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HomeMy WebLinkAboutWI0400164_Monitoring (Report)_20130919 (2)W1 U 'f00 /C� September 16, 2013 Ms. Sharon Cihak Guilford County Environmental Health 400 West Market Street, Suite 300 Greensboro, North Carolina 27405 RE: Active Remedial System Monitoring Report: January Through June 2013 Former BP Site No. 013631 TravelCenters of America 1101 NC Highway 61 Whitsett, Guilford County, North Carolina NCDENR Incident Nos. 6113 (BP), 20054 (TA), and 30318 (TA) NCDENR Risk Ranking: High URS Project No. 38436751 Dear Ms. Cihak: On behalf of BP Products of North America, Inc. (BP), URS Corporation — North Carolina (URS) is pleased to submit one copy of the Active Remedial System Monitoring Report: January Through June 2013 for the above referenced Site. The report provides a summary of groundwater quality data collected on May 21 and 22, 2013. If you have any questions regarding this submittal, please call me at (919) 461-1423. Sincerely, URS Corporation — North Carolina l d Margaret Ness, PG Project Manager cc: Greg Frisch, BP (ENFOS) Project File (electronic) David L. Goodrich, (NCDENR-Aquifer Protection Section) (Hard Copy) RECEIVEDIDENR DWQ SAP 19 2013 Aquifer Protecdon Sect on URS Corporation — North Carolina 1600 Perimeter Park Drive, Suite 400 Morrisville, NC 27560 Tel: 919-461-1 100 Fax: 919-46-1415 ACTIVE REMEDIAL SYSTEM MONITORING REPORT JANUARY THROUGH JUNE 2013 FORMER BP SITE NO.01363 & TRAVELCENTERS OF AMERICA 1101 NC HIGHWAY 61 WHITSETT, GUILFORD COUNTY, NC NCDENR INCIDENT NOS. 6113 (BP), 20054 (TA), AND 30318 (TA) NCDENR RISK CLASSIFICATION: HIGH NCDENR LAND USE: RESIDENTIAL Prepared for Atlantic Richfield Company (ARCC) a BP Products of North America Inc. affiliated company 4850 E. 49th Street MBC-3 Room 155C Cuyahoga Heights, CH 44125 September 12, 2013 URS Corporation — North Carolina 1640 Perimeter Park Drive, Suite 400 Morrisville, North Carolina 27560 Tel. (919)461-1100 Fax. (919) 461-1415 UR5 Project No. 38436751 hp TITLE PACE ACTIVE REMEDIAL SYSTEM MONITORING REPORT JANUARY THROUGH JUNE 2013 FORMER BP SITE NO.01363 & TRAVELCENTERS OF AMERICA 1101 NC HIGHWAY 61 WHITSETT, GUILFORD COUNTY, NC Report Date: September 12, 2013 Responsible Party (RP): Atlantic Richfield Company (ARCO) a BP Products of North America Inc. affiliated company 4850 E. 49th Street MBC-3 Room 155C Cuyahoga Heights, OH 44125 Attn: Greg Frisch (216) 271-8740 F:1 TravelCenters of America 24601 Center Ridge Road Westlake, OH 44145 Attn, Rob Porges (440) 808-7368 Current Land Owner: TravelCenters of America 24601 Center Ridge Rd., Suite 200 Westlake, Ohio 44145-5634 RP Consultant: URS Corporation — North Carolina 1600 Perimeter Park Drive, Suite 400 Morrisville, North Carolina 27560 (919) 461-1100 Site Risk Classification: High Land Use Classification: Residential Release Information: Subsurface gasoline release from the automobile dispenser area discovered in 1990 Release Location: N36°3.808' Latitude: W78° 33.892' Longitude umPi1BPIPrujms%NCW1. 3, HN. L4jftoC. M1CZi.11 [kRrerahfeAlsnunn la June 11113 GW Rrpo;iW41M3 ARSN1 Jan -Jun 2013.dnc it TITLE PAGE This Report was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my thorough inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, az.dte. Margaret M. Ness, PG Project Manager URS Corporation — North Carolina V CA Naia�e�'V/ ri r•'t,�G 01 1 = SEA L 1 2028 a T V ;w7WI Date P:I0"MJeC"CWI363. MN, 2013 r. W Re F"P 111363 ARSNi Jan -Jun :1113.doc iii TABLE OF CONTENTS Section1 Introduction.....................................................................................................................1-1 Section2 Background.....................................................................................................................2-1 2.1 Facility Location and Description...... .................... 2.2 Site History .............................--....................................................... 2-1 2.3 Potable Well Treatment System Installations..................................I....... 2-3 2.4 Local hydrogeologic setting..................................................................... 2-3 Section 3 Sampling and Analysis Procedures..............................................................................3-1 3.1 Groundwater Sampling..............................................._............................ 3-1 3.2 Water Supply Well Sampling ................................................... .............. 3-1 3.3 Remedial System Sampling..................................................................... 3-2 Section 4 Sampling and Analysis Results....................................................................................4-1 4.1 Gauging Results...................................................................................... 4-I 4.2 Groundwater Analytical Results.............................................................. 4-1 4.3 Water Supply Well Analytical Results .................................................... 4-2 ........................... Section5 Remedial System Performance.....................................................................................5-1 Section 6 Risk Classification..........................................................................................................6-1 ' Section 7 Well Integrity Inspection................................................................................................M Section8 Conclusions....................................................................................................................8-1 Section9 Recommendations..........................................................................................................9-1 Section10 References....................................................................................................................10-1 MPi18KVmjrrts04M1361 S1N. W hitwnt NC0,11 De ivembksVanunq to Jnm 2013 GW It"wrt Fi 01X3 ARSM Jan -Jun 201Idnc iv TABLE OF CONTENTS TABLES Table 1 Well Construction Information Table 2 Groundwater Elevation Data (May 21, 2013) Table 3 Groundwater Field Parameters (May 21 and 22, 2013) Table 4 Summary of Groundwater Results Compared to NC 2L Groundwater Quality Standards Table 5A 1301 Piney Grove Treatment System Performance Compared to NC 2L Groundwater Quality Standards Table 5B 1205 N Hwy 61 Treatment System Performance Compared to NC 2L Groundwater Quality Standards Table 6 Potable Well Treatment System Operational Data Table 7 Sample Plan FIGURES Figure 1 Location Map Figure 2 Site Map Figure 3 Vicinity Map Figure 4 Groundwater Contour Map, May 21, 2013 Figure 5 Benzene Concentrations in Groundwater May 2013 Figure 6 IPE Concentrations in Groundwater May 2013 Figure 7 MTBE Concentrations in Groundwater May 2013 Figure 8 Naphthalene Concentrations in Groundwater May 2013 Figure 9 Total Xylenes Concentrations in Groundwater May 2013 Figure 10 Time Trend Graph of Analytical Results and Groundwater Elevations for MW-2R Figure 11 Time Trend Graph of Analytical Results and Groundwater Elevations for MW-3 APPENDICES Appendix Al Historical Groundwater Elevation Data (BP Incident No. 6113) Appendix A2 Historical Groundwater Elevation Data (TA Incident No. 20054) Appendix A3 Historical Groundwater Elevation Data (TA Incident No. 30318) Appendix B Laboratory Reports and Chains of Custody Appendix C1 Historical Summary of Groundwater Analytical Results (BP Incident No. 6113) Appendix C2 Historical Summary of Groundwater Analytical Results — VOCsISVOCs (TA incident No. 20054) Appendix C3 Historical Summary of Groundwater Analytical Results -- VPHIEPH (TA incident No. 20054) Appendix C4 Historical Summary of Groundwater Analytical Results (TA Incident No. 30318) TIMP:16PTmjrcLANCH11361 MN. Whir.+ M NX- 5.9 PeflvembInV anon" to June 2013 GW RM"t1\3P 411363 ARSN Jan•Jan 210.40c v TABLE OF CONTENTS Appendix D Receptor Survey Appendix E Well Abandonment Records UMP:IBPWmjecLSN.NC1U1363. MN. WbItw t, NMI) Uelivemblesllanumn to 3une 2013 GW Repu&BP 1)1363 AKSM Jon -Jan 2013.doe V1 SECTIONONE Introduction URS Corporation — North Carolina (URS) presents this report on behalf of Atlantic Richfield Company (ARCO), a BP Products of North America Inc. (13P) affiliated company, for the TravelCenters of America (TA) site located atl 101 NC Highway 61 in Whitsett, North Carolina (Site - BP Site No. 1363, North Carolina Department of Environment and Natural Resources (NCDENR) Incident No. 6113). This report presents the point -of -entry (POE) remediation system operation and maintenance (O&M) activities conducted from January through June 2013 and the results of Site groundwater sampling on May 21 and 22, 2013. These activities were conducted in accordance with the Revised Corrective Action Plan (CAP), prepared by Piedmont Geologic, P.C. (Piedmont, 2001 b) and Incident No. 20054 as a result of a release discovered in 1990. Due to community releases and NCDENR trust fund issues, TA entered into an agreement with BP, to address issues for TA's active incident numbers 20054 and 30318. This report presents the results of groundwater samples collected on May 21 and 22, 2013 from the three incident numbers. Potable water supply wells are located within 1,500 feet of the Site. This report also summarizes the carbon treatment systems installed to treat methyl tert-butyl ether (MTBE) that was detected in the potable wells located at 1301 Piney Grove Road and 1205 NC Highway 61 South and the results of groundwater samples collected on May 21, 2013. The Site is designated as NCDENR Incident Number 6113, 20054, and 30318, with a current risk classification of High. I= PABPTrvjn1s1-NU411363, ►1%'. Whitwit N"A Ddirmhksllanuary to June 1013 G W ReparftBP 01363 AF-SN Jan -Jun 20116x 1 -1 SECTIONTWO Backurnund 2.1 FACILITY LOCATION AND DESCRIPTION The Site is located at 1101 NC Highway 61 in Whitsett, Guilford County, North Carolina (Figure 1), at the northeastern corner of the intersection of NC Highway 61 and Interstates 85140. The Site property comprises approximately 28 acres and contains the following commercial establishments: ■ TA facility, including truck diesel dispenser islands, BP -branded automobile gasoline dispenser islands, restaurant/service center, truck scales, and truck maintenance garage; • Daystop Motel; • Popeye's Restaurant; and • Burger King Restaurant. Open areas surrounding the commercial establishments are mostly paved with concrete or asphalt and are used for truck and automobile parking. Landscaped and other grassy areas are located along the Site perimeter (Figure 2), The Site topography slopes downward from NC Highway 61 toward the southeast. A storm water retention basin and sanitary sewer lift station are located at the southeastern corner of the Site. 2.2 SITE HISTORY The Site was operated by BP as a TA -branded truck stop from 1988 until 1993. TA was a wholly -owned subsidiary of BP until December 1993, at which time TA and BP became separate entities. The Site is currently owned and operated by TA. BP A petroleum release from a former automobile gasoline dispenser was discovered in 1990 and was assigned NCDENR Incident No. 6113. A Comprehensive Site Assessment (CSA) was prepared by Matrix Technologies, Inc. (Matrix, 1993) to document assessment activities performed at the Site from 1990 to 1993. The Site was originally assigned a priority ranking of 85E by NCDENR, However, a potable water supply well was discovered in the Site vicinity around 1997. In an October 28, 1997 letter to BP, NCDENR reclassified the Site as 85B, a high risk classification. Following the completion of additional assessment activities in 1998 and 1999, a CSA report addendum, (CRA Services, 1999) was submitted to NCDENR. A September 26, 2000 letter from NCDENR to BP granted acceptance of the CSA and CSA Addendum, and requested completion of a CAP. The initial CAP, dated February 14, 2001 (Piedmont, 2001), proposed soil vapor extraction to remediate the soils in the automobile dispenser area and monitored natural attenuation to remediate the groundwater. In an April 2, 2001 letter to BP, NCDENR rejected the natural attenuation approach and requested submittal of a revised CAP. UmF;\BRPmjecIASC-VI1A3, MN. WWisetL NCl_i.ti Deli �vmbksllonumry to hme 2013 GW Rcporl%P01363 ARSM11 Jan -Jun 2913.dec 2-1 SECTICNTWO Background A pilot test of combined soil vapor extraction and air sparging was conducted in May 2001 and a dual -phase vapor extraction (DPVE) pilot test was conducted in June 2001, Batted on the results of pilot testing, DPVE was selected as the remediation technology for the Site and the Revised Corrective Action Plan was submitted by Piedmont on July 15, 2001. The DPVE system was installed between April and June 2002. The DPVE system was constructed and assembled by Product Recovery Management (PRM) of North Carolina. An oil -sealed liquid ring pump extracts water and air from three recovery wells (DP-1 through DP-3). The locations of these recovery points are shown on Figure 2. The recovered liquid and vapor pass through an air/moisture separator. The vapor passes through a particulate filter and then through the liquid ring pump before it is discharged to the atmosphere. The liquid is contained in the moisture separator until the high level float switch activates a transfer pump to move the fluid into the oil/water separator, where the water is separated from any LNAPL that may be present. When the water level in the oil/water separator is high enough to activate a high-level float switch, another transfer pump moves the water through a low -profile air stripper, which removes approximately 98% of the volatile organics in the water. After treatment of the water by the air stripper, it passes through a totalizing flow meter prior to being discharged to the City of Burlington Publicly Owned Treatment Works (POTW). The treated groundwater is discharged under permit number G0026, issued on December 8, 2008. The system start-up occurred on June 28, 2002. After several years of operation, asymptotic levels were reached and the treatment system was shut down in 2012. Remedial measures to advance the Site toward closure are currently being evaluated. TA A diesel fuel release was discovered in the current underground storage tank (UST) area in May 1999 through observations of a light non -aqueous phase liquid (LNAPL) sheen in stormwater originating from the UST area. An investigation of the release indicated that the source was broken seals in the UST drop tubes. This release was assigned NCDENR Incident No. 20054. UST system repairs and initial LNAPL abatement activities were conducted through the remainder of 1999, resulting in the recovery of a reported 13,212 gallons of diesel fuel from the UST pit. Approximately 300 tons of soils were removed from the UST area during the UST repair activities. Petroleum impacted soil was discovered during piping and dispenser upgrades in April 2006 and approximately 102 tons of hydrocarbon impacted soil were removed. NCDENR assigned Incident No. 30318 to this release. At the time of discovery, no active leak was identified and the source is likely from former fuel dispensing operations. A minor amount of LNAPL was reported in March 2009, but has not been detected since. The locations of the Site wells are shown on Figure 2. Monitoring well construction details are presented on Table 1. ImF:MV mjectalNC01363, MN. Wbiwo, N055.0 Dell- mblcAJanuary to,]une 21113 CHRepo rVSP 411363 ARSM Ina -Jun 1013.doe 2-2 SECTICNTWO Backuraund 2.3 POTABLE WELL TREATMENT SYSTEM INSTALLATIONS In a letter dated March 7, 2006, NCDENR requested that BP include the potable well located at 1301 Piney Grove Road in the sampling program due to the presence of MTBE in the water supply well sample. An additional potable well, located at 1205 NC Highway 61 South, was identified by BP and was included in the sampling program. Both wells are south of the Site as shown on Figure 3. On March 5, 2008, POE systems were installed to treat water pumped from wells located at 1301 Piney Grove Road and 1205 NC Highway 61 South. The Piney Grove well is also referred to as the Clapp's Chapel well and services both 1301 Piney Grove Road (a residence) and 1305 Piney Grove Road (Clapp's Chapel). The POE systems were 'installed by Carbonair Environmental Systems, Inc. (Carbonair), and each include two 12x52-inch Granular Activated Carbon (GAC) vessels, one UV light treatment unit, dual five micron filters (one before carbon treatment and one after carbon treatment), one heater unit, and one totalizing meter. Each system is housed in a small wooden shed. 2.4 LOCAL HYDROGEOLOGIC SETTING The Site is located within the Piedmont physiographic province. Bedrock in the Whitsett, North Carolina area is mapped within the Carolina Slate Belt lithologic division of the Piedmont, which consists of metamorphosed volcanic and sedimentary rocks intruded by igneous plutons and dikes. According to the Geologic Map of Region G. North Carolina (Carpenter, 1982), bedrock beneath the Site consists of diorite that is part of a plutonic complex in the Whitsett/Elon College area. Bedrock was encountered in Site borings at reported depths ranging from approximately 10 to 20 feet below land surface (ft bls). Saprolite, described as orange -reddish -brown micaceous silt and clay, overlies the bedrock. Groundwater in the Piedmont province occurs in the overburden under unconfined (i.e., water table) conditions, and in the underlying bedrock under both unconfined and confined conditions. Groundwater in the overburden occurs within pore spaces of the unconsolidated medium. Due to the typically fine-grained nature of Saprolite, the formation normally possesses a relatively low permeability and is not usually utilized for groundwater production. The overburden is recharged by the infiltration of precipitation where the formation is exposed and acts as a storage medium for groundwater that is slowly released to surface water bodies and the underlying bedrock. Groundwater in the underlying bedrock occurs along zones of secondary porosity, such as fractures, bedding planes, foliations, solution voids, etc. Most water supply wells in the Piedmont are completed in bedrock. IMPAB"mjm1sNC0136X MN. WWurtt. N(ISAI In lure 2APS3GW HeportW 101A3 ARSM Jan -Jun 2013dw 2-3 SECTIOMTHREE Sampling and Analysis Procedures 3.1 GROUNDWATER SAMPLING Prior to groundwater sampling, depth -to -water in each monitoring well was measured using an electronic oil/water interface probe, and wells to be sampled were purged of three volumes of groundwater or until dry with a new disposable polyethylene bailer and nylon line. Groundwater samples were collected for laboratory analysis from monitoring wells MW-2R, MW-3, MW-6, MW-8, MW-10, MW-11, MW-15, VE-1, VEW-1, RW-IR, USTMW-1, USTMW-2, USTMW-4, AGM-RW, CSAMW-1, CSAMW-2, CSAMW-3, CSAMW-4, and DDMW-2 during the May 21 and 22, 2013 sampling event. Field duplicates were collected from monitoring wells MW-2R and AGM-RW during the sampling event. Samples were collected from each well using a dedicated bailer, transferred to laboratory -supplied containers, and were placed in a cooler and packed in wet ice. Samples were shipped under chain -of -custody via overnight courier to Accutest Laboratories Southeast [Accutest] in Orlando, Florida. Well locations are shown on Figure 2. All groundwater samples were analyzed for the following (Incident No. 6113, 20054, and 30318): ■ Volatile organic compounds (VOCs) by Standard Method 6200B Groundwater samples collected from AGM-RW, CSAMW-1, CSAMW-2, CSAMW-3, CSAMW-4, DDMW-2, MW-10, MW-11, MW-15, USTMW-1, USTMW-2, and USTMW-4 were also analyzed for the following (Incident Nos. 20054 and 30318 only): ■ Semi -volatile organic compounds (SVOCs) by EPA 625 and ■ Volatile petroleum hydrocarbons (VPH) and extractable petroleum hydrocarbons (EPH) by the Massachusetts Department of Environmental Protection (MADEP) method. 3.2 WATER SUPPLY WELL SAMPLING Two water supply wells are located within 1,500 feet downgradient of the release area (Figure 3). One well serves 1205 NC Highway 61 South and the other well serves both 1301 and 1305 Piney Grove Road. Potable wells were purged for ten minutes prior to samples being collected on November 13, 2012. Influent samples (1301 Piney Grove Road -IN and 1205 NC Highway 61 South -IN) were collected prior to filtration, mid -stream samples (1301 Piney Grove Road -MID and 1205 NC Highway 61 South -MID) were collected after the first filter and before the second, and effluent samples (1301 Piney Grove Road-EFF and 1205 NC Highway 61 South- EFF) were collected after the third filter, prior to entering the residence. Samples were submitted to Accutest for laboratory analysis of VOCs by Standard Method 620013, as described above. P:IBF&rnjerlslNCV) 13i3.MN. WhkseM N".O DdinrahlesVanuan 10 June NO13 GW RepartW BIM3 ARSM Jan -Jun 21113.4ne 3-1 SECTIONTHREE sampling and Analysis Procedures 3.3 REMEDIAL SYSTEM SAMPLING Remedial system influent and effluent sampling activities were not conducted during the May 2013 event due to system shutdown. UMPABPft*jwwNCW1363, MN, Whitwtl, NCl5.0 Iktiveeahk%Van"" to June :Ui3 GH Repnrl\RP01363 ARSM lan•Jon 2013.dm 3-2 SECTIOMFOUR 4.1 GAUGING RESULTS Sampling and Analysis Results Depth -to -groundwater and groundwater elevation data for the May 2013 event are provided in Table 2 and historical groundwater elevations are presented in Appendices Al through A3. Water levels in the monitoring wells ranged from 2.23 (MW-10) to 15,23 (VE-1) feet below top of casing (ft btoc). Based on these measurements, groundwater flow is toward the southeast as shown on Figure 4. This direction of groundwater flow is consistent with previous groundwater gauging events. 4.2 GROUNDWATER ANALYTICAL RESULTS URS Corporation validated analytical results from the May 2013 groundwater monitoring event at the Site. The data review was modeled after the USEPA Contract Laboratory Program (CLP) National Functional Guideline (NFG).fbr Superfund Organic Methods Data Review (EPA, June 2008). Qualitative and quantitative limitations associated with the analytical results were determined based on the results of specific quality control (QC) criteria. Accuracy was determined from the review of spike recoveries. Precision was based on the evaluation of laboratory and field duplicate results. Representativeness was evaluated from the review of holding times and blank data. Sample results have been qualified based on the results of the data review process. Qualified data are valid and usable for their intended purpose. Laboratory analytical reports and chain of custody documents are provided in Appendix B. A summary of field measurements, including pH, specific conductance, and temperature is provided in Table 3_ The May 2013 analytical results from the groundwater samples are Compared to the 15A NCAC 02L .0202 Groundwater Quality (NC 2L) Standards in Table 4. A historical summary of groundwater analytical results is provided as Appendices C1 through C4. Concentrations of benzene. isopropyl ether (IPE), MTBE, total xylenes, ethylbenzene, and/or naphthalene were above their respective NC 2L standards in eight (8) of the 19 monitoring wells sampled in May 2013. Concentrations of bis(2-Ethylhexyl)phthalate, I-Methyinapthalene, 2-Methylnapthalene, and/or naphthalene were above their respective NC 2L Standards in five (5) of the twelve (12) monitoring wells sampled for SVOCs. Aliphatics C9-C18 were detected above NC 2L standards in monitoring wells AGM-RW, DDMW-2, USTMW-1, USTMW-2, and USTMW-4. Aliphatics C9-C22 were detected above NC 2L in AGM-RW, CSAMW-1, DDMW-2, MW-10, USTMW-1, USTMW-2, and USTMW-4. Benzene, IPE, MTBE, naphthalene, and total xylenes isoconcentration maps from the May 2013 sampling event are presented as Figures 5 through 9, respectively. Hydrographs of dissolved constituents of concern (COC) concentrations and depth -to -water versus time for monitoring wells MW-2R and MW-3 are provided as Figures 10 and 11, respectively. CDC concentrations in both wells have decreased overall; however, some analytes (naphthalene in MW-3 as well as toluene and MTBE in MW-2R) have slightly increased since the previous sampling event. i= P:I Trojeru4YCW1363, MN, WAiLwLt, NCZ O Ikllrenb1m\jsnm" to ]une 2013 GM' 6epnri1F1P411343 ARSM JaPiAun M?.da 4-1 SECTIONFOUR Sampling and Analysis Results 4.3 WATER SUPPLY WELL ANALYTICAL RESULTS Tables 5A and SS provide summaries of analytical results of the POE system sampling event (at 1301 Piney Grove Road and 1205 NC Highway 51 South) on May 21, 2013. The only analyte detected in either well alcove NC 21, Standards was 1,2-dichloroethane in the water supply well located at I301 Piney Grove Road. umPABF%PrujrrtAN(101343.14N. WhilWIL :V"A Odlverahksllwnunry to June 200 GW ReporADPRM3 ARSS1 Jai%-J,.k, 1013.d,W 4-7 SECTIQMFIVE Remedial System Perlermance The DPVE system was started on June 28, 2002, and operated until September 29, 2010. NCDENR approved the suspension of the DPVE based on previously presented data via email on October 15, 2010. System O&M site visits and summaries are currently suspended at the Site. However, based on discussions between HP, URS, and NCDENR in the fall of 2012, the system may be reactivated in 2013 due to increasing concentrations in MW-2R. URS is evaluating options for system upgrades or replacement. The POE systems O&M summaries are included in Table 6. Filters were checked at each POE system approximately once a month between January and June 2013, and were changed out at 1205 NC Highway 61 South and at 1301/1305 Piney Grove on January 21, February 28, March 28, April 26, and June 27, 2013. M= PAH"roje uLti[V[363. MN, %'Vhitwtt 1C%5.[I bcii%embkwUznuxry ro7uce 2013 G►4 REPUrI8P01363 IkRSM 1Bsi-!uu?013.dnr 5-1 SECTIONS IX Risk Classification The current risk classification for the Site is high due to the presence of two private potable water supply wells (Piedmont Geologic, February 2001 ) located down gradient within 1,500 feet of the Site, as shown in Appendix D. Seven potable wells are located within 1,000 feet of the Site, however they are all located up -gradient of the Site. The closest wells are located approximately 550 feet to the north (Appendix D, Parcels 14 and 11). As shown on Figures S through 9, the results of groundwater samples taken from upgradient monitoring wells are well below NC 2L Standards and are generally below method detection limits. The pumping of area water supply wells does not appear to influence groundwater flow beneath the Site. Current groundwater flow direction is toward the southeast and is consistent with previous groundwater gauging events. Therefore, the risk to these potential receptors north of the Site is expected to be low. An intermittent stream is located approximately 1,000 feet east of the Site. The risk of the release impacting the stream is estimated to be low based on the distance from the release and overall decreasing concentrations in groundwater observed in monitoring wells. The installation of POE systems has decreased the risk to potential receptors associated with potable wells at 1301 Piney Grove Road and 1205 NC Highway 61 South. Analysis of groundwater samples collected after treatment at 1301 Piney Grove Road and 1205 NC Hwy 61 South did exhibit an NC 2L Standard exceedence for 1,2-dichloroethane in the water supply well at 1301 Piney Grove Road. No other analytes were present above the NC 2L Standards prior to treatment in either supply well. tMP:16PIPen}ecls6tiC'Ip13Q3. 7Sti. ►5hilx4l, %C%5.I] QelivembleWanuary lu Jnne .III} GIV RepnrI�8I' Ill?63.AR%%I jxw. %Pn :111,I.drx 6-1 sECTICMSEVEN Well 101e0FRY Inspection Due to the heavy automobile and truck traffic at the Site, the integrity of many monitoring well pads and monitoring wells themselves have become compromised. Therefore, between July 9 and 11, 2013 the following activities occurred: The concrete pads and flush -mount protective covers were replaced on monitoring wells RW-1R, AGM-RW, VE-1, MW-6, MW-7, and MW-15, and Monitoring wells MW-Z, MW-4, SV-1, OW-lA, and DW-113 were properly abandoned with a bentonite grout mixture according to NCDENR regulations. SAEDACCQ of Fort Mill, South Carolina completed the monitoring well repairs and abandonments under the supervision of URS staff. The well abandonment records are presented as Appendix E. UMI110.11K.7,i14p1Pro}ects1NL101J63. \! \I hilscll. N('34 N[Ivembl1 Vmnuun in June :l11a GW RepnrjVBP00%3 AP'SM Jao-Jun 2[1OACK 7-1 SECTIONEIGHT Conclusions After reviewing the current and historical data, URS has reached the following conclusions: • Groundwater flow beneath the Site is toward the southeast, consistent with previous groundwater gauging events. • Treatment systems installed at 1301 Piney Grove Road and 1205 NC Highway 61 South are working effectively at eliminating contaminant concentrations. • Benzene, MTBE, and naphthalene remain at concentrations above the NC 2L standards in the area west of the dispenser island and extending to the southeast at the Site. • The farthest down -gradient onsite well. MW-8, has had no detectable concentrations of dissolved hydrocarbons with the exception of naphthalene in 2000. • The last exceedance of NC 2L Standards in monitoring well VE-1 was in October 2007 for naphthalene. ■ Monitoring well MW-6 has had no concentrations above NC 2L standards with the exception of naphthalene, last observed in March 1995. • Based on the above conclusions, constituents of concern appear to be contained at the Site. ■ The DPVE system was temporarily suspended on September 29, 2010, due to plume stabilization and low COC concentrations detected in air and groundwater. However. sampling events indicate increases in COCs, particularly benzene and MTBE. UnP:19PI mJo tsVNCM13G3. MN. Wh"L NCO.$ fkUvmbkWanuM to June 1013 C W Bepo3IWP p13lr3 AR.SH Jan -Jun 2013.d" 8-1 SECTION N I NE Recommendatlons Based on the above conclusions, URS recommends: + Continued semi-annual groundwater monitoring of Site wells in accordance with the Site CAPS and sampling plan presented as Table 7. + Reduction from quarterly to semi-annual sampling events for TA wells pertaining to NCDENR Incident No. 20054. BP and TA will be on the same sampling Schedule, thus eliminating the need for multiple mobilizations. Continued operation and maintenance and semi-annual groundwater monitoring (performance sampling) of the two active downgradient potable water supply wells located at 1301 Piney Grove Road and 1205 NC Highway 61 South. + On -site system reactivation or remedial alternatives should be implemented moving forward. ■ Removal of ORC socks related to Incident No. 30318 in October 2013, prior to semi- annual groundwater sampling in November 2013. I= N:%U"mjmbANC1013f.3. M1% WhiLwu4 ti[-�,s.R DM%erWmVanuan m June 2013 GW Reput%BP141363.ARSM Jan. Jan 21,13.d" 9-1 SECTICNTEN References Carpenter, P.A., 1982, Geologic Map of Region G, North Carolina; North Carolina Department of Natural Resources and Community Development, Division of Land Uses, Geological Survey Section, Regional Geology Series 2. CRA Services, 1999, Comprehensive Site Assessment Report Addendum, June 18, 1999, Matrix Technologies, Inc., I993, Comprehensive Site Assessment, November 15, 1993. Piedmont Geologic, P.C., 2001 Corrective Action Plan, February 14, 200I . Piedmont Geologic, P.C., 2001 B, Revised Corrective Action Plan, July 15, 2001. US EPA, 2008, National Functional Guidelines, for Superfund Organic Methods Data Review, US EPA, June 2008. IJRSP:V3P1Prnjcr�slti[1O1363,.y H'ihiucli. \[15.0 QelivrraidesUrnu�nto June 7A113 GW RepnrtWA1363 ARSdS Ina,tun lUl3AW 1 V' 1 TABLES TABLE 1 WELL CONSTRUCTION INFORMATION Former BP Site No. 01363 1101 NC Highway 61 Whitsett, North Carolina Well ID Date Completed Well Type Total Depth (ft bgs) Casing Diameter (in) Screen Interval (ft bgs) TOC Elevevation (ft) MW-2R 12i 11i00 111 25 4 10-215 93.92 M W-3 10/31 /90 If 26 4 11-26 91.13 MW-4 I W-11-40 14 a _5 4 5-t:+ +W:044 MW-6 6/17/91 11 25 4 5-25 91.28 MW-7 6/12/91 11 24 4 9-24 89.95 M W-8 W 17/91 11 23 4 8-23 87.92 MW-9 114100 11 15 2 10-15 90.43 MW-9❑ 115100 I11 50 2 40-50 90.84 MW-10 114100 11 15 2 10-15 91.36 MW-11 114100 11 14 2 10-14 94.21 MW-15 NR 11 NS 2 NS 92.24 RW-1R NR 11 20 2 10-20 92.17 VE-1 6/18/91 IL 40 2 33-40 90.98 VEW-1 NR 11 15 2 NS 96.29 4 1"224 9 i .0 i OW !A 5/16,01 II 2-y - 3-2 41::_' USTMW-1 NR NR 12.5 a NR NS USTMW-2 NR NR 12.4 4 NR NS USTMW-4 NR NR 6.7 4 NR NS AGM-RW NR II NS 4 NR 92.70 CSAMW-1 NR 11 31 2 16 - 31 94.18 CSAMW-2 NR 1I1 70 2 60 - 70 97.75 CSAMW-3 N R 11 25 2 10 - 25 98.39 CSAMW-4 NR 111 75 2 65 - 75 99.09 DDMW-2 NR NR 29.65 2 1518 - 29.65 97.78 NOTES: TOC = top of well casing ft bgs = feet below ground surface in = inches ft = feet NS = well not surveyed NR = no retard 4V 4 = Abandonded 7/9/13 P �BPTrojetu\NOO130, MN, Wuhan, N05 0 DdivereWes•Januan to June 20 13 GW ReportTablevTahle I Well fonm As I of I TABLE 2 GROUNDWATER ELEVATION DATA May 21, 2013 Former BP Site No. 01363 1101 NC Highway 61 Whitsett, North Carolina Well TOC . Depth to Depth to LNAPL Groundwater ID Elevation (ft) LNAPL (ft btoc) Water (ft btoc) Thickness (ft) Elevation tft) MW-2R 93.92 ND 11.87 ND 82.05 MW-3 91.13 N❑ 13.02 N❑ 78.11 MW4 100.00 ND NM N❑ NM MW-6 9L28 N❑ 8.28 N❑ 83.00 MW-8 87.92 ND 11.45 N❑ 76.47 RW-1R 92.17 ND 12.66 N❑ 79.51 VE-1 90,98 ND 15.23 ND 75.75 VEW-1 96.29 ND 7.92 N❑ 88.37 MW-10 91.36 ND 2.23 ND 89.13 MW-11 94,21 N❑ 4.34 ND K87 M W-15 92.24 N D 2.79 ND 89.45 USTMW-1 NS ND 3.97 ND NS USTMW-2 NS ND 3.49 ND NS USTMW-4 NS N❑ 3.52 N❑ NS AGM-RW 92,70 ND 3.72 ND 88.98 CSAMW-1 94.19 ND 7.33 N❑ 86.85 CSAMW-2 97.75 ND 12.47 ND 85.28 CSAMW-3 98.39 N❑ 6.91 ND 91.48 CSAMW4 99.09 N❑ 11.03 ND 88.06 DDMW-2 97.78 N❑ 5.69 ND 92.09 NOTES: TOC = top of well casing LNAPL = light non -aqueous phase liquid ft = feet ft btoc = feet below top of casing ND = not detected NM = not measured NS = well not surveyed P MPIPMma�N"1363, MN, Whi[ dt NC%5 0Wivcnhlesianuary so lunc _GI I GN' Rcpnn TAIce�Tahlr2 GW Elcvaunjcw_7.9 013 1 of I TABLE 3 GROUNDWATER FIELD PARAMETERS May 21 - 22, 2013 Former BP Site No. 01363 1101 NC Highway 61 Whitsett, North Carolina Well Number pH (STU) Temperature {°C) 5peciric Conductance (mS/em) D.0, (m Ili) Redox (mV MW-2R 6J2 21,73 0 776 3,21 -3.2 MW-3 6.81 21.39 0.702 2.00 -63.8 MW-6 7.05 20.57 0.251 4.04 51.2 M W -8 6.92 19.46 0.420 2.67 110.9 RW-1R 6.69 20.73 0.736 1.30 -79.0 VE-1 7.20 23.22 0.883 3.24 11.0 VEW-1 6.64 20.27 1.246 1.56 -16.8 MW-10 6.40 20,27 0.329 2.81 43.8 MW-11 6.75 20.57 0.593 1.83 -105.7 MW-15 6.38 22,49 0.354 2.99 93.6 LISTMW-1 6.93 22.03 0.547 1.23 109.3 USTMW-2 6.96 2332 0.668 1.44 -72 2 USTM W-1 6.82 23.19 1.214 1.02 -144, 9 AGM-RW 6.89 22.29 1.248 2.07 - M0.7 CSAMW-1 6.47 22.83 0.518 1.61 39.8 CSAMW-2 6.92 23.54 1.144 2.59 -44.2 CSAMW-3 7.76 21.35 1.063 >10 56.1 CSAMW4 7.61 22.47 0.572 2.14 -73A DDMW-2 6.44 22.32 0.699 2.22 0.5 Notes: STU = Standard units mg/L = Milligrams per Liter mSlcm = MilliSiemens per centimeter mv = Millivolts °C = Degrees Celsius P %BP1M0L1a6YC%01363. MN, %kN1Wt1. Nc'LS 0 DeGvnablei•Jamtuv to lwK 2013 GW Reporn�Tebles,Table 3 GW Puametvs dsx I of I Table 4 Summary of Groundwater Results Compared to NC 2L Groundwater Quality Standards Farmer Amoco Service Station No. 1363 1101 NC Hwy 61 Whitsett, Guilford County, NC Sample ID: AGM-RW ACM-RW CSAMW-01 CSAMW-02 CSAMW-03 CSAMW-04 DDMW-02 MW-02R MW-02R Collection Date: 5/22/2013 5/22/2013 5/22/2013 5/22/2013 5/22/2013 5/22/2013 5/22/2013 5/21/2013 5/21/2013 Parameters NC 21. I Units DUP 1 DUP(2) VOC l3ciuenc 1 µgli 4 J 4.2 ! r 0.1 r 0.1 UJ ¢ 0.1 UJ ¢ 0.1 0.58 5,230 J 6,540 J Toluene 600 l u. .I tl..; I < 0.1 < 0.1 UJ < 0.1 UJ < 0.1 < 0.1 297 271 E-:thylbenccnc 600 µgA 0.32 J 0.35 .I < 0.1 < 0.1 Uj r 0.1 Uj <0.1 r 0.1 -421 402 XvIcnes (Total) 500 µg/l < 0.22 < 0.22 ¢ 0.22 < 0.22 UJ < 0.22 UJ < 0.22 r 0.22 655 606 Bromodichlornmethane 0.6 < 0.l < 0.1 ¢ 0.1 < 0.1 UJ r 0.1 UJ r 0.1 r 0.1 1. 5 •= 5 Chloromethane 3 PgA 1.1 ! < 0.11 L1J r 0.11 0.14 J < 0.11 UJ < 0.11 r 0.11 < 5.4 < 5.4 ❑ihromochloromethane 0.4 * 1 r 0.1 < 0.1 < 0.1 < 0.1 Uj < 0.1 UJ c 0.1 < 0.1 < 5 < 5 72-Dichloroethane 0.4 1 r 0.1 < 0. ! < 0.1 < 0.1 UJ � 0.1 U! 0.1 < 0. 15 < 5 cis- l,2-Dichloroethene 70 µgll 0.11 J < 0.1 < 0.1 < 0.1 UJ < 0.1 UJ < 0.1 < 0.1 r i .. r, Isopropyl ether 70 µg11 < 0.1 < 0.1 r 0.1 < 0.1 UJ < 0.1 UJ ¢ 0.1 < 0.1 13 l 115 p-Isopropyltoiuene 25 (IT) µg11 < 0.1 < 0.1 < 0.1 E 0.1 Ui < 0.1 UJ < 0.1 < 0.1 Methyl tent -butyl ether 20 µgll ti- ; .1 r1. .1 0.48 J 4.81 8.81 0.171 2.6 2,480 2,410 Naphthalene 6 µgil 190 < 0.15 < 0.15 Uj < 0.15 UJ < 0.15 2.7 151 131 Trichloroethette Acena hthene 3 80 µgll L/L <: 0.1 15 J r 0.1 4.5 .1 r 0.1 < 0.67 < 0.1 UJ < 0.67 < 0.1 UJ = 0.67 < 0.1 < 0.67 +}.1 < 2.7 - NA Benzoic acid 30,000 11 < 96 UJ < 38 UJ < 9.6 LIJ ¢ 9.6 UJ < 9.6 UJ < 9.6 Uj < 38 UJ NA NA Dihenr-ofuran 28 0 1 1 1 < 7.2 3.2 J < 0.72 < 0.72 < 0.72 < 0.72 < 2.9 NA NA 2,4-Dimethy Iphenol 100 µgA < 7.4 < 2.9 UJ < 0.74 r 0.74 < 0.74 ¢ 0.74 ¢ 2.9 NA NA bis(2-E:thylhexy0phthala1e 3 µg11 < 11 r 4.4 < 1.1 < 1.1 < 1.1 r !.I NA NA Fluoranthene 300 < 5.6 ' 2.3 < 0.56 < 0.56 < 0.56 < 0.56 < 2.3 NA NA Fluorene 300 _LLL µgi 1 27.9 .1 12.2 J < 0.73 < 0.73 < 0.73 r 0.73 < 2.9 NA NA 1-Methy[naphthalene l (IT) µgil -160.1 93 J r 0.68 <0.68 < 0.68 < 0.68 ¢ 2.7 NA NA 2-Methylnaphthalene 30 119 1 190 1 115 J < 0.66 < 0.66 < 0.66 r 0.66 r 2.6 NA NA 3&4-Mcthylphenol 40 µg I 1 : I -I < 5.3 U.1 < 1.3 Uj < 1.3 UJ r 1.3 UJ < 1.3 Uj r 5.3 UJ NA NA Naphthalene 0 I<' '1 140,1 93.6 J c 0.61 e 0.61 r 0.61 < 0.61 " 2.4 NA NA Phenanthrene 'un , I 38.9 J 14.4 J < 0.68 < 0:68 < 0.68 r 0.68 < 2.7 NA NA Px rclw Hydrocarbons AIiphatics C5-C8 DO 400 ue1 Pg. I 11.23 4.9J " SX.7 .1 53.1, J <0.65 c 35 <0.65 c 35 <0.65 r 35 <0.65 c 35 <2.6 < 35 NA NA NA NA Aliphatics C9-C 18 ( 1) 700 µgi 1 6,249 J 4,151 J < 130 < 130 < 130 < 130 NA NA Aliphatics Ci9-C36 10,000 µg:'I I.92t] 1.171) < 95 < 95 ¢ 95 < 95 1,090 NA NA Aromatics C9-C22 (2) 200 µgll 2,520 J 2.275 J 244J 194 < 175 r 175 NA NA PABMPrcjects1NM01363, MN, Whitsett, NC15.0 Deliverable5Wnuary to June 2013 GW Reporffablesl1363 -Water - 2013-05 Tables (2013-06-29) 7/1512013. 4:57 PM Table 4 Summary of Groundwater Results Compared to NC 2L Groundwater Quality Standards Former Amoco Service Station No. 1363 1101 NC Hwy 61 Whitsett, Guilford County, NC Sample ID: MW-03 MW-06 MW-08 MW-10 MW-11 MW-15 RW-011% USTMW-01 USTMW-02 Collection Mate: 1-512112013 5/21/2013 5/21/2013 5/22/2013 5/22/2013 5/22/2013 5/21/2013 5/22/2013 5/22/2013 Paramelers NC 2! I Units OR 13cnzene [ µgi i 44.4 - - < 0.1 < 0.1 < 0.1 < 0,1 < 0, lolucnc 600 1.3 C0.1 <0.1 <0.1 <0.1 <0.1 < I <0.1 0.211 Fthr Ibenrene 600 µfill 1.2 .1 ¢ 0,1 < 0.1 r 0.1 < 0.1 r 0.1 66.9 0,11 J 0.27 J Xylenes (Total) 500 Mgll 2.5 J < 0,22 r 0.22 < 0.22 < 0.22 r 0.22 16.9 < 0.22 0.42 J Bromodichloromethane 0.6 < 0.25 < 0.1 r 0.1 < 0.1 < 0.1 r 0.1 < I < 0.1 < 0.1 Chloromethane 3 1 < 0.27 < 0, 11 < 0.11 < 0.11 < 0.11 < 0.11 < 1.1 0.12 J < 0.1 I Dibromochloromethane 0.4 < 0.25 < 0.1 •.• 0. l [ 0.1 < 0.1 < 0.1 < 1 < 0.1 < 0.1 1.2-Dichloroethane 0.4 < 0.25 < 0.1 < 0.1 < 0.1 < 0.1 ¢ 0.1 < 1 r 0.1 < 0.1 cis-1.2-Dichloroethene 70 µgll < 0.25 ¢ 0.1 < 0.1 < 0.1 r 0.1 ¢ 0.1 < I < 0.1 < 0.1 Isopropyl ether 70 µgll 20.3 < 0.1 < 0.1 < 0,1 < 0.1 < 0.1 0.1 < 0.1 p-]sopropy[toluene 25 (IT) }ag11 < 0,25 ¢ 0.1 r 0.1 < 0.1 < 0,1 ¢ 0.1 < I < 0. ] < 0.1 Methyl tent -butyl ether 20 µgll 90.$ <0.1 < 0.1 < 0.1 : 1).1 0.15 J 0.1 0.2 J Naphthalene 6 Agll 1.9 < 0.I5 r 0.15 < tl. ] 5 0,71 < 0.15 ff 97.3 1 richloroethcne 3 µg/I 0,25 C 0.1 < OA <0.1 0.1 u 1 <0.1 SVOC Acena hthcnc 80 1 NA NA NA ¢ 0.67 - 0,67 < 0.67 NA 5.7 17.4 J Sen7oic acid 30,000 11 NA NA NA < 9.6 UJ < 9,6 UJ 9.6 UJ NA < 9.6 UJ < 96 UJ Dibenzofuran 28 IT] 1 NA NA NA < 0.72 < 0.72 < 0.72 NA 3.2 J ¢ 7.2 2.4-Dimcthy]phenol 100 ggll NA NA NA < 0.74 < 0.74 < 0.7.1 NA r 0.74 r 7.4 bis(2-Fthylhexyl)phthalate 3 Ag1] NA NA NA < 1.1 ¢ 1.1 < 1.1 NA < 1.1 < 11 1=tuoranthene 300 11 NA NA NA <0.56 <0.56 < 0.50 NA 0.73 J < 5.6 Fluorene 300 jag/1 NA NA NA ¢ 6.73 0.81 J < 0.73 NA 116 1.4 i 1-Methy1naphthalene 1 (IT) µgll NA NA NA <0.68 <0.68 r0.68 NA 49 130 2-Methylnaphthalene 30 Agll NA NA NA ¢ 0.66 0.8.1 < 0.66 NA 38 155 3&4-Methylphenol 40 µgll NA NA NA r 1.3 U.] < 1.3 UJ c 1.3 UJ NA l..i l :J ] ; l .1 Naphthalene 6 ugll NA NA NA < 0.61 0,85 J ¢ 0.61 NA 27.5 62.8 Phenanthrene 200 1 NA N. NA < 0.68 1 J < 0.68 NA 13.7 58.4 Pyrene Aliphatics C5-C8 200 400 µg/I µfill NA NA NA NA NA NA < 0.65 < 35 < 0.65 < 35 < 0.65 < 35 NA P) .1 15.3 J NA 3 7(F Aliphatics C9-C 18 (1) 700 µgll NA NA NA < 131 < 131 < 130 NA 1.447.3 22.460 Aliphatics CI9-C36 10.000 µg11 NA NA NA 96 r 96 r 95 NA "o 4 7._' 1 0 Aromatics C9-C22 (2) 200 µgll NA NA NA 235 178 J < 175 NA 765 4,112 P-%BPlProjectsVC%01363, MN, Whitsett, 1405.0 DeliverablesUanuary to June 2013 GW Reporffabies11363 -Water - 2013-05 Tables (2013-06-29) 711512013. 4.57 PM Table 4 Summary of Groundwater Results Compared to NC 2L Groundwater Quality Standards Former Amoco Service Station No. 1363 1101 NC Hwy 61 Whitsett, Guilford County, NC Sample ID: USTMW-04 VE-01 VEW-01 Collection Date: 5/22/2013 5/21/2013 5/21/2013 Parameters NC2I. 1 Units VOC -. Benzenc l µgal 5.4 < 0.1 ¢ 0.1 Toluene 600 11 5.6 < 0.1 r 0.1 Ethylhenzene 600 µgll 2.3 r 0.1 < 0.1 Xylenes (Total) 500 µg/l 9.1 < 0.22 < 0.22 13romodichloromethanc 0.6 1 < 0.1 r 0.1 < 0.1 Chlommethane 3 1 0.45 J < 0.1 1 < 0.1 1 Dibromochloromethane 0.4 1 < 0.1 ¢ 0.1 r 0.1 1.2-Dichloroethane 0.4 1 c 0.1 ¢ 0.1 r 0.1 cis- 1.2-Dichloroethene 70 µgll < 0.1 ¢ 0.1 r 0.1 Isopropyl ether 70 µgll < 0.1 0.24 J < 0.1 p-Isopropyholuene 25 (1T) µgll r 0.1 < 0.i <0.1 Nricihy€ tcrt-butyl ether 20 µgll 0.79 2 0.48 .1 Naphthalene 6 µgll 21.3 < 0.15 E 0.15 I richloroethene 11 111 I < 0.I < 0.l SVOC Acena hthene g0 Il < 2.7 NA 77 Benzoic acid 30.000 I] 206 J NA NA Dihenxof'uran 28 (1T) Il r 2.9 NA NA 2.4-Dimethylpheno€ 1()0 µg11 &6 J NA NA his(2-Ethy IhexyI)phthalate 3 µg/I 74.5 NA NA Fluoranthenc 300 II < 2.3 NA NA Fluorene 300 µgll r 2.4 NA NA 1-Methylnaphthalene I (IT)_ µgll 4.8J NA NA 2-Methylnaphthalene 30 µgll < 2.6 NA NA 3&4-Methylphenol 40 µgll 27.5 J NA NA Naphthalene 6 µg/[ J9 3 4 NA NA Phenanthrvne 200 RgA < 2.7 NA NA Ps rene 200 µgll 3.2 .1 NA NA Hydrocarbons Aliphalics C'5-L 8 400 NA NA Aliphatics C9-C 18 (l) 700 µgll 4.590 NA NA AIiphatics C19-06 10.000 µgll 1.'14kl NA NA Aromatics C9-C22 (2) 200 jig/] 1,109.7 NA NA P W\ProjectMNCV 363, MN, Whitsett, NC15.0 ❑eliverablesUanuary to June 2013 GW Report\Tables11363 - Water - 2013-05 Tables (2013-06-29) 7/1512013. 4 57 PM Table 4 Summary of Groundwater Results Compared to NC 2L Groundwater Quality Standards Former Amoco Service Station No. 1363 1101 NC Hwy 61 Whitsett, Guilford County, NC Notes: NC 2L - NC 2L Groundwater Quality 'Standards IT - Interim Maximum Allowable Concentration established under 15A NCAC 2L.0202 < -Not detected at the specified detection limit µglL - Micrograms per liter ❑UP(1) - Field duplicate sample 1D is DUP-2 DUP(2) - Field duplicate sample I is DUP-1 J -Estimated value NA - Not applicable SVOC - Semivolatile organic compounds UJ - Not detected and the limit is estimated VOC - Volatile organic compounds This table presents the results of all VOC. detected SVOC- and petroleum hydrocarbons where a NC 2L has been established. Sample results have been qualified by U R S based on the results of the data review process. which is modeled after the USEPA Conlrael Laboradon, Program National Functional Guidelines for .Superfund Organic Medrodv Data Review (EPA, June 2008). NC Groundwater quality standards f'or the protection of the groundwater are specif ied in 15A NCAC 2L .0200. A bold border with highIighLed value indicales the concentration is greater than the standard. P: %B RProjectsl1400 136 3. MN. Whitsett, NC15M DellvefableMJanuary to June 2013 GW Repo rhTables11363 - Water - 2013.05 Tames (2013-06-29) 7/1512013, C58 PM Table 5A 1301 Piney Grove Treatment System Performance Compared to NC 2L Groundwater Quality Standards Former Amoco Service Station No. 1363 1101 NC Hwy61 Whitsett, Guilford County, NC Location: 1301 Influent 1301 Between Carbon 1301 Effluent Field Sample ID: 1301 PINEY GROVE RD-IN 1301 PINEY GROVE RD-MID 1301 PINEY GROVE RD-EFF Collection Date: 5/21/2013 5/21/2013 5/21/2013 Parameters NC 2L vac Benzene l Units I < 0.10 < 0.10 < 0. 10 Toluene 600 I < 0.10 < 0.10 < 0, l0 Eth ]benzene 600 I < 0,10 ¢ 0.10 < 0.10 K lenes (Total) 500 Rgil < 0.22 < 0.22 < 0.22 Bromodichloromethane 0.6 PWI < 0.10 < 0.10 < 0.10 Chloromethane 3 1 < 0.11 < 0.11 0.24 J ❑ibromochloromethane 0A µgjl < 0.10 < 0.10 < 0.10 1,2-❑ichloroethane 0.4 µgl] J <0A0 <0.10 cis-1,2-DichIoroethene 70 1 0_ 10 E 0.10 � 0.10 Isopropyl ether 74 1 0.214 .I ¢ 0.10 < 0.10 -Iso ro !toluene 25 (IT) 1 < 0.10 < 0.10 r 0.10 Methyl tcrt-butyj ether 20 1 6.2 < 0.10 < 0.10 Naphthalene 6 1 < 0.15 < 0.15 E 0.15 Trichloroethene 3 I = 0.10 < 0.10 < 0.10 ;Votes: NC 2L - NC 2L Groundwater Quality Standards IT - Interim Maximum Allowable Concentration established under ISA NCAC 2L.0202 -Not detected at the spectfied detection limn µg1L -Micrograms per Liter ! -Estimated value VOC - Volatile organic compounds This table presents the results of all analytes. Sample results have been qualified by URS based on the results of the data review process, which is modeled after the USEPA Contract Laboratory Program National Functional Guidelines for Superfund Organic Methods Data Review (EPA, June 2008). NC Groundwater quality standards for the protection of the groundwater are specified in I5A NCAC 2L .0200. A hold border with highlighted value indicates the Lancentration is greater than the standard. P:1BP%Projects1NC101363, MN, Whitsett, NC15.0 ❑eIiverableslJanuary to June 2013 GW Reporffables11363 - Water- 2013-05 Tables (2013-06-29) 7115t2013, 4:56 PM Table 5B 1205 N Hwy 61 Treatment System Performance Crrrnpared to NC 2L Groundwater Quality Standards Former Amoco Service Station No. 1363 1101 NC Hwy 61 Whitsett, Guilford County, NC Location: 1205 influent 1205 Between Carbon 1205 Effluent Field Sample ID: 1205 NC HIGHWAY 61 SOUTH -IN 1205 NC HIGHWAV 61 SOUTH -MID 1205 NC HIGHWAV 61 SOUTH-EFF Collection (late: 5/21/2013 5/21/2013 5121120I3 Parameters Voc Benzene NC 2L 1 Units I < 0.10 e 0.10 a 0.10 To I uene 600 9WI < 0.10 < 0,10 < 0.10 Eth lbenxene 600 I < 0.10 < 0.10 < 0.10 7i lenes (Total) 500 2ELl E 0.22 < 0.22 < 0.22 Bromodichloromethane 0.6 11911 < 0. f 0 < 0.10 < 0.10 Chioromethane 3 1 < 0.11 < 0.1 1 < 0.11 Dibromochloramethane 0.4 1 < 0.10 < 0.10 < 0.10 1.2-Dichloroethane 0.4 1 0.23 J < 0.10 r 0.10 cis-1,2-Dichloroethene 70 !I < 0.10 < 0.10 r 0,10 lsopropyl ether 70 I 0.33 J < 0.10 < 0.10 Iso ry ltoluene 25 {1T) pg!I <0.10 < 0.10 < 0.10 Meth I ten -butyl ether 20 PWI 11.0 r 0.10 r 0. 10 Naphthalene 6 A'l < 0.15 < 0.15 < 0.15 Trichloroethene 3 PWI < 0.10 < 0,10 < 0.10 Notes: NC 2L - NC 2L Groundwater Quoliq Standards 1T. Interim Maximum Allowable Cortcentrauon established under 15A NCAC 2L.0202 a -Not detected at the specified detection limit µglL -Micrograms per Liter ] - Esumated value VOC - Volatile organic compounds This table presents the results of all analytes. Sample results have been qualified by URS based on the results of the data review process, which is modeled after the USEPA Coneracl Laboratory Program Narional Functional Guidelines far Superfund Organic Alwhods Data Review (EPA. ,tune 2008). NC Groundwater quality standards for the protection of the groundwater are specified in 15A NC AC 2L .0200. A bold harder ►rith highlighted value indicates the concentration is greater than the standard. P:%BRProjects%NC101363. MN, Whitsett, NG15-0 De live ra bles\Jan u a ry to June 2013 GW Report\Tables11363 - Water - 2013-05 Tables (2013-06.29) 711512013, 4:56 PM TABLE 6 POTABLE WELL TREATMENT SYSTEM OPERATIONAL DATA Former BP Site No.01363 1101 NC Highway 61 Whitsett, North Carolina Activation Date. March 5, 2008 1301/1305 Piney Grove 120" Hwy. South I)ate rotali[er Water [ sage Heading (gallons) -AL, Filter Replaced Iyeslno) Totalizer 1'1 ater Usage Reading (gallons) Filter Replaced (yes/no) Comments of/21i 13 98,693 ses 155,177 yes Cum p Iewd routine U&M. 02/28/13 102,935 yes 156,744 xes Completed routine O&M. 03/28/13 106,846 yes 157,780 yes Completed routine O&M. 04/26/13 111,220 yes 158,806 ves Completed routine O&M. 05/22/13 114.922 no 159,766 na Inspection onl . 06/27/13 125.949 YLS 160,955 yes Completed routine O&M. NOTES Systems installed by Carbonair on March 5, 2008 Systems each consist of two 12x52 Granular Activated Carbon (GAC) vessels, one LIV light unit_ two 5 micron f Iters and housing, one heater unit, and one totalizing meter. NR=Not Recorded F 11 Frojams NCO1363, MN, Wluu M NRS 0 nebvmhle VanuAm is June 20I3 GW Repon%Tab1m,Ta61c 6 D&M Summ I of I TABLE 7 GROUNDWATER SAMPLING PLAN Former BP Site No. 01363 1101 NC Highway 61 Whitsett, North Carolina Well ID Laboratory Analysis Required VOCs EPA 826013 5VUCs EPA 625 VPHIEPH MADEP Incident No. 6113 Near Automotive Dis ensers M W-2 R x M W-3 x M W-6 x M W-8 x RW-1R x VE-1 x VEW-1 x Incident No. 20054 Near UST Field MW-10 x x x MW-11 x x x MW-15 x x x USTMW-1 x x x USTMW-2 x x x USTMW4 x x x AGM-RW x x x Incident No. 30318 Near Truck Dispensers) CSAMW-1 x x x CSAMW-2 x x x CSAMW-3 x x x CSAM W-d x x x DDM W-2 x x x Notes- VOCs - Volatile organic compounds by USEPA Method 9260B SVOCs - Semi -volatile organic compounds by USEPA Method 625 VPHIEPH - Volatile/extractable petroleum hydrocarbons by MADEP Method P W-Pmjeets NC )1363, MN. W titsm, NCIS 0 Del i%erahles•la am to June 2013 GW ReportTabiesJabie 7 Sampling Plan I of I FIGURES wl 4701 look Aft a 0�r 1 IGRASS 1 GASOLINE AND ' —DIESEL UST FIELD e ' GRASS ;BMW-13 ) �\ Iff r x '6 s Y � Y MW-1419 +ISAGM-J � � - Mw > 1 f A1w- � co 4 CD N ' PARKING LOT a N o �Ylf-8 0 vi � o r a 4 ' U m r ° SOURCE: SAIC, DATED 4-28-09, DRAWING No.: 10049-002. lK WW-4 DDUW-2 TRUCK SCALES TRUCK DIESEL FUELING DISPENSERS AND CANOPY a�CSAMW-4 d �yb SD r I �_x d Y R 3 C8A7Iif_ 1 TRUCK s1d1f-15 GARAGE v l� VEw-1 � of � a WW-2R6 owe DP-i AUTOMOBILE DISPENSERS A A OIL/WATER �� rSEPARATOF NEW AND USED MOTOR OIL AST's '-r DUMPSTER T Tl Ct Ti A T T A MWk, MONITORING WELL USTi4iWS UST FIELD MONITORING WELL ABANDONED MONITORING WELL DUAL PHASE EXTRACTION WELL SOIL VAPOR IMPLANT UNDERGROUND STORAGE TANK OVERHEAD ELECTRIC LINE SANITARY SEWER LINE STORM SEWER LINE STORM TRENCH LINE PRODUCT DISPENSER LINE DRAIN LINE NOTES: 1. TANKS 1, 2, & 3 ARE GASOLINE UST's 2. TANKS 4, 5, 6, 7, & 8 ARE DIESEL FUEL UST's 60' 0 60 SCALE IN FEET Wh itsett Park Dr. err Rd. -FW I I I I y I z�q I � � I I i I { r son Rd. LEGEND I Private Potable Water Supply BP Site No. + Wells , ' 01 3 63 1 '' --_ -- Intermittent Stream I I r Interstate 40/85 1 I - Repide ce 12 5 y 61 S r APPROX. SCALE, ft. I I I Cla is Chapel 1301 1 Grove Rd MILE AS SHOWN w ""� Figure 3. (VOTE. 7 s potable water su y R e s i d e n ca�roo .-AL Ira,,! r�xrc rM-PIMP of Vicinity Map well is sh red by Clapp's Chapel PAF 13SEP06 Former BP Station No. 1363 and the Residence 1305 Piney Grove Rd OkEDU we war Whitsett, North Carolina MMN1'3SEP06 worm � �''� 38436246 1363—VIC O SOURCE: PIEDMONT GEOLOGIC, P.C., DATED: 2-7-01, DRAWING No.: 01363-6. „o,�„I QWW- ».o ' � � AK MW-4 ./88.06 | ./ / � ' .-----_— SO At NEW 4NO DIJ AS) 00 78 WAX AS SHOWN COWDEWM-Aa WPM KSEWM-PROKEN Of - LEGEND MW,q MDN03R|NG WELL OSTMW,s UST FIELD wDw|TO0wG WELL -4 ABANDONED MONITORING WELL DUAL PHASE EXTRACTION WELL ' SOIL VAPOR IMPLANT UNDERGROUND STORAGE TANK OVERHEAD ELECTRIC LINE SANITARY SEWER LINE STORM SEWER LINE STORM TRENCH LINE PRODUCT DISPENSER LINE DRAIN UN[ 715.81 GROUNDWATER ELEVATION (Relative toSite Datum) SCALE IN FEET SOURCE: SAIC, DATED 4--28-09, DRAWING No.: 10049-002 A r bnr=11 a - 0. Ca' 6, VW i � ilW-1 4.2J ��! ,•. MW - 7 W + T � a <d 3 Q 0 P N � b[1Y-88 Q C0.1 vj 0 n r� n. SOURCE: SAIC, DATED 4-28-09, DRAWING No.: 10049-002 JC V, VV - - 4 f CSAMW-3 6 CSAMW-4 <0.1LIJ d� C0.1 DDVW-2 - 0.55 u cl F _ a CSAhFYI-2•. ICSA �'IP�` 1 [0.1 L1J i l: •.: r, � �ilf-15 CQ.1 10 _ 70 .:0 0 MW-2RB 6,5403 •I �D u 7n W 4 i Y / A OIL /WATr R s' �'•EPARATOR NEW A�� USED MOTOR Dll- ASF'S 0U MPST Eta LEGEND MW,& MONITORING WELL USTIWS UST FIELD MONITORING WELL ABANDONED MONITORING WELL DUAL PHASE EXTRACTION WELL SOIL VAPOR IMPLANT UNDERGROUND STORAGE TANK OVERHEAD ELECTRIC LINE SANITARY SEWER LINE STORM SEWER LINE STORM TRENCH LINE PRODUCT DISPENSER LINE DRAIN LINE C0.1 BENZENE CONCENTRATION (ug/L) ---- BENZENE ISOCONCENTRATION Dashed where inferred) J ESTIMATED VALUE LId NOT DETECTED AND THE LIMIT IS ESTIMATE] C NOT DETECTED AT SPECIFIED DETECTION LIMIT SOLI} INDICATES EXCEEDANCE OF NC 2L STANDARD NOTE: NC 2L. STANDARD FOR BENZENE=1.0 ug/L. 60' 0 60 SCALE IN FEET JK+w a i 0 i _s CSAMW-3 & 9CSAM11-4 C0.1 [0.1 LJJ ° 4] A. -.A50I.1"q% ANu 1' DDWW-8 & - Z M1►' its mw 12 m }Tyr :4 .rd J \*AGiI[— \ [0.1 4 ' —`—s's's—y — CSA�dIF-2 "CS/�AMW-1 [0.1 LJJ lIW-1s u r MW V,J MW-1 Sy 3[i. <0.1 0 a MW-15 �J. r-1019 VEW-1 1r �[0.1 ` IfW-2R 131 g AUT©Mt"3BILF o • � . DT5PEN5ER5 GRASS RW-1R F4D? b ,1 3sB DP-3. CO.i B ❑ -1 SOURCE. SAIL, [SATED 4-28-09, DRAWING No.: 10049-002 f � a rA-F 4 c OIL/WATER �� >yFIN AN7 - � USED 10 J10 •� � DiL A5 � 's c �.� DUMPS; ER LEGEND mW& MONffOR�NG WELL USTMWI9 UST FIELD MONITORING WELL r ABANDONED MONITORING WELL DUAL PHASE EXTRACTION WELL SOIL VAPOR IMPLANT UNDERGROUND STORAGE TANK OVERHEAD ELECTRIC LINE SANITARY SEWER LINE STORM SEWER LINE STORM TRENCH LINE PRODUCT DISPENSER LINE DRAIN LINE CO.I IPE CONCENTRATION (ug1Q ---- IPE ISOCONCENTRATION (Dashed where inferred) J ESTIMATED VALUE lJJ NOT DETECTED AND THE LIMIT IS ESTIMATED C NOT DETECTED AT SPECIFIED DETECTION LIMIT BOLD INDICATES EXCEEDANCE OF INC 2L STANDARD NOTE: NC 2L STANDARD FOR IPE=7C ug/L. 60' 0 60' SCALE IN FEET LEGEND MWS MONITORING WELL C15TMW$ UST FIELD MONITORING WELL lABANDONED MONITORING WELL DUAL PHASE EXTRACTION WELL SOIL VAPOR IMPLANT UNDERGROUND STORAGE TANK ► , °1 OVERHEAD ELECTRIC LINE SANITARY SEWER LINE �4 CSA]IdW-3 0 SCSAidW STORM SEWER LINE O. i 7J STORM TRENCH LINE Q PRODUCT DISPENSER LINE NZ-11� , 2.6 _—,! DRAIN LINE V �� �' C� 1S •� , ^ }>E -- _ , — C0.1 MTBE CONCENTRATION (u9/L) V. 1,3 II �� �� x — ' - ---- MTBE ISOCONCENTRATON ,. Dashed where inferred) ESTIMATED VALUE b ` O LIJ NOT DETECTED AND THE 1 W-14� &AA�- q gCSAMW-2 LIMIT IS ESTIMATED �SAi� W-1 4.8J o _i 1I1V -- 7 vW - 0.48J ; _ ; C NOT DETECTED AT SPECIFIED DETECTION LIMIT 0,151 r ' �•- �- HOLD INDCATES ANCE OF NC ZL STANDARD 14i� 2p VEW- .• �� C t'pQ 0.48J pp Ir R 0 MW-2R� 5 �' 0 R ,4$0 NOTE: NC 2L STANDARD FOR MTBE=20 ug/L. CIL/WATFF _ y RV-1R `sE�ARATOR t 149 E NEW AND r ,—USED MOTOR DIL AST', t. /` �DIJ tPSTER �,AR.CliJ':- MW-3 s '! 90.8 60' 0 60' SCALE IN FEET • TIP-B� � ;Y.,: i�f 3 _� - _ _- -r~. -!� �C0.1 ; *2. —1 ' AS SHOWN °"`ee DATE Figure 7_ MTBE Concentrations in „k_ u „pas „m �„vmrrof D,,,,,, ay UATE Groundwater, May 23, 2013 *MW`7 TSH 49J1JL13 Former BP Station No. 1363 u Whitsett North Carolina WP 09JUL13 GOMRALT 40. 'WPR°VM � WE J3- GOOD 1363.01 1363-�7 0 SOURCE: SAIC, DATED 4-28-09, DRAWING No.: 10049-002 Fft,om 041MIR vM WP 09JULl 3 SA: _ )K V, w a CSAMW-3 9 n &CSAMT-4 C0.15uJ C0.15 DDM[W-2 19. . 2.7 MW &CSAUW-2 1 [b-15UJ �C0.15 CI].15 WW-2R' 151 0 it a I � MW-619 Ca.15 0 SOURCE: SAIL, DATED 4-28-09, DRAWING No.. 10049-002 l VEIL-1 $[0.15 &C0.15 ,, *MfY— 7 - T�;;[ � -( , 0 f.. LEGEND MWS MONITORING WELL USTMW& UST FIELD MONITORING WELL ABANDONED MONITORING WELL DUAL PHASE EXTRACTION WELL SOIL VAPOR IMPLANT UNDERGROUND STORAGE TANK OVERHEAD ELECTRIC LINE SANITARY SEWER LINE STORM SEWER LINE STORM TRENCH LINE PRODUCT DISPENSER LINE DRAIN LINE C0,1 NAPHTHALENE CONCENTRATION (ug/L) ---- NAPHTHALENE ISOCONCENTRATION (Dashed where inferred) J ESTIMATED VALUE u J NOT DETECTED AND THE LIMIT IS ESTIMATED C NOT DETECTED AT SPECIFIED DETECTION LIMIT HOLD INDICATES EXCEEDANCE OF NC 2L STANDARD Y 3 r .1i F 41L�'WATEF .—SEPARATOR NEW AN:. —I.15ED MOT'1�. r A5T's r� F)LIMPSI Lk :.r{�L, r- -. N OTE: NC 2L STANDARD FOR NAPHTHALENE=6.0 ug/L. 60' 0 60 SCALE IN FEET X V-*-,t I d CSAMW-3 &CSAMWa —4 C0.22UJ d� DDMW-2 19 r <D.22 a &CSAMW-2 Cs/ry7nMr7�y,77Y=> [0.22UJ 50 CV.22 MW--15 �C0.22 1�_ YEW—ryr1� �t '0CO.22 Sop ' 11W-2R - 655 1 '---AL,P)MOH',i E 0BIf-1Ti t 16.g a r MW J32.5 _ 1 MW—$� r �w I71 iT [0.22 SOURCE: SAIC, DATED 4-28-09. DRAWING No-: 10049-002 LEGEND MW,& MONITORING WELL USTMWIS UST FIELD MONITORING WELL ABANDONED MONITORING WELL DUAL PHASE EXTRACTION WELL SOIL VAPOR IMPLANT UNDERGROUND STORAGE TANK OVERHEAD ELECTRIC LINE SANITARY SEWER LINE STORM SEWER LINE STORM TRENCH LINE PRODUCT DISPENSER LINE DRAIN LINE C0.1 XYLENES (Total) CONCENTRATION (ug/L) ---- XYLENES (Total) ISOCONCENTRATION (Dashed where inferred) J ESTIMATED VALUE ui NOT DETECTED AND THE LIMIT IS ESTIMATED C NOT DETECTED AT SPECIFIED DETECTION LIMIT BOLD INDICATES EXCEEDANCE OF NC 2L STANDARD NOTE: ` NC 2L. STANDARD FOR XYLENES (Tv#al)=500 ug/:-. y OIL/WATEP EPARATOR NEW A•':' AST" �i ` � UilA1Si' ,I4�k D SFlED A'S SHOWN 60' 0 60' SCALE IN FEET 100000 M W-2 R 1 a0 10000 1000 Ethylbenzene 90 Toluene q� J Xylenes i O C 0 * - r > 100 x w � L � � 3 C D 'Q U MTBE 3 0 /L^ V 10 80 1 Benzene 0.1 70 1998 2000 2002 2004 2006 2008 2010 2012 2014 LEGEND + -- Benzene 0 MTBE Toluene Naphthalene Ethyibenzene 14 Groundwater Elevation �r- -- Xylenes NC 2L Standard Note: Open symbols represent detection limit for nondetect results. Former BP Service Station No. 01353 FIGURE 10 1101 NC Highway 61 TIME -TREND GRAPH OF ANALYTICAL RESULTS Whitsett, North Carolina AND GROUNDWATER ELEVATIONS FOR MW-2R Protect Na. 38a3fi75+ 100000 M W-3 100 10000 1000 Ethylbenzene 90 Toluene ay - -- — - d J Xylenes �f = o a 4) 100 W O U MTBE �r G 10 80 0A 70 1998 2000 2002 2004 2006 2008 2010 2012 2014 LEGEND Benzene --0 - MTBE �R Toluene Naphthalene V Ethylbenzene x Groundwater Elevation - Xylenes NC 2L Standard Note: Open symbols represent detection limit for nondetect results. Former BP Service Station No- 01363 FIGURE 11 w 1101 NC Highway 61 TIME -TREND GRAPH OF ANALYTICAL RESULTS U Whitsett, North Carolina AND GROUNDWATER ELEVATIONS FOR MW-3 Protect No 38436751 APPENDIX A HISTORICAL GROUNDWATER ELEVATION DATA Appendix Al Historical Groundwater Elevation Data Former BP Service Station No. 01363 1101 NC Highway 61 Whitsett, North Carolina Well Datum Date Depth To Depth To LNAPL Groundwater Elevation LNAPL Water Thickness Elevation (feet) (feet) (feet) (feet) (feet) MW-1 91.13 8/11/1993 6.36 84.77 3/1/1995 1.10 90.03 8/3/1996 3.97 87.16 3/25/1997 1.43 89.70 12/8/1997 6.96 84.17 10/24/2000 6.32 84.81 6/26/2003 1.00 90.13 9/4/2003 1.52 89.61 3/10/2004 2.20 88.93 9/15/2004 4.06 87.07 6/27/2005 4.24 86.89 5/4/2006 5.16 85.97 MW-10 91.36 1/7/2000 6.37 84.99 7/11 /2000 8.52 82.84 10/23/2000 8.60 82.76 1 /13/2003 2.10 89.26 6/26/2003 1.70 89.66 9/4/2003 1.35 90.01 3/10/2004 2.20 89.16 9/15/2004 3.24 88.12 6/27/2005 3.48 87.88 5/4/2006 3.94 87.42 3/13/2007 3.25 88.11 10/30/2007 4.79 86.57 8/5/2008 4.53 86.83 2/17/2009 3.86 87.50 9/30/2009 4.04 87.32 4/22/2010 3.38 87.98 11/2/2010 4.37 86.99 5/17/2011 2.22 89.14 11/1/201 1 3.61 87.75 11/13/2012 3.99 87.37 5/21/2013 2.23 89.13 MW-11 94.21 1/7/2000 12.73 81.48 7/11 /2000 8.19 86.02 10/23/2000 8.84 85.37 1 / 13/2003 3.61 90.60 6/26/2003 2.80 91.41 9/4/2003 2.99 91.22 3/10/2004 3.95 90.26 9/15/2004 5.75 88.46 6/27/2005 5.65 88.56 5/4/2006 5.83 88.38 3/13/2007 4.02 90.19 September, 11, 2013 Page 1 of 7 Appendix Al Historical Groundwater Elevation Data Former BP Service Station No. 01363 1101 NC Highway 61 Whitsett, North Carolina Well Datum Date Depth To Depth To LNAPL Groundwater Elevation LNAPL Water Thickness Elevation (feet) (feet) (feet) (feet) (feet) M W -11 94.21 10/30/2007 6.99 87.22 8/5/2008 6.83 87.38 2/17/2009 5.20 89.01 9/30/2009 5.80 88.41 4/22/2010 4.53 89.68 11/2/2010 6.72 87.49 11/1/2011 5.10 89.11 5/23/2012 4.34 89.87 11 /13/2012 6.09 88.12 5/21/2013 4.34 89.87 MW-12 92.64 1/7/2000 8.85 83.79 7/11 /2000 8.48 13.37 4.89 79.27 10/23/2000 8.80 10,92 2.12 81.72 1 /13/2003 3.66 3.93 0.27 88.71 6/26/2003 3.34 89.30 9/4/2003 3.26 89.38 3/10/2004 4.00 88.64 9/15/2004 4.96 87.68 6/27/2005 4.55 88.09 5/4/2006 4.89 87.75 3/13/2007 3.95 88.69 10/30/2007 5.80 86.84 8/5/2008 5.83 86.81 2/17/2009 4.52 88.12 9/30/2009 5.23 87.41 4/22/2010 3.94 88.70 11/2/2010 5.46 87.18 MW-2 92.93 8/11/1993 13.68 14.08 0.40 78.85 3/1/1995 13.18 79.75 8/3/1996 12.84 80.09 3/25/1997 11.90 81.03 12/8/1997 13.19 79.74 MW-2R 93.92 12/22/2000 13.92 80.00 1 /13/2003 13.40 80.52 6/26/2003 13.38 80.54 9/4/2003 10.68 83.24 3/10/2004 13.64 80.28 9/15/2004 14.14 79.78 6/27/2005 13.91 80.01 5/4/2006 12.89 81.03 3/13/2007 12.27 81.65 10/30/2007 14.05 79.87 8/5/2008 13.90 80.02 September, 11, 2013 Page 2 of 7 Appendix Al Historical Groundwater Elevation Data Former BP Service Station No. 01363 1101 NC Highway 61 Whitsett, North Carolina Well Datum Date Depth To Depth To LNAPL Groundwater Elevation LNAPL Water Thickness Elevation (feet) (feet) (feet) (feet) (feet) MW-2R 93.92 2/17/2009 13.46 80.46 4/22/2010 13.05 80.87 11 J2J2010 13.33 80.59 5/17/2011 11.36 82.56 11/1/2011 12.88 81.04 5/23/2012 11.88 82.04 5/21 /2013 11.87 82.05 MW-3 91.13 8/11/1993 16.49 74.64 311 J1995 14.85 76.28 8J311996 14.41 76.72 3/25/1997 14.06 77.07 12/8/1997 15.69 75.44 10/23/2000 14.69 76.44 1 /13/2003 14.84 76.29 6/26/2003 15.42 75.71 9J412003 11.74 79.39 3/10/2004 16.40 74.73 9/15/2004 16.82 74.31 6/27/2005 15.72 75.41 5J412006 14.42 76.71 3/13/2007 13.31 77.82 10/30/2007 15.71 75.42 8/5/2008 15.09 76.04 2/ 17/2009 13.89 77.24 9/30/2009 14.85 76.28 4f22J2010 12.53 78.60 11/2/2010 14.59 76.54 5/17/2011 10.68 80.45 11 / 112011 14.31 76.82 5/23/2012 13.02 78.11 11 /13/2012 14.32 76.81 5121 /2013 13.02 78.11 MW-4 100.00 8/11/1993 13.43 86.57 3/1/1995 7.33 92.67 8/3/1996 10.42 89.58 3/25/1997 3.23 96.77 1218J 1997 12.37 87.63 10/24/2000 11.31 88.69 1 /13/2003 3.05 96.95 6/26/2003 2.44 97.56 914J2003 1.70 98.30 3/10/2004 4.25 95.75 9/15/2004 8.52 91.48 6/27/2005 9.02 90.98 September, 11. 2013 Page 3 of 7 Appendix Al Historical Groundwater Elevation Data Former BP Service Station No. 01363 1101 NC Highway 61 Whitsett, North Carolina Well Datum Date Depth To Depth To LNAPL Groundwater Elevation LNAPL Water Thickness Elevation (feet) (feet) (feet) (feet) (feet) MW-4 100.00 5/4/2006 9.57 90.43 3/13/2007 4.01 95.99 10/30/2007 12.25 87.75 8r5/2008 11.95 88.05 2/17/2009 8.43 91.57 9/30/2009 10.84 89.16 4/22/2010 6.25 93.75 MW-5 96.88 8/11/1993 18.47 78.41 3/1/1995 DRY DRY 8/3/1996 DRY DRY 121811997 DRY DRY MW-6 91.28 8/11/1993 12.54 78.74 3J111995 4.43 86.85 8J3J1996 11.81 79.47 3/25/ 1997 12.87 78.41 12/8/1997 12.36 78.92 116J2000 11.78 79.50 10/23/2000 11.77 79.51 1 /13/2003 10.04 81.24 6/26/2003 9.35 81.93 9/4/2003 8.11 83.17 3/10/2004 10.25 81.03 9/15/2004 9.21 82.07 6/27/2005 11.50 79.78 5/4/2006 10.70 80.58 3/13/2007 9.89 81.39 10/30/2007 9.20 82.08 8/5/2008 10.36 80.92 2/17/2009 10.87 80.41 9/30/2009 8.28 83.00 4/22/2010 9.85 81.43 11/2/2010 11.26 80.02 5/17/2011 5.31 85.97 11/1/2011 8.72 82.56 5/23/2012 6.01 85.27 11 /13/2012 6.64 84.64 5121 /2013 8.28 83.00 MW-7 89.95 8/11/1993 16.18 73.77 3J 111995 14.81 75.14 8/3/1996 14.98 74.97 1218/1997 15.02 74.93 10/24/2000 14.09 75.86 1/13/2003 13.35 76.60 September, 11, 2013 Page 4 of 7 Appendix Al Historical Groundwater Elevation Data Former 6P Service Station No. 01363 1101 NC Highway 61 Whitsett, North Carolina Well Datum Elevation (feet) Date Depth To LNAPL (feet) Depth To Water (feet) LNAPL Groundwater Thickness Elevation (feet) (feet) MW-7 89.95 6/26/2003 12.05 77.90 9/4/2003 12.89 77.06 3/10/2004 14.23 75.72 9/15/2004 14.76 75.19 6/27/2005 14.22 75.73 5/4/2006 15.79 74.16 3/13/2007 12.81 77.14 10/30/2007 15.20 74.75 815l2008 14.32 75.63 2/17/2009 13.16 76.79 9/30/2009 14.56 75.39 MW-8 87.92 8/11/1993 15.09 72.83 3/111995 14.14 73.78 8/3/1996 14.00 73.92 3/25/1997 12.69 75.23 12/8/1997 14.59 73.33 1 / 13/2003 12.14 75.78 1/1312003 13.95 73.97 6/26/2003 10.55 77.37 9/4/2003 10.40 77.52 3/10/2004 12.40 75.52 9/15/2004 12.63 75.29 6/27/2005 13.02 74.90 5/4/2006 12.22 75.70 3/13/2007 11.58 76.34 10/30/2007 13.98 73.94 8/5/2008 13.45 74.47 2/17/2009 11.27 76.65 9/30/2009 12.84 75.08 4/22/2010 11.17 76.75 11/2/2010 13.31 74.61 5/ 17/2011 10.92 77.00 11/1/2011 13.26 74.66 5/23/2012 11.61 7U1 11 I1312012 13.45 74.47 5/21 /2013 11.45 76.47 MW -9 90.43 1 /712000 3.72 86.71 7/ 11 /2000 4.55 85.88 10/23/2000 3.37 87.06 6/26/2003 0.00 90.43 3/10/2004 0.00 90.43 9/15/2004 0.89 89.54 6/27/2005 0.94 89.49 5/4/2006 2.30 88.13 September, 11, 2013 Page 5 of 7 Appendix Al Historical Groundwater Elevation Data Former 8P Service Station No. 01363 1101 NC Highway 61 Whitsett, North Carolina Well Datum Elevation (feet) Date Depth To LNAPL (feet) Depth To Water (feet) LNAPL Groundwater Thickness Elevation (feet) (feet) MW-9 90.43 3/13/2007 1.74 88.69 10/30/2007 3.45 86.98 8/5/2008 2.40 88.03 2/17/2009 1.35 89.08 9/30/2009 2.22 88.21 11/2/2010 2.10 88.33 5/17/2011 0.00 90.43 1111 /2011 1.48 88.95 MW-9D 90.84 1/7/2000 5.12 85.72 10/23/2000 5.84 85.00 6/26/2003 0.10 90.74 9/4/2003 0.20 90.64 3/10/2004 1.35 89.49 9/15/2004 5.49 85.35 6/27/2005 4.94 85.90 5/4/2006 5.43 85.41 3/13/2007 1.40 89.44 10/30/2007 9.23 81.61 8/5/2008 6.91 83.93 2/17/2009 2.81 88.03 9/30/2009 6.21 84.63 4/22/2010 1.87 88.97 11/2/2010 6.89 83.95 5/17/2011 1.54 89.30 11/1/2011 6.27 84.57 RW-1 R 92.17 6/27/2005 14.13 78.04 5/4/2006 12.63 79.54 3/13/2007 12.69 79.48 10/30/2007 14.57 77.60 8/5/2008 14.21 77.96 2/17/2009 13.41 78.76 9/30/2009 13.86 78.31 4/22/2010 12.69 79.48 11/2/2010 13.79 78.38 5/17/2011 12.71 79.46 1 1111201 1 13.42 78.75 5/23/2012 12.66 79.51 11 /13/2012 13.53 78.64 5/21/2013 12.66 79.51 VE-1 90.98 8/3/1996 17.78 73.20 3/25/1997 17.93 73.05 12/8/1997 29.88 61.10 10/24/2000 15.18 75.80 September, 11, 2013 Page 6 of 7 Appendix Al Historical Groundwater Elevation Data Former BP Service Station No. 01363 1101 NC Highway 61 Whitsett, North Carolina Well Datum Elevation (feet) Date Depth To LNAPL (feet) Depth To Water (feet) LNAPL Groundwater Thickness Elevation (feet) (feet) VE-1 90.98 1 /13/2003 14.89 76.09 6/26/2003 13.25 77.73 9/4/2003 10.70 80.28 3/ 10/2004 14.75 76.23 9/15/2004 14.99 75.99 6/27/2005 12.52 78.46 5/4/2006 9.11 81.87 3/13/2007 9.65 81.33 10/30/2007 6.02 84.96 8/5/2008 11.30 79.68 2/ 17/2009 12.08 78.90 9/30/2009 5.93 85-05 4/22/2010 11.59 79.39 11 /212010 14.12 76.86 5/17/2011 13.59 77.39 11/1/2011 14.86 76.12 5/23/2012 26.36 64.62 11 /13/2012 21.26 69.72 5121 /2013 15.23 75.75 VEW-1 96.29 8/3/1996 11.52 84.77 3/25/1997 8.98 87.31 12/8/1997 12.42 83.87 9/15/2004 10.88 85.41 6/27/2005 10.02 86.27 5/4/2006 9.50 86.79 3/13/2007 8.03 88.26 10/30/2007 12.36 83.93 8/5/2008 10.78 85.51 2/17/2009 9.95 86.34 9/30/2009 10.84 85.45 4/22/2010 8.24 88.05 11 J212010 10.88 85.41 5/17/2011 7.82 88.47 11/1/2011 10.38 85.91 5/23/2012 7.98 88.31 11 /13/2012 10.91 85.38 5/21 /2013 7.92 88.37 TOC - Top of casing NE - LNAPL not encountered Units are in feet. Elevations surveyed to site datum. Data prior to 2003 were reported by previous suppliers and have not been verified. September, 11. 2013 Page 7 at 7 APPENDIX A2 Historical Groundwater Elevation Data TravelCenters of America 1101 NC Highway 6i WhitseM Guilford County, North Carolina Facility I.D.: 0-029186 Incident Number.- 20054 Well [I) DaftUncorrectedSurface Screened Interval {top to bottom of screen feet Depth to Water- (feet) Free Prod net Thickness (feet) Depth to Water- Corrected (reel) Top of Casing Elevation (feet) Groundwater Elevation (feet) 412W2009 5-20 2.57 2.5' Q ] 13 88. f, 5/2812009 2.81 2.81 91-13 88.32 MW-1 9/1/2009 5.92 5.82 91.13 85 31 1/6/2000 5-20 11.78 11.78 635.48 623.70 9/20/2002 15-43 15.43 98.49 83.06 10/14/2002 12.16 12.16 449 86.33 3/18/2003 7.80 7.80 98-49 90.69 4/18/2003 9.19 9.19 98-49 89-30 5/20/2003 10-48 10.48 98.49 88.01 5/27/2004 10-71 10.71 98.49 87.78 NIW-6 8/2512004 10.96 1096 98-49 87.53 3/27/2009 6.53 6 5 3 9l .28 84-75 4/28/2009 10-28 -- 10-28 91.28 81.00 5/28/2009 5.55 5.55 91.28 85.73 9/1/2009 9.61 9.61 91.28 81-67 5/212013 8.28 8.28 91.28 83.00 in/2000 10-15 3.72 3.72 634.63 630.91 7/11/2000 4.55 4.55 634.63 630.08 9/20/2002 10-43 10.43 98-96 88-53 10/14/2002 9.41 9.41 98-96 89-55 3/18/2003 0.80 0.80 98.96 98-16 4/18/2003 0.91 -- 0.91 98.96 98.05 5120/2003 1.23 -- 1.23 98-96 97-73 MW-9 5/27/2004 3.74 -- 3.74 98-96 95-22 8125/2004 1.11 1.11 98.96 97-85 3/27/2009 1.83 -- 1-83 90-43 88-60 3/30/2009 1.84 -- 1.84 90-43 88-59 4128/2009 0-80 0.80 90.43 89.63 5/28/2009 0-00 -- 0-00 90-43 90-43 9/1/2009 0.95 -- 0.95 90-43 89.48 4/28/2009 40-50 1-50 -- 1-50 90-94 8934 5/28/2009 2.65 -- 2.65 90.94 88.19 9/3/2009 5.97 -- 5.97 90.84 84.87 MW-913 1 /412012 1-66 -- 1-66 90.94 89.18 4/11/2012 1.22 1.22 90.84 89.62 7/24/2012 Well Buried 1/7/2000 l 1 1 6.37 6.37 635-56 629.19 7/11/2000 8.52 8.52 635-56 627.04 9/20/2002 6.10 6.10 98.46 92.36 10/14/2002 2.39 2.39 98.46 96.07 3/18/2003 1.48 1.48 98.46 96.98 4/ 18/2003 1.44 1.44 99.46 97.02 5/20/2003 3.33 3.33 98.46 95.13 MW10 5r2712004 310 3.10 98.46 95-36 8/25/2004 3.34 3.34 98.46 95.12 3/27/2009 178 1.78 91.36 89-58 4/28/2009 2.41 2-41 91.36 88-95 5/28/2009 3.15 - 3.15 91.36 88.21 9/1/2009 4.27 -- 4-27 91.36 87.09 5/21/2013 2 23 2-23 91-36 89.13 1 of 6 APPENDIX A2 Historical Groundwater F.ievation Data Tras•elCeaters of America I101 NC Flighway 61 1lhitsett, Guilford County. North C'arutina Facilit 1.D.: "29186 Incident Numher.: 20053 "Al I Date Screened Iufe" al {top to bottom of Screen feet} Depth to R'9ter- Uncorrected (fret) � Free Product Fiuckoess (feed Depth to'A rater- Corrected ifeet) Top of Casing Fle► ation {feet] Groundwater Surface Elevation (feet) - 117r2000 1 1 1-1 . 12.73 1273 638.41 625.68 711 112000 8-19 8.19 639.41 630-22 9/20/2002 8.36 836 101.16 92- 80 10/14/2002 5.94 594 101.16 95.22 3/18/2003 3.45 -- 345 101.16 97.71 4/18/2003 2.85 - 2.85 101.16 98.31 5/20/2003 3.81 -- 3.81 101.16 97.35 5/27/2004 5.27 -- 527 101.16 95.89 9/25/2004 5.71 -- 5.71 101.I6 95-45 3/23/2009 3.26 -- 3.26 94 21 90.95 312V2009 3.26 3.54 94.21 90A7 3/30/2009 3.97 3 97 94-21 9024 4/29/2009 426 426 94.21 89.95 MW-11 5/28/2009 3.92 3.92 +-t 21 cr0 29 9/112009 651 6.51 94.21 87.70 10/4/2010 5.41 541 94.21 88-80 116t2411 1 6.60 660 94.21 87-61 4/14/2011 Well Buried 7/14/2011 4 55 - 4.55 94.21 89.66 1011812011 5.63 .563 94 21 88.58 1/4/2012 4.38 4.38 94.21 89.83 4/11/2012 4.25 4.25 94.21 89.96 7/24/2012 4.32 - 4.32 94.21 89.89 i 115f2012 6.18 6.18 94.21 88-03 5/21/2013 4.34 4 34 9421 89 87 P712000 10-15 8-85 -- 8 85 636.84 627.99 W1112000 13 37 4 Ky 9.70 636.84 627.14 9/20C1002 7.29 0.25 7.09 99.70 92.61 10/14/2002 4.22 0.08 4.16 99.70 95.54 311M003 3.47 0.25 3 27 99.70 96.43 4/19/2003 4.26 4-26 99.70 95.44 5120/2003 3.77 0 01 3.77 99.70 95.93 5/27/2004 4.46 4-46 99.70 95.24 MW-I2 8125C2004 5-83 -- 5.83 99.70 93.87 3/2712009 3.54 -- 3-54 92.64 89.10 3/31/2009 3.71 - 3-71 92.64 88.93 4/28/2009 3.75 3-75 92.64 88.89 5/28/2009 4.10 - 4.10 92.64 98.54 9/1/2009 5.39 -- 5.39 92.64 87.25 10/4/2010 4.55 -- 4.55 92.64 88.09 116/201 l 5 33 -- 533 92 64 87 31 4/14/201 1 Well Buried or Destroyed 9/20/2002 21, 9.09 9.09 100.81 91.72 10114PM)2 2.14 2-14 100.81 98.67 3/18/2003 0.00 -- 0.00 100.81 100.81 4/18/2003 0.00 0.00 100. 8 ] 100. 81 5/20/2003 1 " -- 1-22 100.81 99.59 kris~,- 11 5/27/2004 + , 4 -- 3-28 100.81 97.53 8/25/2004 3.83 3.93 100.81 96.98 3/27/2009 0.00 0.00 9374 93 74 4/280-009 1 35 1.35 93 74 92.39 5/28/2009 1.89 - 189 93.74 91.85 9/1/2009 5.52 5.52 93 74 88.2? 4/14/201 1 Well Buried or Destroyed if iI APPENDIX A2 Historical Groundwater Elevation Data TravelCenlers oFAmerica 1101 NC highway 61 Whitseit, Guilford County, North Carolina Facifin I.D.: 0-029186 incident Number.. 20054 Well ID Date Screened Interval {top to bottom of screen ftt t Depth to !Pater- Uncorrected [feet] Free Product rhi&ness (feet) Depth to Water- Corrected (feet) Top of Casing Elevation [feet] Groundwater 5urFace Elevation (feet) 9/20/2002 6-20 16-71 16.71 99.91 83-20 10/14/2002 12-31 12.31 99.91 87-60 3/ 19/2003 2.03 2.03 99.91 97.99 4/18/2003 1.52 1.52 99.91 98-39 5/20/2003 3.68 3.68 99.91 96.23 5/27/2004 4-94 4.94 99.91 94.97 M W-14 8125/2004 5.14 5.14 99.91 94.77 3/23/2009 2-21 221 92.86 90.65 3/27/2009 2.85 - 2.85 92.86 90.01 4/28/2009 3-56 3.56 92.86 89.30 5/29/2009 4.34 4.34 92.86 88.52 9/1/2009 7-23 7.23 92.86 85.63 4/14/2011 Well Buried or Destroyed 9/20/2002 4-14 5.78 5.78 98-07 92.29 10/14/2002 3.65 -- 3.65 98.07 94.42 3/18/2003 0-70 0.70 98.07 97.37 4/ 18/2003 1-07 -- 1.07 98-07 97.00 5/20/2003 1-73 - 1.73 98.07 96.34 5/27/2004 4-15 -- 4.15 98.07 93.92 Mw-15 8/25/2004 4-34 -- 4.34 98-07 93.73 3/27/2009 2.84 - 2.84 92-24 89-40 4/28/2009 3-05 -- 3.05 92.24 89.19 5/28/2009 3-53 -- 3-53 92.24 98.71 9/1/2009 5-37 - 5-37 92-24 86-87 5/21/2013 2 79 -- 2.79 92-24 89-45 9120/2002 4-14 7.65 - 7.65 99-29 9164 10/14/2002 0.08 0.08 9929 99-2I 3/18/2003 0.00 - 0.00 99.29 99.29 4/1812003 0.00 - 0-00 99.29 99.29 5/20/2003 0.00 - 0-00 99.29 99.29 5127r2004 1.68 - 1-68 99.29 97.61 MW-16 8/25/2004 1.72 - 1-72 99.29 97.57 3/23/2009 0.00 - 0.00 91.00 91.00 3/27/2009 0.00 0.00 91.00 91.00 4/28/2009 0.00 -- OAO 91.00 91.00 5/28/2009 0.52 - 0.52 91.00 90.48 9/Z/2009 2.47 -- 2.47 91.00 88.53 411412011 Well Buried or Destroyed 9/20/2002 ;-1 ' 6-77 -- 6.77 98-73 91.96 IOJ14/2002 2-33 -- 2.33 98-73 96.40 3/18/2003 2-00 -- 2.00 98-73 96-73 4118/2003 1.92 - 1-92 98-73 96-81 5/20/2003 1-81 -- 1.81 98-73 96-92 M W- I7 5/27/2004 2.62 2-62 98-73 9611 (AW-17) 8/25/2004 2.92 -- 2.92 98.73 95.81 3127120 0 0.00 - 0-00 91.67 91.67 4/28120ij9 0.31 - 0-31 91.67 91.36 5/28/2009 1.08 - 1.09 91.67 90.59 9/1/2009 Could not locate well 41I41201 t Well Buried or Destroyed 3of6 APPENDIX A2 historical Groundwater EWa[ion hats TraveiCenters of America 1101 tiC Highway 61 1►hitseit, Guilford County, North Carolina Facility 1.D.: 0-029186 Incident lumber.: 20054 e Interval f.top to bottom of screen Depth to Water- L nrorrected {feet) Free Product l hirkness (feet) Depth to Water- C:nrrerted (feet) 'f op of Casing Elevation (feet) Groundwater Surface Etev urf a (Fret) 03 2.5-12 5 2.87 2.97 100.53 97.66 tScreened 4/18/2003 03 2.93 - 2.93 100.53 97b0 03 3.76 - 376 100.53 96.77 04 4.91 - 4.91 100.53 95.62 004 5.24 - 524 100.53 95.29 09 3.48 - 3.48 93.52 9004 009 3.38 - 338 9352 90.14 009 4.05 -- 4.05 93.52 89.47 5/28/2009 4.01 - 4.01 93.52 89.51 911 /2009 5.93 5.93 93.52 87.59 l-M W- l 10/4/2010 4.62 4.62 93.52 8890 1/6/2011 5.81 5.81 93.52 87.71 4/14/2011 3.80 - 3.80 93.52 89.72 7/14/2011 3.91 - 3.91 93.52 89.61 10/18/2011 5.95 - 5.95 93.52 87.57 11412012 3.95 -- 3.95 93.52 89.57 4/11/2012 3.86 -- 3.86 93.52 89.66 7/24/2012 3.92 -- 3.82 93.52 89.70 11/5/2012 5.63 -- 5.63 93.52 87.89 5/21 /2013 3.97 3.97 93.52 89.55 3/18/2003 2.12.5 2.63 2.63 100.07 97.44 4/18/2003 2.55 -- 255 100.07 97.52 512W2003 3.32 3.32 100.07 96.75 5/27/2004 4.52 4.52 100.07 95.55 8/25/2004 4.93 -- 4.93 100.07 95.14 3/27/2009 3.09 -- 3.09 92.98 89.89 3/31/2009 3.65 -- 3.65 92.98 89.33 4/28/2009 3.50 -- 3.50 92.98 89.48 5/28/2009 3.22 -- 3.22 92.9$ 89.76 9/1/2009 5.48 -- 5.48 92.98 87.50 USTMW-2 10/4/2010 3.86 -- 3.85 92.98 89.13 1/6/2011 5.54 -- 5.54 92.98 87.44 4/14/2011 3.34 -- 3.34 92.98 89.64 7/14/2011 3.47 3.47 92.98 89.51 10/19/2011 4.89 -- 4,89 92.98 89.09 1/4/2012 3.58 -- 3.58 92.98 99.40 4/11/2012 3.45 -- 3.45 92.98 89.53 7/24/2012 3.30 -- 3.30 92.98 89.68 11/5/2012 4.43 - 4.43 92.98 89.55 5121 f2013 3.49 -- 3.49 92.98 89.49 3/18/2003 15-1 1.5 2.90 -- 2.90 99.36 96.46 4/ 18/2003 3.15 - 3 15 99.36 96.21 5/20/2003 3.30 - 3.30 99.36 96.06 5/27/2004 3.96 - 3.96 99.36 95.40 8/25/2004 4.33 - 4.33 99.36 95.03 3/27/2009 3.13 3.13 92.32 89.19 3/31/2009 3.14 3.14 92.32 89.18 4/28/2009 3.30 3.30 92.32 89.02 5/2812009 3.18 3.18 92.32 89.14 USTMW-3 9/1/2009 4.79 - 4.79 92.32 87.53 1/6/2011 4.93 -- 4.93 92.32 87.39 4/140-011 3.25 3.25 92.32 89.07 7/14/2011 3.34 3.34 92.32 88.98 10/18/2011 3.31 - 4.31 92.32 88.01 114f2012 3.30 -- 3.30 92.32 89.02 4/11/2012 3.16 -- 3.16 92.32 89.16 7/24/2012 3.26 -- 3.26 92.32 89.06 4 of 6 APPENDIX A2 Historical Groundwater Elevation Data TravelCenters of America 1101 NC Highway bI Whitsett, Guilford County, North Carolina Facility I.D.:0-029186 Incident umber.: 20054 Screcned Depth to Hater- Groundwater Interval [top to Free Product Depth to Water- Top of Casing Well In Date [�ncorrcrted Surface Woo of streen Thickness (fect) Corrected (feet) Elevation [feet] (feet) Elevation [feet] feet) _ ti ti ti7 I i 5 r)t E; APPENDIX A2 Ilistorical Groundwater Elevation Data TravelCenters of America I101 NC Ilighway 61 Whitsett, Guilford County, North Carolina Facility 1.d.-0-029186 Incident dumber.: 20054 Well ID ate Screened Interval Ilop to bottom ofsereen feet] Depth to ►%'nice- Uncorrected ed (Pert] Free Product Thickness (feet) Depth to ►Pater- Corrected (feet) Tap of Casing Elevation (feet) Groundwater Surface Elevation [feet) ( 5/20/2003 t, rr .3 n 3.36 NS 5/27/2004 456 4.56 NS -- 8/25/2004 3.71 -- 5.71 NS - 3127f2009 3.11 -- 3.11 93.01 89.90 3/3112009 3.14 -• 3.14 93.01 89.87 4/28/2009 3.56 -- 3 56 93.01 89.45 5/28/2009 3.31 -- 3.31 93.01 89.70 9/1/2009 5.39 -• 5-39 93.01 87.62 MAJ2010 3.90 -- 3.90 93.01 89.11 USTMW-4 1/6/2011 5-64 5.64 93.01 87.37 4/14/2011 3.41 3-41 93.01 89.60 7114f2011 3-45 - 3.45 93.01 89.56 10/18/2011 5.20 - 5-20 93.01 87.81 1/4/2012 3.60 - 3-60 93.01 89-41 4/11/2012 3.44 3-44 93.01 89-57 7/24/2012 3-31 3-31 93.01 99.70 11/5/2012 4.89 489 93.01 88-12 5/21/2013 3-52 3.52 93.01 89-49 9/20/2002 1.111, 7.63 - 7.63 100-21 92.58 10/14/2002 3.91 -- 3.91 100.21 96-30 3/18/2003 3.57 0.45 3.57 100.21 97.00 4/18/2003 3 31 -- 3.31 100.21 96.90 5/20/2003 4.84 - 4-84 100.21 95.37 5/27/2004 4.80 -- 4-90 100.21 _ 95.41 8/25/2004 5.16 - 5-16 100.21 95.05 3/27/2009 3.65 - 3.65 93.12 89.47 3/31/2009 3.87 -- 3.97 9312 89.25 4/28/2009 4.02 4-02 93-12 89.10 5/28/2009 3.69 3.69 93.12 89.43 AGM-RW 9/1/2009 5-63 5.63 93.12 87.49 10/4/2010 441 4.41 93.12 88.71 1/6/2011 5.72 5.72 93.12 87.40 4/14/2011 3.89 3.89 93.12 89.23 7/14/2011 3.92 - 3.92 93.12 89.20 10/18/2011 5.59 -- 5.59 93.12 87.53 1 /412012 4- t 2 -- 4.12 9112 89-00 411 t12012 3.84 -- 3.84 93. l2 89-28 7/24/2012 3-79 -- 3.78 93.12 89-34 11/5%012 5-31 -- 5.31 93.12 87.81 5121MU 3.72 - 3.72 92-70 88.98 NOTES: 1) ft bgs-Feet below grade surface 2] Tap of rasing elevations based on an arbitraury datum of 100 feet 3 Top of casi ng elevations were measured on April 28, 2009. 6of6 :Appendix :'13 Historical Groundwater Elevation Data rraveWenters of :America 110i NC Highway 61 WhWe", Guilford County, North Carolina Facility 1,D,: "29186 Incident Number.: 30318 Well ID Date Screened Interval (top or screen to bottom of screen in feet Depth to Water- L'ncorrreted (ft bgs) Free Product Thickness (feet) Depth to Water- Corrected (ft s Casingon (fret) Top Elevation Groundwater Surface Elevation 3/18/2008 = 1 = 7-52 ; 100.00 92.48 41I12009 0+ 0+ 100.00 >100.00 4/28/2009 5.03 5,03 100.00 94.97 MW-4 5/28/2009 7.21 7-21 100.00 92.79 91112009 10-93 10.93 100.00 89.07 12/22/2009 0+ 10.93 100.00 >100.00 719120E 3 Abandoned 3/27/2009 4-M 2.84 2-94 92-24 89.40 4/28/2009 3-05 - 3-05 92.24 89.19 5/28/2009 3-53 3-53 92.24 88.71 MW-15 9/1/2009 5-37 5.37 92-24 86.87 12/22/2009 1,83 1-83 92.24 90.41 5/21/2013 2-79 - 2-79 92.24 89.45 3/24/2009 16-31 24,80 24.90 94-18 69.38 3/31/2009 7-12 7-72 94.18 86.46 4/1/2009 7-69 7.69 9418 80.49 4/28/2009 8-50 8-50 94-19 85.68 5/28/2009 9-01 - 9-01 94-18 85.17 9/112009 9-82 9-92 94-18 84.36 12/22/2009 6-87 6-87 94-18 87.31 10/4/2010 10.23 10.23 94.18 83.95 CSAMW-1 1/6/2011 1100 11.00 94,18 83.18 4/14/2011 6-81 6-91 94-18 87.37 10118120] 1 10-02 10.02 94-18 84.16 1/4/2012 8-35 8-35 94,18 85.83 4/11/2012 8-00 8,00 94.18 86.18 11/5/2012 8-78 - 8-78 94-18 85.40 5121 /2013 7.33 7.33 94. i 8 86.85 3/31/2009 60-70 18.05 -- 18-05 97-75 79.70 4/28/2009 44.15 - 44-i5 97-75 53.60 5/28/2009 3.22 - 3.22 97.75 94.53 9/1/2009 19.06 -- 19-06 97.75 79.69 12/22/2009 15.70 15.70 97-75 82.05 10/4/2010 16.44 16.44 97.75 81-31 i1612011 17.65 17.65 97.75 80-10 CSAMW-2 4/14/2011 11.52 I1.52 97.75 86.23 10/18/2011 13.89 13-89 97.75 83-86 1/4/2012 14.18 14.18 97.75 83.57 4/11/2012 13.41 13,41 97.75 84-34 11/5/2012 13-72 1172 97.75 84-03 5/21/2013 1247 12 3' 97.75 95.29 3/31/2009 10-25 5.48 ; 44 98.39 92.91 4/1/2009 2.79 - 279 98.39 95.60 4/28/2009 3.30 3-30 98.39 95.09 5/28/2009 3.18 3-18 98.39 95.21 9A/2009 9.88 9.88 98-39 88.51 CSAMW-3 12/22/2009 3.05 3-05 98,39 95.34 10/4/2010 7.57 7-57 98-39 90.82 11612011 10.51 - 10.51 98-39 87.98 4/14/2011 5.12 -- 5.12 98-39 93.27 10/18/201 1 11.95 - 11-95 98-39 86.44 1/4/2012 10.83 - i0-83 98-39 87.56 I of 2 Appendix .1.3 Flistorical Groundwater Elevation Data TravelCeattrs of America 1101 NC Highway 61 WItitsett. Guilford Couaty. North Carolina Facility I.D.:0-029186 Incident Number.. 30318 Well 1D Datt - WEM-MIW� Screened Internal [tap of screen to bottom of screen in feel Depth to d ( ter- i'ntuFFe.[t�t ift I►gsj Free Product 1•birkness (feet) Depth to Water- Corrected {ft I ap ti Casing fet �'.ilVattali (feet) - Groundwater Surface Eltvation - w 4/11/2012 10.46 10-46 98-39 87 v; LSAMW-3 11/52012 11.78 11.78 98.39 M !, l 5/212013 6.91 6-91 98-39 91-48 3/31/2009 65-15 53-10 53.10 99.09 45.99 4128/2009 3.56 3.56 99.09 95-53 5/28/2009 3-31 3.31 99.09 95.78 9/1/2009 13.37 13.37 99.09 85.72 12/2212009 9.97 9.97 99.09 89.12 10/4/2010 13.74 13.74 99.09 85.35 1/6/2011 16.56 16-56 99.09 82.53 C5AMW-4 4/14/201 1 15-15 15.15 99.09 83.94 10/18/2011 13.00 13.00 99.09 86.09 1/4/2012 14.15 14- l5 99-09 84.94 4/11/2012 13.92 13.92 99.09 85.17 11/52012 12.90 12.80 99.09 8629 521/2013 6.91 6.91 98.39 91.49 10/32006 15.29-29.65 _ 16.94 16.94 101.22 84-28 3/31/2009 4.29 0-05 4-33 97-78 93.45 4/28/2009 5.54 - 5.54 9778 9224 5/28/2009 8.05 - 8.05 9778 89.73 9/1/2009 10.43 10.43 9778 87-35 1222/2009 4.29 - 4.28 97.78 93.50 1014i2010 9-56 - 9-56 97-78 88.22 DDMW2 1/6/2011 10-64 - 10.64 97.78 87.14 4/142011 6-65 6.65 97.78 91.13 10/18/2011 11-68 11.68 97.78 86.10 1/42012 12-69 12.68 97.78 85.10 4/11/2012 9.02 - 9.02 97.78 88.76 11/512012 1484 - 14.84 97 78 82.94 521/2013 569 5.69 9778 92.09 2 Qf2 APPENDIX B LABORATORY REPORTS AND CHAINS OF CUSTODY . Southeast E ACCUTE=-E3- " LAU0PAr L]cIk1. Technical Report for Atlantic Richfield Company URSNCM: 51S 1363, 1101 Hwy 61, Whitsett, NC 01363-38436751.106081 Accutest job Number: FA4878 Sampling Date: 05/21/13 Report to: URS Corporation martha. meyers-lee@ urs. cam ATTN: Martha Meyers Total number of pages in report: 16 e-Hardeopy Z 4 t ►llomerfeel Repew I ► ��4 ►th AC CpR6 4 T: b .a t S Test results contained within this data package meet the requirements Harry Behzadi, Ph.D. of the [National Environmental Laboratory Accreditation Conference Laboratory Director and/or state specific certification programs as applicable. Client Service contact: Heather Wandrey 407-425-6700 Certifications: FL (E83510), LA (03051), Its (E-10327). IA (366), IL (200063), NC (573), NJ (FL002), 5C (96038001) DoD FLAP (L-A-13 L2229), CA (04226CA), TX (T104704404), AK, AR, GA, KY, MA, NV, OK. UT. VA, WA, Wl This report shall not be reproduced, except in its entirely, without the written approval of Accutest Laboratories. Test results relate only to samples analyzed. Southeast • 4405 Vineland Road • Suite C. 15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 • hitp!//www.accutesi.com 0 1 of 16 Accutest Laboratories is the sole authority for authorizing edits or modifications to this ®.4CCu'TE�T. FA4878 document. l ]nauthorized modification of this report is strictly prohibited. •,,• •"• , Table of Contents Section 1: Sample Summary..............................1.................................................................... Section 2: Case Narrative/Conformance Summary .............................................................. Section 3: Summary of Hits.................................................................................................... Section 4: Sample Results........................................................................................................ 4.1: FA4878-1: 1301 PINEY GROVE R.D-IN.................................................................... 4.2: FA4878-2: 1301 PINEY GROVE RD-MID................................................................. 4.3: FA4878-3: 1301 PINEY GROVE RD-EFF................................................................. Section5: Misc. Forms...... ..................................................... m ................................ ­.­­ ...... 5.1: Chain of Custody........................................................................................................... Section 6: GUMS Volatilcs - QC Data Summaries.............................................................. 6.1: Method B lank Summary ................................................................................................ 6.2: Blank Spike Summary................................................................................................... 6.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... Sections: 3 4 6 7 8 9 10 11 13 14 15 16 s■ 2 of 16 AG�LJTEST. FA4878 •,......•... Accutest LabLink913:57 05-Jun-2013 Sample Summary 1� Atlantic Richfield Company Job No: FA4878 URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC Project No: 01363-38436751.106081 'ample Collected Matrix Client lumber Date Time By Received Code Type Sample ID FA4878-1 05/21/13 14:55 JWJM 05/22/13 AQ Water FA4878-2 05/21/13 14:50 JWJM 05/22/13 AQ Water FA4878-3 05/21/13 14:45 JWJM 05/22/13 AQ Water 1301 PINEY GROVE RD-IN 1301 PINEY GROVE RD-MID 1301 PINEY GROVE RD-EFF .:. 3 of 16 FA4878 °"""' SAMPLE DELIVERY GROUP CASE NARRATIVE Client: Atlantic Richfield Company Job No: FA4878 1� Site: URSNCM: S/S 1363, 1 101 Hwy 61. Whitsett. NC Report Date 6/5/2013 11:52:51 AM 3 Samples were collected on 05/21/2013 and were received at Accutest SE on 05122/2013 properly preserved at 2.6 Deg. C and intact. These Samples received an Accutest job number of FA4878. A Iisting of the Laboratory Sample 1D, Client Sample lD and dates of collection are presented in the Results Summary Section of this report. Except as noted below, all method specified calibrations and quality control performance criteria were met for this job. For more information, please refer to QC summary pages. Volatiles by GCMS By Method SM 6200B Matrix: AQ Batch ID: VA1265 All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. Sample(s) FA4878-2MS.1 A4878-2MSD were used as the QC samples indicated. Accutest Laboratories Southeast (ALSE) certifies that this report meets the project requirements for analytical data produced for the samples as received at ALSE and as stated on the COC. ALSE certifies that the data meets the Data Quality Objectives for precision, accuracy and completeness as specified in the ALSE Quality Manual except as noted above. This report is to be used in its entirety. ALSE is not responsible for any assumptions of data quality if partial data packages are used Narrative prepared by: Date: June 5. 2013 L.ovelie Metxgar, QA Officer (signature on file) Wednesday, June 05, 2013 Page 1 of 1 min 4 of US ACC LJTEt3T. FA4878 .,.a-..q... Summary Of Hits Page 1 of 1 Job Number: FA4878 Account: Atlantic Richfield Company Project: URSNCM: S/S 1363, 1101 Hwy 61, Whitsett, NC Colleded: 05/21 /13 Lab Sample ID Client Sample ID Result/ Analyte Qua] RL MDL Units Method FA4&7&1 1301 PINEY GROVE RD-IN 1,2-Dichloroethane 0.41 J Di -Isopropyl ether 0.24 J Methyl Teri Butyl Ether 6.2 FA4&7&2 1301 PINEY GROVE RD-MID No hits reported in this sample. FA487&3 1301 PINEY GROVE RD-EFF Methyl chloride 0.24 J 0.50 0.10 ug11 SM 6200B 0.50 0.10 ug11 SM 6200B 0.50 0.10 ugll SM 6200B 0.50 0.11 ugll SM 6200B IC-4 ■■ 5of16 ACClJ7EST. FA4878 °••.. Section 4 . Southeast a ACCUTEST' L Af3oRATpq I[S Sample Results Report of Analysis I: ■ 6of16 ■.4CCUTEST. FA4878 `••""•,� Accutest LabLink@>13:57 05-Jun-Z013 Report of Analysis Client Sample ID: 1301 PINEY GROVE RD-IN Lab Sample ID: FA4878-1 Date Sampled: 05/21/13 Matrix: AQ - Water Date Received: 05/22/13 Method: SM 6200B Percent Solids: nla Project: URSNCM: S/S 1363, 1101 Hwy 61, Whitsett, NC Page I of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0180498.1) 1 06/04/13 TD nla nla VAIZ65 Run #2 Purge Volume Run # 1 10.0 mi Run #2 VOA Specisi List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.10 ugll 75-27-4 Bromodichloromethane ND 0.50 0.10 ugll 107-06-2 1.2-❑ichloroethane 0.41 0.50 0.10 ugll J 108.20-3 Di -Isopropyl ether 0.24 0.50 0.10 ugll J 124-48-1 Dibromochloromethane ND 0.50 0.10 ugll 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ugll 100-41-4 Ethylbenzene ND 0.50 0.10 ugll 99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug11 74-87-3 Methyl chloride ND 0.50 0.11 ug1l 1634-04-4 Methyl Teri Butyl Ether 6.2 0.50 0.10 ug1l 91-20-3 Naphthalene ND 0.50 0.15 uglf 108-88-3 Toluene ND 0.50 0.10 ugll 79-01-6 Trichloroethylene N❑ 0.50 0A0 ugll 1330-20-7 Xylene (lotalj ND 1.5 0.22 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 ❑ibromofluoromethane 97% 70-130% 17060-07-0 1,2-Dichloroethane-D4 98% 70-130% 2037-26-5 Toluene-D8 100% 70.130% 460-00-4 4-Bromofluorobenzene 102% 70-130% ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■m 7of16 AGCIJTEST. FA4878 ••°•• �••• Acculest LahLink@13:57 05-jun-2013 Report of Analysis :it Sample ID: 1301 PINEY GROVE RD-MID Sample ID: FA4878-2 rix: AQ - Water hod: 5M 6200B ect: URSNCM: SIS 1363, 1101 Hwy 61. Whitsett, NC File ID DF Analyzed By Prep Date #1 A0180499.1) 1 06/04/13 TD nla #2 Purge Volume Run #1 10.0 ml Run #2 Page I of I Date Sampled: 05/21/13 N Date Received: 05/22/13 Percent Solids: nla Prep Batch Analytical Batch nla VA1265 VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.10 ugll 75-27-4 Bromodichloromethane N❑ 0.50 0.10 ugll 107-06-2 1,2-Dichloroethane N❑ 0.50 0.10 ugll 108-20-3 Di -Isopropyl ether N❑ 0.50 0.10 ugll 124-48-1 ❑ibromochloromethane N❑ 0.50 0.10 ugll 156-59-2 cis- 1, 2-Dichloroethylene ND 0.50 0.10 ugll 100-41-4 Ethylhenzene N❑ 0.50 0.10 ugll 99-87-6 p-Isopropyltoluene N❑ 0.50 0.10 ugll 74-87-3 Methyl chloride ND 0.50 0.11 ugll 1634-04-4 Methyl Ter( Butyl Ether ND 0.50 0.10 ugll 91-20-3 Naphthalene N❑ 0.50 0.15 ugll 108-88-3 Toluene ND 0.50 0.10 ugli 79-01-6 Trichloroethylene ND 0.50 0.10 ugll 1330-20-7 Xylene (total) N❑ 1.5 0.22 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits. 1868-53.7 Dibromofluoromethane 97% 70-130% 17060-07-0 1,2-Dichloroethane-D4 98% 70-130% 2037-26-5 Toluene-D8 101% 70-130% 460-00-4 4-Bromofluorohenzene 103% 70-130% ND = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range j = Indicates an estimated value B = Indicates analyse found in associated method blank N = Indicates presumptive evidence of a compound ■w 8of16 A.r_=-U' 't;ST. FA4878 .• .....•• Accutest Labl.ink@13:57 05-Jun•2013 Report of Analysis Client Sample ID: 1301 PINEY GROVE RD-EFF Lab Sample ID: FA4878-3 Date Sampled: 05/21/13 Matrix: AQ - Water Date Received: 05/22/13 Method: SM 6200B Percent Solids: nla Project: URSNCM: SIS 1363. 1101 Hwy 61. Whitsett, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0180500.D 1 06/04/13 TD nla nla VA1265 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.10 ugll 75-27-4 Bromodichloromethane N❑ 0.50 0.10 ugll 107-06-2 1,2-Dichioroethane N❑ 0.50 0.10 ugll 108-20-3 Di -Isopropyl ether ND 0.50 0.10 ugll 124-48-1 Dibromochloromethane ND 0.50 0.10 ug11 156-59-2 cis- 1.2-Dichloroethylene ND 0.50 0.10 ugll 100-41-4 Ethylbenzene ND 0.50 0.10 ugll 99-87-6 p-Isopropyltoluene ND 0.50 0.10 ugll 74-87-3 Methyl chloride 0.24 0.50 0.11 ugll j 1634-04-4 Methyl Teri Butyl Ether N❑ 0.50 0.10 ugll 91-20-3 Naphthalene ND 0.50 0.15 ugll 108-88-3 Toluene ND 0.50 0.10 ugll 79-01-6 Trichloroethylene N❑ 0.50 0.10 ugll 1330-20-7 Xylene [(otal} ND 1.5 0.22 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 97% 70-130% 17060-07-0 1,2-Dichloroethane-D4 98% 70-130% 2037-26-5 Toluene-138 102% 70-130% 460-00-4 4-Bromofluorobenzene 103% 70-130% ND = Not detected MDL - Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = indicates analyze found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound mks 9of16 ■ ACCUTEST FA4878 ••'"• "• �• Section 5 Southeast AE;CUTEE;T L A B O R AT OR I E$ Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody A �■ 10 of 16 .occuT�sT FA4818 "•"•• •• •• 7 by orm FA 4$73 Laboratory Management Program LaMP Chain of Custody Racord Page _1— M 1— pP SR. Mpd, 940: 01 W R+q pw Dab. IrMNd&W l: Ice.-..r. W" ran 3M Rrrh 7AT: Yam ^ No X 6F FacYRy NO: Lab YWw* p.n.r NunM.r AO Mrr1. I Frog Add. 1101 U1 MMa1 on. L�pne'KYer UPS Cnryvafv�-Hw G"r AOOr i 6 Y.Mf.N R..o. 6W C-5 0o FL SN 11 mv, sod. jlp Cad. Nomavt MC Prgp No 01361 • ]HSp61 I""I l.b PM Mp0w 91R" mod R.0lialory ApYCy MCDEMR plaal -11ST 5Kupn 1w PM.Ir w PUA Row. $rf. 400 ':.i &. NC 0W b ft— 4074256700 deal ID NP —muw YAna.ela PM wA Bw [ %*" .h SMppnp►m¢ AcaAwl 1CY36f5-3 rho Pruporl No 006LF0000 Gf9-N1 '10o Em.t IIL.m.I Yq'...1..�+. win lib BoM. Gnw Ilo Acmmanp ilo0. PnwMm AL- 000AU _ OOCAM _ Qpp T. Wr1]u Uftm FLrOun mm • w..+y.P Qt-;rft sww 6r AdFrtl4" 81 - OMOA Spend sP — Co "—O _x— P P,." M.r Grp Fn.an Mabl. No. ContiW .r. 1 PIM.rr.p.. R q+]. o d Ar]alyaw Rapon Type • OC Laval up PM?b 71a 2714740 �i 9 f i rrr777��� 51ano.,G F.O D.I. P.MK- gP PM E-0. frp Fn. &* min LAb SM IS paocrpt" pep Tuft CRr*urL.n4 n.a. e..+� rof v.w.i rocN we 13v1 PGrvr. Re.In CJ 71 l3 1 5� x 3 x ] 1301 F'-" Flo -Mtl ILf x 3 K 7 +701 P.y} plpys Rd - FJf Lis % ] x 3 r•e� . w.r l VA. ] W..W* .M RNnquhd d Ry ! AIMMIc l ap TRna Accopl.d Sy I AN MaWn pap Tl— sarnp.r. Ca rww.r uR6 cnRer.lrn NOM Ca.nff... T,4 vil 1 C c!1 <I3 [LfG sbgnl.r. ayawo F.cEx sNP Der � u 'fV1.20 IJrj3 ��[7 Sngm.m Tra¢Lp No Spaelal Inabruebona: R.l.r 1. ^-i 18Prp1. KR A"~lPr .n.ly ,".cop. W wa5. cooled.1.nT. M.n"jL,&a{sl"I.1 s1.1 r.p.rdlY.p 61. py—"Mrdwn.lyf j+wnt P+d.rHl. Mo... THL5 :INE - LAB C$E ONLY �..uTy Soft y Pk" Y..: T t WW Di. %L Yom; No C0o1./'.vnF e^ R�tt 'F2 ifp Bgnl 1'p{ I He My9�$p $.ropy gypnbp Y� 1 No RN..N Y R25052R 6P Rwo *ww. Mv4oF CAC - [111.5).. D.1.. A..pup 27. MI I1 lone 30 2:112 .P L.M. LbC ... r."U'soll FA4878: Chain of Custody Page l of 2 H ■� 11 of 16 � accuTEST PA4878 •••P,•T"I ACrrCUTEST LABORATORIES SAMPLEEI RECPT CONFMMATION -b-bpAccurESs JOB NUMBER: TA 78 _ CLIENT: 66S T'� -' ROIECT: � DAT ellIIbLlr RECEIVED: (MIMMDIYY I4:00� NUMBER OF COOLERS RECEIVED: METHOD OF DELIVERY: FSDYY UPS ACCUTEST COURIER CREVEOUND DELIVERY OTHER AIRBRL NUMBKm tqr-rTZf gQ"E t INF0 FCvj ]30N CUSTODY SEAL NOT PRXSRNT OR NOT INTACT CHAIN OF CUSTODY NOT RECEIVED (COC) ANALYSIS RSQUESrW IS UNCLEAR OR MISSING SAMPLE DATES OR TIMES UNCLEAR OR MISSING TEMPERATURE CRITERIA NOT MET L—JWET ICE PRESENT TRIP HL&M INFORMATION TRIP BLANK PROVIDED BLANK NOT PROVIDED BLANK NOT ON COC TRIP BLANK INTACT TRIP BLANK NOT INTACT RECEIVED WATER TRIP BLANK DRECRIVED SOIL TRIP BLANK NIISC. INFORMATION NUMBER OF ENCORES' NUMBER OF 5035 FIELD KITS ? NUMBER OR LAB FILTERED METALS? 6YIIu I;�.(J'4'L�I y TEMPERATEMPEBA111ZE INEQRMATION IA THERM M CORR, FACi'OR ±- O q - OBSERVED TEMPS: CORRECTED TEMPS: SAMPLE INFORMATION MPL.E LABELS PRESENT ON ALL U07T LIDS CORRECT NUMBER OF CONTAINERS US&D MPLE RECxr*MD IMPROPERLY PRESERVID SUMCIENT VOLUMM FOR ANALYSIS LTESM MISS ON CDC DO NOT MATCH SAMPLE LABEL 'S ON COC DO NOT MATCH LABtL W VIALS HAVE HKAMPAC8 {MACRO BUBBLIM M LES RECILP ien BUT ANALYSIS NOT REQUESTED ) BOTI7.E5 RECXIV'ED FOR ANALYSIS REQUESTED WL IZAR FILTERING OR COMPOSTITNG INSTRUCTIONS AIPL.E CONTAINERS] RItCEIVEI3 BROKEN SOLIDS JAR NOT RECSiVED 35 FIELD KIT VROEEN WITHIN 48 HOUR'S :SWUAL CHLOR]WE PRESENT WFICAS" TO TYA ROB SERMS OR NORTH CAROLWA OROAMCSI TECHNICIANSIGNATtMWATE r REVIF.WERSIGNATVREIDATS Hp 10149 RECEIPT CONFIRMATION 100609 (2)-As rn 3 FA4878: Chain of Custody Page 2 of 2 r:! MR 12 of 16 ACCLJ7EST. FAWS Section 6 . Southeast E ACCLJTEST L AS 0 RAT D R I E S GUMS Volatiles QC Data Summaries Includes the fallowing where applicable: • Method Blank Summaries ■ Blank Spike Summaries • Matrix Spike and Duplicate Summaries ■e 13 of 16 E ACC LJTr=ST. FA4878 ••�• ",•• Method Blank Summary Job Number: FA4878 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC Page 1 of 1 ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batck �A1265-MB A0180488.1) 1 06/04/13 TD nla nfa VA1265 The QC reported here applies to the following samples: Method: SM 6200B FA4878-1, FA4878-2, FA4878-3 CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.10 ugll 75-27-4 Bromodichloromethane ND 0.50 0.10 ugll 107.06-2 1,2-Dichloroethane ND 0.50 0.10 ugll 108-20-3 Di -Isopropyl ether ND 0.50 0.10 ugll 124-48-1 Dibromochloromethane ND 0.50 0.10 ugll 156.59-2 cis- 1,2-Dichloroethylene ND 0.50 0.10 ugll 100-41-4 Ethylbenzene ND 0.50 0.10 ugll 99-87-6 p-Isopropyholuene ND 0.50 0.10 ugll 74-87-3 Methyl chloride ND 0.50 0.11 ugll 1634-04-4 Methyl Ten Butyl Ether ND 0.50 0.10 ugll 91-20-3 Naphthalene N❑ 0.50 0.15 ugll 108-88-3 Toluene ND 0.50 0.10 ugll 79-01-6 Trichloroethylene N❑ 0.50 0.10 ugll 1330-20-7 Xylene (total) ND 1.5 0.22 ugll CAS No. Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 96% 70-130% 17060-07-0 1,2-Dichloroethane-D4 98% 70.130% 2037-26-5 Toluene-D8 102% 70-130% 460-00-4 4-Bromofluorohenzene 100% 70.130% 14 of 16 ACCiJTr=ST. FA4878 ` .......- Blank Spike Summary Job Number: FA4878 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: S/S 1363, 1101 Hwy 61, Whitsett, NC Page 1 of 1 ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batcl IA1265-BS A0180496.D 1 06/04/13 TD nla nla VA1265 The QC reported here applies to the following samples; FA4878-1, FA4878-2, FA4878-3 Spike BSP BSP CAS No. Compound ugll ugll % Limits 71-43-2 Benzene 10 9.9 99 70-130 75-27-4 Bromodichloromethane 10 9.3 93 70-130 107-06-2 1,2-Dichloroethane 10 10.7 107 70-130 108-20-3 DI -Isopropyl ether 10 8.5 85 70-130 124-48-1 ❑ibromochloromethane 10 8.6 86 70-130 156-59-2 cis- 1. 2- Dichloroethylene 10 9.7 97 70-130 100-41-4 Ethylhenzene 10 10.8 108 70-130 99-87-6 p-lsopropyltoluene 10 11.0 110 70-130 74-87-3 Methyl chloride 10 12.1 121 60.140 1634-04-4 Methyl Tert Butyl Ether I0 8.0 80 70-130 91-20-3 Naphthalene 10 10.3 103 70-130 108-88-3 Toluene 10 10.1 101 70-130 79-01-6 Trichloroethylene 10 10.8 108 70-130 1330-20-7 Xylene (total) 30 31.2 104 70-130 CAS No. Surrogate Recoveries BSP Limits 1868-53-7 Dihromofluoromethane 100% 70-130% 17060-07-0 1,2-Dichloroethane-D4 102% 70-130% 2037-26-5 Toluene-D8 100% 70-130% 460-00-4 4-Bromofluorobenzene 97`36 70-130% ' = Outside of Control limits. Method: SM 6200B �a 15 of 16 AJ--MUTEST. FA4878 " Ftl•,•" Matrix 5p ike/Matr ix Spike Duplicate Summary Page 1 of 1 Job Number: FA4878 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: S/S 1363, 1101 Hwy 61, Whi(sett, NC ;ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batcb FA4878-2MS A0180494.1) 1 06/04/13 TD nla nla VA1265 FA4878-2MSD A0180495.1) 1 06/04/13 TD nla nla VA1265 7A4878-2 A0180499.D 1 06/04/13 TD n/a nla VA1265 The QC reported here applies to the following samples: Method: SM 6200B FA4878-1, FA4878-2, FA4878-3 FA4878-2 Spike MS MS MSD MSD Limits CAS No. Compound ugll Q ug/l ugll % ugll % RPD Red"D 71-43-2 Benzene ND 10 9.8 98 9.5 95 3 70-130120 75.27-4 Bromodichlorome(hane ND 10 9.0 90 8.6 86 5 70-130120 107-06-2 1,2-Dichloroethane ND 10 10.3 103 10.4 104 1 70-130120 108-20-3 ❑i-Isopropyl ether ND 10 8.4 84 8.3 83 1 70-130120 124-48-1 Dibromochlorome(hane ND 10 8.2 82 7.8 78 5 70-130120 156-59-2 cis -1,2-Dichloroethylene ND 10 9.4 94 9.2 92 2 70-130120 100-41-4 Ethylhenzene ND 10 10.8 108 10.6 106 2 70-130120 99-87-6 p-Isopropyl(oluene ND 10 10.9 109 10.7 107 2 70-130120 74-87-3 Methyl chloride ND 10 11.4 114 10.6 106 7 60-140120 1634-04-4 Methyl Ter( Butyl Ether ND 10 8.0 80 8.0 80 0 70-130120 91-20-3 Naphthalene ND 10 10A 104 10.7 107 3 70-130/20 108-88-3 Toluene ND 10 10.0 100 9.9 99 1 70-130120 79-01-6 Trichloroethylene ND 10 I0.3 103 10.1 101 2 70-130120 1330-20-7 Xylene {to(al} ND 30 31.3 104 30.7 102 2 70-130120 CAS No. Surrogate Recoveries MS MSD FA4878-2 Limits 1868-53-7 Dibromofluoromethane 99% 100% 97% 70-130% I7060-07-0 1,2-Dichloroethane-D4 100% 101% 98% 70-130% 2037-26-5 Toluene-D8 99% 99% 101% 70-130% 460-00-4 4-Bromofluorobenzene 99% 98% 103% 70-130% * = Outside of Control Limits. ■:_ 16 of 16 O AC(--IJTEST. FA4878 .••°° e-Hardcopy 2.0 Automated Report M Southeast AccuTEST' L A❑❑ R A T❑ R I E 5 Technical Report for Atlantic Richfield Company URSNCM: S/S 1363, 1101 Hwy 61, Whitsett, NC 01363-38436751.106081 Accutest Job Number: FA4887 Sampling Date: 05/21/13 Report to: Corporation mar(ha . meyers-lee @urs . com ATTN: Martha Meyers Total number of pages in report: 32 �$� IN ACC6gQ 'g x�1 i s Test results contained within this data package meet the requirements garryehzadi, Ph.D. of the National Environmental Laboratory Accreditation Conference Laboratory Director andlor state specific certification programs as applicable. Client Service contact: Heather Wandrey 407-425-6700 Certifications: FL (E83510). LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001) Dol) FLAP (L-A-B L2229), CA (04226CA), TX (Ti04704404], AK, AR, CA, KY, MA, NV, OK, UT, VA, WA, WI This report shall not be reproduced. except in its entirety, without the written approval of Amtest Laboratories. Test results relate only to samples analyzed. Southeast • 4405 Vineland Road • Suite C- 15 • Orlando. FL 32811 • tel: 407.425.6700 • fax: 407-425-0707 - http://www.accutest.com : ■ 1 of 32 Accutest Laboratones Is tltc soie authority for authorizing cdivi or mod iIicatsons to this ACCLJTEST. document. t.Inauthoi-mcd mod ifit cat iun of this report is svlcd} prohibiter]. FAM7 Table of Contents -I- Section 1: Sample Summary................................................................................................... Section 2: Case Narrative/Conformance Summary.............................................................. Section3: Summary of Hits.................................................................................................... Section4: Sample Results........................................................................................................ 4.1: FA4887-1: MW-2R.............................................................. 4.2: FA4887-2: MW-3.................................................................................. 4.3: FA4887-3: MW-6.....................................................................................................--.. 4.4: FA4887-4: MW-8........................................................................................................ 4.5: FA4887-5: RW-1R....................................................................................................... 4.6: FA4887-6: VE-1........................................................................................................... 4.7: FA4887-7: VEW-1....................................................................................................... 4.8: FA4887-8: DUP-1........................................................................................................ 4.9: FA4887-9: TRIP BLANK............................................................................................ Section5: Misc. Forms............................................................................................................ 5.1: Chain of Custody........................................................................................................... Section 6: GUMS Volatiles - QC Data Summaries.............................................................. 6.1: Method Blank Summary................................................................................................ 6.2: Blank Spike Summary................................................................................................... 6.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... Sections: 3 5 7 8 9 10 11 12 13 14 15 16 17 18 20 21 25 29 �■ 2 of 32 ACCLJTE3T. FA4887 •••.•••"•,•• Accutest LabLink@ 14:32 05-Jun-2013 Sample Summary Atlantic Richfield Company Job No: FA4887 URSNCM: S/S 1363, 1101 Hwy 61, Whitsett, NC Project No: 01363-38436751.106081 Sample Colleded Matrix Client Number Date Time By Received Code Type Sample ID FA4887-1 05/21/13 14:20 JW 05/22/13 AQ Ground Water MW-2R FA4887-2 05/21/13 13:45 JW 05/22/13 AQ Ground Water MW-3 FA4887-3 05/21/13 12:15 JW 05/22/13 AQ Ground Water MW-6 FA4887-4 05/21/13 12:30 JW 05/22/13 AQ Ground Water MW-8 FA4887-5 05/21/13 14:00 JW 05/22/13 AQ Ground Water RWAR FA4887-6 05/21/13 12:50 JW 05/22/13 AQ Ground Water VE-1 FA4887-6D 05/21/13 12:50 JW 05/22/13 AQ Water Dup/MSD VE-1 FA4887-6S 05/21/13 12:50 JW 05/22/13 AQ Water Matrix Spike VE-1 FA4887-7 05/21/13 13:20 JW 05/22/13 AQ Ground Water VEW-1 FA4887-8 05/21/13 14:30 JW 05/22/13 AQ Ground Water DUP-1 FA4887-9 051Z1113 00:00 JW 05/22/13 AQ Trip Blank Water TRIP BLANK ■® 3 of 32 � .4CC{JT>=5T FA4887 •,•"••�••�• SAMPLE DELIVERY GROUP CASE NARRATIVE Client: Atlantic Richfield Company Job No: FA4887 Site: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC 1� Report Date 6/5/2013 2:34:02 PM 8 Samples and l Trip Blank were collected on 05/21/2013 and were received at Accutest SE on 45/22/2013 properly preserved, at 4.2 Deg. C and intact. These Samples received an Accutest job number of FA4887. A listing of the laboratory Sample ID, Client Sample ID and dates of collection are presented in the Results Summary Section ofthis report. Except as noted he low, all method specified calibrations and quality control performance criteria were met for this ioh. l or more information. please refer to QC summary pages. Valatiles by GCMS By Method SM 6200B Matrix: AQ Batch ID: VA1263 All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. Sample(s) FA4887-6MS. FA4887-6MSD were used as the QC samples indicated. Matrix: AQ Batch ID: VA1264 All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. Sample(s) F'A50024MS. FA50024MSD were used as the QC samples indicated. Matrix Spike Duplicate Recovery(s) for Naphthalene are outside control limits. Probable cause is due to matrix interference. For method performance in a clean matrix, refer to Blank Spike. Matrix: AQ Batch 10: VA1265 All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. Sample(s) FA4878-2MS. FA4878-2MSD were used as the QC samples indicated. Matrix: AQ Batch ID: VE832 All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. Sample(s) FA4924-24MS. FA4924-24MSD were used as the QC samples indicated. Matrix Spike Recovery(s) for Methyl Tent Butyl Ether are outside control limits. Outside control limits due to high level in sample relative to spike amount. Accutest Laboratories Southeast (ALSE) certifies that this report meets the project requirements for analytical data produced for the samples as received at ALSE and as stated on the COC. ALSE certifies that the data meets the Data Quality Objectives for precision. accuracy and completeness as specified in the ALSE Quality Manual except as noted above. This report is to be used in its entirety. ALSE is not responsible For any assumptions of data quality if partial data packages are used Narrative prepared by: Love Iie Metzgar, QA Officer (signature on file) XNrednesda►'. June 05, 2013 Date: ,lime 5. 2013 Page 1 of 1 Ca 4 of 32 accuTEsT FA48sr Summary of Hits Page 1 of 2 Job Number: FA4887 Account: Atlantic Richfield Company Project: URSNCM: S/S 1363, 1101 Hwy 61. Whiisett, NC Collected: 05/21/13 Lab Sample I❑ Chent Sample ID Result/ Analyte Qual RL MDL Units Method FA4887-1 MW-2R Benzene 5230 100 20 ug/l SM 6200E Di -Isopropyl ether 131 Z5 5.0 ug/l SM 6200B Ethylbenzene 421 25 5.0 ug/l SM 6200B Methyl Teri Butyl Ether 2480 25 5.0 ug/l SM 6200B Naphthalene 151 25 7.4 ug/l SM 6200B Toluene 287 25 5.0 ug/I SM 6200B Xylene (total) 655 75 11 ug/l SM 6200B FA4887-2 MW-3 Benzene 44.4 1.3 0.25 ug/l SM 6200B Di -Isopropyl ether 20.3 1.3 0.25 ug/l SM 6200B Ethylbenzene 1.2 j 1.3 0.25 ug/I SM 6200B Methyl Teri Butyl Ether 90.8 1.3 0.25 ug/l SM 6200B Naphthalene 1.9 1.3 0.37 ug/1 SM 6200B Toluene 1.3 1.3 0.25 ug/l SM 6200B Xylene (total) 2.5 ] 3.8 0.54 ug/l SM 6200B FA4887-3 MW-6 No hits reporters in this sample. FA4887A MW-8 No hits reported in this sample. FA4887-5 RW-1R Benzene 251 5.0 1.0 ug/1 SM 6200B Di -Isopropyl ether 178 5.0 1.0 ug/l SM 6200B Ethylbenzene 66,9 5.0 1.0 ug/l SM 6200B Methyl Tert Butyl Ether 149 5.0 1.0 ug/l SM 6200B Naphthalene 32.2 5.0 1.5 ug/l SM 6200B Xylene (total) 16.9 15 2.2 ug/l SM 6200B FA4897-6 VE-1 Di -Isopropyl ether 0.24 ] 0,50 0.10 ug/l SM 6200B Methyl Teri Butyl Ether 2.0 0.50 0.10 ugll SM 6200B FA4887-7 VEW-1 Methyl Teri Butyl Ether 0.48 j 0.50 0.10 ug/l SM 6200B �■ 5 of 32 ACCLJTEST. FA4887 ••"•• '• •• Summary of Hits Page 2 of 2 Job Number: FA4887 Account: Atlantic Richfield Company Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC Collected: 05/21 /13 15 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA4887-8 DUP-1 Benzene Di -Isopropyl ether Ethylbenzene Methyl Tert Butyl Ether Naphthalene Toluene Xylene (total) FA4887-9 TRIP BLANK No hits reported in this sample, 6540 100 20 ugll SM 6200B 115 25 5.0 ugll SM 6200B 402 25 5.0 ugll SM 6200B 2410 100 20 ugll SM 6200B 131 25 7.4 119/1 SM 6200B 271 25 5.0 ugA SM 6200B 606 75 11 ugll SM 6200B ■E 6 of 32 N ACCUTEST. FA4887 •••"•••"".•• Section 4 M. Southeast ■.a.ccu rI=-s-r LAGO RAT ORI[ S Sample Results Report of Analysis a ■■ 7 of 32 N ACCLJTEST. FA4887 "'...... ' Accutest LabLinkO14:32 05-Jun-2013 Report of Analysis Client Sample ID: MW-2R Lab Sample ID: FA4887.1 Matrix: AQ - Ground Water Method: SM 6200B Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC File ID DF Analyzed By Prep Date Run #1 A0180431.D 50 05/31/13 TD nla Run #2 A0180439.D 200 05/31/13 TD nla Purge Volume Run # 1 10.0 ml Run #2 10.0 ml Page 1 of 1 Date Sampled: 05/21/13 A Date Received: 05/22/13 Percent Solids: nla Prep Batch Analytical Batch n/a VA1263 nla VA1263 VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene 5230 a 100 20 ugA 75-27-4 Bromodichloromethane ND 25 5.0 ugA 107-06-2 1,2-Dichloroethane ND 25 5.0 ug1l 108-20-3 Di -Isopropyl ether 131 25 5.0 ugll 124-48-1 ❑ibromochloromethane ND 25 5.0 ugll 156-59-2 cis-1,2-Dichloroethylene ND 25 5.0 ugll 100-41-4 Ethylbenzene 421 25 5.0 ugll 99-87-6 p-Isopropyltoluene ND 25 5.0 ugll 74-87-3 Methyl chloride ND 25 5.4 ugll 1634-04-4 Methyl Ten Butyl Ether 2480 25 5.0 ugll 91-20-3 Naphthalene 151 25 7.4 ugll 108-88-3 Toluene 287 25 5.0 ugll 79-01-6 Trichloroethyiene ND 25 5.0 ug1l 1330-20-7 Xylene (total) 655 75 11 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53.7 Dibromofluoromethane 95% 96% 70.130% 17060-07-0 1,2-Dichloroethane-D4 96% 98% 70-130% 2037-26-5 Toluene-D8 101% 99% 70-130% 460-00-4 4-Bromolluorobenzene 101% 98% 70-130% (a) Result is From Run# 2 ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■■ 8 of 32 MACMU-ra T. FA4887 ...... I—,; Accutest LabLink@14:32 05-Jun-2013 Report of Analysis Client Sample ID: MW-3 Lab Sample ID: F'A4887-2 Date Sampled: 05/21/13 Matrix: AQ - Ground Water Date Received: 05/22/13 Method: SM 6200B Percent Solids: nla Project: URSNCM: S/S 1363, 1101 Hwy 61. Whitsett, NC Page 1 of 1 File ID DP Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0180432.1) 2.5 05/31/13 TD nla nla VA1263 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene 44.4 1.3 0.25 ugll 75-27.4 Bromodichloromethane ND 1.3 0.25 ugll 107-06-2 1.2-Dichloroethane N❑ 1.3 0.25 ugll 108-20-3 DI -Isopropyl ether 20.3 1,3 0.25 ugll 124-48-1 Dibromochloromethane ND 1.3 0.25 ugll 156-59-2 cis-1,2-Dichloroethylene ND 1.3 0.25 ugll 100-41-4 Ethylbenzene 1.2 1.3 0.25 ugll J 99-87-6 p-lsopropylioluene N❑ 1.3 0.25 ugll 74-87-3 Methyl chloride ND 1.3 0.27 ugli 1634-04-4 Methyl Teri Butyl Ether 90.8 1.3 0.25 ugll 91-20.3 Naphthalene 1.9 1.3 0.37 ugll 108-88-3 Toluene 1.3 1.3 0.25 ug/1 79-01.6 Trichloroethyiene ND 1.3 0.25 ugll 1330-20-7 Xylene [total] 2,5 3.8 0.54 ugll J CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 10096 70-130% 17060-07-0 1,2-Dichloroethane-D4 101% 70-130% 2037.26-5 Toluene-D8 100% 70-130% 460-00-4 4-Bromofluorobenzene 99% 70-130% ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■_.i 9 of 32 ■ ^CCU-r1=-srt: FA4887 " °" Acculest LabLinkO14:32 05-Jun-2013 Report of Analysis Client Sample ID: MW-6 Lab Sample ID: FA4887-3 Matrix: AQ - Ground Water Method: SM 6200B Project: URSNCM: SIS 1363, 1101 Hwy 61. Whi(sett, NC File ID DF Analyzed By Prep Date Run #1 E024333.1) 1 05/30/13 TD nla Run #2 A0180440.13 1 05/31/13 TD nla Purge Volume Run #1 10.0 ml Run #2 10.0 nil Page 1 of 1 Date Sampled: 05/21/13 w Date Received: 05/22/13 Percent Solids: n1a Prep Batch Analytical Batch nla VE832 nla VA1263 VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND a 0.50 0.10 ugll 75-27-4 Bromodichloromethane ND 0.50 0.10 ugll 107-06-2 12-Dichloroethane ND 0.50 0.10 ugll 108-20-3 Di -Isopropyl ether N❑ 0.50 0.10 ug11 124-48-1 Dibromochloromethane ND 0.50 0.10 119/1 156-59-2 cis-1.2-Dichloroethylene ND 0.50 0.10 ugll 100-41-4 Ethylbenzene N❑ 0.50 0.10 ugA 99-87-6 p-Isupropyltoluene ND 0.50 0.10 "gll 74-87-3 Methyl chloride ND a 0.50 0.11 ugll 1634-04-4 Methyl Tert Butyl Elher ND 0.50 0,10 ugll 91.20-3 Naphthalene ND 3 0.50 0.15 ugll 108-88-3 Toluene ND a 0.50 0.10 ugll 79-01-6 Trichloroethylene N❑ 0.50 0.10 ug11 1330-20-7 Xylene (total) N❑ 1.5 0.22 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromoiiuoromethane 96% 97% 70-130% 17060-07-0 1,2-Dichloroethane-D4 97% 98% 70.130% 2037-26-5 Toluene-D8 95% 98% 70-130% 460-00-4 4-Bromo#luorobenzene 103% 98% 70-130% (a) Result is from Run# 2 ND = Not delected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range = Indicates an estimated value B = Indicates analyse found in associated method blank N = Indicates presumptive evidence of a compound �■ 40 of 32 ACGLlTE3T. FA4887 •••• "• •• Accutest LabLink@ 14:32 05-fun-2013 Report of Analysis 3ient Sample ID: MW-8 ,ab Sample ID: FA4887-4 Date Sampled: 05/21/13 4atrix: AQ - Ground Water Date Received: 05/22/13 Uthod: SM 6200B Percent Solids: nla -roject: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC Page 1 of 1 File ID DF Analysed By Prep Date Prep Batch Analytical Batch RUT] #1 E024334.D 1 05/30/13 TD nla nla VE832 Run ff2 A0180441.1) 1 05/31/13 TD nla nla VA1263 Purge Volume Run # 1 10.0 ml Run #2 10.0 ml VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.10 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.10 ug11 107-06-2 1,2-Dichloroethane ND 0.50 0.10 ugll 108-20-3 Di -Isopropyl ether ND 0.50 0.10 ugll 124-48-1 ❑ibromochloromethane ND 0.50 0.10 ugll 156-59-2 cis- 1, 2-Dichlaroethylene ND 0.50 0.10 ugll 100-41-4 Ethylbenzene ND 0.50 0.10 ugll 99-87-6 p-Isopropyltoluene ND 0.50 0.10 ugll 74-87-3 Methyl chloride ND 0.50 0.1.1 ug11 1634-04-4 Methyl Teri Butyl Ether ND 0.50 0.10 ugll 91-20-3 Naphthalene ND 8 0.50 0,15 ugll 108-88-3 Toluene ND 0.50 0.10 ugll 79-01-6 Trichloraethylene ND 0.50 0.10 ugll 1330-20-7 Xylene (total) ND 1.5 0.22 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 ❑ibromofluoromethane 95°% 99% 70-130% 17060-07-0 1,2-Dichloroethane-D4 97% 96% 70-130% 2037-26-5 Toluene-D8 100% 1.01% 70-130% 460-00-4 4-Bromofluorobenzene 103% 98% 70-130% (a) Result is from Run# 2 ND = Not detected MDL - Method Detection Limit j = Indicates an estimated value RL = Reporting Lim!( B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■D 11 of 32 W .4CCLJTEST. FA4887 •••"•,•'• Accutest LabLinkO14:32 05-Jun-2013 Report of Analysis Client Sample ID: RW-1 R Lab Sample ID: FA4887-5 Matrix: AQ - Ground Water Method: 5M 6200B Project: URSNCM: 51S 1363, 1101 Hwy 61, Whitsett, NC File ID DF Analyzed By Prep Date Run #1 A0180430.❑ 10 05/31/13 TD nla Run #2 Purge Volume Run #1 10.0 ml Run #2 Page 1 of I Date Sampled: 05/21/13P. 0 Date Received; 05/22/13 Percent Solids: nla a Prep Hatch Analytical Batch nla VA1263 VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene 251 5.0 1.0 ugll 75-27-4 Bromodichloromethane ND 5.0 1.0 ugll 107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug11 108-20-3 Di -Isopropyl ether 178 5.0 1.0 ugll 124-48-1 Dibromochloromethane ND 5.0 1.0 ugll 156-59-2 cis-1,2-Dichloroethylene N❑ 5.0 1.0 ugll 100-41-4 Ethylbenzene 66.9 5.0 1.0 ugll 99-87-6 p-Isopropyholuene ND 5.0 1.0 ugll 74-87-3 Methyl chloride N❑ 5.0 1.1 ugll 1634-04-4 Methyl Teri Butyl Ether 149 5.0 1.0 ugll 91-20-3 Naphthalene 32.2 5.0 1.5 ugll 108-88-3 Toluene ND 5.0 1.0 ugll 79-01-6 Trichloroethylene ND 5.0 1.0 ugll 1330-20-7 Xylene (total) 16.9 15 2.2 11g11 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 100% 70-130% 17060-07 -0 1, 2-Dichloroethane-D4 101 % 70-130% 2037-26.5 Toluene-D8 100% 70-130% 460-00-4 4-Bromofluorobenzene 99% 70-130% ND = Not detected MDL - Method Detection Limit RL = Reporting Limit E = indicates value exceeds calibration range J = Indicates an estimated value B = Indicates analyte found in associated method blank N = indicates presumptive evidence of a compound ■R 12 of 32 � ACCLiTEST. FA4887 °""•�••�• Acculest LabLink@14:32 05-jun-2013 Report of Analysis Client Sample ID: VE-I Lab Sample ID: FA4887-6 Matrix: AQ - Ground Water Method: SM 6200B Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC File ID DF Analyzed By Prep Date Run #1 A0180434.13 I 05/31/13 TD nla Run #2 Purge Volume Run #1 10.0 all Run #2 Page 1 of 1 Date Sampled: 05/21/13 ate, Date Received: 05/22/13 Percent Solids: nla Prep Batch Analytical Batch zila VA1263 VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene N❑ 0.50 0.10 ugll 75-27-4 Bromodichloromethane ND 0.50 0.10 ug1l 107-06.2 1,2-Dichloroethane N❑ 0.50 0.10 ugli 108-20-3 Di -Isopropyl ether 0.24 0.50 0.10 ugli J 124.48.1 Dibromochloromethane ND 0.50 0.10 ugll 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ugll 100-41-4 Ethylbenzene N❑ 0.50 0.10 ugll 99-87-6 p-Isopropyholuene ND 0.50 0.10 ugll 74-87-3 Methyl chloride ND 0.50 0.11 ugll 1634-04-4 Methyl Ter( Butyl Ether 2.0 0.50 0.10 ugll 91-20-3 Naphthalene N❑ 0.50 0.15 ug11 108-88-3 Toluene ND 0.50 0.10 ugil 79-01-6 Trichloroethylene ND 0.50 0.10 ugll 1330-20-7 Xylene {Iota]) ND 1.5 0.22 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromelhane 96% 70-130% 17060-07-0 1,2-Dichloroethane-D4 97% 70-130% 2037-26-5 Toluene-D8 101% 70-130% 460-00-4 4-Bromofluorobenzene 100% 70-130% N❑ = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range j = Indicates an estimated value B = Indicates analyze found in associated method blank N = Indicates presumptive evidence of a compound ■4 13 of 32 E AGCLJTEST. FA4887 ....... o , .. . Accutest LabLink@14:32 05-Jun-2013 Report of Analysis Client Sample ID: VEW-1 Lab Sample ID: FA4887-7 Matrix: AQ - Ground Water Method: SM 6200B Project: URSNCM: SIS 1363. 1101 Hwy 61, Whitsett, NC File ID DF Analyzed By Prep Date Run # 1 A0180503.I) 1 06/04/ 13 TD nla Run #2 Purge Volume Run #1 10.0 ml Run #2 Page 1 of 1 Date Sampled: 05/21/13 y Date Received: 05/22/13 Percent Solids: nla I Prep Batas Analytical Batch nla VA1265 VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.10 ugll 75-27-4 Bromodichioromethane ND 0.50 0.10 ugll 107-06-2 1,2-Dichloroethane N❑ 0.50 0.10 ugll 108-20-3 Di -Isopropyl ether ND 0.50 0.10 ugfI 124-48-1 Dibromochloromethane ND 0.50 0.10 ugll 156-59-2 cis- 1, 2- Dichloroethylene ND 0.50 0.10 ugll 100-41-4 Ethylbenxene N❑ 0.50 0.10 ugll 99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug11 74-87-3 Methyl chloride ND 0.50 0.11 ugll 1634.04.4 Methyl Teri Butyl Ether 0.48 0.50 0.10 ug11 j 91-20-3 Naphthalene ND 0.50 0.15 ugll 108-88-3 Toluene N❑ 0.50 0.10 ugll 79-01-6 Trichloroethylene ND 0.50 0.10 ugli 1330-20-7 Xylene (to(al) N❑ 1.5 0.22 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 98% 70-130% 17060-07-0 1,2-Dichloroethane-D4 100% 70-130% 2037-26-5 Toluene-D8 99% 70-130% 460-00.4 4-Bromofiuorobenxene 102% 70-130% N❑ = Not detected MDL - Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound M.- 14of32 FA4887 °"• I Accutest LabLink@)14:32 05-]un-2013 Report of Analysis Client Sample ID: DUP-1 Lab Sample ID: FA4887-8 Date Sampled: 05/21/13 Matrix: AQ - Ground Water Date Received: 05/22/13 Method: SM 6200B Percent Solids: nla Project: URSNCM: 5151363, 1101 Hwy 61, Whitsett, NC Page 1 of i File ID DF Analysed By Prep Date Prep Batch Analytical Batch Run #1 A0180443.D 50 05/31/13 TD nla nla VA1263 Run #2 A0180444,D 200 05/31/13 TD nla nla VA1263 Purge Volume Rijn # 1 10.0 ml Run #2 10.0 ml VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene 6540 a 100 20 ugll 75.27-4 Bromodichloromethane ND 25 5.0 ugll 107-06-2 1,2-Dichloroethane ND 25 5.0 ugll 108-20-3 Di -Isopropyl ether 115 25 5.0 ugll 124-48-1 Dibromochloromethane ND 25 5.0 ugll 156-59-2 cis-1,2-Dichloroethylene ND 25 5.0 ugll 100-41-4 Ethylbenzene 402 25 5.0 ugll 99-87-6 p-Isopropyltoluene ND 25 5.0 ugll 74-87-3 Methyl chloride ND 25 5.4 ugll 1634-04-4 Methyl Tert Butyl Ether 24103 100 20 ugll 91-20-3 Naphthalene 131 25 7.4 ugll 108-88-3 Toluene 271 25 5.0 ugll 79-01-6 Trichloroethylene ND 25 5.0 ugll 1330-20-7 Xylene (total) 606 75 11 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dihromofluoromethane 96% 96% 70-130% 17060-07-0 1,2-Dichloroethane-D4 96% 97% 70-130% 2037-26-5 Toluene-D8 101% 101% 70-130% 460-00-4 4-Bromofluorobenrene 96% 96% 70-130% (a) Result is from Run# 2 ND = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range I = Indicates an estimated value B = Indicates analyze found in associated method blank N = Indicates presumptive evidence of a compound P. ■■ 15 of 32 ACCLJTEST. FA4887 ..... Accutest LabLink@14:32 05-Jun-2013 Report Of Analysis Page 1 of i it Sample ID: TRIP BLANK A Sample ID: FA4887.9 Date Sampled: 05/21/13 rix: AQ - Trip Blank Water Date Received: 05/22/13 iod: SM 6200E Percent Solids: nla ect: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0180474.D I 06/03/13 TD nla nla VA1264 Run #2 Purge Volume un 11 10.0 ml un #2 VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.10 ugll 75.27.4 Bromodichloromethane ND 0.50 0.10 ugll 107-06-2 1,2-Dichloroethane N❑ 0.50 0.10 ug/l 108-20-3 Di -Isopropyl ether ND 0.50 0.10 ugll 124-48-1 Dibromochloromethane N❑ 0.50 0.10 ug1l 156-59-2 cis- 1, 2 -Dichloroethylene ND 0.50 0.10 ugll 100-41.4 Ethylbenzene ND 0.50 0.10 ugli 99-87-6 p-Isopropylioluene N❑ 0.50 0.10 ugll 74-87-3 Methyl chloride ND 0.50 0.11 ugll 1634-04-4 Methyl Tert Butyl Ether N❑ 0.50 0.10 ugll 91-20-3 Naphthalene ND 0.50 0.15 ugll 108-88-3 Toluene ND 0.50 0.10 ugll 79-01-6 Trichloroethylene ND 0.50 0.10 ugll 1330-20-7 Xylene (total) ND 1.5 0.22 ug/l CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromo#luoromethane 98% 70.130°% 17060-07-0 1,2-Dichloroethane-D4 99% 70-130% 2037-26-5 Toluene-D8 100% 70-130°% 460-00-4 4-Bromofluorobenzene 101% 70-130% ND = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range J = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound ■E 16 of 32 M ACCLJTEr3T. FA48a7 ,I .... •.." Section 5 mom Southeast ACCUTEST L A 13 ❑ R AT OR I E S Misc. Forms Custody Documents and Other Forms Includes the fallowing where applicable: ■ Chain of Custody 10 17 of 32 ACCLJTEST. ody Record f 7AAKIPage -.L Ol - I — o+te[mmlddWy eowrr.e�xa., were Rush TAT: Yes_ Fro x r ardor Number: ieueeMrC-0 treclar: uns Corporamw - Nwh carwr uCOMK4M Promm No. mm • W317e1.1"m ee: 1SM Formew %A ro*M. &M 400. wpn4.ie. tic 276W AM! Mars" tam 91H/5.1100 Emee Mere�e Me7en•Ge�4.a.rom Em Tc MvmmwgewLee Qor -.r Gw- -m-To. SP OX&O K- 1x Requested AndynM Raw Type & C LWd SY�tiva � Fur Date Peakepe Commenri FM. a IMO. rep aw>,.e ••pr .'1d 6e.pr.. eamw. e.o wipe•1w. an era wrr ..r v.ayrre r..w nr.mnd RALE16H.HC Tone Accepted By/ AMILeelon WDIM@TlkmrA?vo 'FIC I Tr p Me- Yee I No M-Mi8O 6eRgle SubmereA Yp! No ap 11• terry 30.2012 up Lew COG wr. T. ♦foam i011 FA4887: Chain of Custody Page 1 of 2 18of32 .o ccu--res-r FAQ"? ... H . . I... . ACCUTEST LABORATORIES SAMPLE RECEIPT CONFIRMATION ACCUmms JOB NUMBERs��+�SB 7 CLIENT: U ;Z S PROJECT: DATE111 X READ. N fHM/DDIYY 24Ap} NUMBER OF COOLERS RFCEIVED;�� METHOD OFDRIdVHRV• �I�DH7�/ UPS ACCUTEST COURIER GREYHOUND DELIVERY 0111ER AIRRILL NUMBERS:_ CqOLER LNFQRMATJULY CUSTODY SEA[. NOT PRFSBNT OR SPOT INTACT CHAIN OF CUSTODY NOT AtCliVED (COC) ANALYSIS REQUESTED IS UNCLLAR OR MISSING SAMPLE DATES OR TIMES UNCLEAR OR MISMG TEMPERATURE CRrMRIA NOT MST wICT ICI PRESENT TRIP BLANK R2pA &n0N TRIP BLANK PROVIDED TRIP BLANK NOT PROVIDED TRIP BLANK NOT ON COC TRIP BLANK INTACT TRIP BLANK NOT INTACT RECEIVED WATER I BLANK RECETVFJD SOD. TRIP BLANK bUSC. INFORMATION NUMIIZR OF ENCORES 7 NUMBER OF 5035 FIELD KITS 7 NUMBER OR LAB FII.77AES3 METALS ? SUMMARY OF I&MPEBATURE INEQRMATION IR THERM ID 3 CORR. FACTOR LO- OBSF.RVED TEMPS: -3PI CORRECTED TEMPS: Y' Z _ SAMPLE INFORMATION SAMPLE LABELS PRESENT ON ALL BOTTLES INCORRECT NUMBER OF CONTAINERS USED SAMPLE RECEIVED IMPROPERLY PRESERVED INSUFFICIENT VOLUME FOR ANALYSIS DATES/TUvIES ON COC DO NOT MATCH SAMPLE LABEL ID'$ ON COC DO NOT MATCH LABEL VOC VIALS 13AVE READSPACE (MACRO BUBBLES) BOTTLES RECEIVED BUT ANALYSIS NOT REQU E-STXD O BOTTLES RECEIVED FOR ANALYSIS REQUESTED UNCLRAR FILTERING OR COMPOMMiG INSTRUCTIONS MPLE CONTAINS RM RECEIVER BROKEN SOLIDS JAR NOT RECEIVED 35 VULLI) KIT FROZEN VIrMI Y 48 HOUR'S SIDUAL CHLOREVX PRESENT {APPICARLY TO EPA q10 SUM OR i1ORM CAROLMA ORGANICS} TECHNICIAN SIGNATURFMATE 4- 1l _REVIEWER SIGNATURFJDA NF ID109 RECEIF'T CONFIRMATION 100609 (2).xis FA4887: Chain OF Custody Page 2 of 2 1 19of32 ,o,ccu-rasT FA4887 "• •• "• �• Section 6 . Southeast E ACCLJTEE3—F L A 6 0 R A T D R I E S RIVAL►►[►y►LilF.M W QC Data Summaries Includes the following where applicable: • Method Blank Summaries ■ Blank Spike Summaries • Matrix Spike and Duplicate Summaries Q ■■ 20 of 32 U.QC4--U- 't=BT. FA4887 `••"""`O""' Method Blank Summary Job Number: FA4887 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: SIS 1363, 1101 Hwy fit. Whilselt, NC Page 1 of 1 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE832-MB E024315.1) 1 05/30/13 TD nla nla VE832 The QC reported here applies to the following samples: Method: SM 6200B FA4887-3 CAS No. Compound Result RL MDL Units Q 75-27-4 Bromodichloromethane ND 0.50 0.10 11911 107-06-2 1,2-Dichloroethane ND 0.50 0.10 ugll 108-20-3 Di -Isopropyl ether N❑ 0.50 0.10 ugll 124-48-1 Dibromochlaromethane N❑ 0.50 0.10 ugll 156-59-2 cis- I2-Dichloroethylene ND 0.50 0.10 ugll 100.41-4 Ethylbenxene ND 0.50 0.10 ugll 99-87-6 p-Isopropyltoluene N❑ 0.50 0.10 ugll 1634-04-4 Methyl Teal Butyl Ether ND 0.50 0.10 ugll 79-01-6 Trichloroethylene ND 0.50 0.10 ugll 1330-20-7 Xylene [(otal) ND 1.5 0.22 ugll CAS Na. Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 95% 70.130% 17060-07-0 1,2-Dichloroethane-D4 97% 70-130% 2037-26-5 Toiuene-D8 99% 70.130% 460-00-4 4-Bromofluorohenzene 103°% 70-130°% In 21 of 32 ACCUTEST. FA4W7r .." ...O"'.• Method Blank Summary Job Number: FA4887 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC Page 1 of 1 Sample File ID DF Analysed By Prep Date Prep Batch Analytical Batch VA1263-MB A0180424.171 05/31/13 TD nla nla VA1263 The QC reported here applies to the following samples: Method: SM 6200B FA4887-1, FA4887-2, FA4887-3, FA4887-5, FA4887-6, FA4887-8 CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.10 ugll 75-27-4 Bromodichloromethane ND 0.50 0.10 ugll 107-06-2 1,2-Dichloroethane ND 0.50 0.10 ugll 108-20-3 Di -Isopropyl ether ND 0.50 0.10 ugA 124-48-1 Dibromachloromethane ND 0.50 0.10 ugll 156-59-2 cis- 1, 2-Dichloroethylene N❑ 0.50 0.10 ugll 100-41-4 Ethylbenzene ND 0.50 0.10 ugA 99-87-6 p-Isopropylioluene N❑ 0.50 0.10 ugll 74-87-3 Methyl chloride N❑ 0.50 0.11 ugll 1634-04-4 Methyl Teri Butyl Ether ND 0.50 0.10 ugA 91-20-3 Naphthalene ND 0.50 0.15 ugll 108-88-3 Toluene ND 0.50 0.10 ugll 79-01-6 Trichloroethylene ND 0.50 0.10 ug1l 1330-20-7 Xylene [total] ND 1.5 0.22 ugll CAS No. Surrogate Recoveries Limits 1868.53-7 ❑ibromolluoromethane 97% 70.130°% 17060-07-0 1,2-Dichloroethane-D4 97% 70-130% 2037-26-5 Toluene-D8 101% 70.130% 460-00-4 4-Bromofluorobenzene 100% 70-130% as 22 of 32 � ACCLJTEST. FA4887 •••�•••"••• Method Blank Summary Job Number: FA4887 Account: BPAMSS Atlantic Richfield Company Project-. URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC Page 1 of 1 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA1264-MB A0180459.D 1 06/03/13 TD nla nla VA1264 The QC reported here applies to the following samples: Method: SM 6200B FA4887-9 CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.10 ug/l 75-27-4 Bromodichforomethane ND 0.50 0.10 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l 108-20-3 Di -Isopropyl ether N❑ 0.50 0.10 ug/l 124-48.1 Dibromochloromethane ND 0.50 0.10 ugli 156-59-2 cis -1,2-Dichloroethylene N❑ 0.50 0.10 ug/l 100-41-4 Ethylbenzene ND 0.50 0.10 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l 74-87-3 Methyl chloride ND 0.50 0.11 ug/l 1634-04-4 Methyl Teri Butyl Ether N❑ 0.50 0.10 ug/l 91-20-3 Naphthalene ND 0.50 0.15 ug/l 108-88-3 Toluene ND 0.50 0.10 ug/l 79-01.6 Trichloroeth-ylene ND 0.50 0.10 ugll 1330-20-7 Xylene (total) ND 1.5 0.22 ug/l CAS No. Surrogate Recoveries Limits 1868-53.7 Dibromofluoromethane 98% 70-130% 17060-07-0 1,2-Dichloroethane-D4 98% 70-130% 2037.26.5 Toluene-D8 100% 70-130% 460-00-4 4-Bromofluorobenzene 103% 70.130% me 23 of 32 W ACCU-MRST. FA4U7 ".....' Method Blank Summary Job Number: FA4887 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: S/S 1363, 1101 Hwy 61, Whitse[t, NC Page 1 of 1 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA1265-MB A0180488.D 1 06/04/13 TD nla nla VA1265 The QC reported here applies to the following samples: Method: SM 6200B FA4887-7 CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.10 ugll 75-27-4 Bromodichloromethane ND 0.50 0.10 ugll 107-06-2 1,2-Dichloroethane ND 0.50 0.10 ugll 108-20-3 Di -Isopropyl ether ND 0.50 0.10 ugll 124-48-1 Dibromochloromethane ND 0.50 0.10 ugll 156-59-2 cis-1,2-Dichloreethylene ND 0.50 0.10 ugll 100-41-4 Ethyibenxene ND 0.50 0.10 ugll 99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug1l 74-87-3 Methyl chloride ND 0.50 0.11 ugll 1634-04-4 Methyl Ter[ Butyl Ether ND 0.50 0.10 ugll 91-20-3 Naphthalene N❑ 0.50 0.15 ugll 108-88-3 Toluene ND 0.50 0.10 ugll 79-01-6 Trichloroethylene N❑ 0.50 0.10 ugll 1330-20-7 Xylene (total) ND 1.5 0.22 ugll CAS No. Surrogate Recoveries Limits 1868-53-7 ❑ibromufluoromethane 96% 70-130% 17060-07-0 1.2-Dichloroethane-D4 98% 70-130% 2037-26-5 Toluene-138 102% 70-130% 460-00-4 4-Bromolluorobenzene 100% 70-130% 100 24 of 32 W ACCu-reST. FA4887 ..... •I, -. Blank Spike Summary Jab Number: FA4887 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: S/S 1363, 1101 Hwy 61, Whitsett. NC Page 1 of i Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE832-BS E024313.1) 1 05/30/13 TD nla a/a VE832 The QC reported here applies to the following samples: FA4887-3 Spike BSP BSP CAS No. Compound ugll ug/l % Limits 75-27-4 Bromodichloromethane 10 9.9 99 70-130 107-06-2 1.2-Dichloroethane 10 10.9 109 70-130 108-20-3 ❑i-Isopropyl ether 10 10.6 106 70-130 124.48-1 Dibromochloromethane 10 9.6 96 70-130 156-59-2 cis- 1. 2-Dichloroethylene 1(1 11.4 114 70-130 100.41-4 Ethylbenzene 10 11.2 112 70-130 99-87-6 p-Isopropylioluene 10 10.2 102 70-130 1634-04-4 Methyl Ter[ Butyl Ether lil 10.6 106 70-130 79-01-6 Trichloroethylene 10 11.4 114 70-130 1330-20-7 Xylene {to(al) 30 35.4 118 70-130 CAS No. Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 97% 70-130% 17060-07-0 1,2-Dichloroethane-D4 96% 70-130% 2037-26-5 Toluene-D8 98% 70.130% 460-00-4 4-Bromofluorohenzene 101% 70-130% = Outside of Control Limits. Method: SM 620013 ME 25 of 32 ACCLJTEST. FA4887 ""�".•• Blank Spike Summary Job Number: FA4887 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: SIS 1363, 1101 Hwy 61, Whilsett, NC Page 1 of 1 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA1263-BS A0180422.D 1 05/31/13 TD nla nla VA1263 The QC reported here applies to the following samples: FA4887-1, FA4887-2, FA4887-3, FA4887-5, FA4887-6, FA4887-8 Spike BSP BSP CAS No. Compound ug11 ugll % Limits 71-43-2 Benzene 10 8.6 86 70-130 75-27.4 Bromodichloromethane 10 8.3 83 70-130 107-06-2 1,2-Dichloroethane 10 9.5 95 70-130 108.20-3 Di -Isopropyl ether 10 8.3 83 70-130 124-48-1 Dibromochloromethane 10 7.9 79 70-130 156-59-2 cis-1,2-Dichloroethylene 10 8.6 86 70-130 100-41-4 Ethylbenzene 10 9.5 95 70-130 99-87-6 p-Isopropyltoluene 10 9.5 95 70-130 74-87-3 Methyl chloride 10 9.6 96 60-140 1634.04-4 Methyl Ter( Butyl Ether 10 8.1 81 70-130 91-20-3 Naphthalene 10 9.5 95 70-130 108-88-3 Toluene 10 8.8 88 70-130 79-01-6 Trichloroethylene 10 9.1 91 70-130 1330-20-7 Xylene (total) 30 26.3 88 70-130 CAS No. Surrogate Recoveries BSP Limits 1868-53-7 ❑ibromolluoromethane 98% 70-130% 17060-07-0 1,2-Dichloroethane-D4 101% 70-130% 2037.26-5 Toluene-D8 100% 70-130% 460-00-4 4-Bromofluorobenzene 99% 70-130% " = Outside of Control Limits. Method: SM 6200B EN 26 of 32 E ACCUTEr^sT. FA4887 ...... I — Blank Spike Summary Job Number: FA4887 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: SIS 1363, 1101 Hwy 61. Whitsett, NC Page 1 of 1 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA1264-BS A0180457,D 1 06/03/13 TD nla nla VA1264 The QC reported here applies to the following samples: FA4887.9 Spike BSP BSP CAS No. Compound ugll ugll % Limits 71.43-2 Benzene 10 9.0 90 70-130 75-27-4 Bromodichloromethane 10 8.8 88 70-130 107-06-2 1,2-Dichloroethane 10 10.0 100 70.130 108-20-3 Di -Isopropyl ether 10 8.9 89 70-130 124-48-1 Dibromochloromethane 10 8.4 84 70-130 156-59-2 cis-1,2-Dichloroethylene 10 8.8 88 70-130 100-41-4 Ethylbenzene 10 10.0 100 70-130 99-87-6 p-Isopropylioluene 10 9.7 97 70-130 74-87-3 Methyl chloride 10 9.9 99 60-140 1634-04-4 Methyl Tert Butyl Ether 10 8.9 89 70-130 91.20-3 Naphthalene 10 10.9 109 70-130 108-88-3 Toluene 10 9.4 94 70-130 79-01.6 Trichloroethyiene 10 9.4 94 70-130 1330-20-7 Xylene [total] 30 27.7 92 70-130 CAS No. Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 99% 70-130% 17060-07-0 1.2-Dichloroethane-D4 100% 70.130% 2037-26-5 Toluene-D8 101% 70-130% 460-00-4 4-Bromofluorobenzene 99% 70-130% * = Outside of Control Limits. Method: SM 6200B SIR 27 of 32 ACCIJT�ST. FA4887 "•••"•.•• Blank Spike Summary Job Number: FA4887 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC Page 1 of 1 ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batel �AI265-BS A0180496.D 1 06/04/13 TD nla nla VA1265 The QC reported here applies to the following samples: FA4887.7 Spike BSP BSP CAS No. Compound ugll ugll % Limits 71-43-2 Benzene 10 9.9 99 70-130 75-27-4 Bromodichloromethane 10 9.3 93 70-130 107-06-2 1,Z-Dichloroethane 10 10.7 107 70-130 108-20-3 Di -Isopropyl ether 10 8.5 85 70-130 124-48-1 Dibromochloromethane 10 8.6 86 70.130 156-59-2 cis-1,2-Dichloroethylene 10 9.7 97 70-130 100-41-4 Ethylhenzene 10 10.8 108 70-130 99-87-6 p-isopropyholuene 10 11.0 110 70-130 74-87-3 Methyl chloride 10 12.1 121 60.140 1634-04-4 Methyl Teri Butyl Ether 10 8.0 80 70-130 91-20-3 Naphthalene 10 10.3 103 70-130 108-88-3 Toluene 10 10.1 101 70-130 79-0I-6 Trichioroethylene 10 10.8 108 70-130 I330-20-7 Xylene [(otal) 30 31.2 104 70-130 CAS No. Surrogate Rewyeries BSP Limits 1868-53-7 Dibromofluoromethane 100% 70-130% 17060-07-0 1,2-Dichloroethane-D4 102% 70.130% 2037-26-5 Toluene-D8 100% 70-130% 460-00-4 4-Bromofluorobenxene 97% 70-130% * = Outside of Control Limits. Method: SM 6200B ■R 28 of 32 ■ ,o.ccu-r�sT FA4887 " Matrix SpikdMatrix Spike Duplicate Summary Page 1 of I Job Number: FA4887 Amount_ BPAMSS Atlantic Richfield Company Project: URSNCM: S/S 1363, 1101 Hwy 61. Whitsett, NC ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch �A4924-24MS E024325.1) 10 05/30/13 TD nla nla VE832 �A4924-24MSD E024326.1) 10 05/30/13 TD nla nla VE832 �A4924-24 a E024322.1) 10 05/30/13 TD nla nla VE832 The QC reported here applies to the following samples: Method: SM 6200B FA4887-3 FA4924-24 Spike MS MS MSD MSD Limits CAS No. Compound ug11 Q ugll ugll % ug11 % RPD Roc/RPD 75-27-4 Bromodichloromethane ND 100 90.8 91 88.2 88 3 70-130120 107-06-2 1,2-Dichloroethane ND 100 110 110 109 109 1 70-130120 108-20-3 Di -Isopropyl ether 5.1 100 118 113 116 ill 2 70-130120 124-48-1 Dibromochloromethane ND 100 74.0 74 76.6 77 3 70-130120 156-59-2 cis- 1, 2-Dichioroethylene ND 100 114 114 ill 111 3 70-130120 100-41-4 Ethylbenzene ND 100 113 113 111 111 2 70-130120 99-87-6 p-Isopropylioluene ND 100 102 102 100 100 2 70-130120 1634-04.4 Methyl Ten Butyl Ether 441 100 573 132* b 569 128 1 70-130120 79-01-6 Trichloroethylene ND 100 115 115 113 113 2 70-130120 1330.20.7 Xylene (total) ND 300 357 119 350 117 2 70-130120 CAS No. Surrogate Recoveries MS MSD FA4924-24 Limits 1868-53-7 Dibromolluoromethane 98% 98% 96% 70-130% 17060.07-0 1,2-Dichloroethane-D4 101% 99% 99% 70-130% 2037-26-5 Toluene-D8 97% 98% 98% 70-130% 460-00-4 4-Bromofluorobenzene I0O% 100% 101% 70-130% (a) Confirmation run for internal standard areas. (b) Outside control limits due to high level in sample relative to spike amount. * = Outside of Control Limits. is 29 of 32 ACCU-rEST. FA4687 •," "•.•• Matrix Spikc/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: FA4887 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: S/S 1363, 1101 Hwy 61, Whitsett, NC ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batcb FA4887-6MS A0180449.D 1 05/31/13 TD nla ala VA1263 FA4887-6MSD A0180450.1) 1 05/31/13 TD n1a nla VA1263 FA4887-6 A0180434.D 1 05/31/13 TD nla nla VA1263 The QC reported here applies to the following samples: Method: SM 6200B FA4887-1, FA4887-2, FA4887-3, FA4887-5, FA4887-6, FA4887-8 FA4887-6 Spike MS MS MSD MSD Limits CAS No. Compound ugll Q ugll ug/l % ugll % RPD Rec/RPD 71-43-2 Benzene ND 10 12.1 121 11.5 115 5 70-130120 75-27-4 Bromodichloromethane N❑ 10 11.1 111 10.6 106 5 70-130120 107-06-2 1,2-Dichloroethane ND 10 12.6 126 12.4 124 2 70-130120 108-20-3 Di -Isopropyl ether 0.24 J 10 10.8 106 10.6 104 2 70-130120 124-48-1 Dibromochloromethane ND 10 9.2 92 9.2 92 0 70-130120 156-59-2 cis- 1, 2- Dichloroethylene ND 10 1L6 116 11.1 111 4 70-130120 100-41-4 Ethylbenzene ND 10 12.9 129 12.6 126 2 70-130120 99-87-6 p-lsopropyltoluene ND 10 13.0 130 12.7 127 2 70-130120 74-87-3 Methyl chloride ND 10 11.8 118 11.3 113 4 60-140120 1634-04-4 Methyl Tert Butyl Ether 2.0 10 12.9 109 12.7 107 2 70-130120 91-20-3 Naphthalene N❑ 10 11.1 111 11.3 113 2 70-130120 108-88-3 Toluene ND 10 11.8 118 11.5 115 3 70-130120 79-01-6 Trichloroethylene ND 10 13.0 130 12.6 126 3 70-130120 1330-20-7 Xylene (to(al} ND 30 36.3 121 35.1 117 3 70-130120 CAS No. Surrogate Recoveries MS MSD FA4887-6 Limits 1868-53-7 Dibromofiuoromethane 101% 100% 96% 70-130% 17060-07-0 1,2-Dichloroethane-D4 101% 97% 97% 70-130% 2037-26-5 Toluene-D8 96% 97% 101% 70-130% 460-00-4 4-Bromoflucrobenzene 93% 94% 100% 70-130% * = Outside of Control Limits. ■a 30 of 32 ■.6.ccurt'�sT FA4887 ,•° °• �• Matrix SpikdMatrix Spike Duplicate Summary Page I of I Job Number: FA4887 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: S15 1363, 1101 Hwy 61, Whitsett. NC ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch 'A5002-4MS A0180471.D 100 06/03/13 TD n1a nla VA1264 'A5002-4MS❑ A0180472.1) 100 06/03/13 TD n1a nla VA1264 'A5002-4 A01804WD 100 06/03/13 TD n1a nla VA1264 The QC reported here applies to the following samples: Method: SM 6200B FA4887-9 CAS No. Compound 71-43-2 Benzene 75-27.4 Bromodichloromethane 107-06-2 1,2-Dichloroethane 108-20-3 Di -Isopropyl ether 124-48-1 ❑ibromochloromethane 156-59-2 cis-1.2-Dichloroethylene 100-41-4 Ethylhenxene 99-87-6 p-Isopropyltoluene 74-87-3 Methyl chloride 1634-04-4 Methyl Tert Buty] Ether 91-20-3 Naphthalene 108-88-3 Toluene 79-01-6 Trichloroethylene 1330-20-7 Xylene [total] FA5002.4 Spike MS MS MSD MSD Limits ug11 Q ugll ugll % ugll % RPD Rec UD N❑ 1000 971 97 961 96 1 70.130120 N❑ 1000 916 92 878 88 4 70-130120 ND 1000 1020 102 1020 102 0 70-130/20 N❑ 1000 837 84 856 86 2 70-130/20 N❑ 1000 866 87 805 81 7 70-130/20 ND 1000 933 93 943 94 1 70-130120 524 1000 1720 120 1740 122 1 70-130120 38.3 J 1000 1120 108 1160 112 4 70-130120 ND 1000 1100 110 1140 114 4 60-140120 ND 1000 811 81 802 80 1 70-130120 305 1000 1600 130 1720 142` 7 70-130120 19.4 J 1000 973 95 989 97 2 70-130120 N D 1000 1110 111 1110 111 0 70-130120 1140 3000 4630 116 4700 119 2 70-130120 CAS No. Surrogate Recoveries MS MSD FA5002-4 Limits 1868-53-7 Dihromofluoromethane 99% 98% 97% 70-I30% 17060-07-0 1,2-Dichloroethane-D4 104% 105% 99% 70-I30% 2037-26-5 Toluene-D8 99% 99% 99% 70-130% 460.00-4 4-Bromofluorohenxene 95% 97% 96% 70-130% * = Outside of Control Limits. ■ 31 of 32 A�CLJTEST. FA4887 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Jab Number: FA4887 Account: BPAMSS Atlantic Richfield Company Project: 11RSNCM: S/S 1363, 1101 Hwy 61, Whitsett. NC sample File ID DF Aaalyzo By Prep Date Prep Batch Analytical Batch 'A4878-2MS A0180494.D 1 06/04/13 TD nla nla VA1265 'A4878-2MS❑ A0180495.D 1 06/04/13 TD nla nla VA1265 'A4878-2 A0180499.D 1 06/04/13 TD n1a nla VA1265 The QC reported here applies to the following samples: Method: SM 6200B FA4887-7 FA4878-2 Spike MS MS MSD MSD Limits CAS No. Compound ugll Q ugll ugll % ugll % RPD Red"D 71-43-2 Benzene N❑ 10 9.8 98 9.5 95 3 70-130120 75-27-4 Bromodichloromethane N❑ 10 9.0 90 8.6 86 5 70-130120 107-06-2 1,2-Dichloroethane N❑ 10 10.3 103 10.4 104 1 70-130120 108-20-3 Di -Isopropyl ether ND 10 8.4 84 8.3 83 1 70-130120 124-48-1 Dihromochloromethane ND 10 8.2 82 7.8 78 5 70.130/20 156-59-2 cis-1,2-Dichloroethylene N❑ 10 9.4 94 9.2 92 2 70-130120 100-41-4 Ethylbenxene ND 10 10.8 108 10.6 106 2 70.130/20 99-87-6 p-Isopropylioluene N❑ 10 10.9 109 10.7 107 2 70-130120 74-87-3 Methyl chloride ND 10 11.4 114 10.6 106 7 60.140/20 1634-04-4 Methyl Tert Butyl Ether ND 10 8.0 80 8.0 80 0 70.130/20 91-20-3 Naphthalene ND 10 10.4 104 10.7 107 3 70-130120 109-88-3 Toluene ND 10 10.0 100 9.9 99 1 70-130120 79-01-6 Trichloroethylene ND 10 10.3 103 10.1 101 2 70-130120 1330-20-7 Xylene (total) ND 30 31.3 104 30.7 102 2 70-130120 CAS No. Surrogate Recoveries MS MSD FA4878-2 Limits 1868-53-7 Dihromofluoromethane 99% 100% 97% 70-130% 17060-07-0 1.2-Dichloroethane-D4 100% 101% 98% 70-130% 2037.26-5 Toluene-D8 99% 99% 101% 70-130% 460-00-4 4-Bromofluorobenaene 99% 98% 103% 70-130% W = Outside of Control Limits. No 32 of 32 ACCUTEST. FA4887 `••'••ie••�• . Southeast ■ �CCUTEST 1. A !1 Li R A T 0 R V E 5 Technical Report for Atlantic Richfield Company URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC 01363-38436751.106081 Accutest Job Number: FA4904 Sampling Date: 05/21/13 Report to: URS Corporation martha.meyers-lee@urs.com ATTN: Martha Meyers Total number of pages in report: 16 e-Hardeopy 2.0 Automated Report 1 . 1 S S Test results contained within this data package meet the requirements garryehzadi, Ph.D. of the National Environmental Laboratory Accreditation Conference Laboratory Director and/or state specific certification programs as applicable. Client Service contact: Heather Wandrey 407-425-6700 Certifications: FL (E83510), LA (03051). KS (E-10327), IA (366). IL (20D063), NC (573), NJ (FL002), SC (96038001) Dul) FLAP (L-A-B L2229), CA (04226CA), TX (T104704404), AK, AR, CA, KY, MA, NV, OK, UT, VA, WA, WI This report shall not he reproduced, except in its entirety, without the written approval of Accutest Laboratories. Test results relate only to samples analyzed. Southeast • 4405 Vineland Road • Sui1e C-15 • 0rlando. FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 • http://www.acculest.corn ' leti.rhutest 1 ralurlcs 1a the suIc authunt} tor authorizing edits or edilicatiuns to [hi' M 1 of 16 ACCLJTEST. , ocurnent i rlatit hirrized modification of this report is strictly prohibited. FA "4 .. o........ Table of Contents Section1: Sample Summary ................................................................................................... Section 2: Case Narrative/Conformance Summary.............................................................. Section3: Summary of Hits.................................................................................................... Section 4: Sample Results........................................................................................................ 4.1: FA4904-1: 1205 NC HIGHWAY 61 SOUTH -IN ........................................................ 4.2: FA4904-2: 1205 NC HIGHWAY 61 SOUTH -MI❑ .................................................... 4.3: FA4904-3: 1205 NC HIGHWAY 61 SOUTH-EFF..................................................... Section5: Misc. Farms............................................................................................................ 5.1: Chain of Custody........................................................................................................... Section 6: GCIMS Volatiles - QC Data Summaries.............................................................. 6.1: Method Blank Summary ................................................................................................ 6.2: Blank Spike Summary................................................................................................... 6.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... Sections: 3 5 6 7 8 9 10 11 13 14 15 16 I2 of 16 ACCiJTEST. FA49M Accutest LabLink916:42 04-Jun-2013 Sample Summary Atlantic Richfield Company URSNCM: SIS 1363, 1101 H 61, Whitsett, NC Project No: 01363-38436751.106081 Job No: FA4904 Sample Collected Matrix Client Number Date Time By Raxdved Code Type Samplc ID FA4904-1 05/21/13 13:10 JWJM 05/22/13 AQ Water FA4904-2 05/21/13 13:05 JWJM 05/22/13 AQ Water FA4904-3 05/21/13 13:00 JWJM 05/22/13 AQ Water 1205 NC HIGHWAY 61 SOUTH -IN 1205 NC HIGHWAY 61 SUUTH- MID 1205 NC HIGHWAY 61 SOUTH- EFF �■ 3 of 16 ACCUTEST. FA49" •••.. SAMPLE DELIVERY GROUP CASE NARRATIVE Client: Atlantic Richfield Company Job No: FA4104 Site: URSNCM: S/S 1363, 1101 Hwy 61, Whitseu, NC Report Date 6/4/2013 4:21:28 PM 3 Samples were collected on 05/21/2013 and were received at Accutest SE on 05/22/2013 properly preserved, at 2.6 Deg. C and intact. These Samples received an Accutest job number of FA4904. A listing of the Laboratory Sample m. Client Sample ID and dates of collection are presented in the Results Summary Section of this report. Except as noted below, all method specified calibrations and quality control performance criteria were met for this job. For more information, please refer to QC summary pages. Volatiles by GCMS By Method SM 6200B Matrix: AQ Batch ID: VE834 All samples were analyzed �vithin the recommended method holding time. All method blanks for this batch meet method specific criteria. Sample(s) FA5002-10MS, FA5002-1 OMSD weere used as the QC samples indicated. Accutest Laboratories Southeast (ALSE) cerlities that this report meets the project requirements for analytical data produced for the samples as received at ALSE and as stated on the COC. ALSE certifies that the data meets the Data Quality Objectives for precision, accuracy and completeness as specified in the ALSE Quality Manual except as noted above. This report is to be used in its entirety. ALSE is not responsible for any assumptions of data quality if partial data packages are used Narrative prepared by: Date: June 4.2013 Lovelie Metagar. QA Officer (signature on file) Tuesday, dune 04. 2013 Page 1 of 1 a■ 4 of 16 ACCUl-rRt3T. FA49W ,.n..,o... Summary of Hits Page 1 of I Job Number: FA4904 Account: Atlantic Richfield Company Project: URSNCM: S/S 1363, 1101 Hwy 61, Whitsetl, NC Collected: 05/21/ 13 Lab Sample ID Client Sample ID Result! Analyte Qual RL MDL Units Method FA4904-1 1205 NC HIGHWAY 61 SOUTH-rN 1,2-Dichioroethane 0.23 J 0.50 Di -Isopropyl ether 0.33 j 0.50 Methyl Tert Butyl Ether 11.0 0.50 FA4904-2 1205 NC HIGHWAY 61 SOUTH MID No hits reported in this sample. FA4904-3 1205 NC HIGHWAY 61 SOUTH-EFF No hits reported in this sample. 0.10 ugll SM 6200B 0.10 ugll SM 6200B 0.10 ug/1 SM 6200B ■R 5ef16 ■ accu-r�sT FA4904 ••' Section 4 Southeast E ACC! JTEE;T L A ❑ R A T 0 R 1 F S Sample Results Report of Analysis G ■I! 6 of 16 N ACCUTEE3-r FA4904 •••�•••" Accutest LaKinkC@16:42 04-Jun-2013 Report of Analysis Client Sample ID: 1205 NC HIGHWAY 61 SOUTH -IN Lab Sample ID: FA4904-1 Matrix: AQ - Water Method: SM 6200B Project: URSNCM: S1S 1363, 1101 Hwy 61, Whitsett, NC File ID DF Analyzed By Prep Date Run #1 E024393.1) 1 06/03/13 TD nla Run #2 Purge Volume Run #1 10.0 ml Run #2 Page 1 of 1 Date Sampled: 05/21/13 L Date Received: 05/22/13 Percent Solids: nla a Prep Batch Analytical Batch nla VE834 VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.10 ugll 75-27-4 Bromodichloromethane ND 0.50 0.10 ug/I 107-06-2 1,2-Dichloroethane 0.23 0.50 0.10 ugll J 108-20-3 Di -Isopropyl ether 0.33 0.50 0.10 ugll J 124-48-1 Dibromochloromethane N❑ 0.50 0.10 ugll 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ugll 100-41-4 Ethylbenzene ND 0.50 0A0 uglf 99-87-6 p-Isopropyltoluene ND 0.50 0.10 ugll 74.87.3 Methyl chloride ND 0.50 0A I ugll 1634-04-4 Methyl Tert Butyl Ether 11.0 0.50 0.10 ugll 91.20-3 Naphthalene ND 0.50 0.15 ugll 108-88-3 Toluene ND 0.50 0.10 ugll 79-01-6 Trichloroethylene ND 0.50 0.10 ugll 1330-20-7 Xylene (total) ND 1.5 0.22 ug1l CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 99% 70-130% 17060-07-0 1,2-Dichloroethane-D4 99% 70-130% 2037-26-5 Toluene-D8 102% 70-130% 460-00-4 4-Bromofluorohenzene 102% 70-130% ND = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range J = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound min 7 of 96 0 ACCLITEBT. FA4904 "••• Accutest Labi.ink@16:42 04-Jun-2013 Report of Analysis Client Sample ID: 1205 NC HIGHWAY 61 SOUTH -MID Lab Sample ID: FA4904-2 hate Sampled: 05/21/13 Matrix: AQ - Water Date Received: 05/22/13 Method: SM 6200B Percent Solids: nla Project: URSNCM: SIS 1363, 1101 Hwy 61, Whilsett, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E024394.1) 1 06/03/13 TD nla nla VE834 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.10 ugll 75-27-4 Bromodichloromethane ND 0.50 0.10 ugll 107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug1l 108-20-3 Di -Isopropyl ether N❑ 0.50 0.10 uglt 1Z4-48-1 Dibromochlornmethane N❑ 0.50 0.10 ugll 156-59-2 cis- 1,2-Dichloroethylene ND 0.50 0.10 ugll 100-41-4 Ethylbenzene N❑ 0.50 0.10 ug1l 99-87-6 p-lsopropyholuene ND 0.50 0.10 ugll 74-87-3 Methyl chloride N❑ 0.50 0.11 ugll 1634-04-4 Methyl Ter( Butyl Ether ND 0.50 0.10 ugll 91-20-3 Naphthalene ND 0.50 0.15 ugh 108-88-3 Toluene ND 0.50 0.10 ugll 79-01-6 Trichloroethylene N❑ 0.50 0.10 ugll 1330-20-7 Xylene [total] ND 1.5 0.22 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 98% 70-130% 17060-07-0 1,2-Dichloroethane-D4 99% 70-130% 2037-26-5 Toluene-D8 101% 70-130% 460-00-4 4-Bromofluorobenzene 101% 70-130% ND = Not detected MDL - Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■sp 8of16 (♦ ACCUTEST. FA4904 •• " •• Accutest LabLink@16:42 04-jun-2013 Report of Analysis :it Sample ID: 1205 NC HIGHWAY 61 SOUTH-EFF Sample ID: FA4904-3 rix: AQ - Water hod: SM 6200B ect: URSNCM: SIS 1363. 1101 Hwy 61, Whitsett, NC File ID DF Analyzed BY Prep Date #1 E024395.1) 1 06/03/13 TD nla #2 Purge Volume Run #1 10.0 ml Run #2 Page 1 of 1 Date Sampled: 05/21/13 w Date Received: 05/22/13 Percent Solids: nla a Prep Batch Analytical Batch nla VE834 VOA Special List CAS No. Compound Result RL MDL Units Q 71.43-2 Benzene ND 0.50 0.10 ugll 75-27-4 Bromodichlorome(hane ND 0.50 0.10 ugll 107-06-2 1,2-❑ichloroethane N❑ 0.50 0.10 ugll 108-20-3 Di -isopropyl ether ND 0.50 0.10 ugll 124-48-1 Dibromochlorome(hane N❑ 0.50 0.10 ugll 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ugll 100-41.4 Ethylbenzene N❑ 0.50 0.10 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.10 ugll 74-87.3 Methyl chloride N❑ 0.50 0.11 ugll 1634-04-4 Methyl Ter( Butyl Ether ND 0.50 0.10 ugll 91-20.3 Naphthalene N❑ 0.50 0.15 ugA 108-88-3 Toluene ND 0.50 0.10 ugll 79-01-6 Trichloroethylene ND 0.50 0.10 ugll 1330-20-7 Xylene (total) ND L5 0.22 ugA CAS No. Surrogate Recoveries Rua# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 99% 70-130% 17060-07.0 1,2-Dichloroethane-D4 100% 70-130% 2037-26-5 Toluene-D8 101% 70-130% 460-00-4 4-Bromofluorobenzene 104% 70-130% ND = Not detected MDL - Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound X© 9of16 ■ ACCUTET. PA4904 •....I - Section 5 . Southeast E ACCuT'EE;-F L A p 0 R A T❑ R 1 E S Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody 0 ON 10 of 16 N .AGCUTEST. FA4W4 •..... bp o Laboratory Managamew Program LaMP Chain of Custody Record T " aeq c1w..N_1—or_i_ 8P S1u 4040 Pam: ❑' 7til Am S7u. Data h mbWdoy7l: 1nair aan 1.w41 Rush TAT: Yea No x RP F.cOhy %a-. Lab Work 0rd.r Numbar. Nsm. Aceuer.e.4.uCNYL -ft A*N� 1101 ll $ HW 51 .JNgTAnks QRS Corpoleam. - NWIK Caw[L . AI�Addmft 44W WrW.d ROWL $u fro adveda- FL na11 . Sbw YIP eaft 1MWel NC v.mr wgsee Np OT]a7. 1as7pil-1 Oi0i1 PM 1Yarw WANSW R""erlApwy NCOENA OWN - UST s.cuun 1a00 P.nnrlr YSA Netd. 9w 400. IlensM., NC 71640 Phc 1 461�3H700 anOM 10 he Pu M. W" Nw shPPny,+trK Aa&ftk 1i7}.+. l" P1ppew No O0SZ&WN 214491-1100 Emsa' IInf1A.lA.p..•lss0uaca.n ab scN O.er N. Yee.' Q�a.1..]n OOC-e.0 QaF�rN E00 To. kW" mw w"a.&+. nm POD Le G.e, or S" eo At ,Fr B1 - OMWA Spend awn TO AP Curo.aw x P Prcpd Mn Q% Fewch Neut. Nu- G..Wle.r. V Pmssmb" Ra qusritOd AAayar Rapers 7yp► • CK L..-I PMVto 2102714740 3 a SL1M..d� r.:: Gab P.paOy — W Erns. 0M.Pr Watq.rpn Lab Na. S—" OGS- PAY TY.N CommanpL nor •• re wgwaid eut s.a Mr P�w....a.•mw�•^v11 uoa Nc ltith•+r e+ s..m • u y1 l i l 3l x a a L E 16 H. 1,. 1 ma Nc wpr.p■ 19e.0-Mo x ] 3 1200 Ne Heft" s 1 Eoud1 ER L�,po x 7 x 0 S.-RWO Ne— J. VIO.. 7 M.e+P. RMRquyhad dy 1 AMwtkm axle Thm Ac PLW 8y! AffMad a DMO I TYrta SwnpW. C.Np..y: uns Comlr.aon -NOM C.IAM %J kLACC U OZ S sr ! � � `-►`cos 6 shvelpd wood: F*MA M" MM de'. —� !2 f 180CA A- stw,,.e tnca.y No: ,1t {y apacW InsbucRow R.r.. m.e.ah.d s...Pl. NR R.wa.r to, a*.yucot.cov- cr C..Le1 N.M. Ll.yan4.a rMw"1.1 11 01 rftffi lnq W —TO —W See Mhlyk eal nensenrerm.ncs I..W►. THM UNE • LAB VSe ONLY C-w* Ba.N M Pk r : YM 1 No I Twrkp B1.nk Y.. f Mu I Co11M T.mp W R. Vt -M T NLNN Tn I No MSV50 4w ft Bypderd' Ym f W FA4904: Chain of Custody Page l of Z 11 of 16 ,c.c�u�esT FA4W4 .••....'• •• ACCUTEST LABORATORIES SAMPLE RECEIPT CONFIRMATION ACCL3TEST'S JOB NUMBER: it) 4 CLIENT: IJ 91 5 PROJECT: 3 6 5 DAYLTIMERECEIVED; S- ?-r 3 � [MMIDDIYY 54:001 NUMBEK OF COOLERS R)LC&IVED:_J_ METHOD OF DLIJVERY: LIPS ACCITTFST COURIER GRiYYHOUN'D DELIVERY OTHER r Amu[,L NUMBxm. [ 6 ) -L COOLER I14MRd6U= TEM12ERATURE LNFQ&MATTQN CUSTODY SEAL. NOT PRESENT OR NOT INTACT SR TUERM ID �J' CORR. FACTOR + nA _ CHAIN OF CUSTODY NOT RECXIVILD (COQ OBSERVED TWA": Y - L ANALYSIS REQUESTED IS UNCLEAR OR MISM4G CORRECTED TEMPS: SAMPLE DATES OR TIMES UNCLEAR OR MISSING SAMPLE MMQBM&DQN TEMPERATURE CRITERIA NOT MET SAMPLE LABELS PRESENT ON ALL BOTTLES � WET ICE PRESENT INCORRECT NUMBER OF CONTAINERS USED TRIP BLA-NK INFORMATION SAMPLE RECEIVED P"ROPBRLY PRESERVED TRIP BLANK PROVIDED INSUFFICIRNT VOLUME FOR ANALYSIS TRIP BLANK NOT PROVIDED DATESrrIME.S ON COC DO NOT MATCH SAMPLE LABEL TRIP BLANK NOT ON COC M'S ON COC DO NOT MATCH LABEL TRIP BLANK INTACT VOC VIALS HAVR BXADSPACE (MACRO BUBBLES) TRIP BLANK NOT E%rTACT BOTTLES RECEIVED BUT ANALYSIS NOT REQUESTED RECEIVBT) WATER TRIP BLANK NO BOTTLES RECEIVED FOR ANALYSIS REQUESTED RLCEIVSD SOIL "TRIP BLANK UNCLEAR FILTERING OR COMPOS=G INSTRUCTIONS SAMPLE CONTAINER(S) RECEIVED BROKEN MISC. !2jF0 MAlIV N % SOL DS JAR NOT RECEIVED NUMBER OF ENCORES ? 5035 FIELD KIT FROZEN WnrlU Y 48 HOUR'S NUMBER OF 5035 FIELD KITS ? RESIDUAL. CHLORWE PRESENT NUMBER OR LAB FILTERED METALS ? {AFTIC&WX TO EPA bop SrJ= OR NORTH CAROLINA MGANICSI SUMMARY OF COMMENTS: TECWaCLAN SIGNATUREIDAT$le-,�'=-tt -tl? _T,REVMWER SIGNATURFmATE NF 10/09 RECEIPT CONFIRMATION 100609 (2).xls FA4904: Chain of Custody Page 2 of 2 I12 of 16 Ah.ccuTi=sr. FA4W4 `" ...•.•• Section 6 . Southeast E ACCUTEST L A O 0 R A T 0 R I E 5 GUMS Voiatiies QC Data Summaries Includes the fallowing where applicable: • Method Blank Summaries • Blank Spike Summaries ■ Matrix Spike and Duplicate Summaries 0 so 13 of 16 W ACGLJTEST. FA4904 `......-.. Method Blank Summary Job Number: FA4904 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: S/S 1363. 1101 Hwy 61, Whitsett, NC Page i of 1 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE834-MB E024377.1) 1 06/03/13 TD nla nla VE834 The QC reported here applies to the following samples: Method: SM 6200B FA4904-1, FA4904-2, FA4904-3 CAS No. Compound ResWt RL MDL Units Q 71-43-2 Benzene ND 0.50 0.10 ugll 75-27-4 Bromodichloromethane ND 0.50 0.10 ugll 107-06-2 1,2-Dichlorcethane ND 0.50 0.10 ugll 108-20-3 Di -Isopropyl ether N❑ 0.50 0.10 ugll 124-48-1 Dibromochloromethane ND 0.50 0.10 ugll 156-59-2 cis-1,2-Dichloroethylene N❑ 0.50 0.10 ugll 100-41-4 Ethylbenzene ND 0.50 0.10 ugll 99-87-6 p-lsopropyltoluene N❑ 0.50 0.10 ugll 74-87-3 Methyl chloride ND 0.50 0.11 ugll 1634-04-4 Methyl Teri Butyl Ether N❑ 0.50 0.10 ugll 91-20-3 Naphthalene ND 0.50 0.15 ugll 108-88-3 Toluene ND 0.50 0.10 ugll 79-01-6 Trichloroethylene ND 0.50 0.10 ug11 1330-20-7 Xylene [to(al) ND 1.5 0.22 ugll CAS No. Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 96% 70-130% 17060-07-0 1,2-Dichloroethane-D4 98% 70-130% 2037-26-5 Toluene-D8 102% 70-130% 460-00-4 4-Bromofluorobenzene 102% 70-130% ■■ 14 of 16 I♦ LkCCUT�ST. FA4904 •"•'••"••• Blank Spiky~ Summary Job Number: FA4904 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: 5/S 1363, 1101 Hwy 61, Whitsett. NC Page 1 of 1 Sample File ID DF Analyzed By Prep Date Prep Bate Analytical Batch VE834-BS E024376.D 1 06/03/13 TD n/a n/a VE834 The QC reported here applies to the following samples: FA4904-1, FA4904-2, FA4904-3 Spike BSP BSP CAS No. Compound ug/I ug/1 % Limits 71-43-2 Benzene 10 12.1 121 70-130 75-27-4 Bromodichloramelhane 10 10.5 105 70-130 107-06-2 1.2-Dichloroethane 10 11.8 118 70-130 108-20-3 Di -Isopropyl ether 10 10.6 106 70-130 124-48-1 ❑ibromochloromethane 10 10.2 102 70-130 156-59-2 cis-1,2-Dichiaroethylene 10 10.9 lag 70.130 100-41-4 Ethylbenzene 10 12.0 120 70-130 99.87.6 p-isopropyltoluene 10 10.6 106 70-130 74-87-3 Methyl chloride 10 10.6 106 60-140 1634-04-4 Methyl Tert Butyl Ether 10 10.6 106 70-130 91-20-3 Naphthalene 10 11.7 117 70-130 108-88.3 Toluene 10 11.9 119 70-130 79-01-6 Trichloroethylene 10 10.8 108 70-130 1330-20-7 Xylene [total] 30 32.2 107 70-130 CAS No. Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 100% 70.130% 17060.07-0 1,2-Dichloroethane-D4 102% 70-130% 2037-26-5 Toluene-138 100% 70.130% 460.00-4 4-13romofluorobenzene 101% 70-130% = Outside of Control Limits. Method: 5M 6200B ME 15 of 16 A( --CUTEST. FA49W ...a...o.,.. Matrix Spike/Matrix Spike Duplicate Summary Page 1 of l Job Number: FA4904 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: S/S 1363, 1101 Hwy 61, Whilsett, NC ;ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batcb A5002-10MS E024390.1) 1 06/03/13 TD nla nla VE834 A5002-10MSD E024391.D 1 06/03/13 TD nla nla VE834 A5002-10 E024382.❑ 1 06/03/13 TD nla nla VE834 The QC reported here applies to the following samples: Method: SM 6200B FA4904-1, FA4904-2, FA4904-3 FA5002-10 Spike MS MS MSD MSD Limits CAS No, Compound ugll Q ugll ugll % ugll % RPD Roe/RPD 71-43-2 Benzene 1.3 10 12.3 110 11.4 101 8 70-130120 75-27-4 Bromodichloromethane ND 10 8.9 89 8.3 83 7 70-130120 107-06-2 1,2-Dichloroethane ND 10 10.9 109 10.4 104 5 70-130120 108-20-3 Di -Isopropyl ether ND 10 8.9 89 8.4 84 6 70-130120 124-48-1 Dibromochloromethane ND 10 7.9 79 7.4 74 7 70-130120 156-59-2 cis-1,2-Dichioroethylene ND 10 10.1 101 9A 94 7 70-130120 100-41-4 Ethylbenzene ND 10 10.6 106 10.1 101 5 70-130/20 99-87-6 p-Isopropylioluene ND 10 9.4 94 8.8 88 7 70.130/20 74-87-3 Methyl chloride 0.22 j 10 12.7 125 11.7 115 8 60-140120 1634-04-4 Methyl Teri Butyl Ether 4.7 10 14.2 95 115 88 5 70-130120 91-20-3 Naphthalene ND 10 10.2 102 9.8 98 4 70-130120 108-88-3 Toluene ND 10 10.6 106 10.0 100 6 70-130120 79-01-6 Trichloroethylene ND 10 9.9 99 9.3 93 6 70-130120 1330-20-7 Xylene (total) ND 30 29.0 97 27.5 92 5 70-130120 CAS No. Surrogate Recoveries MS MSD FA5002-10 Limits 1868-53-7 Dibromofluoromethane 101% 100% 100% 70-130% 17060-07-0 1,2-Dichloroethane-D4 103% 99% 100% 70-130% 2037-26-5 Toluene-DS 99% 100% 99% 70-130% 460-00-4 4-Bromofluorobenzene 100% 100% 101% 70-130% * = Outside of Control Limits. ■N 16 of 16 ■,+,ccu-ras-r FA4904 ,•'•• °• •• . Southeast ACCLJTEE3T L !1 r 0" A i L) F4 1 L '� Technical Report for Atlantic Richfield Company URSNCM: S/S 1363, 1101 Hwy 61, Whitsett, NC 01363-38436751.106081 Accutest Job Number: FA4930 Sampling Date: 05/22/13 Report to: URS Corporation martha . meyers-lee@urs. com ATTN: Martha Meyers Total number of pages in report: 119 e-Hardcopy Z. 0 Automated Report I. �9,60 ACcoR i Test results contained within this data package meet The requirements #aB4ehzjadi, Ph.D. of the National Emrirontnental Laboratory Accreditation Conference Laboratory Director and/or state specific certification programs as applicable. Client Service contact: Heather Wandrey 407-425-6700 Certifications: FL (E83510), LA (03051). KS (E-10327), IA (366), IL (200063). NC (573), NJ (FLO02), SC (960380R1) DoD ELAP (L-A-B L2229). CA (04226CA), TX (TI04704404), AK, AR, CA, KY, MA, NV, OK, LIT, VA, WA, WI This report shall not he reproduced, except in its entirety, without the written approval of Accutest Laboratories. Test results relate only to samples analyzed. Southeast • 4405 Vineland Road • Suite C-15 . Orlando, FL 32911 • tel: 407-425-6700 • fax: 407-425-0707 Accutest I-atx)ratorves is the sole authority for authorizing edits or mLid itications to 01is document. Unauthorized modification of this report is strictly prohibited. • http://www.accuiest.com 1 of 119 �.4CCLJTE=-ST. FA4930 ..•....e.... Sections: Table of Contents -1- Section1: Sample Summary................................................................................................... 3 Section 2: Case Narrative/Conformance Summar►............................................................... 5 Section 3: Summary of Hits................................................................................................... 8 Section4: Sample Results........................................................................................................ 13 4.1: FA4930-1: MW-10....................................................................................................... 14 4.2: FA4930-2: MW-11....................................................................................................... 19 4.3: FA4930-3: MW-15....................................................................................................... 24 4.4: FA4930-4: USTMW-1.................................................................................................. 29 4.5: FA4930-5: USTMW-2.................................................................................................. 34 4.6: FA4930-6: USTMW-4.................................................................................................. 39 4.7: FA4930-7: AGM-RW................................................................................................... 44 4.8: FA4930-8: CSAMW-1................................................................................................. 49 4.9: FA4930-9: CSAMW-2................................................................................................. 54 4.10: FA4930-10: CSAMW-3............................................................................................. 59 4.11: FA4930-11: CSAMW4 ............................................................................................. 64 4.12. FA4930-12: DDAMW-2............................................................................................. 69 4.13: FA4930-13: DUP-2.................................................................................................... 75 4.14: FA4930-14: TRIP BLANK........................................................................................ 81 Section5: Misc. Forms ............................................................................................................ 82 5.1: Chain of Custody........................................................................................................... 83 Section 6: GCIMS Volatiles - QC Data Summaries.............................................................. 86 6.1: Method Blank Summary................................................................................................ 87 6.2: Blank Spike Summary................................................................................................... 90 6.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 93 Section 7: GUMS Semi-volatiles - QC Data Summaries..................................................... 96 7.1: Method Blank Summary.................................................................... •........................... 97 7.2: Blank Spike Summary ................................................................................................... 101 7.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 103 Section 8: GC Volatiles - QC Data Summaries..................................................................... 105 8.1: Method Blank Summary ................................................................................................ 106 8.2: Blank Spike/Blank Spike Duplicate Summary .............................................................. 109 8.3: Duplicate Summary ....................................................................................................... 112 Section 9: GC Semi-volatiles - QC Data Summaries............................................................ 116 9.1: Method Blank Summary ................................................................................................ 117 9.2: Blank Spike/Blank Spike Duplicate Summary .............................................................. 118 9.3: Duplicate Summary ....................................................................................................... 119 �■ 2 of 119 ACCLJTEST. FA4930 "'... •• Accutest La UAED12.11 10-Jun-2013 Sampie Summary Atlantic Richfield Company Job No: FA4930 URSNCM: S/S 1363, 1101 Hwy 61, Whitsett, NC Project No: 01363-38436751.106081 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID FA4930-1 05/22/13 12.30 JWJM 05/23/13 AQ Ground Water MW-10 FA4930-2 05/22/13 12:45 JWJM 05/23/13 AQ Ground Water MW•11 FA4930-3 05/22/13 12:15 JWJM 05/23/13 AQ Ground Water MW-15 FA4930-4 05/22/13 14:30 JWJM 05/23/13 AQ Ground Water USTMW-1 FA4930-5 05/22/13 14:45 JWJM 05/23/13 AQ Ground Water USTMW-2 FA4930-6 05/22/13 15:00 JWJM 05/23/13 AQ Ground Water USTMWA FA4930-7 05/22/13 10:30 JWJM 05/23/13 AQ Ground Water AGM-RW FA4930-8 05/22/13 09:45 JWJM 05/23/13 AQ Ground Water CSAMW-1 FA4930-8D 05/22/13 09:45 JWJM 05/23/13 AQ Water Dup/MSD CSAMW-1 FA4930-8S 05/22/13 09:45 JWJM 05/23/13 AQ Water Matrix Spike CSAMW-1 FA4930-9 05/22/13 09:15 JWJM 05/23/13 AQ Ground Water CSAMW-Z FA4930-10 05/22/13 13:15 JWJM 05/23/13 AQ Ground Water CSAMW-3 FA4930-11 05/22/13 13:20 JWJM 05/23/13 AQ Ground Water CSAMW-4 0 �a 3 of 119 .caccuT�s� FA4930 •...... "' Accutest LabLink@12:11 10-Jun-2013 Sample Summary (continued) Atlantic Richfield Company Job No: FA4930 URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC Project No: 01363-38436751.106081 ample Collected Matrix Client dumber Date Time By Received Code Type Sample ID FA4930-12 05/22/13 14:15 JWJM 05/23/13 AQ Ground Water DDAMW-2 FA4930-13 05/22/13 10:45 JWJM 05/23/13 AQ Ground Water ❑UP-2 FA4930-14 05/22/13 UU:t]D JWJM 05/23/13 AQ Trip Blank Water TRIP BLANK 1� 4 of 119 FA4930 J SAMPLE DELIVERY GROUP CASE NARRATIVE Client: Atlantic Richfield Company Job No: FA4930 Site: URSNC'M: SIS 1363. 1101 Hwy 61, Whitsett, NC Report Date 6/10/2013 11:45:57 13 Samples and I 'Trip Blank were collected on 05/22/2013 and were received at Accutest SE on 05/23/2013 properly preserved. at 2.4 Deg. C and intact. These Samples received an Accutest job number of FA4930. A Iisting of the Laboratory Sample ID. Client Sample ID and dates of collection are presented in the Results Summary Section of this report. Except as noted below_ all method specified calibrations and quality control performance criteria were met for this job. For more information, please refer to QC summary pages. Volatiles by GCMS By Method SM 6200B Matrix: AQ Batch ID: VA1266 All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. Sample(s) FA50784MS, FA50784MSD were used as the QC samples indicated, Matrix Spike 1 Matrix Spike Duplicate Recovery(s) for Ethylbenzene are outside control limits. Outside con"] limits due to high level in sample relative to spike amount. Matrix: AQ Batch ID: VE835 All samples were analyzed within the recommended method holding time. A method blanks for this batch meet method specific criteria. Sample(s) FA4930-2MS. FA4930-2MSD were used as the QC samples indicated. Matrix, AQ Batch ID: VE836 All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. Sample(s) FA4930-8MS. FA4930-8MSD were used as the QC samples indicated. FA4930-9: Sample was not preserved to a pH < 2: reported results are considered minimum values. FA4930-10: Sample was not preserved to a p11 < 2. reported results are considered minimum values. Extractables by GCMS By Method EPA 625 Matrix: AQ Batch ID: OP47046 All samples were extracted within the recommended method holding time. All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. Sample(s) FA4930-8MS. FA4930-8MSD ",ere used as the QC samples indicated. Matrix Spike Duplicate Recovery(s) for Phenol are outside control limits. Probable cause is due to matrix interference. For method performance in a clean matrix. refer to Blank Spike. Sample(s) OP47046-MSD, FA4930-12. FA4930-13 have surrogates outside control limits. Probable cause is due to matrix interference. FA4930-12 for TerphenyI-d 14: Outside control limits. FA4930-13 for 2-Fluorophenol: Outside control limits. FA4930-13 for Phenol-d5: Outside control limits. FA4930-13 for Terphenyl-d14: Outside control limits. FA4930-5: Dilution required due to matrix interference. FA4930-6: Dilution required due to matrix interference. FA4930-7: Dilution required due to matrix interference. FA4930-8 for Phenol: Compound outside limits in associated MSIMSD. FA4930-12: Confirmed by re -extraction and reanalysis beyond holdtime. FA4930-13: Confirmed by re -extraction and reanalysis beyond holdtime. Monday, June 10, 2013 Page 1 of 3 ■� 5 of 119 ■ A.ccurF_sr FA49]0 1� Extractables by GCMS By Method EPA 625 Matrix: AQ Batch ID: OP47154 Sample(s) FA4930-12, FA4930-13 have surrogates outside control limits. Probable cause is due to matrix interference, The following samples were extracted outside of holding time for method EPA 625: FA4930-12, FA4930-13 FA493U-12: Confirmation run. FA4930-13: Confirmation run. Volatiles by GC By Method MADEP VPH REV 1.1 Matrix: AQ Batch ID: GUU178 All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. Samples) FA4930-10DUP. FA4930-8DUP were used as the QC samples indicated. Sample(s) FA4930-7, FA4930-13 have surrogates outside control limits. Probable cause is due to matrix interference. Matrix: AQ Batch ID: GULI179 All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. Sample(s) FA51 13-12DUP was used as the QC samples indicated. Sample(s) FA4930-7, FA4930-13 have surrogates outside control limits. Probable cause is due to matrix interfercnee. FA4930-7 for BFB: Outside control limits due to matrix interference. FA4930-13 for BF13. Outside control limits due to matrix interference. FA4930-4 For Naphthalene: Associated CCV recovery outside control limits. FA4930-4: No sample available for reanalysis. FA4930-5 for Naphthalene: Associated CCV recovery outside control limits. FA4930-5: No sample available for reanalysis. FA4930-6 for Naphthalene: Associated CCV recovery outside control limits. FA4930-6. No samplc available for reanalysis. FA4930-12 For Naphthalene: Associated CCV recovery outside control limits. FA4930.12: No sample available for reanalysis. Matrix: AQ Batch ID: GUU 181 All method blanks for this batch meet method specific criteria. Sample(s) FA5164-12DUP was used as the QC samples indicated. The Following samples were run outside of holding time for method MADEP VPH REV 1.1: FA4930-7, FA4930-13. Samples re -analyzed beyond hold time: reported results are considered minimum values. Sample(s) FA4930-7. FA4930-13 have surrogates outside control limits. Probable cause is due to matrix interference. Extractables by GC By Method MADEP EPH REV 1.1 Matrix: AQ Batch ID: OP47077 All samples were extracted within the recommended method holding time. All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. Sample(s) FA4930-8DUP was used as the QC samples indicated. Sample(s) FA4930-5 has surrogates outside control limits. Probable cause is due to matrix interference. FA4930-5 for 1-Chlorooetadecane. Outside control limits due to dilution. FA4930-5 for 2- Bromonaphth alene: Outside control limits due to dilution. FA4930-5 for o-Terpheny1: Outside control limits due to dilution. FA4930-5 for 2-FluorobiphcnyI- Outside control limits due to dilution. Monday, .June 10, 2013 Page Z of 3 00 6 of 119 1] .4CC4JTEST. FA4930 .,.... ,.- — Accutest Laboratories Southeast (ALSE) certifies that this report meets the project requirements for analytical data produced for the samples as received at ALSE and as stated on the COC. ALSE cenifies that the data meets the Data Quality Objectives for precision, accuracy and completeness as specified in the ALSE Quality Manual except as noted above. This report is to be used in its entirety. ALSE is not responsible for any assumptions of data quality if partial data packages are used Narrative prepared by: Date: June 10. 2013 Lovelie Metzgar. QA Officer (signature on file) Monday, June 10, 2013 Page 3 of 3 ■E 7 of 119 ACCU-rEam FA4930 Summary of Hits Page 1 of 5 Job Number: FA4930 Aooaunt: Atlantic Richfield Company Project: URSNCM: S/S 1363, 1101 Hwy 61. Whitselt. NC Collected: 05/22/13 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA4930-1 MW-10 C11-C22 Aromatics (Unadj.) 235 190 140 ug/I MADEP EPH REV 1.1 C11-C22 Aromatics 235 190 140 ug/I MADEP EPH REV 1.1 FA4930-2 MW-11 Naphthalene 0.74 0.50 0.15 ug/I SM 6200B Fluorene 0.811 4.8 U.73 ug/I EPA 625 2-Methylnaphthalene 0.80 j 4.8 0.66 ug/I EPA 625 Naphthalene 0.853 4.8 0.61 ug/I EPA 625 Phenanthrene 1.0 j 4.8 0.68 ug/I EPA 625 C11-C22 Aromatics (Unadj.) 1783 190 140 ug/I MADEP EPH REV 1.1 C11-C22 Aromatics 178 j 190 140 ug/I MADEP EPH REV 1.1 FA4930-3 MW-15 Methyl Tert Butyl Ether 0.15 j 0.50 0.10 ug/I SM 6200B FA4930-4 USTIAW-1 Ethylbenzene 0.11 J 0.50 0.10 ug/I SM 6200B Methyl chloride 0.12 J 0.50 0.11 119/1 SM 6200B Naphthalene 33A 0.50 0.15 ug/I SM 6200B Acenaphthene 5.7 4.8 0.67 ugA EPA 625 Dibenzofuran 3.2 J 4.8 0.72 u9/1 EPA 625 Fluoranthene 0.73 J 4.8 0.56 ugA EPA 625 Fluorene 11.6 4.8 0.73 ug/I EPA 625 I-Methylnaphthalene 49.0 4.8 0.68 ugA EPA 625 2-Methyinaphthalene 38.0 4.8 0.66 ug/I EPA 625 Naphthalene 27.5 4.8 0.61 ug/1 EPA 625 Phenanthrene 13.7 4.8 0.68 ug/I EPA 625 Pyrene 3.9 J 4.8 0.65 ug/l EPA 625 Naphthalene a 78.3 3 5.0 3.0 ug/l MADEP VPH REV 1.1 C9- C12 Aliphatics (Unadj.) b 57.3 j 100 35 ug/I MADEP VPH REV 1.1 C9- C10 Aromatics (Unadj.) b 244 100 35 ug/I MADEP VPH REV 1.1 C9- C12 Aliphatics b 57.3 J 100 35 ug/I MADEP VPH REV 1.1 C9- C10 Aromatics b 244 100 35 ug/I MADEP VPH REV 1.1 2-Methylnaphthalene 28.6 3.8 1.9 ug/I MADEP EPH REV 1.1 Naphthalene 8.5 3.8 1.9 ug/I MADEP EPH REV 1.1 Phenanthrene 3.2 j 3.8 1.9 u9/1 MADEP EPH REV 1.1 CI I-C22 Aromatics (Unadj.) 562 190 140 ug/I MADEP EPH REV 1.1 CI1-C22 Aromatics 521 190 140 u9/1 MADEP EPH REV 1.1 C9-CI8 Aliphatics 1390 190 96 ug/l MADEP EPH REV 1.1 C19-C36 Aliphatics 394 190 96 ug/l MADEP EPH REV 1.1 Ni 1 ■ 8 of 119 U.4.CCl.JTi=-BT. Summary of Hits Page 2 of 5 Job Number: FA4930 Account: Atlantic Richfield Company Project: URSNCM: S/S 1363, 1101 Hwy fit, Whitsett, NC Collected: 05/22/13 Lab Sample ID Client Sample 1D Result/ Anaiyte Qua! RL MDL Units Method FA4930-5 USTMW-2 Benzene 1.5 0.50 0.i0 ug/l SM 6200B Ethylbenzene 0.27 J 0.50 0.10 ug/l SM 6200B Methyl Ten Butyl Ether 0,201 0.50 0.10 ug/l SM 6200B Naphthalene 97.3 1.0 0.30 ug/l SM 6200B Toluene 0.21 J 0.50 0.10 ug/1 SM 6200B Xylene (total) 0.42 J 1.5 0.22 ug/1 SM 6200B Acenaphthene r 17,4 J 48 6.7 ug/l EPA 625 Fluorene r 31.4 J 48 7A ug/l EPA 625 1-Methylnaphthalene c 130 48 6.8 ug/I EPA 625 2-Methyinaphthalene r 155 48 6.6 ug/l EPA 625 Naphthalene c 62.8 48 6.1 ug/l EPA 625 Phenanthrene 58.4 48 6.8 ug/l EPA 625 Pyrene c 15.3 J 48 6.5 ug/l EPA 625 Naphthalene a 209 J 10 6.0 ug/l MADEP VPH REV 1.1 C9- C12 Aliphatics (Unadj.) b 160 J 200 70 ug/l MADEP VPH REV 1.1 C9- C10 Aromatics (Unadj.) b 612 200 70 ug/l MADEP VPH REV 1,1 C9- C12 Aliphatics b 160 J 200 70 ug/1 MADEP VPH REV 1.1 C9- C10 Aromatics b 612 200 70 ug/1 MADEP VPH REV 1.1 2-Methylnaphthalene 52.1 J 76 38 ug/1 MADEP EPH REV 1.1 C11-C22 Aromatics (Unadj.) 3550 J 3800 2900 ug/l MADEP EPH REV 1.1 C11-C22 Aromatics 3500 J 3800 2900 ug/l MADEP EPH REV 1.1 C9-C18 Aliphatics 22300 3800 1900 ug/1 MADEP EPH REV 1.1 C19-06 Aliphatics 7210 3800 1900 ug/1 MADEP EPH REV 1.1 FA4930-6 USTMW-4 Benzene 5.4 0.50 0.10 ug/l SM 6200B Ethylbenzene 2.3 0.50 0.10 ug/i SM 6200B Methyl chloride 0.45 J 0.50 0.11 ug/l SM 6200B Methyl Tert Butyl Ether 0.78 0.50 0.10 ug/l SM 6200B Naphthalene 21.3 0.50 0.15 ug/1 SM 6200B Toluene 5.6 0.50 0.10 ug/l SM 6200B Xylene (total) 9.1 1.5 0.22 ug/l SM 6200B Benzoic Acid c 206 190 38 ug/l EPA 625 2,4-D methylphenol 6.6 J 19 2.9 ug/l EPA 625 3&4-Methylphenol r 27.5 19 5.3 ug/l EPA 625 bis{2-E(hylhexyl]phthalate c 74.5 19 4.4 ug/l EPA 625 1-Methylnaphthalene 4.81 19 2.7 ug/l EPA 625 Naphthalene c 18.3 J 19 2.4 ug/l EPA 625 Pyrene G 3.2 J 19 2.6 ug/l EPA 625 Benzene b 3.9 1.0 1.0 ug/l MADEP VPH REV 1.1 Ethylbenzene b 1.7 J 2.0 1.0 ug/1 MADEP VPH REV 1.1 ■ 9of119 ■ accU-res-r. FA493U "•"•"•"" • • Summary of Hits Page 3 of 5 job Number: FA4930 Account: Atlantic Richfield Company Project: URSNCM: S/S 1363, 1101 Hwy 61. Whitsett, NC Collected: 05/22/13 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method Methyl Teri Butyl Ether b 1.2 J 2.0 1.0 ug/l MADEP VPH REV 1.1 Naphthalene a 20.3 J 5.0 3.0 ug/l MADEP VPH REV 1.1 Toluene b 3.9 2.0 1.0 ug/1 MADEP VPH REV 1.1 m,p-Xylene b 3.7 J 4.0 2.0 ug/1 MADEP VPH REV 1.1 o-Xylene b 3.2 2.0 1.0 ug/1 MADEP VPH REV 1.1 C9- C10 Aromatics (Unadj.) b 49.7 J 100 35 ug/l MADEP VPH REV 1.1 C9- C10 Aromatics b 49.7 j 100 35 ug/l MADEP VPH REV 1.1 C11-C22 Aromatics (Unadj.) 1060 950 710 ug/l MADEP EPH REV 1.1 C11-C22 Aromatics 1060 950 710 ug/l MADEP EPH REV 1.1 C9-C18 Aliphatics 4590 950 480 ug/l MADEP EPH REV 1.1 C19-06 Aliphatics 1940 950 480 ug/l MADEP EPH REV 1.1 FA4930-7 AGM-R W Benzene 4.0 0.50 0.10 ug/l SM 6200B cis- 1, 2-Dichloroethylene 0.11 j 0.50 0.10 ug/l SM 6200B Ethylbenzene 0.32 J 0.50 0.10 ug/l SM 6200B Methyl chloride 1.1 0.50 0.11 ug/l SM 6200B Methyl Tert Butyl Ether 0.30 j 0.50 0.10 ug/l SM 6200B Naphthalene 190 2.5 0.74 ug/l SM 6200B Toluene 0.30 j 0.50 0.10 ug/l SM 6200B Acenaphthene z 15.0 j 48 6.7 ug/1 EPA 625 Fluorene r 27.9 J 48 7.3 ug/l EPA 625 1-Methylnaphthalene 160 48 6.8 ug/1 EPA 625 2-Methylnaphthalene r 190 48 6.6 ugll EPA 625 Naphthalene c 149 48 6.1 ug/l EPA 625 Phenanthrene c 38.9 j 48 6.8 ug/l EPA 625 Pyrene c 11.2 J 48 6.5 ug/1 EPA 625 Benzene 3.0 1.0 1.0 ug/l MADEP VPH REV 1.1 Naphthalene d 284 50 30 ug/l MADEP VPH REV 1.1 C5- C8 Aliphatics (Unadj.) 92.4 j 100 35 ug/l MADEP VPH REV 1.1 C9- C12 Aliphatics (Uaadj.) d 439 J 1000 350 ug/l MADEP VPH REV 1A C9- C10 Aromatics (Unadj.) d 1250 1000 350 119/1 MADEP VPH REV 1.1 C5- C8 Aliphatics 89.7 J 100 35 ug/l MADEP VPH REV 1.1 C9- C 12 Aliphatics d 439 j 1000 350 ug/l MADEP VPH REV 1.1 C9- C10 Aromatics d 1250 1000 350 ug/l MADEP VPH REV 1.1 2-Methylnaphthalene 44.1 19 9.6 ng/l MADEP EPH REV 1.1 Naphthalene 35.1 19 9.6 ug/l MADEP EPH REV 1.1 C11-C22 Aromatics (Unadj.) 1350 960 720 ug/l MADEP EPH REV 1.1 CII-C22 Aromatics 1270 960 720 ug/l MADEP EPH REV 1.1 C9-C18 Aliphatics 5810 960 480 ug/I MADEP EPH REV 1.1 C19-C36 Aliphatics 1920 960 480 ugA MADEP EPH REV 1.1 10 of 119 ■.cs.�cuT��� FA4930 ......:e.,,. Summary of Hits Page 4 of 5 Job Number: FA4930 Account: Atlantic Richfield Company Project: URSNCM: S/S 1363. 1101 Hwy 61, Whitse(t, NC Collected: 05/22/13 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA4930-8 CSAMW-1 Methyl Teri Butyl Ether 0.48 J 0.50 0.10 ug/l SM 6200B Cll-C22 Aromatics (Unadj.) 244 190 140 ug/l MADEP EPH REV 1.1 C11-C22 Aromatics 244 190 140 ug/l MADEP EPH REV 1.1 FA4930-9 CSAMW-2 Methyl chloride e 0.14 J 0.50 0.11 ug/l SM 6200B Methyl Teri Butyl Ether C 4.8 0.50 0.10 u9/1 SM 62DOB Methyl Teri Butyl Ether 5.3 2.0 1.0 ug/l MADEP VPH REV 1.1 Cll-C22 Aromatics (Unadj.) 194 190 140 ug/l MADEP EPH REV 1.1 CII-C22 Aromatics 194 190 140 ug/l MADEP EPH REV 1.1 FA4930-10 CSAMW-3 Methyl Teri Butyl Ether 0 8.8 0.50 0.10 ug/l SM 6200B Methyl Tert Butyl Ether 9.7 2.0 1.0 ug/l MADEP VPH REV 1.1 FA4930-11 CSAMW-4 Methyl Tert Butyl Ether 0.17 J 0.50 0.10 ug/l SM 6200B FA4930-12 DDAMW-2 Benzene 0.58 0.50 0.10 u9/1 SM 6200B Methyl Teri Butyl Ether 2.6 0.50 0.10 ug/l SM 6200B Naphthalene 2.7 0.50 0.15 ug/l SM 6200B bis(2-Ethylhexyl)phthalate f 5.3 J 19 4.4 ug/l EPA 625 Methyl Ter( Butyl Ether b 3.2 2.0 1.0 ug/l MADEP VPH REV 1.1 Naphthalene a 28.1 J 5.0 3.0 ug/l MADEP VPH REV 1.1 C9- C10 Aromatics (Unadj.) n 122 100 35 ug/l MADEP VPH REV 1.1 C9- C10 Aromatics b 122 100 35 ug/1 MADEP VPH REV 1.1 Cll-C22 Aromatics (Unad).) 400 190 140 ug/l MADEP EPH REV 1.1 Cll-C22 Aromatics 400 190 140 ug/1 MADEP EPH REV 1.1 C9-C18 Aliphatics 2120 190 96 ug/l MADEP EPH REV 1.1 C19-C36 Aliphatics 1090 190 96 ug/1 MADEP EPH REV 1.1 FA4930-13 DUP-2 Benzene 4.2 0.50 0.10 ug/l SM 6200B Ethylbenzene 0.351 0.50 0.10 ug/l SM 6200B Methyl Teri Butyl E(her 0.30 J 0.50 0.10 ug/1 SM 6200B Naphthalene 204 5.0 1.5 ug/l SM 6200B Toluene 0.30 J 0.50 0.10 ug/l SM 6200B on 11 of 119 w ACCIJ"r a -r; FA493a •••P•••""•• Summary of Hits Page 5 of 5 Job Number: FA4930 Account: Atlantic Richfield Company Project: URSNCM: S/S 1363, 1101 Hwy 61, Whitsett, NC Collected: 05/22/13 It Lab Sample ID Client Sample ID Result/ Analyte Qua/ RL MDL Units Method Acenaphthene f 4.5 j 19 2.7 ug/l EPA 625 Dibenzofuran f 3.2 j 19 2.9 ug/1 EPA 625 Fluorene f 12.2 j 19 2.9 ug/l EPA 625 1-Methylnaphthalene f 93.0 19 2.7 ug/l EPA 625 2-Methylnaphthalene f 115 19 2.6 ug/l EPA 625 Naphthalene f 93.6 19 2.4 ug/l EPA 625 Phenanthrene r 14.4 j 19 2.7 ug/l EPA 625 Pyrene f 4.9 j 19 2.6 ug/l EPA 625 Benzene 3.2 1.0 1.0 ug/1 MADEP VPH REV 1.1 Naphthalene d 239 25 15 ugA MADEP VPH REV 1.1 C5- CS Aliphatics (Unadj.) 56.81 100 35 ug/l MADEP VPH REV 1.1 C9- C12 Aliphatics (Unadj.) d 301 j 500 180 ug/l MADEP VPH REV 1.1 C9- C10 Aromatics (Unadj.) d 935 500 180 ug/l MADEP VPH REV 1.1 C5- C8 Aliphatics 53.6 j 100 35 ug/l MADEP VPH REV 1.1 C9- C12 Aliphatics ¢ 301 j 500 180 ug/1 MADEP VPH REV I.I C9- C10 Aromatics d 935 500 180 ug/1 MADEP VPH REV 1.I 2-Methylnaphthalene 94.7 15 7.7 ug/l MADEP EPH REV 1.1 Naphthalene 60.0 15 7.7 ug/1 MADEP EPH REV 1.1 C11-C22 Aromatics (Unadj.) 1500 770 580 ug/l MADEP EPH REV 1.1 C11-C22 Aromatics 1340 770 580 ug/1 MADEP EPH REV 1.1 C9-C18 Aliphatics 3850 770 384 ug/1 MADEP EPH REV 1.1 C19-C36 Aliphatics 1170 770 384 ug/l MADEP EPH REV 1.1 FA4930-14 TRIP BLANK No hits reported in this sample. (a) No sample available for reanalysis. Associated CCV recovery outside control limits. (b) No sample available for reanalysis. (c) Dilution required due to matrix interference. (d) Sample re -analyzed beyond hold time; reported results are considered minimum values. (e) Sample was not preserved to a pH < 2; reported results are considered minimum values. (0 Confirmed by re -extraction and reanalysis beyond holdtime. ■ 1 12 of 119 .CCCIJTEST FA4930 T.""' Section 4 . Southeast ACCLJ-T"E=— E-3T t A a O R A T O R i E S Sample Results Report of Analysis ■o 13 of 119 � ACCUTEST. FA4930 Acculest LabLinkO12:12 10-Jun-2013 Report of Analysis Client Sample ID: MW-10 Lab Sample ID: FA4930-1 Matrix: AQ - Ground Water Method: SM 6200B Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC File ID DF Analyzed By Prep Date Run #1 E024405.D 1 06/04/13 TD nla Run #2 Purge Volume Run # 1 10.0 ml Run #2 Page 1 of 1 Date Sampled: 05/22/13 Date Received: 05/23/13 Percent Solids: n/a Prep Batch Analytical Batch wa VE835 VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.10 ugll 75-27-4 Bromodichloromethane ND 0.50 0.10 ugll 107-06-2 1,2-Dichloroethane ND 0.50 0.10 ugll 108-20-3 Di -Isopropyl ether ND 0.50 0.10 ugll 124-48-1 Dibromochloromethane ND 0.50 0.10 ugll 156-59-2 cis- 1, 2-Dichloroethylene ND 0.50 0.10 ugll 100-41-4 Ethylbenzene ND 0.50 0.10 ugll 99-87-6 p-Isopropyltoluene ND 0.50 0.10 ugll 74-87-3 Methyl chloride ND 0.50 0.11 11911 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ugll 91-20-3 Naphthalene ND 0.50 0.15 ug/l 108-88-3 Toluene ND 0.50 0.10 ugll 79-01-6 Trichloroethylene ND 0.50 0.10 ugA 1330-20-7 Xylene (total) N❑ 1.5 0.22 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 100% 70-130% 17060-07-0 1,2-Dichloroelhane-D4 99% 70-130% 2037-26-5 Toluene-D8 99°% 70-130% 460.00-4 4-Bromo#]uorobenzene 100% 70-130% ND = Not detected MDL - Method Detection limit RL = Reporting Limit E = Indicates value exceeds calibration range j = Indicates an estimated value B = Indicates analyze found in associated method blank N = Indicates presumptive evidence of a compound ■■ 14 of 119 M ACiCUTEST. FA4430 i w .......... Accutest Labl-ink@12:12 10-Jun-2013 Report of Analysis Page 1 of 2 Cliednt Sample ID: MW-10 Lab Sample ID: FA4930-1 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: EPA 625 EPA 625 Percent Solids: nla Project: URSNCM: S/S 1363. 1101 Hwy 61, Whitsett, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 L06371I.D 1 05/29/13 NAF 05/24/13 OP47046 SL3223 Run #2 Initial Volume Final Volume Run #1 1040 ml 1.0 ml Run #2 ABN List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 48 9.6 ugll 95-57-8 2-Chlorophenol ND 4.8 0.68 ugll 59-50-7 4-Chloro-3-methyl phenol ND 4.8 0.78 ugll 120-83-2 2.4-Dichlorophenol N❑ 4.8 0,67 ugll 105-67-9 2,4-❑imethylphenol N❑ 4.8 0.74 ugll 51-28-5 2.4-Dinitrophenol ND 24 5.0 ugll 534-52-1 4,6-Dinitro-o-cresol ND 9.6 1.4 ugll 95-48-7 2-Methylphenol N❑ 4.8 0.69 ugll 3&4-Methylphenol N❑ C8 1.3 ugll 88-75.5 2-Nitrophenol ND 4.8 0.65 ugll 100-02-7 4-Nitrophenol ND 24 4.8 ugll 87-86-5 Pentachlorophenol ND 24 4.9 ugll 108-95-2 Phenol ND 4.8 0.53 ugll 88-06-2 2,4.6-Trichlorophenol ND 4.8 0.75 ugli 83-32-9 Acenaphthene ND 4.8 0.67 ugll 208-96-8 Acenaphthylene ND 4.8 0.67 ugll 120-12-7 Anthracene ND 4.8 0.72 ugll 56-55-3 Benzo(a)anthracene ND 4.8 0.52 ug/l 50-32-8 Benzo(a)pyrene ND 4.8 0.55 ugll 205-99-2 Benzo(b)fluoranthene ND 4.8 0.73 ugll 191-24-2 Benza(g,hJ)peryfene N❑ 4.8 0.64 ugll 207-08-9 Benzo(k)fluoranthene ND 4.8 0.64 ugll 101-55-3 4-Bromophenyl phenyl ether ND 4.8 0.76 ugll 85-68-7 Butyl benzyl phthalate ND 4.8 0.68 ugll 100-51-6 Benzyl Alcohol N❑ 4.8 0.96 ug/l 91-58-7 2-Chloronaphtlialene ND 4.8 0.70 ugll 106-47-8 4-Chloroaniline ND 4.8 0.66 ugll 218-01-9 Chrysene ND 4.8 0.56 ugll 111-91-1 bis(2-Chloroethoxy)methane ND 4.8 0.67 ugll 111-44-4 bis(2-Chforoe(hyl)ether N❑ 4.8 0.69 ugll 108-60-1 his (2-Chloroisopropy1)ether ND 4.8 0.76 ugll 7005.72-3 4-Chlorophenyl phenyl ether N❑ 4.8 0.84 ugll ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound a A. a ETA 15 of 119 �ACCt_3TEST. FA4930 ..... Accutest LabLink012:12 10-Jun-2013 Report of Analysis Client Sample ID: MW-10 Lacs Sample ID: FA4930-1 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: EPA 625 EPA 625 Perot Solids: N'a Project: URSNCM: S15 1363, 1101 Hwy fit, Whitsett, NC ABN List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 95-50-1 1,2-Dichlorobenzene ND 4.8 0.65 ugll 122-66-7 1,2-Diphenylhydrazine ND 4.8 0.62 ugll 541-73-1 1,3-Dichlorobenzene N❑ 4.8 0.75 ugll 106-46-7 1,4-Dichlorobenzene N❑ 4.8 0.67 ugll 91-94-1 3,3'-Dichlorobenzidine ND 4.8 0.71 ugll 53-70-3 Dibenzo(a,h)anthracene N❑ 4.8 0.56 ugll 132-64-9 ❑ibenzofuran N❑ 4.8 0.72 ugll 84-74-2 Di-n-butyl phthalate ND 4.8 0.96 ugll 117-84-0 Di-n-octyl phthalate ND 4.8 0.96 ugll 84-66-2 Diethyl phthalate ND 4.8 0.96 ugA 131-11-3 Dimethyi phthalate ND 4.8 0.77 ugll 117-81-7 bis(2-Ethylhexyl)phthalate ND 4.8 1.1 ugll 206-44-0 Fluoranthene ND 4.8 0.56 ugll 86-73-7 Fluorene ND 4.8 0.73 ugll 118-74-1 Hexachlorobenzene ND 4.8 0.66 ugll 87-68-3 Hexachlorobutadiene ND 4.8 0.92 ug11 77-47-4 Hexachlorocyciopentadiene ND 4.8 0.76 ugA 67-72-1 Hexachloroethane ND 4.8 0.71 ugll 193-39-5 Indeno(1,2,3-cd)pyrene ND 4.8 0.55 ugll 78-59-1 Isophorone ND 4.8 0.61 ugli 90-12-0 1-Methylnaphthalene ND 4.8 0.68 ugll 91-57-6 2-Methylnaphthalene ND 4.8 0.66 ug/I 91-20-3 Naphthalene ND 4.8 0.61 ugll 98-95-3 Nitrobenzene ND 4.8 0.69 ugA 621-64-7 N-Nitroso-di-n-propylamine ND 4.8 0.82 ugA 86-30-6 N-Nitrosodiphenylamine N❑ 4.8 0.96 ugll 85-01-8 Phenanthrene ND 4.8 0.68 ugA 129-00-0 Pyrene ND 4.8 0.65 ug11 120-82-1 1,2,4-Trichlorobenzene ND 4.8 0.58 ug11 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 50% 14-67% 4165-62-2 Phenol-d5 35% 10-50% 118-79-6 2,4,6-Tribromophenol 91% 33-118% 4165-60-0 Nitrobenzene-d5 82% 42-108% 321-60-8 2-Fluorobiphenyt 87% 40-106% 1718-51-0 Terphenyl-d14 82% 39-121% Page 2 of 2 ND = Not detected MDL - Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■ 16of119 ACCLITEST. Accutest LabLinkP12:12 10-Jun-2013 Report of Analysis Page 1 of 1 Client Sample ID: MW-10 Lab Sample ID: FA4930-1 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: MADEP VPH REV 1.1 Percent Solids: nla Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 UU003566.1) 1 06/01/13 MNII nla rlla GUU178 Rijn #2 Purge Volume Run #1 5.0 jnl Run #2 MADEP VPH List CAS No. Compound Result 71-43-2 Benzene ND 100-41-4 Ethylbenzene ND 1634-04-4 Methyl Tert Butyl Ether ND 91-20-3 Naphthalene ND 108-88.3 Toluene N❑ m,p-Xylene ND 95-47-6 n-Xylene ND C5- C8 Aliphatics (Unadj.) ND C9- C12 Aliphatics (Unadj.) N❑ C9- C10 Aromatics (Unadj.) ND C5- CS Aliphatics N❑ C9- C12 Aliphatics ND C9- C10 Aromatics ND CAS No. Surrogate Recoveries Run# 1 460-00-4 BFB 87% 460-00-4 BFB 88% N❑ = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range RL MI)L Units Q 1 A 1.0 ugll 2.0 1.0 ugll 2.0 1.0 ugll 5.0 3.0 ugll 2.0 1.0 ugll 4.0 2.0 ugll 2.0 1.0 ugll 100 35 ugll 100 35 ugll 100 35 ugll 100 35 ugll 10{1 35 ugll 100 35 ugll Run# 2 Limits 70-130% 70-130% J = Indicates an estimated value B = Indicates analyze found in associated method blank N = Indicates presumptive evidence of a compound �a 17 of 119 ACCI�TEST. FA4939 '"•""•re.... Acculest LabLink@12:12 10-jun-2013 Report of Analysis Client Sample ID: MW-10 Lab Sample ID: FA4930-1 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: MADEP EPH REV I A SW846 3510C Perewt Solids: nla Project: URSNCM: 51S 1363, 1101 Hwy 61, Whilselt, NC Page t of 1 File ID DF Analyzed By Prep Date Prep Hatch Analytical Batch Run #1 NN004793.13 1 05/31/13 NMC 05/29/13 OP47077 GNN207 Run #2 Initial Volume Final Volume Run #1 1040 ml 2.0 ml Run #2 MAEPH List CAS No. Compound Result 83-32-9 Acenaphthene ND 208-96-8 Acenaphthylene ND 120.12-7 Anlhracene ND 56-55-3 Benzo(a)anthracene ND 50-32-8 Benzo(a)pyrene N❑ 205-99-2 Benzomnuoranthene ND 191-24-2 Benzo(g.h,i)perylene N❑ 207.08.9 Benzo(k)fluoranthene ND 218-01.9 Chrysene N❑ 53-70-3 Dibenzo(a,h)anthracene N❑ 206-44.0 Fluoranthene ND 86-73-7 Fluorene N❑ 193-39-5 Indeno(1,2,3-cd)pyrene ND 91-57-6 2-Methylnaphlhalene ND 91-20-3 Naphthalene ND 85-01-8 Phenanthrene ND 129-00-0 Pyrene N❑ CII-C22 Aromatics (Unadj.] 235 CII-C22 Aromatics 235 C9-C18 Aliphalics ND C19-C36 Aliphatics N❑ CAS No. Surrogate Recoveries Run# 1 3386-33-2 1-Chlorooctadecane 65% 580.13-2 2-Bromonaphlhalene 78°% 84-15-1 o-Terphenyl 63°% 321.60-8 2-Fluorobiphenyl 77% ND = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range RI., MDL Units Q 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 IA ugll 3.8 1.9 ug11 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 190 140 ugll 190 140 ugll 190 96 ugll 190 96 ugll Run# 2 Limits 40-140% 40-140% 40-140% 40-140% j = Indicates an estimated value B = indicates analyte found in associated method blank N = indicates presumptive evidence of a compound on 18 of 119 ACCLITE7�T. FA4930 °• • Accutest LabLink@12:12 10-Jun-2013 Report of Analysis Client Sample ID: MW-11 Lab Sample ID: FA4930-2 Matrix: AQ - Ground Water Method: SM 6200B Project: URSNCM: SIS 1363. 1101 Hwy 61, Whitsett, NC File ID DF Analymd By Prep Date Run , 1 E024406.13 1 06/04/13 TD Wit Run 42 Purge Volume Hun #1 t0.0 till Ruu #2 Page 1 of 1 Date Sampled: 05/22/13 Date Received: 05/23/13 Percent Solids: nla Prep Batch Analytical Batch ttla VE835 VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.10 ugli 75-27-4 Bromodichloromethane N❑ 0.50 0.10 ugll 107-06-2 1,2-Dichloraethane ND 0.50 0.10 ugll 108-20-3 Di -Isopropyl ether ND 0.50 0.10 ugll 124-48-1 Dibromochloromethane ND 0.50 0.10 ugll 156-59-2 cis-1,2-Dichloroethyiene ND 0.50 0.10 ugll 100-41-4 Ethylbenzene ND 0.50 0.10 ugll 99-87-6 p-Isopropyltoluene ND 0.50 0.10 ugll 74-87-3 Methyl chloride ND 0.50 0.11 ugA 1634-04-4 Methyl Tert Butyl Ether N❑ 0.50 0.10 ugll 91-20-3 Naphthalene 0.74 0.50 0.15 ugll 108-88-3 Toluene ND 0.50 0.10 ugll 79-01-6 Trichloroethylene ND 0.50 0.10 ugll 1330-20-7 Xylene [total] ND 1.5 0.22 ugll CAS No. Surrogate Recoveries Run# 1 Run* 2 Limits 1868-53-7 Dibromofluoromethane 102% 70-130%a 17060-07-0 1,2-Dichloroethane-D4 101% 70-130%4 2037-26-5 Toluene-D8 99% 70-130%n 460-00-4 4-Bromoiluorohenzene 100%a 70-130% ND = Not detected MDL - Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound I19 of 119 ACGUTEE3-r FA4930 ............ Accutest L.abl.ink@12;12 10-Jun-2013 Report of Analysis Page 1 of 2 Client Sample ID: MW-11 Lab Sample ID: FA4930-2 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: EPA 625 EPA 625 Percent Solids: nla Project: URSNCM. SIS 1363, 1101 Hwy 61. Whilsett, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 1-063712.1) 1 05/29/13 NAF 05/24/13 OP47046 SL3223 Run #2 Initial Volume Final Volume Run #1 1040 ml 1.0 ml Run #2 ABN List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 65-85-0 Benzoic Acid N❑ 48 9.6 ugll 95-57-8 2-Chlorophenol ND 4.8 0.68 ugll 59-50-7 4-Chloro-3-methyl phenol ND 4.8 0.78 ugll 120-83-2 2,4-Dichlorophenol N❑ 4.8 0.67 ugll 105-67-9 2,4-Dimethylphenol N❑ 4.8 0.74 ugll 51-28-5 2,4-Dinitrophenol ND 24 5.0 ugll 534.52-1 4,6-Dinitro-o-cresol N❑ 9.6 1.4 ugll 95-48-7 2-Methylphenal ND 4.8 0.69 ugll 3&4-Methylphenol ND 4.8 1.3 ug11 88-75-5 2-Nitrophenol ND 4.8 0.65 u911 100-02.7 4-Nitrophenol ND 24 4.8 ugll 87-86-5 Pentachlorophenol ND 24 4.8 ugll 108-95-2 Phenol ND 4.8 0.53 ugll 88-06-2 2,4.6-Trichlorophenol N❑ 4.8 0.75 ug11 83-32-9 Acenaphthene ND 4.8 0.67 ug1I 208.96-8 Acenaphthylene ND 4.8 0.67 ugll 120-12-7 Arnhracene ND 4.8 0.72 ugll 56-55-3 Benzo(a)anthracene ND C8 0.52 ug11 50-32-8 Benzo(a)pyrene ND C8 0.55 ugll 205-99-2 Benzo(b)fluoranthene N❑ 4.8 0.73 ugll 191-24-2 Benzo(g,h,i)perylene ND 4.8 0.64 ugll 207-08-9 Benzo(k)fluoranthene ND 4.8 0.64 ugll 101-55-3 4-Bromophenyl phenyl ether N❑ 4.8 0.76 ugll 85-68-7 Butyl henzyl phthalate ND 4.8 0.68 ugll 100-51.6 Benzyl Alcohol ND 4.8 0.96 ug11 91-58-7 2-Chloronaphthalene ND 4.8 0.70 ugll 106-47.8 4-Chlaroaniline ND 4.8 0.66 ugll 218-01-9 Chrysene N❑ 4.8 0.56 ugll 111-91-1 bis(2-Chloroethoxy)methane N❑ 4.8 0.67 ugll 111-44-4 his(2-Chloroethyl)ether ND 4.8 0.69 ugll 108-60-1 bis(2-Chloroisopropyl)e1her ND 4.8 0.76 ugll 7005-72-3 4-Chlorophenyl phenyl ether ND 4.8 0.84 ugll ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value RL = Reporting limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■_ 20of119 FA4930 ...... ""' Accutest LabLink912:12 10-jun-2013 Report of Analysis Client Sample ID: MW-11 Lab Sample ID: FA4930-2 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: EPA 625 EPA 625 Percent Solids: nla Project: UR5NCM: 51S 1363. 1101 Hwy 61, Whitsett, NC ASN List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 95-50-1 1,2-Dichlorobenzene ND 4.8 0.65 ugll 122-66-7 1.2-Diphenyihydrazine ND 4.8 0.62 ugll 541-73-1 1,3-Dichlorobenzene ND 4.8 0.75 ugll 106-46-7 1,4-Dichlorobenzene ND 4.8 0.67 ugll 91-94-1 3,3'-Dichlorobenzidine ND 4.8 0.71 ugll 53-70-3 Dibenzo(a,h)anthracene N❑ 4.8 0.56 ugll 132-64-9 Dibenzofuran N❑ 4.8 0.72 ugfl 84-74-2 Di-n-butyl phthalate ND 4.8 0.96 ug11 117-84-0 Di-n-octyl phthalate ND 4.8 0.96 ug1l 84-66-2 Diethyl phthalate ND 4.8 0.96 ugll 131-11.3 Dimethyl phthalate N❑ 4.8 0.77 ugll 117-81-7 bis(2-Ethylhexyl)phthalate ND 4.8 1.1 ugll 206-44.0 Fluoranthene N❑ 4.8 0.56 ugll 86-73-7 Fluorene 0.81 4.8 0.73 ugll j 118-74-1 Hexachlorobenzene ND 4.8 0.66 ugll 87-68-3 Hexachlorobutadiene ND 4.8 0.92 ugll 77-47-4 Hexachlorocyclopentadiene ND C8 0.76 ugll 67-72-1 Hexachloroethane ND 4.8 0.71 ugll 193-39-5 Indeno(1,2,3-cd)pyrene N❑ 4.8 0.55 ugll 78-59-1 Isophorone ND 4.8 0.61 ugll 90-12-0 1-Methyinaphthalene ND 4.8 0.68 ugll 91-57-6 2-Methylnaphlbalene 0.80 4.8 0.66 ug/l j 91-20-3 Naphthalene 0.85 4.8 0.61 ugA J 98-95-3 Nitrobenzene ND 4.8 0.69 ugll 621-64-7 N-Nilroso-di-n-propylamine ND 4.8 0.82 ugll 86-30-6 N-Nitrosodiphenylamine ND 4.8 0.96 ugll 85-01-8 Phenanthrene 1.0 4.8 0.68 ugll j 129-00-0 Pyrene ND 4.8 0.65 ug/l 120-82-1 1,2.4-Trichlorobenzene ND 4.8 0.58 ugll CAS No. Surrogate Recoveries Run# i Run# 2 Limits 367-12-4 2-Fluorophenol 52% 14-67% 4165-62-2 Phenol-d5 38% 10-50% 118-79-6 2,4,6-Tribromophenol 96% 33-118% 4165-60-0 Nitrobenzene-d5 85% 42-108% 321-60-8 Z-Fluorabiphenyl 91% 40-106% 1718-51-0 Terphenyl-d14 89% 39-121% Page 2 of 2 ND = Not detected MDL - Method Detection Limit j = Indicates an estimated value RL = Reporting Limit S = Indicates analyle found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■■ 21 of 119 ■ ALCCU-rt=Sx FA4930 "....I - Accutest LabLink@12:12 10-jun-2013 Report of Analysis Client Sample ID: MW-11 Lab Sample ID: FA4930-2 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: MADEP VPH REV 1.1 Percent Solids: nla Project: URSNCM: 51S 1363, 1101 Hwy 61, Whitsett, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Hatch [tun #1 UU003567.D 1 06/04/13 MM nla nla GUU178 Run #2 Purge Volume Run #1 5.0 ml Run #2 MADEP VPH List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 1.0 1.0 ugll 100-41-4 Ethylbenzene ND 2.0 1.0 ugll 1634-04-4 Methyl Tert Butyl Ether ND 2.0 1.0 ugll 91-20-3 Naphthalene N❑ 5.0 3.0 ugll 108-88-3 Toluene N❑ 2.0 1.0 ugll m,p-Xylene N❑ Co 2.0 ugll 95-47-6 o-Xylene ND 2.0 1.0 ugll C5- C8 Aliphatics (Unadj.) ND 100 35 ugll C9- C12 Aliphatics (Unadj.) ND 100 35 ugA C9- C10 Aromatics (Unadj.) ND 100 35 ugll C5- C8 Aliphatics ND 100 35 ugll C9- C12 Aliphatics ND 100 35 ug11 C9- C10 Aromatics ND 100 35 ug11 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 460.00.4 BFB 91% 70-130% 460-00-4 BFB 93% 70-130% ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound A is 10 22 of 119 ACCUTE:3T. FA4930 .,....,.... Accutest LabL1nk@12:12 10-Jun-2013 Report of Analysis Client Sample ID. MW-lI Lab Sample ID: FA4930-2 Matrix: AQ - Ground Water Method: MADEP EPH REV 1-I SW846 3510C Project: URSNCM: S/S 1363, 1101 Hwy 61, Whitselt, NC File ID DF Analyzed By Prep Date ;Run #1 NN004794.1) 1 05/31/13 NMC 05/29/13 Run #2 Initial Volume Final Volume Run #1 1040 ml 2.0 ml Run #2 MAEPH List CAS No. Compound Result 83-32-9 Acenaphthene ND 208-96-8 Acenaphthylene N❑ 120-12-7 Anthracene ND 56-55-3 BenzoWanthracene N❑ 50-32-8 Benxo(a)pyrene ND 205-99-2 Benxo(b)fluoranthene ND 191-24-2 Benzo(g,h,i)perylene ND 207-08-9 Benzo(k)fluoranthene N❑ 218-01-9 Chrysene ND 53-70-3 Dibenzo(a,h)anthracene ND 206-44-0 Fluoranthene ND 86-73-7 Fluorene ND 193-39-5 Indeno(1,2.3-cd)pyrene ND 91-57-6 2-Methylnaphthalene ND 91.20-3 Naphthalene N❑ 85-01-8 Phenanthrene ND 129-00-0 Pyrene ND C11-C22 Aromatics (Unadj.) 178 C 11-C 22 Aromatics 178 C9-C 18 Aliphatics ND C19-06 Aliphatics ND CAS No. Surrogate Recoveries Run# 1 3386-33-2 1-Chlorooctadecane 60% 580-13-2 2-Bromonaphthalene 74% 84-15-1 o-Terphenyl 55% 321-60-8 2-Fluorobiphenyl 72% ND = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range Page 1 of 1 A Date Sampled: 05/22/13 N Date Received: 05/23/13 Percent Solids: nla Prep Batch Analytical Batch OP47077 GNN207 RL MDL Emits Q 3.8 1.9 ug1I 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugli 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 L9 ugA 3.8 1.9 ugjl 3.8 1.9 ugA 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 I.9 ugll 190 140 ugll j 190 I40 ugll j 190 96 ugll 190 96 ugll Run# 2 Limits 40- I 40% 40-140% 40-140% 40-140% J = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound MR 23 of 119 ■ ACCu-r1=-s-►: Accutest LahLink@12:12 10-jun-2013 Report of Analysis Client Sample ID: MW-15 Lab Sample ID: FA4930-3 Matrix: AQ - Ground Water Method: SM 6200B Project: URSNCM: S1S 1363, 1101 Hwy 61, Whitsen, NC File 1D DF Analyzed By Prep Date Run #1 E024407.D 1 06/04/13 TD nla Run #2 Purge Volume Run #1 10.0 ml Run #2 Page 1 of 1 A Date Sampled: 05/22/13 4, Date Received: 05/23/13 Percent Solids: nla Prep Batch Analytical Batch nla VE835 VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene N❑ 0.50 0.10 ugll 75-27-4 Bromodichloromethane ND 0.50 0.10 ugll 107-06-2 1,2-Dichloroethane ND 0.50 0.10 ugll 108-20-3 Di -Isopropyl ether ND 0.50 0.10 ugl! 124-48-1 Dibromochloromethane N❑ 0.50 0,10 ugll 156-59-2 cis- 1,2-Dichloroethylene ND 0.50 0.10 ugll 100-41-4 Ethylbenzene ND 0.50 0.10 ugll 99-87-6 p-lsopropyholuene ND 0.50 0.10 ugli 74-87-3 Methyl chloride ND 0.50 0.11 ugll 1634-04-4 Methyl Tent Butyl Ether 0.15 0.50 0.10 ugA J 91-20-3 Naphthalene ND 0.50 0.15 ugll 108-88-3 Toluene ND 0.50 0.10 ugll 79-01-6 Trichloroethyiene ND 0.50 0.10 ugll 1330-20-7 Xylene (total) N❑ 1.5 0.22 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromolluoromethane 100% 70-130% 17060-07-0 1,2-Dichloroethane-D4 99% 70-130% 2037-26-5 Toluene-D8 100% 70-130% 460-00-4 4-Bromoftuorobenzene 101% 70-130% ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyse found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Est 24 of 119 ACCUTES-r FA4930 Accutest LahLink@12:12 10-Jun-2013 Report of Analysis Client Sample ID: MW-15 Lab Sample ID: FA4930-3 Date Sampled- 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: EPA 625 EPA 625 Percent Solids: nla Project: i1RSNCM: S1S 1363, 1101 Hwy 61, Whilsett, NC Page I of 2 File ID DF Analyzed By Prep date Prep Batch Analytical Batch Run #1 L063713.D 1 05/29/13 NAF 05/24/13 OP47046 SL3223 Run #2 Initial Volume Final Volume Run #1 1040 ml 1.0 ml Run #2 ABN List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 65-85-0 Benzoic Acid N❑ 48 9.6 ugll 95-57-8 2-Chlorophenol N❑ 4.8 0.68 ugll 59.50-7 4-Chlora-3-methyl phenol ND 4.8 0.78 ugll 120-83-2 2,4-Dichlorophenot ND 4.8 0.67 ugli 105.67.9 2,4-Dimethylphenol ND 4A 0.74 ugll 51-28-5 2,4-Dinitrophenol ND 24 5.0 ugll 534-52-1 4,6-Dinitro-o-cresol ND 9.6 1.4 ugll 95-48-7 2-Methylphenol ND 4.8 0.69 ugll 3&4-Methylphenol ND 4.8 1.3 ugll 88-75-5 2-Nitrophenai ND 4.8 0.65 ugll 100-02-7 4-Nilrophenoi ND 24 4.8 ugll 87-86-5 Pentachlorophenol ND 24 4.8 ugll 108-95-2 Phenol ND 4.8 0.53 ugll 88-06-2 2,4,6-Trichlorophenol ND 4.8 0.75 ugll 83-32-9 Acenaphthene ND 4.8 0.67 ugll 208-96-8 Acenaphthylene ND 4.8 0.67 ugll 120-12-7 Anthracene ND 4.8 0.72 ugll 56-55-3 Benzo(a)anthracene ND 4.8 0.52 ugll 50-32-8 Benzo(a)pyrene ND 4.8 0.55 ugll 205-99-2 Benzo(b)fluoranthene ND 4.8 0.73 ugll 191-24-2 Benzo(g,h,i)perylene ND 4.8 0.64 ugll 207-08-9 Benzo(k)fluoranthene ND 4.8 0.64 ugll 101.55-3 4-Bromophenyl phenyl ether ND 4.8 0.76 ugll 85-68-7 Butyl benzyl phthalate ND 4.8 0.68 ugll 100.51-6 Benzyl Alcohol ND 4.8 0.96 ugll 91-58-7 2-Chloronaphthalene ND 4.8 0.70 ug/1 I06-47-8 4-Chloroaniline ND 4.8 0.66 ugll 218.01-9 Chrysene ND 4.8 0.56 ugll 111-91-1 bis(2-Chioroethoxy)methane ND 4.8 0.67 ugll 111-44-4 bis(2-Chloroethyl)elher ND 4.8 0.69 ugll 108.60-1 bis(2-Chloroisopropyl)ether ND 4.8 0.76 ugll 7005-72-3 4-Chlorophenyl phenyl ether ND 4.8 0.84 ugll ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates anaiyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound on 25 of 119 FA4930 Accutest LabLink@12:12 10-jun-2013 Report of Analysis Client Sample ID: MW-15 Lab Sample ID: FA4930-3 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: EPA 625 EPA 625 Percent Solids: nla Project: URSNCM: S/S 1363, 1101 Hwy 61. Whitsett, NC ABN List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 95-50-1 1,2-Dichlorebenzene ND 4.8 0.65 ug1l 122-66-7 1,2-Diphenylhydrazine ND 4.8 0.62 ugll 541-73-1 1,3-Dichlorobenzene ND 4.8 0.75 ugll 106-46-7 1,4-❑ichlorohenzene ND 4.8 0.67 ugA 91-94-1 3,T-Dichlorobenzidine ND 4.8 0.71 ugll 53-70-3 Dibenzo(a,h)anthracene ND 4.8 0.56 ugll 132-64-9 Dibenzofuran ND 4.8 0.72 ug/l 84-74-2 Di-n-butyl phthalate ND 4.8 0.96 ugli 117-84-0 Di-n-octyl phthalate ND 4.8 0.96 ugll 84-66-2 Diethyl phthalate ND 4.8 0.96 ugll 131-11-3 Dimethyl phthalate ND 4.8 0.77 ugll 117-81-7 bis(2-Ethylhexyl)phthalate ND 4.8 1.1 ugll 206-44-0 Fluoranthene ND 4.8 0.56 ugll 86-73-7 Fluorene ND 4.8 0.73 ugll 118-74-1 Hexachlorobenzene ND 4.8 0.66 ugll 87-68-3 Hexachlorobutadiene ND 4.8 0.92 ugll 77-47-4 Hexachlorocyclopentadiene N❑ 4.8 0.76 ugll 67-72-1 Hexachloroethane ND 4.8 0.71 u911 193-39-5 Indeno(1,2,3-cd)pyrene ND 4.8 0.55 ugll 78-59-1 Isophorone ND 4.8 0.61 ugA 90-12-0 1-Methylnaphthalene ND 4.8 0.68 ugll 91-57-6 2-Methylnaphthalene ND 4.8 0.66 ugll 91-20-3 Naphthalene ND 4.8 0.61 ug/l 98-95-3 Nitrobenzene ND 4.8 0.69 ugll 621-64.7 N-Nitroso-di-n-propylamine ND 4.8 0.82 ugli 86-30-6 N-Nitrosodiphenylamine ND 4.8 0.96 ug1l 85-01-8 Phenanthrene ND 4.8 0.68 ug11 129-00-0 Pyrene ND 4.8 0.65 ugll 120-82-1 1,2,4-Trichlorobenzene ND 4.8 0.58 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 44% 14-67% 4165-62-2 Phenol-d5 31% 10-50% 118-79-6 2,4.6-Tribromophenol 88% 33-118% 4165-60-0 Nitrobenzene-d5 75% 42-108% 321-60-8 2-Fluorobiphenyl 80% 40-106% 1718-51-0 Terphenyl-dl4 81% 39-121% Page 2 of ND = Not detected MDL - Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = Indicates analyze found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound a/ 26 of 119 ■.a.CCI I-r-E-=E5T Accutest LabLink@12:12 10-Jun-2013 Report of Analysis Client Sample ID: MW-15 Lab Sample ID: FA4930-3 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: MADEP VFH REV 1.1 Percent Solids: nla Projed: URSNCM: S/S 1363, 1101 Hwy 61. Whitsett, NC Pagr I of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 U0003568.D 1 06/04/13 MM nla rtla GUU178 Run #2 Purge Volume Run #1 5.0 Sill Run #2 MADEP VPH List CAS No. Compound Result 71-43-2 Benzene ND 100-41-4 Ethylbenzene ND 1634-04-4 Methyl 'Pert Butyl Ether ND 91-20-3 Naphthalene ND 108-88-3 Toluene N❑ m.p-Xylene ND 95-47-6 o-Xylene N❑ C5- C8 Aliphatics (Unadj.) ND C9- C1Z Aliphatics (Unadj.) ND C9- C10 Aromatics (Unadj.) ND C5- C8 Aliphatics N❑ C9- C12 Aliphatics ND C9- CIO Aromatics N❑ CAS No. Surrogate Recoveries Run# 1 460-00-4 BFB 84% 460-00-4 BFB 87% N❑ = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range RL MDL Chits Q 1.0 1.0 ugll 2.0 1.0 ugll 2.0 1.0 ugll 5.0 3.0 ugll 2.0 1.0 ugll 4.0 2.0 ug11 2.0 1.0 ugll 100 35 ugll 100 35 ugll 100 35 ugll 100 35 ugll 100 35 ugll 100 35 ug11 Run# 2 Limits 70-130% 70-130% j = Indicates an estimated value B = Indicates analyte found in associated method Mani: N = Indicates presumptive evidence of a contpuund 27 of 119 ACC!-JTEST. FA333Q "'°""."" Accutest LabLink@12:12 10-jun-2013 Report of Analysis Client Sample ID: MW-15 Lab Sample ID: FA4930-3 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: MADEP EPH REV I.I SW846 3510C Percent Solids: nla Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 NN004795.1) 1 05/31/13 NMC 05/29/13 OP47077 GNN207 Run #2 Initial Volume Final Volume Run #1 1050 ml 2.0 ml Run #2 MAEPH List CAS No. Compound Result RL MDL Units Q 83-32-9 Acenaphthene ND 3.8 1.9 ugll 208-96-8 Acenaphthyiene ND 3.8 1.9 ugll 120-12-7 Anthracene ND 3.8 1.9 ugll 56-55-3 Benzo(a)anthracene ND 3.8 1.9 ugll 50-32-8 Bmo(a)pyrene N❑ 3.8 1.9 ugll 205-99-2 Benzo(b)fluoranthene ND 3.8 1.9 ugll 191-24-2 Benzo(g,hJ)perylene ND 3.8 1.9 ugll 207-08-9 Benzo(k)fluoranthene N❑ 3.8 1.9 ug1l 218-01-9 Chrysene N❑ 3.8 1.9 ugll 53-70-3 Dibenxo(a,h)anthracene ND 3.8 1.9 ugll 206-44-0 Fluoranthene ND 3.8 1.9 ugll 86-73-7 Fluorene N❑ 3.8 1.9 ugll 193-39.5 lndeno(1,2,3-cd)pyrene ND 3.8 1.9 ugll 91-57-6 2-Methylnaphthalene ND 3.8 1.9 ugll 91-20.3 Naphthalene ND 3.8 1.9 ugll 85-01-8 Phenanthrene ND 3.8 1.9 uglf 129-00-0 Pyrene ND 3.8 1.9 ugll C11-C22 Aromatics (Unadj.) ND 190 140 uglf CII-C22 Aromatics ND 190 140 uglf C9-08 Aliphatics ND 190 95 ugll C19-06 Aliphatics ND 190 95 ugll CAS No. Surrogate Rewwries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane fib% 40-140% 580-13-2 2-Bromonaphthalene 85% 40-140% 84-15-1 o-Terphenyl 55% 40-140% 321-60-8 2-Fluorobiphenyl 85% 40-140% ND = Not detected MDL - Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■, 28 of 119 ■,acctJ-r�s� FA4930 Accutest LabLink@12:12 10-Jun-2013 Report of Analysis Client Sample ID: USTMW-1 Lab Sample ID: FA4930-4 Matrix: AQ - Ground Water Method: SM 6200B Project: URSNCM: S/S 1363, 1101 Hwy 61, Whitsett, NC File ID DP Analyzed By Prep Date Run #1 E024409.D 1 06/04/13 TD nla Run #2 Purge Volume Run # 1 10.0 ml Run #2 Page 1 of i Date Sampled: 05/22/13 Date Received: 05/23/13 Percent Solids: nla Prep Batch Analytical Batch nla VE835 VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene N❑ 0.50 0.10 ugll 75-27.4 Bromodichloromethane ND 0.50 0.10 ugll 107-06-2 1.2-Dichloroethane N❑ 0.50 0.10 ugfl 108-20-3 Di -Isopropyl ether ND 0.50 0.10 ugll 124-48-1 Dibromochloromethane N❑ 0.50 0.10 ugll 156-59.2 cis-1,2-Dichloroethylene ND 0.50 0.10 ugll 100-41-4 Eth_ylbenzene 0.11 0.50 0.10 ugll J 99-87.6 p-Isopropyltoluene ND 0.50 0.10 ugll 74-87-3 Methyl chloride 0.12 0.50 0.11 ugll J 1634-04-4 Methyl Teri Butyl Ether ND 0.50 0.10 ugll 91-20-3 Naphthalene 33.1 0.50 0.15 ugll 108-88.3 Toluene ND 0.50 0.10 ugll 79-01-6 Trichloroethylene N❑ 0.50 0.10 ugll 1330-20.7 Xylene (total) N❑ 1.5 0.22 ugll CAS No. Surrogate Recoveries Run* 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 100% 70-130% 17060-07-0 1,2-Dichioroethane-D4 101% 70.130% 2037-26-5 Toluene-D8 99% 70-130% 460-00-4 4-Bromofluorobenzene 101% 70.130% N❑ = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range J = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound ■R 29 of 119 M ACCiJTE=-ST. FA4930 .•.... I-- Accutest LabLink@12:12 10-Jun-2013 Report of Analysis Page 1 of 2 Client Sample ID: USTMW-1 Lab Sample ID: FA4930-4 Date Sampled: 05/22/13 A Matrix: AQ - Ground Water Date Received: 05/23/13 Method: EPA 625 EPA 625 Percent Solids: nla Project: URSNCM: SIS 1363, 1101 Hwy fit, Whitsett, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 L063714.❑ 1 05/29/13 NAF 05/24/13 OP47046 SL3223 Run #2 Initial Volume Final Volume Run #1 1040 ml 1.0 ml Run #2 ABN List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 48 9.6 ugll 95-57-8 2-Chlorophenol ND 4.8 0.68 ugll 59-50-7 4-Chloro-3-methyl phenol ND 4.8 0.78 ugli 120-83-2 2,4-Dichlorophenol N❑ 4.8 0.67 ugll 105-67-9 2,4-Dimethylphenol ND 4A 0.74 ug1l 51-28-5 2,4-Dinitrophenol N❑ 24 5.0 ug1l 534-52-1 4,6-Dinitro-o-cresol N❑ 9.6 L4 uglt 95-48-7 2-Methylphenol N❑ 4.8 0.69 ugll 3&4-Methylphenol N❑ 4.8 1.3 ugll 88-75-5 2-Nitrophenol ND 4.8 0.65 ugll 100-02.7 4-Nitrophenol N❑ 24 4.8 ug11 87-86-5 Pentachlorophenol ND 24 4,8 ugll 108-95-2 Phenol N❑ 4.8 0.53 ugll 88-06-2 2,4.6-Trichlorophenol N❑ 4.8 0.75 ugll 83-32-9 Acenaphthene 5.7 4.8 0.67 ugll 208-96-8 Acenaphthylene ND 4.8 0.67 ugll 120-12-7 Anthracene N❑ 4.8 0.72 ugll 56-55-3 Benzo(a)anthracene N❑ 4.8 0.52 ugll 50-32-8 Benzo(a)pyrene N❑ 4.8 0.55 ugfI 205-99-2 Benzo(b)fluoranthene ND 4.8 0.73 ugll 191-24-2 Benzo(g,h,i)perylene ND 4.8 0.64 ugll 207-08-9 Benzo(k)fluoranthene ND 4.8 0.64 ugll 101-55-3 4-Bromophenyl phenyl ether N❑ 4.8 0.76 ug1I 85-68-7 Butyl benzyl phthalate ND 4.8 0.68 ugil 100-51-6 Benzyl Alcohol ND C8 0.96 ugll 91-58-7 2-Chloronaphlhalene ND 4.8 0.70 ugll 106-47-8 4-Chloroaniiine ND 4.8 0.66 ugll 218.01-9 Chrysene ND 4.8 0.56 ugll 111-91-1 his (2-Chloroelhoxy) methane N❑ 4.8 0.67 ugll 111.44.4 bis(2-Chloroethyl)ether ND 4.8 0.69 ugll 108-60-1 his (2-Chloroisopropyl) ether ND 4.8 0.76 ug/l 7005-72-3 4-Chlorophenoi phenyl ether ND 4.8 0.84 ugll ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■o 30 of 119 ACCUTEST. FA4930 I ..... I-.: Accutest LabLinkP12:12 10-Jun-2013 Report of Analysis Client Sample ID: USTMW-1 Lab Sample ID: FA4930-4 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: EPA 625 EPA 625 Percent Solids: nla Project: URSNCM: SIS 1363, 1101 Hwy 61, Whilsett. NC ABN List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 95-50-1 1,2-Dichlorobemene ND 4.8 0.65 ugll 122-66-7 1,2-Diphenylhydrazine ND 4.8 0.62 ugll 541-73-1 1,3-Dichlorobenzene ND 4.8 0.75 ugll 106-46-7 1,4-❑ichlorobenzene ND 4.8 0.67 ugll 91-94-1 3.3'-Dichlarobenzidine ND 4.8 0.71 ugll 53-70-3 Dibenzo(a,h)anthracene N❑ 4.8 0.56 ugll 132-64-9 ❑ibenzofuran 3.2 4.8 0.72 ugli J 84-74-2 Di-n-butyl phthalate ND 4.8 0.96 ugA 117-84-0 Di-n-octyl phthalate ND 4.8 0.96 ugA 84-66-2 Diethyl phthalate ND 4.8 0.96 ugll 131-11-3 Diethyl phthalate N❑ 4.8 0.77 ugA 117-81-7 bis(2-E1hy1hexy1)ph1ha1ate N❑ 4.8 1.1 ugA 206-44-0 Fluoranthene 0.73 4.8 0.56 ugll J 86-73-7 Fluorene 11.6 4.8 0.73 ugA 118-74-1 Hexachlorobenzene ND 4.8 0.66 ugA 87-68-3 Hexachlorobutadiene N❑ 4.8 0.92 ugA 77-47-4 Hexachlorocyclopeniadiene N❑ 4.8 0.76 ugll 67-72-1 Hexachloroethane ND 4.8 0.71 ugll 193-39-5 Indeno(1,2,3-cd)pyrene ND 4.8 0.55 ugA 78.59.1 Isophorone ND C8 0.61 ugll 90-12-0 1-Methylnaphihalene 49.0 4.8 0.68 ugll 9I-57-6 2-Methyinaphthalene 38.0 4.8 0.66 ugll 91-20-3 Naphthalene 27.5 4.8 0.61 ugli 98-95-3 Nitrobenzene ND 4.8 0.69 ug1l 621-64-7 N-Nilroso-di-n-propylamine N❑ 4.8 0.82 ug11 86-30-6 N-Nitrosodiphenytamine ND 4.8 0.96 ugll 85-0I.8 Phenanthrene 13.7 4.8 0.68 ugll 129-00-0 Pyrene 3.9 4.8 0.65 ugll ] 120-82.1 1,2,4-Trichlorobenzene N❑ 4.8 0.58 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 367-12.4 2-Fluorophenol 37% 14-67% 4165-62-2 Phenol-d5 25% 10-50% 118-79-6 2,4,6-Tribromophenol 91% 33.118% 4165-60-0 Nitrobenzene-6 93% 42-108% 321-60.8 2-Fluorohiphenyl 99% 40-106% 1718-51-0 Terphenyi-d14 80% 39-121% Page 2 of 2 N❑ = Nat detected MDL - Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound A A ■o 31 of 119 w ACCL_fTEST. FA4930 `.........I. Accutest LabLink@12:12 10-jun-2013 Report of Analysis Client Sample ID: USTMW-1 Lab Sample ID: FA4930-4 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: MADEP VPH REV 1.1 Percent Solids: nla Project: URSNCM: S1S 1363, 1101 Hwy 61, Whitsett, NC Pane l of 1 Fite ID DF Analyzed By Prep Date Prep Batch Analytical Bate Run #1 a UU003579.❑ 1 06/05/13 MM n/a nla CUU179 Run #2 Purge Volume Run #1 5,02111 Run #2 MADEP VPH List CAS No. Compound Result 71-43-2 Benzene ND 100-41-4 Ethylbenzene ND 1634-04-4 Methyl Test Butyl Ether ND 91-20-3 Naphthalene b 78.3 108-88-3 Toluene N❑ m,p-Xylene ND 95-47-6 o-Xylene N❑ C5- C8 Aliphatics (Unadj.) N❑ C9- C12 Aliphatics (Unadj.) 57.3 C9- C10 Aromatics (Unadj.) 244 C5- C8 Aliphatics ND C9- C12 Aliphatics 57.3 C9- C10 Aromatics 244 CAS No. Surrogate Recoveries Run# 1 460-00-4 BFB 124% 460-00-4 BFB 112% (a) No sample available for reanalysis. (b) Associated CCV recovery outside control limits. ND = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range RL MDL Units Q 1.0 1.0 ugll 2.0 1.0 ugll 2.0 1.0 ugll 5.0 3.0 ugll j 2.0 1.0 ugll 4.0 2.0 ugll 2.0 1.0 ugll 100 35 ugll 100 35 ugll J 100 35 ugll 100 35 ugll 100 35 ugll j 100 35 ugll Rua# 2 Limits 70-130% 70-130% l = Indicates an estimated value B = Indicates analyle found in associated method blank N = Indicates presumptive evidence of a compound ■ 32 of 119 ■ .accUTE-=s-r. FA4930 "••""re.... Accutest Lab> ink@12:12 10 Jun-2013 Report of Analysis Client Sample ID: USTMW-I Lab Sample ID: FA4930-4 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: MADEP EPH REV IA SW846 3510C Percent Solids: nla Project: URSNCM: S/S 1363, 1101 Hwy 61, Whitsett, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 NN004798.1) 1 05/31/13 NMC 05/29/13 OP47077 GNN207 Run #2 Initial Volume Final Volume Run #1 1040 nil 2.0 mt Run #2 MAEPH List CAS No. Compound Result 83-32-9 Acenaphthene ND 208-96-8 Acenaphthylene ND 120-12-7 Anthracene ND 56-55-3 Benzo(a)anthracene ND 50-32-8 Benzo(a)pyrene ND 205-99-2 Benzo(b)fluoranthene ND 191-24-2 Benzo(g,h,i)perylene ND 207-08-9 Benzo(k)fluoranthene ND 218-01-9 Chrysene ND 53-70-3 ❑ibenzo(a,h)anthracene ND 206-44-0 Fluoranthene N❑ 86-73-7 FIuorene ND 193-39-5 Indeno(1,2,3-cd)pyrene N❑ 91-57-6 2-Methylnaphthalene 28.6 91-20-3 Naphthalene 8.5 85-01-8 Phenanthrene 3.2 129-00-0 Pyrene ND Cll-C22 Aromatics (Unadj.) 562 C11-C22 Aromatics 521 C9-C18 Aliphatics 1390 C19-06 Aliphatics 394 CAS No. Surrogate Recoveries Run# 1 3386-33-2 1-Chlorooctadecane 70% 580-13-2 2-Bromonaphthalene 81% 84-15-1 o-Terphenyl 58°% 321-60-8 2-Fluorohiphenyl 76% ND = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range RL MDL Units Q 3.8 1.9 ugli 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.9 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugli j 3.8 1.9 ugll 190 140 ugll 190 140 ugll 190 96 ugll 190 96 ugll Run# 2 Limits 40-140% 40-140% 40-140% 40-140% j = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound me 33 at 119 E ACCLJ-TEST. Accutest LabLink@12:12 10-Jun-2013 Report of Analysis Client Sample ID: USTMW-2 Lab Sample ID: FA4930-5 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: SM 6200B Percent Solids: nla Project: URSNCM: S/S 1363, 1101 Hwy 61, Whitse(t, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E024408.1) 1 06/04/13 TI) nla nla VE835 Run #2 E024414.1) 2 06/04/13 TD nla nla VE835 Purge Volume Run #1 10.0 ml Run #2 10.0 ml VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene 1.5 0.50 0.10 ugll 75-27-4 Bromodichloromethane ND 0.50 0.10 ugll 107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug1I 108-20-3 Di -Isopropyl ether ND 0.50 0.10 ugll 124-48-1 ❑ibromochloromethane ND 0.50 0.10 ugll 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ugll 100-41-4 Ethylbenzene 0.27 0.50 0.10 ugll J 99-87-6 p-Isopropyitoluene ND 0.50 0.10 ugll 74-87-3 Methyl chloride ND 0.50 0.11 ugll 1634-04-4 Methyl Tert Butyl Ether 0.20 0.50 0.10 ugll J 91-20-3 Naphthalene 97.33 1.0 0.30 ugll 108-88-3 Toluene 0.21 0.50 0.10 ugll J 79.01-6 Trichloroethylene ND 0.50 0.10 ug11 1330-20-7 Xylene [(otal} 0.42 1.5 0.22 ugll J CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 100% 98% 70-130% 17060-07-0 1,2•Dichloroethane-D4 100% 100% 70-130% 2037-26-5 Toluene-D8 98% 101% 70-130% 460-00-4 4-Bromofluorobenzene IDO% 102% 70-130% (a) Result is from Run# 2 ND = Not detected MDL - Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = Indicates analyse found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■R 34 of 118 ACCUTE9T. FA4936 ...... I " - Accutest LabLink012:12 10-Jun-2013 Report of Analysis Page 1 nF 2 Client Sample ID: USTMW-2 Lab Sample ID: FA4930-5 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: EPA 625 EPA 625 Percent Solids: nla Project: URSNCM. SIS 1363, 1101 Hwy 61, Whitsett, NC File ID DF Analysed By Prep Date Prep Batch Analytical Batch Run #1 a L063715.D 10 05/29/13 NAF 05/24/13 OP47046 SL3223 Run #2 Initial Volume Final Volume Run #1 1040 ml 1.01111 Run #2 ABN List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 65-85-0 Benoit Acid ND 480 96 ugll 95-57-8 2-Chlorophenol ND 48 6.8 ug11 59-50-7 4-Chloro-3-methyl phenol ND 48 7.8 ugll 120-83-2 2,4-Dichlorophenol ND 48 6.7 ugll 105-67-9 2,4-Dimethylphenol ND 48 7.4 ugll 51.28-5 2,4-Dinitrophenol ND 240 50 ugll 534-52-1 4,6-Dinitro-o-cresol ND 96 14 ugll 95-48-7 2-Methylphenol ND 48 6.9 ugll 3&4-Methylphenol ND 48 13 ugll 88.75-5 2-Nitrophenol ND 48 6.5 ugll 100-02-7 4-Nitrophenol ND 240 48 ugll 87-86-5 Pentachlorophenol N❑ 240 48 ugll 108-95-2 Phenol ND 48 5.3 ugll 88-06-2 2,4,6-Trichlorophenol ND 48 T5 ug1l 83-32-9 Acenaphthene 17.4 48 6.7 ugll 208-96-8 Acenaphthylene ND 48 6.7 ugll 120-12-7 Anthracene ND 48 7.2 ugA 56-55-3 Benzo(a)anthracene ND 48 5.2 ugll 50.32-8 Benzo(a)pyrene ND 48 5.5 ugll 205-99-2 Benzo(b)1luoranthene ND 48 7.3 ugll 191-24-2 Benzo(g,h,i)perylene ND 48 6.4 ugll 207-08-9 Benzo(k)lluoranthene ND 48 6.4 ugll 101.55-3 4-Bromophenyl phenyl ether ND 48 7.6 ugll 85-68-7 Butyl benzyl phthalate ND 48 6.8 ugll 100-51-6 Benzyl Alcohol ND 48 9.6 ugA 91-58-7 2-Chloronaphthalene ND 48 7.0 ugll 106-47-8 4-Chloroaniline ND 48 6.6 ugll 218-01-9 Chrysene ND 48 5.6 ugll 111-91-1 bis(2-Chloroethoxy)methane ND 48 6.7 ugA 111-44-4 bis(2-Chloroethyl)ether ND 48 6.9 ugll 108-60-1 bis(2-Chloroisopropyl)ether ND 48 7.6 ugll 7005-72-3 4-Chlorophenyl phenyl ether ND 48 8.4 ugll ND = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range J J = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound �S 35 of 119 ACCI...JTEST. FA*30 ...... "" • • Accutest LabLink@12:12 10-Jun-2013 Report of Analysis Client Sample ID: USTMW-2 Lab Sample ID: FA4930-5 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: EPA 625 EPA 625 Percent Solids: nla Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC ABN List for NC, May 2012 CAS No. Compound Result RL MDL Units 95-50-1 1,2-Dichlorohenzene N❑ 48 6.5 ug11 122-66-7 1,2-Diphenylhydrazine ND 48 6.2 ugll 541-73-1 1,3-Dichlorobenzene N❑ 48 7.5 ugll 106-46-7 I A-Dichlorobenzene ND 48 6.7 ugll 91-94-1 3,3'-Dichlorobenzidine ND 48 7.1 ugll 53-70-3 Dibenza(a,h)anthracene ND 48 5.6 ugll 132-64-9 ❑ibenzo€uran ND 48 7.2 ugll 84-74-2 Di-n-butyl phthalate N❑ 48 9.6 ug11 117-84-0 Di-n-octyl phthalate ND 48 9.6 ugll 84-66-2 Diethyl phthalate ND 48 9.6 ugll 131-11-3 Dimethyi phthalate ND 48 7.7 ug11 117-81-7 bis(2-Ethylhexyl)phthalate ND 48 11 ugll 206-44-0 Fluoranthene ND 48 5.6 ugll 86-73-7 Fluorene 31.4 48 7.3 ugll 118-74-1 Hexachlorobenzene ND 48 6.6 ugll 87-68-3 Hexachlorohutadiene N❑ 48 9.2 ugll 77-47-4 Hexachlorocyclopentadiene N❑ 48 7.6 ugll 67-72-1 Hexachloroethane ND 48 7.1 ugll 193-39-5 lndeno(1,2.3-ed)pyrene ND 48 5.5 ug/l 78-59-1 Isophorone ND 48 6.1 ugil 90-12-0 1-Methy1naphthalene 130 48 6.8 ugll 91-57-6 2-Methylnaphthalene 155 48 6.6 uglt 91-20-3 Naphthalene 62.8 48 6.1 ugll 98-95-3 Nitrobenzene ND 48 6.9 ug11 621-64-7 N-Nitroso-di-n-propylamine ND 48 8.2 ug1l 86-30-6 N-Nitrosodiphenylamine ND 48 9.6 ugll 85-01-8 Phenanthrene 58.4 48 6.8 ugll 129-00-0 Pyrene 15.3 48 6.5 ugll 120-82-1 1,2,4-Trichiorobenzene ND 48 5.8 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenal 41% 14-67% 4165-62.2 Phenol-& 27% 10-50% 118-79-6 2,4,6-Tribromophenol 109% 33-118% 4165-60-0 Nitrobenzene-d5 108% 42-108% 321-60-8 2-Fluorobiphenyl 104% 40-I06% 1718-51-0 Terphenyl-d14 84% 39-I21% (a) Dilution required due to matrix interference. E Page 2 of 2 N❑ = Not detected MDL - Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank F = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound A in U ■ 36 of 119 ■.o.ccuT�sT FA4930 ••°"• °• �• Accutest LabLink@12:12 10-Jun-2013 Report of Analysis Client Sample ID: USTMW-2 Lab Sample ID: FA4930-5 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: MADEP VPH REV 1.1 Percent Solids: nla Project: URSNCM: S/S 1363, 1101 Hwy fit. Whitsett, NC Page 1 of I File ID DF Analyzed By Prep Date Prep Bate Analytical Batch Run #1 a UU003584.❑ 2 06/05/13 MM nla nla GUU179 Run #2 Purge Volume Run #1 501111 Run #2 MADEP VPH List CAS No. Compound Result 71.43-2 Benzene N❑ 100-41-4 Ethylbenxene ND 1634-04-4 Methyl Ted Butyl Ether N❑ 91-20-3 Naphthalene a 209 108-88-3 Toluene N❑ m,p-Xylene ND 95-47-6 o-Xylene N❑ C5- C8 Aliphatics (Unadj.) ND C9- C12 Aliphatics (Unadj.) 160 C9- CIO Aromatics (Unadj.) 612 C5- C8 Aliphatics ND C9- C12 Aliphatics 160 C9- C10 Aromatics 612 CAS No. Surrogate Recoveries Run# 1 460-00-4 BFB 124% 460-00.4 BFB 112% (a) No sample available for reanalysis. (b) Associated CCV recovery outside control limits. N❑ = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range RL MDL Units Q 2.0 2.0 ugll 4.0 2.0 ug11 4.0 2.0 ugll 10 6.0 ugll J 4.0 2.0 ugll 8.0 4.0 ugll 4.0 2.0 ugll 200 70 ugll 200 70 ugll J 200 70 ugll 200 70 ugll 200 70 ugll J 200 70 ugll Run# 2 Limits 70-130% 70-130% J = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound P. ■e 37 of 119 ACCU-FaBT. FA493fl ........._ Accutest Labl-ink@ 12:12 10-Jun-2013 Report of Analysis Client Sample ID: USTMW-2 Lab Sample ID: FA4930-5 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Hate Received: 05/23/13 Method: MADEP EPH REV 1.1 SW846 3510C Percent Solids: nla Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 NN004821.D 20 06/03/13 NMC 05/29/13 OP47077 GNN208 Run #2 Initial Volume Final Volume Run #1 1050 ml 2.0 ml Run #2 MAEPH List CAS No. Compound Result RL MDL Units Q 83-32-9 Acenaphthene ND 76 38 ugll 208-96-8 Acenaphthyfene ND 76 38 ugll 120-12-7 Anthracene Nil 76 38 ugll 56-55-3 Benw(a)anthracene ND 76 38 ug/l 50-32-8 Benxo(a)pyrene ND 76 38 ugll 205-99-2 Benxo(b)fluoranthene ND 76 38 ugll 191-24-2 Benxo(g.h,i)perylene ND 76 38 ugll 207.08.9 Benxo(k)fluoranthene ND 76 38 ugll 218-01.9 Chrysene ND 76 38 ug1l 53-70-3 Dibenxo(a,h)anthracene ND 76 38 ugll 206.44.0 Fluoranthene ND 76 38 ugll 86-73-7 Fluorene ND 76 38 ugll 193-39-5 Indeno(1.2,3-cd)pyrene ND 76 38 ugll 9I-57.6 2-Methyinaphihalene 52.1 76 38 ug11 J 91-20-3 Naphthalene ND 76 38 ugll 85-0I-8 Phenanthrene ND 76 38 ugll 129-00-0 Pyrene ND 76 38 ugll CII-C22 Aromatics (Unadj.) 3550 3800 2900 ugll J CII-C22 Aromatics 3500 3800 2900 ugll J C9-08 Allphadcs 22300 3800 I900 ugll C 19-C36 Aliphatics 7210 3800 1900 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane 0% a 40-140% 580-13-2 2-Bromonaphthalene 0%a 40-140% 84-15-1 o-Terphenyl 0% a 40-140% 321-60-8 2-Fluorobiphenyl 0% a 40-140% (a) Outside control limits due to dilution. ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyze found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■; 38 of 119 � ACCUTEST. FA4930 " . """'" Accutest LabLink@12:12 10-Jun-2013 Report of Analysis Client Sample ID: USTMW-4 Lab Sample ID: FA4930.6 Matrix: AQ - Ground Water Method: SM 6200B Project: URSNCM: SIS 1363, 1101 Hwy 61, Whilsett, NC File ID DF Analyzed By Prep Date Run #1 E024416.D 1 06/04/13 TD nla Run #2 Purge Volume Run #1 10.0 1111 Run #2 Page 1 of 1 Date Sampled: 05/22/13 Date Received: 05/23/13 Percent Solids: nla Prep Batch Analytical Batch nla VE835 VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene 5.4 0.50 0.10 ugll 75-27-4 Bromadichloromethane ND 0.50 0.10 ugll 107-06-2 1,2-Dichloroethane ND 0.50 0.10 ugll 108-20-3 Di -Isopropyl ether ND 0.50 0.10 ugll 124-48-1 Dibromochloremethane ND 0.50 0.10 ugll 156-59-2 cis- 1,2-Dichloreethylene ND 0.50 0.10 ugll 100-41-4 Ethylbenzene 2.3 0.50 0.10 ugll 99-87-6 p-Isopropyholuene ND 0.50 0.10 ug1l 74-87-3 Methyl chloride 0.45 0.50 0.11 ugll f 1634-04-4 Methyl Tert Butyl Ether 0.78 0.50 0.10 ugll 91-20-3 Naphthalene 21.3 0.50 0.15 ugll 108-88-3 Toluene 5.6 0.50 0.10 ugll 79-01-6 Trichlorcethylene ND 0.50 0.10 ugA 1330-20-7 Xylene {to(al) 9.1 1.5 0.22 ugll CAS No. Surrogate Recoveries Run# 1 Run# Z Limits 1868-53-7 Dibromofluoromethane 98% 70-130% 17060-07-0 1.2-Dichloroelhane-134 99% 70-130% 2037-26.5 Toluene-D8 101% 70-130% 460-00-4 4-Bromofluorobenzene 102% 70-130% N❑ = Not detected MDL - Method Detection Limit f = Indicates an estimated value RL = Reporting Limit B = Indicates analyze found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■i 39 of 119 0 AMMU-rEST. FA4930 .....,,a.,.. Accutest LahLink@12:12 10-Jun-2013 Report of Analysis Page 1 of 2 Client Sample ID: USTMW-4 Lab Sample ID: FA4930-6 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: EPA 625 EPA 625 Percent Solids: nla Project: UR5NCM: SIS 1363, 1101 Hwy 61, Whitsett, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a 1,063716.1) 4 05/29/13 NAF 05/24/13 OP47046 SL3223 Run #2 Initial Volume Final Volume Run #1 1040 ml 1.0 ml Run #2 ABN List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 65-85-0 Benzoic Acid 206 190 38 ugll 95-57-8 2-Chlorophenol N❑ 19 2.7 ugll 59-50-7 4-Chloro-3-methyl phenol ND 19 3A ugll 120-83-2 2.4-Dichlorophenol ND 19 2.7 ugll 105-67-9 2,4-Dimethylphenol 6.6 19 2.9 ugll 51-28-5 2,4-Dinitrophenol ND 96 20 ugll 534-52-1 4,6-Dinitro-o-cresol ND 38 5.5 ugll 95-48-7 2-Methylphenol ND 19 2.8 ugA 3&4-Methylphenol 27.5 19 5.3 ug1l 88-75-5 2-Nitrophenol ND 19 2.6 ugll 100-02-7 4-Nitrophenol ND 96 19 ugll 87-86-5 Pentachlorophenol ND 96 19 ugll 108-95-2 Phenol ND 19 2.1 uglt 88-06-2 2,4,6-Trichlorophenol N❑ 19 3.0 ugll 83-32-9 Acenaphthene ND 19 2.7 ugll 208-96-8 Acenaphthylene N❑ 19 2.7 ugll 120-12-7 Anthracene ND 19 2.9 ugll 56-55-3 Benxo(a)anthracene N❑ 19 2.1 ugll 50-32-8 Benxo(a)pyrene ND 19 2.2 ugA 205.99-2 Benxo(b)fluoranthene ND 19 2.9 ugll 191-24-2 Bepzo(g,h,i)perylene ND 19 2.6 ugll 207-08-9 Benno(k)fluoranthene ND 19 2.6 ugll 101-55-3 4-Brontvphenyl phenyl ether ND 19 3.0 ugll 85-68-7 Butyl benxyl phthalate ND 19 2.7 ugll 100-51-6 Benxyl Alcohol ND 19 3.8 ugll 91-58-7 2-Chloronaphlhalene N❑ 19 2.8 ugA 106-47-8 4-Chloroaniline ND 19 2.6 ugll 218-01-9 Chrysene ND 19 2.2 ug11 111-91-1 his(2-Chloroethoxy)methane N❑ 19 2.7 ugll 111-44-4 his(2-Chlorcelhyl)elher ND 19 2.8 ug/l 108-60-1 his (2-Chioroisopropyl)ether ND 19 3.0 ugll 7005-72-3 4-Chlorophenyl phenyl ether ND 19 3.3 ugll ND = Not detected MDL - Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = Indicates analyse found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■A 40 of 119 ACCLJTE8T. FA4930 .......n.,.. Accutest LabLink@12:12 10-jun-2013 Report of Analysis Client Sample ID: USTMW-4 Lab Sample ID: FA4930-6 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: EPA 625 EPA 625 Percent Solids: nla Project: URSNCM: 51S 1363, 1101 Hwy 61, Whitsett, NC ABN List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 95-50-1 1,2-Dichlorobenzene ND 19 2.6 ugll 122-66-7 1,2-Diphenylhydrazine ND 19 2.5 ug/l 541-73-1 1,3-Dichlorobenzene ND 19 3.o ug/I 106-46-7 1,4-Dichlorobenzene ND 19 2.7 ugll 91-94-1 3,3'-Dichlorobenzidine ND 19 2.8 ugll 53-70-3 Dibenzo(a.h)anthracene ND 19 2.2 ugll 132-64-9 Dibeazefuran ND 19 2.9 ug/1 84.74-2 Di-n-butyl phthalate ND 19 3.8 ugll 117-84-0 Di-n-octyl phthalate ND 19 3.8 ugll 84-66-2 Diethyl phthalate ND 19 18 ugll 131-11.3 Dimethyl phthalate N❑ 19 11 ugll 117-81-7 1bis(2-E1hylhexy1)phthalate 74.5 19 4.4 ugll 206-44-0 Fluoranthene ND 19 2.3 ugll 86-73-7 Fluorene ND 19 2.9 ug1l 118-74-1 Hexachlorohenzene ND 19 2.6 ugll 87-68-3 Hexachlorobutadiene ND 19 3.7 ugll 77-47-4 Hexachlorocyclopentadiene N❑ 19 3.0 ugll 67-72-1 Hexachloroethane ND 19 2.9 ug/l 193-39-5 Indeno(1,2,3-cd)pyrene N❑ 19 2.2 ugll 78-59-1 Isophorone ND 19 2.5 ugll 90-12-0 1-Methylnaphihalene 4.8 19 2.7 ugll 91-57-6 2-Methylnaphihalene ND 19 2.6 ugll 91-20-3 Naphthalene 18.3 19 2.4 ugll j 98-95-3 Nitrobenzene ND 19 2.8 ugA 621-64-7 N-Nitroso-di-n-propylamine ND 19 3.3 ugll 86-30-6 N-Nitrosodiphenylamine ND 19 3.8 ugll 85-01-8 Phenanthrene ND 19 2.7 ugll 129-00-0 Pyrene 3.2 19 2.6 ugll 120-82-1 1.2,4-Trichlorobenzene ND 19 2.3 ugll CAS No. Surrogate Recoveries Ruin# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 41% 14-67°% 4165-62-2 Phenol-d5 28% 10-50% 118-79-6 2,4,6-Tribromophenol 109% 33-118% 4165-60-0 Nitrobenzene-d5 107% 42-108% 321-60-8 2-Fluorobiphenyl 106% 40-106% 1718-51-0 Terphenyl-d14 80% 39-121% (a) Dilution required due to matrix interference. Page 2 of 2 ND = Not detected MDL - Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound A 0 �0 41 of 119 AGCUTES3T. FA4930 •,•e.,re.... Accutest LabLink@12:12 10-Jun-2013 Report of Analysis lient Sample ID: USTMW-4 ab Sample ID: FA4930-6 latrbL AQ - Ground Water lethod: MADEP VPH REV 1.1 roject: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC File ID DF Analyzed By Prep Date un #1 a UU003580.D 1 06/05/13 MM nla an #2 Purge Volume Run #1 5.0 ml Run #2 MADEP VPH List CAS No. Compound Result 71-43-2 Benzene 3.9 100-41-4 Ethylbenzene 1.7 1634.04-4 Methyl Tert Butyl Ether 1.2 91-20-3 Naphthalene a 20.3 108-88-3 Toluene 3.9 m,p-Xylene 3.7 95-47-6 o-Xylene 3.2 C5- C8 Aliphatics (Unadj.) ND C9- C12 Aliphatics (Unadj.) ND C9- CIO Aromatics (Unadj.) 49.7 C5- C8 Aliphatics N❑ C9- C12 Aliphatics N❑ C9- CIO Aromatics 49.7 CAS No. Surrogate Recoveries Ruff# 1 460-00-4 BFB 106% 460-00-4 BFB 103% (a) No sample available for reanalysis. (b) Associated CCV recovery outside control limits. ND = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range Page 1 of 1 Date Sampled: 05/22/13P. M Date Received: 05/23/13 Percent Solids: nla 9 Prep Batch Analytical Batch nla GUU179 RL MDL Units Q 1.0 1.0 ugll 2.0 1.0 ug11 J 2.0 1.0 ugll J 5.0 3.0 ug/1 J 2.0 1.0 ugll 4.0 2.0 ugll J 2.0 1.0 ugll 100 35 ugll 100 35 ugll 100 35 ugll ] 100 35 ugll 100 35 ugll 100 35 ugll J Run# 2 Limits 70-130% 70-130% ] = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound 6,40 42 of 119 N ACCU-rEST. FA4930 Accutest Labl.ink@ 12: i Z 10-jun-2013 Report of Analysis Client Sample ID: USTMW-4 Lab Sample ID: FA4930.6 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received. 05/23/13 Method: MADEP EPH REV 1. i SW846 3510C Percent Solids: nla Project: LIRSNCM: SIS 1363. 1101 Hwy 61, Whilsett, NC Page l of 1 File ID DF An*zcd By Prep Date Prep Batch Analytical Batch Run #1 NN004822.1) 5 06/03/13 NMC 05/29/13 OP47077 GNN208 Run #2 Initial Volume Final Volume Run # 1 1050 ml 2.0 ml Run #2 MAEPH List CAS No. Compound Result RL MDL Units Q 83-32-9 Acenaphthene ND 19 9.5 ugll 208-96-8 Acenaphthylene ND 19 9.5 ugll 120-12-7 Anthracene ND 19 9.5 ug/I 56-55-3 Senzo(a)anthracene ND 19 9.5 ugll 50-32-8 Benzo(a)pyrene ND 19 9.5 ugll 205-99-2 Benzo(b)fluoranthene ND 19 9.5 ugll 191-24-2 Benzo(g.h,i)perylene ND 19 9.5 ugll 207.08-9 Benzo(k)fluoranthene N❑ 19 9.5 ugll 218-01-9 Chrysene ND 19 9.5 ugll 53-70.3 Dibenzo(a,h)anthracene ND 19 9.5 ugll 206-44-0 Fluoranthene ND 19 9.5 ugll 86-73-7 Fluorene ND 19 9,5 ng1l 193-39-5 Indeno(1,2,3-cd)pyrene ND 19 9.5 ugll 91-57-6 2-Methyinaphthalene N❑ 19 9.5 ugll 91-20-3 Naphthalene ND 19 9.5 ugll 85-01-8 Phenanlhrene N❑ 19 9.5 ugll 129-00-0 Pyrene ND 19 9.5 ugll CI1-C22 Aromatics (Unadj.) 1060 950 710 ugll CII-C22 Aromatics 1060 950 710 ugll C9-C18 Aliphatics 4590 950 480 ugll C 19-C36 Aliphatics 1940 950 480 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane 58% 40-140% 580-13-2 2-Bromonaphthalene 61% 40-140% 84-15.1 o-Terphenyl 50°% 40-140'% 321-60-8 2-Ffuorobiphenyl 69°% 40-140% ND = Nol detected MDL - Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound A Mlle 43 of 119 ACC IJTEST. Accutest LabLink@12:12 10-Jun-2013 Report of Analysis :lient Sample ID: AGM-RW gab Sample ID: FA4930-7 Date Sampled: 05/22/13 4atsix: AQ - Ground Water Date Received: 05/23/13 lethod: SM 6200B Percent Solids: n/a 'roject: URSNCM: SIS 1363, 1101 Hwy 61. Whitsett. NC Page 1 of I File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E024417.D 1 06/04/13 TD nla nla VE835 Run #2 E024437.D 5 06/05/13 TD nla nla VE836 Purge Volume Run #1 10.0 ml Run #2 10.0 ml VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene 4.0 0.50 0.10 ugll 75-27-4 Bromodichloromethane ND 0.50 0.10 ugll 107.06-2 1,2-Dichloroethane N❑ 0.50 0.10 ugll 108-20-3 Di -Isopropyl ether N❑ 0.50 0.10 ugll 124-48-1 Dihromochloromethane N❑ 0.50 0.10 ugll 156-59-2 cis-1,2-Dichloroethylene 0.11 0.50 0.10 ugll J 100-41-4 Ethylbenzene 0.32 0.50 0.10 ugll J 99-87-6 p-Isopropyholuene N❑ 0.50 0.10 ugll 74-87-3 Methyl chloride 1.1 0.50 0.11 ugll 1634-04-4 Methyl Tert Butyl Ether 0.30 0.50 0.10 ugll J 91-20-3 Naphthalene 190 a 2.5 0.74 ugll 108-88-3 Toluene 0.30 0.50 0.10 ugll j 79-01-6 Trichloroethylene N❑ 0.50 0.10 ugll 1330-20-7 Xylene (total) N❑ 1.5 0.22 ugA CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 100% 100% 70-130% 17060-07-0 1,2-Dichloroethane-D4 100% 100% 70-130% 2037-26-5 Toluene-D8 100% 101% 70-130% 460-00-4 4-Bromofluorobenzene 102% 104% 70-130% (a) Result is from Run# 2 ND = Not detected MDL - Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound A ►1 a ■R 44 of 119 E.4CCUTEET. FA4930 ""P"••�"•• Acculest LabLink@12:12 10-Jun-2013 Report of Analysis Page 1 of 2 Client Sample ID: AGM-RW Lab Sample ID: FA4930-7 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: EPA 625 EPA 625 Percent Solids: nla Project: URSNCM. S/S 1363. 1101 Hwy 61, Whitsetl, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a L063717.1) 10 05/29/13 NAF 05/24/13 OP47046 SL3223 Run #2 Initial Volume Final Volume Run #1 1040 ml 1.0 ml Run #2 ABN List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 65-85.0 Benzoic Acid ND 480 96 ugll 95-57-8 2-Chlorophenol ND 48 6.8 ugll 59-50.7 4-Chloro-3-methyl phenol ND 48 7.8 ugll 120-83-2 2,4-Dichlorophenol ND 48 6.7 ugll 105-67-9 2,4-Dimethylphenol ND 48 7.4 ugll 51-28-5 2,4-Dinitrophenol ND 240 50 ugll 534-52-1 4,6-Dinitro-o-cresol N❑ 96 14 ugll 95-48-7 2-Melhylphenol ND 48 6.9 ugll 3&4-Meth_ylphenol N❑ 48 13 ugll 88-75-5 2-Nitrophenol ND 48 6.5 ug/l 100-02.7 4-Nitrophenol ND 240 48 ugll 87-86-5 Pentachlorophenol ND 240 48 ugll 108-95.2 Phenol N❑ 48 5.3 ugll 88-06-2 2,4,6-Trichloraphenol ND 48 7.5 ugll 83.32.9 Acenaphthene 15.0 48 6.7 ugl] 208-96-8 Acenaphthylene ND 48 6.7 ugll 120-12-7 Anlhracene ND 48 7.2 ugll 56-55-3 Benzo(a)anlhracene N❑ 48 5.2 ugll 50-32-8 Benzo(a)pyrene ND 48 5.5 ug1l 205.99-2 Benzo(b)fluoranthene N❑ 48 7.3 ugll 191-24-2 Benza(g,hJ)perylene ND 48 6.4 ugll 207-08-9 Benzo(k)fluoranthene N❑ 48 6.4 ugll 101.55.3 4-Bromophenyl phenyl ether N❑ 48 7.6 ugll 85-68.7 Butyl benzyl phthalate ND 48 6.8 ugll 100-51-6 Benzyl Alcohol N❑ 48 9.6 ugll 91-58.7 2-Chloronaphihalene N❑ 48 7.0 ugll 106-47-8 4-Chlaroaniline ND 48 6.6 ugll 218.01.9 Chrysene N❑ 48 5.6 ugll 11I-91-1 his (2-Chloroe(hoxy)methane ND 48 6.7 ugll 111.44.4 his(2-Chloroethyl)ether N❑ 48 6.9 ugll 108-60-1 bis(2-Chloroisopropyl)ether N❑ 48 7.6 ug11 7005-72-3 4-Chlorophenyl phenyl ether N❑ 48 8.4 ugll J ND = Not detecled MDL - Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyze found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound A V 0 ■ 45 of 119 FA4930 Accutest LabLink@12.12 10-Jun-2013 Report of Analysis Client Sample ID: AGM-RW Lab Sample ID: FA4930-7 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: EPA 625 EPA 625 Percent Solids: nla Project: URSNCM: S/S 1363. 1101 Hwy 61, Whitsett, NC ABN List for NC, May 2012 CAS No. Compound Remit RL MDL Units Q 95-50-1 1,2-Dichloroberzene ND 48 6.5 ug/I 122-66-7 1.2-Diphenylhydrazine ND 48 6.2 ugll 541-73-1 1,3-Dichlorobenzene ND 48 7.5 ugll 106-46-7 1,4-Dichlorobenzene ND 48 6.7 ugA 91-94-1 3,3'-Dichlorobenzidine N❑ 48 7.1 ugll 53-70-3 Dibenzo(a,h)anthracene ND 48 5.6 ug/l 132-64-9 Dibenzofuran ND 48 7.2 ugll 84-74-2 Di-n-butyl phthalate N❑ 48 9.6 ugll 117-84-0 Di-n-octyl phthalate ND 48 9.6 ugll 84-66-2 Diethyl phthalate N❑ 48 9.6 ugll 131-11-3 Dimethyl phthalate ND 48 7.7 ugli 117-81-7 his(2-Ethylhexyl)phthalate N❑ 48 it ugll 206-44-0 Fluoranthene N❑ 48 5.6 ugll 86-73-7 Fluorene 27.9 48 7.3 ugll J 118-74-1 Hexachlorobenzene N❑ 48 6.6 ugll 87-68-3 Hexachlorobutadiene ND 48 9.2 ugll 77-47-4 Hexachlorocyclopentadiene N❑ 48 7.6 ugll 67-72-1 Hexachloroethane ND 48 7.1 ugll 193-39-5 Irrdeno(1,2,3-cd)pyrene ND 48 5.5 ugll 78-59-1 Isophorone ND 48 6A ugll 90-12-0 1-Mezhylnaphthaiene 160 48 6.8 ugll 91-57-6 2-Methylnaphthalene 190 48 6.6 ug/l 91-20-3 Naphthalene 149 48 6.1 ugll 98-95-3 Nitrobenzene ND 48 6.9 ugA 621.64-7 N-Nitroso-di-n-propylamine ND 48 8.2 ugll 86-30-6 N-Nitrosodiphenylamine ND 48 9.6 ug11 85-01-8 Phenanthrene 38.9 48 6.8 ugll J 129.00-0 Pyrene 11.2 48 6.5 ugll J 120-82-1 1,2,4-Trichlorobenzene ND 48 5.8 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 40% 14-67% 4165-62-2 Phenol-d5 25°% 10-50°% 118-79-6 2,4,6-Tribromophenol 103% 33-118% 4165-60-0 Nitrobenzene-d5 102% 42-108% 321-60-8 2-Fluorobiphenyl 98% 40-106% 1718-51-0 Terphenyl-d14 65% 39.121% (a) Dilution required due to matrix interference. Page 2 of 2 ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyze found in associated method blank E = Indicates value exceeds calibration range N W Indicates presumptive evidence of a compound A V a SO 46 of 119 a ACCLJTEST. Accutest Labl-ink912:12 10-Jun-2013 Report of Analysis Client Sample ID: AGM-RW Lab Sample 113: FA4930-7 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: MADEP VPH REV 1.1 Percent Solids: nla Project: URSNCM: S/S 1363, 1101 Hwy 61, Wbitsett, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 00003581.D 1 06/05/13 Mm nla nla CUU179 Run #2 a UU003626.❑ 10 06/06/13 MM nla nla GUU181 Purge Volume Run #1 :i.0 rnI Run #2 5.0 in] MADEP VP11 List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene 3.0 1.0 1.0 ugll 100-41-4 Ethyibenzene ND 2.0 1.0 ugll 1634-04-4 Methyl Ter( Butyl Ether ND 2.o 1.0 ugll 91-20-3 Naphthalene 284 n 50 30 ugll 108-88-3 Toluene ND 2.0 1.0 ugll m,p-Xylene ND 4.0 2.0 ugll 95-47-6 o-Xylene ND 2.0 1.0 ugll C5- C8 Aliphatics (Unadj.) 92.4 100 35 ugll J C9- C12 Aliphatics (Unadj.) 439 a 1000 350 ugll J C9- C10 Aromatics (Unadj.) 1250 h 1000 350 ugll C5- C8 Aliphatics 88.7 100 35 ugll J C9- C12 Aliphatics 439 5 1000 350 ugll J C9- CIO Aromatics 1250 a 1000 350 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 150% r 122% 70-130% 460-00-4 BFB 116% 105% 70-130% (a) Sample re -analyzed beyond hold time; reported results are considered minimum values. (b) Result is from Run# 2 (c) Outside control limits due to matrix interference. ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumplive evidence of a compound V 0 �R 47 of 119 ACCiJT�ST. FA4230 ...... °, •• Accutesl LabLink@12:12 10-Jun-2013 Report of Analysis Client Sample ID: AGM-RW Lab Sample ID: FA4930-7 Matrix: AQ - Ground Water Method: MADEP EPH REV 1.1 SW846 3510C Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitseu. NC File ID DF Analyzed By Prep Date Run #1 NN004856.1) 5 06/04/13 NMC 05/29/13 Run #2 Initial Volume Final Volume Run #1 1040 ml 2.0 ml Run #2 Page 1 of 1 P. Date Sampled: 05/22/13 4 Date Received: 05/23/13 Percent Solids: nla M Prep Batch Analytical Batch OP47077 GNN209 MAEPH List CAS No. Compound Result RL MDL Units Q 83-32-9 Acenaphthene ND 19 9.6 ugll 208-96-8 Acenaphthylene ND 19 9.6 ugll 120-12-7 Anthracene ND 19 9.6 ugll 56-55-3 Benxa(a)anthracene ND 19 9.6 ugll 50-32-8 Benxa(a)pyrene ND 19 9.6 ug11 205-99-2 Benxo(b)fluoranthene ND 19 9.6 ugll 191-24-2 Benzo(g,h,i)perylene ND 19 9.6 ugll 207-08-9 Benxo(k)fluoranthene ND 19 9.6 ugll 218-01-9 Chrysene ND I9 9.6 ugA 53-70-3 ❑ibenxo(a,h)anlhracene ND 19 9.6 ugA 206-44-0 Fluoranthene ND 19 9.6 ugll 86-73-7 Fluorene ND 19 9.6 ugll 193.39-5 Indeno(1,Z,3-cd)pyrene ND 19 9.6 ugll 91-57-6 2-Methylnaphthalene 44.1 19 9.6 ugll 91-20-3 Naphthalene 35.1 19 9.6 ug11 85-01-8 Phenanlhrene N❑ 19 9.6 ugll 129-00.0 Pyrene N❑ 19 9.6 ugll CII -CZZ Aromatics (Llnadj.) 1350 960 720 ugA CI I-C22 Aromatics 1270 960 720 ugll C9-C 18 Aliphatics 5810 960 480 ugll C19-06 Aliphatics 1920 960 480 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane 60% 40.140% 580-13-2 2-Bromonaphthalene 59% 40-140% 84-15-1 o-Terphenyl 47% 40-140% 3ZI-60-8 2-Fluorobiphenyl 62% 40-140% ND = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range J = Indicates an estimated value B = Indicates analyze found in associated method blank N = Indicates presumptive evidence of a compound ■b 48 of 119 E ACC LITEST. Accutest LabLink@ 12:1 Z 10-jun-2013 Report of Analysis Client Sample ID: CSAMW-1 Lab Sample ID: FA4930-8 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: SM 6200B Percent Solids: nla Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC Page 1 of 1 File ID DF Analyud By Prep Date Prep Batch Analytical Batch Run #1 E024433.1) 1 06/05/13 TD nla nla VE836 Run #2 Purge Volume Run #1 10.0 Ili] Run #2 VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.10 ugll 75-27-4 Bromodichloromethane ND 0.50 0.10 ugll 107-06-2 1,2-Dichloroethane ND 0.50 0.10 ugll 108-20-3 ❑i-Isopropyl ether ND 0.50 0.10 ugll 124-48-1 Dibromochloromethane ND 0.50 0.10 ugll 156-59-2 cis- 1,2-Dichloroethylene ND 0.50 0.10 ugll 100-41-4 Ethylbenzene ND 0.50 0.10 ug1l 99-87-6 p-Isopropyltoluene ND 0.50 0.10 ugll 74-87-3 Methyl chloride ND 0.50 0.11 ugll 1634-04-4 Methyl Tert Butyl Ether 0.48 0.50 0.10 ugll J 91-ZO-3 Naphthalene N❑ 0.50 0.15 ugll 108-88-3 Toluene Nil 0.50 0.10 ugll 79-01-6 Trichloroethylene ND 0.50 0.10 ugll 1330-20-7 Xylene (total) ND 1.5 0,22 ugll CAS No. Surrogate Reonvexies Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 98% 70-130% 17060-07-0 1,2-Dichloroethane-D4 99% 70-130% 2037-26-5 Toluene-D8 101% 70-130% 460-00-4 4-Bromofluorobenzene 103% 70-130% ND = Not detected MDL - Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = Indicates analyze found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound P. oo 0 on 49 of 119 AGGUTE��: FA4930 ••""• • •• Accutest LabLink@12:12 10-Jun-2013 Report of Analysis Page 1 of 2 Client Sample lD: CSAMW-1 Lab Sample ID: FA4930-8 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: EPA 625 EPA 625 Percent Solids: nla Project: URSNCM: S/S 1363, 1101 Hwy 61, Whitsett, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Bate Run #1 L063718.D 1 05/29/13 NAF 05/24/13 OP47046 SL3223 Run #2 Initial Volume Final Volume Run #1 1040 ml 1.0 ml Run #2 ABN List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 48 9.6 ugll 95-57-8 2-Chlorophenol ND 4.8 0.68 ugll 59-50-7 4-Chloro-3-methyl phenol ND 4.8 0.78 ugll 120-83-2 2,4-Dichlorophenol ND 4.8 0.67 ugll 105-67-9 2,4-Dimethylphenol ND 4.8 0.74 ugll 51-28-5 2,4-Dinitrophenol N❑ 24 5.0 ugll 534-52-1 4,6-Dinitro-o-cresol ND 9.6 1.4 ugll 95-48-7 2-Methylphenol ND 4.8 0.69 ugll 3&4-Methylphenol ND 4.8 1.3 ugll 88-75-5 2-Nitrophenol ND 4.8 0.65 ugll 100-02-7 4-Nitrophenol ND 24 4.8 ugll 87-86-5 Pentachlorophenol ND 24 4.8 ugll 108-95-2 Phenol a ND 4.8 0.53 ug/I 88-06-2 2,4,6-Trichlorophenol N❑ 4.8 0.75 ugll 83-32-9 Acenaphthene ND 4.8 0.67 ugll 208-96-8 Acenaphthylene ND 4.8 0.67 ugll 120-12-7 Anthracene N❑ 4.8 0.72 ugli 56-55-3 Benzo(a)anthracene ND 4.8 0.52 ugll 50-32-8 Benzo(a)pyrene ND C8 0.55 ugll 205-99-2 Benzo(b)fluoranthene ND 4.8 0.73 ugll 191-24-2 Benzo(g,h,i)perylene ND 4.8 0.64 ugll 207-08-9 Benzo(k)flu oranthene ND 4.8 0.64 ugll 101-55-3 4-Bromophenyl phenyl ether ND 4.8 0.76 ugll 85-68-7 Butyl benzyl phthalate ND 4.8 0.68 ug1I 100-51-6 Benzyl Alcohol ND 4.8 0.96 ugll 91-58-7 2-Chloronaphthalene N❑ 4.8 0.70 ugll 106.47-8 4-Chloroaniline ND 4.8 0.66 ugll 218-01-9 Chrysene ND 4.8 0.56 ugll 111.91-1 his (2-Chloroe(hoxy)methane N❑ 4.8 0.67 ugll 111-44-4 bis(2-Chloroethyl)ether N❑ 4.8 0.69 ugA 108.60-1 bis(2-Chloroisopropyl)ether ND 4.8 0.76 ugll 7005-72-3 4-Chiorophenylphenyl ether ND 4.8 0.84 ugA ND = Not detected MDL - Method Detection Limit .) = Indicates an estimated value RL = Reporting Limit B = indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound A co a ■o SO of 119 w ACCu-rEST. FA4930 Accutest LabLink912:12 10-jun-2013 Report of Analysis Client Sample ID: CSAMW-1 Lab Sample 1D: FA4930-8 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: EPA 625 EPA 625 Percent Solids: nla Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC. ABN List for NC, May 2012 Paw 2of2 CAS No. Compound Result RL MDL Units Q 95-50-1 1,2-Dichlorobenzene N❑ C8 0.65 ug11 122-66-7 1,2-Dipheny1hydrazine ND 4.8 0.62 ugll 541-73-1 1,3-Dichlorobenzene ND 4.8 0.75 ugll 106-46.7 1,4-Dichlorobenzene N❑ 4.8 0.67 ugll 91-94-1 3,3'-Dichlorobenxidine ND 4.8 0.71 ug1l 53-70-3 Dibenzo(a,h)anthracene N❑ 4.8 0.56 ugll 132-64-9 Dibenzofuran ND 4.8 0.72 ug11 84.74-2 Di-n-butyl phthalate ND 4.8 0.96 ug11 117-84-0 Di-n-actyl phthalate ND 4.8 0.96 ugll 84-66-2 Diethyl phthalate N❑ 4.8 0.96 ugll 131-11-3 Dimethyl phthalate ND 4.8 0.77 ugll 117-81-7 bis(2-E1hylhexyl)phthalate N❑ C8 1.1 ugll 206-44-0 Fluoranthene N❑ 4.8 0.56 ugll 86-73-7 Fluorene ND 4.8 0.73 ugll 118-74-1 Hexachlorobenzene ND 4.8 0.66 ug1l 87-68-3 Hexachlorobutadiene ND 4.8 0.92 uglf 77-47-4 Hexachlorocyclopentadiene ND 4.8 0.76 ugll 67-72-1 Hexachloroethane ND CH 0.71 ug11 193-39-5 Indeno(1,2,3-cd)pyrene N❑ 4.8 0.55 ug11 78-59-1 Isophorone ND 4.8 0.61 ugll 90-12-0 I-Methylnaphthalene N❑ 4.8 0.68 ugA 91-57-6 2-Methylnaphthalene N❑ 4.8 0.66 ugll 91-20-3 Naphthalene ND 4.8 0.61 ugll 98-95-3 Nitrobenzene ND 4.8 0.69 ugll 621-64-7 N-Nitroso-di-n-propylamine ND 4.8 0.82 ug1l 86-30-6 N-Nitrosodiphenylamine ND 4.8 0.96 ugll 85-01-8 Phenanthrene ND 4.8 0.68 ug1l 129-00-0 Pyrene ND 4.8 0.65 ugll 120-82.1 1,2,4-Trichlorobenzene ND 4.8 0.58 ugll CAS No. Surrogate Recoveries Run# i Run# 2 Limits 367-12-4 2-Fluorophenol 32% 14-67% 4165-62-2 Phenol-d5 23% 10-50% 118-79-6 2,4,6-Tribromophenol 88% 33-118% 4165-60-0 Nitrobenzene-d5 72% 42-108% 321-60-8 2-Fluorobiphenyl 75% 40-106% 1718-51-0 Terphenyl-d14 67% 39-121% (a) Compound outside limits in associated MSIMSD. ND = Not detected MDL - Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = indicates value exceeds calibration range N = indicates presumptive evidence of a compound MR 51 of 119 0 .accu--E=-sT FA4930 ••O••re.... Accutest LabLink@12:12 10-Jun-2013 Report of Analysis Client Sample ID: CSAMW-1 Lab Sample ID: FA4930-8 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: MADEP VPH REV 1.1 Percent Solids: nla Project: URSNCM: S/S 1363, 1101 Hwy 61, Whitsett. NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 UU003547.D 1 06/04/13 MM nla nla GUU178 Run #2 Purge Volume Run #1 5.0 ml Run #2 MADEP VPH List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 1.0 1.0 ugll 100-41-4 Ethylbenzene ND 2.0 1.0 ugll 1634-04-4 Methyl Teri Butyl Ether ND 2.0 1.0 ugll 91-20-3 Naphthalene ND 5.0 3.0 ug11 108-88-3 Toluene ND 2.0 1.0 ugll m,p-Xylene ND 4.0 2.0 ugll 95-47-6 o-Xylene ND 2.0 1.0 ugll C5- C8 Aliphatics (Unadj.) ND 100 35 ugl] C9- C12 Aliphatics (Unadj.) ND 100 35 ugll C9- C10 Aromatics (Unadj.) ND 100 35 ugll C5- C8 Aliphatics ND 100 35 ugll C9- C 12 Aliphatics ND 100 35 ugll C9- C10 Aromatics ND 100 35 ug11 CAS No. Surrogate Recoveries Run# 1 Run# Z Limits 460-00.4 BFB 85% 70-130% 460-00-4 BFB 85% 70-130% ND = Not detected MDL - Method Detection Limit RL = Reporting limit E = Indicates value exceeds calibration range A oo 0 J = Indicates an estimated value B = Indicates analyze found in associated method blank N = Indicates presumptive evidence of a compound ■:' : 52 of 119 w.4CCL1TE8T. FA4910 Accutest LabLink@ 12:12 10-Jun-2013 Report of Analysis it Sample ID: CSAMW-1 Sample ID: FA4930-8 rix: AQ - Ground Water iod: MADEP EPH REV 1.1 SW846 3510C ect: URSNCM: S/S 1363, 1101 Hwy 61. Whitsett, NC File ID DF Analyzed By Prep Date #1 NN004802.13 1 05/31 /13 NMC 05/29/13 #2 Initial Volume Final Volume un #1 10501111 2.0 ml ,uu #2 Page I of 1 Date Sampled: 05/22/13P. CO Date Received: 05/23/13 Percent Solids: nla a Prep Batch Analytical Batch OP47077 GNN207 MAEPH List CAS No. Compound Result RL MDL [snits Q 83-32-9 Acenaphthene ND 3.8 1.9 ugll 208-96-8 Acenaphthylene ND 3.8 1.9 ugll 120-12-7 Anthracene ND 3.8 1.9 ug/1 56-55-3 Benxa(a)anthracene ND 3.8 1.9 ugll 50-32-8 Benxo(a)pyrene ND 3.8 1.9 ug1l 205-99-2 Benxo(b)fluoranthene ND 3.8 1.9 ug/1 191-24-2 Benxo(g,h,i)perylene ND 3.8 1.9 ug/1 207-08-9 Benxo(k)fluoranthene ND 3.8 1.9 ug/1 218-01-9 Chrysene ND 3.8 1.9 ugll 53-70-3 Dibenzo(a,h)anthracene ND 3.8 1.9 ugll 206-44-0 Fluoranthene ND 3.8 1.9 ugll 86-73-7 Fluorene ND 3.8 1.9 ug/1 193-39-5 Indeno(1,2,3-cd)pyrene ND 3.8 1.9 ugll 91-57-6 2-Methylnaphthalene ND 3.8 1.9 ugll 91-20-3 Naphthalene ND 3.8 1.9 ugll 85-01-8 Phenanthrene ND 3.8 1.9 ugll 129-00-0 Pyrene ND 3.8 1.9 ug/1 C11-4222 Aromatics (Unadj.) 244 190 140 ug11 C11-C22 Aromatics 244 190 140 ug1l C9-08 Aliphatics ND 190 95 ug/1 C19-C36 Aliphatics ND 190 95 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chloroociadecane 71% 40-140% 580-13-2 2-Bromonaphthalene 81% 40-140% 84-15-1 o-Terphenyl 61% 40-140% 321-60-8 2-Fluorobiphenyl 80% 40-140% ND = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range I = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound s■ 53 of 119 ACCLJTEST. FA4430 .,.A...o,.. Accutest LahLinkiPI2:12 10-Jun-2013 Report of Analysis at Sample ID: CSAMW-2 Sample ID: FA4930.9 rix: AQ - Ground Water hod: SM 6200B ect: URSNCM: S/S 1363, 1101 Hwy 61, Whitsett, NC File ID DF Analyzed By Prep Date #1 a E024431-D 1 06/05/13 TD nla #2 Purge Volume Run #1 10.0 ml Run #2 Page 1 of 1 P. Date Sampled: 05/22/13 Date Received: 05/23/13 Percent Solids: nla Prep Batch Analytical Batch nla VE836 VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.10 ugll 75-27-4 Bromodichloromethane ND 0.50 0.10 ugll 107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug11 108-20-3 Di -Isopropyl ether ND 0.50 0.10 ug11 124-48-1 Dihromochloromethane ND 0.50 0.10 ugll 156-59-2 cis-L2-Dichloroethyiene ND 0.50 0.10 ugll 100-41-4 Ethylbenzene ND 0.50 0.10 ugll 99-87-6 p-Isopropylioluene ND 0.50 0.10 ugll 74-87-3 Methyl chloride 0.14 0.50 0.11 ugll j 1634-04-4 Methyl Teri Butyl Ether 4.8 0.50 0.10 ugli 91-20-3 Naphthalene ND 0.50 0.15 ugll 108-88-3 Toluene N❑ 0.50 0.10 ugll 79-01-6 Trichloroethylene ND 0.50 0.10 ugll 1330-20-7 Xylene {to(al} N❑ 1.5 0.22 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluorumethane 100% 70-130% 17060-07-0 1.2-Dichloroethane-D4 101% 70-130% 2037-26-5 Toluene-D8 100% 70-130% 460-00-4 4-Bromofluorobenzene 104% 70-130% (a) Sample was not preserved to a pH < 2, reported results are considered minimum values. N❑ = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range J = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound ■ " 54 of 119 O ACCLJTEST FA4930 Accutest LabLink@12:12 10-Jun-2013 Report of Analysis Page 1 of 2 Client Sample ID: CSAMW-2 Lab Sample ID: FA4930-9 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: EPA 625 EPA 625 Percent Solids: nla Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 L063721.1) 1 05/29/13 NAF 05/24/13 OP47046 SL3223 Run #2 Initial Volume Final Volume Run #1 1040 ml 1.0 ml Run #2 ABN List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 48 9.6 ugll 95.57-8 2-Chiorophenol ND 4.8 0.68 ugll 59-50-7 4-Chloro-3-methyl phenol ND 4.8 0.78 ugll 120.83-2 2,4-Dichlorophenol ND 4.8 0.67 ugll 105-67-9 2,4-Dimeth_ylphenoI N❑ 4.8 0.74 ugll 51-28-5 2,4-Dinitrophenol N❑ 24 5.0 ugll 534-52-1 4,6-Dinitro-o-cresol N❑ 9.6 1.4 ugll 95-48-7 2-Methylphenol ND 4.8 0.69 ugA 3&4-Me1hylphenoi ND 4.8 1.3 ugA 88-75-5 2-Nitrophenol ND 4.8 0.65 ugll 100-02-7 4-Nitrophenol ND 24 4.8 ugll 87-86-5 Pentachlorophenol N❑ 24 4.8 ugA 108-95-2 Phenol ND 4.8 0.53 ugll 88-06-2 2,4,6-Trichlorophenol ND 4.8 0.75 ugll 83-32-9 Acenaphthene N❑ 4.8 0.67 ugll 208-96-8 Acenaphthylene N❑ 4.8 0.67 ug/l 120-12-7 Anthracene N❑ 4.8 0.72 ugll 56-55-3 Benzo(a)anthracene N❑ 4.8 0.52 ugll 50-32-8 Benzo(a)pyrene ND 4.8 0.55 ugll 205.99-2 Benzo(b)fluoranthene ND 4.8 0.73 ugll 191-24-2 Benzo(g,h,i)perylene N❑ 4.8 0.64 ugll 207-08-9 Benzo(k)fluaranthene ND 4.8 0.64 ugll 101.55-3 4-Bromophenyl phenyl ether ND 4.8 0.76 ugll 85-68-7 Butyl benzyl phthalate ND 4.8 0.68 ugA 100-51-6 Benzyl Alcohol N❑ 4.8 0.96 ugll 91.58-7 2-Chloronaphthalene N❑ 4.8 0.70 ugll 106-47-8 4-Chloroaniline ND 4.8 0.66 ugA 218-01-9 Chrysene N❑ 4.8 0.56 ugA 111-91-1 bis(2-Chloroethoxy)methane ND 4.8 0.67 ugll 111-44-4 his(2-Chlnroe1hyl)ether ND 4.8 0.69 ugll 108-60-1 his(2-Chloroisopropyl)ether N❑ 4.8 0.76 ugA 7005-72-3 4-Chlorophenol phenyl ether N❑ 4.8 0.84 ugll ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound �■ 55 of 119 .8.ccurt�s-t: FA4%" `... ", �• Accutest LahLink@12:12 10-Jun-2013 Report Of Analysis Client Sample ID: CSAMW-2 Lab Sample ID: FA4930-9 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: EPA 625 EPA 625 Percent Solids: nla Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC ABN List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 95-50-1 1,2-Dichlorobenzene ND 4.8 0.65 ugli 122-66-7 1,2-Diphenylhydrazine ND 4.8 0.62 ugll 541-73-1 1,3-Dichlorobenzene ND 4A 0.75 ugli 106-46-7 1,4-Dichlorobenzene ND 4.8 0.67 ugll 91-94-1 3,3'-Dichlorobenzidine ND 4.8 0.71 ugfl 53-70-3 Dibenzo(a,h)anthracene ND 4.8 0.56 ugll 132-64-9 ❑ibenzofuran ND 4.8 0.72 ugll 84-74-2 Di-n-butyl phthalate N❑ C8 0.96 ugll 117-84-0 Di-n-octyl phthalate ND 4.8 0.96 ugll 84-66-2 Diethyl phthalate N❑ 4.8 0.96 ugll 131-11-3 Dimethyl phthalate ND 4.8 0.77 ugll 117-81-7 bis(2- Ethyl hexyl)phthaIate ND 4.8 1.1 ugll 206-44-0 Fluaranthene N❑ 4.8 0.56 ugll 86-73-7 Fluorene ND 4.8 0.73 ugll 118-74-1 Hexachlorobenzene ND 4.8 0.66 ugA 87-68-3 Hexachlorobutadiene ND CH 0.92 ugll 77-47-4 Hexachlorocyclopentadiene ND C8 0.76 ugll 67-72-1 Hexachloroethane N❑ 4.8 0.71 ugll 193-39-5 Indeno(1,2,3-cd)pyrene ND 4.8 0.55 ugll 78-59-1 Isophorone ND 4.8 0.61 ug1l 90-12-0 1-Methylnaphthalene N❑ 4.8 0.68 ugll 91-57-6 2-Methylnaphthalene N❑ 4.8 0.66 ugll 91-20-3 Naphthalene ND 4.8 0.61 ugll 98-95-3 Nitrobenzene ND 4.8 0.69 ugll 621-64-7 N-Nitmso-di-n-propylamine N❑ 4.8 0.82 ugll 86-30-6 N-Nitrosodiphenylamine ND 4.8 0.96 ugll 85-01-8 Phenanthrene N❑ 4.8 0.68 ugll 129-00-0 Pyrene ND 4.8 0.65 ugll 120-82-1 1,2,4-Trichlorobenzene ND 4.8 0.58 ugll CAS No. Surrogate Recoveries Run# i Run# 2 Limits 367-12-4 2-Fluorophenol 40% 14-67% 4165-62-2 Phenol-d5 28% 10-50% 118-79-6 2,4,6-Tribromophenol 93% 33-118% 4165-60-0 Nitrobenzene-d5 85% 42-108% 321-60-8 2-Fluorabiphenyl 86% 40-106% 1718-51-0 Terphenyl-d14 56% 39-121% Page 2 of 2 ND = Not detected MDL - Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = Indicates analyze found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound A ea ■• 56 of 119 w ACC:;I ITaE3T. FA4930 `..... tl•••• Accutest LabLink912:12 10-jun-2013 Report of Analysis Client Sample ID: CSAMW-2 Lab Sample ID: FA4930-9 Matrix: AQ - Ground Water Method: MADEP VPH REV 1.1 Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC File ID DF Analyzed By Prep Date Run #1 UU003550.D 1 06/04/13 MM nla Run #2 Purge Volume Run #1 5.0 rill Run #2 MADEP VPH List CAS No. Compound Result 71-43-2 Benzene ND 100-41-4 Ethylbenzene ND 1634-04-4 Methyl Ter( Butyl Ether 5.3 91-20-3 Naphthalene ND 108-88-3 Toluene ND m,p-Xylene N❑ 95-47-6 o-Xylene ND C5- C8 Aliphatics (Unadj.) ND C9- C12 Aliphatics (Unadj.) ND C9- C10 Aromatics (Unadj.) ND C5- C8 Aliphatics ND C9- C12 Aliphatics ND C9- C10 Aromatics ND CAS No. Surrogate Recoveries Run# 1 460-00-4 BFB 87% 460-00-4 BFB 88% ND Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range Page 1 of 1 Date Sampled: 05/22/13P. Date Received: 05/23/13 Percent Solids: nla Prep Batch Analytical Batch n/a GUU178 RL MDL Units Q 1.0 1.0 ugh 2.0 1.0 ugll 2.0 1.0 ugll 5.0 3.0 ugll 2.0 1.0 ugll 4.0 2.0 ugll 2.0 1.0 ugll 100 35 ugll too 35 ugh 100 35 ugll 100 35 ugll too 35 ugll 100 35 ugll Run# 2 Limits 70-130% 70-130% ] = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound ■■ 57 of 119 ^CCU—rEST FA4930 ...n...,... Accutest LabLink@12:12 10-jun-2013 Report of Analysis Client Sample ID: CSAMW-2 Lab Sample ID: FA4930-9 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: MADEP EPH REV 1.1 SW846 3510C Percent Solids: nla Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC Page I of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 NN004804.1) 1 06/01/13 NMC 05/29/13 OP47077 GNN207 Run #2 Initial Volume Final Volume Run #1 1050 ml 2.0 ml Run #2 MAEPH List CAS No. Compound Result RL MDL Units Q 83-32.9 Acenaphthene ND 3.8 1.9 ugll 208-96-8 Acenaphthylene ND 3.8 L9 ugll 120-12-7 Anthracene ND 3.8 1.9 ugll 56-55-3 Benzo(a)anthracene ND 3.8 1.9 ugA 50-32-8 Benzo(a)pyrene ND 3.8 1.9 ugll 205-99-2 Benzo(b)fluoranthene ND 3.8 1.9 ugA 191-24-2 Benzo(g,h,i)perylene N❑ 3.8 1.9 ugA 207-08-9 Benzo(k)tluoranthene ND 3.8 1.9 ugll 218-01-9 Chrysene N❑ 3.8 I.9 ugll 53-70-3 ❑ibenzo(a,h)anthracene N❑ 3.8 1.9 ugll 206-44-0 Fluoranthene ND 3.8 1.9 ugll 86-73-7 Fluorene N❑ 3.8 1.9 ugll 193-39-5 Indeno(1.2,3-cd)pyrene ND 3.8 1.9 ugll 91-57-6 2-Methylnaphthalene ND 3.8 1.9 ugll 91-20-3 Naphthalene ND 3.8 1.9 ugll 85-01-8 Phenanthrene N❑ 3.8 1.9 ugll 129-00-0 Pyreoe ND 3.8 1.9 ugll C11-C22 Aromatics (Unadj.) 194 190 140 ugll C I 1-C22 Aromatics 194 I90 140 ugll C9-CI8 Aliphatics N❑ I90 95 ug1I C19-C36 Aliphatics N❑ 190 95 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane 63% 40.140% 580-13.2 2-Bromonaphthalene 91% 40-140% 84-15-1 o-Terphenyl 63% 40-140% 321-60-8 2-Fluorobiphenyl 96% 40-140% ND = Not detected MDL - Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■A 58of119 N ACCLJTEl3T. FA4930 ....... -. . Accutest LahLink@ 12:12 10-Jun-2013 Report of Analysis Client Sample ID: CSAMW-3 Lab Sample ID: FA4930-10 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: SM 6200B Percent Solids: nla Project: URSNCM: 51S 1363, 1101 Hwy 61, Whitsett, NC Page 1 of i File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a E024432.13 1 06/05/13 I'D n1a nla VE836 Run #2 Purge Volume Run #1 1001111 Run #2 VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.10 ugli 75-27-4 Bromodichloromethane ND 0.50 0.10 ugll 107.06-2 1,2-Dichloroethane ND 0.50 0.10 ugll 108-20-3 Di -Isopropyl ether ND 0.50 0.10 ugll 124-48-1 Dibromochloromethane ND 0.50 0.10 ugll 156-59-2 cls- 1, 2-Dichloroe(hylene ND 0.50 0.10 ugll 100-41-4 Ethylbenxene ND 0.50 0.10 ugll 99-87-6 p-Isapropyltoluene ND 0.50 0.10 ug11 74-87-3 Methyl chloride ND 0.50 0.11 ugll 1634-04-4 Methyl Ter( Butyl Ether 8.8 0.50 0.10 ugll 91-20-3 Naphthalene ND 0.50 0.15 ugll 108-88-3 Toluene ND 0.50 0.10 ug11 79-01-6 Trichloroethylene ND 0.50 0.10 ugll 1330-20-7 Xylene (total) ND 1.5 0.22 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Liasits 1868-53-7 Dibromufluoromethane 99% 70-130% 17060-07-0 1,2-Dichloroethane-D4 100% 70-130% 2037.26-5 Toluene -DO 101% 70-130% 460-00-4 4-Bromofluorobenxene 104% 70-130% (a) Sample was not preserved to a pH < 2; reported results are considered minimum values ND = Not detected MDL, - Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = Indicates analy(e Found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■ 59 of 119 AGCIJTEST FA49]0 Accutest LabLink@12:12 10-jun-2013 Report of Analysis Page 1 of 2 Client Sample ID: CSAMW-3 Lab Sample ID: FA4930-10 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: EPA 625 EPA 625 Percent Solids: nla Project: URSNCM: S/S 1363, 1101 Hwy 61, Whilsett, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run 01 L063722.1) 1 05/29/13 NAF 05/24/13 OP47046 5L3223 Run #2 Initial Volume Final Volume Run #1 1040 ml 1.0 ml Run #2 ABN List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 65-85-0 Benzoic Acid N❑ 48 9.6 ugll 95-57-8 2-Chlorophenol N❑ 4.8 0.68 ugll 59-50-7 4-Chloro-3-methyl phenol N❑ 4.8 0.78 ugll 120-83-2 2,4-Dichlorophenol ND 4.8 0.67 ugll 105-67-9 2,4-Dimethylphenol N❑ 4.8 0.74 ugll 51-28-5 2,4-Dinitrophenol ND 24 5.0 ug/l 534-52-1 4,6-Dinitro-o-Cresol N❑ 9.6 1.4 ugll 95-48-7 2-Methylphenol ND 4.8 0.69 ug11 3&4-Methylphenol ND 4.8 1.3 ugA 88-75-5 2-Nitrophenol ND 4.8 0.65 ugll 100-02-7 4-Nitrophenol ND 24 4.8 ugll 87-86-5 Pentachlorophenol N❑ 24 4.8 ugll 108-95-2 Phenol ND 4,8 0.53 ugll 88-06-2 2,4,6-Trichlorophenol ND C8 0.75 ugll 83-32-9 Acenaphthene ND 4.8 0.67 ugll 208-96-8 Acenaphthylene ND 4.8 0.67 ugll 120-12-7 Anthracene ND 4.8 0.72 ugll 56-55-3 Benzo(a)anthracene N❑ C8 0.52 ugll 50-32-8 Benzo(a)pyrene ND 4.8 0.55 ugll 205-99-2 Benza(b)fluoranthene ND 4.8 0.73 ug11 191.24-2 Benzo(g,h,i)perylene N❑ 4.8 0.64 ugll 207-08-9 Benzo(k)tluoranthene ND 4.8 0.64 ugll 101-55-3 4-Bromophenyl phenyl ether ND 4.8 0.76 ugll 85-68-7 Butyl benzyl phthalate N❑ 4.8 0.68 ugll 100.51-6 Benzyl Alcohol N❑ 4.8 0.96 ugll 91-58-7 2-Chloronaphthalene ND 4.8 0.70 ugll 106-47-8 4-Chloroaniline ND 4.8 0.66 ugll 218-01-9 Chrysene ND 4.8 0.56 ug11 111-91-1 bis(2-Chloroethoxy)methane ND 4.8 0.67 ugli 111-44-4 bis(2-Chloroelhyl)ether ND 4.8 0.69 ug/1 108-60-1 his(2-Chloroisopropyl)ether ND 4.8 0.76 ugll 7005-72-3 4-Chlorophenyl phenyl ether ND 4.8 0.84 ugll ND = Not detected MDL - Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■ 50 of 119 � ACCLJTEST. FA4930 Accutest LabLink@ 12:12 10-jun-2013 Report of Analysis Client Sample ID: CSAMW-3 Lab Sample ID: FA4930-10 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: EPA 625 EPA 625 Percent Solids: nla Project: URSNCM: SYS 1363, 1101 Hwy 61, Whitseu, NC ABN List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 95-50-1 1,2-Dichlorobenxene ND 4.8 0.65 ugll 122-66-7 1,2-Diphenylhydrazine ND 4.8 0.62 ugll 541-73-1 1.3-Dichlorobemene ND 4.8 0.75 ug1l 106.46-7 1,4-Dichlorobenzene ND 4.8 0.67 ugli 91-94-1 3.3'-Dichlorobenzidine N❑ 4.8 0.71 ugll 53-70-3 Dibenzo (a. it) anthracen e N❑ 4.8 0.56 ugli 132-64-9 Dibenzofuran ND 4.8 0.72 ugll 84-74.2 Di-n-butyl phthalate ND 4.8 0.96 ugll 117-84-0 Di-n-octyl phthalate ND 4.8 0.96 ugll 84-66.2 Diethyl phthalate ND 4.8 0.96 ugll 131-11-3 Dimethyl phthalale N❑ 4.8 0.77 ugll 117-81-7 bis(2-Ethylhexy1)ph1hala1e N❑ 4.8 1.1 ugll 206-44-0 Fluoranthene ND 4.8 0.56 ugll 86-73-7 Fluorene N❑ 4.8 0.73 ugll 118-74-1 Hexachlorobenxene ND 4.8 0.66 ugll 87-68-3 Hexachlorobutadiene ND C8 0.92 ugll 77-47-4 Hexachlorocyclopentadiene N❑ C8 0.76 ugll 67.72.1 Hexachloroethane ND 4.8 0.71 ugll 193-39-5 Indeno(1,2,3-cd)pyrene ND C8 0.55 ugll 78-59-1 Isophorone ND C8 0.61 ugll 90-12-0 1-Methylnaphthalene ND C8 0.68 ugll 91-57-6 2-Methylnaphthalene ND C8 0.66 ug11 91.20-3 Naphthalene ND 4.8 0.61 ugll 98-95-3 Nitrobenzene ND 4.8 0.69 ugll 621-64-7 N-Nitroso-di-n-propylamirie ND 4.8 0.82 ugll 86-30-6 N-Nitrosodiphenylamine N❑ 4.8 0.96 ugll 85-01-8 Phenanthrene ND 4.8 0.68 ugll 129.00-0 Pyrene N❑ 4.8 0.65 ugll 120-82-1 1,2.4-Trichlorobenzene N❑ 4.8 0.58 ugll CAS No. Surrogate Recoveries Run# I Run# 2 Limits 367.12-4 2-FIuorophenol 34% 14-67°% 4165-62-2 Phenol-d5 25% 10-50% 118.79-6 2,4,6-Tribroniophenol 82% 33-118% 4165-60-0 Nitrobenzene-d5 75% 42-108% 321-60-8 2-Fluorobiphenyl 81% 40-106% 1718-51-0 Terphenyl-dl4 51% 39-121% Page 2 of 2 ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value RL = Reporting Limit S = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound �ik 61 of 119 ACCUTEST FA49M '"''"" °. Accutest LabLinkP12:12 10-jun-2013 Report of Analysis at Sample ID: CSAMW-3 Sample ID: FA4930-10 rix: AQ - Ground Water aod: MADEP VPH REV 1.1 ect: URSNCM: S/S 1363. 1101 Hwy 61. Whitsett. NC File ID DF Analyzed By Prep Date #1 UU00355i.D 1 06/04/13 MM nla #2 Purge Volume Run #1 5.01111 Run #2 Page 1 of 1 Date Sampled: 05/22/13 Date Received: 05/23/13 Percent Solids: nla Prep Batch, Analytical Bate n!a GUU178 MADEP VPH List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 1.0 1.0 ugll 100-41-4 Ethylbenzene ND 2.0 1.0 ugll 1634-04-4 Methyl Ter( Butyl Ether 9.7 2.0 1.0 ugll 91-20-3 Naphthalene ND 5A 3.0 ugll 108-88-3 Toluene ND 2.0 1.0 ugll m,p-Xylene ND 4.0 2.0 u9/1 95-47-6 o-Xylene ND 2.0 1.0 ugll C5- C8 Aliphatics (Unadj.) ND 100 35 ugll C9- C12 Aliphatics (Unadj.) ND 100 35 ugll C9- C10 Aromatics (Unadj.) ND 100 35 ugll C5- C8 Aliphatics ND 100 35 ugll C9- C12 Aliphatics ND 100 35 ugll C9- CIO Aromatics ND 100 35 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 88% 70-130% 460-00-4 BFB 88% 70-130% ND = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range j = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound ■/ 62 of 119 ■.rwcUUrt[=—sr. FA4930 "•e...,,.. Accutest LabLink@ 12:12 10-Jun-2013 Report of Analysis Client Sample ID: CSAMW-3 Lab Sample ID: FA4930-10 Matrix: AQ - Ground Water Method: MADEP EPH REV I A SW846 3510C Project: URSNCM: 51S 1363, 1101 Hwy 61, Whitsett, NC File ID DF Analyzed By Prep Date Run #1 NN004805.1) 1 06/01/13 NMC 05/29/13 Run #2 Initial Volume Final Volume Run #1 1050 rul 2.0 nil Run #2 MAEPH List CAS No. Compound Result 83-32-9 Acenaphthene ND 208-96-8 Acenaphthylene ND 120-12-7 Anthracene N❑ 56-55-3 Benzo(a)anthracene ND 50-32-8 Benzo(a)pyrene ND 205-99-2 Benzo(b)fluoranthene ND 191-24-2 Benzo(g,h,i)perylene N❑ 207-08-9 Benzo(k)fluoranthene ND 218-01-9 Chrysene ND 53-70-3 Dibenzo(a,h)anthracene ND 206-44-0 Fluoranthene ND 86-73-7 Fluorene ND 193-39-5 Indeno(1,2,3-cd)pyrene ND 91-57-6 2-Methylnaphthalene ND 91-20-3 Naphthalene ND 85-01-8 Phenanthrene ND 129-00.0 Pyrene ND C11-C22 Aromatics (Unadj.) N❑ C11-C22 Aromatics ND C9-C18 Aliphatics ND C19-C36 Aliphatics N❑ CAS No. Surrogate Recoveries Run# 1 3386-33-2 1-Chloraactadecane 70% 580-13-2 2-Bromonaphthalene 82°% 84-15-1 o-Terphenyl 61% 321-60-8 2-Fluorobiphenyi 79% ND = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range Page 1 of 1 A Date Sampled: 05/22/13 v Date Received: 05/23/13 Percent Solids: nla Prep Batch Analytical Batch OP47077 GNN207 RL MDL Units Q 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 u9/1 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ug/l 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 3.8 1.9 ugll 190 140 ugll 190 140 ugll 190 95 ugll 190 95 ugll Run# 2 Limits 40-140°% 40-140°% 40-140°% 40.140% = Indicates an estimated value B = Indicates analyze found in associated method blank N = Indicates presumptive evidence of a compound N;L 63 of 119 W ACCLITEST FA4930 °"° Accutest Labl-ink@ 12:12 10-.dun-2013 Report of Analysis Client Sample ID: CSAMW-4 Lab Sample ID: FA4930-11 Matrix: AQ - Ground Water Method: SM 6200B Project: LIRSNCM: S1S 1363, 1101 Hwy 61. Whilsett, NC File ID DF Analyzed By Prep Date Run #1 E024420.D 1 06/04/13 TD nla Run #2 Purge Volume Run # 1 10.0 ml Run #2 Page 1 of I A Date Sampled: 05/22/13 Date Received: 05/23/13 Percent Solids: nla Prep Batch Analytical Batch n/a VE835 VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.10 ugll 75-27-4 Bromodichloromethane ND 0.50 0.10 ugA 107-06-2 1.2-Dichloroethane ND 0.50 0.10 ug11 108-20-3 Di -Isopropyl ether N❑ 0.50 0.10 ug11 124-48-1 ❑ibromochloromethane ND 0.50 0.10 ugll 156-59-2 cis-1,2-Dichioroethylene N❑ 0.50 0.10 ug/l 100-41-4 Ethylbenzene ND 0.50 0.10 ugll 99-87-6 p-Isopropyholuene ND 0.50 0.10 ug/l 74-87-3 Methyl chloride ND 0.50 0.11 ugll 1634-04-4 Methyl Teri Butyl Ether 0.17 0.50 0.10 ug/I j 91-20-3 Naphthalene N❑ 0.50 0.15 ugll 108-88-3 Toluene ND 0.50 0.10 ugll 79-01-6 Trichloroethylene N❑ 0.50 0.10 ug11 1330-20-7 Xylene (total) ND 1.5 0.22 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868.53.7 Dibromofluoromethane 99% 70-130% 17060-07-0 1,2-Dichloroethane-D4 98% 70-130% 2037-26-5 Toluene-D8 96% 70-130% 460-00.4 4-Bromofluorobenzene 102% 70-130% ND = Not detected MDL - Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = Indicates anaiyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■W 64 of 119 MACCLlTEST. FA493,0 ......""". Accutest LabLink@12:12 10-Jun-2013 Report of Analysis Page I of 2 it Sample ID: CSAMW-4 A Sample ID: FA4930-11 Date Sampled: 05/22/13 rix: AQ - Ground Water Date Received: 05/23/13 hod: EPA 625 EPA 625 Percent Solids: nla Oct: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett. NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch #1 L063723.D 1 05/29/13 NAF 05/24/13 OP47046 SL3223 #2 Initial Volume Final Volume Run #1 1040 ml 1,0 ml Run #2 ABN List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 48 9.6 ug/I 95-57-8 2-Chlorophenol ND 4.8 0.68 ug/I 59-50-7 4-Chloro-3-methyl phenol N❑ 4.8 0.78 ugll 120-83-2 2,4-Dichlorophenol ND 4.8 0.67 ugll 105-67-9 2,4-Dimethylphenol ND 4.8 0.74 ug/I 51-28-5 2,4-Dinitrophenol N❑ 24 5.0 ugll 534-52-1 4,6-Dinitro-o-cresol N❑ 9.6 1.4 ugll 95-48-7 2-Methylphenol ND 4.8 0.69 ugll 3&4-Methylphenol N❑ 4.8 1.3 ug/I 88-75.5 2-Nitrophenol ND 4.8 0.65 ug/l 100-02-7 4-Nitrophenol N❑ 24 4.8 ugll 87-86-5 Pentachlorophenol ND 24 4.8 ugll 108-95-2 Phenol N❑ 4.8 0.53 ug/l 88-06-2 2,4.6-Trichlorophenol N❑ 4.8 0.75 ug/l 83-32-9 Acenaphthene ND 4.8 0.67 ug/l 208-96-8 Acenaphthylene ND 4.8 0.67 ug/l 120-12-7 Anthracene ND 4.8 0.72 ugll 56-55-3 Benzo(a)anthracene ND 4.8 0.52 ug/I 50-32-8 Benzo(a)pyrene ND 4.8 0.55 ugA 205-99-2 Benzo(b)fluoranthene ND C8 0.73 ug/l 191-24-2 Benzo(g,h,i)perylene ND 4.8 0.64 ug/l 207-08-9 Benno(k)iluoranthene N❑ 4.8 0.64 ugll 101-55-3 4-Bromophenyl phenyl ether ND 4.8 0.76 ug/I 85-68-7 Butyl benzyl phthalate ND 4.8 0.68 ugll 100-51-6 Benzyl Alcohol ND 4.8 0.96 ug/I 91-58-7 2-Chiorunaphthalene N❑ 4.8 0.70 ug/I 106-47-8 4-Chloroaniline ND 4.8 0.66 ugll 218-01-9 Chrysene N❑ 4.8 0.56 ug/I 111.91.1 his (2-Chioroethoxy)methane ND 4.8 0.67 ugll 111-44-4 bis(2-Chloroethyl)ether ND 4.8 0.69 ug/I 108-60-1 bis(2-Chloroisopropyl)ether N❑ 4.8 0.76 ug/I 7005.72.3 4-Chlorophenyl phenyl ether ND 4.8 0.84 ug/I N❑ = Not detected MDL - Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyze found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound �■ 65 of 119 ACCLJTE^.3T. FA4930 •..... ° Accutest LabLink912:12 10-Jun-2013 Report of Analysis Client Sample ID: CSAMWA Lab Sample ID: FA4930-11 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: EPA 625 EPA 625 Percent Solids: nla Project: URSNCM: SIS 1363, 1101 Hwy 61. Whitsett, NC ABN List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 95-50-1 1.2-Dichlorobenzene ND 4.8 0.65 ugll 122-66-7 I,2-Diphenylhydrazine ND 4.8 0.62 ugll 541-73.1 1,3-Dichlorobenzene ND 4.8 0.75 ugll 106-46-7 1,4-Dichlorobenzene ND C8 0.67 ugll 91-94-1 3,3'-Dichlorobenzidine ND 4.8 0.71 ug/l 53-70-3 Dibenzo(a.h)anthracene ND 4.8 0.56 ugll 132-64-9 Dibenzofuran ND 4.8 0.72 ugll 84-74-2 Di-n-butyl phthalate ND 4.8 0.96 ugA 117-84-0 Di-n-octyl phthalate ND 4.8 0.96 ugll 84-66-2 Diethyl phthalate ND 4.8 0.96 ugA 131-11-3 Dimethyl phthalate ND 4.8 0.77 ugA 117-81-7 his(2-Ethylhexyl)phthalate ND 4.8 1.1 ugll 206-44-0 Fluoranthene ND 4.8 0.56 ugll 86-73-7 Fluorene ND 4.8 0.73 ugA 118-74-1 Hexachlorobenzene ND 4.8 0.66 ugll 87-68-3 Hexachlorobutadiene ND 4.8 0.92 ugA 77-47-4 Hexachlo ro cyclo pentad iene ND 4.8 0.76 ugll 67-72-1 Hexachloroethane ND 4.8 0.71 ugli 193-39-5 Indeno(1,2,3-cd)pyrene ND 4.8 0.55 ugll 78-59-1 Isophorone ND 4.8 0.61 ugll 90-12-0 1-Methylnaphthalene ND 4.8 0.68 ugll 91-57-6 2-Methylnaphthalene ND 4.8 0.66 ugll 91-20-3 Naphthalene ND 4.8 0.61 ugll 98-95-3 Nitrobenzene ND 4.8 0.69 ugll 621.64.7 N-Nitroso-di-n-propylamine ND 4.8 0.82 ugll 86-30-6 N-Nitrosodiphenylamine ND 4.8 0.96 ug11 85-01-8 Phenanthrene ND 4.8 0.68 ugll 129-00-0 Pyrene N❑ 4.8 0.65 ugli 120-82-1 1.2.4-Trichi orobenzene ND 4.8 0.58 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fiuorophenol 37% 14-67% 4165-62-2 Phenol-d5 24% 10-50% 118-79-6 2,4,6-Tribromophenol 87% 33-118% 4165-60-0 Nitrobenzene-d5 80% 42-108% 32i-60-8 2-Fluorobiphenyl 82% 40-106% 1718-51-0 Terphenyl-d14 59% 39-121% Page 2 of 2 ND = Not detected MDL - Method Detection Limit I = Indicates an estimated value RL = Reporting Limit B = Indicates analyze found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound _ 66 of 119 U ACCLJTEST. FA4930 '" °° Acculest LabLink@12:12 10-Jun-2013 Report of Analysis Page 1 of 1 it Sample ID: CSAMWA Sample ID: FA4930-11 Date Sampled: 05/22/13 -ix: AQ - Ground Water Date Received: 05/23/13 ►od: MADEP VPH REV 1.1 Percent Solids: nla ect: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 UU003552.D 1 06/04/13 MM nla nla GUU178 Run #2 Purge Volume Run 41 5.0 ml Run #2 MADEP VPH List CAS No. Compound Result RL MDL Units Q 71.43-2 Benzene ND 1.0 1.0 ugl! 100-41-4 Ethylbenzene ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 2.0 1.0 ugll 91-20-3 Naphthalene ND 5.0 3.0 ugll 108-88-3 Toluene ND 2.0 1.0 ugll m,p-Xylene ND 4.0 2.0 ugll 95-47-6 o-Xylene N❑ 2.0 1.0 ugll C5- C8 Aliphatics (Unadj-) ND 100 35 ugll C9- C12 Aliphatics (Unadj.) N❑ 100 35 ugll C9- C10 Aromatics (Unadj.) ND 100 35 ug11 C5- C8 Aliphatics N❑ 100 35 ug1l C9- C12 Aliphatics ND 100 35 ugll C9- C10 Aromatics N❑ 100 35 ugA CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 85% 70-130% 460-00-4 BFB 87% 70-130% ND = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range j = Indicates an estimated value B = Indicates analyle found in associated method blank N = Indicates presumptive evidence of a compound M® 67 of 119 E ACCLJTEST. FA4934 Accutest LabLink@l2:12 10-jun-2013 Report of Analysis Page 1 of 1 at Sample ID: CSAMW-4 a Sample ID: FA4930-11 Date Sampled: 05/22/13 rix: AQ - Ground Water Date Received: 05/23/13 dod: MADEP EPH REV 1.1 SW846 3510C Percent Solids: nla ect: URSNCM: SIS 1363, 1101 Hwy fit, Whi(sett. NC File ID DF Analyzad By Prep Date Prep Hatch Analytical Batch Run #1 NN004806.I) 1 06/01/13 NMC 05/29/13 ❑P47077 GNN207 Run #2 Initial Volume Final Volume Run 41 1050 ml 2,0 ml Run #2 MAEPH List CAS No. Compound Resuk RL 11 im Units Q 83-32-9 Acenaphthene ND 3.8 1.9 ugll 208-96-8 Acenaphthylene ND 3.8 1.9 ugll 120-12-7 Anthracene ND 3.8 1.9 ugll 56-55-3 Benzo(a)anthracene ND 3.8 1.9 ugll 50-32-8 Benzo(a)pyrene ND 3.8 1.9 ugll 205-99-2 Senzo(b)fluoranthene ND 3.8 1.9 ugll 191-24-2 Benzo(g,hJ)perylene ND 3.8 1.9 ugll 207-08-9 Benzo(k)fluoranthene ND 3.8 1.9 ugll 218-01-9 Chrysene ND 3.8 1.9 ugll 53-70-3 Dibenxo(a,h)anthracene ND 3.8 1.9 ugll 206-44-0 Fluoranthene ND 3.8 1.9 ugll 86-73-7 Fluorene ND 3.8 1.9 ugli 193-39-5 Indeno(1,2,3-cd)pyrene ND 3.8 1.9 ugll 91-57-6 2-Methylnaphthalene ND 3.8 1.9 ugll 91-20-3 Naphthalene ND 3.8 1.9 ugll 85-01-8 Phenanthrene ND 3.8 1.9 ugll 129-00-0 Pyrene N❑ 3.8 1.9 ugll CI I-C22 Aromatics (Unadj.] ND 190 140 ugll C11-4222 Aromatics ND 190 140 ugll C9-C18 Aliphatics ND 190 95 ugll C19-06 Aliphatics ND 190 95 ugll CAS No. Surrogate Reooveries Ruts# I Run# 2 Limits 3386-33-2 1-Chloroociadecane 72% 40-140% 580-13-2 2-Bromonaphthalene 91% 40-140% 84-15-1 o-Terphenyl 67% 40-140% 321-60-8 2-Fluorobiphenyl 88% 40-140% ND = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range j = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound ■ 68 of 119 ACCLI���u- T. Accutest LabLink@12:12 10-Jun-2013 Report of Analysis %ent Sample ID: DDAMW-2 ab Sample ID: FA4930-12 Date Sampled: 05/22/13 Tatrix. AQ - Ground Water Date Received: 05/23/13 lthod: SM 6200B Percent Solids: nla roject: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett. NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch. Analytical Bate Run # 1 E024421. D 1 06/04/13 TD n/a rif a VE835 Run #2 Purge Volume un #1 10.0 ml un #2 VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene 0.58 0.50 0.10 ugll 75-27-4 Bromodichloromethane ND 0.50 0.10 ugl] 107-06-2 1,2-Dichloroethane ND 0.50 0.10 ugll 108-20-3 Di -Isopropyl ether ND 0.50 0.10 ugll 124-48-1 Dibromochloromethane ND 0.50 0.10 ugli 156-59-2 cis- 1,2-Dichloraethylene ND 0.50 0.10 ugll 100-41-4 Ethylbenxene N❑ 0.50 0.10 ugll 99-87-6 p-lsopro pyltoluene ND 0.50 0.10 ug/l 74-87-3 Methyl chloride ND 0.50 0.11 ugll 1634-04-4 Methyl Tert Butyl Ether 2.6 0.50 0.10 ugll 91-20-3 Naphthalene 2.7 0.50 0.15 ugll 108-88-3 Toluene ND 0.50 0.10 ugll 79-01-6 Trichloroethylene ND 0.50 0.10 ugll 1330-20-7 Xylene (to(al) ND 1.5 0.22 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 98% 70-130% 17060-07-0 1,2-Dichloroethane-D4 100% 70-130% 2037-26-5 Toluene-D8 100% 70-130% 460-00-4 4-Bromofluorobenzene 102% 70-130% ND = Not detected MDL - Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = Indicates analyze found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound A 3 ■® 69 of 119 w.nkOOU-rz=s-r. FA4930 . - ....... Accutest LabLink012:12 10-jun-2013 Report of Analysis Client Sample ID: ❑DAMW-2 Lab Sample ID: FA4930-12 Matrix: AQ - Ground Water Method- EPA 625 EPA 625 Project: URSNCM: S/S 1363, 1101 Hwy 61. Whitsett, NC File ID DF Analyzed By Prep Date Run #1 a U038563-D 4 05/30/13 NAF 05/24/13 Run #2 a T008227.D 4 06/05/13 FS 06/03/13 Initial Volume Final Volume Run #1 1040 ml 1,0 ml Run #2 1040 ml 1.0 ml ABN List for NC, May 2012 Page 1 of 3 a Date Sampled: 05/22/13 N Date Received: 05/23/13 Percxat Solids: nla Prep Batch Analytical Batch ❑P47046 SU1805 OP47154 ST401 CAS No. Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 190 38 ugll 95-57-8 2-Chlorophenol ND 19 2.7 ugll 59-50-7 4-Chloro-3-methyl phenol ND 19 3.1 ugh 120-83-2 2,4-Dichlorophenol ND 19 2.7 ugll 105-67-9 2,4-Dimethylphenol ND 19 2.9 ug11 51-28-5 2,4-Dinitrophenol ND 96 20 ugll 534-52-1 4,6-Dinitro-o-cresol ND 38 5.5 ugll 95-48-7 2-Methylphenol ND 19 2.8 ugll 3&4-Methylphenol ND 19 5.3 ugll 88-75-5 2-Nitrophenol N❑ 19 2.6 ugll 100-02-7 4-Nitrophenol ND 96 19 ugll 87-86-5 Pentachlorophenol N❑ 96 19 ugli 108-95-2 Phenol ND 19 2.1 ugll 88-06-2 2,4,6-Trichlorophenol ND 19 3.0 ugll 83-32-9 Acenaphthene ND 19 2.7 ugll 208-96-8 Acenaphthylene ND 19 2.7 ugll 120-12-7 Anthracene ND 19 2.9 ugll 56-55-3 Benzo(a)anthracene ND 19 2.1 ugll 50-32-8 Benzo(a)pyrene ND 19 2.2 ugA 205-99-2 Benxo(b)fluoranthene ND 19 2.9 ugll 191.24-2 Benzo(g,h,i)perylene ND 19 2.6 ugll 207-08-9 Benzo(k)fluoranthene ND 19 2.6 ugll 101-55-3 4-Bromophenyl phenyl ether ND 19 3.0 ugll 85-68-7 Butyl benzyl phthalate ND 19 2.7 ugli 100-51-6 Benzyl Alcohol ND 19 3.8 ugll 91-58-7 2-Chloronaphthalene N❑ 19 2.8 ugll 106-47-8 4-Chloroaniline N❑ 19 2.6 ugA 218-01-9 Chrysene N❑ 19 2.2 ugll 111.91-1 bis(2-Chloroethoxy)methane ND 19 2.7 ugll 111-44-4 his (2-Chloroethyl)ether N❑ 19 2.8 ugll 108-60-1 his{2-Chloroisopropyl}ether ND 19 3.0 ugll 7005-72-3 4-Chlorophenyl phenyl ether ND 19 3.3 ugll ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyze found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■e 74 of 119 ■.acGu-r��-r. FA4930 ""'"" Accutest LabLink@12:12 10-jun-Z013 Report of Analysis Client Sample ID: ❑DAMW-2 Lab Sample ID: FA4930-12 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: EPA 625 EPA 625 Percent Solids: nla Project: URSNCM: 51S 1363, 1101 Hwy fit, Whitsett, NC ABN List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 95-50-1 1,2-Dichlorobenzene ND 19 2.6 ug11 122-66-7 1,2-Diphenylhydrazine ND 19 2.5 ugll 541-73-1 1,3-Dichlorobenzene ND 19 3.0 ug1l 106-46-7 1,4-Dicblorobenxene ND 19 2.7 ugll 91-94-1 3,3'-Dichlorobenzidine N❑ 19 2.8 ug1l 53-70-3 Dibenzo(a.h)anthracene ND 19 2.2 ugll 132-64-9 Dibenzofuran ND 19 2.9 ugll 84-74-2 Di-n-butyl phthalate N❑ 19 3.8 ugll 117-84-0 Di-n-octyl phthalate ND 19 3.8 ugll 84-66-2 Diethyl phthalate ND 19 3.8 ugll 131-11-3 Dimethyl phthalate ND 19 3.1 ugll 117-81-7 his (2-Ethylhexyl)phthalate 5.3 19 4.4 ugll j 206-44-0 Fluoranthene N❑ 19 2.3 ugll 86-73-7 Fluorene ND 19 2.9 ugA 118-74-1 Hexachlorobenzene ND 19 2.6 ugll 87-68-3 Hexachlorobutadiene ND 19 3.7 ug/l 77-47-4 Hexachlorocyclopentadiene ND 19 3.0 ugll 67-72-1 Hexachloroethane ND 19 2.9 ugll 193-39-5 Indeno(1.2,3-cd)pyrene ND 19 2.2 ugll 78-59-1 Isophorone ND 19 2.5 ugll 90-12-0 1-Methylnaphthalene ND 19 2.7 ugll 91-57-6 2-Methylnaphthalene ND 19 2.6 ugll 91-20-3 Naphthalene ND 19 2.4 ugll 98-95-3 Nitrobenzene ND 19 2.8 ugA 621-64-7 N-Nitroso-di-n-propylamine ND 19 3.3 ugll 86-30-6 N-Nitrosodiphenylamine ND 19 3.8 ug/l 85-01-8 Phenanthrene ND 19 2.7 ugll 129-00-0 Pyrene ND 19 2.6 ngll 120-82-1 1,2,4-Trichlorobenzene ND 19 2.3 ug1l CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 26% 45% 14-67% 4165-62-2 Phenol-d5 24% 36% 10-50% 118-79-6 2,4,6-Tribromophenol 64% 98% 33-118% 4165-60-0 Nitrobenzene-d5 67% 88% 42-108% 321-60-8 2-Fluorobiphenyl 73% 102% 40-106% 1718-51.0 Terphenyl-dl4 28% r 88% 39-121% (a) Confirmed by re -extraction and reanalysis beyond hoidtime. Page 2 of 3 ND = Not detected MDL - Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 71 of 119 ACGUTEST FA4930 •"•e..,e.,.. Accutest LabLinkP12.12 10-Jun-2013 Report of Analysis Client Sample ID: DDAMW-2 Lab Sample ID: FA4930-12 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: EPA 625 EPA 625 Percent Solids: nla Project: URSNCM. S/S 1363. 1101 Hwy fit, Whitsett, NC ABN List for NC, May 2012 CAS No. Compound Result RL MDL Units Q (b) Confirmation run. (c) Outside control limits. Page 3 of 3 ND = Not delected MDL - Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = Indicates anaiyte Found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■o 72 of 119 w ACCLITt_ST. FA4930 iwitl"'""�� Accutest LabLink@12:12 10-Jun-2013 Report of Analysis Client Samplc ID: DDAMW-2 Lab Sample ID: FA4930.12 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Rweived: 05/23/13 Method: MADEP VPH REV 1.1 Percent Solids: nla Project: URSNCM: 515 1363, 1101 Hwy 61, Whilsett, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a UU003582.D 1 06/05/13 MM nla nla GUU179 Run #2 Purge Volume Run #1 5.0 mi Run #2 MADEP VPH List CAS No. Compound Result 71-43-2 Benzene ND 100-41-4 Ethylbenxene ND 1634-04-4 Methyl Teri Butyl Ether 3.2 91-20-3 Naphthalene a 28.1 108-88-3 Toluene ND m,p-Xylene N❑ 95-47-6 o-Xylene ND C5- C8 Aliphatics (Unadj.) N❑ C9- C12 Aliphatics (Unadj.) ND C9- C 10 Aromatics (Unadj.) 122 C5- C8 Aliphatics N❑ C9- C 12 Aiiphatics ND C9- CIO Aromatics 122 CAS No. Surrogatc Recoveries Run# 1 460-00-4 BFB 110% 460-00-4 BFB 103% (a) No sample available for reanalysis. (b) Associated CCV recovery outside control limits. ND = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range RL MDL Units Q 1.0 1.0 ugll 2.0 1.0 ugll 2.0 1.0 ugll 5.0 3.0 ugll j 2.0 1.0 ugll 4.0 2.0 ugll 2.0 1.0 ugll 100 35 ugli 100 35 ug/l 100 35 ugll 100 35 ugll 100 35 ugll 100 35 ug11 Run# 2 Limits 70-130% 70-130% j = Indicates an estimated value B = Indicates analyze found in associated method blank N = Indicates presumptive evidence of a compound ME 73 of 119 I♦ ACGUTEST. FA4930 ......T�"�� Accutest Labl-ink912:12 10-Jun-2013 Report of Analysis Client Sample ID: DDAMW-2 Lab Sample ID: FA4930-12 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: MADEP EPH REV 1.1 SW846 3510C Percent Solids: nla Project: URSNCM: S/S 1363, 1101 Hwy 61, Whitsett, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 NN004807.1) 1 06/01/13 NMC 05/29/13 ❑P47077 GNN207 Run #2 Initial Volume Final Volume Run #1 1040 ml 2.0 ml Run #2 MAEPH List CAS No. Compound Result RL MDL Units Q 83-32-9 Acenaphthene ND 3.8 1.9 ugll 208-96-8 Acenaphthylene ND 3.8 1.9 ugll 120-12-7 Anthracene ND 3.8 1.9 ugll 56-55-3 Benzo(a)anthracene ND 3.8 1.9 ugll 50-32-8 Benzo(a)pyrene ND 3,8 1.9 ugll 205-99-2 Benzo(b)fluoranthene ND 3.8 1.9 ugll 191-24-2 Benzo(g,h,i)perylene ND 3.8 1.9 ugll 207-08-9 Senzo(k)fluoranthene ND 3.8 1.9 ugll 218-01-9 Chrysene ND 3.8 1.9 ugll 53-70-3 Dibenzo(a,h)anthracene ND 3.8 1.9 ugll 206-44-0 Fluoranthene N❑ 3.8 1.9 ugll 86-73-7 Fluorene ND 3.8 1.9 ugll 193-39-5 Indeno(1,2,3-cd)pyrene N❑ 3.8 1.9 ugll 91-57-6 2-Methylnaphthalene ND 3.8 1.9 ug11 91-20-3 Naphthalene N❑ 3.8 L9 ug1l 85-01-8 Phenanthrene N❑ 3.8 1.9 ugll 129-00-0 Pyrene N❑ 3.8 1.9 ug11 C11-C22 Aromatics (Unadj.} 400 190 140 ugll C I 1-C22 Aromatics 400 190 140 ugll C9-C18 Aliphatics 2120 190 96 ugll C19-06 Aliphatics 1090 190 96 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 3386.33-2 1-Chloroociadecane 78% 40-140% 580-13-2 2-Bromonaphthalene 93% 40-140% 84-15-1 o-Terphenyl 66% 40-140% 321.60-8 2-Fluorohiphenyl 88% 40-140% ND = Nat detected MDL - Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■ :; 74 of 119 ■ .accuTEs�: Accutest LabLink@12:12 10-jun-2013 Report of Analysis Client Sample 1D: DUP-2 Lab Sample ID: FA4930-13 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: SM 6200B Percent Solids: n/a Proj ect: URSNCM: S/S 1363. 1101 Hwy 61. Whitsett, NC Page I of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E024434-D 1 06/05/13 TD n/a n/a VE836 Run #2 E024436.I) 10 06/05/13 TD n/a ri/a VE836 Purge Volume Run # 1 10.0 ml Run 02 10.0 nil VOA Special List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene 4.2 0.50 0.10 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.10 ug/1 107-06-2 1,2-Dichloroethane N❑ 0.50 0.10 ug/l 108-20-3 Di -Isopropyl ether ND 0.50 0.10 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l 156-59-2 cis-1.2-Dichloroethylene ND 0.50 0.10 ugll too-41-4 Ethylhenzene 0.35 0.50 0.10 ug/l j 99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/I 74-87-3 Methyl chloride N❑ 0.50 0.11 ug/l 1634-04-4 Methyl Tert Butyl Ether 0.30 0.50 0.10 ug/l j 91-20-3 Naphthalene 204 a 5.0 1.5 ug/l 108-88-3 Toluene 0.30 0.50 0.10 ug/1 j 79-01-6 Trichloroethylene ND 0.50 0.10 ug/1 1330-20-7 Xylene ((otal) ND 1.5 0.22 ugA CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromolluoromethane 99% 99% 70-130% 17060-07-0 1,2-Dichloroethane-D4 99% 99% 70-130% 2037-26-5 Toluene-138 99% 101% 70-130% 460-00-4 4-Bromofluorobenzene 102% 102% 70-130% (a) Result is from Run# 2 ND = Not detected MDL - Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■■ 75 of 119 w A.CCU-TEST. Fh4930 •"....r.,.. Accutest LabLinkPI2.12 10-Jun-2013 Client Sample ID: DUP-2 Lab Sample ID: FA4930-13 Matrix: AQ - Ground Water Method: EPA 625 EPA 625 Project: URSNCM: S/S 1363 File ID DF Run #1 a U038564.1) 4 Run #2 b T008228.1) 4 Report of Analysis Page 1 of 3 A Date sampled: 05/22/13 w Date Received: 05/23/13 Pero mt Solids: nla 9 1101 Hwy 61, Whiisett. NC Analyzed By Prep Date Prep Batch Analytical Batch 05/30/13 NAF 05/24/13 OP47046 SU1805 06/05/13 FS 06/03/13 OP47154 ST401 Initial Volume Final Volume Run #1 1040 ml 1.0 ml Run #2 1040 ml 1.0 ml ABN List for NC, May 2012 CAS No. Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 190 38 ugll 95-57-8 2-Chlorophenol ND 19 2.7 ugll 59-50-7 4-Chloro-3-methyl phenol ND 19 3.1 ugll 120-83-2 2,4-Dichlorophenol N❑ 19 2.7 ugll 105-67-9 2,4-Dimethylphenol N❑ 19 2.9 ugll 51-28-5 2,4-Dinitrophenol ND 96 20 ugll 534-52-1 4,6-Dinitro-o-cresol N❑ 38 5.5 ugll 95-48-7 2-Methylphenol ND 19 2.8 ugll 3&4-Methylphenol ND 19 5.3 ugll 88-75-5 2-Nitrophenol ND 19 2.6 119/1 100-02-7 4-Nitrophenol ND 96 19 ugll 87-86-5 Pentachlorophenol ND 96 19 ugll 108-95-2 Phenol N❑ 19 2.1 ugll 88-06-2 2,4,6-Trichlorophenol ND 19 3.0 ugA 83-32-9 Acenaphthene 4.5 19 2.7 ugA 208-96-8 Acenaphthylene ND 19 2.7 ugll 120-12-7 Anthracene ND 19 2.9 ugll 56.55-3 Benzo(a)anthracene ND 19 2.1 ugli 50-32-8 Benzo(a)pyrene ND 19 2.2 ugll 205-99.2 Benzo(b)fluoranthene ND 19 2.9 ugll 191-24-2 Benzo(g,h,i)perylene ND 19 2.6 ugll 207-08-9 Benzo(k)fluoranthene ND 19 2.6 ugA 101-55-3 4-Bromophenyl phenyl ether N❑ 19 3.0 ugll 85-68-7 Buryl benzyl phthalate ND 19 2.7 ugll 100-51-6 Benzyl Alcohol ND 19 3.8 ugll 91-58-7 2-Chloronaphthalene N❑ 19 2.8 ugli 106-47-8 4-Chloroaniline ND 19 2.6 ugll 218-01-9 Chrysene ND 19 2.2 ugll I11-91-1 bis(2-Chloroethoxy)methane N❑ 19 2.7 ugll 111-44-4 bis(2-Chloroethyl)ether ND 19 2.8 ugll 108-60-1 bis(2-Chloroisopropyl)ether ND 19 3.0 ugA 7005.72-3 4-Chlorophenyl phenyl ether ND 19 3.3 ugll N❑ = Not detected MDL - Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound �■ 76 of 119 .4CCUTES-r FA4930 ......--. Accutest LabLink@1Z.12 10-Jun-2013 Report of Analysis Client Sample ID: DUP-2 Lab Sample ID: FA4930-13 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: EPA 625 EPA 625 Percent Solids: nla Project: URSNCM: SIS 1363, 1101 Hwy 61. Whitsett, NC ABN List for NC, May 2012 CAS No. Compound Result RL MI]L Units Q 95-50-1 1,2-Dichlorobenzene ND 19 2.6 ugll 122-66-7 1,2-Diphenylhydrazine ND 19 2.5 ugll 541-73-1 1,3-Dichlorobenzene ND 19 3.0 ugll 106-46-7 1,4-Dichlorobenxene ND 19 2.7 ugll 91-94-1 3,3'-Dichlorobenzidine ND 19 2.8 ugll 53-70-3 Dibenxo(a,h)anthracene N❑ 19 2.2 ugll 132-64.9 Dibenzofuran 3.2 19 2.9 ugll J 84-74-2 Di-n-butyl phthalate ND 19 3.8 ugll 117-84-0 Di-n-octyl phthalate ND 19 3.8 u9/1 84-66-2 Diethyl phthalate ND 19 3.8 ugll 131-11-3 Dimethyl phthalate N❑ 19 3.1 ugll 117-81-7 bis(2-Ethylhexyl)ph1halate N❑ 19 4.4 ugll 206-44-0 Fluoranthene ND 19 2.3 ugll 86-73-7 Fluorene 12.2 19 2.9 ugll J 118-74-1 Hexachlorobenzene N❑ 19 2.6 ugll 87-68-3 Hexachlorobutadiene ND 19 3.7 ugll 77-47-4 Hexachlorocyclopentadiene ND 19 3.0 U911 67-72-1 Hexachloroethane ND 19 2.9 ugll 193-39-5 Indeno(1,2,3-cd)pyrene ND 19 2.2 ugll 78-59-1 Isophorone ND 19 2.5 ugll 90-12-0 1-Methyinaphthalene 93.0 19 2.7 ug11 91-57-6 2-Methylnaphthalene 115 19 2.6 ugll 91-20-3 Naphthalene 93.6 19 2.4 ugll 98-95-3 Nitrobenzene ND 19 2.8 ugll 6Z1-64-7 N-Nitrose-di-n-propyiamine ND 19 3.3 ugll 86-30-6 N-Nitrosodiphenylamine ND 19 3.8 ugll 85-01-8 Phenanthrene 14.4 19 2.7 ugll 129-00-0 Pyrene 4.9 19 2.6 ugll ) 120-82-1 1,2,4-Trichlorobenzene ND 19 2,3 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 367.12-4 2-Fluorophenol 11% c 43% 14-67% 4165-62-2 Phenol-d5 8% C 32% 10-50% 118-79-6 2,4,6-Tribromophenol 33% 85% 33-118% 4165-60-0 Nitrobenzene-d5 54% 115% 42-108% 3Z1-60-8 2-Fluorobiphenyl 53% 94% 40-106% 1718-51-0 Terphenyl-d14 14% c 85% 39-121% (a) Confirmed by re -extraction and reanalysis beyond holdtime. Page 2 of 3 N❑ = Not detected MDL - Method Detection Limit J = Indicates an estimated value RL = Reporting Limit $ = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 77 of 119 � ACCEJTEST. FA4930 •••""••�••• Acculest LabLink@12:12 10-,dun-2013 Report of Analysis Client Sample ID: DUP-2 Lab Sample ID: FA4930-13 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: EPA 625 EPA 625 Percent Solids: nla Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett. NC ABN List for NC, May 2012 CAS No. Compound Result RL MDL Units Q (h) Confirmation run. [c] Outside control limits. Page 3 of 3 ND = Not delecled MDL - Method Detection Limit ] = Indicates an estimated value RL = Reporting Limit B = Indicates analyze found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■ -1 78 of 119 � ACCLJTEST Accuiest LabLink@12:12 10-Jun-2013 Report of Analysis Client Sample ID: ❑UP-2 Lab Sample ID: FA4930-13 Matrix: AQ - Ground Water Method: MADEP VPH REV I.I Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett. NC File ID DF Analyzed By Prep Date Run #1 UU003583.1) 1 06/05/13 MM nia Run #2 a UU003629.D 5 06/06/13 MM nla Purge Volume Run #1 5.0 nil Run #2 5.0 ml Page 1 of I A Date Sampled: 05/22/13 W Date Received: 05/23/13 Percent Solids: nla a Prep Batch Analytical Batch nla GUU 179 nla GUU181 NL DEP VPH List CAS No. Compound Result RL MDL Chits Q 71-43-2 Benzene 3.2 1.0 1.0 ugli 100-41-4 Ethylbenzene N❑ 2.0 1.0 ugll 1634-04-4 Methyl Teri Butyl Ether ND 2.0 1.0 ugll 91-20-3 Naphthalene 239 b 25 15 ugll 108-88-3 Toluene ND 2.0 1.0 ugll m.p-Xylene ND 4,0 2.0 ugll 95-47-6 o-Xylene ND 2.0 1.0 ug1l C5- C8 Aliphatics (Unadj.) 56.8 100 35 ugll j C9- C12 Aliphatics (Unadj.) 301 b Soo 180 ug/l j C9- CID Aromatics (Unadj.) 935 a 500 180 ugll C5- C8 Aliphatics 53.6 100 35 ug,/l J C9- C12 Aliphatics 301 h 500 180 ugll j C9- C10 Aromatics 935 b 500 180 ugA CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 131%r 127% 70-130% 460-00-4 BFB 114% 104% 70-130% (a) Sample re -analyzed beyond hold time; reported results are considered minimum values. (b) Result is from Run# 2 (c) Outside control limits due to matrix interference. ND = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range j = Indicates an estimated value B = indicates analyze found in associated method blank N = Indicates presumptive evidence of a compound �■ 79 of 119 ^cct +-rEEE3-r. Accutest LabLinkP12:12 10-Jun-2013 Report of Analysis Client Sample ID: ❑UP-2 Lab Sample ID: FA4930-13 Date Sampled: 05/22/13 Matrix: AQ - Ground Water Date Received: 05/23/13 Method: MADEP EPH REV 1.1 SW846 3510C Percent Solids: nla Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC Page 1 of I File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 NN004852.1) 4 06/03/13 NMC 05/29/13 OP47077 GNN208 Run #2 Initial Volume Final Volume Run #1 1040 ml 2.0 ml Run #2 MAEPH List CAS No. Compound Result RL MDL Units Q 83-32-9 Acenaphthene N❑ 1s 7.7 ugh 208-96-8 Acenaphthylene ND 15 7.7 ugll 120-12-7 Anthracene ND 15 7.7 ugll 56-55-3 Benzo(a)anthracene N❑ 15 7.7 ugll 50-32-8 Benxo(a)pyrene ND 15 7.7 ugll 205-99-2 Benxo(b)fluoranthene ND 15 7.7 ugll 191-24-2 Benxo(g,h,i)peryiene ND 15 7.7 ugll 207-08-9 Benxo(k)fluoranthene ND 15 7.7 ugll 218-01-9 Chrysene ND 15 7.7 ugll 53-70-3 Dibenzo(a,h)anthracene ND 15 7.7 ugll 206-44-0 Fluoranthene N❑ 15 7.7 ugll 86-73.7 Fluorene ND 15 T7 ug1I 193-39-5 Indeno(1,2,3-cd)pyrene N❑ 15 T7 ugll 91-57-6 2-Methylnaphthalene 94.7 15 7.7 ugll 91-20.3 Naphthalene 60.0 15 7.7 ugll 85-01-8 Phenanthrene N❑ 15 7.7 ugli 129-00-0 Pyrene ND 15 7.7 ugll CII-C22 Aromatics (Unadj.} 1500 770 580 ugll CII-C22 Aromatics 1340 770 580 ugA C9-C 18 Aliphatics 3850 770 380 ugll C 19-C36 Aliphatics 1170 770 380 ugll CAS No. Surrogate Recoveries Run# I Run# 2 Limits 3386-33.2 1-Chlorooctadecane 68% 40-140% 580-13-2 2-Bromonaphthalene 73% 40-140% 84-15.1 ❑-Terphenyi 58% 40-140% 321-60-8 2-Fluorobiphenyl 75°% 40-140% ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound A L w ■ _ 80 of 119 E ACCLJTEST. FA4930 ...... """" Accutest LabL!nkP12:12 10-fun-2013 Report of Analysis Client Sample ID: TRIP BLANK Lab Sample ID: FA4930-14 Matrix: AQ - Trip Blank Water Method: 5M 6200B Project: URSNCM: 515 1363, 1101 Hwy 61, Whitsett. NC File ID DF Analyzed By Prep Date Run #1 A0180523.1) 1 06/05/13 TD nla Run #2 Purge Volume Run #1 10.0 ml Run #2 Page I of I A Date Sampled: 05/22/13 A Date Received: 05/23/13 Percent Solids: nla Prep Batch Analytical Batch n/a VA1266 VOA Special List CAS No. Compound Resuh RL MDL Units Q 71-43-2 Benzene ND 0.50 0.10 ugll 75.27-4 Bromodichloromethane ND 0.50 0.10 ugil 107-06-2 1.2-Dichloroethane ND 0.50 0.10 ugll 108-20-3 Di -Isopropyl ether ND 0.50 0.10 ugll 124-48-1 Dibromochloromethane ND 0.50 0.10 ugll 156-59-2 cis-1,2-Dichloroethylene N❑ 0.50 0.10 ugll 100-41-4 Ethylbenzene ND 0.50 0.10 ugll 99-87-6 p-Isopropyltoluene N❑ 0.50 0.10 ugll 74-87-3 Methyl chloride ND 0.50 0.11 ug11 1634.04-4 Methyl Teri Butyl Ether ND 0.50 0.10 ugll 91-20-3 Naphthalene N❑ 0.50 0.15 ugll 108-88-3 Toluene ND 0.50 0.10 ugll 79-01-6 Trichloroethylene ND 0.50 0.10 ugll 1330-20-7 Xylene (total) N❑ 1.5 0.22 ugll CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53.7 Dibromofluoromethane 94% 70-130% 17060-07-0 1.2-Dichloroethane-D4 92% 70.130% 2037-26-5 Toluene-D8 101°% 70-130% 460-00-4 4-Bromofluorobenzene 104% 70-130% ND = Not detected MDL - Method Detection Limit RL = Reporting Limit E = Indicates value exceeds calibration range = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound ■E 81 of 119 w AMMU-reST. FA4930 I "...- .. Section 5 ■ Southeast N ACCUTEEE3T L n D U P A I U H I L i., Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody �i ■ 82 of 119 ACCLITEST. FA4930 `.... e,••• G'I (�A FA4930: Chain of Custody Page 1 of 3 �a 83 of 119 ,caccu��sT FA4930 `"�°........ L.6 NNnr AtCod.LJ iwdw .[ AOdi...: 1101 US "11 WU-M. ORS C V.'M n - NOpx C.mir L.h Ad1� a.a6 WIM A Ra.& SAW C-6- DAVAO. FL =11 4. Sim". xP Cwo yd1R..L INC r�VCwtl6 aw p1q.e Rp. a,an • a115i7H.1DWt Ab PM: Heam11 IWtih Ryii.try Alower mco"m Dwm - DST 5-kk. 111a prYn.41 P.A RWd. Srlw 4W. MWMMS. NC 276H Vl��laD Ab P1wr Q7JNoTOO 4bhr 10 NO AM. Y.VM" N... .6$Nppnq Am Aom-L 162&201" Pnp[M1 NG Op6i9{ga1 911-141.1190 Em . k%.Va M&JSWLOBO f c Lmb 9ar.9r11.L NO: 7inM AipLlu.n 7L OCG4&U _ DOC-AM To: A1r1faW>•LiL..�O. �++ i° ° �"�"�`�` a./u SWW 6a Ka" 61 • OMBAI SPA TO up RP FYgw Mr DIM FARM llittk NO. CpRUDNn I PnOMY611Y1 Fggwmmd Am1y.n PAW Type i OC LMi BF FM ph" 216 2714710 p di 3 S 1i flF � i3s lz �5 t � w SWAW s F LA Dm* PwA.p. — A PY Em.. Cw.p.FObd4op own 26mpM Dl.crlpuon Oid 7rn. CrG1111f1n1• �c1.. L.np1. nM ow,1v. cm►7ro 6rrpr n e0imrr wa Vd.-wr.. w no 5,u1w1 5 xz ; ❑q lol -1 awvwa 1s0 -1 1 1, a Z x SAMY" �315 x fa xI Ix !1 a 2 2 � sAAnu+ 1-x�,ip x ,B x x s 7 2 2 x 10 x Y s 2 a j lU�,r 14 10 x x a a 2 : elp B1rd - L.6 itiVF 9-vw."Vm d>.wL.j Map— IWngMYMd my$ A1mIN{on Od11 Tbm A"plld ByIA}I E&M Orr I Tim S.mp1.r. Cq wvv 11RS C. WA- NW& Cdt*WM 1L14� �] 5 x- 133 C.tsi I hp Nlx mamwd F.dex sm-p Dow ! Shvn T. mwq No' Sp.C411naVucVorl.; R.1., m ~h. a*mOk Kk R.WMi I& m.IJMc.l CQM l Malt. Mry.niM 1019-W-161111.p.idkq 4D mwet. n ipL n1d.O.IF11..1 rW.tp.lomvnu w.p... Tw S LINE -LAB USE ONLY Tvro RWm Yp l%* j Ca T.61ppn FjsoW _,. _-"C Tr4 SL MM e w MSn6SD SO pp. $uhn. Y..I W FA4930: Chain of Custody Page 2 of 3 ■W 84 of 119 m ACCUTEST FA497D•,.- ACCUTPSI'S JOB NUMBER: f A 34:� CLIENT: Ll 9, PROJEcy: 01 3 G 3 DArFrrn►u IR$CIIYED= 5 - Z 3 -13 te_15 {lYH4i1tII)IYY 24:091 NIII�IGII of cooLEB3 RIiCIiIYF�f: � NOETHOD OF DELIVERY: AIRBILL NLiMSiRS: �' UPS ACCUIRST COURIER GREYHOUND DELIVERY OTHER IL Q00LF.R JNEQRN&n0N CUSTODY SEAT. NOT PRESENT OR NOT INTACT CHAIN OF CUSTODY NOT n CYJVKD (COC) ANALYSIS VZQUZSrMD IS UNCLEAR OR MISSING SAMPLE DATES OR 17M S UNCLEAR OR MISSING TEhfPERATURE CRrMUA NOT MET WET ICI; PRESENT TRIP BLANK INFORMATION TRIP BLANK PROVIDED TRIP BLAN K NOT PROVIDED TRIP BLANK NOT ON COC TRIP BLANK INTACT TRIP BLANK NOT INTACT RECEIVED WATERTRIP BLANK RECEIVED SOIL TRIP BLANK MISC.IIYF AMATION NUMBER OF ENCORES? NUMBER OF 5035 FIELD KITS T NUMBER OR LAB FILTERED METALS? SUMMARY OF COMMENTS: TEMPERATUM AVFORMAT- WN M THFRM ID 3 CORK. FACTOR OBSERVED TIMPS: 2• 1.6 •"� �. L CORRECTED TKMPS: 2- L• SAMPLE IIY�ATI�N SAMPLE LABELS PRESENT ON ALL BOTTLES INCORRECT NUMBER.OF CONTAINERS USED SAMPLE RECEIVED IMPROPERLY PRESERVED INSUFFICIENT VOLUME FOR ANALYSIS DATTSITIMES ON COC DO NOT MATCH SAMPLE LABEL TDIS ON CDC DO NOT MATCH LABEL VOC VIALS HAVE READSPACE [MACRO BUBBLES] BOTTLES RECEIVED BUT ANALYSIS NOT RFQU93TED NO BOTTLES RECEIVED FOR ANALYSIS REQUFWM UNCLEAR FILTERING OR COMPOSITING INSTRUCTIONS SAMPLE CONTAUMgS) RECEIVED BROKEN % SOLIDS JAR NOT RECEIVED S035 FIELD Kit FR07XN WITHIN 48 HOUR'S RESIDUAL CHLORINE PRESENT [APPICABLL TO EPA 60 SERIES OR NORTH CAROUNA. ORGAMCSI TECHNICIANSIGNATURIJDATE - 23 3 REVIEWERSIGNATURFIDATE NF 10M9 RECEIPT CONFIRMATION 1DD609 (2)xls FA4934: Chain of Custody Page 3 of 3 85 Of 119 A.CGUT��7 FA4930 Section 6 . Southeast ACCLJTEST L A 8 0 R A T❑ R I L S GUMS Volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries ■ Matrix Spike and Duplicate Summaries M. 86 of 119 ■ .o,CCUTEST FA4930 `........�.. Method Blank Summary Job Numbcr- FA4930 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC Paw, Iof' l Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE835-MB E024404-D 1 06/04/13 TD nla nla VE835 The QC reported here applies to the following samples: Method: SM 6200B FA4930-1, FA4930-2, FA4930-3, FA4930-4, FA4930-5, FA4930-6, FA4930-7, FA4930-11, FA4930.12 CAS NG. Compound Result RL MDL Units Q 71-43.2 Benzene ND 0.50 0.10 ugll 75-27-4 Bromodichloromethane N❑ 0.50 0.10 ugll 107.06-2 1,2-Dichloroethane ND 0.50 0.10 ugll 108-20-3 Di -Isopropyl ether ND 0.50 0.10 ugll 124-48-1 Dibromochloromethane ND 0.50 0.10 ugll 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ugll 100-41-4 Ethylbenzene N❑ 0.50 0.10 ugli 99-87-6 p-Isopropyltoluene ND 0.50 0.10 ugll 74-87-3 Methyl chloride N❑ 0.50 0.11 ugll 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ugll 91-20-3 Naphthalene ND 0.50 0.15 ugll 108-88-3 Toluene N❑ 0.50 0.10 ugll 79-01-6 Trichlornethylene ND 0.50 0.10 11911 1330-20-7 Xylene (total) ND 1.5 0.22 ugll CAS No. Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 98% 70-130% 17060-07-0 1,2-Dichloroethane-D4 99% 70-130% 2037-26-5 Toluene-D8 101°% 70-130% 460-00-4 4-Bromofluorobenzene 101% 70-130°% MIA 87 of 119 a ACCLJTE;r3T. FA4930 ...... 1 1- Meffiod Blank Summary Job Number: FA4930 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC Page I of i Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE836-MB E024430.13 1 06/05/13 TD nla nfa VE836 The QC reported here applies to the following samples: Method: SM 6200B FA4930-7, FA4930-8, FA4930-9, FA4930-10, FA4930-13 CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene N❑ 0.50 0.10 ugA 75.27-4 Bromodichloromethane ND 0.50 0.10 ugll 107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l 108.20.3 Di -Isopropyl ether ND 0.50 0.10 ugll 124-48-1 Dibromochloromethane ND 0.50 0.10 ugA 156-59.2 cis-1,2-Dichloroethylene N❑ 0.50 0.10 ugA 100-41-4 Ethylbenzene ND 0.50 0.10 ugA 99-87-6 p-Isopropyltoluene N❑ 0.50 0.10 ugll 74.87-3 Methyl chloride N❑ 0.50 0.11 ugA 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 119/1 91.20-3 Naphthalene ND 0.50 0.15 ugA 108-88-3 Toluene ND 0.50 0.10 ugA 79-01-6 Trichloroethylene N❑ 0.50 0.10 ugll 1330-20-7 Xylene (total) ND 1.5 0.22 ugll CAS No. Surrogate Recoveries Limits 1868.53-7 Dibromofluoromethane 97°% 70-130°% 17060-07-0 1.2-Dichloroethane-D4 99°% 70-130% 2037-26-5 Toluene-138 102% 70.130°% 460-00-4 4-Bromofluorobenzene 102% 70-130°% m 7" i.� ■d 88 of 119 N ACCLFT-EBT. FA4930 Method Blank Summary Job Number: FA4930 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC Page I of 1 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA1266-MB A0180524.1) 1 06/05/13 TD nla nla VA1266 The QC reported here applies to the following samples: Method: SM 6200B FA4930-14 CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.10 ugli 75-27-4 Bromodichloromethane ND 0.50 0.10 ugll 107-06-2 1,2-Dichloroethane ND 0.50 0.10 ugll 108-20-3 Di -Isopropyl ether ND 0.50 0.10 ugll 124-48-1 Dibromochloromethane ND 0.50 0.10 ugll 156-59-2 cis-1.2-Dichloroethylene N❑ 0.50 0.10 ugll 100-41-4 Ethylbenzene N❑ 0.50 0.10 ugll 99-87-6 p-Isopropyltoluene N❑ 0.50 0.10 ugll 74-87-3 Methyl chloride N❑ 0.50 0.11 ugll 1634-04-4 Methyl Tert Butyl Ether N❑ 0.50 0.10 119/1 91-20-3 Naphthalene ND 0.50 0.15 ugll 108-88-3 Toluene ND 0.50 0.10 ugll 79-01-6 Trichloroethylene ND 0.50 0.10 ugll 1330-20-7 Xylene (total) ND 1.5 0.22 ugll CAS No. Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 96% 70-130% 17060-07.0 1,2-Dichloroethane-D4 97% 70-130% 2037-26-5 Toluene-D8 101% 70-130% 460.00-4 4-Bromofluorobenzene 101% 70-130% ■;m 89 of 119 NACCUTEST. FA4930 ....... - .. Blank Spike Summary Job Number: FA4930 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC Page 1 of 1 ;ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch /E835-13S E024412.1) 1 06/04/13 TD n/a n/a VE835 The QC reported here applies to the following samples: Method: SM 6200B FA4930-1, FA4930-2, FA4930-3, FA4930-4, FA4930-5, FA4930-6, FA4930-7, FA4930-11, FA4930-12 CAS No. Compound 71-43-2 Benzene 75-27-4 Bromodichloromethane 107.06-2 1, 2-Dichluroethane 108-20-3 Di -Isopropyl ether 124-48-1 Dibromochloromethane 156-59-2 cis- 1. 2 -Dichloroethylene 100-41-4 Ethylbenzene 99-87-6 p-Isopropyltoiuene 74-87-3 Methyl chloride 1634-04-4 Methyl Tert Butyl Ether 91-20-3 Naphthalene 108-88-3 Toluene 79-01-6 Trichloroethylene 1330-20-7 Xylene (total) CAS No. Surrogate Recoveries 1868-53-7 ❑ibromofluoromethane 17060-07-0 1, 2-Dichluroethane-D4 2037.26-5 Toluene-D8 460-00-4 4-Bromofluorobenzene " = Outside of Control Limits. Spike BSP BSP ug/I ug/1 % Limits 10 11.2 112 70-130 10 9.7 97 70-130 10 11.2 112 70-130 10 9.3 93 70-130 10 9.6 96 70-130 10 10.3 103 70-130 10 11.1 111 70-130 10 10.2 102 70-130 10 11.2 112 60-140 10 9.1 91 70-130 10 11.3 113 70-130 10 11.0 110 70-130 10 10.4 104 70-130 30 31.5 105 70-130 BSP Limits 101% 70-130% 98% 70-130% 101% 70-130% 104% 70-130% m N su 90 of 119 � AGG lJT'EST. Fn493n Blank Spike Summary Job Number: >~A4930 Account: BPAMSS Atlantic Richfield Company project: URSNCM: SIS 1363, 1101 Hwy 61, Whilsett, NC Page i of 1 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE836-BS E024439-D 1 06/05/13 TD n/a n/a V E836 The QC reported here applies to the following samples: FA4930-7, FA4930-8, FA4930-9, FA4930-10. FA4930-13 Spike BSP BSP CAS No. Compound ug/l ug/l % Limits 71-43-2 Benzene 10 11.0 110 70-130 75-27-4 Bromodichloromethane 10 9.6 96 70-130 107-06-2 1,2-❑ichloroelhane 10 10.8 109 70-130 108-20-3 Di -Isopropyl ether 10 8.9 89 70-130 124-48-1 Dibromochloromethane 10 9.2 92 70-130 156-59-2 cis- 1,2 -Dichloroethylene 10 10.1 101 70-130 100-41-4 Ethylbenzene 10 10.9 109 70-130 99-87-6 p-fsopropyltoluene 10 9.8 98 70-130 74-87-3 Methyl chloride 10 11.5 115 60-140 1634-04-4 Methyl Tert Butyl Ether 10 8.7 87 70-130 91-20-3 Naphthalene 10 10.5 105 70-130 108-88-3 Toluene 10 10.8 108 70-130 79-01-6 Trichloroethylene 10 10.2 102 70-130 1330-20-7 Xylene (total) 30 30.5 102 70-130 CAS No. Surrogate Recoveries BSP Limits 1868-53-7 Dihromofluoromethane 99% 70-130% 17060-07-0 1,2-Dichloroethane-D4 102% 70-130% 2037-26-5 Toluene-D8 100% 70-130% 460-00-4 4-Bromofluorobenzene 101% 70-130% * = Outside of Control Limits. Method: SM 6200B S; - 91 of 119 Ili ACCiJTEST FA493Q .,.....o.... Blank Spike Summary ]oh Number: FA4930 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: SIS 1363, 1101 Hwy 61. Whitsett, NC Page 1 of 1 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA1266-BS A0180525.1) 1 06/05/13 TD nla nla VA1266 The QC reported here applies to the following samples: FA4930-14 Spike BSP BSP CAS No. Compound ugll ugll % Limits 71-43-2 Benzene 10 9.9 99 70.130 75-27-4 Bromodichloromelhane 10 9.4 94 70-130 107-06-2 1,2-Dichloroethane 10 10.5 105 70-130 108-20-3 Di -Isopropyl ether 10 8.6 86 70-130 124-48-1 ❑ibromochloromelhane 10 8.7 87 70-130 156-59-2 cis-1,2-Dichloroethylene 10 9.6 96 70-130 100-41-4 Ethylbenzene 10 10.8 108 70-130 99-87-6 p-Isopropyholuene 10 11.2 112 70-130 74-87-3 Melhyl chloride 10 11.9 119 60-I40 1634-04-4 Melhyl Teri Butyl Ether 10 8.1 81 70-130 91-20-3 Naphthalene 10 10.8 108 70-130 108-88-3 Toluene 10 10.1 101 70-130 79-01-6 Trichloroethylene 10 10.8 108 70-130 1330-20-7 xylene (total) 30 31.3 104 70-130 CAS No. Surrogate Recmeries BSP Limits 1868-53-7 Dibromofluoromelhane 99% 70-130% 17060-07-0 1,2-Dichloroethane-D4 101% 70.130°% 2037-26-5 Toluene-D8 99% 70-130% 460-00-4 4-Bromoiluorobenzene 99% 70-130°% * = Outside of Control Limits. Method: SM 6200B ■R 92 of 119 EA--MUTE=-S"t: FA4930 `.....I` - Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: FA4930 Account: BPAMSS Atlantic Lichfield Company Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC 'ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch A4930-2MS E024410.D 1 06/04/13 TD nla nla VE835 A4930-2MSD E02441I.D 1 06/04/13 TD nla nla VE835 A4930-2 E024406.D 1 06/04/13 TD nla nla VE835 The QC reported here applies to the following samples: Method: SM 6200B FA4930-1, FA4930-2. FA4930-3. FA4930.4, FA4930.5, FA4930.6. FA4930.7, FA4930-11, FA4930-12 CAS No. Compound 71-43-2 Benzene 75-27-4 Bromodichloromethane 107-06-2 1, 2-Dichloroethane 108-20-3 Di -Isopropyl ether 124-48-1 Dibromochloromethane 156-59-2 cis-1,2-Dichloroethylene 100-41-4 Ethylbenzene 99-87-6 p-Isopropylioluene 74-87-3 Methyl chloride 1634-04-4 Methyl Teri Butyl Ether 91-20-3 Naphthalene 108-88-3 Toluene 79-01-6 Trichloroethylene 1330-20-7 Xyfene (to(al] FA4930-2 Spike MS MS MSD MSD Limits ugll Q ugll ugll % ugll % RPD Red"D ND 10 ILI ill 10.8 108 3 70-130120 ND 10 9.2 92 8.9 89 3 70-130120 ND 10 11.1 ill 11.0 110 1 70-130120 ND 10 9.1 91 9.0 90 1 70.130/20 ND 10 8.3 83 8.2 82 1 70-130120 ND 10 10.2 102 10 100 2 70-130120 N❑ 10 10.9 109 10.8 108 1 70-130120 N❑ 10 9.9 99 9.8 98 1 70-130120 ND 10 11.9 119 11.5 115 3 60.140/20 ND 10 9.1 91 9.0 90 1 70-130120 0.74 10 12.1 114 12A 114 0 70-130120 ND 10 10.9 109 10.5 105 4 70-130120 ND 10 10.2 102 9.8 98 4 70-130120 N❑ 30 30.5 102 29.9 100 2 70-130120 CAS No. Surrogate Recoveries MS MSD FA4930-2 Limits 1868-53-7 Dibromofluoromethane 101% 101% 102% 70-130% 17060-07-0 1,2-Dichloroethane-D4 102% 100% 101% 70-130% 2037-26.5 Toluene-D8 100% 100% 99% 70-130% 460-00-4 4-Bromofluorobenzene 102% 100% 100% 70.130% * = Outside of Control Limits. ■E 93 of 119 ACCUTEST FA4930 •"•""T'"•r• Matrix Spike/Matrix Spike Duplicate Summary Page 1 of i Job Number: FA4930 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: S/S 1363. 1101 Hwy 61. Whitsett, NC ;ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch 'A4930-8MS E024441.1) 1 06/05/13 TD n/a n/a VE836 'A4930-8MSD E024442.1) 1 06/05/13 TD n/a n/a VE836 'A4930-8 E024433.1) 1 06/05/13 TD n/a n/a VE836 The QC reported here applies to the following samples: Method: SM 6200B FA4930-7, FA4930-8, FA4930-9, FA4930.10, FA4930-13 FA4930-8 Spike MS MS MSD MSD Limits CAS No. Compound ug/1 Q ug/1 ug/l % ugll % RPD Red"D 71-43-2 Benzene N❑ 10 10.8 108 10.8 108 0 70-130/20 75-27-4 Bromodichloromethane ND 10 9.0 90 8.8 88 2 70-130/20 107-06-2 1,2-Dichloroethane N❑ 10 10.9 109 10.9 109 0 70-130/20 108-20-3 Di -Isopropyl ether ND 10 8.9 89 8.9 89 0 70-130/20 124-48-1 Dibromochloromethane ND 10 8.1 81 8.1 81 0 70-130/20 156-59-2 cis -1,2-D ichloroethylene ND 10 10.0 100 9.9 99 1 70-130/20 100-41-4 Ethylbenzene ND 10 10.8 108 10.8 108 0 70-130/20 99-87-6 p-Isopropyltoluene ND 10 9.6 96 9.8 98 2 70-130/20 74-87-3 Methyl chloride ND 10 12.1 121 11.6 116 4 60-140/20 1634-04-4 Methyl Ter( Butyl Ether 0.48 ] 10 9.3 88 9.4 89 1 70-130/20 91-20-3 Naphthalene ND 10 10.5 105 11.1 111 6 70-130/20 108-88-3 Toluene ND 10 10.7 107 10.6 106 1 70-130/20 79-01-6 Trichloroethylene ND 10 10 100 9.9 99 1 70-130/20 1330-20-7 Xylene (total) ND 30 30.3 101 29.9 100 1 70-130/20 CAS No. Surrogate Recoveries MS MSD FA4930-8 Limits 1868-53-7 Dibromoiluoromethane 100% 99% 98% 70-130% 17060-07-0 1,2-Dirhloroethane-D4 101% 102% 99% 70-130% 2037.26-5 Toluene-D8 101% 101% 101% 70-130% 460-00-4 4-Bromalluorobenzene 101% 102% 103% 70-130% = Outside of Control Limits. ■III 94 of 119 w ACC LJTEST. FA4930 •••�•••�••• Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: FA4930 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC 4imple File ID DF Analyzed By Prep Date Prep Batch Analytical Batcb A5078 4M5 A0180527.1) 10 06/05/13 TD rtla nla VA1266 'A5078-4MSD A0180528.13 10 06/05/13 TD nla nla VA1266 A5078-4 A0180530.1) 10 06/05/13 TD nla nla VA1266 A5078-4 A0180529.D 25 06/05/13 TD nla nla VA1266 The QC reported here applies to the following samples: Method: SM 6200B FA4930-14 FA5078-4 Spike MS MS MSD MSD Limits CAS No. Compound ugll Q ugll ugll % ugll % RPD RecWD 71-43-2 Benzene 21.2 100 122 101 118 97 3 70-130120 75-27-4 Bromodichloromethane N❑ 100 84.5 85 84.0 84 1 70.130/20 107-06.2 1,2-Dichloroethane N❑ 100 105 105 102 102 3 70-130120 108-2.0-3 Di -Isopropyl ether 2.0 ] 100 88.7 87 86.7 85 2 70-130120 124-48-1 Dibromochloromethane ND 100 70.8 71 74.9 75 6 70-130120 156-59.2 cis-1,2-Dichloroethylene ND 100 101 101 97.2 97 4 70-130120 100-41-4 Ethylbenzene 1050 b 100 1110 60* a 1080 30* a 3 70.130/20 99-87-6 p-Isopropyltoluene N❑ 100 110 110 109 I09 1 70-130120 74-87-3 Methyl chloride ND 100 134 134 128 128 5 60-140120 1634-04-4 Methyl Tert Butyl Ether 484 b 100 575 91 565 81 2 70-130120 91-20-3 Naphthalene 305 100 412 107 410 105 0 70.130/20 108-88-3 Toluene 3.1 J 100 107 104 105 102 2 70-130120 79-Ul-6 Trichloroethylene ND 100 111 ill 106 106 5 70.130/20 1330-20-7 Xylene [(otal} 41.8 300 369 109 360 106 2 70-130120 CAS No. Surrogate Recoveries MS MSD FA5078-4 FA5079-4 Limits 1868-53-7 Dibromofiuoromethane 100% 99% 98% 98% 70-130% 17060-07-0 1,2-Dichloroethane-D4 100% 97% I00% 98% 70-130% 2037-26-5 Toluene-D8 102% 101% 102% 101% 70-130% 460-00-4 4-Bromofluorobenzene 98% 99% 99% 100% 70-130% (a) Outside control limits due to high level in sample relative to spike amount. (b) Result is from Run #2. * = Outside of Control Limits. we 95 Of 119 .4CC�1`1^IrST. Section 7 ■ Southeast A C C Li -F E ED- -T" L A B 0 R A T❑ R I E 5 GUMS Semi-volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries ■ Blank Spike Summaries • Matrix Spike and Duplicate Summaries ■ 96 of 119 � ACCLJTEST FA4930 `••�""•"��• Method Blank Summary Job Number: FA4930 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: S/S 1363, 1101 Hwy 61. Whitsett, NC Page 1 of 2 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP47046-MB L063653.D 1 05/28r13 NAF 05/24/13 OP-17046 SL3221 The QC reported here applies to the following samples: Method: EPA 625 V FA4930-1, FA4930-2, FA4930-3, FA4930-4. FA4930-5, FA4930-6, FA4930-7, FA4930-8. FA4930-9, FA4930-10, FA4930-11, FA4930-12, FA4930-13 CAS 1`In. Compo+uad Result RL MDI. Units Q 65-85-0 Benzoic Acid ND 50 10 ugll 95-57-8 2-Chlorophenoi ND 5.0 0.71 ugll 59-50-7 4-Chluro-3-methyl phenol ND 5.0 0.81 ugll 120-83-2 2,4-Dichlorophenol N❑ 5.0 0.70 ugll 105-67-9 2,4-Dimethylphenol ND 5.0 0.77 ugll 51-28-5 2,4-Dinitrophenoi N❑ 25 5.2 ugll 534-52-1 4,6-Dial"-o-cresol ND 10 1.4 ugll 95-48-7 2-Methylphenol N❑ 5.0 0.72 ugll 3&4-Methylphenol ND 5-0 1.4 ugll 88-75-5 2-Nitrophenol ND 5.0 0.68 ugll 100-02-7 4-Nitrophenol ND 25 5.0 ugll 87-86-5 Pentachlorophenol ND 25 5.0 ugll 108-95-2 Phenol ND 5.0 0.55 ugll 88-06-2 2,4,6-Trichiorophenol ND 5.0 0.78 ugll 83-32-9 Acenaphthene N❑ 5.0 0.70 ugll 208-96-8 Acenaphthyiene ND 5.0 0.69 ugll 120-12-7 Anthracene ND 5.0 0.75 ugll 56-55-3 Benzo(a)anthracene N❑ 5.0 0.55 ugll 50-32-8 Benzo (a) pyrene ND 5.0 0.57 ugll 205-99-2 Benxo(h)fluoranthene ND 5.0 0.76 ugll 191-24-2 Benzo(g,h,i)perylene ND 5.0 0.66 ugll 207-08-9 Benzo(k)fluoranthene ND 5.0 0.67 ugll 101-55-3 4-Bromophenyl phenyl ether ND 5.0 0.79 ugll 85-68-7 Butyl benzyl phthalate ND 5.0 0.71 ugll 100.51-6 Benzyl Alcohol ND 5.0 1.0 ugll 91-58-7 2-Chloronaphthalene ND 5.0 0.73 ugll 106-47-8 4-Chloroaniline ND 5.0 0.69 ugli 218-01-9 Chrysene ND 5.0 0.59 ugll 111-91-1 bis(2-Chloroethoxy)methane ND 5.0 0.70 ugll 111-44-4 bis(2-Chloroethyl)ether ND 5.0 0.7Z ugll 108-60-1 bis(2-Chloroisopropyl)eiher ND 5.0 0.79 ugll 7005-7Z-3 4-Chlarophenyl phenyl ether ND 5.0 0.87 ugll 95-50-1 1.2-Dichlorohenzene N❑ 5.0 0.68 ugll 122-66-7 1,2-Diphenylhydrazine N❑ 5.0 0.64 ugll 541-73-1 1,3-Dichlorobenzene ND 5.0 0.78 ugll 106-46-7 1,4-Dichiorobenzene ND 5.0 0.69 ugll 97 of 119 FA4930 "......•... Method Blank Summary Job Number: FA4930 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitselt, NC Page 2 of 2 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP47046-MB L063653.D 1 05/28/13 NAF 05/24/13 OP47046 SL3221 The QC reported here applies to the following samples: Method: EPA 625 FA4930-1, FA4930-2, FA4930-3, FA4930-4, FA4930-5, FA4930-6, FA4930-7, FA4930-8, FA4930-9, FA4930.10, FA4930-11, FA4930.12. FA4930-13 CAS No. Compound Result RL MDL Units Q 91-94-1 3,3'-Dichlorobenzidine N❑ 5.0 0.74 ugll 53-70-3 ❑ibenzo(a,h)anthracene N❑ 5.0 0.58 ugll 132-64-9 Dibenzofuran ND 5.0 0.75 ugll 84-74-2 Di-n-butyl phthalate N❑ 5.0 1.0 ugll 117-84-0 Di-woctyl phthalate ND 5.0 1.0 ugll 84-66-2 Diethyl phthalate N❑ 5.0 1.0 ugll 131-11-3 Dimethyl phthalate ND 5.0 0.81 ugll 117-81-7 his(2-E1hyihexyi)phthalate ND 5.0 1.2 ugll 206-44-0 Fluoranthene ND 5.0 0.59 ugll 86-73-7 Fluorene ND 5.0 0.76 ugll 118-74-1 Hexachlorobenzene ND 5.0 0.69 ugll 87-68-3 Hexachlorobuladiene ND 5.0 0.96 ugll 77-47-4 Hexachlorocyclopentadiene ND 5.0 0.79 ugll 67-72-1 Hexachloroethane N❑ 5.0 0.74 ug/l 193-39-5 Indeno(1,2,3-cd)pyrene ND 5.0 0.57 ugll 78-59-1 Isophorone ND 5.0 0.64 ugll 90-12-0 1-Methylnaphthalene N❑ 5.0 0.70 ugA 91-57-6 2-Methylnaphthalene ND 5.0 0.69 ugll 91.20-3 Naphthalene N❑ 5.0 0.64 ugll 98-95-3 Nitrobenzene ND 5.0 0.72 ugll 621-64-7 N-Nitroso-di-n-propylamine N❑ 5.0 0.85 ugll 86-30-6 N-Nitrosodiphenyiamine ND 5.0 1.0 ugll 85-01-8 Phenanthrene ND 5.0 0.71 ug1l 129-00-0 Pyrene ND 5.0 0.68 ugll 120-82-1 1,2,4-Trichlorobenzene ND 5.0 0.61 ugll CAS No. Surrogate Rewveries Limits 367-12-4 2-Fluorophenol 39% 14-67% 4165.62-2 Phenol-d5 29% 10.50% 118-79-6 2,4,6-Tribromophenol 81% 33.118% 4165-60-0 Nitrobenzene-d5 72% 42-108% 321-60-8 2-Fluorobiphenyl 75% 40-106% 1718-51-0 Terphenyl-d14 76% 39-121% ■■ 98 of 119 W.4CCUTEST. FA4930 ......•• Method Blank Summary Job Number: FA4930 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: SIS 1363, 1101 Hwy 61. Whitsett, NC Page 1 of 2 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ❑P47046-MB L063709.D 1 05/29/13 NAF 05/24/13 CP47046 5L3223 The QC reported here applies to the following samples: Method: EPA 625 FA4930-I, FA4930-2, FA4930-3, FA4930-4, FA4930-5, FA4930-6, FA4930-7, FA4930-8, FA4930-9, FA4930-10, ., FA4930-11, FA4930-12, FA4930-13 iv CAS No. Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 50 10 ugll 95-57-8 2-Chlorophenol N❑ 5.0 0.71 ugll 59-50-7 4-Chloro-3-methyl phenol ND 5.0 0.81 ugll 120-83-2 2,4-Dichlorophenol ND 5.0 0.70 ugll 105-67-9 2,4-Dimethylphenol ND 5.0 0.77 ugll 51-28-5 2,4-Dinitrophenol ND 25 5.2 ugll 534-52-1 4,6-Dinitro-o-cresol ND 10 1.4 ugA 95-48-7 2-Methylphenoi ND 5.0 0.72 ugli 3&4-Methylphenol ND 5.0 1.4 ugA 88-75-5 2-Nitrophenol ND 5.0 0.68 ugll 100-02-7 4-Nitrophenol ND 25 5.0 ugll 87-86-5 Penlachiorophenol ND 25 5.0 ug/l 108-95.2 Phenol ND 5.0 0.55 ugA 88-06-2 2,4,6-Trichlorophenol ND 5.0 0.78 ugA 83.32-9 Acenaphthene ND 5.0 0.70 ugll 208-96-8 Acenaphthylene ND 5.0 0.69 ugll 120.12-7 Anthracene ND 5.0 0.75 ugll 56-55-3 BenzoNanthracene ND 5.0 0.55 ugll 50-32-8 Benzo(a)pyrene ND 5.0 0.57 ugll 205-99-2 Benza(b)fluoranthene ND 5.0 0.76 ugll 191.24-2 Benzo(g,h,i)perylene ND 5.0 0.66 ugll 207-08-9 Benzo (k) fluo rant hene ND 5.0 0.67 ugll 101-55-3 4-Bromophenyl phenyl ether ND 5.0 0.79 ugll 85-68-7 Butyl benzyl phthalate ND 5.0 0.71 ugll 100-51-6 Benzyl Alcohol ND 5.0 1.0 ugll 91-58-7 2-Chloronaphthalene ND 5.0 0.73 ugll 106.47-8 4-Chloroaniline ND 5.0 0.69 ugA 218-01-9 Chrysene N❑ 5.0 0.59 ugll 111-91-1 bis(2-Chloroethoxy)methane ND 5.0 0.70 ugll 111.44-4 bis(2-Chloroe(hyl)ether ND 5.0 0.72 ugll 108-60-1 bis(2-Chloraisopropyl)ether ND 5.0 0.79 ug/l 7005.72.3 4-Chlorophenyl phenyl ether N❑ 5.0 0.87 ugll 95-50-1 1.2-Dichlorobenzene ND 5.0 0.68 ugll 122-66-7 1,2-Diphenyihydrazine ND 5.0 0.64 ugll 541-73-1 1,3-Dichlorobenzene ND 5.0 0.78 ugll 106-46-7 1.4-Dichlorobenzene ND 5.0 0.69 ugll /n 99 of 119 WACCLJTEST. FA493U •••"••,'"•• Method Blank Summary Job Number: FA4930 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: SIS 1363, 1101 Hw_y 61, Whi(sett, NC Page 2 of 2 Sample File ID DF Analyzed By Prep Date Prep Bate Analytical Batch OP47046-MB L063709,1) 1 05/29/13 NAF 05/24/13 ❑P47046 SL3223 The QC reported here applies to the following samples: Method: EPA 625 FA4930-1, FA4930-2, FA4930-3, FA4930-4, FA4930-5, FA4930-6, FA4930-7, FA4930-8, FA4930-9, FA4930-10, FA4930-11, FA4930-12, FA4930-13 N CAS No. Compound Result RL MDL Units Q 15 91-94-1 3,3'-Dichlorobenzidine ND 5.0 0.74 ugll 53-70-3 ❑ibenzo(a,h)anthracene N❑ 5.0 0.58 ugll 132-64-9 Dibenzofuran ND 5.0 0.75 ugll 84-74-2 Di-n-bulyl phthalate N❑ 5.0 1.0 ugll 117-84-0 Di-n-actyl phthalate N❑ 5.0 1.0 ugll 84-66-2 Diethyl phthalate ND 5.0 1.0 ugll 131-11-3 Dimethyl phthalate ND 5.0 0.81 ugll 117-81-7 bis(2-E(hylhexyl}phthalate ND 5.0 I.2 ugll 206-44-0 Fluoranthene ND 5.0 0.59 ugll 86-73-7 Fluorene N❑ 5.0 0.76 ugll 118-74-1 Hexachlorobenzene ND 5.0 0.69 ugll 87-68-3 Hexachlorobuladiene N❑ 5.0 0.96 ugll 77-47-4 Hexachloracyclopentadiene ND 5.0 0.79 ugll 67.72-1 Hexachloroethane ND 5.0 0.74 ugll 193-39-5 Indeno(1.2,3-cd)pyrene ND 5.0 0.57 ugll 78-59-1 Isophorone ND 5.0 0.64 ugll 90-12-0 1-Methylnaphthalene ND 5.0 0.70 ugll 91-57-6 2-Methylnaphthalene N❑ 5.0 0.69 ugll 91-20-3 Naphthalene ND 5.0 0.64 ugll 98-95-3 Nitrobenzene N❑ 5.0 0.72 ugll 621-64-7 N-Nitroso-di-n-propylamine ND 5.0 0.85 ugll 86-30-6 N-Nitrosodiphenylamine ND 5.0 1.0 ugh 85-01-8 Phenanthrene ND 5.0 0.71 ugll 129-00-0 Pyrene ND 5.0 0.68 ugll 120-82-1 1,2,4-Trichlorobenzene ND 5.0 0.61 ugll CAS No. Surrogate Recoveries Limits 367-12-4 2-Fluorophenol 43% 14-67% 4165-62-2 Phenol-d5 29% 10-50% 118-79-6 2,4,6-Tribromophenol 80% 33.118°% 4165.60-0 Nitrobenzene-d5 74% 42.108% 321-60-8 2-Fluorobiphenyl 75% 40-106% 1718-51-0 Terphenyl-d14 77% 39-121% ■■ 100 of 119 O.4CClJTEST. FA4930 `.....I " - Blank Spike Summary Job Number: FA4930 Account: BPAMSS Atlantic Richfield Company Project: IJRSNCM: S1S 1363, 1101 Hwy 61, Whitsett, NC Pale 1 of 2 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ❑P47046 BS L063652.D I 05/28/13 NAF 05/24/13 OP47046 SL3221 The QC reported here applies to the fallowing samples: Method: EPA 625 FA4930-1, FA4930-2, FA4930-3, FA4930-4, FA4930-5, FA4930-6, V FA4930-7, FA4930-8, FA4930-9, FA4930-10, FA4930-11, FA4930-12, FA4930-13 =' Spike BSP BSP CAS No. Compound ugll ug/1 °% Limits 65-85-0 Benzoic Acid 100 18.8 19 10-69 95-57-8 2-Chlorophenol 50 39.3 79 52-98 59-50-7 4-Chloro-3-methyl phenol 50 42.6 85 54-103 120-83-2 2,4-Dichlorophenol 50 43.4 87 53-103 105-67-9 2,4-Dimethylphenol 50 38.3 77 43-90 51.28-5 2,4-Dinitrophenol 100 78.7 79 44-112 534-52-1 4,6-Dinitro-n-cresol 100 93.4 93 66-121 95-48-7 2-Methylphenol 50 33.7 67 43-90 3&4-Methylphenot 100 59.4 59 36-88 88-75-5 2-Nitrophenol 50 42.3 85 53-102 100-02-7 4-Nitrophenol 100 30.9 31 18-62 87-86-5 Pentachlorophenol 100 86.0 86 61-115 108-95-2 Phenol 50 20.3 41 19-56 88-06-2 2,4,6-Trichlorophenol 50 43.2 86 59-107 83-32-9 Acenaphthene 50 43.4 87 61-107 208-96-8 Acenaphthylene 50 45.9 92 60-104 120-12-7 Anthracene 50 44.9 90 65-108 56-55-3 Benzo(a)anthracene 50 43.7 87 66-111 50-32-8 Benzo(a)pyrene 50 40.4 81 62-107 205-99-2 Benzo(b)fluoranthene 50 46.0 92 65-114 191-24-2 Benzo(g,h.i)perylene 50 49.0 98 66-116 207-08-9 Benzo(k)fluoranthene 50 44.8 90 65-1I4 101-55-3 4-Bromophenyl phenyl ether 50 44.9 90 65-109 85-68-7 Butyl benzyl phthalate 50 45.3 91 65-112 100-51-6 Benzyl Alcohol 50 36.1 72 46-94 91-58-7 2-Chloronaphthalene 50 42.9 86 57-103 106-47-8 4-Chloroaniline 50 39.9 80 49-105 218-01-9 Chrysene 50 43.4 87 66-111 111-91-1 his(2-Chloroelhoxy)methane 50 42.8 86 51-102 111-44-4 bis(2-Chloroe(hyl)ether 50 40.4 81 53-100 108-60-1 his(2-Chloroisopropyl)ether 50 40.2 80 45-106 7005-72-3 4-Chlorophenyl phenyl ether 50 46.3 93 62-105 95.50-1 1,2-Dichlorobenzene 50 37.4 75 48-97 122-66-7 1,2-Diphenyihydrazine 50 44.4 89 61-110 541-73-1 1,3-Dichlorobenzene 50 36.9 74 45-95 106-46-7 1,4-Dichlorahenzene 50 37.8 76 45.98 * = Outside of Control Limits. 101 of 119 ■ .o.0 c u�-�s� FA4930 Blank Spike Summary Job Number: FA4930 Account: BPAMSS Atlantic Richfield Company Project: LIRSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC Page 2 of 2 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP47046-BS L063652.1) 1 05/28/13 NAF 05/24/13 OP47046 SL3221 The QC reported here applies to the following samples: Method: EPA 625 FA4930-1, FA4930-2, FA4930-3, FA4930-4, FA4930-5, FA4930-6, FA4930-7, FA4930-8, FA4930-9, FA4930-10, FA4930.11, FA4930-12, FA4930-13 Spike BSP BSP CAS No. Compound ugli ugll % Limits 91-94-1 3,3'-Dichlorobenzidine 50 39.7 79 46-117 53-70-3 Dibenzo(a,h)anthracene 50 48.4 97 66-119 132-64-9 ❑ibenzofuran 50 44.6 89 61-106 84-74-2 Di-n-butyl phthalate 50 44.5 89 65-107 117-84-0 Di-n-octyl phthalate 50 49.7 99 62-118 84-66-2 Diethyl phthalate 50 45.4 91 64-108 131-11-3 Dimethyl phthalate 50 45.1 90 63-106 117-81-7 bis(2-Ethylhexyl)phthalate 50 44.9 90 61-117 206-44-0 Fluoranthene 50 44.7 89 63-106 86-73-7 Fluorene 50 43.9 88 62-108 118-74-1 Hexachlorobenzene 50 43.3 87 63-108 87-68-3 Hexachlorobuladiene 50 40.7 81 42-102 77-47-4 Hexachlorocyclopentadiene 50 33.9 68 39-102 67-72-1 Hexachloroethane 50 36.8 74 42-100 193-39-5 Indeno(1,2,3-cd)pyrene 50 48.7 97 64-119 78-59-1 Isophorone 50 36.3 73 43-87 90-12-0 1-Methylnaphthalene 50 44.7 89 53-102 91-57-6 2-Methylnaphthalene 50 43.5 87 51-102 91-20-3 Naphthalene 50 42.8 86 47-100 98-95-3 Nitrobenzene 50 43.7 87 50-104 621-64-7 N-Nitroso-di-n-propylamine 50 42.1 84 52-104 86-30-6 N-Nitrosodiphenylamine 50 44.0 88 64-108 85-01-8 Phenanthrene 50 46.0 92 66-110 129-00-0 Pyrene 50 44.9 90 64-113 1.20-82.1 1,2,4-Trichlorobenzene 50 40.7 81 45-97 CAS No. Surrogate Recoveries BSP Limits 367-12-4 2-Fluorophenol 49% 14-67% 4165-62-2 Phenol-d5 35% 10-50% 118-79-6 2,4,6-Tribromophenol 83% 33-118% 4165-60-0 Nitrohenzene-6 82% 42-108% 321-60-8 2-Fluorobiphenyl 87% 40-106% 1718-51-0 Terphenyl-d14 93% 39-121% * = Outside of Control Limits. ■4 102 of 119 E ACCUTEST. FA4930 `•`�•••�,.•• Matrix Spike/Matrix Spike Duplicate Summary Job Number: FA4930 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: SIS 1363, 1101 Hwy 61. Whitsett, NC Page 1 of 2 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ❑P47046-MS 1-063719.1) 1 05/29/13 NAF 05/24/13 OP47046 SL3223 OP47046-MSD L063720.D 1 05/29/13 NAF 05/24/13 OP47046 SL3223 FA4930-8 L063718.1) 1 05/29/13 NAF 05/24/13 OP47046 SL3223 The QC reported here applies to the following samples: Method: EPA 625 FA4930-1, FA4930-2, FA4930-3, FA4930-4, FA4930-5, FA4930-6, FA4930-7, FA4930-8, FA4930-9, FA4930-10, FA4930-11, FA4930-12, FA4930-13 FA4930-8 Spike MS MS MSD MSD Limits CAS No. Compound ug/l Q ugll ugll % ug/l % RPD Red"D 65-85-0 Benzoic Acid ND 192 122 63 123 64 1 10-69139 95-57-8 2-Chlorophenol ND 96.2 77.4 80 82.8 86 7 52.98/25 59-50-7 4-Chloro-3-methyl phenol ND 96.2 84.1 87 88.1 92 5 54-103123 120-83-2 2,4-Dichlorophenol ND 96.2 81.8 85 86.3 90 5 53.103/26 105-67-9 2,4-DimethylphenoI ND 96.2 69.6 72 72.8 76 4 43-90127 51-28-5 2,4-Dinitrophenol N❑ 192 168 87 165 86 2 44-112125 534-52-1 4,6-Dinitro-o-cresol ND 192 201 105 202 105 0 66-121123 95.48.7 2-Melhylphenol N❑ 96.2 71.5 74 77.6 81 8 43-90128 3&4-Methylphenol ND 192 131 68 142 74 8 36-88/28 88-75-5 2-Nitrophenol N❑ 96.2 80.3 84 86.0 89 7 53-102129 100-02-7 4-Nitrophencl ND 192 115 60 116 60 1 18-62133 87.86-5 Pentachlorophenol ND 192 186 97 187 97 1 61-115126 108-95-2 Phenol ND 96.2 51.7 54 57.5 60• 11 19-56135 88-06-2 2.4,6-Trichlorophenol ND 96.2 86.3 90 87.2 91 1 59-107123 83-32-9 Acenaphthene ND 96.2 83.8 87 85.9 89 2 61-107122 208-96-8 Acenaphthylene ND 961 86.4 90 88.3 92 2 60-104122 120-12-7 Anthracene N❑ 96.2 85.8 89 87.7 91 2 65-108120 56-55-3 Benzo(a)anthracene ND 96.2 90.0 94 90.7 94 1 66-111122 50-32-8 Benzo(a)pyrene N❑ 96.2 82.5 86 82.2 85 0 62.107/23 205-99-2 Benzo(b)fluoranthene ND 96.2 89.7 93 93.1 97 4 65-114123 191-24-2 Benzo(g,h,i)perylene ND 96.2 100 104 96.9 101 3 66-116123 207-08-9 Benzo(k)flueranthene ND 96.2 95.1 99 95.2 99 0 65-114124 101-55-3 4-Bromophenyl phenyl ether ND 96.2 88.1 92 90.3 94 2 65-109123 85-68-7 Butyl henzyl phthalate ND 96.2 92.7 96 93.1 97 0 65-112124 100-51-6 Benzyl Alcohol ND 96.2 80.0 83 88.1 92 10 46.94127 91-58-7 2-Chloronaphihalene ND 96.2 82.2 85 83.8 87 2 57-103123 106-47-8 4-Chloroaniline ND 96.2 70.4 73 72.5 75 3 49-105127 218-01-9 Chrysene ND 96.2 89.6 93 88.8 92 1 66-111122 111-91-1 bis(2-Chloroethoxy)methane ND 96.2 83.2 87 88.2 92 6 51-102128 111-44.4 bis(2-Chloroethyl)ether N❑ 961 78.7 82 83.6 87 6 53-100127 108-60-1 bis(2-Chloroisopropyl)ether ND 96.2 75.0 78 79.8 83 6 45-106126 7005-72-3 4-Chlorophenyl phenyl ether ND 96.2 87.7 91 89.1 93 2 62-105120 95-50.1 1,2-Dichlorobenzene N❑ 96.2 77.1 80 82.4 86 7 48-97124 122-66-7 1,2-Dipheny1h-ydrazine ND 96.2 89.9 93 95.0 99 6 61-110124 541-73-1 13-Dichlorohenxene ND 96.2 75.2 78 79.2 82 5 45-95125 106.46.7 1,4-Dichlorobenzene ND 96.2 75.2 78 80.1 83 6 45-98125 * = Outside of Control Limits. ■ia 103 of 119 ■.accuT��T FA4930 •,•"•,•�• �• Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2 Job Number: FA4930 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: SIS 1363, 1101 Hwy 61. Whitselt, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ❑P47046-MS L063719.1) 1 05/29/13 NAF 05/24/13 OP47046 SL3223 OP47046-MSD 1-063720.1) 1 05/29/13 NAF 05/24/13 OP47046 SL3223 FA4930-8 L063718.1) 1 05/29/13 NAF 05/24/13 OP47046 SL3223 The QC reported here applies to the following samples: Method: EPA 625 FA4930-1, FA4930-2, FA4930-3, FA4930-4, FA4930-5, FA4930-6, FA4930-7, FA4930-8, FA4930-9, FA4930-10, FA4930-11, FA4930-12, FA4930.13 FA4930-8 Spike MS MS MSD MSD Limits CAS No. Compound ugll Q ugli ngll % ugll % RPD Rec/RPD 91.94-1 3,3'-Dichlorobenzidine ND 96.2 63.3 66 63.7 66 1 46-117129 53-70-3 ❑ibenxo(a,h)anthracene N❑ 96.2 96.4 100 93.8 98 3 66-119124 132-64-9 ❑ibenzofuran N❑ 96.2 85.5 89 89.7 93 5 61-106/21 84-74-2 Di-n-butyl phthalate ND 96.2 90.2 94 91.8 95 2 65.107/21 117-84-0 Di-n-octyl phthalate N❑ 96.2 96.6 100 96.0 100 1 62-118124 84-66-2 Diethyl phthalate ND 96.2 90.8 94 91.1 95 0 64-108121 131-11-3 Dimethyl phthalate ND 96.2 88.8 92 89.3 93 1 63-106122 117-81-7 bis(2-Ethylhexyl)phthalale ND 96.2 93.6 97 91.2 95 3 61-117123 206-44-0 Fluoranthene ND 96.2 86.5 90 90.6 94 5 63-106121 86-73-7 Fluerene ND 96.2 83.9 87 85.6 89 2 62.108/20 118-74-1 Hexachiorober►zene ND 96.2 87.6 91 91.3 95 4 63-108122 87-68-3 Hexachlorobutadiene ND 96.2 78.2 81 84.6 88 8 42.102/28 77-47-4 Hexachlorocyclopenladiene ND 96.2 76.6 80 75.3 78 2 39-102129 67-72-1 Hexachloroethane ND 96.2 76.0 79 81.0 84 6 42.100/29 193-39-5 Indeno[1,2,3-cd)pyrene ND 96.2 95.2 99 93.3 97 2 64-119124 78-59-1 Isophorone ND 96.2 70.9 74 74.4 77 5 43.87/25 90-12-0 1-Methylnaphihalene N❑ 96.2 83.6 87 91.2 95 9 53-102127 91-57-6 2-Melhylnaphihalene ND 96.2 83.9 87 89.8 93 7 51-102126 91-20-3 Naphthalene N❑ 96.2 82.0 85 85.8 89 5 47-100129 98-95-3 Nitrobenzene N❑ 96.2 83.4 87 87.5 91 5 50-104128 621-64-7 N-Nitroso-di-n-propylamine ND 96.2 82.1 85 87.8 91 7 52-104125 86-30-6 N-Nilrosodiphenylamine ND 96.2 90.0 94 91.0 95 1 64-108123 85-01-8 Phenanthrene ND 96.2 90.3 94 91.1 95 1 66-110121 129-00-0 Pyrene N❑ 96.2 89.7 93 88.9 92 1 64-113123 120-82-1 1,2.4-Trichlorobenzene ND 96.2 79.2 82 84.4 88 6 45-97128 CAS No. Surrogate Recoveries MS MSD FA4930-8 Limits 367-12-4 2-Fluorophenol 63% 71%* 32% 14-67% 41.65-62-2 Phenol-d5 50% 57%* 23% 10-50% 118-79-6 2,4,6-Tribromophenol 90% 92% 88% 33-118% 4165-60-0 Nitrobenzene-6 82% 87% 72% 42-108% 321-60-8 2-Fluorobiphenyl 84% 88% 75% 40-106% 1718.51-0 Terphenyl-d14 98% 96% 67% 39-121% * _ Outside of Control Limits. ■Rl! 104 of 119 �.ACCLJTEST. Section 8 . Southeast E ACCUTEST L AO OR AT OR I ES GC Volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries ■ Blank Spike Summaries • Matrix Spike and Duplicate Summaries a ■ 105 of 119 1♦accuT��-r FA4930 Method Blank Summary Job Number: FA4930 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC Page 1 of 1 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GUU178-MB UU003546.D1 06/04/13 MM nla nla GUU178 The QC reported here applies to the following samples: Method: MADEP VPH REV L I FA4930-1, FA4930-2, FA4930-3, FA4930-8, FA4930-9, FA4930-10, FA4930-11 CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 1.0 1.0 ugll 100-41-4 Ethylhenzene ND 2.0 1.0 u9/1 1634.04-4 Methyl Teri Butyl Ether ND 2.0 1.0 ugll 91-20-3 Naphthalene ND 5.0 3.0 ugll 108-88-3 Toluene ND 2.0 1.0 ugll m,p-Xylene N❑ 4.0 2.0 ugA 95-47-6 o-Xylene N❑ 2.0 1.0 ugll C5- C8 Aliphatics (Unadj.) N❑ 100 35 ugll C9- C 12 Aliphatics (Unadj.) N❑ 100 35 ugll C9- CIO Aromatics (Unadj.) N❑ 100 35 ugll C5- C8 AIiphatics ND 100 35 ugll C9- C12 Aliphatics ND 100 35 ugll C9- C10 Aromatics ND 100 35 ugll CAS No. Surrogate Recoveries Limits 460-00-4 BFB 74% 70.130% 460-00-4 BFB 76% 70-130% ■■ 106 of 119 ACC u-rs3T FA4930 ...... — ". Method Blank Summary Job Number: FA4930 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC Page 1 of 1 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch CUU179-MB UU003578,D 1 06/05/13 MM nla nla GUU179 The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 FA4930-4, FA4930-5, FA4930-6, FA4930-7, FA4930-12, FA4930-13 CAS No. Compound Result RL MDL [faits Q 71-43-2 Benzene ND 1.0 1.0 ugll 100-41-4 Ethylhenxene ND 2.0 1.0 ugll 1634-04-4 Methyl Tert Butyl Ether ND 2.0 1.0 ugll 91-20-3 Naphthalene ND 5.0 3.0 ugll 108-88-3 Toluene ND 2.0 1.0 ugll m,p-Xylene ND 4.0 2.0 ugli 95-47-6 ❑-Xylene ND 2.0 1.0 ugll C5- C8 Aliphatics (Unadj.) ND 100 35 ugll C9- C12 Aliphatics (Unadj.) N❑ 100 35 ugll C9- C10 Aromatics (Unadj.) ND 100 35 ugll C5- C8 Aliphatics N❑ 100 35 ugli C9- C12 Aliphatics ND 100 35 ugll C9- CIO Aromatics N❑ 100 35 ugll CAS No. Surrogate Recoveries Limits 460-00-4 BFB 98% 70-130% 460-00-4 BFB 100% 70-130% ■ 107of119 ■.acuu�-�s-r. FA4930 ••,'•••`• " Method Blank Summary Job Number: FA4930 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: S/S 1363. 1101 Hwy 61, Whitsett, NC Page 1 of 1 Sample File ID DF Analy� By Prep Date Prep Batch Analytical Batch GUU181-MB UU003625.D1 06/06/13 MM nla nla CUU181 The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 FA4930-7. FA4930-13 ao CAS No. Compound Result RL MDL Units Q 91-20-3 Naphthalene N❑ 5.0 3.0 ugll ��!! C9- C12 Aliphatics (Unadj.) ND 100 35 ugll C9- CIO Aromatics (Unadj.) ND 100 35 ugll C9- C 12 Aliphatics ND 100 35 ugll C9- C10 Aromatics ND 100 35 ugll CAS No. Surrogate Recoveries Limits 460-00-4 BFB 103% 70-130% 460-00-4 BFB 9D% 70-130% ■1 108 of 119 ■.o.ccu-rE=-sr. Blank SpikdBlank Spike Duplicate Summary Job Number: FA4930 Account: BPAMSS Atlantic Richfield Company Projed: URSNCM: S/S 1363, 1101 Hwy 61, Whitsett, NC Page 1 of 1 ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batet :UU178-BS UU003544.D1 06/04/13 MM nla nla GUU178 ;UU178-BSD UU003545.D1 06/04/13 MM nla nla GUU178 The QC reported here applies to the foilow'sng samples: Method: MADEP VPH REV 1.1 FA4930-1, FA4930-2, FA4930-3, FA4930-8, FA4930-9, FA4930-10, FA4930-11 Spike BSP BSP BSD BSD Limits ao iv CAS No. Compound ugll ugll % ugll % RPD Rco'RPD ' 71-43-2 Benzene 80 81.5 102 81.9 102 0 70.130/25 100-41-4 Ethylhenzene 80 78.7 98 79.4 99 1 70.130/25 1634-04-4 Methyl Teri Butyl Ether 80 89.2 112 86.6 108 3 70-130125 91-20-3 Naphthalene 80 72.2 90 70.5 88 2 70.130/25 108-88-3 Toluene 80 81.2 102 80.5 101 1 70-130125 m,p-Xylene 160 154 96 155 97 1 70.130/25 95-47-6 o-Xylene 80 80.1 100 80,9 101 1 70-130125 C5- C8 Aliphatics (Unadj.) 240 253 105 239 100 6 70-130125 C9- C12 Aliphatics (Unadj.) 160 143 89 142 89 1 70.130/25 C9- C10 Aromatics (Unadj.) 80 77.9 97 78.4 98 1 70-130125 CAS No. Surrogate Recoveries BSP BSD Limits 460-00-4 BFB 109% 110% 70-130% 460-00.4 BFB 104% 106% 70-130% * = Outside of Control Limits. ■o 109 of 119 ■ .o.ccu-rtrS-T. FA4930 ,-o" I-- Blank Spike/Blank Spike Duplicate Summary Job Number: FA4930 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: 51S 1363, 1101 Hwy 61, Whitsett, NC Page 1 of 1 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch CUU179-BS UU003575.D1 06/05/13 MM nla nla GUU179 GUU179-BSD UU003576.D1 06/05/13 MM nla nla GUU179 The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 FA4930-4. FA4930-5, FA4930-6, FA4930-7, FA4930-12, FA4930-13 Spike BSP BSP BSD BSD Limits CAS No. Compound ugll ugll % ugll % RPD Red"D N 71-43-2 Benzene 80 83.0 104 84.2 105 1 70-130125 100-41-4 Ethylbenzene 80 79.2 99 78.7 98 1 70-130125 1634-04-4 Methyl Tert Butyl Ether 80 89.9 112 90.1 113 0 70-130125 91-20-3 Naphthalene 80 74.4 93 74.4 93 0 70-130125 108-88-3 Toluene 80 81.6 102 82.4 103 1 70-130125 m,p-Xylene 160 154 96 153 96 1 70-130125 95-47-6 o-Xylene 80 79.6 100 79.3 99 0 70-130125 C5- C8 Aliphatics (Unadj.) 240 270 113 258 108 5 70-130125 C9- C12 Aliphatics [Unadj.] 160 150 94 145 91 3 70-130125 C9- C10 Aromatics (Unadj.) 80 77.4 97 76.9 96 1 70-130125 CAS No. Surrogate Recoveries BSP BSD Limits 460-00-4 BFB 113% I15% 70-130% 460-00-4 BFB 108% 110% 70-130% * = Outside of Control Limits. Elm 110 Of 119 w ACCUTEST: FA030 `•"�,,•••••• Blank Spike/Blank Spike Duplicate Summary Job Number: FA4930 Account; BPAMSS Atlantic Richfield Company Project: URSNCM: S(S 1363, 1101 Hwy 61, Whitsett, NC Page 1 of 1 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch CUU181-BS UU603623.D1 06/06/13 MM nla nla GUU1S1 GUU181-BSD UU003624.D1 06/06/13 MM nla nla GUU181 The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 FA4930-7. FA4930-13 Spike BSP BSP BSD BSD Limits 00 CAS No. Compound ugll ugh % ug/l % RPD Red"D 91-20-3 Naphthalene 80 86.1 108 78.1 98 10 70-130125 C9- C12 Aliphatics (Unadj.) 160 124 78 115 72 8 70-130125 C9- C10 Aromatics (Unadj.) 80 78.5 98 76.3 95 3 70-130125 CAS No. Surrogate Recoveries BSP BSD Limits 460-00-4 BFB 109% 112% 70-130% 460-00-4 BFB 103% 105% 70-130% " = Outside of Control Limits. E■ 111 of 119 FA4930 .... Duplicate Summary Job Number: FA4930 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: SIS 1363. 1101 Hwy 61, Whilsett. NC Page 1 of 1 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Hatch FA4930-IODUP UU003571-D1 06/05/13 MM nla nla GUU178 FA4930.10 UU00355LD1 06/04/13 MM nla nla GUU178 The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 FA4930-1. FA4930-2, FA4930-3. FA4930-9, FA4930-10, FA4930-11 FA4930-10 DUP CAS No. Compound ugll Q ugll 71-43-2 Benzene ND N❑ 100-41-4 Ethylbenzene ND ND 1634-04-4 Methyl Teri Butyl Ether 9.7 10.5 91-20-3 Naphthalene N❑ N❑ 108-88-3 Toluene ND ND m,p-Xylene N❑ ND 95.47.6 o-Xylene N❑ ND C5- C8 Aliphatics (Unadj.) N❑ ND C9- C12 Aliphatics (Unadj.) ND ND C9- C10 Aromatics (Unadj.) ND ND C5- C8 Aliphatics N❑ ND C9- C12 Aliphatics ND ND C9- CIO Aromatics ND ND CAS No. Surrogate Recoveries 460.00-4 BFB 460.00-4 BFB * = Outside of Control Limits. Q RPD Limits nc 50 nc 50 8 50 nc 50 nc 50 TIC 50 nc 50 nc 50 nc 50 nc 50 nc 50 nc 50 nc 50 DUP FA4930-10 Limits 95% 89% 70-130% 96% 89% 70-130% ■ 112 of 119 ■QccLJTES r Duplicate Summary Job Number: FA4930 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: S/S 1363, 1101 Hwy 61, Whitsett, NC Page 1 of 1 Sample File ID DF Analyzed By Prep Date Prep Bath Analytical Batch FA5113-12DUP UU003600.1)1 06/06/13 MM nla nla GUU179 FA5113-12 a UU003599.D1 06/06/13 MM nla nla GUU179 The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 FA4930.4, FA4930-5, FA4930-6, FA4930-7, FA4930-12, FA4930-13 FA5113-12 DUP CAS No. Compound ugll Q ugll Q RPD Limits 71-43-2 Benzene ND ND nc 50 100-41-4 Ethylhenzene ND ND nc 50 1634-04-4 Methyl Teri Butyl Ether ND ND nc 50 91-20-3 Naphthalene ND ND nc 50 108-88-3 Toluene ND ND nc 50 m.p-Xylene ND ND nc 50 95-47.6 o-Xylene ND ND nc 50 C5- C8 Aliphatics (Unadj.) ND ND nc 50 C9- C12 Aliphatics (Unadj.) ND ND nc 50 C9- C10 Aromatics (Unadj.) ND ND nc 50 C5- CS Aliphatics ND ND nc 50 C9- C12 Aliphatics ND ND nc 50 C9- C10 Aromatics ND ND nc 50 CAS No. Surrogate Recoveries DUP FA5113-12 Limits 460-00.4 BFB 117% 120% 70-130% 460-00.4 BFB 105% 107% 70-130% (a) Confirmation run. * = Outside of Control Limits. M■ 113 of 119 ACMU-rEST. FA4930 Duplicate Summary Job Number: FA4930 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: SIS 1363, 1101 Hwy 61, Whitsett, NC Page 1 of 1 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA4930-8DUP UU003627.131 06/06/13 MM Wa nla GUU178 FA4930-8 UU003547.D1 06/04/13 MM nla nla GUU178 The QC reported here applies to the following samples: FA4930-8 Method: MADEP VPH REV 1.1 FA4930-8 DUP CAS No. Compound ugll Q ugll Q RPD Limits 71-43-2 Benzene ND ND ac 50 100-41-4 Ethylbenzene ND ND nc 50 1634-04-4 Methyl Teri Butyl Ether ND ND nc 50 91-20-3 Naphthalene ND ND ac 50 108-88-3 Toluene ND ND nc 50 m, p-Xylene ND ND nc 50 95-47-6 o-Xylene ND N❑ nc 50 C5- C8 Aliphatics (Unadj.) ND ND nc 50 C9- C12 Aliphatics (Unadj.) ND ND nc 50 C9- C10 Aromatics (Unadj.) ND ND nc 50 C5- C8 Aliphatics N❑ ND nc 50 C9- C12 Aliphatics N❑ N❑ ac 50 C9- CIO Aromatics N❑ ND nc 50 CAS No. Surrogate Recoveries DUP FA4930-8 Limits 460-00-4 BFB 106% 85% 70-130% 460.00-4 BFB 95% 85% 70-130% " = Outside of Control Limits. �- 114 of 119 ACCLITE=S7 FnasSo ........... " Duplicate Summary Job Number: FA4930 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: SIS 1363. 1101 Hwy 61, VAdisett. NC Page 1 of 1 Sample File 1D DF Analyzed By Prep Date Prep Batch Analytical Batch FA5164-12DUP UU003651.D1 06/07/13 MM n1a nla GUU181 FA5164-12 UU003650.131 06/07/13 MM nla nla GUU181 The QC reported here applies to the following samples: FA4930-7. FA4930-13 FA5164-12 DUP CAS No. Compound ugll Q ugll 91-20-3 Naphthalene 11.3 12.3 C9- C12 Aliphatics [Unadj.] 49.6 j 46.2 C9- C10 Aromatics (Unadj.) 120 119 C9- C12 Aliphatics ND ND C9- CIO Aromatics 120 119 CAS No. Surrogate Recoveries 460-00.4 BFB 460-00-4 BFB * = Outside of Control Limits. Method: MADEP VPH REV 1.1 Q RP❑ Limits 8 50 1 7 50 1 50 nc 50 1 50 DUP FA5164-12 Limits 108% 111% 70-130% 101% 106% 70-130% M& 115 of 119 ■ A,0MLJTES-r FA4930 "....I ... Section 9 . Southeast W ACCUTEE3T L A B O RAT OR I E S GC Semi-volatiles QC Data Summaries Includes the following where applicable: ■ Method Blank Summaries • Blank Spike Summaries ■ Matrix Spike and Duplicate Summaries I: ■ 116 of 119 ■ cu--i-=sT FA4930 Method Blank Summary Job Number: FA4930 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: S/S 1363, 1101 Hwy 61. Whitset(, NC Page 1 of l ample File ID DF Analyzed By Prep Date Prep Batch Analytical Bawl: )P47077-MB NN004791.D1 05/31/13 NMC 05/29/13 OP47077 GNN207 The QC reported here applies to the following samples: Method: MADEP EPH REV 1.1 FA4930.1. FA4930-2. FA4930-3, FA4930-4, FA4930-5, FA4930-6, FA4930-7, FA4930-8, FA4930-9, FA4930-10, FA4930-11, FA4930-12, FA4930-13 CAS No. Compound Result RL MDL Units Q 83-32-9 Acenaphthene N❑ 4.0 2.0 ugll 208-96-8 Acenaphthylene N❑ 4.0 2.0 ugll 120-12-7 Anthracene N❑ 4.0 2.0 ugll 56-55-3 Benzo(a)anthracene N❑ 4.0 2.0 ugll 50-32-8 Benzo(a)pyrene ND 4.0 2.0 ugll 205-99-2 Benxo(b)lluoranthene N❑ 4.0 2.0 ugll 191-24-2 Benzo(g,h,i)perylene ND 4.0 2.0 ugll 207-08-9 Benzo(k)fluoranthene N❑ 4.0 2.0 ugll 218-01-9 Chrysene N❑ 4.o 2.0 ugll 53-70-3 ❑ibenxo(a,h)anthracene ND 4.0 2.0 ugll 206-44-0 Fluoranthene ND 4.0 2.0 ugll 86-73-7 Fluorene ND 4.0 2.0 ugll 193-39-5 lndeno(1,2.3-cd)pyrene ND 4.0 2.0 ugll 91-57-6 2-Methylnaphthalene ND 4.0 2.0 ugll 91-20-3 Naphthalene ND 4.0 2.0 ugll 85-01-8 Phenanthrene ND 4.0 2.0 ugll 129-00-0 Pyrene ND 4.0 2.0 ugll C11-C22 Aromatics (Unadj.) ND 200 150 ugll C11-C22 Aromatics ND 200 150 ugll C9-C18 Aliphatics ND 200 100 ugll C19-C36 Aliphatics N❑ 200 100 ugll CAS No. Surrogate Recoveries Limits 3386-33-2 1-Chloroociadecane 65% 40-140% 580.13.2 2-Bromonaphthalene 76% 40.140% 84-15-1 o-Terphenyl 60% 40-140% 321-60-8 2-Fluorobiphenyi 78% 40.140% ■■ 117 of 119 wACCLITEST. FA4930 Blank Spike(Blank Spike Duplicate Summary Job Number: FA4930 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: SIS 1363, 1101 Hwy 61. Whitsetl, NC Page 1 of 1 ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch )P47077-BS NN004789.D 1 05/31/13 NMC 05/29/13 OP47077 GNNZ07 1P47077-BS❑ NN004790.D 1 05/31/13 NMC 05/29/13 OP47077 GNN207 The QC reported here applies to the following samples: Method: MADEP EPH REV 1.1 FA4930-1, FA4930-2. FA4930-3, FA4930-4, FA4930-5, FA4930-6, FA4930.7, FA4930-8. FA4930-9, FA4930.10, FA4930-11, FA4930-12, FA4930-13 Spike BSP BSP BSD BSD Limits CAS No. Compound ugll ugll % ug/1 % RPD Rer1RPD 83-32-9 Acenaphthene 100 60.7 61 57.5 58 5 40-140130 208-96-8 Acenaphthylene 100 57.6 58 55.0 55 5 40.140/30 120-12-7 Anthracene 100 66.6 67 62.9 63 6 40-140/30 56-55-3 Benzo(a)anthracene 100 69.3 69 66.0 66 5 40-140130 50-32-8 Benzo(a]pyrene 100 70.7 71 67.8 68 4 40.140/30 205-99-2 Benzo(b)fluoranthene 100 70.5 71 67.3 67 5 40-140130 191-24-2 Benzo(g,hJ)peryIene 100 72.9 73 70.7 71 3 40-140130 207-08-9 BenzoNfluoranthene 100 69.4 69 67.2 67 3 40-140130 218-01-9 Chrysene 100 66.6 67 63.4 63 5 40-140130 53-70-3 Dibenzo[a,h]anthracene 100 71.7 72 69.7 70 3 40-140130 206-44-0 Fluoranthene 100 67.9 68 64.3 64 5 40-140130 86-73-7 Fluorene 100 62.6 63 59.3 59 5 40-140130 193-39-5 Indeno(1,2,3-cd)pyrene l00 72.2 72 70.2 70 3 40-140130 91-57-6 2-Methylnaphthalene 100 54.9 55 52.2 52 5 40-140130 91-20-3 Naphthalene 100 51.5 52 49.1 49 5 40-140130 85-01-8 Phenanthrene 100 66A 66 63.2 63 5 40-140130 129-00-0 Pyrene 100 68.7 69 61.9 62 10 40-140130 C11-C22 Aromatics [Unadj.} 1700 1030 61 989 58 4 40-140130 C9-C18 Aliphatics 600 344 57 363 61 5 40-140130 C19-C36 Aliphatics 800 534 67 579 72 8 40-140130 CAS No. Surrogate Recoveries 3386-33-2 1-Chlorooctadecane 580-13-2 2-Bromonaphthalene 84-15-1 o-Terphenyl 321-60-8 2-Fluorobiphenyl Sample Compound OP47077-BS 2-Methylnaphthalene ❑P47077-BS Naphthalene ❑P47077-BSD 2-Methy1naphthalene OP47077-BSD Naphthalene * = Outside of Control Limits. BSP BSD Limits 65% 68% 40-140% 80% 79% 40-140% 65% 61% 40-140% 82% 80% 40-140% Col #1 Col #2 Breakthrough Limit 54.9 ND 0.0% 5.0 51.5 ND 0.0% 5.0 52.2 ND 0.0% 5.0 49.1 ND 0.0% 5.0 �i 118 of 119 AccuTES-r. FA493e •••�••��•�•• Duplicate Summary Job Number: FA4930 Account: BPAMSS Atlantic Richfield Company Project: URSNCM: S/S 1363, 1101 Hwy 61, Whilsett, NC Page 1 of 1 Sample File ID DF Analysed By Prep Date Prep Batch Analytical Batch OP47077-DUP NN004803.D1 05/31/13 NMC 05/29/13 OP47077 GNN207 FA4930-8 NN004802.D 1 05/31/13 NMC 05/29/13 OP47077 GNN207 The QC reported here applies to the following samples: Method: MADEP EPH REV 1.1 FA4930-1, FA4930-2, FA4930-3. FA4930-4. FA4930-5. FA4930-6, FA4930-7, FA4930-8, FA4930-9, FA4930-10. FA4930-11, FA4930-12, FA4930-13 CAS No. Compound FA4930-8 DUP ugll Q ugll Q RPD Limits 83-32-9 Acenaphthene ND ND nc 303 208-96-8 Acenaphthylene ND ND Inc 30 a 120-12-7 Anthracene ND N❑ nc 30 a 56-55-3 Benza(a)anthraoene ND ND nc 30 a 50-32-8 Benzo(a)pyrene ND ND nc 30 a 205-99-2 Benzo(h)f]uoranthene ND ND nc 30 a 191-24-2 Benxo(g,h,i)perylene ND ND nc 309 207-08-9 Benzo(k)fluoranthene ND ND nc 30 a 218-01-9 Chrysene ND ND nc 30 a 53-70-3 Dibenzo(a,h)anthracene ND N❑ nc 30 a 206-44-0 Fluoranthene ND ND nc 30 a 86-73-7 Fluorene N❑ ND nc 30 a 193-39-5 lndeno(I,2,3-cd)pyrene ND ND nc 30 a 91-57-6 2-Methylnaphthalene N❑ N❑ nc 30 a 91-20-3 Naphthalene N❑ ND nc 30 a 85-01-8 Phenanthrene N❑ ND nc 30 a 129-00-0 Pyrene ND ND Inc 303 C11-C22 Aromatics (Unadj.) 244 ND 200* 30 a C11-C22 Aromatics 244 ND 200* 30 a C9-C18 Aliphatics ND ND nc 30 a C19-C36 Aliphatics ND ND nc 30 a CAS No. Surrogate Recoveries DUP FA4930-8 Limits 3386-33-2 1-Chlorooctadecane 80% 71% 40-140% 580-13-2 2-Bromonaphthalene 79% 81% 40-140% 84-15-1 o-Terphenyl 68% 61% 40-140% 321-60-8 2-Fluorohiphenyl 73% 80% 40-140% (a) Advisory control limits. * = Outside of Control Limits. I119 of 119 ACLU-rEST. FA4930 ••��•,�•• APPENDIX C HISTORICAL SUMMARY OF GROUNDWATER ANALYTICAL RESULTS Appendix C1 Historical Groundwater Analytical Data Former BP Service Station No. 01363 1101 NC Highway 61 Whitsett, North Carolina Well Date Benzene Ethylbenzene Toluene Xylenes MTBE Naphthalene DP-01 1/14/2003 4510 424 3500 1580 17900 150 DP-02 1/14/2003 1180 555 92.1 663 3300 226 DP_03 11/14/2003 363 259 95.1 390 409 175 MW-01 9/11/1993 zl <1 <l <1 <5 300 3/1/1995 • 1 _ <5 9 21 4 8/5/1996 - 1 <1 <l <1 2.8 <5 12/9/1997 <l <1 <5 <1 <5 <10 10/25/2000 7.5 4.3 <5.0 9.3 <5.0 <L0 MW_021 3/1/1995 5000 <1000 6300 5900 43000 251) 8/5/1996 3300 <200 4200 3700 10000 29 12/9/1997 3700 500 3300 3200 13000 110 MW-02R 12/22I2000 11000 410 3800 1900 14000 120 1/14/2003 9910 399 1160 956 13800 371 6/2712003 5890 696 3380 3230 10000 321 9/4/2003 8200 927 4560 3980 14200 272 J 3/10/2004 2170 140 J 604 3553 3290 <100 9/15/2004 1290 1 i' _ _. 352 1730 23.9 J 6/27/2005 1910 254 341 635 2530 <50 10/25/2005 2380 266 427 546 2250 56.3 J 515/2006 2470 227 341 562 3890 56.3.1 3/1312007 1730 240 148 433 1440 62J 10/30/2007 2920 364 213 816 2450 95.91 8/6/2008 2500 270 260 558 2300 76 2/17/2009 2180 J 310 <8&7 U 4573 1990 43.6 J 9/30/2009 2510 275 102 J 432 2030 50.8 4/22/2010 1880 153 130 255 J 1960 60.3 J 11/2/2010 3600 J 346 127 596 3250 72.1 J 5/ 18/2011 4510 J 3793 277 J 540 J 39901 68.3 J 11/2/2011 5450 492 211 957 4440 143 5/23/201 7840 653 568 1590 5660 178 11113/2012 8490 616J 245 790 2130 194 5/21/2013 6540J 421 287 655 2480 151 September 11, 2013 Page 1 of 9 Appendix C1 Historical Groundwater Analytical Data Former BP Service Station No, 01363 1101 NC Highway fit Whitsett. North Carolina Well date Benzene Ethylbenzene Toluene Xylenes MTBE Naphthalene MW-03 8/11/1993 333(1 480 600 500 IbSV 23 3/1/1995 930 250 <5[)O 296 1800 489 8/5/1996 1300 210 80 210 3700 <5 12/9/1997 640 130 39 75 4600 <10 1/712000 610 Rh 11 2100 16 10/24/2000 600 130 <50 1 W 6300 16 1 i 14/2003 470 64.3 4.2 22.2 2000 20 1,12712003 112 27.2 53 19.9 J 274 12.2 }1412003 234 53.2 2,91 1953. 1200 13. l 3/10/2004 299 59 <10 46.5 J 1410 <20 9/15/2004 127 14.4 1.3 J 176 980 49 6/27/2005 146 <2.5 <2.5 7.4 J 419 5.9 J 10/24/2005 114 <5 <5 <10 389 <10 5/5/2006 SO ¢5 <10 385 <10 3/13/2007 195 14.9 4.3 J 21.1 435 8.7 J 10/30/2007 43.3 0.79 J 0.73 J 5A J 288 6 8/5/2008 13 1.13 <0.5 1.4 J 150 1.1 .I 2/17/2009 123 <1 <1.2 <8.2 t1 303 r6.8 9/30/2009 31.9 11 0.3 1.6 J 151 2.3 J 4/22/2010 8.4 <1.1 <1.1 C3.2 159 1.8J 11/2/2010 12.6 ¢1.1 1.1 <3.2 150 ¢1.1 5/ 19/2011 0.45 J 31.8 0,391 1.6 0.27 J 1112120E 1 21.2 2.7 54.3 4.4 12.5 0.7 5/23/2012 96 IA 2.7 8.2 125 L7 11/13/2012 65.2 15 2.4 2.73 116 1.2J 5/2112013 1 444 1 123 1.3 2.5 J 90.8 l.9 September 11, 2013 Page 2 of 9 Appendix C1 Historical Groundwater Analytical Data Former BP Service Station Nv. 01363 1101 NC Highway 61 Whitsett, North Carotina Well Date Benzene Ethylbenzene Toluene Xylenes MTBE Naphthalene MW-04 8/11/1993 ] 1 ¢1 ...1 5 ' 2 o 3/1/1995 ti 14 170 180 r50 5 8/5/1996 1 e1 rI Ei <5 121911997 tl <1 r5 rl r5 r10 10/25/2000 10 7.0 •-5.0 19 t5,0 <1.0 1/14/2003 ¢0.5 ¢0.7 a0.5 ¢1 <0,5 r1 6/27/2003 <0.5 <0.5 <0.5 rl r0.5 rl 9/4/2003 <0.5 r0.5 r0.5 rl <0.5 rl 3/10/2004 <0.5 <0.5 r0,5 rl r0,5 <l 9/15/2004 <0.5 r0.5 1.2 J rl <0, 5 r 1 6R712005 <0.5 r0.5 0.66 J rl 4.9 1 _' ; 10/25/2005 r0.5 r0.5 27.3 <l 0.57 J <l 311312007 <0.5 r0.5 r0.5 <l <0.5 <i 10/30/2007 r0.2 J <0.2 J 0.65 J <0.56 J r015 J r0.44 J 816/2008 0.52 3.6 0.55 38 <0.1 1.6 2/ 17/2009 r0.06 0.063 J <0.06 0,363 r0.06 r0.34 9/30/2009 <0.06 0.065 J <0.06 0.42 J r0.06 r0.34 4122/201U <0.I I r0.11 0.331 0,653 <0.12 0.171 MW_05 9/11/1993 rl <1 <l <1 r5 r2.0 September 11, 2013 Page 3 of 9 Appendix C1 Historical Groundwater Analytical data Former BP Service Station No. 01363 1101 NC Highway 61 Whitsett, North Carolina Well Bate Benzene Ethylbenzene Toluene Xylenes MTBE Naphthalene MW-06 8/11/1993 • 1.0 3/1/1995 <I al <5 <2 <5 210 8/5/1996 a] C] < 1 CI C1 ¢5 121911997 <1 <l <5 <l <5 <10 1/6/2000 <1.0 <1.0 1.1 <1.0 <1,0 <10 1012412000 ¢ 1.0 ¢ 1.0 <5.0 <2.0 <5.0 < l .0 1/14/2003 <0.5 <0.7 <0.5 <1 <0.5 ¢I W27/2003 <0.5 <M <0.5 <] <0.5 rI 9/4/2003 t0.5 <0.5 <0.5 <l <0.5 <I 3/10/2004 <0.5 <0.5 45 <1 <0.5 <1 9115/2004 <0.5 <0.5 <0.5 <l <0.5 ¢1 6/2712005 <0.5 <0.5 <0.5 < I <0.5 <1 10/24/2005 <0,5 <0,5 <0.5 <I <0.5 <1 5/5/2006 <0.5 <0.5 <0.5 <1 <0.5 <1 3/13/2007 <0.5 <0.5 <0.5 <1 <0.5 <1 10/30/2007 <0.2 <0.2 <0.27 <0.56 <0.25 <0.44 8/5/2008 <0.1 <0.I <0.1 <0.2 <0.I <0.1 2/17/2009 <0.06 <0.05 <0.17 U <0.14 <0.06 <0.34 9/30/2009 <0.06 c0.05 <0.06 <0.14 <0-06 < 0,34 4/22/2010 <0. E 1 <0.1 l 0.14 1 <0.32 <0.12 <0.1 I I11212010 <0.11 <0.1I <0.11 <0.32 <0.12 <0.11 5/18/2011 -0.13 <0.15 0.161 <0.3 •413 <0.1 11/1/2011 <0.13 <0.15 0,291 <0.3 50.13 50.1 5/23/2012 <0.13 <0.15 <0.25 U <0.3 <0.13 <0.1 11/13/2012 <0.1 <0.1 0.92 <0.22 <0.I <0.I 5121 /2013 <0. I <0. I 0 1 <0.22 <0. I <0. 15 MW-07 3/1/1995 3400 340 11.1oo 2500 440(1 <1 8/5/1996 9500 1400 8000 6400 7200 390 12/9/1997 6300 1200 3400 3900 5700 210 10/25/2000 E400 400 370 950 970 79 1/14/2003 305 284 87 1070 115 75.6 6127/2003 1.2 3.7 0 58 J 7.8 8.9 1.3 J 9/4/2003 r0.5 3.2 `0.5 6 4.2 1.11 3/10/2004 <0.5 3.9 -!0.5 5.81 <0.5 1.6 J 9/15/2004 <0.5 <0.5 <0.5 ¢1 <0.5 ¢E 6/27/2005 5.1 <0.5 0.55 J <1 6.4 4.1 J 10/25/2005 0.63) <0.5 <0.5 c1 3.3 <1 5/4/2006 60.7 62.8 1.6 7.9 22.4 13 3/13/2007 23.0 35.1 12 6.3 10.4 7.3 10/30/2007 71.1 55.1 1.3 3.5 33 13.1 9/5/2008 <1 < 1 <1 4 1.41 <1 2/17/2009 <0.06 0.371 <0.0811 <0.14 6.7 <0.31 9/30/2009 <0.06 0.27 J <0.06 ;0.14 3 1 z0 ; 3 September 11, 2013 Page 4 of 9 Appendix C1 Historical Groundwater Analytical Data Former BP Service Station No. 01363 1101 NC Highway 61 Whitsett, North Carolina Well data Benzene Ethylbenzene Toluene Xylenes MTB£ Naphthalene MW_08 8/11/1993 1 I i i CS <2.0 3/1/1995 <l 1 <5 Q C5 C1 9/5/1996 <1 1 <l <1 <1 C5 121911997 <1 i 5 <1 t5 <10 10/25/2000 a 1.0 <1.0 <5.0 4.0 <5.0 23 1/14/2003 t0.5 <0.7 <0.5 <l <0.5 ¢1 6/27/2003 <0.5 <0.5 <).5 <1 <0.5 <1 9/4/2003 <0.5 <0.5 <0.5 <1 c0.5 <1 3/ 10/2004 <0.5 <0.5 <0.5 <1 <0.5 <1 9/15/2004 <0.5 <0.5 <0.5 <l <0.5 <1 6/27/2005 <0.5 <0.5 <0.5 <l c0.5 <1 10/24/2005 <0.5 <0.5 0.5 r1 ¢0.5 <1 5/5/2006 <0.5 <0 fj a 1 <0.5 1 3/13/2007 <0.5 [0,5 <0.5 <0.5 I 10/30/2007 <0.2 <0.2 =0.27 <U.5b <015 :0.44 8/5/2008 <0. i <0.1 <0.1 <0.2 <0.1 <0.1 2/17/2009 <0.06 <0.05 <0.06 <0.14 <0.06 <0.34 9/30/2009 <0.06 <0.05 <0.06 <0.14 :0-06 <0.34 412212010 r0.II <0.1I <0.11 <0.32 1112 <0.I1 11/2/2010 <0.II <0.11 <0.11 <0.32 <0.12 <0.11 5/1712011 <0.13 <0.15 <0.13 <0.3 -0.13 <0.1 1I1112011 <0.13 <0.15 <0.13 E0.3 •.=0.13 <0.1 5/23/2012 <0.13 <0.15 a0.13 it + r0.13 <0.1 1 I11312012 <0- I <0.1 <0. i <0.1 <0.15 5/21/2013 <0.1 <0.1 <0.1 mil _'.' <0.1 <0.15 MW-09 1/7/2000 <I.o <1.0 <1.0 <1.0 c1.0 a10 1/11/2000 < 10 7/11/2000 G11.0 <1.0 <1.0 <1.0 <1.0 10/23/2000 ¢ 1.0 r 1.0 <5.0 n.0 <5.0 r 1.0 6/27/2003 <0.5 0.5 <0.5 <l <0.5 I 3/10/2004 <0.5 <O.S <0.5 ¢1 <0.5 <1 9/15/2004 <0.5 <0.5 <0.5 EI <0.5 <1 6/27/2005 <0.5 <0.5 <0.5 <I <0.5 <1 10/24/2005 <0.5 <0.5 <0.5 <l <0.5 <1 5/4/2006 <0.5 <0.5 <0.5 <l <0.5 <1 3/ 13/2007 <0.5 <05 <0.5 <1 <0.5 <1 10/30/2007 <0.2 <0.2 :0.27 e0.56 <0 2 <0.44 8/6/2008 <0. i <0.1 <0.1 <0.2 <0.1 <0_ 2/17/2009 <0.06 <0.05 <0.06 0.14 <0.06 <0.34 9/30/2009 N.06 <0.05 81.8 <0.14 <0:06 <0.34 111212010 <0.II r0.11 0.79 <0.32 10.12 <0.11 5/17/201 1 <0.13 <0.15 0.13 ] <0.3 0.13 <0.1 1I1112011 <0.13 t0.15 <0.13 t0.3 <0.13 <0.1 September 11. 2013 Page 5 of 9 Appendix C1 Historical Groundwater Analytical Data Former BP Service Station No. 01363 1101 NC Highway 61 Whitsett, North Carolina Well Date Benzene Ethylbenzene Toluene Xylenes MTSE Naphthalene MW-09D 117/2000 ¢1.0 -1.0 1.3 ¢1.0 - 1.0 ¢10 10123/2000 <1-0 <1.0 <5-0 <2.0 <5.0 <1-0 9/4/2003 <0.5 <0.5 <0.5 < I <0.5 <1 3/10/2004 <0-5 <0.5 - 0.5 <I <0.5 <l 9/15/2004 <0.5 <0.5 E0.5 <1 1 6/27/2005 <0. <0.5 0.5 <1 1 < l 10/25/2005 <0. <0.5 s0.5 <1 0.541 <l 5/412006 <0-5 <0.5 <0.5 <1 --0.5 <1 3/13/2007 t0-5 t0.5 50.5 tl t0.5 <l 10/30/2007 <0.2 <0.2 <0.27 <0-56 .0.25 <0-44 8/6/2008 <0-I <0.1 <0.1 <0.2 0.12 J <0.1 2/17/2009 <0.06 <0.05 1 <0.06 �0.14 <0-06 <0.34 913012009 r0,06 t0.05 <0.06 <0.14 <0.06 r0.34 412212010 <0.II <0.I1 <0.11 <0.32 <0.12 <0.11 IIrM010 <0.II <0.II <0.11 <0.32 <0.12 <0.11 511712011 <0.13 <0.15 <0.13 <0.3 -'0.13 <0.1 1.111/201.1 <0.13 <0.15 <0.13 <0.3 `0.13 <0.1 MVti'-1i1 1/7/2000 62 <1.0 1.5 <1.0 32 <10 7/11/2000 <1-0 <1-0 <1.0 c1-0 <1.0 1.0123/2000 <1.0 <L0 <5-0 <2-0 <5.0 <1.0 1/14/2003 0-56 J <0.7 <0.5 <1 0.83 3 <1 h12.712003 <0-5 <0.5 <0.5 <l <0.5 <1 914/2003 <0.5 <0.5 <0.5 <l <0.5 <1 3/10/2004 0.811 <0.5 <0.5 <1 11 <1 9/15/2004 <0.5 <0.5 <0.5 <1 <0.5 <1 6/27/2005 <0.5 <0.5 <0-5 <I 2.3 <1 IOJ2412005 <O.5 <0.5 <0.5 <1 7.7 <1 5/4/2006 0.831 <0.5 t0.5 <1 453 <1 3/13/2007 11 <0.5 <0.5 <1 2.7 <I 10/30/2007 7.1 0,723 <0-27 111 9.1 15.6 8/6/2008 -<0-I <0-I <0-1 <0-2 0.15.1 C0.1 2/17/2009 4A 0-07 J [0-063 U <0.14 0.81 2.2 9/30/2009 0.091 J <0.05 <0.06 <0.14 0.2 J <0-34 4/22/2010 <0.1I <0.II r0.11 <0-32 <0.12 <0.11 11/2/2010 <0.1 i <0. I I <0.11 <0-32 (}-15 J <0.1 1 5117120 t 1 E0.13 <0.15 <0.13 <0.3 <0-13 0.371 11 / 112011 2.6 <0.15 0.26 J 0.32 J 0-37 J 44.5 5/23/2012 <0.13 <0 I S <0 13 E0.3 <0 13 0-28 J 11 /13/2012 0-29 J 1 0.1 <0.22 <0.1 0.54 512212013 <0- I I 0.1 <0.22 <0- I <0,15 September 11, 2013 Page 6 of 9 Appendix C1 Historical Groundwater Analytical Data Former BP Service Station No. 01363 1101 NC Highway 61 Whitsett, North Carolina Well Date Benzene Ethylhenzene Toluene Xylernes MTBE Naphthalene M1k'-11 1/11/2000 Cl.0 :I.O •:.I_u <IIj -lt, 7/18/2000 <1.0 <1.0 <1.0 <1.0 1.1 10/23/2000 <1-0 C1.0 <5.0 C2.0 <5.0 <1.0 6/27/2003 <0.5 <0.5 <0.5 < 1 <0.5 < 1 9/4/2003 0.53 J <0.5 <0.5 <1 <0.5 <1 3/10/2004 t0.5 <0.5 <0.5 <1 =0.5 <1 9/15/2004 <0.5 <0.5 <0.5 <1 <0.5 <1 612712005 r0.5 0,88) 2.7 5 16.6 15.4 1012412005 <0.5 <0.5 1.2 2.9 J 0.73 J 10.4 5/4/2006 <0.5 <0.5 <0.5 <1 <0.5 1.81 3/13/2007 <0.5 <0.5 0.5 <1 -0.5 3.1 1013012007 <0.2 <0.2 o.27 0.81 J 0.25 3.7 8/6/2008 I 0.11 J 0.91 1 0.721 <0.1 4.6 2/ 17/2009 s0.06 <0.05 r0.06 <0.1 a <0.06 <0.34 9/30/2009 <0.06 <0.05 <0.06 <0.14 <0.06 <0.34 4/22/2010 <0.1I <0.1I <0.11 <0.32 <0.12 0.29.1 111212o 1 o <0.1 I <0.11 0.3 J <0.32 <0.12 0.86 ] 1/ 1 /201 1 [0.13 ¢0. 15 <0.13 <0.3 <0.13 0.39 J 5i2312012 <0.13 <015 [0.31II <0.3 <0.13 1.1 11/13/2012 <01 [0.1 <0.1 <0.22 <0.1 1.2 5/22/2013 <0.1 [0.I. <0.1 <0.22 <0.1 0.74 MW-12 1/11/2000 22 28 19 1.0 19 c10 6/27/2005 24.5 22.5 -0.5 4.6 53.8 172 10/2412005 14.8 <5 ¢5 ¢ 10 39.2 240 5/4/2006 12.8 4.5 cl 4 17.1 99.2.1 3/13/2007 14.4 2.9 <0.5 ¢1 15.3 126 1013MG07 9.7 1.8 <0.27 <0.56 14.9 107 8/6/2008 6.6 0361 0.59 0.25 J 10 71 2117120D9 5.2 1.6 J <0.6 U.14 6.6 147 9/30/2009 5.6 0.7 0.75 0.17 J 5.9 10ti 4/22/2010 3.5 0.62 <0.11 <0.3F 0.78 65.1 E 1/2/2010 3.3 <0.55 <0.55 r 1.6 3.7 86.3 M W-15 6/27/2005 32A 16 <0.5 1.81 74.8 158 RW-01 3/1/1995 3000 <1000 540D 3800 16000 94 8/5/1996 8200 580 7100 74DO 40000 390 12/9/1997 5700 970 3700 IWO 29000 300 1/7/2000 12000 890 1100 55000 260 10/25/2000 12000 <1000 <5000 30DO 110000 130 5/5/2006 2540 331 116 M 2040 130 September 11, 2013 Page 7 of 9 Appendix C1 Historical Groundwater Analytical Data Former BP Service Station No. 01363 1101 NC Highway 61 Whitsett, North Carolina Well Date Benzene Ethylbenzene Toluene Xylenes MTBE Naphthalene RW-f1 I k h127/2003 <0.5 <0.5 :o.5 1 <0.5 <1 9/4/2003 <0.5 <0. 5 <0.5 < 1 �0.5 r 1 9/15/2004 562 213 88A 717 1450 45.2 6/27/2005 1060 548 61.8 921 1670 159 IW2412005 605 249 25.1 399 887 128 3/13/2007 609 435 30.4 372 455 1.73 10/30/2007 381 288 34.2 302 368 112 8/6/2008 240 350 14 1841 160 110 2/17/2009 259 240 <13.7 U 119 124 91.1 9/30/2009 342 464 30.6 354 124 124 4 '-_': 2010 758 168 13.2 J 104 194 68.5 11/2/2010 47 98.9 10.5 67.3 4 411 5/18/2011 379 239 16.6 149 171 70.9 11/1/2011 54A 120 4.2 93.2 57 45.6 5/23/2012 270 237 7.7 151 183 94.9 11/13/2012 14.6 129 2.3 102 28 58.2 5/21/2013 251 66.9 <1 16.9 149 32.2 VE-01 8/11/1993 38 1 8 40 7835 7 8/5/1996 7.6 <5 <5 <5 2500 <5 12/9/1997 _ <l <5 <1 1700 <10 101251200{] 15 <1.0 <5.O 4.0 1200 ¢1.0 6/27/2003 <0.5 <0-5 <&5 <1 24.4 <1 91412G03 r1.3 <1.3 t13 4.5 110 <2.5 3/10/2004 <0.5 <0.5 <0.5 <1 0.61 J <l 9/15/2004 <0.5 <0.5 <0.5 t] =0.5 <l 6/27/2005 <0.5 <0.5 <0.5 < 1 = 0.5 r 1 10/24/2005 <0.5 <0.5 <0.5 , I 5.4 < 1 5/4/2006 <0.5 <0.5 <0.5 <l <0.5 <1 3/13/2007 E0.5 <0.5 <0.5 <l <0.5 <l 10/30/2007 <0.2 <0.2 <0.27 <0.56 9.7 0.95.1 8/5/2008 <0.1 -<4.1 <0.1 t0.2 0.52 <0.1 2/17/2009 <0.06 C0.05 <0.06 <0.14 0. 21J C0.34 9/30/2009 <0.06 <0.05 <0.06 <0.14 0.21 J <0.34 4/22/2010 <0.1 1 <0. I I <0- 11 <0.32 0. i 4 J <0.11 I 1121201 o <O.l I <0. 11 <0- 11 <0.32 171 <0.11 J 5/17/2011 <0. 13 <0.15 <0.13 0.3 2.1 <0,1 1 1111201 1 <0.13 <0.15 <0.13 <0.3 8A <0,1 5/23/2012 11 1 ; C0.15 ¢0.13 --0.3 7.2 <0.1 11/13/2012 <0.1 <0.1 <0.1 <0.22 6.4 <0.15 5/21 /2013 <0. I <0.1 <0. ] <0.22 2 <0.15 September 11, 2013 Page a of 9 Appendix C1 Historical Groundwater Analytical Data Former BP Service Station No, 01363 1101 NC Highway fit Whitsett, North Carolina Well Date Benzene Ethylbenzene Toluene Xylenes MTBE Naphthalene VE_02 811111y9i _. 5.7 2u 22 17 8/5/1996 I rl <1 <1 37 <5 12/9/1997 i =l <5 <l 46 <10 10/25/2000 l ii DLO t5.0 =2.0 63 <I.0 VEW-01 8/5/1996 CI EI <1 <1 1.6 <5 12J9/1997 <I <1 <5 <1 <5 <10 10125/200t➢ <1.0 <1.0 <5.0 <2.0 <5.0 <1.0 3/10/2004 <0.5 <0.5 <0.5 <1 3.3 <l 9/15/2004 r0.5 <0.5 <0.5 <I 3 <I 6/27/2005 <0.5 <0.5 <0.5 <I 7.2 <l 10125/2005 <0.5 <0.5 <0.5 <I 2.1 <l 5/4/2006 <0.5 <0.5 ­a5 ¢1 4.5 t1 13-2007 <0.5 <0.5 1.5 <1 4.2 t1 1(0012007 <0.2 <0.2 <0,27 <0.56 11.5 <0.44 8/6/2008 <0.1 <O.I <0.1 <0.2 2.4 <0.1 2/17/2009 c0,06 <0.05 <0.06 <0.14 2.9 <0.34 9/30/2009 r0,06 <0.05 <0.06 <0.14 0.78 <0.34 4/22/2010 <O.II <0.11 <O.11 <0.32 1.9 <0.I1 11/212010 <O.II <0.11 <0.11 <0.32 c0.12 <0.11 5/18/2011 <0.13 <0.15 <0.13 <0.3 1.3 <01 11/112011 c0.13 <0.15 <4.13 <03 r0.13 <D.I 5/23/2012 <0.13 <0J 5 <0.13 <0.3 0.71 <O. I 11/13/2012 <O.I <0.1 •-O.1 <0.77 0.58 <D,15 5/21/2013 <0.1 <0.1 <0.1 <0.22 0.48 J <0.15 Notes: Units are in ug/l J = Estimated value NA -Not analvxed U = Below detection limit ND - Not detected BDL - Below method detection limit Both ND and 8D1_ are reported in historiW data K ithout listing detection limits. Data prior to 2003 were reported by previous suppliers and have not been verified. September 11. 2013 Page 9 of 9 AppcndN 0 Historical Summary of Groundwater Analytical Hel911% - ►'f1('SI4V[H-S Tra veWenterx of America lik 110t NC Highway 61 Whitaelt.Guilford County. North Unrolina Facility i.D.: 0-411-9186 Incident Numher.: 200S4 le tp Date ollected Source AreaSam Incident Phaie7-1-19 Contaminant of Concern -h k o * = tc Z,C mr YmNm=a� C ttwmL� _ taode xmL O L ? LL L Z , =■ C ,c�, '• C gj=W9 UST Field CAP <02 <0 16 s037 <024 <0.It <0084 <0.59 <0.11 <013 <013 <0.77 <0.17 <015 r0.19 <019 <0.11 <0.16 4.9 <0 13 <0.074 2.5 1.9 101512010 UST Field CAP 10.99 <0.48 <0 78 r0.95 3.8 J <0.084 <0.59 <0 11 <0. 13 <0.13 <0.17 <0.17 <0.15 <0.19 0.42 J 9.2 <0 16 19 7 2.7 J 47 33 11612011 UST Field CAP <.99 <0.48 <0.78 <0.95 2.8 J <0 084 <0.59 <0.11 10. 13 <0.13 <0.17 <0.17 �0.15 <0.19 <0.19 4.4 J <0.16 16 <0.13 04 J 34 19 411412011 UST Field CAP t10 t10 <1.0 13.0 2.7 1096 1096 <0.19 <0.19 <0 19 <0.19 <0.19 10 19 <0,19 <0.96 4.5 40.19 13.6 16 0.691 3119 16.6 7114l2011 UST Field CAP <7 0 0-661 <1.0 1.7.1 1.8 1097 40.97 <0.19 <0 19 <0 19 40.19 <0 19 <0.19 <0.19 <0.97 3.4 40.19 11.4 2.2 0.48 J 21.2 12.2 10119f2011 UST Fieid CAP 0.0 1 410 <1.0 <3.0 2.2 <0.98 <0.96 10.19 <0.19 <0 19 <0.19 <0.19 <0.19 <0.19 <0.96 4.2 <0.19 7.0 1.9 0.37 23.9 6.5 USTM W-1 105P2012 UST Field CAP 11.0 <1.0 11.0 13.0 1.7 <0.96 s0.96 <0.19 40.19 10.19 <0.19 10.19 10.19 Q1.19 <0.95 3.2 40.19 14.3 2.6 0.37 J 21.4 11.5 4112/2012 UST Field CAP <1 0 <1 0 '10 <3.0 2.0 J ISO <5.0 <5.0 15.0 <5 0 <5.0 <5 0 <5.0 <5.0 <5.0 4.8 J -5.0 %2 2.8 J <5.0 30.0 16.8 7124/2012 UST Field CAP <1.0 <1.0 <1.0 <3.0 1.1 J <4.8 <4.8 <4 8 <4.8 <4.8 <4.8 14.6 14.8 <4.8 <4.5 1.9 J <4.8 -4.8 0.831 c4.8 NA 0.67 J 1115f2012 UST Field CAP '10 <1.0 c1.0 <3.0 2.5 J <5.0 <5.0 15.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 4.6 J 55.0 11.7 3.11 1!5.0 MIS 13.3 Se22W13 UST Field CAP 0.0 0.11 J -1.0 <0.22 6.7 0.73 J 11.6 <5 0 27.6 13.7 3.9 J 49 166J7 9f212009 UST Field CAP 4.2 J 0.37 J <0.37 <0.24 <0 11 <0 084 10.59 <0.11 <0.13 <0 13 <0.17 <0 17 <0.15 ID.19 <0 19 <0.11 10.16 6.8 <013 <0.074 3.8 3 101512010 UST Field CAP 6 <0.48 <0.78 <0.95 4.7 J <0.084 0.77 J <0.11 <013 e0.13 <0.17 10.17 <015 <0.19 10.19 13 10.16 68 12 31 86 84 1f612011 UST Field CAP 6.3 <DAS -0.78 <0.95 6.8 -0.084 2 J I0.11 �0.13 10.13 -0.17 1017 10 15 40.19 10.19 9.6 1'0.16 66 11 2.2 83 110 4114f2011 UST Field CAP 0.78 �1.0 <1 0 <3.0 10.96 1:0.96 <0.96 <0.19 10.19 -0.19 <0.19 0.19 4019 10 19 50.96 0,69 J 10.19 2.4 0.69 J 40.96 3.7 3.1 711412011 UST Field CAP 11.0 41.0 <1.0 <3 0 <0 9B 10.98 10.98 <0 20 <0.20 <0.20 <0.20 �0.20 <0 20 <0.20 00.96 1.1 <0.20 2.6 1.2 0.28 4.6 2.9 lJSTMW-2 1WOr2011 UST Field CAP c1 0 �1.0 <1 0 <3 0 0.97 10.97 10.97 <0.19 10.19 10.19 10.19 10.19 10.19 10.19 W.97 <0.97 <0 19 0.97 <0 97 <0 97 <0.97 4097 IIWC12 UST Field CAP 14 0.24 <1 0 C3 0 2.1 10.97 <0 97 4019 <419 <0 19 40.19 t0.19 10.057 11 4010 1.97 4.6 <0 19 12.2 6.9 1.4 23.4 26.3 4112i2012 UST Field CAP 0.84 J <7 0 11.0 -3.0 1.91 44.8 14.8 �4.8 -4.0 <4.6 14.8 z4 8 <A.5 14.8 <4 B 4.4 J -4.8 26.4 3.5 J 148 40.3 34.6 7i2412012 UST Field CAP 0.30 J 1!7.0 -1.0 1:3.1 <4.9 <4.9 <4.9 <4.9 <4.9 <4.9 <4.9 14.9 -4.9 <4.9 <4.9 <4.9 r4.9 14.9 <4.9 <4.9 NA <4.9 I IIW2012 UST Field CAP 6.3 41.0 C1.0 1.0 J t4.9 44.9 -4.9 c4.9 14.9 <4.9 <4.9 <4 9 c4 9 <4.9 <4.9 <4.9 r4.9 <4 9 <4.9 <4.9 <4.9 <4 9 5f =013 UST Field CAP 1.6 0.27 J 0.21 J 9.42 J 17.4 J <5.5 31.4 J 62.8 68.4 15.3 J 130 166 USTMW-3 9Rj2009 UST Field CAP <0.2 10. 16 r0.37 <0.24 <0.11 <0.084 <0.59 <0.I I <0 13 <0 13 <0.17 <0.17 Kl 15 <0.19 <0 t9 <0.11 <0 16 <0 001 <0 13 <0.074 <0 089 40076 9/272009 UST Field CAP 2.4 J <0 16 <0.31 0.43 J 12.2 <1 7 412 <2.2 12.5 <2.6 13.3 r3.3 13.0 43.1 c3.9 -2.2 t3.3 c1.2 4.6 -1.5 c1.6 11.5 101512010 UST Field CAP <0.99 <0.49 <0.76 <0 95 <1.1 10.84 <5.9 <l.1 <1 3 <1.3 17.7 41.7 <1.5 <7 9 <1 9 <1 1 410 2.6 J <1 3 10 74 10 59 <0 76 1fi oll1 UST Field CAP <0.99 -0.45 10.78 <0.95 <0.55 10.42 <2.9 r0.56 r063 <0.66 <0 83 <0.66 <0.76 <0 94 <0 97 <0 54 <0 82 <0 3 <0.64 6.7 1044 <0 38 4114MI1 UST Fleid CAP 2.2 <5 0 0.46 J c3.0 <0.97 <0.97 <0.97 a0.19 <0.19 <0.19 <0.19 <0.19 WHO J 0.19 <0.97 <0.97 10 19 3.5 <0.97 O.ISJ <0.97 <0.97 USTMVV-4 7114f2011 UST Field CAP 4.7 0.82 J 0.63 J 1.7 J -3.8 <3.6 <3.8 <0.76 <0.76 <0.76 <0 76 <0.76 <0 76 <0.76 <3.6 <J 8 <0 76 12.3 <3 9 38 '3.8 <3 8 10f20r2011 UST Fleld CAP 0.23 J <1 0 17.0 <3.0 <0.99 <0.99 10.99 <0.20 <0.20 <0.20 0.045 J <0.20 0,949 J <0 20 10.99 <0.99 10 20 <0.99 <0.99 10 99 <0 99 <0 99 1&2012 UST Field CAP 2.4 0.21 J 0.23 J <3 0 <0 98 <0 98 <0 98 <020 <0.20 <0.20 <0.20 <020 <0.20 <0.20 <0.98 <0.98 10.20 1.2 10.96 S098 -0 98 <0.98 4112/2012 UST FIe1d CAP &1 0.76 J <1 0 <3 0 <4.8 14 8 14.5 <4.8 <4 8 448 <4 8 <4.8 <4 8 <4 8 <4.8 <4 8 14.8 11.4 <4 8 c4 8 1.4 J c4 S 7f2412012 UST Field CAP 9.0 1.7 OMJ 1.6 J <4.8 <4 6 <4.8 <4.8 14 8 14.8 <4 8 <4.8 r4 8 <4.8 <4 8 <4.0 <4.8 24.2 14 8 0.86 J NA 04 J I of 2 Appendix f -2 Historical Summary ofCround%alcr Cnal}7icaI Results- VOCS1SVpCS rrsv elC'rnun of Am erica It IOt NU Highway 62 Whitseit, Guilford C-ounly, North Carolina Facility i.D.: 0-in9136 Incident Number.: 20054 Sample I❑ Date CoBocled Source Area Incldenl Phaee Contaminant of Concern o m ri in $ c t w C 3 m m X c a t a n u t am- • '�` Q = m m 5 = 01 N 1n m N= mo m t �Q m m Y L w m co m m t [1 n m r v mq O � . f' o� _ o a ? L C c m r v .� OC i. r fs �� 111512012 UST Field CAP 1.9 410 .10 c3.0 2,5 J c4 9 <4 9 <4 9 c4 9 <4 9 <4.9 <4.9 <4-9 <4 9 -4.9 4.9 -4.9 6.6 1.2 J 1.1 J 17.9 5.2 USTMW-4 5f2212013 UST Fieid CAP 5,4 2-3 3,6 9.1 <2.7 -2.3 4-9 18.3 J &2 J 4.8 J 4.6 3/3112009 UST Field CAP -018 c0.2 c0.25 -0.22 -0.D67 0.82 c0-046 <0.11 <0.047 <0.095 c0.17 <0072 c0.07'3 <D.14 c0.054 <0.07 <018 <0099 <0.062 4.038 <0.074 <0.056 MW-6 512212013 UST Field CAP <0.1 <0.1 <0-1 <0.22 MW-9 313112009 UST Field CAP <0.18 <0.2 �O 25 <0.22 r0.067 r0.057 rO 048 SO 11 t0 047 �O 095 c0.17 -D 072 -0.073 c0 14 <0 054 40 01 <0.18 <0.099 <0.062 <0.038 r0 074 <0.055 4114/2011 UST Field CAP Wall Burled or Destroyed I W012011 UST Field CAP <1.0 l 0 �1 0 �3.0 �0.99 0-99 �0.99 <.020 �.020 r.020 E.020 <.020 � 020 020 �0.99 <O 99 <0.99 <0.99 <0 99 <0 99 1099 10.99 Ir1 W-90 1/512012 UST Flaid CAP <10 c10 ti10 <30 <0.95 <096 <0-96 <0.19 <0.19 <0.19 <0.19 b0.19 rO19 -0.96 -0.96 -0-96 50.19 <Q.96 <0.96 W.96 Q.96 411212012 U57Field CAP 110 00 <10 13.0 <49 <4.9 <49 <4.9 14.9 <4.9 r4.9 r4.9 <4.9 W.9 �4.9 -49 r4.9 W.9 c4.9 -4.9 --4.9 <49 712412012 UST Field CAP Well Burled M712009 UST Field CAP 0.62 J r0 2 <0.25 <0.22 <0 067 �0.057 s0.D46 �0.11 �0-047 �0.095 -0-17 1 z0.072 r0:D73 z0.14 <.054 <A 07 �0,18 �0.099 a0.052 <0.036 <0.074 <0.056 MW-10 5122QO13 UST Field CAP -1 0 .0 1 -0 1 �0-22 313112009 UST Field CAP <0 18 �0 2 D,37 J 4022 �0.067 0.84 0,099 J <0 11 c0.047 2 40.17 0,163 <0.073 <0.14 <0.054 0-97 t0 18 <0 099 <0.082 <0.038 <0074 <0.056 1015Ct010 UST Field CAP <0.99 <0.48 <0.76 <0 95 <0 11 <0 OU <0.59 <0 11 <0 13 <0 13 <O 17 <0.17 <0.15 <0.19 <0.19 O.0 J 40.16 0,12 J <0.13 0.13 J 0,12 0.13 1iG120l l UST Field CAP <0.99 <0.4fl <0.78 1095 0.19 J <0.084 <0.59 10.11 <0 13 <0 13 <0 17 <0.17 <0.15 <0.19 <0.19 &GO J s0.16 2.3 J 0.05 J 0.33 J 1.4 J 1.8 J 4114I2ol l UST Field CAP Well Buried 7114/2011 UST Field CAP <1 0 0 0 10 r3.0 <0.98 <0 98 <0.98 �0.20 �0.20 <0.20 <0.20 <0 20 �0.20 4D20 <0.98 r0 98 00.20 r0.98 <0 95 �0.98 �0.96 -0 98 1 10120112011 UST Field CAP <1.0 s10 <1.0 <3.0 <0.98 <0 98 <0.98 10.20 <0.20 <0.20 s0.20 <0.20 <020 <0.20 -0.98 r098 <0.20 K0-98 <0.98 s0.96 s0.98 �0.98 M'N-1 1/5/2012 UST Field CAP s 1 ❑ ' 1 0 <1 0 <3 0 <0 98 <0 98 <0.98 <0.20 �O 20 <0 20 <0 20 <0 20 <0 20 <0.20 rO 98 <0.98 W 20 0,91 J 0.39 J < 98 0.6 J 0.59 J 4112/2012 UST Field CAP <1 0 <1 0 <1 0 <3 0 148 <4 8 <4 8 148 <4 8 <4 8 <4.8 <4 8 <4.8 <4 8 <4 8 d.ilf J <4 8 0,92 J 0.64 J <4 8 0,83 J 0,92 J 7/2412012 UST Field CAP <7.D <1 0 <1 0 <3 0 <4.9 <4 9 <4.9 <4 9 149 <4 9 <4.9 c4 9 149 c4.9 <4.9 <4 9 c4 9 c4 9 149 <4 9 NA 14.9 111512012 UST Field CAP 1.0 <1.0 10 <3 0 <4.9 <4.9k14 �49 <49 r4.9 <4 9 <49 <4.9 <4.9 <4 9 <4.9 <4 9 <4.9 <4.9 <4.9 <4.9 <49 W212013 UST Field CAP 0 0 -1.0 -1.0 -0.22 s0.87 �D.56 0.81J 0.85 J 1 J <0.65 49 130 grMOD9 UST Field CAP 4.6 J 0,62 J <0.37 <0.24 <0.13 <0.1 <0-13 <0.15 <016 <0 2 <0.2 <0.18 <0.23 <0.23 <013 <0.2 3,4 <015 <0.089 2 OJ 10/5/2010 UST Field CAP 3.8 �0.48 �0.78 <Q.95 5.3 -0.084 �0.11 t0.13 r0.13 �Q.17 <0.17 <0.15 m 19 0.66 J 14 rO 16 48 12 3.1J 84 28 116l2011 UST Fielil CAP &7 <0.48 <0.78 <0.95 c011 c0.084 <0.11 <0 13 �0.13 < 17 c0.17 Q.15 50.19 -0.19 9,9 1 <D 16 34 11 2.5 J 83 21 4/14/2011 UST Field CAP Web Burled or Destroyed 312712009 UST Field I CAP <0.15 40.2 <0.25 c0.22 <0.067 <0.067 <0.046 <D.11 <0.047 z0.095 <0. 17 <0-072 40.073 W.14 <0.054 <0.07 1 <0.18 1 <0099 50.W2 <0038 j <0.074 1 00% MW-15 5122r2013 US7 Field CAP z 0.1 r 0 1 t 01 t 0.22 -0.67 <0.56 1 40 73 1 1 <06i 1 <0 68 1 <0.65 <0.68 <0HS 202 .Appeudia C2 - liistorical Sammary of Groandwster AnAI)- icaI Reaulb - VOCSISVQCS iravelCenters of America 1101 NC Highway 61 W hlftdt Wife County. North Caroling PM Facility LID.-. 0-029186 incident N Contaminant of ConcernCIJWLJ °' • ■ r m v =` n ; to y m c i [ r_ r c ^! _ E rr ;, m ;, n Date Incident Sample ID Collected Source Area Phase m c me s p m; u s u 3 c G Y m c t • 3• E E a $ w - c r a c L ^� t t c± ° E 2 e z V 6 2 0 g w L r x i m 4 •� Ca •a La 6p m =�+ m o p 47 t L1 •= ■ c 3 rZ 9a a u as n C W Q m p = U x 6 = C 3f2712009 UST Field CAP �0 18 <0 2 <0 25 <0.22 <0.067 <0 057 -0.046 <0.11 �0 047 <0 095 <0 17 <0.072 <0 073 <0 14 <0 054 <0.07 <0 18 <0.099 <0.062 <0 038 t0.074 <0.056 MW-16 9/2/2009 UST Reid CAP 10 0.62 J i.0 37 =0 24 c0 11 a0 084 t0 59 011 -0 13 <0 13 <0 17 <0 17 < 15 '0 19 <0 19 <0 11 c0 16 13 c0 13 0 G74 17 15 10/5/2010 UST Field CAP 7.9 1 4 <0 78 <0.95 3.6 J -0.084 [0.59 0.24 J <0.13 <0. 13 <0 17 <0.17 -015 <0 19 �0.19 2.5 K0 16 110 IIJ 1,2 J 90 110 AGM-R W 1/612011 UST Fund CAP 9.4 <0 48 <0 78 0.95 3,9 J <0 084 1.3 J <0.11 <0 13 < 13 <0 17 s0 17 0 15 <0 19 c0 19 7 c0 16 100 7.1 1J 59 95 411412011 UST Field CAP 6.3 <1 0 0.93.1 <3.0 6.4 0.67 J e0.96 <0.19 r0 19 <0.19 r0 19 <0 19 <0.19 r0.19 <0 96 8.3 �0.19 102 5.9 0.79.1 63.3 77.9 711412011 UST Field CAP 6.1 0.86 J <1.0 0.69J 2.7 0.51 J -0.95 <0 95 <0 19 s0 19 <0 19 <0 19 <0.19 <0.19 <0.95 6.8 <0.19 108 6.8 1.3 76.7 92.6 1012012011 UST Feld CAP 5.6 0.63 J 0.57 J < 3.0 4.0 '1 0 e1.0 <0.20 K0.20 e0.20 s0 20 <0.20 s0.20 r0.20 0.0 6.3 �0 20 88A L2 OM J 57,9 72.2 1/5/2012 UST Feld CAP 413 0.62 J 0,73 J <3 0 13 0," J .95 <.19 <.19 �.19 <.19 '19 .044 J -.19 �.95 6.6 <.19 711 6.2 i.2 60.6 623 AGM-RW 411212012 UST Field CAP 4.8 '1 0 0,70 J <3.0 Is J r4 8 r4.8 4.8 -4.8 -4.8 14.8 s4 8 <4 8 r4 8 -4.8 6.8 <4 8 94,6 t9 <4.8 76,2 89.9 712402012 UST Fteld CAP 1.8 ' 1 0 <5 0 <3.0 1.6 J 48 e4.8 48 -4 8 <4.8 4.8 e4 6 4.8 <4.8 -4.8 3.4 J 48 3.4 J 2.6 J 0.77 J NA 12,2 11/5/2012 UST Field GAP 3.5 <1 0 <t 0 <3.0 1.6 J <4 9 -4 9 <4 9 -4.9 -4.9 <4.9 <4.9 <4.9 2.3 J �4 9 e4 9 <4 9 <4 9 5.3 -4 9 5/22/2013 UST Field CAP 4 J 0.32 J 0,3 J 50.22 15 J <56 149 J 30,9 J 11.2 J 160 J 190 J 2L Standard (py)Lj 1 600 600 SW 80 200 2,000 0 05 0 005 0 05 200 0 5 5 0.005 300 3W 0 05 6 200 200 1 30 Notes GCL-Gross Cmmtaminatmn Levels . Standard North Farohna Cnoundv aw Qua lily Standards (GWQS) Resul to repuned in pglL d1 reporting limits me at the method detection limn (MDL) µyR.-miupgYams per liter 1-Estimated value between the rqF muig limit and MDL NA -Not Applicable Cnnundwaler sundarde taken from lu 1y 15, 2008 Ouideli ties for Assessment and Cor reru ve Aetim for UST Release. Analytical method 80218 used for volatile organic compounds analyses on March 2tlW9 Analytical method 8270C wed fur pvlyn uclear hydrx4rhon ana lvscs on Alnrch 2004 Hold value indicates detections FPA-Environmental Protection Agency 3of2 Appendix C3 Historical Summary of Groundwater Results VPH & EPH TravelCenters of America 1101 NC Highway 61 Whltsett, Guilford County, North Carolina Facility I.D.: 0-028186 Incident Humber.. 20064 Analytical Method VPH EPH C9-C22 Aromatics (Adjusted) C9-C18 Allphatics (Adjusted) Contaminant of Concern ll_) C5-C8 Ali hatics x C19-C36 Ali hatics SYi Sample ID Date Collected Source Area Incident Phase USTMW-1 9/2/2009 UST Field CAP <9.7 150 J 1,030 700 10/5/2010 UST Field CAP NA NA 930 NA 1/612011 UST Field CAP NA NA 600 NA 4/1412011 UST Field CAP ND 458 1,757 945 7/14/2011 UST Field CAP a100 259 1,262 622 10/19/2011 UST Field CAP 52,6 J 104 830 0 11512012 UST Field CAP <200 205 1,323 377 411212012 UST Field CAP <100 <96 1,060 -26 7/24/2012 UST Field CAP <100 137 566 85 111512012 UST Field CAP <100 315 1,007 789 5/22/2013 UST Field CAP <35 394 765 1,447 USTMW-2 9/2/2009 UST Field CAP 19.1 <36 1,030 150 10/5/2010 UST Field CAP NA NA 1,540 NA 116l2011 UST Field CAP 30 31 1,510 360 4/14/2011 UST Field CAP ND 188 356 277 7/14/2011 UST Field CAP <100 176 473 467 10/20/2011 UST Field CAP <100 <110 a210 124 1/5/2012 UST Field CAP <100 B73 2,763 1,584 4/1212012 UST Field CAP <100 000 712 299 7/24/2012 UST Field CAP <100 <99 141.2 155.8 111512012 UST Field CAP <100 4,330 2,460 9,780 5/22/2013 UST Field CAP <70 7210 4,112 22,460 USTMW-3 9/2/20091 UST Field I CAP <9.7 <36 110 J <12 USTMW-4 9/2/2009 UST Field CAP <9.7 9,300 6,220 26,650 10/5/2010 UST Field CAP NA NA 387A NA 1/6/2011 UST Field CAP NA 1,100 1,810 3,946 4/14/2011 UST Field CAP ND 1,070 1,600 2,130 7/1412011 UST Field CAP 45.9 575 618 1,273 10/20/2011 UST Field CAP <100 1,040 494 559 11512012 UST Field CAP <100 1,620 946 1,570 4/12/2012 UST Field CAP a100 545 589 1,010 7/24/2012 UST Field CAP <100 457 396 308 111512.012 UST Field CAP <500 1,270 3,212 3,805 5/21 /2013 UST Field CAP <35 1940 1,109.7 4,590 MW-6 3/31/2009 UST Field CAP =9.7 42 J 82 J 36 J 5/21/2013 UST Field CAP MW-9 3/31/2009 UST Field CAP <9.7 1 <36 1 120 J <12 4/14/2011 UST Field CAP Well Buried or Destroyed MW-9D 10/20/2011 UST Field CAP <100 a110 410 146 1/5/2012 UST Field CAP <100 <9B <198 <98 4/12/2012 UST Field CAP <100 116 <199 308 7/24/2012 UST Field CAP Well Buried MW-10 3127/2009 UST Field CAP <9.7 51 J 78 J <11.6 5/22/2013 UST Field CAP <35 <96 235 <131 MW-1 i 3/31/2009 UST Field CAP <9.7 <36 130 J <12 101512010 UST Field CAP NA NA 200 NA 1/6/2011 UST Field CAP NA NA 190 NA 4/14/2011 UST Field CAP Well Buried 7/1412011 UST Field CAP <100 <100 <200 a100 10/20/2011 UST Field CAP <100 <99 <199 137 1/5120121 UST Field I CAP <100 <98 <198 <98 4/12/20121 UST Field I CAP I <100 <98 123 J <98 Appendix C3 Historical Summary of Groundwater Results VPH & EPH TravelCenters of America 1101 NC Highway 61 Whitsett, Guilford County, North Carolina _ Facility I.D.: "29186 Incident Number.. 20064 Analytical Method VPH EPH C9-C22 Aromatics [Adjusted] C9-Cl Aliphatics (Adjusted) Contaminant of Concern (}� IL) C5-CS Aliphatics (x) C19-C38 Aliphatics ty) Sample ID Date Collected Source Area Incident Phase MW-11 7124/2012 UST Field CAP c100 <97 <197 <97 11/5/2012 UST Field CAP <100 124 J 156 J <100 5122/2013 UST Field CAP <35 <96 178 J <131 MW-12 902009 UST Field CAP <9.7 49 J 920 150 10/5/2010 UST Field CAP NA NA 990 NA 116/2011 UST Field CAP 14 NA 1,270 280 4/14/2011 UST Field CAP Well Buried or Destroyed MW-15 3/27/2009 UST Field CAP <9.7 <36 86 J <12 5/2212013 UST Field CAP <35 <95 <175 <130 MW-16 3/2712009 UST Field CAP 1 <9.7 240 89 J 11 J AGM-RW 9/2/2009 LIST Field CAP 63 37 J 790 74 101512010 UST Field CAP NA NA 1,280 NA 1/6/2011 UST Field CAP 110 NA 1,120 247 4/14/2011 UST Field CAP 96.7 152 2,218 163 7114/2011 UST Field CAP 81A 790 3,017 2,650 10120/2011 UST Field CAP 128 370 2,147 683 1/5/2012 UST Field CAP 46.6 J 476 2,705 1,269 4/12/2012 UST Field CAP 66.8 J <98 1,977 27 7/24/2012 UST Field CAP <100 246 1,211 403 11/5/2012 UST Field CAP 117 J 414 1,711 1,156 5122/20131 UST Field CAP 88.7 J 1920 2,520 J 6,249 J 2L Standard (pg/L) 420 42,000 1 210 4,200 Notes: GCL-Gross Contamination Levels NA -Not Applicable/Not Analyzed 2I_ Standard=North Carolina Groundwater Quality Standards (GWQS) C9-C22 Aromatic (Adjusted) Results reported in pg/L & reporting limits are at the method detection limit (MDLI C9-C18 Aliphatics (Adjusted) pgfL-micrograms per liter BRL-Below Reporting Limit J-Estimated value between the reporting limit and M D L EPA -Environmental Protection Agency Groundwater standards taken from July 15. 2008 Guidelines For Assessment and Corrective Action for UST Releases Data included on this table not generated by or on behalf of U R S Corporation - North Carolina (URSJ has been taken from documents prepared and submitted to the NCDENR by Others and is included only for ease oFreference: U R S does not assume or accept any responsibility or liability for the quality, accuracy, or completeness of the data included on this table that was not generated by or on behalf of URS. %ppendix C4 Summary ofGroundwaterSampting Rewlls 1'PH & FIN Tra►elCtnttrs of America 1101 N(' Iligh%a5. 61 Whitselt, Guilford County, North Carolino Facility 1.0.: U-029186 Incident Number- 30318 anal)tical 5lcthod 1 I'll I:I'll -19M C9-C22 Aromatics Adjusted C9-C18 Aliphatics Adjusted Contaminant of Concern /L C5-C:8 Ali hatics a C.19-C36 Ali hatics Sample ID bate Collected Source Area Incident Phase CSAMW-I 41117-009 Diesel Dispensers CSA <9.7 e36 1101 23 J 106/2010 Diesel Dispensers CSA NA NA <92.9 NA W14/2011 Diesel Dispensers CSA <35 <85 <135 <67 10/19/2011 Diesel Dispensers CSA <100 10l <200 150 115/201? Diesel Dispensers CSA <100 <100 <200 <100 4/12/2012 Diesel Dispensers CSA <100 140 <200 <100 11/5/2012 Diesel Dis nsers CSA <100 <2000 35.7 J 27.7 J 5/22/2013 Diesel Dispensers CSA <35 <95 2441 <130 CSAMW-2 4/1/2009 Diesel Dispensers CSA <9.7 49 J 130 J 281 10/50..010 Diesel Dispensers CSA NA NA <92.9 NA 7/14/2011 Diesel Dispensers CSA <35 <56 ¢122 <44 10/19/2011 Diesel Dispensers CSA <100 <97 < 197 134 1/5/2012 Diesel Dispensers CSA <100 <100 <200 <100 4/12/2012 Diesel Dispensers CSA ¢100 <96 <196 <96 111512012 Diesel Dispensers, CSA <100 <2000 4,100 39.6 J 5/22/2013 Diesel Dispensers CSA <35 <95 194 <130 CSAMW-3 4/1/2009 Diesel Di ensers CSA 17 J 1,200 L820 3.960 10612010 Diesel Dis cns�rs CSA NA NA 689 NA 7/14/2011 Diesel Dispensers CSA <35 <56 <122 <44 10119/201 1 Diesel Dispensers CSA <100 166 < 195 282 1/5/2012 Diesel Dis nscrs CSA <100 149 <226 282 4/12/2012 Diesel Dispensers CSA <100 <100 <200 257 11/5/2012 Diesel Dispensers CSA <100 <2000 4.100 49.4 J 5/22J2013 Diesel Dispensers CSA <35 <95 <175 <130 CSAMW4 4/1/2009 Diesel Dis nsers CSA <9.7 501 1401 -<12 101512010 Diesel Dispensers CSA NA NA 1 10 J NA 7/14121)1 l Diesel Dispensers CSA ¢35 <56 r122 r44 10/19/2011 Diesel Dispensers CSA <100 <100 <200 101 1/5/2012 Diesel Dispensers CSA <100 <100 - 200 <100 4/12/2612 Diesel Dispensers CSA <100 <98 <199 c98 111512012 Diesel Dispensers CSA <100 <2000 <2.100 <2.000 5/22/2013 Diesel Dispensers C'SA <35 <95 <175 <130 MW, 4 411i2009 Diesel Dispensers CSA <9.7 <36 t 59 J <6.4 7/9/2013 Abandoned M-1; 3/27/2009 Diesel Dispensers CSA <9.7 <36 k6 1 r12 5/22/2013 Diesel Dispensers CSA <35 <95 1,� l30 DDMW-2 I063 2006 Diesel Dispensers LSA NR 1.900.000 800,5,11, 6.400.530 9/2/2009 Diesel Dis users CSA -<9.7 <36 4611 162 12/22/2009 Diesel Dispensers CSA <9.7 700 1.65o 3,150 101512010 Diesel Dis nsers CSA NA NA 291 NA 7/14/2011 Diesel Dispensers CSA <35 201 708 363 10/19/2011 Diesel Dis ensers CSA <100 3680 -1,283 9.523 1/5/2012 Diesel Dispensers CSA <100 986 1,532 1,778 411212012 Diesel Dispensers CSA <100 147 525 583.4 l 1/5/2012 Diesel Dispensers CSA <100 L210 J 9&6 J 999.3 5/22/2013 Diesel Dispensers CSA <35 1090 522 2120 2L Standard t 1 420 41000 210 4.200 l oF2 Notes GCL-Gross Contamination Levels C9-CUP Aromatic (Adjusted) 21. Standard=North Carolina Groundwater Quality Standards (GWQS) C9•C18 Aliphatics (Adjusted) Results reported in NglL - micrograms per titei J-Estimated value between the reporting limit and method detection Iunit (MDL) NA -Not ApplicahlefNot Analy7x"t Available Groundwater standards taken from July 15, 2008 Guidelines for Assessment and Corrective Action for UST Releases EPA -Environmental Protection Agency Data included on this table not generated by or an behalf of URS Corporation - North Carolina (URS) has been taken from documents prepared and submitted to the NCDEN R by Others and is ineluded only for case of reference, URS does not assume or accept any responsibility or liability for the quality. accuracy. or completeness of the data included on this table that was not generated by or on behalf of URS, 2of2 APPENDIX ❑ RECEPTOR SURVEY AREA PROPERTY OWNER ]NAMES/ADDRESSES* Former BP Site No. 01363 1101 NC HWY 61 Whitsett, North Carolina AREA MAP INDEX OWNER NAME/ WELL NO. ADDRESS TYPE OF PROPERTY TYPE OF WELL DEPTH l TA Operating Corporation Business None NA 24601 Center Ridge Rd. Fonner BP Site No. 01363 Westlake, OH 44145 1101 NC HWY 61 2 Morris L. Crafton and Pace Vacant Lot None NA Distributing Company Inc. 7230-7232 Greeson Rd. 150 Stratford Court Winston-Salem, NC 27103 3 NC Department of Transportation Vacant Lot None NA PO Box 14996 7251-7299 Pace Dr. Greensboro, NC 27415-4996 4 NC Department of Transportation Vacant Lot PO Box 14996 7200 Pace Dr. Greensboro, NC 27415-4996 5 TA Operating Corporation Parking Lot None NA 2460I Center Ridge Rd. 7201-7249 Pace Dr. Westlake, OH 44145 6 Kim Haley; C.G. Wheeler; J.D., Vacant Land B.C., Susan Topolka: and Laura 1100-1120 NC HWY 61 Wheeler 7210 Whitsett Park Rd, Whitsett, NC 27377 7 James and Francis Workman Residence Chinking > 300 ft 1010 NC HWY 61 1010 NC HWY 61 Whitsett, NC 27377 8 David and Martha Ingle Residence Well located on Unknown PO Box 176 1008 NC HWY 61 adj. property (7130 Whitsett, NC 27377 Gusenberry Rd) 9 Charles and Robin Moschler Residence Drinking/irrigation 125 ft 1000 NC HWY 61 1000 NC HWY 61 (casing is PO Box 254 25 ft) Whitsett, NC 27377 10 Etta L. Ingle Residence PO Box 24 1019 NC HWY 61 Whitsett, NC 27377 11 G.D. and Linda S. Ingle Residence PO Box 142 7205 Greeson Rd. Whitsett, NC 27377 12 Ronald Lee Key Residence 1017 NC HWY 61 1017 NC HWY 61 Whitsett. NC 27377 P'9"m ecu) c'%0i j . MN. W'huWO. NC'dtepnrns'Deeembv 20W R"'.AppendictsAppendix F - Recepim App f-Property Owners 3-ft doc Pagel o f 4 AREA PROPERTY OWNER NAMES/ADDRESSES* Former BP Site No. 01363 1101 NC HWY 61 Whitsett, North Carolina AREA MAP INDEX OWNER NAME/ WELL NO. ADDRESS TYPE OF PROPERTY TYPE OF WELL DEPTH 13 Timmy and Amy George Residence Drinking 194 ft 7207 Greeson Rd. 7207 Greeson Rd. Whitsett, NC 27377 14 Kibble and Karen Davis Residence 7211 Greeson Rd. 7211 Greeson Rd. Whitsett, NC 27377 15 James and Lana Latham Residence PO Box 1442 7217 Greeson Rd. Burlington, NC 27216-1442 16 Deryn and Angela Rehm Residence 7223 Greeson Rd. 7223 Greeson Rd. Whitsett, NC 27377 17 United States of America Residence Suite 104, Henderson Bldg, 7225 Greeson Rd. 2301 W. Meadowview Rd. Greensboro, NC 27407 18 Steven and Diane Norton Residence Public Water, no 7227 Greeson Rd, 7227 Greeson Rd. well PO Box 271 Whitsett. NC 27377 19 Bessie G. Thomas Residence Drinking > 200 ft PO Box 212 1015 NC HWY 61 Whitsett, NC 27377 20 Cornerstone Baptist Church Church Drinking > 200 ft 5736 Inman Rd. 1.005 NC HWY 61 Greensboro, NC 27410 21 Kimberly Haley Residence 7210 Whitsett Park Rd. 7210 Whitsett Park Rd. Whitsett, NC 27377 22 Joseph G. Whitsett Residence Drinking/irrigation 140 ft 7218 Whitsett Park Rd. 7218 Whitsett Park Rd, Whitsett. NC 27377 23 A.D. Jr. and Jeanne Cobb Residence 7222 Whitsett Park Rd. 7222 Whitsett Park Rd. Whitsett, NC 27377 24 Richard H. Fenwicke Post Office Sanitary Unknown (Louis C. Fenwicke Trustees) 1001 NC HWY 61 (washroom). 5014 Hooper Rd. Bottled water McLeansville, NC 27301 P UWTruj ec"NC%0 116 1, MN. Whiuert, NC1RrNrWDe rnber IKO Report'.AppendicesAppendix F - "tor f-Property Owners 3-115 dou Page 2 of 4 AREA PROPERTY OWNER NAMESIADDRESSES* Former BP Site No. 01363 1101 NC HWY 51 Whitsett, North Carolina AREA MAP INDEX OWNER NAME/ WELL NO. ADDRESS TYPE OF PROPERTY TYPE OF WELL DEPTH 25 United States of America Residence 2301 West Meadowview Rd. 7225 Greeson Rd. Suite 104 Henderson Bldg. Greensboro, NC 27409 26 Charles and Carol Baxter Smith Residence Drinking 110 ft 3291 Herrenhut Rd. 1205 NC HWY 61 South Lithonia, GA 30038 27 Nancy C. Stewart Clapp's Chapel Drinking 370 ft 3801 Halts Chapel Rd, 1301 Piney Grove Rd. Greensboro, NC 27401 28 Clapp's Chapel Residence Drinking PO Sox 98 1305 Pinev Grove Rd. 1301 Piney Grove Rd Whitsett, NC 27377 * Source: Guilford County Tax Records. P �BKPro WSNCW1363, MR. Wh11selt. NC'RrP0mVetemhrr _ Al 9 RrpwtAppcndi�na Appcndix F - KecWur•.App f-Nopem Dwnefs 3.06 dw Page 3 of 4 Whitsett Park Dr. G Rid_. VR 1--- - r-- -- _ 1 R R,R R R ' R Vacant _ r sgn Q LE EN BP Site No. Vacant Private Potable water wall 01363 Property Owner Index No. �l r� + (see table 8) L' C Commercial Usage ve ,, � C O 3 i j r R Residential Usage r ' Intermittent 5treom Interstate 40/85 9 ❑ 400 -�- APPROK SCALE. ft. AS SHOWN Receptor Sur RP Stntinn Mn APPENDIX E WELL ABANDONMENT RECORDS WELL ARANDQNMENT RECORD N"I'lli Caral ilia Ikparlmenl nl'Etiviruml)em and Naitinil R")nrccs- Division t rIA'ntur Quiliity ► ELL CON'f RAUMR CERTIFICATION N 2012 I. W f A. CONTRACYOR. Tim Thomas Weli C unuauim (Ind it•ittrrtll NWnr - SMI)ACCQ Inc Wrll C'+rnlracltx C'ofnlxlln Nnmc ti'1'NF.I_ I' AODkI:Sti 9008 North field dr rant Kill ssc 29707 -- Ctq or lawn SUR l.Ip i'otic I Y- y[704j 309-6645 Am1 cock - 1lhune numllar 2. WELL INFORMATION: 41'l'E 11'l l.l.It1 AI tir t(lplicahlel. ow-111 . ti•IATY W K LL PER1IITH (il'applicalvlel_ COI N3'VWf,I.I.11KUNIIT9ItI'appIioahk) I)W'U ar[37'IIIit 1'l:lifiil7-# [;Capplicahicl W F 1.1. I-"'. (I'hcck appllrehlr w t I ® llnultorinR ❑ Rexlder hit ❑ \lunielpnllllufilic ❑ lntllttitlfrlllC'nemrlenln] ❑ :IRri[ullurlll ❑ It"nWILY ❑ Injection ❑ irriRniiun ❑ [lIhl:r 0I'I usu 3. WELL LOCATION: COUNTY -Guildford— QUA V ANGLE NAME NEARES r rOWN. T;l taktt 1101 ft-fil / I-85 whittaatt (Streerknul Mkox. 4UnllWr, ('ottntunrisY, Sttilri1tKiMII, IA+t No..I!vul, /+p CINIc1 ro l"04 il[A I1111C I LAND S FX I IN6. ❑ sIoN ❑ Vail,;+ ®I lot ❑ Ridge ❑ CHlWr - 1('hcck appropriate setting) LA I I UDF 39. 527596 Mrk% he it+Scprcc�, - nnutrcz, tn,nkh, Or in a LONGNIA)F.-99.141969 dccinml rnm+nt [al![tudcllOnRllude srwrrr: ❑ GPS ❑'i'0pakrllnlllc n111p /Erie (Hum of it L•11 Ill fill he shlosvil On ❑ t 1,Sf S r(+prt male (rill/ Ir1luclmd In thus form II tlw ltshw GPS 1 4n. FACILlT1'• Ili(nturx uNlw ItlWnuve WiPM tlec ,+ell rR Incaud t'nergrletc J;r mu.14b III'll rrsidcnftil well. +1tip4u: crxteplele 4b, well +mtter inTnnmunl tetllt.Y Fr1('11.CI Y I iit11 apj)fit'nhlcl NAME 0l` 1'ACII,f rY ]format BF Site M 01363 S'I'Ri:li r ADDRL$5 1101 NC Highway 61 Whitaatt KC Citg 0r Trnw1 slate /Ill ('1nll• 4h. CY1WACI' PI:R.SONIWELI. ON% F:14: NAIMU URS Snu--v I AI117R1:.55 1600 Rariemter park tar. Ste 400 Morr 6. WELL ULTAli S: a rnlal Devh: 23' - 1. I]tame4x 2" h. Water I.Weel III00 ►' hleHSllrlllk I+nint). Measumog Imint n _ ._ __ R uNivc lunti 1arl;tCe 6, CASING: IXot:111 Diameler II C'unPill; ut_•(1iIt Iirknomly _ R All h Citsing Remomd- ll. 0 in 7. DISINFECTION: la$ (Ainnart ol'654:�7Mb calcium 11ypachiorilc us.•d) H. SEALING MATERIAL; C;=cut 94 1h. Waier. 7 nn HVILOMIC lb l}•pc. ©4ftlm 01161cts Wslcr _ _ _ gal [}Ihrr type mnlerinl Amoum 5itlydL.EMC111 C."ans 111 Wnter -_ __ p, 4. EXPLAIN NI Fi'IIOD OF FHPLAC LM F NTOF WVI'l RIAL: trimsnied from _t:he bottom _up-- R ►vELI-DIAGRAM fern►) it dchailed 4Wich of the well nH Ilk Ivek urthis rorm shtn)ing Iotal dopih, depth and 0lameler of-vrcens 0rany rclstaining ill llle well, grmvi inlenal. Intetcals of cn5ing Ixrforations- and depths anti kvKs of ICI lnuierialsuwd II. DATEH'ELI.AI1A%D0NFI) _71942.013 _— I IX IIVAF.H�'f hit]1FY IIIA1' IIIIN WI..I.I. WAN ABALIH114L•R INkt 1314 ]A,%('I- ►1'1 Ili IS.-1 LC AU A', Wf--L.1. [-I]tvSTRUCCION SI',INL),%XDS- .►ND I1iA l r► C't11'1' of, I lI1S R1i('01413 HAS 41:L%' I'Ht WII*-D I0 Jill: LYIi! 1. t)Mr.WH 7/12/2013 tl.N►Il1aOFC Litt It11.1)►1Ft.l.C(ISIkm IUH 1)►I) �I(�1,111'HlI1FL'}tlL'ATF:11'£L.L[ll'~TlEH:lflAtill[]M1ftiC'flll:lYF:LL Il.►rF: I L•c pnrele well (moicr tenth ba WF netli)idue! ttha %ojl)andmte I•te he+remdemijil "01 ilI :q"ikriirtne4 %vaIF I sal NC ;m, U, 0111.1 PRIYTF1) AA51E (IF I'EWKYN ARAtNPUN ING I I I E 11EL1. Ile, NC. 2 5uhIttit 8 roll) 10 the 0rvner and the 0rialnal to the Divisfnn aT Waler []unllly Ivilhbl 30 thl)s• Fenn GW -3U Aihl: infornlxlMn 111tnnkrmerll. If+17 ?►Iull Srn•Icr [infer - Ralriatt. V[' 27hrriz1Gi7, Phemr in. [+}i91 733-7p1Sr51 4Ci$. [;c1 St[](1 f WELL ABANDONMENT I C RD Noilb CaR)illla 0cpunme111 ttl'I.n► insnlnenl fort! Natural Resources- Division ui' 14'alcr Quality - WELL CONTRACTOR CERTIFICATION # 2012 1. ► EAA. CONTRA[-fC)tf: Tim Thoma■ Wei Coll etat- (Iadit ideal) Name BARDACCID Inc 1►cl1C'rxltruttnrC'nntplln} Name S'rR1:l i A1) wrss 9088 !forth Field dr Fort hill _ sG 29107 L'11'. ter 1't11tn Slow Zip C(x1C 1 1- (704) 309-6645 Area code - Phone 1ILL11111CI 2.11 ELL INFOR►lATION: SI 1'F ►VEIA, il) p I If applicuhle) BV-1 STAL I'E 1► ELL PEILNIIT k (11'Ilpplit:ahlcl- COVN'11- ►V rL1, IlFR4111' a I ifstip]Icab k3 17H'Q ur OTIIF R PIE R7*IIT A ttf appiicahlel_— ►►E1.1. l SE (CIwelt applicable use) ® 1Ltnit+rIll nR ❑ ReMdenllol ❑ A1unlripnUl'nh1lc ❑ InduslriallCnntmercial ❑ Agricullurxl [] Recovery ❑ Injerllori ❑ Irriktaliurl ❑C )[her (hvl use) 3. W EEL LOCATimr: COUNTY Guildford QUAL)RAACLE' NAME NFARRST 10 N 111hiteett 1101 HW.Y, 61 l I-05 Whitteett I\It el•I.1t 1x1d \dt kv- Nun lhrr, I nu ntr 1110V. SI All Ii*I M4141. IApr \u.. I'lowu 1. firl E 114Ic) R)1'L)(iRAIll IIC 11-AN1) ti1:1'I I N C i. ❑ Sloix: ❑ VAicy ®Mat ❑ ILtdkc ❑ 014cr [Check approitriutc vrtsing) LA'IITIi1)F 39.527526 Gins he.11dtytccs. — — — - amides, xecul+ds- , r ul a LONC I I)DI:-99.141968 dcotwi fnrnl++t Latilude4anAltode saume: ❑ CP5 ❑'CopnRrnnitir mail (l.nrrwk+n uf'w4+11+erns? be shviea art n IlSf1h'rryx+map reed urrrrrl+ek!M rhlsfinr'ru {fmrr nvoik 4sG FAC't1.111% IIIe rutntc I+CIIIc hamt%NA where the Ach ■ Imined ('nuydctc Ju Wki,11, It 11 rc+id-IIal well. skip 4o: twinlikit As- n e11 tm•ner Infnrtltation rutlr. ) FAC'11.111' 1D 41il'appiteshle} NAMF OF I'ACILITY Foaroer BP Site # 01363 STRt-.vrADp141:55 1101 NC Highfrax 61 ttfhiteett� RC L'n} ur'Tn►v� titnle Gp Loy h 4h. C04NTAi-I' PF:R.tiONM E.1.L OW N 11R: NAME VU SCH1:f:7 Ail[)1L1 tiff 1600 Perimeter Park Or. Ste 400 Morri a. ► 'I_LL DE All h: u. Tntal lh'ittln 23'- - it lhamt er ; nt. h ►►'titer i.evel 113ehs►t NJ01tru(1ak 1'uinl). _-•- -- 1't-- W1011IT1119 Ixnul N - _ _ 11 Ith s%e land suriacc 6. CANINGIxnyllt Diam Ycr ,I CaKulg Depth Iif knimn) II 4" ul 11 C piny Removal. — -- Il 0 7. DISISIW(MON: le: IAmotinl o1'6Wp-7S°..calciem Irypl+eldrotie used) 8. SE,►I.IN(.7iKrFRiAI.: Neel C EAM %anr:l C'rMent Cement 94 I)S LCtitent`— Ili Water_ -7 —�-- gal water Vol autQnitr llentonitc Ib TypO []Slurm. ❑t'clkHa water_— _ -- — Pat L)lhrr 1\ ,-r malcrial Amount 9. EXPLAIN N11E1'1101) OF 011PLACEIN1F NT OF NIATF.RIAL: trim4 ed from . tho bottom UP, 10. WELL UTAGUNI Draw a dclailed sketch of the ►rrl} tin tltc buck ul' II.:, fnrrn shoe ing Iola dclnh, depllt and 6immHer of sts"irt (iI-any) rent 0InInr in wile ►re1i, gravel interval, intervals of casing perforations. and CIO Pill s and tyIV% oC 611 Maierlals used 11. DATE ANELL ARANDON D 7 9 Z013 I IX) III: EBY (TRI IVY IIIA I I IIIS WI.l.l. WA.S ABANIH1VI:1) IN ACCORL).►t`( I 1►'11$115A WAt' Zt', Wi.1.t. Ut VNS't It 0C..110N SIAN ARIK A)+WIIIAt A rrtl'� I I! I I IIS ItEC01LU ILAS 131'l:k 11ROVI1)h1;l 11) 1111: 1Y1,tj,1)11'i1:FL. 7/12/2013 SIGN ► I t HE OF C'I:R'1'JFIEll ► FLi.0 ONTHAL"I•C)H If ►1F. tilC�\,1IIHtiL)F I'R1►'A7F:11'}I.I.[)►F1Vi:R.Ipdti1)gl/l--tiCi tFtF:1►'F:t.L n;/1'}: 1l llc pritmc ntdl imsics tslust I <ws mlhvullwl wlx+perssmlly6witinns lim1 tr rrmdclnuo well ut attetx uIlLe with 15A NVAC W Cl I I I I PHIVIED NA NIF:01F 11IKMK N AUAtiDON ING I111K W L1.1, i11a, NC. 2 Suhnrll x eup► to the uvrnrr and the nrlglnnl to the t]leisinn of It slier Quxllly Within 30 days. 1 orm (iW •30 ,IIIIt: Inrorot alIan Mtlrlakernen1, 1617 hi it it Sery Ire C-calm - RnWith. NC 27699-1617, 11hone No. (711)) 733-7915 e►t S(rA. Rev. 5105 0-- +1 1 Mt ` ICORD " Mull' [';unlilin De;%triln4ril slITMN iruritllcm mtd Nnlnraf Resources- Divisutrt of 1►;lter Own iiv - - ► ELL CONTRACTOR C'};H'!'11 1C,�`!'1[)N # 2012 11 11 E LI, r ON I RM 'Itl[t, Tim Thomas %% c I I ( ,II)IY,ILif,1 111idit idult11 Wit SAEDACCO JAC -- 11oI C"sulletc[ia CIIMITatl NN:1111r Sl'kl.l I A1)17RI.N6 9089 North Field dr Fort Mill SC 29707 — - ^ {'il± ur E lilt t5 tiwl4 lip ('sxJr i S• {704)30R-6645 A)C.1 tutk - !'louts IIll III ITT 2. ►►1•:I.I. IN FOIL M. k*j-u )•i: ti['I F: 1► I.I.I. I!) N i11�1illl,IlC';1IfICl _>l111—� Cell ii71 ► EI.1.11ERMII N tii'applicthlel_ . ll1►'OlOr0`111Fit JRVHk11'Tit (II'lip111tCahlel WELL l SE (CIrcrk.LI-4A rirhle use I ® M111ihulilig ❑ Iicsidelrlinl [� ]lunirlpalll'nhlir ❑ I,rdu tiri+711r'nmutrreinl ❑ AlLrirttllnral ❑ Itnmeo ❑ [nieetinrt ❑ lrrientiurt ❑ 0"wr I Elst Io0 COI IN I Y Guildford _ [ 1I1AF11{ANULI N V01 !dFAR1-SE I'MYN• MILtaett 1101 RW 51 --95 Nhittaett i%t1 ect eknast %4v%% Vumltcr. t t%llnl, lnnlStiwl{P7,tn. 1 1•, I{)I'r1{I AIll IIC1LANt)sl'1 I M i ❑ Slap. ❑ V0110 ® flat ❑ litdg s ❑ ()thk!l 10teck i1jlr;ollrinte seltlilg] l�lTRi,l)L 39.527595 �fa1 t+su,tla3tltr+. 1111wPILN. I 11V{:ITI'1.11:—99.141960 dcril,cd fI.n11 LitlitridellougHtide srlurrr; [] MIS [j [(IIMI, I'll pl1Er map 11"fit ulinvr ul so V11 A11r%I he sbfotrli all rt I LNGS 14yxl InalI PInd rititn IteditI rlrt.s final y+nN 113ing ;n. I' 1[ 11, U FY Ile• 1u,1,1t' o1'1tw twn141e- %11cnc 111C WCII 14 ltie.IOM ['unilArit; 1.1 41"141. a e•111e+illdi rrll 4114 $11. cumplt�sr its Writ owtio mhln,laluat oalv.l I M ILFI'1' II]MIt- ai1111r.16k) L� \ Ali O1. 1'ALl1.1I Y Farmer Hp Site J. 01363 — SIR11-1 At111Hl.SS 1101 KC >iray fil_ Nhiteett NG Cog at ! will — — SkIle /qi t ,xlr ah. CON IA -1 11 F. it I%ON INN, F. I . 1. {)ll til:It: N A M l 1)RS 5fli1 l I A11!)I{I xy 1500_"Pe setae -_Park or. _Sta 400 Mori it 1'ut:il Dt:ptli: 23' _ li" 1)11111t1t r _4" — In. It Water 1,41YI IliCluts MetirllralL 1141in1l. h100Sit tuly ll01111 w . It alxi%-c land iiurlitce. fi. C.►NINr;: I.crii+tlt Diameter :1. ('3111 llt! I.'h11111 tii krH 51111J- I� 4" ut h C';r4n1c Halsntztl 11. 0 in 7. 111SILNI-FCTION! 102 i Amount o1'6 Ni 75'!;, c;ilcIitln It%'IXKI LIM610 US,%]) al. SEALING ►'IA'l'I:RIAL: C onoll 94 Sand Crnlrur Ill Comm It, W;rter 7 _ _ g:d Wider gal. Nenlnnhe l3emointe III 1's,w [] Slurry ❑Pellet% 11 mer _ _ — g71 MUL 1'VIx Mmelml Anuurm '1. FXI'1.AIN N1F:11101) OF EMI'llACF:]!CN I' M 14ATI?4.[AI.: trimrmi ad from the bottom up. It). 11 l: L L ll AC HA INI lJr ll n delaikd wketrh of Il1ti ucll nn tltc lxtck of tl.. ti limn :halting lntal drp[h. dcpol:rnd d1311100 nl'!MCOIs {d' atry) renla111ing w 111e well, #1w el Inttnit), Intm;d% td casing llerlixlitiow. itnd dclNIII, and Ivllest,l ]ill I w I ol I Lsk 11'al 11. 7/ 9/2013 r'N 1111 k114) ( I klItl• 11JAI �5itls "II.I.I 11 Is WAS1"N11) 1N :It•t't]I01.1,U1'I ? It I5:1t 't . W1 L1. [It"\tiiHl7i 11is� tit l�i).a1115. 1L 1 IIJAI :1i'[)1'1' t11 i15 R1•.4'01M tIAS 111.1.V VR 5N IM l) 1 [1 Ilil: 11'I•I 11111 NI-k. 7/12/2013 �Ic ti t I I kF; [1F' {'l H'I LPIF;h IYFa.1. r"[1\Tit ►['1'111i DA 11-- xl[,\ I t'fit, OF pHu'A"I F: II'F:1,1. (MNF:1t "111.►NDONING, I BE M Y.. Ll. 11.1 r1 i..rt;H¢ r+-1:II ML 110 n401Ix nn ,n,h•tdu:,l n•lu, ikny�{p{1{y uh:,i,ds,n. Ill lit ltI tcs(lrinud t„•li In aec, rslarnc W idt I rA 'K1 A[' R, fit 13.) PHI\ 11.1) NAME OF I'F:liSON ABANDONING l Ilt; 11'I:LL ilia, NC. 2 Sit n cull► to the uirml' and the nrlglnsll to the Uiri�hnr nT►Velrr i�+rxllly sVithln 3[1 rla * l'untl (4W -3p I1in: [nrnnuathln Vllttutti:rnleslt. 1617 Midl Service Center — Huldgli, NC 27677-I617, 191unr No. (919) 733.7015 r*.t 569. Rv% 5.11% k r r WELL ABANDONMENT RECORD Nis rtIi Caro)ina I)emirtnient al'En■ irnnnienI and \ai►fral ltesculrves- f?itisinn (tl- %Yater 011isIity WELL CONTRACTOR OR CERTIFICATION 4 2012 I."VIA. ('UA I'19.1[ I'014: Tian Tho:nar We II (' Nis troclor I htditMint 1) Narnc SMDACCO Inc _ Y;oII C'tanraemr Corltlxlnr kame SI•RFf:l-.A1)1)Itf_yS 9088 Moicth Field dr Fart lain BC 29707 - Cilr of I nlut ilnlr Zip Oide I 1 (704) 309-6645 Ir a Crxlc - lrixmc mi nitel 2, 1► F:I,I, I tiVOKh3.1-E'l(),.- 11) p llf:tppltr:I11tot UK-4_ ti f',1'F'F: 1l C1.1. 11F.RM1'I' a I if nppIlealdal. (-OUNTI 11'F:1.1. I'F RNMI v hl'applit ah(ti•) M1Q nr0111Fit PEItlil'll-a 11fLipp llruhlaI 11 Ei.L I SE t0wck apphrahk n■ei ® xSunitolitty; ❑ ltc.itlen1jnE ❑ It unlciliniN'uhlip ❑ lerhrx[r 4110 minerchil ❑ .%grirtlllnnll ❑ Itrrlt■rr� ❑ Injrrllun ❑ Irrl{;xf Fin ❑ t Tth r r t I im tise I 3.11'F;IA- IA)CA7 ION: C01IN l'1' Guildford 011AI)RANUU NIA M. fwEAKI.S l RJWN. Whiteett _ 1301 I3►ry 61 1 I-85 )rhitteett _ rtillecrllt+:nl k;uIIC. tt"tiller l',auannlily- tiuleln•rs4oll 1 ,a tin.. Harrel, /ip Cl%kI It11'l)C;RAftlllC" 11-ANI1 4I I I l\ii ❑ ~lope ❑ Vnll ti ® I`hIL ©7Cldge ❑ 011Ivr II'heCk :lPltruf,riWe M ilit! I-AIIIIII)F 39.527596 AInv heIIIJCEIcc.- IIIIlimc4. W— oInk a. or [I1 :t I.t)MIIUl)i:-99.141960 deciiiW6intwr Iirtf[u[kllonf[ihrdesnurre: ❑(if'ti ❑ lttpnkrnplllc mtryt I ucrrrrtOf? Of It &'Il,rr,ru he s)revtrrrl rtrr r! l :►[iti fipej 17tr eft iN711 ferrat-hed Ili IN .t•frtrm rl+utr using (I'M.) U FA Ilie nano ul'tiw Ittren+rW, MIWTI: 4V %V1I IY Illrat nl ('tultldCIC Jr ;IIIII•II• rlf,+r>'tic}tpit ;II well. <ktp -IIN. etynlMe I t+cil ntutlet inlbill III rnl»u14.1 EA( 11.1'1'V 11)# if:Ipplicallle) NAME 01: I'ACILI}'Y Foster SP Site # 01363 101(1+(ADIA05 1101 NC Highway Sl 19hiteett SC Cm, im 1[n►rl Stale /Ip l'ntk' 411, C'CINIM-1 F'F:Itti[].�1►►I:E-I. [1►1\r,l;; NANIF URS STRIA"! AI)11RI tiS 1600 Perirrtetez Park Dr, Ste 400 bWrl a THIld 11ep111: 15' 1(. I)1altl@IC(. 4" in- h Witter 1-e■el (1ICIou Mvas tit ►tis I'mF0C _ Ill. MA 'asurntt 146111 is . -.- _ _ Il. al-")w land stirlilce (I. C'ANIN(:: l.rny 111 DiallieMl 1t Casmg Mist Ii (ifknuuul 11 4. m 1+ C'asmtl Reolli■ed 1 0 n t. 1)li1NFF:(71li N: 104 t:ilriutttit of 65'i.751l". Cale itill] Ilppttihfor nt utiLrlI S. STAL.IN(;'1IATF.ItIA1.: Sent l'rmcn3 C emrul._94 y Ili. C onteft[ Ib girl ► itte( Bentonlsr I ierltUlllle Ih I yry ❑ Siurrn ❑prlEt 4 Witter gal )MUL T'.pt: ilia teridI Amount I). EXP1A1N ►1FT110111 (IF F1II"I.A[+.VF N-1' nh ► A'YERIAI-: t;iamtied lr= the bottom up._... Ili, WWI A- I)IACi Itr1]I I)raf■ a cietadrd sketch rsi Ute ■Fell ten the hock nl'lhls I'm Ili shou ins. wtal detnh. dLgxIt and itiunteler of xcmeny (d'rinv I rrtnaulirrg Iry tf c viell, gavel iilie ltit1, trt[ernats ul'cminb tkifonwtrns. Itnd ciep[Its and INIV% ttf lilt lnnlrllals IAw I 11.E!.■1E11'h:l.l..1I3;1�f1C1.4F:11 71912913. I Il[I III tiFHY l7 R1SI Y MAY MIN Wl I I tl',►S •113Ati[]fI\IJ) Iw Ik I I i t I i k Nc.4[' 1(. 11'l.1.1 ( Y N'sI RI n'1 Ills s I:►tit], ROS. ,m.l 111,11 I P1% RI-.001M It k% 111`.1 N t'RMID1.0 Ill 1-11E' 1►'IC1 I- '7/12/2013 I [. ti ►'I' 1' R F. OF 41 I: k'I'I F 11:11►►- ELL 41,11 M 1'R►('1.0k 11 t 11. SFGNA1V LM-1I'HI',.1-tF:1►Lill.(1111FK.1i1.ANINfylti[.IM.uFI.S IslIk. I I Ix tln nllC A%A (m ncr nIN, trl In :us Inl It t ttln:Il ■ilu, pli.tI;t1jk nl>:wLlui:, +i IIC ik.IJ: rII:.I nr�l NI :n rl+[du nee tt int 15;► N(,►[' :[' a 111. i 41I'll NAIII F: (IF PI:RWYN :IIi.1NDONINC rtIF 11'1:1.1. , 19C. 2 Stfhulit Ir rnp! to f hr uwnel' and the original to lilt, Ultil:lltn u(11'nkr [juallly o 1thin 3(I days• }'PIT Ili [ilY•311 Atier. Infurinotirrn VI"nogrluent. 1(117 ►tail Srrvbx ('enter - Italeil;it. SIC- 2761n3.1617, 111inne No. (919) 733.70IS c-�( S4I1I. Ret M)h