WI0400231_APPLICATION FOR PERMIT_20111227

sA
a global professional services company
5724 Summer Trees Drive I Memphis, Tennessee 381341 Telephone [phone] I Facsimile 901-372-2454 I www.ensafe.com
December 27, 2011
Thomas Slusser, UIC Program Manager
UIC Program
Aquifer Protection Section
North Carolina DENR-DWQ
1636 Mail Service Center
Raleigh, NC 27699-1636
Re: Application for Permit to Construct and/or Use a Well(s)for Injection
Walter Kidde Portable Equipment, Mebane, North Carolina
REC Facility ID #NONCD 000 1103
Dear Mr. Slusser:
On behalf of Walter Kidde Portable Equipment Inc. (Kidde), EnSafe Inc. is pleased to submit two copies
of this Underground Injection Permit Application for upcoming remediation activities being performed at
the Kidde facility in Mebane, North Carolina, under the Inactive Hazardous Sites Branch Registered
Environmental Consultant (REC) program. Injections are currently planned for March/April 2012; based
on the dates of entry into the REC program, the REC rules require remedial actions to be completed by
June 7, 2012.
If you have any questions about the Kidde facility or the planned remediation program, please do not
hesitate to contact me at [phone] or via e-mail at [e-mail].
Respectfully Submitted,
EnSafe Inc.
By: Lori Anne Goetz
Project Engineer
CC: John L. Baron, UTC
AECEiVED/DENR/DVi�Q
Attachments (2) quiferPinrActrnR��
DEC 9 2011
engineering I environment I health &safety I technology

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UTC REVIEW SHEET
(II 7i) December 2011
Chad Tripp Date
Technical Services
Primary Author
December 2011
Lori Anne Goetz Date
Environmental Engineer
Senior Review
RECEIVED/DENR/DWQ
Aquifer Protection Section
•
DEC 2,9 2011

State of North Carolina
Department of Environment and Natural Resources
Division of Water Quality
APPLICATION FOR PERMIT TO CONSTRUCT AND/OR USE A WELL(S)FOR INJECTION
Type 5I Wells—In Situ Groundwater Remediation/Type 5T Wells—Tracer Injection
• Do not use this form for remediation systems that extract contaminated groundwater,treat it,and reinject the treated groundwater.
• Submit TWO copies of the completed application and all attachments to the address on the last page of this form.
• Any changes made to this form will result in the application package being retur�ngd. J
Application Number(to be completed by DWQ): \a(�`f-�}( /
GENERAL INFORMATION:
1. Applicant's Name(generally the responsible party): United Technologies Corporation
2. Signing Official's Name*: Richard H.Bennett Title: Vice President,Environment,Health& Safety
* Signing Official must be in accordance with instructions in part VI on page 7.
3. Mailing address of applicant: One Financial Plaza.Mail Stop 503
City: Hartford State: CT Zip: 06101
Telephone number: 860-728-6540 Fax number: 860-493-4177
4. Property Owner's Name(if different from Applicant):
5. Property Owner's mailing address:
City: _ State: Zip:
6. Name and address of contact person who can answer questions about the proposed injection project:
Name: Craig Wise,P.E. Title: Vice President
Company: EnSafe Inc.
Address: 5724 Summer Trees Drive
City: Memphis State: TN Zip: 38134
Telephone number: 901-372-7962 Fax number: 901-372-2454
Email Address: cwise(c�ensafe.com
RECEIVED/DENR/DUV4
Aquifer Protection Section
DEC 9 2011
Revised 6/09 UIC-5I/5T Page 3 of 16

APPLICATION FOR PERMIT TO CONSTRUCT AND/OR USE A WELL(S)FOR INJECTION
Type 5I Wells—In Situ Groundwater Remediation/Type 5T Wells—Tracer Injection
IL PERMIT INFORMATION:
1. Project is: New (Modification of existing permit (Renewal of existing permit without modification
( Renewal of existing permit with modification
2. If this application is being submitted for renewal or modification to an existing permit,provide:
existing permit number_ Not applicable and the issuance date
For renewal without modifications, fill out sections I & II only, sign the certification on the last page of this
form,and obtain the property owner's signature to indicate consent(if the applicant is not the owner).
For all renewals,submit a status report including monitoring results of all injection activities to date.
Revised 6/09 UIC-5I/5T Page 4 of 16

APPLICATION FOR PERMIT TO CONSTRUCT AND/OR USE A WELL(S)FOR INJECTION
Type 5I Wells—In Situ Groundwater Remediation/Type 5T Wells—Tracer Injection
III. INCIDENT&FACILITY DATA
A. FACILITY INFORMATION
1. Facility name: Walter Kidde Portable Equipment,Inc.
2. Complete physical address of the facility: 1394 South Third Street Extended
3. City: Mebane County: Alamance State: NC Zip: 27302
B. INCIDENT DESCRIPTION
1. Describe the source of the contamination: Throughout the 30 plus years of manufacturing onsite, various
chlorinated solvents and other cleaners/degreasers were used throughout the facility. Soil and groundwater
contamination has been investigated and presented in several reports since 2006, including the Comprehensive
Site Assessment Report(CSA) (EnSafe,2006),CSA Addendum(EnSafe. 2007),Remedial Investigation Report
(EnSafe, 2010). Solvent was apparently released at the southeast portion of Distribution Building DC-2 near
monitoring well MW043. Building DC-2 was historically a process area, now used as a warehouse. Historical
releases of solvents have resulted in a groundwater plume that extends nearly 800 feet to the northeast of the
building and into shallow bedrock, albeit at relatively low concentrations. Concentrations and distribution of
contaminants were determined to be indicative of multiple small releases over the life of the facility during
manufacturing operations.
2. List all contaminants present in soils or groundwater at the site (contaminants may be listed in groups,
e.g., gasoline, diesel,jet fuel, fuel oil, chlorinated ethenes, chlorinated ethanes,metals,pesticides/herbicides, etc):
Contaminants of concern in the soil and groundwater at the site are chlorinated ethenes and ethanes. Other
contaminants detected in the groundwater include 1.4-dioxane, bis(2-ethylhexvl)phthalate (BEHP), chromium,
and other various metals.Other contaminants detected in the soil include methylene chloride,chromium(total and
hexavalent). and other various metals.
3. Has LNAPL or DNAPL ever been observed at the site(even if outside the injection zone)?
"VYes If yes, list maximum measured separate phase thickness feet
No If no, list maximum concentration of total VOCs observed at site: 1940 ppb (temporary well near southeast
corner of DC-2,2/28/2006);current maximum concentrations(2011), 230 ppb in MW049,permanent well near southeast
corner of DC-2.
4. Agency managing the contamination incident:
(UST Section 1iSuperfund Section(including REC Program and DSCA sites)
(DWQ Aquifer Protection Section ( Solid Waste Section
(Hazardous Waste Section (Other:
5. Incident managers name: Kim T. Caulk.PG and phone number(919) 508-8451
6. Incident number or other site number assigned by the agency managing the contamination incident:
NCDENR Division of Waste Management Facility#NONCD 000 1103
Revised 6/09 UIC-5I/5T Page 5 of 16

APPLICATION FOR PERMIT TO CONSTRUCT AND/OR USE A WELL(S)FOR INJECTION
Type 5I Wells—In Situ Groundwater Remediation/Type 5T Wells—Tracer Injection
C. PERMITS
1. Hazardous Waste Management program permits under RCRA: CESOG status; EPA ID#NCD067428177
2. DWQ Non-Discharge or NPDES permits: General permit NCG030000,COC Number NCG030417. The
facility has submitted to the State of NC a Request for Rescission as activities in DC2 and DC3 will cease within
the next four months(by April 2012).
3. County or DEH subsurface wastewater disposal permits: None, although the facility does have a letter of
agreement with the City of Mebane allowing discharge of no more than 300 gallons of a floor cleaning solution
15 gals. Simple Green to 45 gals. Water)per week.
4. Other environmental permits required by state or federal law: none
Revised 6/09 UIC-51/5T Page 6 of 16

APPLICATION FOR PERMIT TO CONSTRUCT AND/OR USE A WELL(S)FOR INJECTION
Type 5I Wells—In Situ Groundwater Remediation/Type 5T Wells—Tracer Injection
IV. INJECTION DATA
A. INJECTION FLUID DATA
1. List all proposed injectants.
NOTE: Any substance to be injected as a tracer or to promote in situ remediation must be reviewed by the
Occupational and Environmental Epidemiology Section (OEES) of the Division of Public Health, Department of
Health and Human Services. Review the list of approved injectants or contact the UIC Program to determine if
the injectants you are proposing have been reviewed by OEES.
INJECTION FLUID DATA—SOIL TREATMENT 5 - 5 s'
In the soil source area,which is approximately 2,500 square feet(SF),an initial 32 injection points have been
proposed to deliver approximately 5,121 gallons of emulsified oil with zero valent iron(EZVI). EZVI will be
delivered to the target interval(10 to 25 feet below ground surface [bgs])via direct push technology(DPT). If the
formation does not accept the injectate, additional DPT points will be used to deliver the design quantities.
However,the data below reflect the proposed 32-point grid.
Injectant: Emulsified Oil/Zero Valent Iron(EZVI)in Source Soil Area only
Concentration at point of injection: 160 gallons of EZVI at each point
Percent if in a mixture with other injectants:
INJECTION FLUID DATA—GROUNDWATER TREATMENT
In the groundwater source area,which is approximately 17,500 SF, an initial 56 injection points have been
proposed to deliver the following quantities of substrate.
• 24,600 lbs zero-valent iron(ZVI) 6 .- r• 22,400 lbs Enhanced Hydrogen Compound(EHC)
• 4,930 lbs Hydrolized kelp
• 11,200 lbs Calcium propionate
• 1,680 lbs Sodium sulfite
• 1,680 lbs Yeast extract
• 46,800 g B2
• 6,750 g B12
• 1,680 lbs Nutrients
These substrates will be delivered to the target interval(25 to 50 feet bgs)via DPT. If the formation does not
accept the injectate,additional DPT points will be used to deliver the design quantities. However,the data below
reflect the proposed 56-point grid.
Injectant: ZVI
Concentration at point of injection: 73.3 lbs/75 gallons water per interval or 440 lbs/450 gal water per
point or 24.640 lbs/25,200 gal solution
Percent if in a mixture with other injectants: 32.8%
Injectant: Adventus EHC
Concentration at point of injection: 66.6 lbs/75 gallons water per interval or 400 lbs/450 gal water per
point or 22,400 lbs/25,200 gal solution
Revised 6/09 UIC-5I/5T Page 7 of 16

APPLICATION FOR PERMIT TO CONSTRUCT AND/OR USE A WELL(S)FOR INJECTION
Type 5I Wells—In Situ Groundwater Remediation/Type 5T Wells—Tracer Injection
Percent if in a mixture with other injectants: 29.8%
• Injectant: Calcium Propionate
Concentration at point of injection: 33.3 lbs/75 gallons water per interval or 200 lbs/450 gal water per
i � • r
point or 11,200 lbs/25.200 gal solution
Percent if in a mixture with other injectants: 14.9%
Injectant: Hydrolyzed Kelp
Concentration at point of injection: 14.6 lbs/75 gallons water per interval or 88 lbs/450 gal water per
point or 4,928 lbs/25,200 gal solution
Percent if in a mixture with other injectants: 6.6%
Injectant: Yeast Extract
Concentration at point of injection: 5 lbs/75 gallons water per interval or 30 lbs/450 gal water per point
or 1,680 lbs/25,200 gal solution
Percent if in a mixture with other injectants: 2.25%
Injectant: Sodium Sulfite
Concentration at point of injection: 5 lbs/75 gallons water per interval or 30 lbs/450 gal water per point
or 1,680 lbs/25,200 gal solution
Percent if in a mixture with other injectants: 2.25%
Injectant:Nutrients •- t
Concentration at point of injection: 5 lbs/75 gallons water per interval or 30 lbs/450 gal water per point
or 1,680 lbs/25,200 gal solution
Percent if in a mixture with other injectants: 2.25%
▪ Injectant: Vitamin B2
Concentration at point of injection: 139.36g/75 gallons water per interval or 836.16 g/450 gal water per
point or 46,825.1 g/25.200 gal solution
Percent if in a mixture with other injectants: 0.14%
• Injectant: Vitamin B12
Concentration at point of injection: 20 g/75 gallons water per interval or 120.4 g/450 gal water per point
or 6.744.8 a/25.200 gal solution
Percent if in a mixture with other injectants: 0.02%
IRevised 6/09 UIC-5I/5T Page 8 of 16

APPLICATION FOR PERMIT TO CONSTRUCT AND/OR USE A WELL(S)FOR INJECTION
Type 5I Wells—In Situ Groundwater Remediation/Type 5T Wells—Tracer Injection
2. Source of fluids used to dilute or chase the injectants listed above:
(None
Municipal water supply
(Groundwater from private well or any well within '/4 mile of injection site
(Air
(Other:
3. If any well within VI mile of injection site,a private well, or surface water is to be used as the fluid source, supply
the following information:
a. Location/ID number of source: Not Applicable
b. Depth of source:
c. Formation:
d. Rock/Sediment type:
e. In Attachment C,provide a current,complete chemical analysis of the water from the source well, including
analyses for all contaminants suspected or historically recognized in soil or groundwater on the site.
NOTE:If contaminated groundwater is to be used as the dilution or chase fluid, this is not the proper permit
application form. You must apply for a closed-loop groundwater remediation permit using application form
GWRS.
B. PROPOSED OPERATING PARAMETERS
1. Duration of Injection: approximately 15 days
a. Maximum number of separate injection events: 1
b. Expected duration of each injection event: 15 days
c. Expected duration between events(if more than one event):
2. Injection rate per well: 3-5 gallons per minute(gpm)
3. Total Injection volume: approximately 1500 gallons per day(gpd); gallons per event(if separate
events)
4. Injection pressure: 25 to 175 pounds/square inch(psi)
5. Temperature at point of injection: ambient _°F
6. Briefly describe how the above parameters will be measured and controlled: The injection points will be
advanced via traditional DPT, utilizing a Geoprobe 6620 or 7720. The injection rods will consist of Innovative
Environmental Technologies (MT) Inc's proprietary injection system with retractable injection zones driven to
the desired injection depth using DPT. Once injection at a location is complete, the residual pressure will be
monitored until a safe level is reached. The injection rod will then be withdrawn and the boring will be
abandoned using hydrated bentonite. The different components of the injectant mixture will each be injected in
series via lET's patented process described as:
Step 1-Injection of nitrogen gas:,
Step 2-Injection of the substrate;
Step 3- Second injection of nitrogen gas;
Step 4- Seal the boring with bentonite.
IET's injection trailer is equipped with tanks for mixing the injection solutions.
Revised 6/09 UIC-5115T Page 9 of 16

APPLICATION FOR PERMIT TO CONSTRUCT AND/OR USE A WELL(S)FOR INJECTION
Type 5I Wells—In Situ Groundwater Remediation/Type 5T Wells—Tracer Injection
Municipal water will be used for the solution mixing. All solutions will be injected at ambient temperatures.
Stainless steel pipes will extend from the mixing tank to the injection pump where it will travel through a high
pressure hose to the injection rod. A pressure gauge, shut-off valves, and pressure bleed-off will also be installed
in-line. Injection will be performed using a double diaphragm pump. Injection pressures will be approximately
25 to 175 psi and injection flow rates are estimated between 3 and 5 gpm. The injection pressure will be
monitored continuously using a pressure gauge and the injection rate will be adjusted using the injection pump
and valves. After injection. the injection pump will be turned off and the shut-off valve will be closed. The
residual pressure in the formation will then be monitored until a safe pressure level is reached. The process will
then be repeated at the next injection location.
7. Estimated hydraulic capacity of the well(gpm): No permanent wells will be used for injections; all injections will
be performed via pressurized DPT points. Hydraulic conductivities in the saprolite range from 1E-05 cm/sec to
1E-03 cm/sec. Hydraulic properties onsite vary depending on the primary and secondary porosity of the
formation, as the saprolite retains relict fractures from the original bedrock matrix. DPT injection rates will vary
with injection pressures,depth,and with the number of secondary porosity features proximal to the injection tip.
C. INJECTION WELL CONSTRUCTION DATA
1. Injection will be via:
( Existing well(s)proposed for use as an injection well.Provide the data in(2)through(6)below to the best of
your knowledge.
( Proposed well(s)to be constructed for use as an injection well. Provide the data in(2)through(6)below as
proposed construction specifications.
+4 OTHER: Temporary injection points via Direct Push-Technologv(DPT)
2. Well Drilling Contractor's Name: Probe Technologies(or comparable vendor; contracting has not been completed
at this time)
NC Well Contractor Certification number: 2724-A
3. Date to be constructed: April 2012
Number of borings: Soil Source Zone=32; Aqueous Source Area= 56 (note— number of borings is approximate
and may vary depending on the formation's permeability: the quantities of injected substrate will remain the
same)
Approximate depth of each boring(feet): Soil Source Area=25 feet bgs: Groundwater Source Area=50 feet bgs
4. Screened interval/Injection interval of injection wells:
Soil Source Area : Depth: 10 to 25 feet below ground surface
Aqueous Source Area: Depth: 25 to 50 feet below ground surface
5. Well casing(N/A if injection is through direct push rods):
Type: ( PVC ( Stainless steel( Other: N/A
Casing depth: to ft.
Revised 6/09 UIC-51/5T Page 10 of 16

APPLICATION FOR PERMIT TO CONSTRUCT AND/OR USE A WELL(S)FOR INJECTION
Type 5I Wells—In Situ Groundwater Remediation/Type 5T Wells—Tracer Injection
6. Grout(N/A if injection is through direct push rods):
Type: ( Cement ( Bentonite ( Other:_ N/A
Grout depth: to ft.
Revised 6/09 UIC-5I/5T Page 11 of 16

APPLICATION FOR PERMIT TO CONSTRUCT AND/OR USE A WELL(S)FOR INJECTION
Type 5I Wells—In Situ Groundwater Remediation/Type 5T Wells—Tracer Injection
NOTE: G.S. 89E-18 requires that any geologic plans, reports, or documents in which the performance is related
to the public welfare or safeguarding of the environment be prepared by a licensed geologist or subordinate
under their direction. G.S. 89E-13 requires that all drawings, reports, or documents involving geologic work
prepared or approved by a licensed geologist, or a subordinate under their direction, be signed and sealed by the
licensed geologist.
Document: Underground Infection Control Permit
Responsible Party: Walter Kidde Portable Equipment
Address: 1394 S.Third Street
City: Mebane State: NC Zip Code: 27302
Latitude/Longitude: 36°4'37.2"N/79°17'23.3" W
Inactive Hazardous Sites Branch Number: NONCD 000 1103
I, Ben Brantley, a North Carolina Professional Licensed Geologist for EnSafe Inc. 5724 Summer
Trees Drive, do hereby certify that to the best of my knowledge the geological and hydrogeological
data, assessments, and interpretations enclosed in this application and in the attachments are correct,
complete, and accurate.
featemeatetilvee
-CV4, ,
A sora,
1-11-14.p 1332
RECEIVED/DENR/DWQ
Aquifer Protection Section
DEC 9 2011
Revised 6/09 UIC-51/5T Page 12 of

APPLICATION FOR PERMIT TO CONSTRUCT AND/OR USE A WELL(S)FOR INJECTION
Type 5I Wells—In Situ Groundwater Remediation/Type 5T Wells—Tracer Injection
V. ATTACHMENTS
Provide the following items as separate attachments with the given headings:
A. SITE HISTORY
Provide a brief description of the site history including:
(1) site usage historically and present,
(2) origin of the contamination,
(3) previous remedial action(s).
NOTE: G.S. 89E-18 requires that any geologic plans, reports, or documents in which the performance is related to the
public welfare or safeguarding of the environment be prepared by a licensed geologist or subordinate under their
direction. G.S. 89E-13 requires that all drawings, reports, or documents involving geologic work prepared or approved
by a licensed geologist, or a subordinate under their direction, be signed and sealed by the licensed geologist.
B. HYDROGEOLOGIC DESCRIPTION
Provide a hydrogeologic description,soils description,and cross section of the subsurface to a depth that includes the
known or projected depth of contamination. The hydrogeologic description shall include:
(1) the regional geologic setting;
(2) significant changes in lithology;
(3) the hydraulic conductivity,transmissivity, and specific yield of the aquifer to be used for injection, including a
description of the test(s)used to determine these parameters; and
(4) the depth to the mean seasonal high water table.
C. INJECTION FLUID COMPOSITION
Describe the chemical,physical, biological and radiological characteristics of each injectant.Attach the Material Safety
Data Sheet(MSDS)for each injectant.If a private well or a well within 1/4 mile of the injection site is used as the source
well,include chemical analysis of source fluid here.
D. INJECTION RATIONALE
Attach a brief description of the rationale for selecting the injectants and concentrations proposed for injection, including:
(1) goals of the injection project;
(2) explanation and/or calculations of how the proposed injectant volume and concentration were determined;
(3) a description of the reactions between the injectants and the contaminants present including specific breakdown
products or intermediate compounds that may be formed by the injection; and
(4) summary results of modeling or testing performed to investigate the injectant's potential or susceptibility to change
(biological, chemical or physical) in the subsurface.
E. INJECTION PROCEDURE AND EQUIPMENT
Provide a detailed description of all planned activities related to the proposed injection including but not limited to:
(1) construction plans and materials;
(2) operation procedures;
(3) a detailed diagram of the surface and subsurface portions of the system; and
(4) a planned injection schedule.
Revised 6/09 UIC-5I/5T Page 13 of 16

APPLICATION FOR PERMIT TO CONSTRUCT AND/OR USE A WELL(S)FOR INJECTION
Type 5I Wells—In Situ Groundwater Remediation/Type 5T Wells—Tracer Injection
F. MONITORING PLAN
1 Provide a plan for monitoring the results of the injection, including:
(1) a list of existing and proposed monitoring wells to be used;
(2) a list of monitoring parameters and analytical methods to be used;and
(3) a schedule for sampling to monitor the proposed injection.
NOTE: The selected monitoring wells must be located so as to detect any movement of injection fluids, process by-
products, or formation fluids outside the injection area or zone. The monitoring parameters should include the target
contaminants as well as secondary or intermediate contaminants which may result from the injection and other
parameters which may serve to indicate the progress of the intended reactions, such as pH, ORP, dissolved oxygen, and
other electron acceptors and donors. The monitoring schedule should be consistent with the pace of the anticipated
reactions and rate of transport of the injectants and contaminants.
G. WELL DATA
Provide a tabulation of data on all existing or abandoned wells within '/4 mile of the injection well(s)which penetrate the
proposed injection zone, including, but not limited to, monitoring wells and wells proposed for use as injection wells.
Such data shall include a description of each well's use (water supply, monitoring, etc), total depth, screened or open
borehole depth interval,and well construction or abandonment record,if available.
H. MAPS
Attach the following scaled, site-specific maps:
(1) Area map based on the most recent USGS 7.5'topographic map of the area,at a scale of 1:24,000 and
showing the location of the proposed injection site.
(2) Site map including:
a. all property boundaries;
b. all buildings within the property boundary;
c. existing and proposed injection wells or well field(s)
d. any existing sources of potential or known groundwater contamination, including waste storage,
treatment or disposal systems within 1/4 mile of the injection well or well system;
e. all surface water bodies within'/4 mile of the injection well or well system; and
f. all existing or abandoned wells within'A mile of the injection well(s)which penetrate the proposed
injection zone, including,but not limited to,monitoring wells and wells proposed for use as injection
wells.
(3) Potentiometric surface map(s)including:
a. direction of groundwater movement
b. existing and proposed monitoring wells
c. existing and proposed injection wells
(4) Contaminant plume map(s)including:
a. the horizontal extent of the contaminant plume, including isoconcentration lines
b. existing and proposed monitoring wells
c. existing and proposed injection wells
(5) Cross-section(s)to the known or projected depth of contamination, including:
a. horizontal and vertical extent of the contaminant plume, including isoconcentration lines
b. major changes in lithology
c. existing and proposed monitoring wells
d. existing and proposed injection wells
Revised 6/09 UIC-51/5T Page 14 of 16

APPLICATION FOR PERMIT TO CONSTRUCT AND/OR USE A WELL(S)FOR INJECTION
Type 5I Wells—In Situ Groundwater Remediation/Type 5T Wells—Tracer Injection
VI. CERTIFICATION(to be signed as required below or by that person's authorized agent)
NCAC 15A 2C .0211(b)requires that all permit applications shall be signed as follows:
1. for a corporation: by a responsible corporate officer
2. for a partnership or sole proprietorship: by a general partner or the proprietor,respectively
3. for a municipality or a state, federal, or other public agency: by either a principal executive officer or
ranking publicly elected official
4. for all others: by the well owner.
If an authorized agent is signing on behalf of the applicant,then supply a letter signed by the applicant that
names and authorizes their agent.
I hereby certify under penalty of law that I have personally examined and am familiar with the information
submitted in this document and all attachments therein, and that, based on my inquiry of those individuals
immediately responsible for obtaining said information, I believe that the information is true, accurate, and
complete. I am aware that there are penalties, including the possibility of fines and imprisonment, for submitting
false information. I agree to construct, operate, maintain, repair, and if applicable, abandon the injection well(s)
and all related appurtenances in accordance with the approved specifications and conditions of the Permit.
Printed Name a . Bennett Vice President, Environment,He th& S fety
Signature: Date:
iz z/
RECEIVED/DENR/DO/
Aquifer Protection Section
DEC 9 2011
Revised 6/09 UIC-5I/5T Page 15 of 16

APPLICATION FOR PERMIT TO CONSTRUCT AND/OR USE A WELL(S)FOR INJECTION
Type 5I Wells—In Situ Groundwater Remediation/Type 5T Wells—Tracer Injection
VII. CONSENT OF PROPERTY OWNER (if the property is not owned by the applicant)
("Owner" means any person who holds the fee or other property rights in the well being constructed A well is
real property and its construction on land shall be deemed to vest ownership in the land owner, in the absence of
contrary agreement in writing.)
As owner of the property on which the injection well(s)are to be constructed and operated,I hereby consent to
allow the applicant to construct each injection well as outlined in this application and agree that it shall be the
responsibility of the applicant to ensure that the injection well(s)conform to the Well Construction Standards
(Title 15A NCAC 2C .0200).
Printed Name and Title:
1 Signature: Date:
Submit TWO copies of the completed application package, including all attachments,to:
UIC Program
Aquifer Protection Section
North Carolina DENR-DWQ
1636 Mail Service Center
Raleigh,NC 27699-1636
Telephone[phone]
Revised 6/09 UIC-5I/5T Page 16 of 16

Walter Kidde Portable Equipment,Inc.
Mebane,North Carolina
UIC Permit Application
Attachment A—Site History
ATTACHMENT A—SITE HISTORY
The Kidde Fire & Security (Kidde), formerly the Walter Kidde Portable Equipment, Site, owned by
United Technologies Corporation (UTC), is located at 1394 South Third Street Extended,
Mebane, North Carolina. The Site is currently in the Registered Environmental Consultant (REC)
program, governed by the rules and regulations of the North Carolina Department of the
Environment and Natural Resources (NCDENR), Division of Waste Management (DWM),
Inactive Hazardous Sites Branch (IHSB). The Remediating Party (RP), UTC, entered into an
Administrative Agreement (AA) with the NCDENR on June 7, 2007, and was assigned the facility
number NONCD 000 1103. Historical site usage, contaminant origin, and previous remedial actions
are presented in the following sections.
1. Site Usage, Historically and Present
The site was undeveloped and utilized as pasture/agricultural land prior to 1972. In 1972, Kidde
purchased the site and until 2008, the Kidde facility produced aluminum and steel fire extinguishers
for commercial and residential use. Currently, the site is used for warehousing and product
repacking. The Site's location on a USGS topographical map is shown in Figure H-1 and a
Site Layout Map is shown in Figure H-2, both in Appendix H.
Although the basic fire extinguisher manufacturing processes remained consistent, operations, raw
materials, equipment, and/or processes changed locations over the historical use of the site.
Cylinder manufacturing consisted of extrusion/forming, cutting, threading, necking,
hydrostatic proof testing, cleaning/degreasing, painting/powder coating, filling, re-working, quality
control testing, and distribution. Other activities included powder manufacturing, foam filling,
medical gas filling, Halon wheel unit manufacturing, and manufacturing of large specialty (scuba,
soda, hospital) tanks.
2. Origin of the Contamination
Throughout the 30-plus years of manufacturing onsite, various chlorinated solvents and other
cleaners/degreasers were used throughout the facility. Environmental assessment were conducted
at the Site from 2005 to 2011 to determine the nature and extent of subsurface contaminants,
including the Comprehensive Site Assessment Report (CSA) (EnSafe, 2006), CSA Addendum
(EnSafe, 2007), Remedial Investigation Report(RI) (EnSafe, 2010) and the Engineering Pre-Design
Investigation (EnSafe, pending). These assessments show the primary contaminants of concern at
the site are the chlorinated volatile organic compounds (CVOCs) tetrachioroethene (PCE),
1,1-dichloroethene (1,1,-DCE), and 1,1-dichloroethane (1,1-DCA). The apparent source of
contamination is the southeast portion of Building DC-2 near monitoring well MW043.
Building DC-2 was historically a process area, now used as a warehouse. Historical releases of
solvents have resulted in a groundwater plume that extends nearly 800 feet to the northeast of the
apparent source area and into shallow bedrock, albeit at relatively low concentrations.
Concentrations and distribution of contaminates were determined to be indicative of multiple small
releases over the life of the facility during manufacturing operations.
A-1

Walter Kidde Portable Equipment,Inc.
Mebane,North Carolina
UIC Permit Application
Attachment A—Site History
Two contaminant plumes were observed in the site groundwater. One approximately 7-acre CVOC
plume with concentrations above NC 02L standards extends approximately 800 feet northeastward
from DC-2 to the eastern property line (EPL), where the plume turns north paralleling the local
shallow valley and an ephemeral stream that flows to the north (see figure H-4-1). The apparent
source of this plume is residual contaminant mass in the soil from 10 to 25 feet below ground
surface (bgs) beneath the southeastern corner of the Building DC-2. This residual mass and
groundwater plume was identified for remedial action in the RI. A second, smaller,
low concentration, CVOC plume extends northeastward from the Environmental Shed (DC-4) and
Main Manufacturing Plant (DC-3) towards MW029. Due to low and reducing concentrations in this
second plume, monitoring will track attenuation in this area.
Vertically, CVOCs in the 7-acre groundwater plume are present in the shallow groundwater
(approximately 25 to 50 feet bgs), transition-zone (top-of-bedrock, TOB) groundwater
(approximately 65 to 75 feet bgs), and bedrock (approximately 80 to 105 feet bgs).
Groundwater concentrations decrease with depth, with the lowest concentrations
(slightly exceeding NC 02L standards) present in bedrock.
A summary of CVOC impacted media retained for remedial action is provided below:
• Soil Source Area
This 50 foot by 50 foot by 25 foot deep volume of soil beneath the warehouse building is
characterized by PCE in soil above the soil-to-groundwater Soil Remediation Goals (SRG),
with maximum concentrations of approximately 1 milligram per kilogram PCE.
• Groundwater Source Area
An area of the groundwater plume near the soil source of about 17,500 square feet is
contaminated from 25 feet to 50 feet bgs. Representative PCE and 1,1-DCE concentrations
in the source zone are 140 micrograms per liter (pg/L) and 120 pg/L, respectively. The
depth of contamination indicates that there may be residual mass in this zone which is
acting as an ongoing source of groundwater contamination.
• Top-of-Bedrock Groundwater Plume
Groundwater contamination is observed at the top of bedrock downgradient from the
soil source area. Concentrations of PCE up to 10 pg/L have been observed, with 1,1-DCE
concentrations up to 50 pg/L. Remedial actions in the soil and groundwater source area are
expected to reduce top-of-bedrock concentrations.
• East Property Line(EPL) Plume
The dissolve phase plume of contaminated groundwater follows topography and extends
nearly to the property line approximately 800 feet downgradient from the source areas.
While some wells in this area have exhibited significant decreases in CVOC concentrations,
others have shown increases.
Al

•
Walter Kidde Portable Equipment,Inc.
Mebane, North Carolina
UIC Permit Application
Attachment A—Site History
A map of the CVOC contaminate plume is shown on Figure H-4-1 in Attachment H.
3. Previous Remedial Actions
No remedial actions for CVOCs have been performed at the Site. Prior to 2005, soil contaminated
with petroleum hydrocarbons in the vicinity of the Environmental Shed (DC-4) was removed and
disposed offsite.
A-3

Walter Kidde Portable Equipment,Inc.
Mebane,North Carolina
UIC Permit Application
Attachment B—Hydrogeologic Description
ATTACHMENT B— HYDROGEOLOGIC DESCRIPTION
Data from the Comprehensive Site Assessment Report (CSA) (EnSafe, 2006), CSA Addendum
(EnSafe, 2007), Remedial Investigation Report(RI) (EnSafe, 2010) and the Engineering Pre Design
Investigation (EnSafe, pending) were combined with information from local and regional
U.S. Geological Survey (USGS) studies and other research to develop a conceptual hydrogeological
model for the Site. The following sections provide a regional geologic setting; a site geologic setting
and description of significant changes in lithology; the hydraulic conductivity, transmissivity, and
specific yield of the aquifer to be used for injection; and the depth to the mean seasonal high water
table.
1. Regional Geologic Setting
Geology
The site lies within the Carolina Slate Belt, an area of the Piedmont that is underlain by
metaigneous and metavolcanic rocks. Metamorphic rocks of the Piedmont typically range from
greenschist to amphibolite, whereas unmetamorphosed igneous intrusive rocks are present as
diabase dikes and granitic veins, batholith-scale igneous or felsic intrusions
(Chapman, et. al, 2005). Although less common, sedimentary rocks are locally present within the
region as down-faulted, elongate Mesozoic sedimentary basins. These Mesozoic basins crop out in
a northeast-trending band throughout eastern North Carolina, adjacent to the Piedmont-Coastal
Plain regional boundary. It is this regional boundary that marks the transition from hard,
resistant crystalline rocks of the Piedmont to less resistant sedimentary rocks of the Coastal Plain.
Hydrogeology
Regionally, four distinct hydrogeologic components comprise the Blue-Ridge-Piedmont
groundwater system as a whole; in descending depth, they are: (1) the unsaturated zone of the
regolith, which also contains organic layers of the surface soil, (2) the saturated portion of the
regolith, (3) the lower saturated regolith, which contains the transition zone between weathered
bedrock, termed saprolite, and deeper bedrock, and (4) the deeper fractured crystalline bedrock
system (Harned and Daniel, 1992). Groundwater is contained primarily within the regolith
(i.e., porous alluvium, soil, and saprolitic sediments), or within bedrock fractures. Throughout the
north-central portion of the Piedmont, regolith can vary from 0 to 150 feet thick, and consists of
semi- or unconsolidated sediments ranging from clay- to silt-dominated fractions (Buol, 1985) to
boulders.
The intensive chemical in-place weathering of crystalline metamorphic and igneous rocks of the
Piedmont produces saprolite and soil residuum (i.e., together, termed regolith). Saprolite retains
much of the fabric of its underlying parent rock, whereas weathering of feldspars and
micas produces clay as residuum. As a result, regolith is typically characterized by high porosity
values but low to moderate hydraulic conductivities: groundwater flows through intergranular
pore spaces or through relict fractures in soil and saprolite. In contrast, the underlying
unweathered bedrock is characterized by very low porosities and permeabilities: groundwater must
flow through secondary fractures and planar discontinuities (Chapman, et. al, 2005). Moreover,
B-1

Walter Kidde Portable Equipment,Inc.
Mebane, North Carolina
UIC Permit Application
Attachment B—Hydrogeologic Description
high permeability, often encountered within the "transition zone" at the base of the regolith, may
create a zone of concentrated flow above the unweathered bedrock in some localities. Wells cased
through such regolith/transition zones, and into unweathered bedrock, may be poor groundwater
producers; such completions may reveal a poor connection between the regolith reservoir, the
bedrock fracture system, and the well (Cunningham and Daniel, 2001).
2. Site Geology and Significant Changes in Lithology
The site geology and hydrogeology is based upon assessment of numerous soil and subsurface
rock samples and aquifer data collected across the assessment area, but includes data from a
focused assessment in the vicinity of building DC-2 that is representative of sitewide geology and
hydrogeology. Figure H-5 (in Appendix H) is southwest-northeast trending geologic cross-section
that illustrates the site and selected remedial area.
Site geology can be described as four zones in descending order:
• Fill material/surficial soil (associated with site buildings)
• Regolith
— Mature saprolite
— Immature saprolite
• Transition zone (bedrock fragments mixed in with saprolite)
• Bedrock
Fill Material/Surface Soil
Up to 5 feet of fill/surface material have been encountered beneath the DC-2 area with less fill
associated with DC-3 and DC-4. Fill near DC-2 generally consists of brick-red silty clay that is very
firm and slightly moist. The brick-red clay is also present at the surface in the
northern highland areas.
Regolith —Mature Saprolite
A mature saprolite (clayey silt) is at the surface over a majority of the site and beneath the fill
material in developed areas of the site. X-ray diffraction analysis of clayey silt samples showed the
primary mineral components as Kaolinite (Al2Si2O5), Quartz, and Muscovite (KAI2[Si,AI]4O10[OH]2)
with secondary components of Halloysite (Al2Si2O5[OH]4) and Goethite ([Fe0.93Alo.07]O[OH]). In
some portions of the site the unit can be subdivided into an upper and lower section based on
moisture content. In the southwest portion of DC-2, the drier upper section is
between 15 to 25 feet thick with some inter-fingering wet zones. Color of this unit can vary from
yellowish- and reddish-brown to brown. Relict manganese-filled fractures, manganese porous
zones, and fine laminae have been noted in this zone with increasing presences with depth. Zones
within this unit can be firm (with low relative moisture) to very soft(higher relative moisture).
The top of the lower section of the mature saprolite, where present, begins between 25 and 30 feet
below ground surface (bgs). It is characterized by higher moisture content, and is
B2
I

Walter Kidde Portable Equipment,Inc.
Mebane, North Carolina
UIC Permit Application
Attachment B—Hydrogeologic Description
commonly saturated. Monitoring wells screened in this interval have a horizontal hydraulic
conductivity up to 1E-03 centimeter per second (cm/sec). Field inspection of cores indicates that
relict manganese-filled fractures and porous zones are common, some of which are believed to be
primary preferential groundwater pathways. In most cases the unit has a soft consistency due to
the moisture content.
Regoiith —Immature Saproiite
The lower boundary of the mature saprolite or the upper boundary of the immature saprolite is not
well defined across the area. In some instances a 20- to 25-foot thick section of harder, drier
saprolite is present starting approximately 40 feet bgs and in other areas the wet zones continue to
depth. This is typical of saprolite since the underlying bedrock may weather unevenly. This would
be reflected in the overlying saprolite; i.e., a thicker section of saprolite overlying less resistive
bedrock would be characterized by greater secondary porosities resulting in more moisture being
stored in the unit. The saprolite derived from more resistant bedrock would have less
secondary porosity and thereby would be able to store less moisture.
Color of this unit varies from yellowish- and reddish-brown to brown to olive brown with depth.
Relict manganese-filled fractures, manganese porous zones, and fine laminae are common
throughout the upper and mid-portions of the interval. Based on the slug test data collected in
July 2011, the immature saprolites have lower horizontal hydraulic conductivities compared with the
mature saprolite above by one to two orders of magnitude. Moisture content is variable and
dependent on the presence of secondary porosity features. As explained above, secondary porosity
is dependent on the resistance or lack thereof in the underlying bedrock.
Transition Zone
At approximately 60 to 65 feet bgs the immature section of saprolite becomes harder and drier;
rock fragments begin to appear within the saprolite matrix. This zone is indicative of a more
competent saprolite and has been identified as the upper portion of the transition zone. Based on
previous drilling across the site, the thickness of the transition zone averages approximately 15 feet
in thickness. With depth, bedrock fragments (boulders, panicles, etc.) begin to appear and the
saprolite becomes less weathered as the formation transitions eventually into the parent bedrock.
Due to drill rig limitations, the terminal depth for most borings across the DC-2 area occurred within
the lower portion of transition zone at approximately 64 to 74 feet bgs. The lithology within this
zone consisted of dense firm clayey silt, with weathered rock fragments and mica, little or no
manganese, and very little moisture. The color of the saprolite varied from tannish brown to
light olive brown.
At two monitoring well locations (MW048 and MB051), though, the hard dry saprolite of the
transition zone is a softer moist unit. These softer zones likely represent sections of saprolite that
formed over fractured bedrock where natural chemical weathering was more aggressive. In
MB051, a one-foot interval of sub-angular gravel size rock fragments in the saprolite matrix was
B-3

Walter Kidde Portable Equipment,Inc.
Mebane, North Carolina
UIC Permit Application
Attachment B—Hydrogeologic Description
encountered just above a weathered bedrock/transition zone. It is unknown what the areal extent
of this gravel zone is, or whether it has continuity across the DC-2 area.
Bedrock
Core samples retrieved from deep onsite borings indicate bedrock is metavolcanic (felsic to
intermediate) in composition, a classification that is consistent with hydrogeologic units mapped by
Daniel and Payne (1990). Encountered beneath the facility at depths ranging from approximately
67 feet bgs (location MB006) to 81 feet bgs (location MCO29), many of the bedrock core samples
displayed evidence of ductile deformation, most likely the result of compressional and/or shear
stresses. Other notable features that suggest an initial volcanic origin include epiclastic rocks,
brecciated intervals, lithic fragments, and apparent relict basaltic flow structures. Overall, most of
the bedrock core samples collected onsite were dense, fine-grained, gray to greenish-gray, and
exhibited significant weathering to clays (e.g., chlorite) and other alteration minerals.
3. Hydraulic Conductivity,Transmissivity, and Specific Yield
Remedial injections in the soil source area are proposed from 10 to 25 feet bgs, and in the aqueous
source area from 25 to 50 feet bgs into the immature saprolite. Hydraulic conductivity,
transmissivity, and the specific yield are discussed below organized by zone.
Regolith —Saprolite (Mature and Immature)
Data indicate that porosity and specific yield, although variable, changes only slightly with depth
through the saprolite profile; once the transition zone is reached, porosity and specific yield begin
to decrease sharply. Hydraulic conductivity results from Shelby tube samples ranged from 2.95E-6
to 1.23E-5 cm/sec, with lower values obtained from the 45- to 50-foot zone.
Slug tests were performed on select wells during the course of the CSA and subsequent
investigations. Data are summarized on Table B-1.
Bedrock Groundwater Zone
Porosity and groundwater storage are the major differences in the water-bearing characteristics of
the regolith and bedrock (Daniel and Dahlen, 2002). The majority of groundwater beneath the Site
is held within the porosity of the regolith, and slowly infiltrates the deeper bedrock. Whereas
regolith can store groundwater in pore spaces between particles, the dense crystalline bedrock
does not have any significant intergranular porosity. Instead, groundwater resides in
narrow fractures and other secondary porosity features within the bedrock.
Each well cluster is located within or adjacent to a suspected contaminant source at the site
(i.e., Hazwaste Storage Area, East Environmental Shed, and the former fire extinguisher test area
[FTA]), and includes a shallow, intermediate, and deep well. Under static conditions
(i.e., no pumping), groundwater levels showed a similar pattern, with respect to vertical gradient,
among the wells in each of the three respective clusters. All three clusters show measurable
upward vertical gradients between the respective shallow and intermediate wells. Similarly,
B-4

Walter Kidde Portable Equipment,Inc.
Mebane, North Carolina
UIC Permit Application
Attachment B—Hydrogeologic Description
upward vertical gradients are evident between shallow and deep wells, near MW019 and MW029,
with a downward gradient at MW006. Historical water levels were tracked for multiple monitoring
well clusters. Response to environmental conditions appears to be fairly rapid since the
water levels in all zones respond fairly quickly to changing conditions.
4. Depth to the Mean Seasonal High Water Table.
In general, the groundwater table is encountered between approximately 12 and 25 feet bgs across
the Site. Remedial injections are proposed in the vicinity of MW042, MW043, MW044, MW045,
MW046, MW047, MW048, and MW049. Monitoring wells MW044 to MW049 were installed in 2011,
thus seasonal water level data are lacking. Based on measurements from MW042 and MW043 in
September 2007, November 2008, July 2009, January 2010, and August 2011, the mean seasonal
high water table was observed in January 2010 at 22.33 feet bgs in MW043.
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2 cc eu

Walter Kidde Portable Equipment,Inc.
Mebane,North Carolina
UIC Permit Application
Attachment D—Injection Rationale
ATTACHMENT D—INJECTION RATIONALE
1. Goals of the Injection Project
Groundwater contamination at the site poses no threat to human health, as groundwater is not
consumed on- or offsite as potable water. However, groundwater contamination does exceed
NC 02L groundwater quality (02L GWQ) standards. In accordance with NCAC 02L.0106, "the goal
of any required corrective action shall be restoration to the level of the standards, or as closely
thereto as is economically and technology feasible." Therefore, preliminary remedial action
objectives (RAOs) have been as follows:
• Reduce soil and groundwater source area concentrations
• Minimize shallow groundwater impacts on the ephemeral drainage-way along the
eastern property line
• Minimize shallow groundwater impacts on top-of-bedrock and bedrock groundwater
The goals of this injection project are to promote conditions in-situ for accelerated dechlorination of
chlorinated volatile organic compounds (CVOCs) via abiotic and microbial processes in the soil and
groundwater soil areas. This will be accomplished with the following elements:
• DC-2 Soil Source Area —Injection of Emulsified Oil/ Zero Valent Iron (EZVI)
• DC-2 Groundwater Source Area — Injection of zero valent iron (ZVI), Adventus' Enhanced
Hydrogen Compound (EHC), propionate, hydrolyzed kelp, and nutrients
• Site-Wide Groundwater Monitoring
Proposed areas for injection are displayed in Figure H-4-2 and discussed below.
a. DC-2 Soil Source Area— EZVI
One 50 foot by 50 foot soil source area in the vicinity of Building DC-2 and MW043 will receive
injections of EZVI. In the EZVI approach, nano- and micron-scale ZVI are suspended in
emulsified oil. The injectate is delivered to the subsurface using a high density of DPT points.
Sorbed contamination (which is hydrophobic) partitions preferentially into the oil micelle, where it is
degraded abiotically with the suspended ZVI. Design parameters are shown in Table D-1 below.
D-1

Walter Kidde Portable Equipment,Inc.
Mebane, North Carolina
UIC Permit Application
Attachment D—Injection Rationale
Table D-1
DC-2 Soil Source Area—Injection Design Assumptions
Area 2,500 ft2
Number of Injection Points 32*
1 Total Depth of Contamination 10 to 25 feet bgs
4 intervals per point
• 10 to 12 feet
• 14 to 16 feet
• 18 to 20 feet
Treatment Interval • 22 to 24 feet
Radius of Influence 10 feet
Substrates/application rates per interval 40 gallons EZVI
Notes:
ft2 — square feet
I bgs below grade surface
EZVI emulsified zero valent iron
• — If the formation does not accept the injectate, additional DPT points will be used to deliver the design
quantities.
b. DC-2 Groundwater Source Area—ZVI/EHC/Propionate/Kelp/Nutrients
The groundwater source area, represented by seven 50 foot by 50 foot areas shown on
Figure H-4-2, in the vicinity of and to the northeast of Building DC-2 will receive injections of
ZVI/EHC/Propionate/Kelp/nutrients. In the ZVI/carbon substrate approach, ZVI provides
abiotic treatment via anaerobic iron corrosion reactions, followed by reductive dechlorination of
CVOCs on the iron surface. Carbon substrates (solid phase carbon provided by
Adventus' EHC product, sodium propionate, and hydrolized kelp) are consumed by available
microbes, driving the aquifer deeply anaerobic, making ZVI reactions more efficient. This process
is also compatible with biological reductive dechlorination and existing cometabolic processes. In
this synergistic approach, the following elements are combined in the injectate:
• ZVI
• Adventus' EHC(solid-phase carbon and ZVI)
• Hydrolized kelp
• Calcium propionate
• Sodium sulfite (oxygen scavenger)
• Yeast extract, vitamins (B2, B12), and nutrients
The three carbon sources (calcium propionate, hydrolyzed kelp, and EHC) provide carbon over a
long release profile (0 to 100 days, 60 to 500 days, and 365 to 1500 days, respectively), so that
biological activity is stimulated over the long term.
IIt should be noted that the dissolved, mobile carbon substrates (kelp, propionate) may migrate
with groundwater from the source area and move downgradient (advert) with groundwater flow;
this will stimulate biological processes (via reductive dechlorination or cometabolic processes). For
D2

Walter K/dde Portable Equipment,Inc.
Mebane,North Carolina
UIC Permit Application
Attachment D—Injection Rationale
example, any methane production within or downgradient of the source area will enhance
degradation in downgradient areas. Design parameters are shown in Table D-2 below.
Table D-2
DC-2 GW Source Area—Injection Design Assumptions
Area 17,500 ft2
Number of Injection Points 56
Total Depth of Contamination 25 to 50 feet bgs
6 intervals per point
• 25 to 27 feet
• 30 to 32 feet
• 35to37feet
• 40 to 42 feet
• 44to46feet
Treatment Interval • 48 to 50 feet
Radius of Influence 10 feet
Substrates/application rates per interval ZVI—73.3 lbs
EHC—66.6 lbs
Hydrolized kelp—14.6 lbs
Calcium propionate—33.3 lbs
Sodium sulfite—5 lbs
Yeast extract—5 lbs
B2-139.36g
B12-20g
Nutrients—5 lbs
Notes:
ft2 — square feet
bgs — below grade surface
ZVI — zero valent iron
lbs — pounds
* — If the formation does not accept the injectate, additional DPT points will be used to deliver the design
quantities.
2. Calculations
Volume and concentrations of each injectant were based on the estimated mass and concentration
of CVOCs present in the soil and groundwater at the Site.
The Freundlich equation (qe=KCe 1/n) is an adsorption isotherm that relates the concentration of a
solute on the surface of an adsorbent to the concentration of the solute in a liquid. The Freudlich
equation is used to determine the theoretical mass of contamination adsorbed to the soil. The
mass of contaminant in the soil was determined using the soil adsorption correction.
Soil concentrations in the source area are assumed to be elevated; therefore, an elevated soil
adsorption correction of 10% was used. The K constant is a figure relating the capacity of the
adsorbent for an adsorbate and the 1/n constant is a function of the strength of adsorption
(American Water Works Association, Water Quality and Treatment, 1999). The theoretical values
of K and 1/n are found in the following references: (Dobbs and Cohen, 1980/Faust and Aly, 1983).
1 D3

Walter Kidde Portable Equipment,Inc.
Mebane,North Carolina
UIC Permit Application
Attachment D—Injection Rationale
The proposed remedial technology in the groundwater source zone is a combination of abiotic and
biotic processes incorporating zero valent iron particles and nutrients and hydrogen sources for
accelerated biological mineralization. The concentration of iron and organic hydrogen donors is
based on the current groundwater concentrations. Corresponding injectant dosage calculations
performed by IET are in Table D-3.
For the soil source area, an effective porosity of 20% was assumed in the EZVI treatment area.
Based on the effective porosity of 20% due to the subsurface lithology, a 10% targeted porosity
was used. Corresponding injectant dosage calculations performed by IET are in Table D-3.
3. Description of the Reactions between Injectant and Contaminants
Zero Valent Iron (ZVI): ZVI may chemically be thought of having been the product of the
positively charged metal ions receiving electrons to become the electrically neutral pure metal. The
term "reduction" is applied to any chemical reaction that added electrons to an element. Thus ZVI
is a reduced material. In a similar manner, the chemical term "oxidation" refers to any chemical
reaction that removes electrons from a material. For a material to be reduced, some other material
must be oxidized. In the reduction of a chlorinated compound the zero valent iron is oxidized. ZVI-
enhanced abiotic degradation of CVOCs is essentially a reductive dechlorination process, which uses
granular cast iron as the reducing agent, and produces final reaction products such as ethane,
ethene, and chloride ions in the degradation of TCE. During this treatment process, the corrosion of
iron by water dominates the chemical processes. The corrosion of iron by water results in ferrous
ion generation, hydroxyl ion generation, and hydrogen gas generation. This results in a decrease in
ORP (oxidation/reduction potential; that is, reducing conditions are produced) and an increase in
pH. Accordingly, the end products of this reaction are ferrous iron, chloride ions, and the
dehalogenated compound.
Frequently remedial sites show insignificant or incomplete dechlorination, especially those with high
aquifer sulfate levels. It is generally overlooked that the rapid conversion of sulfate to toxic free
sulfide during bacterial reductive dechlorination plays a significant role in the"stalling"of the biotic
stalling frequently observed. Accumulation of free sulfide is especially important in sites that
display both high sulfate and low available iron. Reductive dechlorination inhibition by free sulfide
has been observed in microcosms conducted for high sulfate field sites. Free sulfide toxicity to
microorganisms can be prevented if ferrous iron precipitates the free sulfide. Further, iron sulfide
mineral precipitates have been shown to catalyze reductive dechlorination of chlorinated solvents at
rates comparable to metallic iron, on a surface area normalized basis. Microcosms performed at
high sulfate sites have been showed to both remove free sulfide toxicity to dehalogenating bacteria
and to enhance catalytic reductive dechlorination when ferrous iron is added. Further, ferrous iron,
itself, may act as an electron donor.
Injected, colloidal reactive iron is a promising technology, which may be applied, in a synergistic
approach with compatible technologies. There are two primary reactions with CAHs that take place
which will consume the iron and require stoichiometric consideration:
D-4

Walter Kidde Portable Equipment,Inc.
Mebane,North Carolina
UIC Permit Application
Attachment D—Injection Rationale
• the anaerobic iron corrosion reaction in which water is disassociated to form hydrogen gas;
and
• the direct adsorption of a chlorinated hydrocarbon onto the surface of the iron, followed by
reductive dehalogenation.
Recent research on elemental iron systems suggests that four mechanisms are at work during the
reductive process:
• First, the Fe° acts as a reductant by supplying electrons directly from the metal surface to
an adsorbed halogenated compound.
• Second, hydrogen gas is generated by the anaerobic corrosion of the metallic iron by water.
• Third, metallic iron may act as a catalyst for the reaction of hydrogen with the halogenated
hydrocarbon using the hydrogen produced on the surface of the iron metal as the result of
anaerobic corrosion with water. Theoretically, these reactions are not kinetically effective
without a catalyst; thus, it is thought that impurities in the iron or surface defects act as
that catalyst.
• Fourth, solubilized ferrous iron can also act as a reductant, albeit at a rate at least an order
of magnitude slower.
Emulsified Oil Zero Valent Iron (EZVI): EZVI is ZVI entrained in emulsified oil. EZVI is a
National Aeronautics and Space Administration- (NASA-) patented product that dechlorinates dense
non-aqueous phase liquids (DNAPLS), such as tetrachloroethylene (PCE) and trichloroethylene
(TCE), leaving only the carbon skeleton of the original molecules, and thereby detoxifying the
original contaminants. Basically, EZVI is an emulsification of vegetable oil with nano- to microscale
iron particles, in which a water droplet containing iron powder is surrounded by a thin layer of oil to
form micelles. The micelles are hydrophobic and denser than water; therefore they sink in the
water table until coming in contact with DNAPLs or high concentrations of PCE and TCE. Because
the micelles containing the iron are hydrophobic, the iron is protected from chemical reactions with
nontargeted chemical species that cannot dissolve through the oil in the outer layer. In other
words, the solubility characteristics of the DNAPLs and EZVI are very similar. Therefore the target
chemicals (DNAPLs or high concentrations of PCE and TCE) preferentially dissolve into the
EZVI micelles where they react with the iron particles and are dechlorinated. In addition to being
very efficient at abiotic remediation of DNAPL, EZVI also stimulates the processes involved with
bioremediation of chlorinated contaminants through the introduction of an available hydrogen
source, emulsified oil.
When EZVI is introduced into the subsurface, dense chlorinated aliphatic compounds such as PCE
and TCE diffuse through the oil membrane of the emulsion particle and undergo reductive
D-5

Walter Kidde Portable Equipment,Inc.
Mebane,North Carolina
UIC Permit Application
Attachment D—Injection Rationale
dechlorination due to the ZVI particles. Reductive dechlorination via ZVI is a surface area-mediated
1 reaction meaning that the reaction only occurs when the contaminant of interest and the ZVI come
in direct contact. Due to the hydrophobic oil surrounding the iron particles, the DNAPL is able to
partition into the hydrophobic oil layer and then come in direct contact with the ZVI. The final
reaction products, ethene and ethane, diffuse out of the hydrophobic media and therefore are
introduced back into the surrounding aqueous phase. EZVI is one of the few methods available
that can directly treat the DNAPL source and is more cost effective than other source area
treatments such as thermal heating, chemical oxidation, and pump and treat. Unlike the other
source area treatment alternatives, EZVI does not cause mobilization of the DNAPL and does not
cause the volatilization of the DNAPL which can cause vapor intrusion and health and safety issues.
The EZVI provided for the Site is composed of 17% iron with a size range of 0.1 to 5 micron. The
EZVI is also composed of 30-40% food grade soybean oil, 1 to 5% sorbitan trioleate, an
emulsifying agent, and 40 to 50% water. The viscosity of the EZVI is between 800 and
1,200 centipoise.
Oxygen Scavenger (sodium sulfite): Reductive dechlorination only occurs in the absence of
oxygen; and, the chlorinated solvent actually substitutes for oxygen in the physiology of the
microorganisms carrying out the process. As a result of the use of the chlorinated solvent during
this physiological process it is at least in part dechlorinated. The site shall have introduced to the
subsurface an oxygen scavenger to ensure that this process would occur immediately.
Propionate: An organic hydrogen donor with an expected release time of zero to 100 days.
Some electron donors are more efficient than others at producing the hydrogen necessary for
dehalogenation, and a fundamental question is why this is the case. One very plausible explanation
is that various groups of microorganisms compete for hydrogen, and that dehalogenating
microorganisms can survive better than others at very low hydrogen concentrations (Fennel et al.,
1995; Smatlak, et al., 1996; Yang and McCarty, 1998). On this basis, slug addition of a compound
such as formate, ethanol, or glucose is not as effective for dehalogenation as propionate because
the former compounds are converted rapidly to hydrogen and acetate, and the latter is not. The
rapid conversion is a result of more favorable thermodynamics with respect to hydrogen formation.
Such rapid conversion places hydrogen in a concentration range where methanogens and sulfate
reducers can compete effectively with dehalogenators.
Hydrolyzed Kelp: An organic hydrogen donor with an expected release time of 60 to 500 days.
Seaweeds such as Ascophyllum nodosum (rockweed, knotted kelp, knotted wrack) are brown algae
that are widely available in both the wild and through cultivation all over the world.
Ascophyllum nodosum is native to the northern Atlantic and has wide variety of important nutrients
beneficial to anaerobic processes. Ascophyllum nodosum has an analyzed chemical composition of:
D-6

Walter Kidde Portable Equipment,Inc.
Mebane, North Carolina
UIC Permit Application
Attachment D—Injection Rationale
• 20 to 26% of sulphate uronic acids
• 5to8% ofMannitol
• 2to5% ofLaminaran
• 5 to 15% of fucoidin
• 2,500 to 2,000 milligrams per kilogram (mg/kg) of Ascorbic acid
• 150 to 300 mg/kg of Tocopherols
• 30 to 60 mg/kg of Carotenes
• 10 to 30 mg/kg of Niacin
• 0.1 to 0.4 mg/kg of Biotin
• 0.2 to 1 mg/kg of Folic acid
• 5 to 10 mg/kg of Riboflavin
• 1 to 5 mg/kg of Thiamine
The species also has an assortment of elements including sulfur, potassium, chlorine, sodium,
magnesium, calcium, phosphorous, bromine, cobalt, copper, iron, iodine, zinc, nickel and
0.004 mg/kg of Vitamin B12i and 10 mg/kg of Vitamin K. Many kelps also are highly alkalizing; as a
consequence their addition counter-acts the natural production of acids produced by-way of
anaerobic dechlorinization. Kelps are commercially available dried, in multiple forms, and in large
quantities. When emplaced in groundwater and soils impacted by chlorinated solvents such as
tetrachioroethane, PCE, trichloroethane, TCE, carbon tetrachloride and their anaerobic daughter
products, the micro-dried seaweed offers all the needed components for effective and rapid
remediation through biological degradation.
When anaerobic bacteria digest sugars and carbohydrates, they convert the sugars and
carbohydrates into gases, most commonly hydrogen. In addition to essential vitamins and
nutrients noted above, the varied soluble carbohydrates in kelp provide a longer lasting source of
organic hydrogen than is commercially available in alternative remedial materials. It also provides
buffering capacity for the sustained, biologically mediated anaerobic dechlorination.
Yeast Extract: An organic hydrogen donor with an expected release time of 150 to 365 days.
Yeast extract provides a variety of organic hydrogen donors capable of slow release profiles as well
as significant biological components not available through other media.. In particular, yeast extract
provides an abundant source of priming ATPase. By pumping protons, ATPase regulates
intracellular pH and provides the driving force for nutrient uptake. ATPase is activated in the
presence of glucose through transcriptional and post-transcriptional mechanisms that increase the
level of ATPase activity in cells. Glucose triggers a transduction signal mechanism leading to the
activation of the plasma membrane ATPase, a complete system acting in this process formed by
specific glucose receptors, G protein(s), internal signals and the phosphorylating and activating
enzyme(s). The glucose-induced activation of ATPase requires the presence of Snf3p (a
glucose sensor) found in abundance in the provided yeast extract.
EHC: An organic hydrogen donor with an expected release time of 365 to 1500 days.
D-7

1 Walter Kidde Portable Equipment,Inc.
Mebane,North Carolina
UIC Permit Application
Attachment D—Injection Rationale
The hydrophilic organic component of EHC, which is composed of cellulose and hemicellulose, may
be treated during the manufacturing process so that the components more easily undergo
hydrolysis to glucose while maintaining an overall longevity of 3 to 5 years. Hydrogen gas is
produced during glucose fermentation via several enzymatic pathways, depending on site
conditions and microbial assemblages:
Glucose + 6H2O —> 6CO2 + 12H2
Glucose + 2H2O —>2Acetate + 2CO2 + 4H2 + 2H+
EHC also contains ZVI, which, as it corrodes, also serves as a source of hydrogen. Water corrosion
of granular iron produces hydrogen and hydroxide resulting in an increase in pH and decline in
redox potential (Eh):
Fe° + 2H2O—. Fe2+ + H2(aq) + 20H-
Nutrient: Critical to the sustained microbial activity and general microbial health is sufficient bio
available nutrient. Nitrogen and o-PO4 will be incorporated into the injection program such that
organelle and ATP-ADP formation is not limited throughout the microbial respiratory process.
Vitamins: Recent studies suggest that metal-containing coenzymes, found in certain types of
anaerobic microorganisms, and can reductively dechlorinate one- and two-carbon solvents.
Cobalt-containing corrinoid cofactors such as vitamin B12 mediate the reductive dechlorination of
carbon tetrachloride and tetrachloroethene. In these biological systems the rate-limiting step to
complete dechlorination to ethylene is the last stage conversion of vinyl chloride. B12 acts as an
electron carrier, and enhances the degradation process. The cobalt core of B12, and the various
oxidation states the cobalt obtains, allow for the electron transfer intra-cellularly. The cobalt core
has also been seen to catalyze the surface reaction of the iron, lowering the necessary activation
energy required for the electron transfer.
4. Summary of Modeling or Testing
The recommendations presented herein are based on research and testing performed by each of
the injectant's providers during the development of their product and IET's experience at over
200 similar sites.
D-8

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Walter Kidde Portable Equipment,Inc.
Mebane,North Carolina
UIC Permit Application
Attachment E—Injection Procedure and Equipment
ATTACHMENT E—INJECTION PROCEDURE AND EQUIPMENT
1. Construction Plans and Materials
As described in Section D.1, treatment in the soil source area includes injection of Emulsified Zero
Valent Iron (EZVI) into 32 locations over an approximately 2,500 square foot area. At each
location, injection will be performed at multiple depths ranging from 10 to 25 feet bgs. Treatment
in the groundwater source area includes injecting IET's proprietary mixture of Zero Valent Iron
(ZVI)/Enhanced Hydrogen Compound (EHC)/Propionate/Kelp/Nutrients into 56 locations over an
approximately 17,500 square foot area. At each location, injection will be performed at multiple
depths from 25 to 50 feet bgs. Materials for the injection event include IET's proprietary injection
system, a direct push technology (DPT) rig, injection substrates, and water supplied by the
municipal system. No waste streams will be generated. Additional information on the
injection procedures and equipment is provided below.
Note: If the formation does not accept the injectate, additional DPT points will be used to deliver
the design quantities. The DPT rig will be offset, and the injection rods will be advanced to the
target interval. All injections will be performed within the treatment area footprint shown in
Figure H-4-2.
2. Operation Procedures
The injection points will be advanced via DPT, utilizing a Geoprobe 6620 or 7720. The injection
rods will consist of IET's proprietary injection system with retractable injection zones driven to the
desired injection depth using the DPT rig. After the DPT rig has advanced the injection tool to the
prescribed depth, the following injection sequence will be performed:
• Nitrogen gas will be injected, at approximately 20 pounds per square inch (psi) for an
EZVI injection, or 175 psi for the ZVI/EHC/Propionate/Kelp/nutrients mixture, into the
stratum to establish delivery pathways and voids in the soil. Since the stratum is targeted
for anaerobic processes, nitrogen gas is utilized so oxygen will not be introduced.
• After the nitrogen gas is delivered, the substrate is immediately injected into the voids.
• Nitrogen gas is re-injected to clear the lines of all injectants and force them into the
stratum.
• All injection down-hole equipment will be removed, and the boring will be abandoned using
hydrated bentonite.
IET's injection trailer is equipped with tanks for mixing the injection solutions. Municipal water will
be used for the solution mixing. All solutions will be injected at ambient temperatures.
Stainless stain pipes will extend from the mixing tank to the injection pump where it will travel
through a high pressure hose to the injection rod. A pressure gauge, shut-off valves, and pressure
bleed-off will also be installed in-line. Injection will be performed using a double diaphragm pump.
E-1

Walter Kidde Portable Equipment,Inc.
Mebane,North Carolina
UIC Permit Application
Attachment E—Injection Procedure and Equipment
Injection pressures will be approximately 50 to 150 psi and injection flow rates are estimated
between 3 and 5 gpm. The injection pressure will be monitored continuously using a pressure
gauge and the injection rate will be adjusted using the injection pump and valves. After injection,
the injection pump will be turned off and the shut-off valve will be closed. The residual pressure in
the formation will then be monitored until a safe level is reached. This process will then be
repeated at each injection location.
3. Diagram of the Surface and Subsurface Portions of the System
A detailed description of IET's equipment is provided below along with a conceptual diagram of the
surface and subsurface components, and a photo of an injection rod.
• Injection Lines: high-pressure stainless steel, braided rubber one-inch diameter hoses
• Injection Trailer: IET self-contained injection trailer, consisting of two 120-gallon conical
tanks capable of maintaining unto 30% solids as a suspension via lightning mixers;
on-board generator, all stainless-steel piping system, 2-inch pneumatic diaphragm pump
with an operating pressure of 110 psi.; on-board 25 cubic feet per minute (CFM)/175
psi-gauge compressor with 120 gallons of air storage; and self-contained eye wash and
safety shower.
• Injection Rods: IET proprietary injection rods with retractable injection zones and
backflow protection. Injection zones of 18-inches are to be used in combination with 24-inch
injection AWJ-Rods where appropriate.
Diagram of Injection System Components
IET Trailer DPT Vendor
II
Injection interval 1 �--
Injection interval 2
Injection interval 3 '
Injection interval 4
E-2

Walter Kidde Portable Equipment,Inc.
Mebane, Noith Carolina
UIC Permit Application
Attachment E—Injection Procedure and Equipment
Photo of Injection Rod
4. Injection Schedule
Injection is anticipated to begin in April 2012. Injection in the soil source area is expected to last
approximately four days. Injection in the groundwater source area is expected to last
approximately ten to fifteen days.
E-3

Walter Kidde Portable Equipment,Inc.
Mebane, North Carolina
UIC Permit Application
Attachment F—Monitoring Plan
ATTACHMENT F— MONITORING PLAN
Soil and groundwater sampling is proposed to gauge the effectiveness of the remedial injection.
Sampling is described below.
1. Remedial Effectiveness Soil Sampling in the Soil Source Treatment Area
Biennial soil sampling is proposed from 2013 to 2015 in the soil source treatment area.
• Soil sampling includes two phases:
— Completing 15 soil borings in the treatment area, and collecting samples from the
10- to 15-foot, 15- to 20-foot, and 20- to 25-foot intervals to gauge treatment
effectiveness.
— Establishing a 50-foot grid across the entire DC-2 remediation area. A random
sampling approach, as outlined in the Registered Environmental Consultant (REC)
guidance, Appendix C, Section C.2.1.3 would be used to collect surface soil samples
(0- to 6-inches) from this grid.
• Samples will be submitted for VOC analysis using SW-846 method 8260B.
2. Remedial Effectiveness Groundwater Sampling
Groundwater sampling is proposed to monitor the effectiveness of the remedy through 2021. The
monitoring program will consist of sampling 12 existing wells in the vicinity of the treatment area
quarterly in 2012; the monitoring frequency will be adjusted following review of quarterly data in
response to the aquifer's reaction rates.
The monitoring wells in the groundwater source area include:
MW042 MW045 MW048 MW052
MW043 MW045 MW049 MW015
MW044 MW047 MW050 MW033
Sample parameters include:
• VOCs by SW-846 Method 8260B
• EPA 300 (sulfate, nitrate, chloride)
• Dissolved gases (methane, ethane, ethene)
• Hydrogen
• Total iron and manganese by SW-846 Method 6010
• Total organic carbon by SW-846 Method 9060
• Alkalinity
F-i

Walter Kidde Portable Equipment,Inc.
Mebane, North Carolina
UIC Permit Application
Attachment F—Monitoring Plan
• Field parameters
— Dissolved oxygen (DO)
- Oxidation/reduction potential (ORP)
— Ferrous iron
— Sulfide
• Supplemental parameters (as needed, parameters may be discontinued if sampling
determines these constituents are not primary constituents of concern in this area)
— Chromium by SW-846 Method 6010
— Hexavalent chromium by SW-846 Method 7196
— 1,4-Dioxane by EPA Method 522
Additionally, site wide groundwater wells outside the treatment areas will be sampled periodically to
gauge contaminant trends through 2021; this includes wells in the top of bedrock and
east property line (EPL) areas, as well as the DC-3, new fire extinguisher testing area (NTA), and
mid-plume areas. From 2021 through 2041, wells inside the DC-2 treatment area will be
incorporated into the monitoring program. Through 2021, this alternative would monitor
select wells outside active treatment areas for CVOCs, 1,4-Dioxane, chromium, and BEHP.
Wells would be monitored to assess potential migration of the plume. A total of 50 wells would be
incorporated into this program, including.
NTA DC-3 Area Mid-Plume Area Dow •radient TOB/EPL Areas
MW002 MW006 MW007 MW016 New downgradient MB051 MW021
(shallow) _
MW003 MB006 MW008 MW018 New downgradient MB019 MW022
(TOB)
MD003 MC006 MW009 MW019 MW025 MC019 MW023
MW035 MW017 MW010 MW020 MW026 MD022 MW024
MW038 MW029 MW027 MW030 4 additional 4 additional
TOB wells EPL wells
MB029 MW028 MW031
MCO29 MW041 MW034
Notes:
TOB—top of bedrock
EPL—east property line
Installation of 10 new monitoring wells will be required to monitor the northeast end of the
groundwater plume, as well as provide supplemental monitoring of the top-of-bedrock and
EPL areas. In accordance with REC program guidelines, the monitoring program would be
quarterly the first year, and then the frequency would be adjusted based on analysis of the
quarterly monitoring data.
F-2

Walter Kidde Portable Equipment,Inc.
Mebane, North Carolina
UIC Permit Application
Attachment G—Well Data
ATTACHMENT G—WELL DATA
Requests to the North Carolina Department of Environment and Natural Resources and the
Alamance County Health Department in October 2011 did not identify any potable/non-potable
(i.e., agricultural) wells offsite within 1/4 mile of the proposed injection locations. One abandoned
well was identified on parcel #163657 (abandoned October 10, 2006), which is immediately outside
the 1/4 mile radius. A windshield survey of properties within the 1/4 mile radius confirmed these
findings.
Multiple groundwater monitoring wells are present onsite, which are used to monitor contamination
at the Walter Kidde Portable Equipment, Inc., facility (Kidde). The enclosed tables provide a
tabulation of data for all existing wells within 1/4 mile of the injection area which penetrate the
proposed injection zone. These tables provide a description of the wells use, total depths,
screened intervals, and analytical results. Analytical results are from sampling conducted in
August 2011.
The facility uses one production well, PW-1, to maintain water levels in a 0.5-acre pond on the
south side of the facility. The well is set in bedrock approximately 256 feet below ground surface
(bgs), and is not expected to be impacted by saprolite remediation efforts in the 10- to 50-foot bgs
interval.
All site monitoring wells, PW-1, and Parcel #163657 are shown on Figure H-2.
G-1

Appendix G,
Table G-1
Volatile Organic Compounds-Groundwater
Sample Location:) M8006 M8019 MB029 MCOD6 MC019 MCO29 MD022 MD022 MW006 MW007 MW008 MW009 MWOI0 MW011 MW012 MW013 MW014 MW015 MW016
Sample ID: KIDGM8006201106 KIDGMB019201106 K10GM8029201106 KIDGMC006201106 010GMC019201106 KIDGMCO29201106 KIDGMD022201106 KIDCMD022201108 KIDGMW006201106 KIDGMW007201106 KIDGMW0 08 20 11 0 6 KIDGMW009201106 KIDGMW010201106 KIDGMW011201106 KIDGMW012201106 KIDGMW013201106 K10GMW014201106 KIDGMW015201106 KIDGMW016201106
Sample Date: 06/21/2011 06/15/2011 06/22/2011 06/21/2011 06/16/2011 06/22/2011 06/15/2011 08/08/2011 06/21/2011 06/23/2011 06/22/2011 06/22/2011 06/23/2011 06/14/2011 06/14/2011 06/13/2011 06/13/2011 06/21/2011 06/23/2011
Method CAS No. Ana242 021.Standard 2011 Unts
-__.
SW8260 71-55-6 1,1,1-Trichloroetlrane 0.2 mg/I 0.000383 0.0005 U 0.0005 U 0.00052 0.00064 0.0005 U ,: 0.0005 U u.Uuut;u •:..,-. c•xs'�s.. 0.00021] 0.0005 U 0.0005 U ,.....xs U 00005 U za.C�a+n U 0.0005 U
SW8260 79-34-5 1,1,2,2-Tetrachloroethane 0.0002 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U N. 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 79-00-5 1,1,2-TridtIoroethane 0.0006 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.00D5 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
5W8260 75-34-3 1,1-Diddoroeth80e 0.006 mg/I 0.00037 3 0.0005 U 0.0005 U 0.00075 0.00063 0.00042 3 NA 0.0005 U 0.00021 3 0.00068 0.00019 3 0.0012 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0006 0.0005 U
SW8260 75-35-4 1,1-01dtloroethene 0.007 mg/I u,,,,.,.. 0.0082 0.00033 3 0.0005 U 0.0112 0.0005 U 0.0054 NA 0.0005 U 0.0018 0.0055 0.0011 0.0054 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0015 0.0033
SW8260 563-58-6 1,1-Dlchlompropene Not Listed mg/I 0.0005 U 5.0095 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 87-61-6 1,2,3-Trichlombenzene Not Listed mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 96-18-4 1,2,3-Trichloropropane 0.0110005 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 120-82-1 1,2,4-Trichlorobenzene 0.07 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 95-63-6 1,2,4-trimethylberome 0.4 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 106-93-4 1,2-Dibromoethane 0.00002 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 95-50-1 1,2-Dichlorobenzene 0.02 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 107-06-2 1,2-Dichloroethane 0.0004 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
5558260 78-87-5 1,2-Dichloropropane 0.0006 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
5W8260 108-67-8 1,3,5-trimethybenzene 0.4 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U , 0.0005 U 0.0005 U
5568260 541-73-1 1,3-Dichlorobenzene 0.2 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
5W8260 142-28-9 1,3-Dlchloropropane 0.0004 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 106-46-7 1,4-Dichlorobenzene D.006 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 123-91-1 1,4-Dimone 0.003 mg/I NA 0.0141 NA NA NA NA NA 0.0029 NA NA NA NA NA NA NA NA NA NA NA
SW8260 594-20-7 2,2-Dichloropropane Not Listed mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 78-93-3 2-Butanone(ME1C) 4 mg/I 0.0025 U 0.0025 U 0.0025 U 0.0025 U 0.0025 U 0.0025 U 0.0025 U NA 0.0025 U 0.0025 U 0.0025 U 0.0025 U 0.0025 U 0.0025 U 0.0025 U 0.0025 U 0.0025 U 0.0025 U 0.0025 U
5158260 95-49-8 2-Chlorotoluene 0.1 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U D.0005 U
SW8260 591-78-6 2-Hexanone Not Listed mg/I 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U NA 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U D.005 U
SW8260 106-43-4 4-Chlarotaluene Not Listed mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U D.0005 U
SW8260 108-10-1 4-Methyl-2-Pentanone(MIBK) Not Listed mg/I 0.0025 U 0.0025 U 0.0025 U 0.0025 U 0.0025 U 0.0025 U 0.0025 U NA 0.0025 U 0.0025 U 0.0025 U 0.0025 U 0.01)25 U 0.0025 U 0.0025 U 0.0025 U 0.0025 U 0.0025 U 0.0025 U
5W8260 67-64-1 Acetone 6 mg/I 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U NA 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U
SW8260 71-43-2 Benzene 0.001 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U D.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 108-86-1 Bromobenzene Not Listed mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 75-27-4 Bromodichloromethane 0.0006 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U D.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U D.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 75-25-2 Bromoform 0.004 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
5W8260 74-83-9 Bromomethane Not Listed mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U D.0005 U 0.0005 U 0.0005 U 0.0005 U
5W8260 56-23-5 Carbon tebachbride 0.0003 mg/I D.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 108-90-7 Chlorobenzene 0.05 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 74-97-5 Chlorobromamethane Not Listed mg/I 0.0005 U 0.0005 U D.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 75-00-3 Chlomethane 3 mg/I 0.0005 U D.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 67-66-3 Chloroform 0.07 mg/I 0.0005 U 0.000313 0.0005 U 0.0005 U 0.00023 3 0.0005 U 0.0005 U NA 0.0005 U 0.0005 0.0001133 0.0004 3 0.00019 3 0.00018 3 0.0005 U 0.0005 U 0.0005 U 0.000283 0.0005 U
SW8260 74-87.3 Chlommethane 0.003 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U D.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.00025 3 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
S1N8260 156-59-2 cis-1,2-Dichloroethene 0.07 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 10061-01-5 cis-1,3-Diddoropropene Not Listed mg/I 0.0005 U D.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 12448-1 Dibromoddoromethane 0.0004 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 75-71-8 Dichlorodifuoromethane 1 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 .64-17-5 Ethanol Not Listed mg/I O.1U 0.1U 0.1U 0.1U 0.1U O.IU 0.1U NA O.lU 0.1U 0.1U 0.1U 0.1U 0.1U 0.1U 0.1U 0.lU 0.1U 0.1U
5W8260 100-41-4 Ethylbemene 0.6 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 108-20-3 Isopropyl ether 0.07 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 98-82-8 Isopmpylbenzene 0.07 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 9999900-05.0 mils Xylene 0.5 mg/I 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U NA 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U
SW8260 1634-04-4 Methyl tert-butyl ether 0.02 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.00046] 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 75-09-2 Methylene chloride 0.005 mg/I 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U NA 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U
5158260 104-51-8 n-Butylbenzene 0.07 mg/I 0.0005 U 0.0005 U 0.0005 U D.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
5158260 103-65-1 n-Propylbenzene 0.07 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 91-20-3 Naphthalene D.006 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 D 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 95-97.6 o-Xylene 0.5 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
I! SW8260 99-87-6 p-Isopropy0nluene Not Listed mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.00115 U 0.0005 U 0.0005 U
SW8260 135-98-8 sec-Butylbe nzene Not listed mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 100-42-5 Styrene 0.07 mg/I 0.0005 U 0.0005 U D.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 98-06-6 tert-Butylbenzene 0.07 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 127-18--I Tetrachloroethene 0.0007 mg/I 0.0005 U 0.0044 0.0005 U 0.0005 U 0.0075 0.0005 U 0.0005 U NA 0.0005 U 0.0004 3 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
5008260 108-88-3 Toluene 0.6 mg/I 0.0005 U 0.00016 3 0.0005 U 0.00016 3 0.00015 7 0.00016 3 0.00018 7 NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 156-60-5 trans-1,2-Dichloroethene 0.1 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 10061-02-6 trans-1,3-Dichloropropene Not Soled mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 79-01-6 Tridrloroethene 0.003 mg/I 0.0005 U 0.0002 3 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U '0.00033 3 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0002 3 0.0005 U
SW8260 75-69-4 Trichloro8uoromethane 2 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U 0.00023] 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U
SW8260 108-05-4 Vinyl acetate Not Listed mg/I 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U NA 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U
SW8260 75-01-4 Vim,I chloride 0.00003 mg:l - 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.00D5 U 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U '" "" ` 0.0005 U 0.0005 U 0 0005 U 0.0005 U 0.0005 U 0.0005 U
Notes:
02L Standard-Tale 15A of the North Carolina Administrative Code,Chapter 02,Subchapter L,Paragraph.0202 Groundwater Quality Standards
•
. Highlighted Exceeds 02L Groundwater Standards
Bold-Detected
NA-Not Analyzed
U-Not Detected
J or E-Concentration Estimated
mg/I-milligrams per liter

Appendix G
Table G-1
Volatile Organic Compounds-Groundwater
Sample Location:) MW017 MW01B MW019 MW020 MW021 MW021 MW022 MWD22 MW023 MW023 MW024 MW024 MW025 MW026 MW027 MW028 MW029 MW029
Sample ID: 61D0MW017201106 KIDGMWO18201106 KIDGMW019201106 KIDGMW020201106 KIDGMW021201106 KIDGMW021201108 KIDGMW022201106 KIDGMW022201108 KIDGMW023201106 KIDGMW023201108 KIDGMW024201106 KIDGMW024201108 KIDGMW025201106 KIDGMW026201106 KIDGMW027201106 KIDGMW028201106 KIDGMW029201106 KIDGMW029201108
Sample Date: 06/16/2011 06/17/2011 06/15/2011 06/17/2011 06/15/2011 08/08/2011 06/15/2011 08/082011 06/15/2011 08/08/2011 06/14/2011 08/082011 06/16/2011 06/14/2011 06/21/2011 06/14/2011 06/22/2011 08/08/2011
Method CAS No. Analgte _021 Standard 2011 Units - -- --- `
SW8260 71-55-6 1,1,1-Trichloroethane 0.2 mgp b VAT,a 0.0005 U 0.0013 0.00048 7 0.0105 0.0135 ,.. 0.005 0.00026] NA J..,-J, 0.0005 U 0.0005 U 0.0005 U NA
5W8260 79-34-5 1,1,2,2-Tetachloroethane 0.0002 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 79-00-5 1,1,2-Trlchloroetharte 0.0006 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0013 NA 0.000427 NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.00074 NA
SW8260 75-34-3 1,1-Dlchloroethane 0.006 mg/I 0.0005 U 0.0005 U 0.00036] 0.001 0.0034 NA 0.0031 NA 0.0019 NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0066 NA
SW8260 75-35-4 1,1-Diddoroethene 0.007 mg/I 0.0005 U 0.00078 0.019 0.009 0.0852 NA 0.0863 NA 0.0416 NA 0.0051 NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0243 NA
SW8260 563-58-6 1,1-Dichlompropene Not Listed mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA ii.. J NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 87-61-6 1,2,3-Trichlorobenzene Not Listed mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 6.0u35 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
5W8260 96-18-4 1,2,3-Trichloropmpane 0.000005 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 120-82-1 1,2,4-Trichlorobenzene D.07 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 95-63-6 1,2,4-bimethylbenzene DA mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 106-93-4 1,2-Dibromoethane 0.00002 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 95-50-1 1,2-Dichlorobenzene 0.02 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW826D 107-06-2 1,2-Dichloroethane 0.0004 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.00016 3 NA 0.00038 3 NA 0.00017 7 NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 78-87-5 1,2-Dichloropropane 0.0006 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
5W8260 108-67-8 1,3,5-trimethybenzene 0.4 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 541-73-1 1,3-Dichlombenzene 0.2 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 142-28-9 1,3-Dichlaropropane 0.0004 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 106-46-7 1,4-Dichlorobenzene 0.006 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA D.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 123-91-1 1,4-Dlotmne 0.663 mg/I NA 0.0133 0.0138 0.002 U NA 0.0059 NA 0.0085 NA 0.0075 NA 0.002 U NA NA NA NA NA 0.0242
5W8260 594-20-7 2,2-Dlchloropropane Not Listed mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 78-93-3 2-Butanone(MIX) 4 mg/I 0.0025 U 0.0025 U 0.0025 U 0.0025 U 0.0025 U NA 0.0025 U NA 0.0025 U NA 0.0025 U NA 0.0025 U 0.0025 U 0.0025 U 0.0025 U 0.0025 U NA
SW8260 95-49-8 2-Chlorotoluene 0.1 mg/I 0.0005 U 0.0005 U D.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SWB260 591-78-6 2-Hemn0ne Not Listed mg/I 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U NA 0.005 U NA 0.005 U NA 0.005 U NA 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U NA
SW8260 106-43-4 4-r7rbraroluene Not Listed mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 108-10-1 4-Methyl-2-Pentanone(MIRK) Not Listed mg/I 0.0025 U 0.0025 U 0.0025 U 0.0025 U 0.01)25 U NA 0.0025 U NA 0.0025 U NA 0.0025 U NA 0.0025 U 0.0025 U 0.0025 U 0.0025 U 0.0025 U NA
SW8260 67-64-1 Acetone 6 mg/I 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U NA 0.01 U NA 0.01 U NA 0.D1 U NA 0.131 U 0.01 U 0.01 U 0.01 U 0.01 U NA
5W8260 71-43-2 Benzene 0.001 mg/I 0.0005 U D.0005 U 0.0005 U D.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 108-86-1 Bromobenzene Not Listed mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 75-27-4 Bromodichloromethane 0.0006 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U D.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 75-25.2 Bromoform 0.004 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 74-83-9 Bromomethane Not Listed mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 56-23-5 Carbon tetrachloride 0.0003 mg/I 0.0005 U 0.0005 U 0.00019] 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 108-90-7 Chlorobenzene D.05 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 74-97-5 Chlorobromomethane Not Listed mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 75-00-3 Chloroethane 3 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 67-66-3 Chloroform 0.07 mg/I 0.00081 0.0005 U 0.00025 3 0.0018 0.00055 NA 0.00033 3 NA 0.00097 NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.00069 NA
SW8260 74.87-3 Chloromethane 0.003 mg/I 0.0005 U 0.0005 U 0.00023] 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.00024 3 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 156-59-2 cis-1,2-Dirhloroethene 0.07 mg/I 0.0005 U 0.0005 U 0.00018] 0.0004] 0.0005 U NA 0.00039] NA 0.000427 NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 10061-01-5 cis-1,3-Didrloropropene Not Usted mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA D.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
5W8260 124-48-1 Dibromochlommethane 0.0004 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 75-71-8 Dichlommdifuoromethane 1 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 64-17-5 Ethanol Not Listed mg/I 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U NA 0.1 U NA 0.1 U NA 0.1 U NA 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U NA
SW8260 100-41-4 Ethylbenzene 0.6 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 108-20-3 Isopropyl ether 0.07 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 98-82-8 Isopropylbenzene 0.07 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0905 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 9999900-05.0 m+p Xylene 0.5 mg/I 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U NA 0.001 U NA 0.001 U NA 0.001 U NA 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U NA
SW8260 1634-04-4 Methyl tert-butyl ether 0.02 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U D.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 75-09-2 Methylene chloride 0.005 mg/I 0.002 U 0.002 U 0.002 U 0.002 U D.002 U NA 0.002 U NA 0.002 U NA 0.002 U NA 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U NA
SW8260 104-51-8 n-Butylbenzene 0.07 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
5W8260 103-65-1 n-Propylbenzene 0.07 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 91-20-3 Naphthalene 0.006 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 9547-6 o-Xylene 0.5 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 99-87-6 p-Isopropyholuene Not Listed mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 135-98-8 sec-Butylbeozene Not Listed mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 100-42.5 Styrene 0.07 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0055 U 13.0005 U 0.0035 U 0.0005 U 0.0005 U NA
SW8260 98-06-6 tert-Butylbenzene 0.07 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
5W8260 127-184 Tetrachloroethene 0.0007 mg/I 0.0005 U 0.0016 0.0117 0.0015 0.0204 NA 0.00059 NA 0.0041 NA 0.0017 NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0012 NA
SW8260 108-88-3 Toluene 0.6 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 156-60-5 trans-1,2-Dichloroethene 0.1 mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.00026] NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
5W8260 10061-02-6 trans-1,3-Didhloropropene Not Listed mg/I 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 79-01-6 Trichlamethene 0.003 mg/I 0.0005 U 0.0005 U 0.00054 0.0006 0.0005 U NA 0.0005 U NA 0.0027 NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
5W8260 75-69.4 Trichlcroluoromethane 2 mg/I 0.0005 U D.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
SW8260 108-05-4 Vinyl acetate Not Listed mg/I 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U NA 0.005 U NA 0.005 U NA 0.005 U NA 0.005 U 0.005 U 0.005 U 0.005 U D.005 U NA
SW8260 75-01-4 VIA I chloride 0.00003 mod D.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA 0.0005 U NA 0.0005 U NA 0 D004 U NA 0.0005 U 0.0005 U 0.0005 U 0.0005 U NA
Notes:
02L Standard-Title 15A of the North Carolina Administrative Code,Chapter 02,Sul
Highlighted-Exceeds 02L Groundwater Standards
Bold-Detected
NA-Not Analyzed
U-Not Detected
3 or E-Concentration Estimated
mg/I-milligrams per liter

Appendix G
Table G-1
Metals-Groundwater
Sample Location: MB019 MB029 MC019 MCO29 MD022 MW006 MW008 MW009 MW010 MW011 MW017
Sample ID: KIDGMB019201106 KIDGMB029201106 KIDGMC019201106 KIDGMCO29201106 KIDGMD022201106 KIDGMW006201106 KIDGMW008201106 KIDGMW009201106 KIDGMW010201106 KIDGMW011201106 KIDGMW017201106
Sample Date: 06/15/2011 06/22/2011 06/16/2011 06/22/2011 06/15/2011 06/21/2011 06/22/2011 06/22/2011 06/23/2011 06/14/2011 06/16/2011
Method CAS No. Anal a 02L Standard 2011 mg/I mg/I moil mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I
SW6010 7440-47-3 Chromium 0.01 NA 0.0016)
SW6010 7439-89-6 Iron 0.3 0.351 1.89 0.119) 20.7 2.51 0.533 0.0494 3 0.888 0.351 1.38 0.0756)
SW6010 7439-96-5 Manganese 0.05 NA 0.00423 0.23 0.223
SW7196 18540-29-9 Chromium(Hexavalent) 0.000043 NA Ilk
Sample Location: MW018 MW019 MW020 MW021 MW022 MW023 MW024 MW026 MW028 MW029 MW033
Sample ID: KIDGMW018201106 KIDGMW019201106 KIDGMW020201106 KIDGMW021201106 KIDGMW022201106 KIDGMW023201106 KIDGMW024201106 KIDGMW026201106 KIDGMW028201106 KIDGMW029201106 KIDGMW033201106
Sample Date: 06/17/2011 06/15/2011 06/17/2011 06/15/2011 06/15/2011 06/15/2011 06/14/2011 06/14/2011 06/14/2011 06/22/2011 06/23/2011
Method CAS No. Analyte 02L Standard 2011 mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I
SW6010 7440-47-3 Chromium 0.01 NA NA
SW6010 7439-89-6 Iron 0.3 0.12) 0.254) 1.06 0.185) 0.364 1.21 0.148) 0.362 0.305 0.05813
SW6010 7439-96-5 Manganese 0.05 0.301 0.0194 0.0052 3 0.0082 3 0.0152 0.0389 ,+ 0.174
SW7196 18540-29-9 Chromium(Hexavalent) 0.000043 NA NA 'IA NA
Sample Location: MW034 MW042 MW043 MW044 MW045 MW047 MW048 MW049 MW050 MW051 MW052
Sample ID: KIDGMW034201106 KIDGMW042201106 KIDGMW043201106 KIDGMW044201106 KIDGMW045201106 KIDGMW047201106 KIDGMW048201106 KIDGMW049201106 KIDGMW050201106 KIDGMW051201106 KIDGMW052201106
Sample Date: 06/16/2011 06/16/2011 06/16/2011 07/20/2011 07/21/2011 07/19/2011 07/19/2011 07/19/2011 07/20/2011 07/19/2011 07/19/2011
Method CAS No. Analyte 02L Standard 2011 mg/I mg/I m,/I mg/I mg/I mg/I mg/I mg/I _ mg/I mg/I mg/I
SW6010 7440-47-3 Chromium 0.01 0.0077 3 0.0198 0.0029 3 0.01 U NA NA NA
SW6010 7439-89-6 Iron 0.3 3.79 NA 22.7 0.0922 3 0.204) 0.657 12.1 0.286) 0.411 0.211) 0.3 U
SW6010 7439-96-5 Manganese 0.05 NA 0.329 0.0627 NA 0.586 0.658 0.453 0.159 0.325 0.119
SW7196 18540-29-9 Chromium(Hexavalent) 0.000043 0.069 0.01 U 0.01 U 0.01 U - NA NA NA NA NA
Notes:
02L Standard-Title 15A of the North Carolina Administrative Code,Chapter 02,Subchapter L,Paragraph.0202 Groundwater Quality Standards
Highlighted-Exceeds 02L Groundwater Standards
Bold-Detected
NA-Not Analyzed
U-Not Detected
J or E-Concentration Estimated

Appendix G
Table G-1
Total Organic Carbon - Groundwater
Sample Location: MB019 MB029 MC019 MCO29 MD022 MW006 MW008 MW009 MW010 MW011 MW017
Sample ID: KIDGMB019201106 KIDGMB029201106 KIDGMC019201106 KIDGMCO29201106 KIDGMD022201106 KIDGMW006201106 KIDGMW008201106 KIDGMW009201106 KIDGMW010201106 KIDGMW011201106 KIDGMW017201106
Sample Date: 06/15/2011 06/22/2011 06/16/2011 06/22/2011 06/15/2011 06/21/2011 06/22/2011 06/22/2011 06/23/2011 06/14/2011 06/16/2011
Method CAS No. Analyte Units mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L
SW9060 9999900-01-4 Total Organic Carbon 1 U 1 U 1 U 1.7 0.82 3 1 U 0.46 3 0.75 3 1 U 1.2 1 U
Sample Location: MW018 MW019 MW020 MW021 MW022 MW023 MW024 MW026 MW028 MW029 MW033
Sample ID: KIDGMW018201106 KIDGMW019201106 KIDGMW020201106 KIDGMW021201106 KIDGMW022201106 KIDGMW023201106 KIDGMW024201106 KIDGMW026201106 KIDGMW028201106 KIDGMW029201106 KIDGMW033201106
Sample Date: 06/17/2011 06/15/2011 06/17/2011 06/15/2011 06/15/2011 06/15/2011 06/14/2011 06/14/2011 06/14/2011 06/22/2011 06/23/2011
Method CAS No. Analyte Units mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L
SW9060 9999900-01-4 Total Organic Carbon 0.283 0.33) 1 U 1 U 1 U 1 U 1 U 1 U 2.7 1 U 1 U
Sample Location: MW034 MW042 MW043 MW044 MW045 MW047 MW048 MW049 MW050 MW051 MW052
Sample ID: KIDGMW034201106 KIDGMW042201106 KIDGMW043201106 KIDGMW044201106 KIDGMW045201106 KIDGMW047201106 KIDGMW048201106 KIDGMW049201106 KIDGMW050201106 KIDGMW051201106 KIDGMW052201106
Sample Date: 06/16/2011 06/16/2011 06/16/2011 07/20/2011 07/21/2011 07/19/2011 07/19/2011 07/19/2011 07/20/2011 07/19/2011 07/19/2011
Method CAS No. Analyte Units mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L
SW9060 9999900-01-4 Total Organic Carbon 4.7 1 U 1 U 0.63) 0.44) 0.56 3 0.31) 0.33) 0.4 3 0.59 3 0.413
Notes:
NA—Not Analyzed
U—Not Detected
]or E—Concentration Estimated
mg/I—milligrams per liter

Appendix G
Table G-1
Methane-Ethane-Ethylene-Groundwater
Sample Location: MB019 MB029 MC019 MCO29 MD022 MW006 MW008 MW009 MW010 MW011 MW017
Sample ID: KIDGMB019201106 KIDGMB029201106 KIDGMC019201106 KIDGMCO29201106 KIDGMD022201106 KIDGMW006201106 KIDGMW008201106 KIDGMW009201106 KIDGMW010201106 KIDGMW011201106 KIDGMW017201106
Sample Date: 06/15/2011 06/22/2011 06/16/2011 06/22/2011 06/15/2011 06/21/2011 06/22/2011 06/22/2011 06/23/2011 06/14/2011 06/16/2011
Method CAS No. Analyte Units µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L
RSKSOP-175 74-84-0 Ethane 1U 1U 1U 1U 1U 1U 1U 1U 1U 1U 1U
RSKSOP-175 74-85-1 Ethylene 1U 1U 1U 1U 1U 1U 1U 1U 1U 1U 1U
RSKSOP-175 74-82-8 Methane 0.5 U 0.5 U 0.5 U 2.17 0.34 3 0.5 U 0.5 U 0.5 U 0.17 3 17.6 0.5 U
Sample Location: MW018 MW019 MW020 MW021 MW022 MW023 MW024 MW026 MW028 MW029 MW033
Sample ID: KIDGMW018201106 KIDGMW019201106 KIDGMW020201106 KIDGMW021201106 KIDGMW022201106 KIDGMW023201106 KIDGMW024201106 KIDGMW026201106 KIDGMW028201106 KIDGMW029201106 KIDGMW033201106
Sample Date: 06/17/2011 06/15/2011 06/17/2011 06/15/2011 06/15/2011 06/15/2011 06/14/2011 06/14/2011 06/14/2011 06/22/2011 06/23/2011
Method CAS No. Analyte Units µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L pg/L µg/L
RSKSOP-175 74-84-0 Ethane 1U 1U 1U 1U 1U 1U 1U 1U 1U 1U 1U
1 RSKSOP-175 74-85-1 Ethylene 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U
RSKSOP-175 74-82-8 Methane 0.45 I 0.5 U 0.19 I 0.5 U 0.17 3 0.5 U 0.5 U 0.5 U 0.17 3 0.5 U 1870
Sample Location: MW034 MW042 MW043 MW044 MW045 MW047 MW048 MW049 MW050 MW051 MW052
Sample ID: KIDGMW034201106 KIDGMW042201106 KIDGMW043201106 KIDGMW044201106 KIDGMW045201106 KIDGMW047201106 KIDGMW048201106 KIDGMW049201106 KIDGMW050201106 KIDGMW051201106 KIDGMW052201106
Sample Date: 06/16/2011 06/16/2011 06/16/2011 07/20/2011 07/21/2011 07/19/2011 07/19/2011 07/19/2011 07/20/2011 07/19/2011 07/19/2011
Method CAS No. Analyte Units µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L
RSKSOP-175 74-84-0 Ethane 1 U 1 U 1 U 1 U 0.51 3 1.3 6.74 0.52 1 U 0.58 1 U
RSKSOP-175 74-85-1 Ethylene 1 U 1 U 1 U 1 U 0.56 3 1.2 1 U 0.48 1 U 1 U 0.49
RSKSOP-175 74-82-8 Methane 0.54 0.5 U 0.5 U 0.28 3 0.74 2.14 0.28 3 0.94 17 1.31 14.7
Notes:
U-Not Detected
J or E-Concentration Estimated
µg/I-micrograms per liter
I

Appendix G
Table G-1
Chloride,Nitrate,&Sulfate-Groundwater
Sample Location: MB019 MB029 MC019 MCO29 MD022 MW006 MW008 MW009 MW010 MW011 MW017
Sample ID: KIDGMB019201106 KIDGMB029201106 KIDGMC019201106 KIDGMCO29201106 KIDGMD022201106 KIDGMW006201106 KIDGMW008201106 KIDGMW009201106 KIDGMW010201106 KIDGMW011201106 KIDGMW017201106
Sample Date: 06/15/2011 06/22/2011 06/16/2011 06/22/2011 06/15/2011 06/21/2011 06/22/2011 06/22/2011 06/23/2011 06/14/2011 06/16/2011
Method CAS No. Analyte 02L Standard 2031 Units mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L m�/L mg/L mg/L
SW9056 9999000-40-8 Chloride 250 4 1.5 3 4.5 1.7 3 1.7 3 3.3 4.5 4 2.5 6.8 4.6
SW9056 14797-55-8 Nitrate(as N) 10 7.7 9.6 0.13 2.1 1.6 4.7 0.22 63.3 1.4
SW9056 14808-79-8 Sulfate 250 4.8 _ 10.5 40.7 2 U
Sample Location: MW018 MW019 MW020 MW021 MW022 MW023 MW024 MW026 MW028 MW029 MW033
Sample ID: KIDGMW018201106 KIDGMW019201106 KIDGMW020201106 KIDGMW021201106 KIDGMW022201106 KIDGMW023201106 KIDGMW024201106 KIDGMW026201106 KIDGMW028201106 KIDGMW029201106 KIDGMW033201106
Sample Date: 06/17/2011 06/15/2011 06/17/2011 06/15/2011 06/15/2011 06/15/2011 06/14/2011 06/14/2011 06/14/2011 06/22/2011 06/23/2011
Method CAS No. Analyte O2L Standard 2011 Units mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L
SW9056 9999000-40-8 Chloride 250 10.5 5.5 2.1 2.8 2.3 2.3 3 3 13.1 4.9 2.7
SW9056 14797-55-8 Nitrate(as N) 10 1.5 4.6 1.2 0.45 0.11 1.1 0.62 0.18 20.1 3 0.78
SW9056 14808-79-8 Sulfate 250 2.8 6.4
Sample Location: MW034 MW043 MW044 MW045 MW047 MW048 MW049 MW050 MW051 MW052
Sample ID: KIDGMW034201106 KIDGMW043201106 KIDGMW044201106 KIDGMW045201106 KIDGMW047201106 KIDGMW048201106 KIDGMW049201106 KIDGMW050201106 KIDGMW051201106 KIDGMW052201106
Sample Date: 06/16/2011 06/16/2011 07/20/2011 07/21/2011 07/19/2011 07/19/2011 07/19/2011 07/20/2011 07/19/2011 07/19/2011
Method CAS No. Analyte O2L Standard 2011 Units mg/L mg/L ma/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L
SW9056 9999000-40-8 Chloride 250 7 5 4.3 3.1 2.7 3.9 2.7 3.1 2.7 2.7
SW9056 14797-55-8 Nitrate(as N) 10 0.069 3 2.3 0.88 0.32 0.054 3 0.7 0.27 0.13 0.084 3 0.06 3
SW9056 14808-79-8 Sulfate 250 23.3 2 U 2 U 4.4 6.4 21.2 1.43 6.8 1.5 3
Notes:
02L Standard-Title 15A of the North Carolina Administrative Code,Chapter 02,Subchapter L,Paragraph.0202 Groundwater Quality Standards
Highlighted-Exceeds 02L Groundwater Standards
Bold-Detected
NA-Not Analyzed
U-Not Detected
3 or E-Concentration Estimated
mg/I-milligrams per liter

Appendix G
Table G-1
Groundwater Field Parameters
Sample Location: MW006 MW007 MW008 MW009 MW010 MW011 MW012 MW013 MW014 MW015 MW016 MW017
Sample ID: KIDGMW006201106 KIDGMW007201106 KIDGMW008201106 KIDGMW009201106 KIDGMW010201106 KIDGMW011201106 KIDGMW012201106 KIDGMW013201106 KIDGMW014201106 KIDGMW015201106 KIDGMW016201106 KIDGMW017201106
Sample Date: 06/21/2011 06/23/2011 06/22/2011 06/22/2011 06/23/2011 06/14/2011 06/14/2011 06/13/2011 06/13/2011 06/21/2011 06/23/2011 06/16/2011
Method CAS No. Anal Units
Field DO meter Dissolved Oxygen meter mg/I 4.8 1.1 3.7 3 3.7 0.49 0.26 5.26 2.72 0.57 0.17 .6.31
Field DO ODO Dissolved Oxygen optical probe mg/I NA NA NA NA NA NA NA NA NA NA NA 6.96
Field 9999001-14-9 Ferrous Iron mg/I 0.12 NA ND 0.95 0.18 0.01 NA NA NA NA NA 0.03
Field 1333-74-0 Hydrogen nM 1.8 NA NA NA NA NA NA NA NA NA NA 1.7
Field ORP Oxidation Reduction Potential millivolts 160.4 233 -38 -85 139 205 165.1 196.9 183.2 161.5 158.9 160.4
Field PH pH SU 4.85 4.26 4.74 5.29 5.14 4.22 4.82 4.37 4.29 4.78 5.48 4.67
Field 18496-25-8 Sulfide mg/I 0.029 NA 0.002 0.07 0.059 0.009_ NA NA NA NA NA 0.009
Sample Location: MW018 MW019 MW020 MW021 MW022 MW023 MW024 MW026 MW027 MW028 MW029 MW031
Sample ID: KIDGMW018201106 KIDGMW019201106 KIDGMW020201106 KIDGMW021201106 KIDGMW022201106 KIDGMW023201106 KIDGMW024201106 KIDGMW026201106 KIDGMW027201106 KIDGMW028201106 KIDGMW029201106 KIDGMW031201106
Sample Date: 06/17/2011 06/15/2011 06/17/2011 06/15/2011 06/15/2011 06/15/2011 06/14/2011 06/14/2011 06/21/2011 06/14/2011 06/22/2011 06/16/2011
Method CAS No. Analyte Units
Field DO meter Dissolved Oxygen meter mg/I 0.81 1.85 3.54 1.26 2.42 2.18 2.74 2.09 2.38 2.72 3.59 0.47
Field DO ODO Dissolved Oxygen optical probe mg/I 0.47 2.16 3.53 1.4 3.21 2.26 2.81 NA NA NA 4.43 NA
Field 9999001-14-9 Ferrous Iron mg/I 0.02 0.27 0.21 0.01 0.01 0.05 0.03 ND NA 0.07 0.02 NA
Field 1333-74-0 Hydrogen nM 2.2 1.5 2.7 2.2 1.6 2.4 NA NA NA NA 1.8 NA
Field ORP Oxidation Reduction Potential millivolts 200.4 170.6 198 144.8 151.7 135.3 169.2 112.1 158.6 205.2 217.6 94.3
Field PH pH SU 4.23 5.45 5.65 5.51 5.56 5.52 4.58 5.84 5.02 5.06 4.57 5.79
Field 18496-25-8 Sulfide m./I 0.005 0.056 0.04 0.016 0.014 0.019 0.024 _ 0.014 NA 0.016 0.005 NA
Sample Location: MW032 MW033 MW038 MW041 MW043 MW044 MW045 MW047 MW048 MW049 MW050 MW052
Sample ID: KIDGMW032201106 KIDGMW033201106 KIDGMW038201106 KIDGMW041201106 KIDGMW043201106 KIDGMW044201106 KIDGMW045201106 KIDGMW047201106 KIDGMW048201106 KIDGMW049201106 KIDGMW050201106 KIDGMW052201106
Sample Date: 06/16/2011 06/23/2011 06/23/2011 06/23/2011 06/16/2011 07/20/2011 07/21/2011 07/19/2011 07/19/2011 07/19/2011 07/20/2011 07/19/2011
Method CAS No. Ana Units
Field DO meter Dissolved Oxygen meter mg/I 0.42 0.23 1 2.8 6.49 4.02 2.2 2.55 6.2 6.74 6.12 5.6
Field DO ODO Dissolved Oxygen optical probe mg/I NA 0.27 NA NA NA 3.95 4.18 3.17 5.1 1.7 2.37 1.45
Field 9999001-149 Ferrous Iron mg/I NA ND NA NA 0.31 ND 0.04 0.15 0.05 0.1 0.07 ND
Field 1333-74-0 Hydrogen nM NA 4.1 NA NA NA NA NA NA NA NA NA NA
Field ORP Oxidation Reduction Potential millivolts 54.9 161.8 70 177 105 227.6 207.9 21.6 123.1 133.1 208.7 159
Field PH pH SU 5.88 5.05 5.42 5.27 5.71 5.19 5.13 6.89 5.4 6.05 5.27 . 5.62
Field 18496-25-8 Sulfide m /I NA 0.019 NA NA 0.05 0.007 0.006 0.028 0.096 0.009 0.019 0.001
Intermediate and Bedrock Wells
Sample Location: MB006 MB019 MB029 MC006 MC019 MCO29 MD022 MB051
Sample ID: KIDGMB006201106 KIDGMB019201106 KIDGMB029201106 KIDGMC006201106 KIDGMC019201106 KIDGMCO29201106 KIDGMD022201106 KIDGMW051201106
Sample Date: 06/21/2011 06/15/2011 06/22/2011 06/21/2011 06/16/2011 06/22/2011 06/15/2011 07/19/2011
Method CAS No. Analyte Units _
Field DO meter Dissolved Oxygen meter mg/I 6.3 3.15 1.3 0.53 3.08 0.65 0.51 2.96
Field DO ODO Dissolved Oxygen optical probe mg/I NA 3.41 NA NA 7.88 NA 0.77 2.28
Field 9999001-14-9 Ferrous Iron mg/I NA 0.04 ND NA 0.06 0.67 0.03 0.17
Field 1333-74-0 Hydrogen nM NA 8.5 5.5 NA 4 2900 NA NA
Field ORP Oxidation Reduction Potential millivolts 74 159.9 -7 -61 170.8 -40 45.6 62
Field PH pH SU 5.8 5.77 6.28 6.2 5.66 6.78 8.01 5.99
Field 18496-25-8 Sulfide m/l NA 0.026 0.02 NA _ 0.01 0.538 NA 0.006
Notes:
NA-Not Analyzed
mg/I-milligrams per liter
nM-nanomolar
SU-standard units

Walter Kidde Portable Equipment,Inc.
Mebane,North Carolina
UIC Permit Application
Attachment C—Injection Fluid Composition
ATTACHMENT C—INJECTION FLUID COMPOSITION
A Material Safety Data Sheet (MSDS) for each injectant is enclosed in Attachment C. A discussion
of the chemical, physical and biological characteristics of each injectant is provided in Section D.3
below. Municipal water will be used as the water supply for injections.
GI

rAN, ADVENTUS Safettil Data
� } Proven Soil,Sediment and Groundwater
Y 1'emediationTechnologes
MATERIAL SAFETY DATA SHEET: EHC® Page: 1 of 3
1. PRODUCT IDENTIFICATION: EHC®
PRODUCT USE: Bioremediation product for the remediation of
contaminated soil and groundwater only.Not for use
in potable drinking water.
MANUFACTURER: EMERGENCY PHONE:
Adventus Americas Inc. Office Hours: 815-235-3503
2871 W.Forest Rd, Suite 2 After Hours: 630-309-1175
Freeport,IL
61032
TRANSPORTATION OF DANGEROUS GOOD CLASSIFICATION:
Not Regulated
WHMIS CLASSIFICATION:
Not Regulated
CONTAINMENT HAZARD:
Any vessel that contains wet EHC or EHC and water must be vented due to potential pressure build up
from fermentation gasses.
2. INGREDIENTS
CHEMICAL NAME: CAS# TLV(mg/m3) LD low(mg/Kg) % in Product
Organic Amendment N/D N/E N/E 52-82
Iron 7439-89-6 5(as iron oxide fume) N/E 18-48
3. PHYSICAL DATA
Physical state Solid Melting point 1371-1480°F
Odour threshold N/A Boiling point 3000°C
Density 0.75 Kg/L Vapour pressure(mm Hg) 1 @ 1787°C
pH N/A Vapour density(air=1) N/A
Solubility in water Insoluble Evaporation rate N/A
Coeff.of water/oil N/A
Appearance&odour Odourless,_TanBrown Flakes
4. FIRE AND EXPLOSION HAZARD DATA
FLASH POINT(Deg.C PMCC): N/A
LOWER UPPER
FLAMMABLE LIMITS IN AIR % BY VOLUME: N/A N/A
AUTO IGNITION TEMP(Deg.C): N/A

(Ai ADVENTUS Safet Data
{roven Soii,Sediment and Groundwater ''
Remediation Technologies
41111
MATERIAL SAFETY DATA SHEET: EHC® Page:2 of 3
EXTINGUISHING MEDIA: Dry chemicals or sand or universal type foam.
SPECIAL PROCEDURES:
Firefighters should wear SCBA and protective clothing.
UNUSUAL FIRE AND EXPLOSION HAZARDS:
Dust can present fire and explosion hazards when exposed to fire,chemical reaction,or contact with
powerful oxidizers.
5. REACTIVITY DATA
STABILITY(NORMAL COND.):
Stable: X Unstable:
CONDITIONS TO AVOID: Contact with powerful oxidizers such as
strong acids.
INCOMPATIBILITY(Materials to Avoid): Powerful oxidizers such as strong
acids.
HAZARDOUS DECOMPOSITION PRODUCTS: Hydrogen,Carbon monoxide,Carbon
dioxide.
6. TOXICOLOGICAL PROPERTIES
ROUTE OF ENTRY:
Inhalation
Ingestion(not likely)
HEALTH HAZARDS:
Acute overexposure may cause eye,nose,mouth and skin irritation.
Carcinogenicity: No Information Available
Signs and Symptoms of Exposure: No Information Available
Medical Conditions Generally
Aggravated by Exposure: No Information Available
7. PREVENTIVE MEASURES
PERSONAL PROTECTIVE EQUIPMENT:
Eye Protection: X Gloves: X Clothing:
RESPIRATORY PROTECTION:

( ADVENTUS Safet_u - Data
Proven Soil,Sediment,and Groundwater NoLzil
Remediation Technologies
MATERIAL SAFETY DATA SHEET: EHC® Page:3 of 3
Use dust mask in severe conditions.
Use good housekeeping practices to keep dust to a minimum.
VENTILATION REQUIREMENTS:
Not normally required.
SPILL AND LEAK PROCEDURES:
Sweep up and return to container.
WASTE DISPOSAL:
Sanitary landfill. Follow Federal,State and Local guidelines.
HANDLING PROCEDURES:
Wear safety glasses for normal use. Avoid generating
excessive dust,wear dust mask in severe conditions.
STORAGE REQUIREMENTS:
Do not store near powerful oxidizers such as strong acids.
Keep dry.
Any vessel that contains wet EHC or EHC and water must be vented due to potential pressure build up
from fermentation gasses.
SPECIAL HANDLING INFORMATION:
Treat as a nuisance dust
8. FIRST AID MEASURES
INHALATION:Remove to fresh air. Seek medical attention.
INGESTION: Seek medical attention.
SKIN CONTACT:Brush off excess. Wash with soap and water.
EYE CONTACT:Flush with running water. Seek medical attention.
9. OTHER INFORMATION
None
10. PREPARATION INFORMATION
Prepared By: Adventus Remediation Technologies Date Prep./Rev.: 10/28/08
1345 Fewster Drive Print Date: 10/28/08
Mississauga,Ontario Phone: [phone]
L4W 2A5 Fax: [phone]
Definitions:
N/D-No Data N/A-Not Applicable N/E-Not Established
EHC®is a registered trademark of Adventus Intellectual Property Inc.

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. Benqinks . !Mien iiiThieembereirM VIM:WA 'I
. .
I'l 410Brekig IM Clam toeMbNlis.
it figerfiret ter tultininellOrgarine
,. ...,.y..... ,e,,.........,.... .1,,pq ..... ...... •••••• .. .... ''.. .. . ... * ';... .
I i
ft.Phygiati anti,chemical psiveriges !
I. .
* batimr iMilme.mt;oneremem
i form 6112 Maar
. line onimuier porky 1,
1 . Caw
litakilsw.11/ ~be Ilitil
-1,6 110Xmli 7
. Breismaliiii z 211 %likuu(41 USF 44dwidittd dem* ..40(4142511* I
I
' ttaieMly Oa*imilAte.wtOpr •4
:. 'pH Wass • A.Ola 14411%fuspiMiAMI ifilefigril 1
1
. '
. .
I.; 'Millitien iiX 011itilime**Milie '
i - .-— ...._..—.........--....•-........••••-mar.—aam......... ar—.cr—Pd.,. .,._ ••11•....fl,RIPP1.!
I JO.ftlitlarandi csuclat4ly i
' --------•••----- ---,--*..1—,ara.91.1.1,9.161.—qoa .-.. 4,...•
Slafear = soak Wiled**tithilfiket Mae/0 in• ,.7
i I ,
. Condlionsiumogo • Mahl
• j.110111314SA odd -bows,a ri I t s 4
.... - 4
..• iliircittreologreal klogailmO• Pen 1
•
• .r
1 • • Agkifeiwkily -. Lox p-voca mots tank**nal -
, extanzioari - cuyist 1:00%441 ens*Pam!. • • 1 .3
, 1 1 Chtimip*may • 1400,EL 1 EntiMm?,;Witt ma KS mak , Iledvt.# .
•
- - • P.eptriduciklIttixddlif - MX iireergetat 1
Ha •• RIM Cregitmainisto ditto ry Alma*2 .!
' - WAS Owe*toingillie$tab Olt • catituovilori) f -2
- imomedy Facalpentraa Gab tor .Genowlitin) , i .. !-
'
. - -I Waving to, 0•510101 gilitivireile I
•
V. Mierfrefi IM. 41Befilii Bit Beilieihm i
• ,,
•
. .
-:'Ur..=Etilleglial Wriginieltkell , : . • .= . -
.—. ..
BB palkfacm •••PterAiVeftliki*Colgi repigibri*
1 . .
-I
---
, .
DA.114101318E{Mimi fr.pligtomitemee eMehilfmr*Via IfpxiBmpe, Pal 3ie
Tog FINJ
4
. .
-- •
•
. . ,

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1
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. l
!e aldo RIZ F ad E#I F'Ty O Wtni 'i
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. La,asposal conildiratloM
r _ - ,. _ . _.;..a
i -
t&Tran4port -
.
i to r mt.tri c mons imano'
F7riasion PArlitnittot tia EOM
• >#e k0-5 kWh(p(uric.. Wag;,oMm
t
I use • ka[i e ;
FARM,,docur rori -,11m1 -
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7.
. _
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Ilia:�ilos�tlei in 64 of, OEM apggl kJiaoed 4ea su[enk cyd 4kk 1 V1140 nae he , 1
1 askarAisE isewitg p. l4 3f_g4A gla kil,Feedt7slR sae
1 .
i
1

1
MSDS
1
Micropowder Iron
' 1
•
' 1
' 1
'•
I
• I
11
II
I1
Li
Li
Li

C.", es.NI A. Cautribus,+ . , f fig}iics wn,PA Sp4nEfi1t1,4L
S8-72I.S283 �..
•
-''.SECTION'01..,.;:,CHEMICAL•PRODUCT AND COM ANY'IDENTIFICA ION
DOMESTIC TRADE NAME: f lCROPO DER IRON GRADE$43706 •
EXPORT TRADE NAME: MlC(O?owDER IRON ERADE S 3.700
•
•
ruiR REGISTRY NO:: 4 3 .• . . - • -
OAS REG18`rRY NAME IRON
SYNONYM_ I+ /'AL.uc TR.ON
idinEcutAn FORMULA: I•'c •
MOLECULAR WEIGHT: 5515
.SECTION 02 - COMPOSITION f FORM4` 'uON 6N�HAZA DOUR INGREDIENTS
ICI'
SECTION 03 -'HAZARDS:IDENTIFICATION -
'`:>"7
* :* * * EMERGENCY €1 V;
RIFORl+1; RREYISI14RONN POWDER, J• .• •
* DUSTING IN AIR WILL PRESENT A. MODERATE DUST EXPLOSION`hAZARD laT . ::.
* SPARK SOURCE 1*'IGNITION ENERGY Or THE POWDER I5 CoHTR,tBII`I•ING EA TOR '
* TO TILE. FIRE/EXPLOSIONHAZA RD.. - F�
• * * * * * * .*,* * * * * * * *•* * * *.* * * * * *.* *
•
-ACUTE TOXICFTY'. .
of ,TOXICiTY:
PAT IEM : M CiX. G;NO EVIDENCE or GROSS PATHOLOGY.
DERMAL TOXICITtr: -NO DATA FOTJND
INHALATION Tc XICFTy -
1.17 ATTJEREFERE CCE.SINDICATESiIGHTHAZARD FROM INHALATION.
SKIN IRRITATION;
I.M ATTIRE REFERENCES INDICATE NO HA2A1tO FROM MN coNTAcr,
g}�77�� ,�+� �,T �ryT q
INi• A� V�AL�YLoG UA INc.
"4 rrsoraw for vnximminentaipreassionckta sett inr pyarup aLtamagive Po iee:

r
r -
•
N5' • 03/umbus,OH . • Doylestown,PA • Sptingfield,IL
' -
1388-7.2.1-82,83
•
° •
SECTION 03 - HAZARDS NTIFICPITION
•
•
rYE IRRITATION:
•
' -'••••HUMAN;MON IN EYE CAUSES RUST RINGS IN CORNEwASSOCTATED WITHliREITATIO ,•
HYPEREMIA.OF CONILJNCIIVA AND INPLAILVT471014.,
SENSITIZER: ,.
NO DATA VOUND. • - •
• .•
DOT CORROSIVE: • • •
NO DATAPOOND„ • •
• •
PRIMARY SOUTEM OF ENTRY: 1.,ATION coNrAer
-MONS AND SYMPTOMS OF EXPDSUR&
• •
' •-
•NO .
SYMPTOMS or INGESTION!
•
EFTELTS OFEXP=IRP.FDIFF.C1117,
.•
SYMPTOMS OF INHALATION:: • • • • . .
NO SPFF.CTS OF EixtiosORE EXprAcrEb, • • . .•
SYMPTOMS OF SKIN CONTACT:: • • • '= •. : '• • ..7;;;,°••• •-••• ;
EFFECTPOF,IT'SPOSURI•111XPBCTEti DUB TO CONT•Aci,'- 'xi41,0Siii+01(i.OA10 • • •
• IRRITATION ORDBrqdkiklm IN SOME Th11:0ED.i•LcaS
. ,
SYMPWOMS OF EYE CONTACT • , S *;• • • '
NO '-1/ ECTS'OFEDCPOSURERXPIXT.EDWITIL'alp kw:Ern&iiiifyossiittinaitATiccm
Ma:MAL CONDITIONS AGGRAVATED BY EXPOSURE: ' . ' " • • '
NO DATA FOUND V - •.
•
-OTHER TOX.ICITt- •
•
OMER ACUTE TOXIOITY1 •
INTBAVENOUa.;RABBIT];075 1.0.1:3-/NO CARBONYL IRON POWDER PIWDUCIUD
'USYTEROBLASTILEMIAIREVERsm,HAFFanL WEEK,
SUB cHRortir ORAL,TOXICITY;
00-DAZ RATI,0.1,1.0,5,0%131E11 I3EMAOLOGIC H1SLOGIC EXAMINATIONS/ 4D
'LlidNALYSIs RESULTS'WZR•13 NORMAL;&TONT INCREASs.tm WEIGHT
SUB CFIRONI 0 INHALATION=CITY:
NO DATA FO ,1DO3
SUB ORRONIGMESOELLANEOUS Toxicirm
INTRATRAcmpa..;PATTDIa 506 11.,(0/NO115 WEEKS:INTERIETTENTLY;NEOFLASTIGENIC- '
AQUATIC TOXIOIT'f.;
NO DATA FOUND •
INNOVATIVE ENVIRONMENTAL TEGEINoLo_Gust INC.
".4 rosourcept erarkorxrapog.Ipmeeseivnes 4c0drist innovebtivg gliericipe m.01.1204054.81

4.ire, I II
r I
EwIng,NI I, Co1umIx4,011 Doielostown.,PA * • Spilikelirad
SBS-721-13282,
SECT ION Oa - EXPOSURE. CONTFIOLS/PERS,ONAL P_FIOTECTION (CONT.)
PERSONAL RYGIEN •
•WAStI TROROUGY AFTER HAND•um,
• •:Th'PROTECTIVE MEASURES•DURING REPAIR/MAINTENANDE OF EQUIPMENT: •
- •--4WASHEQUIPMENT:THORO OGHLY WITH STEAM.O.RWAlm WATER urci-weLEAR•alEtz,- •Art,w
OXYGEN LEVEL WITH AN OXYGEN mETER. IN ALL ciksES.maicrw dcico utiusTkrAL
SAFETY FRAPTWFC IBEFVRIS ENTERING EQUIPMENT: :
EXPOSURE'Linn:
FoR INERT OR,NUISANCE DUST(PARTfeldATSS NOT OTHERWISE REG MATISNOASSIFIP7):
OSHA PELITWA 35 IYIG/M3-TOTAL DUST;5MG/0/43 jagsp1P.AELI3 rMOThl
ACGIH TLV:TWA 10 MG/Mt-INHALE;3MG/M3-EESPIR .
•- • :•
SECTION 09 - PHYSICAL AND CHEMICAL PROPERTIES , ••: :•• • . •
.•
BOILING POINT:„27511 DEG C „_,._ „ . •
VAPOR PRESSURM.NOT V OLA1U
vApoR DENSITYJAIR= ;NOT VOLATILE
WATER SOLIJ1011.0.: INSOLUELE"• ".7AAIA
• ..:MELTING/StE4IND POINT:...-15.35 DEG:"C. ,
A'APOORANCE: 'tyriwcip.MpittwpER • ,:.•• :••••: !••,,,••-
sp.seiwie cow.etirifiTon=::1):NO DATAPOUND
PEROENTAGEVOIATI US$:-NOT,VOLATILE •
EVAPORATION It •NOT VOLATILE • •
•
pH OF SOLUTION: NO DATA Factto '•
ODOR: NO DATA FOUNID •
•
SECTION 10 -, STABILITY AND REACTIVITY
, •
•
STABILITY.: 'STABLE
1-LAZAIRDO US POLYMERIZATION: WILI.NOT ocam.
CONDMONS TO AVOID:
-OXIDT7PS READILY IN NOM AIR, •
INCOMPATIBLE MATERIALS:
REACTS viomormy vorre AODS OR OXIDIZING AGENTS. CHLORINE ThllLUQRIpL
FLUORINE,AhAND NITROGEN/0/OXIDe RAF WITH IRON WITH HICANDEMENCE,
PHOSFH 0 ADS REACTS WWII IRON WITH INCANDESCENCE WHEN EIR4rED.
HAZARDOUS DECOMPOSITION PRODUCTS:
NONE KNOWN
DatiOVATIVE ENviittomaNza,irEceNoLoorrs5.INC. ,
ittorarceforgiwiremmentarprofeissiarwas mm14 itutoagiaa aremaglae me/m0/09w •
• . _

I Ewing.NJ * Colurnhsts OH Doylestown,PA Springfield,IL
$88-721-S2 3
SECTION 11 - TRANSPORT INFORMATION •
•
-DOMESTIC DATA- —�
' -I3OTSNIPPING NAME: NOT X GU1A' p
DOT HAZARD CLASS: NOT ROO[IL T110
HAZARDOUS INGH DID NT(S): NONE
UN NUMSSR. NONE-
•
-EKPORr DATA-
EXPORT SHIPPING NAME; NOT R GU1AATED
EXFORT HAZARD CLASS: NOT REOLIIATE.D • •
HAZARDOUS 9N# RE®IENT(S): NOW.
UN NUMBER: NONE
•
•
•
•
•
•
•
•
•
•
•
•
INNOVATIVE COI M ', IIECHIVOIDGEESiINC'. ,
v a far entilwrizromitcapnakenimals S+eekir.3 fmrwvalikt aii¢rracattoe t ±adapt '

MSDS
rl
Sodium Disulfite
r Y
4 .
1
•
. l

r T • •
w ,NI Caluibue,OHI • DaYieatewn,
Davenport,
888-721-8283
MATMAL SAFETY DATA SHEET
•
soinft-MDISULYJ"IIC
Section I-1DENTW[CekTiON
• PRODUCT:SodiumSuftt
• SYNONYMS:IlisodiuroSuliite
•CHEMICAL DORMULAS;glassy
trillEMICAL AESTRACT NO.:7757-834
PRODUCT CODE NO.:17572
Seeders R-HAZARDOUS INGREDIENTS
COMPOSfrIGN Ivy' IIA1.A192 1 II
Section lit-HEALTH&Fly AID INFORMATION
INHALATION:Breathing dust may irritate the nose and throat and cause 0=011ns and
chest diaccenfort.Remove to fresh air.Give atticeial respiration if not breathing.Get
hozoodhle medic t attention.
INGESTION:If conscious,i nrondiaerIy giving large amounts of water.Get Immediate
rnM•rllcol attention. Do not give anything by mouth to an unoonscioua or coa y alsing
person.
EYE CONTACT: Dusts may irritate the ryes. Immediately flush eyes with Isis of
enure water for 15 minutes, lifting the upper and Iowa eyelids occasionally. Get
immediate medical attention.
SKIN CONTACT:No irritation is likely after brief confect but may be irtitatiag after
Tonged contact. Immediately *nab"akin with lots of aoep and water. Ret
contaminated clothing and alms;wash before reuse.Get medical attention if'irritation •
pcasists after washing.
INNOVATIVE ENVIRONMENTAL TECHNOLOGIES,INC.
resource(o€nviranexental arefessisseis seekimg ingov4titv altrrnat ve teclnmolegCes'

OTHER HEALTH.DATA:
LDSO 950 { pl,mouse;anydroos)
LDSo t 15 mg/kg(intravarcua,tat,.anhydrous)
Section IV-PHYSICAL DATA
MELTING POIN.T. :Lev.
• SPECIFIC GRAVITY{I12O41}:2,63
APPEARANCE AND ODOUR:White crystals or powder
BOILING POIIN Tt ra,aY:
VAPOUR PRESSURE:a.ay.
SOLUBILITY:>10a%
Section V-FIRE AND EXPLOSXON HAZARDS
SPECIAL LIRE FIGHTING PROCEDURES & PRECAUTIONS: Fire fighters
•should wear self io tamed breathing appixahas and fell protective clothing, Use water
spray Wood aaby containers saidstroetatesexposed to Ere.
-UNUSUAL FIRE&EXPIAISION HAZARDS:nnrn
Section VI-REACITVITY
summit Stable
HAZARDOUS POLYMERIZATION:Will net occur
CoNDrno3c-S&MATERIALS TO AVOID: Open Denies,welding arcs,oar high
temperature sotares which may induce thentad dccompo4Bon.Avoid acids,midis*
matte.
HAZARDOUS DECOMPOSITION PRODUCTS;May liberate tedeFdicsidr•gas.
Section VII-EMNPL OYEE PROTECTION

•• 4,
•
( CONTROL MDASURES:Gersual room%oblation reclaim!.An eyewash arul safety
shower should be nearby and ready for use.
RESPIRATORY PROTECTION: If use orations generate dose wear a NIOSTI-
approod topirator appropriate for those emiss' look.Appropziato respirators may he
a full face-piace or a half mash air-purify*edge aspirator with particulate Rem a
self-contained breaibiag apparatus in-the pressure demand mode, or a Supplied•uir
respirator.
PROTECI1VE CLOTITING:Loug-skcved shirk trousers,safety shoes„tubber gloves,
,and rubber apron.
EYE PROTECTION;Safety glasses with:side shields.It is generany recogeized that
outset lenses should not be%Iwo.when*liking with chemicals because outset leases.
may contribute to the severity dun eye injury.
Scotian VIII-ENVIRONMENTAL:PROTECTION
ENVIRONMENTAL PRECAUTION& Remove all combastible material•from spill
site.
SPILL OR.LEAK PRECAUTIONS:Wear goggles,gloves and dust mask.Cerefully
sweep or scoop spilt a salvage contain&and hold for disposal. Wash the spill site
thoroughly to remove oxidising residue.
WASTE DISPOSAL;For large spills,seek the advice of a professional disposal service.
Potion IX-REGULATORY CON . OLS
DEPT. OF TRANSTORTATION:Not regulated under the Tram:gat of Dangerous
Ono&Act
DOT CLASSITICA.TION:N/A
DOT PROPER SHIPPING NAME;WA
OTHER DOT INEORMATION:N/A,
WELMIS CLASSIFICATION: D2A
OTHER REGULATORY REQUIREMEICT;one
Section X-PRECAUTIONS;HANDLING,STORAGE&USAGE,
•
. •

•
tor in a coot,dz ,' `Cll vent:bend place away from tnompatibk t rWKaip bags
or Ma drunas dry at all times.Keep containers tightly closed.Wash t}bozo ghiy after
handling Dr ant get it:eyes,on shin.CT ea clothing.
PREPARED BY.MSDS Department DATE:Update 7aouy 14,202
•
•
•
•
•

1
MSDS
JET- Nutrient
I
._J

; . .
-;;;-
•Al 3
Ewing,NI Columbus,OH • Pylestown,PA - Davenpoit;IA'
88-721-F2E3
MATERIALSAEEntbAnairai
24-HOUR ENIEtioENoYASSITANCE:
INNOVATIVE ENVIRONMENTAL TECHNOLOGIES 1-mse421-2222
CHEMTREC 1402424AM
NiAtAlrACTURER:
INNOVATIVE ENVIROXIMENTAI,TECHNOLOGIES
PEAR TAVEMI ROAD
SUITE Sin
WING.NJ InG.20
aluvr21.,fizam •
PRODUCLICIAPMEI=Ott
TRADE NAME:MO IET4
. •
cI,
COMPONENTO:
thig
Numhe r: er.134
solccrEili! embiuside;Cathenyldiarniite:eir.her/dic AIM
Cbtirka?F•thseht: Mite
14*.cular coin id 0444/0 •
ICaticulaff1M3101.1
2. Jame,emilsem iNbniplialattiomc.
•eas Nernber; '7783-2114
Sraccorion NEIFICIRIUM phasplutle,Thariarsorl any hydlidets phimphale,Etthaee -
afffflegolgm poopli.ade '
chorkmFairilyz Sec
Macula:Famiulat Rt4)21W04
ita4vullarlffeig1Tt 13“6
FironasedEcam man •
CASAiumban. 7361mq
Eyftethygnme. OldrUnk add FikelPhie.: PtiiIng magointic,Sodkon dIgydr.ison
gthimpillah;
Munk*Family: Soh
WAWA+PnarmAa; 14010116
Wit-mai;Weight 11532
MODirMlikZARD SUMMARY).
HM1.114:May int haretruI IrAvallICtwed.May lie terilatiro to,the$tirt„evil and reupiratory tract.Heeled
material'may cause Menial bait ns.
FiAmmAsturv:NorkoHnherailbIe
REAVTIVITY:Stable
.R110.12aCtrkr-ALIFINAgaintitMa4=4:
INNOVATIVE PrIngergilkftiAL TECHNOLOGIES.,INC.
PAGE cl'r ..n resource for n014,10 iimeneliee uhergirIjIM tabllIktfre

•
141r r •'`�i
mowing,hi Culiimrbus., A;;IryiestO 'n,PA I a ettp `s
888-721-S283
INGESIJONe$tiglq(rfy.lbsie:.aornerstic animal are Linn of Urea is 511 Mad Acute oral Ions of
Uianefrifltaeelie:rFe Phosphate is 1OIrG nvitto in Mak ram Msy cause gaatroinbestinal dlstirrhAme ,.
syrptonns may table de Imitation,nausea:'ttnmiting and diarrhea.
t3KI SShpbtly initatIntr.Repealed or y~r tonged i c ntact may cause reddeei:rng,Mang and,
infl tloa.Oimsetwith hoelod realeulal mateauso thermal burns:
EYE:Slightly Whiling.Contact with heated material may raise thermal hams,-
INFIALA1Iose slay taus.respiratory 4rett irritation.
SPECIAL TOXIC EFFE :A thmatie sexposed1,doe%mayMesa•diftit:uhy in breathing.Urea es
eeaturallyr e""6ng'grl eettiirai in tlra ibQdy.oh n'end pxodelet ofprobe'.n metabolism.and Is excreted In
Mooting..
EIRSIAIM
•
tNGESTtD _Do dot Induce eon-Nang I .Keep aiteeled orson warm add et test.Got medical ettterigori, ti 4
stilt;CAVI'ACT;Wash erica of contact trn1ou2h[y°with soapatewetter:lagnder ripping-beam masa.
G
e;t rMlita8 attention if Irritation ad b
palrsi�F.�Ioreontae:twitht�dFf�n�r+c��Iuct,da�l�wVa�tintamtnabsd `•' ':.
clouting Flush,skirt In lately with Ia esacils tit bad et,�atca flrFva�ebla�;sufslvmerg�8ieir fti coin! ; �
waiter:Pack with tee T ermalb'utntterwinrhhmedlataattandon, rr t4:
EYE CCNTACY:Fivali Itt9it stately with tee eanis&twater fnt at ltarit 1 8n ruteiites:t=•yei1 e 5 "'•
.
eihnutd bn held away Trony cycbiail to ereeeethorough rinsta�:Got tt>irlidiral ai AYapn r("rtr,i�etran parslsts • `1 t.
- •• 2 ` i•. it d. i `_ t ;: , �[.
FNHJ `flO1 kern weeofi ea'p aaureadt o f ,iotbnlatiiarig;°ensure opera eCrvaay:: t �Y" �;.:
andfrastiw utmona rare s;eiiaikin ),IFIblo liririgladIticurt,ad,nlnletraxyjenilr ,.,.'
:vaflahle:GieZrertediwatle9ellton_ _
•
EERBONA_PePTECI'l + I M;
YJPROThcTfcYnt Wow'safetygrass rserrieera�lzaTg�otestoparev�en$Vie t:natat�.Count Wear ntae l
t er.Fwhen:working+with tide substance.Revs ay+ee'dashing triennial meowavaiiablewfheroeye - -
I C t occir, • . • •
SKIN PROTECTION:N:Wear bripersrious!loves and ileeteeive erorhirog to tereverrt plain s4ntael.$nggeratnd
Prorectn*titatdr1le bolylrubber,
RESP1IiAtORY PROTECTION:Nurlett inaidy:needed.late[yt 3HorRENA Opp rove detqutpmeretwhorl
eltbarrnn exposure iFa,i1A ars excaeetied,.N11OSIvia)lA appranred breathing cq:aipmentmusl Ue auieltebte,
rot rion-routine Anti emergency EltagiirafillP1RDEMIUM
11.1I POINT: LDeeeeopOtes
SPECIFIC eitattrirVI NA
MELTING PONT:, 113.2111 C(*T1411Py)DAP dgcompoklAt1tl$d.0 tPi3 1`}
%wire et NA
VAPOR PRESSURE! NA
EVAPORATION ATIONRl TEIWAT 1} NA
VAPOR bENSInr(Ar i? thIlk
V1$COnrri NA
MOVAVIVE lifirnoMl NIALTECIINOr1 ,INC-.
Esexpa
P lane 100'gaivari il'macre/praftissiar ;s se�*kin.g iraroap-Ohre ir�ltrrrsrtiue kcituntiyi
P ra

•
riveirm NJ + :n1umhi1s,OH Daykatewn,13A Daaanptin, ;;•"
ORS-72l-8 3 _
%SDLUl11LITY11,1WATER,G1VFItpQGM'::1SC Luca 119
PAP .41
MSP Yi
OCTA.NOL!WATER PARTITION CQEFRCtENT= ND
POUR PONT:. NA
itH ND _
+FPEARAN DOR:White genaes«with Mai to no Oder.Ammonia pilot will develop '
• rperi keg si tteri(1.
FISH POINT:- NA .
AUTDIONaTION TENIERATUNE: .NA ••
r'LAsimAp tm'Y WITS IN AIR t NY LOWER: NA •
Fi.AsuamiiLwe UMl'S IN AIR i16 DYVQLUME)UPPER; NA
ElASIC FIREP/GH IH'O PROCE41 S:Use exilagnishing arfleatlituaMi ble Tor fyhanf_tirreuradinilini,
IViaterin1 Itself burns with great difficulty.ffleulty.Urea beta moot silppezyreeisr i wet.Guard op hot fails,
.UNUSUAL FIRE AND EKPIASIQN HAZARDS!Firemgy proaace paisonsvvs'or irrittIFtag has sumeg ar,
• %ANC&MOIR Cc1ox1C silbsiaraeais may heeniltled open theism deeosiviesitivn E.Ipesed1 rvtHgiiterax
should Weer MailiuNppsit.*purred Salt{:ar:lained iueatlaingapparatus with IU®Fate iniiskand MI
pro iergIviregUlpment.'Un bolt inallyddrop,DAP acrid R.are nggexploaIoi hazards'They row*MI
ertplaslra rnIxtuiesaigkititt 1a splasaiameous don101taltivn when coursoeina% Urith"*t!tonp adds(niirlc,
picric.perch orll pr nitrate rertiltzerr::Ai lcv rwd brnperalairrr dry ureUip midi amrimnlai Wet Doge
may hydroltze Ur.BarT,0iVe 4uulionlum cede nnla.A4 oUs aptut1ca n el Lire.t at elcii,aa**.mperaparss
may dacotaa hi biUhly tazlc lhyd'ra9ea^tylitble'I 'decwripaii upan hi�ai rp t4'ammoniaand
.Polyib.oplindc arid.
!I`r'1 4t t iredt11COMPATlBIL I Y:$i4v when a orcd dry 7R msp to isv t~and:atniosphens*sows.Aveld
conies with strung erasletlieers,adds and hunt.and nitrates.Derr mpa ii airionlar bluraL ,COO
anti:polyftliospotic arid` '
14AZARDOLIS ItEiliopTIONV,DECOMPOSITIONPR0 TS;TnensaidecompothieninedMaliattyba
hoard sus..Urea reS w so Ium or opleiwrrt ttiypochltwiie to tom�tploxive n1 6116 'trtchladde.Uicy
heated with ammonium nlp'ate et 470 C or higher,forma e*pieelve nl ro utnldhne.Diaoemealerla
phesPheti will read whit alikMi to literate a tm4
EALTAL IAEt`-C3fGffi :
SPILL AN RELi=Ase TO TiFE PMARONFIE7ITt flci special pueteedutes ass i teer ad for clera up of this
ttaa erlaL Avoid i selhrds that remit Inwait'?pollution.C4ntien should be exercised regarding,p et'seruri
sates and oxpoauns to the nilittivaa ae eat forth elsewhere in thia rlata sheet
EMER+SENcY ACTION;[tacp unnecessary paopto away.
WMTeGISPOSAfe This substance,When doei ed or disiesed of,Fs nal-specificallyMod fit a
•
harardOus wade in Patter's/regulation:however er it could he hazardous hub considered Mods.
corrosive,Fgn table or lea allot U M:dingtoFederal d_'gfrni1ions(4OOFR 261)611.dilideeally,It could be
designated aooaarerdausAs rlingtost lerhdiulations.ThisStibtfanraacouldadobecameaeammoas
LNNO'VAT1VE 1Rortner'At,TECUNO QLES,!NC-.
CsaFs r5 ��1
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wes‘if II in mixed wilts al'comes In contact-!,v1t1t a ItarkeeklUS t;imiste.If auth goniact qr OsIXtrig have
ceDi+rradr Cincit+la CFR RS1 to determine whether it is of hazardous moats,.If It Is a bnarcieus waste,
reaalatiakaS at 4D eFii"2.263 and 264 apply.
The viir.o:port:310N e Ions a,irsatm Izat and glkposal of this waste iftwirial Aunt he condirgioci in
adropliance with all applizabIt FidOralyilate and Mai ronolans.
SARA TITLE gl INFORMATIM MOW holt are firm hazard ordeciafais far the Stott/4mnd Ara!widosants '
and Re aulltorixotion Act(SARA)Sectleri4111312(40 CFR 470): ' • •
liniticdFale ifitat.14416.-T;oelayed•NitiliodyilzAtre Naned-ca-Predeme Hazand-
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211 .
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,.
. . . • .. . '
REGULACCErtiVINEORMAEM:- .
. • . ; •••„
. .AIJ coinixononis of ifsi plvduct arsBaled oar the Illtiri Nagentery, ,••,•,-',..:;:,. .
All COMPOn (ra 0 this proirect ore Ested on the CavietlieriOSL Inventory.
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ittikkf_liG.- .:-/IA111_1=BAci.E. (SiMfitiO3,p_g- .. : _ ,.
RANcuNc.i3TerRAORT,1$107.50 tigfilly domed containets'in cool.dry,isoinied,iisvii vanilianizil area away
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: .. ., .•
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Bin of Lading Dasixiption fa CFR in.20.2.1 IRO tET-3 •
DAV.Labels Required(49:0FR 174.101).:.: NA
,C.0..T.Placards Rtuaulred NA
INDIEDIDIMANDILMTIMMARiatlaRMTEOlt:
gLOMPANYA DeAlagialig. 91 liguagiBLIVEMBIE.
Dow STA34 me 14 mg,1111°warm intania us iustsseet dug
no Thisilia t Sib
rasp niveo7, 24 is
Revisits&Oafs;4,rifarck 2002
NA la Not Applicable . •
ND:No D014 IMIOVATIVE EIVIRONMENTAL TrktE10 ' '`4 INC.
rriR -resource for mitimillpftil pagEssinEds azzrzill9
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PACE4 OF 4
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.....

NIACET CORPORATION MSDS
400 47th St. NIACET
Niagara Falls, NY 14304 CALCIUM PROPIONATE
Fax[phone]
Ph [phone] Issued: January 2006
EMERGENCY PHONE NUMBER: [phone],[phone]
MATERIAL SAFETY DATA SHEET
CALCIUM PROPIONATE
Page 1 of 2
SECTION I - PRODUCT IDENTIFICATION
Product Name: NIACET Calcium Propionate,FCC
Chemical Synonyms: Cal Prop,CP
Chemical Family: organic acid,calcium salt
Chemical Formula: (C3H502)2Ca
SECTION II- INGREDIENTS %by wt. CAS#
Calcium Propionate(dry basis) 99 min 4075-81-4
Water 5 max 7732-18-5
SECTION III- PHYSICAL DATA
Molecular Weight: 186.22 Appearance: white powder,granules,or crystals
pH of 10%Aq Soln: 7.5 to 10.5 Odor: odorless
Melting Point: 400'C(decomposes) Boiling Point: not applicable
Vapor Pressure: not applicable Bulk Density: approx.45 lbs./cu.ft.
Solubility in Water: 28.5%in water at 20'C Reactivity in Water: does not react
SECTION IV- FIRE & EXPLOSION HAZARD
Flash Point: None by Tag Closed Cup
Flammable Limits: Not Determined Auto-Ignition Temperature: Not Applicable
Unusual Hazards: Avoid dispersion of dust to minimize possible explosion hazard.
Extinguishing Media: Appropriate media for surrounding fire.
SECTION V- REACTIVITY DATA
Hazardous Decomposition Products: Carbon monoxide
Hazardous Polymerization: Will not occur.
Incompatibility: Strong oxidizing agents
SECTION VI-TOXICITY DATA
Calcium Propionate is a non-toxic food chemical Generally Recognized As Safe by the FDA
Occupational Exposure: No exposure limits have been set by OSHA,NIOSH or ACGIH.
Carcinogen: IARC: NO, NTP: NO,OSHA: NO

NIACET CORPORATION MSDS
400 47th St. NIACET
Niagara Falls,NY 14304 CALCIUM PROPIONATE
Fax[phone]
Ph [phone] Issued: January 2006
EMERGENCY PHONE NUMBER: [phone],[phone]
Page 2 of 2
SECTION VII- HEALTH HAZARD INFORMATION
Primary Routes of Exposure:
Ingestion: If swallowed,wash mouth out with water.
Eye Contact: Can cause irritation. Flush with water for at least 15 minutes, hold eyelids open.
Get medical attention.
Skin Contact: May cause irritation of the skin. Wash area with soap and water.
Get medical attention if irritation persists.
Inhalation: If irritation develops, remove to fresh air.
Effects of Overexposure:
Dust, in high concentration, may cause irritation of eyes, nose and throat.
Medical Conditions Aggravated by Exposure:
None identified. Handle with reasonable care.
SECTION VIII - EMPLOYEE PROTECTION
Protective Clothing: Appropriate work apparel. Plastic or rubber gloves optional.
Eye Protection: Safety glasses should always be worn when working with chemicals.
Respiratory Protection: Material should be handled in a manner that does not produce airborne particles.
If dust is a problem a dust mask or respirator is recommended.
SECTION IX-SPILL AND DISPOSAL PROCEDURES
Action to be taken for Spills:
Wear suitable protective clothing including a respirator or dust mask. Sweep up spillage and collect for
disposal. Wash down area with large quantities of water.
Disposal Methods:
Material is biodegradable. Dispose of in accordance with applicable Federal, state and local regulations.
SECTION X-OTHER REGULATORY CONTROLS
Calcium Propionate TSCA Inventory: YES (all ingredients)
OSHA Hazard: NO
Regulated under RECRA: NO
Regulated under CERCLA: NO
Regulated under SARA Title III: NO
The information herein is given in good faith and believed to be accurate and has been compiled from
sources believed to be reliable. Buyer assumes all risk of use,storage and handling of this product in
compliance with applicable federal.State,and local laws and regulations.

341 Christian Street, Oxford, CT 06478 USA
NATURAL SOURCING,. Tel: [phone] Fax: [phone]
Y3t1}`, $nutmllc+, www.naturalsourcinci.com [e-mail]
MATERIAL SAFETY DATA SHEET
ORGANIC KELP POWDER MSDS
(Ascophyllum nodosum)
1. PRODUCT NAME AND COMPANY IDENTIFICATION
Product Name: ORGANIC KELP POWDER(Ascophyllum nodosum)
Product Use: Personal Care Formulations
Company Name: Natural Sourcing
Company Address: 341 Christian Street, Oxford, CT 06478, USA
Date Issued: 7/1/2008
Emergency Telephone Number: Chemtrec Tel: [phone]
2. COMPOSITION/INGREDIENT INFORMATION
Ingredients: Concentration 0/0
Ascophyllum nodosum (Kelp) 100%, Powdered
Hazardous Components: None
3. HAZARDS IDENTIFICATION
Routes of Entry
Eyes: Mild Irritation may occur
Skin: No known hazard
Inhalation: No known hazard
Ingestion: No known hazard
r4. FIRST AID MEASURES
Eyes: Flush with plenty of water or eye wash solution for 15 minutes.
Get medical attention if irritation persists.
5. FIRE FIGHTING MEASURES
Extinguishing Media: Water Spray, Foam, Powder and Carbon Dioxide
Special Firefighting Procedures: N/A
Unusual Fire &Explosion Hazards: N/A
6. ACCIDENTAL RELEASE MEASURES (STEPS FOR SPILLS)
Precautions: N/A
Methods for Cleaning Up: Sweep up or flush with water and dispose of according to local
regulations.
7. HANDLING AND STORAGE
Safe Handling: Wear safety glasses, Wear dusk mask
Requirements for Storage Areas and Keep container closed, away from sunlight and protected from
Containers: humidity.
Page 1 of 2

8. EXPOSURE CONTROL/PERSONAL PROTECTION
Eye: Safety glasses should be worn.
Skin/Body: Gloves should be worn.
Respiratory: Wear dusk mask.
Ventilation: Ensure good ventilation of the work situation.
Other: Evaluate need based on application.
Work/Hygiene Practice: Normal work and hygiene practices
9. PHYSICAL AND CHEMICAL PROPERTIES
Physical State: Powder
Color: Green
Odor: Characteristic, fish-like
10. STABILITY AND REACTIVITY
Stability: Stable
Incompatibility (Materials to Avoid): N/A
Hazardous Decomposition or N/A
Byproducts:
Conditions to Avoid: Avoid contamination of product, sunlight and damp conditions.
11.TOXICOLOGICAL INFORMATION
Toxicity Data: Non toxic
12. ECOLOGICAL INFORMATION
Persistence and Degradability: Easily Degradable
13. DISPOSAL CONSIDERATIONS
Waste Disposal Methods: Dispose of according to local, state and federal regulations.
14. TRANSPORT INFORMATION
DOT Classification: Not classified
15. REGULATORY INFORMATION
No Information
16. ADDITIONAL INFORMATION
This information is provided for documentation purposes only.
This product is not considered hazardous.
The complete range of conditions or methods of use are beyond our control therefore we do not assume any responsibility and
expressly disclaim any liability for any use of this product.Information contained herein is believed to be true and accurate however,
all statements or suggestions are made without warranty,expressed or implied,regarding accuracy of the information,the hazards
connected with the use of the material or the results to be obtained from the use thereof.Compliance with all applicable federal,state,
and local laws and local regulations remains the responsibility of the user.
This safety sheet cannot cover all possible situations which the user may experience during processing. Each aspect of your operation
should be examined to determine if,or where,additional precautions may be necessary. All health and safety information contained in
this bulletin should be provided to your employees or customers.
1
Page 2 of 2

oxicological &
'Environmental
Associates, Inc.
MSDS DATE: 6/12/2008
MATERIAL SAFTEY DATA SHEET
SECTION 1:PRODUCT AND COMPANY IDENTIFICATION
PRODUCT NAME: Emulsified Zero-Valent Iron
SYNONYMS: EZVI
PRODUCT CODES:
MANUFACTURER: Toxicological&Environmental Associates,Inc.
ADDRESS: 10636 Linkwood Ct.
Baton Rouge,LA 70810
EMERGENCY PHONE: [phone]
CHEMTREC PHONE: [phone](Domestic)
703-527-3887(International,Collect Call)
OTHER CALLS:
FAX PHONE:
CHEMICAL NAME: Emulsified Zero-Valent Iron(EZVI)
CHEMICAL FAMILY:
CHEMICAL FORMULA:
PRODUCT USE: Environmental remediation
PREPARED BY: Toxicological&Environmental Associates,Inc.
SECTION 1 NOTES:
SECTION 2:COMPOSITION/INFORMATION ON INGREDIENTS
INGREDIENT: CAS NO. %WT %VOL SARA 313 REPORTABLE
Water 7732-18-5 40-50 NA NA
Soybean oil 8001-22-7 30-40 NA NA
Iron 7439-89-6 8-20 NA NA
Sorbitan trioleate 26266-58-0 1 -5 NA NA
ppm mg/m3
OSHA PEL-TWA: NA NA
OSHA PEL STEL: NA NA
OSHA PEL CEILING: NA NA
ACGIH TLV-TWA: NA NA
ACGIH TLV STEL: NA NA
ACGIH TLV CEILING: NA NA
SECTION 2 NOTES:
PAGE 1 OF 6
1

toxictoxicological &
ological
associates, Inc.
MSDS DATE: 6/12/2008
SECTION 3:HAZARDS IDENTIFICATION
EMERGENCY OVERVIEW:
ROUTES OF ENTRY:
EYES: YES
SKIN: NO
INGESTION: YES
INHALATION:NO
ACUTE HEALTH HAZARDS:NA
CHRONIC HEALTH HAZARDS:None Known
MEDICAL CONDITIONS GENERALLY AGGRAVATED BY EXPOSURE:None Known
CARCINOGENICITY
OSHA: ACGIH: NTP: IARC: OTHER:
NA NA NA NA NA
SECTION 3 NOTES:
SECTION 4: FIRST AID MEASURES
EYES: In case of eye contact,rinse opened eye for 15 minutes then consult a doctor.
SKIN: In case of skin contact,immediately wash with water and soap and rinse thoroughly.
INGESTION: In case of ingestion,after swallowing seek immediate medical advice. Make doctor aware that the following
symptoms may occur:nausea,cramps,gastric or intestinal disorders.
INHALATION:NA
SECTION 4 NOTES:
SECTION 5:FIRE-FIGHTING MEASURES
FLAMMABLE LIMITS IN AIR, UPPER: NA
(%BY VOLUME) LOWER: NA
FLASH POINT:
F: >482°F
C: >250°C
METHOD USED:Closed Cup
AUTOIGNITION TEMPERATURE:
F: >760°F
c: >404°C
PAGE 2 OF 6

oxicological &
environmental
ssociates, Inc.
MSDS DATE: 6/12/2008
NFPA HAZARD CLASSIFICATION*SCALE:4-extreme,3-High,2-Moderate,1-Low,0-Insignificant
HEALTH: 1 FLAMMABILITY: 2 REACTIVITY:1 OTHER:None
HMIS HAZARD CLASSIFICATION
HEALTH: 1 FLAMMABILITY: 2 REACTIVITY:1 PROTECTION:
EXTINGUISHING MEDIA: Extinguishing Powder
SPECIAL FIRE FIGHTING PROCEDURES: Do NOT use water,carbon dioxide,or halogenated extinguishers.
UNUSUAL FIRE AND EXPLOSION HAZARDS: NA
HAZARDOUS DECOMPOSITION PRODUCTS: NA
SECTION 5 NOTES:
SECTION 6:ACCIDENTAL RELEASE MEASURES
ACCIDENTAL RELEASE MEASURES:
Person Related Safety Measures:Wear Protective Equipment,Keep unprotected persons away,Ensure Adequate
ventilation
Environmental Safety Measures:NA
Measures for cleaning/collecting:Dispose contaminated material as waste according to section 7
SECTION 6 NOTES:
SECTION 7: HANDLING AND STORAGE
HANDLING AND STORAGE:
Contain spilled material and recover into drums.
Ensure good ventilation at the workplace. Keep ignition sources away. Do not store together with oxidizing and acidic
materials. Store away from halogens.
SECTION 7 NOTES:
SECTION 8: EXPOSURE CONTROLS/PERSONAL PROTECTION
ENGINEERING CONTROLS: Block off area from unprotected persons
VENTILATION: Ensure adequate ventilation
RESPIRATORY PROTECTION:NA
EYE PROTECTION:Safety Goggles
PROTECTIVE GLOVES:Rubberized gloves(neoprene or pvc)
PAGE 3 OF 6

Toxicological &
Environmental
Associates, Inc.
MSDS DATE: 6/12/2008
PROTECTIVE FOOTWEAR:Slip resistant footwear
SKIN PROTECTION:Outer clothing to minimize dermal contact.
WORK HYGIENIC PRACTICES:Surfaces covered with EZVI are very slick. Exercise care in handling or clean up to avoid
injury due to falls.
SECTION 8 NOTES:
SECTION 9: PHYSICAL AND CHEMICAL PROPERTIES
APPEARANCE:Grey to Black,Viscous Liquid
ODOR:Soybean Oil(cooking oil)odor
PHYSICAL STATE:Liquid
pH AS SUPPLIED:
pH(Other):
BOILING POINT:
F: >572°F
c: >300°C
MELTING POINT:
F: -4°F
C: -20°C
FREEZING POINT:
F: NA
C: NA
VAPOR PRESSURE(mmHg):
F: NA
c: NA
VAPOR DENSITY(AIR=1):
F: NA
C: NA
SPECIFIC GRAVITY(H20=1):
1.05—1.10 g/cm3
EVAPORATION RATE(Butyl Acetate=1):NA
I
SECTION 9: PHYSICAL AND CHEMICAL PROPERTIES(con't)
SOLUBILITY IN WATER:Insoluble
PERCENT SOLIDS BY WEIGHT:10—17%
PERCENT VOLATILE:
BY WT/ BY VOL @
F:NA
C:NA
VOLATILE ORGANIC COMPOUNDS(VOC):
PAGE 4 OF 6

oxicological &
Environmental
ssociates, Inc.
MSDS DATE: 6/12/2008
WITH WATER: NA LBS/GAL
WITHOUT WATER: NA LBS/GAL
MOLECULAR WEIGHT: NA
SECTION 9 NOTES:
SECTION 10:STABILITY AND REACTIVITY
STABLE UNSTABLE
STABILITY: X
CONDITIONS TO AVOID(STABILITY):Avoid improper handling and storage conditions.
INCOMPATIBILITY(MATERIAL TO AVOID):acids,oxidizing agents,halogens
HAZARDOUS DECOMPOSITION OR BY-PRODUCTS:If combined with halogens will produce hydrogen gas.
HAZARDOUS POLYMERIZATION:NA
CONDITIONS TO AVOID(POLYMERIZATION):None
SECTION 10 NOTES:
SECTION 11: TOXICOLOGICAL INFORMATION
TOXICOLOGICAL INFORMATION:NA
SECTION 11 NOTES:
SECTION 12: ECOLOGICAL INFORMATION
ECOLOGICAL INFORMATION:NA
SECTION 12 NOTES:
SECTION 13: DISPOSAL CONSIDERATIONS
WASTE DISPOSAL METHOD:Store waste materials into appropriate drums
RCRA HAZARD CLASS:NA
SECTION 13: DISPOSAL CONSIDERATIONS(con't)
SECTION 13 NOTES:
SECTION 14: TRANSPORT INFORMATION
PAGE 5 OF 6

' oxicological &
'Environmental
associates, Inc.
MSDS DATE: 6/12/2008
U.S.DEPARTMENT OF TRANSPORTATION
PROPER SHIPPING NAME: Emulsified Zero Valent Iron
HAZARD CLASS: NA
ID NUMBER: NA
PACKING GROUP: None
LABEL STATEMENT:
WATER TRANSPORTATION
PROPER SHIPPING NAME: Emulsified Zero Valent Iron
HAZARD CLASS: NA
ID NUMBER: NA
PACKING GROUP: None
LABEL STATEMENTS:
AIR TRANSPORTATION
PROPER SHIPPING NAME: Emulsified Zero Valent Iron
HAZARD CLASS: NA
ID NUMBER: NA
1 PACKING GROUP: None
LABEL STATEMENTS:
OTHER AGENCIES:
SECTION 14 NOTES:
SECTION 15:REGULATORY INFORMATION
U.S.FEDERAL REGULATIONS
TSCA(TOXIC SUBSTANCE CONTROL ACT):NA
CERCLA(COMPREHENSIVE RESPONSE COMPENSATION,AND LIABILITY ACT):NA
SARA TITLE HI(SUPERFUND AMENDMENTS AND REAUTHORIZATION ACT):NA
311/312 HAZARD CATEGORIES:NA
313 REPORTABLE INGREDIENTS:NA
STATE REGULATIONS:NA
INTERNATIONAL REGULATIONS:NA
IMPORTANT:The information contained herein relates only to the specific material identified.Toxicological&
Environmental Associates,Inc.believes that such information is accurate and reliable as of the date of this
material safety data sheet,but no representation,guarantee or warranty,express or implied,is made as to the
accuracy,reliability,or completeness of the information.Toxicological&Environmental Associates,Inc. urges
persons receiving this information to make their own determination as to the information's suitability and
completeness for their particular application.
PAGE 6 OF 6

Autolyzed yeast
0i.
Provesta® 027
I' i Product Code: 50300 i'
PRODUCT SPECIFICATION
Chemical and physical data
- Parameter Unit Min. 1 Max. Method
`Moisture % 7 100 deg F oven.24 hours
[Protein in product % 49 ,AOAC 988.05
Microbiological standard
Parameter Unit Specification Method
Total plate count cfu/g <7,500 48 hrs at 30 deg F
Yeasts and molds cfu/g <50 3 days at 30 deg F
E.coli cfu/g NEG FDA BAM Revision A of 8th Ed,1998 Chp.4
Coliforms efu/g <10 FDA BAM Revision A of 8th Ed, 1998 Chp.4
Staph aureus _ cfu/g <10 FDA BAM Revision A of 8th Ed,1998 Chp.12 _
~Salmonella NEG!375 g NEG AOAC/BAM Method 2004.03
Typical.Nutritional Information
Calorie 371/100g Cholesterol <Img/100gO./
Calories from fat 63/100g _r Ash _ 8g/100g
I Calories from Saturated fat 7.2/100g Sodium 0.1Og/IOOg
Protein 52g/lO0g Potassium 2.5g/100g
Carbohydrates 26g/100g Vitamin A(1U) <44IU/100gti)
Dietary Fiber 5g/100g Vitamin C(ascorbic acid) : <0.5mgl100gt"t
Sugar-Total <lg1100g Tl Calcium 0.015g/100g
Fat--Total 7gllOOg Iron 0.010g/100g
Saturated Fatty Acids _ 0.81;1I00g ,
Trans Fatty Acids , 0.07g1100g
CO)Below Detection Limit
a.
1
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Uititeti States Toll Frm:O3'OO 321 2cc 8.4

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•
' „-__-s $ - .s �� .1 I ` Figure H-1
�i•.`4 6 .� . 1 1 Site Location Map
wits. , -' �K ,r 'sr y , \ Walter Kidde Portable Equipment, Inc.
USGS'Topogri-' ,,Map NationaliG•eograpOic:T,OPO. ` �7 } Mebane, North Carolina
ESRI ArcG*IS Online*Mebane Quadrangle North Carolina k4 i
I/ '�i:.. j�+► .1 t .. ,.° f:14-- ,- \ R�,',,, fit'
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• l3! c !11 E �. 4 1 17 ,I1 i t l t 1 —
12/13/2011 X:IUTCIMebane_NCIProjects\site_location.mxd
I

Kidde Offices
Warehouse
DC-1 a
Legend
1/4 Mile from Injection Area
Parcel #163657
Location
Production Well
Monitoring Well
O MW Top of Bedrock
MW Bedrock
Site Features
• Property Boundary
Building
Structure
Conc-Pavement
Intermittent Drainage
Topographic Contours
Heptane
Shed
Warehouse
DC-2
1 m•3006
_a -
200 100 0
Feet
n1i gelU,SA P 'me
MW0at
4.
t Waterhouse
Proposed Injection Area
Parcel # 163657
1 well record at Alamance County.
Abandoned 10/10/2006.
No other information available.
Figure H-2
Site Layout
UIC Permit Application
Walter Kidde Portable Equipment, Inc.
Mebane, North Carolina
r}.11]:2011 D1projectAUTClMebane1RAP_20111FIgureH 3 PolentlomatrlcConlours201108AZ.mml

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I \ \ TeelingAreaMW020 \\ I r .____
I ';'•
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• \ 628.58 '
1 630.64 \ 1 \ t,
j MW017 � MW015._ \ \ 1 I \ 1,/
1 638:23 MW042 629 33762625
•
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( I I 632.10 caGv V I ti
I
I MC006 `k MW044 - \, \ f /
' 635.67 • 631.40 se MW009 MCO29- I / ',•1'" ;
1• I MW028\ 4 630.77 . f632.58 \ 1 11 1\ 1, 1, ,; / Mw030s ,.•-''
'\ M8006 635.37 � I I ; \ / f 608.76 �`
635.66,\ \ \ i MB829 ! I I \ \ \ ./J-' 1! f.
\ ops , MW007�$ 632.47 1 \ \ / 777% / _-
687 84 • \632.65 MW008 \ MW029 1 1 i MW016 \\ - �-/, ,!c,,I✓ //r�
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' I
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�I
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1 \� ... i
1
Legend I • I \
_ \
Potentiometric Surface
Contour(ft msl,5 ft interval)
Arrow I
I
Location i I
{a Production Well I [ V „..-•
Monitoring Well I
n MW Top of Bedrock _ rT '- Figure H 3
Potentiometric Contours
MW Bedrock = August 2011
Site Features UIC Permit Application
• Property Boundary Walter Kidde Portable Equipment, Inc.
Building Mebane, North Carolina
Structure
Conc-Pavement 100 0 200 EAISAFE
Intermittent Drainage , i
Topographic Contours Feet
i
12/13)2011 D:1p,olecls\UTCVAebeno\RAP 20111FIgureR 3 PolenrometrIcConlours201108 AZmxd

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1 A1:
1
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1 Q�
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1 •
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1
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' I
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t d V
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I • hMW011 * i
1 63S 1
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1 MW041 I
1 •MW040
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1
�MW014 1
1
I I
1 I
I
I I
I I
I J
I / /
1 MW036 '/
1 r /
I / /
I / /
Legend
Location Isoconcentration Potentiometric Contours
Monitoring Well Concentrations in micrograms per liter(pg/I) (08/2011 Data)
n MW Top of Bedrock 1,1-Dichloroethene(11 DCA) '' Arrow Figure H-4-1
MW Bedrock 11 DCA Inferred Contour CVOC Plume Map
UIC Permit Application
Site Features 1,1-Dichloroethene(11DCE) Intermittent Drainage Walter Kidde Portable Equipment,Inc.
— — Property Boundary 11DCE Inferred I Mebane,North Carolina
Building Tetrachloroethene(PCE)
100 50 0 100 £IVSIIFE
Structure .�.�
Conc-Pavement reel
12/13/2011 D:1projects\UTC\Mebane\RAP 20111Figure3 2 CVOC_Plume_Map_AZ .mxd

MW034
N 1 $
AMD003
$ MW003 MW024 r' - ,
$ t 7p •
I MW035 t •
..
0 I
•
MW002 I 1
• 1
1
• ' 1
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t 1
i ._ - - y — 1
MW021 WO -- — _
$ N.
4r I 4
/ •
/ '• t
/ t
• I
. 038 f $
$ o 1
\ ca
0 , MW032
805 MW022
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r
was sr° _ _ _ -
_ ter
MW01: MBO19 . T
OVVO3T—L
_ $ MC019 6rs, s
�� ®MBO51 / $®° AA, Downgradient /
o MWO19 Monitoring $
Groundwater rillkMW052 - '
Injections _ "
Targeted � � � ''"
sw MW0500 -1111b Residual MW020
rr DC-2 •1� Sourceow. - — t
$11P/ AC Pi .-, . .,., * 1
_ Soil Injections / oi .0,1
MWi.. $ j
A 017
� AIME�: MW015
4/ I _ .1°
�� Legend Figure H 4 2
Selected Remedial Approach
tar
f � Potentiometric Contours Isoconcentration (pg/l) Site Features UIC Permit Application
I �. y ""—.l a { Arrow 1,1-Dichloroethene(11DCA) Other Features Walter Kidde Portable Equipment,Inc.
MP" �' — Contour 11DCA Inferred -- — Property Boundary Mebane,North Carolina
Monitoring Well 1,1-Dichloroethene(11DCE) Intermittent Drainage
1 ( 100 50 0 100 MW Top of Bedrock 11DCE Inferred Building alSAFE
.....
_______
_ -
Feet MW Bedrock '- - Tetrachloroethene(PCE) Structure
Intermittent Drainage Cone-Pavement
/‘ r` "fi`Concentrations are in micrograms ger liter s,p}/I J
12/13/2011 D:lprojects\UTC\Mebane\RAP_20111Figure5_1_PropAreas for Remediation AZ.mxd

e
SOUTHWEST D
MW043 SB61/K9 DCIL2ING MW-45/I11
0 : �� PP47
NORTHEAST1STFILL SB66 MW48 H13 SB68/MW49/G13 SB70/MW50/F14 SB72/MW52/E15 SB74/MW51/D15
•
r PFP Fir;°If rad r=rrA Fir,ZOr /
■ (SOIL) PCE = 45.5
10-
r/7 r7TrI7rI f •
(SOIL) PCE = 17.5 (SB61)
il ( 4111
SOIL) PCE = 379 (K9) •
•
/ EZVI SOURCE SOI �
.+. 111111 INJECTION AREA o
PCE = �2 �� �
20 t 1,DCA ;IF ///7777// I '
1,1-DCE = 3 I
i 1 x
501E PCE = 1180 i _ _ La
—.41
wk. <rc4
z.-ArAll 01; .• ,,,, a maio. GROU SOURC INJECTION AREA
30- w I ■r �`AT
. t
AiAer
K=1.6E-3 cm sec IR: Mrr
TD=30' `_
(SOIL) PCE = ND, 1� ��PCE = 37.6
w/ n M 1,1-DCE = 15.5 �I
EN
40- a I of TD=40' w
:: 1.1
TD= r■PCE-= 141, I _
1 (SOIL) PCE = ND 1:1,1-DCA = 10.1 ? ——— ? _ fl P 1-DCA = 7.6 ■ - SOIL SAMPLED
■ 1=DCE-=631-'
:1 11 _ ■f 1,1-DCE = 36.5
--. - �— - - _ — jK=i.27Ecm/sei - SCREENED IN1LRVAL
50- ct J ■ I1 I K=9.74E-5 cm sec 11
rz r
i a ,_ II— VERY MOIST TO WET SAPROLITE
m n
w �1- SLIGHTLY MOIST TO MOIST SAPROUTE
(S+ PCE = 1.2 0 'llll/l/l!i- EZVI SOURCE INJECTION AREA
1.----2_ Q ®- GROUNDWATER SOURCE INJECTION AREA
6�1 0,LZI•TD=60' •� . N PCE SOIL RESULTS (mg/kg) 2011
:oN ♦♦*♦♦♦♦♦1♦♦♦.♦`� A1111.116., La N. La 11E DCA- GROUNDWATER RESULTS (pg/L) 2011
X� . +.:... , 'YiriP- � vr3 I f r .gri 1,1-DCE
7i �� � �«`�� � /1 + ' ���� �` ��*++ * PCE = 1.6
PCE =A 6 1.5 50 0 50
+* *its#+► 4.4;11P i ,i 1e1/4 ►....: ►+ • 4,40.* +�***44:*• .. `► 11* 1,1-DCE = 47.4
*♦♦♦♦♦♦♦♦ ♦♦i/ ♦ ♦♦♦♦♦�♦♦♦+♦♦♦ ♦ ►♦♦ ` HORIZONTAL SCALE FEET
♦�►,�♦♦ ♦*♦♦♦♦ ♦ TRANSITION ZONE ♦ ♦♦♦♦♦♦ ♦♦ ? ♦♦♦♦ n =
+♦♦`♦�►♦+�;♦♦i� ♦+♦♦♦ ♦+♦ ♦ ♦ VERTICAL SCALE: 1 10�♦♦♦♦♦*♦* ♦♦��BEDROCK ROCK FRAGMENTS♦♦`♦♦♦♦♦♦+ ♦� ♦ ♦�
♦♦♦♦♦♦.%... IN SAPROLITE .♦*♦♦♦♦♦♦♦ �r,� FIGURE H-5
8i COMPETENT #♦♦ ir
•♦♦♦♦ ♦+*♦r+ +' ♦+♦♦♦♦♦ ♦41'♦♦♦♦/'*♦♦+�♦♦♦* COMPETENT 74, SOUTHWEST - NORTHWEST
2 AREA
GEOLOGICCROSS SECTION
♦+♦♦♦♦♦♦��,♦ �♦♦*♦++♦♦♦♦*•♦.♦♦+♦`♦♦♦+♦.♦♦�►♦ BEDROCK
a � ♦♦#* 4 � ♦ WATER KIDDE PORTABLE EQUIPMENT, INC.
♦+�♦ ►♦30 79' 11/. ♦... ♦, ♦4♦" ?
REQUESTED BY: MATTHEWS EJI�����
DRAWN BY: BRONSON
THEORIZE FRACTURE ZONE LESS RESISTANT BEDROCK DWG DATE: 12/12/11 Cep ustinkinlutions:
90 [phone]
DWG NO: 10202_B002 www.ensafe.com
I:\2011 PROJECTS BST\10202 UTC NC\Plum\10202-8002—CROSS SEC_A ALYTICAL DATA--D2AREk.KIDDE NC.dwq _ _

Aryl
wit
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Charles Wakild, P.E. Dee Freeman
Governor Director Secretary
February 29,2012
Richard H. Bennett—Vice President of Environmental Health and Safety
United Technologies Corporation
One Financial Plaza, Mail Stop 503
Hartford, Connecticut 06101
•
Ref: Issuance of Injection Permit WI0400231
Walter Kidde Portable Equipment, Inc.
Mebane,Alamance County,North Carolina.
Dear Mr. Bennett:
In accordance with the application received on December 29, 2011 and additional information received on February 20,
2012, we are forwarding permit number WI0400231. This permit is to inject Zero-valent Iron, Adventus EHC, Calcium
Propionate, Hydrolyzed Kelp, Yeast Extract, Sodium Sulfite, Bio IET-3, Vitamin B2, and Vitamin B12 for the dissolution
and facilitated bioremediation of chlorinated solvents, volatile organic compounds, and other substances at the facility
referenced above. This permit shall be effective from the date of issuance until January 31, 2014, and shall be subject to
the conditions and limitations stated therein, including the requirement to submit a final project evaluation as stated in
PART VII—MONITORING AND REPORTING REQUIREMENTS. Please read the entire permit to ensure that you are
aware of all compliance requirements of the permit.
You will need to notify this office by telephone 48 hours prior to initiation of operation of the facility. In order to
continue uninterrupted legal use of the injection facility for the stated purpose, you must submit an application to renew
the permit 120 days prior to its expiration date. Please contact me at 919-807-6352 or at [e-mail] if
you have any questions about your permit.
Best Regards,
David Goodrich, L.G.
Hydrogeologist
cc: Sherri Knight, Winston-Salem Regional Office
Lori Anne Goetz, ENSAFE,Inc.,5724 Summer Trees Drive,Memphis, TN 38134
Kim T.Caulk,Division of Waste Management-Superfund Section
WI0400231 Permit File
AQUIFER PROTECTION SECTION
1636 Mail Service Center,Raleigh,North Carolina 27699-1636
Location:512 N.Salisbury St.,Raleigh,North Carolina 27604 One
Phone:[phone] FAX:[phone] North C arol ina
Internet:www.ncwaterquality.orq
Naturally
An Equal Opportunity\Affirmative Action Employer

AF7A
.17
NCDENR
North Carolina Department of Environment and Natural Resources
a
Division of Water Quality
Beverly Eaves Perdue Charles Wakild, P.E. Dee Freeman
Governor Director Secretary
January 19,2012
Richard H. Bennett—Vice President, Environment,Health, & Safety
United Technologies Corporation
One Financial Plaza
Mail Stop 503
Hartford,CT 06101
Subject: Acknowledgement of
Application No.WI0400231
Walter Kiddie Portable
Equipment,Inc.
Injection In situ Groundwater
Remediation Well(5I) System
Alamance County
Dear Mr. Bennett:
The Aquifer Protection Section acknowledges receipt of your permit application and supporting
documentation received on December 29, 2011. Your application package has been assigned the number
listed above, and the primary reviewer is David Goodrich.
Central and Winston-Salem Regional Office staff will perform a detailed review of the provided
application, and may contact you with a request for additional information. To ensure maximum
efficiency in processing permit applications, the Aquifer Protection Section requests your assistance in
providing a timely and complete response to any additional information requests.
Please note that processing standard review permit applications may take as long as 60 to 90 days
after receipt of a complete application. If you have any questions, please contact
David Goodrich at(919) 807-6352 or [e-mail].
S'-Icerely,
a1 Ualk) I
for Debra J. Watts
Groundwater Protection Unit Supervisor
cc: Winston-Salem Regional Office,Aquifer Protection Section
Craig Wise—EnSafe,Inc.
Permit File S.'I0400231
AQUIFER PROTECTION SECTION
1636 Mail Service Center,Raleigh,North Carolina 27699.1636
Location:512 N.Salisbury St.,Raleigh,North Carolina 27604 One
Phone:[phone] FAX:[phone] NorthCarollna
Internet:www,ncwaterauality.ora Naturally
An Equal Opportunity 1 Affirmative Action Employer

_.
•
Fax Number: [phone]
From: Goodrich, David
Sent: Monday, February 20, 2012 12:48 PM
To: 'Igoetz©ensafe.com'
Subject: Additional Information Request for the Walter Kidde Portable Equipment Co. Injection Permit
Ms.Goetz:
I am working on the injection permit for the subject site in Mebane, NC.
As part of our Division's review,the State's Epidemiology Section examines each of the injectant substances for potential
health effects and long-term impacts.They have requested information on sites where Bio IET Nutrients and Calcium
Propionate have been used in the past for groundwater remediation (not necessarily together).They are particularly
interested in the initial contaminant concentrations detected in the ground water,in the post-injection groundwater
monitoring data which show changes in the concentration of the contaminant,the concentrations of the injectant
substance in the ground water over time,and in any detected chemical changes in the ground water as a result of the
treatment.
Would it be possible for you to provide us with this information,or to direct us to someone who could?
Thank you for your help with this issue.
Regards,
David Goodrich
Aquifer Protection Section Central Office
Office Telphone Number: [phone]
Aquifer Protection Section Main Number: [phone]
Fax Number: [phone]
This electronic message and attachments are sent for convenience and
informational purposes only, unless labeled explicitly as a transmittal of a
final and complete report. Otherwise, this message may represent a summary in
which limitations, conditions, and further explanations may have been omitted in
the interest of brevity and time constraints. The content of this message and
attachments may be preliminary or incomplete, subject to review and revision or
may be in Draft form. If this message contains Findings, Conclusions or
Recommendations, then EnSafe may submit a follow-up hard copy document, which
will serve as the final record and shall govern in the event of conflict between
electronic and hard copy documents. This message and attachments are the
property of EnSafe and are confidential. The information contained herein is
intended solely for the use of the intended recipient; all others should delete
this electronic message and all attachments.
2

•
Goodrich, David
To: Lori Goetz
Subject: RE: Correction to Additional Information Request for the Walter Kidde Portable Equipment Co.
Injection Permit
Lori—
Thank you for clarifying that for me.Additional information on Bio IET Nutrients will not be necessary.
David Goodrich
Office Telphone Number: [phone]
Aquifer Protection Section Main Number: [phone]
Fax Number: [phone]
From: Lori Goetz fmailto:[e-mail]
Sent: Monday, February 20, 2012 5:08 PM
To: Goodrich, David
Subject: RE: Correction to Additional Information Request for the Walter Kidde Portable Equipment Co. Injection Permit
David -
The nutrients proposed for the injection (see attached MSDS from IET) are urea, diammonium phosphate, and
monosodium phosphate, all of which are on the approved substrate list as individual compounds. IET just pre-mixes its
own "blend" before bringing it onto the site rather than bringing them in in separate bags/totes.
- Lori Goetz
From: Goodrich, David [[e-mail]]
Sent: Monday, February 20, 2012 2:27 PM
To: Lori Goetz
Subject: FW: Correction to Additional Information Request for the Walter Kidde Portable Equipment Co. Injection Permit
Ms. Goetz:
This is a correction to my recent email (below) earlier today requesting additional information on Bio IET Nutrients and
Calcium Propionate.
Although Calcium Propionate is on our list of approved injectants, I have not been able to find Bio IET Nutrients on our
list.
Please send us the information on Bio IET Nutrients.
Thank you for bringing this to our attention.
David Goodrich
Office Telphone Number: [phone]
Aquifer Protection Section Main Number: [phone]
1

R_.
MATERIAL SAFETY DATA SHEET
24-HOUR EMERGENCY ASSISTANCE:
INNOVATIVE ENVIRONMENTAL TECHNOLOGIES: 1-888-721-8283
CHEMTREC 1-800-424-9300
MANUFACTURER:
INNOVATIVE ENVIRONMENTAL TECHNOLOGIES
6130 KIT ROAD
PIPERSVILLE,PA 18947
888-721-8283
PRODUCT IDENTIFICATION:
TRADE NAME:BIO IET-3
COMPONENTS:
1. Urea
CAS Number: 57-13-6
Synonym(s): Carbamide;Carbonyldiamine;Carbanidic Acid
Chemical Family: Amide
Molecular Formula: CH4N2O
Molecular Weight: 60.07
2. Diammonomium Phosphate(DAP)
CAS Number: 7783-28-0
Synonym(s): Ammonium phosphate;Diammonium hydrogen phosphate;Dibasic
Ammonium Phosphate
Chemical Family: Salt
Molecular Formula: (NH4)2HPO4
Molecular Weight: 132.0
3. Monosodium Phosphate(MSP)
CAS Number: 7558-80-7
Synonym(s): Sodium acid phosphate; Sodium phosphate monobasic;Sodium
dihydrogen phosphate
Chemical Family: Salt
Molecular Formula: NaH2PO4
Molecular Weight: 119.98
PRODUCT HAZARD SUMMARY:
HEALTH:May be harmful if swallowed. May be irritating to the skin,eyes and respiratory tract. Heated
material may cause thermal burns.
FLAMMABILITY:Non-combustible
REACTIVITY: Stable
PRODUCT HEALTH HAZARD INFORMATION:
INGESTION:Slightly toxic. Domestic animal oral LD50 of Urea is 511 mg/kg. Acute oral LD50 of
Diammonium Phosphate is>1,000 mg/kg in male rats. May cause gastrointestinal disturbances.
Symptoms may include irritation,nausea,vomiting,diarrhea.

Ink
•
SKIN: Slightly irritating. Repeated or prolonged skin contact may cause reddening,itching,and
inflammation. Contact with heated material may cause thermal burns.
INHALATION: May cause respiratory tract irritation.
SPECIAL TOXIC EFFECTS:Asthmatics exposed to dust may have difficulty in breathing. Urea is a
naturally occurring chemical in the body. It is an end product of protein metabolism and is excreted in the
urine.
FIRST AID
INGESTION:Do not induce vomiting. Keep affected person warm and at rest. Get medical attention.
SKIN CONTACT:Wash area of contact thoroughly with soap and water. Launder clothing before reuse.
Get medical attention if irritation persists. For contact with molten product,do not remove contaminated
clothing. Flush skin immediately with large amounts of cold water. If possible,submerge area in cold
water. Pack with ice. Thermal burns require immediate attention.
EYE CONTACT:Flush immediately with large amounts of water for at least fifteen minutes. Eyelids
should be held away from eyeball to ensure thorough rinsing. Get medical attention if irritation persists.
INHALATION:Removed affected person from source of exposure. If not breathing,ensure open airway
and institute cardiopulmonary resuscitation(CPR).If breathing is difficult,administer oxygen if available.
Get medical attention.
PERSONAL PROTECTION INFORMATION:
EYE PROTECTION:Wear safety glasses or chemical goggles to prevent eye contact. Do not wear contact
lenses when working with this substance. Have eye washing facilities readily available where eye contact
can occur.
SKIN PROTECTION:Wear impervious gloves and protective clothing to prevent skin contact. Suggested
protective materials are butyl rubber.
RESPIRATORY PROTECTION:None normally needed. Use NIOSH or MSHA approved equipment
when airborne exposure limits are exceeded. NIOSH?MSHA approved breathing equipment must be
available for non-routine and emergency use.
PHYSICAL PROPERTIES:
BIOLING POINT: Decomposes
SPECIFIC GRAVITY: NA
MELTING POINT: 133-211 C(271-412 F);DAP decomposes at 155 C(311 F)
%VOLATILE: NA
VAPOR PRESSURE: NA
EVAPORATION RATE(WATER-1) NA
VAPOR DENSITY(AIR=1) NA
VISCOS!i'Y: NA
%SOLUBILITY IN WATER,GM/100 GM @ 25C Urea 119
DAP 41
MSP 71
•
OCTANOL/WATER PARTITION COEFFICIENT: ND
POUR POINT: NA
pH ND

APPEARANCE/ODOR: White granules with little or no odor. Ammonia odor will develop upon
long standing
FIRE AND EXPLOSION DATA;
FLASH POINT NA
AUTOIGNITION TEMPERATURE: NA
FLAMMABILITY LIMITS IN AIR(%BY VOLUME);LOWER: NA
FLAMMABILITY LIMITS IN AIR(%BY VOLUME);UPPER: NA
BASIC FIREFIGHTING PROCEDURES:Use extinguishing agent suitable for type of surrounding fire.
Material itself burns with great difficulty. Urea becomes slippery when wet. Guard against falls.
UNUSUAL FIRE AND EXPLOSION HAZARDS:Fire may produce poisonous or irritating gas,fumes or
vapor. Irritating or toxic substances may be emitted upon thermal decomposition. Exposed firefighters
should wear MSHA/NIOSH approved self-contained breathing apparatus with full face mask and full
protective equipment. Uncontaminated Urea,DAP and MSP are not explosion hazards. They may form
explosive mixtures subject to spontaneous dentonation when contaminated with strong acids(nitric,picric,
perchloric)or nitrate fertilizers. At elevated temperature,dry Urea may omit ammonia. Wet Urea may
hydrolyze to corrosive ammonium carbamate. Aqueous solution of Urea at elevated temperature may
decompose to highly toxic hydrogen cyanide. DAP decomposes upon heating to ammonia and
polyphosphoric acid.
REACTIVITY DATA:
STABILITY/INCOMPATIBILITY: Stable when stored dry at up to 160 F and atmospheric pressure.
Avoid contact with strong oxidizers,acids and bases,and nitrates. Decomposes to ammonia,biuret,NOR,
CON,and polyphoshoric acid.
HAZARDOUS REACTIONS/DECOMPOSITION PRODUCTS:Thermal decomposition products may be
hazardous. Urea reactions with sodium or calcium hypochlorite to form explosive nitrogen trichloride.
DAP heated with ammonium nitrate at 170 C or higher forms explosive nitroguinidine. Diammonium
phosphate wil react with alkali to liberate ammonium.
ENVIRONMENTAL INFORMATION:
SPILL OR RELEASE TO THE ENVIRONMENT:No special procedures are required for clean-up of this
material. Avoid methods that result in water pollution. Caution should be exercised regarding personnel
safety and exposure to the material as set forth elsewhere in this data sheet.
EMERGENY ACTION:Keep unnecessary people away.
WASTE DISPOSAL:This substance,when discarded or disposed of,is not specifically listed as a
hazardous waste in Federal regulation;however,it could be hazardous if it is considered toxic,corrosive,
ignitable,or reactive according to Federal definitions(40 CFR 261). Additional,it could be designated as
hazardous according to state regulations. This substance could also become a hazardous waste if it is
mixed with or comes in contact with a hazardous waste. If such contact or mixing have occurred,check 40
CFR 261 to determine whether it is a hazardous waste. If it is a hazardous waste,regulations at 40 CFR
262,263,and 264 apply.
The transportation,storage,treatment and disposal of this waste material must be conducted in compliance
with all applicable Federal,state,and local regulations.
SARA TITLE III INFORMATION:Listed here are the hazard categories for the Superfun Amendments
and Reauthorization Act(SARA)Section 311/312(40 CFR 370):

.
Immediate hazard-no-Delayed Hazard-no-Fire Hazard-no-Pressure Hazard-no Reactivity Hazard-no
REGULATORY INFORMATION:
HANDLING/STORAGE: Store in tightly closed containers in cool,dry,isolated,well ventilated area away
from heat,sources of ignition and incompatibles. Avoid contamination with other"look-alike"materials
that may produce explosion hazard(see Unusual Fire and Explosion Hazards section).
EMPTY CONTAINERS:Empty containers may contain product residue.Do not reuse without adequate
precautions.
TRANSPORTATION REOUIREMENTS:
D.O.T.Proper Shipping Name(49 CFR 172.101) NA
D.O.T.Hazard Class(49 CFR 172.101) NA
UN/NA Code(40 CFR 172.101) NA
Bill of Lading Description(49 CFR 172.202) BIO IET-3
D.O.T.Labels Required(49 CFR 172.101) NA
D.O.T.Placards Required NA
INGREDIENTS AND HEALTH HAZARD INFORMATION:
COMPONENTS CAS NUMBER % EXPOSURE LIMITS.REF
Urea 57-13-6 50 10 mg/m3(total)TLV as nuisance dust
DAP 7783-28-0 25 ND
MSP 7558-80-7 25 ND
Revision Date:April 9,2009
NA=Not Applicable
ND=No Data

{
AQUIFER PROTECTION SECTION -- �ccev D
APPLICATION REVIEW REQUEST FORM �'C.°ept,of ENS
JAN262012
Date: January 23,2012
Winston-Salem
Regional Office
To: ❑ Landon Davidson,ARO-APS ❑ David May,WaRO-
❑ Art Barnhardt,FRO-APS 0 Charlie Stehman,WiRO-APS
O Andrew Pitner,MRO-APS rJv' o X Sherri Knight,WSRO-APS
❑ Jay Zimmerman,RRO-APS
: David Goodrich,Land Application Unit
Telephone: [phone] Fax: [phone]
E-Mail: david.goodrich[7a,ncdenr,gov
A. Permit Number: WI0400231
B. Owner: United Technologies Corporation
C. Facility/Operation: Walter Kiddie Portable Equipment Company
X Proposed El Existing X Facility X Operation
D. Application:
1. Permit Type: ❑ Animal ❑ Surface Irrigation 0 Reuse ❑ H-R Infiltration
❑ Recycle ❑ I/E Lagoon X GW Remediation(ND) 5I Inj.wells
O UIC -(5A7)open loop geothermal
For Residuals: ❑ Land App. El D&M ❑ Surface Disposal
El 503 0 503 Exempt ❑ Animal
2. Project Type: X New El Major Mod. El Minor Mod. ❑ Renewal ❑ Renewal w/Mod.
E. Comments/Other Information: 0 I would like to accompany you on a site visit.
Attached, you will fmd all information submitted in support of the above-referenced application for your
review,comment,and/or action. Within 30 calendar days,please take the following actions:
X Return a Completed APSARR Form. - Please comment
❑ Attach Well Construction Data Sheet.
❑ Attach Attachment B for Certification by the LAPCU.
❑ Issue an Attachment B Certification from the RO.*
* Remember that you will be responsible for coordinating site visits and reviews, as well as additional
information requests with other RO-APS representatives in order to prepare a complete Attachment B for
certification. Refer to the RPP SOP for additional detail.
When you receive this request form,please write your name and dates in the spaces below, make a copy
of this sheet, and return it to the appropriate Central Office-Aquifer Protection Section contact person
listed above.
RO-APS Reviewer: ii---k-kra....(, r Date: i Z
FORM:APSARR 07/06 Page 1 of 1

AQUIFER PROTECTION SECTION- GROUNDWATER PROTECTION UNIT
REGIONAL STAFF REPORT
Date: 2/8/2012 Permittee(s): United Technologies Corporation
Permit No.: WI0400231
To: APS Central Office County: Alamance
Central Office Reviewer: David Goodrich Project Name: Walter Kiddie Portable Equipment,Inc.
Regional Login No:
I. GENERAL INFORMATION
1. This application is(check all that apply): ❑ SFR Waste Irrigation System ❑UIC We11(s)
®New ❑ Renewal
❑Minor Modification❑Major Modification
❑ Surface Irrigation❑Reuse ❑ Recycle❑ High Rate Infiltration❑ Evaporation/Infiltration Lagoon
❑ Land Application of Residuals ❑Attachment B included ❑ 503 regulated ❑ 503 exempt
❑ Distribution of Residuals ❑ Surface Disposal
❑ Closed-loop Groundwater Remediation ® Other Injection Wells(including in situ remediation)
Was a site visit conducted in order to prepare this report? ®Yes or❑No.
a. Date of site visit: 2/7/2012
b. Person contacted and contact information: Dave Warren, EnSafe,Inc., 843-323-1682(ce111,843-884-0029
(Office)
c. Site visit conducted by: Shuying Wang
d. Inspection Report Attached: ❑Yes or®No.
2. Is the following information entered into the BIMS record for this application correct?
❑ Yes or®No. If no,please complete the following or indicate that it is correct on the current application.
For SFR Treatment Facilities:
a. Location:
b. Driving Directions:
c. USGS Quadrangle Map name and number:
d. Latitude: Longitude: Method Used(GPS,GoogleTM,etc.);
e. Regulated Activities/Type of Wastes(e.g., subdivision, food processing,municipal wastewater):
For UIC Injection Sites:
(If multiple sites either indicate which sites the information applies to, copy and paste a new section into the
document for each site. or attach additional pages for each site)
a. Location(s):
b. Driving Directions: Take exit 153 from I40 for NC 119 toward Mebane; turn left onto NC 119N,then take
the 2nd left onto Holmes Rd.; turn right onto S 3rd St. Exd.; then immediately turn left to the gate of the
facility.
c. USGS Quadrangle Map name and number: Mebane,NC,36078-A3-TF-024
d. Latitude: 36.0774558 Longitude: 79.29552247 Method Used(GPS, GoogleTM, etc.)
APS-GPU Regional Staff Report(Sept 09) Page 1 of 6 Pages

AQUIFER PROTECTION SECTION— GROUNDWATER PROTECTION UNIT
REGIONAL STAFF REPORT
IV.. INJECTION WELL PERMIT APPLICATIONS(Complete these two sections for all systems that use injection
wells,including closed-loop groundwater remediation effluent injection wells,in situ remediation injection wells,and heat
pump injection wells.)
Description of Well(s)and Facilities—New,Renewal,and Modification
1. Type of injection system:
❑ Heating/cooling water return flow(5A7)
❑ Closed-loop heat pump system(5QM/5QW)
®In situ remediation(5I)
❑ Closed-loop groundwater remediation effluent injection(5L/"Non-Discharge")
❑ Other(Specify: )
2. Does system use same well for water source and injection? ❑ Yes ®No
3. Are there any potential pollution sources that may affect injection? ❑ Yes ®No
What is/are the pollution source(s)? . What is the distance of the injection well(s)from the pollution
source(s)? ft.
4. What is the minimum distance of proposed injection wells from the property boundary? 2,50 ft.
5. Quality of drainage at site: ® Good ❑Adequate ❑Poor
6. Flooding potential of site: ®Low ❑Moderate ❑High
7. For groundwater remediation systems, is the proposed and/or existing groundwater monitoring program
(number of wells,frequency of monitoring,monitoring parameters,etc.)adequate? ®Yes❑No. Attach
map of existing monitoring well network if applicable. If No, explain and recommend any changes to the
groundwater monitoring program:
8. Does the map presented represent the actual site(property lines,wells, surface drainage)?dYes or❑No. If
no or no map,please attach a sketch of the site. Show property boundaries,buildings,wells,potential pollution
sources,roads, approximate scale,and north arrow.
Injection Well Permit Renewal and Modification Only:
1. For heat pump systems,are there any abnormalities in heat pump or injection well operation(e.g. turbid water,
failure to assimilate injected fluid, poor heating/cooling)?
❑Yes ❑No. If yes, explain:
2. For closed-loop heat pump systems, has system lost pressure or required make-up fluid since permit issuance
or last inspection? ❑Yes ❑No. If yes,explain:
3. For renewal or modification of groundwater remediation permits(pf any type,will
continued/additional/modified injections have an adverse impact on migration of the plume or management of
the contamination incident?❑Yes ❑No. If yes,explain:
APS-GPU Regional Staff Report(Sept 09) Page 4 of 6 Pages

AQUIFER PROTECTION SECTION- GROUNDWATER PROTECTION UNIT
REGIONAL STAFF REPORT
4. Drilling Contractor: Name:
Address:
NC Certification number:
5. Complete and attach NEW Injection Facility Inspection Report,if applicable
Y. EVALUATION AND RECOMMENDATIONS
1. Provide any additional narrative regarding your review of the Application: There is a natural drain manhole
about 30 feet downslope from the injection area. Therefore caution is need with handling injection materials to
prevent injectants running off from the injection area.
2. Attach new Injection Facility Inspection Form, if applicable
3. Do you foresee any problems with issuance/renewal of this permit?❑ Yes ®No. If yes, please explain
briefly.
4. List any items that you would like APS Central Office to obtain through an additional information request.
Make sure that you provide a reason for each item:
Item Reason
•
5, List specific Permit conditions that you recommend to be removed from the permit when issued. Make sure
that you provide a reason for each condition:
Condition Reason
6. List specific special conditions or compliance schedules that you recommend to be included in the permit when
issued. Make sure that you provide a reason for each special condition:
Condition Reason
APS-GPU Regional Staff Report(Sept 09) Page 5 of 6 Pages

AQUIFER PROTECTION SECTION- GROUNDWATER PROTECTION UNIT
REGIONAL STAFF REPORT
7. Recommendation: ❑ Hold,pending receipt and review of additional information by regional office; ❑ Hold,
pending review of draft permit by regional office; ❑ Issue upon receipt of needed additional information;
Issue; ❑ Deny. If deny, please state reasons:-
8. Signature of report Preparer(s): _ 7I {4 � � f7 "
Signature of APS regional supervisor:
Date: / /!2
VI. ADDITIONAL INFORMATION AND SITE MAP(Sketch of site showing house and waste irrigation
system, spray or drip field, location of well(s), and/or other relevant information-SHOW NORTH ARROW)
APS-GPU Regional Staff Report(Sept 09) Page 6 of 6 Pages

Central Files: APS SWP
01/19/12
Permit Number WI0400231 Permit Tracking Slip
Program Category Jro)c ct
Ground Water In review New Project
Permit Type Version 1/44'0141 etYr
Injection In situ Groundwater Remediation Well (51) Individual
Pormy Permit Contact Affiliation
david.goodrich Craig Wise
EP
Coastal SW Rule 5724 Summer Trees Dr
Memphis TN 38134
Permitted Flow
Facility
Facility Name Major/Minor
Walter Kiddie Portable Equipment, Inc. Minor Winston-Salem
Location Addre5 5
1394 S Third St Extended Alamance
Mebane NC 27302 Facility Contact Affiliation
Owner
Owner Name Owner Type
United Technologies Corporation Unknown
Owner Affiliation
Richard Bennett
One Financial Plz
Dates/Events Hartford CT 06101
Scheduled
Orig Issue App Received Draft Initiated Issuance Public Notice Issue Eff
12/29/11
Regulated Activities Requested/Received Events
RO staff report received
RO staff report requested
Outfall NULL
Waterbody Name Stream Index Number Current Class Subbasln

417,4,
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins Dee Freeman
Governor Director Secretary
January 23,2012
MEMORANDUM
To: Dr. Mina Shehee
Epidemiology Section
DHHS -Division of Public Health
1912 Mail Service Center
Raleigh,NC 27699-1219
From: David Goodrich
Hydrogeologist
Subject: Health Risk Evaluation Request
Bio IET-3 Nutrients by IET and Calcium Propionate by Niacet Corporation
Please conduct a health risk evaluation of the subject product, which is intended to be injected via
wells for enhanced degradation of groundwater contaminated with JP-5 jet fuel associated with
aviation activity.
The following contact can provide additional information to aid your review of the subject product:
• IET, ph# 888-721-8283, can provide you with additional chemical information and additional
information about site specific use of Bio IET-3.
• Niacet Corporation, ph# 716-285-1474, can provide you with additional chemical information
and additional information about site specific use of Calcium Propionate.
Please contact me by telephone at 919-807-6352 or email at david. ;oodrielti- ncdenr. ov if you need
any other information to aid your review.
Attachments
AQUIFER PROTECTION SECTION
1636 Mail Service Center,Raleigh,North Carolina 27699-1636
Location:2728 Capital Boulevard,Raleigh,North Carolina 27604
One
PA('Ph [1?q.7Q�,.32')1 t.FAY 1•G10 f;(71c 251p:FAY 2:910 7ir v '7 1^,ge��7mnr Qnn�'�n 1_977.F^ . .�

Goodrich, David
From: Goodrich, David
Sent: Tuesday, February 21, 2012 10:23 AM
To: Rudo, Ken
Subject: RE: Assessment of Bio IET Nutrients and Calcium Propionate
Thanks, Ken!
Office Telphone Number: [phone]
Aquifer Protection Section Main Number: [phone]
Fax Number: [phone]
From: Rudo, Ken
Sent: Tuesday, February 21, 2012 10:17 AM
To: Goodrich, David
Subject: FW: Assessment of Bio IET Nutrients and Calcium Propionate
Mr. Goodrich After reviewing the information you have supplied to me regarding the remediation of the below site in
Mebane, NC, it does not appear that any private drinking water wells are in close proximity to the area described in your
email. Given the sampling plan that is also in the attachment and the worker safety plan that you have included, there
does not appear to be any significant human health risks associated with this remediation plan. Sincerely Kenneth
Rudo, Ph.D, Toxicologist
From: Goodrich, David
Sent: Monday, February 20, 2012 12:26 PM
To: Rudo, Ken
Subject: Assessment of Bio IET Nutrients and Calcium Propionate
Ken,
The injection site for these substances is in a rural area of Mebane, NC and is the site of an industrial facility which
manufactured and tested fire extinguishers and other types of gas containment canisters. I am attaching a written
description of the site herewith.According to the applicant,there are no wells of any sort within a quarter mile radius
(1,320 feet)of the proposed injection wells, except for the monitor wells that have been installed in association with site
assessment and remediation. Maximum contaminant levels at the site are reported as 1940 ppb of Total VOCs in the
ground water.
I will contact the applicant's consultant about obtaining information about case studies that include initial contaminant
concentrations and post-injection groundwater monitoring data where these substances have been applied.
Thank you for your help.
Regards,
David Goodrich
Office Telphone Number: [phone]
Aquifer Protection Section Main Number: [phone]
Fax Number: [phone]
1

Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties by an authorized State
official.Unauthorized disclosure of juvenile,health,legally privileged,or otherwise confidential information,including confidential information relating to an ongoing
State procurement effort,is prohibited by law.If you have received this e-mail in error,please notify the sender immediately and delete all records of this e-mail.
2

Tx:A
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water,Quality
Beverly Eaves Perdue Coleen H. Sullins Dee Freeman
Governor Director Secretary
April 27, 2009
MEMORANDUM
To: Dr. Mina Shehee
Epidemiology Section
Division of Public Health
Department of Health and Human Services
From: Thomas Slusser,715-6164;[e-mail]
Aquifer Protection Section ,v
Division of Water Quality
Department of Environment and Natural Resources
tgro t;
Subject: Health Risk Evaluation Request-
Vitamins itamins B2 and B12, Sodium Sulfite.Nutrients;Propionate,'Nitrogen Gas
Please find attached package submitted by ATC Associates of NC,who is proposing to use the product
to remediate chlorinated solvents in groundwater. We request that you conduct a health risk evaluation
for the products.
Please note that some of the materials in the attached package have already been reviewed and
approved: Yeast Extract,Zero Valent Iron,Hydrogen Release Compound, and EHC.
If you need additional information please call or email me or Genna Olson at(919) 871-0999.
Thank y
1912 Mail Service Center,Raleigh,NC 27699-1219
AQUIFER PROTECTION SECTION
1636 Mail Service Center,Raleigh,North Carolina 27699-1636
Location:2728 Capital Boulevard,Raleigh,North Carolina 27604 One
Phone:[phone] FAX 1:919-715-0588:FAX 2:919.715-60481 Customer Service:1-877-623.6748 NO Caroli a
Internet www.ncwaterauaiftv.om (��K�t�L�
Al Equal Opportunity I Affirmative Acton Employer t L ji

Yam.
(4/W
{
North Carolina Department of Health and Human Services
Division of Public Health • Epidemiology Section
Occupational and Environmental Epidemiology Branch
1912 Mail Service Center•Raleigh,North Carolina 27699-1912
Tel [phone]• Fax [phone]
Beverly Eaves Perdue,Governor Jeffrey P.Engel,M.D.
Lanier M.Cansler,Secretary State Health Director
May 12,2009
MEMORANDUM
TO: Thomas Slusser
Aquifer Protection Section
Division of Water Quality
FROM: Kenneth Rudo, Ph.D, Toxicologist
MERA/OEEB
THROUGH: Mina Shehee,Ph.D, Supervisor Y4
MERA/OEEB
SUBJECT: Health Risk Evaluation Request/Swansboro,NC Remediation Site
I have reviewed the information regarding the remediation package submitted by ATC
Associates of Raleigh. They requested a health risk assessment for using numerous materials to
remediate chlorinated solvents in groundwater at a source area in Swansboro,NC that was
previously a dry cleaning facility. After reviewing the toxicology of the numerous products to be
used in the remediation of this site it appears that the use of these products should not pose an
increased health risk as long as appropriate protective measures to avoid skin and eye contact are
used when handling these products based on information in the MSDS sheets. However, OEEB
has a concern based on a lack of information in the peer reviewed literature and the information
sent to our office for review of potential chemical interactions of these products in groundwater
drinking wells. The Iarge number of individual products combined for the remediation of the
solvents at this site may result in unknown contaminants in groundwater that have not been
addressed in the information available to us for this review. As a result, OEEB would not
recommend using these products for remediation at this site if there are drinking water wells
within 300 feet of the former dry cleaning facility. The information provided to OEEB stated
that ATC Associates believes the nearest wells are 660 feet from the site. Based on this
information, OEEB would recommend an additional site survey to make certain this is the case
and that the results of the follow-up survey are conveyed to Mr.Slusser in the Aquifer Protection
Section.
If you have any further questions regarding this matter,please feel free to contact me at
919-707-5911.
Homycaroling ritHearth _�
NC11 Working forabalthierandseferNorthCarotina
Everywhere.Everyday.Everybody.
Location: 5505 Six Forks Road,2"a Floor, Room D-1 •Raleigh,N.C. 27609 RECEIVED D I 1
Aquifer.Prot:?€:tinn Sea ion

..srArEw�, North Carolina
Department of Health and Human Services `J
• ,41�' tqr„ Division of Epidemiology
�f P.O.Box 29601 •Raleigh,North Carolina 27626-0601
'` ''rr Tel:[phone] Fax: [phone]
.4"""'"e James B:Hunt Jr.,Governor-H.David Bruton,M.D.,Secretary
J.Steven Cline,DDS,MPH,Acting Director
October 2, 1998 ��
C)
CO
MEMORANDUM .
TO: Amy Axon
Underground Injection Control Program ?' =`_
Groundwater Section
I"V
FROM: Luanne K. Williams, Pharm.D., Toxicologist
Medical Evaluation and Risk Assessment Branch
Occupational and Environmental Epidemiology Section
SUBJECT: Health Risk Evaluation Regarding the Use of Certain Products Manufactured by
Peerless Metal Powders and Abrasive in the Treatment of Groundwater at the
DuPont Kinston Plant in Lenoir County
I am writing in response to a request from Mr. Clifford Lee with DuPont for a health risk
evaluation regarding the use of certain products manufactured by Peerless Metal Powders and
Abrasive in the treatment of groundwater at the referenced site. Based upon my review of the
information submitted, I offer the following health risk evaluation:
WORKER PRECAUTIONS DURING APPLICATION
1. Some effects reported to be associated with the products proposed to be used are as
follows: eye, skin, nose, throat, and lung irritation. If the product is released into the
environment in a way that could result in a suspension of fine solid or liquid particles
(e.g., grinding,blending,vigorous shaking or mixing), then proper personal protective
equipment should be used. The application process should be reviewed by an industrial
hygienist to ensure that the most appropriate personal protective equipment is used.
2. Persons working with these products should wear goggles or a face shield, gloves, and
protective clothing. Face and body protection should be used for anticipated splashes or
sprays.
3. Eating, drinking, smoking, handling contact lenses, and applying cosmetics should not be
permitted in the application area during or immediately following application.
ap CCU.OL w,•
North Carolina:Host of the 1999 Special Olympic World Summer Games Y•• ••• ••

Amy Axon Memo
October 2, 1998
Page Two
4. Safety controls should be in place to ensure that the check valve and the pressure delivery
systems are working properly.
5. It is imperative that the Material Safety Data Sheets be followed to prevent incompatible
or adverse reactions and injuries.
OTHER PRECAUTIONS
1. Access to the area of application should be limited to the workers applying the product.
In order to minimize exposure to unprotected individuals, measures should be taken to
prevent access to the area of application.
2. According to the information submitted with the letter dated September 18, 1998, "The
only groundwater production wells within one mile of the study area are DuPont Kinston
Plant wells(used for non-contact cooling water). The nearest public water supply well is
the City of Grifton Well No.2, located 3.4 miles to the northeast. The treatment wall
will be emplaced in the surficial aquifer at the site. This aquifer is not used as either a
public or private source of water;therefore, there will be no impact to any of the
identified wells(which pump groundwater from depths greater than 200 feet). DuPont
Kinston Plant potable water supply is provided by the local municipal water district."
In order to protect public health, it is recommended to confirm the absence of nearby well
users in the area. Measures should be taken to prevent contamination of existing or future
wells that may he located near the application area.
3. According to the information submitted, Beaverdam Branch is the nearest surface water
body located approximately 1,800 feet north of the study area. It is recommended to
contact Ms. Dianne Reid with the Water Quality Section at(919)733-5083 extension 568
to determine if these products or process could impact Beaverdam Branch.
If you have any questions, contact me at(919) 715-6429.
LKW:dg
cc: Ms. Linda Blalock, Groundwater Section
Mr. Bob Cheek, Groundwater Section
Mr. Clifford Lee, DuPont Fibers
Dianne Reid,Water Quality Section

dµ
1
v.w i
North Carolina Department of Health and Human Services
Division of Public Health•Epidemiology Section
1912 Mail Service Center•Raleigh,North Carolina 27699-1912
Tel [phone]•Fax [phone]
Michael F.Easley,Governor Carmen Hooker Odom,Secretary
November 3,2004
MEMORANDUM c.'1
o �
TO: Evan Kane
_ -um
at
Underground Injection Control Program co c3
Aquifer Protection Section -0 Pim
= .-�.7
w
FROM: Luanne K. Williams,Pharm:D.,Toxicologist iu co-
Medical Evaluation and Risk Assessment Unit reP
Occupational and Environmental Epidemiology Branch
North Carolina Department of Health and Human Services
SUBJECT: Use of a Non-Biological Product EHC®by Adventus Remediation Technologies
to Enhance Biodegradation of Groundwater Contaminated with Chlorinated
Compounds at the BASF Technical Marketing Building Site in Enka,North
Carolina.
I am writing in response to a request for a health risk evaluation regarding the use
of use of a non-biological product EHC®,by Adventus Remediation Technologies,to
Enhance Biodegradation of Groundwater Contaminated with Chlorinated Compounds at
the BASF Technical Marketing Building Site in Enka,North Carolina. Based upon my
review of the information submitted, I offer the following health risk evaluation:
PRECAUTIONS DURING APPLICATION
1. Some effects or hazards reported to be associated with the chemical proposed for use are
as follows:
• Exposure can cause irritation of skin, eyes,nose,throat,and lungs(Medical
Management Micromedex TOMEs Plus System CD-ROM Database,Volume 62,
2004)
2. If the products are released into the environment in a way that could result in a
suspension of fine solid or liquid particles(e.g., grinding,blending,vigorous shaking or
mixing),then it is imperative that proper personal protective equipment be used. The
application process should be reviewed by an industrial hygienist to ensure that the most
appropriate personal protective equipment is used. s:
g Location:2728 Capital Boulevard•Parker Lincoln Building•Raleigh,N.C.27604 An Equal Opportunity Employer

•
3. Persons working with this product should at least wear goggles or a face shield,gloves,
and protective clothing. Face and body protection should be used for anticipated splashes
or sprays. Again, consult with an industrial hygienist to ensure proper protection.
4. Eating,drinking, smoking,handling contact lenses,and applying cosmetics should never
be permitted in the application area during or immediately following application. Safety
controls should be in place to ensure that the check valve and the pressure delivery
systems are working properly.
5. The Material Safety Data Sheets should be followed to prevent adverse reactions and
injuries.
6. Access to the area of application should be limited to the workers applying the product.
In order to minimize exposure to unprotected individuals,measures should be taken to
prevent access to the area of application.
7. According to the information submitted,no public or private water supplies were
identified within a 1500-foot radius. Hominy Creek is less than 30 feet to the east of the
injection areas. The nearest residence is greater than 1500 feet from the injection area,
and the nearest workplace is the Buncombe County Offices at 300 feet from the injection
area. Both of these are located upgradient from the injection area. Efforts should be
made to prevent contamination of existing or future wells and nearby surface waters that
may be located near the application area.
Please do not hesitate to call me if you have any questions at(919) 715-6429.
cc: BASF
Mr. Joe McKeon
BASF Safety and Ecology
100 Campus Driver
Mail Stop F-409A
Florham Park,NJ 07932
ENSR Consulting and Engineering,(NC),Inc
Nanjun Shetty,P.E.
7041 Old Wake Forest Road, Suite 103
Raleigh,NC 27616
Adventus Remediation Technologies
Kerry Bolanos-Shaw •
1345 Fewster Drive
Mississauga, Ontario L4W 2A5

d, sm,t. North Carol,
Ak Department of Health and Human Services
Division of Public Health
4.`M # 1912 Mail Service Centers Raleigh,North Carolina 27699-1912
•� �,• 2728 Capital Boulevard• [phone] •Courier 56-32-00
J.Steven Cline,D.D.S.,M.P.H.,Acting Director
August 7,2000
MEMORANDUM
TO: Amy Axon ' s
Groundwater Section
as
r7r
FROM: Luanne K. Williams,Pharm.D.,Toxicologist X7 n
Medical Evaluation and Risk Assessment Unit �• <''
Occupational and Environmental Epidemiology Branch
SUBJECT: -Use of Sodium Bromide as a Tracer
-Use of Yeast Extract and Butyric Acid to Enhance Biodegradation of
Groundwater Contaminated with Tetrachloroethylene at Site 88,Camp Lejeune
Marine Corps Base
I am writing in response to a request for a health risk evaluation regarding the use of
sodium bromide as a tracer,and yeast extract and butyric acid to enhance biodegradation of
groundwater contaminated with tetrachloroethylene at Site 88 Camp Lejeune Marine Corps
Base. Ms. Diane Rosse was listed as a contact for the Groundwater Section but no other contact
information was provided. Please forward this evaluation to her or the appropriate person.
Based upon my review of the information submitted,I offer the following health risk evaluation:
WORKER PRECAUTIONS DURING APPLICATION
1. Some effects reported to be associated with the products following short-term exposure
are as follows:
sodium bromide—drowsiness,irritability,dizziness,skin rashes, decreased blood
pressure,increased heart rate,difficulty breathing,nausea,vomiting,and eye irritation.
In addition,sodium bromide may also cross the placenta and may be detected in milk of
nursing mothers. Case reports suggest that prenatal exposure may cause growth
retardation,craniofacial abnormalities, and developmental delay. See enclosed reference
Meditext®-Medical Management by Micromedex TOMEs Plus System CD-ROM
Database,2000.
butyric acid—nose irritation,throat irritation,eye irritation, skin irritation and severe
bums,nausea vomiting, and difficulty breathing. See enclosed reference Meditext®-
Medical Management by Micromedex TOMEs Plus System CD-ROM Database,2000.
Because of the serious risks associated with the developing fetus and the likelihood of
developing serious burns,conservative safety precautions should be taken while using
these products. Because of the risks to the developing fetus,it is recommended that
INC P women of childbearing age not use this product for application. If the products are
released into the environment in a way that could result in a suspension of fine solid or 41t
Every Where. EveryDay.EveryBody. An Equal Opportunity/A{grmative Action Employer

Amy Axon
August 7,2000
Page Two
liquid particles(e.g., grinding,blending,vigorous shaking or mixing),then it is
imperative that proper personal protective equipment be used. The application process
should be reviewed by an industrial hygienist to ensure that the most appropriate personal
protective equipment is used.
2. Persons working with this product should at least wear goggles or a face shield,gloves,
and protective clothing. Face and body protection should be used for anticipated splashes
or sprays.Again, consult with an industrial hygienist to ensure proper protection.
3. Eating, drinking, smoking,handling contact lenses,and applying cosmetics should never
be permitted in the application area during or immediately following application.
4. Safety controls should be in place to ensure that the check valve and the pressure delivery
systems are working properly.
5. The Material Safety Data Sheets should be followed to prevent adverse reactions and
injuries.
OTHER PRECAUTIONS
1. Access to the area of application should be limited to the workers applying the product.
In order to minimize exposure to unprotected individuals,measures should be taken to
prevent access to the area of application.
2. According to the information submitted(see enclosure),there are no water supplies
within 1,000-foot radius. No documentation was provided to support this statement.
Because of the potential risks associated with the use of this product,every effort should
be made to prevent contamination of existing or future wells that may be located near the
application area.
3. According to the information submitted,these products are not expected to impact nearby
waters including Beaverdam Creek(located approximately 1,500 feet to the northeast)
which flows to Wallace Creek,and Wallace Creek flows to the New River. Because of
the proximity to these waterbodies and the potential risks associated with these products,
it is recommended that you consult with Ms.Dianne Reid with the Water Quality Section
at 919-733-5083 extension 568 to determine if these products could impact these waters.
Please do not hesitate to call me if you have any questions at(919)715-6429.
LKW:mbf
Enclosures
c: Mr. Rick Raines,Marine Corps Base
Dr. Burce Alleman,Battelle Memorial Institute
Ms.Dianne Reid,Water Quality Section,Archdale Building

Kelp and Blue Green Algae.txt
From: Rudo, Ken
Sent: Wednesday, October 20, 2010 3:34 PM
To: Slusser, Thomas
Subject: Kelp and Blue Green Algae bioremediation request
Mr.Slusser I have reviewed the above bioremediation request for a site that was
the location of
a wholesale drycleaning solvent distribution facility from the 1960s to 2001. The
site is currently
occupied by US car Tool and is adjacent to a property owned by csx. Based on the
information
supplied by you, there are private wells with the closest 400 feet from the area
where the injection
of this product will take place as well as three surface water systems with the
closest within 670
feet. After reviewing some of the health risk information available for this product
and blue green
algae toxicity data, it does not appear that this product should impact public
health at this site.
However, if this product is utilized in the manner and at the site described in the
information
packet, I would strongly recommend that a monitoring program be set up to look for
any
evidence of this product or byproducts of this process in the surface water systems
or the
private wells near the injection area as a requirement for this site specific
bioremediation. If any
evidence of these products are detected in the surface water or private wells as a
result of the
monitoring system I recommend, a reevaluation of this process may be warranted
depending on
what is identified. Please feel free to contact me at 919-707-5911 if you have any
questions.
Sincerely Kenneth Rudo, Ph.D, Toxicologist, OEEB
Email correspondence to and from this address is subject to the North Carolina
Public Records Law and may be disclosed to
third parties by an authorized State official . Unauthorized disclosure of juvenile,
health, legally privileged, or otherwise
confidential information, including confidential information relating to an ongoing
state procurement effort, is prohibited by
law. If you have received this e-mail in error, please notify the sender immediately
and delete all records of this e-mail .
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