WQ0028806_Modification_20210201

Initial Review
INITIAL REVIEW
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
Is this a complete
application?* Complete App Date
r Yes r No 02/01 /2021
Project Number* WQ0028806
Applicant/Permittee Davie County
Applicant/Permittee 123 Main St, Mocksville NC 27028
Address
Is the owner in BIMS?
r Yes r No
Owner Type
Facility Name
County
Fee Category
Minor
Signature Authority
County
Davie County
Davie
Signature Authority Title
Signature Authority Email
Document Type (if
non -application)
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Is the facility in BIMS?
r Yes r No
Fee Amount
$245

Admin Reviewer
Below list any additional email address that need notification about a new project.
Email Address
Comments to be added to email notification
Comments for Kendall
Comments for RO
Comments for Reviewer
Comments for Applicant

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
........................................................................................................................................................................................................................................................................................................................................................................
Name * Brent Collins
Email Address*
[e-mail]
Project Information
.......................................................................................
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Permit Number* WQ0028806
Applicant\Permittee * Davie County
Applicant/Permittee 123 Main St, Mocksville NC 27028
Address*
Facility Name * Davie County DCAR
Phone Number*
3367511441
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
(- High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
See cover letter.
Please attach all information required or requested for this submittal to be review here.
Application Formt Engineering Rans, Specifications, Calculations, Etc.)
Permit Modification - WQ0028806.pdf 9.45MB
upload only 1 RDF docurrent. Miltiple docurrents rust be corrbined into one RDF file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper --polka*-ion is required,
be advised, applications accepted' far pre -review until both the paper and eIect-c-,i_ co1)ies nave been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments (calcs, soils report, specs, etc.)
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
MallinE address:
❑iuision of Water Resources1 Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center 1 Aft: Nathaniel Thornburg, 91° Floor, Cfice #942W
----------------------------------------------------------- -----------------------------------------
Raleih, NC 27699-1617 512 N. Salisbury St.
Far questions or problems contact Tessa Monday [e-mail] or 919.707.3560.
* W By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 1/13/2021

g
Inc.
Permit Modification
For
Davie County-WQOO288O6
Distribution of Residual Solids
(503 Exempt)
Prepared By:
EMA Resources Inc.
755 Yadkinville Road
Mocksville, NC 27028
336-751-1441
January 8, 2021
Phone [phone] — Fax [phone]
755 Yadkinville Road — Mocksville, NC 27028

January 8, 2021
Division of Water Resources
Water Quality Permitting Section
Non -Discharge Permitting Unit
1617 Mail Services Center
Raleigh, NC 27699-1617
RE: Permit Modification — WQ0028806
To Whom it May Concern:
EMA Resources is submitting the included permit modification for the Davie County —
DCAR Permit WQ0028806. We are asking to have the Cooleemee WTP #PWS0230015
added as a source to the Davie County - DCAR Permit. There are approximately 834 dry
tons of material to clean out of the 3,000,000 gallon basin. Once those residuals are
cleaned out, it is scheduled for demolition.
If you have any questions concerning this renewal, please contact Brent Collins —
Director of Technical Services
Respectfully,
Brent Collins
Director of Technical Services
brent.collins(cr�,emaresourcesinc.com
[phone]
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

Table of Contents
1. DCAR Form
2. Copy of Current Permit
3. Operation and Maintenance Plan
4. RSC Form
5. Vicinity Map, Process Flow Design
6. Quantitative Justification
7. Laboratory Analytical Reports

1. DCAR Form

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS
FORM: DCAR 11-15
L APPLICANT INFORMATION:
1. Applicant's name: Davie County
Applicant type: ❑ Individual ❑ Corporation ❑ General Partnership p Privately -Owned Public Utility
❑ Federal ❑ State ❑ Municipal ® County
Signature authority's name per 15A NCAC 02T .0106: Johnny Lambert Title: Utilities Director
Applicant's mailing address: 123 South Main St.
City: Mocksville State: NC Zip: 27028-
Telephone number: 3( , 36) 753-6001 Email Address: jlambertkdaviecoun nc.gov
2. Consultant's name: License Number (for P.E.):
Affiliation: ❑ On Staff ❑ Retained (Firm: )
Consultant's mailing address:
City: State: Zip: -
Telephone number: ( ) _- Email Address:
3. Fee submitted: $245 (See Instruction B)
IL PERMIT INFORMATION:
1. Application is for (check all that apply): ❑ new, ® modified, ® renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: W00028806
Date of most -recently issued permit: 08/06/2019
Date of most -recently certified Attachment A (if different than the permit): 08/06/2019
III. FACILITY INFORMATION:
1. Name of residuals processing facility: Cooleemee WTP
City: Mocksville State: NC Zip: 27028-
Coordinates: Latitude: 35' 48' 34" Longitude: 80. 33' 35"
Datum: NAD83 Level of accuracy: Nearest Second
Method of measurement: GPS
County where facility is located: Davie
2. Facility contact (person familiar with residuals preparation):
Name: David Nobles Title: ORC
Mailing address: PO Box 768
City: Cooleemee State: NC
Telephone number: [phone]
Zip: 27014-
E-mail address: davidnobleskyadtel.net
FORM: DCAR 11-15 Page 1 of 3

3. Is the residual process facility also the generator? ® Yes; ❑ No
If No, please specify delivery frequency and quantity of residual to be processed:
4. Length of residuals storage at facility: 1825 days (Note: the Division requires minimum 30 days storage in units that are separate
from treatment system, i.e. not in clarifiers, aeration basins, etc.)
IV. RESIDUALS QUALITY INFORMATION:
1. Specify how these residuals will be distributed:
❑ sold or given away in bags or other containers; ❑ lawn (bulk); ❑ home garden (bulk);
® other (explain); Bulk land application of liquid/cake on crop and hay/pasture land
Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a
load capacity of one metric ton or less.
2. Complete the following if residuals are to be mixed with other materials:
Type of Materials Amounts to be added
Der 1.0 dry ton of residuals (dry ton)
3. Approximate amounts of the residuals received and processed at the facility: 279 dry tons per year.
4. Approximate amounts of the final product (processed residuals) to be distributed: 834 dry tons per year.
5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and
maximum storage times prior to distribution): There are approximately 834 dry tons of material stored in a 3,000,000 gallon
basin. Once removed the basin is scheduled for demolition.
6. Does the facility have a stormwater management plan? ® Yes; ❑ No
Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled:
V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and submit the attached Residuals Source Certification and all associated documentation.
wI
Residuals Source
Certification
FORM: DCAR 11-15 Page 2 of 3

Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units)
I, , attest that this application for
has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge
the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package
may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed
this material and have judged it to be consistent with the proposed design.
North Carolina Professional Engineer's Seal, Signature, and Date:
Applicant's Certification:
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
® Yes [I No, Explain;_
I, Johnny ambert — Utilities Director
(Signature Authority's Name — PLEASE PRINT) (Title)
attest that this application for Davie County — Sparks Road Water Treatment Plant
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water
Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed
and that if all required supporting information and attachments are not included, this application package will be returned to me as
incomplete.
Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.6B, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil penalties up to $25,000 per violation.
Signature: Date: -20z/
FORM: DCAR 11-15 Page 3 of 3

2. Copy of Current Permit

ROY COOPER
Governor
MICHAEL S. REGAN
Secretary
LINDA CULPEPPER
Director
JOHNNY LAMBERT — UTILITIES DIRECTOR
DAVIE COUNTY
123 SOUTH MAID STREET
MOCKSVILLE, NORTH CAROLINA 27028
Dear Mr. Lambert:
NORTH CAROLINA
Environmental Quality
August 6, 2019
Subject: Permit No. WQ0028806
Davie County DCAR
Distribution of Class A
Residuals
Davie County
In accordance with your permit renewal request received May 17, 2019, we are forwarding
herewith Permit No. WQ0028806 dated August 6, 2019, to Davie County for the continued operation of
the subject residuals management program.
This permit shall be effective from the date of issuance through April 30, 2025, shall void Permit
No. WQ0028806 issued February 7, 2014, and shall be subject to the conditions and limitations as specified
therein. The Permittee shall submit a renewal application no later than November 1, 2024.
Please pay particular attention to the monitoring requirements listed in Attachment A for they may
differ from the previous permit issuance. Failure to establish an adequate system for collecting and
maintaining the required operational information shall result in future compliance problems.
Please note that on September 1, 2018, North Carolina Administrative Code Title 15A Subchapter
02T — Waste not Discharged to Surface Waters was readopted. Accordingly, this permit incorporates the
requirements of these rules, therefore, please take the time to review this permit thoroughly.
The Division has removed the following permit conditions since the last permit issuance dated
February 7, 2014:
➢ Old Condition III.8.h. — The condition has been removed and is no longer required.
➢ Old Condition III.9. -- A Utilization agreement is no longer required.
➢ Old Condition I1I.10. —The condition has been removed and is no longer required.
➢ Old Condition IV.6.f. —The condition has been removed and is no longer required.
➢ Old Condition VI.2. The condition has been removed as the permit is not voidable
DEQ5 North Carolina Department of Environmental Quality I Division of Water Resources
512 North Salisbury Street 1 1617 Mail Service Center I Raleigh, North Carolina 27699-1617
V)RTH rAROU ^
�^��+919.707.9000 ^�^+a�T^

Mr. Johnny Lambert
August 6, 2019
Page 2 of 2
2014:
The following permit conditions are new since the last permit issuance dated February 7,
➢ Condition II.6. -- Class A biological residual shall meet one of the vector attraction reduction
alternatives in 15A NCAC 02T A 107(a)
➢ Condition III.6. — Class A residuals may be staged at the land application site for up to 30 days
for biological residuals and 60 days for non -biological residuals.
➢ Condition 111.7. — Adequate measures shall be taken to prevent wind erosion and runoff from
the bulk Class A residual land application sites.
➢ Condition III.8.1. — If new land application sites are located within WS-I, WS-II, WS-III or
WS-IV.
➢ Condition VI.8. — This condition states that the permit shall not be renewed if the Permittee or
any affiliation has not paid the required annual fee.
If any parts, requirements or limitations contained in this permit are unacceptable, the Permittee
has the right to request an adjudicatory hearing upon written request within 30 days following receipt of
this permit. This request shall be in the form of a written petition, conforming to Chapter 150B of the North
Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail Service
Center, Raleigh, NC 27699-6714. Otherwise, this permit shall be final and binding.
If you need additional information concerning this permit, please contact Ranveer Katyal at (919)
707-3661 or [e-mail].
Sincerely,
Dinda Culpepper, Director
ivision of Water Resources
cc: Davie County Health Department (Electronic Copy)
Winston-Salem Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Laserfiche File (Electronic Copy)
Digital Permit Archive (Electronic Copy)
Central Files

NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF ENVIRONMENTAL QUALITY
RALEIGH
DISTRIBUTION OF CLASS A RESIDUALS PERMIT
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as
amended, and other applicable Laws, Rules, and Regulations
PERMISSION IS HEREBY GRANTED TO
Davie County
Davie County
FOR THE
continued operation of a residuals management program for Davie County and consisting of the distribution
of Class A residuals generated by the approved facility listed in Attachment A, with no discharge of wastes
to surface waters, pursuant to the application received May 17, 2019, and in conformity with other
supporting data subsequently filed and approved by the Department of Environmental Quality and
considered a part of this permit. The disposal of residuals is regulated under Title 40 Code of Federal
Regulations Part 257. This permit does not exempt the Permittee from complying with Federal Regulation
40 CFR Part 257.
This permit shall be effective from the date of issuance through April 30, 2025, shall void Permit No.
WQ0028806 issued February 7, 2014, and shall be subject to the following conditions and limitations:
I. SCHEDULES
1. The Permittee shall request renewal of this permit on Division -approved forms no later than November
1, 2024. [15A NCAC 02T .0105(b), 02T .0109]
II. PERFORMANCE STANDARDS
The Permittee shall maintain and operate the subject residuals management program so there is no
discharge to surface waters, nor any contravention of groundwater or surface water standards. In the
event the residuals management program fails to perform satisfactorily, including the creation of
nuisance conditions due to improper operation and maintenance, the Permittee shall immediately cease
distributing residuals, take immediate corrective actions, and contact the Winston-Salem Regional
Office supervisor. [ 15A NCAC 02T .0108(b)(1)(A)]
2. This permit shall not relieve the Permittee of their responsibility for damages to groundwater or surface
water resulting from the operation of this residuals management program. [15A NCAC 02T
.0108(b)(1)(A)]
3. Only residuals generated by the facility listed in Attachment A are approved for distribution in
accordance with this permit. [15A NCAC 02T .1101]
WQ0028806 Version 3.0 Shell Version 190710 Page 1 of 9

4. Pollutant concentrations in distributed residuals shall not exceed the following Ceiling Concentrations
or Monthly Average Concentrations, on a dry weight basis:
Parameter
Ceiling Concentration
Monthly Average
Concentration
(mg/kp)
(mg/kg)
Arsenic
75
41
Cadmium
85
39
Copper
4,300
1,500
Lead
840
300
Mercury
57
17
Molybdenum
75
NIA
Nickel
420
420
Selenium
100
100
Zinc
7,500
2,800
[15A NCAC 02T. I 105(a), 02T. I 105(c)]
5. Class A biological residuals shall meet the pathogen reduction requirements in 15A NCAC 02T
.1106(a). Exemptions to this requirement shall be specified in Attachment A. [I 5A NCAC 02T
.1106(a), 02T .1106(d)]
6. Class A biological residuals shall meet one of the vector attraction reduction alternatives in 15A NCAC
02T .1107(a). Exemptions to this requirement shall be specified in Attachment A. [15A NCAC 02T
.1107(a), 02T .1 107(c)]
7. The facilities and sites herein were permitted per the following setbacks:
a. Setbacks for Class A land application sites are as follows (all distances in feet):
Liquid Cake
Residuals Residuals'
i. Each private or public water supply source: 100 100
ii. Surface waters such as intermittent and perennial streams, perennial 100 25
waterbodies, and wetlands:
iii. Surface water diversions such as ephemeral streams, waterways, and 25 0
ditches:
iv. Groundwater lowering ditches where the bottom of the ditch 25 0
intersects the SHWT:
v. Each well with exception of monitoring wells: 100 100
vi. Bedrock outcrops:
25 0
' Unless otherwise noted in Attachment A, "cake" residuals are those that have greater than 15%
solids by weight and can be stacked without flowing, as well as can be handled, transported
and spread as a solid (e.g., using a backhoe, front end loader, slinger spreader, broadcast
spreader or other equipment designed for handling solid materials) without leaving any
significant liquid fraction behind.
[15A NCAC 02T .l 108(b)]
WQ0028806 Version 3.0 Shell Version 190710 Page 2 of 9

8. Residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in exceedance of
agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen requirements
based on the determined Realistic Yield Expectations (RYE) using any of the following methods:
a. Division's pre -approved site specific historical data for specific crop or soil types by calculating
the mean of the best three yields of the last five consecutive crop harvests for each field.
b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State
University Department of Soil Science (hq:Hnutrients.soil.ncsu.edLyields/indgx.php). A copy
shall be kept on file and reprinted every five years in accordance with Condition IV.6.
c. If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the RYE
and appropriate nutrient application rates reported in any of the following documents:
i. Crop management plan as outlined by the local Cooperative Extension Office, the North
Carolina Department of Agriculture and Consumer Services, the Natural Resource
Conservation Service, or other agronomist.
ii. Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance
Document: Chapter I
(http://www.neagr.szov/SWC/tech/documents/9th Guidance_ Doc_100109.pdf).
iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation
Services (MRCS). These plans must meet the USDA-NRCS 590 Nutrient Management
Standards(fip:op-fc.sc.cgov.usda.gov/NHO/Sractice-standards/standards/590.pdfl.
d. If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall
contact the Division to determine necessary action.
[15A NCAC 02T . 1109(a)(1)(K)]
9. Prior to distributing Class A residuals that have a sodium adsorption ratio (SAR) of 10 or higher, the
Permittee shall obtain and implement recommendations from at least one of the following: the local
Cooperative Extension Office; the Department of Agriculture and Consumer Services; the Natural
Resource Conservation Service; a North Carolina Licensed Soil Scientist; or an agronomist. The
recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a
mechanism for maintaining site integrity and conditions conducive to crop growth. The Permittee shall
maintain written records of these recommendations and details of their implementation. The Permittee
shall notify third -party entities of the effects of a high SAR content residuals on their receiving sites.
[15A NCAC 02T .0108(b)(1)(A)]
WQ0028806 Version 3.0 Shell Version 190710 Page 3 of 9

III. OPERATION AND MAINTENANCE REQUIREMENTS
1. The Permittee shall operate and maintain the residuals management program as a non -discharge system.
[ 15A NCAC 02T .1100]
2. The Permittee shall maintain a Division -approved Operation and Maintenance Plan that shall include:
a. Description of the program, and associated facilities and equipment, in sufficient detail to show
what operations are necessary for the program to function and by whom the functions are to be
conducted;
b. Description of anticipated maintenance of facilities and equipment associated with the program;
c. Include provisions for safety measures, including restriction of access to sites and equipment;
d. Spill control provisions:
i. Response to upsets and bypasses including control, containment, and remediation; and
ii. Contact information for plant personnel, emergency responders, and regulatory agencies;
e. Detailed inspection procedures:
i. Names or titles of personnel responsible for conducting inspections;
ii. Frequency and location of inspections, and procedures to assure that the selected locations and
inspection frequency are representative of the residuals management program; and
iii. Description of record keeping and actions to be taken by the inspector in the event that
noncompliance is observed;
f. Detailed sampling and monitoring procedures:
i. Names or titles of personnel responsible for conducting sampling and monitoring;
ii. Description of monitoring procedures including parameters to be monitored; and
iii. Sampling frequency and procedures to assure that representative samples are collected.
Fluctuation in temperature, flow, and other operating conditions can affect the quality of the
residuals gathered during a particular sampling event. The sampling plan shall account for any
foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to
meet pathogen and vector attraction reduction requirements.
[15A NCAC 02T .1110(a)]
Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC)
classification of the residuals management program, the Permittee shall designate and employ a
certified operator in responsible charge (ORC), and one or more certified operators as back-up ORCs.
The ORC or their back-up shall visit the facilities in accordance with 15A NCAC 08G 0204 and shall
comply with all other requirement in 15A NCAC 08G 0204. [15A NCAC 02T .0117, 08G .02041
4. The Permittee shall ensure that a copy of this permit and the Division -approved Operation and
Maintenance Plan is available when land applying bulk Class A residuals. [ 15A NCAC 02T .1110(b)]
5. The Permittee shall ensure that spill control provisions are available when transporting or land applying
bulk Class A residuals. [15A NCAC 02T .1110(a)(4)]
6. Class A residuals may be staged at the land application site for up to 30 days for biological residuals
and 60 days for non -biological residuals. Class A residuals shall be stored or staged in a manner to
prevent runoff of leachate and other wastewaters generated. [ 15A NCAC 02T .1110(c), 02T .1110(d)]
7. Adequate measures shall be taken to prevent wind erosion and runoff from the bulk Class A residual
land application sites. [15A NCAC 02T .0108(b)(1)(A)]
WQ0028806 Version 3.0 Shell Version 190710 Page 4 of 9

8. Bulk Class A residuals shall not be land applied under the following conditions:
a. If the residuals are likely to adversely affect a threatened or endangered species listed under section
4 of the Endangered Species Act or its designated critical habitat;
b. If the application causes nuisance conditions;
c. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface
water or groundwater standards;
d. If the land is flooded, frozen, or snow-covered, or is otherwise in a condition such that runoff of
the residuals would occur;
e. Within the 100-year flood elevation, unless the residuals are injected or incorporated within a 24-
hour period following a residuals land application event;
f. During precipitation events, or within 24 hours following a rainfall event of 0.5 inches or greater
in a 24-hour period;
g. If the slope of the land is greater than 10% when liquid residuals are surface applied, or if the slope
of the land is greater than 18% when liquid residuals are injected or incorporated;
h. If the land does not have an established vegetative cover crop unless the land is a Division -approved
no -till site, or the residuals are injected, or incorporated within a 24-hour period following the
application of residuals;
i. If the vertical separation of the seasonal high water table and the depth of residuals application is
less than one foot;
j. If the vertical separation of the depth to bedrock and the depth of residuals application is less than
one foot;
k. If the application exceeds agronomic rates;
I. If the land application sites are located within a WS-I watershed pursuant to 15A NCAC 02B .0212
or within the Critical Area of a WS-I1 pursuant to Sub -Item (4)(g) of Rule 15A NCAC 02B .0212,
or within the Critical Area of a WS-III or WS-IV watershed pursuant to Sub -Item (4)(h) of Rules
15A NCAC 02B .0215, and .0216.
[I5A NCAC 02T .I 109(a)(1), 02T .1109(b)]
9. The Permittee shall notify all third -party entities receiving bulk Class A residuals that land application
activities occurring on the third -parry's property shall meet the requirements in 15A NCAC 02T
.1108(b) and 02T .1109(a)(1) (i.e., Conditions II.7.a. and III.8., respectively). [15A NCAC 02T
.1103(a)(4), 02T .1103(a)(5)]
10. Bagged or other container Class A residuals shall have an affixed label or an information sheet provided
to the person receiving the Class A residuals. The label or information sheet shall contain the following:
a. The name and address of the person who prepared the residuals;
b. A statement that residual land application is prohibited except in accordance with the instructions
on the label or information sheet;
c. A statement that the residuals shall be applied at agronomic rates and recommended rates for its
intended use.
[15A NCAC 02T. 1 109(c)]
11. The Permittee shall not distribute bulk Class A residuals to any person or entity known to be applying
residuals contrary to the conditions of this permit. The Permittee shall report to the Winston-Salem
Regional Office any person or entity known to be applying residuals contrary to the conditions of this
permit. [15A NCAC 02T .0108(b)(1)(A)]
WQ0028806 Version 3.0 Shell Version 190710 Page 5 of 9

IV. MONITORING AND REPORTING REQUIREMENTS
1. The Permittee shall conduct and report any Division required monitoring necessary to evaluate this
program's impact on groundwater and surface water. [15A NCAC 02T .0108(c)]
The residuals from each source generating facility shall be analyzed to demonstrate they are non-
hazardous under the Resource Conservation and Recovery Act (RCRA). Residuals that test or are
classified as a hazardous or toxic waste under 40 CFR Part 26I shall not be land applied. The analyses
(i.e., Corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)) shall
be performed at the frequency specified in Attachment A, and the Permittee shall maintain these results
for five years. Any exemptions from the requirements in this condition shall be specified in Attachment
A. The TCLP analysis shall include the following parameters, and the Federal regulatory level (mg/L)
is in parentheses:
Arsenic (5.0)
1,4-Dichlorobenzene (7.5)
Nitrobenzene (2.0)
Barium (100.0)
1,2-Dichloroethane (0.5)
Pentachlorophenol (100.0)
Benzene (0.5)
1, 1 -Dichloroethylene (0.7)
Pyridine (5.0)
Cadmium (1.0)
2,4-Dinitrotoluene (0.13)
Selenium (1.0)
Carbon tetrachloride (0.5)
Endrin (0.02)
Silver (5.0)
Chlordane (0.03)
Heptachlor (and its epoxide)
0.008
Tetrachloroethylene (0.7)
Chlorobenzene (100.0)
Hexachlorobenzene (0.13)
Toxaphene (0.5)
Chloroform (6.0)
Hexachlorobutadiene (0.5)
Trcchloroethylene (0.5)
Chromium (5.0)
Hexachloroethane (3.0)
2,4,5-Trichlorophenol (400,0)
m-Cresol (200.0)
Lead (5.0)
2,4,6-Trichlorophenol (2.0)
o-Cresol (200.0)
Lindane (0.4)
2,4,5-TP (Silvex) (1.0)
p-Cresol (200.0)
Mercury (0.2)
Vinyl chloride (0.2)
Cresol (200.0)
Methoxychlor (10.0)
2,4-D (10.0)
Methyl ethyl ketone (200.0)
[15A NCAC 13A .0102(b), 02T .1101, 02T .1105]
3. The residuals from each source generating facility shall be analyzed at the frequency specified in
Attachment A, and the Permittee shall maintain the results for a minimum of five years. Each analysis
shall include the following parameters:
Aluminum
Mercury
Potassium
Ammonia -Nitrogen
Molybdenum
Selenium
Arsenic
Nickel
Sodium
Cadmium
Nitrate -Nitrite Nitrogen
Sodium Adsorption Ratio(SAR)
Calcium
Percent Total Solids
TKN
Copper
pH
Zinc
Lead
Phosphorus
Magnesium
Plant Available Nitrogen
(by calculation)
[ 15A NCAC 02T .1101 ]
WQ0028806 Version 3.0 Shell Version 190710 Page 6 of 9

4. Residuals shall be monitored for compliance with pathogen and vector attraction reduction
requirements at the frequency specified in Attachment A. The monitoring results shall specify the
stabilization process utilized, and demonstrate compliance with the Class A pathogen reduction
requirements in 15A NCAC 02T .l 106(a), and one vector attraction reduction requirement in 15A
NCAC 02T .1107(a) shall be met. Any exemptions from the requirements in this condition shall be
specified in Attachment A. [ 15A NCAC 02T .1106(a), 02T .1107(a), 02T .1111(c)]
5. Representative samples of residuals that are prepared for distribution shall be collected and analyzed.
[15A NCAC 02T .1 I I l(a)]
6. The Permittee shall maintain records for all bulk Class A residual distribution events. These records
shall include the following:
a. Residuals source (as listed in Attachment A);
b. Date of distribution;
c. Name and address of residuals recipient;
d. Volume of residuals distributed to each recipient; and
e. Intended use of residuals.
[15A NCAC 02T .0I08(c)]
7. One hard copy and one electronic copy of an annual report shall be submitted on or before March V.
The annual report shall meet the requirements described in the Instructions for Residuals Application
Annual Reporting Farms. Instructions for reporting and annual report forms are available at
http://deg . nc. gov/about/divisions/water-resources/water-resources-permits/wastewater-branch/non-
discharge-permitting unit/reporting-forms, or can be obtained by contacting the Non -Discharge Branch
directly. The annual report shall be submitted to the following address:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[15A NCAC 02T .111 l(d)]
8. Noncompliance Notification
The Permittee shall report to the Winston-Salem Regional Office, telephone number [phone],
within 24 hours of first knowledge of the:
a. Any process unit failure (e.g., mechanical, electrical, etc.) rendering the facility incapable of
adequate residual treatment.
b. Any failure resulting in a discharge to surface waters.
c. Any time self -monitoring indicates the program has gone out of compliance with its permit
limitations.
d. Distribution of residuals abnormal in quantity or characteristic.
e. Any discharge from a vehicle or piping system transporting residuals.
Emergencies requiring reporting outside normal business hours shall call the Division's Emergency
Response personnel at telephone number [phone], [phone], or [phone]. All
noncompliance notifications shall file a written report to the Winston-Salem Regional Office within
five days of first knowledge of the occurrence, and this report shall outline the actions proposed or
taken to ensure the problem does not recur. [ 15A NCAC 02T .0108(b)(1)(A)]
WQ0028806 Version 3.0 Shell Version 190710 Page 7 of 9

V. INSPECTIONS
1. The Permittee shall perform inspections and maintenance to ensure proper operation of the Permittee's
storage and distribution facilities. [15A NCAC 02T .1110(f)]
2. The Permittee shall inspect the Permittee's residuals processing, storage, and transport facilities to
prevent malfunctions, facility deterioration, and operator errors that may result in discharges of wastes
to the environment, threats to human health, or public nuisances. The Permittee shall maintain an
inspection log that includes the date and time of inspection, observations made, and maintenance,
repairs, or corrective actions taken. The Permittee shall maintain this inspection log for a period of five
years from the date of inspection, and this log shall be made available to the Division upon request.
[I 5A NCAC 02T .0108(b)(1)(A), 02T .1110(f)]
Division authorized representatives may, upon presentation of credentials, enter and inspect any
property, premises, or place related to the distribution sites or facilities permitted herein at any
reasonable time for determining compliance with this permit. Division authorized representatives may
inspect or copy records maintained under the terms and conditions of this permit, and may collect
groundwater, surface water, or leachate samples. [G.S. 143-215.3(a)(2)]
VI. GENERAL CONDITIONS
1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to a
Division enforcement action. [G.S. 143-215.6A, 143-215.613, 143-215.6C]
2. This permit is effective only with respect to the nature and volume of wastes described in the permit
application, and Division -approved plans and specifications. [G.S. 143-215.1(d)]
3. Unless specifically requested and approved in this permit, there are no variances to administrative codes
or general statutes governing the construction or operation of the facilities permitted herein. [15A
NCAC 02T .0105(n)]
4. The issuance of this permit does not exempt the Permittee from complying with all statutes, rules,
regulations, or ordinances that other jurisdictional government agencies (e.g., local, state, and federal)
may require. [ 15A NCAC 02T .0105(c)(6)]
5. If the permitted residuals program change ownership, or the Permittee changes their name, the
Permittee shall submit a permit modification request on Division -approved forms. The Permittee shall
comply with all terms and conditions of this permit until the permit is transferred to the successor -
owner. [G.S. 143-215.1(d3)]
WQ0028806 Version 3.0 Shell Version 190710 Page 8 of 9

6. This permit is subject to revocation or modification upon 60-day notice from the Division Director, in
whole or part for:
a. violation of any terms or conditions of this permit or Administrative Code Title 15A Subchapter
02T;
b. obtaining a permit by misrepresentation or failure to disclose all relevant facts;
c. the Permittee's refusal to allow authorized Department employees upon presentation of credentials:
i. to enter the Permittee's premises where a system is located or where any records are required
to be kept;
ii, to have access to any permit required documents and records;
iii. to inspect any monitoring equipment or method as required in this permit; or
iv. to sample any pollutants;
d. the Permittee's failure to pay the annual fee for administering and compliance monitoring; or
e. a Division determination that the conditions of this permit are in conflict with North Carolina
Administrative Code or General Statutes.
[ 15A NCAC 02T .0110]
7. Unless the Division Director grants a variance, expansion of the facilities permitted herein shall not
occur if any of the following apply:
a. The Permittee or any parent, subsidiary, or other affiliate of the Permittee has been convicted of
environmental crimes under G.S. 143-215.613, or under Federal law that would otherwise be
prosecuted under G.S. 143-215.613, and all appeals of this conviction have been abandoned or
exhausted.
b. The Permittee or any parent, subsidiary, or other affiliate of the Permittee has previously abandoned
a wastewater treatment facility without properly closing the facility.
c. The Permittee or any parent, subsidiary, or other affiliate of the Permittee has not paid a civil
penalty, and all appeals of this penalty have been abandoned or exhausted.
d. The Permittee or any parent, subsidiary, or other affiliate of the Permittee is currently not compliant
with any compliance schedule in a permit, settlement agreement, or order.
e. The Permittee or any parent, subsidiary, or other affiliate of the Permittee has not paid an annual
fec.
[I5A NCAC 02T .0120(b), 02T .0120(d)]
8. This permit shall not be renewed if the Permittee or any affiliation has not paid the required annual fee.
[I5A NCAC 02T .0120(c)]
Permit issued this the 6` day of August 2019
NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION
�nda Culpepper, Director
v Division of Water Resources
By Authority of the Environmental Manag(cli Commission
Permit Number WQ0028806
WQ0028806 Version 3.0 Shell Version 190710 Page 9 of 9

ATTACHMENT A — APPROVED RESIDUAL SOURCES
cIe
Certification Date: August
6, 2019
Davie County
Permit Number:
WQ0028806
Version: 3.0
Owner
Facility Name
County
Permit
Biological
Maximum
Dr Tons
Monitoring
Frequency for
Monitoring
Frequency for
Monitoring
Freuency for
q
A r
eoved
Minerr alization
Number
Residuals
per Year'
Non -hazardous
Metals and
Pathogen
Rate
Characteristics 2
Nutrients 3,5
Vector
r Attraction
Davie Coun ty
Sparks Road Water
Treatment Plant
Davie
02-30-015
No
500
Once per permit
c
See Table Below I
Reductions' s
See Table Below
0.40
Total 500 r�.
1. Maximum Dry Tons per Year is the amount of residuals approved for land application from each permitted facility.
2. Analyses to demonstrate that residuals are non -hazardous (i.e_, TCLP, ignitability, reactivity, and corrosivity) as stipulated under permit Condition IV.2_
3. Testing of metals and nutrients as stipulated under permit Condition IV.3.
4. Analyses of pathogen reductions as stipulated under permit Condition IVA.
5_ Monitoring frequencies are based on the actual dry tons annlied ner year n-ina the tahlP hPln- -1- ­;flAA .,h_.
Dry Tons Applied (metric tons)
Dry Tons Applied
(short tons per year)
Monitoring Frequency
(40 CFR 503 and 15A NCAC 02T
.1111 c
< 290
< 319
Once per year (Annually)
> 290 to < 1,500
> 319 to < 1,650
Once per quarter (4 x Year)
> 1,500 to < 15,000
> 1,650 to < 16,500
Once per 60 days (6 x Year)
15,000
> 16,500
Once per month (12 x Year)
6_ Class A water treatment plant residuals are exempt from meeting the vector attraction reduction requirements in Condition IV.4, provided they are not mixed with residuals that have been generated
during the treatment of domestic wastewater, the treatment of animal processing wastewater, or the biological treatment of industrial wastewater. The Class A water treatment plant residuals must
be treated and processed in a manner as not to meet the definition of `Biological Residuals" as defined in 15A NCAC 02T .1102(6).
If no land application events occur during a required sampling period (e.g., no land application occur during an entire year when annual monitoring is required), then no sampling data is
required during the period of inactivity. The annual reportshall include an explanation for missing sampling data. Those required to submit the annual report to United States Environmental
Protection Agency (US EPA) may be required to make up the missed sampling. Contact the US EPA for additional information.
WQ0028806 Version 3.0 Attachment A Page 1 of 1

3. Operation and Maintenance Plan

Standard Operating Procedure and Operation and
Maintenance Plan for the Davie County - Sparks
Road WTP Land Application Program
1. Purpose
a. Ensure the requirements of the Sparks Road WTP Distribution of Class A
Residuals Permit# W00028806 are met.
2. Personnel
a. The following is a list of personnel in order they are to be contacted when
information needs to be shared.
i. EMA Resources Inc.
1. Boger Hartsell - Project Manager
2. Roy Whitaker -Director of Business Development
3. Brent Collins - Director of Technical Services
ii. Davie County
1. John K. Eller IV- County Manager
2. Johnny Lambert- Utilities Director
3. Mike Wier - ORC Sparks Road WTP
3. Operational Functions
a. The operational function of this project it going to involve mixing the lagoon
with a tractor powered Houle pump to achieve a well -mixed and consistent
material that is suitable for land application. It is going to be spread at
agronomic rates that are determined using the Realistic Yield Expectations (RYE)
as outlined in the permit, the amount of other nutrient sources the landowner
and operator has applied, and the residuals nutrient and metal sample that is
current for that monitoring period. It is going to be spread with a liquid
applicator that will use pressure to spread the material in such a way as to
achieve a consistent spread pattern. The material is going to be land applied on
fields that have a crop growing on them that are going to either be grazed or cut
for animal feed. Application rates will be reduced by 25% on fields that are
primarily used for grazing in accordance with USDA-NRCS 590. Grazed fields will
be determined by the farmers and EMA project managers.

4. Maintenance Schedule
a. EMA Resources Inc. will follow the maintenance schedule as recommended by
the EMA Resources Operations Manager (Mike Collins) for the equipment
necessary to complete the job.
5. Safety Measures
a. Davie County and EMA Resources Inc. believe in operating in a safety conscious
manner and all employees participate in safety training that is designed to help
employees recognize safety issues and take steps to prevent accidents from
occurring. In addition, EMA Resources employees have the authority to stop
operations if they think any aspect of the operation is going to cause
environmental or personal harm.
6. Spill Response Plan
a. In the unlikely event of a spill, the following action shall betaken immediately.
i. Management of Spill Clean-up Activities: The EMA Resources Project
Manager shall take immediate charge and initiate clean-up activities.
EMA Resources labor and equipment is to be utilized. In the event
additional labor and equipment is required, assistance may be requested
from Davie County, The NC Department of Transportation, and other
private contractors as necessary.
ii. Halt the Source of the Spill: Such as a ruptured container or damaged
transport unit.
iii. Contain the Spill: Form a barrier. Sufficient quantities of straw shall be
used for such purposes. Earthen barriers may be constructed to augment
the straw bale containment area of the spill. The Operations Manager or
the person in charge on the spill site will be advise the clean-up
personnel where to get the straw, lime, and other items necessary to
complete the clean-up operation. le. local farmers, farm supply centers,
nurseries.
iv. Initial Clean-up: Employ front-end loaders, vacuum equipment, sludge
application vehicles, and/or local septic tank service to remove as much
of the spilled material as possible. Straw and/or sand should be scattered
in the spill area to soak up the remaining material. The straw and sand
soaked material will be collected and removed to a disposal area
approved by representatives of the state regulatory agency.
v. Final Clean-up: Employ rotary brush sweeper if needed and apply lime
to the spill area upon the approval of the clean-up efforts by the state
regulatory representative. If the event occurs on private property, the
clean-up will be completed to the satisfactory of the property owner and

state regulatory representatives. The ultimate goal will be restore the
spill area to its original condition if possible.
vi. Notification: As soon as possible after the spill occurs, the EMA
Resources Project Manager or designee will notify the Davie County and
the EMA Resources main office. EMA Resources office staff are then
responsible for notifying other key EMA Resources personnel.
vii. Reporting_ EMA Resources staff will notify the Winston Salem regional
office of the NCDENR by telephone [phone] as soon as possible,
but not more than 24 hours after, or on the next working day following
the occurrence. The EMA Project Manager shall provide a written report
with 48 hours of the spill to the EMA Resources Director of Technical
Services and Davie County staff. The report shall list all relative
information and actions taken. With the assistance of EMA Resources
personnel, and the Davie County personnel, a written report will be filed
with the Winston Salem regional office within 5 days of the occurrence.
For after hours reporting, the Division's emergency number shall be
called to report all incidences [phone].
7. Inspection Plan
a. Inspection for the land application of residuals will conducted on a minimum of
a weekly basis at the land application site during land application activities. The
inspection frequency is based on the time frame that it is going to take to
complete the project and the amount of dry tons to be land applied from this
facility. The inspections will consist of inspecting a current field that is being
applied as well as inspecting random fields that have been completed.
Inspections will be conducted by Jeff Thompson - Project Manager, and Boger
Hartsell - Project Manager. These inspections will consist of the following:
i. Verifying the application rates for each field that plan on receiving
material.
ii. Checking the calculated loads to ensure the correct amount of residuals
are being land applied.
iii. Ensure that all manned equipment has a copy of the permit and the
operation and maintenance plan.
iv. Ensure that the field has been flagged properly and that all buffers are
being adhered to.
v. Ensure proper signage has been posted
vi. Verify that the proper number of samples of the residuals have been
taken and that it meets the criteria for land application.

vii. The records will be kept in the EMA Resources project files in the main
office. Copies of all analyses and records will be forwarded to Davie
County and kept on file.
viii. EMA Resources and Davie County staff will immediately inform the other
part if any of the following conditions are noted.
1. Any occurrence with the distribution program resulting in the
land application of significant amounts of material that is
abnormal in quantity or characteristics.
2. Any failure of the distribution system that results in the release to
surface waters.
3. Any time that self -monitoring indicates that the facility has gone
out of compliance with the permit.
4. Any process failure that results in the system not adequately
treating the residuals.
5. Any spill or discharge from a vehicle or piping system during
residuals transportation.
6. Any release that requires immediate reporting outside normal
business hours shall be called in by EMA Resources staff to DENR
at [phone]. This number is to be called in the event of a
release to surface waters or imminent failure of a storage system
when the event occurs outside of normal business hours.
8. Sampling and Monitoring Plan
a. Sampling for this project consists of sampling the residuals prior to land
application occurring in order to ensure that the residuals are suitable for land
application.
b. The samples will be collected from the storage lagoon that holds the residuals
c. Boger Hartsell, Brent Collins, or other designee will be responsible for sample
collection for nutrient and metal, TCLP, and fecal coliform.
d. Nutrient, metal and TCLP sample aliquots will be collected randomly and consist
of at least 7 individual aliquots mixed together in order to get the composite
sample for these parameters.
e. The residuals will be sampled annually for TCLP including the RClls.
f. Metal and nutrient parameters will be collected and analyzed based on the
requested dry ton numbers in the permit application.
g. Residuals will be sampled for fecal coliform to demonstrate pathogen
requirements have been met. Seven separate samples will be collected and
analyzed.

9. Environmental Impacts
a. The environmental impacts for residuals may be affected by this procedure.
b. This procedure helps assure that land application is conducted in a safe and
efficient manner while ensuring compliance with the laws and regulations and
to minimize exposure, negative environmental impacts and public relation
concerns.

4. RSC Form

RESIDUALS SOURCE FACILITY SUMMARY
Applicant's name: Davie County Cooleemee Lagoon
Status
Code a
Facility Permit Holder
Facility Name
County
Permit Number
Maximum Dry Tons Per Year
Current n
Proposed
M
Davie County
Cooleemee WTP
Davie
PWS0230015
279
834
a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted)
b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility).
SUMMARY FOR FORM: RSC 06-16 Page 1

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Davie County WTP
2. Facility permit holder is: ❑ Federal, ❑ State, ® Local Government, or ❑ Private.
Facility permit issued by: ® Div. of Water Resources, ❑ Div. of Environmental Health,
or ❑ Other (explain: _).
3. Facility contact person and title: David Nobles ORC
Complete mailing address: PO Box 768
City: Cooleemee State: NC Zip: 270148-
Telephone number: [phone] E-mail address: snarksrdwtpkyadtel.net
4. Facility physical address: 264 Main St
City: Cooleemee State: NC Zip: 27014-
Coordinates: Latitude: 35' 38' 34" Longitude: 80. 33' 35"
Datum: NAD83 Level of accuracy: Nearest Second
Method of measurement: GPS
5. Purpose of the facility:
❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater,
® treatment of potable water, ❑ treatment of 100% industrial wastewater,
❑ treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: __E % industrial and % domestic)
❑ other (explain: ).
6. Does the facility have an approved pretreatment program: ❑ Yes ® No
7. Facility permitted/design flow: 3 MGD and facility average daily flow: 1_5 MGD
8. Average amount of residuals being generated at this facility 279 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: NA
Type and volume of residuals storage (i.e., outside of residuals treatment units): One 3 million gallon lagoon
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
❑ 40 CFR Part 503 or ® 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
❑ Biological ® Non -Biological
FORM: RSC 06-16 Page 1 of 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ® no.
If yes, list the number(s):
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: ❑ yes ® no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well
as those for corrosivity, ignitability, and reactivity:
Laboratory: Pace Analytical and Date of analysis: 12/18/2020
Passed corrosivity test: ® yes ❑ no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: ® yes ❑ no. Flashpoint: >170 OF (> 140°F)
Passed reactivity test: W yes Ono. HCN: <0.250 mg/kg (<250) & H2S: <25 mg/kg (<500)
TCLP Parameter
Limit
(mgfi)
Result
(mgfi)
TCLP Parameter
Limit
(mgfi)
Result
(mgfi)
Arsenic
5.0
<0.1
Hexachlorobenzene
0.13
<0.1
Barium
100.0
0.465
Hexachloro-1,3-Butadiene
0.5
<0.1
Benzene
0.5
<0.05
Hexachloroethane
3.0
<0.1
Cadmium
1.0
<0.1
Lead
5.0
<0.1
Carbon Tetrachloride
0.5
<0.05
Lindane
0.4
<0.005
Chlordane
0.03
<0.005
Mercury
0.2
<0.01
Chlorobenzene
100.0
<0.05
Methoxychlor
10.0
<0.005
Chloroform
6.0
<0.25
Methyl Ethyl Ketone
200.0
<0.5
Chromium
5.0
<0.1
Nitrobenzene
2.0
<0.1
m-Cresol
200.0
<0.1
Pentachlorophenol
100.0
<0.1
o-Cresol
200.0
<0.1
Pyridine
5.0
<0.1
p-Cresol
200.0
<0.1
Selenium
1.0
<0.1
Cresol
200.0
<0.1
Silver
5.0
<0.1
2,4-D
10.0
<0.002
Tetrachloroethylene
0.7
0.0692
1,4-Dichlorobenzene
7.5
<0.1
Toxaphene
0.5
<0.01
1,2-Dichloroethane
0.5
<0.05
Trichloroethylene
0.5
<0.05
1,1-Dichloroethylene
0.7
<0.05
214,5-Trichlorophenol
400.0
<0.1
2,4-Dinitrotoluene
0.13
<0.1
2,4,6-Trichlorophenol
2.0
<0.1
Endrin
0.02
<0.005
2,4,5-TP (Silvex)
1.0
<0.002
Heptachlor and its Hydroxide
0.008
<0.005
Vinyl Chloride
0.2
<0.05
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate
the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Waypoint Analytical and Date of analysis: 12/02/2020
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mglkg)
Monthly Average
Concentration Limits
(Class A Only)
(mglkg)
Result
(mglkg)
Arsenic
75
41
7.5
Cadmium
85
39
1.45
Copper
4,300
1,500
74
Lead
840
300
37.8
Mercury
57
17
0.242
Molybdenum
75
n/a
2.68
Nickel
420
420
27.2
Selenium
100
100
<1.67
Zinc
7,500
2,800
203
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: and Date of analysis:
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
❑ > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 19.3 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Waypoint Analytical and Date of analysis: 12/02/20
Parameter
Result
(mg/kg)
Aluminum
48,800
Ammonia -Nitrogen
1,210
Calcium
2,920
Magnesium
3,130
Nitrate -Nitrite Nitrogen
<25.4
pH (Standard Unit)
7.4
Phosphorus
2,860
Potassium
2,140
Sodium
479
Total Kjeldahl Nitrogen
2,590
c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR): 0.64
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and
conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 40 %. This rate
is a (check one): ® default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: The solids are considered
raw undigested with regards to mineralization.
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (1st) Year PAN
Five -Year
Maximum Adjusted PAN
(mg/kg)
(mg/kg)
Surface
1,183
1,513
Injection/Incorporation
1,788
2,118
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:
FORM: RSC 06-16 Page 4 of

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
® A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
❑ Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
❑ Alternative 2 [15A NCAC 02T.I 106(b)(3)(13)] - Alkaline Treatment.
❑ Alternative 3 [15A NCAC 02T. 1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
❑ Alternative 1 [15A NCAC 02T.1106(c)(1)] -Fecal Coliform Density Demonstration.
❑ Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, 9 air drying, ❑ anaerobic digestion,
❑ composting, or ❑ lime stabilization.
c. For Surface Disposal:
❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑ Alternative 1 [15A NCAC 02T.I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
❑ Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization.
❑ Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
❑ Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection.
❑ Alternative 10 [15A NCAC 02T.I107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)].
® Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur
when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of

5. Vicinity Map, Process Flow Design

•• \'--\F-cooi\cooi— Site. owg — 9x11 Nov 30, 2001 — 1:13pm
OLD MILL
BUILDING
PRIMARY INTAKE
RP-1, RP-2\
x
VALVE VAULT Q
+ �x
�X \k
K HSP-3 \k
IBIN HOLDING BASIN /
x �
1 CLEARWELL BACKWASH PSX
FLOC-1 ❑
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+\ ❑
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❑
+ I
STORAGE I
GE SED-4 I I
x
• — I
xx —x�—x —I—x � I
r—
------------- �i
SCALE: 1 "=60'
DAW%+AARTIN P'0WELL & ASSOCIATES, INC.
U MAIN ELECTRICAL
U SERVICE
0
BACKWASH
SUPPLY TANK O
STANDPIPE
0 MILL FIRE TANK
dmpDAVOMU" 2 FIGURE 2-1
�ua�r000�va+ll�,�u1� un
"°N'W° N010INCAROLINA 2= OVERALL WfP LAYOUT

LEGEND
RM
RAPID MIX
FL
FLOCCULATOR
SED
SEDIMENTATION BASIN
FC
FILTER CELL
FWW
FILTERED WATER WELL
FW
FINISHED WATER
BWS
BACKWASH SUPPLY TANK
RAW WATER
-----=-r-
SETTLED WATER
FINISHED WATER
Dd
VALVE
VI
CHECK VALVE
PUMP
PUMP
BLDG
FINISHED 12• FW
WATER
CLEARWELL
16' FW
NOTES:
SCHEMATIC IS NOT TO SCALE
ALL PIPING, VALVES, FITTING, ETC. ARE NOT SHOWN FOR
CLARITY
BASED ON THE PLANS BY OTHERS AND
FIELD VERIFIED BY DMP OCT 2001
Z
(n
m 0
0 �
W J 0
V)(nH
FC-1
PUMP
Fl -1
SED-1
ROOM
FC-2
SED-.2
FC-3
BULK
RM
RROOOOMM
FC-4
FC-5
-
FL-2
SED-3
FC-6
FWW
SED-4
GREY ENGINEERING, INC.
Civil Design and Surveying
P.O. Box 9 Mocksville. N.C. 27028
greyengineering.com [phone]
DRAWN BY: G. BULLARD I PROJ. NO.: 102.101.X
DESIGN BY: G. BULLARD DATE: 09/21/07
PRIMARY
INTAKE
(AT WTP)
VALVE
VAULT
SECONDARY
RAW WATER
PUMP STATION
ml
m TO WWTP
0
DAVIE COUNTY
COOLEEMEE WTP PROCESS SCHEMATIC SHEET
1
OF 3

6. Quantitative Justification for Residuals Production Rate

Quantitative Justification for Residuals Production Rate
Facility:
Cooleemee Basin
Requested Permitted Rate:
834 dry tons/year
Justification:
We are estimating 834 dry tons of water plant residuals stored in the 3,000,000 gallon
basin.
Calculations:
We are estimating one hauling event to clean out the basin, which is scheduled for
demolition once it has been cleaned out. Measurements of the basin and samples analysis
indicates 127,008 cubic feet (952,560 gallons) of residual in place. The analytical results average
along with volume in place calculates to an estimated 834 dry tons.
(952,560 gal) x (21% solids) x (8.34 Ibs/gal) = 834 dt/yr
(2,000 Ibs/ton )

7. Laboratory Analytical Reports

Analytical Results
EMA Resources, Inc.
755 Yadkinville Rd.
Mocksville, NC 27028
Receive Date: 12/07/2020
Reported: 12/08/2020
For: Cooleemee
Comments: GEOMETRIC MEAN: 391 MPN/g
STATESVILLE
C ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
201207-09-01
Fecal Coliforms
1
370
MPN/g
SM92210E-2006
12/07/2020
MD
201207-09-01
Percent Solids
1
18.9
%
SM2540B-2011
12/07/2020
MD
201207-09-02
Fecal Coliforms
2
367
MPN/g
SM92210E-2006
12/07/2020
MD
201207-09-02
Percent Solids
2
19.07
%
SM2540B-2011
12/07/2020
MD
201207-09-03
Fecal Coliforms
3
898
MPN/g
SM92210E-2006
12/07/2020
MD
201207-09-03
Percent Solids
3
18.94
%
SM2540B-2011
12/07/2020
MD
201207-09-04
Fecal Coliforms
4
571
MPN/g
SM92210E-2006
12/07/2020
MD
201207-09-04
Percent Solids
4
19.1
%
SM2540B-2011
12/07/2020
MD
201207-09-05
Fecal Coliforms
5
157
MPN/g
SM92210E-2006
12/07/2020
MD
201207-09-05
Percent Solids
5
19.06
%
SM2540B-2011
12/07/2020
MD
201207-09-06
Fecal Coliforms
6
588
MPN/g
SM92210E-2006
12/07/2020
MD
201207-09-06
Percent Solids
6
18.7
%
SM2540B-2011
12/07/2020
MD
201207-09-07
Fecal Coliforms
7
262
MPN/g
SM92210E-2006
12/07/2020
MD
201207-09-07
Percent Solids
7
19.06
%
SM2540B-2011
12/07/2020
MD
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

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Waypointo
ANALYTICAL
12/11 /2020
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 20-338-0097
Client Project Description: Davie County
Cooleemee, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 12/3/2020 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Ijp,
Page 1 of 8

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2021
Arkansas
State Program
88-0650
02/07/2021
California
State Program
2904
06/30/2021
Florida
State Program
- NELAP
E871157
06/30/2021
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2021
Illinois
State Program
- NELAP
200078
10/10/2021
Kentucky
State Program
80215
06/30/2021
Kentucky
State Program
KY90047
12/31/2020
Louisiana
State Program
- NELAP
LA037
12/31/2020
Louisiana
State Program
- NELAP
04015
06/30/2021
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
415
12/31/2020
Oklahoma
State Program
9311
08/31/2021
Pennsylvania
State Program
- NELAP
68-03195
05/31/2021
South Carolina
State Program
84002
06/30/2021
South Carolina
State Program
84002
06/30/2021
Tennessee
State Program
02027
02/11/2023
Tennessee
A21LA ISO 17025:2017
4313.01
10/31/2021
Texas
State Program
- NELAP
T104704180
09/30/2021
Virginia
State Program
00106
06/30/2021
Virginia
State Program
- NELAP
460181
09/14/2021
Page 1 of 1 00001/20-338-0097
Page 2 of 8

Waypoint
ANALYTICAL
Report Number: 20-338-0097
Client Project Description: Davie County
Cooleemee, NC
Lab No Client Sample ID
89786 Cooleemee V TP Sludge
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Matrix Date Collected
Solids 12/02/202014:45
Date Received
12/03/2020
Page 3 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Davie County
Lab Report Number: 20-338-0097
Date: 12/11 /2020
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 89892
Analyte: Calcium
QC Batch No: L526420
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L526125
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Potassium
QC Batch No: L526420
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Magnesium
QC Batch No: L525778
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Phosphorus
QC Batch No: L525778
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Sulfur
QC Batch No: L526420
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Selenium
QC Batch No: L525778
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Arsenic
QC Batch No: 1-525778/1-525619
C1 failed +/-20% low for As (TJS)
Page 4 of 8

waypANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 20-338-0097
Lab No : 89786
Sample ID : Cooleemee WTP Sludge
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Davie County
Information : Cooleemee, NC
REPORT OFANALYSIS
Report Date : 12/11/2020
Received : 12/03/2020
Danyale Love
Project Manager
Matrix: Solids
Sampled: 12/ 2/ 2020 14:45
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Moisture
80.8
%
1
12/18/2017:15
FMM
SW-DRYWT
Ammonia Nitrogen
1210
mg/Kg -
dry
130
130
1
12/07/20 10:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<25.4
mg/Kg -
dry
25.4
25.4
1
12/07/20 15:54
ZBD
4500NO3F-2011
Organic N
1380
mg/Kg -
dry
260.4
1
12/07/20 10:00
CALCULATION
pH
7.4
S.U.
1
12/04/2015:18
ADM
9045D
Total Solids
19.3
%
0.010
0.010
1
12/07/20 16:13
FMM
2540G-2011
Total Volatile Solids
20.4
%
0.010
0.010
1
12/07/20 16:13
FMM
2540G-2011
Total Kjeldahl Nitrogen
2590
mg/Kg -
dry
260
1
12/08/20 15:47
CLP
4500NORGD-2011
Phosphorus
2860
mg/Kg -
dry
14.4
26.0
1
12/09/20 04:07
DADS
6010D
Aluminum
48800
mg/Kg -
dry
24.1
26.0
1
12/09/20 04:07
DADS
6010D
Arsenic
7.50
mg/Kg -
dry
1.25
2.60
1
12/10/20 20:21
DADS
6010D
Cadmium
1.45
mg/Kg -
dry
0.104
0.521
1
12/09/20 04:07
DADS
6010D
Calcium
2920
mg/Kg -
dry
202
260
1
12/09/20 04:07
DADS
6010D
Chromium
62.0
mg/Kg -
dry
1.23
1.30
1
12/09/20 04:07
DADS
6010D
Copper
74.0
mg/Kg -
dry
1.61
2.60
1
12/09/20 04:07
DADS
6010D
Iron
132000
mg/Kg -
dry
222
260
5
12/10/20 20:36
DADS
6010D
Lead
37.8
mg/Kg -
dry
0.937
1.56
1
12/09/20 04:07
DADS
6010D
Magnesium
3130
mg/Kg -
dry
13.4
26.0
1
12/09/20 04:07
DADS
6010D
Manganese
667
mg/Kg -
dry
1.69
2.60
1
12/09/20 04:07
DADS
6010D
Mercury
0.242
mg/Kg -
dry
0.0182
0.0823
1
12/08/20 10:25
DDB
7471A
Molybdenum
2.68
mg/Kg -
dry
0.703
1.30
1
12/09/20 04:07
DADS
6010D
Nickel
27.2
mg/Kg -
dry
0.625
1.30
1
12/09/20 04:07
DADS
6010D
Potassium
2140
mg/Kg -
dry
32.2
52.1
1
12/09/20 04:07
DADS
6010D
Qualifiers/ DF
Dilution Factor
L
Limit Exceeded
Definitions MQL
Method Quantitation Limit
Page 5 of 8

waypANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 20-338-0097
Lab No : 89786
Sample ID : Cooleemee WTP Sludge
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Davie County
Information : Cooleemee, NC
REPORT OFANALYSIS
Report Date : 12/11/2020
Received : 12/03/2020
Danyale Love
Project Manager
Matrix: Solids
Sampled: 12/ 2/ 2020 14:45
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
<1.67
mg/Kg - dry
1.67
2.60
1
12/09/20 04:07
3ADS
6010D
Sodium
479
mg/Kg - dry
67.7
130
1
12/09/20 04:07
3ADS
6010D
Zinc
203
mg/Kg - dry
4.22
6.51
1
12/09/20 04:07
3ADS
6010D
Sulfur
1990
mg/Kg - dry
27.0
52.1
1
12/09/20 04:07
3ADS
6010D
Sodium Absorption Ratio
0.64
Ratio
0.01
0.01
1
12/09/20 04:07
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
L Limit Exceeded
Page 6 of 8

s
WayPAoi nt ..(2) �79p Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 901.213.240fl °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 20-338-0097
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
T99
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: IHannah R. Brown Date & Time: 12/03/2020 15:49:23
Page 7 of 8

Client Name/Address
Client Project Manager/Contact
Billing Information
For Laboratory Use Only
EMA Resources inc
Brent Collins
Account #46245
755 Yadkinville Rd
Mocksville, NC 27028
Project Description
Prnject/Site Location (City/state)
RUSH - Add iticnai charges apply
Met d of Shipment
Matrix Key
N1
I���'+Date
wc
Special Detection Limits)
Results Needed
Fed Ex ❑UPS �USPS
El CourierEl Client Drop Off
Ww -Wastewater GW-Groundwater
DW - Drinking Water 5 - Soil 1Soiid D - oil
P - Product M - MI!K
Other
Project Number Project Manager Phone-#
Project Manager Email
Purchase Order Number
Site/Facility ID N
336-399-3646
[e-mail]
(¢ z [j)
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0
2790 Whitlen Road "
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Memphis, TN 38133 Unless noted, all containers c
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[phone] per' Table li of AD CFR Part E
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Date Time Sample Identification z
Requ
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Comments/Notes
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Meta15:AI,As,Ca,Cd,Cr,Cu Fe,Pb
Mn,Mg,Mo,Hg,Ni,Se,Na,P,S,K,Zn
I IIIIII IIII III Illlll IIII IIII IIII Ills I la I I�Illpl III ICI ; 245
EMA Retie„urea ln,' 154716
Davie Countv
For
Laboratory Use Only
Sam by(Na e-Print)
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Client Remarks/Comments
Sludge Samples -Report dry Weight
Ice
CSealsy
Lab Comments
7N
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ReEi
Dat 'F'Fme
Received by: (SIGNATURE)
Date Time
Blawcooier Temp
Rellnqu' hed by: (SIGNATURE)
Hate Time
Received by: (SIGNATURE)
Date Time
Relinquished by: [SIGNATURE]
Date Time
R r T
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aceAnalytical
National Center for Testing & Innovation
AW
ANALYTICAL REPORT
June 02, 2020
EMA Resources
Sample Delivery Group
Samples Received:
Project Number:
Description:
Report To:
L1221225
05/22/2020
DAVIE COUNTY
Sludge
Mr. Brent Collins
755 Yadkinville Road
Entire Report Reviewed By
Mocksville, NC 27028
��MJarda ,' P�ti
Cassandra Foster
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources DAVIE COUNTY L1221225 06/02/20 22:26 1 of 21

TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
Cp: Cover Page
1
FP
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
FS
COOLEEMEE WWTP L1221225-01
5
Fn
Qc: Quality Control Summary
7
Wet Chemistry by Method 9012 B
7
Fr
Wet Chemistry by Method 9034-9030B
8
Wet Chemistry by Method 9045D
9
FC
Wet Chemistry by Method D93/1010A
10
F
Mercury by Method 7470A
11
Metals (ICP) by Method 6010D
12
[Al
Volatile Organic Compounds (GC/MS) by Method 8260D
13
Chlorinated Acid Herbicides (GC) by Method 8151A
15
RC
Pesticides (GC) by Method 8081B
16
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
17
GI: Glossary of Terms
19
al: Accreditations & Locations
20
Sc: Sample Chain of Custody
21
ACCOUNT: PROJECT: SDG:
DATE/TIME: PAGE:
EMA Resources DAVIE COUNTY L1221225
06/02/20 22:26 2 of 21

SAMPLE SUMMARY ONE LAB. NATIONWIDE.
Collected by Collected date/time Received date/time
COOLEEMEE WWTP L1221225-01 Waste Roy Whitaker 05/21/2014:00 05/22/20 08:00 , C
P
Method
Preparation by Method 1311
Preparation by Method 1311
Wet Chemistry by Method 9012 B
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9045D
Wet Chemistry by Method D93/1010A
Mercury by Method 7470A
Metals (ICP) by Method 6010D
Volatile Organic Compounds (GC/MS) by Method 8260D
Chlorinated Acid Herbicides (GC) by Method 8151A
Pesticides (GC) by Method 8081B
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Batch
WG1482620
WG1484814
WG1482372
WG1482933
WG1482434
WG1485097
WG1483293
WG1483563
WG1485165
WG1483266
WG1483649
WG1483651
Dilution Preparation
Analysis
date/time
date/time
1 05/27/20 09:20
05/27/20 09:20
1 05/30/2019:59
05/30/2019:59
1 05/27/2016:00
05/27/20 20:06
1 05/27/20 23:50
05/27/20 23:50
1 05/26/20 20:09
05/29/20 08:10
1 06/01/2016:35
06/01/2016:35
1 05/28/20 07:55
05/28/2012:03
1 05/28/2018:42
05/29/20 03:45
1 06/01/2014:18
06/01/2014:18
1 05/28/20 09:29
05/28/20 2143
1 05/28/2016:24
06/01/2015:14
1 05/30/2017:15
05/31/2018:32
Analyst
IDW
CGD
SDL
LDT
KPS
MJA
ABL
TRB
BMB
RP
RP
LEA
Location
FC
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fn
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fr
Mt. Juliet, TN
Mt. Juliet, TN
FC
Mt. Juliet, TN
Mt. Juliet, TN
�GI
SAI
RC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources DAVIE COUNTY L1221225 06/02/20 22:26 3 of 21

CASE NARRATIVE
ONE LAB. NATIONWIDE. *
All sample aliquots were received at the correct temperature, in the proper containers, with the FP
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data. 0
Fr
FC
7
GI
Cassandra Foster
Project Manager
RC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources DAVIE COUNTY L1221225 06/02/20 22:26 4 of 21

COOLEEMEE WWTP
Collected date/time: 05/21/20 14:00
Preparation by Method 1311
SAMPLE RESULTS - 01
L1221225
Result Qualifier
Prep
Batch
Analyte
date / time
TCLP Extraction
5/27/2020 9:20:40 AM
WG1482620
TCLP ZHE Extraction -
5/30/2020 7:59:56 PM
WG1484814
Fluid 1
5/27/2020 9:20:40 AM
WG1482620
Initial pH 6.72
5/27/2020 9:20:40 AM
WG1482620
Final pH 4.99
5/27/2020 9:20:40 AM
WG1482620
Wet Chemistry by Method 9012 B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Reactive Cyanide ND 0.250 1 05/27/2020 20:06 WG1482372
Wet Chemistry by Method 9034-9030B
Result Qualifier RDL
Analyte mg/kg mg/kg
Reactive Sulfide ND 25.0
Wet Chemistry by Method 9045D
Dilution Analysis Batch
date / time
1 05/27/2020 23:50 WG1482933
Result Qualifier Dilution Analysis Batch
Analyte su date / time
Corrosivity by pH 7.18 T8 1 05/29/2020 08:10 WG1482434
Sample Narrative:
L1221225-01 WG1482434: 7.18 at 20C
Wet Chemistry by Method D93/1010A
Result
Analyte Deg. F
Ignitability DNI at170
Mercury by Method 7470A
Qualifier Dilution Analysis Batch
date / time
1 06/01/202016:35 WG1485097
Result Qualifier RDL Limit
Analyte mg/I mg/I mg/I
Mercury ND 0.0100 0.20
Metals (ICP) by Method 6010D
Result
Qualifier RDL Limit
Analyte
mg/I
mg/I mg/I
Arsenic
ND
0.100 5
Barium
0.305
0.100 100
Cadmium
ND
0.100 1
Chromium
ND
0.100 5
Lead
ND
0.100 5
Selenium
0.111
0.100 1
Silver
ND
0.100 5
Volatile Organic
Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL Limit
Analyte
mg/I
mg/I mg/I
Benzene
ND
0.0500 0.50
Carbon tetrachloride
ND
J3 0.0500 0.50
Chlorobenzene
ND
0.0500 100
Chloroform
ND
0.250 6
ACCOUNT:
PROJECT:
EMA Resources
DAVIE COUNTY
Dilution Analysis Batch
date / time
1 05/28/202012:03 WG1483293
Dilution Analysis
Batch
date / time
1 05/29/2020 03:45
WG1483563
1 05/29/2020 03:45
WG1483563
1 05/29/2020 03:45
WG1483563
1 05/29/2020 03:45
WG1483563
1 05/29/2020 03:45
WG1483563
1 05/29/2020 03:45
WG1483563
1 05/29/2020 03:45
WG1483563
ONE LAB. NATIONWIDE. *
Fp
Fc
FS
Fn
Fc
�GI
SAI
Rc
Dilution Analysis
Batch
date / time
1 06/01/202014:18
WG1485165
1 06/01/202014:18
WG1485165
1 06/01/202014:18
WG1485165
1 06/01/202014:18
WG1485165
SDG:
DATE/TIME: PAGE:
L1221225
06/02/20 22:26 5 of 21

COOLEEMEE WWTP
SAMPLE RESULTS
- 01
Collected date/time: 05/21/20 14:00
L1221225
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL Limit Dilution
Analysis
Analyte
mg/I
mg/I mg/I
date/time
1,2-Dichloroethane
ND
0.0500 0.50 1
06/01/202014:18
1,1-Dichloroethene
ND
0.0500 0.70 1
06/01/202014:18
2-Butanone (MEK)
ND
0.500 200 1
06/01/202014:18
Tetrachloroethene
ND
0.0500 0.70 1
06/01/202014:18
Trichloroethene
ND
0.0500 0.50 1
06/01/202014:18
Vinyl chloride
ND
0.0500 0.20 1
06/01/202014:18
(S) Toluene-dH
105
80.0-120
0610112020 14.18
(S) 4-Bromofluorobenzene
100
77.0-126
0610112020 14.18
(S) 1,2-Dichloroethane-d4
ill
70.0-130
061011202014.18
Chlorinated Acid Herbicides
(GC)
by Method 8151A
Batch
WG1485165
WG1485165
WG1485165
WG1485165
WG1485165
WG1485165
WG1485165
WG1485165
WG1485165
ONE LAB. NATIONWIDE. *
Result Qualifier
RDL Limit
Dilution Analysis
Batch
Analyte mg/I
mg/I mg/I
date/time
2,4,5-TP (Silvex) ND
0.00200 1
1 05/28/2020 2143
WG1483266
2,4-D ND
0.00200 10
1 05/28/2020 2143
WG1483266
(S) Z4-Dichlorophenyl Acetic Acid 58.6
14.0-158
051281202021.43
WG1483266
Pesticides (GC) by Method 8081B
Result
Qualifier RDL
Limit
Dilution Analysis
Analyte
mg/I
mg/I
mg/I
date/time
Chlordane
ND
0.00500
0.03
1 06/01/202015:14
Endrin
ND
0.00500
0.02
1 06/01/202015:14
Heptachlor
ND
0.00500
0.0080
1 06/01/202015:14
Lindane
ND
0.00500
0.40
1 06/01/202015:14
Methoxychlor
ND
J4 0.00500
10
1 06/01/202015:14
Toxaphene
ND
0.0100
0.50
1 06/01/202015:14
(S) Decochlorobiphenyl
92.6
10.0-128
0610112020 15.14
(S) Tetrochloro-m-xylene
86.7
10.0-127
0610112020 15.14
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Analyte
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachloroethane
Nitrobenzene
Pyridine
3&4-Methyl Phenol
2-Methylphenol
Pentachlorophenol
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
(S) 2-Fluorophenol
(S) Phenol-d5
(S) Nitrobenzene-d5
(S) 2-Fluorobiphenyl
(S) Z4, 6-Tribromophenol
(S) p-Terphenyl-d14
Batch
WG1483649
WG1483649
WG1483649
WG1483649
WG1483649
WG1483649
WG1483649
WG1483649
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
mg/I
mg/I
mg/I
date/time
ND
0.100
7.50
1 05/31/202018:32
WG1483651
ND
0.100
0.13
1 05/31/202018:32
WG1483651
ND
0.100
0.13
1 05/31/202018:32
WG1483651
ND
0.100
0.50
1 05/31/202018:32
WG1483651
ND
0.100
3
1 05/31/202018:32
WG1483651
ND
0.100
2
1 05/31/202018:32
WG1483651
ND
0.100
5
1 05/31/202018:32
WG1483651
ND
0.100
400
1 05/31/202018:32
WG1483651
ND
0.100
200
1 05/31/202018:32
WG1483651
ND
0.100
100
1 05/31/202018:32
WG1483651
ND
0.100
400
1 05/31/202018:32
WG1483651
ND
0.100
2
1 05/31/202018:32
WG1483651
48.1
10.0-120
051311202018.32
WG1483651
30.1
10.0-120
051311202018.32
WG1483651
65.4
10.0-127
051311202018.32
WG1483651
74.3
10.0-130
051311202018.32
WG1483651
58.5
10.0-155
051311202018.32
WG1483651
86.9
10.0-128
051311202018.32
WG1483651
Fp
Fc
FS
Fn
FA
Fc
F,
SAI
Rc
ACCOUNT:
EMA Resources
PROJECT: SDG: DATE/TIME: PAGE:
DAVIE COUNTY L1221225 06/02/20 22:26 6 of 21

WG1482372 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9012 B L1221225-01
Method Blank (MB)
(MB) R3532323-1 05/27/2019:54
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Reactive Cyanide U 0.0390 0.250
Original Sample (OS) • Duplicate (DUP)
(OS) • (DUP) R3532323-3 05/27/20 20:00
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg %_
Reactive Cyanide ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3532323-2 05/27/20 19:55
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Reactive Cyanide 2.50 2.72 109
Rec. Limits LCS Qualifier
85.0-115
Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) • (MS) R3532323-4 05/27/20 20:09 • (MSD) R3532323-5 05/27/20 20:10
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg
Reactive Cyanide 1.67 1.67 1.63 89.3 86.5 1 75.0-125 2.80 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources DAVIE COUNTY L1221225 06/02/20 22:26 7 of 21

WG1482933
Wet Chemistry by Method 9034-9030B
Method Blank (MB)
(MB) R3532371-1 05/27/20 23:50
MB Result
Analyte mg/kg
Reactive Sulfide U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
7.63 25.0
L1221084-04 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1221225-01
(OS) L1221034-04 05/27/20 23:50 • (DUP) R3532371-3 05/27/20 23:50
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %_
Reactive Sulfide ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3532371-2 05/27/20 23:50
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Reactive Sulfide 100 88.1 88.1
Rec. Limits LCS Qualifier
70.0-130
L1221225-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1221225-01 05/27/20 23:50 • (MS) R3532371-4 05/27/20 23:50 • (MSD) R3532371-5 05/27/20 23:50
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Sulfide 100 ND 95.8 95.5 95.8 95.5 1 70.0-130 0.309 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources DAVIE COUNTY L1221225 06/02/20 22:26 3 of 21

WG1482434 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9045D L1221225-01
Laboratory Control Sample (LCS)
(LCS) R3532973-1 05/29/20 0310
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte su su
Corrosivity by pH 10.0 9.95 99.5 99.0-101
Sample Narrative:
LCS: 9.95 at 22C
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources DAVIE COUNTY L1221225 06/02/20 22:26 9 of 21

WG1485097 QUALITY CONTROL SUMMARY
Wet Chemistry by Method D93/1010A L1221225-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3533850-1 06/01/2016:35 • (LCSD) R3533850-2 06/01/2016:35
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte Deg.F Deg.F Deg.F
Ignitability 124 129 127 104 102 95.6-104 1.57 10
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources DAVIE COUNTY L1221225 06/02/20 22:26 10 of 21

■
WG1483293
Mercury by Method 7470A
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1221225-01
(MB) R3532599-1 05/23/201152
MB Result
MB Qualifier MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
Mercury U
0.00330
0.0100
Laboratory Control Sample (LCS)
(LCS) R3532599-2 05/28/201154
Spike Amount
LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
Mercury 0.0300
0.0300 100 80.0-120
L1221479-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1221479-02 05/23/20 11:55 • (MS) R3532599-3 05/23/20 11:57 • (MSD) R3532599-4 05/23/20 1159
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Mercury 0.0300
ND
0.0304
0.0313 101 104 1 75.0-125 2.80 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources DAVIE COUNTY L1221225 06/02/20 22:26 11 of 21

WG1483563
Metals (ICP) by Method 6010D
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1221225-01
(MB) R3532894-1 05/29/20 0340
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
Arsenic U
0.0333
0.100
Barium U
0.0333
0.100
Cadmium U
0.0333
0.100
Chromium U
0.0333
0.100
Lead U
0.0333
0.100
Selenium U
0.0333
0.100
Silver U
0.0333
0.100
Laboratory Control Sample (LCS)
(LCS) R3532394-2 05/29/20 03:42
Spike Amount
LCS Result
LCS Rec.
Rec. Limits
Analyte mg/I
mg/I
Arsenic 10.0
9.78
97.8
80.0-120
Barium 10.0
9.67
96.7
80.0-120
Cadmium 10.0
9.74
97.4
80.0-120
Chromium 10.0
9.51
95.1
80.0-120
Lead 10.0
9.65
96.5
80.0-120
Selenium 10.0
9.82
98.2
80.0-120
Silver 2.00
1.82
90.9
80.0-120
LCS Qualifier
L1221225-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1221225-01 05/29/20 03:45 • (MS) R3532394-4 05/29/20 03:50 • (MSD) R3532394-5 05/29/20 03:52
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mg/I
mg/I
mg/I
mg/I
Arsenic
10.0
ND
9.59
9.60
95.0
95.2
1 75.0-125
Barium
10.0
0.305
9.76
9.83
94.5
95.2
1 75.0-125
Cadmium
10.0
ND
9.50
9.59
95.0
95.9
1 75.0-125
Chromium
10.0
ND
9.21
9.35
92.1
93.5
1 75.0-125
Lead
10.0
ND
9.44
9.50
94.4
95.0
1 75.0-125
Selenium
10.0
0.111
9.45
9.59
93.4
94.8
1 75.0-125
Silver
2.00
ND
1.76
1.77
87.9
88.3
1 75.0-125
MS Qualifier MSD Qualifier RPD
0.169
0.709
0.968
1.53
0.723
1.52
0.556
ONE LAB. NATIONWIDE. *
RPD Limits
20
20
20
20
20
20
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources DAVIE COUNTY L1221225 06/02/20 22:26 12 of 21

WG1485165 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1221225-01
ONE LAB. NATIONWIDE. *
Method Blank (MB)
(MB) R3533742-3 06/01/201154
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Benzene
U
0.0167
0.0500
Carbon tetrachloride
U
0.0167
0.0500
Chlorobenzene
U
0.0167
0.0500
Chloroform
U
0.0833
0.250
1,2-Dichloroethane
U
0.0167
0.0500
1,1-Dichloroethene
U
0.0167
0.0500
2-Butanone (MEK)
U
0.167
0.500
Tetrachloroethene
U
0.0167
0.0500
Trichloroethene
U
0.0167
0.0500
Vinyl chloride
U
0.0167
0.0500
(S) Toluene-dH
106
80.0-120
(S) 4-Bromofluorobenzene
82.9
77.0-126
(S) 1,2-Dichloroethane-d4
109
70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3533742-1 06/01/20 09:45 • (LCSD) R3533742-2 06/01/2010:53
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/I
mg/I
mg/I
Benzene
0.250
0.261
0.237
104
94.8
70.0-123
Carbon tetrachloride
0.250
0.301
0.239
120
95.6
68.0-126
Chlorobenzene
0.250
0.245
0.230
98.0
92.0
80.0-121
Chloroform
0.250
0.254
0.233
102
93.2
73.0-120
1,2-Dichloroethane
0.250
0.281
0.253
112
101
70.0-128
1,1-Dichloroethene
0.250
0.289
0.268
116
107
71.0-124
2-Butanone (MEK)
1.25
1.17
1.00
93.6
80.0
44.0-160
Tetrachloroethene
0.250
0.269
0.236
108
94.4
72.0-132
Trichloroethene
0.250
0.285
0.247
114
98.8
78.0-124
Vinyl chloride
0.250
0.263
0.220
105
88.0
67.0-131
(S) Toluene-dH
107
105
80.0-120
(S) 4-Bromofluorobenzene
101
102
77.0-126
(S) 1,2-Dichloroethane-d4
110
108
70.0-130
LCS Qualifier LCSD Qualifier RPD
RPD Limits
9.64
20
J3 23.0
20
6.32
20
8.62
20
10.5
20
7.54
20
15.7
20
13.1
20
14.3
20
17.8
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources DAVIE COUNTY L1221225 06/02/20 22:26 13 of 21

ONE LAB. NATIONWIDE. *
WG1485165 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1221225-01
Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) • (MS) R3533742-4 06/01/20 17:45 • (MSD) R3533742-5 06/01/20 13 05
Spike Amount
Original Result MS Result
MSD Result MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte mg/I
mg/I
mg/I
Benzene 0.250
0.246
0.228 98.4
91.2
1 17.0-158
7.59
27
Carbon tetrachloride 0.250
0.256
0.248 102
99.2
1 23.0-159
3.17
28
Chlorobenzene 0.250
0.240
0.216 96.0
86.4
1 33.0-152
10.5
27
Chloroform 0.250
0.260
ND 104
92.8
1 29.0-154
11.4
28
1,2-Dichloroethane 0.250
0.297
0.251 119
100
1 29.0-151
16.8
27
1,1-Dichloroethene 0.250
0.254
0.227 102
90.8
1 11.0-160
11.2
29
2-Butanone (MEK) 1.25
1.60
1.35 128
108
1 10.0-160
16.9
32
Tetrachloroethene 0.250
0.235
0.222 94.0
88.8
1 10.0-160
5.69
27
Trichloroethene 0.250
0.263
0.238 105
95.2
1 10.0-160
9.98
25
Vinyl chloride 0.250
0.222
0.207 88.8
82.8
1 10.0-160
6.99
27
(S) Toluene-dH
106
106
80.0-120
(S) 4-Bromofluorobenzene
99.7
106
77.0-126
(S) 1,2-Dichloroethane-d4
117
115
70.0-130
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
DAVIE COUNTY
L1221225
06/02/20 22:26
14 of 21

WG1483266
Chlorinated Acid Herbicides (GC) by Method 8151A
Method Blank (MB)
(MB) R3532975-1 05/23/20 2006
MB Result
Analyte mg/I
2,4-D U
2,4,5-TP (Silvex) U
(S) Z4-Dichlorophenyl Acetic 64.8
Acid
QUALITY CONTROL SUMMARY
L1221225-01
MB Qualifier MB MDL
MB RDL
mg/I
mg/I
0.000667
0.00200
0.000667
0.00200
14.0-158
Laboratory Control Sample (LCS)
(LCS) R3532975-2 05/23/20 2022
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
2,4-D 0.0500 0.0319 63.8
2,4,5-TP (Silvex) 0.0500 0.0374 74.8
(S) Z4-Dichlorophenyl Acetic 672
Acid
Rec. Limits LCS Qualifier
50.0-120
50.0-125
14.0-158
Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) • (MS) R3532975-3 05/29/20 03:40 • (MSD) R3532975-4 05/29/20 03:57
Spike Amount
Original Result MS Result
MSD Result
MS Rec.
Analyte
mg/I
mg/I
mg/I
2,4-D
0.0500
0.0314
0.0312
62.8
2,4,5-TP (Silvex)
0.0500
0.0368
0.0367
73.6
(S) Z4-Dichlorophenyl Acetic
66.0
Acid
ONE LAB. NATIONWIDE. *
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
62.4
1 50.0-120
0.639
20
73.4
1 50.0-125
0.272
20
66.4 14.0-158
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources DAVIE COUNTY L1221225 06/02/20 22:26 15 of 21

WG1483649
Pesticides (GC) by Method 8081B
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1221225-01
(MB) R3533312-1 06/01/2013:46
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Gamma BHC
U
0.00167
0.00500
Endrin
U
0.00167
0.00500
Heptachlor
U
0.00167
0.00500
Methoxychlor
U
0.00167
0.00500
Chlordane
U
0.00167
0.00500
Toxaphene
U
0.00333
0.0100
(S) Decachlorobiphenyl
96.3
10.0-128
(S) Tetrochloro-m-xylene
88.9
10.0-127
Laboratory Control Sample (LCS)
(LCS) R3533812-2 06/01/20 1400
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
Gamma BHC
0.0100
0.00974
97.4
55.0-129
Endrin
0.0100
0.0101
101
57.0-134
Heptachlor
0.0100
0.00851
85.1
27.0-132
Methoxychlor
0.0100
0.0156
156
54.0-155 J4
(S) Decachlorobiphenyl
94.9
10.0-128
(S) Tetrochloro-m-xylene
90.1
10.0-127
Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) • (MS) R3533312-3 06/01/20 14:30 • (MSD) R3533312-4 06/01/20 14:45
Spike Amount
Original Result MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
Gamma BHC
0.0100
0.00974
0.00942
97.4
94.2
Endrin
0.0100
0.0100
0.00979
100
97.9
Heptachlor
0.0100
0.00851
0.00813
85.1
81.3
Methoxychlor
0.0100
0.0155
0.0150
155
150
(S) Decachlorobiphenyl
83.2
80.6
(S) Tetrochloro-m-xylene
90.1
87.7
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
1 14.0-141
3.34
1 10.0-160
2.12
1 16.0-136
4.57
1 10.0-160
P 3.28
10.0-128
10.0-127
ONE LAB. NATIONWIDE. *
RPD Limits
40
39
40
34
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources DAVIE COUNTY L1221225 06/02/20 22:26 16 of 21

WG1483651 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1221225-01
Method Blank (MB)
(MB) R3533553-2 05/31/201703
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
U
0.0333
0.100
2,4-Dinitrotoluene
U
0.0333
0.100
Hexachlorobenzene
U
0.0333
0.100
Hexachloro-1,3-butadiene
U
0.0333
0.100
Hexachloroethane
U
0.0333
0.100
Nitrobenzene
U
0.0333
0.100
Pyridine
U
0.0333
0.100
2-Methylphenol
U
0.0333
0.100
3&4-Methyl Phenol
U
0.0333
0.100
Pentachlorophenol
U
0.0333
0.100
2,4,5-Trichlorophenol
U
0.0333
0.100
2,4,6-Trichlorophenol
U
0.0333
0.100
(S) Nitrobenzene-d5
56.0
10.0-127
(S) 2-Fluorobiphenyl
64.8
10.0-130
(S) p-Terphenyl-d14
76.5
10.0-128
(S) Phenol-d5
23.9
10.0-120
(S) 2-Fluorophenol
39.5
10.0-120
(S) 2,4, 6-Tribromophenol
476
10. 0-155
Laboratory Control Sample (LCS)
ONE LAB. NATIONWIDE. *
(LCS) R3533553-1 05/31/20 16:47
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
1,4-Dichlorobenzene 0.500
0.345
69.0
18.0-120
2,4-Dinitrotoluene 0.500
0.385
77.0
49.0-124
Hexachlorobenzene 0.500
0.339
67.8
44.0-120
Hexachloro-1,3-butadiene 0.500
0.292
58.4
19.0-120
Hexachloroethane 0.500
0.363
72.6
15.0-120
Nitrobenzene 0.500
0.348
69.6
27.0-120
Pyridine 0.500
0.183
36.6
10.0-120
2-Methylphenol 0.500
0.325
65.0
28.0-120
3&4-Methyl Phenol 0.500
0.326
65.2
31.0-120
Pentachlorophenol 0.500
0.442
88.4
23.0-120
2,4,5-Trichlorophenol 0.500
0.379
75.8
44.0-120
2,4,6-Trichlorophenol 0.500
0.370
74.0
42.0-120
(S) Nitrobenzene-d5
53.2
10.0-127
(S) 2-Fluorobiphenyl
71.3
10.0-130
(S) p-Terphenyl-d14
77.6
10.0-128
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
DAVIE COUNTY L1221225 06/02/20 22:26 17 of 21

WG1483651 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1221225-01
Laboratory Control Sample (LCS)
ONE LAB. NATIONWIDE. *
(LCS) R3533553-1 05/31/20 16:47
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
(S) Phenol-d5 279 10.0-120
(S) 2-Fluorophenol 44.0 10.0-120
(S) 2,4, 6-Tribromophenol 62.5 10. 0-155
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources DAVIE COUNTY L1221225 06/02/20 22:26 18 of 21

GLOSSARY OF TERMS
ONE LAB. NATIONWIDE. *
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J3
The associated batch QC was outside the established quality control range for precision.
J4
The associated batch QC was outside the established quality control range for accuracy.
P
RPD between the primary and confirmatory analysis exceeded 40%.
T8
Sample(s) received past/too close to holding time expiration.
Fp
Fc
FS
Fn
Fr
Fc
SAI
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources DAVIE COUNTY L1221225 06/02/20 22:26 19 of 21

ACCREDITATIONS
& LOCATIONS
ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide
from one location. One phone call, one point of contact,
one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our
single location laboratory is comparable to the collective
totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory
campus. The model is conducive to accelerated
productivity, decreasing
Cp
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium
quality and prompt service allows us to be YOUR
LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace
National.
Fc
State Accreditations
Alabama 40660
Nebraska
NE-OS-15-05
FS
Alaska 17-026
Nevada
TN-03-2002-34
Arizona AZ0612
New Hampshire
2975
Arkansas 88-0469
New Jersey—NELAP
TNO02
Fn
California 2932
New Mexico
n/a
Colorado TN00003
New York
11742
Connecticut PH-0197
North Carolina
Env375
Fr
Florida E87487
North Carolina'
DW21704
Georgia NELAP
North Carolina 3
41
Georgia' 923
North Dakota
R-140
Fc
Idaho TN00003
Ohio—VAP
CL0069
Illinois 200008
Oklahoma
9915
7C71
Indiana C-TN-01 f
Oregon
TN200002
Iowa 364
Pennsylvania
68-02979
Kansas E-10277
Rhode Island
LA000356
Kentucky' 6 90010
South Carolina
84004
Kentucky 2 16
South Dakota
n/a
Louisiana A130792
Tennessee'"
2006
Louisiana' LA180010
Texas
T104704245-18-15
Rc
Maine TN0002
Texas 5
LABO152
Maryland 324
Utah
TN00003
Massachusetts M-TNO03
Vermont
VT2006
Michigan 9958
Virginia
460132
Minnesota 047-999-395
Washington
C847
Mississippi TN00003
West Virginia
233
Missouri 340
Wisconsin
9980939910
Montana CERT0086
Wyoming
A2 LA
Third Party Federal Accreditations
A2LA— ISO17025 1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5 1461.02
DOD
1461.01
Canada 1461.01
USDA
P330-15-00234
EPA—Crypto TN00003
' Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
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ACCOUNT: V PROJECT:
EMA Resources DAVIE COUNTY
ME
MN
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KY
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LA
FL
SDG: DATE/TIME: PAGE:
L1221225 06/02/20 22:26 20 of 21

1J/)
Billing Information:
EMA Resources
Mr. Brent Collins Pres
Chk
'755 Yadkinville Road
755 Yadkinville Road
Mocksville, NC 27028
Mocksville, NC 27028
Email To: [e-mail]
Report to:
Mr. Brent Collins
Prciect
City/State Please Circle:
C�66�N iV PT MT CT ET
Collected: LW Car�ad�c � • 4
Description: Sludge
Client Project # lab P oject #
Phone,336-751-1441
Fax: [phone]
{p
Co l�eled bY/ T`� __ _� ., __!J
Site/Facility ID # P. d
Vrc cow )Ty Z
Immediately
Packed on Ice N — Y
Sample ID
: Matrix:
�S - Soil AIR - Air F - Filter
3W -Groundwater B- Bioassay
NW - WasteWater
]W - Drinking Water
X - Other /
Relinqui
by : (5ign8ture
Relinauished by : (5i9nature}
Rush? (Lab MUST Be Notified) Quote #
Same Day Five Day
Next Day _ 5 Day {Rad Onlyl Date Results Needed
~_Two Day _ 10 Day {Rad Only)
Three Day
Comp/Grab 1 Matrix ` Depth Date Time
ss
Samples returned viia:� Tracking#
UPS _ FedEx V Courier
JDate: Time. q� Received by:
a +
a tJ
O
Z
i
No. �
of
,ntrs ' d
J
2 X X
Date r I -me: IReceived by: (Signature
Date: Time: Rece- fa #by: (I'tature)
pH Temp
Flow Other
Trip Bank Rece
Tl_,l7jy�,( cC Battle
Da t Time:
Chain of Custody Page f- of
1eMa! ical
i
12065 Lebanon Rd �
Mount Juliet, TN 37122 s,-:
Phone:[phone]
phone. goo-767-5859 '
Fax: [phone]
SDG # 7
B06 5
Ta
Acctnum: EMARES
Temp€ate:T11413
Prelogin; P748417
PM: 8077 -Justin Carr l
PB: 1 pt`� ! — '?
Shipped via: FedEX Standard
Remarks Sample M (lab on ly)
SampleR�ce k.
DC Sea IPresent/ 1�.tact: R
Y N
CDC Signed/Accurate:
_,,Y _N
Bottles arrive intact:
rY N
�N
Correct bottles used:
_eY
sufficient volume sent:
Appli+cable
!i _N
If
VOA Zero Headspace:
Y _N
Preservation Correct/Checked:
N
RAD Screen <0.5 mR/hr:�N
If preservation required by Login: Date/Time
Hol
Conditi�
NCF / I� K