Loading...
HomeMy WebLinkAboutNCG510154_Regional Office Historical File Pre 2018NORTHWOOD RAVI N C I December 18, 2014 Mr. Richard Farmer, Water Quality Supervisor Charlotte -Mecklenburg Storm Water Services 700 North Tryon Street Charlotte, North Carolina 28202 Subject: Response to Notice of Violation THE VUE Charlotte Qn f) 215 North Pine Street Charlotte, North Carolina Dear Mr. Farmer: • • • s- • • .• • .• , • • flowedrecords after 3 years, Based on our knowledge of the site drainage system, it has likely been more than three years since water • • Mr. Friday revisited the property on November 26, 2014 and agreed that there had been no flow of water through the treatment system since his previous visit on October 30, 2014, Northwood Ravin is not discharging . into the storm sewer and has shut •- electrical power to the •.. in the sump connected to 'the subsurface drainage system. Thank you for your assistance on this project, If you have questions or need additional information, please call the undersigned at ° iwf Sin rely,, ' Gravid Ravin President Cc: Mr. Ken Friday, Charlotte -Mecklenburg Storm Water Services Mr. 'Robert Foster, t_.Q., AMFC Environment & Infrastructure, Inca 1057 EAST MOREHEAD STREET, SUITE 300, CHARLOTTE, NC 28204 WWW,NORTFIWOODRAVIN.COM MULTIFAMILY DEVELOPMENT PROPERTY MANAGEMENT CONSTRUCTION United States Environmental Protection Agency Form Approved. EPA Washington, D.C. 20460 OMB No, 2040-0057 Water: Compliance Inspection Report Approval expires 8-31-98 Section A: National Data System Coding (i.e, PCS) Transaction Code NPDES yr/mo/day Inspection Type Inspector Fac Type 1 N 5 1 3 NCG510514 ill 12 1 14110/30 117 181 1 19 S 20 Inspection Work Days Facility Self -Monitoring Evaluation Rating B1 CIA ------------ -------Reserved------- __:---- 7 0.0 70 71 N 72 1N 73 74 71 1 1 1 Section B: Facility Data Name and Location of Facility Inspected (For Industrial Users discharging to POTVV, also include Entry Time/Date Permit Effective Date POTW name and NPDES permit Number) 01:38PM 14110/30 07/06/11 The Vue Charlotte W Fifth St Exit Time/Date Permit Expiration Date Charlotte NC 28202 02:40PM 14/10/30 11/09/30 Name(s) of Onsite Representative(s)/Tities(s)/Phone and Fax Number(s) tither Facility Data tl1 Name, Address of Responsible Official/Title/Phone and Fax Number Contacted Mike Murray,150 E Robinson St Ste 200 Orlando FL 328014365/1407- 44-0089t No Section C: Areas Evaluated During Inspection (Check only those areas evaluated) Permit Facility Site Review Effluent/Receiving Waters Section D: Summary of Finding/Comments:(Attach additional sheets of narrative and checklists as necessary) (See attachment summary) Name(s) and Signature(s) of Inspector(s) Agency/OfficelPhone and Fax Numbers Date Marcia Allocco MRO WQ//704-663-1699 Ext.22047 q� d .en Signature of Management Q A Reviewer Agency/Office/Phone and Fax Numbers Date EPA Form 3560-3 (Rev 9-94) Previous editions are obsolete: Page# 1 yrtrrioiday LEJ Inspection Type 18 Page## Permit: NCG510514 Owner - Facility. The Vue Charlotte Inspection Date: 10/30/2014 Inspection Type: Compliance Evaluation Permit Yes No NA NE (If the present permit expires in 6 months or less). Has the permittee submitted a new 0 application? Is the facility as described in the permit? N [l Cl 1:1 # Are there any special conditions for the permit? 0 Is access to the plant site restricted to the general public? Is the inspector granted access to all areas for inspection? 0 El El El Comment: Permit covera e laosed in 2011 when buildina went into foreclosure. Site visit in'2013 could not verify ifs stem was discharaina to sanitary sewer or storm sewer. Facilit was to follow-up with QWQ inspector but nothing in file. Site visit verified that roundwater emediation s stern is connected to the City of Charlotte stormwater s stem and mav have dischar ed since permit coveracte, expired in 2011. lirected Ral h Smith Service Manager with Northwood -Ravin that ermlt covers e will need to be obtained and coDv of renewal application and cleneral Dermit Drovided while on site if it discharges,, Follow-u letter from Northwood Raven dated 12/19/14 notes that the s stem was watched from 10/30/14 to 11 /26/14 and no dischar e occurred. Correspondence notes that oowerto SUMD pumps has been deactivated so discharge cannot occur in future. Effluent Pipe Yes No NA N Is right of way to the outfall properly maintained? 11 Are the receiving water free of foam other than trace amounts and other debris? ,] If effluent (diffuser pipes are required) are they operating properly? El 0 N El Comment: 'Review of buildina plansshows that discharcie of treated aroundwater is connected to ON of Charlotte storm sewer in front of building,' This would necessitate coverage under CG510000 since dischar e would reach surface waters via the Cit 's stgrmwater s stem. ischarae to CM D sanitary system is prohibited. page# 3 FFV Allocco, Marcia From: Friday, Kenneth <Kenneth.Friday@mecklenburgcountync.gov> Sent: Wednesday, November 26, 2014 10:22 AM To: Farmer, Richard; Hunter.hicks@amec.com Cc: Allocco, Marcia Subject: RE: The VUE Attachments: The VUE 10-29-14.JPG; The VUE 11-26-14,JPG 22MM I went back to THE VUE, Tues. Nov. 251h, This was the end of the two week period to determine if there is any accumulation of ground water. I met with Ralph Smith, the service manager, and took pictures of the tank level. There has been no accumulation during the past two weeks; see attached picture, 10-29 and 11-25. Mr. Smith informed me that the system pumps were turned off two weeks ago to avoid any illicit discharge if there had been an accumulation of ground water in the tank. From: Farmer, Richard Sent: Monday, November 10, 2014 2:49 PM To: Hunter. hic s arnec,corn Cc: marcia.allocco_@gcdenr.gov; Friday, Kenneth Subject: The VUE Per our conversation, the float switches will be raised to determine if the water level in the holding tank rises or not. If the level rises, then the accumulated water will need to be discharged which will result in the need to have the permit renewed. if the level does not rise and there is no need to discharge, then there would be no violation and there would not be a need for a permit ( this would need to be demonstrated to NCDENR's satisfaction). If it is determined that no water needs to be discharged then the system would need to be deactivated going forward to ensure there is no illicit discharge in the future. A period of two weeks should be enough to determine if water is accumulating. Please advise the status at the end of the two week period. I Allocco, Marcia From: Farmer, Richard <Richard.Farmer@mecklenburgcountync.gov> Sent: Monday, November 10, 2014 2.49 PM To: Hunter.hicks@amec.com : Allocc, Marcia; Friday, Kenneth Subject: The VU Per our conversation, the float switches will be raised to determine f if the water level in the holding tank rises or not. if the level rises, then the accumulated water will need to be discharged which will result in the creed to have the permit renewed. If the level does not rise and there is no need to discharge, then there would be no violation and there would not be a need for a permit ( this would creed to be demonstrated to NC DENR"s satisfaction). If it is determined that no water needs to be discharged then the system would need to be deactivated going forward to ensure there is no illicit discharge in the future. A period of two weeks should be enough to determine if water is accumulating. Please advise the status at the end of the two week period. t Charlrft�-h?eckte€�bur� STORM 700 Tic>rtb Tryon Street Charlotte, NC 8202 ATER Fax 704.336,4391 3 GV�.pp, � ppryry *3' fit# November 3, 2014 is CERTIFIED MAIL RETURN RECEIPT RFQl1ES D Ralph Smith, Service Manager THE VUE Charlotte On 5th 215 North Pine Street Charlotte, NC 28202 Subject: NOTICE OF VIOLATION CHARLOTTE CITY CODE Chapter 18, Article III: Storm Water Pollution Section 18-81 a Illicit Discharge(s) and Disposal(s) Dear,. Smith: North Carolina General. Statute 16OA-459 authorizes cities to adopt;and enforce a stonn water control ordinance to ;protect water quality and control grater quantity. On October 301h 2014, Kenneth Friday of Charlotte -Mecklenburg Storm Water Services (C MSWS) and Marcia Allocco of the NC Department t of Environmental and Natural Resources ( 'CDE ) conducted an investigation of your property located at 215 North Pine Street in Charlotte, North Carolina, The investigation was nducted by auffiority granted under the City of Charlotte Storin Water Pollution Control Ordinance C'Ord" ance"), Section 18-82 Powers and Authority for Inspection. As a result of that inspection, the conditions described below were found on the property in violation of the Ordinance, Section 18-80 a Illicit Discharge(s)arge(s) and D sposal(s)a THE VUE property located at 215 N. Pie Street is discharging remediated ground water to the storm water system without a permit. Coverage to discharge under a pe 't, (Certificate of Coverage NC G 510514) was issued on June 11, 2007, and expired September 30,2011. You were verbally notified of the violation on October 30'� 2014 and directed. to immediately cease the discharge(s) causing the violation, To achieve compliance with the legal requirements of the Ordinance, you must implement the corrective actions listed below; To report pollution or drainage problems call: 311 http:l/ tormwater. ixarm ck,or Ralph Smith, Service Manager Fags November 3, 201 rstexn. out a Permit. ter. -IA 1,1­ OXAQ"CXI Z frN A4,onitoo fli .se contact meat 704. 36- 'l 2. Please be aware that a meeting request dries not )m completing the corrective actions listed above and does not negate a potential . ,. .., A local, state, or federal regulations. Your prompt cooperation in this matter is requested. Sincerely, Richard Farmer, Water Quality Supervisor Charlotte -Mecklenburg Storm Water Services KLF cc: Craig :hiller, C SWS Rusty R.ozzelle, CMSWS Allocco, Marcia Thursday, October 30, 201 4:t Denard, Derek; Weaver, Charle 'rrsm th@nwrliving.com ; Frida Renewal of NCG511514 - The High r.; i (Kenneth.F(day@mecklenburgcountync.gov) otte, LLC . Wo aas possible. possime. ivitLvutlr/city or c.nanotte is consiaering a Notice oT vioiation Tor aiscriarging xo tneir storm Water system' without a permit so quickapplication and processing by DWR would be weighed in any decision regarding the possible notice. Thanks for your assistance, Marcia w " 'Wet ft**W"W Marcia Allocco, MS — Senior Environmental Specialist NC Crept. of Environment & Natural Resources (NCDENR) Division of Water Resources - Water Quality Regional; Operations 610 East Center Ave., Suite 301,, Mooresville, NC 28115 Phone: (704) 5- 204 Fax: (704) 663-6040 marcia.allocco ncdenr. ov w;n star uali or Please note that effective Oct. 15, 2013, the MRO copy fee is 0,05/page, This applies to all copies; the first 25 pages are no longer free.? E-mail correspondence to and from this address may be subject to the North Carolina Public Records Lair and may be disclosed to third parties finless the content is exempt by statute or offer regulation, 1 ia Pr From: Allocco, Marcia Sent: Thursday, October 30, 2014 4:04 PM To: I rsmith@nwrliving.com' Subject: FW: Renewal of NCG510514 - The Vue Charlotte, LLC Importance: High Mr. Smith, I had your address incorrect in my first attempt to send this e-mail so I am forwarding it under separate cover, Regards, Marcia Allocco Gentlemen, Not sure which one of you will get this permit renewal application (or perhaps someone else in the group) but please be on the lookout for it. There was confusion when the building was foreclosed in 2012 regarding the discharge location of the treated groundwater. Thanks for your assistance, Marcia Of Marcia Allocco, MS — Senior Environmental Specialist NC Dept. of Environment & Natural Resources (NCDENR) Division of Water Resources - Water Quality Regional Operations 610 East Center Ave,, Suite 301, Mooresville, NC 28115 NPDEF 3 L NC516 8 L�j19 1 . 12 21 Inspection Work Clays Facility Self -Monitoring Evaluation Rating B1 CA 87 0.0 70 Lj 71 N 72 73 74 758C? Section 8: Facility Data Name and Location of facility Inspected (For Industrial Users discharging to POTW, also include Entry Time/Date Permit Effective Date P TW name and NPDES permit Number) 01:38P 14110/30 07106111 The Vue Charlotte W Fifth St Exit Time/Date Permit Expiration Date Charlotte NC 28202 0 :40PM 14/10/30 11/09/30 Name(s) of Onsite Representative(s)/Titles(s)/Phone and Fax Number(s) Other Facility Data 1Il Name, Address of Responsible OfficialrTitle/Phone and Fax Number Contacted Mike Murray,150 E Robinson St Ste 200 Orlando FL 328014365//407-244-00891 No Section C: Areas Evaluated During Inspection (Check only those areas evaluated) Permit Facility Site Review ® Effluent/Receiving Waters Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary) (See attachmentsummary) Name(s) and Signature(s) of inspector(s) Agency/Office/Phone and Fax Numbers Cate Marcia Allocco MRO WQ/604-66 -1699 Ext.2204/ Signature of Management Q A Reviewer Agency/OfficelPhone and Fax Numbers Date EPA Form 3560-3 (Rev 9-94) Previous editions are obsolete. Page# l yrtmolday Inspection 11 12 14/10/30 17 18 U Type Paq Permit: NCG510514 Owner - Facility: The Vue Charlotte IP1Inspection Date: 10/30/2014 Inspection Type: Compliance Evaluation Permit Yes Ni_ N (If the present permit expires in E months or less), Has the permittee submitted a new [� application? Is the facility as described in the permit? # Are there any special conditions for the permit? [l Is access to the plant site restricted to the general public? 0 13 El El Is the inspector granted access to all areas for inspection? Comment: hermit covera e la sed in 2011 when buildin went into foreclosure. Site visit in 2013 could not verifv ifs stem was discharaina to sanitary sewer or storm sewer. Facilit was to follow-ur> with DWQ inspector but nothina in file. Site visit verified that aroundwater remedietion s stem is connected to the Cit oaf Charlotte storrrlwater s atom and ma have oiist'taf ed since ermit covers e e° fired in'011. Ctifecteo F�.al smith; aervico Mane er with Northwood-fav"tn that ermit sofa e will need to be cabtained and co of renewal aDdication and aeneral oermit, rovidd whip on site. Effluent Pipe Yes Na NA N Is right of way to the outfall properly maintained? Are the receiving water free of foam other than trace amounts and other debris? 13 El El If effluent (diffuser pipes are required) ; are they operating property? El El N El Comment; review of bull cin lens shows that ischaf e of treated roundweter is connected to Ct of Charlotte storm sewer in front of buildin , This would necessitate covers e undef NCG 10000 since dischaf e would reach surface waters via the Qit °s stormwater s steal. C?ischar e to CtJC} senile s stem is fohlited. Page Allocco, Marcia From: Downs, Tim tdowns@ci.charlotte.nc.us Sent: Monday, October 27, 2014 9:41 A To: Allocco, Marcia; Noal Hudson Subject: RE: The VUE 215 N. Fine Street, Charlotte, NC - treated groundwater discharge Marcia, 1 checked and we have no record of a Ground Water rernediation discharge permit for the sanitary serer being issued t The V JE property. Your records are correct, CMUD was not accepting Ground water during that time frame: Donna Hood did contact me last year and 1 checked then for the permit too and could not find a record of one. Let me knows if you heed anything else: Tim Tim Downs Environmental Compliance Supervisor Environmental Management/System Protection Charlotte -Mecklenburg Utility [department 4222 Westmont Drive Charlotte, NC 28217 From: Allocco, Marcia mailt l.marcia.allocco ncdenr. ov Sent: Friday, October 24, 2014 3:28 PM To: Noal Hudson c: Downs, Tim Subject: RE: The VUF 215 N. Pine Street, Charlotte, NC - treated groundwater discharge Importance: High ME 1 apologize for the lateness in my reply but your e-mail arrived when i was out of the office on training and it got Mast in my inbox until my clear -out today. The Vine property in downtown Charlotte had coverage (Certificate of Coverage NC( 510514) under our general permit to discharge remedated groundwater that was contaminated with petroleum products (NCG510000) to the City of Charlotte's storrnwater system with eventual discharge to surface waters. Coverage under the permit was issued on June 11, 2007, and expired on September 30, 2011, since continued permit coverage was not requested when the general permit was renewed. A site visit was conducted by myself and Donna Hood on Februarys 5, 2013, to ascertain if permit coverage was still required. We met with staff on site from Northwood -Ravin and they showed us the room where the reined ation system had been located at one time but 1 do not remember seeing any carbon filters but 1 may be mistaken. They also noted that they pump water from a sump in the loading area at the northeastern end of the building to a manhole on North Pine Street. It was unclear whether this was a sanitary manhole or a stormwater manhole and from where this water originated. Donna Hood informed the Northwood -Ravin contact that they needed to follow-up with WQ/ WR when they determine to what system the water was being discharged and the source of the water. 1 cannot find any a to the ider our ­4 ­A+L, treatment system. MACTEC's telephone conversation with representatives of the CIVIUD administration division on February 5, 2007, confirmed the City Code." I have copied Tim Downs with CIVIUD's system protection group so he can verify whether approval has been granted by CIVIUD to discharge treated groundwater at this location. Please follow-up with me regarding the status of the discharge from the sump at the northeast end of the building noted during the site visit in 2013 and whether permit coverage under a NPDES permit should be obtained. Regards, Marcia Allocco From: Noal Hudson [mailto:nhudsonL&ebiconsultingcom] Sent: Monday, October 06, 2014 3:43 PM To: All co, Marcia Subject: The VUE 215 N. Pine Street, Charlotte, NC I am conduct an ESA on The VUE in downtown Charlotte. The VUE has a sump in the basement, the collected water is discharged to the sanitary sewer system after carbon filtering. The carbon filters were set in place to address historical UST petroleum releases from onsite (UST #36417) and (UST #06921) adjacent sources. Questions: 1) Is there an NPDES permit associated with onsite sump? What is the current status of this release, my sources show an NFA dated 4/17/2008? 2) What is the current status of City View Towers 425 W. 5th Street (UST #06921)? Reportedly, 2.2 feet of free product existed on site at one point. My site, The VUE, is located down gradient. Noal Hudson Senior Project Scientist Cell: 843-737-3758 nhudsoriftebiconsgaigg= Visit our new website: www. ebiconsulti!2fl.corn 4,iEBI Consulting Please consider the environment before printing this email 2 ►, Marcia 4romz Allocco, Marcia lent: Friday, October 24, 2014 3 28 PM ro: 'Noal Hudson' E : Downs, Tire (tdowns ci.ch rlotte.nc.us) subject. ICE. The V E 215 N. Pine Street, Charlotte, N -:treated groundwater discharge Importance: High goal, ! apologize for the lateness in my reply but your e-mail arrived when I was out of the office on training and it got lost in y Inbox until my clear -writ today. The Vine property in downtown Charlotte had coverage (Certificate of Coverage NCi3510514) under our general permit to discharge rerned�ated groundwater that was contaminated with petroleum products (NCG510000) to the City of Charlotte's stormwater system with eventual discharge to surface waters. Coverage under the permit was issued on June 11, 2007, and expired on September 30, 2011, since continued permit coverage was not requested when the general permit was renewed, A site visit was conducted by myself and Donna Hood on February 5, 2013, to ascertain if permit coverage was still required. We met with staff on site from Northwood -Ravin and they showed us the room where the rerne iation system had been located at one time but I do not remember seeing any carbon filters but I may be mistaken. They also noted that they pump water from a sump in the loading area at the northeastern end of the building to a manhole on North Pine Street. It was unclear whether this was a:sanitary manhole or a stormwater manhole and from where this water originated. Donna flood informed the Northwood -Ravin contact that they needed to follow-up with DWQ/DWR when they determine to what system the water was being discharged and the source of the water. I cannot find any information in the file that Northwood -Ravin personnel had provided an update and Ms. Hood has moved onto a different division within DENR. You noted the following in your e-mail, "The VIDE has a sump in the basement, the collected water is discharged to the sanitary sewer system after carbon filtering" which I find troubling since the original application for coverage under our general wastewater permit completed by MA TEC notes, "A connection with an existing sanitary sewer associated with Charlotte Mecklenburg Utilities Department (CMUU) is not feasible due to City of Charlotte Code (Chapter 2, Appendix III Section 23-29b[141 that disallows the discharge of stormwater or groundwater to the sanitary sewer and wastewater treatment system. MACT C`s telephone conversation with representatives of the CMUO administration division on February 5, 2007, confirmed the City Code." I have copied Tim Frowns with CMUD's system protection group so he can verify whether approval has been granted by €:MUD to discharge treated groundwater at this location. Please follow-up with me regarding the status of the discharge from the sump at the northeast end of the building rooted during the site visit in 2013 and whether permit coverage under a J PDES permit should be obtained Regards, Marcia Alloccea �r 06, 2014 3:43 PM > N. Pine Street, Charlotte, NC n The VUE in downtown Charlol M te. The VUE has a sump in the basement, the collected water is UST petroleum releases from onsite (UST #3 417) and (UST 06 2) adjacent sources. Questions: 1) Is there an NPDES permit associated with onsite sump? What is the current status of this release, my sources show an NFA dated .j1 008? 2) What is the current status of City View Towers 425 W.5th Street (UST #021) Reportedly, 2.2 feet of free product existed on site at one point. My site, The VUE, is located down gradient. oal Hudson Senior Project Scientist Cell. 43-737-3755 nhudonexconsltln ,om Visit our new website. www.ebiconsulting.rnrgi 4ES1 Consulting Please consider the environment before printing this email 2 ppppppp- Allocco, Marcia From: Neal Hudson <nhudsonbiconsulting.com> To: Allocco, Marcia Sent: Friday, October 24, 2014 3:29 PM ` Subject: Read: RE: The VUE 215 N. Pine Street, Charlotte, NC - treated groundwater discharge Your message To: Subject: The VUE 215 N. Pine Street, Charlotte, NC - treated groundwater discharge Sent: Friday, October 24„ 2014 3:29:03 P (UTC-05:00) Eastern Time (US & Canada) was read on Friday, October 24 2014 :28:59 P ( TC-05:00) Eastern Time (US & Canada). 4rMACTEC engineering nd Constructing a better tomorrow May 20, 2008 E I V E D Ms, Dee Browder � , Y � North Carolina Department of Environment and � ;: 2 200 Natural Resources 1 WQ, Surface Water Protection I 610 Fast Center Avenue, Suite 301 t Mooresville, North Carolina 2811 t lon Subject: Notice of Owner Change The Vue Condominium Project 418 "west 5"' Sheet Charlotte, North Carolina NPDES General Permit No. NCG510000 Certificate of Coverage NCG510514 MACTEC Project: t 228-t17-4205 Dear Ms. Browder: This letter is to inform you of a change in ownership of the subject project. The subject permit was issued in 2007 to VUE Charlotte, LLC an entity of Churchill Development in Orlando, Florida. The new owners "The Vue-Charlotte, LLCM are an entity of MOLL Companies, Mr. Randy Grueb, Vice President, should be listed as the permit contact. Mr. Grueb can be reached at 1170 Peachtree Street NNE, Suite 1200, Atlanta, Georgia 30309. Sincerely, MACTEC ENGINEERING AND CONSULTING, INC. Robert C. Foster Principal Geologist Cc: Mr. Randy Grueb MACTEC Engineering and Consulting, Inc: 2801 Yotkmont Road, Suite 100 * Charlotte, NC 28208 + Phone: 704,357.8600 • Fax: 704,357.8 38 www.rnactec.corn PPPPPP` \N%VtN4AT4 Michael F. Easley 0 Governor At"A R William G. Ross, Jr., Secretary 0 7 UEN > North Carolina Department of EnvironmeutanAjiAlival Resources Alan W41) PE 91 WE` of Water Quality June 11, 2007 JUN, Mike Murray 426 East Central Blvd. Orlando, FL 32801 V Subject: General Permit No. NCG510000 Certificate of Coverage NCG510514 Authorization to Construct VUE Charlotte, LLC Mecklenburg County Dear Mr. Murray: General Permit Coverage. In accordance with your application for discharge, the Division is forwarding herewith the subject Certificate of Coverage to discharge under the subject state- ICES general permit. This permit is issued pursuant to the requirements of No Carolina General Statue 143-215 .1 and the Memorandum of Agreement between No Carolina and the US Environmental Protection agency dated May 9, 1994 (or as subsequently amended). The following information is included with your permit package: • A copy of the Certificate of Coverage for your treatment facility • A copy of General Wastewater Discharge Permit NCG510000 • A copy of a Technical Bulletin for General Wastewater Discharge Pennit NCG510000 • Engineer's Certification to be completed and returned. If any parts, measurement frequencies or sampling requirements contained in this general permit are unacceptable to you, you have the right to request an individual permit by submitting an individual permit application. Unless such demand is made, the certificate of coverage shall be final and binding. Please take notice that this Certificate of Coverage is not transferable except after notice to the Division of Water coverage. This permit does not affect the legal requirements to obtain other pennits which may be required by the Division of Water Quality or permits required by the Division of Land Resources, Coastal Area Management Act or any other Federal or Local goverrintental permit that may be required. Authorization to Construct Permit. In accordance with your application for discharge, the Division is also authorizing the construction of a groundwater remethation system consisting of a primary settling tank, oil water separator, oil storage tank, four bag filters (25 gpin each), two GAC vessels (2,000 lbs, each), sedimentation tank (5,000 gallons), a sflow meter, and all associated pumps, piping, and controls with a discharge of 0.024 MGD of treated wastewater into an unnamed tributary to Little Sugar Creek, classified C waters in the Catawba River Basin. This Authorization to Construct pen -nit is issued in accordance with Part 111, Paragraph 2 of NPDES Permit No. NCG550000, and shall be subject to revocation unless the wastewater treatment facilities are constructed in accordance with the conditions and limitations specified in Permit No. NCG550000. In the event that the facilities fail to perform satisfactorily, including the creation of nuisance conditions, the Pennittee shall take inimediate corrective action, including those as may be required by this Division, such as the construction of additional or replacement wastewater treatment or, disposal facilities. Failure to abide by the requirements contained in this N. C. Division of Water Quality / NPDES Unit Phone- (919) 733-5083 1617 Mail Service Center, Raleigh, NC 27699-1617 fax: (919) 733-0719 Internet: h2o,enr,statenc.us DENR Customer Service Center: 1800 623-7748 -,qqqq Authorization to Construct may subject the Permittee to an enforcement action by the Division of Water Quality in accordance with North Carolina General Statute 143-215,6A to 143-215.6C. The Mooresville Regional Office, telephone number 704/663-1699, shall be notified at least forty-eight (48) hours in advance of operation of the installed facilities so that an in -place inspection can be made. Such notification to the regional supervisor shall be made during the normal office hours from 8:00 a.m. until 5:00 p.m. on Monday through Friday, excluding State Holidays. Upon completion of construction and prior to operation of this permitted facility, an Engineer's Certification must be received certifying that the permitted facility has been installed in accordance with the NPDES Permit, the Certificate of Coverage, this Authorization to Construct and the approved plans and specifications. Mail the completed Engineer's Certification to the NPDES Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617. A copy of the approved plans and specifications shall be maintained on file by the Permittee for the life of the facility. NPDES Permit Contact. If you have any questions concerning the requirements of this permit, please contact Sergei Chemikov at telephone number 919/733-5083, extension 594. Sincerely, Coleen H. Sullins cc: Central Files NPDES General Permit Files Michael I DePalma, P.E. MACTEC, 2801 Yorlanont Rd., Suite 100, Charlotte, NC 28208 STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT NATURAL SO CES DIVISION OF WATER QUALITY CERTIFICATE OF COVERAGE NCG510514 GENERAL PERMIT NO. NCG510000 TO DISCHARGE DOMESTIC WASTEWATERS FROM SINGLE FAMILY RESIDENCES AND OTHER DISCHARGES WITH SIMILAR CHARACrERISTICS UNDER THE NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-21,5.1, other lawful standards and regulations promulgated and adapted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, VUE Charlotte, LLC is hereby authorized to construct and operate a groundwater treatment facility consisting of a primary settlingtank, oil water separator, tail storage tank, four bag filters, two GAC vessels, sedimentation tank, flow meter, and all associated pumps, piping and controls for petroleum contaminated groundwater or similar waste streams 'th the discharge of treated wastewater from a facility located at the VUE Charlotte, LLC West Fifth Street and North Time Street Charlotte Alamance County to receiving waters designated as unnamed tributary to Little Sugar Creep in the Catawba River Basin in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts 1, 11, 111 and IV of General Permit NC s51C1000 as attached. This certificate of coverage shall become effective June 11, 2007 This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this clay June 11, 2007 a, X , y Coleen H. Sullins, Director Division of Water Quality By Authority of the Environmental Management Commission "qqq NCG510514 Engineer's Certification L as a duly registered Professional Engineer in the State of North Carolina, having been authorized to observe (periodically, weekly, full time) the construction of the following groundwater treatment system project: Project Name Location For the permittee hereby state that, to the best of my abilities, due care and diligence was used in the observation of the construction such that the construction was observed to be built within substantial compliance and intent of the approved plans and specifications. Signature Registration No. Date Natural tegetati kh� � � " 6 i� �• * ', AV ,Areas 3 ■ tructurss 1115t ." 5trearil Raaclsrepn .. 5 fi RO SrTE 4: c .rt Er a F THE VUE HIGH—RISE CONDOMINIUM DEVELOPMENT NORTH CAROUNA CHARLOTTE, NORTH *�*A No 6 73-05N � IIII � III2I Nn i #� PVSOC PRIORITY PROJECT: No fo: NPDES Unit Water Quality Section Attention: Sergei Chemikov Date: June 4, 2007 NPDES STAFF REPORT AND RECOMMENDATIONS County: Mecklenburg NPDES Permit No.: NCG510514 PART I - GENERAL INFORMATION 1. Facility and address: The VUE Charlotte, LLC 426 East Central Boulevard Orlando, Florida 32801 2. Date of investigation: May 31, 2007 3. Report prepared by, its L. Parker, Environmental Engineer 11 4. Person contacted and telephone nw-nber: Michael DePahna, P.E. (704) 357-8600 5. Directions to site: The site is located at the jet. of West Fifth Street and North Pine Street in the City of Charlotte. 6. Discharge point(s), list for all discharge points: - Latitude: 350 13'50" Longitude: 80" 40'40" Attach a USGS Map Extract and indicate treatment plant site and discharge point on map. USGS Quad No.: G I 5NE T Site size and expansion area consistent with application: Yes. There is arnple area available for the construction of the proposed WWT facilities. & Topography (relationship to flood plain included): The site is relatively flat (currently a down town parking lot), and is far removed from any flood plain. 9. Location of nearest dwelling: None with 500+ feet of the proposed WWTP site. Page Two 10. Receiving stream or affected surface waters: UT to Little Sugar Creek a. Classification: b, River Basin and Subbasin No.: Catawba 030834 C. Describe receiving stream futures and pertinent downstrea uses: The discharge will enter an existing on -site storm sewer system and travel for several hundred feet before entering a surface water drainage channel that eventually runs into the receiving stream. The receiving stream mows through a heavily developed portion of the City of Charlotte and receives stormwater front.a number of sources. PART II - DESCRIPTION OF DISCHARGE AND TREATMENT WORKS 1. a. Volume of wastewater: 0,024 MGD (resign Capacity) br What is the current permitted capacity: N/A C. Actual treatment capacity of current facility (current design capacity): N/A d. Date(s) and construction activities allowed by previous ATCs issued in the previous two years: There, have been no ATCs issued to this facility. e. Description of existing or substantially constructed WWT facilities: There are no existing WWT`facilities (proposed). 1". Description of proposed WW'f facilities: The applicant proposes to construct a GW rem diation treatment system consisting of a primary settling tank, four bag filters, two CAC; vessels, and an effluent flow ureter. The system will also include an oil/water separator and nail storage tank if free product is encountered during excavation. g. Possible toxic impacts to surface waters: Potential toxic impacts are unknown at this time: . Residual handling and utilization/disposal scheme: Residuals generation is not expected, however, should free product be encountered during excavation, waste oil will be collected and disposed of via a waste oil reclamation firm. . Treatment plant classification.: Class I . SIC Code(s): 9999 Wastewater Code(s): 66 MTU Code(s): 53200 PART III - OTHER PERTINENTINFORMATION 1. Is this facility being constructed with Construction Grant Funds or are any public monies involved (municipals only)? No public monies will be used in the construction of this facility. . Special monitoring or limitations (including toxicity) requests: None at this time. e Three Important S )C/JOC or Compliance Schedule dates: This facility is neither under an S C nor is one being considered at this time. Alternative analysis evaluation a. Spray Irrigation: Insufficient area. . Connect to regional sewer system. The local P iTW will not allow wastewater from GW remer adiation systems into their collection system. C. Subsurface: Insufficient area.. d. Other disposal options; None that we are aware. XT I EVALUATION AND RECOMMENDATIONS oleum contaminated GW collected from the excavation and e- A residential and commercial development proposed for a site loci 'fifth Strut and North Pine Street in the City of Charlotte. 4tected t the site have shown the presence of petroleum punted, pre -fabricated CAW -treatment system that will ultimately discharge to the City o Charlotte's stormwater collection system that exists adjacent to the site. The wastewater will travel for several hundred feet before discharging; into a drainage feature that eventually enters the receiving strearn. Pending a final technical review by the NPDES Unit, it is recommended that a GP be issued as requested.. Signature of Report'Preparer ate Water Quality Regional Supervisor Date hAdsrtdsr07VFheV T-.dsr MC&510514 GIS�IE Michael F. Easley { Governor Cej William G. Ross Jr., Secretary North Carolina Department of Environment and Natural Resources S Alan Klimek, P.E. Acting Director Division of Water Quality This application has been assigned to Sergei Chemikov 919/733-5083) Ext. 594 of our NPDES Unit for review. You will be advised of any comments, recommendations, questions or other information necessary for the review of the application. I am, by copy of this letter, requesting that our Regional Office Supervisor prepare a staff report and; recommendations regarding this discharge. If you have any questions regarding this application, please contact the review person listed above. Sincerer/17 , Sergei he ikov, Ph.D. E virc enta Engineer H ICES -West cc: ichael J. le a rya, MACTC Engineering and Consulting, Inc, 801 Yorkmont Road, Suite 190 Charlotte,; NC 28208 ARAW NCD NR Customer Service Division of Water Quality 1617 Mail Service Center Raleigh, NC 7699-1617 (919) T -701 �N A Michael F. Easley Governor 0 C William G. Ross Jr., Secretary North Carolina Department of Environment and Natural Resources Alan Klimek, P.E. Acting Director Division of Water Quality April 4, 2007 Mike Murray 426 East Central Blvd. Orlando, FL 32801 Subject: Application No. NCG510514 The VUE Charlotte, LLC Mecklenburg County Dear Mr. Murray: This is to acknowledge receipt of the following documents on March 23, 2006: x Completed Notice of Intent (Application form), Engineering Proposal (for proposed control facilities), 7 "','RCES x Request for certificate of coverage 9 M R Application processing fee of $50.00. Engineering Economics Alternatives Analysis, x Engineering Plans and Specifications APR C E',tn op Local Government Signoff, Source Reduction and Recycling, Interbasin Transfer, Service and repair receipts. The items checked below are needed before review can begin: — Completed Notice of Intent (Application Form), — Engineering proposal (see attachment), Application Processing Fee of $50.00, Delegation of Authority (see attached), Biocide Sheet (see attached), Engineering Economics Alteratives Analysis, Engineering Plans and Specifications Local Government Signoff, Source Reduction and Recycling, Interbasin Transfer, Other: OMER itomer Service Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 (919)733-7015 4 1114 A' FMACTEC engineering and constructing a better tomorrow February 9, 2007 Mr. Bob Sledge NC>DE NR Department of Water Quality NPDES Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: Notice of Intent for NPDE+ S Coverage, NCG51fltl€l The VUE High -Rise Condominium Development West Fifth and North fine Streets Charlotte, North Carolina MALT `C'. Project 637-tl5-0002 Dear Mr. Sledge: MACTEC? Engineering and Consulting, Inc. (MALT C), on behalf of The VUE Charlotte, , LLC, _G) 51(}000, in accordance with they Nation for Tl-ae VUE site (The VUE) located in up fern coverage under the LEES to d ,er to applicable State receiving waters, r vicinity and site maps, treatment systs was authorized by The VUE Charlotte, LT dlutant Discharge Eliminatit Charlotte, North Carolina. krge treated petroleurn-coal ►tied with this submittal is flans and laboratory analyl provide this NC11 through a by an e-mail dated January A copy of the authorization e-mail is attached to this letter. A site location reap is presented a ' Figure 1. A site plan is presented as Figure 2. PROJECT FORMATION The VUE site is a proposed 51-story mixed residential and comanercial development located in uptown Charlotte, luring precor structic n geotechnical and environmental subsurface investigation, groundwater samples indicated the presence of petroleum 'hydrocarbons. MACTFC is currently providing environmental 'activities including active free product recovery/groundwater r mediation system of a gasoline and diesel release at an adjacent upg-adient property. Based on historical information, there is the potential for groundwater at The Vue site to contain petroleum hydrocarbon contamination from the adjacent property source area. During construction activities, the proposed grade of` "he VUE site shall require excavating and dewatering of the site, Due to the potential of contaminated groundwater to be discharged during de attiring, MACTEC is submitting this NOT on behalf of The VUE Charlotte, LL.C" for coverage under 1` CG510000 to discharge groundwater to the storm water sewer system, operated' by Charlotte -Mecklenburg Storrn Sewer Services. MACTEC intends to install a trailer -mounted pre -fabricated groundwater treatment system which: will include are, oil/water separator, bat; Ater and activated carbon chambers. A settling tank shall' also be incorporated outside the trailer as an initial step in the treatment process. The oil/water separator is included within the treatment design to increase settling time and will be available for free product recovery, if necessary. The treatment system was designed by and will be supplied by Acclua Della, Inc. ( 1), a MACTE '-approved subcontractor. A: treatment system design and MAC`EC Engineering and Consulting, Inc. 2801 Yorkmont Rood,. Suite, 100 0 Charlotte, NC 28208 • Phonc. 704,357,860 * 704,35T8638 www.rnadec,com Notic-. o Intent for NPI)ES Coverage February 9, 2007 The VUE Tower Site, Charlotte, Nonh Carolina IWAC'TEC Project: 63"-05-000 layout is presented as Figure 3. Specific information concerning the design is incorporated in the Notice of latent (NOI) attached to this letter. As an of site source was identified and is currently being rentediated,` MAC` °EC and The VUE Charlotte, LLC have not submitted`` a Corrective Action Flan (CAP) for The VUE site. ANALYTICAL I E A' MAC,TEC proposes to utilize this renrediation system to provide 'additional assurance groundwater discharged to the storm water sewer system shall not adverselyimpact water duality to receiving waters at sewer discharges. Groundwater samples from monitoring wells associated with The VUE site were collected on January 21 2007, at four existing monitoring wells located at the site. The collected samples were analyzed at a North Carolina accredited laboratory for petroleum hydrocarbons via EPA Method 601/602 ' and sertii-volatile organic compounds (SVOCs) by EPA Method 625, Laboratory analytical results indicated benzene, toluene, ethylbenzene, and xylenes (BTE: ), and naphthalene in groundwater at concentrations that exceeded the laboratory reporting limit. Methyl -tertiary -butyl -ether (MTBE), 1,2-dichloroe pane and phenol were not detected in groundwater at concentrations that exceeded the laboratory reporting hinit. An estimation of carbon breakthrough time for the treatment system to be utilized at the site is attached to this letter, The laboratory analytical report is also attached to this letter. ENGINEERED ALTERNATIVE ANALYSIS As required in the NC7l, alternates to direct discharge were reviewed for feasibility. The VUE consists of an approximately 1;.3-acre parcel located within. uptown Charlotte. Due to the development of the surrounding areas and the limited footprint area of the site, subsurface; application (nitrification field, infiltration gallery, etc) is not considered feasible, ;A connection with an existing sanitary sewer associated with the Charlotte Mecklenburg Utilities Department (CMUD) is not feasible due to City of Charlotte Code (Chapter 23, Appendix 111 Section 3-7b water treatment system. MALT C's telephone conversation with representatives of the CMUD administration division on February 5, 2007 confirmed the City Code. Based on these limitations, discharge of. the collected storm water;and groundwater dewatered` from the site shall be released to the storm sewer system under proper NPDES pentritting requirements. Notice of Intent for Februaty 9, 2007 ' The Vue Tower Site, Charlotte, North Carolina UACTEC Project: 6373-05-0002 CLOSING MACTEC is submitting three copies of the NOI as well as associated attachments as requested within the N01 application. If you have any questions concerning this NOI, please contact the undersigned at (704) 357-86K Sincerely, MACTEC Engineering and Consulting, Inc. Michael J. DePalma, P.E. iobert �CFoster P.G� Project Engineer Principal cc: Mr. Michael S. Murray MACTEC file Attachments: ' Mhorization to Proceed (via email) N01 Application Figure 1: Site Location / Surrounding Property Figure 2: Site Map Figure 3: Treatment System Layout Carbon Breakthrough Calculations Laboratory Analytical Report 3 to be submitted with this application. P ) This NPDES permit application applies to which of the following. New or Proposed Does the facility have an approved CAP? E3Yes No If yes, date approved: If no, please contact the Regional Office Groundwater Section to determine the status of CAP approval and/or authorization to proceed if immediate remediation is recommended, Regional Office contact person: Y'. 9 r Site Ranking (A - ). GW incident C3 Modification Please describe the modification: El Renewal Please specify existing permit number and original issue date: Page 1 of 4 04105 NCG510000 N.O.I. toes this facility have any other NPDES permits? 0 Yes R/N 0 If yes, list the permit numbers for all current NPDES permits for this facility: 6) Description of discharge: a) Is the discharge directly to the receiving water? 2(Yes El No If no, submit a site map with the pathway to the potential receiving waters clearly marked. b) Number of discharge points (ditches, pipes, etc. that convey wastewater from the property): c) Volume of discharge per each discharge point (in GPD)- lappi2xim"k 2VOX 6d) 1,�Taem) 7) Discharge frequency: a) The discharge is: 13 Continuous IR(intermittent If the is harge is intermittent, d ascribe when the dischargewill occur: Alr;al achv`el MAIO ad lal� etlw'6! b) What is the source(s) of contamin Lion e.gasoline, die el, solvents,et . cu')wh�e Od ;P51Ae_ General permits may be obtained for gasoline and/or heavy fuel contamination. An individual nermit dpplication must be submitted for sites contaminated with other constituents such as solvents and p eslicides. _ c) Is free product present? DYes No If yes, a product storage tank and an oil/water separator are required. Free product is defined as any measurable accumulation of 1/8" or more in a well or floating on surface water. 8) Treatment system components. Please note: Final design specifications for the actual system that will be installed must be heck all of the following that apply.- E� Oil/Water Separator 0 Air Stripper 8/carbon Adsorption E40tei E(Other.- di;nepj4tl f) ' 1k a) If an Oil/Water separator is present, please provide the following information: 1) Rated flow capacity of the unit (in GPM): ii) Volume of unit (gat): G 2-1 iii) Detention time (min): ; iv) Free product disposal method: "'Vro" , ,, _" b) If an air stripper is present, please provide the following information, i) Rated flow capacity of the unit (in GPM)-. ii) Air provided for stripping (in CFM), iii) Air to Water ratio: iv) Number of trays (if applicable): (Removal efficiencies for all chemicals of concern should be included in this submittal. Efficiencies should be expressed as a percentage, i.e. 981/6 or 0.98) c) If carbon adsorption is present, please provide the following information: i) Rated flow capacity of the unit(s) (in GPM): /00 ii) Number of carbon units and arrangement if number exceeds one (Le., in parallel or in series): iii) Pounds of carbon in each unit- It.'s Page 2 of 4 SWU-213-100101 NCG510000 N.O.I. iv) Specify carbon breakthrough time: V� (The method used to calculate breakthrough time must included in the submittal.) d) If filters are used, please provide the following information: i) Rated flow capacity of each unit(s) (in GPM): ii) Arrangement of particulate filters within the system: 0 parallel 131'series Jj 9) Receiving waters: a) What is the name of the body or bodies of water (creek, stream, river, lake, etc.) that the facility wastewater discharges end up in? If the wastewater dischargp,!p to abeeparate storm sewer system, 4S (4S), name the operator of the (e.g. City of Raleigh). b) Stream Classification (i.e. WS-IV, C, SA, etc)- 10) Alternatives to direct discharge: Address the feasibility of implementing each of the following non -discharge alternatives: a) Connection to a Regional Sewer Collection System - If the facility is existing and currently discharges to a POTW, when will connection be terminated? b) Subsurface disposal (including nitrification field, infiltration gallery, injection wells, etc.) c) Spray irrigation The alternatives to discharge analysis should include boring logs and/or other information indicating that a subsurface system is neither feasible nor practical as well as written confirmation indicating that connection to a POTW is not an option. It should also include a present value of costs analysis as lication requirements: oposed discharges, the following information must be included in triplicate will be returned as incomplete. clearly indicated. b) A site map clearly tracing the pathway of the discharged water from the site to its discharge point, if the discharge is not directly to a stream. c) If the discharge will cross or empty into any easements, right-of-ways, or other public/private property, i.e. DOT, utilities, ditches, etc., before entering the permitted discharge stream, proof that approval was received from the appropriate landowners and/or agencies must be provided prior to issuance of the permit, d) If this application is being submitted by a consulting engineer (or engineering firm), include documentation from the applicant showing that the engineer (or firm) submitting the application has been designated an authorized representative of the applicant. e) Final plans for the treatment system (if application is for a new or modified permit). The plans must be signed and sealed by a North Carolina registered Professional Engineer and stamped -"Final Design -Not released for construction". f) Final specifications for all major treatment components (if application is for a new or modified permit). The specifications must be signed and sealed by a North Carolina registered Professional Engineer and shall include a narrative description of the treatment system to be constructed. Page 3 of 4 SWU-213-100101 N G51 t1000N.O.I. g) Site map identifying the location of the monitoring wells, the recovery wells„ and the treatment system unit. h) Analytical monitoring data which sufficiently characterizes the type and concentration of contaminants on site. This includes a listing of any chemicals found with the maximum observed concentrations reported. The data provided must be no older than gnq_year prior to the elate of this application. At a minimum, .the following_ parameters must be reported: Benzene, Toluene, Ethylbenzene, Xylene, Lead, Phenol, MTB , and 1,-Dichlorethane, l certify that l am familiar with the information contained in this application and that to the best of my knowledge and belief such information is true, complete, and accurate. Printed Name of Person Signing: Af I °", . Title: (Signature of Applicant) (Date .Signed) North Carolina General Statute 143-21 .6 8 () provides that: Any person who knowingly makes any false statement, representation, or certification in any application; record, report, plan or other document filed or required to be maintained under .Article 21 or regulations of the Environmental Management Commission implementing that Article, or who falsifies, tampers with or knowingly renders inaccurate any recording or monitoring device or method required to be operated or maintained under' Article 21 or regulations of the Environmental Management Commission implementing that Article, shall be guilty of a misdemeanor punishable by a fine not to .exceed $10,000, or by imprisonment not to exceed six months, or by both. (18 U.S.G. Section 1001 provides a punishment by a fine of not more than $10,000 or imprisonment not more than 5 years, or both, for a similar offense.) Notice of Intent must be accompanied by a check or money order for $80.00 made payable to: NCDENR Mail three (3) copies of the entire package to: Stormwater and General Permits Unit Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-117 Final Checklist This application will be returned as incomplete unless all of the following items have been included: o Check for $80.00 made payable to NCDPlklR D 3 copies of county map or USGS quad sheet with "location of facility clearly marked on map c7 3 copies of this completed application and all supporting documents o 3 sets of plans and specifications signed and sealed by a North Carolina P.E. (if new or modified permit) o Thorough responses to items 1-11 on this application 0 Alternatives analysis including present value of casts for all alternatives Note: The submission of this document does not guarantee the issuance of an NPD S permit. Page 4 of SWU-13-100101 E INFLUENT, BETWEEN STAGE AND EFFLUENT SAMPLE PORTS HOSE AND CONNECTIONS QUAD BAG FILTER # CONTROL (25 GPM EACH) PANE€. GAC VESSEL GAIN VESSEL (2,000 LB) (2,000 LB) , OIL STORAGE (A NEEDED) FLOW METER WITH FLOAT BOOST tlul PUMP SETTLING TANK TO STORM SEWER OIL/WATER SEPARATOR OIL/WATER SEPARATOR INCLUDED IN "TREATMENT SYSTEM AND AVAILABLE IF PETROLEUM FREE PRODUCT IS ENCOUNTERED. $ EXCAVATION PUMP to WITH FLOAT f"p Of If �A Nh 77� m� REF.: DESIGN FROM ACQUA BELLA, INC. SYSTEM " TO BE PROVIDED BY ACQ A BELLA, INC. INCORPORATED WITHIN MOBILE TRAILER SETUP. SYS M LAYOUT C � THE VUE TOWER ENGINEERING & CONSUCI"fN , INC. CHARLOTTE, NORTH CAROLINA CHARLOTTE, NORTH CAROLINA PREPARE DATA CHECKS DATE NO. FIGURE BY 'i r ~ Ca` 62'73—D5—I�0 3 Page 1, of I Foster, Rob From. Schneider, Rene Sent: Wednesday, January 17, 200710:08 AM To: Anderson,; Scott J.; Foster, Rob Cc: Schmitt, Todd Subject: F1 `. Environmental Per my discussion with Dave yesterday.. / am Milt waiting on the size of the permanent treatment facilities we spoke of on Monday' MAC EC Engineering and Consulting, Inc. R ne' J. Schneider, P.E. 407.253 547 From: Gave Riley [mailto:dav cz vudorlando.eo ] Sent: Tuesday, January 16, 2007 4: 1 PM To: Schneider, Rene Cc: `Suzanna McLeod' Subject: Environmental 1 er ediation Rene, Please proceed immediately with the items'2A, 213, and 2C of the attached proposal summery for Environmental R medi tion Service for the VUE Charlotte. If you have any questions or require any further documentation please let me know. Thanks, Dave Riley Churchill Development Group, LL P 407- 54- 36 F 407-54-5339 21 t200 CHAIN-U1--`L;Ub I UUT I AtIalytit;4I Mt;44UVZ4 The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. ,PakeAnalytical of Page: Section A Section B Section C 1005619 Required Client Information: Required Project Information: Invoice Information: Company Report To,, Attention: 0 NPDES 0 GROUNDWATER 0 DRINKING WATER Addf Copy To: Company Name: A- V UST D RCRA 0 Other� e� r Jr A, Z W Address: DGA [I IL DIN [IMI, OMN QNC Ernail To: Purchase Order No.: Pace Quote Reference: OOH OSC DWI 0 OTHER Phone Fax r Project Name: Pace Project Manager. A'5 C-7 1,,;, q X, 'fP& -3"q, Filtered JYIN) Requested Due Date/TAT: 'r. Project Number: Pace Profile #: Requested Analysis: Section D Required Client Information Valid Matrix Codes M81-%X- g(?QE Q. Preservatives DRINKING WATER DW WATER WT LU WM' 0 a'0 a. Z 20 — — — — — — — SAMPLEID WASTE WATER WW PRODUCT P 0 �0 0 - LU or -AJ S 01USOLID SL OIL OE LIA i�ca COLLECTED w 5z a - go One Character per box, -Z, 0-9 (A WIPE WP AN 2 I < COMPOS17E START COMPOSITE /GRAB 1 0 0 0 X Pace Protect lid Samples JDs MUST BE UNIQUE AIR OTHER OT DATE TIME DATE TIME z U 0 0 (D 3: z (7d FF f J f5 L 6 x" T) -7 'Z SAMPLE CONDITION dditional Comments: 1.11, z z -z z -Z - --z oAtIIIiiao NAM E A ND IiIGNAii*E PRINT Name of SA �,ONATU!Rf, of S�W_Ltfi" DATE Signed (MM DO YY) F REVERSE SIDE FOR INSTRUCTIONS At I On9nrrov.'3 31 maro-5 Pace Analytical Services, inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 2225 Riverside Drive Nuntersville, NC-28078 Asheville, NC 28804 f Phone: 704.875.9092 Phone: 828. 4.7176 t Fax` 704.875.9091 Fax:828.2 2.4618 www.pacelabs.com January''30, 2007 1- Mr. Rob Foster � Mactec_ 2801 Yorkmont Road Suite 100 Charlotte, NC 28208 RE: Lab Project Number: 92136484 Client Project ID: The Vue 6373.05.0002 Dear Mr. Foster: Enclosed are the analytical results for sample(s) ;received by the laboratory on January 22, 2007. Results reported herein conform to the most current NELAC standards, where applicable, unlessotherwise narrated in the body of the report. Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic testing was performed at our Pace Charlotte laboratory unless otherwise footnoted. If you have any questions concerning this report please feel free to contact me. Sincerely, Ci 41 Z. 4L . . Annette Scott annette.scott@pacelabs.cam (704) 875-9092 ext. 233 Project Manager Enclosures Asheville Certification IDs REPORT OF LABORATORY ANALYSISCharlotte Certification lDs NO Wastewater 40 NO Wastewater 12 NO Drinking Water 37712 .This report shall not be reproduced except in full, NO Drinking Water 37706 without the written consent of Pace Analytical Services, Inc.SC 99030 SC 900 FL NELAP E87648c`°R°�� OM FL NELAP E7627 Mace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 2225 Riverside give " Hunters viile, NC 28078 Asheville, NC 28804 J Phone. 7+ 4.87 .9092 Phone: 828. 54.7176 / Fax: 704.875.9091 Fax., 828.252.4618 www.pacelabs.com Lab Project Number: 92136484 Client Project ID: The Vue 6373.05-0002 Date Collected: 0 /21/07 11:10 Lab Sample No: 927922716 Project Sample Number: 92136484.001 Client Sample ID: B•13 Matrix: Water Rate Received: 01/22/07 12:35 Parameters Results UnitsRepont Limit DF Analyzed By CAS No. Qual Re l-mt GUMS SemivolaMes Extractables in Water by 625 Prep/Method: EPA 625 SF / EPA 625 Acenaphthene ND ug/l 5.6 1.1 01/26/07 20:54 BET 83-32.9 Acenaphthylene ND ug/l 5.6 1.1 01/26/07 20:54 BET 208-96-8 Anthracene ND ug/l 5.6 1.1 01/26/07 20:54 BET 120-12-7 Ben idine ND ug/l 56. 1.1 01/26/07 20:54 BET 92.87.5 Benzo(k)fluoranthene ND ug/l 5.6 1.1 01/26/07 20:54 BET 207-08-9 Benzo(b)fluoranthene ND ug/l 5.6 1.1 01/26/07 20:54 BET 205.99--2 Benzo(a)anthracene ND ug/l 5.6 1.1 01/26/07 20:54 BET 56-55.3 Beno(g,h,i)perylene ND ug/l 5.6 1.1 01/26/07 20:54 BET 191-24-2 Benzo(a)pyrene ND ug/l 5.6 1.1 01/26/07 20:54 BET 50-32-8 4•Bromophenylphenyl ether ND ug/l 5.6 1.1 01/26/07 20:54 BET 101-55-3 Butylbenzylphthalate ND ug/l 5.6 1.1 01/26/07 20:54 BET 85.68.7 4-Chloro-3-methylphenol ND ug/l 5.6 1.1 01/26/07 20:54 BET 59-50.7 bis(2-Chloroethoxy)methane ND ug/l 5.6 1.1 01/26/07 20:54 BET 111.91--1 bis(2-Chloroethyl) ether ND ug/l 5.6 1.1 01/26/07 20:54 BET 111-44-4 bis(2-Chloroisoprnpyl) ether ND ug/l 5.6 1.1 01/26/07 20:54 BET 39638.32-9 2-Chloronaphthalene ND ug/l 5.6 1.1 01/26/07 20:54 BET 91-58-7 2-Chlorophenol ND ug/1- 5.6 1.1 01/26/07 20:54 BET 95.57.8 4-C lorophenylphenyl ether ND ug/l 5.6 1.1 01/26/07 20:54 BET 7005-72.3 Chrysene ND ug/l 5.6 1.1 01/26/07 20:54 BET 218-01-9 Dib nz(a,h)anthracene ND ug/l 5.6 1.1 01/26/07 20:54 BET 53-70-3 1,2-Dichlorobenzene ND ug/1- 5.6 1.1 01/26/07 20:54 BET 95-50-1 1.3-Dichlorobenzene ND ug/l 5.6 1.1 01/26/07 20:54 BET 541-73-1 1,4-Dichlorobenzene ND ug/1 5.6 1.1 01/26/07 20:54 BET 106.46-7 3,3°-Dichlorobenzidine ND ug/l 11. 1.1 01/26/07 20:54 BET 91-94-1 2,4-Dichlorophenol ND ug/l 5.6 1.1 01/26/07 20:54 BET '120-83- Diethylphthalate ND ug/l 5.6 1.1 01/26/07 20:54 BET 84.66.2 2,4-Dimethylphenol ND ug/l 5.6 1.1 01/26/07 20:54 BET 105-67.9 Dimethylphthalate ND ug/l 5.6 1.1 01/26/07 20:54 BET 131-11.3 Di-n-butylphthalate ND ug/l' 5.6 1.1 01/26/07 20:54 BET 84-74.2 4.6-Dinitrc-2-methylphenol ND ug/l 28. 1.1 01/26/07 20:54 BET 534.52-1 2,4-Dinitrophenol ND ug/l 28. 1.1 01/26/07 20:54 BET 51-28-5 2,4-Dinitrotoluene ND ug/l 5.6 1.1 01/26/07 20:54 BET 121-14-2 2,6-Dinitrotoluene ND ug/l 5.6 1.1 01/26/07 20:54 BET 606-20 2 Di-n-octylphthalate ND ug/l 5.6 1.1 01/26/07 20:54 BET 117-84-0 bis(2-Ethyl'hexyl)phthalate ND ug/l 5.6 1.1 01/26/07 20:54 BET 117.81-7 Fluoranthene ND ug/l 5.6 1 1 01/26/07 20:54 BET 206-44-0 Fluorene ND ug/1 5.6 1.1 01/26/07 20:54 BET 86-73-7 Date: 01/30/07 Page: 1 of 29 Asheville Certification IN REPORT OF LABORATORY ANALYSIS Charlotte Certification IDs PAC Wastewater 40 NC Wastewater 12 NC Drinking Water 37712 This report shall not be reproduced, except in full, NC Drinking Water 7706 SC 99D30 without the written consent of Pace Analytical Services, Inc. SC 9006 , FL NELAP E87648 E°'ry Ac°� G F FL NELAP E87627 Pace Analytical Services, Inc. Pace Analytical Services, Inc. - 9800 Klncey Avenue, Suite 100 2225 Riverside Drive' Huntersville, NC 28078 ' Asheville, N9 28804 A / 1 0 Phone: 704.875,9092 Phone.' 828.2 4.7176 ace f l ( / Fax: 704,875.9091 Fax., 828,2 2.4618 www.pacelabs.com Lab Project Number: 92136484 Client Project ID: The Vue 6373-05-0002 Lab Sample No: 927922716 Project Sample Number: 92136484-001 Date Collected: 01/21/07 11:10 Client Sample ID: B-13 Matrix: Water Date Received: 01/22/07 12:35 Parameters Results Units Report Limit DF = Anal.vzed By CAS No. Qual RegLmt Hexachloro-1,3-butadiene ND ug/l 5.6 1.1 01/26/07 20:54 BET 87-68-3 Hexachlorobenzene ND ug/l 5.6 1.1 01/26/07 20:54 BET 118-74-1 Hexachlorocyclopentadiene ND ug/l 11. 1.1 01/26/07 20:54 BET 77-47-4 Hexachloroethane ND ug/l 5.6 1.1 01/26107 20:54 BET 67.72-1 Indeno(1,2 3•cd)pyrene ND ug/l 5.6 1.1 01/26/07 20:54 BET 193.39.5 Isophorone ND ug/1 5.6 1.1 01/26/07 20:54 BET 78-59-1 Naphthalene 49. ug/1 5.6 1.1 01/26/07 20:54 BET 91-20-3 Nitrobenzene ND ug/l 5.6 1,1 01/26/07 20:54 BET 98.95.3 2-Ntrophenol ND ug/l 5.6 1.1 01/26/07 20:54 BET 88-75-5 4-N trophenol ND ug/1 28. 1.1 01/26/07 20:54 BET 100-02-7 N-Nitrosodimethylamine ND ug/1 5.6 1.1 01/26/07 20:54 BET 62-75.9 N-Nitroso-di-n-prpylamire ND ug/l 5.6 1.1 01/26/07 20:54 BET "621.64-7 N-Nitrosodiphenylamine ND ug/1 5.6 1.1 01/26/07 20:54 BET 86.30.6 Pentachlorophenol ND ug/l 28. 1.1 01/26/07 20:54 BET 87-86-5 Phenanthrene ND ug/l 5.6 1,1 01/26/07 20:54 BET 85.01-8 Phenol ND ug/l 5.6 1.1 01/26/07 20:54 BET 108-95-2 Pyrene ND ug/l 5,6 1.1 01/26/07 20:54 BET 129-00-0 1,2,4-Trio lorobenzene ND ug/1 5.6 1.1 01/26/07 20:54 BET 120-82-1 2,46•Trichlorophenol ND ug/1 5.6 1.1 01/26/07 20:54 BET 88-06-2 Nitrobenzene-d5 (S) 79 t 1.0 01/26/07 20:54 BET 4165-60-0 2-Fluorobiphenyl (S) 58 X 1.0 01/26/07 20:54 BET 321-60-8 Terphenyl-d14 (S) 86 1.0 01/26/07 20:54 BET 1718-51-0 Phenol-d5 (S) 12 X 1.0 01/26/07 20:54 BET 4165-62-2 2-Fluorophenol (S) 22 % 1.0 01/26/07 20:54 BET 67-12.4 2.4 6-Tribromophenol (S) 82. t 1.0 01/26/07 20:54 BET 118.79.6 Date Extracted 01/23/07 16:21 01/23/07 16:21 GC Vlatil'es Halogen. & Aromatic Vol. Orgs. Method: EPA 601/602 Benzene ND ug/l 20. 20.0 01/27/07 03:03 PPM 71-43- Bromodichloromethane ND ug/l 20. 20.0 01/27/07 03:03 PPM 75-27-4 Bromoform ND ug/l 20. 20.0 01/27/07 03:03 PPM 75-25.2 Bromomethane ND u/1 20. 20.0 01/27/07 03:03 PPM 74-83-9 Carbon tetrachloride ND ug/l 20. 20.0 01/27/07 03:03 PPM 56-23-5 Chlorobenzene ND ug/l 20. 20.0 01/27/07 03:03 PPM "108.90-7 Chloroethane ND ug/1 20. 20:O 01/27/07 03:03 PPM 75-00-3 Chloroform ND ug/l 20. 20.0 01/27/07 03:03 PPM 67.66-3 Chlorometh ne ND ug/1 40. 20:O 01/27/07 03:03 PPM 74-87-3 Dibromochloromethane ND ug/l 20, 20.0 01/27/07 03:03 PPM 124.48.1 Date: 01/30/07 Page: 2 of 29 Asheville Certification IDS ` "�' Charlotte Certification IDs NC Wastewater 40 NC Wastewater 12 NC Drinking Water 377t s report sal This thl not breproduced,t ifull, e except NC Drinking Water 37706 SC 9903(1 out t th with written wren f consent oPace Analytical Cervices, Inc. - .. Sc 99006 FL NELAP E87648 ° ,`" h�G°Rbq� FL NELAP E87627 wa , Pace Analytical Services, laic. Pace Analytical Services, Inc. 9800 K'incey Avenue, Suite 100 2225 Riverside Drive Huntersville, NC 28078 Asheville, NC 28804 Phone.704.875.9092 Phone:828.254.7176 aceAn/ aJ l Pax: 704. 75.9091 Pax: 828.2 2.4618 www.pacelabs.com Lab Project Number: 92136484 Client Project ID: The Vue 6373-05.0002 Lab Sample No: 927922716 Project Sample Number: 92136484.001 Date Collected: 01/21/07 11:10 Client Sample ID: B-13 Matrix: Water Date Received: 01/22/07 12:35 Parameters Results Units Report Limit DF Analyzed BY CAS No. Qual Re Lmt 1,2-Dichlorobenzene ND ug/l 20. 20.0 01/27/07 03:03 PPM 95-50-1 1,3-Dichlorobenzene ND ug/l 20. 20.0 01/27/07 03:03 PPM 541-73.1 1,4-Dichlorobenzene ND ug/l 20. 20.0 01/27/07 03:03 PPM '106-46-7 Dichlorodifluoromthane ND ug/l 20. 20,0 01/27/07 03:03 PPM 75-71-8 1,1-Dichloroethane ND ug/l 20; 20.O 01/27/07 03:03 PPM 75.34-3 1,2-Dichloroethane ND- ug/l 20, 20.0 01/27/07 03:03 PPM '107-06-2 1,1-Dichloroethane ND ug/1 20. 20.0 01/27/07 03:03 PPM 75.35-4 trans-1,2-Dichloroethane ND ug/1 20. 20.0 01/27/07 03:03 PPM 156.60-5 1,2-Dichloropropane ND ug/l 20. 20.001/27/07 03:03 PPM 78.87-5 cis-1.3-Dichloropropene ND ug/l 20. 20.0 01/27/07 03:03 PPM '10061-01.5 , trans-1,3-Dichloropropene ND ug/1 20. 20.0 01/27/07 03:03 PPM 10061-02-6 Diisopropyl ether 75. ug/1 20. 20.0 01/27/07 03:03 PPM "108.20-3 Ethylbenzene 230' ug/1 20. 20.0 01/27/07 03:03 PPM 100.41-4 Methylene chloride ND ug/1 40. 20.0 01/27/07 03:03 PPM 75-09-2 Methyl•tert-butyl ether: ND ug/l 20. 20.0 01/27/07 03:03 PPM 1634.04.4 1,1,2,2-Tetrachloroethane ND ug/l 20. 20.0 01/27/07 03:03 PPM 79-34-5 Tetrachloroethene ND ug/l 20. 20.0 01/27/07 03:03 PPM 127-18-4 Toluene 56 ug/l 20, 20.0 01/27/07 03:03 PPM 108-88-3 1,1',1-Trichloroethane ND ug/l 20, 20.0'01/27/07 03:03 PPM 71-55-6 1,1 2-Trichloroethane ND ug/l 20. 20.0 01/27/07 03:03 PPM 79.00-5 Trichloroethene ND ug/1 20. 20.0 01/27/07 03:03 PPM 79-01-6 Trichlorofluoromethane ND ug/1 20. 20.0'01/27/07 03:03 PPM 75-69-4 Vinyl chloride ND ug/1 20. 20,0 01/27/07 03:03 PPM 75-01.4 m&p-Xylene 780 ug/l 40. 20.0 01/27/07 03:3 PPM o-Xylene 250 ug/l 20. 20.0 01/27/07 03:03 PPM 95.47-6 1-Chloro-3-fluorobenzene CS3 103 % 1.0 01/27/07 03:03 PPM 625-98-9 Date: 01/30107 Page: 3 of'29 Asheville Certification INREPORT OF LABORATORY ANALYSISCharlotte Certification IN C Wastewater 40 NC Wastewater 12 NC Drinking Water 3771 This report shall not be reproduced, except in full, NC Drinking Water 37706 Sc 99030 without the written consent of Pace Analytical Services, Inca Sc 99006 FL NELAP E87648 " a�G°R fi FL NELAP E87627 nor t / aceAnalytical www.pacelabs.com Pace 9800 Analytical Services, Inc. Pace Analytical Services, Inc. Kincey Avenue, Suite 100 2225 Riverside Drive Huntersville, N" 28078 Asheville, NC 28804 Phone: 704,875.9092 Phone: 828,254.7176 Fax: 704.875.9091 Fax., 828.2 2,4618 Lab Project Number: 92136484 Client Project ID: The vue 6373-05-0002 Lab Sample No: 92792724 Project Sample Number: 92136484-002 Date Collected: 01/21/07 11:20 Client Sample ID: B-19 Matrix: Water Date Received: 01/22/07 12:35 Parameters Results Units atR2L1Limit DF Analyzed" CAS No. Qual RegLmt GUMS Semivolatiles Extractables in Water by 625 Prep/Method: EPA 625 SF / EPA 625 Acenaphthene ND ug/l 5.4 1.1 01/26/07 21:18 BET 83.32.9 Aceaphthylene ND ug/l 5.4 1.1 01/26/07 21:18 BET 208.96=8 Anthracene ND ugtl 5.4 1.1 01/26/07 21:18 BET 120-12-7 Benzidine - ND ug/l 54. 1.1 01/26/07 21:18 BET 92.87.5 Benzo(k)fluoranthene ND ug/l 5.4 1.1 01/26/07 21:18 BET 207-08-9 Benzo(b)fluoranthene ND ug/l 5.4 1.1 01/26/07 21:18 BET 205.99.2 Benzo(a)anthracene ND ug/l 5.4 1.1 01/26/07 21:18 BET 56.55.3' Benzo(g,h>i)perylene ND ug/l 5.4 1.1 01/26/07 21:18 BET 191-24-2 Benzo(a)pyrene ND ug/l 5.4 1.1 01126/07 21:18 BET 50-32.8 4-Bromophenylphenyl ether ND ug/1 5.4 1.1 01/26/07 21:18 BET 101.55-3 Butylbenzylphthalate ND ug/l 5.4 1.1 01/26/07 21:18 BET 85-68.7 4-Chloro-3-methylphenol ND ug/l 5.4 1.1 01/26/07 21:18 BET '59-50.7 bis(2-Chloroethoxy)methane ND ug/1` 5.4 1.1 01/26/07 21:18 BET 111-91-1 bis(2-Chloroethyl) ether ND ug/l 5.4 1.1 01/26/07 21:18 BET 111.44-4 bis(2-Chloroisopropyl) ether ND ug/l 5.4 1.1 01/26/07 21:18 BET <39638-32.9 2-Chloronaphthalene ND" ug/l 5.4 1.1 01/26/07 21:18 BET 91-58-7 2•Chlorophenol ND ug/l 5.4 1.1 01/26/07 21:18 BET 95-57-8 4-Chlorophenylphenyl ether ND ug/l 5.4 1.1 01/26/07 21:18 BET 7005-72-3 Chrysene ND ug/l 5.4 1.1 01/26/07 21:18 BET 218-01--9 Dibenz(a,h)anthracene ND ' ug/l 5.4 1.1 01/26/07 21:18 BET 53-70-3 1,2-Dichlorobenzene ND ug/l 5.4 1.1 01/26/07 21:18 BET 95-50.1 1,3-Dichlorobenzene ND ug/l 5.4 1.1 01/26/07 21:18 BET 541-73-1 1,4-Dichlorobenzene ND ug/1 5.4 1.1 01/26/07 21:18 BET 106.46-7 3,3'-Dichlorobenzidine ND ug/l 11. 1.1 01/26/07 21:18 BET ,91-94-1- 2.4-Dichlorophenol ND ug/l 5.4 1.1 01/26/07 21:18 BET 120-83-2 Diethylphthalate ND ug/l 5.4 1.1 01/26/07 21:18 BET 84-66- 2,4-Dimethylphenol ND ug/l 5.4 1.1 01/26/07 21:18 BET 105-67-9 Dimethylphthalate- ND ug/l 5.4 1.1 01/26/07 21:18 BET 131-11-3 Di-n-butylphthalate ND ug/l 5.4 1.1 01/26/07 21:18 BET 84-74.2 4,6-Dinitro-2-methylphenol ND ug/l 27. 1.1 01/26/07 21:18 BET 534-52-1 2,4-Dinitrophenol` ND ug/l 27. 1.1 01/26/07 21:18 BET 51-28-5 2,4-Dinitrotoluene ND ug/l 5.4 1.1 01126/07 21:18 BET "121.14. 2,6-Dinitrotoluene ND ug11 5.4 1.1 01/26/07 21:18 BET ;606.20-2 Di•n-octylphthalate ND ug/l 5.4 1.1 01/26/07 21:18 BET 117.84.0 bis('2-Ethylhexyl)phthalate ND ug71 5,4 1.1 01/26/07 21:18 BET 117-81-7 Fluoranthene ND ug/l 5.4 1:1 01/26/07 21:18 BET '206-44 0 Fluorene ND ug/l 5.4 1.1 01/26/07 21:18 BET 6-73.7 Date: 01/30/07 Page: 4 of 29 Asheville Certification IDsREPORT OF LABORATORY ANALYSIS Charlotte Certification 1Ds NC Wastewater 40 NC Wastewater 12 NC Drinking Water 37712 gNC This report shall n01 be reproduced,except in full,. Drinking Water 37706 Sc 990U w�thc�ut the written consent of Pace Analytical Services, Inc. Sc 99006 FL NELAP E87643 `" aGaa"° FL NELAP E87627 Pace Analytical Services, Inc. lace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 2225 Riverside Drive Huntersville, NC 2807� Asheville, N 28804 + / 0 Phone: 704.875.909 Phone: 828. 4.7176 i✓ nal�r )q y! j Fax: 704.875.9091 Fax: 828.252,4618 www.pacelabs.com Lab Project Number: 92136484 Client Project ID: The Vue 6373-05.0002 Lab Sample No: 927922724 Project Sample Number: 92136484-002 Date Collected:;01/21/07 11:20 Client Sample ID: B-19 Matrix: Water Date Received: 01/22/07 12:3 Parameters Results Units Report Limit DF Analyzed By, CAS No. ual Re Lmt Hexachloro-1,3-butadiene ND ug/l 5.4 1.1 01/26/07 21:18 BET '87-68.3" Hexachlorobenzene ND ug/l 5.4 1.1 01/26/07 21:18 BET _ 118-74-1 Hexachloro yclopentadiene ND ug/l 11. 1.1 01/26/07 21:18 BET 77-47.4 Hexachloroethane ND ug/l 5.4 1.1 01/26/07 21:18 BET 67-72.1 Indeno(1,2 3-cd)pyrene ND ug/l 5.4 1.1 01/26/07 21:18 BET 193.39.5 Isophorone ND ug/l 5.4 1.1 01/26/07 21:18 BET 78-59.1 Naphthalene 22. ug/l 5.4 1.1 01/26/07 21:18 BET 91-20.3 Nitrobenzene ND ug/l 5.4 1.1 01/26/07 21:18 BET 98-95.3 2-N trophenol ND ug/l 5.4 1.1 01/26/07 21:18 BET 88.75.E 4-N trophenol ND ug/l 27. 1.1 01/26/07 21:18 BET 100-02-7 N•Ntrosodmethylamine ND ug/l 5.4 1.1 01/26/07 21:18 BET 62.75- N-Nitroso•di-n-propylamine ND ug/l 5.4 1.1 01/26/07 21:18 BET 621-64.7 N-Nitrosodiphenylamine ND ug/l 5.4 1.1 01/26/07 21:18 BET 86.30-6 Pentachlorophenol ND ug/1 27. 1.1 01/26/07 21:18 BET 87-86-5 Phenanthrene ND ug/l 5.4 1.1; 01/26/07 21:18 BET 85-01-8 Phenol ND ug/l 5.4 1.1 01/26/07 21:18 BET 108-95-2 Pyrene ND ug/l 5.4 1.1 01/26/07 21:18 BET 129.00-0 1,24-Trichlorobenzene ND ug/l 5.4 1.1 01/26/07 21:18 BET 120.82-1 2,4',6•Trichlorophenol ND ug/l 5.4 1.1 01/26/07 21:18 BET 88-06-2 Nitrobenzene-d5 (S) 74 1.0 01/26/07 21:18 BET 4165-60 0 2-Fluorobiphenyl (S) 49 % 1.0 01/26/07 21:18 BET 321-60-8 Terphenyl-d14 (S) 59 % 1.0 01/26/07 21:18 BET 1718-51.0 Phenol-d5 (S) 19 X 1.0 01/26/07 21:18 BET 4165-62.2 2-Fluorophenol (S) 31 % 1.0 01/26/07 21:18 BET, 367-1 -4 2,4 6-Tribromophenol (S); 74 % 1.0 01/26/07 21:18 BET 118-79-6 Date Extracted 01/23/07 16:21- 01/23/07 16: 1 C Volatile Halogen. & Aromatic Vol. Drgs. Method: EPA 601/602 Benzene ND ug/l 1.0 1.0 01/27/07 03:44 PPM 71-43-2 Bromodichloromethane ND ug/l 1.0 1.0 01/27/07 03:44 PPM 75-27.4 Bromoform ND ug/l 1.0 1.0 01/27/07 03:44 PPM 75.25-2 Bromomethane ND ug/l 1.0 1,0 01/27/07 03:44 PPM 74-83-9 Carbon tetrachloride ND ug/l 1.0 1.0 01/27/07 03:44 PPM 56-23-5 Chlorobenzene ND ug/l 1.0 1.0 01/27/07 03:44 PPM '108.90-7 Chloroethane ND ug/l 1.0 1.0 01/27/07 03:44 PPM 75.00.3 Chloroform 16: ug/l 1.0 1.0 01/27/07 03:44 PPM 67-66.3 Chloromethane ND ug/l 2.0 1.0 01/27/07 03:44 PPM 74.87. Dibromochloromethane ND ug/l 1.0 1.0 01/27/07 03:44 PPM 124-48=1 Date: 01/30/07 Page: 5 of 29 Asheville Certification IN REPORT OF LABORATORIVCharlotte Certification IN C Wastewater 40 NC DrinkingWater 37712 This report shall not be reproduced except in full, NC Wastewater 12 Sc 99030 without the written consent of Pace Analytical Services, Inc. NC Drinking Water 3770E Sc 99006 FL NELAP E87648 a o m FL NELAP E 7fi27 t`; -. Pace Analytical Services, Inc. Pace Analytical Services, Inc. 29800 Kincey Avenue, Suite 100 . 2225 Riverside Drive + / Huntersville, NC 2 078 Asheville, N 28804 t ! Phone: 704.875. 09 Phone: 8 8. 4,71 6 acel4nalvtiFax: 704, 7 .9091 Fax: 828.252.4618 ; v.pacelabs.cont Cab Project Number: 92136484 Client Project 1D: The Uue 6373-05.0002 s No- 927922724 Project Sample Number: 921 6484.002 Date Collected: 01/21/07 11:20 iple ID: B-19 Matrix. Water Date Received: 01/22/07 1 :35 Results Units Report Limit DE Analyzed By CAS No, Oual Re Cmt ilorobenzene ND ug/1 1.0 1,0 01/27/07 03:44 PPM .95-50.1 ilorobenzene ND ug/l 1.0 1.0 01/27/07 03:44 PPM 541-73-1 ilorobenzene ND ug/1 1.0 1.0 01/27/07 03:44 PPM 106-46.7 idifluoromethane ND ug/1 1.0 1.0 01/27/07 03:44 PPM 5-71- iloroethane N0 ug/1 1.0 1.0 01/27/07 03:44 PPM 75.34.3 iloroethane ND ug/i 1.0 1.0 01/27/07 03:44 PPM 107.06-2 iloroethene ND ug/1 1.0 1.0 01/27/07 03:44 PPM 75.35.4 2-Dichloroethene ND ug/1 1.0 1.0 01/27/07 03:44 PPM 1.56.60-5 iloropropane ND ug/l 1.0 1.0 01/27/07 03:44 PPM 78-87-5 Dichloropropene ND ug/l 1.0 1.0 01/27/07 03:44 PPM 10061.01-5 3-Dichloropropen ND ug/1 1.0 1.0 01/27/07 03:44 PPM 10061.02-6 pyl ether ND ug/l. 1.0 1.0 01/27/07 03:44 PPM '108-20- zene 13. ug/1 1.0 1.0 01/27107 03:44 PPM 100-41.4 e chloride 26. ug/1 2.0 1.0<01/27/07 03:44 PPM 7-09.2 ert-butyl ether ND ug/l 1.0 1.0 01/27/07 03:44 PPM 1634.04.4 Tetrachloroethane ND ug/l 1.0 1.0 01/27/07 0:44 PPM 79-34-5 orcethene ND ug/i 1.0 1.0 01/27/07 03:44 PPM 127.18-4 ND ug/l 1.0 1.0 01/ 7107 03:44 PPM 108-88.3 ichloroethane ND ug/l 1.0 1.0 01/27/07 03:44 PPM 71-55-6 ichloroethane ND ug/1 1.0 1.0 01/27/07 03:44 PPM 79.00-5 oethene ND ug/l 1.0 1.0 01/27/07 03:44 PPM 79-01-6 ofluoromethane ND ug/1 1.0 1.0 01/27/07 03:44 PPM 75-69-4 loride ND ug/l 1.0 1.0 01/27/07 03:44 PPM 75-01.4 ne 150 ug/l 10. 5.0 01/27/07 03:44 PPM 20. ug/l 1.0 1.0 01/27/07 03:44 PPM 5-47-6' -3-fluorobenzene (S) 112 t 1.0 01/27/07 03:44 PPM 625.98-9 1130/07 Page: 6 of 29 Ligation IN REPORT OF LABORATORY ANALYSIS Charlotte Gertfication ID r 40 NC Wastewater 12 later 37712 This report shall not be reproduced„ except in full, NC Chinking Water 37706 9 030 without the written consent of Page Analytical Services, Inc. Sc99006 E87648 " &"°"° FL NECAP E876 7 4 °: Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 2225 riverside Drive I J Huntersviile, NC 28078 Asheville, NC 28804 1 t� J I I I,n r 1 Phone:704,87,5.909 Phone: 828.2 4. 778 a7ce G+Gt Fax:704.875,909 fax., 828.252,4618 w.pacelabs.eom Lab Project Number: 92136484 Client Project ID: The Vue 6373-05-0002 mple No: 92792272 Project Sample Number: 9216484.003 Date Collected:'01/21/07 11:30 Sample ID: B-20 Matrix: Water Date Received: 01/22/07 1 :35 tens Results Units Raport L1m t DF AnallgEg B.v CAS No. qgL Re Lmt emi vol ati l es ctables in Water by 625 Prep/Method: EPA 625 SF / EPA 625 aphthene ND ug/1 5.5 1.1 01/26/07 21:42 BET 83.32-9 aphthylene ND ug/l 5,5 1.1 01/26/07 21:42 BET" 208.96-8 racene ND a /l 5.5 1.1 01/26/07 21:42 BET 120.1 7 idlne ND ug/l 55. 1.1 01/26/07 21:42 BET 92.87-5 o(k)fluoranthene ND ugtl 5.5 1.1 01/26/07 21:42 BET 207.08-9 o(b)fluoranthene ND ug/l 5.5 1.1 01/26/07 21:42 BET 205-99-2 o(a)anthracene ND ug11 5.5 1.1 01/26/07 21:42 BET 56.55. a(g,h,)perylene ND ug/l 5.5 1.1 01/26/07 21:42 BET 191.24-2 a(a)pyrene ND ug/1 5.5 1.1 01/26/07 21:2 BET 50-32-8 amophenylphenl ether ND ug/1 5.5 1.1 01/26/07 21:42 BET 101-55-3 ibenzylphthalate ND ug/1 5,5 1.1 01/26/07 21:42 BET 85.68.7 Toro-3•methylphenol ND ug/1 5.5 1.1 01/26/07 21:42 BET 59.50-7 ?-Chloroethoxy)methane ND ug/1 5.5 1.1 01/26/07 21:2 BET 111-91-1 ?-Chloroethyl) ether ND ug/l 5.5 1.1 01/26/07 21:2 BET 111.44- ?-Chlorolsopropyl) ether ND ug/1 5.5 1.1 01/26/07 21:42 BET :39638.32-9 loronaphthalene ND ug/l 5.5 1.1 01/26/07 21:42 BET 91-58-7 lorophenol ND ug/1 5.5 1.1 01/26/07 21:42 BET 95.57-8 lorophnylphenyl ether ND ug/l 5.5 1.1 01/26/07 21:2 BET 7005-72-3 sene ND ug/1 5.5 1.1 01/26/07 21:42 BET '218-01- iz(a,h)anthracene ND ugfl 5.5 1.1 01/26/07 21:42 BET 53-70.3, )ichlorobenzene ND ug/1 5.5 1.1 01/26/07 21:42 BET 95-50.1 )ichlorobenzene ND ug/l 5.5 1.1 01/26/07 21:42 BET 541.73-1 )ichlorobenzene ND ug/l 5.5 1.1 01/26107 21:42 BET 106.46.7 Dlchlvrobenzidlne ND ug/l 11. 1.1 01/26/07 21:42 BET 91-94-1 tichlorophenol ND ug/1 5.5 1.1 01/26/07 21:42 BET 120.83- tylphthalate ND ug/l 5.5 1.1 01/26/07 21:42 BET 84.66.2 Elmethylphenol ND ug/l 5.5 1.1 01/26/07 21:42 BET 105-67®9 hylphthalate ND ug/l 5.5 1.1 01/26/07 21:42 BET 131-11-8 butylphthalate ND' ug/l 5.5 1.1 01/6/07 21:42 BET 84-74.2 lnitro-2-methylphenol ND ug/1 27. 1.1 01/26/07 21:42 BET 34-52-1 initrdphenol ND ug/l 27. 1.1 01/26/07 21:42 BET 51-28.5% initr€toluene ND ug/1 5.5 IJ 01/26/07 21:42 BET '121-14-2 initrotoluene ND ug/1 5.5 1.1 01/26/07 21:42 BET 606-20.2 octylphthalate ND a/1 5.5 1.1 01/26/07 21:42 BET '117.84-0 -Ethylhexyl)phthala e ND ug/1 5.5 1.1 01/26/07 21:42 BET 117.81-7 anthene ND ug/l 5.5 1.1 01/26/07 21:42 BET 206-44.0 ene ND ug/1 5.5 1.1 01/26/07 21:42 BET 86.73.7 ertification IN REPORT OFANALYSIS Charlotte Certification IN rater 40 g Water This report shah not be reproduced, except' in fuli, NC Wastewater 12 99030 3N without the written consent of Pace Analytical Services, Inc, `�l i C Drinking Water 9006 Sc ��ti6 E87648 4 FL NEt /tP E87627 w� °� Pace Analytical Servic 9800 Kincey Avenue, & Nuntersville, N( Phone* 704.8acellff ¢¢ 7(i4.8 r.pacelahs.com Lab Project Client ProjE Lab Sample No: 927922732 Project Sample Number: 921'. Inc. Pace Analytical Services, Inc. 100 2225 Riverside Drive 78 ,Asheville, NC 28804 092 Phone: 828.254,7176 091 Fax. 828.2 2,4618 er 92136484 ID: The Vue 6373.05-0002 0 )le ID: B-20 Matrix: later Date Received: 01/22/07 12:35 Results Units Report Limit DF Analyzed By CAS No- ggal g2 Lmt ,o-1,3-butadiene ND ug/1 5.5 1.1 01/26/07 21:42 BET 87-68- ,obenzene ND ug/l 5.5 1.1 01/26/07 21:42 BET 118-74-1 ,oeyclopentadien ND ug/l 11. 1.1 01/26/07 21.42 BET 77-47.4 -oethane ND ug/l 5.5 1.1 01/26/07 21:42 BET 67-72.1 2,3-cd)pyrene ND ug/1 5.5 1.1 01/26/07 21:42 BET 193-39.5 )e ND ug/1 5.5 1.1 01/26/07 21:42 BET 78.59-1` Yne 200 ug/l 27. 5.5 01/26/07 21:42 BET 91.20-3 =_ene ND ug/l 5.5 1.1 01/26/07 21:42 BET 98-95-3 )enol ND ug/l 5.5 1.1 01/26/07 21:42 BET 88.75-5 )enol ND ugll 27. 1.1 01/26/07 21:42 BET 100.02µ7 )dimethylam�ne ND ug/l 5.5 1.1 01/26/07 21:42 BET -75•9 )•di-n-propylamine ND ug/l 5.5 1.1 01/26/07 1:42 BET 21-64-7 )diphenylamine ND ug/l 5.5 1.1 01/26/07 21:42 BET 86.30-6 )rophenol Nil ug/l 27. 1.1 01/26/07 21:42 BET 87.86.5 ,ene ND ug/l 5.5 1.1 01/26/07 21:42 BET 85-01-8 ND ug/1 5.5 1.1 01/26/07 21:42 BET 108-95-2 ND ug/1 5.5 1.1 01/26/07 21:42 BET 129.00-0 chlorobenzene ND ug/l 5.5 1.1 01126/07 21:42 BET 120-82.1 chlorophe of ND ug/l 5.5 1.1 01/26/07 21:42 BET 88-06-2 :ene•d5 (S) 104 z 1.0 01/26/07 21:42 BET 4165-60.0 dphenyl (S) 93 % 1.0 01/26/07 21:42 BET 321-60-8 -d 4 (S) 113 1.0 01/26/07 1:42 BET 171 -51-0 (S) 32 X 1.0 01/26/07 21:42 BET 4165-62-22 Ehenol (S) 50 X 1.0 01/26/07 21:42 BET 367.12-4 bromophenol (S) 118 t 1.0 01/26/07 21:42 BET 118-79-6 1 ,acted 01/23/07 16:21 01/23/07 16:21 it S Aromatic Vol. 4gs, Method: EPA 601/602 2100 ug/l 100 100 01/27107 04:26 PPM 71-43.2 loromethane ND ug/1 100 100 01/27/07 04:26 PPM 75.27-4 ND lag/l 100 100 01/27/07 04:26 PPM 75.25.2 ane ND ug/l 100 100 01/27/07 04:26 PPM 74-83-9 trachloride ND ug/l 100 100 01/7/07 04:26 PPM 6-23.5 " zene ND ug/l 100 100 01/27/07 04:26 PPM 108.90-7 ane ND ug/l 100 100 01/27/07 04:26 PPM 75-00-3 M ND ug/l 100 100 01/27/07 04:26 PPM 67.66-3 have ND ug/l 200 100 01/27/07 04:26 PPM 74.87.3 loromethane ND ug/l 100 100 01/27/07 04:26 PPM 124-48---1 /30/07 Page: 8 of 29 cation U)s REPORTY ANALYSISCharlotte Certification 1 s 40 iter 3771 This report shall not be reproduced, except in full, N Wastewater 12 9900 without the written consent of Pace Analytical Services, Inc. NC Drinking Water 3706 E87648 m"°� f 3C FL NELAP 99006 E87627 W F Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 lfincey Avenue, Suite 100 2225 Riverside Drive 1 Nuntersville, NC 28078 As Seville, 28804 !;aceAnalyficalo Phone: 7`04.875,9092 Phoney 828,254,7176 Fax: 704,875.9091 Fax: 828.2524618 www.pacelahs.com Lab Project Number: 92136484 Client Project ID: The Uue 637.05-0002 ample No: 927922732 Project Sample Number: 92136484-003 Date Collected: 01/21/07 11:30' Sample ID: B-20 Matrix: Water Date Received: 01/22/7 1:35 ?tern Results Units Re rt Limit DP Analyzed By CAS No, Qual Re Lmt �Dichlorobenzene NDug/l 100 100 01/27/07 04:26 PPM 95-50-1 •Dichlorobenzene ND; ug/l 100 100 01/27/07 04:26 PPM '541-73-1 Dichlorobenzene ND; ug/l 100 100 01/27/07 04:26 PPM 106-46-7 ilorodifluoromethane ND ug/1 100 100 01/27/07 04:26 PPM 75-71-8 -Dichloroethane ND ug/l 100 100 01/27/07 04:26 PPM 75-34=3 Dichloroethane ND ug/l 100 100 01/27/07 04:26 PPM 107-06-2 Dichloroethene ND" ug/l 100 100 01/27/07 04:26 PPM 75.35.4 is-1.2-Dichloroethene ND ug/l 100 100 01/27/07 04:26 PPM 156-60-5 Dichloropropane ND ug/l 100 100 01/27/07 04:6 PPM 78-87.5 1,3-Diehloropropene ND ug/1 100 100 01/27/07 04:26 PPM 10061-01.5 is-1,3-Dichloropropene ND u/l 100 100 ' 01/27/07 04:26 PPM 10061-02.6 ;opropyl ether' ND ug/l 100 100 01/27/07 04:6 PPM 108-20-3 ilbenzene 420 ug/1 100 100 01/27/07 04:26 PPM 100-41-4 iytene chloride ND ug/1 200 100 01/27/07 04:26 PPM-75-09. iyl•tert-butyl; ether ND ug/1 100 100 01/27/07 04:26 PPM 1634.04-4 2.-Tetrachloroethane ND ug/l 100 100 01/27/07 04:26 PPM 79-4- �achloroethene' ND ug/l 100 100 01/27/07 04:26 PPM 127.18.4 Gene 560 ug/1 100 100 01/27/07 04:26 PPM 108.88- 1-Trichloroethane ND ug/l 100 100 01/7/07 04:26 PPM 71-55.6 2•Trichloroethane ND ug/l 100 100 01/27/07 04:6 PPM 79-00- :hloroethene ND ug/l 100 100 01/27/07 04:26 PPM 79-01-6 :hlorofluoromethane ND ug/l 100 100 01/27/07 04:26 PPM 75.69.4 rl chloride ND ug/l 100 100 01/27/07 04:26 PPM 75-01.4 Xylene 420 ug/l 200 100 01/27/07 04:26 PPM ,len6 290 ug/l 100 100 01/27/07 04:26 PPM '95-47.6 Eloro-3•fluorobenzene (S) 103 1.0 01/27/07 04:26 PPM 625-98-9 ite: 01/30/07 Page: 9 of 29 Certification INREPORT OF LABORATORY ANALYSIS Charlotte Certification IN water 40 This report shall not be reproduced, except in fold, ' NC Wastewater 1 nU Water 00 without the written consent of Pace Analytical Services, Inc. NC inking dater 37706 9C131 `� Sc9t1(1 E87648 N AC`° ° NELAP E87627 Pace Analytical ,Services, Inc. Pace Analytical ,Services, Inc. 0800 Kincey Avenue, Suite 100 2225 Riverside Drive untersville, N 28078 Asheville, NC 28804 +a / try / Phone: 704,875.9092 Phone: 828.2, 4.71 GrG 1 Itr l Fax 704.875.9091 Fax., 828,252,4618 www.pacelabs.com Lab Project Number: 92136484 Ghent Project ID: The Uue 6373-05-0002 Lab Sample No: 927922740 Project Sample Number: 92136484-004 Gate Collected: 01/21/07 11:40 Client Sample ID: B-21 Matrix: Water Date Received: 1/22/07 12:35 Parameters Results Units Report Limit DF Analyzed By GAS No. ual Re Lmt GUMS Semivolatiles Extractables in Water by 625 Prep/Method: EPA 625 SF / EPA 625 Acenaphthene ND ug/l 5.5 1.1 01/26/07 :06 BET 83.32.9 Aceraphthylene ND ug/1 5.5 1.1 01/26/07 22:06 BET 08-96-8 Anthracene ND ug/l 5.5 1.1 01/26/07 22:06 BET 120.12-7 Benzidine ND u/1 55. 1.1 01/26/07 22:06 BET 92-87.5 Ben o(k)fluoranthene ND ug/l 5.5 1.1 01/26/07 22:06 BET 207.08-9 Benzo(b)fluoranthene ND ug/l 5.5 1.1 01/26/07 22:06 BET 05-99-2 Ben o(a)anthracene ND ug/l 5.5 1.1 01/26/07 22:06 BET 56-55.3 Be ao(g,h, )perylene ND ug/l 5.5 1.1 01/26/07 :06 BET 191.24-2 Benzo(a)pyrene ND ug/l 5.5 1.1 01/26/07 22:06 BET 50.32.8 4-Bromophenylphenyl ether ND ug/1 5.5 1,1`01/26/07 2:06 BET 101.55- Butylbenzylphthalate ND ug/1 5.5 1.1 01/26/07 2:06 BET 85.68.7 4-Chloro-3-methylphenol ND ug/l 5.5 1.1 01/26/07 22:06 BET 59-50.7 bis('2-Chloroethoxy)methane ND ug/l 5.5 1,1 01/26/07 22:06 BET 111-91-1 bis(2-Chloroethyl), ether ND ug/l 5.5 1.1 01/26/07 22:06 BET 111-44-4 bis(2-Chloroisopropyl) ether ND ug/l 5.5 1.1 01/26/07 22:06 BET 39638.32-9 -Chloronaphthalene ND ug/1 5.5 1.1 01/26/07 22:06 BET 1-58-" 2-Chlorophenol ND ug/l 5.5 1,1 01/26/07 22:06 BET 95-57.8 4•Ghlorophenylphenyl ether ND _ ug/l 5.5 1.1 01/26/07 22:06 BET 7005-72-3 Chrsene ND ug/l 5.5 1.1 01/26/07 22:06 BET 18-01-9 Dibenz(a,h)anthracene ND ug/l 5.5 1,1 01/26/07 22:06 BET 3-70- 1,2-Dichlorobenzene ND ug/l 5.5 1.1 01/26/07 22:06 BET 95-50-1 1.3-Dichlorobenzene ND ug/l 5.5 1,1 01/26/07 2:06 BET 541-73-1 1,4-Dichlorobenzene No " ug/l 5.5 1.1 01/26/07 22:06 BET 106-46-7 3,3'-Dichlorobenzidine ND ug/l 11. 1.1 01/26/07 22:06 BET 91-94.1 2,4-Dichlorophenol ND ug/1 5.5 1.1 01/26/07 22:06 BET 120.83- Diethylphthalate ND ug/1 5.5 1.1 01/26107 22:06 BET 4-66- 2,4-Dimethylphenol ND ug/l 5.5 1.1 01/26/07 22:06 BET 105.67-9 Dimethylpht alate ND ug/l 5.5 1.1 01/26/07 22:06 BET 131-11-3 Di•n-butylpthalate No ug/1 5.5 1.1 01/6/07 22:06 BET 84-74.2 4,6-Dinitro-2-methylphenol ND ug/l 27, 1.1 01/26/07 22:06 BET 34-52-1 2,4-Dinitrophenol ND ug/l 27. 1.1 01/26/07 22:06 BET 1.28. 2,4-Dinitrotoluene ND ug/1 5.5 1.1 01/26/07 22:06 BET 121-14-2 2,6-Dinitrotoluene ND ug/l 5.5 1.1 01/26/07 2:06 BET 606-20.2 Di-n-octylphthalate ND ug/l 5.5 1.1 01/26/07 22:06 BET -117-84-0 bis(-Ethylhexyl)phthalate No tag/l 5.5 1.1 01/26/07 22:06 BET 117.81-7 Fluoranthene ND ugrl 5.5 1.1 01/26/07 22:06 BET 06-44-0 Fl orene ND a /l 5.5 1:1 01/26/07 22:06 BET 6-73-7 Rate: 01/30/07 Page. 10 of 29 Asheville Certification IDs ' ° u LABORATORY ANALYSISCharlotte Certification iC) NC Wastewater 40 C Drinking Water 37712 This report shall not be reproduced, except In full, NC Wastewater 12 WaDrinkingWater Sc 9030 without the Written consent of Pace Analytical Services, Inc. NC 37706 37706 FL NELAP E87648 ti " A"°"� It SC FL NELAP E8727 - r Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 2225 Riverside Drive llunlersville, NC 28078 Asheville, NC 28804 / / � Phone: 7£14.875.9t?9 Phone: 828.54.176 1 aCt t t/i Fax.; 704,875.9091 Fax: 828.252.4618 .pacelabssem Lab Project Number: 92136484 Client Project ID The Vue 673-0-0002 Lab Sample No: 927922740 Project Sample Number: 92136484.004 Date Collected. 01/21/07 11:40 Client Sample ID: B-21 Matrix: rater Date Received: 01/22/07 1 :3 ' Parameters Results Units Report Limit DF Analyzed By CAS No. qqal Re Lmt Hexachloro-1,3•butadiene ND ug/l 5.5 1.1 01/26/07 22:06 BET 87-68.3 Hexachlorobenzene< ND ug/l 5.5 1,1 01/26/07 22:06 BET ,118.74.1 Hexachlorocyclopentadiene ND ug/l 11. 1.1'01/26/07 22:06 BET 77-47.4 Hexachlorothane ND ug/l 5.5 1.1`01/26/07 22:06 BET 67.72.1 Indeno(1,23-cd)prene ND ug/1 5.5 1.1 01/26/07 22:06 BET 193.39-5 isophorone ND ug/l 5.5 1.1 01/26/07 22:06 BET 78-59.1: Naphthalene 260 ug/l 27. 5.5 01126/07 22:06 BET "91-2 - Nitrobenzene ND ug/l 5.5 1.1 01/26/07 22:06 BET "98.95- 2-Nitrophenol ND ug/l 5.5 1.1 01/26/07 22:06 BET '88.75. 4-Ntrophenol ND ug/l 27. 1.1 01/26/07 22:06 BET 100.02.7 N-Nitrosodimethylamine ND ug/l 5.5 1.1 01/26/07 22:06 BET 62.75.9 N•Nitroso•di-n-propylamine ND ug/l 5.5 1.1 01/26/07 22:06 BET 621-64.7 N-N trosodiphenylamine ND ug/l 5.5 1.1 01/26/07 22:06 BET 86-30-6 Pentachlorophenol' ND ug/l 27, 1.1 01/26/07 22:06 BET 87-86.5 Phenanthrene ND ug/l 5.5 1.1 01/26/07 22:06 BET 85.01x Phenol ND ug/l 5,5 1.1. 01/6/07 2:06 BET 108.9-2 Pyr ne ND ug/1 5,5 1.1 01/26/07 22:06 BET 129.00-0 1,2,4-Trichlorobenzene ND ug/1 5.5 1,1 01/26/07 22:06 BET, 120-82-1 2,4,6-Trichlorophenol ND ug/l 5.5 1.1 01/26/07 22:06 BET 88-06-2 Nitrobenzene-d5 (S) 95 % 1.0 01/26/07 22:06 BET -4165-60-0 2-Fluorobiphenyl (S) 87 X 1.0 01/26/07 22:06 BET 321-60-8 Terphenyl- 14 (S) 122 % 1.0 01/26/07 22:06 BET 1718-51-0 Phenol-d5 (S) 44 1.0 01/26/07 22:06 BET 4165.62.2 2-Fluorophenol (S) 28 % 1.0 01/26/07 22:06 BET 367-1 -4 2,4'„6-Tribromophenol (S) 114 % 1.0 01/26/07 22:06 BET 118-79x6 1 Date Extracted 01/23/07 16:21 01/2 /07 16:21 GC Volatiles Halogen. & Aromatic Vol. orgs. Method: EPA 601/602 Benzene 580 ug/l 20, 20,0 01/27/07 05:08 RPM 71.43.2 Bromodichloromethane ND ug/l 20. 20.0 01/27/07 05:08 PPM 75-27.4 Bromoform ND ug/l 20. 20:0 01/27/07 05:08 PPM -75-25-2 Bromo ethane ND ug/1 20. 20,0 01/27/07 05:08 PPM 74-83. Carbon tetrachloride ND ug/l 20. 20.0 01/27/07 0508 PPM 56-23. Chlorobenzene ND ug/l 20. 20.0 01/27/07 05:08 PPM 108.90-7 Chloroethane ND ug/l 20. 20,0 01/27/07 0508 PPM 75.00-3 Chloroform ND ug/l 20. 20.0 01/27/07 05:08 RPM 67-66-3 Chloromethane ND ug/l 40. 20.0 01/27/07 05:08 PPM 74�87-3 Dibromochloromethane ND ug/l 20. 20.0 01/27/07 05:08 PPM 1 4-48-1 Date, 01/30/07 rage. 11 of 29 Asheville Certification II)a REPORT OF LABORATORY ANALYSIS Charlotte Certification ;lps NC Wastewater 40 NC Wastewater 1 NC prinking Wafter 37712 This report shall not be reproduced except in full. NC prinking Water 770 SC 99030 without the written consent of Pace Analytical Services, Inc, C 99006 FL NELI P E87648 �� ...._ , �6�.#f FL NELAP E 7627 �++ + / U i t t !/ ' tr l www.pacelabs.com Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 2225 Riverside Drive Huntersville, RUC 28078 Asheville, NC 28604 Phone-704,875,9092 Phone: 828.2 ,7176 Fax': 704.875.9091 Pax., 828.25 ,4618 Lab Project Number: 92136484 Ghent Project ID: The Vue 6373.05-0002 Lab Sample No: 927922740 Project Sample Number. 92136484-004 Date Collected: 01/21/07 11:40 Client Sample ID: B-21 Matrix: Water Date Received: 01/22/07 12:35 Parameters Results Units Report Limit DF Analyzed By CAS No. ual Re Lmt 1,2-Dichlorobenzene ND ug/l 20. 20.0 01/27/07 05:08 PPM 95-50.1 1,-Dichlorobenzene ND ug/l 20, 20.0 01/27/07 05:08 PPM 541-73-1 1.4-Dichlorobenzene ND ug/l 20. 20.0 01/27/07 05:08 PPM 106.46-7 Dichlorodifluoromethane ND ugll 20. 20.0 01/27/07 05:08 PPM 75-71-8 1,1-Dichloroethane ND ug/l; 20. 20A 01/27/07 05:08 PPM 75-34- 1.2•Dichloroethane ND ug/l 20. 20.0 01/27/07 05:08 PPM 107-06-2 I, 1•Dichloroethene ND ug/l 20. 20.0 01/27/07 05:08 PPM 75.35.4 trans-1,2-Dichloroethene; ND ug/l 20. 20.0`01/27/07 05:08 PPM 156.60.5 1,2-Dichloropropane ND ug/l 20. 20.0 01/27/07 05:08 PPM 78-87-5 cis-1,3-Diehloropropene ND ug/l 20. 20.0 01/27/07 05:08 PPM 10061-01.5 trans-1,3.Oichloropropene ND ug/l 20, 20.0 01/27/07 05:08 PPM 10061.02-6 Diisopropyl ether 45: ug/l 20. 20.0 01/7/07 05:08 PPM 108-20-3 Ethylbenzene 410 ug/l 20. 20.0 01/27/07 05:08 PPM 100-41-4 Methylene chloride ND ug/l 40. 20.0 01/27/07 05:08 PPM 75-09- Met l-ter -butyl ether ND ; ug/l 20. 20.0 01/27/07 05:08 PPM 1634-04-4 1.1 2,2-Tetrachloroethane ND ug/l 20, 20.0 01/27/07 05:08 PPM 79-34.5` Tetrachloruethene ND ug/l 20. 20.0 01/27/07 05:08 PPM 7-18.4 Toluene 48. ugll 20. 20.0 01/27/07 05:08 PPM 108-88.3 1,1',1-TricFloroethane NCI ug/l 20, 20.0 01/27/07 05:D8 PPM 71-55-6` 1,1 2-Trichloroethane ND ug/l 20. 20.0 01/27/07 05:08 PPM 79-00.5' Tri hloroethene ND ug l 20. 20.0 01/27/07 05:08 PPM 79-01.6 Trichlorofluoromethane ND ug/l 20. 20.0 01127/07 05:08 PPM 75.69.4 Vinyl chloride ND ug/l 20. 20.0 01127/07 05:08 PPM 75-01-4= mp-Xylene 340 ug/l 40. 20.0 01/27/07 05:08 PPM o-Xylene ND ugtl 20. 20.0 01127/07 05:08 PPM 9 -47.6- 1-Chloro-3-fluorobenzene (S) 105 X 1.0 01/27/07 05:08 PPM 6 5-98-9 Late: 01/30/07 Page: 12 of 29 Asheville ertlfication IN T Charlotte Certification !Cs NC Wastewater 40 NC Wastewater 12 NC Chinking Water 3771 This report shall not be reproduced, except in full;:. NC Drinking Water 7'706 Sc 99030 without the written Consent of Pace Analytical Services, Inc. Sc 99006 FL NELAP E87648 G°a FL NELAP E8727 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kncey Avenue, Suite 100 2225 Riverside Drive t ^► / Huntersvllle, NC 28078 Asheville, NC 28804 l !/ 1t✓ { Phone.- Phone: ,n Fax. 704,875.9091 Fax 828.25 .4618 www.pac,elahs.com Lab Project Number. 92136484 Client Project ID: The Vue 6373.0 -0002 PARAMETER FOOTNOTES Dilution factor shown represents the factor applied to the reported result and reporting limit due; to changes in sample preparation, dilution of the extract, or moisture content Method 9071B modified to use ASE All pH, Free Chlorine, Total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended immediate hold time. Depending on the moisture content the PRLs can be elevated for all soil samples reported on a dry weight basis. 2-Chlorpethyl vinyl ether has been shown to degrade in the presence of acid. ND Not detected at or above adjusted reporting limit NC Not Calculable J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit MDL Adjusted Method Detection Limit (S) Surrogate C11 Acid surrogate recovery outside of control limits, The data was accepted based on valid recovery of the two remaining acid surrogates. Date; 01/30107 Page: 13 or 29 Asheville Certification INREPORT OF LABORATORY ANALYSIS Charlotte Certification lDs NC Wastewater 40 This report shall not be reproduced, except in full, NC Wastewater 1 NC Chinking Water 7712 NC Drinking Water 37706 Sc 9 030 without the written consent of Pace Analytical Services, Inc. Sc 9 006 FL NELAP E87648 `��° FL NELAP E87627 n ;ry Pace Analytical Services, Inc. Face Analytical Services, Inc. 9800 Krncey Avenue, Suite 100 2225 Riverside Drive lluntersville, N 28078 Asheville, C 28804 / # ^► j Whine.704,875,9092 Phone. 8 8.2 4, 7176 t✓ t t l Fax. 704.875.9 91 Pax. 828.252,4618 www.pacelabs.com QUALITY CONTROL DATA, Lab Project Number: 92136484 Client Project ID: The Vue 6373.05.0002 ach: 178989 Analysis Method: EPA 601/602 thud: EPA 601/602 Analysis [description: Halogen. & Aromatic Vol. orgs. �.ab Samples: 927922716 927922724 927922732 927922740 <: 97938258 _ab Samples: 927922716 927922724 927922732 927922740 Blank Reporting Units Result Limit Footnotes ug/l ND 1.0 ^omethane ug/l ND 1.0 ug/l ND 1.0 ug/l ND 1.0 achloride ug/l ND 1.0 ie ug/l ND 1.0 ug/l ND 1.0 u/l ND 1.0 le ug/l ND 2.0 ,omethane ug/l ND 1.0 )benzene ugtl ND 1.0 )benzene ug/l ND 1.0 )benzene ug/l ND 1.0 Iuoromethane u/l ND 1.0 )ethane - ug/l ND 1.0 )ethane ug/l ND 1.0 )ethane ug/l ND 1.0 ihloroethene ug/l ND 1.0 )propane a /l ND 1.0 )loropropene ug/l ND 1.0 chloropropene u/l ND 1.0 ether u/l ND 1.0 ug/l ND 1.0 iloride ug/l ND 2.0 butyl ether ug/l ND 1.0 achloroethane ug/l ND 1.0 �thene ugll ND 1,0 ug/l ND 1.0 eroethane ug/l ND 1:0 oroethane ug/l ND 1.0 ene u /l ND 1,0 30/07 Page: 14 of 29 ation INREPORT OF LABORATORY ALYSI harlotte ertiflcation lDs 40 er 3771 This report shall not be reproduced, except in full, NC Wastewater 12 99030 without the written consent of Pace Analytical Services, Inc. C Drinking Water 37706 E87648 ol� `° ° Sc 99006 FL NELAP E87627 r -n r Pace Analytical Services, Inc. ' Pace Analytical Services, Inca 9800 Kincey Avenue, Suite 100 2225 Riverside Drive Hunfersville, NC 28078 Asheville, IUC 28804 t� % ^► / Phone. 704.875.9092 Phone. 828,2 4,717 �V t 1.r l Fax., 704.875,9091 Fax. 828.252,4618 www.pacelabs.com QUALITY CONTROL DATA Lab Project Number»-92136484 Client Project ID: The Uue 6373-05-0002 927938258 ab Samples: 927922716 927922724 927922732 927922740 Blank Reporting Units Result Limit Footnotes Droethne ug/1 ND 1.0 je ug/l ND 1.0 ug/l ND 2.0 ug/l ND 1.0 luorobenzene CSl X 100 3NTROL SAMPLE: 927938266 Spike LCS LCS Units Conc. Result Rec Footnotes ug/l 20.00 21.08 105' imethane ug/l 20.00 20.64 10 ug/l 20.00" 21.27 106 ug/1 20.00 17.71 8 hloride ug/l 20.00 25,34 12 a ug/l 20.00 19.80 99 ug/1 20.00 1937 99 ug/l 20.00 20.97 105 ug/l 20.00 13.84 69 )methane ug/l 20.00 20.48 10 benzene ug/1 20.00 19.50 :' 98 aenzene u/1 20.00 20.57 103 aenzene' ug/1 20.00 21.95 110 loromethane ug/1 20.00 16.09 80' =thane ug/1 20.00 21.44 107 ethane ug/1 20.00 19.09 95 :there ug/l 20.00 20.04 100 .hloroethene ug/l 20.00 20.21 101 ropane u /l 20.00 19,99 100 loropropene u /l 20.00 20.45- 102 hloropropene u/l 20.00 19.61 98 ther ug/1 20.00 19.19 96 ug/l 20.00 20.60 103 oride ug/l 20.00 24.66 12 iutyl ether ug/l 20.00 19.14 9 0t97 Paget 15 of 29 Lion IDsREPORT OF LABORATORY ANALYSIS Charlotte Certiticatlon IN 40 37712 This report shall not be reproduced, except in full„ NC Wastewater 12 r 9030 without the written consent of Pace Analytical Services, Inc. NC Drinking Water 37706 SC 99006 E87648 A �A� FL NELRP E8767 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, ,Suite 100 2225 Riverside Drive Huntersville, NC 28078 Asheville, NC 28804 % c na ! + j Phone: 704,87 :9092 Phone: 828,254,7176 t# 1 Fax. 704,875.9091 Fax: 828.252,4618 wwr : acelabs.cnnr QUALITY CONTROL DATA Lab Project Number: 92136484 Client Project ID. The Vue 6373-05-0002 LABORATORY CONTROL SAMPLE: 9279 8266 Spike LCS LCS Parameter Units Conc. Result X Rec Footnotes 1.1,2,2.Tetrachloroethane ug/l 20.00 22.00 110 Tetrachloroethene ug/l 20.00 20.29 101 Toluene a/1 20,00 20.37 102 1.1,1-Trichloroethane ugfl 20.00 2.99 120 1,1.2-Trichloroethane ug/l 20.00 24.09 120 Trichloroethne ug/l 20.00 19.58 9 Trich`iorofludromethane u/l 20.00 20.06 100 Vinyl chloride ug/l 20.00 18.41 92 m&p-Xylene u/l 40.00 39.84 100 o-Xylene ug/l 20.00 19.28 96 1-Chloro-3-fluorobenzene t l 9 MATRIX SPIKE: 927938282 927932673 Spike MS MS Parameter Units Result Conc. Result X Rec Footnotes Benzene a/1 0 20,00 21.24 106 Bromodichloromethane u /l 0 20.00 19,18 96 Bromoform u /1 0 20.00 20,08 100 Bromo ethane ug/1 0 20,00 21,16 106 Carbon tetrachloride u/l 0 20.00 23.67 118 Chlorobenzene u/l 0 20.00 19.67 98 Chloroethane' ug/1 0 20.00 23.73 11 Chloroform ug/1 0 20.00 2.66 113 Chloromethane ugil 0 20,00 19.81 99 Dibromochlorumethane ug/1 0 20.00 18.51 93 1.2•Dichlorobenzener ug/l 0 20.00 2035 104 1,3-Dichlorobenzene ug/l 0 20.00 19.73 99 1,4-Dichlorobenzene ug/l 0 20.00 20.88 104 Dichlorodifluoromethane ug/l 0 20.00 20.32 102 1,1-Dichloroethane ug/l 0 20.00 22.93 115 1.2•Dithloroethane ug/1 0 20.00 19.00 9 1.1-Dichloroethene ull 0 20.00 23.25 116 trans- ,2-Dichloroethene ug/i 0 20.00 23.22 116 1,2-Dichloropropane u /l 0 20.00 1939 99 cis-1,-Dichloropropene ug/1 0 20.00 17.46 87 Date: 01130/07 Page: 16 of 29 Asheville certification 1DsREPORT OF LABORATORY ANALYSIS Charlotte Certification IN NC Wastewater 40 NC Drinking Water 37712 This report shall not be reproduced, except in full, NC Wastewater 12 Sc 99030 without the written consent of Pace Analytical Services; lnc, NC Drinking Water 37706 FL NELAP E87648 SC 99006 FL NELAP E87627 + j F e ear, a Hr r Pace Analytical Services, Inc. Pace Analytical Services, Inc,; 800 Kincey Avenue, Suite 100 2225 Riverside strive Nuntersville, N6 28078 Asheville, N6 28804 �++ // t + l Phone: 704,875.90 Phon6:828,254,7176 t✓ t 1t✓ f Fax. 704.875. 0 1 Fax. 828.252,4618 www.pacelabs.com QUALITY CONTROL DATA Lab Project Number: 92136484 Client Project ID: The Vue 6373-05.0002 MATRIX SPIKE: 92793828 927932673 Spike MS MS Parameter Units Result Conc,; Result X Rec Footnotes trans-1,3-Diehloropropene ug/l 0 20.00 1.13 86 Diisopropyl ether ug/l 0 20.00 19.68 98 Ethylbenzene ug/l 0 20,00 20.47 10 Methylene chloride ug/l 0 20.00 26.50 132 Methyl -tent -butyl ether ug/l 0 20.00 19.60 98 1,1,2 2-Tetrachloro thane ug/l 0 20.00 22.89 114 Tetrahloroethene ug/l 0 20.00 21.53 108` Toluene ug/l 0 20.00 20.57 10 1,1,1-Trichloroethane ug/l 0 20.00 22.66 11 1,1,2-Trichloroethane ug/l 0 20.00 22.18 111 Trich oroethene ug/l 0 20,00 20,88 104 Trichlorofluoromethane ug/l 0 20,00 21.56 108 Vinyl ;chloride ug/l 0 20.00 19.74 99 m p-X lene ug/l 0 40.00 39.75 99 o-Xylene ugfl 0 20,00 19.59 98 1•Chloro-3-fluorobenzene (S) 105 SAMPLE DUPLICATE: 9798274 927918318 DUP Parameter Units Result Result RPD Footnotes Benzene ug/l ND ND NC Bromodichloromethane ug/l ND ND NC Bromo orm ug/l ND ND NC Bromo ethane ug/1 ND No NC Carbon tetrachloride ug/l ND Ng NC Chlorobenzene ug/l ND ND NC Chloroethane ug/l ND ND NC Chloroform ug/l ND ND NC Chloromethane ug11 ND ND NC Dibromochloromethan ucjll ND ND NC 1,•Dichlorobenzene; ugll ND ND NC 1.-Dichlorobenzene ugdl ND ND NC 1,4-Dichlorobenzene ugll ND ND N Dichlorodi luoromethane ug/l ND ND NC 1.1-Dichloroethane ug/1 ND ND NC Date: 01/30/07 Page: 17 of 29 Asheville Certification INREPORT OF LABORATORY ANALYSIS Charlotte Certification IN NC Wastewater 40 NC Drinking Water 37712 _ This report shall not be reproduced, except in fuel, NC Wastewater 12 Sc 99030 without the written consent of Pace Analytical Services, Inc. PVC Drinking Water 37706 Sc 99006 FL N LAP E87648 " AC FL NELAP E87627 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, ;Suite hill 2225 Riverside Drive liuntersville, NC 8078 ; Asheville, Ott* 28804 t t % Phonel 704.8 5,90 Phone: 828,2 4.71 ` Ci 1 1 Fax: 704,875.9091 Fax: 828,252,4618 www.paceiabs.com QUALITY CONTROL DATA Lab Project Number. 92136484 Client Project ID The Vue 6373.05•0002 SAMPLE DUPLICATE. 927938274 927918318 DUP Parameter Units Result Result RPD Footnotes 1,2•Dichloroethane ug/l ND ND NC 1,1-Di hloroethene u /l ND ND NC trans-1,2-Di hloroethene ug/l ND ND NC 1,2-Dichloropropane ug/l ND ND NC cis-1 3-Dichloropro ene u /l ND ND NC trans-1,3-Dichloropropene ug/1 ND ND NC Diisoropyl ether u/1 ND ND NC Ethylbenzene ug/l ND ND NC Methylene chloride ug/1 ND ND NC Methyl -tent -butyl ether ug/l ND ND NC 1,1,2 2-Tetrachloroethane ug/l ND Nil NC Tetrachloroethene ug/l ND ND NC Toluene ug/1 ND ND NC 1,1,1-Trichloroethane ug/l ND ND NC 1,1,2-Trichloroethane ug/l ND ND NC Trichloroeth ne ug/l ND ND NC Trichlorofluoromethane ug/1 ND ND NC Vinyl chloride a /l ND ND NC m&p-X,ylene ug/l ND ND NC o-Xyl ne a /l ND ND NC ; I-Chlero-3-fluorobenzene (S) 1€6 108 Elate: 01/30/07 Page: Is of 29 Asheville Certlficatirrn IDs Charlotte Certification IN NC Wastewater 40 N Drinking Water 3771 This report shall not be reproduced, except in full, NC Wastewater 12 SC 9903Q without the written consent of Pace Analytical Services, Inc. NC Drinking Water 7706 FL NELAP E87648 R`"° CC 99006 FL NELAP E8767 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9880 Kincey Avenue, Suite 100 2225 Riverside Chive hiuntersvitie, NC 28078 Asheville, tV 28804 + j + / Phone. 704.875,9 Phone.- 828. 4.71 6 tr ! t✓ ! Fax: 704,875,9091 Pax: 828,252,4618 ww.pacelabs.com QUALITY CONTROL DATA Lab Project Number.: 92136484 Client Project ID: The Vue 637-05-0002 QC Batch: 178502 Analysis Method: EPA 625 QC Batch Method. EPA 625 SF Analysis Description: Extractables in Water,by625 Associated Lab Samples. 97922716 927922724 9272732 97922740 METHOD BLANK: 927927137 Associated Lab Samples: 9279716 927922724 9279732 92792274O Blank Reporting' Parameter Units Result Limit Footnotes Acnaphthene ug/I NO 5.0 Acenaphthylere ug/l NO 5.O Anthracene ug/l ND 5.9 Benzidine a /l NO 50. Benzo(k)fluoranthene ug/l NO 5,O Benzo(b)f*luoranthene ug/l NO 5,O Benzo(a)anthracene ug/I NO 5.0 Benzo(g,h.i)perylene ug/l NO 5.O Benzo(a)pyrene ug/I NO 5.0 4-Bromophenylphenyl ether sg/I NO 5.0 Butylenylphthalate ug/l NO 5.0 4•Chlcro•3-methylphenol ug/1 NO 5.0 bis(2-Chloroetho y)methane a /l NO 5.0 bis(2-Chloro thyl) ether u /l NO 5.0 bis(2-Chloroisopropyl) ether ug/l NO 5.0 2-Chloronaphthalene ug/I NO 5.0 2-Chlorophenol ug/I NO 5.0 4-Chlorophenylphenyl ether ug/1 NO 5.0 Chrysene ug/l NO 5.0 Oibenz(a,h)anthracene ug/l NO 5.0 1.2.Oi'chlorobenzene u /1 NO 5.O 1,3•Dichlorobenzene ug/l NO 5.0 1,4.Oichlorobenzene ug/l No 5.0 3,3'-Oichlorobenzidine ug/l NO 10. 2,4-Oichlorophenol u/l ND 5.0 Oiethylphthalate Ug/1 ND 5.0 2,4-Oimethylphenol ug/l NO 5.0 Oimethylphthalate ug/1 NO 5.0 Di•n-butylphthalate ug/1 NO 5.0 4,6-Oinitro-2-methylphenol ` ug/l NO 25. 2.4-Oinitrophenol ug/l NO 25, Date: 01/30/07 Page. 19 of 29 Asheville Certification INREPORT OF LABORATORY ANALYSIS Charlotte Certification IN C Wastewater 40 NC Drinking Water 37712 This report shall not be reproduced, except in full, Wa NC Wastewater 12 Sc 9903 with0ut the written consent of Pace Analytical Services, Inc. NC Dristen Water 37706 FL NELAP E87648 ° " �`°"° ,�. wy Sc 0706 EL NELAP E87627 w � Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 2225 Riverside Drive Huntersville, NC 28078 Asheville, N 28804 / t ( Phone: 704,875,9092 Phone: 828,254,7176 1 ceAnaFax: r I 704.875.9091 Fax. 828.252.4618 www.pacelabs.com QUALITY CONTROL DATA Lab Project Number: 92136484 Client Project ID: The Vue 6373.05-0002- METHOD BLANK: 927927137 tw"s mated-,Lab,Samples.., . ,.92792g716,�,*�-- 9 792 7244 ' 279 4 279 274i? .° Blank Reporting Parameter Units Result Limit Footnotes ,4-Dinitroteluene ug/l NO 5.0 2,6-Dinitrotoluene ug/1 NO 5.0 Di-n-octylphthalate ug/1 ND 5.0 bis(2-Ethylhexyl)phthalate ug/l NO 5.0 Fluoranthene ug/l ND 5.0 Fluorene ug/l NO 5.0 Hexachloro-13-butadiene ug/1 ND 5.0 Hexachlorobenzene ug/l NO 5.0 Hexachlorocyclopentadiene ug/l NO 10. Hexachloroethane ug/1 ND 5.0 Indeno(1,2,3-cd)pyrene ug/l N0 5.0 Isophcrone ug/l NO 5.0 Naphthalene ug/1 ND 5.0 Nitrobenzene ug/l ND 5.0 2•Nitrophenol ug/l ND 5.0 4-Nitrophenol ugrl NO 25. N-Nitrosodimethylamine a /l ND 5.0 N-Nitroso-di-n-propylamine ug/l ND 5.0 N-Nitrosodiphenylamine ug/1 ND 5.0 Pentaehlorophenol ug/l NO 25. Phenanthrene ug/l ND 5.0 Phenol i ug/l NO 5.0 Pyrene ug/l ND 5.0 1,2,4•Trichlorobenzene ug/l ND 5.0 ,4,6-Trichlorophenol u /1 ND 5.0 Nitrobenzene- (S) X 72 2-Fluorobiphe yl (S) % 78 Terphenyl-d14(S) 96 Phenol-d5 (S)' z 22 2•Fluorophenol () 30 2,4,6-Tribromophenol (S) X 90 Date: 01/30/07 Page: 20 of 29 Asheville Certification IDsREPORT OF LABORATORY L. Charlotte Certification IN NC Wastewater 40 NG Drinking Water 37712 This report shall not be reproduced, except in full, NC Wastewater 1 C 99030 without the written consent of Pace Analytical Services, Inc. NC Drinking Water 37706 FL NELAP E87648 Sc 9906 FL NELAP E87627 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 lfincey Avenue, Suite 100 2225 lliversirfe Drive Huntersville, NC 28078 Asheville, NC 28804 l/ t / hone.* 704.8 5,9UJ2 Phone, 828. 4,7176 aceAnI aFax. t ! 704,875,9091 Fax., 828.252,4618 ► ww.pacelabs.com QUALITY CONTROL DATA Lab Project Number: 92136484 Client Project 11): The Vue 6373.05-0002 BORATDRY CONTROL SAMPLE: 927919845 Spike LCS LS rameter Units Conc. Result t Rec Footnotes enaphthene ug/l 50.00 42.18 84 enaphthylene ug/1 50.00 42.85 86 thracene ug/l 50,00 48.88 98 nzi ine ug/1 100.00 11,51 12 nzo(k)fluoranthene ug/l 50.00 42.28` 85 nzo(b)fluoranthene u/l 50.00 41.18 8 nzo(a)anthrwacene ' ug/l 50.00 50M 100` nzo(g,h,i)gerylene ug/l 50.00 44,45 89 nzo(a)pyrene u/1 50.00 56.96 114 Bromophenylphenyl ether ug/1 50.00 47.76 96 tylbenzylphthalate ug/l 50.00 51.2 102 Chloro-3-methylphenol u/1 50.00 39.22 78 s(2-Chloroethoxy)methane ug/1 50.00 33.47 67; s(2•Chloroethyl) ether ug/l 50.00 34.63 69 s( -Chloroisopropyl) ether a /l 50.00 34.98 70 Chloronaphthalene ug/l 50.00 38.55 77 Chlorophenol ug/l 50.00 35.34 71 Chlorophenylphenyl ether u/1 50.00 44.0 89 rysne ug/1 50.00 51.26 103 bent(a,h)anthracene ug/1 50.00 49.30 99 2-Dichlorobenzene' ug/l 50.00 31.60 63 3-D chlorobenzene ug/l 50.00 28.70 57' 4-Dichlorobenzene a /l 50.00 3032 61 a'-Dichlorobenzid ne ug/l 100.00 29.16 29 4-Dichlorophenol ug/l 50.00 38,59 77 ethylphthalate u/l 50.00 51.06 102 4-Dimethyllhenol ug/l 50.00 3335 67 tethylphth late ug/l 50.00 50,50 101 -n-butylphthalate'- ug/l 50.00 49.07 98 5-Dinitro-2•methylphenol ug/l 50.00 19.07 38 4-Dinitrophenol ug/l 50.00 1.126 2 4-Di`nitrotoluene ug/l 50.00-' 50.22 100 5-Dinitrotoluene ug/1 50.00 50.76 10 .n•octylphthalate ug/1 50.00 52.65 105 5(2•Ethylhexyl)phthalate ug/l 50.00 52.71 105 ioranthene ugll 50.00 49.31 99 jorene ug/1 50.00 44.64 89 Date: 01/30/07 Page; 21 of 29 grille Certification lCs REPORTLABORATORYA►L. Charlotte Qertification IN lastewater 40 rinking Water 3771 This report shall not be reproduced, except in full, NC Wastewater 12 99030 without the Written consent of Pace Analytical Services, Inc. NC Drinking Water 37706 Sc 99006 FLAP E8768 �v a� FL NELAP E87627 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 2225 Riverside Drive Huntersville, l C 28078 Asheville, NC 28804 �� j + Phone: 04.875, 90 Phone. 8 8. ,54, 7176 I Cr Fax. 704.875.9091 Pax. 828,252,4618 www.pacelabs.com QUALITY CONTROL DATA Lab Project Number. 92136484 Client Project ID: The Vue 6373.05-0002 LABORATORY CONTROL SAMPLE.>97919845 Spike LCS LCS Parameter Units Conc. Result t Rec Footnotes Hexachloro-1,3-butadiene ug/1 50.00 28.71 57, Hexachlorobenzene ug/l 50.00 47.82 96 Hexachlorocyclopentadiene ug/l 50.00 33.81 68 Hexachloroethae ug/1 50.00 30.22 60 Indeno(1,2,3-cd)pyrene ug/l 50.00 48.11 96 Isophorone ug/l 50.00 56.74 113 Naphthalene ug/1 50.00 29.31 59 Nitrobenzene ug/1 50.00 36.60 73 2-Nitrophenol ug/l 50.00 36.55 73' 4-Nitrophenol ug/l 50.00 6.844 14 N-Nitrosodimethylamine ug/1 50,00 9.000 18 N-Nitroso•di•n•proplamine ugll 50.00 42.25 84 N-Nitrosodiphenylamne ug/1 50.00 50.66 101 Pentachlorophenol ug/l 50.00 38.22 76' Phenanthrene ug/l 50.00 47.76 96 Phenol ug/l 50.00 14.78 30 Pyren ug/1 50.00 4.78 100 1„2,4-Trichlorobenzene ug/l 50.00 30J6 60 2.4,6-Trichlcrophenol ugtl 50.00 46.60 93 Nitrobenzene-d5 (S) 70 2-Fluorobiphenyl (S) 85 Terphnyl-d14 (S) 98 Phenol-d5 (S) 27 2-Fluorophenol (S) 39 2,4.6-Tribromophenol (S) 107 LABORATORY CONTROL SAMPLE: 927927145 Spike LCS LCS Parameter Units Conc. Result I Rec Footnotes Acenaphthene ug/l 50.00 43.14 86 Acena thylen ug/l 50.00 4331 87 Anthracene ug/l 50.00 48.57 97 Benzid ne ug/l 100.00 21.17 21 Benzo(k)fluoranthene ug/l 50.00 34.81 70 Benzo( )fiuoranthene ug/l 50.00 44.42 89 Cute: 01/30/07 Page; 22 of 29 Asheville Certification [Ds REPORT OF LABORATORYANALYSISCharlotte Certification IN NC Wastewater 40 NC Drinking Water 37712 This report shall not be reproduced, except in full, NC Wastewater 1 C 9 030 without the written Consent of =Pace Analytical Services, Inc. NC Drinking Water 37706 FL NELAP E87648 a Sc9006 FL NELAP E87627 � F Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 2225 Riverside Drive Nuntersville, N 28078 Asheville, tV 28804 / / Phone: 704.87 .9092 Phone., 828. 4,71 6 G c1 ni� 1 l=ax:704.875.9091 Fax: 828.2 2,4618 www.paceiabs.com QUALITY CONTROL DATA Lab Project Number: 92136484 Client Project ID; The Vue 6373-05-0002: LABORATORY CONTROL. SAMPLE: 927927145 Spike LCS LCS Parameter Units Conc. Result Rec Footnotes Benzo(a)anthracene ug/l 50.00 51.12 10 Benzo(g,h,i)perylene ug/l 50.00 49.74 100 Benzo(a)pyrene ug/l 50.00 54.57 109 4-Broophenylphenyl'ether ug/1 50.00 43.87 88 Butylenzylpthalat ug/l 50.00 56.86 114 4-Chlcro-3-m thylphenol ug/1' 50.00 35,73 72 bis(2-Chloroethoxy)methane, ug/l 50.00 33.27 66 bis(2-Chloro thyl) ether a /l 50.00 36.33 73 bis(2-Chloroisopropyl) ether ug/1 50.00 34.19 68 2-Chloronaphthalene ug/l 50,00 39.87 80 2-Chlurophenol ug/l 50.00 34,63 69 4•Chl rophenylphenylether a /l 50.00 44.38 89 Chrysene ug/l 50.00 49,46 99 Dibenz(a,h)anthracene u /l 50.00 51.17 102 1,2•Dichlorobenzene ug/l 50,00 31.92 64 1,3-Dichloro enzene ug/l 50.00 27.80 56 1.4-Dichlorobenzene u/l 50.00 31.60 6 3.3'-Dichlorobenzidine ug/l 100.00 30.05 30 2.4•Dichlorophenol a /l 50.00 37.79 76 Diethlphthalate ug/l 50.00 50.61 101 2.4-D methylphenol a /l 50.00 31.77 6 Dimet ylphthalate u /l 50,00 49.55 99 Di-nwutylphhalate ug/1 50.00 49.72 99 4.6-D nitro-2-methylphenol u /l 50.00 22.99 46 ,4-Dinitrophenol ug/l 50.00 7.113 14 2,4-D nitrotoluene ug/l 50.00 50.41 101 2,6-Dinitrotoluene ug/l 50.00 50.09 100 Di-n-octylphthalate ug/l 50.00 57.07 114 bis(2-Ethylhexyl)phthalate ug/l 50.00" 56.89 114 Fluoranthene ug/l 50.00 49,59 99 Fluorene ug/l 50.00 45.00 90 Hexac lord-1 3-butadiene ug/l 50,00 27.60 55 Hexachlorobenzene ug/l 50.00 47.29 95 Hexachlorocyclopentadiene ug/1 50,00' 37.63 75 Hexachloroethane ug/l 50.00 29.15 58 Indeno(1,2.3-cd)pyrene ug/1 50.00 50.41 101 Isophorone ug/l 50.00 55,25 110 Date: 01130/07 Page: 23 of 29 0sheuille Certification IN REPORT OF LABORATORYANALYSIS Charlotte Certification lus NC Wastewater 40 NC Wastewater 1 NC Drinking Water 3771 Il This report shall not be reproduced, except in full, NC Drinking Water 37706 Sc 99030 without the written consent of Pace Analytical Services, Inc. Sc 99006 FL NELAP E8748 AG FL NELAP E8767 Pace Analytical Services, Inc. Pace Analytical Services, Inc, 9800 Kincey Avenue, ,Suite 100 22.25 Riverside Chive Hunte svill , N 28078 Asheville, NC 288li4 +t t + / Phone.' 7 4.875.9092 thane: 8 8.254.7176 t✓t It ! Pax: 704.875.9091 Fax.' 828.252.4618 www.pacelabs.com QUALITY CONTROL DATA Lab Project Number: 92136484 Client Project ID: The vue 6373-05.000 LABORATORY CONTROL SAMPLE. ° 927927145 Spike LCS LCS Parameter Units Conc. Result X Rec Footnotes Naphthalene ug/l 50.00 29.66 59 Nitrobenzene ug/l 50.00 37.11 74 2-Nitrophenol ug/1= 50.00 37.28 75 4-Nitrophenol ug/l 50,00 8.727 18 N-Nitrosodimethylam ne ug/l 50.00 19.49 39 N-Nitroso-di-n-propylamine u /l 50.00 39.77 80 N-Nitrosodiphenylamine ug/l 503 00 48.30 97 Pentachlorophenol ug/l 50.00 27.56 55 Phenanthrene ug/l 50.00 46.66 93 Phenol u /l 50.00 14,72 29 Pyrene a /l 50,00 54.25 108 1, ,4-Trichlorobenzene a /l 50.00 30.47 61 ,4,6•Trichlorophenol ug/l 50.00 46.60 9 Nitrobenzene-d5 (S) 65 2•Fluorobiphenyl (S) 8 Terphenyl-d14 (S) 95 Phenol•d5 (S) 24 2•Fluorophenol (S) 3 2.4,6•Tribromophenoi (S) 9 LABORATORY CONTROL SAMPLE: 927929992 Spike LCS LCS Parameter Units Conc. Result t Rec Footnotes Acenaphthene ug/l 50.00 44.83 90 Acena hthylene ug/l 50.00 46.01 92 Anthracene ug/l 50.00 52.26 105; Benzidine ug/l 100.00 18.19 1 Benzo(k)fluoranthene ug/l 50.00 38,16 76 Benzo(b)fluoranthene ug/l 50.00 42.66 85 Benzo(a)anthracene a /l 50.00 51.55 103 Benzo(g,h,i)perylene ug/l 50,00 51.70 103, Ben of )pyren ug/l 0.00 53.68 107 4-Bromophenylphenyl ether ug/l 50,00 47.51 95 Butylb n ylphthalate ug/l 50.00 53.96 108 4-Chloro-3-methylphe of ug/l 50.00 41.50 83 Date. 01/30/07 Page. 24 of 29 A he�rille Certlflcation REPORT OF LABORATORY ANALYSIS Charlotte Certification �� C Wastewater 40 NC Chinking Water 37712 This report shall not be reproduced, except in fall; NC Wastewater 12 SC 99030 without the written consent of Pace Analytical Services, Inc. NC Chinking Water 377116 FL NELAP E8T648Cc°° �. Sc r306 FL NLAP E87627 LABt Para bis( bis( bis( Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 2225 Riverside Drive t f t f /� / Hunter ville, ABC 28078 Asheville, NC 28804 V t' 11 1 [r ! Phone: 704.87 .909 Phone: 828,2 4. 1 6 Fax., 704. 75.9091 Pax. 828,252,4618- www-pacelabs-com QUALITY CONTROL; DATA Lab Project Number: 916484 Client Project ID: The Vue 6373-05.0002 t CONTROL SAMPLE: 927929992 Spike LCS LC Units Conc. Result X Rec Footnotes )roethoxy)methane u /l 50.00 39.04 78 )roethyl) ether ug/l 50.00 45.76 92 )roisopropyl) ether u /l 50.00 43.28 87 iphthalene ug/l 50.00 42.09 84 ienol ug/l 50.00 45.67 91 ien 1pheny ether ug/l 50.00 46.48 93 u/l 50.00 49.47 99 7)anthracene u/l 50.00 51.91 104 )robenzene u/l 50.00 42.06 84 )robenzeneu/l 50.00 37.24 74 )robenzene ug/l 50.00 41.08 82' orobenzidine u /l 100.00 32,20 32 >rophenol u/l 50.00 45.27 90 ;halate ug/1 50.00 53.69 107 iylphenol a /l 50.00 37.38 75` ithalate ugtl 50.00 51.77 104 phthalate ugll 50.00 51.96 104 �o--methylphenol ug/l 50.00 35.18 70' -ophenol u /l 50,.00 14.89 30 °otoluene ugll 50.00 50.77 102 ,otoluene u/l 50.00 50.66 101 phthalate ug/l 50.00 56.17 112 ,lhexyl)phthalate ug/l 50.00 55.88 112 ,ne ug/l 50,00 52.69 105 ugll 50.00 48.04 96 .1:3.butadiene ugtl 50,00 33.72 67 benzene u/l 5000 50.85 102 cyclopentadiene ugtl 50:00 40.51 81 ethane ug/l 50:00 38.36 77 ,3-cd)pyrene ug/l 50 00 51.13 10 ugly 50.00 63.46 127 e ug/l 5000 36.58 73 ne' a /l 50:00 43.73 88 nol ug/l 50.00 43.65 87 -Nitaphenol u /l 50.00 13.81 28 -Nitrosodimethylamine ug/l 50,00 16.83 34 -Nitroso-di-n-propylamine ug/l 50:00 50.06 100 Date: 01/30/07 Asheville Certification I NC Wastewater 40 f acul of r if- 99030 8764 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of • ee Analytical Services, Inc, i Page: 25 of 25 Charlotte Certification IN NC Wastewater' 1 NC unnKing Water 37706 SC 99006 FL NELAP E87627 Pace Analytical Services, Inc. Pace Analyllcal ,services, Inc. 9800 Kincey Avenue, Suite 100 2225 Riverside Drive fluntersville, 28078 Asheville, C 28804 / �G I! ! Phone.,04.875.909 Phone. 828, 2' 4.217`8 f ' ! G G# Fax: 704.875.9091 Fax: 828,252,4618 www.pacelabs.com QUALITY CONTROL ' DATA Lab Project Number: 92136484 Client Project ID; The Vue 6373-05-0002 ATORY CONTROL SAMPLE. 927929992 Spike LCS LCS Ater Units Conic. Result X Rec Footnotes rosodiphenylamine ug/l 50.00 51.64 103 ~hlorophenol ug/I 50.00 34.34 69 7threne ug/1 50.00 49.76 100 i ug/1 50.00 14.28 29 ug/l 50.00 52.64 105 -Trichiorobenzene ug/l 50.00 37.32 75 -Trichlcrophenol ug/l 50.00 50.53 101 )enzene•d5 (S) 80' arobiphenyl (S) 86 =nyl-d14 (S) 97' i`-d5 (S)i 32' arophenol (S) 50 •Tribromophenol (S) 103- { SPIKE & MATRIX SPIKE DUPLICATE. 927919852 927919860 92790705 Spike MS MSD MS MSD =ter Units Result Cone Result Result Rec Rec RPD Footnotes hthene ugll 0 100.00 W 26 73.80 80 7 8 )hthylene ug/l 0 100.00 81.42 73.90 81 74 10 rcene ug/l 0 100.00 92.60 81.04 93 81 1 tine ug/1 0 200.00 0 0 0 0 0 1,1 :k)fluoranthene ug/l 0 100.00 87.36 93.78 87 94 7 'b)fluoranthene ug/l 0 100.00 99.90 119.5 100 120 18 a)anthracene ug/1 0 100.00 91.31 80.82 91 81 1 g,h,i)perylene ug/1 0 100.00 61.12 67.99 61 68 11 a)pyrene ug/1 0 10Q.00 111.5 127.3 112 127 13 ophenylphenyl ether ugtl 0 100.00 89.24 75.37 89 75 17 kenzylphthalate' ug/1 0 100.00 99.44 90.88 99 91 9 ro-3•methylphenol ug/l 0 100.00 81.99 89.54 82 90 9 Chloroetho y)methane ug/l 0 100.00 72.55 77.04 72 77 6 Chloroethyl) ether ug/l 0 100.00 80.41 87.36 80 87 8 hloroisopropyl) ether ug/l 0 100.00 83,64 86.92 84 87 4 ronaphthalene ugly 0 100.00 73.71 66.28 74 66 11 ropheno ug/1 0 100.00 84.99 85.21 85 85 0 rophen 1phenyl`ether ug/l 0 100,00 88,33 82.26 88 82 7 ate. 01130/07 Page; 26 of 29 Certification INREPORT OF LABORATORY ANALYSIS Charlotte Certification IDs .water 40 ing Water 37712 This report shall not be reproduced, except in full, NC Wastewater 1 99030 without the written consent of Pace Analytical Services, Inc. NC Drinking Water 37706 ' E87648 ,F Sc 99006 EL NELAP E87627 n nir" f, Pace Analytical Services, Inc. Pace Analytical Services, Inc.' 9800 Kincey Avenue, Suite 100 2225 Riverside Drive' 2aceAnalyticale Huntersville, NC 28078 Asheville, 28804 Phone: 704.875,9092 Phone: 8 8,254.71 6 Fax: 704,875.9091 Fax: 828,252,4618 www.pacelabs.com QUALITY CONTROL DATA Lab Project Number.: 92136484 Client Project ID The Vue 6373-05-0002 SPIKE K MATRIX SPIKE DUPLICATE: 927919852 927919860 927909705 Spike MS MSD MS MSD =ter Units Result Conc. Result Result X Rec X Rec RPp Footnotes me ug/l 0 100.00 96.45 81.84 96 82 16 :(a,h)arrthracene ug/1 O 100.00 71.78 81.72 72 82 13 chlorobenzene ug/l 6 100.00 79,39 77.52 79 78 2 chlorobenzene' u /l 0 100.00 69.94 67,66 70 68 3 chlorobenzene u /l 0 100,00 71,21 72,01 71 72 1 d chlorobenzidine ug/l 0 100.00 19.25 20.79 19 21 8 chlorophenol ug/l 0 100.00 85,10 91.78 85 92 8 tlphthalate ug/1 0 100,00 96.65 91.09 97 91 6 methylphenol ug/l 0 100.00 73.81 80.55 74 81 9 iylphthalate ug/l 0 100.00 94.30 89.35 94 89 5 outylphthalate u /l 0 100.00 92,54 78.92 92 79 1 nitro•2-methyl>phenol ug/1 0 100.00 65,82 57.8 66 58 1 nitrophenol ug/1 0 100.00 49,51 31.19 50 31 45 2 nitrotoluene ug/l 0 100.00 93.00 89.49 93 90 4 nitrotoluene ' ug/l 0 IOO.00 88,77 86.20 89 86 3 ictylphthalate ug/l 0 100.00 99.65 86,89 100 87 14 Ethylhexyl)phthalate ug/l 0 100.00 99.82 90,18 100 90 10 nthene ug/l 0 100.00 90.89 79.99 91 80 13 ,ne ug/l 0 100.00 WOO 83.53 88 84 5 cloro-1,3•butadiene a /l 0 100.00 66.72 66,65 67 67 0 4lorobenzene ug/1 0 100.00 88.33 81.35 88 81 8 lorocyclopentadiene ug/l 0 100.00 29.67 26.60 30 27 11 loroethane ug/l 0 100.00 68.53 66.52 68 66 3 (1,2„3-cd)pyrene ug/l 0 100.00 70.98 80.35 71 80 12 rune u /l 0 100.00 125.7 134.5' 126 134 7 aiene ug/l 0' 100.00 65.24 66.71 65 67 2 enzene u/1 0 100.00 89.02 91.12 89 91 2 ophenol: u /l 0 100.00 84.82 88.92 85 89 5 ophenol ug/l 0 100.Oo 19.41 20,64 19 21 6 ` osodimethylamine ug/1 0 100.00 9.914 8.068 10 8 21 "1 oso-di-n-propylamine ug/1 0 100,00 99.55 105.6 100 106 6 osodiphenylamine u /l 0 100.00 95.74 88.05 96 88 8 hlorophenol ug/l 0 100.00 85.35 78.30 85 78 9 threne ug/1 0 100.00 89.73 80.52 90 80 11 ug/l 0 100.00 34.80 37.35 35 37 7 ug/l 0 100.00 100.2 88.55 100 88 12 irichlorobenzene ug/1 0 100.00 68.74 68.70 69 69 0 ite: 01/30/07 Page., 27 of 29 Certificatlon IN REPORT OF LABORATOR*Irf ANALYSIS Charlotte Certification IDs water 417 37712 9 Water This report shall not he reproduced, except in full, N Wastewater 12 99030 without the written consent of Pace Analytical Services, Inc, NC Drinking Water 99006 Sc t706 E137648 A`° ° 9 wh c a EL NELAP E7627 Pace Analytical Services, Inc. Pace Analytical Services, l`nc. 9800 Alticey Avenue, ,Suite 100 2225 Riverside Drive Huntersvrlle, NC 28078 Asheville, NC 28804 + t % Phone. 704,875,9092 thane. 82 . 4.71 6 i✓ f ! 1 Fax. 7048 5.9091 Fax. 82&25 .4618 www.pacelabs.com QUALITY CONTROL DATA Lab Project Number: 92136484 Client Project I0. The Vue 6373.05-0002 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 927919852 927919860 927909705 Spike MS MSD MS MSD Parameter Units Result Conc. Result Result X Rec Rec RPD Footnotes 2,4,6-Trichlorophenol ugdl 0 100.00 96.80 92.30 97 92 5 Nitro enzene-d5 () 77 84 -Fluorobiphenyl (S) 83 84 Terpheny1-d14 (S) 98 8 Phenol-d5 (S) 32 37 -Fluorophenol (S) 44 46 ,4,6-Trlbromophenol (S) 102 101 Date: 01130l07 Page: 28 of 29 Asheville Certification IDsREPORT OF LABORATORY ANALYSIS Charlotte Certification IN NG Wastewater 40 NO Drinking Water 37712 This report shall not be reproduced, except in full, NC Wastewater 12 SO 99030 without the written consent of Pace Analytical Services, Inc. NO Drinking Water 37706 FL NELAP E87648 " A"°`° ti F u+ ac SC 99006 FL NELAP E87627 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, ,Suite 100 2225 Riverside Drive Huntersville, NC28078 Asheville, NC 28804` Phone: 704.875.9092 aceAnl Phone: 828.254.7176 / aFax: 704.875.9091 Fax.' 828,2 2.4618 w.pacelabs.co Lab Project Number: 92136484 Client Project ID: The Vue 6373-05.0002' QUALITY CONTROL DATA PARAMETER FOOTNOTES Consistent with EPA guidelines, unrounded concentrations are displayed and have been used to calculate X Rec and RPD values. LCS(D) Laboratory Control Sample (Duplicate) M(D) Matrix; Spike (Duplicate) DUP Sample Duplicate ND Not detected at or above adjusted reporting limit NC Not Calculable J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit DL Adjusted Method Detection Limit RPD Relative Percent Difference (S) Surrogate Ill The surrogate and/or spike recovery was outside acceptance limits. [21 RPD value was outside control limits, however both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness, a Date: 01/30/07 Page; 29 of 29 Asheville Certification IDsREPORT OF LABORATORY ANALYSIS Charlotte Gertification IDs NC Wastewater 40 NC Drinking Water 37712 This report shall not be reproduced, except in full; NC Wastewater 12 c 99030 without the written consent of Pace Analytical Services, Inc. NC Drinking Water 37706 4' " Ac° FL NELAP E87648 4k. Sc 99006 FL NELAP E87627