NCS000370_2020 DMR_20210118

BRIDGESTONE AMERICAS
TIRE OPERATIONS, LLC
January 7, 2021
Wilson Plant
P.O. Box 1139
Wilson, North Carolina 27894-1139
North Carolina DEMLR
Raleigh Regional Offices
3800 Barrett Drive
Raleigh, North Carolina 27609
Re: Storm water Sampling Year 11, Period 1 Analytical Results
Dear Sir or Madam:
The BATO-Wilson facility operates under National Pollutant Discharge Elimination
System (NPDES) permit number NCS000370. The permit requires semi-annual
quantitative sampling of storm water at the facility's two outfalls. The outfalls are named
by their geographic locations, South and East. Please find the analytical results and
Storm Water Outfail Discharge Monitoring Reports for the Sampling Year 11 Period 1
for the South and East outfalls in the Attachment. The samples were collected on
December 20, 2020. The analytical results were received from the laboratory via
electronic mail at BATO Wilson on January 6, 2020. As required, the original and one
copy are enclosed.
If you have any questions concerning this report, please contact Tausha Fanslau at
[phone].
Sincerely,
Vergil Norrod
Plant Manager
BATO — Wilson Plant
cc: BATO Wilson Environmental Department
p:\My Documents\Water-Stormwater\Files20

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(�IacieAnalytical"
WWW.Pmlaba.eam
January 05, 2021
Allen Henricks
Bridgestone Americas
RE: Project: Stormwater Sampling
Pace Project No.: 92513629
Dear Allen Henricks:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on December 23, 2020. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNIINELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
VC1l-a
Amanda Payne
[e-mail]
[phone]
Project Manager
Enclosures
cc: Tausha Fanslau, Bridgestone Americas
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 15

aceAnalytical
www.pacelabs.com
Project: Stormwater Sampling
Pace Project No.: 92513629
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services Charlotte
9800 KinceyAve, Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
FloridalNELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia[VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 15

5ceAna1j&a1
WW.pacelabs.com
SAMPLE ANALYTE COUNT
Project: Stormwater Sampling
Pace Project No.: 92513629
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92513629001 South EPA 1664B
CJM
1
PASI-C
EPA 200.7 Rev 4.4 1994
KQ
1
PASI-A
SM 2540D-2011
MJP
1
PASI-A
EPA 9040C
SMK
1
PASI-A
SM 5220D-2011
JP1
1
PASI-A
92513629002 East EPA 1664E
CJM
1
PASI-C
EPA 200.7 Rev 4.4 1994
KQ
1
PASI-A
SM 254OD-2011
MJP
1
PASI-A
EPA 9040C
SMK
1
PASI-A
SM 5220D-2011
J131
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 15

aceAnalytical
www.pacelflaxem
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Stormwater Sampling
Pace Project No.: 92513629
Sample: South Lab ID: 92513629001 Collected: 12/20/20 07:55 Received: 12/23/20 10:16 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
1664 SGT-HEM, TPH
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg1L 5.0 1 12/28/20 11:33
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4A 1994
Pace Analytical Services - Asheville
zinc
66.3 ug/L 10.0 1 0110512100:54 01/0512112:22 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Pace Analytical Services -Asheville
Total Suspended Solids
18.6 mg1L 2.7 1 12/24/20 15:07
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services -Asheville
pH at 25 Degrees C.
6.4 Sid. Units 0.10 1 12/30/20 13:28 H3
5220D COD
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Pace Analytical Services -Asheville
Chemical Oxygen Demand
ND mglL 25.0 1 12/29/20 18:11 12/30/20 05:37
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/05/2021 02:53 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 15

(�15'neAnalytica(
www.pacelabs.eem
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Stormwater Sampling
Pace Project No.: 92513629
Sample: East Lab ID: 92513629002 Collected: 12/20/20 08:05 Received: 12/23/20 10:16 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 16648
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mglL 5.0 1 12/28/20 11:33
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Zinc
91.9 ug1L 10.0 1 0110512100:54 01/0512112:26 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services -Asheville
Total Suspended Solids
12.1 mglL 2.5 1 12/24/20 15:07
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services -Asheville
pH at 25 Degrees C
5.4 Std. Units 0.10 1 12/30/20 13:32 H3
5220D COD
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Pace Analytical Services - Asheville
Chemical Oxygen Demand
48.5 mglL 25.0 1 12/29/20 18:11 12/30/20 05:38
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/05/2021 02:53 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 15

laneAnalytical"
www.pacelabs.com
QUALITY CONTROL DATA
Project: Stormwater Sampling
Pace Project No.: 92513629
QC Batch: 589533 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 SGT HEM, TPH
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92513629001, 92513629002
METHOD BLANK: 3113841 Matrix: VVgter
Associated Lab Samples: 92513629001, 92513629002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Petroleum Hydrocarbons mg1L ND 5.0 12/28/20 11:33
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
3113842
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Total Petroleum Hydrocarbons
mg/L
20 16.3
82
64-132
MATRIX SPIKE SAMPLE:
3113843
92511721003 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
ND 20
5.0
24
64-132 M1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/05/2021 02:53 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 15

aceAnalytical
www.pacotab3.com
Project: Stormwater Sampling
Pace Project No.: 92513629
QC Batch: 590579
QC Batch Method: EPA 200.7 Rev 4.4 1994
Associated Lab Samples: 92513629001, 92513629002
METHOD BLANK: 3118106
Associated Lab Samples: 92513629001, 92513629002
Parameter Units
Zinc ug1L
QUALITY CONTROL DATA
Analysis Method: EPA 200.7 Rev 4A 1994
Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services -Asheville
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 10.0 01105/2108:51
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 3118107
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Zinc uglL 500 480 96 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3118108 3118109
MS MSD
92513593001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Zinc uglL 57.5 500 500 562 553 101 99 70-130 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 01/05/2021 02:53 PM without the written consent of Pace Analytical Services, LLG.
Page 7 of 15

lacieAnalydcal"
W".pacalabsxam
Project: Stormwater Sampling
Pace Project No.: 92513629
QC Batch: 589415
QC Batch Method: SM 2540D-2011
Associated Lab Samples: 92513629001, 92513629002
MFTHnD BLANK- 3113506
Associated Lab Samples: 92513629001, 92513629002
Parameter Units
Total Suspended Solids mg/L
LABORATORY CONTROL SAMPLE: 3113507
Parameter Units
Total Suspended Solids mg1L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 2544D-2011
Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services -Asheville
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 12124/2015:06
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
250 228 91 90-110
SAMPLE DUPLICATE: 3113508
92513700002 Dup
Parameter Units Result Result
Total Suspended Solids mg1L 225 189
RPD Qualifiers
17
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/05/2021 02:53 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 15

aceAnalytical
www.pacelabs.com
Project:
Stormwater Sampling
Pace Project No.:
92513629
QC Batch:
589465
QC Batch Method:
EPA 9040C
Associated Lab Samples: 92513629001, 92513629002
QUALITY CONTROL DATA
Analysis Method: EPA 9040C
Analysis Description: 9040 pH
Laboratory: Pace Analytical Services -Asheville
SAMPLE DUPLICATE: 3113630
92512065001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 6.5 6.5 0 H3
Pace Analytical Services, LLC
9800 Kincey Ave. Suite t00
Huntersville, NO 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/05/2021 02:53 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 15

lacieAnalXicale
www,pocelabs.com
Project: Stormwater Sampling
Pace Project No.: 92613629
QC Batch: 589801
QC Batch Method: SM 5220D-2011
Associated Lab Samples: 92513629001, 92513629002
METHon RI ANK: 3114779
Associated Lab Samples: 92513629001, 92513629002
Parameter Units
Chemical Oxygen Demand mg/L
QUALITY CONTROL DATA
Analysis Method: SM 5220D-2011
Analysis Description: 5220D COD
Laboratory: Pace Analytical Services - Asheville
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25.0 12/30/20 05:32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 3114780
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg1L 750 762 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3114781 3114782
MS MSD
92512387008 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg1L 496 100 100 585 582 89 86 90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3114783 3114784
MS MSD
92512392001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg1L 193 100 100 289 298 96 105 90-11 D 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 0110512021 02:53 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 15

aceAnalyfical
www.pacclabs.com
QUALIFIERS
Project: Stormwater Sampling
Pace Project No.: 92513629
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PQL - Practical Quantitation Limit,
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
Aseparate vial preserved to a pH of 4-5 is recommended in SW846 Chapter for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN - The NELAC Institute.
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
Mt Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in Full,
Date: 01/05/2021 02i53 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 15

leAnalyfical
www.pacalabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Stormwater Sampling
Pace Project No.: 92513629
Lab ID Sample ID QC Batch Method QC Batch
92513629001
South
EPA1664B
589533
92513629002
East
EPA1664B
589533
92513629001
South
EPA 200.7 Rev 4.4 1994
590579
92513629002
East
EPA 200.7 Rev 4.4 1994
590579
92513629001
South
SM 2540D-2011
589415
92613629002
East
SM 2540D-2011
589415
92513629001
South
EPA 9040C
589465
92513629002
East
EPA 9040C
589465
92513629001
South
SM 5220D-2011
589801
92513629002
East
SM 5220D-2011
589801
Date: 01/05/2021 02:53 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Analytical Method Batch
EPA 200.7 Rev 4.4 1994 590594
EPA 200.7 Rev 4.4 1994 590594
SM 5220D-2011
SM 5220D-2011
589943
589943
Page 12 of 15

CBArel imi"
Document Name:
Sample Condition Upon Recelpt(SCUR)
Document Revised: OCtobEr 28, 2020
Page 1 of z
Document No.:
F-CAR-CS-033-Rev.07
IssuingAuthority:
Pace Carolinas Quality Office
Laboratory receiving Samples:
Asheville ❑ - Eden❑ Greenwood ❑ Huntersville ❑ Ralelgh§< Mechanicsville❑ Atlanta❑ Kernersville❑
ReceiptSampleCoUpon Client [Name: Project Il: WO# : 92513629
Courier:[]Fed Ifx []UPS USP5 []client 11111111111111111111
❑ Commercial 4pace ❑other: 92513629
Custody Seal Present? ❑Yes ErNo Seals Intact? []Yes NNo
t]ate/1nftlais Person Examining Contents: Z.AWlx-7-3'2,9
Packing Material: ❑Bubble Wrap ❑Bubble Bags RNone ❑ other Biological Tissue Frozen?
Thermometer: ❑Yes [f Na ON/A
ElIRGun 10: (fp5 S[�Wet ❑Blue []None
Type of (ce:
Correction Factor: /�
Cooter Tamp: Z ' 7 Add/Subtract VC) d 0 Temp should be above freezing to VC
❑Samples out of temp criteria. Samples on Ice, cooling process
Cooler Temp Carreeted (°C): 7 has begun
USDA Regulated Soil (DEN/A, water sample)
Did samples originate In a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (intematknally,
MY.. 11Nn Inrludlrp Hawall and Puprtn Rlroi? l—lYes FINo
Comm ents/Olscrepan cy:
Chain of Custody Present?
Yes
EINo
❑N/A
1,
Samples Arrived within Hold Time?
Yes
[]Na
N/A
2.
Short Hold Time Analysis <72 hr.)?
Yes
allo
N/A
3.
Rush Turn Around Time Requested?
QYas
WNO
N/A
4.
Sufficient Volume?
Yes
QNo
[]N/A
S.
Correct Containers used?
-Pace Containers Used?
s
s
t
No
No
❑N/A
❑N/A
6.
Contalners-Intac"
Yer—
No — _ N/A--
-7... --- -- ---
-Dissolved analysis: 5amples Field Filtered?
Yes
ONO
N/A
8,
Sample Labels Klatch COC?
-includes Date/Time/ip/Analysis Matrix: W
®Yes
❑No
❑N/A
9.
Heads ace in VOA Vials >5-6mm)?
ElYes
[]NO
M N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
Yes
❑No
- ❑No
KN/A
11 /A
il.
COMMENTS/SAMPLE DISCREPANCY
ii
1°
F
l T
Field Data Required? []Yes❑Na - : I }
Lot ID ofsplit containers: I !
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Protect Manager SCURF Review:
Project Manager SRF Review:
Date/Tlme:
Gate:
Date:
- 1
Page 13 of 15

Document Name:
document Revised:October28, 2020
1 2 Anal icaI4
Sample Condltlon Upon Receipt SCUR
Pa o 2 of 2
Document No.:
issuing Authority:
F-CAR-G-033-Rev,07
Pace Carolinas qualfty Office
'Check mark top half of box If pH and/or dechlorination Is
verified and within the acceptance range for preservation
samples.
EKceptlons: VOA, Conform, TOC, oil and Grease, 0110/8015 (Water) DOC, LLHg
*"Bottom half of box is to list number of bottles
Project WO# : 92513629
PM: RP Due Date: 12/31/20
CLIENT: 92-BFUSA
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Type of preservative
pH upon receipt
Date preservation adjusted
Time preservation
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Lot 0
Note. Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this rerm vAll ee sent to the North Carolina ULHNR Certlticalion OhICG (i.e.
Out of hold, Incorrect preservative, out of temp, Incorrect containers,
Page 14 of 15

ITEM 4
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Page 15 of 15