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NCG140398_2020 DMR_20210106
ANNUAL SUMMARY DISCHARGE MONITORING REPORT (DMR) — STORMWATER SUBMIT TO CENTRAL OFFICE* General Permit No. NCG140000 Calendar Year 2020 *Report ALL STORMWATER monitoring data on this form (include "No Flow /"No Discharge" and Benchmark Exceedances) from the previous calendar year to the DEQ by MARCH 1 of each year. Certificate of Coverage No. NCG14 13❑ 9❑ 8 Facility Name: Carolina Ready Mix and Builders Supply, LLC County: Madison Phone Number: (828 ) 686-3040 Certified Laboratory Pace Analyticial Lab # 40 Lab # Total no. of SDOs monitored 1 Stormwater Discharge Outfall (SDO) No. 001 VMA Outfall? Yes ❑ No ❑✓ Is this outfall currently in Tier 2 for any parameter? Yes ❑ No ✓❑ Was this outfall ever in Tier 2 during the past year? Yes ❑ No ❑✓ If this outfall was in Tier 2 last year, was monthly monitoring discontinued? Yes, enough consecutive samples below benchmarks to decrease frequency ❑ Yes, received approval from DEMLR to reduce monitoring frequency ❑ Other ❑ Outfall No. Total Rainfall, inches Total Suspended Solids (TSS), m /I pH, SU Non -polar O&G (EPA Method 1664 SGT-HEM)) , ( mg/I (VMA) Napplicable New Motor Oil Usage (gal/mo.) lfapplicable Stormwater Benchmarks Date Sample Collected, mo/dd/ r 05/18/20 Indicate NO FLOW if applicable 2.25 Circle Benchmark 100/50 43.2 6.0-9.0 15 8.4 NA >55 allmo. average requires TSS and g g Non -polar OaG monitoring NA 11 /11 /20 1.25 13.2 8.4 NA NA Permit Date 8/1/2017 — 6/30/2022 Last Revised 8-22-2015 Certificate of Coverage No. NCG14 0❑ 3❑ 9�® CERTIFICATION "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." [Required by 40 CFR §122.22] Signature'�1C`-!�. Date 01 /06/21 Mail Annual Summary Stormwater DMR to the NCDEQ Central Office: Note the address is correct — Central Files is housed in DWR (not DEMLR) N.C. Department of Environmental Quality (DEQ) Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 Central Files Telephone (919) 807-6300 Questions? Contact DEMLR Stormwater Permitting Staff in the Central Office at: (919) 707-9220 Permit Date 8/1/2017 — 6/30/2022 Last Revised 8-22-2015 NCDEQ Division of Energy, Mineral and Land Resources Stormwater Discharge Monitoring Report (DMR) Form for NCG140000 Ready -Mixed Concrete Click here for instructions Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office. Certificate of Coverage No. NCG14 0 3 9 8 Person Collecting Samples: Gary Kilker Facility Name: Carolina Ready Mix and Builders Supply, LLC Laboratory Name: Pace Analytical Facility County: Madison Laboratory Cert. No.: 40 Discharge during this period: ❑■ Yes ❑ No (if no, skip to signature and date) rHas your facility implemented mandatory Tier response actions for any benchmark exceedances? ❑ Yes ❑■ No If so, which Tier (I, Il, or III)? Part A: Analytical Monitoring Requirements for Outfalls with Industrial Activities— Benchmarks in (Red) Parameter Parameter Outfall Outfall Outfall Outfall Outfall Code N/A Receiving Stream Class Trout N/A Date Sample Collected MM/DD/YYYY 05/18/20 46529 24-Hour Rainfall in inches 2.25 C0530 TSS in mg/L (100 or 50*) 43.2 00400 pH in standard units (6.0-9.0) 8.4 Non -Polar Oil & Grease in 00552 mg/L (15) for drainage areas that use > 55 NA gal/mo of new hydraulic oil on average NCOIL Estimated New Motor/Hydraulic Oil NA Usage in gal/month * Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HOW), Trout Waters (Tr) and Primary Nursery Areas (PNA) have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 mg/L. Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 4 ittee or Delegated Authorized Individual 01.06.21 Date Li 0 LL Z R 0 Z S0 G Q •E CA C 1 L m 3 C m L L V V 41 W � Z ❑t.7 W � J W O a uLU zr aa0 0 z LAJ W h1 06 0 W a ~ z LL U } ui � J U LL L. N L 0 Li LO r a z a IS W = Z v ❑ N Oc H ❑ �C W } N El�4 .•. M1. U H z 0 Ln 3 z J z N a Q o W J a Q Q z H u W J J O u z O N O: W a LL z J a z 0 H a 0 21 r N C t IA L Q, c E LA w N O m N > C O .. C o f o C to a+ O � ,= Y i C , > LLI •E 7 J m LA kA w N \0 ~ E ry)A J E L _ 'C 4+ Q C C Qi L W W I aJ °C O " o £ 2 ;.3 tti H 0UJ O ' LL a 41 p \ O O E Z�h 1 O z 1 1 . �1 s \ m \ n Q1 N � w- �> O a1 K a1 N do N J d Y oj ai > O a ru c a aJ o (9 a) a� v c Q N E N C O a1 Q Y a i N E aJ f6 E aJ O h aJ Ln ca Uo �v c s O v 3 m v v = W o d _ 7 n to O ? Y "O L u v a c o w a) Y 2 -0 C7 o0 3 + N Q (� p C = v O E Y rz N_ m v o 0 = m Co M O u 0 C Y Z C N do O. i 0-'U a o w a u i N N O '—Z o o a 3 y O Ou u aJ v L v m x > +� (Uc � — w -4 w = Z3 W o C 3 c c E^ 4 Q Q O o N O _ -0 -1 -0 m U r a aJ r p u 0 ra z E O X > 6 \ v O aJ 'Q ` Q O . @ -r- aO u 10 p ra a Y z > o � °� E } 2 a`j a n a u u s H N C L C o a a 0 E A � � hA H C ++ T L 0 = L i+ O N C 2 E I 3 � v � Z S C 0 •fp V � d' C in a+ O W C +' a� 3 i C � W 0 V 1 4! 'O C J C 0 0cc0 fn yOj E m 0 t- 0 o uj _ ven J "IE 'In r ,_ � 3 _ o tz � 1 1 � CL r- C to H V i 1 � tL (i M E c u 4-6 3 Z O o a J Q f— O W z O r z Q Q V) LU Lu z ❑ W O W z U X ❑w Y (n Q W r U z W m N• or O W O c C G G W Q � � Z O W v Q o z =LLJO r u U U U z LL W Ov O J O Z W O V) > (7 Q Q W = _ = kA L Ln O z C 7 U C In 4- O e--1 � fT O U r\ ] L N a) C 0 3 c Lz aJ ' p � — v o C LL L (E a + u U O ' > L t ZN 0 L/) i O O 0 � z L O Ln o ❑ _ U c .OJ .0 ❑ Q CY ai 0 o v y Q E E CU u E y O U 7 E � � y O CL 6 C u c a O m E c c a c 0 O O f11 N L > aj o E O 0 E o O 'Z3 O C C ZS O C N O N E y L L — O O 0 Q1 m -6 4J m v y y v E E 7 ai -0 C � o ._ (1J C @ a) E 'O 2 3 E E o 'v o E •E � •E — N 7 � v N E � txo o O L vi U y Q1 4J tlA txo C i 3 C C C O ' + p fl- i I a) L L v v v tv C- "- i y i v :3 v) 1 0- :_ y 0 ++ I L Q) �F ¢' t)J f4 : v v 1 v� O E (6 E Ln r-I O N \ O m _ O d � M i+ 0 E N L \ \ �H O a N L ra 3 ❑ � y m d t nvironmento/ Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit https:Hdeq.nc.gov/about/divisions/energy-mineral-land-resources/ npdes-stormwater-gps Permit No.: N/C/ / / / / / / / or Certificate of Coverage No.: NcAgr. / "Y /U Facility Name: �° �C' lV� - �� gg14Al- [..-- County: f ) A1>1s,aht Phone No. &) 9 - Af /,-� . -7 D `/G Inspector: kc Date of Inspection: >� Time of Inspection: % / O c' Total Event Precipitation (inches): c2• 0 5 .............- ............ --- —__-__........ _........... _.._---_...... _... - ....................... ....- - ..._-.. ....... --- All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the pennittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: Of Permittee or Designee) 1. Outfall Description: Outfall No. a):Z Structure (pipe, ditch, etc.): d,' k-j, Receiving Stream: eveg -Rle e ,4A ?r t;e r - Describe the industrial activities that occur withinthe outfall drainage area: !! Page 1 of 2 SWU-242, Last modified 06/01/2018 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors:��- 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): ny CVlrz— 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 1 �,;` 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: L., 2 3 4 5 7. Is there any foam in the stormwater discharge? 0 Yes Q No. 8. Is there an oil sheen in the stormwater discharge? OYes c@, No. 9. Is there evidence of erosion or deposition at the outfall? O Yes 0 No. 10. Other Obvious Indicators of Stormwater Pollution: List and describe Po kV Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 06/01/201 S o ' a,� ceAnalydical www,pacslabs.c0M June 01, 2020 Gary Kilker Carolina Ready Mix 606 Old US Highway 70 Ridgecrest, NC 28770 RE: Project: STORMWATER 051820 Pace Project No.: 92478058 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Dear Gary Kilker: Enclosed are the analytical results for sample(s) received by the laboratory on May 19, 2020. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the face Network: • Pace Analytical Services -Asheville If you have any questions concerning this report, please feel free to contact me, Sincerely, 4— Chris Derouen christopher.derouen@pacelabs.com (828)254-7176 Project Manager Enclosures h� O REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, 4 without the written consent of Pace Analytical Services, LLC. %9eQg�.Sp , Page 1 of 13 (��aoeAnalXical www.pacelabs.com Project: STORMWATER 05182D Pace Project No.: 92478058 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 FloridalNELAP Certification M E87648 Massachusetts Certification M M-NC03D North Carolina Drinking Water Certification 4: 37712 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 CERTIFICATIONS North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 UrginiaNELAP Certification M 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 13 aceAnalAcal wwvt.pacelabs.cam Project: STORMWATER 051820 Pace Project No.: 92478058 Lab ID Sample ID 92478058001 _ MARSHALL 9247BOSS002 FLETCHER 9247BD58003 SWANNANOA PASI-A = Pace Analytical Services -Asheville Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254.7176 SAMPLE ANALYTE COUNT Method Analysts Analytes Reported Laboratory SM 254OD-2011 MJP 1 PASI-A EPA 9040C SMK 1 PASI-A SM 254OD-2011 MJP 1 PASI-A EPA9040C SMK 1 PASI-A SM 2540D-2011 MJP 1 PASI-A EPA9040C SMK 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 113 _ ;a'ceAnaljd1cal' www.pacelahs,com ANALYTICAL RESULTS Project: STORMWATER 05182D Pace Project MD.: 92478058 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: MARSHALL Lab ID: 92478058001 Collected: 05/1812011:20 Received: 05/19/20 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services -Asheville Total Suspended Solids 43.2 mg/L 25.0 1 05/21/2011:42 9040 pH Analytical Method: EPA 9040C Pace Analytical Services -Asheville pH at 25 Degrees C 8.4 Sid. Units 0.10 1 05/D1/20 15:23 H3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/01/2D20 04:25 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 13 Pace Analytical Services, LLC 2225 Riverside Dr. ,1!;1axAnalyticalo Asheville, NC 28804 www,pacelahs.com (828)254-7176 ANALYTICAL RESULTS Project: STORMWATER 051820 Pace Project No.: 9247SD58 Sample: FLETCHER Lab ID: 92478058002 Collected: 05/18/20 07:10 Received: 05/19/20 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services -Asheville Total Suspended Solids 61.3 mg/L 12.5 1 05121/2011:43 9040 pH Analytical Method: EPA D040C Pace Analytical Services - Asheville pH at 25 Degrees C 8.2 Std. Units 0.10 1 0610112015:14 H3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/01/2020 04:25 PM without the written consent of pace Analytical Services, LLC. Page 5 of 13 ��aceAnalXical" www.pacelabs.com ANALYTICAL RESULTS Project: STORMWATER D51820 Pace Project No.: 92478058 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, ND 28804 (828)254-7176 Sample: SWANNANOA Lab ID: 92478058003 Collected: 05/18/20 08:35 Received: 05/19/20 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 254DD-2011 Pace Analytical Services -Asheville Total Suspended Solids 31.7 mg/L 6.2 1 05/2112011:43 9040 pH Analytical Method: EPA 9040C Pace Analytical Services -Asheville pH at 25 Degrees C 7.8 Sid, Units 0.10 1 06101/2015:16 H3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in lull, Date: 06/01/2020 04�25 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 13 (��IaceAnalyfical www.pacolabs.com QUALITY CONTROL DATA Project: STORMWATER 051820 Pace Project No.: 92.478058 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QC Batch: 542864 Analysis Method: SM 254OD-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92478058001, 9247BD58002, 92478058D03 METHOD BLANK: 2891867 Matrix: Water Associated Lab Samples: 92478058001, 92478058002, 92478D58003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 05/21/2011:42 LABORATORY CONTROL SAMPLE: 2891868 Spike LCS LCS %Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 266 106 90-110 SAMPLE DUPLICATE: 2891869 92478197001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 268 272 1 SAMPLE DUPLICATE: 2891870 92478214001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 6D7 618 2 Results presented on this page are In the units Indicated by the "Units" column exceptwhere an alternate unit Is Presented to the rlghtof the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Dale: 00/01/4020 04:25 PM without the written consent of Pace Analytical Services, I.I.C. Page 7 of 13 VaceAnalytical" ._. www.pacefabs.wm QUALITY CONTROL DATA Project: STORMWATER 051820 Pace Project No.: 92478058 QC Batch: 544392 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92478058001, 92478058002, 92478058003 SAMPLE DUPLICATE: 2898995 92477877D01 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 7.1 7.0 1 H3 SAMPLE DUPLICATE: 2898997 92478588001 Dup Parameter Units Result Result RPD Qualifers pH at 25 Degrees C Sid. Units 7.8 7.8 0 H3 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Results presented on lhls page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/01/2020 04:25 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 13 loon Pace Analytical services, LLC p 2225 Riverside Dr. aceAnapical Asheville, NC 28804 www.paceiabs.com (828)254-7176 QUALIFIERS Project: STORMWATER 051820 Pace Project No.; 92478058 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazinedecomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chioroethylvinyl ether. A separate vial preserved to a pH of 4-5 Is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. Date: 06/01/2020 04:25 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written coiseni of Pace Anaytical Services, LLC. Page 9 of 13 (�IaceAnalytical www,pacalabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: STORMWATER 051820 Pace Project No.: 92478058 Lab ID Sample ID QC Batch Method 92478058001 MARSHALL SM 254OD-2011 92478058002 FLETCHER SM 2540D-2011 92478058003 SWANNANOA SM 2540D-2011 92478058001 MARSHALL EPA 9040C 92478058002 FLETCHER EPA 9040C 92478058003 SWANNANOA EPA 9040C Date: 06/01/2020 04:25 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QC Batch Analytical Method 542864 542864 542864 544392 544392 544392 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Li-C. Analytical Batch Page 10 of 13 j� �� Sample >°dG2mcallCf1I Document Name: Document No.: F-CAR•CS-033-Rev Document Revised: February 7, 2018 Page 1 of 2 issuing Authority: Pace Carolinas Quality Office Laboratory receiving sa ples. Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑ Asheville Eden❑ WO# ' 92478058 Client Name: Project #: Cho �s ts� Tull C 1 Courier: ❑Fed Ex ❑UPS USPS Client III IIII I IN 11111111111 ❑ Commercial ❑Pace ❑other;, 92478058 Custody Seal Present? ❑)ZNo Seals Intact? Dyes ONO t JYes Datejlnitials Person Examining Contents; rr 7 Packing Material: ❑Bubble wrap []Bubble Bags None ❑ Other Biological Tissue Frozen [-]yes ❑No PN/A Thermometer: �� G w Type of Ice: JZWet ❑Blue ZI Ilt Gun ID: ❑None Cooler Temp (°C): b,5 Correction Factor: Add/Subtract (°C) D. 0 Tamp should be above freezing to 6°C S Cooler Temp Corrected VC)-- ❑Samples out of ternp criteria. Samples on ice, cooling process has begun Ills USDA Regulated Soil (7f N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, Ha%vai! and Puerto Rico)? Elves []No []Yes ❑No Including Comments/Dlscrepa ncy: Chain of Custody Present? Yes LJN2 LJN/A A. Samples Arrived within Hold Time? Yes No []N/A 2. Short Hold Time Analysis (<72 hr.)? Yes No ❑N/A 3• Rush Turn Around Time Requested? .-Yes No ❑N/A 4• Sufficient Volume? Yes No N/A 5. Correct Containers Used? Yes []No [I NIA G. -Pace Containers Used? Yes ❑No ❑N/A Containers Intact? Yes [0No ❑N/A 7. Dissolved analysis: Samples Field Filtered? IlYes No Z ❑N/A S. Sample Labels Match COC? Yes ❑No ❑N/A 9. 19eacispace in VOA Vials ❑Yas ©No N/A 10. Trip Blank Present? W ❑Yes �jNo N/A 11. Trip Blank Custody Seals Present? ❑ytrs MNO N/A ,,{ Field Data Required? ©Yes X..IFJo COMMENTS/SAMPLE DISCREPANCY / — Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/Time: Date: Project Manager SCURF Review: Date: Project Manager SRF Review; Page 11 of 13 ,� Document flame: sample Condition Upon Receil �weAnai�ical Document No.: F-CAR-CS-033-Rev,06 *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/801S (water) DOC, LLHg **Bottom half of box Is to list number of bottle x Z) C z •iC E fJ E N E �' � E � E O to E � O E C' .F d E a m m c N m H w H m m m a m a m ll7 3 t�.7 d l�7 a lM'J ¢ 1 \ + i 2 3 l �4 5 y 6 7 \ 8 9 10 11 J2 Document Revised: February 7, 2018 Page 1 of 2 Issuing Authority: Pace Carolinas Quality Office Project N W®# : 92478Q58 PM; COI Due Date: 06/03/20 CLIENT: 93—CarolinaR pH Adjustment Log for Preserved Samples Time Sample ID Type of PrepH upon receipt Date preservation adjusted pdr)useryAmount dation aervative added servative h;ote: Whenever there is a discrepancy affectln8 North Carolina compliance samples, a copy of this form wia be sent to Ilte North Carolina DEHNR Cei Out of hold, incorrect preservative, out of temp, lncormct containers, on Lot W page 12 of 13 £ b iO E 6 06ed W O CV- 0 i easrT:j® (jeuy teyi0 loueylew £ONZBN HOON 104 dill �71 rn o; N� W G •° nj a^ -ZI I # WBIIe- (NIA} i�etul � so�dwag NIA te�oop Pains (NrA) nj uo paya0aa 0 u! d w31 J �S r .h a W J a CL z z 7 *I £ 610 £ 6 OBd (NO, � la� NI ,l000 alea b sn WA) `14 ol 0�7 C� uo Payaaaa (NIA) oul,olyo lenp{saa 0 u! dW31 a � � a h a ° s � w 17111 � e Nld ;ssl see�S{euy �': 9 ,ay!a y SOMON ts m HOaN \ A y m IOH { IL CONH z o ti osz c I �i L g Patiaseldu( P: w moo Jo SH3iY1 n Q a. o. a - J W NGI1G3llo31V d1Y3131dfYV8 w 3 a a J Q a s a z J w E z �3 O Q Cf o s•'1 ,�,.,,: Q a N x rdwoa�v edtt�•01 HdA13ldVVS CQ <p t ZV U E O E (pa�o{fapm plan ws) 3dGO XI?llYYi 3 iu CL O n N a m z# W M N cr n W ` r x J `u m S pp �vy r r r V r9i o[ cr w a NCDEQ Division of Energy, Mineral and Land Resources Stormwater Discharge Monitoring Report (DMR) Form for NCG140000 Ready -Mixed Concrete Click here for instructions Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring; Report (DMR) Upload form within 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office. Certificate of Coverage No. NCG14 0 13 19 18 Person Collecting Samples: Gary Kilker Facility Name: Carolina Ready Mix and Builders Supply, LLC Laboratory Name: Pace Analytical Facility County: Madison Laboratory Cert. No.: 40 Discharge during this period: ❑■ Yes ❑ No (if no, skip to signature and date) Has your facility implemented mandatory Tier response actions for any benchmark exceedances? ❑ Yes ❑■ No If so, which Tier (I, 11, or III)? Part A: Analytical Monitoring Requirements for Outfalls with Industrial Activities— Benchmarks in (Red) Parameter Parameter Outfall Outfall Outfall Outfall Outfall Code N/A Receiving Stream Class Trout N/A Date Sample Collected MM/DD/YYYY 11/11/20 46529 24-Hour Rainfall in inches 1.25 C0530 TSS in mg/L (100 or 50*) 13.2 00400 pH in standard units (6.0 — 9.0) 8.4 Non -Polar Oil & Grease in 00552 mg/L (15) for drainage areas that use > 55 NA gal/mo of new hydraulic oil on average NCOIL Estimated New Motor/Hydraulic Oil NA Usage in gal/month * Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA) have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 mg/L. Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 01.06.21 Permittee or Delegated Authorized Individual Date I.L. 0 LL z_ R 0 F— z 00 G fa L Q .^E W Ln 1 0 0 Ln v Q W cc Q t2 v ) 0 cc cc RI uj ❑ I i❑ J L Q N (L E ui O❑ N o �N I ❑ Q IA L } L to O❑Q u O M O0, -in-2 ;,,� o>c ui Z O Z J L Z > a a z Z 2 :) O U Ln V) Ou a Q 0 001 CI m OI R* r-I 0 V Z *k � M M J J Id O m V Z i J �C L = °- d O O Z Q LL ui U O O w m LU a o Q Q Z u U y Z uw LL O LL J w U OTC 0~C L Q L L U I1 a U f rt Z d ~ ry C � c E N cO C N O n• C y a+ O F C r T O i _ 2 O a Q C r C in ++ O av r Y � � > C 1 O L o E N r J � E o fC N H E v> 3 N v OLL v ° o O e- o E Z 0 Z r O 7 O O M c-I n N N N > O Q! � K N N N W M 4J J CL E > a O u Q � � C a v o � v v a. aJ C Q E v co c o Y v i N EfB � m v O F- N N O 'CIO w bD O i C � Y v E y Y Y � v L E c L O ayci 01 3 � v Y Y 2 d Q O mw v E E 3 m v 3z�L � � LL o0 o -0 c ; Y p o E v u a 2 u I-- O 0 0 � •y- N O N w aj m 3 p 7 2 L � U/ v o o s ro w O u c E � � L NV O N m V N j a y O N YO LL N O o N 3 y Z c Q O O v c d Y M X > � v v — E in w on O CD c N Q o 00 v O U y v v O U" O — v O O n L U O z X > -O \ o Q v n O .N , I y J V u R O M2 E C _ Ln o v m a LL O N ++ N OC 0 v a E O O 0A L i 'L H � O T O O 5 g o O s L }I 0 w C SO O N E = 3 m cu Z a c. C in O a) ar � m L = w 3 'E � V ar v c C 0 a -0 .� ' OH E � r.. O F- O t W 2 In �tn Q O � CL = O +— o� C O =r- a) Q -0 a) � E ' Ny ar 0 0 o V E O 3 Z 0 In J a O Lu O T z LU Q U z w LUO LU U Z LU X ❑ Y CC V) aW � r u z LLJ co r c Z 00 w z s O w .ZT _ in H Q 0 = W H F Q J � v z O U O O> > W a Q a; o ° v y Q CU E E O bD a) C L c E a) ° •° v dA 9 C u .> v E u. w o ai .c 3 3 5 o u C Y C O .— O O O- -o C u C a1 o m E c c a) c O aD O C i -0 N O a) v a a ) 0 E a) y Y O o_ � c `o •� o c c a N u .T T L = T O O *' 0 cu E ° •- n 0 v o v cu C CO 3 y y a) E on v 0 m 'E ° v - c u =3 o .S Q � •y O O QJ 'y ♦+ 3 ro o ro v E c E c p •v O S a) N � O— y y t@ � E c @ O y co � E L C ° a, 0 y al a) M y ; � m 0 O � a) c 3 v�N _ c ° Q N ° v C O. 4_• L Y N O C 01 6LA C L O O u vO O E _ h N M N_ O N o TID Ln 0 N 0 m O 4J � N ci c-1 C:) N CL O N 3 � i+ y E N d i "I 11.: rwiro)2Jiten tal Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit https:Hdeq.nc.gov/about/divisions/energy-mineral-land-resources/ npdes-stormwater-gps Permit No.: N_/C/ / / / / / / / or Certificate of Coverage No.: N_/C/G/ Facility Name: Nk,2 I"Aoj Za n/, County: &4 n `SO,v' Phone No. Inspector: ,44n'! Date of Inspection: Time of Inspection: Total Event Precipitation (inches): ... I I All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the pennittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Sign re of Permittee or Designee) 1. Outfall Description: Outfall No. 60. L Structure (pipe, ditch, etc.): r- Receiving Stream: Describe the industrial activities that occcur within the outfall drainage area: Page 1 of 2 SWU-242, Last modified 06/01/2018 2. Color: Describe the color of the discharge using basic (light, medium, dark) as descriptors: 0) (red, brown, blue, etc.) and tint 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): /1/ U © q?,2 h 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1� 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: (3�11 2 3 4 5 7. Is there any foam in the stormwater discharge? Q Yes Q� No. 8. Is there an oil sheen in the stormwater discharge? OYes A� No. 9. Is there evidence of erosion or deposition at the outfall? O Yes 'Q No. 10. Other Obvious Indicators of Stormwater Pollution: List and describe no nle Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 06/01/2018 aceAnalytical www.pacelahs.tom December 01, 2020 Gary Kilker Carolina Ready Mix 606 Old US Highway 70 Ridgecrest, NC 28770 RE: Project: Stormwater 11/11 Pace Project No.: 92505579 Dear Gary Kilker: Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Enclosed are the analytical results for sample(s) received by the laboratory on November 12, 2020. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services -Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, 4—��- Chris Derouen christopher.derouen@pacelabs.com (828)254-7176 Project Manager Enclosures �.fQ pCFO 2`/ REPORT OF LABORATORY ANALYSIS v This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 15 ace Analytical"' www.pacelabs.com it i Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 CERTIFICATIONS Project: Stormwater 11/11 Pace Project No.: 92505579 Pace Analytical Services Charlotte 9800 KinceyAve. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 15 aceAnalXical www.pacelabs.com SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Stormwater 11/11 Pace Project No.: 92505579 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92505579001 MARSHALL SM 2540D-2011 ALP 1 PASI-A EPA 9040C NAL 1 PASI-A 92505579002 FLETCHER SM 2540D-2011 ALP 1 PASI-A EPA 9040C NAL 1 PASI-A 92505579003 SWANNANOA PLANT EPA 1664E CJM 1 PASI-C EPA 1664B CJM 1 PASI-C SM 2540D-2011 ALP 1 PASI-A EPA 9040C NAL 1 PASI-A PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 15 Pace Analytical Services, LLC Analytical 2225 Riverside Dr. d ;a7ceAnalyt ca Asheville, NC 28804 www.pacelabs.com (828)254-7176 i ANALYTICAL RESULTS Project: Stormwater 11/11 Pace Project No.: 92505579 Sample: MARSHALL Lab ID: 92505579001 Collected: 11/11/20 16:05 Received: 11/12/20 08:19 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services - Asheville Total Suspended Solids 13.2 mg/L 2.5 1 11/14/20 12:02 9040 pH Analytical Method: EPA 9040C Pace Analytical Services - Asheville pH at 25 Degrees C 8.4 Std. Units 0.10 1 11/30/20 17:27 H3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/01/2020 09:23 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 15 Pace Analytical Services, LLC 2225 Riverside Dr. aceAnalytical Asheville, NC 28804 www.pacelabs.com (828)254-7176 i ANALYTICAL RESULTS Project: Stormwater 11/11 Pace Project No.: 92505579 Sample: FLETCHER Lab ID: 92505579002 Collected: 11/11/20 12:40 Received: 11/12/20 08:19 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services - Asheville Total Suspended Solids 43.1 mg/L 2.5 1 11/14/20 12:02 9040 pH Analytical Method: EPA 9040C Pace Analytical Services -Asheville pH at 25 Degrees C 8.7 Std. Units 0.10 1 11/30/20 17:26 H3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/01/2020 09:23 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 15 ;7 6 /�ceAnalXical www.pacelabs.com ANALYTICAL RESULTS Project: Stormwater 11/11 Pace Project No.: 92505579 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828 )254-7176 Sample: SWANNANOA PLANT Parameters Lab ID: 92505579003 Collected: 11/11/20 10:05 Results Units Report Limit DF Received: 11/12/20 08:19 Matrix: Water Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Oil and Grease ND mg/L 5.0 1 11/25/20 12:06 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 5.0 1 11/25/20 12:06 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services -Asheville Total Suspended Solids 31.7 mg/L 2.5 1 11/14/20 12:02 9040 pH Analytical Method: EPA 9040C Pace Analytical Services - Asheville pH at 25 Degrees C 8.6 Std. Units 0.10 1 11/30/20 17:25 H3 Date: 12/01/2020 09:23 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 15 01,101 11,,RalceAnalytical www.pacelabs.com i' i QUALITY CONTROL DATA Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Stormwater 11/11 Pace Project No.: 92505579 QC Batch: 582959 Analysis Method: EPA 1664E QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92505579003 METHOD BLANK: 3082581 Matrix: Water Associated Lab Samples: 92505579003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 11/25/20 12:06 LABORATORY CONTROL SAMPLE: 3082582 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 34.5 86 78-114 MATRIX SPIKE SAMPLE: 3082583 35589884015 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Limits Qualifiers Oil and Grease mg/L 2.6J 40 33.6 78 78-114 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/01 /2020 09:23 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 15 aceAnalXical www.pacelabs.com Project: Stormwater 11/11 Pace Project No.: 92505579 QC Batch: 582960 QC Batch Method: EPA 1664B Associated Lab Samples: 92505579003 METHOD BLANK: 3082591 Associated Lab Samples: 92505579003 Parameter Units Total Petroleum Hydrocarbons mg/L QUALITY CONTROL DATA Analysis Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH Laboratory: Pace Analytical Services - Charlotte Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 11/25/2012:06 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 LABORATORY CONTROL SAMPLE: 3082592 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 19.6 98 64-132 MATRIX SPIKE SAMPLE: 3082593 35589884015 Spike MS MS % Rec Parameter Units Result Conic. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 5.01.1 20 10.2 38 64-132 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/01/2020 09:23 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 15 / .ceAnalytical www.pacelabs.com i i QUALITY CONTROL DATA Project: Stormwater 11/11 Pace Project No.: 92505579 QC Batch: 580382 Analysis Method: SM 2540D-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92505579001, 92505579002, 92505579003 METHOD BLANK: 3070275 Matrix: Water Associated Lab Samples: 92505579001, 92505579002, 92505579003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 11/14/20 12:00 LABORATORY CONTROL SAMPLE: 3070276 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 3070324 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 3070325 Parameter Units Total Suspended Solids mg/L Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 228 91 90-110 92505572001 Dup Result Result 51.4 52.2 92505597001 Dup Result Result 202 275 RPD Qualifiers 2 RPD Qualifiers 31 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/01 /2020 09:23 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 15 aceAnalytical " r www.pacelabs.com QUALITY CONTROL DATA Project: Stormwater 11/11 Pace Project No.: 92505579 QC Batch: 583262 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92505579001, 92505579002, 92505579003 SAMPLE DUPLICATE: 3084062 92505579003 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 8.6 8.6 0 H3 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/01/2020 09:23 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 15 �aceAnapicai www.pacelabs.com i QUALIFIERS Project: Stormwater 11/11 Pace Project No.: 92505579 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazini decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H3 Sample was received or analysis requested beyond the recognized method holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/01/2020 09:23 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 15 1!zAnalyfical' www.pacelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Stormwater 11/11 Pace Project No.: 92505579 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92505579003 SWANNANOA PLANT EPA 1664E 582959 92505579003 SWANNANOA PLANT EPA 1664B 582960 92505579001 MARSHALL SM 2540D-2011 580382 92505579002 FLETCHER SM 2540D-2011 580382 92505579003 SWANNANOA PLANT SM 254OD-2011 580382 92505579001 MARSHALL EPA 9040C 583262 92505579002 FLETCHER EPA 9040C 583262 92505579003 SWANNANOA PLANT EPA 9040C 583262 Date: 12/01 /2020 09:23 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Batch Page 12 of 15 <ceAnayical' Sa Document Name: Condition Upon Rec Document No.: Document Revised: October 28, 2020 Paae i of 2 issuing Authority: Pace Carolinas Quality Office Laboratory receiving samples: Asheville/ Eden[] Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑ Atlanta[] Kernersville(- Wa# a 9PV055 1 J Client Name: Project � Courier: ❑F d Ext ❑UPS ❑Ui S r Client 92505579 ❑ Commercial ❑Pace ❑Other: Custody Seal Present? []Yes ❑No Seals Intact? []Yes []No r Jt�/ Dr 2 Dale/Initials Person ExaminingContents:./ Packing Material: ❑Bubble Wrap ❑Bubble Bags E]None ❑ Other Biological Tissue Frozen? ❑Yes ❑No []N/A Thermometer: 1 ©wet ❑Blue Q IR Gun ID: c- , ij Cst Type of ice: / ❑Ncae Correction Factor: Cooler Temp: Add/Subtract (°C) Temp should be above freezing to VC ❑ia 1ptes out of temp criteria. Samples on ice, cooling process Cooler Temp Corrected (°C): l ! has begun USDA Regulated Soil ( P N/A, water sample) Did samples originate irt'a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples orginate from a foreign source (internationally, Dyes ❑No mcluomgnav m Corn me nts/ Discrepancy: Chain of Custody Present? MYes ONO ©N/A 1. Samples Arrived within Hold Time? Short Hold Time Analysis J<7Z hr.)? ffyes Oyes ©No ONo ❑N/A ❑N/A 2. 3. Rush Turn Around Time Requested? Oyes J No N/A 4. Sufficient Volume? r7lYes ❑No ❑N/A 5. Correct Containers Used? -Pace Containers Used? [nYes Oyes ONO ONO ❑N/A ❑N/A 6. —_ Containers Intact? QYes ONO ON 7. Dissolved analysis: Samples Field Filtered? yes ❑No , N/A 8. Sample Labels Match COC? -includes Date/lime/ID/Analysis Matrix: Headspace in VOA Vials (>5-6mm)7 Trip Blank Present? Trip Blank Custody Seals Present? [Yes 1 k ❑yes ❑Yes ❑Yes ©No rJNo []No ONO ❑N/A EIL A �j/ N/A NIA g• 10. 11. COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes (JNo Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Date/Time: X Date: Date: Page 13 of 15 Document Name: Sample Condition Upon Recei c7C6At7c7/YtICc71 ^ Document No.: F-CAR-CS-033-Rev.07 *Check mark top half of box if pH and/or dechlorination is Project # verified and within the acceptance range for preservation samples, Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLH8 **Bottom half of box is to list number of bottles Document Revised: October 28, 2020 Page 2 of 2 Issuing Authority: Darn rarnlin�;c n11,4Iity nffire WO# a 921.51)5579 PM: CD1 Due Date: 11/30/20 CLIENT: 93—CaralinaR I....._... . O H 4 Z W v a v v v r✓ y v z v z ? y m > Z rs c V V N C ? ON Q Z > _.-. °' z > U Z N v 2 ._ 2 U F r 2 2 .Y a 4 E Q ¢ E ¢J o `� Q� > Q O> O O > ii. w a v :n sv 'nC ? Q .� J E a J E E J E �: J E E J E J E Q a o y E m E J E J E E ,� A > 11 t > L E o E n o F 0 N e1 N D p `i p `f q '7 p 4 �p i N o N eN^! N to ri N M sir N yr M Q M S N H Ot t7r L. on Q l'J Io. N M t7 d a. L a a 6 6 4 3 'i t:) ei l9 a M U' a e-1 t7 a t7 a U' a V' o > > > > f> i o H m a > 0 m m m m m m co m a 2 I 3 5 6 7 i i 8 ; I 10 a i 12 -- pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot adjusted added t FHNR Certification Office (i.e. Note: Whenever there is a discrepancy affecting North Carouna compnance samplu,, a wp) Out of hold, incorrect preservative, out of temp, incorrect containers. Page 14 of 15 S L to S l abed (NIA) 1 helW SaldweS z NIA ialoo0 Q. poleaS R osn U (NI),) eJI (NIA) auu014) lenpisey (' 0 ul dW31 H K _ S h �f m o'. U u � n� gyp � w rA 6q aseat0 Due lip X z n SSl x x X o NlJ teal sas/ieuy p ta410 eloueglavl \ c y COZSNN a .. _, HOUN A � IOH CONH Q i a R, z m m 70SZH ur 4 coo o n�. a paruasoidu0 d0 it o v m R m ¢ U Q a a a Sa3Nl'1110� NDLL03l-M IV dmi 31dMIS ` Z W w p W p a R i- z 0 a ul _ _ F O y O (d Yf00=J evaO-ol 3dA13ldRYVS w +'� fuel of topoo Allan eas) g©�O 1(I i11VRY � � O F O a h m z i! O a Y gs3�a°S3za 'c s o c � d g E J d� K� `3c u 2 s O v # W 311 *- N M v N CO 3w CO 01 r E o` 9: 'E' n a U 4 \J