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HomeMy WebLinkAboutWQ0036723_Residual Annual Report 2020_20210119Reviewer Thornburg, Nathaniel Is this submittal an application? (Excluding additional information.) * Yes No Annual Report Year* Permit Number (IR)* Applicant/Permittee Town of Mooresville Applicant/Permittee Address PO Box 878, 369 Johnson Dairy Rd, Mooresville, NC 28115 Is the owner in BIMS? Yes No Is the facility in BIMS? Yes No Owner Type Facility Name Rocky River Wastewater Treatment Plant - Town of Mooresville County Fee Category v Fee Amount Is this a complete application?* Yes No Complete App Date I Signature Authority Signature Authority Title Signature Authority Email Document Type (if non -application) Email Notifications Does this need review by the hydrogeologist? * O Yes Q No Regional Office CO Reviewer Admin Reviewer Kendall.Williams@ncdenr.gov Below list any additional email address that need notification about a new project. Email Address Ada Comments to be added to email notfication Comments for Kendall Comments for RO Comments for Reviewer Comments for Applicant Project Contact Information Rease provide information on the person to be contacted by f DB Staff regarding electronic submittal, confirmation of receipt, and other correspondence. Name * Matthew R Herman Email Address* mherman@mooresvillenc.gov Project Information Application/Document Type * Phone Number* 7046632460 c' New (Fee Required) r Modification - Major (Fee Required) c' Renewal with Major Modification (Fee Required) r• Annual Report r Additional Information r Other Permit Type:* r Wastewater Irrigation r Other Wastewater r Closed -Loop Recycle c' Single -Family Residence Wastewater Irrigation r Modification - Minor C Renewal c' GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 r Residual Annual Report c' Change of Ownership r High -Rate Infiltration r Reclaimed Water r Residuals r Other Permit Number:* WQ0036723 Rbs Qarrent Existing permit nun-ber Applicant/Permittee * Town of Mooresville Applicant/Permittee Address* PO Box878, 369 Johnson Dairy Rd, Mooresville, NC 28115 Facility Name * Rocky River Wastewater Treatment Plant - Town of Mooresville Please provide comments/notes on your current submittal below. We had already submitted 3 hard copies to NC DWQ via USPS Priority Mail prior to receiving the email that directed us to digitally submit our annual Class A report. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form Engineering Rans, Specifications, Calculations, Eic.) 2020 Class A Report Complete (SCAN).pdf 30.5MB Wload only 1 RDF docurrent (less than 250 NB). IVLltiple docurrents rrust be combined into one RDF file unless file is larger than upload limit. * P By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature * "Mow+_611E� Submission Date 1-19-21 Is filled in autorratically once submitted. ROCKY RIVER W. W.T.P TELEPHONE (704) 662-8470 Town of Mooresville FAX (704) 662-8473 NORTH CAROLINA POST OFFICE BOX 878 MOORESVILLE, NC 28115 2020 Annual Class A Report, WQ0036723 Rocky River Wastewater Treatment Facility Mooresville, N.C. 28115 Town of Mooresville NORTH CAROLINA U.S. EPA Region 7 ATTN: BIOSOLIDS CENTER W WPD/WENF 11201 Renner Boulevard Lenexa, Kansas 66219 ROCKY RIVER W.W.T.P TELEPHONE (704) 662-8470 FAX (704) 662-8473 POST OFFICE BOX 878 MOORESVILLE, NC 28115 11 /4/20 Subject: 2020 Annual Sludge Report, WQ0036723 Distribution of Class A Residuals Following is the information requested to accompany our Class "A" Annual report. 1) Facility - Rocky River Wastewater Treatment Facility 369 Johnson Dairy RD. Mooresville, N.C. 28115 Phone: 704-663-2840 2) Responsible official and facility contact — Larry Hendren, Bio-solids Coordinator P.O. Box 878 Mooresville, NC 28115 Phone: 704-799-4063 3) Class "A" dried biosolids were distributed under Town of Mooresville permit 4 WQ0036723 4) (Part A) and (Part B) Distribution of Class "A" Residuals for 2020 were transported to, Joe Hampton (Garrin Klutz) in Mt. Ulla, NC, Doug Carrigan in Mooresville, NC, Rob Bailey in Mooresville, and Randy Boyd in Mt. Ulla, NC. Total = 898.28 dry metric tons (See Attached Hauling Summary Sheets). Laboratory data from quarterly TCLP analyses have been included in this report. During our sampling event in July we had a very strange and questionable result on our fecals. We believed this was a lab error and resampled for that parameter in August as soon as we were made aware of the discrepancy. The results from that resample were in our normal range. All sample results are included in this report for your review. 5) (Part C) I certify, under penalty of law that the above information is, to the best of my knowledge and belief, true and accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Prepared by: Larry Hendren, Bio-solids Coordinator Reviewed by: Jamie Levis WWTP Plant Manager Signature: Date Signatur . r /-/ - t'nz� Date Town of Mooresville NORTH CAROLINA NCDENR-DWQ Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699 ROCKY RIVER W, W.TT TELEPHONE (704) 662-8470 FAX (704) 662-8473 POST OFFICE BOX 878 MOORESVILLE, NC 28115 11 /4/20 Subject: 2020 Annual Sludge Report, WQ0036723 Distribution of Class A Residuals Following is the information requested to accompany our Class "A" Annual report. 1) Facility - Rocky River Wastewater Treatment Facility 369 Johnson Dairy RD. Mooresville, N.C. 28115 Phone: 704-663-2840 2) Responsible official and facility contact — Larry Hendren, Bio-solids Coordinator P.O. Box 878 Mooresville, NC 28115 Phone: 704-7994063 3) Class "A" dried biosolids were distributed under Town of Mooresville permit # WQ0036723 4) (Part A) and (Part B) Distribution of Class "A" Residuals for 2020 were transported to, Joe Hampton (Garrin Klutz) in Mt. Ulla, NC, Doug Carrigan in Mooresville, NC, Rob Bailey in Mooresville, and Randy Boyd in Mt. Ulla, NC. Total = 898.28 dry metric tons (See Attached Hauling Summary Sheets). Laboratory data from quarterly TCLP analyses have been included in this report. During our sampling event in July we had a very strange and questionable result on our fecals. We believed this was a lab error and resampled for that parameter in August as soon as we were made aware of the discrepancy. The results from that resample were in our normal range. All sample results are included in this report for your review. 5) (Past C) I certify, under penalty of law that the above information is, to the best of my knowledge and belief, true and accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Prepared by: L Hendren Bio-solids Coordinator Reviewed by: Jamie Levis, WWTP Plant Manager Signature: ,.-� - �� Date Signature- , �'- /'7— X Date Town of Mooresville 2020 Class A Hauling Summary Sheet DATE TONS TRANSPORTER DESTINATION COMMENTS 1/6/2020 27.8 Town of Mooresville AFH Sod Farm- 5 loads Mooresville 1/9/2020 20.8 Town of Mooresville AFH Sod Farm- 4 loads Mooresville 1/23/2020 26.2 Town of Mooresville AFH Sod Farm- 5 loads Mooresville 3/10/2020 33.1 Town of Mooresville Doug Carrigan 6 loads 3/11/2020 62.6 Town of Mooresville Doug Carrigan 10 loads 3/12/2020 21.3 Town of Mooresville Doug Carrigan 3 loads 3/16/2020 24.6 Town of Mooresville Doug Carrigan 4 loads 4/22/2020 12.4 Town of Mooresville Doug Carrigan 2 loads 4/29/2020 3.0 AFH Sod Farm AFH Sod Farm- 1 load Mooresville 4/30/2020 3.0 AFH Sod Farm AFH Sod Farm- 1 load Mooresville 5/4/2020 7.9 AFH Sod Farm AFH Sod Farm- 1 load Mooresville 5/5/2020 6.1 AFH Sod Farm AFH Sod Farm- 1 load Mooresville 5/6/2020 6.5 AFH Sod Farm AFH Sod Farm- 1 load Mooresville 5/7/2020 7.5 AFH Sod Farm AFH Sod Farm- 1 load Mooresville 5/11/2020 4.3 AFH Sod Farm AFH Sod Farm- 1 load Mooresville 5/12/2020 4.6 AFH Sod Farm AFH Sod Farm- 1 load Mooresville 5/13/2020 3.5 AFH Sod Farm AFH Sod Farm- 1 food Mooresville 6/15/2020 35.5 Town of Mooresville Doug Carrigan 6 loads 7/2/2020 12.1 Town of Mooresville Doug Carrigan 2 loads 7/6/2020 40.1 Town of Mooresville Doug Carrigan 6 loads 7/14/2020 29.7 Town of Mooresville Boyd Farm 4 loads 7/15/2020 7.6 Town of Mooresville Boyd Farm 1 load 7/20/2020 7.2 Town of Mooresville Boyd Farm 1 load 7/21/2020 6.9 Town of Mooresville Boyd Farm 1 load 7/21/2020 30.3 Town of Mooresville Garrin Klutz 4 loads 7/22/2020 47.1 Town of Mooresville Garrin Klutz 6 loads 7/23/2020 37.0 Town of Mooresville Garrin Klutz 5 loads 7/24/2020 14.6 Town of Mooresville Garrin Klutz 2 loads 7/28/2020 38.9 Town of Mooresville Garrin Klutz 5 loads 7/28/2020 15.0 Town of Mooresville AFH Sod Farm- Mooresville 2 loads 7/29/2020 15.5 Town of Mooresville Garrin Klutz 2 loads 7/29/2020 7.4 Town of Mooresville AFH Sod Farm- Mooresville 1 load 7/30/2020 23.7 Town of Mooresville AFH Sod Farm- Mooresville 3 loads 8/4/2020 7.4 Town of Mooresville AFH Sod Farm- Mooresville 1 load 9/4/2020 5.2 Town of Mooresville AFH Sod Farm- Mooresville 1 load 9/8/2020 25.9 Town of Mooresville Doug Carrigan 4 loads 9/9/2020 7.4 Town of Mooresville Doug Carrigan 1 load 10/1/2020 27.6 Town of Mooresville Garrin Klutz 4 loads 10/2/2020 21.8 Town of Mooresville Garrin Klutz 3 loads 10/5/2020 27.4 Town of Mooresville Garrin Klutz 4 loads 10/6/2020 38.9 Town of Mooresville Garrin Klutz 6 loads 10/7/2020 22.1 Town of Mooresville Garrin Klutz 3 loads 10/14/2020 29.1 Town of Mooresville Garrin Klutz 4 loads 10/15/2020 15.5 Town of Mooresville Garrin Klutz 2 loads 10/16/2020 7.7 Town of Mooresville Garrin Klutz 1 load 10/27/2020 36.0 Town of Mooresville Garrin Klutz 5 loads 10/30/2020 6.0 Town of Mooresville Doug Carrigan 1 load 11/3/2020 6.1 Town of Mooresville Doug Carrigan 1 load 11/4/2020 7.9 Town of Mooresville Doug Carrigan 1 load Total tons 935.90 Avg. % solids 0.96 Dry tons 898.28 Conversion factor 0.907184 Metric tons 849.0 Dry metric tons 814.9 Calculation: Dry metric tons= total tons * avg.% solids* conversion factor NC Certification No. 492 Case Narrative Waypoint. NC Drinking Water Cart No. 37735 1/28/20 16:58 ANALYTICAL SC Certification No. 99G12 Town of MODresvilleIRR WWTP Whitney Munroe P. O. Box 878 Mooresville, NC 28115 Project: Class A Dried Sludge Lab Submittal Date: 01/14/2020 Work Order: 0010195 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually an each sample. A key reference for the data qualifiers appears at the end of this case narrative. Narrative Notes: PAN Equation = 0.3 * (TKN - Ammonia) + 0.5 * (Ammonia) + Nitrate -Nitrite Equation uses Mineralization Rate (MR) for Aerobically Digested Solids (0.3) PAN = 0.3 * (38000 - 3100) + 0.5 * (3100) + 2.6 PAN = 12000 mg/kg Analysis note for SAR: SAR = [ Na ] I SQRT { ( [Ca] + [Mg] ) / 2 } SAR = [ 171/23 ] / SQRT { { [213/20] + [85.5112.2] )12 } SAR = 2,494 Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates taking the square root of the operand in parentheses. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical . 449 Springbrook Road - P.o. Box 240543 - Charlotte, NC 23224.0543 Phone_ 7041529-6364 -Toll Free Number: 1-8001529-6364 -Fax: 7041525-0409 Page 1 of 1 fi Please call if you have any questions relating to this analytical report. Respectfully, WAYPOINT ANALYTICAL Terri W. Cole Project Manager Data Qualifiers Key Reference: Reviewed By Terri W. Cole Project Manager DM Sample diluted and RL increased due to the matrix. SE Surrogate recovery outside of the QC limits due to emulsion. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 -Toll Free Number: 1.8001529-6364 -Fax: 7041525-0409 Page 2 of 16 0 Waypoint. ANALYTICAL Sample Receipt Summary 01/28/2020 Work Order: 0010195 Client Sample ID Lab Sample ID Matrix Date/Time Sampled DatelTime Received Class 0010195-01 Solid 01/14/20 8:36 01/14/20 12:05 Samples were received in good condition at 5.3 degrees C unless otherwise noted. This report should not he reproduced, except in its entirety, without the written consent of WaypoirtAnalyftaI. 449 Springbrook Road - P,O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 L Page 3 of 16 0 0 Laboratory Report Waypoint. 01/28/2020 ANALYTICAL Town of Mooresville/RR WWTP Project: Class A Dried Sludge Client Sample ID: Class A Attn: Whitney Munroe Sample ID: 0010195-01 P. O. Box 878 Work Order: 0010195 Mooresville, NC 28115 Sample Matrix: Solid Time Collected: 01/14/20 08:36 Time Submitted: 01/14/20 12:05 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Llmit Factor Date7Time ID General Chemistry Parameters Plant Available Nitrogen 6500 mglkg dry 1600 830 20 *Calculation 1128120 9:17 CLB [CALC] % Solids 95.9 % by 0.100 0.100 1 *$M2540 G 1116/20 14:09 ENV POAD228 Weight Ammonia as N 3100 mglkg dry 9.5 2.4 1 *SM4500-NH3 C 1121120 14:40 BMS POA0307 Nitrate/Nitrite as N BRL mglkg dry 6.2 1.4 1 "SM4500-NO3 F 1117120 12:03 CLB POA0258 pH 6.2 pH Units 1 *9045D 1116120 11:10 CLB POAD236 Phosphorus -Total 2600 mglkg dry 100 32 20 *SM4500-P F 1/23120 11:27 CLB POA0313 Total Kjeldahl Nitrogen 20000 mglkg dry 5200 2800 20 *351.2 1128120 9:17 CLB POA0420 Temperature 22.4 pH Units 1 *90450 1/16120 11:10 CLB POA0236 Microbiological Parameters Fetal Coltforms 2 MPNIg dry 0.2 1 *SM9221 E 1114120 12:26 BMS POA0213 TCLP Extraction by EPA 1311 TCLP Extraction Complete NIA 1 *1311 ZHE 1121/20 7:14 TBL POA0287 TCLP Extraction Complete NIA 1 *1311 1121120 8:55 EDV POA0301 TCLP Metals Mercury BRL mg1L 0.010 0.000034 1 *7470A 1/21120 18:27 JAB POAC323 Arsenic BRL mg1L 0.10 0.030 1 *6010D 1123120 12:32 JAB POA0320 Barium BRL mg1L 5.0 0.010 1 *6010D 1123/20 12:32 JAB POAD320 Cadmium BRL mglL 0.025 0.0020 1 *601OD 1123120 12:32 JAB POA0320 Chromium BRL mglL 0.25 0.015 1 *601OD 1/23120 12:32 JAB POA0320 Lead BRL mglL 0.050 0.020 1 *6010D 1/23120 12:32 JAB POA0320 Selenium BRL mg1L 015 0.063 1 *6010D 1123120 12:32 JAB POAD320 Silver BRL mg1L 0.25 0.0045 1 *6010D 1123120 12:32 JAB POAC320 TCLP Organochlorine Pesticides by GCIECD Chlordane BRL mglL 0.0025 0,00090 1 *8081B 1124/20 9:53 NMB POAD380 Dieldrin BRL mg1L 0.00050 0.000068 1 *8081B 1/24/20 9:53 NMB POA0380 Fndrin BRL mglL 0.00050 0.000068 1 *8081B 1124120 9:53 NMB POA0380 gamma-BHC BRL mglL 0.00050 0.000030 1 *8081B 1/24120 9:53 NMB POAD380 Heptachlor BRL mglL 0.00050 0.000065 1 *8081B 1124/20 9:53 NMB POAC380 Heptachlor Epoxide BRL mglL O.00050 0.00011 1 *8081B 1124/20 9:53 NMB POA0380 Melhoxychior BRL mg1L 0.00050 0,000090 1 *8081B 1124/20 9:53 NMB POA0380 Toxaphone BRL mg1L 0.025 0,0018 1 *8081B 1124120 9:53 NMB POA0380 Surrogate Decachlorobiphenyl Tetrachlo ro-m-xylene Recovery Control Limits 14 % 13-186 26 % 40-134 SE TCLP Semivolatile Organic Compounds by GC/MS 2,4,5-Trichlorophenol BRL mg1L 0.25 0.0036 1 *8270E 1123120 17:54 JMV POA0343 2,4,6-Trichlorophenol BRL mg1L 0.10 0.0D45 1 *8270E 1123/20 17:54 JMV POA0343 2,4-Dinitrotoluene HRL mg1L 0.012 0.0042 1 *8270F 1123120 17:54 JMV POAD343 This report should not be reproduced, except in its entirely, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 -Toll Free Number: 1-800I529-6364 - Fax: 7041525-0409 Page 4 of 16 Laboratory Report Waypoint, D1/28/2020 ANALYTICAL Town of Mooresville/RR WWTP Project: Class A Dried Sludge Client Sample ID: Class A Attn: Whitney Munroe Sample ID: 0010195-01 P. O. Box 878 Work Order: 0010195 Mooresville, MC 28115 Sample Matrix: Solid Time Collected: 01/14/20 08:36 Time Submitted: 01/14/20 12:05 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DatefTime ID 2-Methylphenol BRL mg/L 0.050 0.0024 1 *8270E 1123120 17:54 JMV ROAC343 314-Methylphenol BRL mg1L 0.050 0.0026 1 *8270E- V23/20 17;54 JMV POA0343 Hexachlorobenzene BRL mg1L 0.020 0.0039 1 *8270E 1/23/20 17:54 JMV POA0343 Hexachtorobutadiene BRL mg1L 0.060 0.0045 1 *8270E 1123120 17:54 JMV POA0343 Hexachlorcethane BRL mg/L 0.060 0,0037 1 *827DE 1/23120 17:54 JMV POAD343 Nitrobenzene BRL mg/L 0.060 0,0038 1 *8270E 1123120 17:54 JMV POA0343 Pentachlorophenol BRL mg/L 0.25 0,011 1 *8270E 1123120 17:64 JMV POA0343 Pyridine BRL mg/L 0.25 0,0016 1 *8270E 1123120 17:54 JMV POA0343 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 30 % 43-140 SE 2-Fluorobiphenyl 25 % 44-119 SE 2-Ruorophenot 21 % 19-119 Nitrobenzene-d5 24 % 44-120 SE Phenol-d5 14 % 11-52 Terphenyl-d14 29 % 50-134 SE TCLP Volatile Organic Compounds by GCIMS 1,1-Dichlorcethylene BRL mg/L 0.035 0.0035 10 *8260D 1/23120 22:02 JLB. POAC381 1,2-Dichloroethane BRL mg1L 0.025 0.0041 10 *8260D 1123120 22:02 JLB POA0381 1,4-Dichlorobenzene BRL mg1L 0,38 0.0042 10 *8260D 1123/20 22:02 JLB POA0381 Benzene BRL mg1L 0.025 0.0034 10 *8260D 1/23/20 22:02 JLB POA0381 Carbon Tetrachloride BRL mg1L 0.025 0,0055 10 *8260D 1/23120 22:02 JLB POA0381 Ch[orobenzene BRL mg1L 5.0 0.0034 10 *826013 1/23120 22:02 JLB POA0381 Chloroform BRL mg/L 0.30 0.0048 10 *8260D 1123/20 22:02 JLB POA0381 Methyl Ethyl Ketone (2-Butanone) BRL mglL 10 D.0078 10 *8260D 1123120 22:02 JLB POA0381 Tetrachioroethylene BRL mg/L 0.035 0.0031 10 *8260D 1/23120 22:02 JLB POA0381 Trichloroethylene BRL mg1L 0.025 0.0046 10 *8260D 1123120 22:02 JLB POAC381 Vinyl chloride BRL mg1L 0.010 0.0041 10 *8260D 1/23/20 22:02 JLB POA0361 Surrogate Recovery Control Limits 4-Bromof[uorobenzene 94 % 80-124 Dibromotluoromethane 93 % 75-129 Toluene-0 95 % 77-123 Total Metals Aluminum BRL mglkg dry 2600 570 100 *6010D 1/25/20 1:49 JAB POA0373 Mercury BRLDM mg/kg dry 0.26 0.090 5 "7471B 1/21120 10:46 JAB POA0289 SAR Soil Preparation Complete g 1 `2-78-054 1121120 14:30 EDV POAC305 SAR Percent Moisture 71.5 % by 0.100 0.100 1 *2-78-054 1122120 14:34 EDV POA0333 Weight Arsenic 2.6 mglkg dry 1.0 0.14 1 *60100 1124120 13:31 JAB POA0373 Sodium Absorption Ratio 2.5 [blank] 0.30 0.016 1 *2-78-054 1/27/20 15:29 JAB POA0332 Cadmium BRL mg/kg dry 0.52 0.035 1 *6010D 1/24120 13:31 JAB POA0373 Calcium 13000 mglkg dry 100 27 1 *6010D 1/24120 13:31 JAB POAD373 This report should not be reproduced, except in its entirety, without the written consent of WaypcintAna lytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 -Toll Free Number; 1-8001529-6364-Fax: 7041525-0409 Page 5 of 16 Waypoint- 0 ANALYTICAL Town of Mooresville/RR WWTP Attn: Whitney Munroe P. O. Box 878 Mooresville, NC 28115 Project: Class A Dried Sludge Sample Matrix: Solid Laboratory Report 01/28/2020 Client Sample ID: Class A Sample ID: 0010195-01 Work Order: 0010195 Time Collected: 01/14/20 08.36 Time Submitted: 01/14/20 12:05 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Calcium, SAR 210 mg1L 100 1.0 100 "6010D 1/27/20 15:29 JAB POA0332 Copper BRL mglkg dry 260 35 100 *6010D 1125/20 1:49 JAB POA0373 Lead 7.0 mglkg dry 1.0 0.17 1 *6010D 1124120 13:31 JAB POA0373 Magnesium 2200 mglkg dry 26 2.4 1 *6010D 1124/20 13:31 JAB POA0373 Magnesium, SAR 86 mg1L 10 0.86 100 *6010D 1127/20 15:29 JAB POA0332 Molybdenum 7.2 mglkg dry 1.0 0.13 1 *6010D 1/24120 13:31 JAB POA0373 Nickel 11 mglkgdry 1.0 0.31 1 *6010D 1/24120 13:31 JAB POA0373 Potassium 2800 mglkgdry 100 11 1 *6010D 1124120 13:31 JAB POA0373 Selenium 1.8 mglkg dry 1.0 0.29 1 *6010D 1124120 13:31 JAB POA0373 Sodium 850 mglkg dry 100 14 1 "6010D 1/24120 13:31 JAB POAC373 Sodium, SAR 170 mg1L 50 1.8 100 *6010D 1127120 15:29 JAB POA0332 Zinc BRL mg/kg dry 1000 150 100 *6010D 1125120 1:49 JAB POA0373 This report should not be reproduced, except in its entirety, without the written consent of WaypointAnalytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0543 Phone: 7041529.6364 -Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 6 of 16 Sample Extraction Data Prep Method: 351.2 Lab Number Batch Initial Final DateMme 0010195-01 POA0420 0.05 g 25 mL 01/27/20 10:25 Prep Method: SM4500-NH3 B Lab Number Batch initial Final Daterrime 0010195-01 POA0307 1.1 g 50 mL 01/21120 9:20 Prep Method: SM4500-PB5 Lab Number Batch Initial Final Date/Time 0010195-01 POA0313 1 g 50 mL 01/21/20 11:42 Prep Method: Solids, Dry Weight Lab Number Batch Initial Final DatelTime 0010195-01 POA0228 30 g 30 g 01/16/20 8:09 Prep Method: 1311 Lab Number Batch Initial Final Daterrime 0010195-01 POA0287 12.5 g 250 mL 01/20/20 13:15 0010195-01 POA0301 100 g 2000 mL 01/20/20 16:45 Prep Method: 3010A Lab Number Batch Initial Final Datelrme 0010195-01 POAC320 10 mL 50 mL 01/21/20 10:45 Prep Method: 7470A Lab Number Batch Initial Final Daterrime 0010195-01 POA0323 20 mL 30 mL 01/21/20 12:30 Prep Method: 3510C GC Lab Number Batch Initial Final Datemme 0010195-01 POA0380 200 mL 10 mL 01123/20 13:00 Prep Method: 3510C MS Lab Number Batch Initial Final Daterrime 0010195-01 POA0343 200 mL 1 mL 01/23120 9:00 Prep Method: 5030B Lab Number Batch Initial Final DatelTime 0010195-01 POA0381 10 mL 10 mL 01123/20 12:00 Prep Method: 3010A Lab Number Batch Initial Final DatelTime 0010195-01 POA0332 50 mL 50 mL 01/21/20 14:30 0010195-01 POA0332 50 mL 50 mL 01/21/20 14:30 Prep Method: 3050B Lab Number Batch Initial Final Date/Time 0010195-01 POA0373 2 g 50 mL 01/23/20 9:39 0010195-01 P0A0373 2 g 50 mL 01/23/20 9:39 This report should not be reproduced, except in its entirety, without the wrltteri consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529.6364- Fax: 7041525-0409 Page 7 of 16 Sample Extraction Data Prep Method: 7471B Lab Number Batch Initial Final Date/Time 0010195-01 POA0289 0.6 g 50 mL 01120120 11:21 Prep Method: SAR 2-78-054 Lab Number Batch Initial Final Date/Time 0010195-01 POA0305 250 g 250 g 01/20/20 14:30 Subcontracted Analyses The following analyses were subcontracted to Analytical Environmental Services, Inc. Lab Number Analysis 0010195-01 Herbicides TCLP (Sub) This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Sprin9brook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 704/529-6364 -Toll Free Number: 1.800/529-6364 - Fax: 7041525-0409 Page 8 of 16 `LkT—! q 5 -2 S,3 ,R i S MI Full -Service Analytical��`.. I Environmental Solutions � R.tMMATORIEB we 449 Springbrook Road • P.O. Box 240543 • Charlotte, NC 28224-OM Phone: 704/529-6364 a Fax:_—�704�W1525-04M A �y Client Company Name; i 6 r A 1 ' 1k Report To/Contact Name: Reporting Address; ef, 0 , J3d Phone: ` A�j6 ax (Yea) Email (Yes) (No) Empll AddressA& ► V EDD Type: PDF i/ Excel_Other_ Site Location Name: Site Location Physical Address: _ CHAIN OF CUSTODY RECORD PAGE J OF__12? QUOTE N TO ENSURE PROPER BILLING: Project Name: �S�'DR a S i4'C- Short Hold Analysis: Ye ) (No) UST Project: es) *Please ATTACH any project specific reporting (GC LEV�i I III 1V) provisions and/or OC Requirements Invoice To: i o w -- atA dmoct Address: Samples INTACT upon arrival? Received ON WET ICE? Temp PROPER PRESERVATIVES indIcated? Received WITHIN HOLDING TIMES? CUSTODY SEALS INTACT? VOLATILES rec'd WIOUT HEAOSPACE? PROPER CONTAINERS used? Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL VRequested Due Date ❑ 1 Day ❑ 2 Days p 3 Days Ll 4 Days ❑ 5 Days Certification: NELAC USACE FL NO "Working Days" q 6-9 Days tandard 10 days , Rush Work dust Be Samples received after 15:00 will be processed nexi business day. SC_ OTHER N/A Turnaround time fs based on business days, excluding weekends and holidays, Water Chlorinated: YES _ NO �— (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES RENDERED BY PRISM LABORATORIES, INC. TO CLIENTi Sample Iced Upon Collection: YES i-�N O TIME MATRIX SAMPLE CONTAINER CLIENT DATE COLLECTED (SOIL, SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR *TYPE HOURS SLUDGE) SEE BELOW I No- SIZE U"s f ' U ANALY5E8 REQUESTED ' PRESERVA• it� ah �� 1� PRISM TIVESq 4a REMARKS LAB ID NO. Xk j i ! Sampled By (Print Name) LA,', Affiliation this Chain o ustody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be i to the Prism Project Manager. There will be charges for any changes after analyses have been initialized. Date tiz0 Ltbb Additional Com ents: *�� VP 1 �St%mi bj > s gatpn gz�40 SAMPLES ARE NOT ACCEPTED AND VERIFIED-40MMST CDC UNTIL RECEIVED AT THE LABORATORt. ❑ Fed Ex ❑ UPS J Hanoi-deliverad 2! Prism Flak] Service O other v {1' 1J' J III � " TVP ES: UST: GROUNDWATER; DRINKING WATER: SOLID WASTE: RCRA: { CERCLA LANDFILL I OTHER: ❑ SCj ❑ NC ❑ SC ❑ NO ❑ SC ❑ NO ❑ SC � C ❑ SC I Cl NC ❑ SCl 0 NC ❑ SC ; ❑ NC ❑ SC ❑ NC ❑ SC *CONTAINS; ?E CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap A = Volatile Organics Analysis (Zero Head Space) She Arrival Time: Site Departure Time; Field Tech Fee: Mileage: ORIGINAL P R 1 S Environmental Analytical s Environmental Solutions ��. LABORATORIES, INC. 449 Springbrook Road • Charlotte, NC 28217 Phone 7041529.6364 + Fax: 704JS25-0489 Client Company Name: ov VL &— MDI�fP,6V1,4�. Report To/Contact Name: { Reporting Address; e 0 ,_ 0- D- Email Address: l� Ofe EDD Type: PDF Excel —Other. Site Location Name: Site Location Physical Address: CLIENT I DATE SAMPLE DESCRIPTION I COLLECTED Gass _r4 Sampler's SignaturQr'�.��� Upon relinquishing, this Chain eptustod submitted in writing to the Prism Project u V TIME COLLECTED MILITARY HOURS MATRIX (SOIL, WATER OR SLUDGE) 083` ka 1 CHAIN OF CUSTODY RECORD PAGE � OF..000TE # TO ENSURE PROPER BILLING: Project Name: SS Short Hold Analysis: (fq�A (No) UST Project: (Yes) � *Please ATTACH any project specific reporting (QC LEVF. I I III I _ provisions andfor QC- Requirements Invoice To: M t2tg u l Lk Address: LAB USE •NLY YNO NIA Samples INTACT upon amval? (0 Received ON WET ICE? _ PROPER PRESERVATIVES Indicated? _% D Received WITHIN HOLDING TIMES? ✓ CUSTODY SEALS INTACT? VOLATILES rec'd WIOUT HEADSPACE?_ PROPER CONTAIN use ed? _ 9 TEMA: TheFnc ID: ILA ObseNed- ' C I Carr,__.°C Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Requested Due Data ❑ 1 Day O 2 Days ❑ 3 Days ❑ 4 Days ❑ S Days Certification: NELAC DOD FL NC "Working Days" ❑ 6-9 Day*, andard 10 days €3 Pfeshh Work Must Be Samples received after 14:00 will be processed next business day. rov SC OTHER NIA Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO—� (btrz REVERSE RTERMS & CONDITIONSREGARDING SERVFCES RENDERED BY PRISM LABORATORIES•.CLISample Iced Upon Collection: YES 6" "NO SAMPLE CONTAINERS ANALYSIS REQUESTED PRESERVA- % �/ i% PRISM SE BELOW NO. SIZE T€VES h�y REMARKS ID NO. A= Sampled By (Print Name) .L+� «'�-� t�ty\Acle-Wl\ Affiliation 10 �1AI is your authorization for Prism to proceed with the analyses as requested above. Any changes must be anager. There will be Ggrges for any changes after analyses have been initialized. — uo rut lurymours Additional Comments: (ID c9S2) 12 e WJ R w By: (srgilaturfl Date�j atur r� Received For Prism Latsaratar3es By. pas ,141, iter NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSP RT TION TO THE LABORATORY COO Group No.' w1 r Zk 1 SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CDC UNTIL RECEIVED AT THE LABO TORY. ❑ Fed Ex ❑ UPS o Hand -delivered r rn Field Service ❑ Other 0010 1 q S 11, `1 1") "1, DRINKING SWAYER: �S0J-ICD WASTE: `❑ FILL ❑ NC ❑ SC� q NC ©SC ❑ C ❑ SCTER 0 NC I NC I 5C O❑ NC ❑ 5C ❑ NC ❑ SC I ❑ NC ❑ SC ❑ ❑ E ORCR ❑ *CONTAINF 'PE CODES: A = Arnber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Ca _ )A = Volatile Organics Analysis (Zero Head Space) SAe Arrival Time: Site Departure Time: Field Tech Fee: Mileage- JGINAL ACCESS ANALYTICAL, INC. ANALYTICAL REPORT CLIENT Waypoint Analytical PO Box 240543 Charlotte NC 282240543 ATTENTION Terri W. Cole PROJECT ID 0010195 LABORATORY REPORT NUMBER 2001F26 DATE January 22, 2020 Primary Data Review By Secondary Data Review By Ashley Amick Chris Pafford Project Manager, Access Analytical Project Manager, AES aamick(7aaxs-inc.com PLEASE NOTE: Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc), 3080 Presidential Drive, Atlanta, GA 30340. - AES is SCDHEC certified laboratory # 98016, NCDEN11 certified lab # 562, GA certified lab # FL-E87582, NELAP certified laboratory # E87i82 AIHA-LAP,LLC Laboratory 1D:100671 for Industrial llygiene samples (Organics, Metals, PCM Asbestos, Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal) Direct Examination. - Local support services lbr this project are provided by Access Analytical, Inc. Access Analytical is a representative ofAES serving client in the SC/NCIGA areas. All questions regarding this report should be directed to your local Access Analytical representative at 803.781.4243 or toll 14 at 883.315.4243 Page page 11 of 16 YYaypoint ANALYTICAL SURCONTRACT ORD R CertiF•,116(111: NE LAC USACE_ lb'aypointAnalytical y .. SC� Other 0010195 NrA SENDING LABORAI'ORY! RVC -EAVI .' L HORA'I'( Y.- Waypoint Analytical Annlyticai FnvirontnenW Servjcrs, Inc. P.O. Box240543 3080 Presidential Parkway Clsarlotte, NC 28224-0543 Atlanta, GA 30340 Phone: 800-529-6364 Phone :(770) 457-8177 Fax. 704-525-0409 } ax: NA Projcct Manager: Terri W. Cole Analysis rive EYpires Laboratory 11) Comments Sample ID: D014145-01 Solid Samykd:41i13P0 08:36 Elerbicidcs TCLP (Sub) U I r: Xi30 08:36 f +r�7rrr+:i s .Sri}y ti`ri - am 1,!ci,r; Pag Page 12 of 16 Analytical Environmental Services, Inc Date: 22-1ao-20 Client: Waypoint Analytical Client Sample ID: CLASS A Lab Order 200IF26 TagNnmber: 001005-01 Project Name: 0010195 Collection Date: 1/14/2020 9,36:00AM Lab ID: 200IF26-001A Matrix: Solid Analyses HERBICIDES, TCLP SWUM8151A 2,4,5-TP (Silvex) 2,4-D Sum DCAA Qualifiers: > Value exceeds maximum —1.1-4nt lei el BRL Not Detected at MDL H Holding iiinaa for preparation or analysis cxcccdcd ti Analyze nal NELAC ccrtificd 8 Armlyie detwed in the assoarated nicibod blank Result Qual MDL Reporting Limit Units BatchlD DF Date Analyzed Analyst (SW35100 BRL 0.030 0.20 inglL 291181 1 01/22120201034 HB BRL 0.051 0.20 mg/L 291181 1 03122/202010:34 HE 89.2 0 49,4-120 %REC 291181 1 011221202010:34 HB E Esruaated-1- abaer quamimnon range S Spike Rcro-v.umde Ikmns due io mamx Greater tbw, Result selnc J >=sumaicd+slue ddevi d below Reporting Lima i.esc than Resnq c,,jut Page Page 13 of 16 T.iYl7R03iTl4:M'AL DES Srxm`mcmrair. 1, client Name, Access Anal ytiea1, Inc. 2 Carrier: Fed Ea `r UPS C LISPS Client Courier Other SAMPLE/COOLER RECEIPT CHECKLIST AU Work Order Number: 2O0IF26 clear Save as Shipping container/cooler received in good conditlon? • damaged J leaking i I other Custody seals present on shipping container? Custody seals intact on shipping container? Temperature blanks present? • Cooler temperawrels) within limits of 0.6kC? )See item 13 and 14 for temperature recordings] Q o O Cooling initialed far recently collected samples / ice present C Chain of Custody (COC) present? • Chain of Custody signed, dated, and timed when relinquished and received? r Sampler name and/or signature on CDC? • Were all samples received within holding time? ■ TAT marked on the COC? It no TAT lrtdsated, pm ceedad with standard TAT per Terms&Candilions, i 13. Cooler i 7emperalurc to °e Cooler 2 Temperature °C Cooler 3 Temperature °C Coaler 4 Temperature aC 14. Cooler Siemperature °C Cooler 6 Temperature °C Cooler 7 Temperature oC Cooler g Temperature °C 15. Comments: 16, 37 29, 19. 20. 21 22 23 24 25 26. I certify that I have completed sections 1-15 )dated Initials). M11/16/20 Were sample containers intact upon receipt? • Custody seals present on sample containers? Custody seals intact an sample Containers? ■ Do sample container labels match the CDC? 00 ©. Incompleteinfo F— illegible no label L other Are analyses requested indicated on the COCA • Were all of the samples listed on the COC received? © samples received but not listed an COC samples listed on COC not received Was the sample collection date/time noted? Did we receive sufficient sample volume for indicated analyses? Were samples reteiwd in appropriate oontatners? Were VOA samples received without rreadspare )e 1/4" bubble)? Weir cop blanks submitted? r 11istedoncoc F-1 not listed on LOC F 27 CornmenW This section only applies to samples where pH can be l certify that I have completed sections 16-27 [dated initials), checked al Sample Receipt. Yes No N/A Details Comments 29 29 30, LM 1115/20 Have containers needing chemical preservation been checked? ` Containers meet preservation guidelines? - NaW Certain analyses requhe chemical presemallon but must he checked in the laboratory and not upon Sample Recetpl such as Gnlilvrrns, VOCs and Oil S 0reaseRPH I certify that i have completed sectjans 29-30 (dated Initials) Checklist 6 9 17 Rev 2 Lacked LM 1126/20 Page 4 of 6 Page 14 of 16 Analytical Environmental Services, Inc Client: Waypoint Analytical Project Name: DO10195 Workorder: 2001F26 Date. 22-3an-20 ANALYTICAL QC SUMMARY REPORT Batch[D: 291181 Sample 1D: MB-291181 Client 1D: Units: mglL Prep Date; 01120/2020 Ran No: 416535 SampleType: MBLK TeslCOde: HERBICl0ES,TCLP SWt3]11g151A Batch1D:291131 Analysis Date: 01/21/2010 SegNo: 9399770 Analyte Result RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit Qua! 2,as= I P {Sllvex) BRL 0.20 2,4-D BRL 0.20 Sun: DCAA 0.4096 0 0300D 81.9 49.4 120 iample ID: LCS-291181 Client 1D: Units: mg/L Prep Dale: 01120/2020 Run No: 4I6535 iampleType: LCS TestCode: HERBICIAES,TCLP M3lIIa151A BntchlD: 291181 Analysis Date: 0112112020 SegNo: 9399771 4nolytt Result RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit Qual 2.4,5-TP(Silvex) 0.4644 0.20 0.5000 92,9 49 120 2,4-D 0,4518 0.20 05000 90.4 50.9 120 Sun: DCAA 0.4659 0 0,5000 93.2 49.4 120 Sample ID: 2001F57401 BMS Client ID: __. [!nits: mg/L Prep Date: 01120/2020 Run Nw 41ti535 SompleType: MS TestCode: HERRICIOMTCLP SW3311A1t51A BatchID:291181 Analysis Date: 01121/2020 SegNo: 0399773 Analyte Result RPT Limit SPK value SPK Ref Val %REC Low Limii High Limit RPD WWI %RPD RPD Limit Qual 2.4,5-TP (Siivex) 0,4281 0.20 0,5000 95.6 48.2 120 2A-D 04062 0.20 0,500 812 45 130 Sun: DCAA 04560 0 0.5000 91 2 49A 120 QusE3n n- t::.::,.a 14 .t r .,r,.;ills: •~• �_ < L.xs ih:.n X-1, r-,W IIXI. Wk. l,, I, 1�._„�.npil rtn::iFe.:,laxxk:xonn r,i,E:1 ,.N dlyu N A, -h ,."n, Nt: AC 'tl.,n, X.Tprti,IS L.n:•:, .N .S"kA R":.m-".': l„ner<J.w ;O,nahn fl A,uh,nJ.�,,.J n. `.:.,v�ec•,J „klhal hl.�i: t+ Ilnl.,nt,unnfo, ry.li ,:n,l nr .,n ih,+;a.y.�,Lxl Page 5 of 8 Page 15 of 16 End of Report Page Page 16 of 16 • NC Certification No. 402 Case Narrative Waypoint- NC drinking Water Cent No, 37735 4/24/20 14:38 SC Certification No, 99012 ANALYTICAL Town of Mocresville/RR WWTP Whitney Munroe P. O. Box 878 Mooresville, NC 28115 Project: Class A Dried Sludge Lab Submittal Date: 04/13/2020 Work Order: 0040158 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, ail samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Narrative Notes: Analysis note for SAR: SAR = [ Na ] / SQRT { ( [Ca] + [Mg] )/2 } SAR = [ 140123 ] I SQRT { { [110/20] * [98/12.2] )12 } SAR = 2.3 Concentrations for Na, Ca, and Mg are expressed in mill iequivalents per liter, and SQRT designates taking the square root of the operand in parentheses. PAN Equation = 0.3 * (THN - Ammonia) + 0.5 * (Ammonia) + Nitrate -Nitrite PAN = 0.3 * (17000 -- 1400) + 0.5 * (1400) + 2.6 PAN = 5300 mg/kg Equation uses Mineralization Rate (MR) for Aerobically Digested Solids (0.3) This report should not be reproduced, except in its entirety, without the written consent of WaypointAnalytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 -Toll Free Number: 1-8001529.6364 - Fax: 7041525-0409 Page 1 of 16 Please calf if you have any questions relating to this analytical report. Respectfuliy, WAYPOINT ANALYTICAL Terri W. Cole Project Manager Data Qualifiers Key Reference: A ECCV failed low. Samples were re -analyzed with confirming results. Initial data reported. SE Surrogate recovery outside of the QC limits due to emulsion. BRL Beiow Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of WaypointAnalytical. 449 Spring brook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toil Free Number: 4-8001529-6364- Fax: 7041525-0409 Page 2 of 16 0 Waypoint. ANALYTICAL Sample Receipt Summary 04/24/2020 Work Order: 0040158 Client Sample ID Lab Sample 1D Matrix Date/Time Sampled Date/Time Received Class A 0040158-01 Solid 04/13/20 8:23 04/13/20 14:35 Samples were received in good condition at 5,5 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 2622441543 Phone: 704/529-6364 - Toll Free Number: 1-81IW529-6364 - Fax: 704/525-0409 Page 3 of 16 • 0 Waypoint. ANALYTICAL Town of Mooresville/RR WWTP Attn: Whitney Munroe P, Q. Box 878 Mooresville, NC 28115 Project: ClassA Dried Sludge Sample Matrix: Solid Laboratory Report 04/24/2020 ClientSar lelD: ClassA Sample ID: 0040158-01 Work Order: 0040158 Time Collected: 04/13/20 08:23 Time Submitted: 04/13/20 14:35 Parameter Result Units Report MOL Dilution Method Analysis Aralyst Batch Limit Factor Datorrime ID General Chemistry Parameters Plant Available Nitrogen 5300 mglkg dry 2000 1000 25 *Calculation 4120120 12:10 CLB [CALL] Solids 95.6 % by 0.100 0.100 1 *SM2540 G 4116120 9:08 EDV POD0222 Weight Ammonia as N 1400 mg/kg dry 10 2.6 1 *SM4500-NH3 C 4117120 17:35 BMS POD0267 Nitrate/Nitrite as N BRL mg/kg dry 5.2 1.4 1 *SM4500-NO3 F 4120120 12:10 CLB POD0264 PH 6.2 pH Units 1 *9045D 4114120 11:10 CLB POD0198 Phosphorus -Total 13000 mglkg dry 520 160 100 *SM4500-P F 4116120 10:20 CLB POD0217 Total Kjoldahl Nitrogen 17000 mglkg dry 6500 3500 25 *351.2 4120120 10:45 CLB POD0268 Temperature 19.7 pH Units 1 *9045❑ 4114120 11:10 CLB POD0198 Microbiological Parameters Fecal Collforms TCLP Extraction by EPA 1311 3 MPNIg dry 0.2 1 *SM9221 E 4/13120 15:33 BMS POD0203 TCLP Extraction Complete NIA 1 *1311 4/15/20 5:20 EDV POD0199 TCLP Extraction Complete N/A 1 *1311 ZHE 4/21/20 14:30 ANG P0D0319 TCLP Metals Mercury BRL mglL 0.010 0.000034 1 *7470A 4/17120 13:06 JAB POD0256 Arsenic BRL mglL 0.10 0.030 1 *6010D 4116120 16:07 JAB POD0215 Barium BRL mglL 6.0 0.010 1 *6010D 4116/20 16:07 JAB POD0215 Cadmium BRL mg1L 0.025 0.002C 1 *6010D 4116120 16:07 JAB POD0215 Chromium BRL mg1L 0.25 0,015 1 *60100 4/16120 16:07 JAB POD0215 Lead BRL mg1L 0,050 0.020 1 *6010D 4116/20 16:07 JAB POD0215 Selenium BRL mg1L 0.15 0.063 1 *6010D 4116120 16:07 JAB POD0215 Silver BRL mglL 0.25 0.0045 1 *6010D 4/16120 16:07 JAB POD0215 TCLP Organochlorine Pesticides by GCIECD Chlordane BRL mglL 0.0025 0.00090 1 *8081B 4116120 14:17 NMB POD0231 Dieldrin BRL mglL 0.00050 0.000068 1 *8081B 4116/20 14:17 NMB POD0231 Endrin BRL mg1L 0.00060 0.000068 1 *8081B 4/16120 14:17 NMB POD0231 gamma-BHG BRL mg1L 0.00060 0,000030 1 *8081B 4116120 14:17 NMB POD0231 Heptachlor BRL mg1L 0.00050 0,000065 1 *8081B 4116/20 14:17 NMB POD0231 Heptachlor Epoxide BRL mglL 0.00050 0.00011 1 *8081B 4116/20 14:17 NMB POD0231 Methoxychlor BRLA mglL 0.00060 0.000090 1 *8081B 4/16/20 14:17 NMB POD0231 Toxaphene BRL mg1L 0.025 0,0018 1 *8081B 4116120 14:17 NMB POD0231 Surrogate Recovery Control Limits Decachlorobiphenyl 14 % 13-186 Tetrachloro-m-xylene 18 % 40-134 SE TCLP Semivolatile Organic Compounds by GCIMS 2,4,5-Trichlorophenol BRL mg1L 0.25 C.0036 1 *8270E 4116120 12:59 JMV POD0216 2,4,6-Trichlorophenol BRL mglL 0.10 0.0045 1 *8270L 411612C 12:59 JMV POD0218 2,4-Dinitrotoluene BRL mglL 0.012 00042 1 *8270E 4/16120 12:59 JMV P000218 This report should not be reproduced, except in its entirety, without the written consent of waypointAnalytical. 449 Springbrook Road - P.O. Box 240W - Charlotte, NC 28224-0543 Phone: 7041529-6364 -Toll Free Number: 1-8001529.6364 -Fax; 7041525-0409 L Page 4 of 16 0 0 Laboratory Report Waypoint- 04/24/2020 ANALYTICAL Town of Mooresville/RR WWTP Project: Class A Dried Sludge Client Sample ID: Class A Attm Whitney Munroe Sample 1D: 0040158-01 P. O. Box 878 Work Order: 0040158 Mooresville, INC 28115 Sample Matrix: Solid Time Collected: 04/13/20 08:23 Time Submitted: 04/13/20 14:35 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 2-Methylphenol BRL mg1L 0.050 0.0024 1 *827OF 4116120 12:59 JMV POD0218 314-Met}tylphenoi BRL mglL 0.050 0.0025 1 *8270E 4116/20 12:59 JMV POD0218 Hexachlorobenzene BRL mglL 0.020 0.0039 1 *8270E 4f16120 12:59 JMV POD0218 Hexachlorobutadiene BRL mglL 0.050 0.0045 1 *8270E 4116120 12:59 JMV POD0218 Hexachleroethane BRL mg1L 0.050 0.0037 1 *8270E 4116120 12:59 JMV POD0218 Nitrobenzene BRL mg1L 0.050 0.0038 1 *8270E 4/16/20 12:59 JMV POD0218 Pentachlorcphenol BRL mg1L 0.25 0.011 1 *8270E- 4/16/20 12:59 JMV POD0218 Pyridine BRL mg1L 0.25 0.0016 1 *8270E 4/16120 12:59 JMV POD0218 Surrogate Recovery Control Limits 2,4,6-7r1bromcphenol 39 % 43-140 SE 2-Fluorobiphenyl 32 % 44-119 SE 2-Fiuorophenol 24 % 19-119 Nitrobenzene-d5 31 % 44-120 SE Phenol-d5 19 % 11-52 Terpheny1-d14 38 % 50-134 SF TCLP Volatile Organic Compounds by GC/MS 1,1-Dichloroethylene BRL mg1L 0.035 0,0035 10 *8260D 4/22/20 0:22 JLB POD0328 1,2-Dichloroethane BRL mglL 0.025 0.0041 10 *8260D 4122120 0:22 JLB POD0328 1,4-Dichlorobenzene BRL mglL 0.38 0.0042 10 *8260D 4122120 0:22 JLB ROD0328 Benzene BRL mg1L 0.025 0.0034 10 *8260D 4/22120 0:22 JLB POD0328 Carbon Tetrachloride BRL mg1L 0.025 0.0055 10 *8260D 4/22/20 0:22 JLB POD0328 Chlorobenzene BRL mg1L 5.0 0.0034 10 *8260D 4/22/20 0:22 JLB POD0328 Chloroform BRL mg1L 0.30 0.0048 10 "8260D 4122120 0:22 JLB PODO328 Methyl Ethyl Ketone (2-Butanone) BRL mglL 10 0,0078 10 *8260D 4/22120 0:22 JLB POD0328 Tetrachloroethylene BRL mglL 0,035 0,0031 10 *8260D 4/22/20 0:22 JLB POD0328 Trichlcroethylene BRL mg1L 0,025 0.0046 10 *8260D 4122/20 0:22 JLB POD0328 Vinyl chloride BRL mg1L 0,010 0,0041 10 *8260D 4/22/20 0:22 JLB POD0328 Surrogate Recovery Control Limits 4-Bromolluorobenzene 98 % 80-124 Dibromofluoromethane 103 % 75-129 Toluene -dB 92 % 77-123 Total Metals Aluminum 14000 mglkg dry 260 57 10 *6010D 4117120 11:33 JAB POD0190 Mercury 0.30 mglkg dry 0.26 0.090 5 *74718 4116120 11:54 JAB POD0238 SAR Soil Preparation Ccmplete g 1 *2-78-054 4/15120 8:55 EDV POD0196 SAR Percent Moisture 77.0 % by 0.100 0.100 1 " 2-78-054 4116/20 8:55 EDV POD0223 Weight Arsenic 2.0 mglkg dry 1.0 0.14 1 *6010D 4116120 11:06 JAB POD0190 Sodium Absorption Ratio 2.3 [blank] 0.30 0.016 1 *2-78-054 4117120 12:28 JAB P000220 Cadmium BRL mg/kg dry 0.52 0.035 1 *6010D 4116/20 11:06 JAB POD019C Calcium 13000 mglkg dry 100 27 1 *6010D 4116120 11:06 JAB POD0190 This report should not be reproduced, except in its entirety, witheut the written consent of WaypointAnalytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 -Toll Free Number: 1-8001529.6364 - Fax: 7041525-0409 Page 5 of 16 0 Waypoint_ ANALYTICAL Town of Mooresville/RR WWTP Attn: Whitney Munroe P. O. Box 878 Mooresville, NC 23115 Project: Class A Dried Sludge Sample Matrix: Solid Laboratory Report D4/24/2020 Client Sample ID: Class A Sample ID: 0040158-01 Work Order: 0040158 Time Collected: 04/13/20 08:23 Time Submitted: 04/13/20 14:35 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Calcium, SAR 110 mg1L 5.0 Copper 200 mglkg dry 26 Lead 7.4 mglkg dry 1.0 Magnesium 3500 mglkg dry 26 Magnesium, SAR 98 mglL 0.50 Molybdenum 10 mglkg dry 1.0 Nickel 12 mglkg dry 1.0 Potassium 4800 mglkg dry 100 Selenium 2.2 mglkg dry 1.0 Sodium 1000 mglkg dry 100 Sodium, SAR 140 mg1L 2.5 Zinc 360 mglkg dry 100 0.050 5 *6010❑ 4117120 7:33 JAB POD0220 3.6 10 *6010D 4/17120 11:33 JAB POD0190 0.17 1 *6010D 4116/20 11:06 JAB POD0190 2.4 1 *6010D 4116120 11:06 JAB POD0190 0.043 5 *6010D 4/17120 7:33 JAB POD0220 0.13 1 *6010D 4116120 11:06 JAB POD0190 0.31 1 *6010D 4116/20 11:06 JAB POD0190 11 1 *6010D 4116120 11:06 JAB POD0190 0,29 1 *6010D 4/16120 11:06 JAB POD0190 14 1 *6010D 4116120 11:06 JAB P000190 0.090 5 *6010D 4/17120 12:28 JAB POD0220 15 10 *6010D 4/17120 11:33 JAB POD0190 This report should not be reproduced, except in its entirety, without the written consent of Waypoi nt Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041,925-0409 Page 6 a# 16 Sample Extraction Data Prep Method: 351.2 Lab Number Batch Initial Final Datefrime 0040168-01 POD0268 0.05 g 25 mL 04/17/20 16:00 Prep Method: SM4500-NH3 B Lab Number Batch Initial Final Date/Time 0040158-01 POD0267 1.02 g 50 mL 04/17120 14:28 Prep Method: SM4500-PB5 Lab Number Batch Initial Final Date/Time 0040158-01 POD0217 1 g 50 mL 04/15120 9:50 Prep Method: Solids, Dry Weight Lab Number Batch Initial Final Date/Time 0040158-01 POD0222 30 g 30 g 04/15/20 12:40 Prep Method: 1311 Lab Number Batch Initial Final DatelTime 0040158-01 POD0199 100 g 2000 mL 04114/20 12:55 0040158-01 POD0319 250 mL 250 mL 04/20/20 20:30 Prep Method: 301OA Lab Number Batch Initial Final DateMme 0040158-01 POD0215 10 mL 50 mL 0415120 5:31 Prep Method; 7470A Lab Number Batch Initial Final DateMme 0040158-01 POD0256 20 mL 30 mL 04/17/20 6:57 Prep Method: 3510C GC Lab Number Batch Initial Final Datefrime 0040158-01 POD0231 200 mL 10 mL 04/15/20 1815 Prep Method: 3510C MS Lab Number Batch Initial Final Date/Time 0040158-01 POD0218 200 mL 1 mL 04115/20 8:45 Prep Method: 5030B Lab Number Batch Initial Final DatelTime 0040158-01 POD0328 10 mL 10 mL 04/21/20 14:00 Prep Method: 3010A Lab Number Batch Initial Final Datefrime 0040158-01 POD0220 50 mL 50 mL 04/15/20 8:56 0040158-01 POD0220 50 mL 50 mL 04/15/20 8:55 0040158-01 POD0220 50 mL 50 mL 04/15/20 8:55 Prep Method: 3050B Lab Number Batch Initial Final DatelTime 0040158-01 PODO190 2 g 50 mL 04/14/20 6:18 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0543 Phone: 7041529-6364 -Toll Free Number: 1.8001529-6364 - Fax: 704/525-0409 Page 7 of 1 Fi Sample Extraction Data Prep Method: 3050B Lab Number Batch Initial Final DatelTime 0040158-01 POD0190 2 g 50 mL 04/14/20 6:18 Prep Method: 74718 Lab Number Batch Initial Final Date/Time 0040158-01 POD0238 0.6 9 50 mL 04116/20 715 Prep Method: SAR 2-78-054 Lab Number Batch Initial Final Date/Time 0040158-01 POD0195 250 g 250 g 04/14/20 8:55 Subcontracted Analyses The following analyses were subcontracted to Analytical Environmental Services, Inc. Lab Number Analysis 0040159-01 Herbicides TCLP (Sub) This report should not be reproduced, except In its entirety, without the written consent of Waypoint Analytical, 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 Page 8 of 16 Waypoint... NALVTiCAL 449 Springbrook Road • Charlotte, NC 21217 Phone 7041529-6364 Fax:704i525-0409 Client Company Name:- 0 P 1 Cace*At Report To/Contact Name: _Wh mtA11t'&r Reporting Address: P ►� . Box ig 4t 1� Alt- PT- Y7_il J_I-A rr CHAIN OF CUSTODY RECORD ONLY PAGE —1OF A QUOTES TO ENSURE PROPER BILLING:.- I YES NO Nli 10 _ u JS .' B c�+ Project Name: r 7 rt, eQ' `5r " I Samples INTACT upon arrival? Received ON WET ICE? X _ Q Short Hold Analysis L� y ) (No) UST Project: {Yes) { PROPER PRESERVATIVES indicated? � 'Please ATTACH any project specific reporting (QC LEVEL I�I III IVj Rived WITHIN HOLDING TIMES? provisions and/or QC Requirements I CUSTODY SEALS INTACT7 D Invoice To: VOLATILES reed WlOUT HEADSPACE? Address: PROPER CONTAINERS used? _ r��C: TEMP: Therm ID.Observed �'C 1Cors. ` I-- ' � ' �" �" FOA I r"'tI' "'1' Purchase Order No-18itling Reference TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL Email Address: WrnWAQC&irY1D&T4Al1tAe-�9C V Requested Due Date ❑ 1 Day ❑ 2 Days 0 3 Days ❑ 4 Days ❑ 5 Days EDD Type: PDF✓ Excel --Other y y days Rush Work Must Be Certification: NELAC FL NC l� yp "Working Da s" ❑ 6-9 Da s tandard i0 da Pre Approved SC OTHER NIA Site Location Name: Samples received after 14:00 will be processed next business day Site Location Physical Address' Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO (SEE REVERSE FOR TERMS a, CONDITIONS REGARDING SERVICES RENDERED BY WAYPOINT ANALYTICAL, LLC TO CLIENT) Sample Iced Upon COlioetion: YES✓ NO_ TINE MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED CLIENT DATE COLLECTED ! Si SAMPLE DESCRIPTION COLLECTED MILITARY WATE (SOIL,PRESERVA- % TYPE NO. SIZE TICS REMARKS ID NO. HOURS SLUDGE) SEE BELOW 4 PRESS D.COPIES Sampler's Signature Sampled By (Print Name) Affiliation -TOV-1h Upon relinquishing, this Chain of Custody Is your authorization for Waypoint nalytical to oceed with the analyses as requested above. Any changes must be submitted In writing to the Waypaint Analytical Project Manager. There will b (3harges for any chpgqs after analyses have been initialized. R my ishCdB :(Slgnalurol Rccu:wd6,:ISEgur7uroj -. �, Da MitumyMaur� AdditionalGommenlS• SlbeArrivalTime: Relinquished By: ra) Received BY (STputure) /ate �O •� Site Deparlu-6 Time: Relinquished By. (Signature) Received Nor inl Analysral 6Y Date Field Tech Fee: -t3s �'.3s Mileage: MethudofShlpment NOTE: LSAMPL.ECOOLERS SHOULD BETAPEDSHUT WnNCUST EALSFORTRANSPORTATION ToTHE LABORATortY COCGraupAm SAMPL ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY, 0 Fed Ex ❑ UPS ClHand-darmwed ypointAnalytical Field Service 0 OLhar ER: SEE REVERSE F:OR C 'WEOS: NC q SC T£R LI NCB ❑ SC ATER• NC O SC E• O❑ NCRCRA ❑ SC I NC ❑ SC o NC 1=LISC ❑ NC ❑ SC TERMS N CONDITIONS SC 0 NC ❑ SC ILI— ❑ ❑ -CUP! IA110 K TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Car, VOA = Volatile Organics Analysis (Zero Head Space) '-IGINAL P R I S M Enviro rmce Analytical s Environmental Solutions LABORATORIES. INC. 449 Sprtngbrook Road • Charlotte, NC 28217 Phone 7041529-6364 - Fax:7041525-0409 Client Company Name: Tv—w,, J- Awyelu4� Report To/Contact Name: / W4-- -- Reporting Address: -• O,'aO DO,a4,J 114 AJG I r 9.Ar CHAIN OF CUSTODY RECORD PAGE F 1.r�_ lQUOTE III TO EKOURE PROPERf BILLING; Project Name:. ma-,-S 0 1) riej Short Hold Analysis: es (No) UST Frroject: (Yes) ( OW `Please ATTACH any prbVict specific reporting (QC LEVEOf I Ili IV) provisions andlor QC Requirements InvoiceT'o: ok", MDDIi'b'IOLe Address: YES NO N/A Samples INTACT upon amval? Received ON WET ICE?CD mac_ PROPER PRESERVATIVES indicated? _� Y Received WITHIN HOLDING TIMES? a) CUSTODY SEALS INTACT? VOI.ATILI S revd WtOUT HEADSPACE? PROPER C014TAINERS use 7 TEMP. ThNrm ID:_LL -M Observed:. A_°C I Corr: - 7 °C rnvne: r� . rrtu� --ter rax (rest (tva); Purchase Order No.IB!llfng Reference Email Address: _" �( �c 'cRequested Due Date U 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 flays Q 5 Days EDD Type: POF,,,ZExcelOther "Working Days" ❑ 6-9 pays�Standard 10 days ❑pre Approvedust Be Site Location Name: Samples received after 14:00 will be processed next business day. TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL , f Certification: NELAC DOD FL NU' SC OTHER N/A Site Location Physical Address' Turnaround time is based on business days, excluding weekends and holidays. (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) Water Chlorinated: YES_ _ NO Sample Iced Upon Collection: YES NO CLIENT DATE SAMPLE DESCRIPTION COLLECTED TIME COLLECTED MILITARY HOURS MATRIX (SOIL, WATER OR SLUDGE SAMPLE CONTAINER PRESi_RVA- TIVES ANALYSIS REQUESTED ' '� �►- REMARKS f Q PRISM LAB ID NO, SEE LOW NO, SIZE I — 1 �. .• Sampler's Signature `"' Sampled By (Print Name) Lrr � rlAffiliation ltti� Upon relinquishing, this Chain of Custody is your authorization for Prism to procee wlth a analyses as requested above. Any changes must be submitted in writing to the Prism Project Manager. There will be charges for any ch ges after analyses h e been Initialized, PRISM USE ONLY ReH quls ad 6y: (Signature) � ece v y: Slgnatural l t Oat MuitarylHaurs Additional Comments: Site Arrival Time: r�9r'11 /fin G 1F� C Relinquished By: (Sig re) Received By: (Signature) Jv Ds '1fJr1+A 1`��e`(r�-'�I— - lA'l,4t Site Departure Time: RaGngwsned By: (Signature) Received For Prism La[tnraterf a 6y: - aLe I '.rlC` Field Tech Fee: �/' (�' [r, • 5 ;�A, r' flNl Mileage: Method of hlpment: NOTE: A L SAMPLE COOLERS SHOULD BE TAPED HUT WRH 3TODY SEALS FOR TRA RTATION TO THE LABORATORY, 000 Gmp o. 1 /Y �,1~� j � I SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY.(/ i ❑ Fed Ex ❑ UPS ❑ Hand -delivered prism Field Service L7 Other ES: UST: GROUNDWATER: DRINiClNG WATER: S ID WASTE: RC RA: i CERCLA tANI7FILL OTHER: '' NC ❑ SC ❑ NC ❑ SC Q NC ❑ SC ❑ NC ❑ Sc C ❑ Sc ❑ NC ❑ SC I ❑ NC C3 SC ❑ NC ❑ Sc 0 NC C SCCONDITIONS El Li *CONTAIN (PE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Ct: )A = Volatile Organics Analysis (Zero Head Space) ]G INAL ALC1;s5 ANALYTICAL, INC. ANALYTICAL REPORT CLIENT Waypoint Analytical PO Box 240543 Charlotte NC 282240543 ATTENTION Teri W. Cole PROTECT iD 0040158 LABORATORY REPORT NUMBER 2004C55 DATE April 22, 2020 Primary Data Review By Seeondary Data Review By 4 r`/ Ashley Amick Chris Pafford Project Manager, Access Analytical Project Manager, AES aamick(7a axs-ine.corn PLEASE DOTE: Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc), 3080 Presidential Drive, Atlanta, GA 30340. AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certitled lab # FL-E87582, NELAP certified laboratory # E87582 All-]A-Ls'LP,LLC Laboratory IDA00671 for Industrial livgicnc samples (Organics, Metals, PCM Asbestos, Gravimetric), Environmental Lead (Paint, Soil, Dtlst Wipes, Air), and Environmental Afiernbiology (Fungal) Direct Examination. Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a represeniaiive ofAES serving client in the SC/NCIGA areas. All questions regaarding this report should be directed ID your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243 Pag page 11 of 16 WayR t do011css SUBCONTRACT ORDER Certificatinn NELAC USACF WaypointAnnlytica! NCv SC_ Other 0040158 NIA SE-NDING .AHORA UY: 17FC:£!YlNG LAFi IATORY.- WaypointAnalytical An&lytical Environmental Services, Inc. P. 0. Box 240543 3080 Presidential Parlcwoy Charlotte, NC 28224-0543 Atlanta, GA 30340 P11011e:800-529-6364 Phone :(770) 457-8177 FEM 704-525-0409 Fax: NA Project 4lanagcr. Terri W. Cole Analysi4 Due Expires Labormory iD Comments Sumptclt):004a1tti-pl Solid 1;amp1rd;04/13/260$_23 C1Ck..s i [C11 �kI'1`. Page Page 12 of 16 Analytical Environmental Services, Inc Date; 22-Apr-20 Dient: Waypoint Analytical Client Sample 1D; CLASSA Lab Order 2004C55 Tag Number: 0040158-01 'roject Name: 0040I58 Collection Date: 4/13/2020 823;00AM �abID: 2004C55-001A Matrix: Solid Analyses Result Reporting Y Qua[ MDL Limit Units BatcblD DF DateAnalyzeJ Analyst HERBICIIIES, TCLP SW I311/8151A 2,4,5-TP (Silvex) 8RL 2,4-D l3RL Surr: DCAA 64.9 Qualifiers: \;chic ccucds madman ronlammam Iei el ©RL \al nulccted m MDL 1i Iloldrne nnres for preP;lrauon or anahsis--ded \ Anal, 1e nol\[I.•\C CCrI IIicd B • ,ii I, is lb l[—ed In the aSS-IaIW nWhal blank (SW3510C) 0030 0.20 ineL 295795 1 04121/202017:20 UH 0.051 0.20 ing/1 ' 295795 1 04/21 /2020 17:20 UH 0 50.3-120 %REC 295795 1 04121/202017:20 UH E Es m.d -1- aborc panlliallo,, ra nce S Spuke Rn- er) omslda Innis due io minx Grrnlcr Iban Rcsuil salve f E;un nmd %a I dcl¢riril bel- Rulwnma Linnl Less rhnn RCSIl$ iaiue Page Page 13 ofi 1 AFS 1. Client Name: Access Analytical, Inc. 2. Carrier: Fed Ex . s UPS C USPS._ Clil Courier Othel Clear SAMPLE/COOLER RECEIPT CHECKLIST AEs Work order Number: 2004C5S vac Nn role netniir r..........,« Save as Shipping container/cooler received in good condition? ti damaged L] leaking L] other�J Custody seals present on shipping container? Lustodyseals intact on shipping container? Temperature blanks present? r Cooler temperatures) within limits of 0-600 (See item 13 and 14 for temperature recordings 1 0 Q O Cooling initiated for recently collected samples / ice present Chain of Custody (COE) present? • Chain of Custodysigned, dated, and timed when relinquished and received?• Sampler name and/or signature on COC? Were all samples received within holding time? • TAT marked on the COCA :ifnOTAThidf=clJ, nNacePdedwith standard TAT rTrrms&Conditions. 21 13 Cooler 1 Temperature 0-3 °C Cooler 2 Temperature °C Cooler 3 Temperature oC Cooler 4 Temperature °[ 14, C-1-STemperature` °C Cooler 6 Temperature °c Cooler 7 Temperature °C Cooler 8 Temperature 'C 1S Comments: t5. 17 7 E. 19 ao, a1, I' 23- 34. 75, 26. I certlty that I have completed sections 1-1S (dated initials). AP 4135/20 Yes N. Nra nPtailc r—...x. Were sample containers intact upon recelpt? Custody seals present on sample containers? Custody seals intact on sample containers? Do sample container labels match the COC?• © O Incomplete info illegible �! nolabel C, other F—j Are analyses requested indicated on the COC? • Were all of the samples listed an the COC received? it O © O samples received but nut fisted on COC r- samples listed on CDC not received F Was the sample colleulon date/time noted? ■ Did we receive sufficient sample volume for indicated analyses? Were samples received in appropriate containers? + Were VOA samples received without headspace (<1/4.. bubble)? ! �' Were trip blanks submitted? • listed on MC n not listed on CDC C 27 Comments: This section only applies to samples where pH can be 1 certify that I have completed sections 26-27 {dated initials). checked at Sample Receipt Yes No N/A Details comments 23. 29 30. Was pH OR'/16/20 Havr Containers oetding chemical pca�erv4ndrt been checked?' • Cnntainntz meet preservationguidrlmr:? • NOIe: Certain analyses requite chemical ptesewalion hot must be checked in the laboralory and not upon Sample Aeceipl such as Colilorms, VOCS and Oil & GreaserTFIH I certify that I have completed sections 28-30 {dated initials) Checklist 6.9.17 Reu 2 LQeked RR 4/16120 Page 4 of 6 Page 14 of 16 Analytical Environmental Services, Inc Client: WaypointAnalytical Project Name: 0040159 Workordcr, 2004C55 Date; 22-Apr-20 ANALYTICAL QC SUMMARY REPORT BatchlD: 255795 Sample ID: MB-295795 Client ID: Units: ang/L Prep Date; 04/21/2020 Run No: 423616 iampleType: MBLK TestCode: HERSICt6ES,TC1.1' SW1311181SIA Batch1D:295795 Analysis Dale: 04121/2020 Seq No: 9584328 Analyle Result RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limil Qual 214,5-TP (Silvex) BRL 0.20 2,4-D BRL 0.20 Sun: DCAA 03494 0 0.5000 69.9 50.3 120 Sample ID: LCS-295795 Client ID: Units. mg/L. Prep Date: 04/21/2020 Run No: 423616 SampleType: LCS TeslCode: nE111'1C1t1ES.TCL1' SZV7311 fa151A BatchlD: 295795 Analysis Date; 04/21/2020 Seq No: 9584330 Analyte. Result RPT Limit SPK value SPK Ref Val %REC Low LimiI High Limit RPD Ref Val %RPD RPD Liinil Qual 2,4,5-TF (Sil ex) 0,3497 0.20 05000 69,9 494 120 2.4-D 03239 0.20 0.5000 64.9 50,2 120 Sort: DCAA 0.3694 0 05000 739 50.3 120 Sample ID: 2004C55-001AMS Client ID; CLASS A 4 Units: metL Prep Date: 042112020 Run No: 423616 SampleType: MS TestCodo: HERS1CJVES.TCLP SW131118151A BatchlD: 295795 Analysis Date: 041212020 Seq No: 9584332 Analyte Resell RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Lilnit Qual 2,4,5 7P (Sihvec) 0.3170 0,20 05000 63.4 49.2 120 2,4-D 03065 0.20 05000 61.3 45 Ia0 Sun: DCAA 0.11199 0 0 5000 640 503 120 Qndlfkr lirais Iun N. nk+.1u < I—.1,m Rr.k riGu nN� 1k�A�.•�,� .. iinnl t' � el.Jf ..i. aloe. rw:iutiniwi r�na�) 1 is n�nswl.;do-•�l•..Iul hli�.. legnn�m-I.iinn N .ual.u-rrI TI:I.tL—I.f I k1. Iun ky>,i nn_ I m+a ti yoke 1I.—I nix.rJ. lini"J.. In muinr t1 .WW... v;wlal m urcnw.rnl.J;rs;'z hlons iI IInW,«In„;lar ly ryan-:a.nn„ 6.�y�„x.Jd t[T9)n.•aJ. Tim. :Jnrin n�xm Page 5 of 6 Pagel 5of16 End of Report Page Page 16 of 16 • NC Certification No. 402 Case Narrative Waypoint_ NC Drinking Water Cert No. 37735 7130/20 15:21 SC Certification No. 99012 ANALYTICAL Town of Mooresville/RR WWTP Whitney Munroe R O. Box 878 Mooresville, NC 28115 Project: Class A Dried Sludge Lab Submittal Date: 07/13/2020 Work Order: 0070145 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Narrative dotes: This is a Revised Report and supercedes the original laboratory report dated 7/29/20 12:31 PAN and SAR calculations were added to the Case Narrative. PAN Equation = 0.3 * (TKN - Ammonia) + 0.5 * (Ammonia) + Nitrate -Nitrite PAN = 0.3 * (4300 - 1400) + 0.5 * (1400) + 2.6 PAN = 1600 mg/kg Equation uses Mineralization Rate (MR) for Aerobically Digested Solids (0.3) Analysis note for SAR: SAR -[NaI/SQRT {( [Ca]+[Mg] )12} SAR = [ 200123 ] 1 SQRT { ( [410/20] + [150/12.2]) / 2 } SAR = 2.1 Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates taking the square root of the operand in parentheses. This is a Revised Report and supercedes the original laboratory report dated 7/29f20 12:32. PAN and SAR calculations were added to the Case Narrative. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364- Fax; 7041525.0409 Page 1 of 17 Please call if you have any questions relating to this analytical report. Respectfully, WAYPOINT ANALYTICAL ��/✓u cc�Ce�c� Terri W. Cole Project Manager Data Qualifiers Key Reference: FIT Sample received and analyzed outside of the hold time. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except In its entirety, without the written consent Of WaypeintAna lytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax; 7041525-0409 Page 2 of 17 0 Waypoint_ ANALYTICAL Sample Receipt Summary 07/30/2020 Work Order: 0070145 Client Sample ID Lab Sample ID Matrix Dateffime Sampled Dateffime Received Class A 0070145-01 Solid 07/13/20 7:55 07/13/20 14:20 Samples were received in good condition at 2.0 degrees C unless otherwise noted, This report should not be reproduced, except in its entirety, without the written consent of WaypointAnalocaI 449 Springb rook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 L Page 3 of 17 (, Laboratory Report Waypoint. 07/30/2020 ANALYTICAL Town of Mooresville/RR WWTP Project: Class A Dried Sludge Client Sample ID: Class A Attn: Whitney Munroe Sample ID: 0070145-01 R O. Box 878 Work Order: 0070145 Mooresville, NC 28115 Sample Matrix: Solid Time Collected: 07/13/20 07.55 Time Submitted: 07/13/20 14:20 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DaterTime ID General Chemistry Parameters PiantAvailable Nitrogen 1600 mglkg dry 320 110 2 *Calculation 7/23/20 10:50 CLB [CALC] % Solids 96.2 % by 0,100 0.100 1 *SM2540 G 7/16/20 10:48 ENV POG0194 Weight Ammonia as N 1400 mg/kg dry 10 2.6 1 *SM4500-NH3 C 7/17120 13:50 BMS POG0245 Nitrate/Nitrite as N BRL mglkg dry 5.2 1.4 1 *SM4500-NO3 F 7/20120 11:47 CLB POG0268 PH 6.6 HT pH Units 1 *904513 7115I20 12:40 CLB POG0209 Phosphorus -Total 13000 mglkg dry 520 210 100 *SM4500-P F 7121120 9:07 CLB POG0289 Temperature 22.0 HT °C 1 *SM2550 B 7/15/20 12:40 CLB POG0209 Total Kieldahl Nitrogen 4300 mglkg dry 1000 350 2 *351.2 7123120 10.50 CLB POG0433 Microbiological Parameters Fecal Coliforms 2500 MPNIg dry 0.2 1 *SM9221 E 7113120 14:30 BUIS P000178 TCLP Extraction by EPA 1311 TCLP Extraction Complete NIA 1 *1311 7116/20 7:50 EDV POG0210 TCLP Extraction Complete NIA 1 *1311 ZHE 7117120 8:04 TBL POG0234 TCLP Metals Mercury BRL mg1L 0.010 0.000034 1 *7470A 7/20/20 14:13 EDV POG0275 Arsenic BRL mglL 0.10 0.037 1 *60100 7/16120 16:41 JAB POG0223 Barium BRL mglL 5.0 0.0080 1 *6010D 7/16/20 16A1 JAB POG0223 Cadmium BRL mg1L 0.025 0.0020 1 *6010D 7/16/20 16A1 JAB POG0223 Chromium BRL mg1L 0.25 0.010 1 *6010D 7116/20 16:41 JAB POG0223 Lead BRL mg1L 0.050 0.012 1 *6010D 7116/20 16:41 JAB POG0223 Selenium BRL mg1L 0.15 0,050 1 *6010D 7/16120 16:41 JAB POG0223 Silver BRL mg1L 0.25 0.0035 1 '6010D 7116120 16:41 JAB POG0223 TCLP Organochlorine Pesticides by GCIECD Chlordane BRL, mg1L 0.0025 0.00090 1 *8081B 7/20120 9:40 NM5 POG0250 Dieidrin BRL mg1L 0.00050 0.000068 1 *8081B 7120120 9:40 NMB POG0250 Endrin BRL mg1L 0.00050 0.000068 1 *8081B 7120/20 9:40 NMB POG0250 gamma-BHC BRL mglL 0.00050 0.000030 1 *8081B 7120120 9:40 NMB POG0250 Heptachlor BRL mg1L 0.00050 0.000065 1 *8081B 7120120 9:40 NMB POG0250 Heptachlor Epoxide BRL mglL 0.00050 0.00011 1 *8081 B 7120120 9:40 NMB POG0250 Methexychlar BRL mglL C.00050 0.000090 1 *8081B 7/20/20 9:40 NMB POG0250 Toxaphene BRL mglL 0.025 0.0018 1 *80813 7120120 9:40 NMB POG0250 Surrogate Recovery Control Limits Decachlcrobiphenyl 68 % 13-186 Tetrachloro-m-xylene 65 % 40-134 TCLP Semivolatile Organic Compounds by GC/MS 2,4,5-Trichlorophernol BRL mg1L 0.25 0.0036 1 *8270E 7117/20 12:27 JMV P000231 2,4,6-Trichlorophenol BRL mg1L 0.10 0,0045 1 *827DE 7117l20 12:27 JMV P000231 2,4-Dinitrotoluene BRL mg1L 0.012 0.0042 1 "8270E 7117/20 12:27 JMV P000231 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical, 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364-Toll Free Number:l-8001529-6364- Fax: 7041525-0409 Page 4 of 17 GLaboratory Report Waypoint- 07/30/2020 ANALYTICAL Town of Mooresville/RR WWTP Project: Class A Dried Sludge Client Sample ID: Class A Attn: Whitney Munroe Sample ID: 0070145-01 P. O. Box 878 Work Order: 0070145 Mooresville, NC 28115 Sample Matrix: Solid Time Collected: 07/13/20 07:55 Time Submitted: 07/13/20 14:20 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DateMme ID 2-Methy[phenci BRL mg/L 0.050 0.0024 1 '8270E 7117/20 12:27 JMV POG0231 314-Methylphenoi BRL mg1L 0.050 D.D025 1 '8270E 7/17120 12:27 JMV ROG0231 Hexachlorobenzene BRL mglL 0.020 0.0039 1 '8270E 7117/20 12:27 JMV POG0231 Hexachlorobutadiene BRL mglL 0.050 0.0045 1 '827CE 7117120 12:27 JMV P060231 Hexachloroethane BRL mg/L 0.050 0.0037 1 '8270E 7/17/20 12:27 JMV P060231 Nitrobenzene BRL mg1L 0.050 0.0038 1 '8270E 7117120 12:27 JMV POG0231 Pentachlorophenol BRL mg1L 0.25 0.011 1 '8270E 7/17120 12:27 JMV POG0231 Pyridine BRL mg1L 0.25 0.0016 1 *8270E 7/17/20 12:27 JMV POG0231 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 71 % 43-140 2-Fluorobipheny[ 48 % 44-119 2-Fluorophenol 38 % 19-119 Mtroben7eneA5 45 % 44-120 Phenol-d5 28 % 11-52 Terphenyl-d14 56 % 50-134 TCLP Volatile Organic Compounds by GC/MS 1,1-Dichloreethylene BRL mg1L 0A35 0.00083 10 '8260D 7121120 15:07 JLB POG0328 12-Dichloroethane BRL mg1L 0.025 0.00065 10 *8260D 7/21120 15:07 JLB P0G0328 1,4-Dichlorobenzene BRL mg/L 0.38 0.00050 10 *8260D 7121/20 15:07 JLB POG0328 Benzene BRL mglL 0.025 0.00048 10 *8260D 7/21120 15:07 JLB POG0328 Carbon Tetrachloride BRL mglL 0.025 0,0011 10 *8260D 7/21/20 15:07 JLB POG0328 Chlorobenzene BRL mg1L 5.0 0,00062 10 '8260D 7121120 15:07 JLB POG0328 Carbon disulfide BRL mg1L 0.050 0.00075 10 *8260D 7/21120 15:07 JLB POG0328 Chloroform BRL mg1L 0,30 0.00076 10 '8260D 7/21120 15:C7 JLB POG0328 Methy[ Ethyl Ketone (2-Butanone) BRL mg1L 10 0.0024 10 *8260D 7121/20 15:07 JLB POG0328 Tetrachloroethylene BRL mg1L 0,035 0.OD098 10 '8260D 712112D 15:07 JLB POG0328 Trichloroethylene BRL mg]L 0,025 0.00078 10 *82601) 7121/20 15:07 JLB POG0328 Vinyl chioride BRL mg1L 0,020 0.00097 10 '8260D 7121/20 15:07 JLB POG0328 Surrogate Recovery Control Limits 4-B romofluorc benzene 100 % 80-124 Dibromofluoromethane 115 % 75-129 Toluene-d8 100 % 77-123 Total Metals Aluminum 150000 mglkg dry 5200 980 200 *6010D 7117120 16:15 JAB POG0241 Mercury 0.60 mgJkg dry 0.26 0.078 5 *7471B 7115120 14:13 ICP POG0196 SAR Soil Preparation Complete g 1 *2-78-054 7116/20 8:23 EDV POG0191 SAR Percent Moisture 64.1 % by 0.100 0.100 1 *2-78-054 7117120 9:23 EDV POG0229 Weight Arsenic 4.1 mgJkg dry 1.0 0.13 1 *6010D 7117/20 17:38 JAB P000241 Sodium Absorption Ratio 2.1 [blank] 0.30 0.016 1 *2-78-054 7/17120 9:29 JAB POG0228 Cadmium BRL mgJkg dry 0.62 0,049 1 *6010D 7117120 17:38 JAB POG0241 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 5 of 17 0 Laboratory Report Waypoint. 07/30/2020 ANALYTICAL Town of Mooresville/RR WWTP Project: Class A Dried Sludge Client Sample ID: Class A Attn: Whitney Munroe Sample ID: 0070145-01 P. O. Box 878 Work Order: 0070145 Mooresville, NC 28115 Sample Matrix: Solid Time Collected: 07/13/20 07:55 Time Submitted: 07/13/20 14:20 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DatelTime 0 Calcium 16000 mglkg dry 1000 Calcium, SAR 410 mg& 16 Copper 210 mg/kg dry 26 Lead 9.9 mglkg dry 1.0 Magnesium 2800 mglkg dry 260 Magnesium, SAR 150 mglL 1.0 Molybdenum 7.3 mg/kg dry 1.0 Nickel 14 mg/kg dry 1.0 Potassium 2600 mg/kg dry 100 Selenium 2.7 mglkg dry 1.0 Sodium 890 mglkg dry 100 Sodium, SAR 200 mg1L 5.0 Zinc 440 mg/kg dry 100 190 10 *6010D 7117120 16:22 JAB POG0241 0.10 10 *6010D 7117/20 9:29 JAB POG0228 15 10 *6010D 7/17120 16:22 JAB POG0241 0.12 1 *6010D 7117/20 17:38 JAB POG0241 27 10 *6010D 7117120 16:22 JAB POG0241 0.086 10 *6010D 7/17/20 9:29 JAB POG0228 0.11 1 *6010D 7117120 17:38 JAB POG0241 0.40 1 *6010D 7117120 17:38 JAB POG0241 23 1 *6010D 7117120 17:38 JAB POG0241 0.19 1 *6010D 7117120 17:38 JAB POG0241 16 1 *6010D 7117/20 17:38 JAB POG0241 0.18 10 *6010D 71l7120 9:29 JAB P000228 12 10 *6010D 7117120 16:22 JAB POG0241 This report should not be reproduced, except in its entirety, without the written consent of Waypoi nt Analytical . 449 Springbrook Road - P,o. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529.6364- Fax: 704/525-0409 Page 6 of 17 Sample Extraction Data Prep Method: 351.2 Lab Number Batch Initial Final DatefTime 0070145-01 POG0433 0,05 g 25 mL 07/22/20 12:46 Prep Method: SM4500-NH3 B Lab Number Batch Initial Final Date/Time 0070145-01 POG0245 1 g 50 mL 07/17/20 9:55 Prep Method: SM4500-PBS Lab Number Batch Initial Final Datefrime 0070145-01 POG0289 1 g 50 mL 07/20/20 14:45 Prep Method: 1311 Lab Number Batch Initial Final Date/Time 0070145-01 POG0234 12.5 g 250 mL 07/16/20 12:59 0070145-01 POG0210 100 g 2000 mL 07/15/20 15:40 Prep Method: 3010A Lab Number Batch Initial Final Datemme 0070145-01 POG0223 10 mL 50 mL 07/16/20 10:04 Prep Method: 7470A Lab Number Batch Initial Final Date/Time 0070145-01 P0G0275 20 mL 30 mL 07120120 9:17 Prep Method: 3510C GC Lab Number Batch Initial Final Datelrme 0070145-01 POG0250 200 mL 10 mL 07/17/20 10:50 Prep Method: 3510C MS Lab Number Batch Initial Final Date/Time 0070145-01 POG0231 200 mL 1 mL 07/16/20 12:10 Prep Method: 5030B Lab Number Batch Initial Final Date/Time 0070145-01 POG0328 10 mL 10 mL 07/21/20 10:00 Prep Method: 3010A Lab Number Batch Initial Final Date/Time 0070145-01 POG0228 50 mL 50 mL 07116/20 8:23 0070145-01 POG0228 50 mL 50 mL 07116120 8:23 Prep Method: 3050B Lab Number Batch Initial Final Datefrime OC70145-01 POG0241 2 g 50 mL 07/17/20 8:03 0070145-01 POG0241 2 g 50 mL 07/17/20 8:03 0070145-01 POG0241 2 g 50 mL 07/17/20 8:03 Prep Method: 7471B Lab Number Batch Initial Final Date/Time This report should not be reproduced, except in its entirety, without the written consent of WaypointAnalrical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/629-6364 - Toll Free Number: 1-8001529.6364- Fax: 704/525-0409 Page 7 of 17 Sample Extraction Data Prep Method: 7471B Lab Humber Batch Initial Final Date/Time 0070145-01 POG0196 0.6 g 50 mL 07/15/20 9:57 Prep Method: SAR 2-78-054 Lab Number Batch Initial Final Daterrime 007CI45-01 POG0191 250 g 250 g 07/15/20 8:23 Subcontracted Analyses The following analyses were subcontracted to Waypoint Analytical Lab Number Analysis 0070145-01 Herbicides TCLP (Sub) Thfs reporl should not be reproduced, except in its entirety, without the written consent of Waypoint Analyt[cal. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525.0409 Page 8of17 i 4x, V WaY- oint- ANALYTICAL 449 Springbrook Road • Charlofte, NC 21217 Rhone 7041529-6364 - Fax: 7041325.0409 Client Company Name: owls uri Report 7o1Contact Name: V4KM- Reporting Address: o D u►LLt . CHAIN OF CUSTODY RECORD PAGE l OF ga-L QU//O��TE�� l# TOENSURE PROPER BILLING:.- Project Name: ias 4 -.ires Sl Short Hold Analysis i" (No) UST Protect: (Yes) (V "Please ATTACH any p ct specific reporting (QC LEVE II III IV) provisions and/or QC Re uiremonts Invoice To: �vw a(,' %N W- +A-&,, _ _ Address: YES NO N1 r Samples INTACT upon arrival? Received ON WET ICE? f � 0 PROPER PRESERVATIVES indicated? % 0) Received WITHIN HOLDING TIMES? -� CUSTODY SEALS INTACT? VOLATILES ree'd WICUT HEADSPACE? PROPER CONTAINERS used? TEMP: Thermlo_„1iL CIS Observed ty `ClCorr.__�"C' _ Phone:-� -r-� le Fax (Yes)(No): Purchase Order No./Billing Reference Email Address: ffte YI wft%N16 Ae .4nJ Requested Due Date Q 1 Pay -J 2 Days ❑ 3 Days J 4 Days J 5 Days EDD Type: PDF ✓Excel —Other 'Working Days" ❑ 6r9 DaysStandard 10 daysusiWorit Must Be re ppravad Site Location Name: samples received after 14:00 will be processed next business day TO BE FILLEDIN BY CLIENTISAMPLING PERSONNEL Certlficatlon: NELAC FL NC__z SC- SC OTHER N!A Site Location Physical Address: Turnaround time Is based on business days, excluding weekends and holidays. (SEE REVERSE FOR TERMS 6 CONDITIONS REGARDING SERVICES RENDERED BY WAYPOINT ANALYTICAL, LLC TO CLIENT) I Water Chlorinated: YES_ ND t! Sample Iced upon Collection: YES -,NO-- CLIENT SAMPLE DESCRIPTION DATE COLLECTED TIME COLLECTED MILITARY HOURS MATRIX (SOIL, WATER, OR SLUDGE) SAMPLE CONTAINER PRESERVA- TIVES ANALYSIS REQUESTED � �y,� V . � REMARKS ���JJJ •1 fD NO, *TYPE SEE BELOWNO. SIZE ss - -7-o-xt d Z ,D 1 D i --� .. COPIES Sampler's Signature Sampled By (Print Name) foliation Upon relinquishing, this Chain of Custody Is your authorization for Waypolnt Analytical to proceed with the analyses as requested above. Any changes must be USE ONLY submitted in writing to the Waypoint Analytical Project Manager. There will be{ arges for any charWeafter analyses have been initialized. " ellnq L! Ely. (Sign re) p � Reeved By, (S,pna j / i [ D�ateq^� MlI laryrHoxa gddi#ional Comments: Site Arrlvai Time: L Relinquished By Ignalure) Recanted By: (S[9FsftDate Site Departure Time: Relinquished By (Signelure) ` Racebfea3 F " lyrical By: }Care` Field Tech Fee: Mileage. Men7od of Shipment NOTE: ALL SAMPLE COOLERS SHMILD BE TAPED s#iuT WffH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COG Group Na SAMPLES ARE NOTACCEPTED AND VERIFIED AGAINST CDC UNTIL RECEIVED ATTIRE LABORATORY. l/� I 1 �� S ❑ Fed Ex ❑ UPS UlHend-delhmred nt Analytical Feld Service ❑ 0iher _ _..-....___.._.__.__�. Q0 1 NPDES LIST: GROUN DRI NG ID FLD .❑ SC I ❑ I OTHER: XrNC ❑ SC ❑ NC ❑ SC ❑ NC ❑DSC TER ❑ NC'❑ SC WATER: El NLC ❑ SC NCN ❑ SC ❑ NC LANDFILL❑ SC NC ❑ SC • ©NC ❑ ❑ ❑ --O El ❑ O 'CONTAI► -R TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cr.. VOA = Volatile Organics Analysis (Zero Head Space) ' �I G INAL P R I S n n I Full -Service Analytical & f V � Environmental Solutions LASCMTORIEa, [NC 449 Springbrook Road • Charlotte, NC 28217 Phone 704/529-6364 • Fax: 7041525-0409 Client Company Name: 7d—K, Report To/Contact Name: Reporting Address: Phone: D- 1p Fax (Yes) (No): Email Address: WYY+4tylftc#Avp� ' tU!/�C, y EDD Type: PDFVExcel �Other— Site Location Name: Site Location Physical Address: CLIENT DATE SAMPLE DESCRIPTION I COLLECTED CHAINOF CUSTODY RECORD PAGE Onn��— OF QUOTE # TO ENSURE PROPER BILLING: Project Name: �_-Ar _b CIX O uJoe Short Hold Analysis: 1'e (No) UST Pr ject: (Yes) *Please ATTACH any project specific reporting (QC LEVE0I 1 III I provisions andlor QC Requirements Invoice To; Jib r 1LC Address: Samples INTACT upon arrival? Received ON WET ICE? PROPER PRESERVATIVES Indicated? Received WITHIN HOLDING TIMES? CUSTODY SEALS INTACT? VOLATILES redd W10UTHEADSPACE? PROPER CONTAINERS used? TEMP Therm lD: ifi.'f Observed YES NO NIA r Corr: Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL Requested Due Date ❑ 1 Day Ll 2 Days Q 3 Days U 4 Days U 5 Days Certification: NELAC DoD FL NC ✓ "Working Days" ❑ 6.9 Days>(.Standard 10 days ❑ Rush Work Must Be Pre -Approved Sc— OTHER NIA Samples received after 14:00 will ba processed next business day. Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES NOL-'� (SEE REVERSE FOR TERMS 3 CONDITIONS REGARDING SERVICES RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) Sample Iced Upon Collection: YES NO TIME MATRIX SAMPLE CONTAINER COLLECTEp � (SOIL, PRESERVA- MILITARY WATER OR `TYPE NO SIZE TIVES HOURS i SLUDGE) SEE BELOW 07" ANALYSIS REQUESTED PRISM �XREMARKS LAS ID NO. Sampler's Signature N ZlU )VV I Sampled By (PFint Name) / t.-1 M�r1 I A#tlliation �►14IN Upon relinquishing, this Chain of Custody is your authorization for Pris to proceed with the analyses as requested above. Any changes must be submitted in writing to the Prism Project Manager. There will be charge for any changes aft analyses have been initialized. RK5fl-u", y: ( ignEL rn Received By; lgnatura ale lltary can j y Additional comments: Relinquishes y: { a « } 1 +�1 JA SAMPLES ARE NOT ACC&TEDAND VERIFIED AGAINST COG UNTIL RECEIVED AT THE LABORATORY- ❑ Fed Ex 4 UAS fl Hand-detivered WPnsm Field Service 4 Othor NPjjES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: I RCRA: ❑ bdNCCISC NC ❑SC El NC El SC ❑NC ❑SC ❑NC ❑SC ❑NC❑SC *CONTAINER E CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap 0010,0 ❑ NC ❑ SC I ❑ NC ❑ SC I ❑ NC LJ SC ❑ ❑ ❑ = Volatile Organics Analysis (Zero Head Space) 1- tl Mol Pb111�ar f K, �I( 7-h I f'S Site Departure Time: I I Field Tech Fee: Mileage; t- .FINAL Waypoint(2) ANALYTICAL 7/23/2020 Waypoint Analytical Charlotte Ms. Terri Cole P.O. Box 240543 Charlotte, NC, 28224-0543 Ref: Analytical Testing Lab Report Number: 20-197-0064 Client Project Description: Subcontract # 0070145 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypoi nta nalytica Isom Dear Ms. Terri Cole: Waypoint Analytical, LLC. received sample(s) on 7/15/2020 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a'—' symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, - & kW141Z t Andrea R Brownfield Project manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 11 of 17 Page 1 of 7 Waypointo ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2021 Arizona State Program AZ0816 08/30/2020 Arkansas State Program 88-0650 02/07/2021 California State Program 2904 05/10/2020 Florida State Program - NELAP E871157 06/30/2021 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2020 Illinois State Program - NELAP 200078 10/10/2020 Kentucky State Program 80215 06/30/2021 Kentucky State Program KY90047 12/31/2020 Louisiana State Program - NELAP LA037 12/31/2020 Louisiana State Program - NELAP 04015 06/30/2021 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2020 Oklahoma State Program 9311 08/31 /2020 Pennsylvania State Program - NELAP 68-03195 05/31/2021 South Carolina State Program 84002 06/30/2021 South Carolina State Program 84002 06/30/2020 Tennessee State Program 02027 02/11/2023 Tennessee A21-A ISO 17025:2017 4313.01 10/31/2021 Texas State Program - NELAP T104704180 09/30/2020 Virginia State Program 00106 06/30/2021 Virginia State Program - NELAP 460181 09/14/2020 Washington State Program C1018 07/31/2020 Page 1 of 1 00q Page 12 of 17 Page 2 of 7 (2) z79D Whitten Road, Memphis, TN 38133 Waypoint, Main 901.213.2400 ° fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 20-197-0064 Client Project Description: Subcontract # 0070145 Lab No Client Sample ID Matrix Date Collected 89711 Class A Solid 07/13/2020 07:55 Date Received 07/15/2020 Page 3 of 7 Page 13 of 17 Waypointo ANALYTICAL Project Subcontract # 0070145 Information: Waypoint Analytical Charlotte Ms. Terri We P.O. Box 240543 Charlotte, NC 28224-0543 Report Number: 20-197-0064 Report Date: 7/23/2020 Sample Results Class A Date Collected 07/13/2020 07:55 WPA Lab No 89711 Date Received 07/15/2020 Matrix Solid 1311 Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch NA NA NA 1 7/16/2020 13:01:00 W L501614 CAS# Parameter TCLP Herbicide Extraction 8151A Result MQL Units Leachate Prep Date Prep Batch Prep Method Sample Dilution Analysis Date By Analytical Batch 07/20/2020 17:00 L502178 8151A 50 mL 1 7/22/2020 22:13:49 MCB L502646 CAS# Parameter Result MQL Units 94-75-7 TCLP 2,4-D ND 0.0200 mg/L 93-72-1 TCLP 2,4,5-TP (Silvex) ND 0.0020 mg/L CAS# Surrogate % Recovery Rec. Limits 19719-28-9 DCAA 48.20 20-120% Qualifiers/ MQL Method Quantitation Limit Definitions Page 4 of 7 Page 14 of 17 w • Waypoint. 2790 Whitten Road, Memphis, 3 Main 901.213.2400 °Fax 901.21213.24A.2440 ANALYTICAL www.waypointanalytical.com Quality Control Data Client ID: Waypoint Analytical Charlotte Project Description: Subcontract # 0070145 Report No: 20-197-0064 QC Prep: L502178 QC Analytical Batch(es): L502646 QC prep Batch Method: 8151A Analysis Method: 8151A Analysis Description: Phenoxy Acid Herbicides - GC/ECD (TCLP) Lab Reagent Blank LRB-LS02178 Matrix: TCL Associated Lab Samples: 89711 Blank MQL Analyzed % % Rec Parameter Units Result Recovery Limits TCLP 2,4-D mg/L < 0.0200 0.0200 07/22/20 20:31 TCLP 2,4,5-TP (Silvex) mg/L < 0.0020 0.0020 07/22/20 20:31 DCAA (S) 07/22/20 20:31 46.2 20-120 Laboratory Control Sample & LCSD LCS-1-502178 LCSD-L502178 Spike LCS LCSD LCS LCSD a/o Rec Parameter Units Conc. Result Result %Rec o/n Rec Limits RPD Max RPD TCLP 2,4-D mg/L 0.1000 0.0337 0.0501 33.7 50.1 20-120 39.1* 20.00 TCLP 2,4,5-TP (Silvex) mg/L 0.0100 0.0030 0.0046 30.0 46.0 20-120 42.1* 20.00 DCAA (S) 38.0 56.6 20-12C * QC Fail Date: 07/23/2020 03:53 PM Page 15 of 17 Page 5 of 7 • Waypoi nt H0 2790 Ma Whitten Road,3.240 Memphis, TN 39133 21.2440 Main 9d1.213.248D°Fax 901.213.2440 ANALYTICAL www.waypointanalytica1.com Shipment Receipt Form Customer Number: 25657 Customer Name: Waypoint Analytical Charlotte Report Number: 20-197-0064 Shipping Method 40 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: 99 Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers/boxes received F 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No 0 Not Present Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No 0 NIA Water - VOA vials free of headspace 0 Yes 0 No 0 NIA Trip Blanks received with VOAs 0 Yes 0 No 0 NIA Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 NIA High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr) High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes 0 No Comments: Signature: ory Phillips Date & Time: 7/15/2020 10:47:26 Page 16 of t 7 Page 6 of 7 Waypoint ANALYTICAL St BCOM I R %C T QiiDER Certification: NE LAC' E)5 AC'1: 11 a lanir�E :�rr<ti� tical a;(• N, St Other 0070145 N/A — SENDING 11ABORATOR) t RUTAVIM, i,AHt1RATORY: 'A'aypoint Anaklical W;npoint Analyfical P. 0, Box 240543 2790 Whilml Roinl Charlotte, NC 28?24-11543 klemphis.'M 38133 Phone: 800-529-6364 ],])one :((H)1) ? I;-2.100 Fux: 704-525-0409 Fax: 001) 213-2440 Project 41anagcr. Terri 11. Cole AuRI)sis Dw Expires Luhorntar+ Il) C•ommenlr SamptclU: 00711L45_01 Solid "Amplyd: U7f10 3120';55 lu% A Heihiodcs TC1.P (Sub( (17+27121i n7 5i C oa(auters tiuppleed- c} (61 Fe de Released R Rcicased Be Rcleaxd I{s fi7M IN m J111FIN11r11r1rrr z�77-OG64 WiNmu tAnafvncaf Charloffe 07-15-2020 Suboonrract # 0070145 104623 i Received By Receil'Ci11;+' f Recei Rec mal Page 7 of 7 tklte Ikac VA rage 1 +tr I Page 17 of 17 0 Waypoint. ANALYTICAL Town of Mooresville/RR WWTP Whitney Munroe P. O. Box 878 Mooresville, NC 28115 NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Project: Class A Dried Sludge Lab Submittal Date: 08/10/2020 Work Order: 0080131 Case Narrative 8/ 18/20 11:33 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, WAYPOfNTANALYTICAL (o 665-') Terri W. Cole Project Manager Data Qualifiers Key Reference: BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Spring brook Road - P.C. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: [-8001529-6364- Fax: 7041525-0409 Page 1 of 5 0 Waypointd ANALYTICAL Sample Receipt Summary 08/18/2020 Work Order: 0080131 Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received Class 0080131-01 Solid 08/10/20 8:37 08/10/20 12:30 Samples were received at 13.2 degrees C. See case narrative for further information. This report should not be reproduced, except in its entirety, without the written consent of Waypolnt Analytical. 449 Spring brook Road - P.O. Box 240W - Charlotte, NC 28224-0543 Phone: 7041529-6364 -Toll Free Number: 1-8001529-6364 - Fax: 704/525.0409 Page 2 of 5 • 0 Waypoi nt- ANALYTICAL Town of Mooresville/RR WWTP Attn: Whitney Munroe P. O- Box 878 Mooresville, NC 28115 Project: Class A dried Sludge Sample Matrix: Solid Laboratory Report 08/18/2020 Client Sample ID: Class A Sample ID: 0080131-01 Work Order: 0080131 Time Collected: 08/10/20 08:37 Time Submitted: 08/10/20 12:30 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Datefrime ID General Chemistry Parameters % solids 95.1 % by 0.100 0A00 1 `SM2540 G 8/17120 11:30 EDV POH0199 Weight Microbiological Parameters Fecal Coliforms 3 MPNIg dry 0.2 1 'SM9221 E 8110120 13:30 BMS P01-10125 This reportshould not be reproduced, except in its entirety, without the written consent of Waypoint Analytical . 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364-Toll FreeNumber: 1-8001529-6364-Fax; 7041525-0409 Page 3 of 5 Prep Method: Solids, Dry Weight Lab Number Batch India[ 0080131-01 POH0199 30 g Sample Extraction Data Final DatelTime 30 g 08/14/20 12:01 This report should not be reproduced, except in its entirety, without the written consent of WaypointAnalytical. 449 Spring brook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 4 of 5 0 Waypoint. ANALYTICAL 449 Spri 7tgrook Road • Charlotte, NC 21217 Phone 7041529-6354 • Fax:7041525-0409 Client Company Name: 7rs lli JI awm� I Report To/Contact Name:- IA 1V ��+�� (M - Reporting Address: 0 Rhnna-+iil`I rrH/ii�;9 ♦Z/_ r _�r.i_r. CHAIN OF CUSTODY RECORD PAGE. ).OF gUOTE k TpENSURE PROPER BILLING: - _ -- Project Name: _ -._ "Sd . +' _... ,. Short Hold Analysis es (Not UST -. Project;_ a— (1(es) NO *Please ATTACH any p specific reporting (QC LEVg1 1 III provisions andlor QC Requirements Invoice To: Dtxt�►��e Address: YES NO NIA Samples INTACT upon arrival? Received ON WET ICE? PROPER PRESERVATIVES Indicated? VVV Received WITHIN HOLDING TIMES? — I CUSTODY SEALS INTACT? C VOLATILES rec'd WfOUT HEADSPACE? _ — I PROPER CONTAINERS used TEMP' Therm lD _IS, Observed_t_- �, ' 1Canrj : C """"' , -' == max t'Cs1t""r' --- Purchase Order No./Billing Reference_ __ ..,_-_. __ m--. .... - Email Address: Ww,l�Anf '�vxooriCf,�i1ik Requested Due Dale J 1 Day J 2 Days J 3 Days J 4 Days Oa' EDl] Type: PDF ✓Excel_Other� Rush Work Must Be ---- "Working Days" > 6-9 Days J Standard 10 days -I Pre Approved Site Location Name: Samples recinved after 14:00 will be processed next business day. TO BE FILLED IN BY CLIENT/SAMPLING iPEf3,SONNEL Certification: NitLACFL,-_ INC r/ - SC--- — OTHER NIA Site Location Physical Address: Turnaround time is based on business days, excluding weekends and holidays. (SEE REVERSE FOR rmms 6 CONDITIONS REGARDING SERVICES _— RENDERED BY WAYPOtNT ANALYTICAL. LLC TO CLIENT) Water Chlorinated: YES _ NO Sample Iced Upon Collection: YES- `NO _. CLIENT SAMPLE DESCRIPTION - DATE COLLECTED S 16 TIME MATRIX COLLECTED I (SOIL, MILITARY WATER, OR HOURS SLUDGE) !!ry y.-- ..I--- 0 3 'SPA �- SAMPLE CONTAINER _ `TYPE I NO, SIZE SEE BELOW PRESERVA- TIVE S _ t�C ANALYSIS REQUESTED Aft REMARKS ID NO. `S �1 — i I Samplers Signature _. J'✓'�L_ Sampled By (Print Name),,. I" �! f�? _T! Affiliation Th s w Upon relinquishing, this Chain of Custody is your authorization for Waypoint Analytical to proceed with the analyses as requested above. Any changes must be submitted in writing to the Waypoint Analytical Project Manager. T re wilt be charges for any changes after analyses have been init€alized, inquished BY: (signatur) Re By:sl�nature) -- Mflitaryrtiours Additional Comments: Site Arrival Time; R Date Site Departure Time; F2e shed sy: {Signalu r - _ RecniUact Far Wnypars3 Anaiyta al By. -- Date Field Tech Fee: Mileage: -- M14alhod at Shipnent, NOTE: ALL SAMPLE COOLERS SHOUr� HE TAPED SHUT WITH CUSTODY SEALS FOR TRANS RTATION Td THE LABORATORY. � COC Group No. SAMPLES ARE NO CCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LAB TORY. J Fed Ex .d UPS J HandEelrvered ypoirtt Analytical Field Service :J Other._,. UU 3 NPD S: LIST NG .THER-- 11190AMMI . J NC J SC I J NC J SC -1 C J SC TER.I J NCKir] SC A7ER: NLCD -SC >=. I J NC -1 SC 1 J NCN JLSC JAN LANDFILL SC I O NC J Sc *CONTAINER TYPE CODES: A = Amber C - Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) Page 5 of 5 NC Certification No. 402 Case Narrative Waypoint- NC Drinking Water Cert No. 37735 10/29/20 11:37 ANALYTICAL SC Certification No. 99012 Town of Mooresville/RR WWTP Whitney Munroe P. O. Box 878 Mooresville, NC 28115 Project: Class A Dried Sludge Lab Submittal Date: 10/19/2020 Work Order: 0100266 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Narrative Notes: Analysis note for SAR: SAR = [ Na ] 1 SQRT ( ( [Ca] + [Mg] ) 12 SAR = [ 150123 ] 1 SQRT { ( [270/20] + [72/12.21 ) / 2 } SAR = 2.1 Concentrations for Na, Ca, and Mg are expressed in mill iequivalents per Liter, and SQRT designates taking the square root of the operand in parentheses. PAN Equation = 0.3 * (TKN — Ammonia) + 0.5 * (Ammonia) + Nitrate —Nitrite PAN = 0.3 * (66000 — 1400) + 0.5 * (1400) + 2.55 PAN = 20000 M9/k9 Equation uses Mineralization Rate (MR) for Aerobically Digested Solids (0.3) TCLP Herbicides, TCLP Semi-volatiles, TCLP Pesticides analysis was subcontracted to Waypoint Memphis. Laboratory report is attached. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.D. Box 240543 - Charlotte, NC 2U24-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 22 Please call if you have any questions relating to this analytical report. Respectfully, WAYPOINT ANALYTICAL , 3 66�L 'q/�O Terri W. Cole Project Manager Data Qualifiers Key Reference: A Sample difficult to homogenize; this might be the reason for the low recovery. HT Sample received and analyzed outside of the hold time. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of WaypointAnalytical. 449 5pringbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 -Toll Free Number: 1-8001529.6364 - Fax: 7041525-0409 Page 2 of 22 Waypoint,Q) ANALYTICAL Sample Receipt Summary 10/29/2020 Work Order: 0100266 Client Sample ID Lab Sample ID Matrix DatelTime Sampled Date/Time Received Class A 0100266-01 Solid 10/19/20 9:52 10/19/20 13:30 Samples were received at 11.2 degrees C. See case narrative for further information. This report should not be reproduced, except in its entirety, without the written consent of WaypointAnalytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 26224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 3 of 22 • 0 Waypoint_ ANALYTICAL Town of Mooresville/RR WWTP Attu: Whitney Munroe P. O. Box 878 Mooresville, INC 28115 Project: Class A Dried Sludge Sample Matrix: Solid Laboratory Report 10/29/2020 CiientSamplelD: ClassA Sample ID: 0100266-01 Work Order: 0100266 Time Collected: 10/19/20 09:52 Time Submitted: 10/19/20 13.30 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time 1D General Chemistry Parameters Plant Available Nitrogen 20o00 mglkg dry 15000 5300 100 `Calculation 10/27/20 11:57 CLB iCAl % Solids 97.1 % by 0.100 0.100 1 *SM2540 G 10/21120 14:02 JAB POJ0382 Weight Ammonia as N 1400 mglkg dry 9.0 2.3 1 *SM4500-NH3 C 10127/20 10:50 BMS POJ0489 Nitrate/Nitrite as N BRL mglkg dry 5.1 1.4 1 'SM4500-NO3 F 10/23/20 11:55 CLB POJ0440 pH 6.2 pH Units 1 *90451) 10/21/20 12:20 CLB POJ0375 Phosphorus -Total 9600 mglkg dry 510 210 100 *SM4500-P F 10/23/20 8:10 CLB POJ0426 Temperature 20.9 HT °C 1 *SM2550 B 10/21/20 12:20 CLB POJ0375 Total Kleldahl Nitrogen 66000 A ni dry 51000 18000 100 *351.2 10/27/20 11:57 CLB POJ0476 Microbiological Parameters Fecal Coliforms 25 MPNIg dry 0.2 1 *SM9221 E 10/19/20 13:20 BMS POJ0371 TCLP Extraction by EPA 1311 TCLP Extraction Complete N/A 1 *1311 ZHE 10122/20 7:00 TBL POJ0383 TCLP Extraction Complete NIA 1 *1311 10122/20 7;15 EDV POJ0404 TCLP Metals Mercury BRL m9i 0.010 0.000034 1 '7470A 10126/20 13:18 EDV POJ0473 Arsenic BRL mg1L 0.10 0.037 1 '6010D 10/23120 15:30 JAB POJ0429 Barium BRL mglL 5.0 0.0080 1 '6010D 10/23/20 15:30 JAB POJ0429 Cadmium BRL mglL 0.025 0.0020 1 *601OD 1CI23/20 15:30 JAB PDJ0429 Chromium BRL mg1L 0.25 0.010 1 '6010D 10/23/20 15:30 JAB POJ0429 Lead BRL mg1L 0.050 0.012 1 *6010D 10123/20 15:30 JAB POJ0429 Selenium BRL mglL 0.15 0.050 1 *6010D 10/23/20 15:30 JAB POJ0429 Silver BRL mg1L 0.25 0.0035 1 *6010D 10/23/20 15:30 JAB POJ0429 TCLP Volatile Organic Compounds by GC/MS 1,1-Dichloroethylene BRL mg1L 0,035 0.00083 10 *8260D 10/23/20 20:05 JLB POJ0459 1,2-Dichloroethane BRL mglL 0.025 0.00066 10 *8260D 10/23/20 20:05 JLB POJ0459 1,4-Dich lorc benzene BRL mglL 0.38 0.00050 10 *8260D 10/23/20 20:05 JLB PDJ0459 Benzene BRL mglL 0.025 0.00048 10 '8260D 10/23/20 20:06 JLB PDJ0459 Carbon Tetrachloride BRL mg1L 0.025 0,0011 10 *8260D 10/23/20 20:05 JLB POJ0459 Chlorobenzene BRL mg1L 5.0 0.00062 10 '8260D 10123/20 20:05 JLB POJ0459 Carbon disulfide BRL mglL 0.050 0.00075 10 '8260D 10/23/20 20:05 JLB POJ0459 Chloroform BRL mglL 0.30 0.00076 10 '8260D 10/23120 20:05 JLB POJ0459 Methyl Ethyl Ketone (2-Butanone) BRL mg1L 10 0.0024 10 *8260D 10/23/20 20:05 JLB POJ0459 Tetrachlaroethylene BRL mglL 0.035 0.00098 10 *8260D 10/23/20 20:05 JLB POJ0459 Trichloroethylene BRL mglL D.025 0.00078 10 '8260D 10/23/20 20:05 JLB PDJ0459 Vinyl chloride BRL mglL 0.020 0.00097 10 '5260D 10/23/20 20:05 JLB PDJ0459 Surrogate Recovery Control Limits 4-BrOmofluorcbenzene 102 % 80-124 Dibromofluoromethare 111 % 75-129 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone:7041529-6364-Tall Free Number: l-8001529-6364- Fax: 704/525-0409 Page 4 of 22 0 Laboratory Report Wayp of nt- 1012912020 ANALYTICAL Town of Mooresville/RR WWTP Project: Class A Dried Sludge Client Sample ID: Class A Attn: Whitney Munroe Sample ID: 0100266-01 P. O. Box 878 Work Order: 0100266 Mooresville, IBC 28115 Sample Matrix: Solid Time Collected: 10/19/20 09:52 Time Submitted: 10/19/20 13:30 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DatelTime ID Toluene-d8 100 % 77-123 Total Metals Aluminum 31000 mglkg dry 510 97 20 Mercury 0.48 mglkg dry 0.051 0,015 1 SAR Soil Preparation Complete g 1 SAR Percent Moisture 71.9 % by 0.100 0.100 1 Weight Arsenic 5.0 mglkg dry 1.0 0.13 1 Sodium Absorption Ratio 2.1 (blank] 1.0 0.016 1 Cadmium 0.57 mglkg dry 0.51 0.048 1 Calcium 15000 mglkg dry 2100 380 20 Calcium, SAR 270 mg1L 5.0 0.050 5 Copper 240 mglkg dry 51 29 20 Lead 12 mglkg dry 1.0 0.12 1 Magnesium 2300 mglkg dry 26 2.6 1 Magnesium, SAR 72 mg1L 0.50 0.043 5 Molybdenum 7.2 mglkg dry 1.0 0.11 1 Nickel 13 mglkg dry 1.0 0.40 i Potassium 2800 mglkg dry 100 22 1 Selenium 2.1 mglkg dry 1.0 0.18 1 Sodium 950 mglkg dry 100 16 1 Sodium, SAR 150 mg1L 2.5 0.090 5 Zinc 530 mglkg dry 210 23 20 *6010D 10/21120 16:18 JAB POJ0380 *7471 B 10/22/20 15:12 EDV POJ0417 '2-78-054 10/23/20 10:04 EDV POJ0413 *2-78-054 10/26/20 7:50 EDV POJ0451 *6010D 10/21/20 15:34 JAB POJ0380 *2-7M54 10123120 16:21 JAB PGJ0447 *60101) 10/21/20 15:34 JAB POJ03BO *6010D 10/21/20 16:18 JAB POJ0380 *6010D 10/23/20 16:21 JAB POJ0447 *601013 10121/20 16:18 JAB PGJ0380 *6010D 10/21120 15:34 JAB POJ0380 *6010D 10/21/20 15:34 JAB PDJ0380 *6010D 10123/20 16:21 JAB POJ0447 *6010D 10121120 15:34 JAB POJ0380 *6010D 10/21/20 15:34 JAB POJ0380 *601010 10/21/20 15:34 JAB POJ0380 *6010D 10/21/20 15:34 JAB POJ0380 *6010D 10/21/20 15:34 JAB POJ0380 *6010D 10/23/20 16:21 JAB POJ0447 *6010D 10/21/20 16:18 JAB POJ0380 This report shouId not be reproduced, except in its entirety, without the written consent of WaypointAna lyticaI 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free N um be r: 1-8001529-6364 - Fax: 7041525-0409 Page 5 of 22 Sample Extraction Data Prep Method: 351.2 Lab Number Batch Initial Final Daterrime 0100266-01 POJ0476 0.05 g 25 mL 10/26120 13:28 Prep Method: SM4500-NH3 B Lab Number Batch Initial Final Daterrime 0100266-01 POJ0489 1.14 g 50 mL 10/27/20 7:52 Prep Method: SM4500-PBS Lab Number Batch Initial Final DatefTime 0100266-01 POJ0425 1 g 50 mL 10/22/20 13:46 Prep Method: Solids, Dry Weight Lab Number Batch Initial Final Datelrime 0100266-01 POJ0382 30 g 30 g 10/21/20 9:C2 Prep Method: 1311 Lab Number Batch Initial Final DatefTime 0100266-01 POJ0383 12.5 g 250 mL 10/2/120 12:22 0100266-01 POJ0404 10C g 2000 mL 10/21/20 15:12 Prep Method: 3010A Lab Number Batch Initial Final Datefrime 0100266.01 POJ0429 10 mL 50 mL 10/22/20 11:51 Prep Method: 7470A Lab Number Batch Initial Final DatelTime 0100266-01 POJ0473 20 mL 30 mL 10/26120 8:07 Prep Method: 5030B Lab Number Batch Initial Final DateMme 0100266-01 POJ0459 10 mL 10 mL 10/23/20 10:00 Prep Method: 3010A Lab Number Batch Initial Final Date/Time 0100266-01 POJ0447 50 ml_ 50 mL 10/23/20 10:04 0100266-01 POJ0447 50 mL 50 mL 10/23/20 10:04 Prep Method: 3050E Lab Number Batch Initial Final DatefFime 0100266-01 POJ0380 2 g 50 mL 10/21/20 828 D100266-01 POJ0380 2 g 50 mL 10121/20 8:38 Prep Method: 7471E Lab Number Batch Initial Final DatefTime 0100266-01 POJ0417 0.6 g 50 mL 10122120 11:25 Prep Method: SAR 2-78-054 Lab Number Batch Initial Final DaterrIme 0100266-01 POJ0413 250 g 260 g 10122/20 10:04 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical, 449 Springbrook Road - P.0, Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 6 of 22 Subcontracted Analyses The following analyses were subcontracted to Waypoint Analytical Lab Number Analysis 0100266-01 8091 TCLP 0100266-01 8M TCLP D100266-01 Herbicides TCLP (Sub) This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 L Page 7 of 22 0 Waypoint.. ANALYTICAL 449 Springbrook Road: Charlotte, NC 21217 Phone 704/529.63134 Fax: 704/525.0409 Client Company Name: oF- o Report To/contact Name: I Reporting Address: 0 o $ - Phone-.a+:'O_ JD- —5 A$ �y Fax (Yes)(No): Email Address: W rp _ i1�14n-a�OJ EDD Type: PbF� Excel Other Site Location Name: Site Location Physical Address: TIME MATRIX CLIENT DATE COLLECTED (SOIL, SAMPLE DESCRIPTION COLLECTED MILITARY WATER, OR HOURS SLUDGE) CHAIN OF CUSTODY RECORD PAGE J OF -,Q-QUOTE # TOENSURE PROPER {BILLING: Project Name: ' C ass A- ltt ,, Short Hold Analysis es (No) UST Proje t- (Yes) , &03 `Please ATTACH any pro ect specific reporting (qC LEVE©II III IV) provisions and/or QC Requirements Invoice To: tin p MDVeX Address: YES NO NIA Samples INTACT upon arrival? x Received ON WET ICE?. PROPER PRESERVATIVES indicated? Received WITHIN HOLDING TIMES? CUSTODY SEALS INTACT? ?C VOLATILES reed WIOUT HEADSPACE? PROPER CONTAINERS used? X TEMP: Therm 1D. - f' Observed _ C /Corr.-J1.'L°l Purchase Order No./Billing Reference TO BE' FILLEOIN BY CLIENTISAMPILING P�R�SONNEL Requested Due Date ❑ 1 Day ❑ 2 D ys ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC FL NC "Working Days" Q 6-9 Days Standard 10 days q'Rush Work Must. Be ' Samples received after 14:00 will 6e processed next business day, Pre Approved SC OTHER NIA Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES— NO (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES RENDERED BY WAYPOINT ANALYTICAL, LLC TO CLIENTI Sample lead Upon Collection., YES V MO� SAMPLE CONTAINER ANALYSIS PgQUESTED 'TYPE IN SIZE PRTIVESVA /�► �b l� x / REMARKS ID NO. SEE BELOW hhh Samplers Signaturee I Sampled By (Print Name)-f1l^r..► nA [ t,� J Affiliation �tM/,/ Upon relinquishing, this Chai ustody is your authorization for Waypoint Analytical to proceed with the analyses as requested above. Any changes must be 'submitted in writing to the Waypoint Analytical Project Manager. There will be charges far any changes after analyses have been initialized. Relinquished By: Signature) Received B nalarey Dale . MililarylHours Ads !d Za 13 Z, Rel By: (Signet Ref6hred By: (Signature) p Reli ed By: Signature) R etl Far Waypoint Anelyliral By Dale ��� Method o Shipment: NOTE: ALL SAMPLE COOLERS SHOULD aE TAPEp SHUT WfFH CUSTOD B SF' TRANSPORTATION TO THE LABORATORY. C up No. - _"- SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RE ED AT THE LABORATORY. /t ❑ Fed Ex OURS ❑ Hand -delivered ws inlAnalybcal Field Service OOther - (+/ ❑ NC ❑ SC 1 ❑ NC ❑ SG I ❑ NC q SC ❑ NC ❑ SC NC Q SC ❑a NC ❑ SC f Ll NC ❑ SC NC ❑ SC o❑ Nc ❑ sc ❑ ❑ ❑ ❑ "CONTAINER TYPE CODES: A =Amber C = Clear G= Glass P = Plastic; TL TTeflon-Lined Cap VOA -Volatile Organics Analysis (Zero Head Space) 0 Comments: Site Arrival Time: Site Departure Time: Field Tech Fee: Mileage. SEE REVERSE FOR TERMS & CONDITIONS Page 8 of 22 Waypoint-0 ANALYTICAL 449 Springbrook Road i Charlotte, NC 21217 Phone 7041529-6904 • Fax:7041525-0409 Client Company Na: OW Qrl�� Report To/Contact N�ame: l�t+ niK1Reporting Address.n . oactsAt afst .47' Phone: 401-10 0 320P Fax (Yes)(No). Email Address: Itavltltt�t.Qllnbplt6vi41� M . e e1/ EDD Type: PDF-ZExcel,Other Site Location Name: Site Location Physical Address: _ CLIENT OATS SAMPLE DESCRIPTION COLLECTED to -19- Sampler's Signature Upon relinquishing, this Chain o Cu submitted in writing to the Waypoint CHAIN} OF CUSTODY RECORD PAGE � OF QUOTE fl TO ENSURE PROPER BILLING: Project Name: �A" lad .St b Short Hold Analysis Tre j (No) UST Project: (Yes) *Please ATTACH any project specific reporting (QC LEVEOI III IV) provisions and/or QC Requirements Invoice To: d� Ofr�t Address: Samples INTACT upon arrival? Received ON WET ICE? PROPER PRESERVATIVES indicated? Received WITHIN HOLDING TIMES? CUSTODY SEALS INTACT? VOLATILES reed WIOUT HEADSPACE? PROPER CONTAINE used? TEMP: Therm ID: IQ TT-k Observe( YES NO NIA Purchase Order No.lBiliing Reference TO BE FILLEDIN BY CLIENTISAMPLING PERSONNEL Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days Q 4 Days u 5 Days Certification: NELAC FL --NC P"" "Working bays" ❑ 6-9 Day tandard 10.days ❑ Rush Work Must Be Pre Approved SC OTHER NIA_ Samples received after 14:00 will a processed next business day. Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES NO (SEE REVERSE FOR TERMS $ CONnITIONS REGARDING SERVICES RENDERED BY WAYPOINT ANALYTICAL, LLC TO CLIENT) Sample Iced Upon Collection; YES�O TIME MATRIX SAMPLE CONTAINER COLLECTED (SOIL, PRESERVA- MELETARY WATER, OR `TYPE Na SIZE TIVES H011RS SLUDGE) SEE BELOW :5,;;t,I 4n- ANALYSIS REQUESTED tt==t Sampled By (Print Name) I—ta� i nclre .r�_ I Affiliation 112KA," is your authorization for Waypoint Analytical to proceed with the analyses as requested above. Any changes must be tical Project Manager. There will he charges for any changes after analyses have been initialized. SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECQJEO AT THE LABORATORY. ❑ Fed Ex ❑ UPS Q Hand -delivered REMARKS 1 Ib NO. Additional Comments: ❑NC❑SC ❑NC ❑SC IggNC ❑5C I LING qSC IaNC ❑SC LING I❑SC ONC ❑SC O❑NG ❑SC ONG ❑SC I~ ti q } "CONTAINER TYPE CODES: A =Amber C =Clear G=Glass P plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero }lead Space) C 61 7- It Site Arrival Time. - Site Departure Time: Field Tech Fee: Mileage: Page 9 of 22 (2) Waypoint ANALYTICAL 10/28/2020 Waypoint Analytical Charlotte Ms. Terri Cole P.O. Box 240543 Charlotte, NC, 28224-0543 Ref: Analytical Testing Lab Report Number: 20-295-0162 Client Project Description: 0100266 2790 Whitten Road, Memphis, TN 39133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanaiytical.com Dear Ms. Terri Cole: Waypoint Analytical, LLC. received sample(s) on 10/21/2020 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a'--' symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report ofAnalysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, J�& kwi4j' Andrea R Brownfield Project manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 10 of 22 Page 1 of 13 • Waypoint. 27090 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2021 Arkansas State Program 88-0650 02/07/2021 California State Program 2904 06/30/2021 Florida State Program - NELAP E871157 06/30/2021 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2021 Illinois State Program - NELAP 200078 10/10/2021 Kentucky State Program 80215 06/30/2021 Kentucky State Program KY90047 12/31/2020 Louisiana State Program - NELAP LA037 12/31/2020 Louisiana State Program - NELAP 04015 06/30/2021 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2020 Oklahoma State Program 9311 08/31 /2021 Pennsylvania State Program - NELAP 68-03195 05/31 /2021 South Carolina State Program 84002 06/30/2021 South Carolina State Program 84002 06/30/2021 Tennessee State Program 02027 02/11/2023 Tennessee A21-A ISO 17025:2017 4313.01 10/31/2021 Texas State Program - NELAP T104704180 09/30/2021 Virginia State Program 00106 06/30/2021 Virginia State Program - NELAP 460181 09/14/2021 Page 1 of 1 Page 2 of 13 00Page 11 of 22 (2) 2790 Whitten Road, Memphis, TN 38133 Waypoint, Main 901.213.2400 ° Fax 901.213.2440 ANALYTICAL www.waypointanalocal.com Sample Summary Table Report Number: 20-295-0162 Client Project Description: 0100266 Lab No Client Sample ID Matrix Date Collected Date Received 92447 Class A Solid 10/19/2020 09:52 10/21/2020 Page 12 of 22 Page 3 of 13 Waypdlont(z) ANALYTICAL Client: Waypoint Analytical Charlotte Project: 0100266 Lab Report Number: 20-295-0162 Date: 10/28/2020 2790 Whitten (toad, Memphis, TN 38133 Main 902.213.2400 0 Fax 902,213.2440 www.waypointanalytical.com CASE NARRATIVE Semivolatile Organic Compounds - GC1MS (TCLP) Method 8270D Sample 92447 (Class A) QC Batch No: L518998/L518753 Surrogate(s) were flagged for recoveries in the associated project sample. During the extraction step, the extraction technician noted that a significant emulsion formed. Batch QC samples (Method Blank and Laboratory Control Samples) all showed surrogate recoveries within QC limits, indicating that the biased recoveries were due to the sample matrix. Page 13 of 22 Page 4 of 13 Waypdlont,(2) ANALYTICAL 25657 Waypoint Analytical Charlotte Ms. Terri Cale Project 0100266 P.O. Box 240543 Information Charlotte , NC 28224-0543 Report Number: 20-295-0162 2790 Whitten Road, Memphis, TIC 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com REPORT OFANALYSIS Report Date : 10/28/2020 Received : 10/21/2020 Lab No : 92447 Sample ID : Class A Matrix: Solid Sampled: 10/19/2020 9:52 Analytical Method: 1311 Test Results Units MQL DF Date I Time By Analytical Analyzed Batch TCLP Herbicide Extraction Leachate 1 10/22/20 14:30 PHE L518149 TCLP Pesticide Extraction Leachate 1 10/23/20 14:24 PHE L519088 TCLP SVOC Extraction Leachate 1 10/23/20 14:24 PHE L519088 Analytical Method: 8081A Prep Satch(es): L518793 10/27/20 12:00 Prep Method: 3510C Test Results Units MQL DF Date 1 Time By Analytical Analyzed Batch TCLP Chlordane <0,008000 mg/L 0.008000 10 10/28/20 02:21 VIC L519048 TCLP Endrin <0.001600 mg/L 0.001600 10 10/28/20 02:21 VIC L519048 TCLP gamma-BHC <0.001600 mg/L 0.001600 10 10/28/20 02:21 VIC L519048 TCLP Heptachlor <0.001600 mg/L 0.001600 10 10/28/20 02:21 VIC L519048 TCLP Heptachlor Epoxide <0.001600 mg/L 0.001600 10 10/28/20 02:21 VIC L519048 TCLP Methoxych[or <0.001600 mg/L 0.001600 10 10/28/20 02:21 VIC L519048 TCLP Toxaphene <0.01200 mg/L 0.01200 10 10/28/20 02:21 VIC L519048 Surrogate: Decachlorobipheny[ 36.71 Limits: 36-1I6% 10 10/28/20 02:21 VIC L519048 Surrogate: Tetrachloro-m-xylene 33.38 Limits: 25-123% 10 10/28/20 02:21 VIC L519048 Analytical Method: 8151A Prep Batch(es): L518647 10/26/20 17:00 Prep Method: 8151A Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP 2,4-D <0.0200 m9/L 0.0200 1 10/27/20 22:21 VIC L519054 Qualifiers/ * Outside QC Limit Definitions MQL Method Quantitation Limit DF Dilution Factor Page 5 of 13 Page 14 of 22 Waypointo ANALYTICAL 25657 Waypoint Analytical Charlotte Ms. Terri Cole Project 0100266 P.O. Box 210543 Information Charlotte , NC 28224-0543 Report Number : 20-295-0162 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com REPORT OFANALYSIS Report Date : 10/28/2020 Received : 10/21/2020 Lab No : 92447 Matrix: Solid Sample ID : Class A Sampled: 10/19/2020 9:52 Analytical Method: 8151A Prep Batch(es): L518647 10/26/20 17:00 Prep Method: 8151A Test Results Units MQL DF Date I Time By Analytical Analyzed Batch TCLP 2,4,5-TP (Mvex) <0.0020 mg/L 0.0020 1 10/27/20 22:21 VIC L519054 Surrogate: DCAA 90.00 Limits: 20-120% 1 10/27/20 22:21 VIC L519054 Analytical Method: 8270D Prep Batch(es): L518753 10/27/20 09:50 Prep Method: 3510C Test Results Units MQL DF Date 1 Time By Analytical Analyzed Batch TCLP 2-Methylphenol <0.100 mg/L 0.100 5 10/27/20 22:22 CCB L518998 TCLP 3&4 Methylphenol <0.200 mg/L 0.200 5 10/27/20 22:22 CCB L518998 TCLP 2,4-Dirtratoluene <0.100 mg/L 0.100 5 10/27/20 22:22 CCB L518998 TCLP Hexachlorobenzene <0.100 mg/L 0.100 5 10/27/20 22:22 CCB L519998 TCLP Hexachlorobutadiene <0.100 mg/L 0.100 5 10/27/20 22:22 CCB L518998 TCLP Hexachloroethane <0.100 mg/L 0.100 5 10/27/20 22:22 CCB L518998 TCLP Nitrobenzene <0.100 mg/L 0.100 5 10/27/20 22:22 CCB L518998 TCLP Pentachlorophenol <0.200 mg/L 0.200 5 10/27/20 22:22 CCB L518998 TCLP Pyridine <0.100 mg/L 0A00 5 10/27/20 22:22 CCB L518998 TCLP 2,4,5 Trichlorophenol <0.100 mg/L 0,100 5 10/27/20 22:22 CCB L518998 TCLP 2,4,6-Trichlorophenol <0.100 mg/L 0.100 5 10/27/20 22:22 CCB L518998 Surrogate: TCLP 2,4,6-Tribromophenol 44.5 Limits: 42-102% 5 10/27/20 22:22 CCB L518998 Surrogate: TCLP 2-Fluorobiphenyl 29.3 Limits: 24-86% 5 10/27/20 22:22 CCB L518998 Surrogate: TCLP 2-Fluorophenol 13.1 Limits: 13-371/o 5 10/27/20 22:22 CCB L518998 Surrogate: TCLP 4 Terphenyl-d14 47.5 Limits: 30-122% 5 10/27/20 22:22 CCB L518998 Surrogate: TCLP Nitrobenzene-d5 24.1 * Limits: 25-781/10 5 10/27/20 22:22 CCB L518998 Surrogate: TCLP Phenol-& 9.45 Limits: 9-2711/a 5 10/27/20 22:22 CCB L518998 Qualifiers/ * Outside QC Limit DF Dilution Factor Definitions MQL Method Quantitation Limit Page 15 of 22 Page 6 of 13 Waypoeinto ANALYTICAL 25657 Waypoint Analytical Charlotte Ms. Terri Cole Project 0100266 P.O. Box 240543 Information Charlotte , NC 28224-0543 Report Number:20-295-0162 Qualifiers/ Definitions MQL Outside QC Limit Method Quantitation Limit 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 1 Fax 901,213.2440 www.waypointanalytical.com REPORT OFANAL YSIS Report Date : 10/28/2020 Received : 10/21/2020 DF Dilution Factor Page 16 of 22 Page 7 of 13 r Waypoint, 2790 Whitten Road, Memphis, TIN 38133 Main 901.2I3.24OO 0Fax 901.21213.2440.2440 ANALYTICAL www.waypointanalytical.com Quality Control Data Client ID: Waypoint Analytical Charlotte Project Description: 0100266 Report No: 20-295-0162 QC Prep. L518793 QC Analytical Batch (es): L519048 QC Prep Batch Method: 3510C Analysis Method: 8081A Analysis Description: Organochlorine Pesticides by GC (TCLP) Lab Reagent Blank LRB-L518793 Matrix: TCL Associated Lab Samples: 92447 Blank MQL Analyzed % % Rec Parameter Units Result Recovery Limits TCLP Chlordane mg/L < 0.008000 0.008000 10/28/20 00:23 TCLP Endrin mg/L < 0,001600 0.001600 10/28/20 00:23 TCLP gamma-BHC mg/L < 0,001600 0.001600 10/28/20 00:23 TCLP Heptachlor mg/L < 0.001600 0.001600 10/28/20 00:23 TCLP Heptachlor Epoxide mg/L < 0.001600 0.001600 10/28/20 00:23 TCLP Methoxychlor mg/L < 0.001600 0.001600 10/28/20 00:23 TCLP Toxaphene mg/L < 0.01200 0.01200 10/28/20 00:23 ecachlorobiphenyl (S) 10/28/20 00:23 83.2 36-116 Tetrachloro-m-xylene (S) 10/28/20 00:23 53.9 25-123 Laboratory Control Sample & LCSD LCS-L518793 LCSD-L518793 Spike LCS LCSD LCS LCSD % Rec Parameter Units Conc. Result Result %Rec % Rec Limits RPD Max RPD TCLP Endrin mg/L 0.008000 0.005294 0.005830 66.1 72,8 45-117 9.6 20.00 TCLP gamma-BHC mg/L 0,008000 0.005318 0,006375 66.4 79.6 41-102 18.0 20.00 TCLP Heptachlor mg/L 0.008000 0.005056 0.005771 63.2 72.1 40-110 13.2 20.00 TCLP Heptachlor Epoxide mg/L 0.008000 0.005713 0.006636 71.4 82.9 42-115 14.9 20.00 TCLP Methoxychlor mg/L 0,008001) 0.006318 0,006778 78.9 84.7 39-140 7A 20.00 Decachlorobiphenyl (S) 60.1 78.2 36-116 Tetrachloro-m-xylene (S) 54.2 60.5 25-123 Date: 10/28/2020 05:36 PM Page 17 of 22 Page 8 of 13 (2) iWaypont, 2790 Whitten Memphis, 3.240 Main 901.213.240Q °Fax 9Q1.213.2440 21.2440 ANALYTICAL www.waypointanalytical.com Quality Control Data Client ID: Waypoint Analytical Charlotte Project Description; 0100266 Report No: 20-295-0162 QC Prep: L518647 QC Analytical Batch(es): L519054 QC Prep Batch Method: 8151A Analysis Method: 8151A Analysis Description: Phenoxy Acid Herbicides - GC/ECD (TCLP) Lab Reagent Blank LRB-L518647 Matrix: TCL Associated Lab Samples: 92447 Blank MQL Analyzed % % Rec Parameter Units Result Recovery Limits TCLP 2,4-D mg/L < 0.0200 0.0200 10/27/20 20:13 TCLP 2,4,5-TP (Silvex) mg/L < 0A020 0.0020 10/27/20 20:13 DCAA (5) 10/27/2D 20:13 56.0 20-120 Laboratory Control Sample & LCSD LCS-L518647 LCSD-L518647 Spike LCS LCSD LCS LCSD % Rec Parameter Units Conc. Result Result %Rec % Rec Limits RPD Max RPD TCLP 2,4-D mg/L 0.1000 0.0482 0.0496 48.2 49.6 20-120 2.8 20.00 TCLP 2,4,5-TP (Silvex) mg/L 0.0100 0.0044 0.0046 44.0 46.0 20-120 4.4 20.00 DCAA (S) 52.0 52.6 20-120 Date: 10/28/202D 05:36 PM Page 18 of 22 Page 9 of 13 Waypoint.0 ANALYTICAL_ 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www-waypointanalytical.com Quality Control Data Client ID: Waypoint Analytical Charlotte Project Description: 0100266 Report No: 20-295-0162 QC Prep: L518753 QC Analytical Batch(es): L518998 QC Prep Batch Method: 3510C Analysis Method: 8270D Analysis Description: Semivolatile Organic Compounds - GC/MS (TCLP) Lab Reagent Blank Associated lab Samples: 92447 Parameter Units LRB-L518753 Blank Result MQL Matrix: TCL Analyzed % Recovery % Rec Limits TCLP 2-Methylphenol mg/L < 0,0200 0.0200 10/27/20 18:51 TCLP 3&4 Methylphenol mg/L < 0.0400 0.0400 10/27/20 18:51 TCLP 2,4-Dinitrotoluene mg/L < 0.0200 0.0200 10/27/20 18:51 TCLP Hexachlorobenzene mg/L < 0,0200 0.0200 10/27/20 18:51 TCLP Hexachlorobutadiene mg/L < 0.0200 0.0200 10/27/20 18:51 TCLP Hexachloroethane mg/L < 0.0200 0.0200 10/27/20 18:51 TCLP Nitrobenzene mg/L < 0.0200 0.0200 10/27/20 18:51 -LP Pentachlorophenol mg/L < 0.0400 0.0400 10/27/20 18:51 TCLP Pyridine mg/L < 0.0200 0.0200 10/27/20 18:51 TCLP 2,4,6-Trichlorophenol mg/L < 0.0200 0.0200 10/27/20 18:51 TCLP 2,4,6-Tribromophenol (S) 10/27/20 18:51 44.0 42-102 TCLP 2-Fluorobiphenyl (S) 10/27/20 18:51 47.2 24-86 TCLP 2-Fluorophenol (S) 10/27/20 18:51 19.8 13-37 TCLP 4-Terphenyl-d14 (S) 10/27/20 18:51 62.5 30-122 TCLP Nitrobenzene-d5 (S) 10/27/20 18:51 38.2 25-78 TCLP Phenol-d6 (S) 10/27/20 18:51 12.3 9-27 Laboratory Control Sample & LCSD LCS-L518753 LCSD-L518753 Parameter Units Spike Conc. LCS Result LCSD Result LCS %Rec LCSD % Rec % Rec Limits RPD Max RPD TCLP 2-Methylphenol mg/L 0.200 0.0812 0.0798 40.6 39.9 22-97 1.7 20.0 TCLP 3&4 Methylphenol mg/L 0.200 0.0818 0.0742 40.9 37.1 21-96 9.7 20.0 TCLP 2,4-Dinitrotoluene mg/L 0.200 0.129 0.142 64.5 71.0 24-147 9.5 20.0 TCLP Hexachloro benzene mg/L 0.200 0.147 0.154 73.5 77.0 18-136 4.6 20,0 'CLP Hexachlorobutadiene mg/L 0.200 0.0819 0.0847 40.9 42.3 22-109 3.3 20.0 TCLP Hexachloroethane mg/L 0.200 0.0733 C.0766 36.6 38.3 16-107 4.4 20.0 Date: 10/28/2020 05:36 PM Page 19 of 22 Page 10 of 13 Waypdiont.(2) ANALYTICAL 2790 Whitten Road, Memphis, TN 98133 Main 901.213,2400 ° Fax 901.213,2440 www.way po i nta nalyti ca Lcam Quality Control Data Client ID: Waypoint Analytical Charlotte Project Description: 0100266 Report No: 20-295-0162 QC Prep: L518753 QC Analytical Satch(es): L518998 QC Prep Batch Method: 3510C Analysis Method: 8270D Analysis Description: Semivolatile Organic Compounds - GC/MS (TCLP) Laboratory Control Sample & LCSD Parameter Units LCS-L518753 Spike Conc. LCSD-L518753 LCS Result LCSD Result LCS %Rec LCSD % Rec % Rec Limits RPD Max RPD TCLP Nitrobenzene mg/L 0.200 0.0938 0.0942 46.9 47.1 27-117 0.4 20.0 TCLP Pentachlorophenol mg/L 0.200 0.0921 0.103 46.0 51.5 17-142 11.1 20.0 TCLP Pyridine mg/L 0.200 0.0405 0.0345 20.2 17.2 10-71 16.0 20.0 TCLP 2,4,5-Trichlorophenol mg/L 0.200 0.123 0.138 61.5 69.0 26-118 11.4 20.0 TCLP 2,4,6-Trichlarophenol mg/L 0.200 0.123 0.136 61.5 68.0 26-115 10.0 20.0 TCLP 2,4,6-Tribromophenol (S) 54.0 55.7 42-102 TCLP 2-Fluorobiphenyl (S) 46.2 48.7 24-86 TCLP 2-Fluorophenol (S) 18.5 18.7 13-37 TCLP 4 Terphenyl-d 14 (S) 59.2 66.2 30-122 TCLP Nitrobenzene-d5 (S) 36.2 34.5 25-78 TCLP Phenol-d6 (S) 12.7 12.9 9-27 Date: 10/28/2020 05:36 PM Page 20 of 22 Page 11 of 13 • Waypo n ti (D 273p n901Whitten Road, Memphis, TIDE .2440 Main 901.213.2400 0 Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Shipment Receipt Form Customer Number: 25657 Customer Name: Waypoint Analytical Charlotte Report Number: 20-295-0162 Shipping Method Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier (D Other: Thermometer ID: `i `iT100 Shipping container/cooler uncompromised? 9 Yes 0 No Number of coolers/boxes received Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No NIA Water - VOA vials free of headspace 0 Yes 0 No NIA Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No NIA �_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr) F_ High concentration pre -weighed (methanol -14 d) [_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? Comments: 0 Yes • No Signature: Maka la Weaver Date & Time: 10/21/2020 17:56:30 Page 21 of 22 Page 12 of 13 I I Y q 7 25657 4 � WaVpUintAnalYlrcal Charlotte 10-21-2026 S WaypoNnt- 0100266 17:54-56 ANALYTICAL. S\DING LABORATORI': Waypoint Analytical P. O. Box 240543 Charlotte, NC 28224-0543 Phone: 800-529-6364 Fas: 704-525-0409 Protect Manager. Terri W. Cole Sl'BCONTRACT ORDER 771f3 Z S Cerlircation: NELAC USACE WaypointAnslytical NC k SC— Other 0100266 NiA—__— Waypoint Analytical 2790 Whitten Road Memphis, TN 38133 Phone :(941) 213-2400 Fait: (901) 213-2440 Analysis Due Expires Laboratory ID Cam Sample 1D:0100266-01 Solid Sampled: 10/19/28 09:51 Class Herbicides TCLP (Sub) 1 I /02120 09 51 Supplied. v C_Gl L; k- 10.2t.2,0 re T e X Released By Date Rcccn ed 13� trace Released By Date ReccwW By Date Page I of I Page 22 of 22 Page 13 of 13 YEAR ZD 2--0 Daily Dryer Cog tan Feb Mar Apr May Jun Jul Aug Sept Oct Nov Dec X i�Ts�LT3i #,�• ' � �sL'i�Il�Lsa.�w �, ��� �� y' - �['� . , . i�!�[�■�/L���i►���.� I �'a� '�� :lad � • �� 11.E F m i ., �' ,���� YEAR 2020 Daily Dryer Log 0 Jan Feb Mar Apr May Jun Jul Aug Sept Oct Nov Dec YEAR 2020 Daily Dryer Log Jan Feb Mar Apr May Jun Jul Aug Sept Oct Nov Dec ?;Un -*P YEAR 2020 Daily Dryer Log Jan Feb Mar Apr S:) Jun Jul Aug Sept Oct Nov Dec YEAR 2020 Daily Dryer Log Jan Feb Mar Apr May Jun Jul Aug Sept Oct Nov Dec YEAR 2020 Daily Dryer Lag Jan Feb Mar Apr May Jun ru, Aug Sept Oct Nov Dec YEAR 2020 Daily Dryer Log Jan Feb Mar Apr May Jun Jul Aug Sept Oct Nov Dec k1k YEAR 2020 Daily Dryer Log Jan Feb Mar Apr May Jun Jul Aug Sept Oct Nov Dec YEAR 2020 Daily Dryer Log Jan Feb Mar Apr Date Feed rate 8AM Ibs/hr Time Temp %DS lnitiafs 1 y �SU � 9,7 A%� Ltk 2 y : o,52 of 3 0 07 q3 Hai `If 4 jSyO "7 � MM 5 0" ('44 6 7 8 9 10 11 35 S-0 12 3s 13 L� 14 3sso 155�7 16 C77 c 17 773 S g 1, i 18 wp Dyl " 19 arf" 1,Li CIA 20 j 21 094 14171 %V 22 5'S7 fit` P770 G319% LA 23 �500 �'�' 3 5' -7 " LI-A 24 3 0jtj K7 $ 15y 2s 1CbO OfV7A- I IYO Isx 26 27 Ct I& Nt4w 28 29 =3 5r6 0 a 30 s1 ySo Z -2-02- 3 5 May Jun Jul Aug Sept pc Nov . Dec YEAR 2020 Daily Dryer Log Jan Feb Mar Apr May Jun Jul Aug Sept Oct Nov Dec YEAR 2020 Daily Dryer Log Jan Feb Mar Apr May Jun Jul Aug Sept Oct Nov Dec TOWN OF MOORESVILLE CLASS A BIOSOLID PELLETS UTILIZATION AGREEMENT DISTRIBUTED UNDER NC DWQ PERMIT # WQ0036723 I. CONTACT INFORMATION THIRD PARTY INFORMATION Name Randy Bo d Mailing Address 280 Edmiston Rd. Mount Ulla; NC 28125 Phone Number 04 235-8714 Email TOWN OF MOORESVILE INFORMATION Larry Hendren. (Pertnittee Designee) P.O. Box 878, Mooresville NC 28115 704-799-4063 Ihendren@mooresviIIenc.gov II . DESCRIPTION This is pelletized material produced from the heat treatment of residuals from municipal wastewater. This product meets the standards for a Class A biosolid product according to the EPA's 40 CFR Part 503 regulations. III. RESTRICTIONS Residual land application is prohibited except in accordance with the instructions on this Utilization Agreement; 1. If the residuals are likely to adversely affect a threatened or endangered species listed under section 4 of the Endangered Species Act or its designated critical habitat 2. If the application causes prolonged nuisance conditions 3. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface water or groundwater standards 4. If the land is flooded, frozen, or snow-covered, or is otherwise in a condition such that runoff of the residuals would occur 5. Within the 100 year flood elevation, unless the bulk residuals are injected or incorporated within a 24- hour period following a residuals land application event 6. During a measurable precipitation event (i.e. greater than 0.01 inch per hour), or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period 7. If the soil pH is not maintained at 6.0 or greater, unless sufficient amounts of lime are applied to achieve a final soil pH of at least 6.0, or if an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the specified crop 8. If the land does not have an established vegetative cover unless the residuals are incorporated or injected within a 24-hour period following a residuals land application event 9. If the vertical separation between the seasonal high water table and the depth of residuals application is less than one foot 10. If the vertical separation of bedrock and the depth of residuals application is less than one foot 11. Biological Residuals shall not be stockpiled for more than 30 days prior to distribution 12. The Third Party accepting the residuals shall provide the Permittee with all other nutrient applications (i.e. organic and/or inorganic fertilizers) 13. A copy of this Utilization Agreement shall be maintained at the site when bulk residuals are being applied 14. The residuals shall be prevented from entering any public or private water supply source (including wells) and any surface waters (e.g. streams, lake, river, wetland) 15. Residuals should be land applied at agronomic rates 0 2016 Town of Mooresville 16. Submission of Soil Samples prior to distribution of product 17. The Permittee shall not distribute bulk residuals to any person or entity known to be applying residuals contrary to the condition of the signed Utilization Agreement IV. SETBACKS Applicable setbacks in accordance with 15A NCAC 02T .1108(b): V. APPLICATION RATES Application Rates should not exceed the calculated nitrogen requirements based on the Realistic Yield Expectation for a particular crop and the predominant soil series within the application area. This product has a North Carolina Fertilizer label of 5% Nitrogen —1 % Phosphorus — 0% Potassium ratio, but given that it is generated from aerobically digested residual biosolids it is assumed that a 30% mineralization rate (Organic Nitrogen to Plant Available Nitrogen) is used to calculated the Plant Available Nitrogen (PAN). The PAN listed below should be used along with other nutrient application to determine agronomic rates. NUTRIENT RANGES Percent Solids. 9_ 4-98% Total Nitrogen: 22-100 lbs ton Ammonia Nitrogen: 0.4-6 lbs/ton Nitrate/Nitrite Nitrogen: 0 - 0.01 lbs ton PAN: 7-401b ton Total Phosphorus: 20-28 lbs/togas P,05� Total Potassium: V. AGREEMENT 0-10 lbs/ton (as K0) 14a�4 of Mooresville Date Approximate Density:15 - 20 lbs/W kANd � Z4j Third arty (Printed Name) Z444 7 - 9 -,7 Third arty (Signature) Date 0 2016 Town of Mooresville