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Home My WebLink AboutWQ0028653_Residual Annual Report 2020_20210208Initial Review Reviewer Thornburg, Nathaniel Is this submittal an application? (Excluding additional information.)* r Yes r No If not an application what is the submittal type?* r Annual Report r Residual Annual Report r Additional Information r Other Annual Report Year* 2020 Permit Number (IR)* WQ0028653 Applicant/Permittee Pilgrim's Pride Corporation Email Notifications Does this need review by the hydrogeologist?* r Yes r No Regional Office Raleigh CO Reviewer Admin Reviewer Submittal Form Project Contact Information Rease provide inforration on the person to be contacted by N B Staff Name * Robert T. Branch Email Address* bbranch@branchrs.com electronic subnittal, confirmation of receipt, and other correspondence. Project Information ........ ......... .......................................................................................................................................... Application/Document Type* r New (Fee Req ui red) r Modification - Major (Fee Required) r Renewal with Major Modification (Fee Required) r Annual Report r Additional Information r Other Phone Number* 3363129007 O Modification - Minor C Renewal C GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 r Residual Annual Report r Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* r Wastewater Irrigation r High -Rate Infiltration r Other Wastewater r Reclaimed Water r Closed -Loop Recycle r Residuals r Single -Family Residence Wastewater r Other Irrigation Permit Number:* WQ0028653 Fbs Current Existing perrrit number Applicant/Permittee Address* 484 Zimmerman Road Facility Name * Pilgrim's Pride - Sanford DCAR Please provide comments/notes on your current submittal below. As per your request no hardcopy will be sent At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form Engineering Rans, Specifications, Calculations, Bc.) PP_2020_AR_final.pdf 933.41 KB Upload only 1 PCFdocurrent (less than 250 fvB). NLRiple documents rust be combined into one FDFfile unless file is larger than upload limit. * V By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date 2/8/2021 2020 ANNUAL REPORT PILGRIM'S PRIDE CORPORATION WATER TREATMENT PLANT SANFORD, NORTH CAROLINA PERMIT #WQ0028653 Prepared For: Pilgrim's Pride Corporation 484 Zimmerman Road Sanford, N.C. 27331-3668 Prepared By: Branch Residuals & Soils, LLC 1735 Heckle Blvd. Suite 103-291 Rock Hill SC, 29732 February 2021 BRANCH RESIDUALS & SOILS, LLC 1735 Heckle Blvd, Suite 103-291, Rack Hill, SC 29732 PHONE (336) 312-9007 February 8, 2021 North Carolina Department of Environmental Quality Division of Water Resources 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Reference: 2020 LAND APPLICATION ANNUAL REPORT Pilgrim's Pride Corporation. Sanford, North Carolina Permit No. WQ0028653 BR&S Project No. 2007-66 Information Processing Unit: Branch Residuals & Soils is submitting all monitoring and reporting information as required in the referenced permit on behalf of Pilgrim's Pride Corporation for their facility in Sanford, North Carolina. This report includes: 1) Distribution and Marketing Certification and Summary Forms, 2) Annual Residual Sampling Summary Form, 3) Annual Metals Field Loading Summary Forms, 4) Annual land application Field Summary Forms, 5) Residual Analysis Lab Sheets, 6) TCLP Lab Sheets, 7) Pathogen & Vector Attraction Form, 8) Pathogen and Vector Attraction Reduction Documentation, 9) Soils Lab Data 10) 2020 Application Summary Table, and 11) 2020 Application Condition Summaries. A total of 828,000 gallons (111.52 dry tons) of alum residuals were distributed to sites on the Pilgrim's Pride Facility at Sanford, NC in October of 2020. If any further information is required regarding this land application program, please do not hesitate to contact me at (336) 312-9007. Sincerely, r Robert T. Branch, L.S.S. Land Application/Residuals Operator #15676 RTB Enclosures TABLE OF CONTENTS SECTION NO. TITLE I Distribution and Marketing Certification and Summary Forms II Annual Residual Sampling Summary Form III Annual Metals Field Loading Summary Forms IV Annual Land Application Field Summary Forms V Residual Analysis Lab Sheets VI Toxicity Characteristics Leaching Procedure (TCLP) Analysis Report VII Pathogen and Vector Attraction Reduction Form VIII Pathogen and Vector Attraction Reduction Documentation IX Soil Analysis Report X 2020 Application Summary Table XI 2020 Application Condition Summaries DISTRIBUTION AND MARKETING CERTIFICATION AND SUMMARY FORM CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM WQ PERMIT #: WON28653 FACILITY NAME: Pilgrim's Pride Corporation PRONE: (919) 774-7333 COUNTY: Lee OPERATOR: Denali Water FACILITY TYPE (please check one): p Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) [21 Distribution and Marketing (complete Parts A, % and C) Was the facility in operation during the past calendar year? Yes L No I —► If No skip parts A. B. C and certify form below Part A*• Part B*• Month Sources(s) (include NPDES # if a PPlicable ) Volumed tons Recipient Information Amendment/ Bulkin A ent Residual In Product Out Nam s �) Volumed tons (D' ) Intended u ems) January February March April May June Jul August September October PWS 03-53-130 0 NA 111.52 Pilgrim's Pride Corporation 111.52 Soil Amendment November December Total from FORM DMSDF (sup) 0 0 0 0 Totals: Annual (dry tons): 0 I 0 111.52 111.52 Amendment(s) used: I Bulking Agent(s) used: (supp)): Total Number of Fonn DMSDF (Supp) * If more space is required, attach additional information sheets (FORM DMSDF Part C: Facility was compliant during the past calendar year with all conditions of the land application permit Yes (including but not limited to items 1-3 below) issued by the Division of Water Quality: No ---► If No, Explain in Narritive 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. fell t Signature of Permittee Dalt a QA.�!l�l,x Signature of Preparer** (if different from Permittee) a-y-a1 Date **Preparer is defined in 40 CFR Part 503.9(r) and ISA NCAC 2T .1102 (26) DENR FORM DMSDF (12I2M) ANNUAL RESIDUAL SAMPLING SUMMARY FORM ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0028653 Facility Name: Pilgrim's Pride Corporation Residual Source WQ # or NPDES #: PWS 03-53-130 WWTP Name: Pilgrim's Pride Corporation Sanford NC WTP Residual Analvsis Data Laboratory: 1) Waypoint Analyltical 2) 3) 4) 5) Pammeter �mSkg) Ceiling Conc. Limit Sam le or Com site Date 8/I3/2020 Percent Solids (%) NA 3.23 Arsenic 75 <15.6 Cadmium 85 <3.13 Copper 4,300 142.00 Chromium NA 0.00 Lead 840 12.30 Mercury 57 <0.481 Molybdenum 75 <7.81 Nickel 420 25.10 Selenium 100 <15.6 Zinc 7,500 70.60 Total Phosphorus NA 1.820 TKN NA 28,300 Ammonia -Nitrogen NA 1,390 Nitrate and Nitrite NA <155.00 ' For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer 2-y-al Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26) DENR FORM DMSDF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORMS ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Pilgrim's Pride Corporation Total Dry Tons Applied (Annual): WQ0028653 Cation Exchange Capacity (non 503 only): Pilgrim's Pride Corporation Owner: Pilgrim's Pride Corporation Predominant Soil Series 9.74 Acres Permitted: 9.74 Site #: 1 Field #: 27.48 n/a StA Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): 20-226-0012 1 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): IBM "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the inform tion su mitted. I am aware that there are significant penalties for submitting false information, in t sibility of fines and imprisonment for knowing violations" ZZ�/zr Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Pilgrim's Pride Corporation Total Dry Tons Applied (Annual): Permit #: WQ0028653 Cation Exchange Capacity (non 503 only): Operator: Pilgrim's Pride Corporation Owner: Pilgrim's Pride Corporation Predominant Soil Series Acres Used: 16.9 Acres Permitted: 16.9 Site #: 1 Field #: 84.05 n/a ToB Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): 20-226.0012 Total Phos- phorusMENEENEENEEN Annual Heavy Metal Field Loadings (Calculated in lbs/acre): MRS t Total Phos- .. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, in n sibility of fines and imprisonment for knowing violations" �L Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL LAND APPLICATION FIELD SUMMARY FORMS ANNUAL LAND APPLICATION FIELD SUMMARY FORMS LEGEND All nutrients and metals concentrations listed on the following annual land application field summary forms are on a pound per acre basis. The following is a list of symbols and abbreviations used on the field loading rate report: %TS — Percent Solids DT/ACRE — Dry Tons Applied per Acre lb/ac — Pounds per Acre Metals (lbs/ac) As — Arsenic Cd — Cadmium Cr — Chromium Cu — Copper Pb — Lead Hg — Mercury Mo — Molybdenum Ni — Nickel Se — Selenium Zn — Zinc Nutrients (lbs/ac) PAN — Plant Available Nitrogen P — Phosphorus K — Potassium Annual Totals — lbs/ac applied during the calendar year. Cumulative Totals — lbs/ac applied during the lifetime of field use. ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Pilgrim's Pride Corporation WQ Permit #: WQ0028653 Field #: 1 Acres Utilized: 9.74 Owner: Pilgrim's Pride Corporation Annual Dry Tons Applied: 27.48 Site #: 1 Acres Permitted: 9.74 Operator: Pilgrim's Pride Corporation Predominat Soil Series StA Cation Exchange Capacity (non 503): NA Crop 1 Name: Fescue Crop 1 Max PAN: 176.00 Crop 2 Name: NN1A Crop 2 Max. PAN #N/A 3 p fD o Snecify Totals Per Acre o o Solids As Decimal Volume Applied per Acre DT Ac Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc.) Site Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. Inches 3 o a �. O w 0. ' < _: w w * N * w 0 K S' m * 0, TKN m k g z a GO o m k 19 Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Must Select Crop 1 or Crop 2 Gal. Cu.Yd. Report p Totals in Gal. Crop 1 Crop 2 Crop 1 Crop 2 Oct-20 204,000 20,945 3.23 2.82 Pilgrim's Pride WTP S 0.50 0.40 28,300 1,390 155 65.53 X TOTALS: 20,945 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime A lied Annuallbs/acre 0.09 0.02 0.00 0.80 0.07 0.00 0.04 0.14 0.09 0.40 10.27 65.53 0.00 Date lbs/ac Current Cumulative lbs/acre 0.90 0.23 NA 87.44 2.23 0.04 NA 2.92 0.41 8.70 0.81 0.21 NA 86.64 2.16 0.04 NA 2.78 0.32 8.30 36 34 NA 1,338 267 15 NA 374 89 2,498 176.00 Aug-05 2,600 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accoraance witn a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are signM t penaltie for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation ` **Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading POft FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Pilgrim's Pride Corporation WQ Permit #: WQ0028653 Field #: I Acres Utilized: 16.90 Owner: Pilgrim's Pride Corporation Annual Dry Tons Applied: 84.05 Site #: 2 Acres Permitted: 16.90 Operator: Pilgrim's Pride Corporation Crop 1 Name: Fescue Predominat Soil Series Crop 1 Max PAN: 180.00 ToB Crop 2 Name: Cation Exchange Capacity (non 503): HN/A Crop 2 Max. PAN NA #N/A p o �- o '' Specifv Totals Per Acre o /o Solids As Decimal Volume Applied per Acre DT Ac Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc.) Site Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches D 3 v s - 0 c� a < � =: F w * N * ° o' � K 5' � g m * * m TKN m k . Z Y 00 CD = c �' mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Must Select Crop 1 or Crop 2 Gal. Cu-.Yd-. Report Totals in Gal. Crop 1 Crop 2 Crop 1 Crop 2 Oct-20 624,000 36,923 3.23 4.97 Pilgrim's Pride WTP S 0.50 0.40 28,300 1,390 155 115.52 X TOTALS: 36,923 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.16 0.03 0.00 1.41 0.12 0.00 0.08 0.25 0.16 0.70 18.10 115.52 0.00 Date lbs/ac Current Cumulative lbs/acre 0.58 0.10 NA 44.51 0.44 0.02 NA 0.71 0.36 2.97 0.43 0.07 NA 43.10 0.32 0.02 NA 0.46 0.20 2.27 :.. . 36 34 NA 1,338 267 15 NA 374 89 2,498 . :::::..:.:...:.:.:. .. . :. ..:.:.:.::: . :: .....:.. .. ::::::::::::::::.:.:::. ::::... 180.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my durection or supervision in accoraance witn a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significa enalti submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading $ft FORM FSF (12/2006) RESIDUAL ANALYSIS LAB SHEETS (2) WayPAoint„ NALYTICAL 8/25/2020 Branch Residuals and Soils LLC Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill, SC, 29732 Ref: Analytical Testing Report Number: 20-226-0012 Project Description: Pilgrims Pride Alum 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Dear Bob Branch: Waypoint Analytical Virginia, Inc. received sample(s) on 8/13/2020 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, 4 � ' L d C-ir Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 6 (2) 7621 Whitepine Road, Richmond, VA 23237 Waypoint. Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 20-226-0012 Client Project Description: Pilgrims Pride Alum Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 73367 Pilgrims Pride Sanford Solids 08/13/2020 08/13/2020 SM-4500-NH3C WP MTN 73367 Pilgrims Pride Sanford Solids 08/13/2020 08/13/2020 SM-4500-NH3C-TKN WP MTN 73367 Pilgrims Pride Sanford Solids 08/13/2020 08/13/2020 4500NO3F-2011 WP MTN 73367 Pilgrims Pride Sanford Solids 08/13/2020 08/13/2020 6010D WP MTN 73367 Pilgrims Pride Sanford Solids 08/13/2020 08/13/2020 SW-7471B WP MTN 73367 Pilgrims Pride Sanford Solids 08/13/2020 08/13/2020 9045D WP MTN 73367 Pilgrims Pride Sanford Solids 08/13/2020 08/13/2020 SM-254OG WP MTN WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 2 of 6 (1r�•--`y7•ry�f Waypoint ANALYTICAL 46368 Branch Residuals and Soils LLC Project Bob Branch 1735 Heckle Blvd Information Suite 103-291 Rock Hill , SC 29732 Report Number : 20-226-0012 Lab No : 73367 Sample ID: Pilgrims Pride Sanford Test 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Pilgrims Pride Alum REPORT OFANALYSIS Results Units MQL Report Date : 08/25/2020 �Received: 08/ 13/2020 L M t CwQp Wy Pauric Mc Groary Ph.D., CPA Agronomist Matrix: Solids Sampled: 8/13/2020 0:00 DF Date / Time By Analytical Analyzed Method Moisture 96.8 % 0.010 1 08/17/2016:32 FMM SM-2540G Test Results Units MOL DF Date /Time Analyzed By Analytical Method Ammonia Nitrogen 1390 mg/Kg - dry 781 1 08/20/20 15:00 JPJ SM-4500-NH3C Nitrate+ N itrite- N <155 mg/Kg - dry 155 1 08/18/20 15:47 ZBD 4500NO3F-2011 PH 6.7 S.U. 1 08/18/2015:20 ADM 9045D Total Solids 3.23 % 0.010 1 08/17/20 16:32 FMM SM-2540G Total Kjeldahl Nitrogen 28300 mg/Kg - dry 7810 1 08/20/20 10:00 JPJ ;M-4500-NH3C-TKP Phosphorus 1820 mg/Kg - dry 156 1 08/18/20 20:51 TJS 6010D Aluminum 178000 mg/Kg - dry 156 1 08/18/20 20:51 TJS 6010D Arsenic <15.6 mg/Kg - dry 15.6 1 08/25/20 04:43 ]ADS 6010D Calcium <1560 mg/Kg - dry 1560 1 08/18/20 20:51 TJS 6010D Cadmium <3.13 mg/Kg - dry 3.13 1 08/18/20 20:51 TJS 6010D Copper 142 mg/Kg - dry 15.6 1 08/25/20 04:43 ]ADS 6010D Iron 15800 mg/Kg - dry 313 1 08/18/20 20:51 T]S 6010D Lead 12.3 mg/Kg - dry 9.38 1 08/25/20 04:43 ]ADS 6010D Magnesium 888 mg/Kg - dry 156 1 08/18/20 20:51 T]S 6010D Mercury <0.481 mg/Kg - dry 0.481 1 08/19/20 11:42 DDB SW-7471B Molybdenum <7.81 mg/Kg - dry 7.81 1 08/18/20 20:51 TJS 6010D Nickel 25.1 mg/Kg - dry 7.81 1 08/25/20 04:43 ]ADS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 3 of 6 0 7621 Whitepine Road, Richmond, VA 23237 waypoint Main 804-743-9401 ° fax 804-271-6446 ANALYTICAL www.waypointanalytical.corn 46368 Branch Residuals and Soils LLC Project Pilgrims Pride Alum Bob Branch Report Date : 08/25/2020 1735 Heckle Blvd Information : Received : 08/13/2020 Suite 103-291 C�2o w'V Rock Hill , SC 29732�'t Pauric Mc Groary Ph.D., CPA Report Number : 20-226-0012 REPORTOFANALYSIS Agronomist Lab No : 73367 Matrix: Solids Sample ID : Pilgrims Pride Sanford Sampled: 8/13/2020 0:00 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Potassium 691 mg/Kg - dry 313 1 08/25/20 04:43 JADS 6010D Selenium <15.6 mg/Kg - dry 15.6 1 08/25/20 04:43 JADS 6010D Sodium 1030 mg/Kg - dry 781 1 08/18/20 20:51 TJS 6010D Zinc 70.6 mg/Kg - dry 39.1 1 08/25/20 04:43 ]ADS 6010D Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit L Limit Exceeded Page 4 of 6 • 7621 W -7 Road, Richmond, Waypoint Main n 27 -6446 804-743-9401 'Fax 804-271-b446 80 ANALYTICAL www.waypointanalytical.com Shipment Receipt Form Customer Number: 46368 Customer Name: Branch Residuals and Soils LLC Report Number: 20-226-0012 Shipping Method Fed Ex US Postal Lab Other UPS Client Courier Thermometer ID: Shipping container/cooler uncompromised? 0 Yes No Number of coolers/boxes received F1 Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of Custody (COC) present? Yes No COC agrees with sample label(s)? Yes No COC properly completed Yes No Samples in proper containers? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test(s)? Yes No All samples received within holding time? Yes No Cooler temperature in compliance? Yes No Cooler/Samples arrived at the laboratory on ice. Yes No Samples were considered acceptable as cooling process had begun. Water - Sample containers properly preserved Yes No N/A Water - VOA vials free of headspace Yes No N/A Trip Blanks received with VOAs Yes No N/A Soil VOA method 5035 — compliance criteria met Yes No N/A r High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr) High concentration pre -weighed (methanol -14 d) [_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? Comments: Yes 0 No L Signature: Brandi Watson Date & Time: 08/13/2020 1237.44 Page 5 of 6 The followiparameters nerd to be analyzed on sample Pilerim; Pride Alum Re�:,ular Nutrient and Metal Residuals Analysis Arsenic Lead / Nickel ✓ Aluminunlo." O "hotal Solids Potassium-/ C'alCiLIIIl, Iron Collected on: Collected by: Bob Branch Branch Residuals & Soils ;36 510-0340 Cadnliu111 N,lercury ---� Selenium An1111onia-Nitrogen plI TIN ./ N,laL;nes1U111 g.l ;,2020 Project: Pilgrims Pride Sanford Project No 2007-66 Copper I/ ,MoIN'bdcnunI zinc'' Nitrate -Nitrite Nitrogen Phosphorus ✓ Sodlll111./ �� ,�, t, .b I D _6D 'Dw Tx Page 6 of 6 TOXICITY CHARACTERISTICS LEACHING PROCEDURE (TCLP) ANALYSIS REPORT TOXICITY CHARACTERISTICS LEACHING PROCEDURE (TCLP) ANALYSIS REPORT TCLP analyses are required once every five years by permit. PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION The current permit, WQ0028653, does not have vector attraction requirements but does have Class A requirements for pathogens. The form is marked to reflect these requirements. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Pilgrim's Pride Corporation WQ Permit Number: WQ0028653 WWTP Name: Pilgrim's Pride Corporation Sanford NC WTP _ NPDES Number: PWS 03-53-130 Monitoring Period: From 1/l/2020 To 12/31/2020 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/tem) [7 All B (Alk Treatment) ❑ Alt. C (Prior Testing) 17 A1t.D (No Prior Test) ❑ 1 Process to Farther Reduce Padloseggs U If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Li Heat Drying ❑ Heat Treatment ❑ Thetmo hilic U Beta Ra ❑ Gamma Ray p Pasteurization ❑ Class B: Alt. 1) Fecal Density ❑ 1 Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed Class B only) indicate "Process to Si uificantly Reduce Pathogens": Lime Stabilization ElAir Drying�❑ Composting ❑ jAerobic Digestion D Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the followmit monitoring data: Parameter Allowable Level in Sludge 8 Pathogen Density Numoer at Excee- Frequency of Analysis Y Sample Type aly ica Tech- nimp inimu Geo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) 5.19 7.124817 24.9 Gram' 0 Annually Grab 18 922 I C E , Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) vector Attraction Reduction (15A IVCAC 02T .1107) -Please indicate alternative performed - Alt. 1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-daybench) Alt. 4 (Spec. OZ uptake) 0 Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) J jAlt. lNo 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) 1-] vector attraction reduction alternatives were performed O CERTIFICATION STATEMENT (please check the appropriate statement) El "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the my system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and Imprisonment." Ms. Tina Pedley, WTP Lagoons ORC Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date DENR FORM DMSDF (12/2006) PATHOGEN AND VECTOR ATTRACTION REDUCTION DOCUMENTATION PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION DOCUMENTATION The current permit, WQ0028653, does not have vector attraction requirements but does have Class A requirements for pathogens. Documentation is attached to reflect these requirements. Pilgrim's Pride VffP Sanford, North Carolina WQ0028653 August, 2020 Data Analyzed Uab........... .............. ........... ............. r. M . ..... ............ .............. 86099-01 7 0.824 86099-02 6 0.808 86099-03 6 0.780 86099-04 5 0.715 86099-05 5 0.720 86099-06 5 0.726 86099-07 25 1.396 Mean Colonies / Gram ............. Average 0.8.53. Fecal Coliform/gram Fecal Col-iform values are less than 2,000,000 and meets the Class B pathogen reduction requirement 5 y { S'rwssii s p r., r « �t tt t 1! i� S 6 •� r For: Branch Residuals & Soils 1735 Heckle Blvd Suite 103-291 Rock Hill, SC 29732 Attn: Bob Branch Client Sample ID: PP1 Site: Branch Residuals & Soils Parameter Method % Solids SM 2540B Fecal Coliform SM 9221 C E-2006 Result 270 <6.67 Client Sample ID: PP2 Site: Branch Residuals & Soils Parameter Method Result Solids �_...__—.....__.__.�__._.--.. 5M 2540E .._ �_--- -- 3.08 Fecal Coliform SM 9221 C E-2006 6.42 Report of Analysis 8/13/2020 11111111!ll1t'f! ♦�,..� ti- Cy,9 w CC ° • cn r iq NC #34 z: NC 937701 Lab Sample ID: 86099-01 Collection Date: 8/12/2020 12:17 Units —Analvst Analvsis Date/Time — % AW 8/12/2020 mpn/g TS BJ 8/12/2020 1710 Lab Sample ID: 86099-02 Collection Date: 8/12/2020 12:20 Units Analyst Analysis DatelTime % AW 8/12/2020 mpn/g TS BJ 8/12/2020 1710 Client Sample ID: PP3 Lab Sample ID: 86099-03 Site: Branch Residuals & Soils Collection Date: 8/12/2020 12_25 — Parameter Method Result Units Analyst Analysis Date/Time % Solids SM 2540B 2.94 % AW 8/12/2020 Fecal Coliform SM 9221 C E-2006 <6.03 mpn/g TS BJ 8/12/2020 1710 Client Sample ID: PP4 Lab Sample ID: 86099-04 Site: Branch Residuals & Soils Collection Date: 8/12/2020 12_28 Parameter Method Result Units Analyst Analysis DatelTime Solids SM 2540B 3.38 % AW 8/12/2020 Fecal Coliform SM 9221 C E-2006 <5 19 mpn/g TS BJ 8/12/2020 1710 P 0 Box 473 106 Short Street Kernersvdle. North Carolina 27284 Tel 336-996-2841 Fax: 336-996-0326 www randalabs corn Page 1 Client Sample ID: PP5 Site: Branch Residuals & Soils Parameter Method % Solids SM 2540B Fecal Coliform SM 9221 C E-2006 Client Sample ID: PP6 Site: Branch Residuals & Soils Parameter Method % Solids SM 2540B Fecal Coliform SM 9221 C E-2006 Client Sample ID: PP7 Site: Branch Residuals & Soils Parameter Method % Solids SM 2540B Fecal Coliform SM 9221 C E-2006 Report of Analysis 8/13/2020 Lab Sample ID: 86099-05 Collection Date: 8/12/2020 12.32 Result Units Analyst Analysis Date/Time 3.45 % AW 8/12/2020 <5.25 mpn/g TS BJ 8/12/2020 1710 Lab Sample ID: 86099-06 Collection Date: 8/12/2020 12:36 Result Units Analyst Analysis Date/Time 3.36 % AW 8/12/2020 <5.32 mpn/g TS BJ 8/12/2020 1710 Lab Sample ID: 86099-07 Collection Date: 8/12/2020 12:40 Result Units Analyst Analysis DatelTime 312 % AW 8/12/2020 24.9 mpn/g TS BJ 8/12/2020 1710 NA = not onolyzed P O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel- 336-996-2841 Fax' 336-996-0326 www randalabs corn Page 2 RESEARCh & ANA[yTiCAl LABORATORIES, INC. CHAIN OF CUSTODY RECORD Analytical / Process Consultations Phone (3361996-2841 1 WAl ER I WASTEWATER COMPANY 6 -1 S'v 'I j JOB NO c z n- /q.- 0 IZ RECUESTED ANA Lyllo STREr:T ADUR�:SS PR(,)Jt I" S p- ZIP SAN3ELER HSAE (PLFASC I'llipil) CONTACT PHOUE sl �'%ILE 1,"%1111 U." DATE TIME SAMPLFR SIGNgTIIRE J SAMPLE LOCATION 11.0- - - - - - - - - - - -H±L- REdmDU'l-i ED BY �'7 ..lw Ut f ET t,! E 'N� I R E CF 1-1 REMARKS: SAMPLE TEMPERATURE AT RECEIPT RELINCUISIlDBY DATE"W4E U-0- SOIL ANALYSIS REPORT SOIL ANALYSIS REPORT Soil Samples were sent to a lab for testing. Results are not available at the time of the report. Lime will be added if needed. Soil samples will be provided as soon as they are available from the lab. 2020 APPLICATION SUMMARY TABLE PILGRIM'S PRIDE CORPORATION SANFORD, NC WATER TREATMENT PLANT MARKETING AND DISTRIBUTION PROGRAM PERMIT NO. WQ0028653 2020 APPLICATION SUMMARY Tract/ Dry Tons / Farmer Site Field Acres Date Spread Gallons Dry Tons Acre Crop PAN Pilgrim's Pride 1 1 9.74 Oct-20 204,000 27.48 2.82 Fescue 65.53 2 16.9 Oct-20 624,000 84.05 4.97 Fescue 115.52 Totals I 1 L. 26.64 . 828 000 111.52 Branch Residuals & Soils, LLC Confidential 2/3/2021 Page 1 2020 APPLICATION CONDITION SUMMARIES Pilgrim's Pride WTP Sanford, North Carolina Denali Water Solutions WQ0028653 Annual 2020 Water Treatment Plant Farmer: Pilgrim's Pride Acres: 9.74 Site/Tract: 1 Application Method: Surface Field: 1 Percent Solids : 3.23 Residual Report No.: 20-226-0012 Crop: Fescue ..... . .... Date Field No. Subfield Gallons Soil Conditions Weather Conditions Prev. 24 Hour Rainfall 10/19/20 1 186,000.0 Moist Warm, Clear 0.00 10/20/20 1 18,000.0 Moist Warm, Clear 0.00 a Gallons `204;90Total Q,0 Pilgrim's Pride WTP Sanford, North Carolina Denali Water Solutions WQ0028653 Annual 2020 Water Treatment Plant Farmer: Pilgrim's Pride Acres: 16.9 Site/Tract: 1 Application Method: Surface Field: 2 Percent Solids : 3.23 Residual Report No.: 20-226-0012 Crop: Fescue Date Field No. Subfield Gallons Soil Conditions Weather Conditions Prev. 24 Hour Rainfall 10/20/20 2 156,000.0 Moist Warm, Clear 0.00 10/21/20 2 168,000.0 Moist Warm, Clear 0.00 10/23/20 2 186,000.0 Moist rm, Partly Clo 0.00 10/23/20 2 114,000.0 Moist rm, Partly Clo 0.00 Total Gallons 62� 004 0