reproduced, except in full, E��vwr�rirrtntaE 99
Mthout the written consent of Pace Analy icgi Services, Inc

Pace Analytical Services, Inc.
't;
14LI , U �[p� "[% V`." Ali
Houston IX 77,053
{Bone 48831810
4! www.pacelahs,com
Pace Analyticat Services, Inca
Lair Project Number: 8518556
9800 Kincey Avenue
Client Project 1D. TOX/921 715/spectraum
Suite 100
Suntersvi t te, NC 2807E
Attn: Ms. Fetecia Grogan
Phone; (704)875-909
Lab Sample No: 921334959
Project Sample
N r: 851 556- 01hate Collected:
11/17/00
Client Sample Ib: MW-1
Matrix: hater bate Received:
11/17/00
Parameters Results
knits.
PRL Dilution Analyzed Analyst CAS#
Ftnote limit
Vat Chemistry
'Totat Organic Hairsgens
Method EPA 9020i3
Prep Method: EPA 90208
Total organic Halides 20.6 ug/l
10,0' 2»0 12/05/00 07;'00 BJAC
Lab Sample No: 921334976
Project Sample
Number: 8518556.002 bate Collected:
11117/00
Client Sample ID: MW-2
Matrix. dater Date Received:
11/17/00
Parameters Results
Units-
PR'L Dilution Analyzed Analyst CAS#
ftnote Limit
Wet Chemistry
Total Organic iiatogens
Method: EPA 9020B Prep Method: EPA 90208
Total organic Halides ND
ucg/t
5.00 1,0 12/05100 07:00 SJAv
Page.: "1
REPORT LABORATORY

Fees py (( �' if li ry Services, Inc.
p
ncejy
Huntersw rlle, NC 28078
Fax ,7048759091
DATE: 12/06/00
PACE;
Pace Project Number: 9171
Client Project IDNovember 2000
PARAMETER FOOTNOTES
NO Not detected
NC Not Calculable
PRL Pace Reporting Limit
App. tlp Applied Dilution Factor
l l r to C rt ti tLQp IQF,Lames l r C t t[plti r�
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS R7 Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in trill, TN UST List
SC 99006without the written consent of Pace Anal fical Services. inc. VA Drinking Water 2131

Blom
EvOk
thed Otte -
a hilueot (09)
0 0fluent (9
OrWME11 QUAUTY
WATER staloN - PEAMn Arixi,cooLfik
No 27626AS78 kbn�. 010) 7"
_F-
Values should reflect dissolved and
colloidal conaentrations.
Date sarnple collected. t Dalo sample 1
Laboratory Name:
46-74
Certification No.
MAMETE.,ft,13 (Samples for metals were collected tan flit ered —YES ---NO
and field acidified
—YES NO)
COD
M ("! I
Nitrite (NO2) as N
frig/1
Ni - Nickel ----.—
M911
Coliform: IVIF Fecal
/100ml
Nitrate (NO3) as N
mg/1
Pb - Lead--
Zinc
m9/1
MO/I
Coliform: MF Total
/I 00m]
Phosphorus: Total as P
mg/l
Zn -
(Note: Use MPN method for highly turbid 3afopleS)
Orthophosphate
mg/1
Arnim onia Nitrogen
mg/l
Dissolved Solids: Total
rn(j/1
A] - Alurninurn
mg/l
Other (Specify COMPOUnds and Concentration
flails)
pH (when analyzed)
Units
Ba - Barium
mg/I
TOC —7
rUg/I
Go - Calcium
1119/1
---
Chloride 9-1
mg/I
tad - Cadmiurn
rng/I
Arsenic
mg/I
Chromium: Total VIT" mg/l
Grease and Oils
mg!l
CLI-Copper
"NP n Ig/l
Phenol
mg/l
Fe - Iron
mg/l
ORGANICS: (GC,GC/MS,riPLC)
Sulfate
mg1l
Hg - Mercury . .. .. ; rrig/I
(Specify test and method #, Attach lab report.)
No
Specific Conductance
umhos,
K - PotassiUm__
Mg/I
Report Attached? Yes_(1)
(0)
Total Ammonia
frig/I
Mg - Magnesityp"
mg/I
voc method rf
TKN as N
mg/I
Mn - Manganed ' "7 2 t7,
mg/I
method 0
Ar"viry":
vl,
method 0=
GW-59 r1ev. 4/98

GROUNbWATERWALITY MONITQRING*
WA I I tll= vr:**WT� r_*I
Plea,st, PrIfirl Clearly or
che(A One,
tj Influent (00)
El Effluent (99)
1011 WI
PA f3OX 29578
J trA tilGlit Ne 2106-657fi Phone: I �)Ltxl ��Zt
EXPIRAHON 0A'l 111�
UIC r
Non-Discharge-_0
NPDES
J)TE-_QFLE U:JM OPERATION BEING, IVIONI I OK-0
Lagoon _Rernefttion- infiltrillojr'Gialfery
Spray Field neinediation' ,
Rosary DIstdbutor Land AppflCallon ofBudow
01hor
PAx,Am W tnetals wiero collected onflitered-YES --NO nod field acidiffed --YES - NO)
GOD Z n
n1(j0
Write (NO2) as N
rng/l
Coliform. MF Fecal
/1 offint
Nitrate (NO3) as N
rng/l
Coliform: MF Total
11 00tyll
Phosphorus- Total as P
mg/1
(Note- Use MPN Method for highly turbid samples)
Orthophosphate
mg/I
Dissolved Solids: Total t
mq/l
A[ - Aluminum ____
mg/1
pN (when analyzed)
units
Ba - Barium
m91I
TOE
mg/l
Ca - CalG1unr____
rug/l
Chloride 4 X<
mg/I
Cd - Cadmiurn-_
mg/l
Arsenic
Mg/I
Chromium: Total
mg/I
Grease and Oils
mg!l
Cu, - Copper
mg/l
Phenol
mg/I
Fe - Iron
mg/l
Sulfate 1;1
mg/I
I -Irk - Mercury
mg/I
Specific Conductance
Umhos
K - Potassium-_
ing/I
Total Ammonia
air
Mg - Magnesium
rug/I
TIN as N
mg/l
Mn - Manganese-
mg/I
Ph - baud __�- M9/1
Zn - Zinc mg/l
Ammonia Nitrogen mg/1
Other (Specify Compounds and Concentration Units)
ORGANICS: (GC,GC/MS,HPLC)
(specify test and melhod #. Attach lab report.)
Report Attached" s_(I) No _(0)
VOC method # =
method II
Inethod ft =

Pace Analytical Services, Inc,
r
,98old incey Avpnue Suite 100
Hunter ville n k(,' 2 078
fox 704.E°5.9091
i
DATE:
05125/00
PAGE:
2'
Pace Project Number: 9214056
Client Project ID: 2nd Quarter 2000
Pace Sample No: 92995489
Date
Collected:
05/15/00
Matrix:
Water
Client Sample ID: MW-2
Date
Received:
05/15/00
Parameters
Results
Units
PRL
App.
DF Analyzed Analyst CAS#
Footnotes
wield Services
M,anitoring Well Data
Method:
Prep Method:
Collected 5y
6JC
1.00
05/16/00 SNH
Collected Date
/15/ZOOO
1.00
05/16/00 SNH
Collected Time
1620
1.00
05/16/0SNH
Field pH
6.31
Std. Units
1.00
05/16/00 SNH
Field Specific Conductance
180
umhos/cm
1,00
05/16100 SNH
Field Temperature
18.6
deg C
1.00
05/16/00 SNH
Static Water Level
17.73
teen
1,00
05/1£/00 SNH
Total Well Depth
45.70
feet
g
1.00
05/16/00 SNH
Odor
none
No units
0
1.00
05/16/00 SNH
Field Appearance
turbid
No units
D
1,00
05/16/00 SNH
Well Volume Purged
31&dry
No units
0
1.00
05/16/00 SNH
Wet Chemistry
Total Dissolved Solids
Method:
EPA 160,1
Prep Method; EPA
160.1
Total Dissolved Solids
120
mg/l'
16
1.00
05/17/00 DJR
Chloride (Ferricyanide, auto.)
Method:
EPA 325.2"
Prep Method: EPA
325.2
Chloride
ND
mg/l
5
1.00
05/18/00 RAG
Srllfate,Automated Calorimetric
Method:
EPA 375.2
Prep Method: EPA
3751
Sulfate
12
mgll
5
1.00
05/23100 KAD
Chemical Oxygen Demand
Method.
EPA 410.4
Prep Method: EPA
410,
Chemical Oxygen Demand
ND
Mg/l
25
1,00
05/16/00 CDJ
i
t.a story ertifrc flan I11 L htdatorvLLqi —fI =an1D—s
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NG Drinking Water 37706 This report shall not be reproduced, except in full,. TN LIST fist
SC 99006 without the written consent of Pace Analytical Services, Inc: VA Drinking Water 21

Face Analytical Services, Inc.
�, Ravenscrrarl Dnn
Asheville, N 8801
Phone 828'25 ,. 17
Fax 828 2. Arta l "
DATE: 0505/00
PAGE;:
Peace Project Number: 9312978
Client Project ID: SPECTRUM - 9214056
pace Sample No. 92995489 rule Ctatlected: 05/15100 Matrix;: Water
-Lient Sampte 10, MW-2Cate Received-, 05f17/6
ar neters Results Units PRL Analyzed Analyst GAS# Footnotes
4et Chemistry
Total organic Carbon Method: 5M 5310C Prep Method: SM 5310C
fatal organic Carbon 13 mg/l 2' 05/24/00 AA5 7440-44-0
for to-T eriifi =mn-11 a REPORT OF LABORATORY
ANALYSIS Lnratar vertu[ ! n l
NC Wastewater Ott TN Drinking Pater 0 0
Drinking Water �7i1 This report Shall not be reproduced, except in full, Environmental �e�
without the written consent of Pace Analytical Services, Inc
r __

Pace Analylkal Seivices, Inc,
9800,KncPyAvenuo Sunte 100
aneAnalyfical"' Huntersville, NC 28,378
Phone: 704,87-5909?
Fax' 704,8775-9091
DATE: 05/25/00
PAGE: 3
Pace Project Number® 9214056
Client Project ID: 2nd Quarter 2000
PAPWETER FOOTNOTES
ND Not Detected
NC Not Calculable
PRL Pace Reporting Limit
App. DF Applied Dilution Factor
UhQLaLor1LLrf—if ijaL SnI Lab Lratory CLrtifiqaJgQa ID --- J-s
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 9009G
NC Drinking Water 37706 This report shall not be reproduced, except in lull, TN UST List
S9 99936 without the written consent of Pace Analytical Services, ins. VA Drinking Water 213

The Chain -of -Custody is a LEGAL OOCUMENT, All relevant fields 1dust be compleW accurately.
RaceAnalj6cal 941368
Required Client Information: Section A Required 0ent lnfounatrom Section B [Page: of To Be Cornplaind by PIlco Analyliczlt it rld 010"t Section C
Quote Reference.
Company Report To: Client inlanna Ch k t
P.�wn Manager.
Inv=e To'
'Turnaround wnes less 9hml 14 days subpcl to ect
laborat ry and contractual ob4gafions and 6 may result a
�y —tL— I , 0 -0`i�—,F'10
Project Narnw Rush Jumaround Surchwile,
Turn Around Ttnre (TAT) m cWendar days,
— Requoi—D -"-s—t#rFA dots is
Piro e fax 1ecj Number
FPre�er
Required Client Information: Valgd Marrix Code 0 Preservatives
Section D WATER vff In LU 13
MATRIX 09qE Lu
A 2! , N
0 0 -0
Soft. SL 0 �c LU 2
SAMPLEID OIL OL j-)
WP g.
WIPE C
One character per box. AH a:
0 0
4t AfR 0 " q 11�
2 l-, (1) z
(A-Z, 0-9 TISSUE TS ;T( 0 C 6 Remarks I Lab ID
D U�
Sample IDs MUST BE UNIQUE QT-HER- mm I dd I yy hh� mm a/p '4
�7(/
7-- 00, 1 ,
T 5- �114
Temp in 'C� emp in "C' E-, Y N
let:
Intact:
0
Received on ICE: Y,,,/ N
S e
C
E ooIN
ealed Co
Samples Intact: Y N
LAdditional Comments,
PRINT Name,
SIGNATUR�Lc
REERSE SIDE FOR INSTR6
SEE V
CTIONS
Y A—TE —Sgned—.fM?0 �
.10 0 0
Pace Analytical Ser0ces, Inc, Form COG01 02/00

Face Analytical Services, Inc.
ce Analytical"" 4sl erfl(e, NC28861
Pax: 828 5,? 4618
DATE: 05/2 t t1
PAGE:
Pace Project Number: 9312978
CLient Project ID: SPECTRUM 9214056
FA .AME T ER 'FQCYT�iDTE
hC Not Cetotte
NE Not CatcutabL
P2 Pace Reporting Limit
Labor tor,+ ertificaticn IBIS r .- .P Lti � it
a tewater 5N Drinking Water 02980
N
N Writ Drinking Water 9 719 This report sfrail not be reproduced, except in fuH, SC rrvironrnenntai 99030
without the written consent of Pace Anahyticai Services, inc.

') 0 b 1ti i I I 8 rj I , v d a, J 14 j
I INS=-
'MONITORING.
)RM
Please Print Clearly or Type
For Groundwater Tmalinent Systeniis
ched orte.
0 Influent (98)
El Etflu6tit (99)
Mill WIN Lj1j1t'1MjM!&-Mz
#0
I DIVISION OF WATE It QUALITY
-MMK -eowekltt vhm�
8
'r-, -4�10L Phone: (440 M. 't
N,Q,'I—r-, Values should reflect dissolvedand
colloidal concentrations.
Date sample collected: Date sample analyzed:
Laboratory Narne: PAc-r-
Certification No.
YES NO)
Ni - Nickei---C�)
ma/l
Pb - Lead--
mg/l
Zn - Zinc w..mg/I
Ammonia Nitrogen
MnIl
Other (Specify Compounds and ,,Conlt ".ion Units)
z So
is
ORGANICS: (GC,GC/MS,l-lPLC)
(Specify test and method ft. Attach tab report.)
Report Attached? Yec—(1) No
--(0)
voc method #
mothod
(TIC010d It

!' "'
aciel4nalyfica
Spectrum Dyed Yarns
P.(l, Box 1006
Belmont, NC 2801
F
Pace Anatytie 1 Servives, Inc.
98id,Ki ncey/l enve $blimp totl
untersvrtle, NC280 8
Phone, 704.875.9092
DATE: 02/24/00
PAGE: 1
Pace Project Number, 9211960
Client Project 1D: ist Quarter 2000
{
31
Attnd Mr Terry star
Phone; [phone]
Solid results are reported on a dray weight basis
Pace Sample No: 92847516 Date Collected; 02/15100 Matrix: dater
Client Sample 111. MWI Date Received; 02/15/00
Parameters Results units PRL App. OF Analyzed Analyst CAS# Footnotes
Field Services
Monitoring Well Data Method: Prep Method:
Collected By
JJQ
1,00
D2/15/UU SNH
Collected Date
2/15/'200
1.00
02/15/00 SNH
Collected Time
1200
1.00
02/15/00 SNIT
Field pH
6,33
Std Units
1,00
02/15/00 SNH
Field Specific Conductance
260
umhos/cm
1.00
02/15/00 SNIT
Field Temperature
182
deg C
1,00
02115/00 SNH
Static stater Level
10.27
feet
1.00
02/15/00 SNH
Total Well Depth
26:63
feet
U
1.00
02/15/00 SNH
Odor
none
No units
(t
1.00
02/15/00 SNH
Field Appearance
cloudy
No units
t'
1.00
02115100 SNH
Well 'Volume Purged
3. &dry
No units
6
1.0
02/151D SNH
Wet Chemistry
Total Dissolved Solids
Method:
EPA 160.1
Prep Method: EPA
160.1
Total Dissolved Solids-
180
rig/l
10
1.00
02/22/90 RMN,
Chloride (Ferricyanide, auto.)
Method:
EPA 325.E
Prep Method; EPA
325,2
Chloride
22
mg/l
5
1.0
02/17/00 DJD
5ulfat ,Automated Coldrimetric
Method:
EPA 375,2
Prep Method: EPA
375
Sulfate
16
mg/i
5
1.0
02/22100 Kit
Chemical Oxygen Demand
Method:
EPA 419.4
Prep Method. EPA
410.4
Chemical Oxygen Demand
ND
/l
50
2.00
2/21/00 RM
%borer .� rtlti,a iori ills
NBC Wastewater 1
M6 Chinking Water 3770
SS 99006
without the written consent of Pace Analytical Sar0cm Inc.
RR OF WORM"
ANALYSIS
This rePO4 shall not be reproduced, except in full,
Laufa—toru-'GQtitdCatIGn
KY Drinking Water 9GI090
TNT UST List
VA DrinkingWater 213

Pace Analytical Servicos, Inc.
aceAnalXilcal
Asheville, NC 28,301
Phone: 828,254,71,76
Fay, 2ll. 252 461
DATE:
02/24/00
PACE:
PASI Inc. Charlotte
Pace Project N er:
931108
9800 Klncey Ave.
Client Project ID:
SPECTRUM
- 9211960
Smite 100
Huntersvi t te* NC 280' S
Attn: Project Management
_w
Phone: (C4)5?5-9Q92
Solid results are, reported on a wet weight basis
Pace SarVLe No: 92847516
pate Collected: 02/15/00
Matrix:
Water
Client Sample l M 1
Date Received: 02/1 /00
Parameters Results Units
PRG Analyzed AnalystGAS#
Footnotes
Wet Chemistry
Total Organic Carbon Method: SM 5310C
Prep Method: SM 5310
Total Organic Carbon NO mg/L
2 02/24/00 JDA 440"44-5,
kahCratllr . rtrla :ion litS REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 TN Drirxksric4 W er 02 2,`,
C Srurrlrr Water 37712 This report shad not be reproduced, except err full, En°airar�rrYer• l ���+'�
{rithout the written onseot of Pace Analytical services Inc.

Pace Analytical Services, Inc. a
(7800 incey Aventwo Smite 1,010
Huntersrille, S' 2SO76 a'ceAnalyfical"',
Phone [phone]
Fax T 4. « ;75.9091
DATE: 02/24/00
PAGE;
Pace Project Number: " 2119E9
Client Project ID: let Quarter 2000
PARAMETER FOOTNOTE
NO Not Detected
NC Not Calculable
PRL Pace Reporting Limit
App, OF Applied Dilation Factor
Lab r r rr , t r) 0s REPORT OF LABORATORY ANALYSIS
a r tifiit !� lU;
NO Wastewater 12 KY Drinking W-er 900
NC Drinking Water 37706 This report shall not be reproduced, except in iuH, TN LIST List
Q 99006 without the w6tten consent of lace Analytical Services, inn. VA Drsnking Wa-er. 2`

N1 - NII
ickeL_­11_
I
ORGANIGS: (GG,GCtM9,HPLC)
(SpecIty test and method #� Attach lab raped.)
fleportAttached? Yo;g�(1) No_(0)
voc method
Melhod
fdr Gr6ortMater Tivatmont System
Check MO.,
100rit
_-_RMIT #: EXPIRATION DATE:
Non-Dischar(U e UIC
NPE)ES
JYEEDj-2__rLjM.[U,[-:P_ OPERATION 13EING MONITORED
Lagoon -Rernediallon: Infiltration Gallery
Spray Field - Ramediation-
Rotary Distributor -Land Application of Sludge
Othor,
�Coflloldat concentrations.
Date sample collected: Dole sample, analyzed:
Laboratory Name:
Certification
MINIMUM
all
GW-59 flov. 4190

Pace Anal ffcaf Services, Inc
laceAnalyficafo
9800 Ki'ncey Avenue, Suite 106
quo ws'n;tt°A
71
Fair A04 875.909t
DATE:
02/24100
PAGE:
Pace Project Number: 9211960
-.
Client Project ID: 1st Quarter 2000
_
Pace Sample No: 92847524
Date
Collected:
02/15/00
Matrix:
Water
f
Ghent Sample ID: M 2
Date
Received:
02/15/00
Parameters
Results
Units
PRL
App,
DF Analyzed Analyst CAS#
Footnotes
Field Services
Monitoring Well Data
Method:.
Prep Method:
Collected By
JJQ
1.00
02/1.5/00 SNH
Collected Date
2/15/2000
1..00
02/15/00 SNH
Collected Time
1230
1.00
02115100 SNH
Field phi
5.25
St , Units
1.00
02/15,/00 SNH
Field Specific Conductance
179
umhos/cm
1.00
02/1.5/00 SNH
Field Temperature
15.5
deg C
1.00
02/15/00 SNH
Static Water Level
17.41
feet
1.00
02/15/00 SNH
Total Well Depth
45,45
feet
0
1.00
0 /15100 SNH
Odor
none
No units
0
1.00
02/15/00 SNH
_Field Appearance
turbid
No units
0
1.00
02/15/00 SNH
Well Volume Purged
33,0&dry
No units
0
1.00
02/"15/00SNH
Wet Chemistry
Total Dissolved Solids
Method.
EPA 160.1
Prep Method: EPA
150.1
Total Dissolved Solid's
150
MgJl
10
1,00
02/22100 RMH
Chloride (Ferrid anide auto.)
Method.
EPA 325.2
Prep Method: EPA
325.E
Chloride
ND
rag/l
5
1,00
02/17/00 DJ11
Sulfate.Auto ated Calorimetric
Method:
EPA 375.2
Prep Method: EPA
375.2
Sulfate
10
mg/1
5
1.00
02/22/00 KAAD
Chemical Oxygen Demand
Method:
EPA 410.4
Prep Method; EPA
410.4
Chemical Oxygen Demand
120
rag/l
50
2.00
02/21/00 RM
3
mm Certiflc fine Ir
C Wastewater 12 LABORATORYREPORT OF
NC Chinking dater 37705 This report shall not he reproduced* except in full.
SIC 99006 without the Mitten consent of Pace Analytical Services, Inc.
Laboratory Certifigat on f
KY Drinking "dater 90090
TN UST List
VA Drinking Water 213

Pace Analytical Services„ Inc.
A Ravenscrott Drive
Ash,eville. NC 2880
Phone: 8 8. 8 . 71,
SATE. 02/ 4/00
,r
PAGE: 3^,
Pace Project Number: 9311084
Ghent Prospect Its. SPECTRUM 9211960
PARAMETER FOOTNOTES
NO Not Detected
No Not CatcuLabte
PRL Pace Reporting Limit
i
lturtfofYSIS TN 'ing Vterrinlt7 w
NG Wastewater 40This report shall not be reproduced, except if' full, SC Envuonr°�,P�'tai g °
NG DrMingWater 37712 without the written consent of Pace Analytical Services, Inc;

%.## I A %OlI64 0 1 r% I I 4A I Y k A %w" 1 9 &%a0A-04L A ks%om 9,6
The Chain -of -Custody is a LEGAL DOCUMENT A If relevant fields must be completed accurately.
Tht�Right Qrenfistrv, The Rl�xht '�olution"`
500133
Required client ion: Section A
Client Information:
Section B
Pof
age:
To Be Completed by Pace Analytical and Client Section C
.tWormat—Required
Company
Reportro:
CK UII�TeX
Client Informatrion 'Ch k t / tract
A up a con _')
'TAT3
Quote Reference:
—kess'
Addres?
InvoTce Tw
Requested Due a TAT
rd"
Progict Manager,
11�v
lro,
U_ 14 day m,,m%Tr1d.vbiRrc+ttot
JALO,
Contractual obligations and may resuit in a Rush
project Namw
Turnaround Surcharge,
-nme
Profile JV
Phom Pax
Project Number,
Tom Around (TAT) M calen der days.
Requeste d AnWysis,
9
Section D Required Glient information,
Preservatives
Uj — — —
SAMPLEID
WATER
SOIL
wr
SIL
TV
0
8
t--
Lu
U/
OIL
WIPE
OL
0 0
ft
One character per box,
AM
AS
0 C)
CL 0
(A-Z, 0-9
w Sample )0s MUST BE UNIQUE
TISSUE
TS
2
09
0 C z
n 3: X Z Z
mm I dd I yy mm: tilttiltalp M
R emarks Lab ID
0
[AT t 'higrwa: (MM f uu d T w I
721
Farce ArIalytical Services, Iric Form C0001.XLS 08/98

FEB
18 2000
irk$ " 1. ? lr itiyw SiiBMI t' F ORM ON YE
LISM PAPER ONLY
Fir
l r' r %RM"f
F . "", : e i° r � 4r t Fkllt ill!tli T # F i {C1ld . � l:10, 13 AM) G(% i' l ll�tlT ,
�.1t° CEa -I;r lint , f� ;.� ri a F Al.O. t1011 ti ra .. I �� t,
tiA#;ltifrrlt� I# 7e21a•asPli
EAGIL11I % Pluatsra Plint cidasl y titlylraa
Q �-t l _ ri ` PEFIMI 1` 0: lm t#'fFi t iCliil t A l t T
Facility �talrae.
Pat "lit Naaiae (it d#llaarast ;
1 - r r r Carr Nun-Disc#aarijrr
Fracifflgr Addttass't_— lama NPD
ES
a MO of- [0aoe9 c �01 County Sira PL—Q LLIMLl..IL-112Oi'FHAIION III -I G h1i NII 11E: l
Contact Person: Ter f ��� '! d sa Telephoner � ��- � � � LuUoon Flente #la#icn:Irriallra lon Gal#ery
Well Localloref Site Naaraeo r tad � iloi of ells to noSallipl d: � irrrrry Field Firacr allarirara;
rrcrm r,mra Pnuiaay Distrii ulor I,mld ApOicatloar of Slud o
oil Identification auraiat Ilrorra Perniltl; _tAj or'Groundwater Tiralmerrl Systems three; pre, E
, all Depth: _A(P-L?5 If, Well Ditanaetrir; ­2— In. Check no;
creen d Interval. IL to — ii, I ElInfuse (98) .LValues should rolled dissolved and
LMDjeplah to &dater Level; O it. below rueesaat#riagpoint.- El Intent colloidal concenttallons.
easurinrg Point Is It. shove fated surl ce,tillcirans of waist Pont eratliaiied liafoPe sattallnr. gala stintpia ccllacicIm �lfe ertalaf raraalzect:
elanalysts„ pi I Specific ariciuc#aFiCe allot#eras t.alararafor latrie, d tr
Taint)..._.*d�M Odor ti � Appearance� a edifi aliran No. I
M M (Samples fortnetals were ollecied orifillerod Y 140 arm liela acfdilled YES N
COD 4,25 rrig/l Nllrif ( s C _ mull N1- Nickel trial!
alllarrti. MF Fecal / 1 Veit! Nitrate ( )Pas N ha ll Pb - Leart ttirg/l
olllorun: MF Total _ 1100IT11 PhOsphorus: J'olaal as p in/1 Zil - Zinc __ Pii ll
Itfrrtea else MP U trtelliod rat highly turbid sarrapleal ofthophosphato _ unj/l / rriftitanla Niltogen - rn /I
Dissolved Solids: Total _ InjIll At - Aluminum uFt rtagll Other I aectly oolpaaunds and Concentration t.trattsi
l-I (whon analyzed) urill alltun fig/l Oct/ yit
TOE Mg/l Ca - Calcium ln1g/l � �

tlBMI V L't"tIMI ON YULQW I'API-11 ONLY
r
w C.e+� I'`It f+i�@" K eaa,�., taa.�b st a^e• dd " .i 4 e:,�
6° , r M"—,,rr4
a r�tdSdorrtlf=wrtfErTt�arAttTY sTY J :1.. }.. ° l • .}� G, *e �k• ficanlo 7 aE 10H - f' lttoll n CtMP iMIC ItdTFonw,
:., �,. � � 1�,t1tElratl frr: 7�a .tlTlt •..1�15d3iSP% t 7,�,3�21�t t l ; dtrarse Print f:learly or TypoFacility Narrle; CtFUn 'r, d`� �''� rns- ft: � f_ l _ I PH1 I ION DAI E:
faarrnit Nantta (if dlflesrertt : I �r r� sSifi C a titan fiiactrar e i
I acltft Address:
1 t' tl t c l4lPD i
0 Mo l 1 r r only s r a ILJt LItLtt.l-I l: U OIIt lI l ION I)EIN(A KJON I t RED
>rrrarla t I'erscart. +2r r a,r J11"► i t f rrlrrfr@rr rrr f Lagoon IT rr odiaiian: inlillr tlon Gallery
well Location/ Site hJarne. � �Jrr" cf fields tca taco �rerralalr d: � � �� .3trauy Held OnOw iallart;
r+a+� "'"ra fIota,
y 01stalbolor , Land U trscatloap Of luct€U0
11 Identification NUN nl.aer (Irian Paruill): �� For Groundwater Treatment Systems t� r3tiseu,
rswc"Feened
It Depth: .to-( IL gall Diatueler; I"- hock Onafi
Interval; ft. to . It. � lf�l'IrtrTrTt � dli E-I Values should reflect dissolved and
Li
eptll ttr 4dVater Level: l - ft. below measuring point, f Effluent � � colloidal concerlrratlons,
Meascstlnc Poi t Is ft. a ove land surface, � f f.-1'l�
11 - 1 �-`1
t�allral rrt satin porn el-1/bailed before sarrlplln - -" hale srattllale cnllecletl: --� [ to srtttTlal arlalyzect.
Ield rinrTtysi pI I Specific calltlltclertce 1 I lrh� hos Laboratory Narrtra. Iraq Cam.
Tentp 1 ° , Odor Appearance Gar Codification No.
PA AMLIffla
t anipl� forinatef were collected unflllered YE Alt and field acidified YES NO)
ID ung/I Nitrito (NO2) as N IT1911 till - Nlt koi —
ollfefftt; M fecal _ /I0011ll' Nitrate (NO3) as N ftt /l b - Lea tog/1
rtllferun: MF Total /1001111 Phosphorus: '11,01al as P rltd/I Zil - Zinc C:�L_ 1#0/1
(trader Marx d PII rrlelhod for b1ghly turbid saarmie:) Orthophosphate � ._ nigil Aininonla Nitrogen) rll /1q
Dissolved Solids: Total rtt )tl ` At - Aluminum IIAU/I astir IS aeolly C gnrpounds and Concerlr n U60 )
�-
)rltli altrtler) _ lltWlll tea _ FrtflufTt Ill/1 at tf�
TOC (QAQ_ rng/l Ca - CaIGIUM
Chloride irac /1 Cadmium rrr 11 M,
Arsenic mall C1tron lurrt: Total fa /I Grease and Oils rn /l Cu r CopperrTtt��l
henot flip/l Fe - Iran _ rttr /1 ORGANICS: (G,G /MSj I L )
{lllalt3 nth/l I -lid - tvdttlr trf " ° Ifu A ( Specify test aria nvelliod If. Alltaclr Iata face
Specific C on frr lane rrl` llo K - frt /1 I'leport AllT chet1 'YN) No _ f(0
Total Arnmeonirt trig/l Mg - Ma ntT ltdflt aIgA V C inellr d tt
TIM as N Ing/I Mn - Man ane e _ __ _ Inn/1 inoiliod tf
rnethod It
wrayrraaaa teat AsmlirtrrtxCat AtgQarlt draarta ��rrl t 1810� I'9aa drel11r aaa Irtxe
tilaaaf�arp cst t'r;rraas`94ep tcaa Acxlttualzurl Wl�r~raal ft&,rC�l

Strum Dyed Yarns
P,C, Box 1006
Be'mont, NC 28012
At-.n: Mr. Terry Ward
Pmne: [phone]
Solid results are reported on a dry weight basis
IM111121
T61: 104475�90
6
Fa�xh 704-875-901
DATE*. 12/09199
PAGE- I
Pace Project Number: 9210231
Client Project ID: Quarterly -November
Pase Sample Not 92726629
Date
Collected;
11/18/99
Matrix: Water
Client Sample ID: MW1
Date Received:
11/18/99
Parameters
Results
Units
PRL
......
App.
........
BE Analyzed
... ....
Analyst CAS# Footnotes
..... .... ......
Field Services
Sonitioring Well Data
Method:
Prep Method:
Collected By
RS
1.00
11/22/99
SNH
Collected Date
11/18/99
1.00
11122/99
SNH
Collected Time
1200
1,00
11/22/99
SNH
Field pH
6,27
Std, Units
1.00
11/22/99
SNH
Field Specific Conductance
279,9
umhos/cm
1.00
11/22/99
SNH
Field Temperature
203
deg C
1,00
11/22/99
SNH
Static Water Level
10.95
feet
1.00
11/22/99
SNH
Total Well Depth
26.65
feet
0
1,00
11/22/99
SNH
Odor
none
No units
0
1,00
11/22/99
SNH
Field Appearance
clear
No units
0
1.00
11/22/99
SNH
Well Volume Purged
3,08dry
No units
0
1.00
11/22/99
SNH
Total Dissolved Solids
Total Dissolved Solids
Chloride (Ferricyanide, auto.)
Chloride
Sulfate,Automated Calorimetric
Sulfate
Chemical Oxygen Demand
Chemical Oxygen Demand
NC Wastewater 12
NC Drinking Water 37706
99006
Method: EPA 160,1
200 mg/1 10
Method: EPA 325.2
25 Mg/l 5
Method: EPA 375.2
13 mg/l 5
Method; EPA 410.4
ND mg/1 25
Prep Method: EPA 160,1
1,00 11/23/99 AST
Prep Method; EPA 325,2
1.00 11/23/99 DJD
Prep Method: EPA 375.2
1,00 11/23/99 OJO
Prep Method: EPA 410.4
1.00 11/18/99 KAG
REW O� LASOWOV ANAMIS
This report shall not be reproduced, except in foiti
thii written Consent of Oice�oalytioal Se�hfices, lnc�
7771

l
Tel, 704-875.9092
Fax [phone]
DATE:
12/09J99
PACE
Pace Project. Number: 9210231
Client Project ID: Quarterly
-November
;�:jce Simple No: 92726637
Date
Collected:
11/18/99
Matrix:
rater
:-ient SampTe ID: MW2
Date
Received:
11/18/99
.rameters
Results
Units
PRE
App.
UP Analyzed Analyst
CAS#
Footnotes
---jd Services
Monitoring Well Data
Method":
Prep Method;
Collected 6y
RS
1,00
11/22199 SNH
Collected Date
11./18/99
1.00
1 122/99 SNH
Collected Time
1130
1.00
11/22/99 SNH
Field PH
6.67
Stet. (Inns
1,00
11/22/99 SNH
Field Specific Conductance
236,2
umhos/crl
1.00
11/22/99 SNH
Field Tmperature
17.4
deg C;
1.00
11/22/99 SNH
Static Water Level
19,70
feet
1.00
11/22/99 SNH
Total Well Depth
46.29
feet
0
1.00
11/22/99 SNH
Odor _
none
No units
0
1.00
11/22/99 SNH
Field Appearance
muddy
No units
0
1.00
11/22/99 SNH
Well Volume Purged
27.0&dry
No units
it
1.00
1.112.2/99 SNH
'mot -Chemistry
Total Dissolved Solids
Method:
EPA 160.1
Prep Method: EPA
160.1
Total Dissolved Solids
160
mg/l
10
1,00
11/23/ 9 ASS
Chloride (Ferriryanide. auto.)
Method:
'EPA 325.2
Prep Method: EPA
325.2
Chloride
ND
rag/'l
S
1,00
11/ 3/99 DJD
Sulfate„Automated Colorimetrid
Method:
EPA 376.2
Prep Method: EPA
35.
Sulfate
9.4
Mg/1
S
1.00
11./23/99 DJD
Chemical Oxygen Demand
Method:
EPA 410.4
Prep Method: EPA
410.
Chemical Oxygen Demand""
ND
mg/1
25
1.00
11/18/99 KAG
NC Wastewater 1
NC Drinking Water 37706
SC '006
REPORTKY Drinking Water 90090
��boratory �iit�tiear� �97
TN LIST List
This report shad not be reproduced, except in full,, VA Drinking )"Water 213
without the written consent of face Analytical Services, Inc,

Pace Analytical Services, Inc,
900 Gemini Avenue
Houston, TX 77058
TO 81-488-1810
Fax: [phone]
DATE: 12/0819
PACE
:eate knalyticat Services, Inc.
Pace Project Number: 851299E
1'800 k;ncey Avenue
Client Project to: TOX/9210231/Spectruis
-Ate .00
�,4nte"svi l l e, NC 2807
4t'tn. 141. t;nerri Howard
:°^cane; f70y875-9092'
,vtio results are reported can a wet weight basis
>ace sample No: 851251355
gate
Collected:
11118199 Matrix:
Suter
rtient sa ` Le I0., 726629/MW-1
Date
Received:
11/19/99
Sara tern
Results Units
PRL
Asp.
DF Analyzed Analyst GAS#
Footnotes
wet Chemistry
Total Organic Halogens
Method: EPA 9020B
Prep Method: EPA 902013
Total organic Halides
7.2 ug/l
5
1.00
1 /03/99 KMUI
ace Sample No-, 851251363
Date
Collected:
11/18/99 Matrix:
Water
�!Jent Sample tom 7 6637/MW-2
Date
Received:
11/19/99'
oararreters
Results Units
PRL
App. :
DF Analyzed Analyst CAS#
Footnotes
wet Chemistry
Total organic Halogens
Method: EPA 90208
Prep Method: EPA 902013
Total Organic Halides
ND ug/t
5
1.00
12/0 /99 KMUL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services; Inc,

Face Analytical Services, Inc,
4 Ravenscrott Greve
Ant
Ica
Asheville, SIC 28801
Tel: [phone]
Fax: [phone]
DATE: 11/24/99
PAdE: 1
PA.S1 Inc. Charlotte
Pace Project Number:
93943 '
9&"�,D Kincey Ave.
Client Project ID:
Spectrs 9214231
S,�-te 100
II:tersvi t le, LAC 28078
Attn: Project Management
P'none: l704l875-9E92
Solid results are reported on a
wet Freight basis
P .e Sample No: 93414332
Date Collected 11/18/99
Matrix: Water
Client Sample eta: SPECTRUM
726629 MU1
elate Received: 11/19/99
Parameters
Results Units
PRG Analyzed Anatysr CAS#
Footnote
Wet Chemistry
Total organic Carbon
Method: EPA 9060
Prep Method: SM
5310C
Total Organic Carbon
6.6 mg/t
2- 11/23/99 Jf1A 7440-44-0
Laboratory ,ertih aWm IDS bor tcry erklNtAtler+ ll3s
NC Waste -water 40 REPORT OF LABORATORY ANALYSIS N Drinking haler 02
NC Drinking Water37712 This report shall not be reproduced, except in fall, SC Environmental 99030
wrrthrat the written consent of Pace Analytical Services, Inc:

Pace Analytical Services, inc,
34 Raverascrott drive
Asheville, NC 28801
Tel: [phone]
Fax: [phone]
DATE: 11/24/99
PAGE: 2
Pace Project N nrber: 939432'
Client Project ID: Spectrwn 9210231
mace Sample No: 93414340 Date Collected: 11/18/99 Matrix: later
:Henc Samlole tD; SPECTRUM 726637 MW2 Date Received: 11/15/99
�arwvzers Results Units PRL, Analyzed Analyst CAS# Footnote
.yet Cnemiswr
'fatal Or anic Carbon Method: EPA 9060 Prep Method: SM 5310C
Total Organic Carbon RD M911, 2 11/23/99 JDA 7440-44-0
�` t rtilactitrn IC3R
C Wastewater Ott
NC Drinking Water 37712
REPORT OF LABORATORY ANALYSISTN Drinking Water 02980
This report shall hot be reproduced, except in full, SC Environmental 99030
without the written consent of Pace An lyticai Services, Inc.

t`���llw�t ttft
it tAttaiyukwW.
The
Chain -cif -Custody is a LEGAL DOCUMENT All relevant fields must be completed accurately.
'lie Right '"iratarai" t,11, 77je ffight ,`iedraaiwi'°
4952
Required Client Information: Section A Required Client
Informattlaw
Section B
Page: ��
Ffr tits t talrncw � {'�rro 5 tf14t ,ut � �� i ! � k
�.._.....o (1k.»sty
�� �
o �..._._ m� ... ...
company -'rr J'F, �r 7 Report TO: !
%r f �""� +�*Ja✓f
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touotp Rplprppop.
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knvrke�p 'r+a:_
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TAT
�"r�p�GY 14Ap>ram g
�.�
Under 14 day l urnarorund scublml to Islx
F'rrga rt�
contractual obligarijohS and may rpsutt in a Rush
f+" ct a*Tn '
Turnaround Surcharge.
proble 0::.
Trim Around Time (TAT) In calendar days,
Ar
�
pt ranee Fax Project Number,*
Requested Wp
Section Required Client Inloumation:
Valid Matrix Cordes -u ---_�,
TRIX qQ AE
C5 iPreservatives� ✓ " '
Lu
WATER+hrT
i
One character r box,
R
11aF
R
we
An
cc
�
0 sx
�
w (A— 0-� �
TISSUE
TS
C
ra
g $� p
pyy y jLab
GSG"ri M6Le IS3SLd
Remarks
Sample IDs MUST E UNIQUE
s��rl l�:....,u,.
fir_ _.
mm t dd ! yet trrn`hh sip
_
�-,
�'
yr" i✓.
FL
Bangle Condition
ufGN�.TUFi� ii
SEE RELEASE SIEGE FOR INSTRUCTIONS
O1,�
DATE ign d. (MM t 1
Dace Ana}ytical Services, Inc. Form t

Pace Analytical Services, Inc.,
9809 Psncey Avenue, Suite 100
Ica I
Huntersville NC 28978
Tel: [phone]
Fax:[phone]
DATE! 12 9/99
PACEd
Pace Project Number; 921923
Client Project ID: Quarterly -November
FCCiTNl1iE
PAP METER �
RD Not Detected
r4c Not Calculable
FEE Face Reporting Limit
App. 11F Applied Dilution Factor
Lgiboratory Qertfficgt0JJ2a
NC Wastewater 1REPORT
hit # erti + ati+ n It s
OF TORY ANALYSISDrinking Water 090
NC Chinking Water 770
TN LIST gist
C 99006
This report shall not be reproduced, except in full„ VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

mmm
sIt Identification Number Ilieani aimill: L1V for CFttt6rq&tw3ter irealmerrt Systemsila�r
Well Di,araaeate
e: _
Iri. (A1eCk one:
raeraset Interval; Ite to __ _ j.
"Dslaltr to Water Level: It below r ieasFFillag poliitt`
1­1 Influent 1 )
tjQj -1 Values should reflect dissolved and
t Measiar#rlct I aliat #sq— it. above land surface,
EffIttettt 199
colloidal concerdralion s.
tI �
�'`'ilw:
Gallons of �
1aelrrae �
17aatea saiFn x
�
.�. trite salrr rte ariaf
y � '
sie1analysis:tar �llsrralrer�ctrr►Ite�et
t
�artar��li�r4i';;
q t ill C n tier,#ancee _...
i'
+rt��w.:�.�.�
i�, � t
rrttiaeas
#.artaars#carl~li�tarise��leae#:._;�
y
. t'�rl�.l ��..
l
smite. 11
* , Odor - rt Appeaaranco a t . ! ,
Ge dfli allon No.
'PAIMMETE.H5 l aaarnples for rnalars were acallectaari untiltaraacl — Y a , _#lei .
aand tlold a cidilled
--YES Eta NO)
°
COD�
r mg/1
Nitrite 02 s N _
MU/1
NI - Nickel
lI
r 111 rrlt;Fecal
'Fatal
_ / l t olltl
Nitra lra NO,, its M
Ing/1'
Pb - t_ ar
1 11
olll rm: MF . _ _.
_ l t (l llttl'
I'llr sl llril �. r "t ril l ray
Irl ll
art - lrtr
t�i 1
ric h u r pli (11filhod iue Wrii ly tearaatcl Samples)
trlltiil�l trial allrilil �.
Fri /l
,rtt#rfear�l Nitrogen
ill
Dissolved It+t e1 tatlel Total
_ .... tiirlll
t litltllriiirlt a... _
� �. urg/1
t 111 r (Specify Compounds and once Bt llrar�� ails)
pli (a�tl�eirl ati'll�+ el .__
_ Mplap 1
I:I
l
i a .. __�.._.
(rr(p/l
o — t"rrlr{l#fill
Chloride..� _� �
rm/I
Cd- Cadmitim _ �
Frig/1
Arsenic w
Grease
_ Ill/1
Irrrirtilirrn: Total
afidOils
I't41/1
Gil -
phenol � �
� bill/I
F0 - Irealt M �.� � �
��. � lilt1/1
I1 NIGS: I C,GC1M a [PLC)
I to - Merri,ilry
iatlrjlPl
(Specify
lost rrel rrralla e, Attara Isla roporl.lspeciie
Fai/I
I'lepartAllached " __(1)
ta (O
Total rm rFili,
rrilf/1
�tr l� tvta Fter�lirrrr
rrtcl/1
Jc ralire0 .
tKN as
inelhad it .
inerh ad # -
Lm
1
GW-59 rlev, 4/91t

k[F- TYMON11,011ING.,
fj'Q Ll A I-
11
EAWL11-Y-111EQUIATIQU Ploase P11111 Clearly or Typo
� v Q d (-L (1, 1 t)(cf, Ycvrri�
Facility Name-,--- ---�4
Painnil Naum (it dlikike 1"to(k
Facility Acldross�- VJ fl'(
r r a l l eatk6-
Telephone
Well Localioirt arts I Mine: No, of Wells to no Sampled:
SE11 Idenflilcallon, tfinubar (front Perinilp _jjj&Lj—
It Depth.,-121a IL Well tflaincler,
'reened Interval: IL to It.
Ile Fib h to Water LeveL -LI It. below rurrasuf Ing Writ. Me
-astjrinfj Point Is it, above land surface.
�allons 01 water pumped/bailed before smopling.- 3-0 1
j
For Groundwater Dealment Systems
ha. Check one;
[A Influent (90)
El Effluent (99)
I) I-. 44.L , , - # JIU6 Ili UM UMance
I amp, Oder Appearance A —6�
WATEn OUALITY"
M
VEFIMIT M EXPIRATION DATE:
Nan-Dischatge RI l co) (X)os' UIC
NPDES
J P. -,QE1EDldI1j1Q OPERATION BEING MOM ronED
-�,4— Lagoon —flernediallon: Intilltallon Gallery
Spray Field Hornediallan:
nanny Dhidbulor Land Aprificallon of Sinclair
tlQ_IE.- Values should reflect dissolved and
colloidal concentrations. Cf I- � - "
Dalo sample coliecled: --2-LiLLU D is
1105 Laboratory Ne, amOfNci�!37
U
JILIA(rl (('k Gerlificallon No.
PABANIFITE115 (Somplos for naelaha were collected unflitered—YES NO ,
and field a0diflod
GOD
I'liq/1
Nitrito (NO2) as H
Coillafrw MF Fecill
Ffilrale (VIO.
3) as
CoIllorm: MF *1 olid
/100[h]
Phosphorim Total as P-----
ing/l
JIM#; use MPII 111411tod lof h1ohly bubld
samf46*1
00hophosphato
ing/I
Dissolved Solids: l'otal
fligIf
Al - Altunintim
nig/l
[A I (Whell anafyzu'd ro.Ifflits
Ha -
ing/I
TOG
futill
Ca - calcitial
rig/1
filu'll
Cd - Cadaduni
Mg/I
Arsenic
nigil
chrorrillitil: 'I Olaf
Greaso and Oiks,
... ..... nlg/l
Go -
Ing/l
Phonot — --- --------
11111/1
1 - a - I r o I 1
(11(111
I I Ig/I
I I if - M e r c i i t y
rm 1 1/1
Sp e cl Ile C 0 n (I t I C I i➢I lc: 0
it M I 10 a
K - Pot
Total Arnmorflij
111f 11
U
Mg - Mrigriositiro
RUA
P
TIM as M
1110/1
I'Vill, - maiq) alleso
nql/l
YES NO)
NI - Nickel
Pb - Leari
'MgA
Arnmonla Nitrogen
'Pg/f
ifig/l
Other (Spectly Compounds and Gone -" "bail WIT Urills)
2:3
OTIGANICS: (GG,GC/MSjlPLrC)
fSpecify lost ant] method Al. Allach lab toportj
I'leport Atlaclied? Yes —(I) No (0)
voc method It -
method # -
method It -
I

r, y PA
PEER ONLY IWAY TO A15
QUALITY MONITORING*
oWSION 6F WATER OOALITY
GROUNDWATER SECTION ; PERMITS AND COMPLIANCE UNIT
,GROUNbWATER
COMPLIANCE REPORT FORM
RALEIGH, NO 27C26-0578 Phone: f919) -733-2221
FACILITY INf!_Qa­_MA1LQ_t4 Please Print Clearly or Type
EXPIRATION
Facility Name, 0 A,
PERK411i 00: DATE:
Non-Dis harge—_,_UIC
Permit Name (if diffqrenf):
NPDES
Fa 1 A
�ou V.,
OPERATION BEING' MONITORED
n ty�
y
Lagoon _Rerne�falion: lnfillrat�on(3allery _o
t P_
a �r e eph n -
Coot n, one
parson.
0. of �'Vel
Well on S,Et e Nlame, Wells to be Sampled, _2
i
Spray Fie�d Rerriediation:
�`6,
Rotary DmIributor —Land Appli--al i
Well Identification Number (from Permit): For Ground%2ter Treatment Systems
Other:
Well Depth., ft, Well Diameter: in, Check One -
ft, ft.
JUL 29
Screened Inter to 0 Influent (98)
Values should reflect dlssolved and
Depth to Water Level: It. below measuring point.
0 Effluent (99)
colloidal concentrations.
Measuring Point is tt above land surface,
& -I 7-q q
Gallons of water pump ailed before sampling:
Date sample collected: Late sa'rriple,priaiyz#!:�:�
Field analysis: Specific onductance ufAhos
L3 boratory Name: _RA R
Temp. _2=LOC, Odor. ,Appearance kKl
Certification No.
a (Samples for metals we
EABAM.=j;-3 -re collected unfiltered —YES —NO
and field acidified
COD
mgn
Nitnte (NO2) as N
mg/I
Coliform. f,4F Fecal
/I 00ml
Nitrate (NO3) as N
mg/l
Coliform: MF Total
/1 00ml
Phosphorus: Total as P
mg/I
{:Mott Use mpN rnethod for highly turoid samptes)
Cirthophosphate
mg/I
Dissolved Solids: Total r-r mg
At - Aluminum
mgA
pH (when analyzed)
units
Ba - Barium
mg/l
TOC _jz_
mg11
Ca - Calcium
mg/1
Chloride <
mg/l
Cd - Cadmium
mg/I
Arsenic
mg/I
ChromiumTotal
mg/I
Grease and Oils
mg/l
Cu - Copper
mg/I
Phenol
mil
Fe - Iron
mg/I
Sulfate
mg/I
Hg - Mercury
mg/I
Specific Conductance
0.1hos
K - Potassium
mg1
Total Ammonia
mg/l
Mg - Magnesium
ring/I
TKNasN
Mg/l
fAn - f,,`langanese
mg/l
pndufto the po"Miyattmesaw "Iftv'""'!W
—YES NO)
Ni - Nickel
Pb - Lead-
Zn - Zinc
Ammonia Nitrogen
Other (Specify Compounds
7—,. A— I — I—V
E
ORGANICS: (JtCGC"SHPLC)
(SpiacIfy1est brid method 9. Attach tab report)
Report Attached? Yes_(I) Nd_(0)
VOID method 4
method #
method #

PAR Laabcsr tfori sr Inca
2217 arahom Park drive
LABORAWRIES WC PO Box 411483
Charlotte, NC 211 1-1453
hone: 704- 88-5333; Fax: 04 88�833
NC COO a 20, SC C ee f # 99(,703001
REPORT OF ANALYSES
Attn: TERRY WARD
SPECTRUM DYED YARNS (BELMO ) PROJECT fE: N 99
PO BOX 1006 DATE: 00/15/99
BELMONT, NC 1501 MONITORING WELLS
SAMPLE NUMBER- 13990 SAMPLE ID- SiY MW-2 GRAB AMPLE PIATRI
LATE SAMPLED- 06/03/99 TIME SAMPLED- 1420
DATE RECEIVED- 06/03/99 SAMPLES- GREG JOHNSON RECEIVED BY-- ML
TIME RECEIVED- 1520 DELIVERED - GREG JOHNSON TYPE SJV41PLEGrab
Page 2 of T
ANALYSIS,
ANALYSIS METHOD DATE TIME BY RESULT UNITS
FIELD TEMPERATURE THERM. 0 /03/99 1420 GJ 21 degrees E
R VALUE EPA 150.1 1 /03/99 1420 GJ 6.5 units
CHLORIDES EPA 325.3 06/1.0/ 9 1000 MIS < ,10 P rt
CHEM-OXY.DEMA14D EPA 410,4 0 /11/99 1350 CT 11 P
pm
TOTAL DISSOLVED SOLIDS EPA 160.1 06/07/99 1350 CT 269 ppm
SULFATE EPA 375.4 06/09/99 1510 CT 18 pprn,
TURBIDITY EPA 180,1 06/0,4/99 1E10 CT 2.70 NTU
NOTE: TOO RESULTS WILL FOLLOW WHEN COMPLETED
LABORATORY DIRECTOR

PAR Labc>rcitcries, Inc.
2217 Graham Park Drive
:ha0ott G 282-41-1,488
Phone, 704 588 8333; Fax- 704-. 88-8335
REPORT OF ANALYSES
Attn. TERRY WARD
SPECTRUM DYED YARNS (BEL ONT) PROJECT NAME:
PO BOX 1006 DATE: 06 29/9
BELi4ONT, NC 28012-
MONITORING,WELLS TOO RESULTS
S
SAMPLE PER- 14337 SAMPLE ID- MW-:2 GRAB SAMPLE KATRI - W
LATE SAMPLED- PLEB- 06/17/99 TIME SAMPLED- 13E8
DATE RECEIVED- 0 /1"7/99 SAMPLER- GREG JOHNSON RECEIVED BY- 1^iT.
TIME RECEIVED- 1425 DELIVERED BY- GREG JOHNSON TYPE SAMPLE- Grab
Page 2 of
ANALYSIS
ANALYSIS METHOD PATE TIME BY REEI.7LT UNITS
FIELD TEMPERATURE THERM.. 0 /1"7/ 9 1350 GJ 21 degrees
pH VALUE EPA 150.1 0 /17/99 1350 GJ 6.5 writ
TOT.ORGANIC CARBON EPA 415,1 0 /29/ 9 0900 PAK 1.10 mg/L
LABORATORY DIRECTOR

F—
CHAIN OF CUSTODY
tABORA TORIES, wc PAR Laboratories, I no
wm� Phone [phone]
W
Lmi Fax [phone]
www.pariabs.com
Shipping: Mailing;
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
it is essential that all Information recorded an this Chain of Custody document (Or acceptance by PAR Laboratories, Inc and the Norih
Carolina Department of Environmental and Natural Resources.
Corm
n, Name lblln) COMMENTSiSPECIAL
INSTRUCTIONS
4ddrea
P
City, State & Zi'p Code
4—
oi,%' It T e i-p 7-1
—L<A—�o
Point of Contact & Tale Number
v
Sample taken by:
IS THIS FOR STATE or EPA REPORTING? YES NO
*Sample type, DW _ WW G4fd!MW25� HW_ Sofj— it
Sample Temp upon receipt: OC
Preserved: YesK No
— Teflon Lineri zero Headspa ce: Yes _ No N/A
f1,,e­ptS-8Mp le I . ()�- — — I—
S more Set Up Collection Analyses
Sample Location I Number) Comp Grab Present. Date/Time DatelTime Requested
-1 -713 3 0 &
C =Composite G =Grab DW =Drinking Water WW =Wastewater GWMW =Groundwater Monitoring Well sitar = Hazardous Waste
See Other Side

p
LL
CAROLINAENVIRONMENTAL LA' BORATORIES, U
FINAL REPORT Or ANALYSES�-
PAR Laboratories, Inc. PROJECT NAME- June 1999
Arms: Margaret Rice REPORT Ohm 89999
PO Box 411453
Charlotte, NC 28241-1483
SAMPLE BERG- 13262 SAMPLE 1 - 14337 MW-2 SAMPLETRIX- GW
DATE PL D- 85/1799 TIME PLED- 1350
DATE RECEIVED- /18/99SAMPLER- acre Johnson 'RECEIVED Y- HCG
TIME RECEIVED- 1135 DELI ` D -- UP
Page 1 of I
YS IS
ANALYSIS MBTHOD DATE BY RESULT UNITS LRL
Total Organic P 118 06/ 9 "99 PAX, 1.10 L 1.
L L Lower Reporting Lima
LABORATORY DIRECTOR
229 N rtlr Horner BoulevarJ, Satiforl, North Carolina 27330 919/776-1880Fax 1 -
NC "rtGV 306 NC DW 37741 SC 99035

i F 0;z
GROUNDWATER QUALITY MONITORING.
comPLIANCE_ REPORT FORM
�B:'-iiily Name--
Fe-Mit Nlame 1'�'
Well Loaationj Siie
PfEz-ce Prh-I Clearly or 7,),Pe
7
eiephone
NC. of Vieft to be Sampled.-
Well Identifiz,Zt1or', t'4jar (from Permit):U] �` �P�ee .094 1
L De meter- -
Vvlelf p1h %,Vell '-Ea, _r. in,
S:reenetl tt,
Depth to Water Lever 0 ft. belowmeasuring pxnt,
Measuhn) F':Jnt s ft, above land surface.
Gallons of water purn 'dafl ej dr
11 t , i tiefore sampling-, 3
Field analysis: pH - L Specific Conductance
ALITY,
M26_057a Phnno- ftrol z sus
PERMIT EXAPIRAT ION DA7Z
Non-Dischaute —y—tilc
14 P D E- S
Lagoon Rerns 41ailon: Gallery
Spray Field _;ReT;atian:
RctarY DiVribulDr — Land Anp5cation, of Siudge
For Groundnter Trm.atnerit Syste:r, 01her,
El -
Che_-kOne:
0 Influent (908)
13 Effluent (991
era. r oC, Odor APPearance
Values should reflect dissolved and
-orloidal conceintrallons.
data SaMple Colie::1 e-4,
at sa" ana&j:
C= 6M
Certification Na:
EA, 13arnples for metals were collected unfiltered_YES -NO
and field acidified
COD
Mg'q
Nitrite (,NOs) as N
Mg/I
colito"Mi .. IAF Fe�a-1
1100ml
Nitrate (NO3) as t4
M g/I
Coliforrn: MF Total
11 Domf
Phosphorus: Total as P
mg/l
(Note. Use MPN melhod bar highly tumid %arnpilesj
Dissolved Solids: Total mg,11
Orthophosphale
Aluminum
mg/I
Mg/I
pH (when ana!yzedf)-
Ljnjls
Pa - Barium
mgM
TOO
Mg/l
Ca - Calcium
rn g 1
Chloride
Mg/1
Cd - Cadmium
mg/I
Arsenic
rng,'I
Chromium: Total
Mg/l
Grease "and Oils
mg/l
Cu - Copper
Mg/I
Phenol
Mg!I
Fe - Iron
Mg/I
ilin 0.4 Afi
Sulfate
Mig""'I
leg - Mercury
mg/I
Specific Conduct-ance
0,1hos
K - Potassium-
mgA
Total Amrnor,-ia
"n g.1
f,1g - J`,�Iagnesium
Mg/I
TKN as N
mg'l
fAn - t,langanese
rng/'l
-Y=SO
N)
W4
M - Nickel
Fro - Lea
M
At-nmonis Nitrogen
Other (SPe:Ify Com,Pouncls
ant C�,nzentraltin Uni's)
ORGANICS: (GC,GC,'fAS,HPLC)
(Specify test end method #. Attach lab report°)
Reporl Attached? Yes_(1) 1`40
VOIC method
�� =
m et h o d 0
method
'e
Gk%1-59 Rev, 4!f49

PAR2217
PAR Laboratories, s, Inc.
Graham Park Drive
LABO �ATOPIE n ass
PO Boas411483
hartotte, 28241-1 8
Phone: 7'04-588.8333; Pax; 7`04-588-833.5
Nip Corr # 20 C Con # l030o j
REPORT OF ANALYSES
Attn: TERRY WARD
SPECTRUM DYED YARNS (BELMOINT) PROJECT N E s JUN 99
PC RCN 1006 DATE: 0 6/ 1. 5./ 9 9
BELMONT", NC 28012-
MONITORING WELLS
SAMPLE NUMBER- 13989 SAMPLE ID- STAY W- 1 GRAB SAMPLE MATRIX- W
DATE SAMPLED- 06/03 99 TIME SAMPLED- 1440
DATE RECEIVED- 06/03/9,9 PJQLER- GREG JOHNSON RECEIVED BY- ML
TIME RECEIVED- 1.520 DELIVERED BY- GREG JOHNSON TYPE SAMPLE- Grab
Page 1 of
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
FIELD TEMPERATURE THERM. . 06/03/99 1440 GJ 20 degrees C
pH VALUE EPA 1SO.1 06/03/99 1440 GJ 6.4 units
CHLORIDES EPA 325.3 06 1.0/99 1000 ML < .10 pp
CHEM,OMDEMAND EPA 410.4 06/11/99 1350 CT 4 pp
TOTAL DISSOLVED SOLIDS EPA 160.1 06/07/99 1350 CT" 123 ppm
SULFATE EPA 375,4 06 / 09/99 1510 CT 10 ppr
TURBIDITY EPA; 180,1 06 "04/99 1.610 CT 5.30 NTil
NOTE: TOG RESULTS WILL FOLLOW WHEN COMPLETED,
LA130RATORY DIRECTOR

PAR Lc;borcitcnies, Inc.
PAR 2217 Graham Park Errve
CARGR TORIt~ ,air . PO Box 411483
Charlotte, NC 282 1-1453
Phane..704,588-8333„ Fax: [phone]
REPORT -E ANALYSES
Attu: TERRY WARD
SPECTRUM DYED Y (BELMO T) PROJECT NAME-. ,1U14 99
PO BOX 1006 DATE 06/29/9
9ELVIONT, NO 28012
MONITORING ,WELLS TOO RESULTS
SAMPLE NUMBER- 1 336 SAMPLE ID W- 1 GRAB SAMPLE N1ATRI - WA
DATE SAMPLED- 06/17/99 TIME SAMPLED- 1335
DATE RECEIVED-- 06/17/99 SAMPLER- AEG JOHNSON RECEIVED BY- ML
TIME RECEIVED- 1425 DELIVERED BY- GREG JOHNSON TYPESAMPLE- Crab
Page 1 of 2
ANALYSIS
ANALYSIS S METHOD DATE TIME BY RESULT UNITS
FIELD TEMPERATURE THERM. 06/17/99 1335 GJ 20 degrees C
pH VALUE ERA.. 150. 06/17/99 1.335 GJ 6,5 units
TOT.ORGANIC CARBON BO EPA 415.1 06/29/99 0900 PAK c 1.00 /T
LABORATORY DIRECTOR L 8 �e- e- �

CAROUNAENviRoNmENTAL
LABORATORiEs,
LLC
FINAL OF ANALYSES
PAR Laboratories, Inc. PROJECT WAKE: June 199,154
Atta- Margaret Rice REPORT VAT8 06/29/99
PO Box 411483
Charl tt , NC 1-14 3
SAMPLE ER 13261 SAMPLE ID- 14331E _ . SAMPLE MATRIX- CW
DATE SAMPLED- 06/17/99 TIME SAMPLED- 133
DATE RECEIVED- 06/18/99 SAMPLER- Greg Johnson RECEIVED Y- HCG
TIME RECEIVED- 133S DELIVEREDBel- UPS
Page 1 of I
AUALYSIS
ANALYSIS METHOD DATE BY RESULT UNITS LRL
"Total Organic Caren 5310 9/99 PAX 1.00 /
LRL v Lower Reporting Limit
LABORATORY DIRECTOR
1229 Notth Horner Boulevara, SanfcrJ, North Carolina 27330 919/775-18$0fax[phone]
1 SC 99035

11 CHAIN OF CUSTODY
PAR
"BORATORIES. INC PARLaboratories, Inc
Phone( 4) 588-8333
Fax 4) 33-33 a
wWW-Paa s. tit
Shipping:
Mallin
2217 Graham Park Drive Pit Box 411483
Charlotte, NC 28273 Charlotte, NC 2 241-14 3
tt is essential that ati mforrnatmn recorded on Mir Chain of Custody document for acceptance by PAR Laboratories, Inc: and the North
Carolina Department of Environmental and Naturat Resources,
Company hdarrte iilingJ
OMM TSPSP IAL
w l TRUCTIONS,
Address
City, State Zip Co + 2-
Prnnt of Contact & Telephone Number
Sample takers by:
IS THIS FOR STATE or EPA REPORTING? "DES X NO
*Sample type: W ' M HW Sall Other
Sample Temp upon receipt:
* « Preserved: 'des . X— No Teflon Lined Zero He dsp ee: "des — No N/A
I ens a gle l l]. Set Up oile fion Analyses
(Sarng le Location 1 Number) Comp grab Preserv. Date/Time Date/Time Requested
Relinquished by: I3atelTrrrte lie tied by l aQert i�te
Re nquished by:
l7ateJTime Fie t ed by l�ateiTinte
=Composite G ==Grab DW=Drinkinq Water WW=Wastewater GWMW=Ground ater Monitoring Welt HWHazardous Waste
. * See tither Side

ATE R QUALITY MONITORING:
CE REPORT FORM
�[_y t Please Print Clearly or Tilpe
�asilily "came'.
F%ermit Name (if, ciffe­?nt)e:
Well identifisatQn Nurnber (from Permit): For Ground%sler Treatrnent Syslems
Well Depth: —ila _.ft. Welt DTarneter: Che:k One:
Screened —&— ft. to —&92— ft, 13 Influent (93)
Depth to Water Leve�, /_M_ft bei-ow rneasudrig pnint, 13 Effluent (99)
Measuring Point is J— fit, above land sunrace. —
Gallons of water pumped tailed beefora sampling,---j—
'Field analys's: PH Specific Conductance Mhos
Zl—'C, Odcr APpearance
'V
,>5_057 a Phone*. (919) 733-2,221
PERMIT "-: All V EXPIPA7 ION DA-7'E'_
Non- 0ischargeX_U`1C
NPDES
ELP�=OF P RMI—M =71 OPERATION f�jL-)NITOR:�9
Lagoon irjriitrztion
Spray Fietd _:;errie-dialion:
Ro"ary DstribLjtor —Land Anppli:aliori of Siude eill
01her:
Values should reflect dissolved and
colloidal con.-entration.s. �40
Data sample colle--led,
Laboratory Name: 10,4,0 k,4A
Certification No.
A M = 7 collected unfiltered —YES No
(Samples for mea!s were
and field acidified
— YES NO)
_R
COD
mg/l
Nitrite (NO2) as N
Mg/I
Ni - Nickel ric I
Coliforrn: MF Fesai
1100ml
Nitrate (NO,3) as N
Mg/l
Pb - Lead........
Coliform. NIF Total
/1 30MI
Phosphorus: Total as P
rn, g ,'I
M�g
Zn - Zinc "j
(Note: Use MPN methos for highiy WrDld SSMPleS)
Orthoph-osphate
mg/I
A
Ammonia Nitrogen g1l
Dissolved Solids: Total __g,l
A] - Aluminum
mgA
Other ispecify OMPOUn-C'S ant C,071ZeT`,*7s,i-_n U;Ii'S)
pH (when ana!),zsip) ____6_,_2__uni1s
Bin - Barium
M g,�1
TDC
Mg/l
Ca - Calcium
rTig!l
Chloride
1`19=tl
Cd - Cadmium
mg/l
Arsenic
M91"l
Chromium: Total
MgtI
Grease and &1s
mg,11
Cu - Copper
Mg/I
Fhenol
Mg,"I
Fe - Iron
mg/l
ORGANICS: (GC,-,_,C/fAS,HF1LC)
S S talie Mg/I
Hg - Mercury
rn g/I
(Specify test bnd method #. Attach lab report)
Specific Conn uctanCe
uf,lhcs
K - Potassium
mg�l
Report Attached? Yes _(1) NO — (0)
Tol,31 Ammonia
Mg!I
tlg - Magnesium
mg/I
VOA m e!ho d
TKIN as N
mg'l
tart- Mlanganese
mg/l
rne*,hod9-_4iLq_C
method
Gw,59 Rev- 4".--9
112 / 2- -,y ,�
Pe , nnnf�e iw Paj1huRt,,e1 Ageno NJ,�, -� Me - PZise pr;ni or type
ITT-1)

PAR Laborotories, Inc.
2217 Graham Park Drive
PO Box Al IA83
Charlotte, NC 28241-1483
NC Cart # 20, SC Cert # 990=0 I
REPORT OF ANALYSES
Attn: TERRY WARD
SPECTRUM DYED YARNS �RELMONT) PROJECT NAME: MAY 99
PO BOX 1006 DATE: 05/18/99
BELMONT, NC 28012-
MONITORING WELLS
SAMPLE NUMBER- 13249 SAMPLE ID- SDY MW-1 GRAB SAMPLE MATRIX- WW
DATE SAMPLED- 05/03/99 TIME SAMPLED- 1305
DATE RECEIVED- 05/03/99 SAMPLER- GREG JOHNSON RECEIVED BY- ML
TIME RECEIVED- 13SO DELIVERED BY- GREG JOHNSON 'TYPE SAMPLE- Grab
Page 1 of 2
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
FIELD TEMPERATURE THERM. 05/03/99 1305 GJ 19 degrees C
pH VALUE EPA 150.1 05/03/99: 1305 GJ 6.7 units
CHLORIDES EPA 325.3 05/14/99 1600 ML <.10 PPM
CHEM.OXY.DEMAND EPA 410.4 05/07/99 1540 CT 11 PPM
TOTAL DISSOLVED SOLIDS EPA 160,1 05/07/99 1630 CT 121 ppm
SULFATE EPA 375,4 05/14/99 1500 CT 16.9 ppm
TURBIDITY EPA 180.1 05/04/99 1615 CT 22.00 NTU
NOTEi TOO results will follow when completed.
LABORATORY DIRECTOR

06oratories, Inc.
2217 Graham Park Drive
LARCRAiRIES, PVC PO Box A 11483
ChaSI
C C 28241-IA83
NC Cwt # 20:SC Cart# 99W3001
ai .-
REPORT OF ANALYSES
Attn: TERRY WARD
SPECTRUM DYED YARNS (BELMONT) PROJECT NAME: MAY 99
PO BOX 1006 DATE: 05/28/99
BELMONT, NC 28012-
MONIT'GRIN G WELLS
SAMPLE NUMBER- 13611 SAMPLE ID- SLY MW-1 GRAB SAMPLE MATRIX- WA
DATE SAMPLED- 05/14/99 TIME SAMPLED- 1045
DATE RECEIVED- 05/14/99 SAMPLER- GREG JOHNSON RECEIVED BY- ML
TIME RECEIVED- 1155 DELIVERED BY- GREG JCS SON TYPE SAMPLE- Grab
Page 1 of 2
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
FIELD TEMPERATURE THERM. 05/14/99 1045 GJ 19 degrees C
pH IwTALUE EPA 1501 05/14/99 1045 GJ 6.7 units
TOTyORGANIC CARBON EPA 415.1 05/28/99 1000 PAK < 1.0 mg/L
LABORATORY DIRECTOR

CHAIN OF CUSTODY
PAR Laboratories, Inc
Phone [phone]
Fax [phone]
Shipping: Mailing'.
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NG 28241-1483
It is essentrat that ati information recorded on this Chem of Custody document for acceptance by PAR Laboratories, tnc and the North
Carolina Department of Environmental and Natural Resources,
Company Name (billing) COMMENTSISPECIAL
INSTRUCTIONS
Address
7
City, State & Zip, Code
P, - 1 4- ITeT— ij
Point of Contact & Telephone NumbeFr,,,
Sample taken by: VA
IS THIS FOR STATE or EPA REPORTING? YES X
N O
V
*Sample type: DW _ Ww
—
GMW HW—
W
Sofi Other
Sample Temp upon receipt:
0C
Preserved: Yes —X— No
Tefton L. zero Headspace: Yes, —
No — NIA
Sample I.D.
Set Up
Collection
nalyses
'e -
,le Location I Number) Comb Grab Preserv, Daterrime
6a-te-,-Ti,�e
Daterrime
nested
nested
L
%
C. "D
hi ct/ — 7—
E
I t I 1i
61 0
-L I
--------------
C" r.- Ilk Jill-/
Tc,'11"
Refinquished Dateffirne Received by: Dateffinde
3/2'
Relinquishe by DatefTime R,4Mved by: Daterrime
G=Compostte G=Grab DW=Drinking Water WW =Wastewater GWMW =Groundwater Monitoring Well HW =Hazardous Waste
* See Other Side

'0AR CHAIN OF CUSTODY
LABORArORJEs. INC PAR Laboratories, inc
Phone [phone]
Fax [phone]
Shipping. Mailing:
17 Graham Park Drive PO Sox 411,483
Charlotte, NC 28273 Charlotte, NC 28241-1483
It m dssentsal that ail information recorded on toss Chain of Custody document for acceptance by PAR taboratones, Inc and the North
Carotina rrepartmern of Environmental and Natural Resources,
Company Name tbtlti gD COMMEN SI P Ct w
tNT � 'FiONs
. ' tit
Address r
City, StatA &Zip tode
L44-
+ '
Point of Contact & Telephone Number
Sample taken by: e-1 tk4oj-
IS THIS FOR STATE or EPA REPO ? �"S mple type. D�P M HW1t Soil Other
Sample Temp upon receipt;
Preserved; Yes w, No Teflon Liner/ Zero Hea slaa e: Y I
AX
Client Sample I D, Set Up Collection nalyse
(Sample tctution r Number) comp Grab Preserv, Datetrin e Datef ime equested
�A
�"- l .
-F
l nquished by: aster
—J-101 In
el'nquished b Datef l'irne F bred lay. _ Cat lTime,
C=Composite G=Crab DW =Drinking water WW =WastewaterC = round ater Monitoring Well HW aHazardous't, Waste
See Other situ

TVZZE A<I.)Nof
Olt
zcr
x
t 30t OBed
it -XH a3ldaAT12ra -Ci
z -.off aaAT9324 U09tzqop sole - 1 - I
r [ a -Caqdwvs Siva
O U Od
t° l x ; U
JIV
Jo 4,4042fa IVNIJ
'9iqIY0J4V90ffY7 7VINYNNO91ANy VNI70XVO
I
.,, �., �. a „_-� . .-- -: , � _� �� .-- r� o.a •-t p n r � "'� o x � k 9 ..,t i'a � 1 �4 � `: a.` e' "' iF 4 0 .W �.

CARouNA,E,NrV7R0zvmE,,VTAL LABORATORIES,, LLC
1229 M HORNER E3LVM - SANF-opo, NC 27330
(9 19) 775- 1880 a FAx (919,) 776-5724
PAR Labcraturf es, Irlc, Contact: Margaret Rice
rss PO Box 411483
Charlotte State: NC Zip: 2�8241
CHAIN OF CUSTOM
Page —J— tit
N

GROUNbWATER OUALITY MONITORING,-
COMPLIAf4CFE REPORT FORM
MAU
-4-�l 4 T �11
2 I T =1 t L
Please Print OJearly or Tj-pe
PERMIT R". 4- 11Y1
EXPIRAT ION DA i:-:
=3,i1tty Name*
NnDi:hage-
as�r
TIC1�
Permit NlaWhy e �if dif(e
i r
-A
NPDES
---"I
�PKI
�=F- �­
0?�=RATlON BEIN,3 [.JOW6DR�11
County
may" 44:-2c,
I - - ,- -
—A Lagoon
—Rerned�aflDr: lnrfltrafi:�n Gafle�y
"
No. of Wells to be Sampled: ^
Ffo-mT*-rmfti
— Sp, -ay Field
Rotary Dstributnr
—Land Azphcnaticin of SU Q -
Well Idenfifioation Mjmtter (from Permit):
& t�A�e$�NOI-
For Groundwater Trsatnient Systerns
_ Other.
Well Depth., Well Diameter: -6— in. Che-k one:
S=eenet14 Interval'­10— ft, 10 —.z �- ft. 1 Influent (98)
�ep,,tt to Water Levei: _LL— ft. bsisw -neasuring Effluent (99)
Measuring Point ,s --�— ft, anove land sur:ane.
Gallons of water pjmPed!b0ed ba-fore sampling.---,2.
f::ield analysis: pH , Specific Conductance !tLz Z UMhos
T e mo Cr for Appeaance
!,4 Values should reflect dissolved and
-olloidal con-.entrallions.
9?
Cale sample collec.1 d: Date sample anal},Zed:
Laboratory Name'.
Certification No,
m --T= M V NO
�3a (Samples for me' is were collected unfiltered—. -S
and field acidified
--------
COD
M g'I
Nitrite (NO2) as N
rn g 11
Coflfon--m: MIF Fel--3,t
11 C) 0 m I
Nitrate (NO3) as N
mg/1
Coliform: Mk"Total
P", DoI m
:ohosphorus: Total
I as P
Mg/1
(Note: Lim MP14 me hod lof highly tuMi.' sarnpies)
Orthophosphatee
mg/I
mg/I
Dissolved Solids: Total mgl
A[ - Aluminum
pH (when analyzed)
units
Ba - Barium
mgA
TO C
Mg/l
Ca - Calcium
mg/,f
C,hlo,ride
1- 119 1
Cd - Cadmium
Mg/I
ksenic
rng!l
Chromium: Total
Mg/1
Grease a, -Id O's
mg!l
Cu - Copper
Mg/1
Mg/l
Phenol
Mg!1
Fe - Iron—
C 0 q
Sulfate
mgtl
Hg - f,,iercury
Mg/I
SpecIfic Conductance
0,1hos
K - Potassium_
mg/l
Tot-il Ammon1a
rng�'l
Ivig - 1,,iagnesium
m g 11
TN K!`4 as
M91
t,,In - f.1anganese
mg 11
- YES NO)
Ni - Nickef MgI
Pb - Leari
zn - Zinc
rl1� g!]
�rnmonia Nitrogen
Other (specify Corn.nounc4s and, C:*M:e-.'a4 Tjn ps)
7-0 A" h 0 Alllrt)
ORGANICS: (GC,GC,'MS,HPLC)
(Specify test nd method #. Attach lab report-)
Report Attached? Yes_(INO
voc me!hod
m, elhod
rnelhod

PAR LciborcLori es, Inc.
PAR2217 Graham Park Drive
LABORATORIES, WC PO Box 411483
Charlotte, NC 28241-1483
NC Cart # 20; SC Cart # 99W3001
May, 18. 1999
'Ferry Ward
Spectrum Dv Yarns, Belmont
P.O. Box 1606
Belmont, NC28012
Dear Terry,
This letter is in follow up to our conversation Monday regarding the VOC samples for
As you are aware, we subcontract the VOC analyses to another lab. Unfortunately, one
of the 2 vials of samples was lost in transit by UPS, We have re -sampled the wells and
sent the samples for analysis.
We will forward results as soon as they are completed,
I apologize for the inconvenience,
C,
Sincereks,
Russell M. Everett
Administrator

111"M 111111111
Well Identification Number from Permlo: VE 2, For Groundwiler Treatment Systems
Well Depth, ft. well Diameter: 10- Check One:
Screened Interval, It. to _2up—, — ft. IJ Influent (98)
Depth to Water Level: _11— It. below measuring point, Effluent (99)
Measuring Point Is ft. above land surface.
Gallons of water p urn pert/ba fled before sampling:
Field analysis: pli Specific Conductance umhos
Temp. Odor --hkag—E Appearance
IYEE�011REW -OPE c3EING MONITO
Lagoon infiltration 641lik
Spray Field V1
70—
nolar�Distflb6ldr Land Application of Sirtte
othort
Nom Val"dA miottlal reflect dissolved and
colloidal
Date sarnole 6ollectea. 4�-\4qa Date samptd7briq tped: ik��
Laboratory—Natuo!
f3artiffbatiott
PABAMEM1,101, (Samples for metals were collected unfiltered —YES _NO
and field acidified
—YES NO)
COD
MO
Nildle (NO,?) as N ---
mg/I
NI - Nickel Mg/l
Coliform: IVIF Fecal
_11001nl
Nitrate (NO3) as N
Ing/l
fib -Inn 'YN"NN mg/I
Cotiform: MF Total
_/100ml
Phosphorus: Total as P
mu/I
Zn - Zinc Mgt[
(Note- Use LIPH method for ter ghlyturbai
samples)
Orthophosphate
Mg/1
Ammonia Nitrogen mg/l
Dissolved Solids: Total
M(j/I
Al - Aluminum
mg/I
Other (Specify Compounds and Cor�Eentration Units)
pH (when analyzed)
(I'a I
Units
Ba - Hadrim—
MO/I
---
roc
mq/1
a- GaICiLIM a
Mg/I
Chloride
Mg/I
Cd - Cadr-nium—
mg/I
Arsenic
Mg/I
Chromium: Total
mg/l
Grease and Oils
rng!l
CIS - Copper
mg/I
Phenol . .....
mg/I
Fe - Iron
mg/I
ORGANICS: (GC,GC/Ms',HPLC)
Sulfate
mg/l
Hg - Mercury
M911
(Specify test and method #. Attach tab report.)
Specific Conductance
_uMhos
K - Potassium—____
rnq/I
Report Attached? Yes-X-(I) No — (0)
'rotal Ammonia
Mg/I
Mg - Magnesium
mg/l
VOC method ft
TKN as N
mg/I
Mn -
mg/I
triethod It
P f"
a

.It , , , z W, , , 1i
Facility Narne:_�� �_�
. armit arne (if differanh*_
PWSe PtItit Cwtv or 706� 17-
FPERMIT It: EXPIRATION DATE�M
UIC
I —MR 13 Check One:
t4thleat (94)
lu t (99)
Values should reflect dissolvedand
X:
colloidal concentrations.
Date sample collected: AAA Date -sample analyzed: Lglr-4�-
Laboratory Name: 0M), L_P02MrC>
I-arfifirnfinn
PARAMIETIER19 (Samples for metals were collected unflitered—YES —NO
and field acidified
—YES NO)
GOD
2 MqA
Nitrite (NO2) as N
mg/1
N1 - Nickel Mg/l
Calif orm: MF Fecal
/100IT11
Nitrate (NO3) as N
Mg/I
Ph - Mg/I
Zinc mg/I
Coliform-, MF Total
drawl
Phosphorus: Total as P
Mg/I
Zn -
(Notea Use MPN method for highly turbld samplos)
orthophosphate
Mg/I
Ammonia Nitrogen mg/l
Dissolved Solids: Total
moll
A[ - Alurninurn
Mg/I
Other (Specify Compounds and Qbncentrallon Units)
pH (when analyzed)
units
Ra - Baritim—
mg/I
—1 iA B _,a a ac—
TOC
MO/I
Ca - Calcium
mg/I
Chloride
m(I/I
lid - Gadinium
net
Arsenic
mg/I
Ghrorflit,lln: _FOtal
_,Mg/I
Grease and Oils
mg!I
Ctt - Copper
mg/I
Phenol
rnq/I
Fe - Iron
rng/I
OnGANICS: (GC,,GG/MS,riPLG)
Sulfate
mg/I
Hg, - Mercury
Mq/I
(Specify test and method #. Attach lab report.)
Specific Conductance
uMhos
K - Potassium
Mg/I
Report Attached? Yes_X__(I) No — (0)
Total Arnmonia
Ing/I
Mg - Magnesium
Mg/I
Voc method A
TKN as N
mUlf
Mn - ran Tarr
mg/I
method 11
re dared it
Gw-59 nov. driga
rV-)
ful,1111tee for Atjthodzed Agent) Nz ml T p
I , lease print or
V

PAR Loborcitories, Inc..
2217 Graham Park Drive
PO Brix 41 15
Charlotte, NC 28241-1483
Nc Cart Carr 4 990woo
REPORT OF ANALYSES
Antra, BUDDY BU Ct4'
SPECTRUM DYED YARNS (BELMO ); PROJECTNAME: NOV 98
PC BOX 1006 DATE: 11/25/98
BELMONT, NO 28812-
MO ITORING WELLS
SAMPLENUMBER- 9273 SAMPLE ID- Sail' ill #2 SAMPLE TYIA 'R1 - WW
DATE SAMPLED- 11/10/98 TIME SA14PLEI3 _ 1050
DATE RECEIVED- 11/10/98 SAMPLER- CR:EC JOHNSON RECEIVE R"Y- RE
TIME RECEIVED- 1630 DELIVERED Big`- GREG JOHNSON "TYPE SAMPLE- Grab
Page 2 of 2
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
FIELD TEMPERATURE THERM 11/10/98 1050 CS22 degrees C
pH VALUE EPA 158.1 11`10/98 1958 GJ 6.2 units
TOT.ORGANIC CARBON EPA 415.1 11/16/98 1400 PAK < 1.00 gag/
CHLORIDES EPA 325.3 11/25/98 0855 CT 285 ppm
CHEM.OXY.DEIMAND EPA 413.4 11,/23/98 1515 CT 20 ppm
TOTAL DISSOLVED SOLIDS EPA 160,1 11, 13 / 8 1505 GJ 259 pp
SULFATE EP.A 3'75.4 11/1 / 8 110S CST' 42 ppm
TURBIDITY EPA 1801 11/11/98 180CT 2,52 NTU
VOLATILE ORGANIC COMPOUNDS 11/12/98 PAF
SEE ATTACHED SHEETS FOR VOC RESULTS.
LABORATORY DIRECTOR

NOV-19-98 THra
A aCAROLINA ENV. LABS
19197765724
P. 1
CARoLiNA
LABORAwRiEs,
LL C
•<R Laboratories,
.0
Charlotte, NC . .
FINALRT OF ANALYSES
PROJECT NAME.- November 1998
REPORTDA'TSt 11/19/90
NUMBER -SAMPLE 9794 SAMPLE ID- 9273 SDI -
DATE SAMPLED- 11.110 /
DATE RECEIVED- 11/13 98 SAMPLER- Greg Johnson
TIME EIV- 153 LI D BY UPS'
Page 1 of 3
ANALYSIS
ANALYSIS
DATE
Total organic Carbon
531
11 /1 /98 PAIK
Volatile Organic Compounds
8 21A
11/1 /98 PAX
Benzene
82
Bro en ene
211
Bromodichloromethane
6021A
Bromotorm
4021A
m ame't an
021
a-autylbonxene
5 21a,
t-Butylbenzene
8021A
Carbon tetrachloride
521A
Chlorobenzene
8 2
Chlorodibrommethane
OQ21A
Chloroathane
80214
Chloroform
8021A
Chloromethane
9 21.
2- hloroto en
2 A
4- lorotol e
50 1A
1,2-Digs - -c11 p o a
8 21
1,2-Dibromoethane
8 21
MATRIX -SAMPLE ;WW
TIME SAMPLED- 15
RECEIVED BY- HCG
RESULT UNITS LRL
1. g/L 1..
Q.5u/L
r . g1L
* 0.5 U /
.5 g/I+
0.5 a 1
.5 /
.5 ug/L
0.5 leg/
.5 1L
.5 ug/
0.5 ug/L
0.5 ug/L
_ . /
.., ug/L
O<5 uq/L
5 Ug/;L
O 5 g/L
.5 g/
0.5 ug/L
c ll xl ` ar a 7 9191775-1880 Fax I d - 7
24,
i /O'W 306 NC DV 37741 5C 99036

NOV-19-98 'T U CAROL-INA ENV.CAROL-I LAPS
1919776$724
P.20
CAROUNAENwRoNmNTAL
LABORAToRms,
LLC
Page 2 of
CONTINUATION OF DATA FOR SAMPLE NUMBER 9794
ANALYSIS
ANALYSTSBY
RESULT UNITS
LRL
Dibromomethane
8021A
<
0.5 ug/L
0
1.2- ichlorobeo e le
8021A
<
0.5 ug/L
0.
1, 1- ichl roben ene
8021A
<
0.S ug/L
0
1.4- ichl robe ene
6021
0.
0
ichlorodifluor meth' a
8021A
c
O.S ug/L
0
1.1- icbl roethane
802
O.S Ug/L
0.
1,2-Dichloroethane
8021A
<
O-S ug/L
0.
1,1- ichl rceth ne
8021A
cia-1 , - Dich r ethe a
8021A
<ww
-:..
..
trade-1, 2- ichlo et ene
8021A
<
0.s Ug/L
0.5
1, -0ichl ro r pale
8021A
<
0.5 ug/L
0.5
1, -Lichl ro parse
8021
0,S " ug/L
0 § ,
. 2 -14chloropropane,
802
0.0 a /L
0.
1,1-Dichloropropene
0021A
c
0.s ug/L
0.5
cis-1, -D chlo p ope e
8021A
0. , ug/L
0
trans-1. -Di hloro ropene
00211#
<
0.5 ug
0m
Ethylbenzene
0021A
0.5 gag/I
0.
Rexachlozobutadiene
8021A
0.5 ug/L
0.
I opro yl en e
0.5 ug/L
0.
p-loopropyltoluene
8021A
<
0.5 ug/L
0.5
Methylene Chloride
8021
<
0. g/L
0.
Naphthalene
00211
<
0.5 a /L
0..
n-Propylbenzene
8021A
ug/"L
0.5
Styrene
0.5 ug/L
0.
1.1,1.2-Tetrachloroetb a
0021A_
. ug/L
0.
1,1 2,2-T trachlor°oet a
8021A
<
0.5 a /t
0.:
Tetrachloroeth xs
802
I - 5 ugr ' �
0.5
Toluene
0021A
ug L
0.
1, 2,1-Trichlorobell e
8021A
<
0.5 ug/L
0.s
1, 2-Tri;cL or 'ben eue
9021A
O.S Ug/L
0.
1,1,1-Trichloroothane
8021A
0,.
1229 North

hiOY-1 THU 1 CAROLINA ENV., LAPS
19197724
P. 1
CAROLINA ENVIRONMENTAL LABORATORIES,
LLC
Page 3 of 3
OF DATA FOR SAMPLE NUMBER 9794
METHODCONTXNUATIO14
ANALYSIS D= BY
RESULTITS
1,14-Trich1Q,roethane 6 21A
< 0.5u /L
0.5
T '1 %1 roe h rse 0021A
,Y .
d
Trichlorofluoromethane 0021A
< ' .. 9' L....
07
1,2.3-TrichlorQpropane 8021A
< 0�5ug/L
0.5
1. 3 j grime hyl n ne 90 1A
u / .
0.5
1, 3 -T imeth lben n 8 21A
< 0.5 ug/L
0.5
vinyl Chloride 8021A
< O'sug/L
0.5
. - 1 ne 8021A
< 0.5 u /L
0.5
LRL = Lower Repor ingr Limit
LABORATORY DI
1229 Nord Horntr Boultvaxd, Sanford, NoA Carohna 27330
9191775-1880 Pa%9191776-6724

PAR Labc>ratories, Inc.
2217 Graham Pork Drive
ORATORIESINC PO Box A 11483
G harlotte, NO 28241-1488
Bw
PVC Cart # 2D, SC Carr # 99 3003
REPOPT OF ANALYSES
Attn: UDD BURCH
SPEcrRUM DYED CARDS (SELF" T) PROJECTNAME: NOV98
PO BOX 1006 DATE: 11 /28
BE L MON`"T , NO 2 8 011,v
MNITORING WELLS
SAMPLENUMBER- 9272 S 1PL D- SDY MW `I SAMPLE MATRIX- WW
DATE SAMPLED- 11/10/98 TIME SAMPLED- 1040
DATE RECEIVED- 11./10/98 SAMPLER- DREG JOHNSON RECEIVED B RR
TIME RECEIVED- 1630 DELIVERED BY- G1REG1 JOHNSON TYPE SAMPLE- Crab
Page 1 of 2
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
FIELD TEMPERATURE THERM; 11/10/98 1040 GJ 19 degrees ,C
B VALUE EPA 10.1 11/10/98 1040 B.T 6.2 units
TOT.ORGANIC CARBON EPA 415.1 11/16/98 1400 PAR 3.47 tag/L,
CHLORIDES EPA 325.3 11/25/98 OB55 CT 95 pPm
CH EM . OXY e DENIAIM EPA 410.4 11 / 2 3 / 9 8 1515 IT 2, 2 Ia ttti
TOTAL DISSOLVED SOLIDS EPA 1609 1.1/13/98 1505 GJ 123 ppm
SULFATE, EPA 375.4 11/1 /98 11105 CT" c 10 pram
TURBIDITY EPA 180,1 1.1/1 /98 1600 CT 1.30 NT13
VOLATILE ORGANIC COMPOUNDS 11/12/98 PAK
SEE ATTACHED SHEETS FOR VOC RESULTS.
LABORATORY DIRECTOR

CARO.LIAFAENVIRONMENTAL.LABO.RAToRI,USI LLC
FINALy ANALYSES
PAR Laboratories, Inc.
PRNovember
1998
Attn: Margaret Rice
REPORT DATE:
11/1 / 8
PO Box 411483
Charlotte, NC 28241-1483
SAMPLE NtjNBER 9793 PL
1 t- 9272 S y'K"_j
SAMPIE MATRIX- WW
DATE SAMPLED- 11 /88
TIME SAMPLED- 104
DAT9 R 1v L 11./'13/ 98 L - Oreq Johnson
RECEIVED Y 11 cq
I ® 1530 DELIVERED BY- UPS
Page 1 of
y81
ANALYSIS
METHOD DATE BY RESULT 11'
LRL
Total Organic Carbon
5310C 11116198 PAX
3.47 m /L
1,
Volatile Organic Compounds8021A
11/18/98 PAK
Benzene
881A
< 8,5 u/L
0.5
Bromobenzene
8021A
< 0is u" /L'
0.5
Bromochloromethant
80 1A
8.5 u+ /L
8.
Bron*dichloromethane
6021A
0.5 ug/L
Qs
aromotorm
11021A
<0.5 uq/L
0.5
Bromomethane
88 1A
8.5 a /L `
8.5
a- utylbenzane
88 1A
0.5 U /b
8.5
a- utylben ene
8021A
< O.S u /L
8.
- utylben ene
8831A
< 0.5u /L
8.5
Carbon tetrachloride
00 1A;
< 0.5 a /L
8.5
hl ruben ene
88
.5 ug/L
8.5
hl r br omethan ,
e
881A
8.5 u/L
8.5
Chloroethane
88 1A
< 0.5 a /L
8.
Chloroform
88 1A
< 0.5 u /L
0.5
hl romethane
88 1
8.5 UqA
015
I-Chlorotoluene
8 31A
4 0.5 a /L
9 5
4-ChloroLoluene
0021A
0.5 a /L
0.5
1, -Dibr m -3«ehl ru r ane
4021A
0.5u /I®
0.5
1, - ibrom ethane-
0021A
4 O.S ug/L
0.5;
1229 North roar Boulevard, Sanforti,,North Carolina 27330 9
NC VVIGW 306 NC DV 37741

L.MouNAENVIRONMENTAL
a_
LABORAToms,'
LLC
Page 2 of 3
CONTIMATION OF DATA FOR SAMPLZ NUMBER 9793
AMLYSIS
ANALYSIS
0 DATE
BY R B L` UNITS
Dibromomethane
5021 t
0.5 gag/L
0.5
1,2-Dichlorobonzene
60271A
0.5 ug/L
O.
1,3-Dichlorobenzene
0021A
0.5 U91b
0.5
., 1,4-Dichlorobenzene
0021
ug/L
0
K� Lichl odi lu ra ethane
02CC
1,1n-Liehl.ornethane
6021A
c
03 u4/L
0.5
1,2-I)ichloxoethane
0021A
t
03 ug/L
0.5`
1, -Diehl r eth ne
8021A
c
0.5 ugC/L
0 �5
t -1,2- lichl roethene
8021
.5 ug/L
0.5
1, 2 -ilic°hlrprpane
8021A
0.5 dug/L
0.5
1,3-Dichloropropane
0021A
0.5 ug/L
0.'
2,2-Dichloropropane
6021A
<
0.S /L
0.
1,1-Di hl r propene
8021A
0.5 /L
0o5
ere-1., 3-Diehlrar pease
8021A
<
0.5 ,ug/L
0.
r s-1. - ichlorep pen0
8021i
0.5 ug/L
0a5
thyl.'h+en ane
802114
0.5 Ug/L
0.5
hexa hl r butadlene-
8021A
0.5 ug/L
0.5
l,sopr pyl en ene
802
0.5 /
0 � 5
p-16opropyltoluene
0021A
<
0.5 ug/L
0 5,
Methylene Chloride
002
0.5 ug/L,
0.5
,Naphthalene
0021A
<
0.5 Ug/L
0.5
n-Propylbenzene
802
0...5 ug/ r
0.5
Styrene
8021.A
<
0.5 a /L
O r 5'
1,1,1,2-Te ra hlnroethane
002
O,S ug/L
0.5
1.1, 2, 2- etra ur+ a hane
8021
0, 5 u /L
0.5
Tetra hlor ethene
0021
O.5 ug/L
0.5
`oWene
8021A
0.5 ug/L.
0.5
1,2, - r.ae lOr hena ne
8021A
<
0.S ug/L
0.5
1,2,4- riehl r ben ene
8021A
4
0.5 ug/l
0�5
1.1,1-Trichloroethane
8021A
A
0.5 g/L
O.S
W
1229 North Horner B e e xr , Sanford, North Carolina 27330 919/776-1880 Fax[phone]
NC VVIGV 306DV 37741 SC 99035

CuouNAENvi-RONMENTAL LABORAToms, LLC
Page 3 of
CONTINUATION OF VATA FOR SAMPLE'9791
ANALYSIS
ANALYSISHOD DATE BY RESULT U14ITSLR
1,1, - "ri h r ether ne 0021A K 0,S u /L 0.5
Trichloroethene 8021A < 0.5 /L 0.5
Tri hl r flu r e h a 80 1Fto < 0.5 Ong/L 8.5
1, .3-T i Ll r p a 88 1A < 0.5 tag/L 8.
, , 4- ri neth l e e 8 .5 ug/L 0,5
1, ,5-Tri e ylben a 85 .5 a /L 0.s
Vinyl Chloride 80 1.A .5 a /L 0.5
o-Xylene 88 1 0.5 tag/L 0.5
m,p-Xylemc 0021A < 0.5 U91L 015
L L a Lower Reportiog Limit
LABORATORYDIRECTOR
a
w
Ter i '9-a ray
12,29
rev VTIGW 3o6 NC DV 4

CHEMICAL&ENIIIIZ()PNMENTALTECHNOLOGY, INC.
FINAL 'REPORT OFANALYSES
Pr -asp` LABORATORIES, Ta w
2217 GRARAM PARK AVE,
REPORT DATE: 27/17/9SA
Attn: MARGARET RICE
`'�. ° L= a�t i L�
SAMPLE NUMBER- �4 � 60
`"^, .G PYj .+.,..", �s � i.:.w "' a� Ta i:`: 5...� .G R �1. ."t� V�'i i GRAB
v NII SPECTRUM
g y { W
SAMPLE MATRIX- t5. � k�i�YV
DATE SAMPLED- 7 ?'4
TIME SAMPLER- L"LSJR.,..., 083..G.
DATE RECEIVED- 06/30rr:98
SAMPL R- CR C; JOHNSON
RECEIVED BPEE
TIME RECEIVED- 1000 0
DELIVERED BY- UPS
ANALYSIS
ANALYSIS
METHOD DATE By RESULT UNITS
PQL
TOTAL ORGANIC CARBON
EPA 415.2 07 aS/98 AEK <1 ,rig
L 1.0
F S,r}! = Practical y`u Gant" 1 4> a° t i o n. Limit,
Results followed by the
letter J are estimated concentrations,
v
x 4 CERTIFICATIONS:
,T
WATER
LABORATORY DIRECTOR
e
r�
41
P.t1 Box 12299 • Research Trran le Park, NC 27709 Shipp ntjt 102-A Woodwinds 8ndat triaat Court Cary, NC 27511
T&ephona )91 9) 4 7- 0
Fax # l $ 4671

CAROUNA ENviRONMENTAL
FINAL REPORT OF ANALYSES
Par Laboratories, Inc,
PROJECT EI E Vocs
P 0 Box 411483
RESORT DATE: 12/"29/97
Charlottes, NC 28241-1 83
l
Attna Margaret Pace
C�otT�t
� t�
SAMPLE NUMBE, 1717 SAMPLE Its- 97
474 -1 O ttl
SAMPLE NIATRIX- GW
DATE SAMPLED- 12/',1 / 7
TIME SAMPLED-0825
DATE RECEIVED- 12'/1 ,/ '7 SAMPLER- H
RECEIVED
BY- CAP
TIME RECEIVED1230 DELIVERER BY--
UPS
;
Page 1 of
ANALYSIS
DET
AILALYSIS
METHOD
DATE BY RESULT
ITS
LIMIT
Volatile Organic Compounds
8021A
12/23/" 7 P &{
Benzene
8021A
< 0.5
ug/L
O.S
Bromoben ene
8021A
< 0.5
ug/L
, 5
Brom act' loromet ane
8021A
< 0.5
ug/L
0,5
E omodichlromet an
8021A
< 0.5
ug/L
0.5
Brrmof r m
802IA
< 0,5
ug/L
0.5
Bromomethane
8021A
< 0,5
ug/L
O, S
n-Buty ben ene
13021A
< 0,5
ug/L
0.5
-Luty ben ,ene
8021A
< O5
u /I,
5 e 5"
t-llutyl.ben ene
8021A
< 5.5
ug/L
CM. a
Carbon tetrachloride
8021A
< O.5
ug/L
0.5
C"hloroben ere
8021A
< CC � 5
ug/L
O. 5
Chlort dibromomet. ane
8021
< O,5
ug/L
0,5
CF} l.oroethane
8021A
< CI . S
ug/L
01 5
Chloroform
8021A ,
< 0.5
ug/L
O.5
Cli lorom than e
8021A
c 0.5
ug/L
0.5
2 - hlorotol ene
8021A
< 0.5
ug/L
0.5
4--Clilorotoluene
8021A
< OI 5
ug/L
0.5
1,s 2-III bromo 2 chlorcp rpane
8021A
< 0.5
ug/L
S . S:
1,2-L?ibromoetharie
8021A
< 0.5
ug/L
O.
Dibromomethane
80211I
< 0.5
ug/L
0.s
t229 North I lorner Boulevard, Sanford, , orth Carolina 27330 91.9/ a° - ,880 Fax 9 1.9
1 6 -572

Page 2 of 3
CONTINUATION OF DATA FOR SAMPLE NUMBER 5 76
ANALYSIS
DET
ANALYSIS
METHOD `
DATE BY RESULT
UNITS
LIMIT
1,2-Dichlorobenzene
8021
<
0.5
ug/L
0.5
1„ 3-Dichlcarobexr ene
8021A
<
0. 5
ug/L
0, 5
1,4-Dichlcroben ene
8021A
<
0.5
ug/L
0.5
Dichloro i luor methane
0021
<
0.5
/L
0.5
1., 1-Dichloroethane
8021A
<
0.5
ug/L
0.5
1,2-Dichloroethaiie
0021
<
0.5
ug/L
0,5
1 , 1-Dichloro thene
8021A
,,
O,5
ug/L
0.5
ci 41,2'-Dichlcroethen
5021
<
0.5
ug/L
0.5-
trans -1, 2-Dichloroethene
8021
<
O,5
ug/L
O.5
1. 2-Dichloro rrta cane
8021A
<
0.5
ug/L
0.5
1, 3m-Dichloropropaaae
0021
<
0.5
ug/L;
0.5
2 2-Di hlcarcprcpa a.e
6021
<
0,5
ug/L
0.
1,1-Di hl ropro ene
5021
.
0.5
ug/L
0.5
ci -1, 3-Dichl roproperre
5021
<
0.5
ug/L
0.5
trans-1, -D hloroaropene
8021
<
0.5
ug/L
0.5
Rth,=lben eue
8021A,
<
0.5
9/1
O. a
He achlor butad e ze
0021A
<
0.5
ug/L
0.5
Isopropylbenzene
8021A
<
0.5
ug/I,
0.5
p-Isopr py toluene
8021
<
0.5
ug/L
0.5
Methylene Chloride
0021
<
0.5,
ug/L
0.5
Naphthalene
0021
<
0.5
ug/L
0a5
n-Propylben ene
0021
<
0.5
ug/L
0,5
Styrene
0021
<
0.5
ug/L
0.5
, 1, 1 2-Tet achl roethane
8021
<
0.5
ug/L
0 r5
1, 1, , 2- etrachl oethane
5021r
0,5
ug/L
0 n 5
Tetrachloroethene
5021A
<
0.5
ug/L
0.5
Toluene
0021
<
0,5-
ug/L "
0.5
1, 2, 3-- 'rxchloroben ene
8021A
<
0.5
ug/L,
0.5
1 2,-Trac.hlorob,en ene
0021
<
0.5
ug/L
0.5
1,, 1, 1-'T'x ichlorcethane
0021A
<
0,5
ug/L,
0. 5
1,, 1,-Tra_chloroet bane
0021
<
O . S
ug/L
0 , 5
1229 Nordi I le,rn r° 13OLde art , Sanfo rr € Nord-, Carolina 27330
0

CAROUNA
Page 3 cad'
CONTINUATION OF DATA FOR
P DER 5757
ANALYSIS
ANALYSIS
D Ta
METHOD DATE
BY RESULT UNITS LIMIT
Tr:ichloroethene
8 2I
Tr ich3.c rofluorometh e
8021A
0. 5 u /L
0,5
1, , 3--` richlciz pa n
021
0.5 a /L
0, 5
1,2,4-Trimethylberizene
0021A
O,5 ug/L
O5
1,5„5-�Tri�aethylben n
50 1
uq/L,
fl y
Vinyl Chloride
8021A
O-S
0.5 ;�a/L
0.5
o-Xylene
0021
0.5 u/L
0.5
m,p-Xylene
502I
c 0.5 ug L
0.5
0.5 u /L
0,5

CAROUNAENwRONMENTAL
FINAL REPORT OF ANALYSES
Luau Laboratories, Inc,
PROJECT NAME: VOCs,
P C- Box 411453
REPORT DATE. 12/29/97
Charlotte, NC 28241-1483
Attn: Margaret Rice
SAMPLE NUMBER- 766 SAMPLE
ID- 97
7 _ 2a 'SAMPLE
MATRIX- Chi
LATE SAMPLED- 12,/1 / 7
j .
TIME PLED- 0844
DATE RECEIVED- 12/1 /97 SAMPLER-
CH
Alto,
RECEIVED
BY- CR
TIME RECEIVED- 1230 DELIVERED
BY-
UPS
Page I of
ANALYSIS
lET ,,
ANALYSIS
METHOD
LATE BY RESULT
UNITE
LIMIT
Volatile organic Compounds
8021
1 /23/ '7 PALI ;
Benzene
8021A
< O b 5
ug/ L
0, "
gr moben ene
8021A
< 0,5
ug/L
O.5
Bromochloromethan
8021
< 0.5
ug/L
Bromodichl.oromethan
8021A
< 2.5
ug/L
0.5
Bromoform
8021A
< 0.5
ug/L
O
Llromomethan€
8021A
<; 0.5
ug,/L
0,5
n-Eutylben en
021A
< 0.5
g/L
0.5
a -Rut lben ene
8021.
O .5
Ug/L
O,5
t- utylben ene
8021A
< Q,5
big/L
0.5
Carbon tetrachloride
8021A
< 0.5
ug✓L
0.5
Chloroben ene
8021A
< OL 5
ug/L
0,5
Chlorodibromomethane
8021A
< O,5
L1C1 / L
0,5
Chl:oroethano
8021,A
< 4.5
ug/L
0.5
Chloroform
802
, 54
ug
0 a 5
Chloromethane
8021A
<, 0. 5
uc /L
O.5
2 -Chlorotol.uene
8021A
0. 5
ug6
O„ S
4-Chlorotol.uene
8021A
e2.5
ug/L
0.5
1, 2-Dibromo--3-chlo -opropane
8021A
< O e S
a /L
0.5
1,2-LibromoetLane
8021A
< 0.5
tag/L
0.5
Dibromomethane
8021A
< 0.5
ug/L
05
1229 Nordi Horner Boulevard, Sanford, Nordi Carolina 2 330 919Y -1 0 Fax [phone]

CAROUNA ENviRONMENTAL
Page 2 of
CONTINUATION OF DATA FOR SAMPLE
NUMBER 5765
ANALYSIS
DDT.
ANALYSIS
METHOD HOD DATE
BY RESULT
UNITS
LIMIT
1,2-Dichloroben ene
8021A
<
0.5
ug/L
0,5
1 , 3 - Dichloroben ene
8021A
<
0.5
ug/L,
0.5
1, 1-Dic zlarcbenze e
8021A
<
0. 5
ug/l,
0.5
Di'chlaaradi luoromethane
8021A
<
0.5
,ug/L
0.5
i<1-Dichloroethane
8021A
<
0.5
ug/L
0,5 a
1,-Didhloroethane
8021A
<
0.5
ug/L
015
1, 1-Di hl roetherie
8021A
<
0.5
ug/L
0.5
cis 1,2-Dichloroethene
8021A
<
0.5
ug/L
0.5
trans-1 , 2-Di hloroethene
8021A
<
0,5
ug L
0.5
1,2--Dichloropropar
8021A
<
0.5
ug/L
0.5
1, 3-Dichlaroproparle _
8021.
<
0.5
ug/L
0.5
2, 2 ... Di c rloropropane
8021A
<
0,5
ug/L
0.5
1,1-Dichlero roper
B021
<
0.5
ug/L
0.5
cis-1,3_-Dichl ropropene
8021k
<
0.5
ug/L
0.5
trans-1 , 3 -Diehl roproperie
8021A
<
O�5
ug/L
O,5
Fthlaeae
8021A
<
0.5
ug/L
0.
Hexachlorobu adi ene
8021A 21A
<
0.5
ug,/ L
0.5
lscprcpl.ben ene
8021A
<
0.5
ug/L+
0.5
p-isoprap ltoluen
8021A
<
0.5
ug/L,
0.5
Methylene Chloride
8021A
<
0.5'
ucd/L
0.5
Naphthalene
8021A
<
0.5'ug/L
0.5
n- ropyl.ben ene
8021A.;
<
0.5
ug/L
0.5
Styrene
8021A
<
0.5
ug/L
0,5
1, 1, 1, 2 Tetr hloroeth ne
8021A
<
0.5
ug/L
O .5
1, 1, , , 2;-'T"etrachloroeth ne
8021A
<
0., 5
ug/L
0.5
°T' t °achloroe here
8 21 a
1 .8
gag/L
0.5
Toluene''
8021A
<
`0;"S
ug/L`
0.5
1 2,3-F ichl srcbe e
8021A
Oi 78':ug/L
O.5
1 2 4-Trichl oroben en
8021
<
'O*: &
-Arg/L
0.5
1,1,1 °richloroethane
8021
<
0.5
ug/L
0,5
1 1.2-Tr.ichloroethane
8021A
<
0.5
uq/L
0.5
1 29Not-th lim-ncr Boulevard, Sanford, tNordi Carolina 27330 919/775-1880 Fax 919 a76- 2

CAROUNA ENVIRONMENTAL LABORATORiEs, LLC
Page 3 o1
CONTINUATION OF DATA FOR SAMPLE NUMBER
S'768
ANALYSIS
DET
ANALYSIS
METHOD
DATE
BY RESULT
UNITS
LIMIT
Tr i chloro theuue
8 21A
< 0.5
ug / L
0 1 5
Tz: chloro luoromethane"
88 1A
< 0.5
_ u /L
0.5
1, , 5-'T ichloro rc an
8021A
< 0.5
'ug/L
O
1, 2,4-T methyl en ene
88 1A
< 0,5
a,u+g/L
0.5
1, 3, 5-"S"rioi thylbn
80 1
< 0.5
'tu /L
0,5
Vinyl Chloride
80 1A
< 0.5
ug/L
0,5
4 a- ylene
80 1A
< 8.5
u/L
O.5
m,p-Xylene
88 1A
< 0,5
ug/L
O.5
LABORATORY
DI F T R
1229 Nortb Horner t3ottlevarJ, Sanford, North Carolina 27330
91917 5-1 0 Fax 91 9/`/ 16-5724

CAROLIATA I-FATV-1RONMENTAI, LABORM)KUE_`�, LLC CHAIN OF CUSTODY
1229 N. HORNER LVD, 0 SANFORD, NC 27330 Page of
[phone] - FAX [phone]
7—
1 ANALYSES REQuIRED
CLIENT IL L-) —contact: ILL TO,
Address:__./_lA, ry-A" L Phone # �411k7s Fax # (a_ , ) �z:;,)-,3 �-S—
Cfty: State: Zip: Purchase Order
PROJECT NO:
PROJECT NAME.
Turnaround Time-,
ZL Normat (2 weeks) C] Rush (i week)*
COLLECTED BY.- (Signature) PRINTED NAME [I Rush (48 hours)' Rush (24 hours)*
Is the sampte cNorinated? Yes NPRESERVATIVES o PRESERVED IN FIELD
W
PRESERVED IN LAS El j
monitor�ng purposes7 Yes No z CC 0I the resets be used for re
0 a) 0 RECEIVED ON ICE
Z
SAMPLE t DATE � TIME COMP GRAB` SAMPLE €,D, Z L) z
SAMPLE *Clc i
> oo z
MATRIX CONT�RNERS
t REMARKS
Q-7
mm
RELINQUISHED BY--- DATE /TIME RECEIVED BY DATE I TIME
C_
ri
BUSH WORK MUST BE APPROVED PRIOR TO SAMPLE SUBMISSION. ADDJTIONAl
ADDITIONAL INSTRUCTIONS
iES MAY APPLY,

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PAP Laboratories,
2217 GRAHAM PARK DRIVE
s t �
+ d g s
December 1, 1996
Reference en N 4584, 96 4585
Made Spectrum Dyed Yarns
Attention.,
Analysis Of:
Marked:
PO Box 1006
Belmont, Nip 28012
Buddy Burch
Groundwater Monitoring Wells
Sample 1. MW #1, 11/21/96 Grad
Sample 1 , 11/ 1 i Grid
Received On: 1 1 21 /96
Analysis:
6230D Compounds
96 4584 96 4585
1_
(p
Benzene
1
<1
Bromobenzene
<1
<1
romochl r o m t harmd
<1
<1
Bromodichloromethan8
<1
<1
Bromoform
<1
<1
Bromomethane
<1
<1
sec-Butylbenzene1
<1,;
tert-Butylbenzene
<1
<1
Carbon Tetrachloride
<1
<1
Chlorobenzene
<1
<1
Chloroethane
<1
<1
Chloroform
<1
<1
1m 1 r o m t a n
1
<1
2 mI o rot o I uene
< 1
<1
4 Ch l rot ail uene
<1
< 1
r1drmoch1oro than
1 ,-Dimlmrddrr
1
<1
1, :3- r 1 h 1 rt rt rr
1
<1
1,4-Dichlorobenzene
<1
<1
ichl rm ditl rtharm
<1
<1
1,1-Dichloroethane
<1
<1
1 , -pich] mrthan
1
<1
1,1-Dichloroethene
<1
<1
continued.....

page 2
Reference no- 96 4584, 96 4585
96 4584
trans-1,2-Dichloroethene
<1
1,2-Dichloropry pane
<1
1,3-Dichloropropane
<1
2,2-Dichloropropane
<1
1,1-Dichloropropene
<1
cis-1,3-Dichloroproper e
<1
trans-1,3-Dichloropropene
<1
Ethylbenzene
<1
Hexachlorobut adiene
<1
Isopropylbenzene
<1
4-1sopropyltoluene
<1
Methylene Chloride
<1
Naphthalene
<1
Propylbenzene
411
Styrene
<1
1 1 1 2-Tetrachloroethane
<1
1,1,2,2-Tetrachloroethane
<1
Tetrachloroethene
1.2
Toluene
<1
1,2,3-Trichlorobenzene
<1
1,2,4-Trichlorobenzene
<1
1,1,1-Trichloroethane
<1
1,1,2-Trichloroethane
<1
Trichloroethene
el
Trichlorofluoromethane
<1
1,2,3-Trichloropropane
<1
1,2,4-Trimethylbenzene
<1
1,3,5-Trimethy1benzene
<1
Vinyl Chloride
<1
Total Xylenes
<1
Respectfully
Submitted:
PAR Laboratories,
Inc.
S. Rice
Laboratory Director
<
<
<
<
<
<1
<
<
<1
<
<
<
<
<
<
<1
<
<
<
<
<
<
<
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Laboratories,PAR
Inc.
2217 GRAHAM PARK DRNE
=;;I
P.G. BOX 41148
CHARLOTTE, NC 28241-1483
7041588-8333
December 10,_ 1996
Reference No: 96 4584
Made For: Spectrum Dyed Yarns (Belmont)
P.O. Box 1006
Belmont, NC 28012
Attention: Buddy Burch
Analyses Of: Monitoring Well
Marked: MW 1 11/21/96 Graff
Received n 11/21/96
Analyses:
pH Val.(SU)11121 0813 CH
i T l
Turb(NTd) 18.00 11/22 1538 CH
()
r 52 11/25 0900
Chlorides 11a 11 1421 CH
Sulfates 11/ 1 1415
T S 129 11/ r 1600 G
TOE 2.59 11/27 1530 F
Respectfully submitt d
PAR Laboratories, Inc.
j0 dS.R i

Reference No:
Made For:
r4l,rGRAHAM PARK DRIVE
IR Laboratories, Inc.
5 4583
Spectrum Dyed `urns
PO Box 1006
Belmont, NC 28012
Terry Ward'
Analyses of: _ Monitoring Well Sample for Volatile
Compounds S S J
Marked: MW #1 Upstream 1 55 Graff
Received On: 1155
Analyzed n 15 @2100
Benzene
Bromob nz n
Brom chloromethan
Brd cdich1ormathan
Bromoform
Br amour than
n utylban n
c-Brrt,ylb nz n
t rt Butylb nz n
Barron t ctrachlr r i
hlor b nz n
hrnthann
Chloroform
Chloromethane
- hlorot lu n
Cii bromochloromethand
1 , -h ibrom --S- hlor pr pan
1 ,Dibrrxratha,nr
ibromom thane
1 , -h i chlorob n nd
1 , - Dichlor b nz n ,
1 , -Di c'hl r b nz n
Dichlorodiflr,s r r th n
1,1-Dichi1 r h n
1, 2- D i c`h l r;cr a t h a n
1,1-Dichloroethene
continued
(Ppb
.5
<.
.5
.
e.
.5
.
.
<.5
.5
.5
<.5
.
<.5
<.5
.5
.5
.
.
.5
Organic

Reference No.: 95 4583
Page 2
(ppb)
cis-1,2-Dichloroethen'5
trans -1,2-Di chloroethene <.5
1,2-Dichloropropane <.5
1,3-Di chloroprop ane <.5
2,2-Dichloro,prop ane <.5
1,1-Dichloropropene <.5
Ethylben zene <.5
Hexachlorob utadiene <.5
Isopropylhen zene <.5
p-Isopropyltoluene <.5
Methylene chloride <.5
Napthalene <.5
n-Propylbenzetie <.5
Styrene <.5
1,1,1,2-Tetrash lorot have <-5
1,1,2,2-Tetrachloroethan e <.5
Tetrash loroethene <.5
Toluene <.5
1,2,3-Trichlorobenzene <.5
1,2,4-Trichlorobenzene <.5
1,1,1-Trichloroethane <.5
1,1,2-Trichloroethane <.5
Trichloroethene <.5
Trichloroflu oromethane <.5
1,2,3-Trichloropropane <-5
1,2,4-Trimethyl[5emane <.5
1,3,5-Trimethylbenzene <.5
Vinyl chloride <.5
o-Xylene <.5
M-Xylene <.5
P-Xylene
Respectfully Submitted:
PAR Laboratories, Inc.
id?S. Rice
Laboratory Director

PARPAR Laboratories,, Inc.
LABORATORIE ,INC 17 GRAHAM PARK DWE
P.O. BOX 411488
CHARLOTTE, NC 28241-1483
7041588.8888
December 14 1995
Reference No: 95 458
Made For: Spectrum Dyed Yarns (Belmont)
P.O. Box 1006
Belmont, NC 28012
Attention: Terry Ward
Analyses Of: Monitoring Well
Marked: MW #1 Upstream 1 1, 30/ 5 Grab
Received On: 1 1 /30/95
Analyses._
(NTU
1"urb(NTU) .54 11/30 1610
(pp)
COD 75 16 0751
Chlorides 3.88 111 117
Sulfates 1 101 1145
TDS 123 12101 141
TOO <1.00 12111 1130
Respectfully submitted:
PAR Laboratories, Inc.
J S. Ric
Laboratory Director

CHAIN OF CUSTODY
PAR Laboratories, Inc.
Phone [phone]
Shipping FAX [phone] Mailing
2217 Graham Park Drive P.0, Box 411483
Charlotte, NC 28273 Charlotte, NO 28241-1483
It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc,
and the Nouth Carolina Department of Environmental Health and Natural Resources.
Company Name,(Bilfing)
Comments,
Address
City, State & dip Code
Feint of Contact & Telephone Number
Sampled By: ­1 i��
11
IS THIS, FOR STATE or EPA
REPORTING? YES
�f NO_
*SampleType: DW— WW—GWMW ?o HW Soil
Other
1/1'
Samples:MaIntained 9 <4"C Yes -"No
—
_ Rec'vd @ <4*C YesZ;�No Preserved: Yes',�' No
Sample Location &
Set Up
Collection
Analyses
Station Number C
G Date/Time
Date/Tirne
Requested
(n
to
W/
L Re,flnquisheP,b�: - ) Date/Time
4-
elinquish6dy: Date/Time
Received by: Date/Time
L-Q-0-0
Received by: DafetTime
;0 U=Urab%)WDrinking water *WW=Wastewater *GWl)AW= Groundwater monitoring well "HW�,Hazardous waste
WP 12i'M94

Laboratories, inc.
1..�BORATORIE INC, 221 GRAHAM PARK DRIVE
PAR PAR
i P.O� P 411483
CHARLOTTE, NC, 8241.1483;
7041588-8333
December 14, 199
Reference No: 95 4584
Made For: Spectrum Dyed Yarns
PO Box 1006
Belmont, 01
Attention: , `erMry Ward
Analyses of: Monitoring Well mple for Volatile
Compounds ( )
Marked: W #2 Downstream 11/30/95 Grab
Received On: 1 1 g
Analyze On: 12/04/95 @2100
Analyses:
Benzene
Rromobenzene
Rromochl rom th ne
Bromodichlormethane
RrcamoforT
Rromomet hang
n-Butyl benzene
sec-Rutylbenzen
tert Butylbenzene
Carbon tectrachloride
hlorobe zen
hlroethne
Chloroform
horometne
-hl r toluene
4- hlor toluene
ibromochlor metgene
1,2 Dibromo- chloro ro ne
1 , i brmet`1ne
Dibromor ethane'
1 , ---- i ch orobenzhne
1 , - Di nh l or beriz ne
1 , 4- Di chloroenz ne
ic�hlo rod if luoromethane
1 , 1-is loroeth ne
1, -Dic for ethane
1 , 1- i chl roet here
continued....
organic

Reference o. 8
Page,
pph
cis 1, - i r i n.
t r rr -1 , l rahl r t en
1 , -Di hl rr pr ap n .
1 ,, -Di hl ropropdrr .5
2, Di hl r pr p rr <.
1,1- i hlc r prop rr . <
Hexachlorobutadiene p 5
Isopropylbenzene
p-Isopropyltoluene <.5
Methylene chloride .5
N pt h 1 n .
rr prop l b n n .
t 'rrr < . 5
1,1,1,-T trashlor th r°r .5
1,1, ,2-T tr hl'groath n .5
Tetrachloroethene 1.
Toluene <. 5
1 , :, -Tri hlor benze r .5
1 , , -Tri hl r bonze r .
1,1,1 Tr1 h r th n .5
1,1, Tri hloro th r .5
Trl hloro th rr .5
Trf hl r rflu r th rr
1 , , --Tri hlor r p rr .
1, , -r i m h l d r ri . 5
Vinyl chloride <,5
o-Xylene .
m-Xylene <.5
P-Xylene .
tespectfully Submitted:
PAR Laboratories, Inc.
qa�
JO S. Rice
Laboratory Director

PARPAR Laboratories, Inca
LAB ORATORIES, IVC 2217 GRAHAM PARK DRIVE
R.O. BOX 41148
CHARLOTTE, NC 28241-1483
704/588-8333
December 14, 1995
Reference No 4584
Made For. Spectrum Dyed "urns (Belmont)
R , . Box 1006
Belmont, NC 28012
Attention: Terry Ward
Analyses f Monitoring 1
Marked: 1 #2 Downstream 11/30/95 Grad
Received On: 11/30/95
Analyses:
Td
T rb NTU 11/30 1610
1 60 12/06 0751
Chlorides 44.19 1 / 1 1130
Sulfates <5 1/01 1145
TDS 226 1 / 1 1415
TOC <1.001/11 1130
Respectfully sub itt da
PAR Laboratories, Inch
qa-L
JfS. Rica
Laboratory Director

CHAIN
PAR Laboratories, Inc.
Phone [phone]
FAX [phone]
Shipping Mailing
17 Graham Park Drive P.O. Box 411483
Charlotte, hits 28273 Charlotte, NC 28241-1483
It is essential that all information be recorded on this Chain of Custody document for acceptance by Pad Laboratories, Inc.
and the-Nouth Carolina Department of Environmental Health and Natural Resources.
Company 1` (Billing)
omrnents
Ljfl:��
Address
City, State & Zip cods ._
Point of Contact & oiophone Number
MM
pie
---
IS THISFOR STATE°I
YES NO
*Sample Type: .— —
MW " HW
Soil Other
at ple aintained @ <40C Yes
R c'vd @ <4'C
Yes Ao Preserved:
Yes N
Sample Location &
Set Up
C0ection
Analyses
Station Number C
G DatefTime Date/Time Date/Time
Requested
1A�
w
Relinquished by: Datel"ime Received by; ate i e
d A :.r.`=
linqui hec y: Dateffirne Received by: Datefrime
ompcsite G=Grab "D =Drinking water 'WW= astowater "tD v`tutW= round atar monitoring well 'H =Hazardous waste
HA,t k.WP 12., 071'24

! .4. DF!' 1', O
tJ1
C
Li
w rxYeLm� �{, y$,,k e4'im �BSd1 [e
October 3, 1995 DYED YAPNS. INC.
Mr. Steve lorad
Hydrogeologist
Groundwater Section
919 N. Main Street
Mooresville, NC 281J5
Facility: Snectrum Dved Yams. Inc:
Piedmont Plant Belmont N
Dear Mr. orad:
This letter is written in reference to the Notice of Violation issued to Spectrum Dyed `urns"
Belmont, NC facility;
On March 1, 1993, Spectrum purchased Dixie fe Yarns, Enc.'s Piedmont Processing Plant. After
e purchase, the plant was renamed Spectrum Dyed Warns' Piedmont Plant. Before the
purchase was complete, a thorough site assessment occurred at the facility and groundwater;
contamination was discovered'. The buy/sell. agreement notes these findings and states that Dixie
Yarns has sole responsibility for clean-up of the site. A trust fund was also set-up in orderfor
monies to he available when needed.
The contaminants which were listed in the NOVare not contained in any dyes or chemicals that
Spectrum Dyed -Yarn uses or have used since the facility was purchased. Additional
information, including purchasing records can be provided if needed.
From the information provided., 1 would hope the NOVto Spectrum could be rescinded. Please
review this information and contact me' if you have any questions or need any additional
information.
Sincerely;
Rick 1ilpatricl3
Safety & Environmental affairs Manager
2 TH FLOOR CUSTOMER SERVICE 136 PA PERSON RD, 422 15eh ST, SW 161 MEOMONT ST.
1450 BROADWAY Phom 800-828 2078 (SPUN) P0. BOX 609 P.0, BOX 1308 P.11e BOX 1006
NEW YORK, NY 10018 Fax: [phone] " KINGS MOUNTAM, NC 28086 HICKORY, NC 28603 ORMONT, NO 28012
Phone: 212 391-BIOI 1-000-831.6343 (FILAMENT) Phom 704-739-740t Plaof 704-322-1663 1e:704-826.1614
1.800-382.4760 Fax:[phone]-9456 Fax:[phone] Fax:[phone]
Fax: [phone] Fax: [phone]

gate of North CarolinaK AWA S
Department of Environment, PF'Pr-
Health and Natural Resources �
Division of Environmental Management �
Jcrr s B. Hunt, Jr., Gover=
Jonathan B. Howes, Secretary
A. Preston Howard, Jr., ., Director
DIVISION OF ENVIRONMENTAL N'
October 11, 199
_CERTIFIED I,:
RET E E PT REQUESTED
Spectrum Dyed Yarns
Post OfficeBox9
Kings Mountain, North Carolina 28086
Attention: Mr. Rick Kilpatrick
RE: Notice of Regulatory Requirements
15A NCAC 2L Classifications and
Water Quality Standards Applicable
to the Groundwatersi
Piedmont Plant
AtoC 1021181-0005
Gaston County, N.C.
Dear Mr. Kilpatrick:
ick
Chapter 143, North 'Carolina General Statutes, authorizes and
directs the Environmental Management Commission of the Department
of Environment, Health, and Natural Resources to protect and;
preserve the grater and air resources of the State. The Division
of Environmental Management has the delegated authority t
enforce adopted: pollution control rules. This Notice, dated
tuber 11, 1995 supersedes a Notice of Violation datod September
22, 1995,
Eased upon a review of your groundwater compliance
monitoring data submitted on 1 /1 /95, 4/ 0/95 and: / 3/95 as a
requirement of the ,subject permit, the Division has reason to
believe that the permitted activities have resulted in the
groundwater standards being exceeded. The standards can be found
at 1 5A NCAC
R.O. Box 29535. Rd i h, North Ccrofina 7 1` i ph ne 1 - 33-701 FAX[phone]
An Equal Opportunity Affirmative Action Employer recycled/ 10% pcst-consumor paper

pppppp,-
spectr--Ir"7. Dyed Yarns
Piedmont Plant
October 11, 1995
Page Two
Specific constituents which are exceeding the groundwater
standards are as follows;
Con stitUent
& Well No., Date Samvled Concentration* 2L Standard*
Well #1
Tetrachloroethane 12/6/94 2.34 MDL
Well #2
Tetrachloroethane 3/20/95 3.46 MDL
11213-
Tetrachlorobenzene, 3/20/95 0.93 MDL
Tetrachloroethene 7/31/95 2.7 0.7
1,2,3-
Tetrachlorobenzene 7/31/95 1.3 MDR
*Concentrations reported in parts per million
MDL Method detection limit
Commission Rule 15A NCAC 2L .0106(d) states:
Any person conducting or controlling an activity which
results in an increase in the concentration of a substance
in excess of the groundwater standards as a result of
activities conducted under the authority of a permit issued
by the state, shall, where such concentrations are detected
at or beyond a review boundary demonstrate, through
predictive calculations or modeling, that natural site
conditions, facility design and operational controls will
prevent a violation of standards at the compliance boundary;
or submit a plan for alteration of existing site conditions,
facility design or operational controls that will prevent a
- violation at the compliance boundary, and implement that
plan upon its approval by the Director.
The modeling information or a plan for alteration must be
submitted within thirty (30) days of receipt of this letter.
in addition, you are required to submit a topographic map
drawn to scale depicting the location of the waste boundaries,
all property boundaries, and monitor wells. The above should be
submitted within 30 days of receipt of this letter.
W

ppppp�
Spectzum Dyed ar
Piedmont Plant
October 11 1995
Page "three
voluntarily achieve compliance may result in the recommendation
of enforcement action, including the issuance of a Special, Order
against you under the authority of General Statute 143-215.2
and/or revocation of your permit;
"Your response and/or questions should be directed to Steven
Bocrad
Sincerely
H. Keith Overcash,
Regional Supervisor_
cc,: Bob Cheek, Permits and Compliance Unit
Rex Gleason, Mooresville Water Quality Section
BB

"4MO 'NT, 11VALT11 _NME
&NATURAL RFSOUR('"
OCT 2 0 1995
DWISION of ONk"
MOOR'sVit"[E
t
%E,Cffw
October 17, 1.995 DYED YAPNS, M,
Mr. Steve Boral
Hydrogeologist
Groundwater Section
919 N. Main Street
Mooresville, NC 28115
Facility: 5pgqnWLPygderns, Inc.
Piedmont PlantBelmont., NC
AtoC #21181-0005
Dear Mr. Bograd:
This letter is written in reference to the Notice of 'Regulatory Requirements issued to Spectrum
Dyed Yams' Belmont, NC facility, dated October 11, 1995:
On March 1, 1993, Spectrum purchased Dixie Yarns, Inc.'s Piedmont Processing Plant. After
the purchase, the plant was renamed Spectrum Dyed Yams' Piedmont Plant. Before the
purchase was complete, a thorough site assessment occurred at the facility and groundwater
contamination was discovered. The buylsell agreement notes these findinggs and states that Dixie.
Yarns has sole responsibility for clean-up of the site. A trust fund was also set-up in order for
monies to be available when needed. Karen Walker with the Division of Enviromnental
Management is currently overseeing the project for the state, the project has been issued
Groundwater Incident No. NC 9957;
The contaminants which were listed in your notice are not contained in any dyes or chemicals
that Spectrum Dyed Yarns uses or have used since the facility was purchased. Additional
information, including purchasing records can be provided if needed.
From the infortnation provided, 1, would hope this notice to Spectrum could be rescinded and
forwarded to the responsible party being Dixie Yams, Inc., Chattanooga, TN. Please review
this information and contact ine if you have any questions or need any additional information.
Sincerely,
, Pick Kilpatri
Safety & Environniental Affairs Manager
28TH FLOOR CUSTOMER SERVICE 136 PATTERSCU RD, 422 15 th T. SW 161 NEDMONT ST,
1460 BROADWAY Phone: [phone] ISPUNI P.OBOX 609 P.C.Y. Box 1308 P.O. Box 1006
NEW YORK, NY 10018 Fax: [phone] KINGS MOUNTAIN, NC 28086 HICKORY, NC 2B603 SELMONt NC 28012
Phonc 212-3911181 1-800-831,5343 flUkMENTPhom 704-739-7401 Phonw 704-322-1663 Rvww 704-82$,1514
1-800-382-4760 Fax: 704-322,16613 $00-221-9456 Fax: [phone] Pax: 704-825-4471
Fm 212-921-9139 Fax! 704-739-7257

. Steve
h�&vgeotogist
Groundwater Settnn
919 N. Main
Mooresville, NC 1.15
Facility;T
] ltntnt.
Dear Mr. n
This letter is written in referenceto the Noticeof Violation tin issued to Spectrum Dyed
Belmont, NC facility.
On Match 1, 1993, Spectrum purchased Dixie Yarns, �'s Piedniont Processing Plant. After
the purchm, the plant was renamed Spectrum Dyed Yam' Piedmont Plant. lbre the
purchase was complete, it thorough site assessment occurred at the facility and groundwater
contamination was discovered. The b y s li agreement notes these findings and states t Dixie
Yams Ims soleon ibility;for clean-ur of the site. A trust fund was also set-up in order for
mordes to be available when
e contaminants which were listed in the NOVare not contained in any dyes or chemicals that
Spectrum Yarns uses or have used since facility Nvas purchased. Additional
information, including purchasing records can be providedof
From the information provided, I rind hope the NOV to Spectrumd be rescinded. Please
vier this information atW contact me if you have any tions or need any additional
information.
-
rely,
a
lick-0l
Safety & Environmentala."Manager
2IT4 PtOOA CUBTOMER 9~CO 134 PEA N 40. 492 1 Pth 8T. 8W
1460 6ROMWAY Phow SM8,26-2076 ISKNI P.11 BOX 000 PA ROX008 #UOYt
WW Y Km NY 10014 Pat 104-74*4104 KtRW60 140WAYm NC 29803 RaACWW28012
MWAI 12- i• i t i - f 3,*3 *LAMM Phomi 7 • -7401 Rmv ,32 -1 R , 16t
i^ '#08 4764t Pax: 704.3124$06 -2..21 465 'Fax. 704.3 2.1 8 Fax. 7 20 77.
Pm" 43-661-si FOB 764438.1118
4°" wndioa& GT:Lt

State of North Carolina
Department of Environment, , and Natural Resources
Mooresville Regional Office
James G.Martin, Governor Albert F Hilton, Regional Manager
William W. Jr,, Secretary
DIVISION OF ENVIRONMENTALMANAGEMENT
December 5, 1991
William Burch
Dixie "urns, Inc,
Poet Office Box 100
Belmont, North Carolina 28012
RE: TOX Sampling
Piedmont Processing
Gaston County, NC
Dear Mr. Burch:
On December 3, 1991, the; Groundwater Section of the
Mooresville Regional office received the compliance monitoring
reports for the subject site. Please not the following analysis
changes
Volatile organic compound analysis requires test meth A
"Standard methods for the Examination of Water and Wastewater"
or Method 502.2 "Methods for the Determination of Organic
Compounds in Drinking Water". TOX is no longer acceptable.
If you have any questions regarding this matter, I may be
reached at 0.
Sincerely,
�,p
Tony McManus
Hydroge logical Technician
TLM/ds
91North plain s t, Moormille, NC 28115* Ieltphone 3-169 s 3
An Equal Oppominity Affirmative Action Employer

F. 7TCh.ck ondition of

Ct E
Health and n Natural Resources
Jomes B, Haunt, Jr_ Governor
Jonathan B, Howes, Secretary
Linda D�ane Long, Regionol Manager
DIVISION R ENVIRONMENTAL
September 22, 1995
ER JfLE MAC
RETURNR R R
Piedmont Processing Company
poet office Box 1006
Belmont,, north Carolina 28102
Attention. Mr. Buddy Burch
E: Notice of Violation
15A NCAC 2L Classifications and
Water Quality Standards Applicable
bl
to the Groundwaters
:P-*,edmont Processing company
Gaston County, N.C.
Dear Mr. Burch:
Chapter 143, North Carolinas General Statutes,t authorizes and
directs the Environmental Management Commission Of the Department
of Environment, Health, and Natural Resources to protect an
preserve thewaiter and air resources o the State. Division
i si+ n
of Environmental na ement has the delegated authority to
enforce adopted pollution control rules.
Based aeon e review of your groundwater compliance
monitoring data submitted on 1 1 / 5, 4/201 5 and 8/23/95 as a
requirement of the subject permit, the Division has reason to
relieve that the permitted activities have resulted in the
groundwater , standards being exceeded. The standards can be found
at 15A NCAC 2L.
919 North stain Street, Mooresville, North Carolina 28115 Telephone 704-663,1699 FAX a - 3-6040
An Equal Opportunity AffirmotNe Action Employer 50%, recycled/ 1 % post -consumer popeer

p _ ,
Page
specific constittients Which are exceedexceedinq the groun«
stand4tds are as follows:
DAIS d
wall
Well #2
w .e« -
Tetrachlorobenzene
Tetrachloroothene
3/20/95
3.4
3/20/95
0.93
MDL
"7/3 : 9
7/31/95
1.
*concentrations , parts piat million
Method detection
commission«
tj
.. awe, � � � r` •. ��� �« � •�* �� � ^°•. « «

PPPPF-
Piedmont Processing Company
September 22, 1995
Page Three
of enforcement action, including the issuance of a Special order'
against you under the authority of General Statute 1.4 1 .
and/or revocation of your permit.
Your response and/or questions should be directed to Steven
ograd,
Sincerely,
B. Keith Overcash,
Regional Supervisor
Enclosures: m lian e Monitoring letter
e Bob Cheek, Permits and Compliance Unit
Rex Gleason, Mooresville Water Quality Section

DATE. T °
iCD: s SUBJECT:„ Pik' 2
4 r
„
69,
f
r x
ti.e. �� i we„a� w Via. ..•
"
"
a
From

State at North Carolina f
Department at Environment
Health and latural Resources
Mooresville Regional Office
��l
James B. Hunt, Jr. Governor F=
Jonathan B, Howes, Secretary
Linda L i ne Long, f e ionaE Manager
DIVISION OF ENVIRONMENTAL
September 22, 1995
11
REIPM E
Piedmont Processing mean
Fast Office ox 1006
Belmont, North Carolina 28102
Attention: Mr. Buddy Burch
RE: - m lian e Monitoring
Gaston County,
®ear Mr. Burch:
A review of your compliance monitoring data indicates that
analytical results for pH and total organic carbon (IOC) have not
been submitted for the following samplingevents:
November, 14
March, 1995
July, 1995
You are requested to submit 'analytical results for pH and
TOC for the monitoring reports sited above within 14 days of
receipt of this letter or an explanation why you cannot
omply
Should you have any questions concerning these requirements
please contact sae at 1 , ext. 241.
Sincerely,
g
Steven Bogral
Hydrogeological` Technician
SEB
919 North Main Street. MooresVille, North Cora€inca 115 Telephone [phone] FAX 7 - -6040
n Eqtid Opportunity Affirmative Action Errrpbyerrecycled/ 10 post -consumer pope€

DEHNR
. SVE1 BOGRAD
HYDROGENOLOGICAL TECH.
FROM: s
1 BUDDY BURCH
SPECTRUM DYED YARNS
PIEDMONT DIVA
BELMONT, N.C. 28012
SUBJECT;
LETTER OF VIOLATION DATED SEPT. 22--,1 (RECEIVED LETTER �2 /95);
THIS LETTER IS TO CONFIRM OUR CONSERVATION I HAD WITH YOU 9/ 5 AT ABOUT 1I 00
ON THE "FAILURE TO SEND PEADINCS ON THE PH AND TOC FROM OUR MONITOR WELL AS PAR AS I
CAN DETERMINE 'AS .THROUCH AN OVERSIGHT. DO NOT HAVE ANYTHINC SUCH AS A PERMIT
WITH THE CUIDELINES, ON THEM TO GO BY. WE DO NOT HAVE A COPY OF THE EASE SAMPLES BEFORE
E PUT ANY WASTE WATER IN THE HOLDING POND. IN THE 14 OAFS WE WILL CET SAMPLESFROM!
THE WELLS AND SE D YOU A COPY CP THE PH AND TOC. PAR LABS OF CHARLOTTE WILL HE H
AFTER LUNCH TO DAY FOR THE SAMPLES. THEY ARE THE ONES THAT DO ALL OUR MONITOR WELL
TESTI
CIS THE � HEER VIOLATIONS UR, HEALTH AND ODFFLIANCE OFFICER FOR ALL SPEC" 'PLANTS,, RICK
KILPATRICK HAS BEEN NOTIFIED TO HELP TEAL WITH THIS. HE HAS A COPY Or THE LETTER,
YOU SUGGESTED T TOTE COM TO YOUR OFFICE WITH OVR.RECORDS AND YOU CAN CHECR ,YOU
RECORDS WITH US AND MAYBE WE CAN GET TOCETHER ON WHAT WE SHOULD BE DOING, WE WILL
UA THAT. W14EN WE CET TWE PR AND 'T C REPORT RACK FROM PAR LAD9 WE WILL CAlt YOU
D SEE WHEN WE CAN COME TO YOUR OFFICE..
IN THE 141ANTIME WE WILL BE LOOKINa THE PROBILM,UVVX. .IT WILL BE HARD SINCE LTD
NOT HAVE DIXIE YARNS RECORDS WHEN SPECTRUM PURCHASED TRIS PLANT.
BUDDY BURCH
SE'F-CTRUM PIEDMONT DIVISION
161 PIEDMONT ROAD
P.O. BOX 100
RETZON T, NC. 28012
COP TO! BILL, EICK,A D FILE
F C12,
} STEV H . U—SOH
DENNR
CORESVILL NC 28115

L MANAGEMENT - GROUNDWATER SECTION
I EGROU:NDWATER QUALITY,, MONITORING::
P.O.
C PLI:
For: add PALE10H
NC 2 s
COMPL1A:N:CE:REPOAT," f RM
t: 1 Pk
PERMIT NUMBER: (REQUIRED)
Facility Name SPECTRUM DYED YARNS INCPIEDMONT DTI. � Non -Discharge
Noun 1 FRAitON BONGMONITORED
Well Location � � �_ � Lagoon Septic i Grain Reld
Well Identification Number _�_Ft.
Well Diameter �.. Sample (Screened) IntorvaJ _ Ft. T Ftn ld Subsurface Low -Pressure
Piping (LPP)
Depth to Water Le fk, below measuring in (before sampling) Und Applicaton of Sludw
rinpoint i — f1. above land surfaceOther
ai of meter pub l before sampling _ � . S 1S' PH ARotary Distributor
Fief Analysis: p Specific ConductanuMhos Temp. o Odor .-- Appearance —
Date Samplee Collected ?-3t-95gate Lab Sample Analyzed
Laboratory Name Gedification No.-20
GOD _ r gil Nitrite ( ) as N rng/l Ni _ mgA
Co
llt '1 1rnl NitratemgA mg/1
lit ® M E Total /1 00MI orris; Total asmgA Zh x Zinn it
for highly turbidSamples) At w Aluminum mgA Pesticides/Herbicides
DISSOIVed Solids.Total 2 5 c gj Turn rnt (Specify Compounds) x f
(whenpH analyzed) _ -unit - Calcium mgA � ug l
TOC 'rngll i1 rr1 1I ug/l
Ch
1 rl + _. _. _._ gel Chromium: Taal _ m. _. mgA
ugA
Arsenic_ _ gel Cu mgA Other (Specify Compounds and cic
Grease`l rngfl E - Iron r°nl Concentration units)
r° ri m Total mgAg' - Mercury � g
Phenol rr1g11 Potassium rng/I
Sulfate rng/l Mg - Magnesium rig/l NNA 'v,z
Specific Conductance-___�uMhos Mn - Manganese---_-- g/l � Ai
Total Ammonia _ mg/l Na- Sodium ._ mgA
TKN as N rng/l Turb T PPS _... .
6 t sib
udWsbWed and
l CERTIFYTHAT THIS E l TRUE ACCURATE. o
3
Antrations. (see 42 on back)
Instructions,Soo back for
ignatur o CrTlltt kt��int t Submit blue, green, � low co only t r� above.
'
Gam"-aGW-59 REV, 4 1

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PAR
PAR Laboratories, Inc.
!ABC?�?ATORIES WC
= 9;7
2217 GRAHAM PARK DRIVE
P 0, BOX 411483
CHARLOTTE, NC 28241-1483
704!-988-8333
April 13, 1995
Reference No:
95 1120
Made For:
Spectrum Dyed Yarns (Belmont)
PO Box 1006
Belmont, NC 28012
Attention:
Terry Ward
Analysis Of:
Groundwater Monitoring Wells
Marked:
Sample 1: MW #1 3/20/95 Grab
Sample 2: MW #2 3/20/95 Grab
Received On:
3/20/95
Analysis:
Date Analyzed 3/22/95
Dichlorodifluoromethams
Ch I oromethane
Vinyl Chloride
Bromomethang
Chloroethane
Flu orotrichloromethane
1,1-Dichloroethylene
Dichloromethan
e
t rans- 1 , 2-D i ch I o roet hy I ene
1,1-Dichloroethane
Dich1oropropane
cis-1,2-Dichloroethylene
Chloroform
Bromochloromethang
1,1,1-Tr ichlcarat hane
1,1-Dichloropropane
Carbon Tetrachloride
Benzene
1,2-Dichloroethane
Trichloroethylene
1,2-Dichloropropane
Bromodichloromethane
Dibromomethane
1,3-Dichloropropane
Toluene
<.5
<.5
.5
<.5
<.5
.92
<.5
<.5
<.5
5
5
<.5
< .5
<.5
<.5
<.5
<.5
<.5
<.5
<.5
<.5
<.5
5
- 2--
<.5
<'5
<.5
<.5
<.5
<.5
<.5
.66
<.5
<.5
<,5
<.5
.5
.5
<.5
<.5
<.5
<.5
< - 5
.52
<.5
<.5
<.5
<.5
<.5
continued .....

PAR Laboratories, Inc.
LABORA
��� `. _ O 41148
'HARLOTT , He 28 41-14 "
7 4 /5 8- 8 3
April 13, 1995
Reference No: 95 113
Made For: Spectrum Dyed Yarns (Belmont)
P.O. Box 1006
Belmont, NC 28012
Attention: Terry Ward
i
Analyses Of: Monitoring Well
Marked: Sample #1 - MW #1 3/, 35 Graff
Sample # - MW # /20/95 Grab
Received On m 3/20/ 5; /3 5
Analyses:
Sample 1 3 TESTED
NTU}
Tur b(NTU) .80 1.60 /2 1331
pp
SOS <5 <6 13
Chlorides 3.91 52.83 3/22 1400
Sulfates <5 13 3 23 153+
TS 1 1 1500
Respectfully sa mitt
AR Laboratories, Inc
S. ice
Laboratory Director
x:.r

PARPAR Laboratories, Inc.
1 AHA . r �iw , l � .: )
LASORa . r .
P.O. B , -4 1
HARLC
i418. a
Reference NO: 94 4780A
Made or: Spectrum hayed
Varna (Belmont)
PO Box 1006
Belmont, NC 28012
Attention: Terry hard
Analysis of: Groundwater Monitoring Wells,
Marked: Sample 1 : MW
#1, 1 05 4 Grad
Sample : MW
#2, 1 /06/94 Graff
Received on: 12/06/94
Analysis:
6230D Compounds
Date Analyzed
1 /09
12/09
p
i hl r ifl r r e har e
.
<.
hl r methane
.5
Vinyl Chloride
<.
B romomet hane
.®. 5
hlor sethane
.5
.5
Bler r richlnr met an
.5
.5
1,1- airhl r ethy ene
.5
,5
Diehl-oromet hane
. 5
.5
trans-1, ,- i hlnr eth lene
,5
.5
1,1-ihlnrethane
.5
, --Diehl r pro axle _
.5
.5
is-1, iehloroe h "l ne
.5
Chloroform
. 5:
. 5
Bromoc h l ornmet hang
. 5
<.5
1,1,1-Tri hl ethane
.5
_.5
1, 1-jai r l r propane
. 5
a 5
Carbon Tetrachloride
.5
5
Benzene
. 5-
.5
, -D chl roethane
5.;
<.5
T`ri hlc r ethylene
.5
.5
1,-ilroprpan
,5
e..5
Br modiehl romethane
.5
5
i rret hane
.
. 5
1,3-D hle r pr pane
.5,
.5
Toluene
. 5
.5
continued .....

page
94 4 O
Cells JAN
1 � �..
1 , 1 , -Tri hl roeth ne
Tet r eh l roet h .ne
2.34
1 , B tli hl ropr sp ne
.
Cibromochl r ethane
m
Chlrbenzene
W
thylbenzene
1, 1, 1, -Tet rash l oroet h n
.
Total Xylenes
Styrene
.B
Isprnpylbenzene
wB
1, 1, 2, -Tet rach I o romet have
1,,-Trihl+rnprne
,,
h-Prnpylbenzene
Bromoben ene
1,,-Trirrethlbenzen
-Ch'l rot l ene
-Chlor t aluene
.
ert-But y benzene
1, ,4-Tr methylbenzene
<.
en-Butylbenzene
Is propyltnlgene
.
1,3-Bi hlorobenzene
.
1 ,4-Di hlc robenzene
n-Brut yl benzene
-Di hlor benzene
1 , ,4-Tr chlorobenzen
.
Hexachlorobutadiene
phtnlene
1, ,B Tr hlor benzene
1.0
1
--
ppb
Method 504 Compounds
Analyzed on 1 /9
Ethylene dibromide (BBB).0
1, -Dibr Chl r propene .0
RespectfullySubmitted:
PAR Laboratories, Inc.
J01® ice
Laboratory Director
12/9
.0
.0

State of North Carolina
Department of Environment,
Health and Natural sources 4
Mooresville le e ion ffie
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
Vivian Burke, Regional Manager
DIVISION OF ENVIRONMENTAL MANAGEMENT
July 16, 1993
a
l
. William Burch
,Spectrum Dyed Yarns
Past Office Box 1006
Belmont, North Carolina 801
RE: Compliance Monitoring
Piedmont Processing
Gaston County, N.C.
Dear Mr. Burch
The Groundwater Section of the Mooresville Regional Office
has received the compliance monitoring 'e rt for March 1993 for
the subject site. Currently we are still awaiting the November
1992 monitoring report with the extended analysis for volatile
organic compounds ( C If the November reporting has not been
accomplished, our July monitoring samples must include the
analysis for O' a by Method 6230D or 502.2. TOX is no longer a
acceptable method as stated in our December 5, 1991 letter.
Additionally, please submit a detailed, scaled site mad
showing the relationship the two monitor wells to the waste
water equalization basin.
Should you have any n e tion , please contact me at, (704)
83-F1899, ext.241.
Sincerely,
Robert B . Krebs
Hydrogeological Technician
Attachment: December 5, 1991 Letter
RBK/sc
919 North Moin Street, Moore it , North Ccrolina 28116 Telephone 7 -1
An Equot Opportunity Affumative Action Employer 6ft recycled/ 1 post -consumer poper

PAR Laboratories, r .
97 GRAHAM PARK
DRNE
TC,,,,,,ES OvC P,0 BOA; 41148
9
' CHARLOTTE, NC 8 1-14 3
704688-8333
May 31, 1994
Made For: Spectrum Dyed
Yarns (Belmont)
PO Box 1005
to
r
urn
Attention: Terry Ward"
Analysis Of: Groundwater monitoring
well
For March 1994
xw
Marked: Sampl 1 :
1 , 5 16 Grad
.�
�
Sample
, 5, 1 5 Crab
rn
Received On: May 16, 1994
Analysis:
1
6230D Compounds
Date Analyzed
5/1
5/1
( p
i ha l s r d i f l uo rome hang
<.5
.5
Chlor metharl
<.
.5
romomet hana
;,
Q 5
C h f o r e. t a n e.
tea, ..t
w 5
1 1- i hlr roethyle
,.
(.25)
Dichloromethane
.55
.78
trans-1 , .- i hloroethyl n
.5
.5
cis-1 -Di hlor thrylar
.5
(.10
Continued ...

pb1
Chloroform
a 1
r m hlorm than
...
1,1,1-Tri hl a hana
(.30)
1,1- i h1 r pr an
M
Carbon Tetrachloride
<.5
<.
�
-.
Benzene
1 , - i hl r than
ri hloroethylana
.
1 , - l hl oropropar
. 1 1
rom i h 1 romet harp
".
Dibr mom than
.
1 , _ l hl ropr par a
Toluene
.
5
, 1 , - Tri hlor athan
.
Ttra hl rt than
1.61
1, -D hl ropr pan
, a
i t mo h l r mat ha
.
1, ,1, -T tra hl r th n
.
Total Xylenes
<.5
Styrene
.
a
Continued...

PARPAR Laboratories,
Inc.
. 7e . =r>. ;. ' 7 GRAHAM PAR ERNE
y P.O. BOX 411483
CHARLOTTE, NC
8241.148
784 888-8333
Reference No: 94 173
Free 3 of 4
,...
2 _.
(b
I opr py benzen
.5
rcry fore
n
.
1, 1, , --Tet r ch 1 oro et h n
1, ,.-Trichl ropr p ne
x5
a5
n-Prc pyl benzene
, 5
rom benzen
.5
1 , 3, 5-Tr meth' i benzene
.5 _
. 5
- hl r t,ol ne
®5
a5
P. ~nrtltee
.5
:5
C,
tert-But l benzene
, 5
1' , , 4-Tri et h l ber zene,
. 5
5
.
sec- tylbenzene
,5
-I c pr pylte l en
.5
.5
.5
r
a
1,3- ichl r b nzene
,5
...5
1,4- ichl lr benzene
.5
.5
n - ut y1 benzne> `
. 5
5
--D i ch l or ben ene
. 5
.5
1, , -Tri hl benzene
.5
.5
Hexachlorobutadiene
.5
c,5
N pht harp l ene
_„ 5"
1, , S-aTr i h 1 orober zene
. 5
5
Continued .

PAR Laboratories, Inc.
WRIES ANC 2217 GRAHAM PARK DRIVE
P,O. BOX 411483
CHARLOTTE, NC 28241-1483
704/588-8333
Reference No: 94 1732 A
Page 4 of 4
-1 2
(ppb)
Method 504 Compounds
Analyzed on 5/23 5/23
Ethylene dibromide (EDB) <.02 <.o2
1,2-Dibromo-3-Chloropropane
Respectfully Submitted:
PAR Laboratories, Inc.
J n S. Rice tv
0 S'
r�
L story Director
7*0
tZIM
;00
C> rn

i
N. C. Department of Environmental Health
and Natural Resources
919 N. Main Street
Mooresville,North Carolina 11
May 5, 1994
Attention; Mr, Robert Krebs
Gentlemen:
Subject: Monitor Wells Test Results
After receiving test results from our testing la. , we found
that the wrong Tent Method was used, (Vol 2 ) Ref erring to your
letter of September 1, 1993, you stated Test Method, 624would n
longer be used e are collecting the samples again and will b
using Test Method 623 OD of 502.2 stated in your letter.
The results will be seat to you as soon as we receive the
results.
Sincerely yours,
SPECTRUM DYED YARNS, l
Pie mont Plant
William P. Burch
ah
1459 BROAL1WAY,
NEW Y RK, NY 10018
Phone° 212 391 8181
Fax212,921-9139
CUSTOMER SERVICE P, 0BOX 609
P 0, BOX 130
Phorw 800-828-2078 PINGS MTN, NC 2 086
HICKORY, NG 28683
Fax 704-739•4754 Phone [phone]
PhOW 7 -32 1663
8 0,221 9 56
Fax. 794•322-1 68
Fax [phone]
P. O. BOX 1006
BELMONT, NC 28012
Phone: [phone]
Fax [phone]

PAR Laboratories, Inc.
PAR 2217 GRAHAM PARK DRIVE
CHARLOTTE, NC 28241.148
7041588-8333
opr" .' a
Reference N 3160 A
RIVISION
Made For: Spectrum Dyed Yar - �
p 1006
Belmont, NC 2801
Attention* Terri' Ward
Analysis Groundwater Monitoring 'ell
Marked: Sample 1 : MW #1, 8/8 Grab
Sample , 8'8 Grab
Received n August 8, 188
Analysis:
1',,2,'3Q,D Compounds
Date Analyzed 8/2 8/23
i hl r ditl rom than .8
hlrrrethan ,.
Vinyl Chloride.8
r momet hand
hlrethane .
lta r tr hlororre pane .8 .
, 1- i hl roe hyl ne .8 .8
ri hl ro ethane 8
trans1,-ihlrethylene .
1 , 1 i hl oroet han+ .
, 2 i hl r propane . 8 . 8
cis-1,i'ihlrethylne
Continued ...

.."panel u
I
OUDJA4S
"
(
(1
'
.
q L J -, °
"
qL
'S.>
ouezueqojo[43
L. L
OUV4L40eJIOI
quantoi
"9.>
OuRdOJdOJOL40LO-e'�
")
9
8U8LAt4l9O-J0Lt40LJi
®quezuee
"
L «Ly 1 uoqjpo
(i
09 L :ON OOUOJ9�98

Reference N 16
Page 3 of
1
(p
I opr pylb n n
.
.
Br m f ri
, ,
1,1; , -Tr `oro
.
.
1,2,-Tricblorc pr p n
.B
.
n-P opyl benzene
.
Brow b n n
.
1, 3, 5-Tr m t yi rtz n
g
o-Chlorotoluene
p- blcrotnl n
.
.
t rt-Butylbenz n
.B
1,2, -` rim thylb nz nd
.
sec- Butyl nz n
.
.
p-Ise rpy ltlurn
.B
1 ,Dicblorbnzn
1, - ical rob nz n
;.
n-B tylb nzn
.
c-[1ic lnrob n n
1,2, •-Tricolor b z n
.
Hexachlorobutadiene
<.
<.
N pht and n
.
.
1 , ,-Trichlc rob nz n
.
<.
Continued...

Reference N l
Page
(b
Method 504 Compounds
Analyzed on
2
/2
Ethylene dlbr mile (
.02
. 2
1 , 2 1 br mo-3- hl r+ r~ paha
. 2<.02
Respectfully , Submitted:
PAR barlaa n,E
S. Rice
Laboratory Director

..gym-•---^-^.^F.;t
PAR
PAR Laboratories, Inc.
[
2217 GRAHAM PARK DRIVE
LA?8CO�,RRARIES,WC.
f
WMWCHARLOTTE,
nRg O G (y p .g 83
7041588-8333
ggpp
�b ra Ew N.w"
y�.0 y�v
D cembe 0
1993
Reference o.
93 3964A
Made For:
Spectrum dyed Yarns
P.O. Box Ira
Belmont, NC 28012
Attention:
Everette Dillard
Analyses, of:
Monitoring Wells
Marked:
Sample 1 µ MW -1
Sample MW-
Received on:
11/22/93
Date Analyzed: 11/ 12/1/93
Analyses;.
Compound
BIromo ethane
.
romoben ene
.
g
Bromochloromet
Carbon tetrachloride
.
b.lnroben.. en.e
.
r.
`..
1. b rn y lope ene
< .
: lorroe'than '.
W..:w
Chloromethane
+. Sy
r
Ned
kt��s�1{�yoro e1�han
^d •
<
�R^Jq'1.�1�'ca
Di bJ'r rr�'ye t,,Q�$�.j�. ne
is
< .
, -Diehl Groben ene
n
.
Continued ..

PAR Laboratories, Inc.
17 GRAHAM PARK OLIVE
r. t7 P.0, BOAC 411483
CHARLOTTE, NC 28241-1483
704/588-8333
Samples
yp
(ppbf "..
'� -
L. , 2 , T e t: ac h l o & 6f e t h a e
\ . fie'
< .
, ." T ,L i is & Fes+ 6p&. ,� e
,
.
< . 5
--y1 �y � .i. y,,
1 , .f4�.:., `� c .5 o r e 7��°t3�. c& ng e
< . 5
< .
�9ppq� rye+` yi
� yi+aa +may
— L .1 .3G.'4.r 4.tl'r4J�p. A 4F SA..A+1e
< . 5
: .
Vinyl chloride
<.5
<.5
�¢` l "o " ` 4 q.
4o F o $�i'"y r n
< .
<
"fir
,�&-us ply
1 , �'-D2c lor�oe . k ^'1 ilk*
< .. +
< . 5
Dichloromet
Benzene
<.
< .
yy
T r fir'J. L3 r o e Cgg.y�'l. e e
< .
<. 5
Toluene
< . 5
< . 5
Totall ene
< . 5
< .
Styrene-
<<.5
<<.5
c
o yf l
1py3 2.b +'v:' E 4.e
',�.++� .
< .
p mob*
n-Propene
2 , , 5®"Trethyen en
< .
<.
""' ..,1.. e n
. .{,. o*.
d/
.
< .
A� X
y ' yZro" �, �«y'.
,<
'wry'
x5
exert-- tyl n ene
<.
<.5
1 ,, 2 , ,-y r iethylgylen en
<+' . 5y
.
ate} a e z e
< .
}<
p�5�q
. 5
qn �k-:y., .y
"1V``..`- �v�q^.'g4'.�1. �,.t
s4pry+1.
,'�'*0..
onta.nued . . b

State of North Carolina
Department of Environment,
Health and Natural Resources
Mooresville Regional Office
James B. Hunt, Jr., Governor
Jonathon B. Howes, Secretary
Vivian Burke, ReJonal Manager
DIVISION OF ENVIRONMENTAL MANAGEMENT
September 1, 1993
r�
Mr. William Burch
Spectrum Dyed yarn
Post Office Box 1006
Belmont, North Carolina 28012
RE Compliance Monitoring'
Spectrum Dyed yarn
NCO006521'
Gaston County, N.C.
Dear Mr. Burch:-
The Groundwater at ti a of the Mooresville Regional Office
received the compliance monitoring report for July 1993 for the
subject site. The lab sheets indicated that the 'volatile Organic
Compounds ' ) analysis was performed using test Method 624.
As stated in our December 5, 1991 and July 16, 1993
correspondence, VOC's rust be analyzed using test Method 6230D or
502.2. The July 1993 monitoring report will be accepted using
Method 624, but future analysis must t be submitted in accordance
with the above guidance.
Should you have and questions, please contact me at(704)
-1, et. 241.
Sincerely,
Robert B. Krebs
Hydrogeological Technician
RBK/sc
919 North MainStreet, Mooresville. North Carolina 28115 T l p n 7 1 F1 9FAX[phone]
An Equal Opportunity AffirmativeAffirmatrve Action Employer r c yc l d/ 1 C post -consumer paper

So G DEPT. OT NATURAL
RrSOURCEi AND
COMMUNITY DEVELOPNIF'VT
AG 2 6 1993
WISION OF
MOORESVILLE REGIONAL 0if ICE
August. 18 1993
Reference No:: 88 2609
Made For: Spectrum Died Yarn
PO Box 1006
Belmont, NC 28012
Attention: Sam Sanders
Analyses of: Groundwater Samples for EPA 624
Marked: Sample 1: MW1 7/15/93 Graff
Sample : M 2 7/1Grab
Received On: 7/15/93
Analyzed n: 88
;Analyses:
Sample 1
2
pp
Dichlorodifluoromethene
<1
hlcarcameth ne
<1
<1
Vinyl Chloride
<1:
<1
Bromomethane
<1
<1
1,1-Dichloroethene
<1
<
Methylene chloride
<1
<1
trans-1,-D1chl arne ,hene
<1
<"1
1,1-Dichloroethane
<1
<1
Chloroform
<1
<
1 , 1 ,1-Trichl roethane
<1.
<1
Carbon tetrachloride
<1
<1
Benzene
<1
<1
1, -Dich o hdn
<1
<1
Trichloroethene
<1
<1
f`h1oroethane
<1
<1.
ridhlorofluoret e h ne
<1
<1
Continued...

R
PAR Laboratories, Inc.
2217 GRAHAM PARK DRIVE
A TORIES, 0vC
aW
P.O BOX 411483
CHARLOTTE, NC 28241-1483
7041588-8333
Reference No:
93 2609 A
Page 2
(ppb)
1,2-Dichloropropane
<1
<1
Bromp dichloromethane
<1
<1
2-Chloroethyl-vinyl ether
<1
<1
cis-1,3-Dichloropropene
<1
<1
Toluene
<1
<1
trans-1,3-Dichloropropene
<1
<1
1-Chloro-2-bromopropane
<1
<1
1,1,2-Trichloroethane
<1
<1
1,1,2,2-Tetrachloroethene
<1
<1
Dibromochloromethane
<1
<1
Chlorobenzene
<1
<1
Ethyl benzene
<1
<1
Brow oform
(i
<1
1,1,2,2-Tetrachloroethane
<1
<1
1,3-Dichlorobenzene
<1
<1
1,4-Dichloroben zene
<1
<1
1,2-Dichlorobenzene
<1
<1
Tetrachloroethene
<1
<1
Respectfully
submitted:
PAR Laboratories,
Inc.
LJohn
Rice
Labor cart' Director

PAR
PAR Laboratories, Inc.
c r r',r r� 17 GRAHAM RK DRIVE
7
8.. BOX 4114�
HARL,IBC 41r14
�"Iw�`
704ji�ry -B3
August 13, 1993
Reference No:
Made For:
Spectrum Dyed Yarns
P.O. Box 1006
Belmont, NC 28012
Attention:
Sari Sanders
Analyses Of:
Gr undw r Samples
Marked:
Sample #1_ M 1 7%1
Grab
Sample 02 - MW2 7/15/93
Graff
Received
7 "1 /, 7/15/93
Analyses:
Sample
TESTED
R
COD
20 21 7/19
1310
Chlorides
.7 7/19
1300
Sulfates15
26 7
TDS
146 299 7/ 7
1330
TOC
6 3 7 e
1300
Respectfully
submitted:
PAR Laboratories, n .
John S Rice
Laboratory
r r
i
'! Y
AUG, pay ' k�03

MEMO
CARTE: �L4A o ..—
. .F q ,JN a
e
s v r i
r'
v�
From:

w
State of NorthCarolina
Department of'Environment, Health, and Natural Resources
wile Fei-nil i
James G. Martin, Govemor
Wil r r , Jr., Secretary{
Albert F. Hilton, Regional Manager
DIVISION OF ENVIRONMENTAL NA EMEN°1
Cyr. William Burch
Dixie Varna, Inc.
Post Office Box 1006
Belmont, North Caroling 28012
RECompliance Monitoring Report
Piedmont Processing
Gaston County, N
Dear Mr. Burch
On July 20, 1992, the Groundwater Section of the Mooresville
Regional Office received compliances monitoring reports for the
subject site.
The levels of total organic carbon ) and chemical oxygen
demand (COD) of the downstream monitor well are 212mg/l and 645
m/l, respectively. These levels indicate that additional
sampling is necessary. Please sample for 604 and 611, and 6230D
r 502.2 within sixty 60) days of receipt this notice, is
order to identify a specific organic compound.
Should you have and questions, please contact me at (704)
a6-16g .
RM
Sincerely,
"""
Karen nWalker
H drolaologioal Technician
PO &ax 950, 919 North Main Street Mooresolle, NC 29165 50 + Telephone [phone] FAX 73 tt )
,An Frival Opportunity Aff rmathe Action Employer

X. C. DVPTOF NATURAL
DIXIE YARNS.- Inc. Rj,�,,SOL'RCLS AN U
SPINNERS o PROCESSORS * DYERS * KNITTERS O(MMUTNITY PEVELOPNf— T
PIEDMONT PROCESSING DIVISION 0 11 1992
P. BOX 1006 e PTA CV NORI'H CAROLINA 28012
TELEPHONE a [phone] FAX [phone]
pan or vvcz,,-ksw1
RuVIUMAL
August 31, 1992
Ms. Karen Walker
Hydrogeological Technician
State of North Carolina
Dept. of Environment, Health, and Natural Resources
P. 0. Box 950
Mooresville, NC 28115-0950
Dear Ms. Walker:
The enclosed reports are in response to your letter
of August 6, regarding PDES #NCO006521.
Please let us know if you need additional information.
Sincerely,
f"Y'
/XJ
William P. Burch
Superintendent of Maintenance
a h
Enclosures

PPPF-
5EAFt
w 1 .e 0r
"#RFSOURICES iNl)
,QQ
992
trig* of North Carolina U r SV t RU9301 Oft
Dcpartrnent of Environment, Health, and NatUn. I Resources
him", t w,. Ntirtira, (rc5wrrrtir I t F Ffiltoti, RegiesriA Min,
DIVISION OF ENVIRONMENTAL MANAGEMENT
August 6, 1992
r. William Burch
Dixie Yarns, Inc.
Pest Office Box 1006
Belmont, North Carolina 28012
RE: Compliance Monitoringpert
Piedmont Processing
NPDES #NC0006521
Gaston Count
Dear Mr. Burch:
n July 20, 1992, the Groundwater Section of the Mooresville
Regional Office received compliance monitoring reports for the
subject site.
They levels of total organic carbon t t and chemical oxyger,
demand (COD) of the downstream monitor well are 212 mg/1 and 645
m l , respectively.. These levels indicate that additional
sampling is necessary. Please sample for fr o and 611, and 6230D
or 502.2 within sixty (0) days of receipt of this notice, in
order to identify a specific organic compound.
Should you have and questions, 'pleases contact ma at { 704
663-1699.
a
c r 0'pz.:.
Kern Walker
Hydrogeological Technician
V(k I'ao, 9- 1 1114 a`^S,wh Nton 1,mt°t M—ta—,31, N( ?)MiC@ if) 0 11 �cv6o,, 111 tq'0lf,"y'l 'W 1AX mgw"IUM(l
An 1 rr6#.ai AI61163AM11' & win h1 phi y{,,

PAR i , Inc.
22r7GRAHAM PARKDRW
PO BOX 411483
tT SOUR(A' `a'a 0
CHARLOTTE, NC 28241-1 83
r rr rar..Vr:rcrVM
704288
o o 12
y
Reference N o ;
92 3049
$ y
Made a_1 e For: 3 r ,.
:
p )
Dixie Yarns, ,pi 2 4 k e a:.
t
jj'4,. y �{�p
ox
Belmont, NC 28012
Attention:
Buddy Birch
dti
Ana.z y s e s o &... a
�y�„
Water Sample for o r EPA 624
is 2 . 0.... )
Md'a .`E,ed:
Downstream Monitor Well
#11,(Piedmont Processing)
Received On:
8/7/92
i pb
2-_ltccl a, ri o n e
Tetrachloroethane
Dl..cn h.Tor°crdi I' fl a.trrr"omether'rar
Vinyl Chloride
Brarraorr e lrr:rtr
J -Dic;h orynrrthy l c'.rre
Methylene chloride
trans-1 ,2--Turd':hlarer;.4ethr:>ne
1 , I -V l c,h1 crr c; e l.hnn
Chloroform
H r orarcac.°h.l cr r.c.rrr e hrrrarr
Carbon Tetrachloride
Benzene
Trichloroethene
1. , 2-llichlorrrproprrrrr
q;t-ChTar~raaet.hySsvir'yl ether

PAR Laboratories, Inc.
2217 GRAHAM PARK DRWE
qULS,
P,O, BOX 411483
CHARLOTT& NC 28241-1483
7041588-8333
W. C. r
. . .. ,"72
Reference No:
92 3049
Page 2
(ppb)
Tol"ene
<1
trans-1,3-Dichlarapropene
<1
I-Chloro-2-bromopropane
0,
1,1,2-Trichloroethane
<1
1,1,2,2-Tetrachloroethene
<1
Dibromachloromethane
<1
ChLorobenzene
<1
Ethylbenzene
<1
BromafDrfll
<1
1,4-Dichlorubutane
<1
1,1,2,2-Tetracdel oroethane
<1
1,3-Dichlorobenzene
<1
1,4-Dich1orobenzene
<1
1,2-Dichlorobenzene
<1
2-Butanone
0''
Tetrachloroethane
A,
wXylene
<1
p-Xylene
A
wXylene
<1
Respectfully submitted:
PAR Laboratories,
Inc.
lye
Nil
S. Me
A boratory Director

State of North Carolina
Department of Environment, Health, and Natural
M(x)resville Regional Office
James 7, Martin,, Govcrnor Albert F. Hilton, Regional Manager
William W {.:obey, Jr,, Secrt,.tary
DIVISION OF ENVIRONMENTAL MANAGEMENT
August t 6, 199
Tyr. William Burch
Dixie Ferns, Inc.
Post Office Box 1006
Belmont, North Carolina 2801
RE: Compliance Monitoring Report
Piedmont Processing
NPDES #NCO006521
Gaston County, NC
Dear Mr. Burch:
On July 20, 1992, the Groundwater Section of the Mooresville
Regional Office received ompli n monitoring reports for the
subject site.
The levels of total organic carbon OC and chemical oxygen
demand (COD) of the downstream monitor well are 212 mg/l and 645
m 1, respectively. These levels indicate that additional
sampling is necessary.. Please sample for 604 and 611, and, 6230D
or 502.2 within sixty (6 ) days of receipt of this notice, in
order to identify specific organic compound.
Should you have and questions,please contact me at(704)
66-1699
Sincerely,
Karen Walker
Hydrogeological Technician
P,0. Box 940, 99 North Main St et ," loort-m Ile, NC, 280-0950 0 1i.1e bona 7(4-663-I0a & 6,AX 704-66i-(AgO
An Equal t.,?T, ,)rtunityAffirmative Ntion .Eai pk)ver~.

PPPP-
m
pip
State of North Carolina
Department f Natural Resources and Communi"r Development
Nloor s011e Regional nal fficr
James G,Martin, Governor filbert F. Hilton, Regional Manager
William W Cobey, .1r., Ser retary
DIVISION OF ENVIRONMENTAL MANAGEMFNT
Aarll. 1, 19
CERTIFIED lL
RETURN RECEIPT H TED
Mr.William P. Burch
Piedmont processing Company
Belmont, N. C. 28102
p Piedmont processing Company
Wastewater Equalization Basin
Permit No: 1.1 1-000
Gaston County, i > C.
Dear Mr. Burch:
closed are -groundwater quality monitoring report forms. It is required
that all future groundwater sampling results reported for the above referenced
treatment facility be submitted can these forms.
The information .on requested in the upper left corner must also be completed
for each well. The monitoring results must be submitted to the Division of
Environmental Management, er t, roundwat r Section, at the address located at the
top of the form., Additional forms can be obtained throughthe Raleigh Central
Office.
Page No. 2 of Permit No. 21181-0005 requires that the wells be monitored
eery March, JulY and November. The results moat be submitted within thirty
days after the sampling event. (attached)
919 North Main :street, P.O.Box 950,Mooresville, N,,C,, 28115,0950 0 deph(,,, eme 7()4-6i3 16
An Eqnal Opwturrity Affirmatlw Actin Employer ..

PP
Wlll:ia . Bu h
April. 1, 1989
Page Two
If you should have any questions, please contact this office at(704)
-1699 ,
eel,
041"Z'
-Jesse We Wells
Hydrogeological Technician
Approved by)
l ric,,,° . Klingel, Ph.D., C.P.G.
Hydrogeological Regional Supervisor
ee Mr. Bill Reid
M. hex'Gleason
JWW:pb

V
{
<14JA
2 w x
February 21, 1989
FEB 01-S
Regional _Supervisor
State of 'North Carolina,
Department of Natural Resources
& Community Dev.
R. 0. Box 950
Mooresville, NC 28115-0950
Gentlemen:
Test results of well
samples for comparison to base
samples are enclosed.
Sincerely,
k
William R. Burch
a & i
Enclosure
c. Department of Natural Resources
Community Development
Div.. Environmental Management - Groundwater Section
Raleigh, NC 27611
Messrs. Ken Wright and George Shan
Dixie Yarns, Inc.

ppppp
P RL4504TCAls PAR LABORATORIES, INC.
INCO P09*1ED 4400 OLOINEVILLE ROAD
a P.
r wew-
0. BOX 240722 m `q
CHARLOTTE, NC 282240-00 �.-
704/527-7598
FEBRUARY 1 � 1989
.�
ANALYSES LSE OF WELL WATER SAMPLES
REFERENCE NO- 8
MADE FORT 'I EDI-1 NT PROCESSING
DIVISION LSE T I -L: E� INC.
P. 0. BOX loos
ATTENTION:BUDDY BURCH
MARKED. -SAMPLE 1 - MONITOR ITO TEST WELL NUMBER 1 UPSTREAM
SAMPLE #2 - MONITOR TEST WELL NUMBER I DOWNSTREAM
RECEIVED ON 01118189
ANALYSES:
pH VALUE 6.5 6.8
( E EI°al
COD 25 3
TOTAL LEI°SS Lkl"EC SOLID 227 'CI
CHLORIDES .,2.98 10.91
TOTAL SULFATES 14 1
TOTAL_ ORGANIC EEON 1.
ANALY2ED BY:
PAR LABORATORIES, INC.
ryE
S. RICE
AEI rEATE aDIRECTOR

SPINNERS*DIXIE YARNS, Inc.
PROCESSORS* DYERS
EKVIR tNMENTA
FEB 5 lggl January 25, 1990
81 is nn of Environmental Management
ent
Groundwater Section
P. 0. Box 2787
Raleigh, NC 27611
Gentlemen:
Enclosed is our groundwater report on sample taken
11 /9/89. Please send us another supply of "Compliance Moni-
toring Report Forms".
Thank you
Sincerely .ours,
PIEDMONT PROCESSING DIVISION
William P. Burch
ah
Enclosures

DIVISION OF ENVIRONMENTAL MANAGEMENT
October 8, 1987
MEMORANDUM TO: Bill Reid
THROUGH: Eric J. Klingel
FROM: Bill Crawford
SUBJECT: Regional Non -Discharge Permit Review
Piedmont Processing Company (GW 87125)
Wastewater Equalization Basin
Gaston County, N. C.
I have reviewed the above subject application arid the following comments/
recommendations are submitted:
(1) Water levels taken by Subsurface Investigations in two test borings
at the facility are questionable since the measurements were re-
corded one hour or less after termination of boring.
(2) The water levels measured were taken during a period of seasonally
dry weather (August, 1987) and, as Subsurface Investigations indicated,
do not represent the seasonal high water table. They predict a rise
of 3-5 feet could be expected before'a seasonal high water table was
reached. However, the water level observation well of the GWS
at the Daniel Shaver residence (Well.,P64yl.) in Mecklenburg County
has shown yearly flucuations of up to eight feet. While this
observation well is located some distance from the subject facility
(approximately 20 miles) it does raise some questions as to
w.
whether a minimum separation distance of four feet can be mdintainsd
between the liner in the bottom of the basin and the seasonal
high water table at this site.
Should you have questions, please call me.
WHC:pb

pp -
DIVISION OF fwlftvmAL
RECORD E WASTE DISPOSALPERMIT APPLICATION
REVIEW Y.
1 d , 87
FIELD INVESTIGATION y.- DATE:
FACILITY
TOWN COUNTY'. Gaston
LOCATION: di on t Road
TYPE OVDISPOSAL SYSTEM
DESIGNED P CI )•
WASTE PHYSICAL CHARACTERISTIC: Textile
DESCRIPTION OF FACILITY#"
CHEMICAL ANALYSES AND OTHER ys.
DATA AVAILABLE: (CHECK THOSE APPLICABLE AND ATTACHCOPIES):
AMBIENTED TE CITY (WATER TABLE) RAW WASTE ED OTHER
AMBIENTT ITREATED
--prary-
NAME OF NEAREST STREAM:. DISTANCE:
DISTANCE TO NEAREST WELL: DEPTH: U ING RATE -
PROPOSED METHOD FOR PREVENTINGTER CONTAMINATION
STRUCTURE, LITHOLOGY AND PERMEABILITY CE SURFICIAL MATERIALS: .
HYDRAULIC RELATIONSHIP BETWEEN WATER TABLE AND ARTESIANAQUIFERS:
DEPTH TO BEDROCK: � �y � �DEPTH TO SEASONAL A IC AVERTABLE:`
MONITORING FACILITIES NEEDED (ATTACH TECH ,
RECOMMENDEO SAMPLING SCHEDULE AND PARAMETER REQUIRED:
=,'_7 Reiff
REMARKS AND RECOMMENDATIONS
Revised

PAR LABORATORIES, INC.
Illfcc-lRpc"l[tl 4400 OLD PIN ILL ROAD
BOX 240722
CHARLOTTE, NC 28224
704/527-7598
JUNE '---,,0 1 1 9,e8 RECEIVED
r1wYmournAt
At"IALYSES OF (4ELL tIATER SAMPLES
AtIC 10 1988
REFERENCE NO: G'8 12 -16
Quo
MADE FOR: PIEC)MONT PROCESSING
DIVISION OF TI-CAROI I tJ C .
P. 0. BOX 1006
BELI-10t�',!T, 1142 28012
AT TENT I ON - BUDDY SURCH
MARKED: SA-11FLE 4-1 I&IELL #I; U PSTREAll 24 DEEP
A H P L E 4 2 LJ E L L 'T4121- DOI,°JINSTREA11; 1-8 DEEP
RECEIVED Cql-4: 061141se
ANA LY S E S
'SAl"lPLE I
pH VALUE 6- 5 6. 7
COD 46 76
TOTAL DISSOLVED SOLI DES' 311 311
CH'LORI DES 6.45 14. 89
TOTAL `.�'ULFATES <1 < I
TOTAL.. ORG3�,HIC 2 3
ANALYZED BY:
PAR LABORATORIES, INC.
YC E
CJLD PlNtfl()ILLE K01`0 -.>g 1988
CHAR'L OTTE, NIC 28,21-i
GROUNDWATER SECTION
RALEIGH, NC

rr�
P%R\
November 2 1988
Mr. Ronald C. McMillan
Regional Supervisor
State of North Carolina
Department of Natural Resources & CommunityDev.
P. 0. Dux 950
Mooresville, NC 28115-0950
Dear Mr. McMillan
Test results of well samples for comparison to base samples
are enclosed.
Sincerely
William P . Burch
an
Enclosure
Cc Dept, of Natural Resources
Community Development-
Div. Environmental Management - Groundwater ;Section
Raleigh, NC 211

�� I A LABORATORIES,
INC RAT
P. . BOX 240722
CHARLOTTE, N 4
TR 31, 1988
LYSES OF WELL WATER SAMPLES
REFERENCE NO: 88 2067
EAR FOR PIEDMONT PROCESSING
DIVISION TIR# I
P. . Box 1006
ATTENTION: BD E R H
MARKED: SAMPLE 1WELL 1 1 UPSTREAM
SAMPLE WELL 1 DOWNSTREAM
RRRR CAE 10/04/88
ANALYSES:
SAMPLE 1
pH VALUE 6.5 6.7
(PP "
COD
TOTAL DISSOLVED SOLIDS 43 305
CHLORIDES
TOTAL, SULFATES< 1 < 1
TOTAL L ORGANIC RBON
ANALYZED BY:
PAR OR TOR S� I
e
YO HN 'S. SR I C E
LABORATORY DIRECTOR

oil
tbmpuiko�t MONITORING
= T P01W !d
Facility Name PIEDMONT PROCE.SSINC CO DIV Qr D IX I F AAM-S-
Address
BELMONT NC 28012
Well Location UP STREAM
County cz 11 , Iq
Permit Number:
Non -Discharge —,x
NPDES
Well Identification Number E Well Depth _4_5___Ft, Water Use
Ail
Well Diameter Sample (Screened) Interval-! —I Ft. To L4 _5 Ft„ Injection Well
Depth to Water Level ___24_L_ It, below measuring point, (bofore sampling) Well Construe ti on 3 5 0 3 5 2 14M 0 10 8
Measuring point is �_2 feet above land surface 0 t h e r
Gallons of water pumped/bailed before sampling
Field Analysis: PH 6.5 Specific Conductance _uMhos Temp. 0 C Odor —_ Appearance
Date Sample Collected 11-21-90 —_ Date Lab Sample Analyzed _-1-1-22-90
PAR LABS 2217 GRAHAM Pik DR CHARLOTTE NC 28 20
Laboratory Name OTTE �Mijlcaficin No.
COD
mg/l
Coliform: MF Fecal
/100ml
CoWorm: MF Total
/100ml
Dissolved Solids.- Total
mg/I
pH (when analyzed) 6.5
units
TOO
mg/Il
2­§9
Chloride
mg/I
Arsenic
mg/l
Grease and Oils
mQ/I
Hardness" Total,---
mg/t
Phenol
Sulfate
mg/I
Specific Conductance ____._uMhoS
Total Ammonia(NH t NH
3 4)--
mg/I
TKN as N ____
mg/l
NO2 as N
mg/I
NO,,a as N
—mg/l
Phosphorus., Total
as P mg/l
Al Alumnurri
--mg/l
Ba Barium
mg/I
Ca Calcium
rng/I
Cd Cadmium—
mg/I
Chromium: Total
_��C�E_IV�E�rng/l
Cu - Copper
mg/I
Fe - Iron
rraJ
Hg - Mercury
K - Potassium__-,
g
Mg - Magnesium________._mg/I
Mn - Manganese—
Mg/1
No - Sodium
m g / I
I CERTI L Y THAT THIS REPORT lS TRUE AND ACCURATE,
TOX el
iL 0
0 1
St NATURE ERMITTEE (OR AUTHORIZED AGENT*)
GW-59 Revised 6/88
Ni Nhcke I mo/I
Pb a Lead
Zn Zinc mg/I
Pesficides/Herbicides (Specity Compounds)
to
ug
Other (Specify)
U q
Sil " "tk fik ki
gag
ug/l
ug/l
N o I e �
:A101ild rW�R( I Tok'31 C01Weritralion,',

low loom millimillillillil
I'll, _00NOM
Division of Environmental Management
COMPLIANCE MONITORING
Groundwaxter Section
P.O. Ro27687
REPORT FORM
Rallei f4.C. 27611
�
l forms please write or : (91r)
For additionacafl 733-32211
Facility Name PIEDMONT PROCESSING CO DI OF DIXIE YARNS TNC
( ounty GAS`
C
Address 161 PIEDMONT RD PO BOX l00._6__­_______'__
PermTt Numbor:
TMO'NBI,,,r NC28012
plon-Dtscharge____x
Well Location
NPDES
WeH identification Number Well
Water Use
Well Diarneter",_ Sample (Screened) lntervaj_11_Ft, To-2-a—Ft,
Injection Well
Depth to Water Level ft. below measuring point. (before sampling)
Well Construction
Measuring point is feet above land surface
Other
(,'aallons of water pumped/bailed before sampling
Field Analysis. pH _fi - _4 Specific Conductance — uMhos Temp.
0 C Odor _ Appearance
Date Sample CollectAl-22-90 Date Lab Sampte Analyzed
11-22-90
Laboratory NamePAR LAB 221L7,-CRAHAM PK DR CHAORTTE NQ 28241 Certification No.
C 0 1) _U_ mg/1 NO2as N
mg/1 Ni nickel --mg/1
Coliform. MF Fecal 1tTiCml NO3as N —mg/l
Pb Lead
Coliforml- MF Total /100ml Phosphorus-, Total as P
mgil ri Zinc mg/l
Dissolved Solids- Total 194 mg/l Al Aluminum
mg l Pesficides/Herbiitides (Specify Compounds)
pH (when analyzed) _iL_&_ units Ba Barium
mg/t - Ug/l
TOO ___ _J-__ TT)g/l Ca Calcium
Chloride 1 mg/I Cd Cadmiurr)_.__mg/I
Arsenic -_
mg/I
Grease and 00s
mg/l
Hardness; Total
mg/I
Phenol
Sulfate
Mg/1
Specific Conductance
uMhos
Total Ammonia(NH 3 t NH 4)
mg/I
TKN as N
mg/1
TOX a
Chromium: Total --mg/l
Cu Copper MO/I
Fe IronRECEJVECf mg/i
Hg mercury
K - PoTaSSiUMMQ/J
DFC,
Mg - Magnesium T-n g
Mn - Manganese _Mg/l
Na - Sodium mg/1
urt/i
Other 104ty) ___ug/f
"Ug/l
ug/1
ug It
Uq
ug/I
Na to -
Va$ues shot reflocl total concentrations
S" b4O
bW* ao4l g4o coollos to addroiss

0,01, Structurat,
Inc.Frank B. Hicks Associates, Brudge, Roadway,
ay,
Env ronmraemW
Consulting a Su Plannersany gaettar,
4660 Old Pineville Road * Charlotte NC 28217 (704)52'7-1686 Engineers
April 20, 1988
Mr. Tony Parker
N. C. Department of Natural Resources
and Cominunity Development
Division of Land Resource
Land Quality Section
Mooresville Regional Office
P. 0. Box 590,
Mooresville, N. C., 28115
RL Piedmont: Processing
Monitoring Well Location
Dear Mr. Parker
Confirming our conversation of today, we are attaching three () copies of
the proposed monitor well location shorn on the Site Plan and Tpo for this
Piedmont Processing equalization basin.
Please review these and call, me as to their acceptable location or how you
want them moved then when we submit A - ui l is of the end of the project we
will show the final location and pertinent data relative to them,..
Many Thanks
Very truly yours
FRANK B. HICKS ASSOCIATES, ". -I ,
p,.
u ,
e
z
Frank B. Hicr-.... ,
' F Jr/d
Encl.
cc: Mr. muddy Burch / ncl
Trr
Crmrr:�
,
41316 u t
Our 2111 Year

RECEIVED
**VON ofa s p February 1' , 1989
APR 4 1989
Regional SupervisorJay
State of North Carolina
Department of Natural Resources & Community Des.
P. 0. Box 950
Mooresville, 11d 28115-0950
Gentlemen: SEC TION
gg
Test results of well samples for comparison o base
samples are enclosed.
Sincerely,
William ). Burch
A
Enclosure
c: Department of Natural Resources
Community° Development
Div. Environmental Management - Groundwater Section
Raleigh,
'IV 11
Messrs. Ken Wright and George Shan
Dixie Yarns, Inc

PAR LABORATORIES, INC.
CHARLOTTE, NC 28224
704/527-7598
ANALY�EIES OF tdELL
WATER SAMPLES
MADE FOR:
PIM-10t,4T PROCESSING
ATTENTION:
BUDDY BURCH
SAMPLE #2 MONITOR TEST
WELL t',M-IBER
2; DMNSTPEAtl
RECEIVED ON:
PH VALUE
6.5
6.8
TOTAL DISSOLVED SOLIDS
227
204
TOTAL SULFATES
14
14
TOTAL ORGANIC CARBON
1
2

Frank B. Hicks Associates, Inc.
�u Y�
Consulting Engineers • SMOYOfs Plannem ar¢vaanftary
S
M 46W Cold Plnoville I oad ��"r3�� szMisss
had tt* C 6 10 . anda € 3tsry
September 1, 1987 SPRII
Mr.. J. William Reid
Environmental engineer
Division Environmental Management
State of North Carolina Department of °.
Natural Resources & Community Development
P. 0. Box 27687
Raleigh, R. C., 27611-7687 1
987
R Piedmont Processing Company _It SECOTIO i
Wastewater gull i zation Basin
Gaston County
AC0006521/GW87125
Dear Mr. Reid
Responding to your letter to Mr. Buddy Burch of dune 26, 1987 and in the
orders of yourcomments:
I. A general location sketch is shown on the drawing Site Plan Sheet
1..
2. There are no wells ;within 500 ft. of this project in that the
project is in the Town ;of Belmont and the plant and all the
adjacent owned properties of the dill are on City water.
. Chemical analysis of the wastewater over the last year are included;
with this submittal.
4. A hydrogeologic profile/soil study is included from Subsurface
Investigations, Inca
5. The Basis of Design did stipulate a 45 mil hypalon liner; however,
the manufacturer recommended that a 30 mil would be sufficient for
this installation and waste and a 30 mil will be used.
If you need additional information or clarification, please call us.
Many Thanks,
Very truly,your,
FRANK B. HICKS ASSOCIATES ,,w- l
ran :" c s , r. ,
FBH;jr/
Encl.

State of North Carolina
Department of Natural"' urces and Community Development
Division of Environmental Management
512 North Salisbury Street * Raleigh, North Grofina 27611
James G. Martin, Governor R. hul Wilm'
S Thomas Rhodes, Secretary GROUNDWATER SECTION Director
June 26, 1987
Mr. Bobby Burch
Piedmont Processing Company
P.O. Box 1006
Belmont, NC 28012
Dear Mr. Burch:
SUBJECT: Piedmont Processing Co.
Wastewater Equalization Basin
Gaston County
AC,0006521/GW87125
As part of the Division of Environmental Management's
comprehensive approach in addressing the impact of waste
treatment, storage, or disposal projects on the environment,
your permit application has been forwarded to us for assessment
of the potential impact of the project on groundwater quality.
Our initial review indicates that the data submitted is
not sufficient to make this assessment.
Before your application can be processed therefore, you
are requested to submit the following information to the
Groundwater Section. This information should be submitted in
full within 60 days of the date of this letter. Failure to
comply may result in the returning of this application as
incomplete.
1. A general location map, showing orientation of the
facility with reference to at least two (2)
geographic references (numbered roads, named
streams/rivers, etc.
2. A site map which shows the location of any wells
within 500, ft. of the proposed wastewater
equalization basin. The,wells should be labeled
as to their primary usage (drinkinq water, process
water, monitoring etc.)
Pollution Prevention Pays
PO Box 27697, Rate*h, North Carolina 27611-7697 Telephom 919-733-7015
An Equal Opportunity Affinnattvi: Action Emplom

chemical analysis which fully characterizes the
inorganicand organic including synthetic
organic) constituents in the wastewater which will
he discharged to the equalization basin.
. A hydrogeologic profile, via two nail auger
borings, to a depth of 20 feed or partially
weathered bedrock, whichever is less. The borings
should be conducted at the proposed equalization
basin site and define
a. the lit a lcgy of the underlying strata
to a depth of the borings.
b. the estimated Vertical hydraulic
conductivity of the most impermeable
strata encountered.
C, depth of the meat seasonal high water
table (if definable from soil morphology
or from evaluation of Bather applicable
available data
. The Basis of resign, provided with the
application indicates that the interior' of the
basin will use lined with a 45 mil by alen liner.
However the specifications, in Section 53. Rubber
Sheet Pond Lining, stake that the liner shall have
a nn aminal thic kneaa of 3 mil and mil minimu c
thickness Please clarify.
Please feel free to contact the Groundwater Section, at
919 733 3 1 if clarification or information is required.
Sincerely,
Fs
r'
i` William Reid
Vironmen al Engineer
cc. Central Files
Permit Issuance
Eric Ylingel
Gil Vinzani
Frank B. Hicks Associates, Inc..
4560 Old ' Pineville d
Charlotte, NC 28217

Fn �F
DIVISION OF ENVIRONMENTALMANAGEMENT
GROUNDWATER SECTION
June 11, 1987
MEMORANDUM
TO: Eric liVnl
�rv�
FROM:Bill Reid
SUBJECT: Applicatiz for Renewal/Amendment of ExistingPermit
New Permit:
Facility Name` Piedmont Processing
County Gaston
Type> of Project Wastewater Equalization Basin iU-"amp AND
Applicable Permit Numbers : AC001
Gib87125 , 2 25T
We have i ve copy of the above t
whichwas sent to your regional office for ob"�
June 9, 1987.
You a ld review the application package for completeness
and adequacy of relevant information and submit your request
for additional information to me (via telephone or mama) b
June , 1987 so that all required information can be requested
from the applicant at one time. A copy of our formal request to
the applicant for additional information will be provided to you.,
If you do not require additional information from the
applicant to cBa al your evaluation of the project, you should
review the application package and ' submit your comments
July 2, 1987.
If a copy of the ,application packaqe has not been madam
available to your office, PLEASE LET ME KNOW.
Permit Issuance File

SUMMARY REPORT OF GEOTECHNICALO N ATI N
INVESTIGATION AN
ENGINEERING EANo UA T I N
PIEDMONT PROCESSING COMPANY
WASTEWATER EQUALIZATION BASIN
DNvM NT ROAD
LMONT O NORTH CAROLINA
OUR PROJECT NUMBS A
GROUNDWATER SECU33
SUBSURFACE INVESTIGATIONS, INC.
' °CHARLOTTE, N.C. E3 T t '

SUBSURFACE INVESTIGATIONS, INC.
P,O, SOX 241204
CHARLOTTE, No 28224- t 204
August 21, 1987 (704� 334-0819
SEP
Piedmont Processing FRANK & HICKS A40CIATES P. 0. Box 1006
Belmont, North Carolina 23012
SUBJECT: SUMMARY REPORT OF HYDROGEOLOGIC PROFILE
PIEDMONT PROCESSING COMPANY
WASTE WATER EQUALIZATION BASIN
EDGEMONT ROAD
SEA MONT,, NORTH CAROLINA
OUR PROJECT NUMBER 2225A
Cent lmen
:
Subsurface Investigations, Inc. has completed the geologic
profile for the planned Waste Water Equalization Basin. This
report summarizes our Findings.
HERE=
This site is located in the Pied mon,t physiographic province of
North Carolina. Typically, the its have weathered in -place from
parent bedrock. Weathering is not uniform due to joints and
variable mineral composition. Underlying rock types in the
Belmont area have been mapped as predominantly a metamorphosed
quartz diorite.
Two auger borings were drilled at the Basin as shown an the
attached plan.
The following general soil strata are present at the Basin site.
Residual, or weathered in -place, soil appears to be present
at the ground surface. Texturally, this residual soil is a
sandy, silt with mica present at various depths. At the sampled
depths these silts were soft to firm in consistency based on the
Standard Penetration Resistance (A TM D-1586).
These sandy, silt residual soils have estimated permeabilities in
the range of I x 10-" to I x 10--,4 cm/s.
No partially weathered rock or auger refusal strata was en-
countered within the depths sampled.
GEOTECHNICAL ENGINEERS
CONSTRUCTN. QUALITY CONTROL
- ------------- -

Ground water was encountered at the time of boring at 25.5 and 20
feet below present grade at Barings 2-1 and 8-2, respectively.
Measurements at 48 hours resulted in a caved depth of 25 and 19
feet at Borings B-1 and 8-2, respectively. These measurements
were taken during a period of seasonally dry weather and may
rise 3 to 5 feet with the return of normal seasonal moisture
conditions or in the high water table periods of late winter and
earl'spring.
These 48 hour measurements with a 105 feet spacing between
borings result in a gradient of about 0.95%. This indicates that
the ground water flows along a higher to a lower ground surface
elevation on a flat slope.
The basin bottom at 11 + feet below present grade will be above
the ground water level at the time of this investigation.
If you have any questions on this summary report or if you need
additional information, please contact us.
Sincerely,
SUBSURFACE INVESTIGATIONS, INC.
Richard Greene
Geotechnical Engineer
William G. Smith
President

'TABLE
,SUMMARY OF AUGER BORING DAT
PIEDMONT PROCESSING COMP N
WASTEWATER EQULI TI N BASIN
EDGEMONT ROAD
C M NT, NORTH CAROLINA
OUR PROJECT NUMBER
TEST BORING GROUNDSURFACE GROUND` WATER ROUN WATER'
NUMBER ELEVATION DEPTH(l) GRADIENT
-1 119 25.0' «,
8-2 113 19.0 0.95
t' 1 Caved dry at 48 hours after- time of boring.
t

140ME CLATU t AND SYMSOLS
UVOISTUAlto sA^Mit CU41 *ECOVEAt'o,
unONSTUAILEI SAAPLI (UO) 40t AECOTEAE4
STANDA4 tntTAA?1OM RESISTANCE (Astm 4158647
PEnEIrAT10n AESISTAMtT O TAent4 1SIM0 T*j *CUjCMTA# #tAt Lt
P MtTMOo(T(* , IAIV. VANE 1S APPRCNtAATELT T E Sint AS TMt STAMOAA
PEMETAATGO* AESISTAMEE
t0411" *U'&EA OF Et 1100E TO 04NWE Tait SfOCo A Mkoll4 4F I CMESttE-
AMw®M,Ma Cw4( *AAA'EL llzfs wwatw 041`44Mcosts I-Ii®,N-S!6 aft4 t-Nfs aMC ES
I" OaA-ETEMC, RtSPECTlVti'P..
& PEMttM*A,t Of ROT* toot *ECGiEMO
*00 A tM gUALITT OES O TI-js— Or COME SE ;*E,aT 4 If Moot €Mt"(S tomC
w..;,rtt TABLE AT LEAST it ko,.AS AFrte 0eakLIN
"- oATEe TA Lt 04E 040 4A LESa -"TtM OMaa,L'*G
4035 OF Dalkt,gl4c OATEN
A: AT"CAREAO 1.¢w17 TEST M *r0A*t
C CC%SOkwQ*TaOM TtST PE034m( 4
GS 014$4 SITE TEST PEANOM.S
TMaA114L "EAR TEST P(Xr3*-Ep:
P' Ns:MOtT A COmOAM040 TEST PtA€om,EO
TaELO V44E S*tAA TEST PEANOAME
Ar�aA a3t At COMT(kr tAtACtATt
AS 104040it SMtAA TEST 0(004^1
so SETTLE1At T otilti TEST otaralktic:
Unified it ClA e#tL atiotoy ri&u*l inspection)
PENEr4ArjoN RESISTANCE NtSuS,T
APPAOUMATt
hO, F OLIVE.* N kAT1Tt O(NSNTY
VENT 41543E
N4 k043t
AR S 11 -20 F 1 NM1
I 50 OEmSt
tN SO VENT OtkA(
C SISTt*CT
4 # WENT sort
- 34FT
S - f1NN4
SITS RAO CLAYS 1I . N STNFF
E6 30 PERT St►F
It • 'S4 4^44
OVER S4WENT AAAO
N9L4Iri P010 EOLIAES
%Ott SAPPLINC AMO' JTAMOAXO PINCTRATtOk TESTING PERFORMED 10 ACCORDANCE
VITA ASTM 0 i5tli- T, lot STAMdANO PEMETRAT! AESaSrAMCt I TFt muktitit OF
11LOWS 4F A 144 P taMO n tN FALLING JO I*CMES TO DRIVE A 2 1*CM 0,11., 1A
I MI L,11. SPLIT S TtER I t TOOT. CORE O ILLEMG N ACC00AACE Witit
ASTR #ES14 T14 1N -s T. to( 1 gST *AEO SAMPLIM4 POOCE001' It OtSCU41
ST AS ,A$'CCIFNCATt 0 15$ -i :

REMARKS: GROUNDWATER AT 1/2 HOUR 25.5*
BORING No. B-1
CAVED DRY AT 25' AT 48 HOURS
BORING TERMINATED 8-20-87
PROJECT 2225
PENETRATION RESISTANCE
OIL OESCRWTIOX,
19L OV4 PER T)
100
RED BROWN FINE TO MEDIUM SANDY SILT
8.0
)
UIRM RED TAN G TO I SANDY
10.ERED
SILT
TAN GRAY FINE TO-11EDIUM SANDY
i
18.0
SILT
SOFT BROWN TAN GRAY FINE TO MEDIUM
SIAGHTLY
BROWN TAN FINE TO MEDIUM SANDY SILK
,
BORING IN TE
41"EST BORING
RECORD
SUBSURFACE INVESTIGATIONS, INC. SHEET OF

REMARKS, GROUNDWA'
CAVED
PROJECT
T ' AT 48 HOURS
BORINGTERMINATED
i
PENETRATION RESISTA14CE
19LOM PER T)
10 20 40 so so 100

ran
r t 1 rEPAR LABORATORIES, INC.
INCORPORATED 4400 OLDPI EVILLE ROAD'
Po O. BOX 240722
7 4/ 7.7 '
LILY 21 1987
ANALYSES OF WASTEWATER'
PP 1130
MADE FOR PIEDMONT PROCESSING
DIVISION TI-CARDJ It-4c.
P. 0. BOX 1006
ELMONT, ML. 4- 01 2
ATTENTION: BUDDY BIRO
RECEIVED : 016/17/87 GROUNDWATER EC
A�:1; � !
i
ANALYSES:
pH VALUE
5PpmA
O 13
T
C" L1 .34
TOTAL L NITROGEN 6.
TOTAL L PHOSPHORUS {' 3.31
OIL & GREASE 9t
Ag <.02
Cd <.008
T-C .0
u . 1
Hg <Y2100
Ni <.0
Pb <.f1 x
ci'.072
n <.
ANAL"
PAID LABORAT P ES; INC.
Cya
JIHN S. RICE
LABORATORY DIRECTOR
: DTI

-........ ..
PAR LABORATORIES, INC.
INCORPORATED 44 0OLD PINEVILLE ROAD`
.r
P. 0. BOX 24 722
CHARLOTTE, NC 2 224 °
704/527-759
AUGUST 26, 1987
ANALYSES OF WASTEWATER
REFERENCE 87 1503
MADE FOR: PIEDMONT PROCESSING
DIVISION OF TI-CAFO, INC.
P. 0. BOX100
ATTENTION: BUDDY I FC
RECEIVED ON: QC "1 /8
ANALYSES. -
pH
VALUE t0.2
'' p
OD—C 1 -3
TS``"
NH/3 as Itl 14.00
TOTAL NITROGEN
T N 9.70
NITRATES .24
TOTAL PHOSPHORUS 218-60
ANALYZE Y
PAR LABORATORIES, INC.
I ¢7
LABORATORY DIRECTOR
: JIM JOHNSC411

PAR LABORATORIES, INC.
OLD PINEVILL PAS
P. 0. BOX 240722
CHARLOTTE, NC 28224
704/527-7598
JULY 31, 1987
ANALYSES 6F WASTEWATER
REFERENCE C 7 1306
MADE FOR: PIEDMONT PROCESSING
DIVISION OF TI—CHARO, 11-1C.
P. 0. 'COX 1006
0
SFLi`°1Ot,IT , t IC " 8Cl 1
ATTENTION: BUDDY BIRCH
RECEIVED ON: 7/1 /
ANALYSES -
pH
VALUE 10.
p pt-1:
1 °°=
TSS 1
TOTAL NITROGEN
TKN 10 e a
tJ,TFT 3
TOTAL PHOSPHORUS 1.30
NL'Y`FD'
FAR LABORATORIES, INC.
.
'OHN S . RICE'
LABORATORY DIRECTOR
C TY',CF FFLMON
ELMONT NC 2801
ATTN.- JIM JC1tNSON
�k

IT 1111,11
PAR LABORATORIES, INC.
PAR
1NC8 1tT .s 4400 OLD PINEVILLE ROAD
E". . BOX 240722_.*
CHARLOTTE, NO 28224
704/527-,7598
MAY 'I', 1987
I
ANALYSES F WASTEWATER
REFERENCE .
MADE FOR.- PIa DM h T PROCESSING
DIVISION OF T —CARD, INC.
P. . BOX 1006
LMtT, NO 28012
ATTENTION.- BUDDY BIRCH
MARKED. . .# 17169
RECEIVED . 05/13/87
AiAL`"C1
P VALUE1 .
(FFM
BOD-5 137
TSB 1
NH M 3.92
TOTAL NITROGEN 9.07
TOTAL PHOSPHORUS 9.80
ANALYZED BY:
PAR LABORATORIES, , INC.
.; RICE''r
LABORATORY, -DIRECTOR
c. ,.., CIT `, F BELMONT
R . 0., BOX 431
LM;T, fO, 1
ATTN. AIM JOHNSON

t
P I L 27, 198
ANALYSES E WA TE'VJ
TE
REFERENCE NO.
87 697
MADE ECG
PIEDMONT R EES IN
DIVISION E TI—CARO, INC.
P. 0. BOX 1006e
ATTENTION:BUDDY
BIRCH
'i
RECEIVED ON:04/15/87
i
ANALYSES. -
pH VALUE 10.
p pm
BOD-5 133
2..
TSS
NFL .76
TOTAL NITROGEN 7.28
t
TOTAL PHOSPHORUS 15.50
s
ANALYZED E
EAR LABORATORIES,
INC.
L
t
J1 S. RICE
LABORATORY DIRECTOR
c c JIM JOHNSM,l
WGRATORIE& PAR LABORATORIES, INC.
P. 0. BOX 240722
CHARLOTTE. NC 28224
704/527-7598

d
LA60 ATORIE , P LABORATORIES, INC.
1C5�#T� L�'tC4`E�.I. Rya'
P. CHARLOTTE,M BOX 240722
'N 2522
7 4/527-75 5
P IL 1987
ANALYSES OF WASTEWATER
REFERENCE NO: 1
MADE FOR: PIEDMONT PROCESSING
DIVISION T I - C: :$ INC.
C.
P. 0. BOX1006
LMO T , NC 28012
ATTENTION: BUDDY BIRCH
hit . . ## 17169
RECEIVED ON: 03/18/87
ANALYSES:
< ''m'
BOD-5 103
T
S 12
NH/3 as N 1.68
TOTAL NITROGEN 6.38
TOTAL PHOSPHORUS
ANALYZED BY:
PAR LABORATORIES, INC.
3 4_'(L_
S. RICE
L BC�T DIRECTOR
CITY t= BELMONT
P. 0. BOX 421
r TTt°h1: J S M JOHNSON

PRRL48 RATORIE . PAR LABORATORIES, INC,
INCORPORATED 4400 OLD PINEVILLE ROAD
P. O. BOX 240722
CHARLOTTE, NC 2822
704/527-7598
MARCH +, 1987
ANALYSES OF WASTEWATER
REFERENCE NO: 87 354
MADE FOR: PIEDMONT PROCESSING
DIVISION P T I --CAROB INC.
P. 0. E30X 1
BELMONT, NC 28012
ATTENTION: BUDDY BIRCH
MARKED: P.'.# 17169
RECEIVED O02/19/87
ANALYSES. -
pH VALUE '.`
4 PP1
BOD-5
TSS 1
NH/3 as -lei 1.01
TOTAL NITROGEN ,, 1
TOTAL PHOSPHORUS
ANALYZED BY:
PAR LABORATORIES, INC.
C J HIS S. RICE
LABORATORY I RR TOR
CITE" OF PRL O T
P . 0. BOX 431
BELMONT, NO 28012
t TTN: JIM JOHNSON

n
LABORATORIES. PAR LABORATORIES, INC.
4400 OLD PINEVILLE ROAD
INCORPORATED
..
P. O< BOX 240722
CHARLOTTE, NC 28224
7 4/5 7-7598
FEBRUARY 2, 198
ANALYSES OF WASTEWATER
REFERENCE 180
MADE FOR: PIEDMONT PROCESSING
DIVISION OF TI—CINC.
I '.; . Box 1006
ATTENTION: BUDDY BIRCH
RECEIVED ON:01/14/87
ANALYSES:
H VALUE 1 .
P`
BOD-5 118
TSS 1
NH N .67
TOTAL NITROGEN l?.97
TOTAL PHOSPHORUS
ANALYZED
PAR LABORATORIES., INC.
I HN S. RICE
LABORATORY DIRECTOR
c J 1M JOHNSO