Loading...
HomeMy WebLinkAboutWQ0000461_Monitoring - 09-2020_20201102Certified Mail — 7017 0660 00010015 3984 Return Receipt Requested October 28, 2020 Information Processing Unit NCDEQ - DWR 1617 Mail Service Center Raleigh, NC 27699-1617 Subject: Groundwater Sampling Results, September 2020 Permit No. WQ0000461 Louisiana-Pacific Corporation To Whom It May Concern, Please find attached two copies of Forms GW-59 and GW-59A and lab sample results for sampling conducted during the month of September as required by Condition III.11 of Permit No. WQ0000461. Note that we detected nitrates equal to or above the established standard in well DS 1-MW I, DS1-MW5, and DS1-MW9. We continue to not spread on the fields adjacent to these wells. If there are any questions regarding this report, please contact me at (336) 696-3448. Sincerely, Chad Witherspoon Plant EQ Manager LSS Black Belt Chad.witherspoonAlpcorp.com Office — 336 696 3448 Cell - 336 452 3036 Nov 0 2 z020 ADDRESS 1068 ABTCO Road North Wilkesboro, NC 28659 TEL 336.696.2751 FAX 336.696.3443 WEB www.lpcorp.com GW-59A COMPLIANCE REPORT FORM Permit #440060g6l (Submit one each monitoring period with GW-59 jorms.) I Enter date monitoring results were due. (I D ) Will this monitoring report (GW-59 and GW-59A) YES NO be submitted after the established due date? L 2 Was any required information missing on the G«'-59 report forms? YES NO IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? if the answer is "Yes ", contact the Regional Office for guidance. 4 Are any monitored constituents equal to or above the established standards? YES NO If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: as, l a5 I -�►nWq Pi�ra�as 13 •? mgl V X bs t-MW ► N:tra{�S "4- t61-Mw5- 19,3 "4- 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). �S �- MW � Nikrct-��S 15� n�►gl�- Q�al�� I�1 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located, contact the Regional Office. v 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties. * 1,,J cxpp,iu/�ipl'1 &&'need oo 4,e C.f'�✓� -A eJ5 Ct4Pr aou 8 The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Com GW-59A) is true and complete to the best of my knowledge. 4 Signature of Permittee (or Authorized Agent) Date (,A\ -4;9 V 1 1 8 I-_IlWi SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: �1617 DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM MAIL SERVICE CENTER, RALEIGH, INC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 10/31/20 Facility Name: Louisiana Pacific Corp. Non -Discharge WQ0000461 UIC Permit Name (if different): NPDES NC0005266 Other Facility Address: 1068 ABTCO Rd. TYPE OF PERMITTED OPERATION BEING MONITORED North Wilkesboro NC 28659 CountyWilkes El Lagoon ❑Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: Contact Person: James Boles Telephone#: 336-696-3348 ❑ Rotary Distributor ❑■ Land Application of Sludge Well Location/Site Name: DS1-MW1 No. of wells to be sampled: ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW1 Date sample collected: 9/28/2020 FIELD ANALYSES: WAS Well Depth: 19' ft. Well Diameter: 4 in. pH 00400: 4.81 units Temp. 000lo: 22.7 °C DRY at Depth to Water Level 82546: 9'8" ft. below measuring point Screened Interval: 9 ft. to 19 ft. Spec. Cond. 00094: 564 µMhos — time of sampling, Measuring Point is 4 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 12 gallons Appearance Clear here: ❑ Samples for metals were collected unfiltered: Z YES ❑ NO and field acidified: ® YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 9/30/20,10/2/20,10/6/20,10/7/2020 Laboratory Name: Meritech Inc. Certification No. 165 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 25.1 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note. Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 193 mg/L Al -Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 1.0 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑■ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # Total Ammonia 00610 <0.1 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3as N, Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Scott Cranston, Plant Manager Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.2/2010 t Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: James Boles Report Date: 10/9/2020 Client: Louisiana-Pacific Corp. NPDES#: NC0005266 1068 ABTCO Rd Land App. Permit#: WQ0000461 North Wilkesboro, NC 28659 Date Sample Rcvd: 9/29/2020 Meritech Work Order # 09292044 Sample: DS1-MW1 Grab 9/28/20 Parameters Result Analysis Date Reporting Limit Method Total Dissolved Solids 193 mg/L 9/30/20 10 mg/L SM 2540C Chloride 1.0 mg/L 10/6/20 0.5 mg/L SM 4500 Cl B Ammonia, Nitrogen <0.1 mg/L 10/7/20 0.1 mg/L EPA 350.1 Nitrate, Nitrogen 25.1 mg/L 10/2/20 0.10 mg/L EPA 353.2 TKN <0.20 mg/L 10/6/20 0.20 mg/L EPA 351.1 Nitrate/Nitrite, Nitrogen 25.1 mg/L 10/2/20 0.10 mg/L EPA 353.2 Nitrogen, total 25.1 mg/L 10/6/20 0.20 mg/L EPA 353.2 8260 Attached 9/30/20 - - EPA 8260 I hereby certify that 1 have reviewed and approve these data. Y- 0- 111 hx, Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Client: Project: Client Sample ID: Sample Collection: Acetone Acrylonitrile Benzene Bromodichloromethane Bromochloromethane Bromoform Bromomethane 2-Butanone (Iv1EK) n-Butylbenzene sec-Butylbenzene Carbon disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,4-Dichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1, 1 -Dichloroethene cis- 1,2-D i chloroethene trans-1,2-Dichloroethene trans-1,4-Dichloro-2-butene 1,2-Dichloropropane 1,3-Dichloropropane 1,1-Dichloropropene 1,2-Dichloropropene MERITECH, INC. Environmental Laboratories A Division of Water Technology and Controls, Inc. Louisiana Pacific Corp. Meritech ID#: 09292044 WQ0000461 DSI-MW-1 09/28/20 < 5.00 ug/L < 5.00 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 5.00 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L Analysis: 09/30/20 Analyst: VW Dilution Factor: 1 Report Date: cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethanol Ethyl benzene Hexachlorobutadiene 2-Hexanone Isopropylbenzene p-Isopropyltoluene Methylene chloride Methly Isobutyl Ketone (MIBK) Methyl iodide Naphthalene n-Propylbenzene Styrene 1, 1, 1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethee (PCE) Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene (TCE) 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,2,3-Trichloropropane Trichlorofluoromethane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride m/p-Xylenes o-Xylene Additional Compounds Methyl-tert-butyl ether (MTBE) Isopropyl ether (IPE) I hereby certify that I have reviewed and approve these data. 10/08/20 < 0.500 ug/L < 0.500 ug/L < 50.0 ug/L < 0.500 ug/L < 0.500 ug/L < 1.00 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 1.00 ug/L < 0.005 ug/L < 1.00 ug/L < 0.500 ug/L < 0.500 ug/L P0 ug/L Lab tory Re tative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax MERITECH, INC. Environmental Laboratories A Division of Water Technology and Controls, Inc. Client: Louisiana Pacific Corp. Meritech ID#: 09292044 Project: WQ0000461 Analysis: 09/30/20 Client Sample ID: DSI-MW-1 Analyst: VWV Sample Collection: 09/28/20 Dilution Factor: 1 Sample Volume: 5m1 purge Report Date: 10/08/19 % solid N/A Batch Blank = Below Reporting Limit (Yes ) / No Internal Standards method criteria acceptable es / No Surrogate Recoveries Spike Conc Spike Recovery Limits Dibromofluoromethane 30 ug/L 115% 51-141% Toluene-d8 30 ug/L 94% 67-151% Bromofluorobenzene 30 ug/L 86% 45-161% Laboratory QC Check Matrix Spike Recoveries Acceptable Spike Compound Spike Cone Spike %Rec. 1,1-Dichloroethene 25 ug/L 52% Benzene 25 ug/L 112% Trichloroethene 25 ug/L 91% Toluene 25 ug/L, 74% Chlorobenzene 25 ug/L 79% # - Fails Limit Check * - If "no" is selected, see third page for details. (Yes) / No Duplicate % Rec. RPD RPD Limits OC Limits 52% 1 20 40-133 112% 1 20 40-168 91% 0 20 42-143 75% 2 20 58-154 82% 3 20 48-136 I hereby certify that I have reviewed and approve these data. Labora ry Reprpsedative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax 5.9-2016 Chain of Custody Record (COC) NPDES#: NC0005266 Client: Louisiana Pacific Corp. Phone:_ 336-696-3348 Address:_ 1068 ABTCO Rd. Fax: North Wilkesboro, NC 28659 Email:_ iames.boles@Ipcorp.com Project:_ WQ0000461 P.O.#: Atteni James Boles Turn Around Time* How would you like your report sent? *RUSH work needs prior approval. Stcl 10days) 3-5 Da s 24-48Hrs Emai Circle all that apply: preferred) , Fax M E RITECH INC. 1 ENVIRONMENTAL LABORATORIES 642 Tamco Rd. Phone: 336-342-4748 M Reidsville NC 27320 Fax: 336-342-1522 Email: info@meritechlabs.com www.meritechiabs.com Sample Location and/or ID # Sampling Dates & Times Person ing Samp (Sign/Print): Lab Use Only Start End comp? Grab? # of Cont. Test (s) Required on Ice? Y s / No pH OK? Cl OK? Date Time Date Time DS1-MW-1 9/28/20 11:45 9/28/20 11:45 G 2 Chloride, TDS G 2 NH3, Ntot, NO3 G 3 8260(w/HCI) Temperature Upon ' J� K' Receipt: �},JJ t Method of Shipment: *** Dechlorination <0.5 m) of Ammonia, Cyanide, Phenol and TKN sam les must be done in the field prior to reservation. *** Comments: Compositor # ❑ UPS Jug # ❑ Fed Ex Are these results for regulatory purposes? Yes ❑ No ❑ Report results in: mg/L ❑ mg/kg ❑ ug/L ❑ ❑ Hand Delivery Relinquished D te: Time: _ Received y O Time: ZZii ❑ Other J Time: Received by: Da e: Time: 11461i6quished y: Date: Time: Recei y lab `�_qD%, Time: SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733.3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 10/31/20 Facility Name: Louisiana Pacific Corp. Non -Discharge W00000461 UIC Permit Name (if different): NPDES NC0005266 Other Facility Address: 1068 ABTCO Rd. TYPE OF PERMITTED OPERATION BEING MONITORED North Wilkesboro "``'' NC 28659 County Wilkes ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: Contact Person: James Boles Telephone#: 336-696-3348 ❑ Rotary Distributor ❑■ Land Application of Sludge Well Location/Site Name: DS1-MW3 No. of wells to be sampled: ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW3 Date sample collected: 9/29/20 FIELD ANALYSES: WAS Well Depth: 89' ft. Well Diameter: 4 in. pH 00400: 5.38 units Temp. 000lo: 18.0 °C DRY at Depth to Water Level 82546: 53'3" ft. below measuring point Screened Interval: 79 ft. to 89 ft. Spec. Cond. 00094: 112.5 µMhos time of sampling, Measuring Point is 0.5 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 22 gallons Appearance Clear here: ❑ Samples for metals were collected unfiltered: 0 YES ❑ NO and field acidified: ® YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 9/30/20,10/6/20,10/7/20 Laboratory Name: Meritech Inc. Certification No. 165 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 1.82 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note. Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 703oo 39 mg/L Al -Aluminum ol1o5 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 0.5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑■ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732 method # Total Ammonia 00610 <0.1 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3asN, Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Scott Cranston, Plant Manager Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.212010 jk Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: James Boles Client: Louisiana-Pacific Corp. 1068 ABTCO Rd North Wilkesboro, NC 28659 Meritech Work Order # 09292045 Sample: DS1-MW3 Grab Parameters Result nalysis Date Report Date: 10/9/2020 NPDES#: NC0005266 Land App. Permit#: WQ0000461 Date Sample Rcvd: 9/29/2020 9/28-29/20 Reg Limit Method Total Dissolved Solids 39 mg/L 9/30/20 10 mg/L SM 2540C Chloride 0.5 mg/L 10/6/20 0.5 mg/L SM 4500 Cl B Ammonia, Nitrogen <0.1 mg/L 10/7/20 0.1 mg/L EPA 350.1 Nitrate, Nitrogen 1.82 mg/L 9/30/20 0.10 mg/L EPA 353.2 TKN <0.20 mg/L 10/6/20 0.20 mg/L EPA 351.1 Nitrate/Nitrite, Nitrogen 1.82 mg/L 9/30/20 0.10 mg/L EPA 353.2 Nitrogen, total 1.82 mg/L 10/6/20 0.20 mg/L EPA 353.2 8260 Attached 9/30/20 - - EPA 8260 1 hereby certify that 1 have reviewed and approve these data. Anlfza L) a Q'-x k' Laboratory epresentative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 MERITECH, INC. Environmental Laboratories A Division of Water Technology and Controls, Inc. Client: Louisiana Pacific Corp. Meritech ID#: 09292045 Project: WQ0000461 Analysis: 09/30/20 Client Sample ID: DSI-MW-3 Analyst: VWV Sample Collection: 09/29/20 Dilution Factor: 1 Report Date: 10/08/20 Acetone < 5.00 ug/L cis-1,3-Dichloropropene < 0.500 ug/L Acrylonitrile < 5.00 ug/L trans-1,3-Dichloropropene < 0.500 ug/L Benzene < 0.500 ug/L Ethanol < 50.0 ug/L Bromodichloromethane < 0.500 ug/L Ethyl benzene < 0.500 ug/L Bromochloromethane < 0.500 ug/L Hexachlorobutadiene < 0.500 ug/L Bromoform < 0.500 ug/L 2-Hexanone < 1.00 ug/L Bromomethane < 0.500 ug/L Isopropylbenzene < 0.500 ug/L 2-Butanone (MEK) < 5.00 ug/L p4sopropyltoluene < 0.500 ug/L n-Butylbenzene < 0.500 ug/L Methylene chloride < 0.500 ug/L sec-Butylbenzene < 0.500 ug/L Methly Isobutyl Ketone (MIBK) < 0.500 ug/L Carbon disulfide < 0.500 ug/L Methyl iodide < 0.500 ug/L Carbon Tetrachloride < 0.500 ug/L Naphthalene < 0.500 ug/L Chlorobenzene < 0.500 ug/L n-Propylbenzene < 0.500 ug/L Chloroethane < 0.500 ug/L Styrene < 0.500 ug/L Chloroform <0.500 ug/L 1, 1, 1,2-Tetrachloroethane <0.500 ug/L Chloromethane < 0.500 ug/L 1,1,2,2-Tetrachloroethane < 0.500 ug/L 2-Chlorotoluene < 0.500 ug/L Tetrachloroethene (PCE) < 0.500 ug/L 4-Chlorotoluene < 0.500 ug/L Toluene < 0.500 ug/L Dibromochloromethane < 0.500 ug/L 1, 1, 1 -Trichloroethane < 0.500 ug/L 1,2-Dibromo-3-chloropropane < 0.500 ug/L 1,1,2-Trichloroethane < 0.500 ug/L 1,2-Dibromoethane (EDB) < 0.500 ug/L Trichloroethene (TCE) < 0.500 ug/L Dibromomethane < 0.500 ug/L 1,2,3-Trichlorobenzene < 0.500 ug/L Dichlorodifluoromethane < 0.500 ug/L 1,2,4-Trichlorobenzene < 0.500 ug/L 1,1-Dichloroethane <0.500 ug/L 1,2,3-Trichloropropane <0.500 ug/L 1,2-Dichloroethane < 0.500 ug/L Trichlorofluoromethane < 0.500 ug/L 1,4-Dichlorobenzene < 0.500 ug/L 1,2,4-Trimethylbenzene < 0.500 ug/L 1,2-Dichlorobenzene < 0.500 ug/L 1,3,5-Trimethylbenzene < 0.500 ug/L 1,3-Dichlorobenzene < 0.500 ug/L Vinyl acetate < 1.00 ug/L 1, 1 -Dichloroethene < 0.500 ug/L Vinyl chloride < 0.005 ug/L cis-1,2-Dichloroethene < 0.500 ug/L m/p-Xylenes < 1.00 ug/L trans-1,2-Dichloroethene < 0.500 ug/L o-Xylene < 0.500 ug/L trans-1,4-Dichloro-2-butene < 0.500 ug/L 1,2-Dichloropropane < 0.500 ug/L Additional Compounds 1,3-Dichloropropane < 0.500 ug/L Methyl-tert-butyl ether (MTBE) ug/L 1,1-Dichloropropene < 0.500 ug/L Isopropyl ether (IPE) n<O.ug/L 1,2-Dichloropropene < 0.500 ug/L I hereby certify that I have reviewed and approve these data. ve 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax MERITECH, INC. Environmental Laboratories A Division of Water Technology and Controls, Inc. Client: Louisiana Pacific Corp. Project: WQ0000461 Client Sample 11): DSI-MW-3 Sample Collection: 09/29/20 Sample Volume: 5m1 purge % solid N/A Batch Blank = Below Reporting Limit Internal Standards method criteria acceptable (Yes ) / No es / No Meritech ID#: 09292045 Analysis: 09/30/20 Analyst: VWV Dilution Factor: 1 Report Date: 10/08/19 Surrogate Recoveries Spike Conc Spike Recovery Limits Dibromofluoromethane 30 ug/L 119% 51-141% Toluene-d8 30 ug/L 95% 67-151% Bromofluorobenzene 30 ug/L 90% 45-161% Laboratory QC Check Matrix Spike Recoveries Acceptable Spike Compound Spike Conc Spike %Rec. 1, 1 -Dichloroethene 25 ug/L 52% Benzene 25 ug/L 112% Trichloroethene 25 ug/L 91% Toluene 25 ug/L 74% Chlorobenzene 25 ug/L 79% # - Fails Limit Check * - If "no" is selected, see third page for details. es / No Duplicate % Rec. RPD RPD Limits OC Limits 52% 1 20 40-133 112% 1 20 40-168 91% 0 20 42-143 75% 2 20 58-154 82% 3 20 48-136 I hereby certify that I have reviewed and approve these data. 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax 5-57016 Chain of Custody Record (COC) NPDES#:_ NC0005266 Client: Louisiana Pacific Corp. Phone:_ 336-696-3348 Address:_ 1068 ABTCO Rd. Fax: North Wilkesboro, NC 28659 Email:_ iames.boles@Ipcorp.com Project:_ WQ0000461 P.O.#: Attent James Boles Turn Around Time* How would you like your report sent? *RUSH work needs prior approval. Circle all that apply(:mai referred), Fax, ED Std loch s) 3-5 Days SOS M E R I T E C H INC, / \ ENVIRONMENTAL LABORATORIES 642 Tamco Rd. Phone: 336-342-4748 N Reidsville NC 27320 Fax: 336-342-1522 Email: info@meritechlabs.com www.meritechlabs.com Sample Location and/or ID # Sampling Dates &Times Person mple (Sig rint): Lab Use Only Start End comp? Grab? ft of Cont. Test (s) Required n Ice? 4s, / No pH OK? Cl OK? Date Time Date Time DS1-MW-3 9/28/20 9:45 9/29/20 8:30 G 2 Chloride, TDS S^ G 2 NH3, Ntot, NO3 G 3 8260(w/HCI) Temperature Upon Receipt: �(" Method of Shipment: *** Dechlorination <0.5 m of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to reservation. *** Comments: Compositor # ❑ UPS Jug # ❑ Fed Ex Are these results for regulatory purposes? Yes ❑ No ❑ Report results in: mg/L ❑ mg/kg ❑ ug/L ❑ Hand Delivery Relinquished by Date: _ Time: Received te: Time: /a A aC� ❑ Other �y , Time: Received by: Date: Time: Re in fished by: Date:%G/ Time: Recei d by La • ] )�-2&ate: Time: /Y� SUBMIT FORM ON YELLOW PAPER ONLY �. DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 10/31/20 Facility Name: Louisiana Pacific Corp. Non -Discharge W00000461 UIC Permit Name (if different): NPDES NC0005266 Other Facility Address: 1068 ABTCO Rd. TYPE OF PERMITTED OPERATION BEING MONITORED North Wilkesboro NC 28659 County Wilkes ❑ Lagoon ❑ Remediation: Infiltration Gallery °r' """' "' ❑ Spray Field ❑ Remediation: Contact Person: James Boles Telephone#: 336-696-3348 ❑ Rotary Distributor Land Application of Sludge Well Location/Site Name: DS1-MW4 No. of wells to be sampled: ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW4 Date sample collected: 9/28/2020 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 4 in. pH 00400: 5.26 units Temp. 000lo: 19.4 °C DRY at Depth to Water Level 82546: 9'6" ft. below measuring point Screened Interval: 6 ft. to 16 ft. Spec. Cond. 00094: 512 µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 15 gallons Appearance Clear here: ❑ Samples for metals were collected unfiltered: 91 YES ❑ NO and field acidified: ® YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 9/30/20,10/6/20,10/7/2020 Laboratory Name: Meritech Inc. Certification No. 165 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 6.09 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note. Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 154 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 mg/L Ca - Calcium oo91s mg/L Chloride 00940 1.5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑■ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # Total Ammonia 00610 <0.1 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3as N, Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.2/2010 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Contact: James Boles Report Date: 10/9/2020 Client: Louisiana-Pacific Corp. NPDES#: NC0005266 1068 ABTCO Rd Land App. Permit#: WQ0000461 North Wilkesboro, NC 28659 Date Sample Rcvd: 9/29/2020 Meritech Work Order # 09292046 Sample: DS1-MW4 Grab 9/28/20 Parameters Result Analysis Date Reporting Limit Method Total Dissolved Solids 154 mg/L 9/30/20 10 mg/L SM 2540C Chloride 1.5 mg/L 10/6/20 0.5 mg/L SM 4500 Cl B Ammonia, Nitrogen <0.1 mg/L 10/7/20 0.1 mg/L EPA 350.1 Nitrate, Nitrogen 6.09 mg/L 9/30/20 0.10 mg/L EPA 353.2 TKN <0.20 mg/L 10/6/20 0.20 mg/L EPA 351.1 Nitrate/Nitrite, Nitrogen 6.09 mg/L 9/30/20 0.10 mg/L EPA 353.2 Nitrogen, total 6.09 mg/L 10/6/20 0.20 mg/L EPA 353.2 8260 Attached 9/30/20 - - EPA 8260 I hereby certify that I have reviewed and approve these data. J dl t Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 MERITECH, INC. Environmental Laboratories - A Division of Water Technology and Controls, Inc. Client: Louisiana Pacific Corp. Meritech ID#: 09292046 Project: WQ0000461 Analysis: 09/30/20 Client Sample ID: DSI-MW-4 Analyst: VW Sample Collection: 09/28/20 Dilution Factor: 1 Report Date: 10/08/20 Acetone < 5.00 ug/L cis-1,3-Dichloropropene < 0.500 ug/L Acrylonitrile < 5.00 ug/L trans-1,3-Dichloropropene < 0.500 ug/L Benzene < 0.500 ug/L Ethanol < 50.0 ug/L Bromodichloromethane < 0.500 ug/L Ethyl benzene < 0.500 ug/L Bromochloromethane < 0.500 ug/L Hexachlorobutadiene < 0.500 ug/L Bromoform < 0.500 ug/L 2-Hexanone < 1.00 ug/L Bromomethane < 0.500 ug/L Isopropylbenzene < 0.500 ug/L 2-Butanone (MEK) < 5.00 ug/L p4sopropyltoluene < 0.500 ug/L n-Butylbenzene < 0.500 ug/L Methylene chloride < 0.500 ug/L sec-Butylbenzene < 0.500 ug/L Methly Isobutyl Ketone (MIBK) < 0.500 ug/L Carbon disulfide < 0.500 ug/L Methyl iodide < 0.500 ug/L Carbon Tetrachloride < 0.500 ug/L Naphthalene < 0.500 ug/L Chlorobenzene < 0.500 ug/L n-Propylbenzene < 0.500 ug/L Chloroethane < 0.500 ug/L Styrene < 0.500 ug/L Chloroform < 0.500 ug/L 1, 1, 1,2-Tetrachloroethane < 0.500 ug/L Chloromethane < 0.500 ug/L 1,1,2,2-Tetrachloroethane < 0.500 ug/L 2-Chlorotoluene < 0.500 ug/L Tetrachloroethene (PCE) < 0.500 ug/L 4-Chlorotoluene < 0.500 ug/L Toluene < 0.500 ug/L Dibromochloromethane < 0.500 ug/L 1, 1, 1 -Trichloroethane < 0.500 ug/L 1,2-Dibromo-3-chloropropane <0.500 ug/L 1,1,2-Trichloroethane <0.500 ug/L 1,2-Dibromoethane (EDB) < 0.500 ug/L Trichloroethene (TCE) < 0.500 ug/L Dibromomethane < 0.500 ug/L 1,2,3-Trichlorobenzene < 0.500 ug/L Dichlorodifluoromethane < 0.500 ug/L 1,2,4-Trichlorobenzene < 0.500 ug/L 1, 1 -Dichloroethane < 0.500 ug/L 1,2,3-Trichloropropane < 0.500 ug/L 1,2-Dichloroethane < 0.500 ug/L Trichlorofluoromethane < 0.500 ug/L 1,4-Dichlorobenzene <0.500 ug/L 1,2,4-Trimethylbenzene <0.500 ug/L 1,2-Dichlorobenzene < 0.500 ug/L 1,3,5-Trimethylbenzene < 0.500 ug/L 1,3-Dichlorobenzene < 0.500 ug/L Vinyl acetate < 1.00 ug/L l,l-Dichloroethene <0.500 ug/L Vinyl chloride <0.005 ug/L cis-1,2-Dichloroethene <0.500 ug/L. m/p-Xylenes < 1.00 ug/L trans-1,2-Dichloroethene < 0.500 ug/L o-Xylene < 0.500 ug/L trans-1,4-Dichloro-2-butene < 0.500 ug/L 1,2-Dichloropropane < 0.500 ug/L Additional Compounds I,')-Dichloropropane < 0.500 ug/L Methyl-tert-butyl ether (MTBE) < 0.500 ug/L 1,1-Dichloropropene < 0.500 ug/L Isopropyl ether (IPE) .500 ug/L 1,2-Dichloropropene <0.500 ug/L I hereby certify that I have reviewed and approve these data. Tabckatory ntative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax MERITECH, INC. Environmental Laboratories A Division of Water Technology and Controls, Inc. Client: Louisiana Pacific Corp. Project: WQ0000461 Client Sample ID: DSI-MW-4 Sample Collection: 09/28/20 Sample Volume: 5m1 purge % solid N/A Batch Blank = Below Reporting Limit Internal Standards method criteria acceptable (Yes ) / No Yes / No Meritech ID#: 09292046 Analysis: 09/30/20 Analyst: VWV Dilution Factor: 1 Report Date: 10/08/19 Surrogate Recoveries Spike Cone Spike Recovery Limits Dibromofluoromethane 30 ug/L 119% 51-141% Toluene-d8 30 ug/L 95% 67-151% Bromofluorobenzene 30 ug/L 90% 45-161% Laboratory QC Check Matrix Spike Recoveries Acceptable Spike Compound Spike Cone Spike %Rec. 1,1-Dichloroethene 25 ug/L 52% Benzene 25 ug/L 112% Trichloroethene 25 ug/L 91% Toluene 25 ug/L 74% Chlorobenzene 25 ug/L 79% # - Fails Limit Check * - If "no" is selected, see third page for details. (Yes) / No Duplicate % Rec. RPD RPD Limits OC Limits 52% 1 20 40-133 112% 1 20 40-168 91% 0 20 42-143 75% 2 20 58-154 82% 3 20 48-136 I hereby certify that I have reviewed and approve these data. Labo tory R-epresehtative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax 5-9.2016 Chain of Custody Record (COC) NPDES#:_ NC0005266 Client: Louisiana Pacific Corp. Phone:_ 336-696-3348 Address:_ 1068 ABTCO Rd. Fax: North Wilkesboro, NC 28659 Email:_ iames.boles@lpcorp.com Project:_ WQ0000461 P.O.#: Attenl James Boles Turn Around Time* How would you like your report sent? *RUSH work needs prior approval. referred), Fax Std 10da s) 3_ S_Days z�s Circle all that apply O M E R I T E C H INC. J ENVIRONMENTAL LABORATORIES 642 Tamco Rd. Phone: 336-342-4748 W Reidsville NC 27320 Fax: 336-342-1522 Email: info@meritechlabs.com www.meritechiabs.com Sample Location and/or ID # Sampling Dates & Times PersonTakin mple (Si Print): Lab Use Only Start End Comp? Grab? #of Cont. Tests) Required On Ice? s / No pH OK? CI OK? Date Time Date Time DS1-MW-4 9/28/20 11:50 9/28/20 12:30 G 2 Chloride, TDS L4 �{ G 2 NH3, Ntot, NO3 IG 3 8260(w/HCI) Temperature Upon Receipt: Cs Method of Shipment: *** Dechlorination <0.5 m of Ammonia, Cyanide, Phenol and TKN samples must be done In the field prior to preservation. *** Comments: Compositor # ❑ UPS Jug # ❑ Fed Ex Are th,c4e results fo regulatory purposes? Yes ❑ No ❑ Report results in: mg/L ❑ mg/kg ❑ ug/L ❑ E] Hand Delivery Relinquished by: - Da e: Ti — Received A Timy� ❑ Other. ' Time: Received Date: Time: Re Inquished by: Date: Time: Received by L b: Time: yt� SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Pnnt Clearly or Type PERMIT Number: Expiration Date: 10/31/2020 Facility Name: Louisiana Pacific Corp. Non -Discharge W00000461 UIC Permit Name (if different): NPDES NC0005266 Other Facility Address: 1068 ABTCO Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery North Wilkesboro ' NC 28659 County Wilkes ❑ Spray Field ❑ Remediation: Contact Person: James Boles Telephone#: 336-696-3348 ❑ Rotary Distributor ❑■ Land Application of Sludge Well Location/Site Name: DS1-MW5 No. of wells to be sampled: ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW5 Date sample collected: 9/28/2020 FIELD ANALYSES: WAS Well Depth: 17-17" ft. Well Diameter: 4 in. pH 00400: 5.26 units Temp. 000lo: 21.3 °C DRY at Depth to Water Level 82546: 8'9" ft. below measuring point Screened Interval: 7.5 ft. to 17.5 — ft. Spec. Cond. 00094: 443 µMhos time of sampling, Measuring Point is 1.5 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 12 gallons Appearance Clear here: ❑ Samples for metals were collected unfiltered: W3 YES ❑ NO and field acidified: ® YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 9/30/2020,10/2/2020,10/6/2020,10/7/2020 Laboratory Name: Meritech Inc. Certification No. 165 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 19.3 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 136 mg/L Al -Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 0.5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑■ Yes (1) ❑ No (0) Specific Conductance 00095 pMhos K - Potassium 00937 mg/L VOC 78732 method # Total Ammonia 00610 <0.1 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3asN, Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Scott Cranston, Plant Manager Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.2/2010 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: James Boles Client: Louisiana-Pacific Corp. 1068 ABTCO Rd North Wilkesboro, NC 28659 Meritech Work Order # 09292047 Sample: DS1-MW5 Grab Parameters Result Analysis Date Report Date: 10/9/2020 NPDES#: NC0005266 Land App. Permit#: WQ0000461 Date Sample Rcvd: 9/29/2020 9/28/20 Reporting Limi Method Total Dissolved Solids 136 mg/L 9/30/20 10 mg/L SM 2540C Chloride 0.5 mg/L 10/6/20 0.5 mg/L SM 4500 Cl B Ammonia, Nitrogen <0.1 mg/L 10/7/20 0.1 mg/L EPA 350.1 Nitrate, Nitrogen 19.3 mg/L 10/2/20 0.10 mg/L EPA 353.2 TKN <0.20 mg/L 10/6/20 0.20 mg/L EPA 351.1 Nitrate/Nitrite, Nitrogen 19.3 mg/L 10/2/20 0.10 mg/L EPA 353.2 Nitrogen, total 19.3 mg/L 10/6/20 0.20 mg/L EPA 353.2 8260 Attached 9/30/20 - - EPA 8260 1 hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Client: Project: Client Sample ID: Sample Collection: Acetone Acrylonitrile Benzene Bromodichloromethane Bromochloromethane Bromoform Bromomethane 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene Carbon disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Di bromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane Dichlorodifluoromethane 1, 1 -Dichloroethane 1,2-Dichloroethane 1,4-Dichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene l , l -Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene trans-1,4-Dichloro-2-butene 1,2-Dichloropropane 1,3-Dichloropropane 1,1-Dichloropropene 1,2-Dichloropropene MERITECH, INC. Environmental Laboratories A Division of Water Technology and Controls, Inc. Louisiana Pacific Corp. Meritech ID#: 09292047 WQ0000461 DSI-MW-5 09/28/20 < 5.00 ug/L < 5.00 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 5.00 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L Analysis: 09/30/20 Analyst: VWV Dilution Factor: 1 Report Date: cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethanol Ethyl benzene Hexachlorobutadiene 2-Hexanone Isopropylbenzene p4sopropyltoluene Methylene chloride Methly Isobutyl Ketone (MIBK) Methyl iodide Naphthalene n-Propylbenzene Styrene 1, 1, 1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene (PCE) Toluene 1, I,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene (TCE) 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,2,3-Trichloropropane Trichlorofluoromethane 1,2,4-Trimethyl benzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride m/p-Xylenes o-Xylene Additional Compounds Methyl-tert-butyl ether (MTBE) Isopropyl ether (IPE) I hereby certify that I have reviewed and approve these data. 10/08/20 < 0.500 ug/L < 0.500 ug/L < 50.0 ug/L < 0.500 ug/L < 0.500 ug/L < 1.00 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 0.500 ug/L < 1.00 ug/L < 0.005 ug/L < 1.00 ug/L < 0.500 ug/L < 0.500 ug/L 0.500 ug/L Laboratory tative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax MERITECH, INC. Environmental Laboratories A Division of Water Technology and Controls, Inc. Client: Louisiana Pacific Corp. Meritech ID#: 09292047 Project: WQ0000461 Analysis: 09/30/20 Client Sample ID: DSI-MW-S Analyst: VWV Sample Collection: 09/28/20 Dilution Factor: 1 Sample Volume: 5ml purge Report Date: 10/08/19 % solid N/A Batch Blank = Below Reporting Limit (Yes) / No Internal Standards method criteria acceptable (Yes) / No Surrogate Recoveries Spike Conc Spike Recovery Limits Dibromofluoromethane 30 ug/L 121% 51-141% Toluene-d8 30 ug/L 96% 67-151% Bromofluorobenzene 30 ug/L. 91% 45-161% Laboratory QC Check Matrix Spike Recoveries Acceptable Spike Compound Spike Cone Spike %Rec 1,1-Dichloroethene 25 ug/L 52% Benzene 25 ug/L 112% Trichloroethene 25 ug/L 91% Toluene 25 ug/L 74% Chlorobenzene 25 ug/L 79% # - Fails Limit Check * - if "no" is selected, see third page for details. es / No Duplicate % Rec. RPD RPD Limits OC Limits 52% 1 20 40-133 112% 1 20 40-168 91% 0 20 42-143 75% 2 20 58-154 82% 3 20 48-136 I hereby certify that I have reviewed and approve these data. F�-- Labo4ory R esent tive 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax 5.-i.p1fi Chain of Custody Record (COC) NPDES#:_ NC0005266 Client: Louisiana Pacific Corp. Phone:_ 336-696-3348 1068 ABTCO Rd. Fax: North Wilkesboro, NC 28659 Email:_ iames.boles@lpcorp.com Project:_ WQ0000461 P.O.#: Atteni James Boles Turn Around Time* How would you like your report sent? *RUSH work needs prior approval. Circle all that apply: ai eferred), Fax, Std 30da s) 3-5_Days ZOs M E R I TE C H INC. 1Address:_ ENVIRONMENTAL LABORATORIES 642 Tamco Rd. Phone: 336-342-4748 N Reidsville NC 27320 Fax: 336-342-1522 Email: info@meritechlabs.com www.meritechlabs.com Sample Location and/or ID # Sampling Dates & Times PersonT 'ngSampl (sign/Print): p Lab Use Only Start End Comp? Grab? # of Cont. Test(s) Required On Ice? y s / No pH OK? CI OK? Date Time Date Time DS1-MW-5 9/28/20 15:00 9/28/20 15:25 G 2 Chloride, TDS G I 2 NH3, Ntot, NO3 G 3 8260(w/HCI) TU�on Temperature / Receipt: r t Method of Shipment: *** Dechlorination (<0.5 m of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to reservation. Comments: Compositor # ❑ UPS Jug # ❑ Fed Ex Are these results for regulatory purposes? Yes ❑ No ❑ Report results in: mg/L ❑ mg/kg ❑ ug/L () Hand Delivery Relinquished Dat Time: Received by: Time; A C) Other s G Time: ,tom �-�L/ Received b : Date: Time: Relinquished by: Date: Time: Rec bed by 1pb:_� ) e _pate: Time: L9 SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733.3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 10/31/2020 Facility Name: Louisiana Pacific Corp. Non -Discharge WQ0000461 UIC Permit Name (if different): NPDES NC0005266 Other Facility Address: 1068 ABTCO Rd. TYPE OF PERMITTED OPERATION BEING MONITORED North Wilkesboro NC 28659 County Wilkes ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: Contact Person: James Boles Telephone#: 336-696-3348 ❑ Rotary Distributor A Land Application of Sludge Well Location/Site Name: DS1-MW6 No. of wells to be sampled: ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW6 Date sample collected: 9/29/2020 FIELD ANALYSES: WAS Well Depth: 21.4 ft, Well Diameter: 4 in. pH 00400: 6.02 units Temp. 0001o: 20.6 °C DRY at Depth to Water Level 82546: 13'5" ft. below measuring point Screened Interval: 11.25 ft. to 21_25 ft. Spec. Cond. 00094. 379 µMhos time sampling, Measuring Point is 1.5 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 14 gallons Appearance Dingy here: Samples for metals were collected unfiltered: 0 YES ❑ NO and field acidified: ® YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 9/30/2020,10/6/2020,10/7/2020 Laboratory Name: Meritech Inc. Certification No. 165 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 rng/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 <0.10 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note. Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 703oo 74 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 <0.5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑■ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # Total Ammonia 00610 0.5 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3as N, Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Scott Cranston, Plant Manager Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.212010 Meritech, Inc. Environmental Laboratory if Laboratory Certification No.165 . Contact: James Boles Report Date: 10/9/2020 Client: Louisiana-Pacific Corp. NPDES#: NC0005266 1068 ABTCO Rd Land App. Permit#: WQ0000461 North Wilkesboro, NC 28659 Date Sample Rcvd: 9/28/2020 Meritech Work Order # 09292048 Sample: DS1-MW6 Grab Parameters Result Analysis Date 9/28-29/20 Reporting Limit Method Total Dissolved Solids 74 mg/L 9/30/20 10 mg/L SM 2540C Chloride <0.5 mg/L 10/6/20 0.5 mg/L SM 4500 Cl B Ammonia, Nitrogen 0.5 mg/L 10/7/20 0.1 mg/L EPA 350.1 Nitrate, Nitrogen <0.10 mg/L 9/30/20 0.10 mg/L EPA 353.2 TKN 0.49 mg/L 10/6/20 0.20 mg/L EPA 351.1 Nitrate/Nitrite, Nitrogen <0.10 mg/L 9/30/20 0.10 mg/L EPA 353.2 Nitrogen, total 0.49 mg/L 10/6/20 0.20 mg/L EPA 353.2 8260 Attached 9/30/20 - - EPA 8260 I hereby certify that I have reviewed and approve these data. aboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 MERITECH, INC. Environmental Laboratories ^' A Division of Water Technology and Controls, Inc. Client: Louisiana Pacific Corp. Meritech ID#: 09292048 Project: WQ0000461 Analysis: 09/30/20 Client Sample ID: DSI-MW-6 Analyst: VW Sample Collection: 09/29/20 Dilution Factor: 1 Report Date: 10/08/20 Acetone < 5.00 ug/L cis-1,3-Dichloropropene < 0.500 ug/L Acrylonitrile < 5.00 ug/L trans-1,3-Dichloropropene < 0.500 ug/L Benzene < 0.500 ug/L Ethanol < 50.0 ug/L Bromodichloromethane < 0.500 ug/L Ethyl benzene < 0.500 ug/L Bromochloromethane < 0.500 ug/L Hexachlorobutadiene < 0.500 ug/L Bromoform < 0.500 ug/L 2-Hexanone < 1.00 ug/L Bromomethane < 0.500 ug/L Isopropylbenzene < 0.500 ug/L 2-Butanone (MEK) < 5.00 ug/L p-Isopropyltoluene < 0.500 ug/L n-Butylbenzene < 0.500 ug/L Methylene chloride < 0.500 ug/L sec-Butylbenzene < 0.500 ug/L Methly Isobutyl Ketone (MIBK) < 0.500 ug/L Carbon disulfide < 0.500 ug/L Methyl iodide < 0.500 ug/L Carbon Tetrachloride < 0.500 ug/L Naphthalene < 0.500 ug/L Chlorobenzene < 0.500 ug/L n-Propylbenzene < 0.500 ug/L Chloroethane < 0.500 ug/L Styrene < 0.500 ug/L Chloroform < 0.500 ug/L 1, 1, 1,2-Tetrachloroethane < 0.500 ug/L Chloromethane < 0.500 ug/L 1,1,2,2-Tetrachloroethane < 0.500 ug/L 2-Chlorotoluene < 0.500 ug/L Tetrachloroethene (PCE) < 0.500 ug/L 4-Chlorotoluene < 0.500 ug/L Toluene < 0.500 ug/L Dibromochloromethane < 0.500 ug/L 1, 1, 1 -Trichloroethane < 0.500 ug/L 1,2-Dibromo-3-chloropropane < 0.500 ug/L 1,1,2-Trichloroethane < 0.500 ug/L 1,2-Dibromoethane (EDB) < 0.500 ug/L Trichloroethene (TCE) < 0.500 ug/L Dibromomethane < 0.500 ug/L 1,2,3-Trichlorobenzene < 0.500 ug/L Dichlorodifluoromethane < 0.500 ug/L 1,2,4-Trichlorobenzene < 0.500 ug/L 1,1-Dichloroethane < 0.500 ug/L 1,2,3-Trichloropropane < 0.500 ug/L 1,2-Dichloroethane < 0.500 ug/L Trichiorofluoromethane < 0.500 ug/L 1,4-Dichlorobenzene < 0.500 ug/L 1,2,4-Trimethylbenzene < 0.500 ug/L 1,2-Dichlorobenzene < 0.500 ug/L 1,3,5-Trimethylbenzene < 0.500 ug/L 1,3-Dichlorobenzene < 0.500 ug/L Vinyl acetate < 1.00 ug/L 1,1-Dichloroethene <0.500 ug/L Vinyl chloride <0.005 ug/L cis-1,2-Dichloroethene < 0.500 ug/L m/p-Xylenes < 1.00 ug/L trans-1,2-Dichloroethene < 0.500 ug/L o-Xylene < 0.500 ug/L trans-1,4-Dichloro-2-butene < 0.500 ug/L 1,2-Dichloropropane < 0.500 ug/L Additional Compounds 1,3-Dichloropropane < 0.500 ug/L Methyl-tert-butyl ether (MTBE) < 0.500 ug/L 1, 1 -Dichloropropene < 0.500 ug/L Isopropyl ether (LPE) 500 ug/L 1,2-Dichloropropene < 0.500 ug/L I hereby certify that I have reviewed and approve these data. Lab atory res tative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax MERITECH, INC. Environmental Laboratories - A Division of Water Technology and Controls, Inc. Client: Louisiana Pacific Corp. Project: WQ0000461 Client Sample ID: DSI-MW-6 Sample Collection: 09/29/20 Sample Volume: 5m1 purge % solid N/A Batch Blank = Below Reporting Limit Internal Standards method criteria acceptable (Yes ) / No es / No Meritech ID#: 09292048 Analysis: 09/30/20 Analyst: VWV Dilution Factor: I Report Date: 10/08/19 Surrogate Recoveries Spike Conc Spike Recovery Limits Dibromofluoromethane 30 ug/L 120% 51-141% Toluene-d8 30 ug/L 95% 67-151% Bromofluorobenzene 30 ug/L 90% 45-161% Laboratory QC Check Matrix Spike Recoveries Acceptable Spike Compound Spike Conc Spike %Rec 1, 1 -Dichloroethene 25 ug/L 52% Benzene 25 ug/L 112% Trichloroethene 25 ug/L 91 % Toluene 25 ug/L 74% Chlorobenzene 25 ug/L 79% # - Fails Limit Check * - If "no" is selected, see third page for details. (Yes ) / No Duplicate % Rec. RPD RPD Limits OC Limits 52% 1 20 40-133 112% 1 20 40-168 91% 0 20 42-143 75% 2 20 58-154 82% 3 20 48-136 I hereby certify that I have reviewed and approve these data. Labor ory rese tative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax 5-9-2016 Chain of Custody Record (COC) NPDES#:_ NC0005266 Client: Louisiana Pacific Corp. Phone:_ 336-696-3348 Address:_ 1068 ABTCO Rd. Fax: North Wilkesboro, NC 28659 Email:_ iames.boles@lpcorp.com Project:_ WQ0000461 P.O.#: Atteni James Boles Turn Around Time* How would you like your report sent? *RUSH work needs prior approval, Circle all that apply: eferred), Fax,Q Std 10 days) 3 - s D I zO s M E R ITE C H INC. 1 \ ENVIRONMENTAL LABORATORIES 642 Tamco Rd. Phone: 336-342-4748 M Reidsville NC 27320 Fax: 336-342-1522 Email: info@meritechlabs.com www.meritechlabs.com Sample Location and/or ID # Sampling Dates & Times Person Taking5a le (Sign/P ' ): Lab Use Only Start End Comp? Grab? # of Cont. Test(s) Required On Ice? s / No pH OK? Cl OK? Date Time Date Time DS1-MW-6 9/28/20 12:35 9/29/20 8:10 G 2 Chloride, TDS G 2 NH3, Ntot, NO3 G 3 8260(w/HCI) Temperature U,po� Receipt: lJ Method of Shipment: *** Dechlorination (<0.5 m) of Ammonia, Cyanide, Phenol and TKN samples must be done In the field prior to reservation. *** Comments: Compositor # ❑ UPS Jug # ❑ Fed Ex Are these r sults for regulatory purposes? Yes ❑ No ❑ Report results in: mg/L ❑ mg/kg ❑ ug/L ❑ Hand Delivery Relinquished by: D te: Time: _zzl Received by: G� t Time�2 / El Other n d Time: Received b : Date: Time: 11611uished by: ate: Time: Reqoived by La `r1 11 _Date: Time: U Vtx ct tRnAIT FnRnA nN YFI I nW PAPFR ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM M • , DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES • DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 10/31/2020 Facility Name: Louisiana Pacific Corp. Non -Discharge WQ0000461 UIC Permit Name (if different): NPDES NC0005266 Other Facility Address: 1068 A13TC0 Rd. TYPE OF PERMITTED OPERATION BEING MONITORED North Wilkesboro st-0 NC 28659 County Wilkes ❑ Lagoon ❑ Remediation: Infiltration Gallery cil„ Spray Field ❑ Remediation: Contact Person: James Boles Telephone#: 336-696-3348 ❑ Rotary Distributor ❑■ Land Application of Sludge Well Location/Site Name: DS1-MW9 No. of wells to be sampled: El Source Heat Pump ElOther: (from Permit) If WELL SAMPLING INFORMATION WELL ID NUMBER (from Permit): MW9 Date sample collected: 9/28/2020 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 4 in. pH 00400: 5.97 units Temp. 00010: 21.4 °C DRY at time of Depth to Water Level 82546: 13'1" ft. below measuring point Screened Interval: 6 ft. to Mhos 16 ft. Spec. Cond. 00094: 597 µ sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 10 gallons Appearance Clear here: ❑ Samples for metals were collected unfiltered: 0 YES ❑ NO and field acidified: ® YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 9/30/2020,10/2/2020,10/6/2020,10/7/2020 Laboratory Name: Meritech Inc. Certification No. 165 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 13.7 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 198 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 mg/L Ca - Calcium oo916 mg/L Chloride 00940 0.5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑■ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # Total Ammonia oo610 <0.1 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3as N, Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent i oiai vvus: iliyr� GW-59 Rev.2/2010 Meritech, Inc. Environmental Laboratory Laboratory Certification No.16S Contact: James Boles Report Date: 10/9/2020 Client: Louisiana-Pacific Corp. NPDES#: NC0005266 1068 ABTCO Rd Land App. Permit#: WQ0000461 North Wilkesboro, NC 28659 Date Sample Rcvd: 9/29/2020 Meritech Work Order # 09292049 Sample: DS1-MW9 Grab Parameters Result Analysis Date 9/28/20 Reporting Limit Method Total Dissolved Solids 198 mg/L 9/30/20 10 mg/L SM 2540C Chloride 0.5 mg/L 10/6/20 0.5 mg/L SM 4500 Cl B Ammonia, Nitrogen <0.1 mg/L 10/7/20 0.1 mg/L EPA 350.1 Nitrate, Nitrogen 13.7 mg/L 10/2/20 0.10 mg/L EPA 353.2 TKN <0.20 mg/L 10/6/20 0.20 mg/L EPA 351.1 Nitrate/Nitrite, Nitrogen 13.7 mg/L 10/2/20 0.10 mg/L EPA 353.2 Nitrogen, total 13.7 mg/L 10/6/20 0.20 mg/L EPA 353.2 8260 Attached 9/30/20 - - EPA 8260 I hereby certify that I have reviewed and approve these data. {,�rd Q Ha � Labor toa - -Repres�entative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 MERITECH, INC. Environmental Laboratories A Division of Water Technology and Controls, Inc_ Client: Louisiana Pacific Corp. Meritech ID#: 09292049 Project: WQ0000461 Analysis: 09/30/20 Client Sample ID: DSI-MW-9 Analyst: VWV Sample Collection: 09/28/20 Dilution Factor: 1 Report Date: 10/08/20 Acetone < 5.00 ug/L cis-1,3-Dichloropropene < 0.500 ug/L Acrylonitrile < 5.00 ug/L trans-1,3-Dichloropropene < 0.500 ug/L Benzene < 0.500 ug/L Ethanol < 50.0 ug/L Bromodichloromethane < 0.500 ug/L Ethyl benzene < 0.500 ug/L Bromochloromethane < 0.500 ug/L Hexachlorobutadiene < 0.500 ug/L Bromoform < 0.500 ug/L 2-Hexanone < 1.00 ug/L Bromomethane < 0.500 ug/L Isopropylbenzene < 0.500 ug/L 2-Butanone (IMIEK) < 5.00 ug/L p4sopropyltoluene < 0.500 ug/L n-Butylbenzene < 0.500 ug/L Methylene chloride < 0.500 ug/L sec-Butylbenzene < 0.500 ug/L Methyy Isobutyl Ketone (MIRK) < 0.500 ug/L Carbon disulfide < 0.500 ug/L, Methyl iodide < 0.500 ug/L Carbon Tetrachloride < 0.500 'ug/L Naphthalene < 0.500 ug/L Chlorobenzene < 0.500 ug/L n-Propylbenzene < 0.500 ug/L Chloroethane < 0.500 ug/L Styrene < 0.500 ug/L Chloroform <0.500 ug/L 1, 1, 1,2-Tetrachloroethane <0.500 ug/L Chloromethane < 0.500 ug/L 1,1,2,2-Tetrachloroethane < 0.500 ug/L 2-Chlorotoluene < 0.500 ug/L Tetrachloroethee (PCE) < 0.500 ug/L 4-Chlorotoluene < 0.500 ug/L Toluene < 0.500 ug/L Dibromochloromethane <0.500 ug/L 1, 1, 1 -Trichloroethane <0.500 ug/L 1,2-Dibromo-3-chloropropane < 0.500 ug/L 1,1,2-Trichloroethane < 0.500 ug/L 1,2-Dibromoethane (EDB) < 0.500 ug/L Trichloroethene (TCE) < 0.500 ug/L Dibromomethane < 0.500 ug/L 1,2,3-Trichlorobenzene < 0.500 ug/L Dichlorodifluoromethane < 0.500 ug/L 1,2,4-Trichlorobenzene < 0.500 ug/L 1, 1 -Dichloroethane < 0.500 ug/L 1,2,3-Trichloropropane < 0.500 ug/L 1,2-Dichloroethane < 0.500 ug/L Trichlorofluoromethane < 0.500 ug/L 1,4-Dichlorobenzene < 0.500 ug/L 1,2,4-Trimethylbenzene < 0.500 ug/L 1,2-Dichlorobenzene < 0.500 ug/L 1,3,5-Trimethylbenzene < 0.500 ug/L 1,3-Dichlorobenzene < 0.500 ug/L Vinyl acetate < 1.00 ug/L 1,1-Dichloroethene < 0.500 ug/L Vinyl chloride < 0.005 ug/L cis-1,2-Dichloroethene < 0.500 ug/L m/p-Xylenes < 1.00 ug/L trans-1,2-Dichloroethene < 0.500 ug/L o-Xylene < 0.500 ug/L trans-1,4-13ichloro-2-butene < 0.500 ug/L 1,2-Dichloropropane < 0.500 ug/L Additional Compounds 1,3-Dichloropropane < 0.500 ug/L Methyl-tert-butyl ether (MTBE) < 0.500 ug/L 1,1-Dichloropropene < 0.500 ug/L Isopropyl ether (IPE) 500 ug/L 1,2-Dichloropropene < 0.500 ug/L I hereby certify that I have reviewed and approve these data. Laboratory resentative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax MERITECH, INC. Environmental Laboratories A Division of Water Technology and Controls, Inc. Client: Louisiana Pacific Corp. Meritech ID#: 09292049 Project: WQ0000461 Analysis: 09/30/20 Client Sample ID: DSI-MW-9 Analyst: VWV Sample Collection: 09/28/20 Dilution Factor: 1 Sample Volume: 5ml purge Report Date: 10/08/19 % solid N/A Batch Blank = Below Reporting Limit (Yes) / No Internal Standards method criteria acceptable es / No Surrogate Recoveries Spike Conc Spike Recovery Limits Dibromofluoromethane 30 ug/L 120% 51-141% Toluene-d8 30 ug/L 97% 67-151% Bromofluorobenzene 30 ug/L 91% 45-161% Laboratory QC Check Matrix Spike Recoveries Acceptable Spike Compound Spike Conc Spike %Rec 1,1-Dichloroethene 25 ug/L 52% Benzene 25 ug/L l 12% Trichloroethene 25 ug/L 91% Toluene 25 ug/L 74% Chlorobenzene 25 ug/L 79% # - Fails Limit Check * - If "no" is selected, see third page for details. (Yes ) / No Duplicate % Rec. RFD RPD Limits OC Limits 52% 1 20 40-133 112% 1 20 40-168 91% 0 20 42-143 75% 2 20 58-154 82% 3 20 48-136 I hereby certify that I have reviewed and approve these data. Laboratory resentative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax Chain of Custody Record (COC) NPDES#:_ NC0005266 Client: Louisiana Pacific Corp. Phone:_ 336-696-3348 Address:_ 1068 ABTCO Rd. Fax: North Wilkesboro, NC 28659 Email:_ iames.boles@lpcorp.com Project:_ WQ0000461 P.O.#: Attent James Boles Turn Around Time* How would you like your report sent? *RUSH work needs prior approval. Stcl 10da s) 3-5_D�s Z�s Circle all that apply] ►S - eferred) , Fax, Ma � ME R I TE C H INC. 1 ENVIRONMENTAL LABORATORIES 642 Tamco Rd. Phone: 336-342-4748 Reidsville NC 27320 Fax: 336-342-1522 Email: info@meritechiabs.com www.meritechlabs.com Sample Location and/or ID # Sampling Dates & Times PersonTaki ample (Sly/Print): Comp? >Cont.Test(s) Required Grab? ont Lab Use Only Start End On Ice? Y s / No pH OK? Cl OK? Date Time Date Time DS1-MW-9 9/28/20 14:15 9/28/20 14:50 G 2 Chloride, TDS G 2 NH3, Ntot, NO3 G 3 8260(w/HCI) Temperata upon Receipt: j Qc 1 Method of Shipment: *** Dechlorination <0.5 m of Ammonia, Cyanide, Phenol and TKN samples must be done In the field prior to reservation. *** Comments: Compositor d ❑ UPS Jug # ❑ Fed Ex Are these results for regulatory purposes? Yes ❑ No ❑ Report results in: mg/L ❑ mg/kg ❑ ug/L ❑ ❑ Hand Delivery Relinquished by: Date: Time; Received by%%y Time, ❑ Other ' a ed b . Jz7p f, TimeL5 ry� U d/ Received by: Date: Time: Re inq ished by: Date: Time: Receive b llab: �in -re: Time: n (1