WQ0028547_Residual Annual Report 2020_20210209

Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?* r Annual Report
r Residual Annual Report
r Additional Information
r Other
Annual Report Year* 2020
Permit Number (IR)* WQ0028547
Applicant/Permittee Town of Yanceyville
Email Notifications
Does this need review by the hydrogeologist?* 0 Yes r No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Rease provide inforration on the person to be contacted by N B Staff
Name * Brent Collins
Email Address*
[e-mail]
electronic subnittal, confirmation of receipt, and other correspondence.
Project Information
........ ......... .......................................................................................................................
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
3363993646
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* W00028547
Fbs Current Existing permt number
Applicant/Permittee Address* PO Box727, Yanceyville, NC 27379
Facility Name * Town of Yanceyville RLAP
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Specifications, Calculations, Bc.)
2020 Yanceyville Annual Report - WQ0028547.pdf 5.04MB
Upload only 1 FLFdocurrent (less than 250 `VB). NLRiple documents rust be contained into one FDFfile unless file is larger than
upload limit.
* V By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
ff &kgw
Submission Date 2/9/2021

February 9, 2021
DENR/Water Quality Section
Non -Discharge Compliance Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2020 Annual Report — Town of Yanceyville
Treatment and Land Application of Residuals
Permit No. WQ0028547
Dear Sir or Madam:
Enclosed is one copy of the 2020 Annual Report for the above referenced land
application permit.
During 2020 EMA Resources, Inc. land applied 80.49 dry tons of wastewater residuals to
48.9 acres of private farmland. Please contact Brent Collins - Director of Technical
Services if you have any further questions regarding this report.
Sincerely,
Z�fz G;2�
Brent Collins
Director of Technical Services
brent.collins(cr,,emaresourcesinc.com
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0028547 County:
Facility Name (as shown on permit):
Land Application Operator.
Caswell County Year:
Town of Yanceyville
EMA Resources Inc.
2020
Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar fear?
21 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
A- Residuals Application Su
Total number of anulication fields in the Dennit:1 17
Total number of fields utilized for land application during the year: 2
Total amount of dry tons applied during the year for all application sites: 80.49
Total number of acres utilizes for land application during the year:1 48.9
Part B - Annual Comniance Statement
Facility was compliant during calendar year 2020 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. U Yes ❑ No
If no please, provide a written description nhy the facility was not compliant, the (lates, and explain corrective action
taken.
1) Only residuals approved fir this permit were applied to the permitted sites.
2) Soil pH was adjusted as Specified in the permit and lime was applied (if needed) to achieve a soil pl I of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies ofcertified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T . I I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and renaediations.
1 1) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoffof residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"1 certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility
of lines and imprisonment for knowing violations."
Brian Collie - Tot, <uiager
Permittee Name and Titl pe or print)
'11611"
Signature of Permittee Date
1r21;2021
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T 1102 (26) DENR FORM ACF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
Facility Name:
Residual Source WQ # or
NPDES #:
WWTP Name:
Residual Anaivsis Data
WQ0028547
Town of Yanceyville
NCO040011
Yanceyville WWTP
Laboratory:
1)
2)
3)
4)
5)
Waypoint Analytical
Parameter
(mg/kg)
Conc.
Limit
(mg/ )a
Sample or Composite Date
1/6/20
Percent Solids (%)
NA
3.18
Arsenic
75
14
Cadmium
85
1.65
Copper
4,300
15.1
Chromium
NA
6.33
Lead
840
4.97
Mercury
57
1.8
Molybdenum
75
4.33
Nickel
420
5.5
Selenium
100
16.3
Zinc
7,500
123
Total Phosphorus
NA
1 150
TKN
NA
44000
Ammonia -Nitrogen
NA
6870
Nitrate and Nitrite
NA
166
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false infor :ss including the possibility of fines and imprisonment for knowing violations."
0,� I
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
Facility Name:
Residual Source
NPDES # or WQ#:
WWTP Name:
Residual Analvsis Data
WQ0028547
Town of Yanceyville
NCO040011
Yanceyville WWTP
Laboratory:
1)
2)
3)
4)
5)
Waypoint Analytical
Parameter
(mg/kg)
Sample or Composite
Date
1/6/20
Aluminum
830
Calcium
1440
Magnesium
328
pH
6.7
Potassium
3280
Sodium
1460
PAN
14740
SAR
1.61
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
signet penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
_el/oJ
Date
DENR FORM RSSF - B (1212006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
Facility Name:
Residual Source WQ # or
NPDES #:
WWTP Name:
Residual Analysis Data
WQ0028547
Town of Yanceyville
02-17-010
Yanceyville WTP
Laboratory:
1)
2)
3)
4)
5)
Waypoint Analytical
Parameter
(mg/kg)
Conc.
Limit
(mg/kg)"
Sample or Composite Date
1/6/20
Percent Solids (%)
NA
3.76
Arsenic
75
15
Cadmium
85
1.77
Copper
4,300
186
Chromium
NA
6.79
Lead
840
8.29
Mercury
57
0.18
Molybdenum
75
4.64
Nickel
420
5.89
Selenium
100
17.5
Zinc
7,500
87.9
Total Phosphorus
NA
190
TKN
NA
9460
Ammonia -Nitrogen
NA
3960
Nitrate and Nitrite
NA
177
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties r submitting false information, including the possibility of fines and imprisonment for knowing violations."
�/0 I /0
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26)
Date
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
WQ0028547
Facility Name:
Town of Yanceyville
Residual Source
NCO040011
NPDES # or WQ#:
WWTP Name:
Yanceyville WTP
Residual Analvsis Data
Laboratory:
1)
2)
3)
4)
5)
Waypoint Analytical
Parameter
Sampleor • •• Date
------------
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
�/0/A,
Date
DENR FORM RSSF - B (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Yanceyville Total Dry Tons Applied (Annual): 92.26
Permit #: WQ0028547 Cation Exchange Capacity (non 503 only):
Operator: Glen Hodges Owner: Jennifer Hodges Predominant Soil Series: FbB2
Acres Used: 38 Acres Permitted: 38 Site #: CS09 Field #: 11
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonismMENEEMENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1 1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
1.72
0.71
Arsenic
0.051
0.016
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.067
Cadmium
0.006
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Copper
0.638
0.249
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.888
Chromiuni
0.023
0.078
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.101
Lead
0.028
0.092
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.121
Mercury
0.001
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
0.016
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
denum
Nickel
0.020
0.023
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.043
Selenium
0.060
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.078
Zinc
0.302
1.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.321
Total
Phos-
0.652
6.152
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
6.804
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 1/21/2021
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Town of Yanceyville
Jennifer Hodges
Operator: Glen Hodges
Crop 1 Name:
Fescue -Pasture
WQ Permit #: WQ0028547 Field #:
Annual Dry Tons Applied: 92.26 Site #:
Predominant Soil Series: Fb132
Crop 1 Max. PAN:
141
Crop 2 Name:
11 Acres Utilized: 38
CS09 Acres Permitted: 38
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
F '5
w
*
o
o'
7�
* N
* w
o
TKN
mg/kg
o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
5/4
110500
3.76
0.456
Yancey WTP
D
<.5"
S
0.5
0.3
9460
3960
177
3.471
NA
Fescue
5/5
78000
3.76
0.322
Yancey WTP
D
<.5"
S
0.5
0.3
9460
3960
177
2.450
NA
Fescue
5/7
156000
3.76
0.644
Yancey WTP
D
<.5"
S
0.5
0.3
9460
3960
177
4.901
NA
Fescue
5/8
71500
3.76
0.295
Yancey WTP
D
<.5"
S
0.5
0.3
9460
3960
177
2.246
NA
Fescue
0.000
1
1
0.000
0.000
4/10
169000
3.84
0.712
Unifi, Inc.
Dry
<.5"
S
0.5
0.3
18700
8470
132
10.591
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
o
SsS000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
23.660
0.000
Lime Applied
Annuallbs/acre
0.067
0.008
0.888
0.101
0.121
0.002
0.021
0.043
0.078
1.321 6.804
0
1.321
1 2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.067
0.008
0.888
0.101
0.121
0.002
0.021
0.043
0.078
Permitted C. P. L. R. * * * *
1 36
34
1 1338
267
1 15
374
1 89
Permit PAN Limit 1 st/2nd Crop
1
141
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/21/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Yanceyville Total Dry Tons Applied (Annual): 15.28
Permit #: WQ0028547 Cation Exchange Capacity (non 503 only):
Operator: Jon Crispin Owner: Bonnie Crispin Predominant Soil Series: FbB2
Acres Used: 10.9 Acres Permitted: 10.9 Site #: CS82 Field #: 4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonisMENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1 1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
1.40
Arsenic
0.042
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.042
Cadmium
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Copper
0.522
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.522
Chromiuni
0.019
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.019
Lead
0.023
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.023
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
denum
Nickel
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Selenium
0.049
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.049
Zinc
0.246
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.246
Total
Phos-
0.533
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.533
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 1/21/2021
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Town of Yanceyville
Bonnie Crispin
Operator: Jon Crispin
WQ Permit #: WQ0028547 Field #:
Annual Dry Tons Applied: 15.28 Site #:
Predominant Soil Series: FbB2
Crop 1 Name: Fescue -Hay Crop 1 Max. PAN:
188
Crop 2 Name:
Acres Utilized: 10.9
CS82 Acres Permitted: 10.9
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.y
Past 24
Hrs.
inches
'5L
0 w
*
o
* w
o
rt
*
o
TKN
mg/kg
>
o E�
vc o
E�.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
5111
97500
3.76
1.402
Yancey WTP
D
<.5"
S
0.5
0.3
9460
3960
177
10.679
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALs:
0
9�Soo
As
Cd
Cu
Cr
Pb
H
Mo
Ni
Se
Zn P
10.679
0.00o
Lime A lied
Annuallbs/acre
0.042
0.005
0.522
0.019
0.023
0.001
0.013
0.017
0.049
0.246 0.533 1
4.955
5.201
2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.049
0.009
2.552
1 0.276
0.441
1 0.001
0.038
0.2
0.06
Current Cumulative lbs/ac
0.091
0.014
3.074
0.295
0.464
0.002
0.051
0.217
0.109
Permitted C. P. L. R.****
36
34
1338
1 267
15
1
374
1 89
Permit PAN Limit 1 st/2nd Crop
1
1 188
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/21/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Waypointo
ANALYTICAL
1 /17/2020
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 20-008-0107
Client Project Description: Yanceyville WWTP
2790 Whitten Road, Memphis, TIN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 1/8/2020 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015
Mississippi California #2904
Kentucky #90047 Tennessee #TN02027
VA NELAP #460181
NC #415
EPA #TN00012
Texas #T104704180 Arkansas #88-0650
Oklahoma #9311 SC #84002
Kentucky UST #80215 PA DEP #68-03195
Page 1 of 7

Waypoint
ANALYTICAL
Report Number: 20-008-0107
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Client Project Description: Yanceyville WWTP
Lab No Client Sample ID
92062 Yanceyville WWTP
Matrix Date Collected Date Received
Solids 01/06/2020 09:00 01/08/2020
Page 2 of 7

Waypoint
ANALYTICAL
Client: EMA Resources Inc
Project: Yanceyville WWTP
Lab Report Number: 20-008-0107
Date: 1/17/2020
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Analyte: Aluminum
QC Batch No: L473047
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L473047
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 3 of 7

i
Wa2790 Whitten Road, Memphis, TN 38133
ypoint.Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Mr. Brent Collins Project Yanceyville WWTP Report Date : 01/17/2020
755 Yadkinville Rd Information : Received : 01/08/2020
Mocksville , NC 27028
Report Number : 20-008-0107 REPORT OFANALYSIS Danyale Love
Project Manager
Lab No : 92062
Matrix: Solids
Sample ID : Yanceyville WWTP
Sampled:
1/6/2020
9:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
97.0
%
1
01/10/2012:08
JDT
SW-DRYWT
Ammonia Nitrogen
6870
mg/Kg -
dry
833
1
01/17/20 14:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<166
mg/Kg -
dry
166
166
1
01/16/20 14:26
ZBD
4500NO3F-2011
Organic N
37130
mg/Kg -
dry
81.33
4067
1
01/14/20 15:40
CALCULATION
pH
6.7
S.U.
1
01/15/20 06:46
JSL
9045D
Total Solids
3.18
%
0.010
0.010
1
01/12/20 13:47
ADM
2540G-2011
Total Volatile Solids
47.6
%
0.010
0.010
1
01/12/20 13:47
ADM
2540G-2011
Total Kjeldahl Nitrogen
44000
mg/Kg -
dry
4070
1
01/14/20 15:40
CLP 4500NORGD-2011
Phosphorus
1150
mg/Kg -
dry
85.7
167
1
01/11/20 07:16
KKM
6010D
Aluminum
830
mg/Kg -
dry
67.7
167
1
01/11/20 07:16
KKM
6010D
Arsenic
<14.0
mg/Kg -
dry
14.0
16.7
1
01/11/20 07:16
KKM
6010D
Cadmium
<1.65
mg/Kg -
dry
1.65
3.33
1
01/11/20 07:16
KKM
6010D
Calcium
1440
mg/Kg -
dry
560
833
1
01/11/20 07:16
KKM
6010D
Chromium
<6.33
mg/Kg -
dry
6.33
8.33
1
01/11/20 07:16
KKM
6010D
Copper
15.1
mg/Kg -
dry
4.83
8.33
1
01/13/20 16:51
BKN
6010D
Iron
500
mg/Kg -
dry
141
167
1
01/11/20 07:16
KKM
6010D
Lead
<4.97
mg/Kg -
dry
4.97
10.0
1
01/11/20 07:16
KKM
6010D
Magnesium
328
mg/Kg -
dry
74.0
167
1
01/11/20 07:16
KKM
6010D
Manganese
20.1
mg/Kg -
dry
6.10
16.7
1
01/11/20 07:16
KKM
6010D
Mercury
1.80
mg/Kg -
dry
0.110
0.497
1
01/14/20 15:14
TJS
7471A
Molybdenum
<4.33
mg/Kg -
dry
4.33
8.33
1
01/11/20 07:16
KKM
6010D
Nickel
<5.50
mg/Kg -
dry
5.50
8.33
1
01/11/20 07:16
KKM
6010D
Potassium
3280
mg/Kg -
dry
99.3
167
1
01/14/20 19:13
BKN
6010D
Qualifiers/ DF Dilution Factor
L
Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 4 of 7

i
Waypoint.
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 20-008-0107
Lab No : 92062
Sample ID : Yanceyville WWTP
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Yanceyville WWTP
Information :
REPORT OFANALYSIS
Report Date : 01/17/2020
Received : 01/08/2020
Danyale Love
Project Manager
Matrix: Solids
Sampled: 1/6/2020 9:00
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
<16.3
mg/Kg - dry
16.3
16.7
1
01/11/20 07:16
KKM
6010D
Sodium
1460
mg/Kg - dry
257
833
1
01/11/20 07:16
KKM
6010D
Zinc
123
mg/Kg - dry
36.0
41.7
1
01/11/20 07:16
KKM
6010D
Sulfur
387
mg/Kg - dry
163
167
1
01/11/20 07:16
KKM
6010D
Sodium Absorption Ratio
<2.22
Ratio
2.22
5.00
1
01/11/20 07:16
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
L Limit Exceeded
Page 5 of 7

•
WayPAoi nt ..(2) 2790 Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 9fl1.213.2400 °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 20-008-0107
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
#56
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: rRory Phillips Date & Time: 01/08/2020 12:45:40
Page 6 of 7

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Page 7 of 7

Waypointo
ANALYTICAL
1 /17/2020
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 20-008-0189
Client Project Description: Yanceyville WTP
2790 Whitten Road, Memphis, TIN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 1/8/2020 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015
Mississippi California #2904
Kentucky #90047 Tennessee #TN02027
VA NELAP #460181
NC #415
EPA #TN00012
Texas #T104704180 Arkansas #88-0650
Oklahoma #9311 SC #84002
Kentucky UST #80215 PA DEP #68-03195
Page 1 of 7

Waypoint
ANALYTICAL
Report Number: 20-008-0189
Client Project Description: Yanceyville WTP
Lab No Client Sample ID
92253 Yanceyville WTP
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Matrix Date Collected Date Received
Solids 01/06/2020 08:30 01/08/2020
Page 2 of 7

Waypoint
ANALYTICAL
Client: EMA Resources Inc
Project: Yanceyville WTP
Lab Report Number: 20-008-0189
Date: 1/17/2020
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 92253 (Yanceyville WTP)
Analyte: Aluminum
QC Batch No: L473047/L472108
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L473047/L472641
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 3 of 7

i
Wa2790 Whitten Road, Memphis, TN 38133
ypoint.Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Mr. Brent Collins Project Yanceyville WTP Report Date : 01/17/2020
755 Yadkinville Road Information : Received : 01/08/2020
Mocksville , NC 27028
Report Number : 20-008-0189 REPORT OFANALYSIS Danyale Love
Project Manager
Lab No : 92253
Matrix: Solids
Sample ID : Yanceyville WTP
Sampled:
1/6/2020
8:30
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
97.2
%
1
01/13/20 09:20
JDT
SW-DRYWT
Ammonia Nitrogen
3960
mg/Kg -
dry
893
1
01/17/20 14:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<177
mg/Kg -
dry
177
177
1
01/16/20 14:27
ZBD
4500NO3F-2011
Organic N
5500
mg/Kg -
dry
62.50
3121
1
01/14/20 15:58
CALCULATION
pH
6.5
S.U.
1
01/15/20 06:46
JSL
9045D
Total Solids
3.76
%
0.010
0.010
1
01/10/20 12:12
VBW
2540G-2011
Total Kjeldahl Nitrogen
9460
mg/Kg -
dry
3120
1
01/14/20 15:58
CLP 4500NORGD-2011
Phosphorus
190
mg/Kg -
dry
91.8
179
1
01/11/20 07:22
KKM
6010D
Aluminum
20900
mg/Kg -
dry
72.5
179
1
01/11/20 07:22
KKM
6010D
Arsenic
<15.0
mg/Kg -
dry
15.0
17.9
1
01/11/20 07:22
KKM
6010D
Cadmium
<1.77
mg/Kg -
dry
1.77
3.57
1
01/11/20 07:22
KKM
6010D
Calcium
7713
mg/Kg -
dry
600
893
1
01/11/20 07:22
KKM
6010D
Chromium
<6.79
mg/Kg -
dry
6.79
8.93
1
01/11/20 07:22
KKM
6010D
Copper
186
mg/Kg -
dry
5.18
8.93
1
01/13/20 17:01
BKN
6010D
Iron
5040
mg/Kg -
dry
151
179
1
01/11/20 07:22
KKM
6010D
Lead
8.293
mg/Kg -
dry
5.32
10.7
1
01/11/20 07:22
KKM
6010D
Magnesium
396
mg/Kg -
dry
79.3
179
1
01/11/20 07:22
KKM
6010D
Manganese
339
mg/Kg -
dry
6.54
17.9
1
01/11/20 07:22
KKM
6010D
Mercury
0.1803
mg/Kg -
dry
0.117
0.529
1
01/14/20 15:15
TJS
7471A
Molybdenum
<4.64
mg/Kg -
dry
4.64
8.93
1
01/11/20 07:22
KKM
6010D
Nickel
<5.89
mg/Kg -
dry
5.89
8.93
1
01/11/20 07:22
KKM
6010D
Potassium
1480
mg/Kg -
dry
106
179
1
01/14/20 19:28
BKN
6010D
Selenium
<17.5
mg/Kg -
dry
17.5
17.9
1
01/11/20 07:22
KKM
6010D
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions L Limit Exceeded
MQL
Method Quantitation Limit
Page 4 of 7

i
Waypoint.
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Road
Mocksville , NC 27028
Report Number : 20-008-0189
Lab No : 92253
Sample ID : Yanceyville WTP
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Yanceyville WTP
Information :
REPORT OFANALYSIS
Report Date : 01/17/2020
Received : 01/08/2020
Danyale Love
Project Manager
Matrix: Solids
Sampled: 1/6/2020 8:30
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Sodium
6143
mg/Kg - dry
276
893
1
01/11/20 07:22
KKM
6010D
Zinc
87.9
mg/Kg - dry
38.6
44.6
1
01/11/20 07:22
KKM
6010D
Sulfur
864
mg/Kg - dry
175
179
1
01/11/20 07:22
KKM
6010D
Sodium Absorption Ratio
<2.22
Ratio
2.22
5.00
1
01/11/20 07:22
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
J Estimated value
MQL Method Quantitation Limit
Page 5 of 7

•
WayPAoi nt ..(2) 2790 Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 9fl1.213.2400 °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 20-008-0189
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
#56
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: rRory Phillips Date & Time: 01/08/2020 16:05:23
Page 6 of 7

Client Name/Address
Client Project Manager/Contact
Billing Information
For Laboratory Use Only
EMA Resources Inc
Brent Collins
Account #46245
755 Yadkinville Rd
Mocksville, NC 27028
Project Description
Project/Site Location (City/State)
RUSH — Additional charges apply
Method of Shipment
Matrix Key
5pecial Detection Umit(s)
0 Fed Ex OUSPS
WW — Wastewater GW — Groundwater
Date Results Needed
SUPS
❑ Courier Client Drop Off
DW - Drinking Water 5 - Soil /Solid 0 - Oil
P - Product M - Mist
Other
Project Number
Project Manager Phone tt
Project Manager Email
Purchase order Number
Site/Facility ID d
336-399-3646
brent Collins@emaresources com
T
Z
w
A Cool t 10C Na2S203 (Micro only)
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Memphis, TN 3SI33
noted, all containers
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per Table II of 40 CFR Part
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Sample Identification
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Comments/Notes
`
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Metals:Al,As,Ca,Cd.Cr,Cu,Fe,Pb
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Mn, Mg, Mo,Hg,Ni,Se, Na, P,S,K,Zn
Illlll llii llll llllll �lll ill llfl 111111111111111111 I 1111 -20209
EMA Resources Inc. 16 04.18
Yancey WTP
For Laboratory Use Only
Sam
by
[Name — Print]
Client Remarks/Comments
Sludge Samples Report Dry Weight
Ice
Custody
Lab Comments
N
Sea is
C '
-
Relin [SIGNAT —
to Tim
Received (SIGN RE}
Date Time
y
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Page 7 of 7

aceAnalytical
National Center for Testing & Innovation
ANALYTICAL REPORT
January 15, 2020
EMA Resources
Sample Delivery Group
Samples Received:
Project Number:
Description:
Site:
L1176796
01/07/2020
YANCEYVILLE
Sludge
YANCEYVILLE WWTP
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By: Jw C4V1--
Justin Carr
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources YANCEYVILLE L1176796 01/15/20 08:19 1 of 22

TABLE OF CONTENTS
ONE LAB. NATIONWIDE. *
Cp: Cover Page
Tc: Table of Contents
Ss: Sample Summary
Cn: Case Narrative
Sr: Sample Results
YANCEYVILLE WWTP L1176796-01
Qc: Quality Control Summary
Wet Chemistry by Method 9012 B
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9045D
Wet Chemistry by Method D93/1010A
Mercury by Method 7470A
Metals (ICP) by Method 6010D
Volatile Organic Compounds (GC/MS) by Method 8260D
Chlorinated Acid Herbicides (GC) by Method 8151A
Pesticides (GC) by Method 8081B
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
GI: Glossary of Terms
al: Accreditations & Locations
Sc: Sample Chain of Custody
1
2
3
4
5
5
7
7
9
10
11
12
13
14
16
17
18
20
21
22
ACCOUNT: PROJECT: SDG: DATE/TIME:
EMA Resources YANCEYVILLE L1176796 01/15/20 08:19
PAGE:
2 of 22

YANCEYVILLE WWTP L1176796-01 Waste
SAMPLE
SUMMARY
Collected by
Roy Whitaker
Collected date/time
01/06/2012:45
ONE LAB. NATIONWIDE.
Received date/time
01/07/20 08:40
FP
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
date/time
date/time
F
Preparation by Method 1311
WG1407184
1 01/07/2016:42
01/07/2016:42
CGD
Mt. Juliet, TN
Preparation by Method 1311
WG1407767
1 01/08/2016:18
01/08/2016:18
IDW
Mt. Juliet, TN
Wet Chemistry by Method 9012 B
WG1408346
1 01/10/20 08:52
01/13/2012:39
JER
Mt. Juliet, TN
Wet Chemistry by Method 9034-9030B
WG1408122
1 01/08/20 22:50
01/08/20 22:50
LDT
Mt. Juliet, TN
Wet Chemistry by Method 9045D
WG1407889
1 01/10/2014:00
01/11/2015:00
MSP
Mt. Juliet, TN
Fn
Wet Chemistry by Method D93/1010A
WG1410345
1 01/14/2018:07
01/14/2018:07
MJA
Mt. Juliet, TN
Mercury by Method 7470A
WG1407696
1 01/08/2013:23
01/08/20 2135
TCT
Mt. Juliet, TN
Metals (ICP) by Method 6010D
WG1407712
1 01/09/20 08:46
01/09/2010:43
TRB
Mt. Juliet, TN
Fr
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1408517
1 01/09/2018:22
01/09/2018:22
BMB
Mt. Juliet, TN
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1409359
1 01/10/2018:29
01/11/201145
RP
Mt. Juliet, TN
FC
Pesticides (GC) by Method 8081B
WG1407420
1 01/08/2016:20
01/11/2013:47
RP
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG1407418
1 01/08/2016:41
01/10/20 02:28
JNJ
Mt. Juliet, TN
GI
SAI
RC
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
YANCEYVILLE
L1176796
01/15/20 08:19
3 of 22

CASE NARRATIVE
ONE LAB. NATIONWIDE. *
All sample aliquots were received at the correct temperature, in the proper containers, with the FP
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data. 0
Fr
FC
GI
Justin Carr [Al
Project Manager
RC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources YANCEYVILLE L1176796 01/15/20 08:19 4 of 22

YANCEYVILLE WWTP
Collected date/time: 01/06/20 12:45
Preparation by Method 1311
SAMPLE RESULTS - 01
L1176796
Result Qualifier
Prep
Batch
Analyte
date / time
TCLP Extraction
1/7/2020 4:42:13 PM
WG1407184
TCLP ZHE Extraction -
1/8/2020 4:18:10 PM
WG1407767
Fluid 1
1/7/20204:42:13 PM
WG1407184
Initial pH 7.01
1/7/20204:42:13 PM
WG1407184
Final pH 4.98
1/7/2020 4:42:13 PM
WG1407184
Wet Chemistry by Method 9012 B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Reactive Cyanide ND J3 J6 0.250 1 01/13/202012:39 WG1408346
Wet Chemistry by Method 9034-9030B
Result Qualifier RDL
Analyte mg/kg mg/kg
Reactive Sulfide 39.6 25.0
Wet Chemistry by Method 9045D
Dilution Analysis Batch
date / time
1 01/08/2020 22:50 WG1408122
Result Qualifier Dilution Analysis Batch
Analyte su date / time
Corrosivity by pH 7.13 T8 1 01/11/202015:00 WG1407889
Sample Narrative:
L1176796-01 WG1407889:7.13 at20.4C
Wet Chemistry by Method D93/1010A
Result
Analyte Deg. F
Ignitability DNI at170
Mercury by Method 7470A
Qualifier Dilution Analysis
date / time
1 01/14/202018:07
Result Qualifier RDL Limit
Analyte mg/I mg/I mg/I
Mercury ND 0.0100 0.20
Metals (ICP) by Method 6010D
Result
Qualifier RDL Limit
Analyte
mg/I
mg/I mg/I
Arsenic
ND
0.100 5
Barium
0.168
0.100 100
Cadmium
ND
0.100 1
Chromium
ND
0.100 5
Lead
0.135
0.100 5
Selenium
ND
0.100 1
Silver
ND
0.100 5
Volatile Organic
Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL Limit
Analyte
mg/I
mg/I mg/I
Benzene
ND
0.0500 0.50
Carbon tetrachloride
ND
0.0500 0.50
Chlorobenzene
ND
0.0500 100
Chloroform
ND
0.250 6
ACCOUNT:
PROJECT:
EMA Resources
YANCEYVILLE
Batch
WG1410345
Dilution Analysis Batch
date / time
1 01/08/2020 2135 WG1407696
Dilution Analysis
Batch
date / time
1 01/09/202010:43
WG1407712
1 01/09/202010:43
WG1407712
1 01/09/202010:43
WG1407712
1 01/09/202010:43
WG1407712
1 01/09/202010:43
WG1407712
1 01/09/202010:43
WG1407712
1 01/09/202010:43
WG1407712
ONE LAB. NATIONWIDE. *
Fp
Fc
FS
Fn
Fc
�GI
SAI
Rc
Dilution Analysis
Batch
date / time
1 01/09/202018:22
WG1408517
1 01/09/202018:22
WG1408517
1 01/09/202018:22
WG1408517
1 01/09/202018:22
WG1408517
SDG:
DATE/TIME: PAGE:
L1176796
01/15/20 08:19 5 of 22

YANCEYVILLE WWTP SAMPLE RESULTS
Collected date/time: 01/06/20 12:45 L1176796
Volatile Organic Compounds (GC/MS) by Method 8260D
- 01
Result
Qualifier RDL Limit Dilution
Analysis
Batch
Analyte
mg/I
mg/I mg/I
date/time
1,2-Dichloroethane
ND
0.0500 0.50 1
01/09/202018:22
WG1408517
1,1-Dichloroethene
ND
0.0500 0.70 1
01/09/202018:22
WG1408517
2-Butanone (MEK)
ND
0.500 200 1
01/09/202018:22
WG1408517
Tetrachloroethene
ND
0.0500 0.70 1
01/09/202018:22
WG1408517
Trichloroethene
ND
0.0500 0.50 1
01/09/202018:22
WG1408517
Vinyl chloride
ND
0.0500 0.20 1
01/09/202018:22
WG1408517
(S) Toluene-dH
98.4
80.0-120
0110912020 18.22
WG1408517
(S) 4-Bromofluorobenzene
99.5
77.0-126
0110912020 18.22
WG1408517
(S) 1,2-Dichloroethane-d4
104
70.0-130
011091202018.22
WG1408517
Chlorinated Acid Herbicides (GC) by Method 8151A
Result
Analyte mg/I
2,4,5-TP (Silvex) ND
2,4-D ND
(S) Z4-Dichlorophenyl Acetic Acid 76.2
Pesticides (GC) by Method 8081B
Qualifier RDL
Limit
Dilution Analysis
Batch
mg/I
mg/I
date / time
0.00200
1
1 01/11/20201145
WG1409359
0.00200
10
1 01/11/20201145
WG1409359
14.0-158
011111202011.45
WG1409359
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Chlordane
ND
0.00500
0.03
1 01/11/202013:47
WG1407420
Endrin
ND
0.00500
0.02
1 01/11/202013:47
WG1407420
Heptachlor
ND
0.00500
0.0080
1 01/11/202013:47
WG1407420
Lindane
ND
0.00500
0.40
1 01/11/202013:47
WG1407420
Methoxychlor
ND
0.00500
10
1 01/11/202013:47
WG1407420
Toxaphene
ND
0.0100
0.50
1 01/11/202013:47
WG1407420
(S) Decochlorobiphenyl
53.3
10.0-128
0111112020 13.47
WG1407420
(S) Tetrochloro-m-xylene
72.1
10.0-127
0111112020 13.47
WG1407420
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Analyte
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachloroethane
Nitrobenzene
Pyridine
3&4-Methyl Phenol
2-Methylphenol
Pentachlorophenol
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
(S) 2-Fluorophenol
(S) Phenol-d5
(S) Nitrobenzene-d5
(S) 2-Fluorobiphenyl
(S) Z4,6-Tribromophenol
(S) p-Terphenyl-d14
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
mg/I
mg/I
mg/I
date/time
ND
0.100
7.50
1 01/10/2020 02:28
WG1407418
ND
0.100
0.13
1 01/10/2020 02:28
WG1407418
ND
0.100
0.13
1 01/10/2020 02:28
WG1407418
ND
0.100
0.50
1 01/10/2020 02:28
WG1407418
ND
0.100
3
1 01/10/2020 02:28
WG1407418
ND
0.100
2
1 01/10/2020 02:28
WG1407418
ND
0.100
5
1 01/10/2020 02:28
WG1407418
ND
0.100
400
1 01/10/2020 02:28
WG1407418
ND
0.100
200
1 01/10/2020 02:28
WG1407418
ND
0.100
100
1 01/10/2020 02:28
WG1407418
ND
0.100
400
1 01/10/2020 02:28
WG1407418
ND
0.100
2
1 01/10/2020 02:28
WG1407418
41.2
10.0-120
0111012020 02.28
WG1407418
24.5
10.0-120
0111012020 02.28
WG1407418
50.6
10.0-127
0111012020 02.28
WG1407418
69.5
10.0-130
0111012020 02.28
WG1407418
75.0
10.0-155
0111012020 02.28
WG1407418
83.9
10.0-128
0111012020 02.28
WG1407418
ONE LAB. NATIONWIDE. *
Fp
Fc
FS
Fn
FA
Fc
F,
SAI
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources YANCEYVILLE L1176796 01/15/20 08:19 6 of 22

WG1408346 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9012 B L1176796-01
Method Blank (MB)
(MB) R3490255-1 01/13/201233
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Reactive Cyanide U 0.0390 0.250
L1177102-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1177102-01 01/13/2012:42 • (DUP) R3490255-5 01/13/2012:45
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %_
Reactive Cyanide ND 0.000 1 0.000 20
L1177103-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1177103-01 01/13/2012:46 • (DUP) R3490255-6 01/13/2012:47
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg
Reactive Cyanide ND 0.000 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3490255-2 01/13/2012:34
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Reactive Cyanide 2.50 2.51 100
Rec. Limits LCS Qualifier
50.0-150
L1176796-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1176796-01 01/13/20 12:39 • (MS) R3490255-3 01/13/20 12:40 • (MSD) R3490255-4 01/13/20 12:41
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 1.67 ND 1.27 0.738 76.4 44.3 1 75.0-125 J3 J6 53.3 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources YANCEYVILLE L1176796 01/15/20 08:19 7 of 22

WG1408346 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9012 B L1176796-01
L1177424-10 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1177424-10 01/13/20 13:03 • (MS) R3490255-7 01/13/20 13:04 • (MSD) R3490255-8 01/13/20 13:05
Spike Amount Original Result MS Result (dry) MSD Result MS Rec. MSD Rec.
(dry) (dry) (dry)
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 2.15 2.27 3.87 3.89 74.3 75.4
Dilution Rec. Limits
75.0-125
MS Qualifier MSD Qualifier RPD
J6 0.588
ONE LAB. NATIONWIDE. *
RPD Limits
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources YANCEYVILLE L1176796 01/15/20 08:19 3 of 22

WG1408122
Wet Chemistry by Method 9034-9030B
Method Blank (MB)
(MB) R3439156-1 01/03/20 22:50
MB Result MB Qualifier MB MDL
Analyte mg/kg mg/kg
Reactive Sulfide U 7.63
Laboratory Control Sample (LCS)
(LCS) R3489156-2 01/08/20 22:50
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Reactive Sulfide 100 72.5 72.5
QUALITY CONTROL SUMMARY
L1176796-01
MB RDL
mg/kg
25.0
Rec. Limits LCS Qualifier
70.0-130
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources YANCEYVILLE L1176796 01/15/20 03:19 9 of 22

WG1407889 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9045D L1176796-01
Laboratory Control Sample (LCS)
(LCS) R3489925-1 01/11/201500
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte su su
Corrosivity by pH 10.0 9.97 99.7 99.0-101
Sample Narrative:
LCS: 9.97 at19.8C
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources YANCEYVILLE L1176796 01/15/20 08:19 10 of 22

WG1410345 QUALITY CONTROL SUMMARY
Wet Chemistry by Method D93/1010A L1176796-01
L1176796-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1176796-01 01/14/20 18:07 • (DUP) R3490735-2 01/14/20 18:07
Original Result DUP Result Dilution DUP RPD
Analyte Deg. F Deg. F
Ignitability DNI at170 DNI at170 1 0.000
Laboratory Control Sample (LCS)
DUP Qualifier DUP RPD
Limits
i
10
(LCS) R3490735-1 01/14/201807
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte Deg. F Deg. F
Ignitability 82.0 84.5 103 97.0-103
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources YANCEYVILLE L1176796 01/15/20 08:19 11 of 22

WG1407696 QUALITY CONTROL SUMMARY
Mercury by Method 7470A L1176796-01
Method Blank (MB)
(MB) R3439144-1 01/03/20 2109
MB Result MB Qualifier MB MDL
MB RDL
Analyte mg/I mg/I
mg/I
Mercury U 0.00330
0.0100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3439144-4 01/03/20 21:25 • (LCSD) R3439144-5 01/03/20 2127
Spike Amount LCS Result LCSD Result
LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I
Mercury 0.0300 0.0281 0.0269
93.7 89.5 80.0-120 4.53 20
L1176623-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1176623-01 01/03/20 21:15 • (MS) R3439144-2 01/03/20 2117 • (MSD) R3439144-3 01/03/20 2119
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Mercury 0.0300
ND
0.0278
0.0282 92.5 93.9 1 75.0-125 1.44 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources YANCEYVILLE L1176796 01/15/20 08:19 12 of 22

WG1407712
Metals (ICP) by Method 6010D
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1176796-01
(MB) R3439297-1 01/09/20 09:56
MB Result
MB Qualifier MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
Arsenic U
0.0333
0.100
Barium U
0.0333
0.100
Cadmium U
0.0333
0.100
Chromium U
0.0333
0.100
Lead U
0.0333
0.100
Selenium U
0.0333
0.100
Silver U
0.0333
0.100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3489297-2 01/09/20 09:58 • (LCSD) R3489297-3 01/09/20 10:01
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/I
mg/I
mg/I
Arsenic
10.0
9.64
9.62
96.4
96.2
80.0-120
Barium
10.0
9.80
9.81
98.0
98.1
80.0-120
Cadmium
10.0
9.54
9.57
95.4
95.7
80.0-120
Chromium
10.0
9.51
9.49
95.1
94.9
80.0-120
Lead
10.0
9.62
9.65
96.2
96.5
80.0-120
Selenium
10.0
9.77
9.85
97.7
98.5
80.0-120
Silver
2.00
1.75
1.75
87.7
87.4
80.0-120
L1174116-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1174116-05 01/09/20 10:04 • (MS) R3489297-5 01/09/20 10:09 • (MSD) R3489297-6 01/09/20 10:12
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
Arsenic
10.0
ND
9.68
9.67
96.8
96.7
Barium
10.0
ND
9.88
9.88
98.1
98.0
Cadmium
10.0
ND
9.56
9.57
95.6
95.7
Chromium
10.0
ND
9.43
9.43
94.3
94.3
Lead
10.0
26.0
34.4
37.9
84.3
119
Selenium
10.0
ND
9.83
9.96
98.3
99.6
Silver
2.00
ND
1.77
1.80
86.3
87.7
LCS Qualifier LCSD Qualifier RPD
RPD Limits
0.197
20
0.145
20
0.297
20
0.152
20
0.323
20
0.830
20
0.263
20
Dilution Rec. Limits
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
MS Qualifier MSD Qualifier RPD
0.0699
0.0680
0.114
0.00206
9.56
1.32
1.62
ONE LAB. NATIONWIDE. *
RPD Limits
20
20
20
20
20
20
20
ACCOUNT:
EMA Resources
PROJECT:
YANCEYVILLE
SDG:
L1176796
DATE/TIME:
01/15/20 08:19
PAGE:
13 of 22

WG1408517 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1176796-01
ONE LAB. NATIONWIDE. *
Method Blank (MB)
(MB) R3489465-3 01/09/201700
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Benzene
U
0.0167
0.0500
Carbon tetrachloride
U
0.0167
0.0500
Chlorobenzene
U
0.0167
0.0500
Chloroform
U
0.0833
0.250
1,2-Dichloroethane
U
0.0167
0.0500
1,1-Dichloroethene
U
0.0167
0.0500
2-Butanone (MEK)
U
0.167
0.500
Tetrachloroethene
U
0.0167
0.0500
Trichloroethene
U
0.0167
0.0500
Vinyl chloride
U
0.0167
0.0500
(S) Toluene-dH
97.2
80.0-120
(S) 4-Bromofluorobenzene
99.4
77.0-126
(S) 1,2-Dichloroethane-d4
102
70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3489465-1 01/09/2012:36 • (LCSD) R3489465-2 01/09/2015:21
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/I
mg/I
mg/I
Benzene
0.250
0.241
0.257
96.4
103
70.0-123
Carbon tetrachloride
0.250
0.288
0.274
115
110
68.0-126
Chlorobenzene
0.250
0.254
0.260
102
104
80.0-121
Chloroform
0.250
0.252
0.257
101
103
73.0-120
1,2-Dichloroethane
0.250
0.256
0.259
102
104
70.0-128
1,1-Dichloroethene
0.250
0.264
0.251
106
100
71.0-124
2-Butanone (MEK)
1.25
1.15
1.24
92.0
99.2
44.0-160
Tetrachloroethene
0.250
0.275
0.272
110
109
72.0-132
Trichloroethene
0.250
0.252
0.263
101
105
78.0-124
Vinyl chloride
0.250
0.258
0.285
103
114
67.0-131
(S) Toluene-dH
98.3
102
80.0-120
(S) 4-Bromofluorobenzene
104
106
77.0-126
(S) 1,2-Dichloroethane-d4
104
102
70.0-130
LCS Qualifier
LCSD Qualifier RPD
6.43
4.98
2.33
1.96
1.17
5.05
7.53
1.10
4.27
9.94
RPD Limits
20
20
20
20
20
20
20
20
20
20
ACCOUNT:
EMA Resources
PROJECT: SDG: DATE/TIME: PAGE:
YANCEYVILLE L1176796 01/15/20 08:19 14 of 22

WG1408517 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1176796-01
L1176822-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1176322-02 01/09/20 13:43 • (MS) R3439465-4 01/09/20 19:03 • (MSD) R3439465-5 01/09/20 19:23
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
Benzene
0.250
ND
0.217
0.264
86.8
106
Carbon tetrachloride
0.250
ND
0.168
0.256
67.2
102
Chlorobenzene
0.250
ND
0.240
0.276
96.0
110
Chloroform
0.250
ND
0.244
0.288
97.6
115
1,2-Dichloroethane
0.250
ND
0.289
0.326
116
130
1,1-Dichloroethene
0.250
ND
0.153
0.255
61.2
102
2-Butanone (MEK)
1.25
ND
1.40
1.58
112
126
Tetrachloroethene
0.250
ND
0.185
0.256
74.0
102
Trichloroethene
0.250
ND
0.194
0.249
77.6
99.6
Vinyl chloride
0.250
ND
0.171
0.247
68.4
98.8
(S) Toluene-dH
99.6
98.1
(S) 4-Bromofluorobenzene
100
100
(S) 1,2-Dichloroethane-d4
105
102
ONE LAB. NATIONWIDE. *
Dilution Rec. Limits
MS Qualifier MSD Qualifier
RPD
RPD Limits
1 17.0-158
19.5
27
1 23.0-159
J3
41.5
28
1 33.0-152
14.0
27
1 29.0-154
16.5
28
1 29.0-151
12.0
27
1 11.0-160
J3
50.0
29
1 10.0-160
12.1
32
1 10.0-160
J3
32.2
27
1 10.0-160
24.8
25
1 10.0-160
J3
36.4
27
80.0-120
77.0-126
70.0-130
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources YANCEYVILLE L1176796 01/15/20 08:19 15 of 22

WG1409359
Chlorinated Acid Herbicides (GC) by Method 8151A
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1176796-01
(MB) R3489972-1 01/11/20 03 06
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
2,4-D U
0.000667
0.00200
2,4,5-TP (Silvex) U
0.000667
0.00200
(S) Z4-Dichlorophenyl Acetic 79.0
14.0-158
Acid
Laboratory Control Sample (LCS)
(LCS) R3439972-2 01/11/20 0319
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
2,4-D 0.0500
0.0550
110
50.0-120
2,4,5-TP (Silvex) 0.0500
0.0499
99.8
50.0-125
(S) Z4-Dichlorophenyl Acetic
86.2
14. 0-158
Acid
L1176151-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1176151-01 01/11/20 03 33 • (MS) R3439972-3 01/11/20 03 47 • (MSD) R3439972-4 01/11/20 09:01
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
2,4-D
0.0500
ND
0.0519
0.0534
104
107
2,4,5-TP (Silvex)
0.0500
ND
0.0485
0.0504
97.0
101
(S) Z4-Dichlorophenyl Acetic
86.8
92.2
Acid
Dilution Rec. Limits
1 50.0-120
1 50.0-125
14.0-158
MS Qualifier MSD Qualifier RPD
2.85
3.84
ONE LAB. NATIONWIDE. *
RPD Limits
20
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources YANCEYVILLE L1176796 01/15/20 08:19 16 of 22

WG1407420 QUALITY CONTROL SUMMARY
Pesticides (GC) by Method 8081B L1176796-01
Method Blank (MB)
(MB) R3439720-1 01/09/20 09:01
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Gamma BHC
U
0.00167
0.00500
Endrin
U
0.00167
0.00500
Heptachlor
U
0.00167
0.00500
Methoxychlor
U
0.00167
0.00500
Chlordane
U
0.00167
0.00500
Toxaphene
U
0.00333
0.0100
(S) Decachlorobiphenyl
86.7
10.0-128
(S) Tetrochloro-m-xylene
82.7
10.0-127
Laboratory Control Sample (LCS)
(LCS) R3489720-2 01/09/20 0913
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
Gamma BHC
0.0100
0.0115
115
55.0-129
Endrin
0.0100
0.0112
112
57.0-134
Heptachlor
0.0100
0.0112
112
27.0-132
Methoxychlor
0.0100
0.0116
116
54.0-155
(S) Decachlorobiphenyl
88.7
10.0-128
(S) Tetrochloro-m-xylene
96.8
10.0-127
L1176151-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1176151-01 01/09/20 09:25 • (MS) R3439720-3 01/09/20 09:38 • (MSD) R3439720-4 01/09/20 09:50
Spike Amount
Original Result
MS Result
MSD Result MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Gamma BHC 0.0100
ND
0.0104
0.0112 104
112
1 14.0-141
7.41
40
Endrin 0.0100
ND
0.0102
0.0108 102
108
1 10.0-160
5.71
39
Heptachlor 0.0100
ND
0.0103
0.0109 103
109
1 16.0-136
5.66
40
Methoxychlor 0.0100
ND
0.0117
0.0120 117
120
1 10.0-160
2.53
34
(S) Decachlorobiphenyl
83.4
86.5
10.0-128
(S) Tetrochloro-m-xylene
94.0
98.9
10.0-127
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
YANCEYVILLE
L1176796
01/15/20 08:19
17 of 22

WG1407418 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1176796-01
Method Blank (MB)
(MB) R3489275-2 01/03/20 2347
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
U
0.0333
0.100
2,4-Dinitrotoluene
U
0.0333
0.100
Hexachlorobenzene
U
0.0333
0.100
Hexachloro-1,3-butadiene
U
0.0333
0.100
Hexachloroethane
U
0.0333
0.100
Nitrobenzene
U
0.0333
0.100
Pyridine
U
0.0333
0.100
2-Methylphenol
U
0.0333
0.100
3&4-Methyl Phenol
U
0.0333
0.100
Pentachlorophenol
U
0.0333
0.100
2,4,5-Trichlorophenol
U
0.0333
0.100
2,4,6-Trichlorophenol
U
0.0333
0.100
(S) Nitrobenzene-d5
73.2
10.0-127
(S) 2-Fluorobiphenyl
82.6
10.0-130
(S) p-Terphenyl-d14
85.3
10.0-128
(S) Phenol-d5
28.7
10.0-120
(S) 2-Fluorophenol
48.8
10.0-120
(S) 2,4,6-Tribromophenol
82.5
10.0-155
Laboratory Control Sample (LCS)
ONE LAB. NATIONWIDE. *
(LCS) R3489275-1 01/08/20 2326
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
1,4-Dichlorobenzene 0.500
0.345
69.0
18.0-120
2,4-Dinitrotoluene 0.500
0.465
93.0
49.0-124
Hexachlorobenzene 0.500
0.412
82.4
44.0-120
Hexachloro-1,3-butadiene 0.500
0.352
70.4
19.0-120
Hexachloroethane 0.500
0.333
66.6
15.0-120
Nitrobenzene 0.500
0.333
66.6
27.0-120
Pyridine 0.500
0.0744
14.9
10.0-120
2-Methylphenol 0.500
0.339
67.8
28.0-120
3&4-Methyl Phenol 0.500
0.350
70.0
31.0-120
Pentachlorophenol 0.500
0.416
83.2
23.0-120
2,4,5-Trichlorophenol 0.500
0.470
94.0
44.0-120
2,4,6-Trichlorophenol 0.500
0.426
85.2
42.0-120
(S) Nitrobenzene-d5
60.2
10.0-127
(S) 2-Fluorobiphenyl
79.7
10.0-130
(S) p-Terphenyl-d14
84.7
10.0-128
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
YANCEYVILLE L1176796 01/15/20 08:19 18 of 22

WG1407418 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1176796-01
Laboratory Control Sample (LCS)
(LCS) R3489275-1 01/08/20 2326
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
(S) Phenol-d5 30.7 10.0-120
(S) 2-Fluorophenol 48.7 10.0-120
(S) 2,4,6-Tribromophenol 88.5 10.0-155
L1176151-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1176151-01 01/09/20 00:09 • (MS) R3489275-3 01/09/20 00:31 • (MSD) R3489275-4 01/09/20 00:53
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
0.500
ND
0.339
0.346
67.8
69.2
2,4-Dinitrotoluene
0.500
ND
0.457
0.492
91.4
98.4
Hexachlorobenzene
0.500
ND
0.418
0.432
83.6
86.4
Hexachloro-1,3-butadiene
0.500
ND
0.355
0.362
71.0
72.4
Hexachloroethane
0.500
ND
0.336
0.343
67.2
68.6
Nitrobenzene
0.500
ND
0.331
0.328
66.2
65.6
Pyridine
0.500
ND
0.0860
0.133
17.2
26.6
2-Methylphenol
0.500
ND
0.329
0.337
65.8
67.4
3&4-Methyl Phenol
0.500
ND
0.341
0.345
68.2
69.0
Pentachlorophenol
0.500
ND
0.438
0.448
87.6
89.6
2,4,5-Trichlorophenol
0.500
ND
0.455
0.489
91.0
97.8
2,4,6-Trichlorophenol
0.500
ND
0.417
0.433
83.4
86.6
(S) Nitrobenzene-d5
61.7
60.5
(S) 2-Fluorobiphenyl
81.3
83.1
(S) p-Terphenyl-d14
87.9
88.0
(S) Phenol-d5
31.6
32.6
(S) 2-Fluorophenol
48.3
49.4
(S) 2,4,6-Tribromophenol
90.0
95.0
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
1 17.0-120
2.04
1 39.0-125
7.38
1 35.0-122
3.29
1 12.0-120
1.95
1 10.0-120
2.06
1 12.0-120
0.910
1 10.0-120
J3 42.9
1 10.0-120
2.40
1 10.0-120
1.17
1 10.0-128
2.26
1 33.0-120
7.20
1 26.0-120
3.76
10.0-127
10.0-130
10.0-128
10.0-120
10.0-120
10.0-155
ONE LAB. NATIONWIDE. *
RPD Limits
40
25
24
34
40
30
37
30
36
37
31
31
ACCOUNT:
EMA Resources
PROJECT:
YANCEYVILLE
SDG: DATE/TIME:
L1176796 01/15/20 08:19
PAGE:
19 of 22

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
ONE LAB. NATIONWIDE. *
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
u
Fc
FS
(dry)
Results are reported based on the dry weight ofthe sample. [this will only be present on a dry report basis for soils].
MDL
Method Detection Limit.
Fn
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Fr
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Fc
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
F
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
Rc
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J3 The associated batch QC was outside the established quality control range for precision.
J6 The sample matrix interfered with the ability to make any accurate determination, spike value is low.
T8 Sample(s) received past/too close to holding time expiration.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources YANCEYVILLE L1176796 01/15/20 08:19 20 of 22

ACCREDITATIONS
& LOCATIONS
ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide
from one location. One phone call, one point of contact,
one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our
single location laboratory is comparable to the collective
totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory
campus. The model is conducive to accelerated
productivity, decreasing
Cp
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium
quality and prompt service allows us to be YOUR
LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace
National.
Fc
State Accreditations
Alabama 40660
Nebraska
NE-OS-15-05
FS
Alaska 17-026
Nevada
TN-03-2002-34
Arizona AZ0612
New Hampshire
2975
Arkansas 88-0469
New Jersey—NELAP
TNO02
Fn
California 2932
New Mexico
n/a
Colorado TN00003
New York
11742
Connecticut PH-0197
North Carolina
Env375
Fr
Florida E87487
North Carolina'
DW21704
Georgia NELAP
North Carolina 3
41
Georgia' 923
North Dakota
R-140
Fc
Idaho TN00003
Ohio—VAP
CL0069
Illinois 200008
Oklahoma
9915
7G1
Indiana C-TN-01 f
Oregon
TN200002
Iowa 364
Pennsylvania
68-02979
Kansas E-10277
Rhode Island
LA000356
Kentucky' 6 90010
South Carolina
84004
Kentucky 2 16
South Dakota
n/a
Louisiana A130792
Tennessee'"
2006
Louisiana' LA180010
Texas
T104704245-18-15
Rc
Maine TN0002
Texas 5
LABO152
Maryland 324
Utah
TN00003
Massachusetts M-TNO03
Vermont
VT2006
Michigan 9958
Virginia
460132
Minnesota 047-999-395
Washington
C847
Mississippi TN00003
West Virginia
233
Missouri 340
Wisconsin
9980939910
Montana CERT0086
Wyoming
A2 LA
Third Party Federal Accreditations
A2LA— ISO17025 1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5 1461.02
DOD
1461.01
Canada 1461.01
USDA
P330-15-00234
EPA—Crypto TN00003
' Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
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OR
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VWY
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ACCOUNT: V PROJECT:
EMA Resources YANCEYVILLE
ME
MN
WVI NY
MI T
IA T PA 4
OH
Mo
IL Ihi
T T WV
VAT
KY
N * r�
AR
Ms AL GA
LA
FL
SDG: DATE/TIME: PAGE:
L1176796 01/15/20 08:19 21 of 22

4
•
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Chain of Custody Page of
EMA Resources Mr. Brent Collins L
7SS Yadkinville Road
ceAnalytical'
75S Yadkinville Road Mocksville, NC 27028�0`�""�
Mocksville, NC 27028
Report tc Email To: [e-mail]
Mr. Brent Collins
_
1065LebxanRd �i Q
Mount Juliet, 7N 37122
phone: [phone]
Phone:80P-767-s8s9 x }ff
Fax: [phone]
Project City/State �// �/ /1
Description: Sludge Collected: y,tdc0- ✓atz-, �(�
Please Circle:
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Phone: 336-7S1-1441
ClientProjects
lab Project s
Fax: 336-7S 1-1442
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GW- Groundwater B- Bioassay ICOC signed/Accurate: N
WW - Waste Water Correct bottles used: !_N
DW - Drinking Wa Sufficient volum,' sent: rLI _ N
Samples ret ed via:
OT - Other Tracking p(i'l 3�_A2P93i�
UPS FeclEx Courier 1 7 7 / VOA Zero Headspace: Y _N
Reline h d by : na rey Date: Time: Received by: (Signature) Trip Blank Received: Yes/coPreservation Correct/checked: �� _N
--- // RAD Screen <0.5 mR/hr: ,/Y _N
HCL/ MeoHA.
TBR
RjXquishecld : e D e: Time: Received by: (Signature) Temp: �� Bottles Received- If preservation required by Login: Date/Time
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Conditio
NCF /�

aceAnalytical
National Center for Testing & Innovation
ANALYTICAL REPORT
January 20, 2020
EMA Resources
Sample Delivery Group
Samples Received:
Project Number:
Description:
Site:
L1177368
01/08/2020
YANCEYVILLE
Sludge
YANCEYVILLE WTP
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By: Jw C4V1--
Justin Carr
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources YANCEYVILLE L1177363 01/20/2014:27 1 of 23

TABLE OF CONTENTS
ONE LAB. NATIONWIDE. *
Cp: Cover Page
Tc: Table of Contents
Ss: Sample Summary
Cn: Case Narrative
Sr: Sample Results
YANCEYVILLEWTP L1177368-01
Qc: Quality Control Summary
Wet Chemistry by Method 9012 B
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9045D
Wet Chemistry by Method D93/1010A
Mercury by Method 7470A
Metals (ICP) by Method 6010D
Volatile Organic Compounds (GC/MS) by Method 8260D
Chlorinated Acid Herbicides (GC) by Method 8151A
Pesticides (GC) by Method 8081B
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
GI: Glossary of Terms
al: Accreditations & Locations
Sc: Sample Chain of Custody
1
2
3
4
5
5
7
7
9
10
11
12
13
15
17
18
19
21
22
23
ACCOUNT: PROJECT: SDG: DATE/TIME:
EMA Resources YANCEYVILLE L1177363 01/20/2014:27
PAGE:
2 of 23

YANCEYVILLEWTP L1177368-01 Waste
SAMPLE
SUMMARY
Collected by
Roy Whitaker
Collected date/time
01/06/2013:00
ONE LAB. NATIONWIDE.
Received date/time
01/08/20 09:00
FP
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
date/time
date/time
F
Preparation by Method 1311
WG1408214
1 01/09/20 08:50
01/09/20 08:50
BAA
Mt. Juliet, TN
Preparation by Method 1311
WG1408380
1 01/09/2012:02
01/09/2012:02
CGD
Mt. Juliet, TN
Wet Chemistry by Method 9012 B
WG1410341
1 01/14/201109
01/14/2018:49
JER
Mt. Juliet, TN
Wet Chemistry by Method 9034-9030B
WG1409180
1 01/11/2017:00
01/11/2017:00
LDT
Mt. Juliet, TN
Wet Chemistry by Method 9045D
WG1409190
1 01/14/2015:00
01/14/20 20:00
MSP
Mt. Juliet, TN
Fn
Wet Chemistry by Method D93/1010A
WG1412116
1 01/20/2010:15
01/20/2010:15
MJA
Mt. Juliet, TN
Mercury by Method 7470A
WG1408995
1 01/10/2010:30
01/13/2010:12
ABL
Mt. Juliet, TN
Metals (ICP) by Method 6010D
WG1409034
1 01/11/2012:29
01/12/2016:05
CCE
Mt. Juliet, TN
Fr
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1409088
1 01/13/20 0127
01/13/20 0127
BMB
Mt. Juliet, TN
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1411034
1 01/14/2018:22
01/16/20 03:16
LEL
Mt. Juliet, TN
FC
Pesticides (GC) by Method 8081B
WG1409135
1 01/12/2016:58
01/13/2015:04
HMH
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG1409132
1 01/12/2018:00
01/13/20 07:58
AO
Mt. Juliet, TN
GI
SAI
RC
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
YANCEYVILLE
L1177363
01/20/20 14:27
3 of 23

CASE NARRATIVE
ONE LAB. NATIONWIDE. *
All sample aliquots were received at the correct temperature, in the proper containers, with the FP
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data. 0
Fr
FC
GI
Justin Carr [Al
Project Manager
RC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources YANCEYVILLE L1177363 01/20/20 14:27 4 of 23

YANCEYVILLEWTP
Collected date/time: 01/06/20 13:00
Preparation by Method 1311
SAMPLE RESULTS - 01
L1177368
Result Qualifier Prep
Batch
Analyte
date / time
TCLP Extraction
1/9/202012:02:38 PM
WG1408380
TCLP ZHE Extraction
- 1/9/2020 8:50:29 AM
WG1408214
Fluid
1 1/9/202012:02:38 PM
WG1408380
Initial pH
6.43 1/9/202012:02:38 PM
WG1408380
Final pH
4.91 1/9/202012:02:38 PM
WG1408380
Wet Chemistry by Method 9012 B
Result Qualifier RDL
Analyte mg/kg mg/kg
Reactive Cyanide ND 0.250
Wet Chemistry by Method 9034-9030B
Result Qualifier RDL
Analyte mg/kg mg/kg
Reactive Sulfide ND 25.0
Wet Chemistry by Method 9045D
Dilution Analysis Batch
date / time
1 01/14/202018:49 WG1410341
Dilution Analysis Batch
date / time
1 01/11/202017:00 WG1409180
Result Qualifier Dilution Analysis Batch
Analyte su date / time
Corrosivity by pH 6.75 T8 1 01/14/2020 20:00 WG1409190
Sample Narrative:
L1177368-01 WG1409190: 6.75 at 22.7C
Wet Chemistry by Method D93/1010A
Result
Analyte Deg. F
Ignitability DNI at170
Mercury by Method 7470A
Qualifier Dilution Analysis Batch
date / time
1 01/20/202010:15 WG1412116
Result Qualifier RDL Limit
Analyte mg/I mg/I mg/I
Mercury ND 0.0100 0.20
Metals (ICP) by Method 6010D
Result
Qualifier RDL Limit
Analyte
mg/I
mg/I mg/I
Arsenic
ND
0.100 5
Barium
0.120
0.100 100
Cadmium
ND
0.100 1
Chromium
ND
0.100 5
Lead
ND
0.100 5
Selenium
ND
0.100 1
Silver
ND
0.100 5
Volatile Organic
Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL Limit
Analyte
mg/I
mg/I mg/I
Benzene
ND
0.0500 0.50
Carbon tetrachloride
ND
0.0500 0.50
Chlorobenzene
ND
0.0500 100
Chloroform
ND
0.250 6
ACCOUNT:
PROJECT:
EMA Resources
YANCEYVILLE
Dilution Analysis Batch
date / time
1 01/13/202010:12 WG1408995
Dilution Analysis
Batch
date / time
1 01/12/202016:05
WG1409034
1 01/12/202016:05
WG1409034
1 01/12/202016:05
WG1409034
1 01/12/202016:05
WG1409034
1 01/12/202016:05
WG1409034
1 01/12/202016:05
WG1409034
1 01/12/202016:05
WG1409034
ONE LAB. NATIONWIDE. *
Fp
Fc
FS
Fn
Fc
�GI
SAI
Rc
Dilution Analysis
Batch
date / time
1 01/13/2020 0127
WG1409088
1 01/13/2020 0127
WG1409088
1 01/13/2020 0127
WG1409088
1 01/13/2020 0127
WG1409088
SDG:
DATE/TIME: PAGE:
L1177363
01/20/20 14:27 5 of 23

YANCEYVILLEWTP SAMPLE RESULTS
Collected date/time: 01/06/20 13:00 L1177368
Volatile Organic Compounds (GC/MS) by Method 8260D
- 01
Result
Qualifier RDL Limit Dilution
Analysis
Batch
Analyte
mg/I
mg/I mg/I
date/time
1,2-Dichloroethane
ND
J4 0.0500 0.50 1
01/13/2020 0127
WG1409088
1,1-Dichloroethene
ND
0.0500 0.70 1
01/13/2020 0127
WG1409088
2-Butanone (MEK)
ND
0.500 200 1
01/13/2020 0127
WG1409088
Tetrachloroethene
ND
0.0500 0.70 1
01/13/2020 0127
WG1409088
Trichloroethene
ND
0.0500 0.50 1
01/13/2020 0127
WG1409088
Vinyl chloride
ND
0.0500 0.20 1
01/13/2020 0127
WG1409088
(S) Toluene-dH
84.8
80.0-120
0111312020 01.27
WG1409088
(S) 4-Bromofluorobenzene
90.8
77.0-126
0111312020 01.27
WG1409088
(S)1,2-Dichloroethane-d4
109
70.0-130
011131202001.27
WG1409088
Chlorinated Acid Herbicides (GC) by Method 8151A
Result
Analyte mg/I
2,4,5-TP (Silvex) ND
2,4-D ND
(S)2,4-DichlorophenylAcetic Acid 65.8
Pesticides (GC) by Method 8081B
Result
Analyte
mg/I
Chlordane
ND
Endrin
ND
Heptachlor
ND
Lindane
ND
Methoxychlor
ND
Toxaphene
ND
(S) Decochlorobiphenyl
77.9
(S) Tetrochloro-m-xylene
62.0
Qualifier RDL
Limit
Dilution Analysis
Batch
mg/I
mg/I
date / time
0.00200
1
1 01/16/2020 03:16
WG1411034
0.00200
10
1 01/16/2020 03:16
WG1411034
14.0-158
0111612020 03.16
WG1411034
Qualifier RDL Limit Dilution Analysis Batch
mg/I mg/I date / time
0.00500
0.03 1
01/13/202015:04
WG1409135
0.00500
0.02 1
01/13/202015:04
WG1409135
0.00500
0.0080 1
01/13/202015:04
WG1409135
0.00500
0.40 1
01/13/202015:04
WG1409135
0.00500
10 1
01/13/202015:04
WG1409135
0.0100
0.50 1
01/13/202015:04
WG1409135
10.0-128
011131202015.04
WG1409135
10.0-127
011131202015.04
WG1409135
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
1,4-Dichlorobenzene
ND
0.100
7.50
1 01/13/2020 07:58
WG1409132
2,4-Dinitrotoluene
ND
0.100
0.13
1 01/13/2020 07:58
WG1409132
Hexachlorobenzene
ND
0.100
0.13
1 01/13/2020 07:58
WG1409132
Hexachloro-1,3-butadiene
ND
0.100
0.50
1 01/13/2020 07:58
WG1409132
Hexachloroethane
ND
0.100
3
1 01/13/2020 07:58
WG1409132
Nitrobenzene
ND
0.100
2
1 01/13/2020 07:58
WG1409132
Pyridine
ND
0.100
5
1 01/13/2020 07:58
WG1409132
3&4-Methyl Phenol
ND
0.100
400
1 01/13/2020 07:58
WG1409132
2-Methylphenol
ND
0.100
200
1 01/13/2020 07:58
WG1409132
Pentachlorophenol
ND
0.100
100
1 01/13/2020 07:58
WG1409132
2,4,5-Trichlorophenol
ND
0.100
400
1 01/13/2020 07:58
WG1409132
2,4,6-Trichlorophenol
ND
0.100
2
1 01/13/2020 07:58
WG1409132
(S) 2-Fluorophenol
48.3
10.0-120
0111312020 07.58
WG1409132
(S) Phenol-d5
32.4
10.0-120
0111312020 07.58
WG1409132
(S) Nitrobenzene-d5
74.0
10.0-127
0111312020 0758
WG1409132
(S) 2-Fluorobiphenyl
80.3
10.0-130
0111312020 0758
WG1409132
(S) 2,4,6-Tribromophenol
79.0
10.0-155
0111312020 0758
WG1409132
(S) p-Terphenyl-d14
84.4
10.0-128
0111312020 0758
WG1409132
ONE LAB. NATIONWIDE. *
Fp
Fc
FS
Fn
FA
Fc
F,
SAI
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources YANCEYVILLE L1177363 01/20/20 14:27 6 of 23

WG1410341 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9012 B L1177368-01
Method Blank (MB)
(MB) R3490744-1 01/14/20 13 45
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Reactive Cyanide U 0.0390 0.250
L1177368-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1177363-01 01/14/2013:49 • (DUP) R3490744-3 01/14/20 13 51
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %_
Reactive Cyanide ND 0.000 1 0.000 20
L1177903-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1177903-02 01/14/20 18:58 • (DUP) R3490744-6 01/14/20 18:59
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg
Reactive Cyanide ND 0.000 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3490744-2 01/14/20 18:46
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Reactive Cyanide 2.50 2.56 102
Rec. Limits LCS Qualifier
50.0-150
L1177903-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1177903-01 01/14/20 13 53 • (MS) R3490744-4 01/14/20 13 54 • (MSD) R3490744-5 01/14/20 13 55
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 1.67 ND 1.31 0.957 78.6 57.5 1 75.0-125 J3 J6 31.1 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources YANCEYVILLE L1177363 01/20/20 14:27 7 of 23

WG1410341 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9012 B L1177368-01
L1178351-13 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1173351-13 01/14/20 19:14 • (MS) R3490744-7 01/14/20 19:15 • (MSD) R3490744-8 01/14/20 1916
Spike Amount Original Result MS Result (dry) MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
(dry) (dry) (dry)
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 2.02 0.315 0.703 2.64 19.2 115 1 75.0-125 J6 J3 116
ONE LAB. NATIONWIDE. *
RPD Limits
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources YANCEYVILLE L1177363 01/20/20 14:27 3 of 23

WG1409180
Wet Chemistry by Method 9034-9030B
Method Blank (MB)
(MB) R3489923-1 01/11/201700
MB Result
Analyte mg/kg
Reactive Sulfide U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
7.63 25.0
L1176569-02 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1177368-01
(OS) L1176569-02 01/11/2017:00 • (DUP) R3439923-3 01/11/2017:00
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %_
Reactive Sulfide 44.7 45.5 1 1.85 20
Laboratory Control Sample (LCS)
(LCS) R3439923-2 01/11/20 17:00
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg
Reactive Sulfide 100 91.4 91.4 70.0-130
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG1409190 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9045D L1177368-01
Laboratory Control Sample (LCS)
(LCS) R3490750-1 01/14/20 20:00
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte su su
Corrosivity by pH 10.0 9.94 99.4 99.0-101
Sample Narrative:
LCS: 9.94 at 20C
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources YANCEYVILLE L1177363 01/20/20 14:27 10 of 23

WG1412116 QUALITY CONTROL SUMMARY
Wet Chemistry by Method D93/1010A L1177368-01
L1177848-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1177343-01 01/20/2010:15 • (DUP) R3492211-3 01/20/2010:15
Original Result DUP Result Dilution DUP RPD
Analyte Deg. F Deg. F
Ignitability 149 148 1 0.674
DUP Qualifier DUP RPD
Limits
i
10
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3492211-1 01/20/2010:15 • (LCSD) R3492211-2 01/20/201015
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte Deg.F Deg.F Deg.F
Ignitability 82.0 79.9 79.9 97.4 97.4 97.0-103 0.000 10
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG1408995 QUALITY CONTROL SUMMARY
Mercury by Method 7470A L1177368-01
Method Blank (MB)
(MB) R3490165-1 01/13/20 0925
MB Result MB Qualifier MB MDL
MB RDL
Analyte mg/I mg/I
mg/I
Mercury U 0.00330
0.0100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3490165-2 01/13/20 09:27 • (LCSD) R3490165-3 01/13/20 09:29
Spike Amount LCS Result LCSD Result
LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I
Mercury 0.0300 0.0300 0.0285
100 95.1 80.0-120 5.10 20
L1176194-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1176194-01 01/13/20 09:35 • (MS) R3490165-4 01/13/20 09:37 • (MSD) R3490165-5 01/13/20 09:39
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Mercury 0.0300
ND
0.0311
0.0290 104 96.5 1 75.0-125 6.99 20
L1177408-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1177403-01 01/13/20 09:41 • (MS) R3490165-6 01/13/20 09:43 • (MSD) R3490165-7 01/13/20 09:45
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Mercury 0.0300
ND
0.0307
0.0297 102 98.9 1 75.0-125 3.32 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources YANCEYVILLE L1177363 01/20/20 14:27 12 of 23

WG1409034
Metals (ICP) by Method 6010D
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1177368-01
(MB) R3490023-1 01/12/2015:00
MB Result
Analyte mg/I
MB Qualifier MB MDL
mg/I
MB RDL
mg/I
Arsenic 0.0600
J 0.0333
0.100
Barium U
0.0333
0.100
Cadmium U
0.0333
0.100
Chromium U
0.0333
0.100
Lead U
0.0333
0.100
Selenium U
0.0333
0.100
Silver U
0.0333
0.100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3490028-2 01/12/2015:02 • (LCSD) R3490028-3 01/12/2015:05
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/I
mg/I
mg/I
Arsenic
10.0
9.91
9.89
99.1
98.9
80.0-120
Barium
10.0
9.87
9.87
98.7
98.7
80.0-120
Cadmium
10.0
9.63
9.61
96.3
96.1
80.0-120
Chromium
10.0
9.36
9.37
93.6
93.7
80.0-120
Lead
10.0
9.80
9.80
98.0
98.0
80.0-120
Selenium
10.0
10.2
10.1
102
101
80.0-120
Silver
2.00
1.72
1.72
86.1
86.1
80.0-120
L1176194-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1176194-01 01/12/20 15:07 • (MS) R3490023-5 01/12/20 15:12 • (MSD) R3490023-6 01/12/20 1515
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
Arsenic
10.0
ND
9.40
9.51
94.0
95.1
Barium
10.0
ND
9.58
9.69
95.8
96.9
Cadmium
10.0
ND
9.43
9.54
94.3
95.4
Chromium
10.0
0.262
9.26
9.33
90.0
90.7
Lead
10.0
ND
8.81
8.88
88.1
88.8
Selenium
10.0
ND
9.69
9.83
96.9
98.3
Silver
2.00
ND
1.72
1.74
86.1
86.8
LCS Qualifier LCSD Qualifier RPD
RPD Limits
0.210
20
0.0250
20
0.241
20
0.0285
20
0.00270
20
0.495
20
0.00651
20
Dilution Rec. Limits
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
MS Qualifier MSD Qualifier RPD
1.15
1.20
1.19
0.687
0.790
1.46
0.770
ONE LAB. NATIONWIDE. *
RPD Limits
20
20
20
20
20
20
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources YANCEYVILLE L1177363 01/20/20 14:27 13 of 23

WG1409034 QUALITY CONTROL SUMMARY
Metals (ICP) by Method 6010D L1177368-01
L1178016-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1173016-01 01/12/201517 • (MS) R3490023-7 01/12/20 15:20 • (MSD) R3490023-8 01/12/20 15:22
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits MS Qualifier
Analyte
mg/I
mg/I
mg/I
mg/I
Arsenic
10.0
ND
10.1
10.0
101
100
1 75.0-125
Barium
10.0
ND
9.99
10.0
99.5
99.7
1 75.0-125
Cadmium
10.0
ND
9.69
9.72
96.9
97.2
1 75.0-125
Chromium
10.0
ND
9.45
9.48
94.5
94.8
1 75.0-125
Lead
10.0
0.333
10.2
10.2
98.7
98.8
1 75.0-125
Selenium
10.0
ND
10.3
10.2
103
102
1 75.0-125
Silver
2.00
ND
1.75
1.75
87.3
87.6
1 75.0-125
ONE LAB. NATIONWIDE. *
MSD Qualifier RPD
RPD Limits
0.664
20
0.157
20
0.282
20
0.302
20
0.153
20
0.965
20
0.310
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG1409088 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260D L1177368-01
Method Blank (MB)
(MB) R3490297-3 01/12/20 2150
MB Result MB Qualifier
Analyte
mg/I
Benzene
U
Carbon tetrachloride
U
Chlorobenzene
U
Chloroform
U
1,2-Dichloroethane
U
1,1-Dichloroethene
U
2-Butanone (MEK)
U
Tetrachloroethene
U
Trichloroethene
U
Vinyl chloride
U
(S) Toluene-dH
83.1
(S) 4-Bromofluorobenzene 89.6
(S) 1,2-Dichloroethane-d4 103
Laboratory Control Sample (LCS)
(LCS) R3490297-1 01/12/20 18:53
Spike Amount
LCS Result
Analyte
mg/I
mg/I
Benzene
0.250
0.250
Carbon tetrachloride
0.250
0.276
Chlorobenzene
0.250
0.226
Chloroform
0.250
0.260
1,2-Dichloroethane
0.250
0.334
1,1-Dichloroethene
0.250
0.232
2-Butanone (MEK)
1.25
1.91
Tetrachloroethene
0.250
0.207
Trichloroethene
0.250
0.259
Vinyl chloride
0.250
0.191
(S) Toluene-dH
(S) 4-Bromofluorobenzene
(S) 1,2-Dichloroethane-d4
MB MDL
mg/I
0.0167
0.0167
0.0167
0.0833
0.0167
0.0167
0.167
0.0167
0.0167
0.0167
LCS Rec
100
110
90.4
104
134
92.8
153
82.8
104
76.4
85.9
91.0
116
MB RDL
mg/I
0.0500
0.0500
0.0500
0.250
0.0500
0.0500
0.500
0.0500
0.0500
0.0500
80.0-120
77.0-126
70.0-130
Rec. Limits LCS Qualifier
70.0-123
68.0-126
80.0-121
73.0-120
70.0-128
71.0-124
44.0-160
72.0-132
78.0-124
67.0-131
80.0-120
77.0-126
70.0-130
J4
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources YANCEYVILLE L1177363 01/20/20 14:27 15 of 23

WG1409088 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1177368-01
ONE LAB. NATIONWIDE. *
L1177408-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1177403-01 01/13/20 02:06 • (MS) R3490297-4 01/13/20 03:05 • (MSD) R3490297-5 01/13/20 03:25
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
Benzene
0.250
ND
0.283
0.296
113
118
Carbon tetrachloride
0.250
ND
0.309
0.348
124
139
Chlorobenzene
0.250
ND
0.251
0.269
100
108
Chloroform
0.250
ND
0.285
0.315
114
126
1,2-Dichloroethane
0.250
ND
0.331
0.357
132
143
1,1-Dichloroethene
0.250
ND
0.300
0.333
120
133
2-Butanone (MEK)
1.25
ND
1.65
1.97
132
158
Tetrachloroethene
0.250
ND
0.237
0.272
94.8
109
Trichloroethene
0.250
ND
0.295
0.308
118
123
Vinyl chloride
0.250
ND
0.251
0.260
100
104
(S) Toluene-dH
87.8
87.8
(S) 4-Bromofluorobenzene
89.9
90.8
(S) 1,2-Dichloroethane-d4
ill
118
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 17.0-158
4.49
27
1 23.0-159
11.9
28
1 33.0-152
6.92
27
1 29.0-154
10.0
28
1 29.0-151
7.56
27
1 11.0-160
10.4
29
1 10.0-160
17.7
32
1 10.0-160
13.8
27
1 10.0-160
4.31
25
1 10.0-160
3.52
27
80.0-120
77.0-126
70.0-130
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG1411034
Chlorinated Acid Herbicides (GC) by Method 8151A
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1177368-01
(MB) R3491211-1 01/16/20 0100
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
2,4-D U
0.000667
0.00200
2,4,5-TP (Silvex) U
0.000667
0.00200
(S) Z4-Dichlorophenyl Acetic 65.2
14.0-158
Acid
Laboratory Control Sample (LCS)
(LCS) R3491211-2 01/16/20 0113
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
2,4-D 0.0500
0.0447
89.4
50.0-120
2,4,5-TP (Silvex) 0.0500
0.0435
87.0
50.0-125
(S) Z4-Dichlorophenyl Acetic
79.2
14. 0-158
Acid
L1176194-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1176194-01 01/16/20 0127 • (MS) R3491211-3 01/16/20 0141 • (MSD) R3491211-4 01/16/20 0155
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
2,4-D
0.0500
ND
0.0411
0.0436
82.2
87.2
2,4,5-TP (Silvex)
0.0500
ND
0.0353
0.0382
70.6
76.4
(S) Z4-Dichlorophenyl Acetic
63.4
65.0
Acid
Dilution Rec. Limits
1 50.0-120
1 50.0-125
14.0-158
ONE LAB. NATIONWIDE. *
MS Qualifier MSD Qualifier RPD RPD Limits
5.90 20
7.89 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG1409135
Pesticides (GC) by Method 8081B
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1177368-01
(MB) R3490334-1 01/13/201210
MB Result
Analyte mg/I
MB Qualifier MB MDL
mg/I
MB RDL
mg/I
Gamma BHC
U
0.00167
0.00500
Endrin
U
0.00167
0.00500
Heptachlor
U
0.00167
0.00500
Methoxychlor
U
0.00167
0.00500
Chlordane
U
0.00167
0.00500
Toxaphene
U
0.00333
0.0100
(S) Decachlorobiphenyl
96.3
10.0-128
(S) Tetrochloro-m-xylene
69.2
10.0-127
Laboratory Control Sample (LCS)
(LCS) R3490334-2 01/13/2012:22
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
Gamma BHC
0.0100
0.0101
101
55.0-129
Endrin
0.0100
0.00999
99.9
57.0-134
Heptachlor
0.0100
0.00997
99.7
27.0-132
Methoxychlor
0.0100
0.0113
113
54.0-155
(S) Decachlorobiphenyl
90.0
10.0-128
(S) Tetrochloro-m-xylene
75.4
10.0-127
L1177103-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1177103-01 01/13/20 13:24 • (MS) R3490334-3 01/13/20 13:37 • (MSD) R3490334-4 01/13/20 13:49
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mg/I
mg/I
mg/I
mg/I
Gamma BHC
0.0100
ND
0.00956
0.00979
95.6
97.9
1 14.0-141
Endrin
0.0100
ND
0.0102
0.0102
102
102
1 10.0-160
Heptachlor
0.0100
ND
0.00970
0.00967
97.0
96.7
1 16.0-136
Methoxychlor
0.0100
ND
0.0114
0.0116
114
116
1 10.0-160
(S) Decachlorobiphenyl
78.1
80.9
10.0-128
(S) Tetrochloro-m-xylene
69.1
69.0
10.0-127
ONE LAB. NATIONWIDE. *
MS Qualifier MSD Qualifier RPD RPD Limits
2.38 40
0.000 39
0.310 40
1.74 34
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources YANCEYVILLE L1177363 01/20/20 14:27 13 of 23

WG1409132 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1177368-01
Method Blank (MB)
(MB) R3490117-2 01/13/20 0042
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
U
0.0333
0.100
2,4-Dinitrotoluene
U
0.0333
0.100
Hexachlorobenzene
U
0.0333
0.100
Hexachloro-1,3-butadiene
U
0.0333
0.100
Hexachloroethane
U
0.0333
0.100
Nitrobenzene
U
0.0333
0.100
Pyridine
U
0.0333
0.100
2-Methylphenol
U
0.0333
0.100
3&4-Methyl Phenol
U
0.0333
0.100
Pentachlorophenol
U
0.0333
0.100
2,4,5-Trichlorophenol
U
0.0333
0.100
2,4,6-Trichlorophenol
U
0.0333
0.100
(S) Nitrobenzene-d5
67.0
10.0-127
(S) 2-Fluorobiphenyl
76.9
10.0-130
(S) p-Terphenyl-d14
76.0
10.0-128
(S) Phenol-d5
24.9
10.0-120
(S) 2-Fluorophenol
37.E
10.0-120
(S) 2,4,6-Tribromophenol
75.0
10.0-155
Laboratory Control Sample (LCS)
ONE LAB. NATIONWIDE. *
(LCS) R3490117-1 01/13/20 0020
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
1,4-Dichlorobenzene 0.500
0.310
62.0
18.0-120
2,4-Dinitrotoluene 0.500
0.433
86.6
49.0-124
Hexachlorobenzene 0.500
0.392
78.4
44.0-120
Hexachloro-1,3-butadiene 0.500
0.299
59.8
19.0-120
Hexachloroethane 0.500
0.281
56.2
15.0-120
Nitrobenzene 0.500
0.318
63.6
27.0-120
Pyridine 0.500
0.151
30.2
10.0-120
2-Methylphenol 0.500
0.266
53.2
28.0-120
3&4-Methyl Phenol 0.500
0.281
56.2
31.0-120
Pentachlorophenol 0.500
0.415
83.0
23.0-120
2,4,5-Trichlorophenol 0.500
0.408
81.6
44.0-120
2,4,6-Trichlorophenol 0.500
0.380
76.0
42.0-120
(S) Nitrobenzene-d5
54.5
10.0-127
(S) 2-Fluorobiphenyl
77.5
10.0-130
(S) p-Terphenyl-d14
75.2
10.0-128
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
YANCEYVILLE L1177368 01/20/20 14:27 19 of 23

WG1409132 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1177368-01
Laboratory Control Sample (LCS)
(LCS) R3490117-1 01/13/20 0020
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
(S) Phenol-d5 277 10.0-120
(S) 2-Fluorophenol 42.1 10.0-120
(S) 2,4,6-Tribromophenol 84.0 10.0-155
L1176194-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1176194-01 01/13/20 03:36 • (MS) R3490117-3 01/13/20 03:57 • (MSD) R3490117-4 01/13/20 0419
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
0.500
ND
0.180
0.304
36.0
60.8
2,4-Dinitrotoluene
0.500
ND
0.237
0.420
47.4
84.0
Hexachlorobenzene
0.500
ND
0.195
0.372
39.0
74.4
Hexachloro-1,3-butadiene
0.500
ND
0.223
0.308
44.6
61.6
Hexachloroethane
0.500
ND
0.196
0.293
39.2
58.6
Nitrobenzene
0.500
ND
0.197
0.312
39.4
62.4
Pyridine
0.500
ND
0.0755
0.162
15.1
32.4
2-Methylphenol
0.500
ND
0.181
0.272
36.2
54.4
3&4-Methyl Phenol
0.500
ND
0.196
0.291
39.2
58.2
Pentachlorophenol
0.500
ND
0.184
0.343
36.8
68.6
2,4,5-Trichlorophenol
0.500
ND
0.252
0.409
50.4
81.8
2,4,6-Trichlorophenol
0.500
ND
0.226
0.378
45.2
75.6
(S) Nitrobenzene-d5
34.6
54.6
(S) 2-Fluorobiphenyl
44.5
76.5
(S) p-Terphenyl-d14
38.8
73.4
(S) Phenol-d5
23.3
30.5
(S) 2-Fluorophenol
30.3
46.9
(S) 2,4,6-Tribromophenol
45.1
78.0
ONE LAB. NATIONWIDE. *
Dilution Rec. Limits
MS Qualifier MSD Qualifier
RPD
RPD Limits
1 17.0-120
J3
51.2
40
1 39.0-125
J3
55.7
25
1 35.0-122
J3
62.4
24
1 12.0-120
32.0
34
1 10.0-120
39.7
40
1 12.0-120
J3
45.2
30
1 10.0-120
J3
72.8
37
1 10.0-120
J3
40.2
30
1 10.0-120
J3
39.0
36
1 10.0-128
J3
60.3
37
1 33.0-120
J3
47.5
31
1 26.0-120
J3
50.3
31
10.0-127
10.0-130
10.0-128
10.0-120
10.0-120
10.0-155
ACCOUNT:
EMA Resources
PROJECT:
YANCEYVILLE
SDG: DATE/TIME:
L1177363 01/20/20 14:27
PAGE:
20 of 23

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
ONE LAB. NATIONWIDE. *
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
u
Fc
FS
(dry)
Results are reported based on the dry weight ofthe sample. [this will only be present on a dry report basis for soils].
MDL
Method Detection Limit.
Fn
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Fr
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Fc
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
F
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
Rc
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification ofthe analyte is acceptable, the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J6 The sample matrix interfered with the ability to make any accurate determination, spike value is low.
T8 Sample(s) received past/too close to holding time expiration.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources YANCEYVILLE L1177363 01/20/20 14:27 21 of 23

ACCREDITATIONS
& LOCATIONS
ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide
from one location. One phone call, one point of contact,
one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our
single location laboratory is comparable to the collective
totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory
campus. The model is conducive to accelerated
productivity, decreasing
Cp
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium
quality and prompt service allows us to be YOUR
LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace
National.
Fc
State Accreditations
Alabama 40660
Nebraska
NE-OS-15-05
FS
Alaska 17-026
Nevada
TN-03-2002-34
Arizona AZ0612
New Hampshire
2975
Arkansas 88-0469
New Jersey—NELAP
TNO02
Fn
California 2932
New Mexico
n/a
Colorado TN00003
New York
11742
Connecticut PH-0197
North Carolina
Env375
Fr
Florida E87487
North Carolina'
DW21704
Georgia NELAP
North Carolina 3
41
Georgia' 923
North Dakota
R-140
Fc
Idaho TN00003
Ohio—VAP
CL0069
Illinois 200008
Oklahoma
9915
7G1
Indiana C-TN-01 f
Oregon
TN200002
Iowa 364
Pennsylvania
68-02979
Kansas E-10277
Rhode Island
LA000356
Kentucky' 6 90010
South Carolina
84004
Kentucky 2 16
South Dakota
n/a
Louisiana A130792
Tennessee'"
2006
Louisiana' LA180010
Texas
T104704245-18-15
Rc
Maine TN0002
Texas 5
LABO152
Maryland 324
Utah
TN00003
Massachusetts M-TNO03
Vermont
VT2006
Michigan 9958
Virginia
460132
Minnesota 047-999-395
Washington
C847
Mississippi TN00003
West Virginia
233
Missouri 340
Wisconsin
9980939910
Montana CERT0086
Wyoming
A2 LA
Third Party Federal Accreditations
A2LA— ISO17025 1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5 1461.02
DOD
1461.01
Canada 1461.01
USDA
P330-15-00234
EPA—Crypto TN00003
' Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
MT ND
OR
ID SD
VWY
` NV T NE
T UT
CA co
KS
W o �AZ NM O�
T TX
AK
� . b
C,
fo • B HI 4 S
ACCOUNT: V PROJECT:
EMA Resources YANCEYVILLE
ME
MN
WVI NY
MI T
IA T PA 4
OH
Mo
IL Ihi
T T WV
VAT
KY
N * r�
AR
Ms AL GA
LA
FL
SDG: DATE/TIME: PAGE:
L1177363 01/20/20 14:27 22 of 23

EMA Resources
755 Yadkinville Road
Mocksville, NC 27028
Billing Information:
Mr. Brent Collins LPCrhk
755 Yadkinville Road
Mocksville, NC 27028b`°a`�
A
r Pr
;PrattvP
Chain of Custody Page T of
ceAnalytical
1206S Lebanon Rd �I❑
Mount Juliet, TN 37122 L7
Phone: 61S-7S8-S8S8
Phone: 800-767-SBS9
Fax: [phone] a
y
-
z
U
J
U
cc:
ai
o
J
U
F
I
y
Report to:
Mr. Brent Collins
Email To: [e-mail]
Project
Description: Sludge
Clty/State �'//pp
Collected: /It/dcC-Y I/t�El M`
Please Circl
PT MT CT
Phone: [phone]
Fax: [phone]
Client Project u
/f%1`<<( `f t��C L C
Lab Project u
SDG u `li 77-S 06,
Table l J086
I—
Acctnum: EMARES
Template:T11413
Prelogin: P748415
PM: 807 - Justin Carr
C, - r
;Shipped via: FedEX Standard
Qee'cte y (print -
`/ o�fiy�j�
Site Facility ID # /
��fCG`/vu (� W
P.O. 11
C011e ted b ign ure):
me ly
Packed on Ice fi _ Y
Sample ID
- —
P
Rush. (Lab MUST Be Notified) Quote #
Same Day _ Five Day
_ Next Day _ 5 Day (Rad Only) Date Results Needed T
Two Day _ 10 Day (Rad Only) I NO
_ Three Day I of
Comp/Grab Matrix ` Depth Date Time Intrs
- II
Remarks Sample t(IaD only)
�/�rICL-i�✓f�ll�
�
ss
/
/ It
�- �D p�'t
2
X
X
--G
pH Temp
Flow Other
• Matrix:Remarks:
SS - Soil AIR - Air F- Filter
GW- Groundwater B- Bioassay
WW - WasteW
DW- Drinki a r
OT - Oth I
Sample c
-Receipt
tcNP
COC Seal Present/Intact:•. ✓PR Y N
COC Signed/Accurate: /l _N
Bottles arrive intact: Y N
correct
Suffiicienttvolumetles ssent:
Ig Applica 1
VOA Zero Headspace: Y N
_ _
Preservation Correct/Checked: Y N
RAD Screen <0. 5 mR/hr: ✓iN
Samples re ned via:
UPS _ FedEx Courier
Tracking 11 �/ �%-� S
D v
Relin is �d by : Signature
ma „? Time:
i G
CoPwt
Received by: (Signature)
Trip Blank Received: Yes /
HCL / M H
TBR
RMq' uished by : (Signature)
Da4e: 7 Time:
Received by: (Signature)
Temp: -c Bottles Received-
In, 1�,1^
If preservation required by Login: Date/Time
Relinquished by : (Signature)
Date: Time:
Received for lab by: (Signature)
Date: Time:
Hold:
Condition:
NCF '

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Yanceyville WQ Permit Number: WQ0028547
WWTP Name:
Monitoring Period
Yanceyville WTP
NPDES Number: 02-17-010
From 1 / 1 /2020 To 12/3 l /2020
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
I Alt. C (Prior Testing)❑
Alt.D (No Prior Test)
I Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
=Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
JAIL (1) Fecal Density❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ 1
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring
data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number of
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -pique
Minimum
Geo. Mean
MaximumUnits
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1635
2440
3105
col/9
0
Annualy
G
SM9222D
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliforrn)
3 MPN per 4 grams
total solid (dry
I weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable)
1Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed v❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
William Shreve - Area Manager
Brent Collins; Director of Technical Services
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
1/7/2020
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Page 1
Contact: Brent Collins Report Date: 1/14/2020
Client: EMA Resources, Inc
7SS Yadkinville Road
Mocksville, NC 27028 Date Sample Rcvd: 1/7/2020
Meritech Work Order # 01072031 Sample: Y #1 Grab 1/7/20
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 4.20 % 1/7/20 0-100 % SM 2S40B
Fecal Coliform (Sludge) 1190S col/g dry wt 1/7/20 130 col/g dry wt SM 9222D
Meritech Work Order # 01072032 Sample: Y #2 Grab 1/7/20
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 4.24 % 1/7/20 0-100 % SM 2S40B
Fecal Coliform (Sludge) 21226 col/g drywt 1/7/20 130 col/g drywt SM 9222D
Meritech Work Order # 01072033 Sample: Y #3 Grab
Parameters
Result Analysis Date
1/7/20
ReportingLimit Method
% Total Solids 4.46 % 1/7/20 0-100 % SM 2S40B
Fecal Coliform (Sludge) 11211 col/g dry wt 1/7/20 130 col/g dry wt SM 9222D
Meritech Work Order # 01072034 Sample: Y #4 Grab 1/7/20
Parameters
Result
Analysis Date
Reporting Limit
Method
% Total Solids
4.23 %
1/7/20
0-100 %
SM 2S40B
Fecal Coliform (Sludge)
11820 col/g drywt
1/7/20
130 col/g drywt
SM 9222D
Meritech Work Order # 0107203S Sample: Y #S Grab
Parameters Result Analysis Date
% Total Solids 3.94 % 1/7/20
Fecal Coliform (Sludge) 15228 col/g dry wt 1/7/20
1/7/20
Reporting Limit Method
0-100 % SM 2S40B
130 col/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Meritech Work Order # 01072036 Sample: Y #6 Grab
Parameters Result Analysis Date
% Total Solids 4.48 % 1/7/20
Fecal Coliform (Sludge) 11161 col/g dry wt 1/7/20
Page 2
Report Date: 1/14/2020
Date Sample Rcvd: 1/7/2020
1/7/20
Reporting Limit Method
0-100 % SM 2540B
130 col/g dry wt SM 9222D
Meritech Work Order # 01072037 Sample: Y #7 Grab
Parameters Result Analysis Date Reporting Limit
% Total Solids 4.58 % 1/7/20 0-100 %
Fecal Coliform (Sludge) 10917 col/g dry wt 1/7/20 130 col/g dry wt
1/7/20
ethod
SM 2540B
SM 9222D
I hereby certify that I have reviewed and approve these data. f a � -� k)
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

5-9-2016 Chain of Custody Record (COC)
NPDES#:
Client: EMA Resources Inc. Phone:[phone]
Address:_ 755 Yadkinville Rd Fax: [phone]
Mocksville NC 27028 Email:
Project:
P.O.#:
Attention:_ Brent Collins Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply: StdJio days) 3�s z�S
pp y: (preferred) , Fax, Mail dal
L J
M E RITECH INC.
4
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
Sample Location and/or ID #
Sampling Dates & Times,
�_S°4na tfL-I-l—s int)� I I / I
�o A!� UUWfs�,Frle '�i�
Lab Use Only
Start
End
�
d6mp?
Grab?
#of
Cont.
Tests)
Required
on Ice?
Y / No
pH OK.
Cl OK?
Date
Time
Date
Time
Y#1
7/?0
5.4SU,,
C
�Ccol
Y #2
j
Y #3
I
}
Y #4
l
I
Y #5
Y #6
I I
Y #7
I �%
a��
v r
1
Temperature Upon
Receipt:
Method of
Shipment:
*** Dechlorination (1, Phenol and TKN samples must be done in the field prior to preservation. ***
0.5 p m) of AmmoniaCanide,
Comments:
Compositor #
❑ UPS
JJUg #
❑ Fed Ex
Are t�f4p rys/I f r regulatory purposes? Yes No ❑
Report resul s in: mg/L ❑ mg/kg CLI-- ug/L ❑
❑ Hand Delivery
Relinquishedb Date: Time:
v� ��j
Received b Date: Time:
v� � i-% 2d f , &40'I
❑ Other
Relinquished by: /%/� / Date/ 7_� Time:
v�j�
Received by: Date: Time:
Relinquished by: Date: Time:
'""
Lapp i �a/e1 T e::
L

Analytical Results
EMA Resources, Inc.
755 Yadkinville Rd.
Mocksville, NC 27028
Receive Date: 05/05/2020
Reported: 05/06/2020
For: Yanceyville
Comments:
STATESVILLE
C ANALYTICAL
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
200505-32-01
% Volatile Solids
Dig IN
0.14
%
SM2540G
05/05/2020
WC
200505-32-01
Percent Solids
Dig IN
0.19
%
SM2540B-2011
05/05/2020
WC
200505-32-02
% Volatile Solids
Dig OUT
1.39
%
SM2540G
05/05/2020
WC
200505-32-02
Percent Solids
Dig OUT
2.96
%
SM2540B-2011
05/05/2020
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 3

Volatile Solids IN 0.14
%Total Solids IN 0.19
Fractional Volatile Solids IN 0.737
Volatile Solids OUT 1.39
Total Solids OUT 2.96
Fractional Volatile Solids OUT 0.470
Volatile Solids
As a decimal
Volatile Solids In 0.737
Volatile Solids Out 0.470
Volatile Solids Reduction 1 68.4

Condition of Receipt
Sample Number 200505-32-01 Temp on Arrival:
Parameter Schedule: Percent Solids
Parameter Schedule:
Sample Number 200505-32-02 Temp on Arrival:
Parameter Schedule:
Received on Ice
Received on Ice
Received on Ice
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 3

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name:
WWTP Name:
Town of Yanceyville
Yanceyville WTP
WQ Permit Number: WQ0028547
NPDES Number: 02-17-010
Monitoring Period: From l/l/2020 To 12/31/2020
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑
Alt. C (Prior Testing)❑
Alt.D (No Prior Test)
I Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density❑ I
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring
data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g y
um er of
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -pique
fMinimum
Geo. Meanmaximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
193
196
198
col/g
0
Annualy
G
SM9222D
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
colifonn)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑Alt.
4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
William Shreve - Area Manager Brent Collins; Director of Technical Services
Preparer Name and Title (type or print) Land Applier Name and Title(ifapplicable)(type or print)
1/7/2020
Signature of Preparer* _ Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Page 1
Contact: Brent Collins
Report Date:
1/14/2020
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Date Sample Rcvd:
1/7/2020
Meritech Work Order # 01072038 Sample: YW #1 Grab
1/7/20
Parameters
Result Analysis Date
Reporting Limit
Method
% Total Solids
3.53 % 1/7/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<258 col/g dry wt 1/7/20
258 col/g dry wt
SM 9222D
Meritech Work Order # 01072039 Sample: YW#2 Grab
1/7/20
Parameters
Result Analysis Date
Reporting Limit
Method
% Total Solids
3.52 % 1/7/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<258 col/g dry wt 1/7/20
258 col/g dry wt
SM 9222D
Meritech Work Order #
01072040 Sample: YW #3 Grab
1/7/20
Parameters
Result Analysis Date
Reporting Limit
Method
% Total Solids
3.57 % 1/7/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<255 col/g dry wt 1/7/20
255 col/g dry wt
SM 9222D
Meritech Work Order #
01072041 Sample: YW #4 Grab
1/7/20
Parameters
Result Analysis Date
Reporting Limit
Method
% Total Solids
3.40 % 1/7/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<267 col/g dry wt 1/7/20
267 col/g dry wt
SM 9222D
Meritech Work Order #
01072042 Sample: YW #5 Grab
1/7/20
Parameters
Result Analysis Date
Reporting -Limit
Method
% Total Solids
3.61 % 1/7/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<252 col/g dry wt 1/7/20
252 col/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Meritech Work Order # 01072043 Sample: YW #6 Grab
Parameters Result Anal Date
% Total Solids 3.54 % 1/7/20
Fecal Coliform (Sludge) <257 col/g dry wt 1/7/20
Meritech Work Order # 01072044 Sample: YW #7 Grab
Parameters Result Analysis Date
% Total Solids 3.54 % 1/7/20
Fecal Coliform (Sludge) <257 col/g dry wt 1/7/20
Page 2
Report Date: 1/14/2020
Date Sample Rcvd: 1/7/2020
1/7/20
Reporting Limit Method
0-100 % SM 2540B
257 col/g dry wt SM 9222D
1/7/20
Reporting Limit Method
0-100 % SM 2540B
257 col/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data. J
Laboratory Relfresentative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

5-92016 Chain of Custody Record (COC)
NPDES#:_ - -
Client:EMA Resources Inc. Phone:_ 336-751-1441
Address:— 755 Yadkinville Rd Fax: [phone] —
Mocksville NC 27028 Email: Brent.collins(@emaresourcesinc.com
Project:
P.O.#:
Attention:_ Brent Collins Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
s� Slodays) 3s Za�asHrs
Circle all that appl • Email referred), Fax, Mail
ME RITECH INC.
1 \
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
WWW.merltechlabS.COm
Sample Location and/or ID #
Dates &Times
Per akig_(Si not:
7�Sampling c_
i LAnDuW Gt/asrXKcma]
Lab Use Only
Start
End
60p ,
Grab?
#of
cont.
Test
(s) Required
On Ice?
Cep / No
pH OK?
Cl OK?
Date
Time
Date
Time
YW#1
YW #2
YW #3
iT
IU
............................ 7
YW #4
YW #5
J
YW#6
+
YW #7
Temperature Upon
Receipt:
Method of
Shipment:
*** Dechlorination <0.5 22211 of Ammonia Cyanide, Phenol and TKN samples must be done in the field prior to preservation. ***
Comments:
Compositor #
[� UPS
Jug #
Fed Ex
Are thesVes is/or/�eg/atory purposes? Yes No ❑
Report resins in: g/L ❑ mg/kg ug/L ❑
n Y
Hand Deliver
Relinquished by: - �- v .t4�� Date: / Time:
`
Received by: /L /� _ n /_ /►/ Date:��� Time:
o r rlj/ —f�f 6 T/�/�'•
❑ Other
Relinquished by: a` Date: p T'y Time: jej , /.
J
Received by: Date: Time:
�
eived by L j/4-- tO ! TI ;
Relinquished by: Date: Time:

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY21-SL005465
�5' �141..tiL
Client: Jennifer Hodges
Advisor: Brent Collins
Predictive
2388 Allison Rd
EMA Resources Inc
;•
Pelham, NC 27311
755 Yadkinville Rd
f'. Soil Report Mehlich-3 Extraction
+_
Mocksville, NC27028
Sampled County : Caswell
Links to Helpful Information
Client ID: 309118
Advisor ID: 405413
Sampled: 09/11/2020 Received: 09/22/2020 Completed: 10/01/2020
Farm: C509
Sample ID: 0011
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg S Mn Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0
120-200 40
10 0 0 0 0
0 0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.18 1.04 5.8 83 1.0 5.9 40 70
60 17
100 203 139 65 65
87 0.1 2
Noah 0' olina
i
I Awl'
Futacii frum fuWCurnml5skm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY21-SL005466
�5' �141..tiL
Client: Bonnie Crispin
Advisor: Brent Collins
Predictive
6116 Blanch Rd
EMA Resources Inc
;•
Blanch, NC 27212
755 Yadkinville Rd
f'. Soil Report Mehlich-3 Extraction
+_
Mocksville, NC27028
Sampled County : Caswell
Links to Helpful Information
Client ID: 475625
Advisor ID: 405413
Sampled: 09/11/2020 Received: 09/22/2020 Completed: 10/01/2020
Farm: C582
Sample ID: 00004
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg S Mn Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0
120-200 130
100 0 0 0 0
0 0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.32 1.10 5.5 83 0.9 6.1 8 21
57 24
34 2132 1295 40 40
56 0.1 2
Noah 0' olina
i
I Awl'
fotciW frum fuWCurnml5skm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture