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Home My WebLink AboutNCG030006_MONITORING LAB REPORT_20190725aceAnalytr'cal fNetlarialCenterlorTestingBlnnovetfon I ANALYTICAL REPORT August 01, 2019 Piedmont Geologic Sample Delivery Group: Samples Received: Project Number: Description: Site: Report To: L112 2303 07/25/2019 1751 ABB Inc. PINETOPS, NC Pete Dressel 6003 Chapel Hill Rd Ste 145 Raleigh, NC 27607 Entire Report Reviewed By: 4�j Heather J Wagner Project Manager Results relate only to the Items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where appllcabie, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV•SOP•MTJL-0067 and k; ENV-SOP-MUL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, . and as the samples are received. ACCOUNT: PROJECT: Sli DATEMME: PAGE: Piarimnnt r:cnl—I, 17G7 1.11777[1Q - nRln111Q 1ii.11r) 1 of 17 TABLE OF CONTENTS ONE LAB, NATIONWIDE, 40 Cp: Cover Page Tc: Table of Contents Ss: Sample Summary Cn: Case Narrative Sr: Sample Results OUTFALL-001 L1122303-01 Qc: Quality Control Summary Gravimetric Analysis by Method 2540 D-2011 Wet Chemistry by Method 1664E Metals (lCP) by Method 200.7 Metals (ICPMS) by Method 200.8 GI: Glossary of Terms Al: Accreditations & Locations Sc: Sample Chain of Custody 1 2 FP 3 4 Fs5 5 F 6 rsr 7 ro$ C 9 F 10 11 F 12 Sc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: P iPrimnnt f;onlnnir 17ri1 i 1"?'4f14 nA1l1111q 1,9.in 7 of 19 SAMPLE SUMMARY ONE LAB, NATIONWIDE. Collected by Collected dateltime Received dateltime OUTFALL-001 L1122303-01 WW Nathan Beauchamp 07123n915:50 07/25l1908:45 `J e'.h ;d Balch Dilution Preparation Analysis Analyst Location dateltime dateltime GravimetriC Analysis by Method 2540 D-2011 WG1317766 1 07/2V91522 07128n915:52 TH Mt. Juliet, TN Wet Chemistry by Method 1664B WG1320160 1 07/30/19 07.49 07/3V1912:39 AMG Mt. Juliet, TN Metals VCP) by Method 200.7 WG1317669 1 0712711914:09 07/29A910:41 CCE Mi. Juliet, TN Metals (VMS} by Method 200.8 WG1318106 1 07128l1919:09 07129/19 08:48 LAT Mi, Juliet, TN ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Ala'l nm f=onlnnir . 17S5 I eE9�-Zn9 ownwo ig to 'A of 17 C096100VA \ MA IM ONE LAB, NATIONWIDE. All sample aliquots were received at the correct temperature, in the proper containers, with the FP appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FTChave been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FS knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. 0 Fr 4�Z ro-C F Heather J Wagner Project Manager E E ACCOUNT: PROJECT: S DG: DATEM ME: PAGE: Pig Ni not r-ni—ir .17ci1 1 1077(1q (lg niiiq 1A.1f1 d nf.17. OUTFALL-001 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. � Collected daleltime: 07123119 15:50 1-1122303 Additional Information Result Units FP Analyte pH (On Site) 7.4 su C FT Gravimetric Analysis by Method 2540 D-2011 F Result Qualifier RDL DilutionAnalysis Batch Analyte ug11 ugtl date I time F Suspended Solids 60000 25000 1 07/281201915:52 WG1317766 Wet Chemistry by Method 1664B 0 Result Qualifier RDL Dilution Analysis Batch 6 Analyte ug11 ugll date 1 time Q C TPH - Oil & Grease ND 5810 1 07131/201912:39 WG1320160 El Metals (ICP) by Method 200.7 Result Qualifier RDL Dilution Analysis Batch `AI Analyte ug/I ugn date 1 time Lead ND 5.00 1 07/291201910:41 WG1317669 9 Zinc ND 50.0 1 071291201910:41 WG1317669 SC Metals (ICPMS) by Method 200.8 Result Qualifier RDL Dilution Analysis Batch Analyse ugll ugly date 1 time Copper 2.66 1.00 1 07/29/2019 08:48 WG1318106 ACCOUNT: PROJECT: SDG: DATElTIME: PAGE: Alorimnnt r,anlnnlr 1761 1 I'1737M nAN11AC 1A•1r1 S of 19 WG1317766 Gravimetric Analysis by Method 2540 D-2011 QUALITY CONTROL SUMMARY L1122303.01 ONE LAB. NATIONWIDE. Method Blank (MB) (MB) R3435574-1 07128/1915:52 HIB Result MB Qualifier MB MDL M3 RDL Analyte ugA ug/I ugA l C Suspended Solids U 350 2500 L1122139-01 Original Sample (OS) • Duplicate (DUP) Fn] (OS) L1122139-01 07/28n9 15:52 • (DUP) R3435574-3 07/2BA915:52 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Sr Analyte ugA ugA % % Suspended Solids 36000 33000 1 8.70 P1 5 Laboratory Control Sample (LCS) 7G1 (LCS)R3435574-2 07128/1915152 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier 7 —71 Analyte ugA ug/I % % Suspended Solids 773000 776000 100 85.0-115 9Sc ACCOUNT: PROJECT: SOG: DATEMME. PAGE: WG1320160 QUALITY CONTROL SUMMARY ONE LAS. NATIONWiDE. Wet Chemistry by Method 1664B L1122303-01 Method Blank (MB) i Cp (MB) R3435995-1 07/31/19 12:39 MB Result MB Qualifier MB MDL MB ROL Analyte ugA ug4 ❑gll TPH - Oil & Grease U 725 5000 3 Ss Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) [TCn] (LCS) R3435995-2 07/31179 12:39 • (LCSD) R3435995-3 070119 12:39 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec, Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ugA ugll ugll % % % % % FrTPH - 0i1 & Grease 20000 21200 20000 106 100 64.0-132 5.33 34 'GI �AI 9 S� ACCOUNT: PROJECT: SDG3 DATEMME: PAGE' WG1317669 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Metals (ICP) by Method 200.7 L1122303.01 Method Blank (MB) FP1 (MB) R3435267-1 07129/19 10:24 MB Result MB Qualifier MB MDL MB RDL 'TC Analyte ugA ugA ugA Lead 2.52 J 2.00 5.00 FS Zinc 5.48 J 3.40 50.0 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) 4Cn (LCS) R3435267-2 07/29/19 10:26 • (LCSD) R3435267-3 07/29/19 10:29 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Sr r Analyte ugA ugp ugA % % % % % Lead 1000 1030 1020 103 102 85.0-115 0.567 20 Zinc 1000 1040 1040 104 104 85.0-115 0.189 20 7G1 L1121822-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (05) U121822-01 07/29/19 10:31 • iMSJ R3435267-5 07/29/19 10:36 - (MSD) R3435267.6 07/29/19 10:39 aAl Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ugA ugA ugA ugA % % % % % g SC Lead 1000 ND 1060 1030 105 103 1 70.0-130 2.39 20 Zinc 1000 ND 1080 1050 106 104 1 70.0-130 2 40 20 L1122303-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1122303-01 07/29/19 10:41 • (MS) R3435267-7 07/29/19 10:44 • (MSD) R3435267-8 07/29/19 10:46 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec, Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ugA ugA ugA ugA % % % % % Lead 1000 ND 1050 1020 104 102 1 70.0-130 2.39 20 Zinc 1000 00 1076 1050 105 104 1 70.0-130 1.17 20 ACCOUNT: PROJECT: SDG: DATVTIME: PAGE: WG1318106 QUALITY CONTROL SUMMARY ONE LAB, NATIONWIDE. Metals (ICPMS) by Method 200.8 L1122303-01 Method Blank (MB) (MB) R3435178-1 07/29/19 08:01 El MB Result MB Qualifier MB MDL MB RDL Analyte ugll ugA ugA ITC Copper u 0.270 1.00 �Ss Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) F�n] (LCS) P3435178-2 07729/19 08;05 • (LCSD) R3435178-3 07/29119 08:08 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec- Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ugA ugll ugA % % % % % $ Sr Copper 50.0 49.1 48A 96.1 96.8 85.0-115 0.649 20 L1122427-01 Original Sample (OS) - Matrix Spike (MS) • Matrix Spike Duplicate (MSD) 7 (OS) L1122427-01 07/29/19 08:11 - (MS) R3435178-5 07/29/19 0818 - (MSD) R3435178-6 07/29119 08:21 GI Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ugA ugll u9A ugA % % % % % UAI Copper 50.0 ND 47.6 46.8 94.7 92.9 1 70.0-130 1.86 20 FC L1122831-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1122831-01 07129/19 08:25 • (MS) R3435178-7 07129/19 08:28 - (MSD) R3435178-8 07/29/19 08:31 Spike Amount Original Result M5 Result MSD Result M5 Rec. MSD Rec. Dilution Rec- Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ugA ugll ugA ugll % % % % % Copper 50.0 ND 48.7 48.7 96.2 96.3 1 70.0-130 0.0493 20 ACCOUNT: PROJECT: SDG: DATETTIME: PAGE: GLOSSARY OF TERMS ONE LAB_ NATIONWIDE. 4* Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not F intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit limits, Project Name, FTCSample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received. and Definitions ESAbbreviations MDL Method Detection Limit, ND Not detected at the Reporting Limit (or MDL where applicable). En: RDL Reported Detection Limit. Rec. Recovery. s RPD Relative Percent Difference. Sr SDG Sample Delivery Group. U Not detected at the Reporting Limit (or MDlL where applicable). C IQ Analyze The name of the particular compound or analysis performed, Some Analyses and Methods will have multiple analyzes reported. If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the Dilution standa,d, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. F These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. 9 The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control Original Sample SC sample. The Original Sample may not be included within the reported SDG. This column provides a letter anWor number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. if there was no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry) Confidence level of 2 sigma. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (Oc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report wM provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary {Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description J The identification of the analyte is acceptable; the reported value is an estimate. Pi RPD value not applicable for sample concentrations less than 5 times the reporting limit. ACCOUNT: PROJECT: SDG: DATE/'TIME; PAGE: .Piarirnnnr ranlnnir nsi i mvvn� nQrnviq 1R fin In of 19 ACCREDITATIONS & LOCATIONS ONE LAB, NATIONWIDE. Pace National is the only environmental laboratory accreditedlcertiried to Support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our Industry. The most significant benefit to ourone location design is thedesign ofour laboratorycampus. The model is conducive toaccelerated productivity, decreasing Ep turn -around time, and preventing cross contamination, thus protecting sample integrity. Our Focus on premium quality and prompt service allows us to he YOUR LAB OF CHOICE. Not all certifications held by the laboratory are applicable to the results reported in the attached report. Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. FTc State Accreditations Alabama _ 40660 _ _ — Nebraska - NE-OS-15-05 _- 3 SS Alaska _ 17.026 — Nevada TN-03-2002.34 Arizona AZ0612 New Hampshire 2975 Arkansas 68-0469 New Jersey-NELAP TN002 F California 2932 New Mexico' n1a Colorado TN00003 New York 11742 F Connecticut PH-0197_ Carolina Env37S Florida E87487 _North North Carolina' DW21704 _ - Georgia — NELAP North Carolina 41 _ Georgia 9 923 �- �� —. -. North Dakota R-140 _C rQ Idaho TN00003�� Ohio-VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 -- Oregon TN200002 E Iowa - 364 —-- Pennsylvania 68-02979 Kansas _ _ -- E-10277 -�- _ - Rhode Island _ LA000356 _ Kentucky 16 90010 South Carolina_—_ 84004 Kentucky 7 16 -South Dakota _ -� nla Louisiana A130792 Tennessee' ` 2006 Louisiana ` LA180010 Texas T104704245.18-15 Fc Maine TN0002 Texas s LABO152 Maryland _ _324 _ Utah TN00003 Massachusetts _M-TNO03 Vermont - VT2006 Michigan 9958-_-_-___ Virginia........_..._ __�__.._..._..»........-_._.-_ 460132....-._--....._.__ Minnesota 047-999-395 Washington C847 Mississippi TN00003 West Virg in is 233 Missouri 340 _ Wisconsin R980939910 Montana CERTGO86 Wyoming A21 Third Party Federal Accreditations A2LA - ISO 17025 _ 1461,01 AIHA-LAP,LLCEMLAP 100789 _ ARA - ISO 17025 s 1461,02 DOD 1461.01 Canada 1461,01 USDA P330-15-00234 EPA-Crypto T N00003 ' Drinking Water z Underground Storage Tanks 'Aquatic Toxicity ° ChemicaUMicrobiological 'Mold 6 Wastewater nla Accreditation not applicable Our Locations Pace National has sixty-four client support centers that provide sample pickup andlor the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. Pace National performs all testing at our central laboratory, T WA Mi tA T NO OR MN T ID SD T VA NY T T WYMI A PA TOHT NV T UT T COT T IL Ify WV CA KS MO T KY VAT T TAZ NM O� AR ? T T SC MS AL GA T TX ! LA �S T AK T T p FL ACCOUNT: PROJECT: Si DATFJTIME: PAGE: PiPrimnnt r,.nlnnin 1757 -... I.31i'i4(19 f1p)ni/iq 1prin 11 of 11 • Billing information: Anatysi5IContainer/Preservative Chain OfCuzurdY PageotPiedmont Geologicaccounts Llh;- Payable 6003 Chapel Hill Rd Ste 145CEka is 6003 Chapel Hill -Rd Raleigh, NC 27607 f Ste 145 unlaioFr WC 77Kn7 _ Report to: Emait To: pjdressel@Dpledmontgeologiccorn; , L, s F 12M$ Lebanon Rd Pete D_tessel, + imurphreyfpledmontgeoiogic:com:AW. - MowNiofe67N121P2 rrone6tsTsa-sass ' Project Clry/State Collected: pjoAaer �J.r C. ! fir,. Z U IrZ '- »„• -us ' � e -1. �r f3" F , Pt+u+e: a00.767.5659 Fs�:67S-75F5659 Q Description: ABS Inc. sk y.' f 1 tf , fit! , • ivJ b 2•- ? j y aient Project # ca Lab Project # Phone:919.854.9700 r 1751 PIEGEO-ABS 0. ; ;�:. Fax: 919-8S4-9532 , =+s u _ _' 4•_ �_ ❑�� ► p:, ti ..'r-i _ Collected by (Print : Slte/Faaflity tR p P.R. # ,� ( itcctritrm P1EGE0 IUa+41,Ax eta-e%rRn,� PINETOPS, NC f i4• Oash: 4e } Template T129400 " Collected by (signature): Quote q Rush? Lab MUST Be Notified) t _3 4 4c�Ritf^ same Day Five Day � U 2 y'¢ ' ; '", a �i F!relogtn P707.494��1,� Next Day 5 Day (Rad Only) Date Results Needed � - V i, W 873�`Heather,J 4V`agner � immediately 4 Two Day 10 Day fftd Only) Nc Three Day Z' ^ ` w ° ^" •+ "L y� * =�' w a PB'-'! `t Paeked on tce N Y bf, jN L U+ {7`? y; °kr •� t ntrs Shipped Via. FedEX�GTound: - Sample ID comp/Grab Matrix • Depth Date Tim y .m„'• .�`' "� -E �;' �.' •Remxik! SarrlPki{I+b Dory) OLITFALL=001 �� WW 7 i �S0 ,x- x _ Xs _y,.�, ; '+, ; OF."J , _ a r ' -� �1�' E Y + _ - _ _ � _x=•. r .SK IT �� .! - rye �..nA � •� 1 - - - aa: a-. ,tl4 . ;n'�;.�7•4--: y �:.f � _ � S�ek. - +•Y':• �µ a'� t w• ' 1 MN +- _ _ i r � �� - �.. •.11 +"�- 't- �� tic' k 4 ' Matrix emarks: r SS • sail Ail; •Air ! - Ftlier ! + *_ 2C Present /Into_ c NP ; yrY�, • l{' H Tem P p y5eaV ` GW - Groundwater B = $lcassay *fit %Sr > N €, _''�9igned/Accuzaca? VutN -wastewater ' ` +':_ 6 plow Other eoYrecC.bottlesiused; � �i �{ XN iF W""Diinki+ig'Wa1 , Satre 1 e sir* .. 'r `F ry � 5uff2clsat'volume.serst': 1j!{`. OT = Other uPS Fedi x Louder r�x y Trackrn&_ a /!/5�. : �... f �" VOIt -sera. tiredspeae Pr��+a�+axpvac��po�n�,C/o►scect/�j eMeked y Relinquished by' (Signature}' - Date: Time: Received by: (Sighatur Trip Siank eceived: Ye / tJo. \[�I ;•7;. �; �r• :,� �'�-ay!i e? G1YiLU. * - yr� �r C/7 .. - J[� ! - r ! "bif��'S, as : �; a�'.. :i! :� -r.. °. w r .. •r'• 'fie �Jl�h. `f F Relinquished by : (S' n a1. Date: Time; ecei_v ature . _� ttotues Received • if preiervatian required by Login :Dateli{me n -4: _ - Re ed b t Y • - ate:.Tie: 06C ed fn la Sr iiature - s W I l? } .. , a � D• a �Ti at me: . a _t •t` `-' s ^ Hall , ; Conditt _ . -r r •. tit +, �; -�vif G .�_ -J_, '' -�