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Home My WebLink AboutWQ0006594_Residual Annual Report 2020_20210208Initial Review Reviewer Thornburg, Nathaniel Is this submittal an application? (Excluding additional information.)* r Yes r No If not an application what is the submittal type?* r Annual Report r Residual Annual Report r Additional Information r Other Annual Report Year* 2020 Permit Number (IR)* W00006594 Applicant/Permittee Unifi Manufacturing, Inc Email Notifications Does this need review by the hydrogeologist?* 0 Yes r No Regional Office Winston-Salem CO Reviewer Admin Reviewer Submittal Form Project Contact Information Rease provide inforration on the person to be contacted by N B Staff Name * Brent Collins Email Address* brent.collins@emaresourcesinc.com electronic subnittal, confirmation of receipt, and other correspondence. Project Information ........ ......... ....................................................................................................................... Application/Document Type* r New (Fee Req ui red) r Modification - Major (Fee Required) r Renewal with Major Modification (Fee Required) r Annual Report r Additional Information r Other Phone Number* 3363993646 O Modification - Minor C Renewal C GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 r Residual Annual Report r Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* r Wastewater Irrigation r High -Rate Infiltration r Other Wastewater r Reclaimed Water r Closed -Loop Recycle r Residuals r Single -Family Residence Wastewater r Other Irrigation Permit Number:* W00006594 Fbs Current Existing permt number Applicant/Permittee Address* PO Box 1437, Reidsville, NC 27323 Facility Name * Unifi Manufacturing DCAR Please provide comments/notes on your current submittal below. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form Engineering Rans, Specifications, Calculations, Bc.) 2020 Unifi Annual Report - WQ0006594.pdf 4.09MB Upload only 1 FDF docurrent (less than 250 fvB). NLRiple documents rust be contained into one FDF file unless file is larger than upload limit. * V By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature ff &kgw Submission Date 2/8/2021 February 8, 2021 DENR/Water Quality Section Non -Discharge Compliance Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: 2020 Annual Report — Unifi, Incorporated Treatment and Land Application of Residuals Permit No. WQ0006594 Dear Sir or Madam: Enclosed is one copy of the 2020 Annual Report for the above referenced land application permit. During 2020 EMA Resources, Inc. land applied 408.64 dry tons of wastewater residuals to 233.16 acres of private farmland. Please contact Brent Collins - Director of Technical Services if you have any further questions regarding this report. Sincerely, Z�fz G;2� Brent Collins Director of Technical Services brent.collins(cr,,emaresourcesinc.com Phone 336.751.1441 — Fax 336975191442 755 Yadkinville Rd — Mocksville, NC 27028 CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM WQ PERMIT#: WQ0006594 FACILITY NAME: Uniti, Incorporated PHONE: COUNTY: Rockingham OPERATOR: Unit, Inc. FACILITY TYPE (please check one): i] Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) ❑ Distribution and Marketing (complete Paris A, B, and C) Wac thr farility in aneration during the nast calendar year? Yes 21 No ❑ —► If No shin parts A, IS, C and certify form below Part A*: Part B*• Month Sources(s) (include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) January February March April May June July August September October November December Total from FORM DMSDF (sup) 0 408.64 408.64 408.64 Totals: I Annual (dry tons): 0 408,64 408.64 408.64 Amendments usedj Bulking A ent(s) used: * If more space is required, attach additional information sheets (FORM DMSDF (supp)): Part C: Total Number of Form DMSDF (Supp)l 1 Facility was compliant during the past calendar year with all conditions of the land application permit 21 Yes (including but not limited to items 1-3 below) issued by the Division of Water Quality: © No PP If No, Explain in Narritive 1. All monitoring was done in accordance with the pen nit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." �Ldh 62 Oy 2j Signature of Permittee Date **Preparer is defined in 40 CPR Part 503.9(r) and ISA NCAC 2T .1 l02 (26) Signature of Preparer** (if different from Pennittee) Date DENR FORM DMSDF (1212006) CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM Supplemental Information WQ PERMIT #: WQ0006594 FACILITY NAME: Unifi, Incorporated PHONE: COUNTY: Rockingham OPERATOR: Unifi, Inc. FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only) ❑ Distribution and Marketing (complete Parts A, and B) Part A*: Part B*: Month Sources(s) (include NPDES 1i if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) April Unifi Inc. Plant No. 2 Reidsville 18.73 18.73 James Blackwell 18.73 Soil Amendment April Unifi Inc. Plant No. 2 Reidsville 59.33 59.33 Glenn Hodges 59.33 Soil Amendment April Unifi Inc. Plant No. 2 Reidsville 27.06 27.06 Jennifer Hodges 27.06 Soil Amendment April Unifi Inc. Plant No. 2 Reidsville 37.47 37.47 Gordon Hodges 37.47 Soil Amendment July Unifi Inc. Plant No. 2 Reidsville 111.37 111.37 Ronnie Marshall 111.37 Soil Amendment September Unifi Inc. Plant No. 2 Reidsville 64.1 64.1 Ronnie Marshall 64.1 Soil Amendment October Unifi Inc. Plant No. 2 Reidsville 90.58 90.58 Ronnie Marshall 90.58 Soil Amendment Totals: Annual (dry tons): 0 408.64 408.64 408.64 Amendment(s) used: I Bulking Agent(s) used: * If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)l I DENR FORM DMSDF (Supp) (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0006594 Facility Name: Unifi, Incorporated Residual Source WQ # or NPDES #: WWTP Name: Residual Analvsis Data M-0I04 Unifi, Inc. Plant No.2 Reidsville Laboratory: 1) Waypoint Analytical 2) 3) 4) 5) Parameter (mg/kg) Cone. Limit (mg/kg)a Sample or Com osite Date 4/9/20 10/12/20 11/3/20 12/1/20 Percent Solids (%) NA 3.84 t.68 1.67 1.63 Arsenic 75 11 14.1 14.1 14.1 Cadmium 85 t.3 1.18 1.18 1.18 Copper. 4,300 175 170 I22 218 Chromium NA 54.7 57.5 37.3 70 Lead 840 64.7 78.8 53.5 91.2 Mercury 57 0.811 0.776 0.19 0.688 Molybdenum 75 3.42 9.29 7.94 7.94 Nickel 420 16.2 16.9 15.10 22.3 Selenium 100 12.9 18.8 18.8 18.8 Zinc 7,500 716 682 460 818 Total Phosphorus NA 4320 38 t0 2620 4490 TKN NA 18700 12100 22200 15200 Ammonia -Nitrogen NA 8470 5560 1960 5550 Nitrate and Nitrite NA 132 4990 5410 2990 ' For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant �pen tes for s�itfing information, including the possibility of fines and imprisonment for knowing violations." t'Jllt d Signature of Preparer * Da e *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (1212006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - S Report all sampling analysis results for parameters not listed in FORM RSS€' that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQ0006594 Facility Name: tJnifi, Incorporated Residual Source NPDES fi or WQl#: WWTP Name: Residual Analvsis Data M-0104 Unifi, Inc. Plant No.2 Reidsville Laboratory: 1) Waypoint Analytical 2) 3) 4) 5) Sample or Composite Date Parameter (mg/kg) 4/9/20 10/12/20 11/3/20 12/l/20 Aluminum 15100 I2100 8470 14200 Calcium 20800 23500 16800 28200 Magnesium 11000 12100 9470 14100 PH 7.7 8.2 7.6 7.9 Potassium 2300 2840 2800 3170 Sodium 15300 34500 39400 37200 PAN 7436 9732 12462 8660 SAR 4.17 5.88 7.76 3.74 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure at qualified personnel properly gathered and evaluated the information submitted. I am aware that there are signif ,, nnnt��penaltie for submitting false information, including the possibilityoftines and imprisonment for knowing violations." �.�f Q - Signature of Preparer * Date *Preparer is defined in 40 CFR Part 5039(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF - B (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Unifi, Inc Total Dry Tons Applied (Annual): 90.68 Permit #: WQ0006594 Cation Exchange Capacity (non 503 only): Operator: James Blackwell Owner: James Blackwell Predominant Soil Series: FbB2 Acres Used: 26.6 Acres Permitted: 26.6 Site #: CS06 Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 0.31 3.10 Arsenic 0.007 0.050 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.057 Cadmium 0.001 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Copper 0.110 2.074 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.184 Chromiuni 0.034 0.321 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.355 Lead 0.041 0.289 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.330 Mercury 0.001 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Molyb- 0.002 0.057 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.059 denum Nickel 0.010 0.391 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.401 Selenium 0.008 0.050 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.058 Zinc 0.448 13.669 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 14.117 Total Phos- 2.704 124.614 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 127.318 horus "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 1/28/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: Operator: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Unifi, Inc WQ Permit #: WQ0006594 Field #: 2 Acres Utilized: James Blackwell Annual Dry Tons Applied: 90.68 Site #: CS06 Acres Permitted: James Blackwell Crop 1 Name: Fescue -Pasture Predominant Soil Series: Crop 1 Max. PAN: 141 FbB2 Crop 2 Name: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 26.6 26.6 0 O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 11rs. inches a F '5 w * o o' 7� * N o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4/10 52000 3.84 0.313 Unifi, Inc. Dry <.5" S 0.5 0.3 18700 8470 132 4.655 NA Fescue 0.000 0.000 0.000 8/12 65000 6.33 0.645 Northside WWTP Dry <.5" S 0.5 0.3 39050 8187.5 188.98 17.469 NA Fescue 8/13 247000 6.33 2.451 Northside WWTP Dry <.5" S 0.5 0.3 39050 8187.5 188.98 66.382 NA Fescue 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 1 88.507 0.00o Lime Applied Annuallbs/acre 0.057 0.011 2.184 0.355 0.330 0.008 0.059 0.401 0.058 14.117 127.3181 0 14.117 1 2498 Date lbs/ac Prior Years Cumulative lbs/ac 0 0 0 0 0 0 0 0 0 Current Cumulative lbs/ac 0.057 0.011 2.184 0.355 0.330 0.008 0.059 0.401 0.058 Permitted C. P. L. R. * * * * 36 34 1 1338 267 15 374 1 89 Permit PAN Limit 1 st/2nd Crop 1 141 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/28/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Unifi, Inc Total Dry Tons Applied (Annual): 10.40 Permit #: WQ0006594 Cation Exchange Capacity (non 503 only): Operator: James Blackwell Owner: James Blackwell Predominant Soil Series: FbB2 Acres Used: 12.72 Acres Permitted: 12.72 Site #: CS06 Field #: 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 0.82 Arsenic 0.018 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.018 Cadmium 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Copper 0.286 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.286 Chromiuni 0.089 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.089 Lead 0.106 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.106 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 denum Nickel 0.027 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.027 Selenium 0.021 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.021 Zinc 1.171 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.171 Total Phos- 7.068 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 7.068 horus "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 1/28/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: Operator: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Unifi, Inc WQ Permit #: WQ0006594 Field #: 5 Acres Utilized: James Blackwell Annual Dry Tons Applied: 10.40 Site #: CS06 Acres Permitted: James Blackwell Crop 1 Name: Fescue -Pasture Predominant Soil Series: Crop 1 Max. PAN: 141 FbB2 Crop 2 Name: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 12.72 12.72 0 O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 11rs. inches a F '5 w * o o' 7� * N o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4/10 65000 3.84 0.818 Unifi, Inc. Dry <.5" S 0.5 0.3 18700 8470 132 12.169 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 0 6500o As Cd Cu Cr Pb Hg Mo Ni Se Zn P 12.169 o.000 Lime Applied Annuallbs/acre 0.018 0.002 0.286 0.089 0.106 0.001 0.006 0.027 0.021 1.171 7.068 0 0 0 0 0 0 0 0 0 0 0.018 0.002 0.286 0.089 0.106 0.001 0.006 0.027 0.021 1.171 36 34 1 1338 267 15 374 1 89 1 2498 1 141 Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R. * * * * Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/28/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Unifi, Inc. Total Dry Tons Applied (Annual): 87.06 Permit #: WQ0006594 Cation Exchange Capacity (non 503 only): Operator: Glenn Hodges Owner: Glenn Hodges Predominant Soil Series: CgB2 Acres Used: 37 Acres Permitted: 37 Site #: CS09 Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 0.59 1.76 Arsenic 0.013 0.028 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.041 Cadmium 0.002 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 Copper 0.207 1.181 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.387 Chromiuni 0.065 0.183 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.247 Lead 0.076 0.165 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.241 Mercury 0.001 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Molyb- 0.004 0.032 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.036 denum Nickel 0.019 0.223 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.242 Selenium 0.015 0.028 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.043 Zinc 0.846 7.779 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 8.626 Total Phos- 5.106 70.921 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 76.027 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fZ4;��_ Signature of Land Applier 1/11/2020 Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Unifi, Inc. Glenn Hodges Operator: Glenn Hodges Crop 1 Name: Fescue -Pasture WQ Permit #: WQ0006594 Field #: Annual Dry Tons Applied: 87.06 Site #: Predominant Soil Series: Cg132 Crop 1 Max. PAN: 156 Crop 2 Name: Acres Utilized: 37 CS09 Acres Permitted: 37 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches F '5 w * o o' 7� * N o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4/8 136500 3.84 0.591 Unifi, Inc. Dry <.5" S 0.5 0.3 18700 8470 132 8.786 NA Fescue 0.000 0.000 0.000 7/21 195000 6.33 1.391 Northside WWTP Dry <.5" S 0.5 0.3 39050 8187.5 188.98 37.676 NA Fescue 7/22 52000 6.33 0.371 Northside WWTP Dry <.5" S 0.5 0.3 39050 8187.5 188.98 10.047 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 0 3s35oo As Cd Cu Cr Pb Hg, Mo Ni Se Zn P 56.509 0.00o Lime Applied Annuallbs/acre 0.041 0.007 1.387 0.247 0.241 0.005 0.036 0.242 0.043 8.626 76.027 0 8.626 1 2498 Date lbs/ac Prior Years Cumulative lbs/ac 0 0 0 0 0 0 0 0 0 Current Cumulative lbs/ac 0.041 0.007 1.387 0.247 0.241 0.005 0.036 0.242 0.043 Permitted C. P. L. R. * * * * 1 36 34 1 1338 267 15 374 89 Permit PAN Limit 1 st/2nd Crop 1 156 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/28/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Unifi, Inc. Total Dry Tons Applied (Annual): Permit #: WQ0006594 Cation Exchange Capacity (non 503 only): Operator: Glenn Hodges Owner: Glenn Hodges Predominant Soil Series: Acres Used: 18.4 Acres Permitted: 18.4 Site #: CS09 Field #: 37.46 FpD 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 2.04 Arsenic 0.045 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.045 Cadmium 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Copper 0.713 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.713 Chromiuni 0.223 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.223 Lead 0.263 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.263 Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 denum Nickel 0.066 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.066 Selenium 0.053 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.053 Zinc 2.916 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.916 Total Phos- 17.591 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 17.591 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fZ4;��_ Signature of Land Applier 1/28/2021 Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Unifi, Inc. Glenn Hodges Operator: Glenn Hodges Crop 1 Name: Fescue -Pasture WQ Permit #: WQ0006594 Field #: Annual Dry Tons Applied: 37.46 Site #: Predominant Soil Series: FpD Crop 1 Max. PAN: 118 Crop 2 Name: Acres Utilized: 18.4 CS09 Acres Permitted: 18.4 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches F '5 w * o o' 7� * N * w o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4/7 195000 3.84 1.697 Unifi, Inc. Dry <.5" S 0.5 0.3 18700 8470 132 25.238 NA Fescue 4/8 39000 3.84 0.339 Unifi, Inc. Dry <.5" S 0.5 0.3 18700 8470 132 5.048 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 01 234000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 30.285 FO.000 Lime Applied Annuallbs/acre 0.045 0.005 0.713 0.223 0.263 0.003 0.014 0.066 0.053 2.916 17.591 0 0 0 0 0 0 0 0 0 0 0.045 0.005 0.713 0.223 0.263 0.003 0.014 0.066 0.053 2.916 36 1 34 1338 1 267 15 1 374 1 89 1 2498 1 118 Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R. * * * * Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/28/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Unifi, Inc. Total Dry Tons Applied (Annual): 92.26 Permit #: WQ0006594 Cation Exchange Capacity (non 503 only): Operator: Glenn Hodges Owner: Jennifer Hodges Predominant Soil Series: FbB2 Acres Used: 38 Acres Permitted: 38 Site #: CS09 Field #: 11 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 0.71 1.72 Arsenic 0.016 0.051 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.067 Cadmium 0.002 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Copper 0.249 0.638 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.888 Chromiuni 0.078 0.023 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.101 Lead 0.092 0.028 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.121 Mercury 0.001 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- 0.005 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.021 denum Nickel 0.023 0.020 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.043 Selenium 0.018 0.060 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.078 Zinc 1.020 0.302 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.321 Total Phos- 6.152 0.652 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 6.804 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 1/28/2021 Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: Operator: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Unifi, Inc. WQ Permit #: WQ0006594 Field #: 11 Acres Utilized: Jennifer Hodges Annual Dry Tons Applied: 92.26 Site #: CS09 Acres Permitted: Glenn Hodges Crop 1 Name: Fescue -Pasture Predominant Soil Series: Crop 1 Max. PAN: 145 FbB2 Crop 2 Name: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 38 38 0 O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches a F '5L C) w * o o' * N o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4/10 169000 3.84 0.712 Unifi,Inc. Dry <.5" S 0.5 0.3 18700 8470 132 10.591 NA Fescue 0.000 0.000 0.000 5/4 110500 3.76 0.456 Yancey WTP D <.5" S 0.5 0.3 9460 3960 177 3.471 NA Fescue 5/5 78000 3.76 0.322 Yancey WTP D <.5" S 0.5 0.3 9460 3960 177 2.450 NA Fescue 5/7 1 156000 1 3.76 0.644 Yancey WTP D <.5" S 0.5 0.3 9460 3960 177 4.901 NA Fescue 5/8 71500 3.76 0.295 Yancey WTP D <.5" S 0.5 0.3 9460 3960 177 2.246 NA Fescue 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: o SsS000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 23.660 F 0. 000 Lime Applied Annuallbs/acre 0.067 0.008 0.888 0.101 0.121 0.002 0.021 0.043 0.078 1.321 6.804 1 0 1.321 1 2498 Date lbs/ac Prior Years Cumulative lbs/ac 0 0 0 0 0 0 0 0 0 Current Cumulative lbs/ac 0.067 0.008 0.888 0.101 0.121 0.002 0.021 0.043 0.078 Permitted C. P. L. R. * * * * 1 36 34 1 1338 1 267 1 15 374 1 89 Permit PAN Limit 1 st/2nd Crop 1 1 145 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 4/�j� *Application Method: S - Surface, IN - Injection, INC - Incorporation ��''-- 1/28/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Unifi, Inc. Total Dry Tons Applied (Annual): Permit #: WQ0006594 Cation Exchange Capacity (non 503 only): Operator: Glenn Hodges Owner: Gordon Hodges Predominant Soil Series: Acres Used: 16.75 Acres Permitted: 16.75 Site #: CS15 Field #: 37.47 FbB2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 2.24 Arsenic 0.049 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.049 Cadmium 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Copper 0.783 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.783 Chromium 0.245 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.245 Lead 0.289 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.289 Mercury 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- 0.015 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.015 denum Nickel 0.072 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.072 Selenium 0.058 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.058 Zinc 3.203 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.203 Total Phos- 19.328 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 19.328 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fZ4;��_ Signature of Land Applier 1/28/2021 Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: Operator: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Unifi, Inc. WQ Permit #: WQ0006594 Field #: 1 Acres Utilized: Gordon Hodges Annual Dry Tons Applied: 37.47 Site #: CS 15 Acres Permitted: Glenn Hodges Crop 1 Name: Fescue -Pasture Predominant Soil Series: Crop 1 Max. PAN: 141 FbB2 Crop 2 Name: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 16.75 16.75 0 O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches a F '5 w * o o' 7� * N * w o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4/7 195000 3.84 1.864 Unifi, Inc. Dry <.5" S 0.5 0.3 18700 8470 132 27.724 NA Fescue 4/8 39000 3.84 0.373 Unifi, Inc. Dry <.5" S 0.5 0.3 18700 8470 132 5.545 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 0 23400o As Cd Cu Cr Pb Hg Mo Ni Se Zn P 33.269 0.00o Lime Applied Annuallbs/acre 0.049 0.006 0.783 0.245 0.289 0.004 0.015 0.072 0.058 3.203 19.328 0 3.203 1 2498 Date lbs/ac Prior Years Cumulative lbs/ac 0 0 0 0 0 0 0 0 0 Current Cumulative lbs/ac 0.049 0.006 0.783 0.245 0.289 0.004 0.015 0.072 0.058 Permitted C. P. L. R. * * * * 1 36 34 1 1338 267 1 15 374 1 89 Permit PAN Limit 1 st/2nd Crop 1 1 141 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/28/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Unifi, Inc. Total Dry Tons Applied (Annual): Permit #: WQ0006594 Cation Exchange Capacity (non 503 only): Operator: Ronnie Marshall Owner: Ronnie Marshall Predominant Soil Series: Acres Used: 69 Acres Permitted: 69 Site #: RC001 Field #: 404.00 CgB2 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 2.83 3.03 Arsenic 0.062 0.064 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.126 Cadmium 0.007 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.010 Copper 0.991 1.125 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.116 Chromiuni 0.310 0.287 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.597 Lead 0.366 0.125 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.491 Mercury 0.005 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Molyb- 0.019 0.019 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.038 denum Nickel 0.092 0.126 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.218 Selenium 0.073 0.044 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.117 Zinc 4.053 0.315 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.367 Total Phos- 24.451 8.954 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 33.405 horus "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 1/28/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Unifi, Inc. Ronnie Marshall Operator: Ronnie Marshall Crop 1 Name: Fescue -Hay WQ Permit #: WQ0006594 Field #: Annual Dry Tons Applied: 404.00 Site #: Predominant Soil Series: Cg132 Crop 1 Max. PAN: 209 Crop 2 Name: Acres Utilized: 69 RC001 Acres Permitted: 69 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches F '5 w * o o' 7� * N o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 7/6 58500 3.84 0.136 Unifi Inc. Dry <.5" S 0.5 1 0.3 18700 8470 132 2.019 NA Fescue 7/7 240500 3.84 0.558 Unifi Inc. Dry <.5" S 0.5 0.3 18700 8470 132 8.300 NA Fescue 7/8 253500 3.84 0.588 Unifi Inc. Dry <.5" S 0.5 0.3 18700 8470 132 8.749 NA Fescue 7/9 143000 3.84 0.332 Unifi Inc. Dry <.5" S 0.5 0.3 18700 8470 132 4.935 NA Fescue 9/16 1 130000 3.84 0.302 Unifi Inc. Dry <.5" S 0.5 0.3 1 18700 8470 1 132 4.487 NA Fescue 9/21 39000 3.84 0.091 Unifi Inc. Dry <.5" S 0.5 0.3 18700 8470 132 1.346 NA Fescue 9/22 84500 3.84 0.196 Unifi Inc. Dry <.5" S 0.5 0.3 18700 8470 132 2.916 NA Fescue 9/23 147000 3.84 0.341 Unifi Inc. Dry <.5" S 0.5 0.3 18700 8470 132 5.073 NA Fescue 10/5 123500 3.84 0.287 Unifi Inc. Dry <.5" S 0.5 0.3 18700 8470 132 4.262 NA Fescue 0.000 1 1 1 0.000 0.000 8/24 78000 4.4 0.207 Reidsville WTP Dry <.5" S 0.5 0.3 6070 3410 975 1.443 NA Fescue 8/25 117000 4.4 0.311 Reidsville WTP DrV <.5" S 0.5 0.3 1 6070 1 3410 975 2.164 NA Fescue 0 942500 2.506 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 17.433 0.000 TOTALS: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 63.129 o.000 Lime Applied Annuallbs/acre 0.126 0.010 2.116 0.597 0.491 0.005 0.038 0.218 0.117 4.367 33.405 0 0 0 0 0 0 0 0 0 0 0.126 0.010 2.116 0.597 0.491 0.005 0.038 0.218 0.117 4.367 36 34 1 1338 267 15 374 1 89 1 2498 209 Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R. * * * * Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 4��j/ *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/28/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM Supplemental Information PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Unifi, Inc. WQ Permit #: WQ0006594 Field #: 5 Acres Utilized: 69 Land Owner: Ronnie Marshall Annual Dry Tons Applied: 403.995 Site #: RC001 Acres Permitted: 69 Operator: Ronnie Marshall Predominant Soil Series: CgB2 Cation Exchange Capacity (non 503): Crop 1 Name: Fescue -Hay Crop 1 Max. PAN: 209 Crop 2 Name: Crop 2 Max PAN: o Q Volume applied (enter one) Cu. Yds Gallons 156000 o /o Solids 4.4 Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. D (Dry, e ' Moist) preci p. Past 24 Hrs. inches � w * C o 7 w * ?j ; t, TKN mg/kg Z o 5 o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of CropType yp ReceivingResidual Application Crop 1 Crop 2 Crop 1 Crop 2 8/26 0.415 Reidsville WTP Dry <.5" S 0.5 0.3 6070 3410 975 2.886 NA Fescue 8/27 136500 4.4 0.363 Reidsville WTP Dry <.5" S 0.5 0.3 6070 3410 975 2.525 NA Fescue 8/28 130000 4.4 0.346 Reidsville WTP Dry <.5" S 0.5 0.3 6070 3410 975 2.405 NA Fescue 8/31 13000 4.4 0.035 Reidsville WTP Dry <.5" S 0.5 0.3 6070 3410 975 0.240 NA Fescue 9/8 117000 4.4 0.311 Reidsville WTP Dry <.5" S 0.5 0.3 6070 3410 975 2.164 NA Fescue 9/9 84500 4.4 0.225 Reidsville WTP Dry <.5" S 0.5 0.3 6070 3410 975 1.563 NA Fescue 9/10 156000 4.4 0.415 Reidsville WTP Dry <.5" S 0.5 0.3 6070 3410 975 2.886 NA Fescue 9/11 149500 4.4 0.398 Reidsville WTP Dry <.5" S 0.5 0.3 6070 3410 975 2.765 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 TOTALS: 0 942500 2.506 17.4331 0.000 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/28/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date ***C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (SUPP) (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Unifi, Inc. Total Dry Tons Applied (Annual): 70.78 Permit #: WQ0006594 Cation Exchange Capacity (non 503 only): Operator: Ronnie Marshall Owner: Ronnie Marshall Predominant Soil Series: CgB2 Acres Used: 14.69 Acres Permitted: 14.69 Site #: RC001 Field #: 6 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phonis Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 LOJ 11 12 DT/Ac./ App. Event 4.82 Arsenic 0.106 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.106 Cadmium 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013 Copper 1.686 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.686 Chromiuni 0.527 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.527 Lead 0.623 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.623 Mercury 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Molyb- 0.033 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.033 denum Nickel 0.156 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.156 Selenium 0.124 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.124 Zinc 6.899 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 6.899 Total Phos- 41.628 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 41.628 horus "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�fz 1/28/2021 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Unifi, Inc. Ronnie Marshall Operator: Ronnie Marshall Crop 1 Name: Fescue -Hay WQ Permit #: WQ0006594 Field #: Annual Dry Tons Applied: 70.78 Site #: Predominant Soil Series: Cg132 Crop 1 Max. PAN: 209 Crop 2 Name: Acres Utilized: 14.69 RC001 Acres Permitted: 14.69 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 0 O N Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches F '5 w * o o' 7� * N * w o TKN mg/kg o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 10/5 123500 3.84 1.346 Unifi Inc. Dry <.5" S 0.5 1 0.3 18700 8470 132 20.021 NA Fescue 10/6 91000 3.84 0.992 Unifi Inc. Dry <.5" S 0.5 0.3 18700 8470 132 14.752 NA Fescue 10/7 71500 3.84 0.779 Unifi Inc. Dry <.5" S 0.5 0.3 18700 8470 132 11.591 NA Fescue 10/8 78000 3.84 0.850 Unifi Inc. Dry <.5" S 0.5 0.3 18700 8470 132 12.645 NA Fescue 10/9 1 78000 3.84 0.850 Unifi Inc. Dry <.5" S 0.5 0.3 1 18700 8470 1 132 12.645 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: o200o As Cd Cu Cr Pb Hg Mo Ni Se Zn P 71.653 0.000 Lime Applied Annuallbs/acre 0.106 0.013 1.686 0.527 0.623 0.008 0.033 0.156 0.124 6.899 41.628 0 6.899 1 2498 Date lbs/ac Prior Years Cumulative lbs/ac 0 0 0 0 0 0 0 0 0 Current Cumulative lbs/ac 0.106 0.013 1.686 0.527 0.623 0.008 0.033 0.156 0.124 Permitted C. P. L. R. * * * * 1 36 34 1 1338 267 1 15 374 1 89 Permit PAN Limit 1 st/2nd Crop 1 209 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 4��j/ *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/28/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) Waypointo ANALYTICAL 4/21 /2020 EMA Resources Inc Brent Collins 755 Yadkinville Rd Mocksville, NC, 27028 Ref: Analytical Testing Lab Report Number: 20-101-0029 Client Project Description: Reidsville, NC 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Dear Brent Collins: Waypoint Analytical, LLC. received sample(s) on 4/10/2020 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Danyale Love Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Ijp, Page 1 of 7 Waypointo ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 2/28/2021 Arizona State Program AZ0816 8/30/2020 Arkansas State Program 88-0650 2/7/2021 California State Program 2904 5/10/2020 Georgia State Program C044 2/18/2023 Georgia State Program 04015 6/30/2020 Illinois State Program - NELAP 200078 10/10/2020 Kentucky State Program 80215 6/30/2020 Kentucky State Program KY90047 12/31/2020 Louisiana State Program - NELAP 04015 6/30/2020 Mississippi State Program MS 5/10/2020 North Carolina State Program 415 12/31/2020 Oklahoma State Program 9311 8/31/2020 Pennsylvania State Program - NELAP 68-03195 5/31/2020 South Carolina State Program 84002 5/10/2020 South Carolina State Program 84002 6/30/2020 Tennessee State Program 02027 2/11/2023 Tennessee A21LA ISO 17025:2017 4313.01 10/31/2021 Texas State Program - NELAP T104704180 9/30/2020 Virginia State Program - NELAP 460181 9/14/2020 Washington State Program C1018 7/31/2020 Page 1 of 1 00001/20-101-0029 Page 2 of 7 Waypoint ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Sample Summary Table Report Number: 20-101-0029 Client Project Description: Reidsville, NC Lab No Client Sample ID Matrix Date Collected Date Received 87923 Unif. Solids 04/09/202010:30 04/10/2020 Page 3 of 7 WayP �'��' 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 ANALYTICAL www.waypointanalyiical.com 46245 EMA Resources Inc Brent Collins Project Reidsville, NC Report Date : 04/21/2020 755 Yadkinville Rd Information : Received : 04/10/2020 Mocksville , NC 27028 Q�ln Report Number : 20-101-0029 REPORT OFANALYSIS Danyale Love Project Manager Lab No : 87923 Matrix: Solids Sample ID : Unif. Sampled: 4/9/2020 10:30 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Moisture 96.2 % 1 04/13/2016:06 JDT SW-DRYWT Ammonia Nitrogen 8470 mg/Kg - dry 658 1 04/20/20 12:00 JPJ 4500NH3C-2011 Nitrate+Nitrite-N <132 mg/Kg - dry 132 132 1 04/16/20 14:10 ZBD 4500NO3F-2011 Organic N 10260 mg/Kg - dry 26.32 1316 1 04/20/20 12:00 CALCULATION pH 7.7 S.U. 1 04/21/20 05:09 JSL 9045D Total Solids 3.84 % 0.010 0.010 1 04/14/20 16:59 ADM 2540G-2011 Total Kjeldahl Nitrogen 18700 mg/Kg - dry 26.3 1320 1 04/21/20 16:20 CLP 4500NORGD-2011 Phosphorus 4320 mg/Kg - dry 67.6 132 1 04/13/20 17:34 TJS 6010D Aluminum 15100 mg/Kg - dry 53.4 132 1 04/13/20 17:34 TJS 6010D Arsenic <11.0 mg/Kg - dry 11.0 13.2 1 04/13/20 17:34 TJS 6010D Cadmium <1.30 mg/Kg - dry 1.30 2.63 1 04/13/20 17:34 TJS 6010D Calcium 20800 mg/Kg - dry 442 658 1 04/13/20 17:34 TJS 6010D Chromium 54.7 mg/Kg - dry 5.00 6.58 1 04/13/20 17:34 TJS 6010D Copper 175 mg/Kg - dry 3.82 6.58 1 04/13/20 17:34 TJS 6010D Iron 4740 mg/Kg - dry 112 132 1 04/13/20 17:34 TJS 6010D Lead 64.7 mg/Kg - dry 3.92 7.89 1 04/13/20 17:34 TJS 6010D Magnesium 11000 mg/Kg - dry 58.4 132 1 04/13/20 17:34 TJS 6010D Manganese 165 mg/Kg - dry 4.82 13.2 1 04/13/20 17:34 TJS 6010D Mercury 0.811 mg/Kg - dry 0.0876 0.397 1 04/13/20 11:48 DDB 7471A Molybdenum <3.42 mg/Kg - dry 3.42 6.58 1 04/13/20 17:34 TJS 6010D Nickel 16.2 mg/Kg - dry 4.34 6.58 1 04/13/20 17:34 TJS 6010D Potassium 2300 mg/Kg - dry 78.4 132 1 04/13/20 17:34 TJS 6010D Selenium <12.9 mg/Kg - dry 12.9 13.2 1 04/13/20 17:34 TJS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 4 of 7 waypANALYTICAL 46245 EMA Resources Inc Brent Collins 755 Yadkinville Rd Mocksville , NC 27028 Report Number : 20-101-0029 Lab No : 87923 Sample ID : Unif. 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Project Reidsville, NC Information : REPORT OFANALYSIS Report Date : 04/21/2020 Received : 04/10/2020 Danyale Love Project Manager Matrix: Solids Sampled: 4/9/2020 10:30 Test Results Units MDL MQL DF Date / Time Analyzed By Analytical Method Sodium 15300 mg/Kg - dry 203 658 1 04/13/20 17:34 TJS 6010D Zinc 716 mg/Kg - dry 28.4 32.9 1 04/13/20 17:34 TJS 6010D Sulfur 7340 mg/Kg - dry 129 132 1 04/13/20 17:34 TJS 6010D Sodium Absorption Ratio 4.1 Ratio 2.2 5.0 1 04/13/20 17:34 CALCULATION Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit L Limit Exceeded Page 5 of 7 s WayPAoi nt ..(2) �79p Whitten Road,3.240 Memphis, TN 38133 21.2440 Main 901.213.240fl °Fax 901.213.2440 N A LYT I C A L www.waypointanalytical.com Shipment Receipt Form Customer Number: 46245 Customer Name: EMA Resources Inc Report Number: 20-101-0029 Shipping Method ® Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: t45 Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers/boxes received F-71 Custody seals intact on shipping container/cooler? 0 Yes 0 No ! Not Present Custody seals intact on sample bottles? 0 Yes 0 No ® Not Present Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No ® N/A Water - VOA vials free of headspace 0 Yes 0 No ® N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes ® No Comments: Signature: ICarleen Qualls Date & Time: 04/10/2020 10:38:16 Page 6 of 7 Client Name/Address Client Project Manager/Contact Billing Information For Laboratory Use Only EMA Resources tnc Brent Collins Account ##46245 755 Yadkinviile Rd Mocksville, NC 27028 Project Description Project/Site Location (City/State) RUSH — Additional charges apply Method of Shipment Matrix Key special Detection Limits) Fte aFed Ex �USPS WW —Wastewater GW — Groundwater II Ge dsv i f I 'NL Results Needed eUPS I—t Courier Client Drop Off L� OW — Drinking Water 5—Sail/Solid O — Oil P - Product M - Misc Other Project Number Project Manager Phone u Project Manager Email Purchase Order Number Site/Facility ID fi 336-399-3646 brent.collins@emaresources.com lJn,-f'i. Z V) A Cool < 16C NaZS203 (Micro Only) '►`�J` ~ ♦o -E - B Cool �= 6C ^ T p C H2SO4p�H<2 ■ ■aypVint ANALYTICAL ra b Y o o C C � O ❑ ❑ None Required E NaCIH pH>lo 2790 Whitten Road w �j U7 a F HNO3 pHt2 Memphis, I N 38133 Unless noted, all containers CE Z � > � G kCL pH<2 {901} 213-24[)0 per Table li of 40 CFR Part a`+ E x m Q H H3PO4 pH<2 I Cool <= 6C NA25203 135. 3 z ` e.? Date Time Sample Identification Required Analysis / Preservative Comments/Notes `t19 /O._n j;n;�, � C t. V Meta Is:A1,As, Ca, Cd,Cr,Cu,Fe, Pb Mn, Mg, Mo, Hg, N i,Se, Na, P,S. K, Zn 0 II�I� II�I� �Ilu IIII � IIlI�i 1��! II��II Efl�ll III! IN�1I�I�1I11� 4 zv2v9 0.38 00 Reidsville, NC Sampled by (Name — Print) &e't t //�ll' A5 � Client Remarks/Comments Sludge -Samples - Report Dry Weight For Laboratory Use Only Ice Custody Seals Lab Comments N 0 y � ) Relin 'shed by: (Sl ATURE) Date Time Received by: (SIGNATURE) Date Time /_ -,.- � zlp�� y/i 3.IQ7.n ' Blank/ oler em - Relinquished by: (SIGNATURE) Date Time Received by: {SIGNATURE} Date Time L{I i 49 Relinquished by: (SIGNATURE) Date Time IT WeC Date Time r VyIGNATURE) {� — Waypointo ANALYTICAL 10/23/2020 EMA Resources Inc Brent Collins 755 Yadkinville Rd Mocksville, NC, 27028 Ref: Analytical Testing Lab Report Number: 20-287-0056 Client Project Description: Reidsville, NC 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Dear Brent Collins: Waypoint Analytical, LLC. received sample(s) on 10/13/2020 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Danyale Love Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Ijp, Page 1 of 7 Waypointo ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2021 Arkansas State Program 88-0650 02/07/2021 California State Program 2904 06/30/2021 Florida State Program - NELAP E871157 06/30/2021 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2021 Illinois State Program - NELAP 200078 10/10/2021 Kentucky State Program 80215 06/30/2021 Kentucky State Program KY90047 12/31/2020 Louisiana State Program - NELAP LA037 12/31/2020 Louisiana State Program - NELAP 04015 06/30/2021 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2020 Oklahoma State Program 9311 08/31/2021 Pennsylvania State Program - NELAP 68-03195 05/31/2021 South Carolina State Program 84002 06/30/2021 South Carolina State Program 84002 06/30/2021 Tennessee State Program 02027 02/11/2023 Tennessee A21LA ISO 17025:2017 4313.01 10/31/2021 Texas State Program - NELAP T104704180 09/30/2021 Virginia State Program 00106 06/30/2021 Virginia State Program - NELAP 460181 09/14/2021 Page 1 of 1 00001/20-287-0056 Page 2 of 7 Waypoint ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Sample Summary Table Report Number: 20-287-0056 Client Project Description: Reidsville, NC Lab No Client Sample ID Matrix Date Collected Date Received 89244 Unif: Solids 10/12/2020 08:30 10/13/2020 Page 3 of 7 Waypointo ANALYTICAL 46245 EMA Resources Inc Brent Collins 755 Yadkinville Rd Mocksville , NC 27028 Report Number : 20-287-0056 Lab No : 89244 Sample ID : Unif: Project Reidsville, NC Information : 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com REPORT OFANALYSIS Report Date : 10/23/2020 Received : 10/13/2020 Danyale Love Project Manager Matrix: Solids Sampled: 10/12/2020 8:30 Test Results Units MDL MQL DF Date / Time Analyzed By Analytical Method Moisture 98.3 % 1 10/19/2017:30 FMM SW-DRYWT Ammonia Nitrogen 5560 mg/Kg - dry 1470 1470 1 10/21/20 14:00 JPJ 4500NH3C-2011 Nitrate+Nitrite-N 4990 mg/Kg - dry 284 284 1 10/14/20 14:56 ZBD 4500NO3F-2011 Organic N 6553 mg/Kg - dry 2941 1 10/21/20 14:00 CALCULATION pH 8.2 S.U. 1 10/15/2015:10 ADM 9045D Total Solids 1.68 % 0.010 0.010 1 10/19/20 17:07 FMM 2540G-2011 Total Volatile Solids 67.6 % 0.010 0.010 1 10/19/20 17:07 FMM 2540G-2011 Total Kjeldahl Nitrogen 12100 mg/Kg - dry 2940 1 10/22/20 16:39 CLP 4500NORGD-2011 Phosphorus 3810 mg/Kg - dry 162 294 1 10/16/20 18:24 DADS 6010D Aluminum 12100 mg/Kg - dry 272 294 1 10/16/20 04:11 DADS 6010D Arsenic <14.1 mg/Kg - dry 14.1 29.4 1 10/16/20 04:11 DADS 6010D Cadmium <1.18 mg/Kg - dry 1.18 5.88 1 10/16/20 04:11 DADS 6010D Calcium 23500 mg/Kg - dry 2280 2940 1 10/16/20 18:24 DADS 6010D Chromium 57.5 mg/Kg - dry 13.9 14.7 1 10/16/20 04:11 DADS 6010D Copper 170 mg/Kg - dry 18.2 29.4 1 10/16/20 04:11 DADS 6010D Iron 5550 mg/Kg - dry 501 588 1 10/16/20 04:11 DADS 6010D Lead 78.8 mg/Kg - dry 10.6 17.6 1 10/16/20 18:24 DADS 6010D Magnesium 12100 mg/Kg - dry 152 294 1 10/16/20 04:11 DADS 6010D Manganese 179 mg/Kg - dry 19.1 29.4 1 10/16/20 04:11 DADS 6010D Mercury 0.7763 mg/Kg - dry 0.192 0.871 1 10/15/20 13:08 DDB 7471A Molybdenum 9.293 mg/Kg - dry 7.94 14.7 1 10/16/20 04:11 DADS 6010D Nickel 16.9 mg/Kg - dry 7.06 14.7 1 10/16/20 04:11 DADS 6010D Potassium 2840 mg/Kg - dry 364 588 1 10/16/20 04:11 DADS 6010D Qualifiers/ DF Dilution Factor J Estimated value Definitions L Limit Exceeded MQL Method Quantitation Limit Page 4 of 7 • Waypoint 27090 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 ANALYTICAL www.waypointanalyiical.com 46245 EMA Resources Inc Project Reidsville, NC Brent Collins Report Date : 10/23/2020 755 Yadkinville Rd Information : Received : 10/13/2020 Mocksville , NC 27028 Danyale Love Report Number : 20-287-0056 REPORT OFANALYSIS Project Manager Lab No : 89244 Matrix: Solids Sample ID : Unif: Sampled: 10/12/2020 8:30 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Selenium <18.8 mg/Kg - dry 18.8 29.4 1 10/16/20 04:11 DADS 6010D Sodium 34500 mg/Kg - dry 765 1470 1 10/16/20 04:11 DADS 6010D Zinc 682 mg/Kg - dry 47.6 73.5 1 10/16/20 04:11 DADS 6010D Sulfur 9530 mg/Kg - dry 305 588 1 10/16/20 18:24 DADS 6010D Sodium Absorption Ratio 5.93 Ratio 0.01 0.01 1 10/16/20 04:11 CALCULATION Qualifiers/ DF Dilution Factor Definitions J Estimated value Page 5 of 7 s WayPAoi nt ..(2) �79p Whitten Road,3.240 Memphis, TN 38133 21.2440 Main 901.213.240fl °Fax 901.213.2440 N A LYT I C A L www.waypointanalytical.com Shipment Receipt Form Customer Number: 46245 Customer Name: EMA Resources Inc Report Number: 20-287-0056 Shipping Method ® Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: T101 Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers/boxes received F-71 Custody seals intact on shipping container/cooler? 0 Yes 0 No ! Not Present Custody seals intact on sample bottles? 0 Yes 0 No ® Not Present Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No ® N/A Water - VOA vials free of headspace 0 Yes 0 No ® N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes ® No Comments: Signature: IMakayla Weaver Date & Time: 10/13/2020 11:06:33 Page 6 of 7 Client Name/Address Client Project Manager/Contact aching Information For Laboratory Use Only EMA Resources Inc Brent Collins Account #46245 755 Yadkinville Rd Mocksville, NC 27028 Project oescriptlon Project/Site Location (Clty/State) - Additional charges apply Methed or Shi ment Matrix Key IdSvcil�-Urr HRUSH Special Detection LimitW al4d E. UPS �USPS WW - Wa�ewater GW -Groundwater ((;� ��'t' Date Results Needed El [Hurter Client Dtop Off DW-DrifLidng Water 5 - Sod /Solid O - Oil P•Product M - Mist Other Project Number Project Manager Phone p Project Manager Email Purchase Order Number Site/Facility ID q 336-399-3646 brent.coilins@emaresources.com ��;�; U&S, r E A Coo€� LOC Noa52O1 (Mitre Only) waypoint r u 0 E lu -Q g Cool <= 6C 1) equi ANALYTICAL � `a SL a c Ca S � E � ❑ ❑ (n tl atone Required None E N20HPH>10 _2790 Whitten Road Unless noted, all r,ontainers o 4 C N M Q -@ co CO U F HNQ3 pHK2 r HCL pH<2 Memphis, TN 38133 c 4-> lSrC1!} �13-LSL10 P er Table II of 40 CFR Part E r n ` a)w z ❑ ti it3P0a pH�a I Coal <= tiC NA25203 136, 7 x Date Time Sam le Identification Re aired Anal sts / Preservative L/ Comments/Notes Metals.Al,As,Ca,Cd,Cr,Cu,T-e,F'b JcJrx 8:321 t)n;.L: } 44W C V, >% M n, Mg, Mo, Hg. Ni,Se, Na, R S. K,Zn 11111lid1II I111 iH1IN11111111I1 Gz43-z02o EMA Resources Inc 11:06 13 Reidsville. NC For Laboratory Use Only Sampled by (Name - Print) Iern �!n Client Remarks/Comments Sludge Samples - Report Dry Weight Ice Custody Seals Lab Comments ReIInquf k,y: I NATURE} pate Time Received by: (SIGNATURE) Date 7lmr y y /C r J.3go� Blan osier mp Relinquished by: (SIGNATURE) Date Time Received by: (SIGNATURE) Date Time t7L Relinquished by: (SIGNATURE) Date Time ei by: (S Date TimeM Waypointo ANALYTICAL 11 /12/2020 EMA Resources Inc Brent Collins 755 Yadkinville Rd Mocksville, NC, 27028 Ref: Analytical Testing Lab Report Number: 20-310-0140 Client Project Description: Reidsville, NC 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Dear Brent Collins: Waypoint Analytical, LLC. received sample(s) on 11/5/2020 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Danyale Love Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Ijp, Page 1 of 9 Waypointo ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2021 Arkansas State Program 88-0650 02/07/2021 California State Program 2904 06/30/2021 Florida State Program - NELAP E871157 06/30/2021 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2021 Illinois State Program - NELAP 200078 10/10/2021 Kentucky State Program 80215 06/30/2021 Kentucky State Program KY90047 12/31/2020 Louisiana State Program - NELAP LA037 12/31/2020 Louisiana State Program - NELAP 04015 06/30/2021 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2020 Oklahoma State Program 9311 08/31/2021 Pennsylvania State Program - NELAP 68-03195 05/31/2021 South Carolina State Program 84002 06/30/2021 South Carolina State Program 84002 06/30/2021 Tennessee State Program 02027 02/11/2023 Tennessee A21LA ISO 17025:2017 4313.01 10/31/2021 Texas State Program - NELAP T104704180 09/30/2021 Virginia State Program 00106 06/30/2021 Virginia State Program - NELAP 460181 09/14/2021 Page 1 of 1 00001/20-310-0140 Page 2 of 9 Waypoint ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Sample Summary Table Report Number: 20-310-0140 Client Project Description: Reidsville, NC Lab No Client Sample ID Matrix Date Collected Date Received 96466 Unifi Solids 11/03/2020 08:30 11/05/2020 Page 3 of 9 Waypointo ANALYTICAL Client: EMA Resources Inc Project: Reidsville, NC Lab Report Number: 20-310-0140 Date: 11 /12/2020 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 fax 901.213.2440 www.waypointanalytical.com CASE NARRATIVE Metals Analysis Method 601 OD Analyte: Aluminum QC Batch No: L521196 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Copper QC Batch No: L521196 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Copper QC Batch No: L521789 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Iron QC Batch No: L521196 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Iron QC Batch No: L521789 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Potassium QC Batch No: L521196 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Potassium QC Batch No: L521789 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Sodium QC Batch No: L521196 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Phosphorus QC Batch No: L521196 Page 4 of 9 Waypoint".0 ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 fax 901.213.2440 www.waypointanalytical.com The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Lead QC Batch No: L521196 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Sulfur QC Batch No: L521196 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Selenium QC Batch No: L521196 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Selenium QC Batch No: L521789 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Zinc QC Batch No: L521196 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 5 of 9 Waypointo ANALYTICAL 46245 EMA Resources Inc Brent Collins 755 Yadkinville Rd Mocksville , NC 27028 Report Number : 20-310-0140 Lab No : 96466 Sample ID : Unifi Project Reidsville, NC Information : 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com REPORT OFANALYSIS Report Date : 11/12/2020 Received : 11/05/2020 Danyale Love Project Manager Matrix: Solids Sampled: 11/3/2020 8:30 Test Results Units MDL MQL DF Date / Time Analyzed By Analytical Method Moisture 98.3 % 0.010 1 11/09/20 17:05 FMM SW-DRYWT Ammonia Nitrogen 1960 mg/Kg - dry 1470 1470 1 11/12/20 14:30 JPJ 4500NH3C-2011 Nitrate+Nitrite-N 5410 mg/Kg - dry 278 278 1 11/12/20 15:45 CLP 4500NO3F-2011 Organic N 20220 mg/Kg - dry 1471 1471 1 11/10/20 17:09 CALCULATION pH 7.6 S.U. 1 11/09/2016:44 ADM 9045D Total Solids 1.67 % 0.010 0.010 1 11/09/20 17:05 FMM 2540G-2011 Total Volatile Solids 67.9 % 0.010 0.010 1 11/09/20 17:05 FMM 2540G-2011 Total Kjeldahl Nitrogen 22200 mg/Kg - dry 2940 1 11/10/20 17:09 CLP 4500NORGD-2011 Phosphorus 2620 mg/Kg - dry 162 294 1 11/10/20 01:28 DADS 6010D Aluminum 8470 mg/Kg - dry 272 294 1 11/10/20 01:28 DADS 6010D Arsenic <14.1 mg/Kg - dry 14.1 29.4 1 11/10/20 01:28 DADS 6010D Cadmium <1.18 mg/Kg - dry 1.18 5.88 1 11/10/20 01:28 DADS 6010D Calcium 16800 mg/Kg - dry 2280 2940 1 11/10/20 01:28 DADS 6010D Chromium 37.3 mg/Kg - dry 13.9 14.7 1 11/10/20 01:28 DADS 6010D Copper 122 mg/Kg - dry 18.2 29.4 1 11/11/20 22:12 TJS 6010D Iron 3760 mg/Kg - dry 501 588 1 11/10/20 01:28 DADS 6010D Lead 53.5 mg/Kg - dry 10.6 17.6 1 11/10/20 01:28 DADS 6010D Magnesium 9470 mg/Kg - dry 152 294 1 11/10/20 01:28 DADS 6010D Manganese 135 mg/Kg - dry 19.1 29.4 1 11/10/20 01:28 DADS 6010D Mercury <0.191 mg/Kg - dry 0.191 0.865 1 11/12/20 11:00 DDB 7471A Molybdenum <7.94 mg/Kg - dry 7.94 14.7 1 11/10/20 01:28 DADS 6010D Nickel 15.1 mg/Kg - dry 7.06 14.7 1 11/10/20 01:28 DADS 6010D Potassium 2800 mg/Kg - dry 364 588 1 11/11/20 22:12 TJS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 6 of 9 • Waypoint 27090 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 ANALYTICAL www.waypointanalyiical.com 46245 EMA Resources Inc Project Reidsville, NC Brent Collins Report Date : 11/12/2020 755 Yadkinville Rd Information : Received : 11/05/2020 Mocksville , NC 27028 Danyale Love Report Number : 20-310-0140 REPORT OFANALYSIS Project Manager Lab No : 96466 Matrix: Solids Sample ID : Unifi Sampled: 11/3/2020 8:30 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Selenium <18.8 mg/Kg - dry 18.8 29.4 1 11/11/20 22:12 TJS 6010D Sodium 39400 mg/Kg - dry 765 1470 1 11/11/20 22:12 TJS 6010D Zinc 460 mg/Kg - dry 47.6 73.5 1 11/10/20 01:28 JADS 6010D Sulfur 9820 mg/Kg - dry 305 588 1 11/10/20 01:28 JADS 6010D Sodium Absorption Ratio 7.83 Ratio 0.01 0.01 1 11/10/20 01:28 CALCULATION Qualifiers/ DF Dilution Factor Definitions L Limit Exceeded Page 7 of 9 s WayPAoi nt ..(2) �79p Whitten Road,3.240 Memphis, TN 38133 21.2440 Main 901.213.240fl °Fax 901.213.2440 N A LYT I C A L www.waypointanalytical.com Shipment Receipt Form Customer Number: 46245 Customer Name: EMA Resources Inc Report Number: 20-310-0140 Shipping Method ® Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: T99 Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers/boxes received F-71 Custody seals intact on shipping container/cooler? 0 Yes 0 No ! Not Present Custody seals intact on sample bottles? 0 Yes 0 No ® Not Present Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No ® N/A Water - VOA vials free of headspace 0 Yes 0 No ® N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes ® No Comments: Signature: IMakayla Weaver Date & Time: 11/05/2020 18:28:01 Page 8 of 9 Client Name/Address Client Project Manager/Contact Billing Information Resourcees Inc Brent Collins Account #46245 0-31 -01AO 7EMA 55 �111111111111I1111I�N1lllllllti1111111111lilt 1$1H111111111 11-05-2020 MpckSville, NC 27D28 18.27 37 cMA Resources I+,c: Met d of Sh Reidsville. NC Project Description Project/Site Location (City/State) RUSH - Additional charges apply Special Detection Limits] Id Ex s D� d5� If IN Date Results Needed j� Courier rl lL JJ P Product M - Misc Other Project Number Project Manager Phone p Project Manager Email Purchase Order Number Site/Facility ID # 336-399-3646 brent.collins@emaresources com on., 4 ; Z W A Cool < 10C Na25I03 (Micro Only) r 6 Cool <= 5C WayWaypoint CD C point. Y Q � � 0 Q NoneH2SOeqq it O NuneRe aired ANALYTICAL O S E p Q rrnn vl r UJ E NaOH PI 279U LNhillen Road Unless o M V J F 'NO3 pH�2 G HCL pH<2 Memphis, TN 3A133 noted, all containers m `E o Z (9I11) 213-2900 per Table Il CFR Para £ y m Fes-- .`� Z r 1 LJ H H3PO4 I p 3 Cool <= 6C NA25203 135. 3 , 3 z l7 Date Time Sample Identification Required Analysis / Preservative Comments/Notes >f ,I Metals:Al,As,Ca,Cd,Cr,Cu,Pe,Pb M n, Mg, Mo, Hg , N i , Se, Na , P, S , K, Zn For Laboratory Use Only Sampled by (Name - Print) Client Remarks/Comments Sludge Samples - Report Dry Weight Ice Custody LabCvmments / N Se als 15'-'1 611-1s Retinq hed by, IGNATURE) Date Time Received by: (SIGNATURE) Date Time + Y ( CN J ► /:3-5-30?/77 Blank/ oeler T Relinquished by: (SIGNATURE) Date Time by: (SIGNATURE) Date Time C Relinquished by: (SIGNATURE) Date Time eceived b • [SI REj D e UWe Q o rj�J Waypointo ANALYTICAL 12/10/2020 EMA Resources Inc Brent Collins 755 Yadkinville Rd Mocksville, NC, 27028 Ref: Analytical Testing Lab Report Number: 20-337-0057 Client Project Description: Unifi Reidsville, NC 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Dear Brent Collins: Waypoint Analytical, LLC. received sample(s) on 12/2/2020 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Danyale Love Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Ijp, Page 1 of 9 Waypointo ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2021 Arkansas State Program 88-0650 02/07/2021 California State Program 2904 06/30/2021 Florida State Program - NELAP E871157 06/30/2021 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2021 Illinois State Program - NELAP 200078 10/10/2021 Kentucky State Program 80215 06/30/2021 Kentucky State Program KY90047 12/31/2020 Louisiana State Program - NELAP LA037 12/31/2020 Louisiana State Program - NELAP 04015 06/30/2021 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2020 Oklahoma State Program 9311 08/31/2021 Pennsylvania State Program - NELAP 68-03195 05/31/2021 South Carolina State Program 84002 06/30/2021 South Carolina State Program 84002 06/30/2021 Tennessee State Program 02027 02/11/2023 Tennessee A21LA ISO 17025:2017 4313.01 10/31/2021 Texas State Program - NELAP T104704180 09/30/2021 Virginia State Program 00106 06/30/2021 Virginia State Program - NELAP 460181 09/14/2021 Page 1 of 1 00001/20-337-0057 Page 2 of 9 Waypoint ANALYTICAL Report Number: 20-337-0057 Client Project Description: Unifi Reidsville, NC Lab No Client Sample ID 89233 Unifi 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Sample Summary Table Matrix Date Collected Solids 12/01/2020 08:30 Date Received 12/02/2020 Page 3 of 9 Waypointo ANALYTICAL Client: EMA Resources Inc Project: Unifi Lab Report Number: 20-337-0057 Date: 12/10/2020 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 fax 901.213.2440 www.waypointanalytical.com CASE NARRATIVE Metals Analysis Method 601 OD Analyte: Aluminum QC Batch No: L525778 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Calcium QC Batch No: L525778 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Copper QC Batch No: L525643 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Analyte: Iron QC Batch No: L525778 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Potassium QC Batch No: L525778 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Magnesium QC Batch No: L525643 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Analyte: Manganese QC Batch No: L525778 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Phosphorus QC Batch No: L525778 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Lead QC Batch No: L525643 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Page 4 of 9 Waypoint".0 ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 fax 901.213.2440 www.waypointanalytical.com Analyte: Sulfur QC Batch No: L526002 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Zinc QC Batch No: L525643 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Page 5 of 9 Waypointo ANALYTICAL 46245 EMA Resources Inc Brent Collins 755 Yadkinville Rd Mocksville , NC 27028 Report Number : 20-337-0057 Lab No : 89233 Sample ID : Unifi Project Unifi Information : Reidsville, NC 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com REPORT OFANALYSIS Report Date : 12/10/2020 Received : 12/02/2020 Danyale Love Project Manager Matrix: Solids Sampled: 12/1/2020 8:30 Test Results Units MDL MQL DF Date / Time Analyzed By Analytical Method Moisture 98.3 % 1 12/08/2016:57 FMM SW-DRYWT Ammonia Nitrogen 5550 mg/Kg - dry 1470 1470 1 12/07/20 10:00 JPJ 4500NH3C-2011 Nitrate+Nitrite-N 2990 mg/Kg - dry 272 272 1 12/07/20 15:51 ZBD 4500NO3F-2011 Organic N 9629 mg/Kg - dry 2941 1 12/07/20 10:00 CALCULATION pH 7.9 S.U. 1 12/03/2016:00 ADM 9045D Total Solids 1.63 % 0.010 0.010 1 12/07/20 16:13 FMM 2540G-2011 Total Volatile Solids 66.5 % 0.010 0.010 1 12/07/20 16:13 FMM 2540G-2011 Total Kjeldahl Nitrogen 15200 mg/Kg - dry 2940 1 12/08/20 15:44 CLP 4500NORGD-2011 Phosphorus 4490 mg/Kg - dry 162 294 1 12/08/20 08:07 TJS 6010D Aluminum 14200 mg/Kg - dry 272 294 1 12/08/20 08:07 TJS 6010D Arsenic <14.1 mg/Kg - dry 14.1 29.4 1 12/09/20 19:28 JADS 6010D Cadmium <1.18 mg/Kg - dry 1.18 5.88 1 12/08/20 08:07 TJS 6010D Calcium 28200 mg/Kg - dry 2280 2940 1 12/08/20 08:07 TJS 6010D Chromium 70.0 mg/Kg - dry 13.9 14.7 1 12/08/20 08:07 TJS 6010D Copper 218 mg/Kg - dry 18.2 29.4 1 12/08/20 08:07 TJS 6010D Iron 6470 mg/Kg - dry 501 588 1 12/08/20 08:07 TJS 6010D Lead 91.2 mg/Kg - dry 10.6 17.6 1 12/08/20 08:07 TJS 6010D Magnesium 14100 mg/Kg - dry 152 294 1 12/08/20 08:07 TJS 6010D Manganese 204 mg/Kg - dry 19.1 29.4 1 12/08/20 08:07 TJS 6010D Mercury 0.6883 mg/Kg - dry 0.203 0.918 1 12/07/20 10:48 DDB 7471A Molybdenum <7.94 mg/Kg - dry 7.94 14.7 1 12/08/20 08:07 TJS 6010D Nickel 22.3 mg/Kg - dry 7.06 14.7 1 12/08/20 08:07 TJS 6010D Potassium 3170 mg/Kg - dry 364 588 1 12/08/20 08:07 TJS 6010D Qualifiers/ DF Dilution Factor J Estimated value Definitions L Limit Exceeded MQL Method Quantitation Limit Page 6 of 9 Waypointo ANALYTICAL 46245 EMA Resources Inc Brent Collins 755 Yadkinville Rd Mocksville , NC 27028 Report Number : 20-337-0057 Lab No : 89233 Sample ID : Unifi Project Unifi Information : Reidsville, NC 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com REPORT OFANALYSIS Report Date : 12/10/2020 Received : 12/02/2020 Danyale Love Project Manager Matrix: Solids Sampled: 12/1/2020 8:30 Test Results Units MDL MQL DF Date / Time Analyzed By Analytical Method Selenium <18.8 mg/Kg - dry 18.8 29.4 1 12/08/20 08:07 TJS 6010D Sodium 37200 mg/Kg - dry 765 1470 1 12/08/20 08:07 TJS 6010D Zinc 818 mg/Kg - dry 47.6 73.5 1 12/08/20 08:07 TJS 6010D Sulfur 11200 mg/Kg - dry 305 588 1 12/08/20 08:07 JTR 6010D Sodium Absorption Ratio 5.88 Ratio 0.01 0.01 1 12/08/20 08:07 CALCULATION Qualifiers/ DF Dilution Factor Definitions J Estimated value Page 7 of 9 s WayPAoi nt ..(2) �79p Whitten Road,3.240 Memphis, TN 38133 21.2440 Main 901.213.240fl °Fax 901.213.2440 N A LYT I C A L www.waypointanalytical.com Shipment Receipt Form Customer Number: 46245 Customer Name: EMA Resources Inc Report Number: 20-337-0057 Shipping Method ® Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: T100 Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers/boxes received F-71 Custody seals intact on shipping container/cooler? 0 Yes 0 No ! Not Present Custody seals intact on sample bottles? 0 Yes 0 No ® Not Present Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No ® N/A Water - VOA vials free of headspace 0 Yes 0 No ® N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes ® No Comments: Signature: IHannah R. Brown Date & Time: 12/02/2020 12:52:15 Page 8 of 9 Client Name/Address Client Project Manager/Contact Billing information For Laboratory Use Only EMA Resources Inc Brent Collins Account #46245 755 Yadkinville Rd Mocksville, NC 27028 Project Description project/Site Location (City/State) RUSH - Additional charges apply Method of Shipment Matrix Key Special Detection umlt[s) Tod Ex �USPS WW -Wastewater GW -Groundwater IA;C date Results Needed SUPS Courier ClientOropOH DW- Drinking Water S -Soil/Solid 0-0d P Product M - Mist r Other Project Number Project Manager Phone 4 Project Manager Email Purchase Order Number Site/Facility !D # 3 3 5- 3 9 9- 3 5 46 brent.collins@emaresources.con"I L7�, T z (4 A Cool < 1RC Na252O3 (Micro Only) _ 11 � 8 Cool = 6C a �� tu a y il�� Y " a C)E O C p� C C H2SO4 pH�2 0 None Required ANALYTICAL a ° E E 00 E NaoH pH>10 2790 Whitten Koad Unless noted, all containers o cc [L1 (13 T Cow V E HNO3 pH<2 G HCL pH[2 Memphis, TN 38133 0 C) (901) 213.2400 per Table II of 4a CFR Part E a `L. H H3PO4 pHa2 Cool <= 6C NA25203 136- r¢ L7 Date Time Sample Identifitatian Required Analysis / Preservative Comments/Notes ��, [ ti �� ,� Metals:Al,As,Ca,Cd,Cr,CLI,Fe,Pb Mn, Mg, Mo, Hg, N i, Se, Na, R S, K, Zn eSOUF lC-S 1��11f 1� as2as7-0asr Unrrr nc 12-02-2020 12;SP 39 For Laboratory Use Only Sampled by (Name - Print) ��„� .�s Client Remarks/Comments Sludge Samples - Report Dry Weight Ice Custody Lab Comments Seats i6 N Relinqui d by: (SIGNATURE) Date Time Received by: (SIGNATURE) Date lime Y / BIan4 Coa emp Relinquished by: (SIGNATURE) Date Time Received by: (SIGNATURE) Date Time C� . l} mac. Relinquished by: (SIGNATURE) Date TimeVa ed.:AT ) Date Timeocl r /�o I to n aceAnalytical National Center for Testing & Innovation ANALYTICAL REPORT April 20, 2020 EMA Resources Sample Delivery Group: L12O7769 Samples Received: 04/10/2020 Project Number: Description: Sludge Site: UNIFI Report To: Mr. Brent Collins 755 Yadkinville Road Mocksville, NC 27028 Entire Report Reviewed By: Jw C4V1-- Justin Carr Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1207769 04/20/20 09:11 1 of 23 TABLE OF CONTENTS ONE LAB. NATIONWIDE. * Cp: Cover Page Tc: Table of Contents Ss: Sample Summary Cn: Case Narrative Sr: Sample Results UNIFI L1207769-01 Qc: Quality Control Summary Wet Chemistry by Method 9012 B Wet Chemistry by Method 9034-9030B Wet Chemistry by Method 9045D Wet Chemistry by Method D93/1010A Mercury by Method 7470A Metals (ICP) by Method 6010D Volatile Organic Compounds (GC/MS) by Method 8260D Chlorinated Acid Herbicides (GC) by Method 8151A Pesticides (GC) by Method 8081B Semi Volatile Organic Compounds (GC/MS) by Method 8270E GI: Glossary of Terms al: Accreditations & Locations Sc: Sample Chain of Custody 1 2 3 4 5 5 7 7 9 10 11 12 13 14 16 18 19 21 22 23 ACCOUNT: PROJECT: SDG: DATE/TIME: EMA Resources L1207769 04/20/20 09:11 PAGE: 2 of 23 SAMPLE SUMMARY ONE LAB. NATIONWIDE. Collected by Collected date/time Received date/time UNIFI L1207769-01 Waste Brent Collins 04/09/2010:30 04/10/2008:30 C P Method Preparation by Method 1311 Preparation by Method 1311 Wet Chemistry by Method 9012 B Wet Chemistry by Method 9034-9030B Wet Chemistry by Method 9045D Wet Chemistry by Method D93/1010A Mercury by Method 7470A Metals (ICP) by Method 6010D Volatile Organic Compounds (GC/MS) by Method 8260D Chlorinated Acid Herbicides (GC) by Method 8151A Pesticides (GC) by Method 8081B Semi Volatile Organic Compounds (GC/MS) by Method 8270E Batch Dilution Preparation date/time W G 145 9743 1 04/13/2 012 :24 WG1460768 1 04/15/20 08:27 W G 1461613 1 04/16/20 1118 WG1460703 1 04/15/20 00:00 W G1460878 1 04/15/20 1148 W G 14 6 0141 1 04/15/20 18 :19 W G 14 6 02 6 5 1 04/14/2 010 : 58 W G 14 6 03 83 1 04/14/2 013 : 55 W G 1461433 1 04/16/20 12 :3 6 WG1460597 1 04/14/20 22:02 WG1461793 1 04/16/20 23:22 W G 14 610 9 5 1 04/15/20 18 : 58 Analysis date/time 04/13/2012:24 04/15/20 08:27 04/16/2017:12 04/15/20 00:00 04/15/2014:35 04/15/2018:19 04/14/2016:48 04/14/2016:50 04/16/2012:36 04/16/2014:28 04/17/2010:48 04/16/20 03:04 Analyst IDW IDW SDL LDT KPS SL RIDS EL BMB LEL RP JNJ Location FC Mt. Juliet, TN Mt. Juliet, TN Mt. Juliet, TN Mt. Juliet, TN Mt. Juliet, TN Fn Mt. Juliet, TN Mt. Juliet, TN Mt. Juliet, TN Fr Mt. Juliet, TN Mt. Juliet, TN FC Mt. Juliet, TN Mt. Juliet, TN �GI SAI RC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1207769 04/20/20 09:11 3 of 23 CASE NARRATIVE ONE LAB. NATIONWIDE. * All sample aliquots were received at the correct temperature, in the proper containers, with the FP appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FC have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FS knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. 0 Fr FC GI Justin Carr [Al Project Manager RC Project Narrative All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B. All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1207769 04/20/20 09:11 4 of 23 UNIFI Collected date/time: 04/09/20 10:30 Preparation by Method 1311 SAMPLE RESULTS - 01 L1207769 Result Qualifier Prep Batch Analyte date / time TCLP Extraction 4/13/202012:24:22 PM WG1459743 TCLP ZHE Extraction - 4/15/2020 8:27:38 AM WG1460768 Fluid 1 4/13/202012:24:22 PM WG1459743 Initial pH 7.26 4/13/202012:24:22 PM WG1459743 Final pH 4.98 4/13/202012:24:22 PM WG1459743 Wet Chemistry by Method 9012 B Result Qualifier RDL Dilution Analysis Analyte mg/kg mg/kg date / time Reactive Cyanide ND 0.250 1 04/16/202017:12 Wet Chemistry by Method 9034-9030B Result Qualifier RDL Analyte mg/kg mg/kg Reactive Sulfide ND J6 25.0 Wet Chemistry by Method 9045D Batch WG1461613 Dilution Analysis Batch date / time 1 04/15/2020 00:00 WG1460703 Result Qualifier Dilution Analysis Batch Analyte su date / time Corrosivity by pH 8.01 T8 1 04/15/202014:35 WG1460878 Sample Narrative: L1207769-01 WG1460878: 8.01 at 20.2C Wet Chemistry by Method D93/1010A Result Analyte Deg. F Ignitability DNI at170 Mercury by Method 7470A Qualifier Dilution Analysis Batch date / time 1 04/15/202018:19 WG1460141 Result Qualifier RDL Limit Analyte mg/I mg/I mg/I Mercury ND 0.0100 0.20 Metals (ICP) by Method 6010D Result Qualifier RDL Limit Analyte mg/I mg/I mg/I Arsenic ND 0.100 5 Barium 0.115 0.100 100 Cadmium ND 0.100 1 Chromium ND 0.100 5 Lead ND 0.100 5 Selenium ND 0.100 1 Silver ND 0.100 5 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier RDL Limit Analyte mg/I mg/I mg/I Benzene ND 0.0500 0.50 Carbon tetrachloride ND 0.0500 0.50 Chlorobenzene ND 0.0500 100 Chloroform ND 0.250 6 ACCOUNT: PROJECT: EMA Resources Dilution Analysis Batch date / time 1 04/14/202016:48 WG1460265 Dilution Analysis Batch date / time 1 04/14/202016:50 WG1460383 1 04/14/202016:50 WG1460383 1 04/14/202016:50 WG1460383 1 04/14/202016:50 WG1460383 1 04/14/202016:50 WG1460383 1 04/14/202016:50 WG1460383 1 04/14/202016:50 WG1460383 ONE LAB. NATIONWIDE. * Fp Fc FS Fn Fc �GI SAI Rc Dilution Analysis Batch date / time 1 04/16/202012:36 WG1461433 1 04/16/202012:36 WG1461433 1 04/16/202012:36 WG1461433 1 04/16/202012:36 WG1461433 SDG: DATE/TIME: PAGE: L1207769 04/20/20 09:11 5 of 23 UNIFI SAMPLE RESULTS Collected date/time: 04/09/20 10:30 L1207769 Volatile Organic Compounds (GC/MS) by Method 8260D - 01 Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time 1,2-Dichloroethane ND 0.0500 0.50 1 04/16/202012:36 WG1461433 1,1-Dichloroethene ND 0.0500 0.70 1 04/16/202012:36 WG1461433 2-Butanone (MEK) ND 0.500 200 1 04/16/202012:36 WG1461433 Tetrachloroethene ND 0.0500 0.70 1 04/16/202012:36 WG1461433 Trichloroethene ND 0.0500 0.50 1 04/16/202012:36 WG1461433 Vinyl chloride ND 0.0500 0.20 1 04/16/202012:36 WG1461433 (S) Toluene-dH 109 80.0-120 0411612020 12.36 WG1461433 (S) 4-Bromofluorobenzene 93.6 77.0-126 0411612020 12.36 WG1461433 (S) 1,2-Dichloroethane-d4 96.0 70.0-130 041161202012.36 WG1461433 Chlorinated Acid Herbicides (GC) by Method 8151A Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time 2,4,5-TP (Silvex) ND 0.00200 1 1 04/16/202014:28 WG1460597 2,4-D ND 0.00200 10 1 04/16/202014:28 WG1460597 (S) Z4-Dichlorophenyl Acetic Acid 38.2 14.0-158 041161202014.28 WG1460597 Pesticides (GC) by Method 8081B Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time Chlordane ND 0.00500 0.03 1 04/17/202010:48 WG1461793 Endrin ND 0.00500 0.02 1 04/17/202010:48 WG1461793 Heptachlor ND 0.00500 0.0080 1 04/17/202010:48 WG1461793 Lindane ND 0.00500 0.40 1 04/17/202010:48 WG1461793 Methoxychlor ND 0.00500 10 1 04/17/202010:48 WG1461793 Toxaphene ND 0.0100 0.50 1 04/17/202010:48 WG1461793 (S) Decochlorobiphenyl 75.8 10.0-128 0411712020 10.48 WG1461793 (S) Tetrochloro-m-xylene 72.9 10.0-127 0411712020 10.48 WG1461793 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Analyte 1,4-Dichlorobenzene 2,4-Dinitrotoluene Hexachlorobenzene Hexachloro-1,3-butadiene Hexachloroethane Nitrobenzene Pyridine 3&4-Methyl Phenol 2-Methylphenol Pentachlorophenol 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol (S) 2-Fluorophenol (S) Phenol-d5 (S) Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Z4, 6-Tribromophenol (S) p-Terphenyl-d14 ACCOUNT: EMA Resources ONE LAB. NATIONWIDE. * Fp Fc FS Fn FA Fc F, SAI Rc Result Qualifier RDL Limit Dilution Analysis Batch mg/I mg/I mg/I date/time ND 0.100 7.50 1 04/16/2020 03:04 WG1461095 ND 0.100 0.13 1 04/16/2020 03:04 WG1461095 ND 0.100 0.13 1 04/16/2020 03:04 WG1461095 ND 0.100 0.50 1 04/16/2020 03:04 WG1461095 ND 0.100 3 1 04/16/2020 03:04 WG1461095 ND 0.100 2 1 04/16/2020 03:04 WG1461095 ND 0.100 5 1 04/16/2020 03:04 WG1461095 ND 0.100 400 1 04/16/2020 03:04 WG1461095 ND 0.100 200 1 04/16/2020 03:04 WG1461095 ND 0.100 100 1 04/16/2020 03:04 WG1461095 ND 0.100 400 1 04/16/2020 03:04 WG1461095 ND 0.100 2 1 04/16/2020 03:04 WG1461095 25.5 10.0-120 0411612020 03.04 WG1461095 15.9 10.0-120 0411612020 03.04 WG1461095 30.0 10.0-127 0411612020 03.04 WG1461095 40.5 10.0-130 0411612020 03.04 WG1461095 48.6 10.0-155 0411612020 03.04 WG1461095 49.0 10.0-128 0411612020 03.04 WG1461095 PROJECT: SDG: DATE/TIME: PAGE: L1207769 04/20/20 09:11 6 of 23 WG1461613 Wet Chemistry by Method 9012 B Method Blank (MB) (MB) R3519368-1 04/16/201655 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Reactive Cyanide U 0.0390 0.250 L1207631-01 Original Sample (OS) • Duplicate (DUP) QUALITY CONTROL SUMMARY L1207769-01 (OS) L1207631-01 04/16/2017:02 • (DUP) R3519363-3 04/16/2017:03 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD (dry) (dry) Limits Analyte mg/kg mg/kg %_ Reactive Cyanide ND 0.000 1 0.000 20 L1208077-01 Original Sample (OS) • Duplicate (DUP) (OS) L1203077-01 04/16/2017:15 • (DUP) R3519363-6 04/16/201716 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/kg mg/kg Reactive Cyanide ND 0.000 1 0.000 20 Laboratory Control Sample (LCS) (LCS) R3519368-2 04/16/201656 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/kg mg/kg Reactive Cyanide 2.50 2.63 105 85.0-115 L1207631-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1207631-03 04/16/2017:04 • (MS) R3519363-4 04/16/20 17:07 • (MSD) R3519363-5 04/16/20 17:08 Spike Amount Original Result MS Result (dry) MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD (dry) (dry) (dry) Analyte mg/kg mg/kg mg/kg mg/kg Reactive Cyanide 1.96 ND 1.16 1.02 59.1 51.8 1 75.0-125 J6 J6 13.2 ONE LAB. NATIONWIDE. * Cp ITC] FSS [Cn] 5 Sr �GI 1711 FSc RPD Limits 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1207769 04/20/20 09:11 7 of 23 WG1461613 QUALITY CONTROL SUMMARY Wet Chemistry by Method 9012 B L1207769-01 L1208077-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1203077-02 04/16/20 17:17 • (MS) R3519363-7 04/16/20 17:20 • (MSD) R3519363-8 04/16/20 17:21 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD Analyte mg/kg mg/kg mg/kg mg/kg Reactive Cyanide 1.67 ND 1.52 1.58 91.2 94.5 1 75.0-125 3.63 ONE LAB. NATIONWIDE. * RPD Limits 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1207769 04/20/20 09:11 3 of 23 WG1460703 Wet Chemistry by Method 9034-9030B Method Blank (MB) (MB) R3513640-1 04/15/20 00:00 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Reactive Sulfide U 7.63 25.0 QUALITY CONTROL SUMMARY L1207769-01 Laboratory Control Sample (LCS) (LCS) R3513640-2 04/15/20 00:00 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Reactive Sulfide 100 91.8 91.8 70.0-130 L1207769-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1207769-01 04/15/20 00:00 • (MS) R3513640-3 04/15/20 00:00 • (MSD) R3513640-4 04/15/20 00:00 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD Analyte mg/kg mg/kg mg/kg mg/kg Reactive Sulfide 100 ND 87.7 88.0 63.7 64.0 1 70.0-130 J6 J6 0.308 ONE LAB. NATIONWIDE. * Cp ITC] FSS [Cn] 5 Sr �GI RPD Limits SAI 20 FSc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1207769 04/20/20 09:11 9 of 23 WG1460878 QUALITY CONTROL SUMMARY Wet Chemistry by Method 9045D L1207769-01 Laboratory Control Sample (LCS) (LCS) R3518927-1 04/15/20 1435 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte su su Corrosivity by pH 10.0 10.0 100 99.0-101 Sample Narrative: LCS:10.01 at19.1C ONE LAB. NATIONWIDE. * ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1207769 04/20/20 09:11 10 of 23 WG1460141 QUALITY CONTROL SUMMARY Wet Chemistry by Method D93/1010A L1207769-01 L1207395-02 Original Sample (OS) • Duplicate (DUP) (OS) L1207395-02 04/15/2013:19 • (DUP) R3513932-3 04/15/201319 Original Result DUP Result Dilution DUP RPD Analyte Deg. F Deg. F Ignitability 68.2 68.0 1 0.294 DUP Qualifier DUP RPD Limits i 10 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3518982-1 04/15/2018:19 • (LCSD) R3518982-2 04/15/201819 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte Deg.F Deg.F Deg.F Ignitability 82.0 84.2 82.2 103 100 95.6-104 2.40 10 ONE LAB. NATIONWIDE. * ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1207769 04/20/20 09:11 11 of 23 ■ WG1460265 Mercury by Method 7470A Method Blank (MB) (MB) R3518591-1 04/14/201621 MB Result MB Qualifier MB MDL Analyte mg/I mg/I Mercury U 0.00330 Laboratory Control Sample (LCS) (LCS) R3518591-4 04/14/2016:58 Spike Amount LCS Result LCS Rec. Analyte mg/I mg/I Mercury 0.0300 0.0281 93.8 QUALITY CONTROL SUMMARY L1207769-01 MB RDL mg/I 0.0100 Rec. Limits LCS Qualifier 80.0-120 L1206857-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) ONE LAB. NATIONWIDE. * (OS) L1206357-01 04/14/2016:26 • (MS) R3513591-2 04/14/2016:23 • (MSD) R3513591-3 04/14/2016:34 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I mg/I Mercury 0.0300 ND 0.0275 0.0248 91.6 82.8 1 75.0-125 10.1 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1207769 04/20/20 09:11 12 of 23 WG1460383 Metals (ICP) by Method 6010D Method Blank (MB) QUALITY CONTROL SUMMARY L1207769-01 (MB) R3518622-1 04/14/201613 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I Arsenic U 0.0333 0.100 Barium U 0.0333 0.100 Cadmium U 0.0333 0.100 Chromium U 0.0333 0.100 Lead U 0.0333 0.100 Selenium U 0.0333 0.100 Silver U 0.0333 0.100 Laboratory Control Sample (LCS) (LCS) R3513622-2 04/14/20 1615 Spike Amount LCS Result LCS Rec. Rec. Limits Analyte mg/I mg/I Arsenic 10.0 9.46 94.6 80.0-120 Barium 10.0 9.33 93.3 80.0-120 Cadmium 10.0 9.31 93.1 80.0-120 Chromium 10.0 9.12 91.2 80.0-120 Lead 10.0 9.43 94.3 80.0-120 Selenium 10.0 9.46 94.6 80.0-120 Silver 2.00 1.77 88.7 80.0-120 LCS Qualifier L1206857-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1206357-01 04/14/20 16:13 • (MS) R3513622-4 04/14/20 16:23 • (MSD) R3513622-5 04/14/2016:26 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Analyte mg/I mg/I mg/I mg/I Arsenic 10.0 ND 9.55 9.52 95.5 95.2 Barium 10.0 0.264 9.69 9.65 94.2 93.8 Cadmium 10.0 ND 9.39 9.38 93.9 93.8 Chromium 10.0 ND 9.35 9.30 93.5 93.0 Lead 10.0 ND 9.55 9.55 95.5 95.5 Selenium 10.0 0.113 9.58 9.58 94.6 94.7 Silver 2.00 ND 1.81 1.80 90.3 90.1 ONE LAB. NATIONWIDE. * Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits 1 75.0-125 0.306 20 1 75.0-125 0.391 20 1 75.0-125 0.135 20 1 75.0-125 0.551 20 1 75.0-125 0.00780 20 1 75.0-125 0.0803 20 1 75.0-125 0.141 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1207769 04/20/20 09:11 13 of 23 WG1461433 Volatile Organic Compounds (GC/MS) by Method 8260D Method Blank (MB) (MB) R3519174-3 04/16/201012 QUALITY CONTROL SUMMARY L1207769-01 ONE LAB. NATIONWIDE. * MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I Benzene U 0.0167 0.0500 Carbon tetrachloride U 0.0167 0.0500 Chlorobenzene U 0.0167 0.0500 Chloroform U 0.0833 0.250 1,2-Dichloroethane U 0.0167 0.0500 1,1-Dichloroethene U 0.0167 0.0500 2-Butanone (MEK) U 0.167 0.500 Tetrachloroethene U 0.0167 0.0500 Trichloroethene U 0.0167 0.0500 Vinyl chloride U 0.0167 0.0500 (S) Toluene-dH 103 80.0-120 (S) 4-Bromofluorobenzene 96.8 77.0-126 (S) 1,2-Dichloroethane-d4 105 70.0-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3519174-1 04/16/20 03:30 • (LCSD) R3519174-2 04/16/20 03 50 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I Benzene 0.250 0.224 0.212 89.6 84.8 70.0-123 5.50 20 Carbon tetrachloride 0.250 0.221 0.220 88.4 88.0 68.0-126 0.454 20 Chlorobenzene 0.250 0.241 0.236 96.4 94.4 80.0-121 2.10 20 Chloroform 0.250 0.212 0.208 84.8 83.2 73.0-120 1.90 20 1,2-Dichloroethane 0.250 0.243 0.222 97.2 88.8 70.0-128 9.03 20 1,1-Dichloroethene 0.250 0.224 0.213 89.6 85.2 71.0-124 5.03 20 2-Butanone (MEK) 1.25 1.24 1.13 99.2 90.4 44.0-160 9.28 20 Tetrachloroethene 0.250 0.236 0.253 94.4 101 72.0-132 6.95 20 Trichloroethene 0.250 0.234 0.228 93.6 91.2 78.0-124 2.60 20 Vinyl chloride 0.250 0.214 0.200 85.6 80.0 67.0-131 6.76 20 (S) Toluene-dH 104 103 80.0-120 (S) 4-Bromofluorobenzene 95.9 91.4 77.0-126 (S) 1,2-Dichloroethane-d4 97.4 92.6 70.0-130 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1207769 04/20/20 09:11 14 of 23 WG1461433 QUALITY CONTROL Volatile Organic Compounds (GC/MS) by Method 8260D L1207769-01 L1207590-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) SUMMARY ONE LAB. NATIONWIDE. C (OS) L1207590-01 04/16/201135 • (MS) R3519174-4 04/16/201725 • (MSD) R3519174-5 04/16/201745 p Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I mg/I % % % % % z TC Benzene 0.250 ND 0.211 0.202 84.4 80.8 1 17.0-158 4.36 27 Carbon tetrachloride 0.250 ND 0.248 0.243 99.2 97.2 1 23.0-159 2.04 28 FS Chlorobenzene 0.250 ND 0.225 0.215 90.0 86.0 1 33.0-152 4.55 27 Chloroform 0.250 ND 0.204 0.200 81.6 80.0 1 29.0-154 1.98 28 1,2-Dichloroethane 0.250 ND 0.213 0.207 85.2 82.8 1 29.0-151 2.86 27 [Cn] 1,1-Dichloroethene 0.250 ND 0.269 0.290 108 116 1 11.0-160 7.51 29 2-Butanone (MEK) 1.25 ND 0.923 0.958 73.8 76.6 1 10.0-160 3.72 32 5Sr Tetrachloroethene 0.250 ND 0.244 0.232 97.6 92.8 1 10.0-160 5.04 27 Trichloroethene 0.250 ND 0.240 0.235 96.0 94.0 1 10.0-160 2.11 25 Vinyl chloride 0.250 ND 0.242 0.230 96.8 92.0 1 10.0-160 5.08 27 (S) Toluene-dH 105 102 80.0-120 (S) 4-Bromofluorobenzene 89.8 91.7 77.0-126 7G1 (S) 1,2-Dichloroethane-d4 97.8 976 70.0-130 [Al L1207838-04 Original Sample (OS) • Matrix Spike (MS) (OS) L1207333-04 04/16/20 13:33 • (MS) R3519174-6 04/16/20 13 06 FSC Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier Analyte mg/I mg/I mg/I Benzene 0.250 ND 0.243 97.2 1 17.0-158 Carbon tetrachloride 0.250 ND 0.287 115 1 23.0-159 Chlorobenzene 0.250 ND 0.265 106 1 33.0-152 Chloroform 0.250 ND 0.254 102 1 29.0-154 1,2-Dichloroethane 0.250 ND 0.254 102 1 29.0-151 1,1-Dichloroethene 0.250 ND 0.300 120 1 11.0-160 2-Butanone (MEK) 1.25 ND 1.14 91.2 1 10.0-160 Tetrachloroethene 0.250 ND 0.294 118 1 10.0-160 Trichloroethene 0.250 ND 0.287 115 1 10.0-160 Vinyl chloride 0.250 ND 0.267 107 1 10.0-160 (S) Toluene-dH 103 80.0-120 (S) 4-Bromofluorobenzene 97.4 77.0-126 (S) 1,2-Dichloroethane-d4 102 70.0-130 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1207769 04/20/20 09:11 15 of 23 WG1460597 Chlorinated Acid Herbicides (GC) by Method 8151A Method Blank (MB) (MB) R3519127-1 04/16/20 08:44 MB Result Analyte mg/I 2,4-D U 2,4,5-TP (Silvex) U (S) Z4-Dichlorophenyl Acetic 772 Acid MB Qualifier MB MDL mg/I 0.000667 0.000667 Laboratory Control Sample (LCS) (LCS) R3519127-2 04/16/20 08:57 Spike Amount LCS Result LCS Rec. Analyte mg/I mg/I 2,4-D 0.0500 0.0401 80.2 2,4,5-TP (Silvex) 0.0500 0.0471 94.2 (S) Z4-Dichlorophenyl Acetic 80.0 Acid QUALITY CONTROL SUMMARY L1207769-01 MB RDL mg/I 0.00200 0.00200 14.0-158 Rec. Limits LCS Qualifier 50.0-120 50.0-125 MIMAN L1207208-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) ONE LAB. NATIONWIDE. * (OS) L1207203-01 04/16/20 09:11 • (MS) R3519127-3 04/16/20 09:25 • (MSD) R3519127-4 04/16/20 09:39 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I mg/I 2,4-D 0.0500 U 0.0404 0.0384 80.8 76.8 1 50.0-120 5.08 20 2,4,5-TP (Silvex) 0.0500 U 0.0484 0.0463 96.8 92.6 1 50.0-125 4.44 20 (S) Z4-Dichlorophenyl Acetic 81.2 73.8 14.0-158 Acid L1207211-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1207211-01 04/16/20 09:52 • (MS) R3519127-5 04/16/20 10:06 • (MSD) R3519127-6 04/16/20 10:20 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Analyte mg/I mg/I mg/I mg/I 2,4-D 0.0500 U 0.0382 0.0425 76.4 85.0 2,4,5-TP (Silvex) 0.0500 U 0.0461 0.0510 92.2 102 (S) Z4-Dichlorophenyl Acetic 75.8 83.4 Acid ACCOUNT: EMA Resources PROJECT: Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits 1 50.0-120 10.7 20 1 50.0-125 P P 10.1 20 14.0-158 SDG: DATE/TIME: PAGE: L1207769 04/20/20 09:11 16 of 23 WG1460597 QUALITY CONTROL SUMMARY Chlorinated Acid Herbicides (GC) by Method 8151A L1207769-01 L1207215-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1207215-01 04/16/20 10:34 • (MS) R3519127-7 04/16/20 10:47 • (MSD) R3519127-8 04/16/20 1101 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Analyte mg/I mg/I mg/I mg/I 2,4-D 0.0500 U 0.0416 0.0415 83.2 83.0 2,4,5-TP (Silvex) 0.0500 U 0.0503 0.0506 101 101 (S) Z4-Dichlorophenyl Acetic 81.8 82.0 Acid L1207219-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1207219-01 04/16/20 1129 • (MS) R3519127-9 04/16/201142 • (MSD) R3519127-10 04/16/20 1156 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Analyte mg/I mg/I mg/I mg/I 2,4-D 0.0500 U 0.0424 0.0403 84.8 80.6 2,4,5-TP (Silvex) 0.0500 U 0.0502 0.0481 100 96.2 (S) Z4-Dichlorophenyl Acetic 85.0 78.0 Acid ONE LAB. NATIONWIDE. * Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits 1 50.0-120 0.241 20 1 50.0-125 P P 0.595 20 14.0-158 Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits 1 50.0-120 5.08 20 1 50.0-125 4.27 20 14.0-158 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1207769 04/20/20 09:11 17 of 23 WG1461793 Pesticides (GC) by Method 8081B Method Blank (MB) QUALITY CONTROL SUMMARY L1207769-01 (MB) R3519593-1 04/17/20 03 45 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I Gamma BHC U 0.00167 0.00500 Endrin U 0.00167 0.00500 Heptachlor U 0.00167 0.00500 Methoxychlor U 0.00167 0.00500 Chlordane U 0.00167 0.00500 Toxaphene U 0.00333 0.0100 (S) Decachlorobiphenyl 90.9 10.0-128 (S) Tetrochloro-m-xylene 75.8 10.0-127 Laboratory Control Sample (LCS) (LCS) R3519593-2 04/17/20 09:09 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I Gamma BHC 0.0100 0.00817 81.7 55.0-129 Endrin 0.0100 0.00814 81.4 57.0-134 Heptachlor 0.0100 0.00852 85.2 27.0-132 Methoxychlor 0.0100 0.00895 89.5 54.0-155 (S) Decachlorobiphenyl 90.8 10.0-128 (S) Tetrochloro-m-xylene 81.1 10.0-127 L1207769-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1207769-01 04/17/2010:43 • (MS) R3519593-3 04/17/2011:01 • (MSD) R3519593-4 04/17/201113 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Analyte mg/I mg/I mg/I mg/I Gamma BHC 0.0100 ND 0.00810 0.00814 81.0 81.4 Endrin 0.0100 ND 0.00822 0.00820 82.2 82.0 Heptachlor 0.0100 ND 0.00824 0.00854 82.4 85.4 Methoxychlor 0.0100 ND 0.00886 0.00882 88.6 88.2 (S) Decachlorobiphenyl 73.9 71.5 (S) Tetrochloro-m-xylene 79.2 77.6 Dilution Rec. Limits 1 14.0-141 1 10.0-160 1 16.0-136 1 10.0-160 10.0-128 10.0-127 ONE LAB. NATIONWIDE. * MS Qualifier MSD Qualifier RPD RPD Limits 0.493 40 0.244 39 3.58 40 0.452 34 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1207769 04/20/20 09:11 13 of 23 WG1461095 QUALITY CONTROL SUMMARY Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1207769-01 Method Blank (MB) (MB) R3519070-2 04/16/20 0135 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I 1,4-Dichlorobenzene U 0.0333 0.100 2,4-Dinitrotoluene U 0.0333 0.100 Hexachlorobenzene U 0.0333 0.100 Hexachloro-1,3-butadiene U 0.0333 0.100 Hexachloroethane U 0.0333 0.100 Nitrobenzene U 0.0333 0.100 Pyridine U 0.0333 0.100 2-Methylphenol U 0.0333 0.100 3&4-Methyl Phenol U 0.0333 0.100 Pentachlorophenol U 0.0333 0.100 2,4,5-Trichlorophenol U 0.0333 0.100 2,4,6-Trichlorophenol U 0.0333 0.100 (S) Nitrobenzene-d5 46.4 10.0-127 (S) 2-Fluorobiphenyl 59.9 10.0-130 (S) p-Terphenyl-d14 65.3 10.0-128 (S) Phenol-d5 22.6 10.0-120 (S) 2-Fluorophenol 36.6 10.0-120 (S) 2,4, 6-Tribromophenol 66.0 10. 0-155 Laboratory Control Sample (LCS) ONE LAB. NATIONWIDE. * (LCS) R3519070-1 04/16/20 0112 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I 1,4-Dichlorobenzene 0.500 0.280 56.0 18.0-120 2,4-Dinitrotoluene 0.500 0.333 66.6 49.0-124 Hexachlorobenzene 0.500 0.322 64.4 44.0-120 Hexachloro-1,3-butadiene 0.500 0.287 57.4 19.0-120 Hexachloroethane 0.500 0.250 50.0 15.0-120 Nitrobenzene 0.500 0.216 43.2 27.0-120 Pyridine 0.500 0.138 27.6 10.0-120 2-Methylphenol 0.500 0.220 44.0 28.0-120 3&4-Methyl Phenol 0.500 0.229 45.8 31.0-120 Pentachlorophenol 0.500 0.328 65.6 23.0-120 2,4,5-Trichlorophenol 0.500 0.305 61.0 44.0-120 2,4,6-Trichlorophenol 0.500 0.293 58.6 42.0-120 (S) Nitrobenzene-d5 36.2 10.0-127 (S) 2-Fluorobiphenyl 55.8 10.0-130 (S) p-Terphenyl-d14 578 10.0-128 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1207769 04/20/20 09:11 19 of 23 WG1461095 QUALITY CONTROL SUMMARY Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1207769-01 Laboratory Control Sample (LCS) (LCS) R3519070-1 04/16/20 0112 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I (S) Phenol-d5 22.6 10.0-120 (S) 2-Fluorophenol 35.1 10.0-120 (S) 2,4, 6-Tribromophenol 72.0 10. 0-155 L1207769-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1207769-01 04/16/20 03:04 • (MS) R3519070-3 04/16/20 03:26 • (MSD) R3519070-4 04/16/20 03:43 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD Analyte mg/I mg/I mg/I mg/I 1,4-Dichlorobenzene 0.500 ND 0.223 0.196 44.6 39.2 1 17.0-120 12.9 2,4-Dinitrotoluene 0.500 ND 0.320 0.293 64.0 58.6 1 39.0-125 8.81 Hexachlorobenzene 0.500 ND 0.306 0.285 61.2 57.0 1 35.0-122 7.11 Hexachloro-1,3-butadiene 0.500 ND 0.235 0.215 47.0 43.0 1 12.0-120 8.89 Hexachloroethane 0.500 ND 0.193 0.174 38.6 34.8 1 10.0-120 10.4 Nitrobenzene 0.500 ND 0.179 0.161 35.8 32.2 1 12.0-120 10.6 Pyridine 0.500 ND 0.102 0.0820 20.4 16.4 1 10.0-120 21.7 2-Methylphenol 0.500 ND 0.179 0.159 35.8 31.8 1 10.0-120 11.8 3&4-Methyl Phenol 0.500 ND 0.182 0.169 36.4 33.8 1 10.0-120 7.41 Pentachlorophenol 0.500 ND 0.322 0.299 64.4 59.8 1 10.0-128 7.41 2,4,5-Trichlorophenol 0.500 ND 0.265 0.252 53.0 50.4 1 33.0-120 5.03 2,4,6-Trichlorophenol 0.500 ND 0.261 0.237 52.2 47.4 1 26.0-120 9.64 (S) Nitrobenzene-d5 31.0 28.0 10.0-127 (S) 2-Fluorobiphenyl 46.8 42.1 10.0-130 (S) p-Terphenyl-d14 59.9 53.3 10.0-128 (S) Phenol-d5 17.3 16.1 10.0-120 (S) 2-Fluorophenol 27.4 24.1 10.0-120 (S)2,4,6-Tribromophenol 66.5 62.5 10.0-155 ONE LAB. NATIONWIDE. * RPD Limits 40 25 24 34 40 30 37 30 36 37 31 31 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1207769 04/20/20 09:11 20 of 23 GLOSSARY OF TERMS Guide to Reading and Understanding Your Laboratory Report ONE LAB. NATIONWIDE. * The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative. Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received. Abbreviations and Definitions u Fc FS (dry) Results are reported based on the dry weight ofthe sample. [this will only be present on a dry report basis for soils]. MDL Method Detection Limit. Fn ND Not detected at the Reporting Limit (or MDL where applicable). RDL Reported Detection Limit. Fr Rec. Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. Fc Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and (S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. F Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the Rc result reported has already been corrected for this factor. These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry) Confidence level of 2 sigma. Case Narrative (Cn) Quality Control Summary (Qc) Sample Chain of Custody (Sc) Sample Results (Sr) Sample Summary (Ss) Qualifier J6 P T8 A brief discussion about the included sample results, including a discussion of any non -conformances to protocol observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe samples from the time of collection until delivery to the laboratory for analysis. This section ofyour report will provide the results of all testing performed on your samples. These results are provided by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Description The sample matrix interfered with the ability to make any accurate determination, spike value is low. RPD between the primary and confirmatory analysis exceeded 40%. Sample(s) received past/too close to holding time expiration. ACCOUNT: EMA Resources PROJECT: SDG: DATE/TIME: PAGE: L1207769 04/20/20 09:11 21 of 23 ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing Cp turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. Not all certifications held by the laboratory are applicable to the results reported in the attached report. Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. Fc State Accreditations Alabama 40660 Nebraska NE-OS-15-05 FS Alaska 17-026 Nevada TN-03-2002-34 Arizona AZ0612 New Hampshire 2975 Arkansas 88-0469 New Jersey—NELAP TNO02 Fn California 2932 New Mexico n/a Colorado TN00003 New York 11742 Connecticut PH-0197 North Carolina Env375 Fr Florida E87487 North Carolina' DW21704 Georgia NELAP North Carolina 3 41 Georgia' 923 North Dakota R-140 Fc Idaho TN00003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 7G1 Indiana C-TN-01 f Oregon TN200002 Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky' 6 90010 South Carolina 84004 Kentucky 2 16 South Dakota n/a Louisiana A130792 Tennessee'" 2006 Louisiana' LA180010 Texas T104704245-18-15 Rc Maine TN0002 Texas 5 LABO152 Maryland 324 Utah TN00003 Massachusetts M-TNO03 Vermont VT2006 Michigan 9958 Virginia 460132 Minnesota 047-999-395 Washington C847 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin 9980939910 Montana CERT0086 Wyoming A2 LA Third Party Federal Accreditations A2LA— ISO17025 1461.01 AIHA-LAP,LLC EMLAP 100789 A2 LA — ISO 17025 5 1461.02 DOD 1461.01 Canada 1461.01 USDA P330-15-00234 EPA—Crypto TN00003 ' Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable Our Locations Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. Pace National performs all testing at our central laboratory. WA MT ND OR ID SD VWY ` NV T NE T UT CA co KS W o �AZ NM O� T TX AK � . b C, fo • B HI 4 S ACCOUNT: V PROJECT: EMA Resources ME MN WVI NY MI T IA T PA 4 OH Mo IL Ihi T T WV VAT KY N * r� AR Ms AL GA LA FL SDG: DATE/TIME: PAGE: L1207769 04/20/20 09:11 22 of 23 Billing Information: j A WN 's Container I Pr qprvativL :halm of Custody Page of EMA Resources Mr- Brent Collins [Prey 755 Yadkinville Road ceAnalytical' 755 Yadkinville Road Mocksville, NC 27028 Mocksville, NC 27028 12065 Lebanon Rd ❑`■.$� �■ Report to: Email To brent.collins@emaresourcesinc.com Mr. Brent Collins Mount) 15-75 37122 C# ;` Phone: 65-758-5858 Phone:800-767-5859 K1 Faa�_fi15-758-5859 ■--i-t I �E �+ Project ProJ City/State )) / 44r�,;//t Please Circle: PT MT CT ET Description: Sludge Collected: /VC_ SDG p 1 Client Project $1 Lab Project A Phone:336-751-1441 i�71 97}rint): Fax 336 751-1442 6' d Collected by ((p Site/Facility 10 It P.Q. # Z Template:T11413 Collected by (signature): Rush. (Lab MUST Be Notified) Quote If L C J Prelogin: P748420 Same Day Five Day Next Day 5 Day (Rad only) Date Results Needed i PM: 807 -Justin Carr Immediately / _ _ _Two Day _ SO Day (Rad Only) No. [ PB: Packed on Ice N_ Y ✓ _ Three Day of I Shipped Via: FedEX Standard Sample ID Comp/Grab Matrix' Depth Date Time ntrs U Remarks sarnplea{iaho 1yl ss S' yy/zo io:v,., 2 X X .v r - — — 91' ReCeir�hPcklrist Matrix: emarks: SS - Soil AIR - Air F- Filter pH Temp COC Sea! Present/intact: _NP Y N COC signed/Accurate: LY _N GW Groundwater B- Bioassay aottles arrive Flow Other WW - WasteWater Correct bottleslused: _e4 _N DW - Drinking Wat Samples returned via: Sufficient volume sent: OT - Other UPS _Courier Trdtking# b 4 �j V0A Zero Headspacelicable Y N o _FeclEx Reiinquished y : (Sig tur Date: Time: Received by: (Signa_ure) Trip Blank eived: Yes / No Preservation Correct/Checked: wry _N RAD Screen n Co mect/ / y N HCL / Meohl -' TBR Relinquished by: (Signature) Date Time: Received by, (Signature) T R3 -C Bottles Received: If preservation required by Login: Date/Time 'f sc7 f , -) 07 Relinquished by: (Signature) Date Time: Received for y (Signature) Date: Time: Hold: Conditio N C F / OK