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HomeMy WebLinkAboutWQ0002127_CEIARR_NOVNOI2018PC0172_RESP_20180525CITY OF MORGANTON NORTH CAROLINA WATER RESOURCES DEPARTMENT May 25, 2018 G. Landon Davidson, Regional Supervisor Water Quality Regional Operations Section NCDEQ-Division of Water Resources 2090 US Highway 70 Swannanoa, NC 28778 Subject: Notice of Violation: NOV-2018-PC-0172 Permit No. WQ0002127 Dear Mr. Davidson, I have reviewed the permit violation referenced in NOV-2018-PC-0172 for our 2017 DCAR Report. After reviewing and discussing this with plant staff, it was determined that the reason for the residuals source monitoring for TCLP, Nutrients & Metals not being done during the permit cycle March 13, 2009 — February 29, 2018 was merely an oversite by the ORC. This monitoring has been planned with sampling schedule for the week of May 286, 2018. Your office will be notified when the analysis is completed. I hope that the details explained in this letter will be taken into consideration when the determination of a civil penalty assessment is made. The staff is a little embarrassed by this error but is committed to keeping a closer eye on the compliance schedule moving forward. If there are any questions please call 828-438-5276. Sincerely, Brad Boris Water Resources Director Telephone (828) 437-8863 305 East Union Street, Suite A100 PO Box 3448 www,ci.morganton.nc.us Morganton, NC 28655 Morganton, NC 28680-3448 July 12, 2018 G. Landon Davidson, Regional Supervisor Water Quality Regional Operations Section NCDEQ — Division of Water Resources Swannanoa, NC 28778 Subject: Notice of Violation: NOV-2018-PC-0172 Compost Sludge TCLP 2018 Permit No. WQ0002127 Dear Mr. Davidson This is in response to the violation notice Re: NOV-2018-PC-0172. The City of Morganton Composting staff has taken full responsibility to fulfill the requirements for our residual source monitoring for TCLP, Nutrients, and Metal. Enclosed you will find the test results for Compost Sludge TCLP 2018. Sincerely Tim Corpening Wastewater Superintendent City of Morganton PO Box 3448 Morganton, NC 28680 Receive Date:08/24/2018 Reported:09/27/2018 For:Sludge Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 180824-04-01 Aluminum Sludge 95500 mg/kg EPA 200.7 rev4.4 1994 09/27/2018 MD 180824-04-01 Ammonia Nitrogen Sludge 17593.9 mg/kg SM4500NH3BE-1997 08/28/2018 MD 180824-04-01 Arsenic - Solid Sludge 0.21 mg/kg SM3113 B-2004 09/04/2018 MD 180824-04-01 Cadmium - Solid Sludge 0.552 mg/kg SM3111B-1999 09/04/2018 MD 180824-04-01 Calcium Sludge 8380 mg/kg EPA 200.7 09/10/2018 MD 180824-04-01 Copper Sludge 317 mg/kg EPA 200.7 09/07/2018 MD 180824-04-01 Lead -Solid Sludge 6.513 mg/kg SM3113B 08/24/2018 MD 180824-04-01 Magnesium Sludge 2270 mg/kg EPA 200.7 09/10/2018 MD 180824-04-01 Mercury Solid Sludge 0.001 mg/kg SM3112B-2011 09/06/2018 MD 180824-04-01 Molybdenum Sludge 5.7 mg/kg EPA 200.7 09/10/2018 MD 180824-04-01 Nickel - Solid Sludge 8.544 mg/kg SM3113 B 09/10/2018 MD 180824-04-01 Nitrate/Nitrite - Solids Sludge 6.89655 mg/kg SM4500F/A 09/05/2018 CL 180824-04-01 PAN Sludge 4068 mg/L Calculation 09/18/2018 CL 180824-04-01 Percent Solids Sludge 26.1 %SM2540B-2011 08/27/2018 MD 180824-04-01 pH Sludge 7.9 Std. Units SM4500HB-2011 08/24/2018 MD 180824-04-01 Potassium - Solid Sludge 1220 mg/kg EPA200.7 09/04/2018 ENCO 180824-04-01 SAR Sludge 0.80 %Calculation 09/18/2018 CL 180824-04-01 Selenium Solid Sludge 0.958 mg/kg SM3113B 09/07/2018 MD 180824-04-01 Sodium - Solid Sludge 100 mg/kg SM 3111 B 09/11/2018 MD 180824-04-01 T. Phosphorus Solid Sludge 8352 mg/kg SM4500PE-2011 08/31/2018 CL 180824-04-01 TKN Sludge 51494.3 mg/kg SM4500Norg B-2011 08/31/2018 CL 180824-04-01 Zinc Sludge 707 mg/kg EPA 200.7 09/04/2018 MD Respectfully submitted, Analytical Results PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 13 Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 13 Condition of Receipt Sample Number 180824-04-01 Temp on Arrival:6.0 pH on Arrival: <2 Parameter Schedule: Nitric Acid Received on Ice Chemicals in containers, lab Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Arsenic - Solid Nitric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Cadmium Nitric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Cadmium - Solid Nitric Acid Chemicals in containers, lab Received on Ice pH on Arrival: <2 Parameter Schedule: Copper Nitric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Nickel Nitric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Nickel - Solid Nitric Acid Chemicals in containers, lab Received on Ice pH on Arrival: <2 Parameter Schedule: Sodium Nitric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Sodium - Solid Nitric Acid Chemicals in containers, lab Received on Ice pH on Arrival: <2 Parameter Schedule: Nitric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Potassium Nitric Acid Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 13 pH on Arrival: <2 Parameter Schedule: Potassium - Solid Nitric Acid Chemicals in containers, lab Received on Ice pH on Arrival: <2 Parameter Schedule: Nitric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Received on Ice Chemicals in containers, lab Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: pH Received on Ice pH on Arrival: <2 Parameter Schedule: Nitrate/Nitrite Sulfuric Acid Chemicals in containers, lab Received on Ice pH on Arrival: <2 Parameter Schedule: Nitrate/Nitrite - Solids Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Phosphate, Total as P Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: TKN Sulfuric Acid Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 13 pH on Arrival: <2 Parameter Schedule: Ammonia Nitrogen Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Received on Ice Parameter Schedule: Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 13 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 6 of 13 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 7 of 13 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 8 of 13 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 9 of 13 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 10 of 13 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 11 of 13 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 12 of 13 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 13 of 13 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 blueridgelabslerloir©gma il.cam Client : Attention: Date Received: Report Date: Sample Date: BRL #: Lab Sample ID: Client Sample ID: Parameter City of Morganton P. O. Box 3448 Morganton, NC 28655 Ms. C. Benton 04-Jun-18 29-Jun-18 04-Jun-18 BRL-201 8-0386 LSID-2018-01620 Compost TCLP Hg by Cold Vapor AAS TCLP Extraction Metals Ag As Ba Cd Cr Pb Se Reported By: Result MQL * 0.002 extracted * 0.5 * 0.5 * 5 * 0.1 * 0.2 * 0.5 * 0.05 Unit Method mg/1 7470A 1994 SW-846-1311 mg/1 SW-846-6010 mg11 SW-846-6010 mg/I SW-846-6010 rng/l SW-846-6010 mg/1 SW-846-6010 mg/1 SW-846-6010 mg/l SW-846-6010 ohnson, D.R. Wessinger Analysis Analysis Time Date Analyst 6/8(2018 Summit Summit 6/11/2018 Summit 6/11/2018 Summit 6/11/2018 Summit 6/11/2018 Summit 6/11/2018 Summit 6/8/2018 Summit 6/8/2018 Summit * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 1 of 6 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 blueridgelabslenoir@gmail.corn Client : Attention: Date Received: Report Date: Sample Date: BRL #; Lab Sample ID: Client Sample ID: Parameter City of Morganton P. O. Box 3448 Morganton, NC 28655 Ms. C. Benton 04-Jun-18 29-Jun-18 04-Jun-18 BRL-2018-03 86 LSID-2018-01621 Compost TCLP TCLP Semi-VOC Extraction Cresols (Total) Dichlorobenzene. 1,4 Dinitrotoluenc, 2,4- Hexach loro-1,3-Butadiene Hexachlorobenzene Hexachloroethane Nitrobenzene Pentachlorophenol Pyridine Trichlorophenol, 2,4,5- Trichlorophenol, 2,4,6- Reported By: Result extracted * 4 * 0,08 0,04 * 0,016 * 0.04 0.08 0.08 * 0.2 * 0.2 * 0.2 * 0.25 MQL Unit Method S W-846-1311 mg/1 SW-846-8270 mg/1 SW-846-8270 mg/1 SW-846-8270 mg/1 SW-846-8270 mgfl SW-846-8270 mg/1 SW-846-8270 mg/1 SW-846-8270 mg/1 SW-846-8270 mg/1 SW-846-8270 mg/1 SW-846-8270 mg/1 SW-846-8270 nson, D.R. Wessinger Analysis Analysis Time Date Analyst Summit 6/14/2018 Summit 6/14/2018 Summit 6/14/2018 summit 6/14/2018 Summit 6/14!2018 Summit 6/14/2018 Summit 6/14/2018 Summit 6/ 1412018 Summit 6/14/2018 Summit 6:1412018 Summit 6/14/2018 Summit * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 2 of 6 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client : Attention: Date Received: Report Date: Sample Date: BRL #: Lab Sample ID: Client Sample ID: City of Morganton P. 0, Box 3448 Morganton, NC 28655 Ms. C. Benton 04-Jun-18 29-Jun-18 04-Jun-18 BRL-2018-0386 LSID-2018-01622 Compost TCLP • Parameter TCLP ZHE Volatiles Extraction Benzene Carbon Tetrachloride Chlorobenzene Chloroform Dichloroethane. Dichloroethene, MEK Tetrachloroethene Trichloroethene Vinyl Chloride Reported By: Result extracted MQL Unit Method SW-846-I 311 50 ug/1 SW846-8260 50 ug/1 SW846-8260 50 ug/l S W 846-8260 50 ug/l SW846-8260 50 ug/l SW846-8260 50 ug/1 SW846-8260 250 ug/1 SW846-8260 50 ug'1 SW846-8260 50 ug/1 SW846-8260 20 ugll SW846-8260 S 'or Johnson, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 3 of 6 Analysis Time Analysis Date Analyst Summit 6/11/2018 Summit 6/11/2018 Summit 6/1112018 Summit 6/11/2018 Summit 6/11/2018 Summit 6/11/2018 Summit 6/11 `2018 Summit 6111/2018 Summit 6/11/2018 Summit 6/11/2018 Summit Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client : Attention: Date Received: Report Date: Sample Date: BRL #: City of Morganton P. O. Box 3448 Morganton, NC 28655 Ms. C. Benton 04-Jun-18 29-Jun- i 8 04-Jun-18 BRL-2018-03 86 Lab Sample ID: LSID-2018-01623 Client Sample ID: Compost TCLP Parameter TCLP Semi-VOC Extraction 2,4,5-TP (Silvex) 2,4-D Chlordane Endrin Heptachlor Heptachlor Epoxide Lindane Methoxychlor Toxaphene Reported By: Result MQL extracted • 500 * 1000 * 20 • 2 * 2 * 2 • 2 * 2 * 40 Unit Method SW-846-1311 ug/1 SW-846-8080 ug/1 SW-846-8080 ug/1 SW-846-8080 ug/1 SW-846-8080 ug/I SW-846-8080 ug/I SW-846-8080 ug/I SW-846-8080 ug,il SW-846-8080 ug`l SW-846-8080 S � ohnson, Q.R. Wessinger Analysis Time Analysis Date Analyst Summit 6/15/2018 Summit 6/ 15/2018 Summit 6/12/2018 Summit 6/12/2018 Summit 6/12/2018 Summit 6/12/2018 Summit 6/12/2018 Summit 6/12/2018 Summit 6/12/2018 Summit Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 4 of 6 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client : City of Morganton P. O. Box 3448 Morganton, NC 28655 Attention: Ms. C. Benton Date 'Received: 04-Jun-18 Report Date: 29-Jun-18 Sample Date: 04-Jun-18 DRL #: BRL-2018-0386 Lab Sample ID: LSID-2018-01624 Client Sample ID: Compost TCLP Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Ignitability Not Ignitable 70 Deg. F. 1030 SW-846 11:02 6/5/201$ kcj Corrosivity as pH 6.7 0 1 su 9045C SW-8 10:15 6i5/2018 KCJ Reported By: hnson, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 5 of 6 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 blueridgelabsienoir@gmail.com Client Attention: Date Received: Report Date: Sample Date: BRL #: Lab Sample ID: Client Sample ID: Parameter Reactivity as CN Reactivity as Sulfide City of Morganton P. O. Box 3448 Morganton, NC 28655 Ms. C. Benton 04-Jun-18 29-Jun-18 04-Jun-18 BRL-201_ 8-03 8 6 LSID-2018-01625 Compost TCLP Result MQL * 1 * 5 Reported By: Unit Method rngfkg SW-846-7.3.3 mg/kg SW-846-7.3.3 Johnson, D.R. Wessinger Analysis Analysis Time Date Analyst 15:25 6/8/2018 KCJ 10:15 6/8/2018 KCJ * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 6 of 6 +urnm.i 1.m/n NrnGrn,>.'R'(hr 18866299 p n1alp p;tr/<1ur r4ro . aJ,__ Dale Reponedat2lam r-?:r„•3-4:/1/41 ?Ju,.5?-a4w Comport!. Blue Ridge Labs, Inc Ir; h.rrr hrry nnw,lrrrwA arm :Address 1' t1 Boe 2940 I claw :CC 28b4.5 Receiscd t1 n 2018 Pri€,i1 I . I6'0 1641 10, TCLP \Fetal. Anal>si',(SW 1311/6010) Client 110 Lab Mk Collected Analyse Rep I nit Result l nits %latris Method DF Regivl Run :lush.' 1620/162111622/1623 001 6r4/2018 TCLP Arsen,c!Ast ND mg,L Soxd EPA 6010 t 5 00 6/11/2018 KMS 0 1520/162111622/1623 001 6/41201e TCLP BBrn,,mi6a1 5 00 N0 mg/L Sold EPA 6010 1 100 8/11201.6 KMS 0 162011621/1622r1623 001 6/4/2018 TCLP Caami.enICal 0 100 ND myi Sold EPA 6010 1 1 00 6/112018 KMS 0 1620'162111622.11623 001 6/4f2016 TCLP Chromalr><i Co 0 200 ND mg/L Sold EPA 6010 1 5 00 601 /2018 KMS 0 172U11621/lb2111623 g111 04/2U€6 rCLP Le11a1Pb; U 5UL1 N1J mg/L Said EPAb01U 1 50Li 601/2018 KMS 0 15201162171622r'523 001 6'4'2018 TCLP Selan..:rn{Se( 0 0500 NO mgrL Sciia EPA 0010 1 00 6.111201e KMS 0 1620(1621r1822/1623 001 6/4f2018 TCLP Soven Ag€ 0 500 ND mg/L Swig EPA 5010 1 5 00 6/11/2018 KM$ 0 TCLN Mercury lnaty six 1S11 1311!747I4 Client 1110 Lab 1D6 t'allr.•cted lnxhte R1p Lon Result Llnits Nix tris Method OE Re I.s1 Run lnalrst 1620/1621/1622/1623 001 $/412016 TCLP Merc:rri :'16t200 NO mg/L Sold EPA 7470 A 1 u 200 5/8/21)1 E EAM T('LI' Pesticides %liaEy.is Itill IS11180811 Client 11)a Lab 11)6 Collected _%n/ll le Rep Lntt Result 1 nils 70,talris Nletliod DF Rcal.I Run :>.nalyst 16200621/162211623001 6/4/2018 Cnlardane totem 200 N0 Irg'L Soid EPA80618 2 30.0 6/12/2018 JBN 1620/1621(1622r1623 001 6/4/2019 Toeapherle r 400 ND 1,g/1_ Soid EPA80518 2 500 611212018 JBN 1620/1621/162211623 001 6'44.'018 Cr. d1 r.. 2 00 NC a /L Sold EPA 8081E 2 20 0 6/12/2018 JON 1620/1621062201623001 614i2018 ymnlne-Bi1C • 200 /40 pg/L 6061 EPA80810 2 400 60212018 JBN 16200621115220623 001 614/2019 Hepta0n0r ' 2 CO NO 411. So4o EPA 8061 B 2 6.00 002/2018 JBN 162011621062.11623 001 514/2171e lierachu eP0ae • 2 00 NO pg:L So1,a EPA 80818 2 8 00 81122018 JBN 1620/1621(1622r1623 001 6E4,2015 Me1lu.ycnio? . Z CO N4 141. Solo EPA B0618 2 10000 6/12/2018 JBN 1620/1621i16221523 001 6(4r2015 Surf TCMX 10-119 56 1 %Ret 50€0 EPA 8061E 2 6/12/2418 JON 1620./18211162211623 001 5.4/2018 Surr 008 10-119 75 4 %Roc Sold EPA 60818 2 8(12/2016 JBN TCI.1' IIcrbicides.Inalysis OM 1311181511 Client 1D# Lab ID# Collected Analyte Rep I_m1 I1tsblt I. nits Matrix Method DV RegLv1 Run Analyst 162006210622 1623 001 6/4/2018 2 4-0 15200521(162211623 001 5/4/20€5 2 4 6-TP 1520/ 1621(1622'1623 001 614/2016 Sri.r DCAA ND ulyL Sato EPA 8151 A 9. 10000 6/1512018 JBN 511 NLi iv(. Spud EPA 8151 A 1 l rim 5/16(201R .ION ,:3-140 32 g %Rai So14 EPA 815! A 5,15/2018 .BN Page 5 of 15 ( ltt•Ill 1117+ 4..11100! 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(SIC 1311:82"f1) 1st11 IUD r nlleeu•,l Anal) ov Rep i nu Recslll 1 nil,. \Eatrit \IeIRud DF Rrg!_01 Riin Ann1rs1 1620116211162211623 001 1820116211162211623 061 1620/152111622,1623 001 1620/1621 /18220623 001 1620(162171b2211h4/ {1,)1 15201102111622' 14423 401 18201162111622+1623 001 1620/16211162211623 001 .9201152111522+'623 001 162011621/162211623 001 •5201462...922rE,21 ^•_ 1620'16211162211623 041 162£Y162111622/1823 001 1620/16211162211623 001 1620f162111622/1623 001 1620115211162271623 001 1620n521n82211623 001 4/2018 6/412019 6472015 6141701P 614rcu1rl 514.2C 19 6147201E 6f4/201a 64/918 6:412919 914 2319 6+4/2018 61412018 614r2419 6,412018 6/4(2018 614i2016 t 4•DCcniorobenzene r 0 0800 ND mg/L 2 4 5-Trp,iprophen0, • 0 209 ND mg/L 2.4 6-Tr creczop?ter,o: • 0 209 ND nil 24-0rMrornl,Imre 4 00400 ND mg./1 C:re6046 r01e1 • 4 ( 1 NU !ng+t I iecatll0-e.` 3- • C.2160 ND mg.L ra.la:lere 1-le,eari4cDue,4y�,e • 0 0400 ND mg/L Hexachlotoelrane 1 0 0800 ND mg1L NJr:0enaero • 0 0800 ND m^y1L Pentachi4:ppherlpl• 0200 ND rr:g/L P.rr.�nn, • 20,7 ND Surr 2.F ',crap:nem), 10.109 12 a %Re: Sur, Prtenoio6 10-109 15 5 %Ret $urr N.ttooenrene- 16-120 20 7 1 Re: 05 So! 2 4 6- Tn0rorngpne n) Sur 2- 22-117 20 1 %Rec FIi eooioheny: Surr p-Terphenyr• 34-116 65 3 %Re: ,J14 10-12C 23 2 %Ret Sow Bond Solxf Sclut S000 Sotto Solru SO4b 6n1:a Solid Sa10 SO4 So,0 Sa10 Solid So+a EPA 8270 D EPA 8270 D EPA 6270 ❑ EPA 8270 D EPA 42; V D EPA 82713 D EPA 8270 0 EPA 8270 EPA 82?0 EPA 8270 ❑ EPn 52"' D EPA 8270 ❑ EPA 8270 0 EPA 5270 D EPA 8270 D EPA 8270 D EPA 6270 2 7 50 6/14/2015 BJH 2 400 6114(2016 BJH 2 2 00 6/14r2018 BJH 2 0170 8714/201A BJH 200 6+14/2915 BJH 2 0500 &1412018 BJH 2 0 130 6,1412018 BJH 2 3 00 6/14/20113 BJH 2 2 00 6/14(2018 BJH 2 100 6/14.2018 BJH 2 590 6,14,2918 BJH 6114/2018 BJH 2 6114/2018 BJH 2 6114/2018 BJH 2 6114/2018 BJH 2 611412018 BJH 2 6114,2018 BJH Page 7 of 15 -T ' F_ .lxrxrurr fm,r.rvwenrxl /r< drw.+r.Vn•., !ra 321r. AM Sr 11141 ..p, :SF-a4 tiv IlrF,n. 01I17, .1.1 .rrfr( r, vn a (1 18ne6299 Dine Repotted 8121I2n18 Cowan!, blue Ridge Labs. Inc Address P tl Bo20411 Lenoir NC 281.1 Rece.Red h112018 Prows -It: 4011 11,01 T(-i-P kna[ssis <•iient 1110 I ub 1I 1 Oakwood •lnnlrte Rep 1.m1 11 • .Ilt I nil% \Writ Nlethnd [1 Regl.N1 Run Analp,t 1620(16I111622/1623 001 614r1018 1 1•D+chloraethene • 500 ND ug/L Sally EPA 8260 8 10 700 611112018 CT8 1620r1621/1622/1623 001 674/2015 1 2-Dlcnloroelrane . 500 ND /,g/L Sofa EPA 8260 8 10 500 6111/2018 CTB 16201162111622/1623 001 8/40018 MEK . 250 ND µ9/1. Sand EPA 8260 6 10 200000 61112018 CIE 762011621/162211021 001 6.412013 13e1/zer+e • SC• 5 645 1,0. 5c1d EPA 82200 8 10 550 611//2018 CT8 1620/1621r1622/1623 001 614/2014 Cwboel /elrae IorRle . .50.0 ND usyL Sr u13 EPA 8260 8 10 500 6111120i8 CIS 1620r1621/162211623 001 6/42018 Chaoroterzene . 50 a ND 411_ 5014 EPA 8260 8 10 100000 6/112018 CIE 16201162111622/1623 OO1 6r412018 Chlorntanll . 5G 7 ND u1YL 5044 EPA 8260 8 10 6000 6'11/2018 CTB 16200621/1622/1623001 6142D18 Telteehiaroelr1ere, 503 ND regal Soo EPA 8260B 10 700 6/11/2018 CIE 16200621/1522/1623001 6/4(2G15 7r411101oel0en., 54,: ND u94L 5011d EPA 82608 10 500 61112018 CT8 1620/1621 /1622/1623 00$ 6/4/2018 V'nyl()Ibr,Ot• 200 ND Ngll. Sal+d EPA82608 10 200 6/11,2018 CTE 1620r1021/1622.1623001 614/2018 S,.rr41 70-130 959 %Rec 50)>0 EPA 8260a 10 6111/2018 CTB Brun-auarmerver•.e 1620/1821/1622/1621001 61412018 Surr 70-130 105 %Rec. Solq EPA 82608 10 6(11l2016 CT8 D Ibromdfluprornglhyve 1820/1521/1622n623 001 6/ef2019 gun. Tnkwr*-P 7n.I 5 en 5 ar,Rec Solo FPA 62608 10 6/112018 CT8 Page 6 of 15 'rrIRRr111 Jfr'Ir.ylmifllil it. lllx.+<+21. 1.;: J$l it fl!1! t'xxuh.y;.l kWh, (7h. 44::? Fi N;n,n; ma, Analytical Report +::+l.s+rl%daltt:l Lti ()= 18060991 Late Reported 6/10/20I8 CLIENT: Blue Ridge Labs. [nc Project: 1601 i.ub I1): L804,119'7I-tHr1 ['Beni Sample IA 1681 Cullectlon Dale: f, h'_ !I8 Nlatt'ix: DitiESS':\Ti: :1ual{!es Result POE. ()DWI I. nits DF Date Anahzed METALS (EPA 200.71 8omnt8! Titanium! Tn 0 245 0 WO mglL 0 954 0 0200 mpiL E200.7 E200,7 Analyst KMS 6/19/2018 2 12 20 PM 6/1912018 212 20 PM IslEtnal I'ag: 4 of 7 1 Blue Ridge Labs, Inc. P.O. Box 2940 Lenoir, NC 28645 Telephone (528) 728-0149 Fax (828) 728-0131 CI-IAIN OF CUSTODY RECORD NPDS Reporting Groundwater Sanitary Landfill Hazardous Waste _ industrial or QC Non State Reporting *le icree— Report To: —L ,1 e •M , ki.4IC�(/5 Bill To: JJ Project Name: AO-) saiebt Jap20/S PO Number Sample ID Sample Type Date • •--- Time & Temp Sulfide HR:MM °C Check YES NO Sulfide Present/ Removed ftesid. Chlor. Field Check De- chlorination r-rCJC! VdLlVGS pH LIEU Resid Chlor P or A ',A MU;n Temp °C Sampler Initials Requested Analysis 'Ll� YES NO YES NO YES NO kl Jj ��/f CJA A'1d d Jr W / /S l� r•�/ 'b ✓ ✓ ►/ ,y� 7�: / %�C�L' J/ COirpSl fjt/il`l/ Page of Rev. 11/02/10 Upon submission of samples, buyer agrees that invoices are due at the time work is completed. Open accounts are due 20 days following the invoice date. A finance charge of 1.5% per month will be imposed on all past -due accounts When relinquishing sample to Blue Ridge Labs (BRL), buyer authorizes BRL to perform only the analysis indicated above and also agrees to pay collection and attorneys fees if the account becomes deiinquent. BRL reserves the right to deny all QA/QC documentation for any work where payment has not been made. Without payment, BRL owns all the documentation and reserves the right to notify any government agency (local, state, or federal) that there will be no QA/QC support for the data. BRL also does not guarantee that any work submitted will be accepted by any regulatory authority; therefore, it is the clients' responsibility to verify the required tests with the appropriate regulatory agency. All work for state reporting is under the jurisdiction of the Laboratory Section of NC DENR.