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HomeMy WebLinkAboutWI0400176_APP FOR PERMIT RENEWAL W/ MOD_20130204or License No. C-6281 CIVILISANITARYIENVIRONMENTAL ENGINEERS Municipal Services SITE PLANNINGISUBDIVISIONS January 30, 2012 Mr. Thomas Slusser, P.G. Aquifer Protection Section NC DENR --- Division of Water Quality 1636 Mail Service Center Raleigh, NC 27699-1636 Re: Injection Well Permit Renewal with Modification SOLID WASTE MANAGEMENT E . ineering Company, P.A. SUBSURFACE UTILITY ENGINEERING (SUE) Surry County Closed C&D Over MSW Landfill - Mt. Airy SWS Permit #86-02 UIC Permit No. W 10400176 (Issued 516J11) RECENEDIDENRIDN G12181.4 FEB 0 4 2413 Dear Mr. Slusser: Aquifer Protection SeCWTl Enclosed for your review is an Auviication for Permit Renewal with Modification for the subject landfill. Two modifications to the existing permit are requested, as described below: Modification # 1) It is requested that EOS Pro be allowed as a substitute for EOS 5981342. According to Sheri Knox, P.E., of EOS Remediation, the two products are the same except that EOS Pro has neutral pH while 598B42 is acidic. For additional information, Sheri Knox may be reached at sknox(&eosremediation.com or 919.873.2204 extension 174. Modification #2) It is requested that Surry County be allowed to reduce post -injection monitoring frequency from quarterly to semi-annually. The justification for this is that groundwater flow through the saprolite-bedrock aquifer could still be effectively tracked at a decreased sampling frequency due to the slow groundwater flow rate within the aquifer. With average hydraulic conductivity of 6.93 x 10-4 cm/sec and average gradient of 0.155, average seepage velocity at the landfill is estimated to be approximately 2 ft/day, assuming effective porosity of 15%. Given this flow rate, the average travel time from injection well to monitoring well at the Iandfill is approximately 5.1 months. Taking into consideration the delaying effects of retardation due to adsorption, the true travel rate of contaminants and injectant is expected to be even lower. Based on the hydrologic characteristics of the aquifer and other factors, it is recommended, therefore, that post -injection monitoring frequency be reduced from quarterly to semi-annually. PO Box 97, Garner, North Carolina 27529 (919) 772-5393 PO Box 349, Boone, NC 28607 (828) 262-1767 Copies of the most recent injection event reports and a renewal application are attached. Please contact me at the telephone number below or mdurwaya,mesco.com if you have any questions or need additional information. Thank you for your assistance. Sincerely, MUNICIPAL ENGINEERING SERVICES,Q,, P.A. CRR�f :,F��,�u• :�y • SEA-i e � D. Mark Durway, L.G. Geologist •NzF °4q� \4219K cc: Dennis Bledsoe, Surry County Director of Public Works RECEIVED1DENWDWQ ftifer Protection Section MUNICIPAL ENGINEERING SERVICES CO., P.A. Post office Box 97 Garner, N.C. 27529 (919) 772-5393 FAX (919) 772-1176 TO: Mr. Thomas Slusser, P.G. Aquifer Protection Section NCDENR Please find enclosed: Post office Box 349 Boone, H.C. 28607 (828) 262-1767 FAX (828) 265-2601 TRANSMITTAL Corporate License#: C-0281 DATES 1 /31 /13 PROJ. G 12181.0 NO. ATTENTION: Mr. Slusser RE: Injection Well Permit Renewal with Modiicalions Surry County Closed Landfill -Mt. Airy COPIES DATE DESCRIPTION 2 1/30/13 Injection Well Permit Renewal with Modification 2 Multiple Copies of "Status Reports" which entails four Quarterly Water Quality Monitoring Reports 1 1/31/13 QuarteYY Water Quality Monitoring Report for latest event October 23-24, 2012 (Copy of Oct. 23-24, 2012 has also been mailed & emailed to Winston Salem office Mr. Slusser, Enclosed are duplicate copies of the Injection Well Permit Renewal with Modification. The four Quarterly Water Qualify Monitoring Reports which serves as the status report are also included. The first three reports have previously been submitted and the latest one (Oct. 23-24, 2012) is included now. We eagerly await your response concerning the modification of the monitoring schedule which as proposed will be more consistent with the rate of transport of the injectants and contaminants. We would be very appreciative if you would expedite the review process so we can plan accordingly. We intend to follow up within the next few weeks. Th nk You. 0 athan Pfohl RECEIVEDIDENR1DWQ FEB a 4 2013 Aquifer Protection Secom If enclosures are not as noted, kindly notify us at once. North Carolina Departrnent of Environment and Natural Resources APPLICATION FOR PERMIT TO CONSTRUCT AND/OR USE A WELL(S) FOR INJECTION In Situ Groundwater Remediation I Tracer Injection Do not use this form for the following: ■ in situ remediation, tracer, or aquifer test injection wells permitted by rate (ref. 15A NCAC 02C .0217) ■ remediation systems that reinject treated contaminated groundwater (ref. 15A NCAC 02T .1600) Application Number (to be completed by DW& I -J (z;f f I �q r I. APPLICATION INFORMATION 1. Project is: [ ] New ( ] Modification [ ] Renewal without modification [X ] Renewal with modification 2. If this application is being submitted for renewal or modification to an existing permit, provide: existing permit number WI0400176 and the issuance date 5/6/11 For renewal without modifications, fill out sections I & 11 only, sign the certification on the last page of this form, and obtain the property owner's signature to indicate consent (f the applicant is not the owner). For all renewals, submit a status report including monitoring results of all injection activities to date. H. WELL OWNER (generally the responsible party) 1. Name: SURRY COUNTY PUBLIC WORKS 2. Signing Official's Name*: DENNIS BLEDSOE Title: DIRECTOR OF PUBLIC WORKS * Signing Official must be in accordance with instructions in Part IX on page 5. 3. Mailing address of applicant: SURRY COUNTY PUBLIC WORKS PO BOX 342 City: DOBSON State: NC Zip: 27017 4. Telephone number: (336) 401-8375 Email: PublicWorks@co.sugy.nc.us S. Status (choose one): Individual Business/Org. Federal State X County Municipality III. PROPERTY OWNER (if different than well owner) 1. Name: 2. Physical address: 237 LANDFILL RD City: 3_ Mailing address: City: 4. Telephone number: State: Zip: 27030 State: Email: IIH. PROJECT CONTACT — Person who can answer technical questions about the proposed injection project. 1. Name: D. MARK DURWAY, L.G. Title: GEOLOGIST 2. Company: MUNICIPAL ENGINEERING COMPANY, PA 3. Address: PO BOX 97 4. City: GARNER State: NC Zip: 27529 5. Telephone number: 919 772-5393 Email: mdurway(a)mesco.com RECEIWEDIDENU Revised 10/8/2012 FEB (14 Z M UIC-5115T Page] of 5 Aquiter Protection Sedan APPLICATION FOR PERMIT TO CONSTRUCT AND/OR USE A WELL(S) FOR INJECTION In Situ Groundwater Rernediation J Tracer Injection V. FACILITY INFORMATION 1_ Facility name: SURRY CLOSED MSW LANDFU LL - MT. AIRY 2. Ph#: (336) 401-8375 3. Mailing address: (See Section 11) City: County: State:NC Zip: 3. Geographic Coordinates. Latitude: 36.4.41139 N Longitude: 80.569639 W Reference Datum: weigh scales _ _ _ Accuracy: Google Earth Method of Collection: personal computer _ 4. Brief description of business: closed landfill V1. INCIDENT DESCRIPTION 1. Source and date of contamination: landfilied waste since 1973 2. List all contaminants present in soils or groundwater at the site (contaminants maybe listed in groups, e.g., gasoline, diesel, jet fuel, fuel oil, chlorinated ethenes, chlorinated ethanes, metals, pesticideslherbicides, etc): chlorinated and non -chlorinated organic compounds-, misc. others _ 3. Has LNAPL or DNAPL ever been observed at the site (even if outside the injection zone)? [ ] Yes If yes, list maximum measured separate phase thickness: feet [X ] No if no, list maximum concentration of total VOCs observed at site: 0 - 2,369* ppb (*MW9 on 5/1/03) 4. Agency managing the contamination incident: [ j UST Section [ ] Superfund Section (including REC Program and DSCA sites) [ ] DWQ Aquifer Protection Section [X ] Solid Waste Section [ ] Hazardous Waste Section [ ] Other: 5. Incident manager's name: Jacklynne _Drummond Ph#: (919) 707-8294 6. Incident number or other incident mgmt. agency tracking number: Landfill Permit 86-02 VII. PERMITS List all applicable permits or construction approvals issued for the facility or incident: 1. Hazardous Waste Management program permits under RCRA:_ Not Applicable (N/A) 2. DWQ Non -Discharge or NPDES permits: NCG120076 3. County or DISH subsurface wastewater disposal permits: NIA 4. Other environmental permits required by state or federal law: Landfill Permit 86-02 Revised I d/W012 UIC-5V5T Page 2 of 5 APPLICATION FOR PERMIT TO CONSTRUCT AND/OR USE A WELL(S) FOR INJECTION In Situ Groundwater Rernediation I Tracer Injection VM. ATTACHMENTS — provide the following information in separate attachments. The attachments should be clearly identified and presented in the order below to expedite review of the permit application package. 1. INJECTION ZONE — Specify the horizontal and vertical portion of the subsurface within which the proposed injection activity will take place and beyond which no violations of groundwater quality standards shall result from the injection as determined by an approved monitoring plan. The determination shall be based on the hydraulic properties of the specified zone. Provide any supporting documentation in a separate attachment. 2. HYDROGEOLOGIC EVALUATION — Provide a hydrogeologic evaluation of the injection zone that includes all of the following: (A) Regional and local geology and hydrology; (B) Changes in lithology underlying the facility; (C) Depth to bedrock; (D) Depth to the mean seasonal high water table; (E) Hydraulic conductivity, transmissivity, and storativity, of the injection zone based on tests of site -specific material, including a description of the test(s) used to determine these parameters; (F) Rate and direction of groundwater flow as determined by predictive calculations or computer modeling; and (G) Lithostratigraphic and hydrostratigraphic logs of any existing test and injection wells. 3. INJECTANT INFORMATION — List each injectant in the space below and provide the following information for each injectant. NOTE: Approved injectants can be found online at http:Ilparta1 ncdenr.arglweblwglanslgwnro. All other substances must he rev' d by the Division of Public Health, Department of Health and Human Services. Contact the UIC Program far more inAlGation Ph# 919-507-6496j. -� — (A) MSDS, concentration at the point of injection, and percentage if present in a mixture with other injectants; (B) The source of fluids used to dilute, carry, or otherwise distribute the injectant throughout the injection zone. If any well within the area of review of the injection facility is to be used as the fluid source, then the following information shall be submitted: location/ID number, depth of source, formation, rock/sediment type, and a chemical analysis of the water from the source well, including analyses for all contaminants suspected or historically recognized in soil or groundwater on the site; (C) A description of the rationale for selecting the injectants and concentrations proposed for injection, including an explanation or calculations of how the proposed injectant volumes and concentrations were determined; (D) A description of the reactions between the injectants and the contaminants present including specific breakdown products or intermediate compounds that may be formed by the injection; (E) A summary of results if modeling or testing was performed to investigate the injectant's potential or susceptibility for biological, chemical, or physical change in the subsurface; and (Ii) An evaluation concerning the development of byproducts of the injection process, including increases in the concentrations of naturally occurring substances. Such an evaluation shall include the identification of the specific byproducts of the injection process, projected concentrations of byproducts, and areas of migration as determined through modeling or other predictive calculations. 4. INJECTION PROCEDURE — Submit a table with a detailed description of the proposed injection procedure that includes the following: (A) The proposed average and maximum daily rate and quantity of injectant; (B) The average maximum injection pressure expressed in units of pounds per square inch (psi); and (C) The total or estimated total volume to be injected. Revised 10/$12012 UIC-5I15T Page 3 of APPLICATION FOR PERMIT TO CONSTRUCT AND/OR USE A WELL(S) FOR INJECTION In Situ Groundwater Remediation I Tracer Injection 5. FRACTURING PLAN (if applicable) — Submit a detailed description of the fracturing plan that includes the following: (A) Material Safety Data Sheets of fracturing media including information on any proppants used; (B) a map of fracturing well locations relative to the known extent of groundwater contamination plus all buildings, wells, septic systems, underground storage tanks, and underground utilities located within the Area of Review; (C) a demonstration that buildings, wells, septic systems, underground storage tanks, and underground utilities will not be adversely affected by the fracturing process; (D) injection rate and volume; (E) orientation of bedding planes, joints, and fracture sets of the fracture zone; (F) performance monitoring plan for determining the fracture well radius of influence; and (G) if conducted, the results of geophysical testing or pilot test of fracture behavior conducted in an uncontaminated area of the site. G. WELL CONSTRUCTION DETAILS — Submit the following information in tabular or schematic form as appropriate for each item: (A) number and depth of injection wells; (B) number and depth of borings if using multi -level or "nested" well systems; (C) indication whether the injection wells are existing or proposed; (D) depth and type of casing; (E) depth and type of screen material; (F) depth and type of grout; (G) indication whether the injection wells are permanent or temporary "direct push" points; and (H) plans and specifications of the surface and subsurface construction details. 7. MONITORING PLAN — Submit a monitoring plan that includes the following: (A) target contaminants plus secondary or intermediate contaminants that may result from the injection; (B) other parameters that may serve to indicate the progress of the intended reactions; (C) a list of existing and proposed monitoring wells to be used; and (D) a sampling schedule to monitor the proposed injection. Monitoring wells shall be of sufficient quantity and location to detect any movement of injection fluids. injection process byproducts, or formation fluids outside the injection zone. The monitoring schedule shall be consistent with the proposed injection schedule. pace of the anticipated reactions, and rate of transport of the injeclants and contaminants. 8. WELL DATA TABULATION — Provide a tabulation of data an all existing or abandoned wells within the area of review of the injection well(s) that penetrate the proposed injection zone, including monitoring wells and wells proposed for use as injection wells. Such data shall include a description of each well's type, depth, and record of construction or abandonment. 9. MAPS AND CROSS -SECTIONS — Provide scaled, site -specific site plans or maps depicting the location, orientation, and relationship of facility components including the following: (A) area map based on the most recent USGS 7.5' topographic map of the area, at a scale of 1:24,000 and showing the location of the proposed injection site; (B) topographic contour intervals showing all facility related structures, property boundaries, streams, springs, lakes, ponds, and other surface drainage features; (C) all existing or abandoned wells within the area of review of the wells listed in the well data tabulation that penetrate the proposed injection zone; (D) potentiometric surface map(s) that show the direction of groundwater movement, existing and proposed wells; (E) contaminant plume map(s) with isoconcentration lines that show the horizontal extent of the contaminant plume in soil and groundwater, and existing and proposed wells; (F) cross -sections) to the known or projected depth of contamination that show the horizontal and vertical extent of the contaminant plume in soil and groundwater, major changes in Iithology, and existing and proposed wells; and (G) any existing sources of potential or known groundwater contamination, including waste storage, treatment, or disposal systems within the area of review of the injection well or well system. Revised 10/812012 UIC-5I/5T Page 4 of 5 I.X X. APPLICATION FOR PERMIT TO CONSTRUCT AND/OR USE A WELL(S) FOR INJECTION In Situ Groundwater Remediation I Tracer Injection CERTIFICATION* (to be signed as required below or by that person's authorized agent*) NCAC 15A 02C .02 l 1(e) requires that all permit applications shal i be signed as fol lows: 1. for a corporation: by a responsible corporate officer 2. for a partnership or sole proprietorship: by a general partner or the proprietor, respectively 3. for a municipality or a state, federal, or other public agency: by either a principal executive officer or ranking publicly elected official 4. for all others: by the well owner. *If an authorized agent is signing on behalf of the applicant, then supply a letter signed by the applicant that names and authorizes their agent. "I hereby certi)� under penalty of law that I have personally examined and am familiar with the information submitted in this document and all attachments therein, and that, based on my inquiry of those individuals immediately responsible for obtaining said information. 1 believe that the information is true, accurate, and complete. I am aware that there are penalties, including the possibility of fines and imprisonment, for submitting false information. 1 agree to construct, operate, maintain, repair, and if applicable, abandon the inyection well(s) and all related appurtenances in accordance with the approved specifications and conditions of the Permit. " Printed NameAlhd Title: J�eAIZ4A � � _ &1011 -- re r Signature: Date:_ - �013 CONSENT OF PROPERTY OWNER (if the property is not owned by the permit applicant) "Owner" means any person who holds the fee or other property rights in the well being constructed. A well is real property and its construction on land shall be deemed to vest ownership in the land owner, in the absence of contrary agreement in writing. "As owner of the property on which the injection well(s) are to be constructed and operated, I hereby consent to allow the applicant to construct each injection well as outlined in this application and agree that it shall be the responsibility of the applicant to emure that the injection wells) conform to the Well Construction Standards (Title 15.4 NCAC 02C , 0200). " Printed Name and Signature: Date: Submit TWO copies of the completed application package, including all attachments, to: DWQ - Aquifer Protection Section 1636 Mail Service Center Raleigh, NC 27699-1636 Telephone (919) 807-6464 Revised 10/8/2012 UIC-5I/5T RECEIVEDIDENRIM FEB 0 4 2013 Aquifer Protection Sedon page 5 of 5 February 9-10, 2012 Quarterly Water Quality Monitoring Report Prepared for Surry County Closed C&D and Closed MSWLF, Mt. Airy Mt. Airy, North Carolina February 2012 TAC Permit Number:WI0400176 SWS Facility Permit Number: 86-02 MESCO Project Number: G10061.0 Submitted: July 25, 2012 THuniripat �� Eagiaeeriag Gw-.•. NC '�� 11�wgT1C P.O. Box 97 RECEIVEDIDENRIDWQ 1uSuru[Ga} er ind Boo e. North Carolina P A. Garner, NC 27529 Garner and Boone, Nonh Carolina License No. C-0281 FEB 0 4 2013 Aquifer Protection Section TABLE OF CONTENTS Introduction and Background l Sampling Procedure Page I Field Parameter 2 Laboratory Results­---------puo�2 Groundwater 2 Groundwater Churaoterizadion_________9age2 Findings___ ..... ....... ___...... ....... ......... ________________PoQe2 FIGURES Topographic Map with Site Louab ' l Potendoonctr{oMaoof Uppermost Aquifer w/VOCoDetected Above 2L iguro % Time Series Graph of Total Cumulative VOC Concentrations,--. 3 Sampling and l Detections that Attain orare Above 8W8Lor%l (Appendix I) % Indicator Parameter Data Sonznuu/y Hydrologic Properties o1Monitoring We] io APPENDICIES Laboratory Analysis Report and Chains of Custody---- - —Appendix A License No. C-0281 CIVIL 15ANITARYIENVIRONMENTAL ENGINEERS SLM WASTE MANAGEMENT [Municipal ESUBsuSUROFACE ngineering Services Company, P.A. SRE PLAN NING7SUBDIVISIONS UTILITY ENGINEERING (SUE) July 25, 2012 Mr. Thomas Siusser, P.G. Aquifer Protection Section -Underground Injection Control Program Division of Water Quality North Carolina Department of Environment and Natural Resources 1636 Mail Service Center Raleigh, NC 27699-1636 Re: Quarterly Wafer Quality Monitoring Report Surry County Closed C&D and Closed MSWLF, Mt. Airy 237 Landfill Road Mount Airy, NC 27030 SW S Permit No. 86-02 UIC Permit No. WI0400176 MESCO Project No. G 10061.0 Dear Mr. Slusser: Introduction and Background Municipal Engineering Services Company, PA (MESCO), on behalf of Surry County, appreciates the opportunity to \ present this brief Quarterly Water Qualiry Report that details a water quality monitoring event performed at the Surry County Closed C&D and Closed Unlined Municipal Solid Waste Landfill (MSWLF) Facility (Permit # 86-02) on February 9-10, 2012. As directed by the Under -ground Injection Control (UC) program, this is the first post injection quarterly water quality monitoring event. A topographic facility map is presented as Figure 1. Per the NC Solid Wasate Section (SWS) approved Corrective Action Plan enhanced bioremediation via substrate and tracer injection was initiated in accordance with requirements outlined in the Injection iPell Permit Application and Well Permit No. WI0400176 (5/6111). EGS®598B42 plus Ix16 oz EGSO Vitamin Sit supplement and sodium bromide tracer were injected into four wells on November 2-3, 2011 in an effort to reduce low level aliphatic and aromatic chlorinated hydrocarbons in groundwater to below the North Carolina Groundwater Standards (2L Standards). Injections were performed through 1W-1, IW-2, IW-3 and IW-5 and details are provided in the Injection Event Record dated November 4, 2012. Sampling Procedure MESCG personnel performed this sampling event following the parameters, frequency and well locations established by the UIC. Groundwater samples were collected and analyzed from nine wells which includes MW-3R, MW-12S, MW-12D, MW-13, MW-15, MW-16, MW-18, MW-19 and upgradient background well MW-1. Additionally, water within the injection wells were measured and visually evaluated in an effort to determine the amount of residual organic substrate remaining in the wells which may help evaluate the viability of these wells to be used for future water quality analysis. Monitoring locations are depicted on Figure 2. PO Box 97. Gamer North Carolina 27529 (919) 772-5393 Pr? Sox 349, Ronne, NC 2rr6o7 (828)262-1761 Sampling was performed per the protocols outlined in the SWS approved Groundwater and Surface Water Sampling and Analysis Plan which was submitted with the Corrective Action Plant (CAP) revision 2 dated December 10, 2010. The depth to water in each well was electronically gaged prior to purging to quantify the static water level elevation. Low -flow pumping, methodology or bailing was utilized to adequately purge the wells a minimum of three well volumes or until dry. During purging the stabilized field parameters were recorded. The samples were then placed into laboratory -prepared, pre -preserved containers via a new disposable polyethylene bailer. Samples were kept on ice, and transported to a NC -certified laboratory under proper chain of custody (C-O-C) protocols. Field Parameter Data Field parameters recorded included pH, specific conductance, temperature, dissolved oxygen (DO), oxidation reduction potential (ORP), total dissolved solids (TDS) and visual turbidity. A summary of the field parameter data is presented in Table 3. Laboratory Results Pace Analytical Laboratories (PACE) of Huntersville and Asheville, NC performed the majority of the laboratory analysis. Groundwater samples were analyzed for all the parameters requested by the 1]IC which includes constituents listed in Appendix 1 of 40 CFR 259, alkalinity, sulfate, chloride, total organic carbon and biochemical oxygen demand. Environmental Conservation Laboratories (ENCO) of Cary, NC analyzed the samples for the tracer bromide. A sampling and analysis table summarizing the locations, target parameters and laboratory methods is presented as Table 1. Water samples were reported at the laboratory specific Method Detection Limits (MDL), which are quantifiable at or below the current Solid Waste Section Limits (SWSL). Laboratory results and C-D-Cs are presented in Appendix A. Groundwater Samples Appendix I total metals were not detected in levels above 2L Standards. The wells with Appendix I VOCs detected in concentrations above the SWSL and in exceedance of their respective 2L Standard during this event include NM-13 (vinyl chloride, 1,1-dichloroethane), MW-15 ( vinyl chloride, l,l-dichloroethane, TCE, PCE, benzene) and MW-16 (1,4-dichlrobenzene, 1,2-dichloropropane, vinyl chloride). Table 2 summarizes Appendix I constituents detected in the water samples in concentrations above the current SWSL or North Carolina Groundwater Standards (2L). Table 3 summarizes indicator parameters quantified by the laboratory. A site map depicting the spatial distribution of VOC concentrations detected above the 2L Standard during this event is presented on Figure 2. Groundwater Characterization A potentiometric map of the uppermost aquifer created from static groundwater elevations recorded during the October 2011 event is included as Figure 2. Groundwater flow rates and directions were calculated via modified Darcy's equation and are included in Table 4. Groundwater flows in the unconfined and upper bedrock water - bearing zones in a general southwesterly direction away from the waste limits. Calculated groundwater velocities were variable but consistent compared to historical observations. Findings The quarterly laboratory results indicate that low level dissolved phase VOCs consisting primarily of chlorinated hydrocarbons continue to be detected in groundwater samples collected from MW-13, MW-15 and MW-16 which are located within 250 feet of the waste boundary. Contamination continues to not be identified in samples collected from the other six wells sampled during this event. All VOCs detected in concentrations above the 2L Standard during this event remain within their own respective historically identified range. The total cumulative VOC concentrations detected in the nine wells monitored during this event decreased by 34% (267 ugll to 176 ugll) compared to the moving average of the five events that proceeded [lie injections (Figure 3). Total cumulative VOC concentrations within MW-16, downgradient of IW-3, exhibited a relatively large 64% (125 ugll to 45 ugll) reduction following injection compared to its own respective five event moving average (Figure 3). Visual evaluation of the injection wells (IW-1, IW-2, IW-3, IW-5) indicate that a considerable amount of white highly viscous residual organic substrate and its byproducts remain in each of these wells. It was confirmed that the injection into IWA was unsuccessful as a total of less than 3 gallons of substrate has been introduced to the fractured bedrock aquifer at IW-1. The depth to substrate as measured in IW-1 had only subsided a total of approximately 15 feet in 98 days (r2"Iday) and had yet to reach pre -injection static level. Bromide tracer was only detected in low non -quantifiable `i-qualified" concentrations in MW-12S, NM-13 and MW-1 G. Closing Corrective action to remediate the VOCs as detected in groundwater is expected to continue. The second post injection quarterly water quality monitoring was performed on May 29-June 1, 20 12 and the report will be submitted to UIC and SWS upon completion. If you have any questions or comments regarding this report, please contact us at (919) 772-5393 or by email at Jpfahl@mesco.coffl. Sincerely, MUNICIPAL ENGINEERING SERVICES CO., P.A. �_Lq-v Jonathan Pfohl Environmental Specialist Enclosures cc: Mr. Dennis Bledsoe Surry County Ms. Jaclynne Drummond SWS-Compliance Branch Figures Topographic Map with Site Location Surry County Closed C&D and Closed MSWLF, Mt. Airy .. ,` `�''fir+ i '—... ••..ti ti.- j t w _. T } z o• .. .i ~ _ L .TR'. . is " _ '"�-.� iy'• Uosed a l Landfill �'.Y.. 47 rw _�: • rye . r� ��.;..-.. p'� ROAD CLASSIFICATION � ❑ 1 MILE Primary highway, Light -duty road• hard or -- hard surface improved surface Secondary highway, hard surface Unimproved road z=___F FIGURE I 0 Interstate Route 19 U. S. Route 0 State Route I NO W OR FORMERS Y 0 WNEO 1 6 Y JONNIV Y COX r i" Ir ❑ WNED B Y SLIRR Y COUNTY LEGEND =SnNG CWTOURS PACA-ERTY f]09nWc PAW+ Po Tf7N1immc cuoITXR pallzfTT) c] SEDIMENT BASIN -- ...-... EXTCNT or Co"w CLAr CLoszw upw CLoS�e My W ANo C*0 COMPllwCC ROLWaARY p5o. rRom Eow a w- rRw p*apD?TY LN1r) ..+ ■ MONITORING NEU sz ■ WWACE WATER MONITORING POINT w p INJECTION WEU f i ! ] OWNED 6Y i SURRY COUNTY I NOW OR FORMERLY OWNED BY Sr -IA WNA SLIMMERS FIGURE 2 i a CLOSED C&DAND CLOSED AaSWLF +g MT. A(RY Municipal Engineerin Company, P.A. i o POIEHTKIMMC YAP Cr I]PKPWDST AOUFM SURRY COUNTY R ./ YOC DETECWNS AMW a STANVAWS NORTH CAROLINA Figure 3 Time -Series Graphs of Total Cumulative VOC Concentrations October 22, 2009 - February 10, 2012 Tote! Cumuwtive voc Concentrations - SWSL or 2L standard Nwo-Wdi TmeSMes df+Ph 550 i00 150 r i 50 r w ry r N sample Dam •AAM-16 -W-13 -&W 15 aAlLIC Wells •MW-12S MAN 12D -WM 1 •MW 3R +MW 18 4W 19 1 1 e- Z Well ID Oct 2009 (uglL) May 2010 (uglL) Oct 2010 (ug1L) May 2011 (uglL) Oct 2011 (ug/L) Five Event Moving Average (ug/L) Feb 2012 (ug1L) Difference (uglL) Difference {°/ej _ MW-1 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0-OD0.00 MW-3R 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0-00 MW-12S 0.00 0.00 0.00 0.00 5.40 U8 0.00 -1.08 -100.00 MW-12D 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0,00 MW-13 61.00 50.60 74.20 87.30 72.50 69.12 59.10 -10.02 -14.50 MW 15 96.13 63.89 55.00 78A0 64.06 71.44 72.40 0.96 1.34 MW-16 137.90 113.60 135.70 12110 115.30 124.94 44.90 -80.04 -64.06 MW-18 0.00 0.00 0.00 a00 0.00 0.00 0X0 0-00 0.00 MW-19 0.00 0.00 0,00 0.00 0.00 0.00 0.00 0.00 0A0 Combined Total 295.03 228.09 264.90 286.60 258.26 266.58 176.40 -90.18 -33.82 Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Tables Table 1 Sampling and Analysis Summary February 9-10, 2012 A I MNA Traver v rx E o z � C y 'E C cLO a U U m o m Y 22 5 1-- U D G7 Q E D W 7 F— ¢ 0 U m OD Q a m 0 C w Q Q N C,M CO a Q a M p C) Ir g C)m r ¢ ED LU U] CO) N t17 N U!7 m N 0- EL MW-1 x x x x x x x x MW-3R x x x x x x x x MW-12S x x x x x x x x MW-12D x x x x x x x x MW-13 x x x x x x x x MW-15 x x x x x x x x MW-16 x x x x x x x x Mllw16 x x x x x x x x MW-19 x x x x x x x x App I = from current 40 CFR 258 Surry County Closed CRb and Closed MSWLF. Mt. Airy Pane 1 of 1 Table 2 Detections that Attain or are Above SWSL or 2L Standard (Appendix I) February 9-10, 2012 Sample parameter NameSample a mte a Result Unit MDL r SWSL 3 2L; Exceedance MW-1 Barium, total 02J10112 116 uglL 5 100 700 MW-1 Thallium, total 02/10/12 T7 uglL 5A 5.5 NE MW-1 Zinc, total 02J10112 38.7 uglL 10 10 1050 MW-3R Thallium, total 02/09/12 8 uglL 5.4 5.5 NE MW-13 cis-1.2-Dichloroethene 02/09/12 36.4 uglL 0.19 5 70 MW-13 Cobalt, total 02/09/12 15.4 uglL 5 10 NE MW-13 Zinc, total 02/09/12 20.2 ug1L 10 10 1050 MW-13 Trichloroethene 02/09/12 2 uglL 0.47 1 3 MW-13 Vinyl chloride 02/09112 1.2 ug1L 0.62 1 0.03 1.17 MWA3 1,1-Dichloroethane 02/09112 10 ug1L 0.32 5 6 4 MW-13 1,4-Dichlorobenzene 02/09/12 5.7 uglL 0.33 1 6 MW-13 Chlorobenzene 02/09/12 3.8 uglL 0.23 3 50 MW-15 1,1-Dichloroethane 02/09/12 22.2 ug1L 0-32 5 6 16.2 MW-15 1,4-Dichlorobenzene 02/09/12 3.9 uglL 0.33 1 6 MW-15 cis-1,2-Dichloroethene 02/09/12 35.7 ug1L 0.19 5 70 MW-15 Zinc, total 02/09/12 11.1 uglL 10 10 1050 MW-15 Vinyl chloride 02/09/12 1.5 ug1L 0.62 1 0.03 1.47 MW-15 Trichloroethene 02109/12 4.4 ug1L 0.47 1 3 1.4 MW-15 Tetrachloroethene 02109/12 1.9 ug1L 0.46 1 0.7 1.2 MW-15 Benzene 02/09/12 2.8 uglL 0.25 1 1 1.8 MW-16 cis-1,2-Dichloroethene 02/09/12 31.7 uglL 0.19 5 70 MW-16 Zinc, total 02/09/12 13 uglL 10 10 1050 MW-16 Cobalt, total 02/09/12 208 uglL 5 10 NE MWA6 1,4-Dichiorobenzene 02/09112 8.6 uglL 0.33 1 6 2.6 MW-16 1,2-Dichloropropane 02/09112 1.5 uglL 0.27 1 0.6 0.9 MW-16 Vinyl chloride 02/09112 3.1 ug1L 0.62 1 0.03 3.07 MW-19 Zinc, total 02/09/12 13.8 ug1L t Table contains Appendix I constituents detected at or above SWSL or 2L h1DL = Method Detection Limit a SWSL = Solid Waste Section Reporting Limit 4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard SOLD = Concentration > 2L Standard N E = Not Established 10 14 1050 Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Table 3 Indicator Parameter Data Summary February 9.10, 2012 Parameters Method MOL' Units MW 1 MW-3R MW-125 I MW-12D MW-13 MW-15 MW-16 MW-18 MW 19 2/10/12 219112 219112 2/10112 219A 2 219112 219112 2110/12 219112 Alkalinity SM 2320B 5000 ug/L 57400 123000 109000 81200 57400 48700 99600 10800 11900 Sulfate EPA 300.0 5U0U ug/L 6330 <5000 33100 7220 <5000 <5000 7170 <5000 <5000 Chloride SM 4500-CI-E 5000 u L <5000 <5000 6610 <5000 34400 <5000 10200 d <5000 <5000 TOC SM 5310B 1000 ug/L 2930 3820 3480 3780 10700 11100 14200 8350 2530 SOD SM5210B 2000 ug/L <2000 <2000 <2000 4440.0 <2000 2460 <2000 9930 <2000 Temperature Field Instrument 0.0 C 14.4 15.1 15.1 15.4 13.8 14.2 14.3 15.2 15.0 ❑RP Field Instrument -900 mV 128 88 126 -62 363 -92 44 305 309 DO Field Instrument 0.0 mglL 2.9 2.3 5.0 1.1 0.7 2.3 4.4 4.6 4.1 pH Field Instrument 0.00 SU 6.83 7.08 5.89 7.19 5.33 7.03 5.78 6.42 5.62 Bromide (Tracer) EPA 300.0 0.024 mg1L <0.024 <0.024 0,034 <0.024 0.240 <0.024 0.038 <0.024 <0.024 Sp. Conductance Field Instrument 0 us/cm 300 270 380 150 220 260 420 0 10 Depth to Water Field Instrument 0.00 ftbtoc 25.70 41.65 13.10 0.00 26.56 52.17 26.65 9.01 9.41 Water Elevation Calculation 0.00 Ftamsl 1108.65 975.85 1012.70 1027.05 981.92 1023.79 972.89 NA 936.86 Notes: MDL' = Lab Method Detection Limit or lowest field measurement possible. Constituents detected below quantifiable limits are shown as a ME)L value, Surry County Closed C&0 and Closed MSWLF, Mt. Airy Page i of 1 Table 4 Hydrologic Properties at Monitoring Well Locations October 12, 2011 Groundwater Average Groundwater Hydraulic Effective Hydraulic Linear Groundwater Potentiometric Monitoring Conductivity Porosity Gradient Velocity Rate Flow depth Elevation Screened Interval Well (cm/second) (%) (feetJfeet) (feetlyear) J Direction (feet btoe) (feet amsi) Lithology MW-1 4.30E-05 15 0.085 25 S16W 26.03 1108.32 Clay 0-2 4.30E-05 15 0.155 45 542E 42,55 1026.31 Clay MW-13 2.06E-04 23 0.102 95 S27E 27.35 981.13 Saprolite MW-18 2.04E-03 15 na na na 8.26 na Saprolite MW-19 1.10E-03 3 0.122 4,633 S13W 9.57 936.70 PWR Minimum 4.30E-05 3 0.085 25 - 8.26 936.7 - Average 6.86E-04 14 0,116 1,200 - 22,75 1013.12 - Maximum 2.04E-03 23 0.155 4,633 - 42.55 1108.32 - MW-3R 2.40E-04 5 na na na 42.82 974.68 Fractured Rock IW-3 2.40E-05 5 0,174 86 S33W 34.13 986,44 Fractured Rock 0-5 1.50E-05 5 0.072 22 SO4W 43.15 1037.03 Fractured Rock MW-12S na 3 0.089 na 524E 15.03 1010.77 Fractured Rock MW-12D 1.30E-06 5 na na na 0,00 1027.05 Fractured Rock MW-15 721 E-05 3 0.188 469 S03W 53.02 1022.94 Fractured Rock MW-16 2.82E-05 3 0.192 187 S38W 27.55 971.99 Fractured Rock Minimum 1.30E-06 3 0.072 22 - 0,00 971.99 - Average 6.34E-05 4 0.143 191 - 30.81 1004.41 - Maximum 2.40E-04 5 0.192 469 - 53.02 1037,03 - NOTE: Values for hydraulc conductivity determined via stug test by GAI, MESCO, or Joyce. Hydrologic gradient from water levels recorded on October 12, 2011, Wells screened entirely in rock were not utilized for flow directions/gradients- Screens that traverse both rock and regolith assumed flow in regolith dominates. na = Not available/applicable Average Linear Velocity (q) is defined by the equation: K A K= hydraulic conductivity where Q - - - • --- ne= effective porosity n dl dh= head difference r dl= horizontal distance Surry County Closed C&D and Closed MSWLF, Mi. Airy Page 1 of 1 Appendix A Laboratory Analysis Reports Chains of Custody Appendix A Laboratory Analysis Reports Chains of Custody acewytical" February 28, 2012 P..: AnElyYul lnYleEy Inc. Pip AWYNIP" W ". Me. PRw AnMyIM i S-1-k 4-- riSEatkM.-d wrt 70'su1.1A 22�5 Rw�rrG lx EOOII rM� EW.1W Ed., NC 27;ar ftfto rr. JdC NW4 FAmYnA�- NC 26DIE nXW3�21 47E]254-7"N pMOV M Mr. Jonathan Pfohl Municipal Engineering Services PO Box 97 Garner, NC 27529 RE: Project: SORRY CLOSED LF Pace Project No.. 92111951 Dear Mr. Pfohl- Endosed are the anaIyVcal results far samples) received by the laboratory on Fatxuary 10. 2012. The results relate only to the samples Included In this report. Results reported hereln conform to the rnost current TIN standards and the laboratory's 0uslltyAssurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location Indicated on the sample anal yte page for analysis unless othetwise footnoted. If you have any questions concerning Ihis report. please feet free to contact me. Sincerely, Kevin Godwin ke vi n. g odwin@pacelshs. corn Project Manager REPORT OF L.A60RATORYANALYSIS Tl np" nr nn W %gM*XW. —Pt a M. •rwl h wd1EP eon Cr Ps Awr"jmN v.6c P404 I of 39 ��..pp .{,,., f ) P.- An.Irac.1 a.hlca., Ina. Pa.. Aryl yu..1 unto.., Ine. P..e Anl.yVice1 i.n.Iga, Ina, LGaiiyVal• 2A Feet al.a Road-S.awA =Rwo—oi Or OW RYxar Ave SdwM 69.n. NC 77M A ,awa Ha "" Nun —A.. NC 7607E P.ly SURAY CLOSED LF Pace Projaci No.- Oi111951 eharinRa Caditaalnn ID. 9e00 %ercay Ave. Ste l00. leimtenlv,le, NC 20076 Nora) Cwo4ne Drhlrnq NMer C.r9aee9en i. 37704 N9rfi Cwdna HoW Services Cartllca9on •- 5342 N9nh Cualne Motawalor Certillcallon 9: 12 Swth C."nm C■r911ulkm 9: 99006001 Seulh CuOAna Dgnbny NAtu Cut 9. 09DOW03 ViFgws Dweing V Mw Cen nilcbn 9: 00213 AehevKA Ca AlRsellnn IDS 2225 RlIverWa Dr..AahavMe. NC 2UN Fbrld"ELAP CerHka6on 9. E67046 Massock ote Cer5ea 9.m a: M.NG030 Noah Cerv4le Drinkalo IAYIae CW"-Nn a 37712 Nom Cu91na YNeuwelu Combeawn 0, e0 i E3e147)�21 1wffip5 717E f7M l6rS9097 CERTIFICATIONS C9ryreGRlll cd4ficidon is P144404 R96deMELAP CeIr511w6en is E67627 KanWcky UST Cor01a0on!' 64 Laalslans D161 Drinianl N(aler f LA 100031 VWal lhplrll i Csr6 Acailon 9: 357 Vt,"I&VELAP C.r64ca9on a. 46014e Sonar Cuallna Car6 E coiJw 9-90030001 yhglnl. Cw6llc.u.-* 00972 naval vkylr+. Caleece6Pn r- 356 V,10l lVSLAP Ca.uA"uw 01400147 REPORT OF LABORATORY ANALYSIS Trw neon Y1.. npr qr npr9aupO, eaup n AA, w1Md"rrr can caca.nl of Als A1yrpL�y 5a rvio.e, irc . pe0r: p13S j aceR�a�yti�a�' I arolecl- SURRY CLOSED LF Pace P1eJaci No.: 0311 %SI Lab 1D Sample 111 "111951001 k111*1 92,T11511002 MW-11t 6 11Sa1003 mw-7S 92,111 IWA 10100-111 921119E1006 MW-11 921119S1006 MAI.129 92111951007 MY6W120 92111161006 MW13 f7111151006 M1N•18 Pa ea Analya.al aervlaar, Ini. Pace An.I y11..I la micas, In.. Pes. An.,yeu1 as i—. In, 795 E aN 1A. rC9w N w 0 - e A 2777 R'".60. Or 960011.re.1 k. 5�. I OO Edrn, NC Mw R.neW, NC 2& W Hunwwib. NC 2ad7e jOEelenaa7l ja7e)75a-71 Is 110.]a7faO0] SAMPLE SUMMARY Mehl: Cab. Col lam led Cale M-1-d Mier MIW1200:20 0V1Oil 214:24 VAIeI 0210911212:00 0211W17143e 1M.I.r 021Q91121510 ODIV121424 Walw MMIJI214:00 WWI 21i24 Wale C100li217:00 OV101f21424 Ywtar IlMi 1211:00 02110d1214:24 Nwter 0211011264AS owwl2 4424 Mtar 0V091121315 0N10J42 44:24 mtu 0211W 2090o 0T1101S2 42e REPORT OF LABORATORY ANALYSIS lIa repom .n., ra1 W—ducaa...eap[ y Mn. r C-1 r ..-ftan mount el Pau An,yucal S.rwd.. I- P-g. 3 .1 10 t Paca AnA1yoW Mel/es. in.. P.- AnMylicel S.rvlc rc, Ine� Paea Anrlyy.wl Hams, Inc. • 'J�p� /,, vP ec Analy9[al Banle.a, Ine ►.P. AnaI YIIsa1 Mrod.s, Irw. Pao. An.ly11P.1 Brnlo.., mo. aceAna)ytical ;95 ea0 Msaeew Aea6 - S.ap.A R21 R-a 9. M IBM ran .r A. A.A. 10C p,,,, TQL�IV fdlytl� CZl 205 Ea+ Marva. Rwe . Su n Yii3 RM rEe Lk 9A00 Ke Ava Stela Tov „w p.nypay� Ewn NC 27Z60 W,wNN. NC z6b3A 11unlrrnAC NC;Buieam,,, Eda •. �.L7f:aF AY1.r�-NG 286W rwm.r..>.r. r.0 2Bu7e i77Q62NY21 1628105a-7T7B 170035MI02 •JA. r;: A::• 16OQJ4-7179 I7:MN1i6�P SAMPLE ANALYTE COUNT SAWLE ANALYTE COUNT Pr PJrP1: BURRY CLOSED LF PlolerL: SORRY CLOSEO LF Pace Pr.wo N. 92111951 P-- Prplw No.. 9Z111961 0.ndyles A"'Yeer L..h ID Semple Ip Molhvd A—l"r. R.PPrted L.b—Wry Lah 10 Samp le lO Method An4IYvs R.perlad LPynntery 82111901001 N--Y&I EPA $AID JOA 15 PASI-A SM 232D6 AES 1 PASI-A E PA 829D KJM 52 PASI-e SM 52106 AES 1 PASI.A SM 21:06 AES I PAST -A EPA SOO.Q SAE 1 PAV-A SM SIMS AES I PAS1.A 6M 4500-CI-E JOA 1 PAS" EPA SOOk SAJ 1 PA.V-A SM 531Ug 6AI 1 PASJ.A SM 4500-CI-E JOA I PASI.A 92111961007 MW-120 EPA 601D JDA 15 PASI-A SAF$1108 SA7 1 PAS. -A EPA 0250 KJM 52 PASI-C 9z1t1G61502 MWJR EPA Ul0 JOA :5 PAS, A SM 23206 AES 1 PAS1-A EPA 6260 KJM 52 PASI-C SM 52108 AES 1 PASI-A 30,23208 AES I. PAS1•A EPA 300.0 SAE 1 PASI-A SM 5210$ AES 1 PASI•A Sm ASO Q-Cl-E JDA 1 PASI-A E PA 3000 SAJ 1 PASi-A SM 53108 SAE 1 PASI-A SM OD0•CI-E JbA 1 PAS•A 11111MOD6 MW17 EPA 6010 JDA 15 PASI•A SM 51106 5AJ 1 PASI-A EPA 8260 KJM 52 PASI-C 121 tII'd 1 ad MYe•f8 EPA 9010 JpA 15 PASI.A SM 238D11 AES 1 PASI-A EPA 6260 KJA4 A2 PASI•C SM 112109 AES 1 PASI-A SM 23209 AES 1 PA$1-A EPA 300.0 SAE 1 PAS A SAB $2108 AES 1 PASI-A SM 4500-0I-E JDA I PA$I.A EPA 100.0 SAJ 1 PASI A SM 53106 SAE I PASI-A SM dSQO-CI-E JaA 1 PASI-A 921110510DI MW16 EPA 6011) JDA 15 PASI-A SM SS1021 SJU 1 PASI-A EPA BMW KWIr1 52 PASI-C 9I711961004 OA.*pI6 EPA 6010 JDA 15 PASI-A SM 23208 AES 1 PASI-A EPA 8290 KJM 52 PASI-C SM 5218B AES I PAST -A SM MOD AEG 1 PASI.A EPA 300.0 SAE 1 PA& -A SM 5i10g AES 1 PASI.A SM 4500ZI-E JOA I PASFA EPA 3000 SAW 1 PASI A SM 53108 SAE I PASI-A SM 4500-C1.E JDA 1 PASI-A SM 53106 SAW 1 PASI-A 92M961005 MW-16 EPA6010 JDA 15 PASI-A EPA 12" KJM 52 PASkC SM I32o6 AES I PA514 SM 5ZM AES I PASI-A EPA 300 0 SAJ I PASI A SM 4500-GI-E JOA I PASI.A i1r1 5310 SAJ 1 PASI A 97111961006 MW-125 EPA 61)10 JOA 15 PASI-A EPA 8250 Kim 52 PASI-C REPORT Or LABORATORY ANALYSIS P4pq 4 nl 39 REPORT Or LA 9O RATO RY ANALYSIS Ped6 5 N 39 T1re 1.0m --1 M nplvtlk.Q _.P1 r r r.pvrl enac ml w nPretluc.v. uupl h IW .1n M. B. eenwnl eI Pad A -Wry l Sarrxae elno.x C1. wnd.n =vnrenl 0 P.c. Aarrnry 5,— In[ 26AMIytical' Pa..Arr"-t 9.rvraaa, me Pan Awylkn lanane, Me- Pan A.Wydeal Leven., lea �s Eon Ylaaaew Read � s.w H V25 RYw..ltl. 0- 9ddox , A.. 5VM 10D Ed.n, NC 2711d A.naNw. NC 2aa04 aArMaraH., NC iMl14 [57a167>•Ory71 t42a1234.71r6 1704)eyd. B7 ANALYTICAL RESULTS Praper. BURRY CLOSED LF PaG Proy.c[ Ho.: 92111951 9arrlpla: MW-1 L.MD: 62111661001 Cuk lad: 0& W209-39 R-Wwl: 0 JIVI114-24 Me6Sr Vk%4. R"ri P.ramer.n Reeuila unto urnll MOL OF Pnparad Analyzed CAS No. Oua1 s07a 1CP Oraundweyr AnMyticM M%Mod: EPA 6010 PreP.r%OM Melhod EPA 3410 Ardimony NO uBL 6.0 SA 1 02OW12 WAS 02/16112 00-39 7440b36-0 AiaeMc NO ugrL 10.0 6-0 1 0211 V1211:45 02AWI200:39 7410,-36.2 9an.,m 179 uglL 1Do 50 1 0N1 N1211:45 0211V2003q 744049-3 9.ry4lum NOugIL 1-11 1-1 1 MI1111111Al 071161i200:1:7440a1.7 CodMum ND uWL 1-0 1.0 1 00116r121La5 0211110 2 007744043.9 Chremwrn 7.11 4& 10.0 5.0 1 MMW1211'45 =Wt200:19 744447.3 caboll 1,61 uD0. 10.0 5.0 t Wdfl211:45 O711 N1200:32 7440.464 Copper cu uWL 10,0 1.0 1 021t6112 TT,45 02116f 1200;19 7440�"4 Load NO ug1L 10,0 S.0 1 0211 N1211:4S 021 WI200139 Mg-02.1 Nickel 6.3.3 upt 50.0 5.0 1 021151t211AS 0211WI2 DO:32 7440-a2.0 Selenurm NO MOA 10.0 1DA I 92116H211 AS 02J1NIa 003E 776249.2 Saw NO ug(L 101 5-0 1 021&1211AS 0&1N12 D0:19 7440-22-4 TTalkum 71 ugk 5-5 5.4 1 02116rl211AS 02AW12 D019 744S•26.0 Vanadum Ito) uplL 25A 6,9 1 DWW1211A5 0211a111200:34 744042-2 21nC W7 uVL 1g-o 10-0 1 W012 11:45 DWI NQ 00:39 744M-6 1290 MSV Low Lwd L.nd1111 A-F"Qd Me Mod: EPA 6260 Acelen. NO udl IM 22 1 0271Y1216:37 67-"-1 AttylorlklM NO uo& 200 1 9 I. 02z1111211,37 167.13.1 6. 14H6 ND uyL 1-0 025 1 02 M211`37 M43.2 Br.mpohlorpmathen. NO u91L 1.0 0-17 1 02113112 13:37 74-27-S prnmedlWerem.ln.n. No LOLL t-0 Oil 1 a211r12 1g37 75-274 Br9rrw7orm NO uyL 3A 0.25 1 02JIM218:37 75-25-2 Brpmamatr,sno ND uok 10,0 0," 1 02h'YI214:17 74•13-9 2-Bulanon. tMEK) ND u011 100 Dim 1 o2n3ilz 16:37 76-93.3 Carbondlwlede NO ug& 10D 12 1 021b12 71:37 75.15.0 Carbon tlC.dum14e NO ug1L 1.0 025 1 Owl 3012 11;37 36.23•5 ChkxoEanzena NO ujyL 310 0.23 1 0211Y12 1837 106.90.7 Chl.roam- NO ug& 1010 034 1 0213112 W37 75-00.3 ChluoNrm ND ugtL 6,0 0.14 1 02113112 1437 g7.6Nb Chlwomolhm- NO UO& 1.0 a.Tf T 02t N1210:37 7447-3 1 ,2•pprpmo-Schlorapropene NO ugL $3.0 2.5 1 0211N21A!37 06.12.E Dwamochl.rumemana ND upiL 3.0 02% t 02013112 It 37 1244S-1 12J11bromw1ft1n. [EOEI1 NO wok 1.9 0-27 1 02 W12 111:37 106.03.4 O1MwM0MIhlne NO UWL 10,0 0-21 1 07 W1216:77 74.9S•5 12�01chlorobanz... NO uR& 5-0 0.30 1 02/13112 18,37 95.50.1 t,4.OkMw6b.nlane NO uO& 1.0 0133 1 02/11112 16 37 M-46.7 trw•1 a-0Icmwo•2•bman. ND uy 100 to 1 0211312 I6.37 $10.57-0 M-Dkfuwda*o4 o NO VA 5-0 0.32 1 0MIQ Ml? 75-34.3 124Dk19wcowsno NO uW1 1-0 0,12 1 0wwQ 11:37 to7.p6.2 1,1-DWal roanune NO uWL 5,0 0.56 1 021t311216:37 75.35-4 ds•0-aeNvoeNona NO vok 5.0 DA I 027t3112 15:37 156.59.2 tlYlu-1.2-Dleldoroetnene NO uyL 5-0 049 1 02113n214:37 154d0-5 12-Dw,Nw.Propena NO mak 1.0 0.27 1 02H31216:17 7947.5 S,S•Okheoropropano ND upL 1-0 02B 1 021311216:37 142.20.9 rM-1,S-Ordrkr7opropane NO ++A 1.0 6.11 1 OVIV12 16:27 1006f-01-5 Date: =2612012a9:64AM RE PORT 0FLABORATORYANALYS13 Palo 64139 Trw MW 014 not G rapmuocw. -P1 n U. .aaaut"MAaan mo nt at f4" Amgfto SarAom. p1e Pae. Aulye ut hin Pa.. An4lyanAl 6aM.aa, I", Pa.. A,LWYM. .l aarvH.e . Mtoe cppppnslca 205Enhi-dwRad•S "Sap"'"0r 1. Ed... HC 272ba Aah.N.. HC 2doo Hunyrw�a.. NC 29371 t3M*2341971 t0201254.7175 17M 475 9W2 ANALYTICAL RESULTS Project: SURRY CLOSED LF Psa Projoa No 911/105/ 3-pl.1 MW-1 Lab ID: 1,1111151001 Coll. clad: O2MV1209:20 Ra-F-d: 02110r1214:24 M.oh: VYYter Report puamatere Resulta Unlls Llmlt Mot OF Prepared Analyzed CAB No OVAL 0260 MSV Low Leval L.ndUll Analylkat Me01od EPA6260 trans-1,1-OlWoroprapana NO ugrL 1.0 0.25 1 OVIU1216:17 10061.02.6 E1hylbenaone N13 aryl $.0 0.30 t 0213112 16:17 10041.4 2-Na.anena NO upY 50.9 0.45 1 02AU1216:37 591-76-6 Iodomatharte NO uWL 100 0.32 1 07113r1216:37 74.04-4 N1.1Nywa CNOM& NO ug - t.a 0.97 1 M, 3112 t6!37 754W2 4-Matm�1-YpeM1gnonf{MIBIQ NO uok 100 0.31 1 M20211:37 106.10.1 Srynne NO uplL 110 0.2E 1 4WINQ 11:37 1p0.42-a 1,1,1,2-106 dqq-1h.n. NO ug14 6,0 0.33 1 021131T219:37 09.20.5 1,12,2-Teka0111era.11ans ND ugrL 0,0 040 1 021131121017 ?"-5 Tatranlloroolhan. NO ujvL 1.0 0.46 1 0211Y121637 127.16.4 704wne NO uWL 1,0 0.2E I 02131121637 105-66.3 1,1,1-T0rdlrvoa6ren. NO uWIL to 0.4E 1 02131219:37 71-5S-4 1,t,2-Trk3lcaraelnana NO uWL 1,0 0.29 1 0213112 Igr37 79-DO.5 TricMvoaof.hs rID uWL 1.0 0.47 t 021311218,37 79.014 Trkhlowduiwomethartk NO upt 1.0 0.20 1 OVIU1218:37 75-68-4 1,2,3.T,whWaprOpan• NO uWL 1.0 0.41 1 0711311218:17 9611A Yat11 Lunn NO .04. S0.0 0.25 1 OW1302 ISM 101- W Vinyl cWffwe NO uyL fA 0.62 t 0211 at T216:37 7"1.4 Xylone [T.Aap ND UA 5.0 0.66 1 07/13117 16:37 1330-20.7 Sur7ouales 4 Ek."I aobmaan. (31 97 % TO-110 t OW131121627 1604K" OwramvM.vamunane is) 104 % 7003D 1 021311211:17 168641.7 1 ,2-0kNvoethnw44 [SS 105 % 70-IN 1 0211111216:77 17050-07-0 Tolwna-d6 �S} 94 % 74130 1 02MU12 10:37 2a37.2" 23209 Alkarinlry Anstyhcu Moinod. SM 23HB AAAH.Lty, ToW as CaCO1 67400 uok 5000 SND I 0217112 M-00 921a5 000, 3 day A"ytkai Medlod' SAi 52t0S 1100.5 day NO up4 2000 2000 1 OW102 17:10 DVIGO$2 17:20 94 3091 IC Anlcna 26 Days M51Yudal Method: EPA N00-0 Sul nte 9330j WgA- 250000 6000 I 0212011221:14 14600.794 4600 ChlOndo AnmMtcal Mslhod: SM 4500•CI•E Chlenda ND u01L 5000 woo 1 OWD1120937 IW7404 6710E TOC Anskoin1 Me lnod: SM 521 OB Total O.OaNt: Carbon I930"a& 1090 1000 1 02aW122251 7440-44-0 0e1e: 02!'WO 209. 5a AM REPORT OF LA BO RATORY ANA LYS IS 7f" r.ppn %AAA nw M nrp.anc a, slap In Nk, Mykl•A M rntran oerra.nt Of Pap M/a11" 5brA rf. IM Page 7 of 39 A.rr A n.lya..16.nnnr• Inv we. A- yraa, ArrWcn,,m. Pan A na,yarar A-leaa, Ina `aceAnafytrcal 706 E.N 4.efew Re.d - SWe A 2d73 9 -H . Hem Ifnca, Mr. arp rm w...��am. Ed.n, NC 372. Ayyrry. kC 76601 WnM+.Nlr NC 7D079 1?7e 2+ 44701761-Wrl {79a4759= ANALYT;CAL RESULTS P-Ject $URAY CLOSED V pace Pfger No. 02111951 Sample: MAI-7R L.ah la: 1211199IWZ C040 Clad. 0710i712 T2'00 Rfulred: 0271 all 210:24 McOM: VWINF ;I.Pwt pfla.dl.n Rap Wt. Lbulr LonN MDL OF Prapmed Analyzed CAS No. Qua, 00101CP Oroundwalar Anuma+y /uaanic 6ar�yln her yllx+m Gr6nxun it+fOrrNWm C06e„ COppe. Lead µeleel Selsrwm Sol- Thfl+um Vanadium Zhc 11260 IASV Low Level Lfndrlll A4.lepe AayW,tnla 6QniMf &OmoWaomemrne 6rP �r�od d+loromalh one 13romefOrm 8romd"llianr 2•6Aanone (MEK1 Conran Iaw16de Carbon telfasnlarld. 4 h io.o W np.na C hlorPeinenr Chlweform rh FV er+anr 1,2-D6romr+ 3-ph19r9Pr9Pfn. OM0flgonierer6elhane I ,2•DA><ompnri.na IE061 DiwcT malhfna 1 bDklwuvpenrme 1 ,a.DkMoeOhencena Neer-1,4.p1 W oro-2 fwlrne 1,1.OkhlorOelMnr 1 ,2•Q1CMProa9Ylnf I,5•Q�chroroem.n. As-1 2 •d,cnlofvalhfna Irene- l,.', •01dNofdrm&ft 12•DtcNwopropona I ,3•Dtehlorm.pana aim I,O.OIQd twopen. Vale: MM2012 09:56AM Pnalyllcal Math" EPA 1101 D Pr04 .l,on MflhodEPA 3010 No ugR 6.0 5A 1 0211&121145 O21I 6+12 DO 50 7440.36-0 NOVWL 10.0 50 1 O271W$211-45 O21IW1200:50 7440.3a-2 1141VGfL 100 6.0 i MW1211:46 02f16fl200:50 1440.39.3 ND uyl In In 1 021167121143 O211 WI200:50 744"1.7 ND ugfL 10 1.0 1 O21S 671211-4$ V7l16r120O: 50 746043.13 NO uprL 100 5.0 1 awl IV) 2 11-4$ OF I&12 DO: 50 744047.3 No ugfL 10.0 5.0 1 927IWI2 11:45 O2l16112 00:50 7440.494 ND ug& 10.0 5.0 1 OZOIW1211:45 0211611200:S0 744040-6 NO uQfL 10o 50 1 07l1 W1211 �5 07116r1200�50 7"11.924 ND u91L 100 5.0 1 WIV127,:a5 02fI6ftZ00-50 7440-W-0 NO u$L 10.9 10.0 1 WIW1211:45 QZW200-50 7712d9.2 NO uOrL 100 S.0 I 02116f1211:45 U211811200-60 7440.224 0-0 uyL 55 SA 1 02AW1211:e6 02AW1209:50 7440.2E-0 NO up+L 250 50 1 O&IW721145 02116f 12 D"(I 1440.62.2 NO PyL 100 10O 1 02176f121145 Q211N1200.50 7440464 AnAlyDmP Method: EPA 6260 NO u91L 100 22 1 0211362 W03 6744.1 ND uyt 200 19 1 0LT311219;01 M7.13.1 NO u0'L 1 0 02S 1 OFTN12 19-03 71.43.2 NO 'A1 0 0 T7 1 u"A2 11i'03 74.97-5 NO o9f1 1 0 0.1E I owl 11219n1 M27.4 NO uyL 3.0 0.26 1 0211301219:07 75.25.2 NO upL 100 029 1 020311210:03 74.13.9 ND uuk 100 0.96 1 02f1N19 19:03 mll3-] NO not 100 12 1 OFI37I219;03 75-IS•6 ND upt 1.0 0.2E 1 QW431I2Io:03 30.23.5 NO WL 30 9.22 1 OFty1219;03 10A-90.7 ND upfl 10n 01% 1 OVINIZ 19;03 r500-3 ND uWL 5.0 0.14 1 02f13rlZ IW113 67.6R3 NO LrA I.0 0.11 T 07l13y12 1913 7447.3 NO ugiL 13.0 2.5 1 02f11r12 Ions 66.12.E NO vg& 3.0 021 1 OF1 N1219:03 124d6.1 NO opt 1.0 1.21 4 Owl 31121003 106.93-4 NO uO& 100 021 1 0211N12 190 74.95.7 RD up'L S.0 0.70 1 OFINI219;03 95-50-1 NO uyL 1.0 0.33 I OVIN1219J :03 I066-1 NO UWL 100 1.0 1 02HN12 19;03 110.574 ND upL 5.0 0.12 1 OFI371210;03 M34•5 NO upfL 10 012 T 0211N1219:03 107.06-: NO up4 50 9.56 1 0211N12 19:03 75-564 NO UWL 5-0 11.19 1 02f1N1I 19:03 155.59.2 ND UWL 5-0 0.49 1 OFly1219:03 1364P-5 ND up& 1-0 027 1 02113r1219!03 M17-5 ND UWL 1.0 0.29 1 Oir1Y12 19:03 142.26.9 NO ug1L 10 013 1 OMNI219n3 10081.01.5 REPORT OF LABORATORY ANALYSIS TAN •.aOR N a nvi � nywj4 ..agp1 n rf -WA n ra waMr1 W "Mel P.q Anol}vgl $*-ec f� Pen An.1 y11. E.rx14H, Ina Pfr. Anfly9aal pnn4aa, kro- Par. AnNylreal rrrxlea., ,m. aceAnaVicale C3 Eaa+M.a6aiRo.d-E JMA 222S R""""P 9600 nworl Mr $Ae Ion €d.n. Ns 272AA Aan.rah, NC 26600 11yn1a,rwa, Ny M76 (7761621 M71 I676125.1176 1 NY *759p92 ANALYTICAL RESULTS proJecl: WARY C.1.D9E0 LF prce proved No.; 5211196I Semple MWAR Lab ID: 62111951002 Calladed. 021O911i S2.o0 Remo vod; 0211IN121424 Maetd. VV ler Report P mra rnelar9 P:0104 unto LATH MQL OF P+ep.re6 &.eryted CAS NP. Q-rM 6290 MSV Law Leval Landfrii Ane:0.81 M.M.d: EPA 6260 Inns-1,3-9fftfYoroprvP.n. ND VWL to 0.26 1 021T3112 19A3 10061 02.6 Elhythsnzfno NO upfL T.9 0.30 1 0711N121903 100.414 2klexanons ND upWL 50.0 0.4E 1 92f131Iz 1P.03 591.784 lodemallanf 01D up4 10.0 0.32 1 Ov1112 19;03 74.60-4 Mo$ryIens CNulde ND uA 1.0 097 1 02A 31,219:03 75.09.2 4•Megryl.2-p.nulwn. IM16Kl 140 VgrL 100 0.33 I DW311219:03 IW10.1 6ryren. NO VOL 1,0 0.26 I 0211YI219:03 10042.5 1,1,1,2-TepfOMMDe7ione ND uOk 5.0 0.33 1 02113r1I19;03 630.204 1.12,241rtrach4or0solane ND VQ4 3.0 0,40 1 ozfIWI219;03 79.34.5 TabaWaoe9+ene NO v91L 1.a 0.4E 1 07JIU1219:03 127.1E-4 T91ua*s NO u9R 10 0.26 I OFIN1219,03 1064a.s 1. 1. 1-Trlohlore fe+ one NO p9fL I 0,4E 1 Owl Y1219.03 71.554 1,1,2-TnMlefeem.na NO u9k r 0 0.29 I 0F1 N1219'113 79.00.5 TrkNor0e1h4ne NO uVfL I 0.47 1 OVIN1219:01 794114 TrkM6r0Au0r0me1hAns NO ug1L t 0 0.20 I OVIN12 19�3 73.694 1,2, 3-TdoNoreproP.ne NO OL 10 0.41 1 OL13712 19-03 96-16d wyry ocatale NO ug[4 70 0 0,25 1 0271N12 19-03 10646-a Vinyl chiorld4 NO UVL 1.0 OS2 1 OF13n21003 75-01.4 Xylone(T01aIJ ND up1L 50 0B6 1 02JIU1219:03 1330.20.7 4-apH. 4dir6m6AuaoLan tone (S) 96 % 74130 1 OFINI2 19:03 e60.00.4 pi0r0munno.r,melhfne 151 107 % 701)0 1 OV13012 19-03 186E-63-7 1 ,2.OIcMwxth.n F-(R (6} 10A K 70-130 1 02lINI2 i713 17060-07.0 Tduenf•04(S) 91 % 70.130 1 OF1311211107 2037-Z6.5 2320E Aloslhtlly Ansyucfl M4dmd: 8M 23709 A4alnlly, TOlal By CoC01 1230d0 ugAL 5000 man 1 09/17112 12:00 32Ian 900, r day Ane".pl Melhed $M 5210E 800, 5 day ND up4 2040 2000 1 VVI1112 11 00 d2716712 19.47 20.0 IC Anions 26 Days Anaylku Mamod: EPA 300.9 Skd(214 NO uok 250009 5000 1 02r2WT22120 14408.79.4 46" C1ltvndr Analyi,efl M49ivd. SM 4S00-0-6 ;hW6de NQ u0ti 5000 %00 I 02720112 09.3E 16097.00-8 631" TOC MMyllarl Melhod. SM 5310E Total QFQ-IQ Gorton 3620 690rL 1000 1000 1 OH2OAZ 2);01 7M0-44-0 Pepe 6 al3i Dab: C117WO12 0.56AM REPORT OF LABORATORY ANALYSIS T1q nw. NM +W W .9104 lad .-PC- W. mrout ire xntNn K*aM Of Pere Arwhaw ame RAMS Pape 0 Of 39 r Pee: Ar ".al 5arvleea, In.. Paw Anaryeeal aaMe.a, I" Peer Anayed l Somi- Inc. a�Analytical 2m E1n 4aaswa Rwa • 9wt.A 7776 wNrruda Or BeOo weay A r 9, 100 Edrn NC 772M AeM . MC M04 Hun�re nu.. NC 26070 473ekI73AG0h 1e761234-1175 170c}!15-9097 ANALYTICAL RESULTS praleet SURFRY CLOSED LF Pau Project Na.. 92/17951 Sample: NW-16 Lah 10: 112111541041.11 C6149 ad' OVOW12 15:00 ReceNad: OVi Oil 14:24 Matrior Mist Report Parunelera R6au0: Unit, Llmll k1DL OF Prepared Aneiyzed CAS No. QUA 6010 PCP 0n dwatar Antimony Anionic Barium 8erylllum Cadrrlum Chr6mkrm Coball Capper Lead Nickel S40mwrl SiNer Thmleurn Vanadlum Z.. 8260 MSV Low Level Londflll Acalone Acrylonanle sonlen1 8ralrWChPMOrrNih.ne Bremodchtoremrthma aw"%hm 8m maehena 2.1t.rtanene f MEK P Cotoan aaulAd: Carbon tatraohlwlde Chlero0anlane Cnloroelhena ChI0f0kIIm chlor6melhm. 12-Mr omo-3•00aroptopanei DioromeGdoromemane 1 a-OEa PrrIPa9lan a IBDBI D17remornenana 12.OlcMorohonllone }.4.OIaNarooenaene vem-1,4-01d4aro-2 butenr t,l.plworwenane 12.OkMoraelhom 1,1-0kNoroolhene elt 1,Z-0Ichroroe0i one Ima•174HWOrolN me t,2-WcNwopropane ],S-Dlehloroprppelle tla-1,]-0lcnlofoprppene Anaryuul Malhad; EPA K10 PrapantiM MethodEPA 1010 NO uWL 11.0 5.0 1 WIWI211;45 OVIV1200:33 7440-31-0 N9 u04 t0.0 5.0 1 OVI611211:45 0711V120OL53 7440-39-2 31,8J up& 10o 5.0 1 OVIV1211:4S 0211 NJ20013 7440-19.3 NO UWL 1.0 1-0 1 0211 VI211:45 0201 V 1200:53 744041-7 NO uV1 1.0 10 I OVIW12 IIA% OWN 1?00:53 7440J3-9 ND v01L 10.0 SO 1 MI W1211'AS Owl AM 2 00:53 7440.47.3 NO uprL 10-0 SR 1 07116f12 11:43 02116/52 00'S3 74404" NO UWL 10-0 6.4 1 0011 1912 11 AS 021T81}2 SOW 7446.5048 NO up+L IO.O 5.0 1 MV102 ll;" OVWIZ 00:53 7439-92-1 NO uWL 60-0 5.0 T OZ118112 11 A5 OVIV12 00,63 7446.0241 NO vI $O.O 10.0 t 02MG92$1 45 Owl V1200:53 7732.49.2 NO u01L 10.0 5.0 1 OWM2IT%6 02JI Vt 200:13 7440-22.4 40 u01L 5,5 6.4 1 WV1211:AS 0211 V129013 7440.2e4 NO ugfL 25,0 5.0 1 OVIV1211AS OVI N1201013 744UZ•2 11.1 vgIL 10.0 $0.0 1 0211 V1z 11:4s 021+VI200:53 744OM-6 Ana!,Aka1 Method EPA 8250 ND uWL 100 22 1 02 V12 1926 57.64.1 NO uWL 200 t.9 I 071151t2 1921 S07.11.1 2.8 ug& 1.0 025 1 W V tZ $920 7141.2 NO mg& 3.0 D.57 1 02 W1216;26 74.97.3 NO u04 1-0 0.10 1 07113112+926 75.27.4 NO ugrL 3-0 0.20 1 OV131121929 75.25.2 NO up'L 10.0 0.29 } 0211711219:26 7463-9 NO uA 100 0.95 1 02f13Nz 1929 7o-93-3 NO ugo. 100 1-2 } 02) W 21926 75•+6-0 ND ugx 1.0 023 1 02111f1219:2a 56.23•S 2.3J uryl 3.0 023 1 07113rl2 is28 l(PIP- .7 NO uOrL 10.0 O.S4 1 67113112 1926 MOO-3 NO vy 5.9 0-14 1 02fIV121926 57.643 NO uVI. 1.0 0.11 1 02)1 Vt2 t9:29 74-97.3 NO u01L 13-0 215 1 07112112 T926 96.17•S NO uA 3-0 0.21 1 02M VI2 4:20 +24.48-1 NO ayL 1.0 027 1 02/13112 1926 106.93.4 NO uok 10.0 0.21 1 021TSit2 19:26 74-95-3 NO uWL SA 0.30 1 OV13112110:25 9S•60-1 3.0 uWL IA 0.31 1 QVIW121926 tO6i6-7 NO uA 19C 1.0 1 02A 3112192E 110.57-6 22-2 u0A- 6.0 0.32 1 OVIU1219.28 7S-34-3 NO u4rI, 1.0 0-12 1 021131219,26 10746-2 NO uA 5.0 0,58 1 OVIU121928 MIS-4 58.7 v911 5.0 0.19 1 OV 131121948 159.59.2 NO uyfL 50 0-49 1 OVIU12 19-23 1S8.60-S NO uVL 1.0 021 1 O&13112 1921 7627.5 ND uA 1.0 0.26 I Owl Nt21S:26 $42.21-9 N01 uVL 1.0 0.12 1 07)13R2 1926 +0061-01.6 PI"A na10", woo.. IAL Pro A"Iy -I a"ltra• Mr. 0... A-Pvy :r 9-1-, Ina- +, ;alcmnalyticx' XIS E.N Mood- Awd - S.m A 2221 Tw-ua 0. Wo ainea7 Art Sulr 100 Eden. NC 272.E Ar.allhr. MC 7aa6. HuM -11e. NC 2ee1e l]]eleri-6921 Ig26y26.•1170 f7e41675.9092 i ANALYTICAL RESULTS Projeel- SLIRRY CLOSED LF Pace Project Na.: 92+11951 6empla: MW-16 LAb ID: *21119111003 Coleded- CWW 1215:00 Received: OVIV12 t424 Motrte; Mist Repen p.mm.lara Reatmo tkdh Urril MDL OF Prepared Analyzed CAS No. 0u41 e3a0 lA6V Law Leya1 Landfill 41rt-1,3-01chlorepropene E9ryWenzene 2•Meaen6ne lodemetlme PA."ma CNorlde 4•MeOhyl$•panlanonA IMISY4 Bhlene 1,1,1,2•T�Oaclaoroefione 1,1,2,2-T:trachloroeihane Telnehloaoalhono Toluene 1,1,+-rd9rddr9et+me 1,1,2•Tdchlaplplane Trkhloroalhons TrkhioroPkwPomelhma 12.}Td4Ne+9prOParhe Vinyl aoelate 1nnv+ehtarlde Xyfene (701a0 3w *gulls 4-111-11uuehenaene (S] nhuomoAvo7omemonl jSl i,2-DkhlGoetlhane-04 (SP 76krena•d6 [SI 23300 Alkalinity Aik.an lei, Taul as CaCO3 52168 000.8 day BOO- S day 30OA PC Anlona 26 Day* Sullole 4 SOO C hlorlde Chloride III0E TOC 1T tiW Orgmic Carbon 0e16: 0712812012 00.56 AM REPORT OF LABORATORY ANALMS peoe l4 6T 39 n6te 0N78r7O $2 69:56 AM try6+sw e1161 net be elProduMd. 60.0 a1 MA. .ftw wr llarme eerlrrnt 0 Pan Auyenl s.weea Me. Anelydul M&Mmt EPA 6260 ND uq& 1.0 NO uyL 1.0 NO uyL 50.0 NO ug1L 100 NO uWL 1.0 110 uplt 100 NO UOL 1.0 NO u04 5.0 N0 Up& 3.0 11 Von- t.0 NO u00. $A NO upR 1.0 ND WWI. 1.0 4A ulyL 1-0 NO uOfL 1.0 NO u9R 1k NO uWL 60.0 1.9 uRk 1.8 NA up1L 5.0 96 % M130 105 4L 70.130 103 % 70.130 93 % 70.130 Melylkel Method: SM 23200 49700 .91. 5006 MINOGer 14e010d SM 52105 2494 u01L 2060 Arui"-1 Melhed: EPA 300.0 NO uWL 250000 AAMIy9Col M1th0p: SPA 4500•0FE NO UA 5000 M vUml Method: SM 60108 MOO uOrL 1000 0.26 1 Owl 31121"a }0061-07$ C." 1 O2113f12 10:21 }00.4t-4 0.46 1 Ml Vt21928 501.78.6 0-32 1 0211301219•2S 7410" 097 1 DZUV121925 75.00.2 0.3 3 1 0711302 10:211 106.10- l 0.26 1 02MVI2 19111 100424 0.33 1 OV131121920 E30.204 0A0 T OVi 3112192a 79-345 0 48 1 07N L12 1926 127.1 Rr 0 26 1 OZH V12 1928 106.88.3 0.40 1 02JIU12 t9:26 71-554 0.29 1 OZIW1219:26 7940.5 0.47 1 Mao I219:28 70.01.4 0.20 1 021TV1210:26 76$9d 00 1 OVI3112 19:28 SS-16.4 035 1 02A.V12 19:28 I06.OS-4 062 1 07JI31121928 75-01.A 0.66 I CPJIW12 19.:28 1330.20.7 1 41VIV121928 460-W4 1 OVIV121928 t868.53.7 t 021131121026 OOS"7.4 1 WIV12 426 2037-M•5 500G I OZIT7112 1700 2000 1 W1111211 00 DVIV1215A7 5000 t 021,1y1221,42 11806.79.E 5000 1 42R V 12 00 rt0 1666740.E 1000 1 DVM1223:13 7440-444 REPORT OF LABORATORY ANALYSIS rwr report NM wI ha ropmduera. -010 M. ..•.•out lh.-,u. ry wm or Pre. A--,e satyr1a Ire 04.65 Pogo 11 e09 ��'� ' � '�1' Pt ea An.rrd.N Im1r.4. I n4. :05 f.w Me. nwQ • 6•.M n Paw Arulylle.l somtea t, Ine. 2M R-n . d Pic. Aearyme.l a.ryl.a., lna fK0 K-z Ar. 4w 100 p p�� �`FP71121��� '�!, P.44 Anolytf W lahheu,:mA 705 E.0 a3.4Qow Rv.d - 5� A Fact R1+Yy11N4f 8afHa.. rns. 2225 Rlr .u. pr Pap Ar,mytl.al f.rWee. Ina. =0%" A. 6,0. 100 ,,,1i eye Ed.n. MC x7:56 4.hr.N+.. NC 20WA M, *46 NC 2101E - 1 w.+lraMt �, Ee.e NC ]7211 A.i•.wn., NC 71�4 t1,n;..W. NC 24D71 f33a1623-6021 jatat7t4-7.76 (70y07S9092 [3261123.692+ Io25Ps4.l,fs t704475-109x ANALYTICAL RESULTS ANALYTICAL RESULTS vroj-L BURRY CLOSED LF Project; SURRY CLOSEO LF ph- Prplecl No 92111951 P.C4 Project No: 4711 t151 S-itld: MMIA LaelO: 92111951004 O011m Clad: OVD9f12 l4'00 R-1vod: 02JIO/t21424 Mm". Wa1ec Sample: AIM16 LWDr 92111861DOA Code ded: 0710911114:00 Rnc.W.d. 621101,2 14:24 M11YkNMler Rapwl Repefl Parameler. Reoulta idols unit MDL Or ptapared AnaArled CAS No. Oua1 ParanSetet4 Rewn* UNta L3m11 MM OF Prepared Analyead CAS No. Our 6010 l0P o•r9MndrMlw Analylkal Mehod- EPA 001D Preparalon Method; EPA 30$0 6260 MSV Law L4reI Landfill Molykal Me Y+od: EPA 62S0 Anumanr NO uyL 00 50 4 021M11211'4S OwiW12 D0:57 7440-36-9 V.- 1 3-Or.Wrape vpene NO uyL %.0 0.2E 1 DW13I12 19:54 00061-02.6 knefNc NO uyL 10.1; 5.0 t OLS611211:45 02016112 o0; 57 7440.31-2 Elhylb.mmne NO uyL $A 0.9 1 Owl Y1219:60 100-41-4 fler•um 44.91 uyL 100 SA 1 OWN1211,46 0211111I 09:57 2-Mexanone NO uyL 50.0 0.46 I 071f Yi2 19154 541.71.0 fleyyllmor NO uyL I.0 i.0 1 ;"0.394 Di11611211:AS O71l1!l200:67 14i0d1.7 IodomeNane NO uyL 10.o D.3I I 02yf Y1219.54 74-16i Cadnvum NO uyL t 0 = 0 1 02f16r1211 �S 02111r12 Do:37 7i{6-13-5 Methylene Cnlwltl. Hp uyL 1 0 0.17 1 ON17117 19:54 IS-09.2 ChromNwm NO uyL 100 $-0 1 071t6r1211,45 O7f1N12 DO-S7 7440-47.3 4�1,1e mrl•2-penian9ne (Ml ElsQ ND uyL 100 OA3 1 027tY12 19:54 I'm 10.4 OebaR 204 uyL 1 D.0 SO 1 o2f16112 11.4S OV W 2 00.67 7u4140-4 slyr.ne NO uyL 1-0 0.26 1 0214Y12 19:54 100-42.5 Capper NO uyL T0.0 SO 1 02ft6f1211 45 OPr I N 1200.67 741450.E 111.2•TmNcNNorn4lr one NO uyL 5.0 0.33 1 02113W lIl:54 130.74E Lead SO uyL 19.0 1,1 I o21f61I2 11;15 02l16112 W-57 71.1.1 1.1,2.2-Totraekloroilhin. NO WA 3.0 0.40 1 0711311219:54 7IL34.5 NI:4al 9.IJ uyL 50.0 5.9 I 021161f271:45 0211 IVi200'S7 7440.02.0 Tou.chlorvamone NO uyL 1-0 0.4E 1 027131121934 127-I&c 5eler4um NO Vol. 40.0 10.0 1 Dy16f1211;45 Owl W12 COW 7712.49.2 TowMe NO ugfL 1.0 0.26 1 =131121P54 100-16•] Surer No uyL 10.0 5,0 ! Dy16112 +1145 Qy11ff2 cc:57 744Q-n-A 1,1,1•Tnohlcaa 4na NO uyL 1-0 0.4E 1 02r13f1211:54 71.51.5 TholNum Np uyL 5 S S,i l 02111R2 +1;4S 02116/l2 00;57 74i 0.2E-0 1,1.2•TncMN6ethana NO uge- 1.0 0.29 1 0y131f 219.54 71-)45 Vanamum NP uyL 25-0 5,0 1 O?Jlwl21145 Owl P12 00;57 7440.42.2 Trlch1woothene D.54J uIXL 10 OAT 4 021f Y1219.54 19.01•6 Xtnc 110 uyl t0 0 10.0 1 02116f12 11'45 OV1111; DD•57 144036i Ttkh1w61uorum44hen. NO uyL 1 0 0.20 t Oah31121114 754M 4 1,2. 70chImmoporte NO uyL 1.D 0.41 1 c211Y12 19:54 96.114 a260 MEV Law Love Landllll Anatr0c41 M.lhvd' EPA 1260 VYtO acatale ND uyL 10-0 0-25 1 owl ulz 19;54 10S-05.4 Acelp NO MO+L 400 2.2 T 021t k 12 f9:54 67.84.1 Vmyl eh1wide 1.1 u9+L 10 0.62 1 Y2H5y12 t1;54 7541.4 AerywnPraa ND uyL 200 +p 1 DV 31 1 59'S4 107.53-1 %yl. ne{Tv1a1y NO uyL a-0 I, so 1 Owl Y1219.54 133040.7 Benzene 0.751 uyL 1.0 0.23 1 O21f Yt2 f05 71 AM Sf V*f.a &pmeC410l fna D+.h4 NO uok 3 0 D. I IV$341219:54 74.97.5 4•Brpmv[uvr96en=ene lSl o7 Si 10 30 1 OW:U12 19:64 46DA0.4 6rerne&040'p 10'ane NO uyL 1 0 1.10 1 021t Y12 19:54 T5-21.4 Olbtom iburuoffloul [Sl 4O3 % 70.130 1 Oyn 1rt211YH t161-13-1 [lromnarm ND uyL 30 0.79 1 021f Y12111'54 7S-25-2 1s•alcNwoerhane•W (SI 11) A 70.130 ! 0211311219,54 1706g•07-0 Bremvmellane NO uyL To.O 0.79 1 QZn W'1Z 19:54 7.-03.9 ToWane-d5 (Sj 94 94 70,110 4 02113112 f1:54 2037.26.5 2-5danano fMEN NO 4yL 100 0.9E 5 W11N2 19:54 76.93.3 2348 AlkoIInRy An.tyllcal Method: SM 23206 Carbon til"INk NO uyL 100 17 1 C21t3112 19:14 75.1" Cemen I. br.d lenw ND uyL 1 0 0.21 t Owl Nt2103A Wn5 AIkohily. Talal as CaCO3 19100 uyL 5000 5000 f un a112 $200 Chl-tra e.n. a." uyL 3.0 073 1 02f13112 19:SA 104.90.7 5210It BOD• 5 day An.11flcel Me mod. SM 52106 Gnivochan4 0.77J ug+L 10.0 0.54 1 O211Y1219:34 73-00.3 ChIolvinrm NO VWL S.0 Old 1 D2r131f2 19,54 67.E&3 SOD, 5 illy NO uyL 2DOO 2000 1 oaN IA21I,n DVIW1215:47 W,83 ChImamelmon. NO uyL to 0.11 ! owl via 2 t9:54 7417.3 12•bihromo-1•Chgrpp,ppan. NO VA 13.0 2.5 1 Owl x12111s4 111-I2-! ]DO,D IC Anions 21 Qoya An4>ritcol MelKod: EPA 30D.0 Oafrom6chlorome+h4ne NO uyL &a 0.24 1 0211]1121g:54 124J6.1 50fale 717W uyL 250o0O SDOO 1 DN20112 21:55 1410149.1 1 �•plbromuel+.n. 1EDS1 NO uyL 1,9 1.21 1 OWN, 219:54 106.93d Abtomcmem4ne NA uyL 10,0 0.2T 1 0211311211A4. 74-91-3 4100 Chtodd. Analypcal Maraud; SM 4500-CF-E f 2 Otcnlpahentane Lu VWL 50 0 311 1 ON43112 19,54 95.50.1 Chlonde 10200 uyL 5000 3o0o I NIM12 09.0 16167A0-S 4 ,i•Olpnw9tren2Mo 11 uyL 10 0.33 1 0211Y121934 f06iE-7 Van. 1,{ DI�Ne10-2-hulana NO uyL too 1.0 t Owl 31ta 11'34 510-bt4 531011 TOG Analytical Me 0f0p: SM Sat 08 1,I-Dlahlvt0e1harla 3.4J uyL 5-0 0.52 1 0711 U1219;54 75-34.7 rnlal Opp -Carbon 14M uWL Iwo 109E I OMW22323 144D-4" 1-2.0ictdw9emane NO VWL 1,0 0.12 $ 0211N72 19:54 1O7•o6.2 1,1-❑chlereethint NO uyL 5.0 0-31 1 Carl N1219.54 75-354 da-+ 2-DKnwroetn.ne 31.7 uyL 5.0 0,11 1 Oyt Y1219;54 155 5" Ifeno•7,7-pknlvreed+ane ND uyL 5-0.aAl: 1 ON1311211, SA t56-00-5 1,2.OIct9ololxopano 1.5 uyL 1.9 9�27 1 0211311219:54 7"7.5 + ]�O+CNwoprepane NO uyL 1.0 c.21 1 oV 3112 49:54 142.26.9 Cls-1,3•DkoNo oprop ant NO VOL 1.0 0 IS 1 Odf12114Z 101y1 lwl-o1.3 Omit: 021214012D9.56AM REPORT OF LABORATORY ANALYSIS Pag612 0I39 Pilo: 0L21R01209:"AM R EPO FIT OF LA 0 O RATORY ANALYST S Pg. 13 pr 39 T.. ntou-N q-e Wnsmd wd -Pt n h.r, 7"rota" Mal MIN monod+4:.d.1c.Pt h hA , r-0y . -re, mn..rA e1 Pop Aty,f-, 5.n+cP. rx re.ewlY,. wrnsn wnrM of Pau I,n.irbtM $amu. Imo[ P...AnpydAer a.nlw., Ire. F... An4 VWl a.MNf, Me- PA 04 Analyf0[IMryle.i, ln[ • Pan. An.lyb ul a.Mtwr, 16t. P.- A.61,4.1 e.MM.lee Prr4 analytleal5anere /.a �,1�.�}'�..�� (�� aC.G1'11lW icaf. 7Do E.0 N..do,r Ro.e • 1W1. A 2225 Rir6r it 96o91Wle.y Fw. Sun 1G0 p �j �.�j (��/ p��p1r !(11 �4Qi 7C1 FAY N..eo.r RP.d • 5uia A i22S Al""do G WM w.e.r n.e Emu t�0 1' ed.n NC i77ee A.MN NC 26e04 ywn -Wa, NC 26076 y pe3� Ed... NC 2725e AsM NC 25W4 ANnNr.N. NC 2W79 t1M6 V] 71 I52.)2M-7176 (704075411M i3]6)QI 21 102e)2U-717e f70AA _9M ANALYTICAL RESULTS ANALYTICAL RESUTS P,*.c suRRY C1,.O5FD LF pwpre l BURRY CLOSEO LF Pay. P1e14c) No.: 9211/951 Pace Pmlecr No„ 02111951 Samoa: MIRV-H LablO: 921179a1006 Cpuaited 0VM$217:00 Rd -Nod: 02 INIZ14:24 Maert: YAW Sampla: WAM10 Lab to: 22111951001 CoWaMed: 02AO11217:0C Re"Ned: 02/10/12 IC24 Waft: Wlalor R.PmT Repvn FaromeWra Re.ul1. unik LImW MOL OF Prepared Anaryad CAS No. Oua1 PoramellFt Rouft Emits LImI1 MOL OF Pmm,sd AMhd:ad cm No. Cga1 Gala ICP Rrouncwal" Am""l McOwd. EPA6010 Prepar.uon Ma01od: EPAJ010 8240 MSV Low Level Landfill Mol"ear Melhod- EPA8260 AriRnony NO.01. 6O 50 1 02n ail 211:46 0211 a11201,01 7440-ut Iran.-1,3.01Worvpropane NO uo;L IA 0.26 t OWlWl220:" 1OGS142-6 Arsenic NO.9& 10.0 5.0 1 021161121,:48 0211N120,:0, 7440.3" Ea1ylb.ntaea NO upL 1.0 O.SO 1 02)S31W225:19 IM41.4 Serum 291J v;?L 100 5.01 ='N1211s45 02fIAM2 O1 01 7440.3C-0 2.KdxanA" NO ug& 50.0 C46 t 021M 1220:19 is 1.75-0 Selrlwm NO uWL 1.0 1.0 1 0211N12 11:45 02156112 01.05 744041.7 lodamelnene 61D UP& 10.0 a 32 1 OV%W122019 74-a" Cadmium NO upL I o 1,0 1 0211411211A 0V IV 201:01 744@47-o tAMEry1.n. Chbnda 610 up4 l.0 O.o7 1 0211112 20:19 75-09.2 Chrorrly- NO uWL 100 5.0 1 021M2I sAS OVI111201:01 744o4M 4•Me lnyl•2-pontanom(MISK) NO USA. 100 0.33 1 02A311220:19 IMI0.1 C6baW NO uWL 10.0 5.0 t OVIM2 MAS 0211 N1201A1 7440.464 Sryfen. MO VWL It 9-26 1 021131220:19 100,42.5 Copper NO upl 10.0 5.0 1 Oa161121f AS 0211 Sri 201191 744o-" 1,1,1,2-Tatraehkrvva+arH NO uglL SA 0-al 1 02/13112 MI 630.20-0 L.ad NO pyL 10A 4.0 1 112,1111, 11;45 0211 N1201:51 7439A2.1 1,1,2,2-Tana dlbree 6l am NO ug1L 1-5 C.40 I 0211311220-19 n-34.5 "coal NO ugot SOA 5.0 1 0 J.1211:45 O211N120131 '440,02-0 Talvaehimeolnena NO uge. I1 0.45 1 0WWI2 20-19 127.11,4 9wnhAm HO u9rL SOA 10.0 1 MWI21145 02f 1N1201:DI7752.19.2 Town. NO ug1L It 0.26 1 O2l131122019 106-11W Saver NO W. 15.5 5.0 1 0211N12 IIA5 OVIN1201-01 7440.22-4 i,1,1-Tdchloroathane NO uyL I.0 0.46 I o2n31220-1: 11.55{ Thalkum NO ugf. 5.S SA 1 0211N1211AS UP&1201:01 7440.204 1,1,2-Trlchldroe0lane No ug4 I.0 0.29 1 0211311220:19 T",5 vanadum NO ugfL 25.0 SA 1 OWM211:45 0211N1201.01 744042.2 T1k41lwceviene NO uWL 1.0 o,e7 1 02l13I220.19 79.Ot-a ZLlc I" vyl 10.0 10.0 I 'WIWI211:45 N2AW2 a, 101 7440.6" T+ITIor.4P.rpm.lhana NO uyL 1.0 0.20 I OZI N12 20-111 76-694 1,2,17dd11oloPropena NO uWL 1.0 0.41 1 0211111220'10 911-1814 11260 L1SV Low Ler41 L�thf111 Ane11M11W1 fdetllpd: EPA MO Vhyl acau5a NO uyL sop 0.33 1 02/13/12 20-16 f Oa-0S-4 Action. NO uglL 100 22 1 02r1311220:15744.1 VRry1 CPJWWe NO US& 1.0 0.62 1 0211312 20:119 75-01-4 AoryWnlvl4 NO uyL 200 1 9 1 0211311220: 1: 107.Ur.1 x"Une 1TefaO NO ug�L 5.0 .0." 1 07113112 20:11 1330.20.7 Senxana NO og& 1.0 0.25 1 OVUM20A: 7143-2 smroOafu SMmacnlprPrnsTMm NO OA 30 0.17 1 I'M Ul220;174.07•S 4.8ro mdeuwv0►n=.na(S) 06 % 70•150 1 OL1312 ZO:s9 460.00.4 OremedrNvr6meQi.n. No u01L 110 0.16 s o21131,220, is 75-274 O"Omoeu owmelh.ne(s1 t07'A 70•t1C 1 OL1V 220. 1665-53.7 Era I." NO uWL 3.0 1128 1 02H311220�19 75-26.2 1,2.Cklnvroerhane,d4 ISl 105 `6 70430 1 02AY$220;$9 17066.07-0 9romomaQ�.na HO uyl 10.0 029 S 9211711220.19 74•a3.9 Tow.na-66(sj o4% 70•SSo 1 021t31220:19 2037-26-S 2-8ulanona (MEKI NO uyi 100 096 1 0211WI2 20:19 7& 1.1 23208 AIR alI.W An.Fypur Ma0woi SM 25208 Carbon dlumco NC upiL 100 1,2 1 02113I22a.IS 7515-0 Carbon tetrachloride ND uM& 1.0 0A 1 OW,W1220:10 56-23-6 Nkaanlry, Toret a. C. CO3 11100 uyL 511300 5000 1 11121+Ina 1290 ChofQbWTena NO ugrL at 0.23 1 02n312 20:10 t0a•90.7 62108 ISOO, 6 day Anery9eal 3Aafivd- SM 52108 CRida"ifNne NO UO& 10.0 0.54 1 5211 W1220:t6 75-00-3 Chhwabrm NO +,QIL S-0 0.14 1 02113li2 20:10 51419-7 000, 5 day NO UWL 2000 2000 1 MMV1211:00 OVION213:47 84.95 Chbro"lli'm NO ug& 1.0 0-11 1 0211 Liz 20:59 74-17-3 %2.0&ornA 3-OkFr propane NO 4& 13A 2" 1 02112M 20;to 95-12-a 360.0 IC Anlvna 74 Oay+ Analytical Melhod: EPA 000A pWemoenl«wneoAenr N0 uA ]A 0.21 1 021f3t220:f0 124.46.1 Sulrafa NO uwt 2S0000 5090 1 02rM 1222.01 146064" t]-0R]rGnpemane JEO81 NO up1L 1,0 0.27 1 02JI311220f0 118-:14 Ok7omomamane NO uQ& 10.0 0.21 1 OL13112 ":19 4_9.3 4a00 Chloride An"cal Ma616d: SM 4500•0•E 1,2-acNorpbmxene NO uprL 5.0 0.30 } OVI341220:19 95.50.1 0116111N NO ugrL SIWO 5000 1 o2ROr52 OM2 46667.90.6 1.4-OkNaebenxen. NO upd- 1.0 0113 1 0211711220:1: IM4&7 9ana•1,4.OAc++brv-2 LutknA NO uyt 100 110 1 0211312 20;19 1101-57-0 Sal SO Toe AnaM"I Ma01od: SM S3108 i,S.OloNproeWne 1.91 UgL S,0 0-32 1 0211311220:10 7"-] 12 AIclaorwrMna NO UWL It 0-12 1 OVIU1220:10 107-06.2 TOW0,nu.nle Carbon 2630 LWL 1000 1000 1 02RO+i223:35 7440.44-0 1,1-0kMprpelhen. NO U911 SA02hy1220;19 78.35.4 da- 1X•0rchlvfc6th.n. 2.2J uyL SA 0.10 1 O2111112.:19 156.59.2 Yana-12 OIclnorueth.n. ND uq% 5.0 0.a9 1 O21131220.19 155-m-5 1,2-Olcnlvropopane lL NO W 1-0 O-V 1 o2ri31122C19 7447-5 1,3-Ns, N.P-. NO uWL 1-0 02a 1 b2113r1220-19 le2.2a-9 d1"L21-plrhlp-W.pene NO 41. 1.0 0.13 1 M101220:10 t0081-01•6 W.:02RN20t2 095a AM REPORT OF LA90RATORY ANALYSIS Page 14 vt34 Date- 6712ar25T2 69:SSAM REPORT QF LABORATORY ANALYSIS Page IS 0 39 TN. r.pon Y1.f nord laleedc.d...-Pt.• KA. T nq •A port .nrr wq a mprodu d..enrA.M MI. 1MegA aw "no. en ... p.. Anaiyaal Ue . Inc ,• r.-. u wnbsn --?or Pr.. MfryEeY Sa-k rK r Pa.e Analytla.l earv10a1, Inc Pie. A"yocal lnYlv.., Mo. Pace Anal y4ul Sanlar, Ine. Para An.lyeul 11 v1@v r, Inv. Paw A" llydl 6etrlerr, Inr. Paw A.Wyecel Service" Irb. n�r � fl 1j� al 7u5 E+M Yrwir. +aatl - 5,... • rYC pr.arrdr [H 6E0C w�cer An Sul. lop �1,,n 1� �.117lfR i `^ i 7M Ee a.4.dcw Rod • S-A 7775 nnti..da p 9e00 x: "A- 9. 6 too - Evan NC z7M A0.voa Hr 74a04 rhnr,.yA. NL 2a07a -' wnra c� Ftlm NC 212M Aan.rlih N0 7kk114 Huny..rYld H0 7007e 13361623�921 50211254.71 r1 I7M1a75-Wd2 1=Sv1E73-1921 1a7a17ia.]1]e rMA*7'Yk09i ANALYTICAL RESULTS ANALYTICAL RESULTS PloJec l' BURRY CLOSED L` Prdlect: BURRY CLOSER V Pece P,.pel No.92111951 PEce Propcl No.: 0211,95, Sample: MNf-128 Lah10h 102111111111006 CMeMd Obu0+1211 00 Rucelrad: 0211011' 1414 Mash WNter Semyir: MYW175 LAO 10: 0211f161G06 CoMGea: 0200911211:00 Rd"I"d: 02AQ11214:24 M"k Vwpr Reppa Report Paremel.ra R...;I* Umu Lwnl1 MDL op Prepdrad Andlyxed GAS No- QW01 P6rNmeler4 Rd4.rlla unto 1.111111 MOIL OF Propmed Anahxad CJ15 N. ❑udl 9010 fOP Groun4walor Analyllcel Melhnd: EPA 6010 Pr eparalnn MPlned. EPA 0o 1O aliN MSV Low Love Landfill Analyliokl Mdlhod: E17A 4260 A"tnony NO rg,L 6.0 50 1 OWIfl12 if 45 0Z11111201,i.M 744D-36-0 tr+rla-1,3-DrphlOroprppene NOIWL 1.13 026 1 021131122DA5 10061-023 Al+anlc NO MOIL 10.0 5.0 1 OVIV12 1145 O2J1 So 1201:04 7440.3a-2 EIIlybeluane ND uOIL 1 0 0.30 f 02f!]d1220M5 100414 5anum 20.34 uWL Too 5.0 1 0211911211AS a21t er1201A4 7440.39.3 2•Nexdnone NO uWL 50.0 046 1 OVI311220:4S 591-79.5 OftyOwn, NO rp+L t.0 1 0 1 O2R611211y15 021161t201:04 744041.7 Iadomathlow NO uyL 10.0 0.12 1 112AY1220AS 79.S6A LddrNum ND uyL 10 I.0 I OV1&121t 45 021t//120104 744043-9 M ethylene Chlerlde NO uyL 10 097 1 O2fl311220.A5 75.09-2 CI..gnlum NO.Wl too 5.0 1 021161t2 It 4S o2n 611201:04 744047-3 4a4emy1-2-penlanme tMlglq NO uWL 100 0.31 1 D&IWI220:A5 to-M-1 Cvvall NO uyL 100 5.0 t BVIS02 I a3 02715/12 01:04 7440-40-0 Styrene NO uWL 1.9 D.26 1 02r13112 20:4a 100J2-S Cwpar HD 1V10L 10.0 5.0 1 021t61121145 0271&1205.04 7441;,K-6 1, 1. 1, 2-Teh+cNvrveb+ne NO uyL 5.0 0.33 1 P7113112 RVAS 530-20-5 Le.d NO uyL too 5.0 1 OL9Nf211,45 0211 N120t:04 7439.92.1 1,7,2,2•TdlrocNwoen+nd NO uyL 10 040 1 02113f1220-45 79.34.5 mckal ND UWL 50.0 5.0 1 0211611211:465 02110112 01:04 7449-42.0 Te9ad11oroelhene ND uyL 1.0 0 46 1 02 WT2 20:45 127-10-4 9elwMm ND MprL 100 10.0 1 O21S61121f A5 02JI W 1201,04 77a249.2 Toluene NO uyL 1.0 0.26 I 02 V1220:AS 106-8&3 Shyer ND uyL 10.0 50 t 0V1&1211.46 021107V 04 744042.4 t,l,l•7r1 d111Nvelhana ND uyL 1.0 0.45 1 OZ113MI ZOAS 11-S5-0 Thallium NO uyL 5.5 54 1 O2r1a11211-45 92111v12 Di 04 7440-25-0 1,1,2-Tr6ahIa,ere..ne NO upfL 1 0 0.29 1 02113112 2046 MOO -So Vanadum NO uyL 250 5.0 1 0211&It211:i5 OV IV1201:04 7440.62.2 Trtdllotoelhono NO MOIL 1.0 OAT 1 Ov1711220:45 7101,01 Zinc NO MOIL 10.0 NSA t 0211SH2 tt:i5 OV IS11201-04 7440-164 Trlohlprp4M9rvrnetI1Ana NO uyL 1.0 o.20 1 OVI3112 MAO 7669.4 625Q M8V Low Le -1 L+ndflll AnAVIWAl Melhaa EPA e260 1,2,3•Tncilldropvepan o NO uWL 1.O QAN 1 DWI 311220:45 015-$ J V":tolm4 NO uyL SO.0 0 36 I 021S3r12 M45 11141-054 Ae elan* NO uVL top 22 1 02JI 3112 20-45 07.64.1 VInN NMI" NO MWL MI 0.62 1 pvt3112 20:45 15.014 Acrylprnlrlle NO uyL 7D0 1.9 1 Owl 311229-45 107.13-1 ><yhne IToleq NO up4 50 0.66 1 OVIVf220:46 1130.20.7 Sall rend NO uyL +0 0.25 1 02113f 1220AS 1t-43-2 Sw7OORN+ aremod1ro19me1h.r4 ND uyL 3.0 0.11 1 02113f 1220:45 74-97.5 4.6rvr..vfuolpvend3ne IN 9A % 70.130 1 0211311220:45 ASO.00-4 9.m,.ed.c1lorvmelh- ND uyL 1 D CIS 1 9211111220:43 M27.4 O14rdmdauwomathand [S} 105 % 70-130 1 0211375220:45 1664i3-7 Bromorofm NO uyL 30 13,26 1 E7113112 20A5 76.26.2 1,2-DrchtDf oeindne•d4(3) 105% 70.1311 1 'DWI 37t220-46 1100-07.0 BF-Urno MrI4 NO uWL 10.0 0 Z9 1 OW X12 M45 74.113.0 Tvl-AS (8) 94 % 10-134 1 0211 V12 20:45 2037,4E-5 1-6utdnnna ftlki ND uyL Epp 096 I 02f171122OA5 7643-3 2320H AlhalInky An alylIcal Method. SM 2120E carnlnd:.M94. NOMg'L 100 12 1 021131t229!45 7s160 C. rhon levan>tpnde NO uyL 1.0 0.25 1 QVIVi220:45 56-234 A1kolpay, Tolel AN Ca CO3 1a6v0v ugfL woo 5000 1 0211711212.00 Cl,lo.uvtlnelne ND uyL 3 0 0.23 1 0211,V$2 20;45 109-PO-7 92106 SOD, a daV Andlyllut Malhod: SM 62106 CMordelhmr NO uyL 4 0 a P54 I QV$V$220.40 75-00.1 1:41 .. rvrm NO uyL 3 0 a $4 1 Ovi31t2 2O 45 57-66.3 DOD. 5 day NO ug1L 2000 2000 1 02111A21119 02/16112 15:41 84.0M Gdo.cmamana NO u0R 1 0 0.11 1 OV13112 Z0-45 7447r-1 1,2.Oh. o.ao-]•d.Io.eprvpar.. ND MgIL 130 23 1 0211011220:45 W12.6 OOOA 1C Anwnd 26 Oaya AndlyllCat Mamod EPA 300 0 Dlbrvmacnlorvme9iane NO MOIL 3 D 0.21 1 021i Q112 211AS 124.44.1 Sul tale 33100J U2,L 250000 MOO 1 02f22112 15:03 1006.79-6 1,2.02r w11ve1Mne(EM NO uyL 10 0.27 1 p211311229.45 106.934 Dwrvmomalhana NO uOA. 10.D 0.21 1 02/12152 20:45 74.95.3 65DO Chlende A-VN dl Mehod SM 4500-0,E 1,2-OCN-henrene NO uyL 6.0 0.30 I 0211 VQ N:45 95.50.1 CNlorlde HIS uyL 5000 500Q 1 021011209.43 16581-DO-0 !,A•D1cMofoven7ene ND uyL 1.0 0.33 1 o7Ji]11220A5 106.46-7 ean4. 1.4.01chlvro-2 Put+na NO uWL 100 10 I 021131t2 WAS 110.57-6 S.1 We TOC Anoymml Method 9Ae 53108 1,S4741Nv:pethane 1.2J uWL 5.0 0.32 1 Ov$W1220AS M34.0 1 ,2•Dkhloroefhane NO n& 1.0 0.12 1 021t31t220:45 107-011•2 TerolOrgenlcCarhon 1400 401L 1000 ION 1 O&M011223:45 7440-04-0 1,1-grpMoelrll,rne NO uyL S.0 054 1 0215L1220:45 75.35A tld-l2-Oltnlprv.lh.nr 7,9J uyL 5.0 Dt9 1 OPJ$30220:45 156-59,2 vfA.• 1.2•Dicnlmvelhene NO..p4 50 0.41 1 OL5111220;45 156410•5 I,ZZkhlaeop.oaane NO uWL 1 0 027 1 Ovt U$2 20:A5 7111-674 I,]•DlchlvrpprOpene NO OWL 4.0 0.21 1 OVI.W12 MATS 142.26-9 pa•1.]-DlchlwmNWene NO uyL 1.0 GO 1 021t W t220.45 10041-01.5 Data: Q2R512Q1209:5SAM REPORT OF LA BORATORY A NALYSI S Rep 10 of 39 Dale, O2J26QD12IM J5 AM REPORT OF LABORATORY ANALYSIS Pepe 17 0139 TNe report enar net d fap,vd�"-pl AAA T.. T.'"■,.e-. ew nprpp,od,.-M.F Mawr Pw enryn p "m of P- Arnlr.pel S.- Iz or-k lw -e*. pa. mor Pad MaryGUl Seale*. .rc n,,,,■ y Pa.. Analy"W i.nlw., Ine Pa" A"yueal 6.frk.s, on, Pant AnNytlul l.m..N k.- aCeAf fl oiCaj • 25 E.M Yrrd.• Road • 6,n.A 2225 P-Wd. Df 6400+f.•C.y A.: 5v I00 f ,J • Ed-. NC 2771E A� wl.. WC 25034 H-U, rl... NC IW79 4330KQ3-0 :, +a2.1254-701 [70AW&S012 ANALYTICAL RESULTS Pr.0.1 SORRY CLOSE0 LF Pan prujua Ne.: "111651 Sample: AIW12D Lob IO: 12111961007 Calttcl.d' 0211001291;16 Race[yM- 02 W12 74:24 Mole! Y.Mlu Raw Puomelers RtouR. 11111N LIMA MOL OF Pmpmred Anoly2ed CAS No. QUO 60101CP Un-hdb.t.t Antlmony Ara.Nc Bulum eatrilwni C2,11N. n Chromium Ceb.1 Goppor 1.6441 NkW S.ludum Swu Tnallum Vanadum Iln c 92U MSV Low L-1 LandN11 Acetone Banlan4 &omon,l-rh.n. 8=ddu0rnm*11-6 Oreme W. &omom40,er.. 2•Bu1.n4n4 (M EK} Carbon d-M4. Carbon ravacnlo.+e. Chlorob.nxen. Chw=sna Chlefolenn Chlof than. 12-0M Omo•]-4hlorop opens Owlorn4churomatliane 12-D6xomoolMne(EDB) D.nrwlw meOl.ne r ]-L1kNorobenr.ne t Okh,wobMwe 1reno-t,4OlcNoro-2-bulen. 1.1-DkN.r..th.n. .na 1.2-DWOVe4+h 1,1.O1cN4feelMne dt S2-0IrNWwlhme u.f.a- t,i•dd4oroal.one 1,2-D1eNn.apreptna I,]-DkWoropfpp.r.a do• 1.3.Oldauoprop.na Dou 02RN2012 09.66 AM Am"nl Mom& EPA 101 O Pr spotolm Malhod: EPA 3070 NO upL 9.0 5D 1 0IWIZ 11:41 O2R&1201'11 7"(1-SE-0 NO uOIL ID O 10 1 02n&12 WAS O21r&1201;11 7H0-3e-2 6.7.) uQ& 100 5.0 1 OWM2 $1.45 0711&12011A 7410-39.3 NO pq4 1.0 1.0 r 0215611211%5 0211&12 O1;16 7440-41.7 NO upl 4A I.0 1 0211&}211:45 0211&124116 7410i3.9 NO up4 109 50 1 OW I Sri 211r45 02f1&12011a 744047-3 NO uQm, f0.0 50 1 0i116rl211A5 021161t20r:11 1140484 RD UWL f0.0 59 1 =I &,211--45 02111f1201!11 7440.104 ND upL 10-0 5.0 1 0211&1211-45 Ml&12OI111 7434�92.1 ND upL 10.0 5.0 1 D2116h211.45 0&&1201�16 7440.02-0 NOuOk 10.0 100 1 OT1601211:45 0211&t20116 7762-49-2 NO UWL 70.0 5.0 I OXIV1211:4S 021W201;f6 7440-22-4 NO ug1L 6,5 5A 1 M01121,;45 021161$2, 1: 7440.26-0 ND UWL 25.0 5.0 1 0211111211A9 02111f120116 7440•62.2 NO uWL r0A SO9 t O211NI211:45 0211&1201:16 74460ddi Analybt* Mmolwd-EPA 8240 HD upL 100 212 1 IIVII1122t'10 87414-I NO u91L 200 1.9 1 OZh N1221:f0 107-Ml ND uq+L 1.0 035 1 02113f1221:10 71d}2 ND VVL 3A 0.17 1 02f1311221:r0 74.97.E RO uqA. SA 0-10 1 02N Ul2 VA 75.27-A NO ugfL 3-0 0.2E 1 021131122110 75.2$-2 NO 4L 100 029 1 =1311221:10 7413.9 NO RO'L 100 O-9d 1 02hW1221AD 74F93.3 NO uWt, 100 M 1 02/13112 21-1O 75-15.0 ND nWL 1- -D o-25 1 D2f131'221-10 W23.5 ND uqL 30 0.23 1 DW3f1221:10 10&9D-7 NO upL 10.0 0-64 1 OVIW1221:f0 75.00.3 NO uW1 8.0 0-146 1 4211 W1221-10 87.66.3 NO uyL I.0 0.r1 I DIM 311221 �t0 74.97.3 NO uplL i3.0 2d 1 0211311221; 10 66.12.1 ND ug1L 3.0 0.21 I 02/13/1221 :'a 124�6.1 NO upll 1,0 0,21 1 0211311221:10 f06-93.4 NO ugeL lOA 0.21 1 027131,221: in 74.15-3 ND VO& 5.0 0.30 1 1121%Y122T.10 06.50-1 NO UD& 1.0 031 1 0211711221:10 10446.7 HD uWL 100 1.0 1 02113f1231;10 110.57-8 NO UWL 5.11 0.32 1 02N 311221:f0 75.34.3 NO uiVL 1.0 0-12 1 OVIU1221;10 10746-2 NO u9+L 5A 0-36 1 owl W1211;10 75.35.4 W NO u 5.0 0.1E 1 0211Y1221:10 IWW2 NO uWL 6.0 0-41 1 0211311221,10 156d0.5 NO upL 10 027 1 O211 W1221'1C 71.17.5 NO uQL r-0 0.2E r 02f1511221-10 142.28.6 NO upL IA 0.13 1 0NI211221-19 10061-01-5 REPORT OF LABORATORY ANALYSIS Ilw f.pan nr M1 he ,.prneuced. -m lo, 7 . rs4.wrt T,. amlre co -t P acts A--V+ Sena... oN Poe. A ulyeaal=lt.s-Ina P." Anoyma.l..Mow M.. Ps" Anelye.d 6.rvl.at, M.. MS EOM M..Mw Aof d-S,.. 7TZ1 rr",W.ov 66001pr vA.: swi. 100 f tl.n Nr 272" A.h.44. HC M1D. NunMr4na. NC 260r6 153e 47]-002, 1621p54-717a (IO111769 W7 ANALYTICAL RESULTS Prat- Sl7RRY CLOSED LF p.0 prel.c{ No.: 921 t } IS I SamPlo: MN-12D Lab ID: 62111461007 Coloded. CVIW1206:15 RacNytd: 02IM1214-24 MmOa-fats Report poramolert Rotube 9MOt Umil MDL DF Prepmred malyoel CASNe. Quo, 1260 MaV Low Loyal Landflll Anotyflcal Method: EPA 62410 bar.a•5,3.O1dJ...W.p.ne ND uA $ 0 0." 1 021t WI221:10 10061-02-6 Edlyhelv.ne NO upL 10 0.10 t 0211]11221-10 10041.4 2aioaonont NO UWL 50.0 OAS 1 0211311221A0 691.79.E ladamolh.ne NO upL 10-0 0.32 1 02 I V12 21'.10 74.16.4 M.d,yl.ne 0311pflde NO uqA, 1,0 0-47 1 02/13012 21-10 75.04.2 {-Mo1,y1.2-pammnon.(WIK) ND u�A. 100 0.33 1 O lU,211:10 106.16.1 9tyrult ND uO+L 1.0 0.26 I 02)13r1221-115 1042.5 1,2-7e oe duoroeF ona ND UQ& S.Q O.S] I 0211 L127r:1Q 830-ZM 1,r2,2-TvtrApdoroe6l one NO uok 3.0 0,40 1 {ZIW1221.1a 79.34-6 Tehrchkroelh.ne NO uWL I.D C46 1 0271311221.10 127.114 Tolvar.. NO upL 1-0 ON 1 02n311221:10 106.19.3 1-Trkhkamethano NO upL I'D 0.41 I 021t311221 10 71.55.6 i,1,2-TrIG1kr4Nhana NO UWL 1.0 0.29 1 02AW$221;10 79.00.5 Trkbkrmmano ND 904 1.0 0.47 1 QVIN1221:10 YM14 TNchuro#uuomNh.no ND Riax 1.0 0.20 1 0211211221AO 79.60.4 12,3-Trld,lormapone NO UWL 1.0 0.41 1 OVIU122110 1&114 VMy1-"ham NO upL SOA 0.3E 1 12113112010 106-05-4 VW,0cNoclds NDu,1L 7A CAI l O211L1x21-10 75-01.4 7Ly1.n.(Tapl) NO upL 5.0 0.66 I OV 311221'10 1330-20.7 Sa pof a 4Aremeltlev.b.xu.n. IS1 941L 74130 1 MM1 221:10 460-00i Ombom4mua.m.lpon. f61 100 % 70-130 I 02MV 221:10 1666.93.7 t,2-DIc1,tw P4thane44 IS) 107 % 2D-130 r W71311221;10 17060-07-0 Toluono•d3(S) 93 % 70-130 t OVIV1221:10 2037-25-5 21208 Al"lonlly +4,oW01 Method: SM 23208 Alke9nIN. YE1al et CeCO3 11200 ugfL 5000 5000 1 DW7012 1210 WOW aOD. 6 day Anelol l mo md. SM 52109 900. 5 day 444D uq?L 2000 2000 1 02111117 17--30 WJ7102 17]0 390.0 IC Ardpm 21 Do" Ans"DI1 Matl.od: EPA 300 0 SOW. 7220 uWL 25000D woo 1 OZf1Z1121S-µ ""ice-N-0 4600 Chlorlda Anaryenl Melhoe: SM 43DD-d•E Chlorles ND upL 5000 two 1 OW20112 NA3 15167-0" 4310B TOC Anstoc4 Malnod SM 53168 Told Ofpmnlc Carbon 3710 u01L IOOO Iwo I 02123112 19'45 7440-44-0 P.q. 11 41 ]9 D.I.: 0y2512612 69 58 AM REPORT OF LABORATORY ANALYStS TN ,.pert M..-1 b. npt hd d,..Aeptn M, Aoe M N m w,.anl of Pm AnaMul SaM & Inr 54 P.qe t9 nr 39 P4e4 Anely6eel ■4ryte41. Inp, POW An41y1IGO "I.44, Ise. Poo knaly90el e.MMN. Inv. Yee. A nxydcAl e4 I -.Ise, 06- AWY11601 6NyleM, MA. P..e A.Mytleer eervlaN, Irw. ceAnalytical• iBE.q wpe. Rwd-J.eA 2I25Rw: KAR aw9 mrcy Av. Auh 1W aceAna�ytr�a�F X5 ENN Wed-Reed-5u1.A 322s RwwW Dr 76W u.7 Are SW.1W ... ysr. - Calm, NC Z .Ea A4hen.r nG _ GN lirlww6. HC 9W79 n.� Ed.n, NC 2778E ANy.e1., wG'MMA Himu,Nwae. NL 2e07a I}76,�7!•6021 40Je)254.1110 17mw6 9061 i336182010971 16761254•7111 IT0116754;W ANALYTICAL RESULTS ANALYTICAL RESULTS Arync1: SURRY CLOSED LF P[cl.ct SL RRY CL09 ED LF P.a. R.FC1 N6 921T+951 P.ee Prepcl Na. 9311 *51 sadvo.-- 61YM-+3 Lab'ID; n11116100a Cv/ad.d: 02@9112 13-31 Received021101+2 t4.24 Mm". %%tn sa np+.: MW-13 Lab ID: 92111161008 CcPeclsd. 0210P+12 13'35 J14GCIYed' 0NL 01% 14:24 Morn V63mv Rep-1 R.pprl P... -If" Reaulll LRMIs Llmil MOL DP Prepat" Analyzed CAM No Du.I P4r... Id4 9.4WI4 11nils UW MDL OF Arepa[ed Analysed GAS N.. 6W11 "101c7 6roundw star Ana"Ical M.Ihad: EPA Soto Prep4r40on Melhad: EPA 3010 8260 M5V Low LavoI LandRll An mlylN sr Melhad. EVAS260 Anbmvny NO u9f. 0.0 50 t n1E0+21145 02111f120112 7440.1E-0 Irene-1,3.Dwnl... W.V. a NO uyL 1.0 0.26 1 Ovi Y1221.35 10001-02.6 A14.nic NO uyL 10.0 50 ! 02n 6A2 t1!45 021+ N 1201,227440.36.2 Elhyb-2.ns NO L1WL 10 030 1 ON1 N1221:3510041.4 Maiwm 14.+J uyL 100 50 I 021011 },A 021tW120l22 7440�31.3 2-SIGNMN. Np u91L 50.0 0.46 1 02JI31122+: 35 591.784 Beryllum NO uyL 1.p 10 1 07JI611241;45 OS15En2 O1:22 744011.7 Iadorn.Vlmne NO LVL 10-0 0.32 1 ov Y1225:35 14.8e-4 DAdmlum NO u91L I p I p I 0Zfl6ft211;0 02J18f f201:22 7110-43A M.Ihyl ens Chloride NO WR 10 0.17 t OZIW1221:3S 75.OG-2 QMMWm NO uOA, ID.O 50 1 07J 10)121145 02J161120122 744047.1 4-Me11yl•2-panlarlvn.(MMX) ND UVL 100 0.93 + 02J1311221'15 108•10.1 Cd94p 16.4 uyL 10.0 5-0 1 "1G+2 +145 01111.1;1 0122 111048-1 styrene NO uyL 1.0 0 26 + 02J1311221:35 100-4;-5 Capps ND uyL 190 S.0 4 M d1211'45 021+L1201'22 7440.50.E +,1.1,2-Ta9.rfllPr9eplen. NO 491L 50 0.33 + 02J1311221: 38 630.20.E Lnd ND uyL ID 5.0 1 ON I8y+21T:45 0271Nsz 0122 1435142.1 f,1,2,2Tab.a+huveriene NO uyL 3.0 0-40 1 OPJ1 N I221:311 71.24.5 Nic ND uyL s0.0 1.0 1 ON+W+2 ++:45 ON1d120132744p02A 7.b.phlwaeVlen4 Np upfL I.0 O.i6 t 0711311225;351z7-+a.4 ENenylm No'is& tD.p too } Iov 160121TA5 07J1 N12 a1:22 77,1249.2 Toluene NO RyL I.0 026 t 02n3H221; 311 10641.3 31WU ND uyL $D-O 5A 4 00116012+5:45 ON161120122 7440.2b4 1,1,+-rdgJNAee0lme No uyL 1.a 0.46 1 121131f 221:35 11.55.5 Tn4IWm NO uyL 5.5 6A } OL t8112 it -As 0211 M120122 7u0-26.0 s,1,;.r11ch1erP.ttl.ne NO .@& I.0 p 29 + OZN N+22 1 7140.5 Vanmdum ND uyL 25.0 11.5 1 021I N5211x5 OV181120122 74,"2.2 Trlchlw0e01ene 2-0 uyL 1.0 0.47 1 02JI U1221 U 7a-01.6 Inc 201 uyL 11.0 too 1 02116J1211:45 021W1205.22 7410-a-0 Trkhfefcluorom.Ih- No uyll. 1.4 010 1 02J1311221-n 75,69•4 12,3-Trlcnler9prepen4 NO uyL 1.0 a4s 1 0221112 25 9&11� HGO MEY Low Laval Lan[p III AnWipucal M."d: EPA E2E0 Vinyl:75 nyl S"Imle NO uyL 50.0 0.35 1 p211V1221-35 106.05.4 Avatone NA ayL 100 2.7 1 Ovl1 "221 ss V-64-t Vlny+cnlande 12 uyL 1.0 0.62 1 O2H311221:35 75.95.4 Acryl"wil. NO uyL no 1.1 5 p2113J122,:35 107•12.1 x0one(Two!) P40 uyL 1.0 0.1E 1 ONIUIZ 21:35 +330.20.7 Bm2en. 0-67J uyL 1.0 02S 1 ON171122145 71.43d S.-Crafts &omq[11Iw9meM.ne No uyL 3.(I 077 1 p2fs31122i:35 74.17.7 9.Brorinlumobenxene l5) 9e % 70-+30 1 02n311221.36 450.00.4 BmwallahloremY6lmn. ND uA IQ Ole 1 Oz113H221A5 75.214 Dare -a fluafam41hm: 16) 101 % 70-130 1 02n 3n2 21:35 1a11-53.7 Btelno+wm ND uyL 3.0 0.2E S 0Zf1311221-75 7'r2F2 1 ]-0knlwoelherH-d1 ISI +OS % 70.+30 1 02113f12 21:35 1.7060-07.0 ofom inael.ne NO uyL 10.0 0.21 5 p2J13J1221;15 74.6Ya Tolu4ne•tlB ICI 9a % 70.130 1 07J13f12 71.11 2fl37-21-8 2-a.P-e iM EX) HD uyL 100 0.9E T 62JI711225]S 71-93.3 23208 Madflntly An.1Mlcal Mothov: SM 23208 DO=dav1ld. NO uyL 100 12 5 021131122i �35 76.1A•0 e Arbon 1eVAclaarlde NO uyL 1 0 025 1 02n 31122t.55 Sax3-5 AA.IINw, Tool ee CaCO3 17401 uyL 5.1 6000 1 0y17J4.2 $2:00 Chlmob.nzene SA vg1L 1.0 0 u 1 p221N1225:35 101.9a7 b710B BOO.6 day Afloo..l Method: SM S0i08 ChIPr0eA16ne 0.96J u91L top 0.14 t 021131127f.35 75-0d0 CHlvr04Prm ND uyL so 0.11 1 ON13112 21:35 67-H-3 MOO, 5 day NO IIyL 2090 2900 1 02111f 12 11 AO Ob 0112 15:47 84,8E CMor.n.e.ia-e ND uyL 10 0 tt t Ozfl Y1221:3S 74.67•1 + 2.1}Nplome.7-r htproprape n. ND "OIL SSA 2.5 5 02J13112 2135 16.12•e ]OOA IC Anion. 26 0sy1 AnA1y1N1tl M.Ih.d: EPA ]00A �uranwdtivrem.fh.ne NO uyL 3.0 011 t 02J11J1221: 35 12.4.41-1 swept. NO uyL 250000 5000 1 0&72112 t5.57 14608-79.0 12 DiLromc-Man. IF DBI NO uyL 1.0 011 T 02J1all 221: 73 106.93-4 D-brcmam.lnamt NO ayL 100 1.21 1 02J13J1221:35 79.95.3 4500 CF11ond. Analylkal Ma 'had: SM 4500•CFE +2-DlcnlwPbenaene 0.731 uyL 50 O.SO 1 07J1311221:55 9$.50.1 chwdde 34400 uyL $000 8000 I 02Rpf 12 D9194 1E6E7.00-6 T.4-9lcnlvrobanaena 6J uyL t.0 0.13 + 9z11311221:35 fO6J8-1 bane-+,4'OWvNWe•2•bulenl NO Wt.100 1.0 1 0211311221:35 1W-57.6 8316B roc MAyllcel Me lh.d: Ski 531 oB I t-D1cMor0elhene 10 uyL 5.0 032 T 02J1311221:35 7&34.] TPIci Orp en:�CarBvn 10700 uyL 7000 TN* I 02123I2 20-07 7440j4.0 t 2 "":.":than: NO uyL 10 0.12 t GZf131122135 107-M2 tj-OtmwPe6len No hyL 59 056 1 02f V 221-35 75.35-4 'Ie. I,2•p4chlPmeln.n. 34.4 uyL 59 0.19 1 021 Wl221:y5 15E-SF2 tram- 1.2.Oknler.allam. NO uyL S.0 04a 1 112J1 M122133 156. 0,5 12-plGMweprOpane OA1J uyL 1.0 0.47 1 ON13J1z RI r33 7e•67•S f 3-iklaa 6PrRPmn4 No uRrL 10 0.2E 1 07J1711221:35 142.2E-a GIf 1,1•DIFhIGre51r9pen. NO uyL to 0.13 t 021131122US 10061.01.5 Omit: 02r292012 0916AM REPORT OF LABORATORY ANALYSIS Pago ZO aI30 D.Ir:92J28J2012 04 56AM REPORT OF LABORATORY ANALYSIS Pa9.210139P 1n♦,.Pen r'ml wi w .meews u:.PI n M r. .�. ,. n.. n.reellM a+ltin �n..nl of Para M.Irmyl 5emo.m rv� rnn ��[ P•. .mvn=en.enr �r [ r_. � _a _er•v. M Rn.lytleal 11 vlest, Inc P." arwlyd-1 l.rNen, 1, a Paw AnalyuW l.rYlwa, Ins. �CE1'S1 f� 1C0.�• 70! EaY N.wa. nwe - Sul. A i236 Rntrvda Cr YILO �r Rr. a�Nl tdd Ed.e. NC 777aa A"M - NC 21MA N.nl.fwla.. NC 2107E p]ela73ay71 lada175t-717a 11 W la7b-om ANALYTICAL RESULTS P,.Jecc BURRY CLASEO lF Pon Poled No.. 82111951 aarrrpl.l 49W11 Lah10: 92t11111069 CnHeWe 0211W12D1;00 Recolyed: 02f1N121424 Maabl; VNW1er A ep¢rt Potom.w. R".ft unity umn MOL OF Preplrad Ans"d CAS Nc. Dual 4010 iCP aroundwanr Analylka! Malhad: EPA 0010 Pr epae.6an Method: EPA 3010 Andmmy NO4A 6.0 5.0 1 DVIW121145 OZ111N20117 7440-34.0 Are.nle NO VA 1D.0 5.0 1 02/16/12 W45 02M VI201-27 7449-31-2 Baum14.21 uyL 100 S.0 1 02f16r12 11 AS ow'! 811201_37 7440.30.3 B"oum NC u9A. 1,0 1A 1 027fa712"" owl1M20" 741041.7 C4deKem NO ,WL 5.0 1A 1 02r1 11A5 1721111120, 27 .0-43-0 G12 Chmmlum NO ua& 10A SA 1 =I Ella WAS 02M1112 0127 144047-3 Cohan NO UG4 10-0 SA 1 0711611211:45 02HW1201:27 744048.4 Capps NOuyL 10.0 50 1 0211111211-43 DW&1201:27 7440-50-8 Lead NO UWL 10.0 5.0 1 DZIW1211:45 021181120127 7439.12.1 141010l NO "A 50.0 5.0 1 QW1N1211:41 D21 W" 11127 7L40-02-0 S.4eium NO uyL 10.0 100 1 OTW211:45 0271 1111201:27 7712,15.2 S11- NO V14- 10.0 6.0 1 WAn211:4l Owl 0120117 7448-n4 ThalNum NO uO& 6.6 6.4 1 02119112 It:45 Owl 111120127 7"C4214) V-.11um NC u91L 2S.0 5.0 1 12114912 11:4S 071111M20127 74400.2 zh. NO a otL 10.0 10.0 1 O711NV1I MIPS Owl9112 011.7 74404" 1294 AIeV Low L.r.l Landflll AfNlylkal M.mCdEPA 02M A..r¢ne NO u01l 100 22 1 07H V 12 22'.01 157.14.1 AayWnX1H. NO uWL 200 1.9 1 0211112 22-01 W-13.1 Banns. NO uyL 1 0 0.25 1 WAW12 MI 7143.2 BroaloalYta<6m411ana NO uyL S D 0.17 1 owl W12 22,01 74-17.5 &amodahaolemaVw- NO 4gPL 10 D.ia 1 OWN $222'01 76.27.4 Brom calm NO uyL 3.0 0.20 1 Qraf12 22;01 75-VI-2 6ramomellane NO u9d. IC.O 0.20 1 ON13112220T 74.93.9 2-BIA.n¢na 1ME3a1 NO u914 100 099 1 Owl W,222A1 7a13-3 C4r6m dWlda NO u01L Ix 12 1 Owl 311222:01 75.15-0 Carom two m1an" NO u91L 10 0.25 1 02" W1222-01 W27-5 Chl.fe6.ntan. NO uyL 3.0 0.23 1 WI112221.01 106.1E-7 Chkf Pallana NO uyL 10.0 0-54 1 02M11222.01 7500.3 U Wr0leym NO uyL so 0.14 1 0201112 2"l 1725. 3 Chl.wmah.n. NO uWL 10 0-11 1 0711311222-01 7447-3 1,2-D&M-3-hlor.proq.n. N0 uyL 13.D 25 1 WIW1222:01 W12-0 01-Mar.mmhm. NOugA. 3.0 021 1 OS1311222.01 124-4" I ,2-0alamwatan4 lEOB) NO 1ryL 1.0 0.27 1 0211Y1222:01 IN-934 dWfelrmm.lvna NO u044 1DD 621 1 021U11222:01 74-111r3 12.Ok1Yorphriz.n4 NO UOX 5.0 0.30 1 ml311222:0t 05.50-1 tA.01aNwobwIshm NO dyL 1 6 0.33 1 O2H 3112 211 t 106i47 barl4-1,4-pWa¢ra-Zbu1en. NO PyL 160 1.0 1 owl U1222:o1 11467-0 1,1.Old4proanrn4 NO uyL S.0 0.32 1 IIVIY1222111 IS-34-1 1y01ammoolhan4 40 u911 1.0 0 12 1 02111122211 107-06-2 1,1.0kNlaloaD14n4 NO uWL 6.0 0-56 1 Oy1341222b1 7S7ar4 da-1,2-ploMuoalh4na NO u9R. 50 0-10 1 02HS121?_01 1S&H-2 Irani-1,2-0iolaoroeDlane NO uWL 5.0 0 49 1 011112 22)01 15154*4 1,2�0INtoruprop.ne NO aryl 1.9 027 r 0211112 22.91 7a-a7.5 1,3406hloropropan4 NO uyL 1.0 0.2a 1 WA 3 %2 22,01 142.21-1 q1-1,3-0IcMoropeapen. NO uyL 1.0 0.13 1 Owl U1222:01 10011-01.5 Pa C. An.l yecal as,l sal, Ise. Pees Analyde al Aafrlcae, ins. w An nyu-, atrvlsa., w. acieleRr�aJyticai' T 5 EtN Nr.0 w R.4 - Bw4 A 72M 91..• Cr Pa 0bD0 5 cq h• Su1. f 00 1 ��anv E..n W -.744 Rena.a. NC �EBW-unYfwt. 4c 2667E 03d 15:3 r471 {a7e17m 211E i7a R7sa3n ANALYTICAL RESULTS Pf olecl SURRY CLOSED LF PICA Projacl NO. 92 111 951 Sample- A19y-16 Lad IO: 2.1111111510011 Cullecle6: 021*12 01A0 ROCANOO: OMW121414 Marm: WAll41 Report PRO"14% ReM1a LA1na LI1A, VIOL OF Prepaml Anatlaed CAS Na. Cara, 1210 M9V Low Leyrl LandRll Anaydcal Method: EPA8200 Irin.-1,3-dlahl... prapene NO uyL 1.0 0,24 1 O7H Sn222-01 10041-02-9 E9Ny6en2.ne NO uWL 14 0-50 r =IU1222:01 $00,41.4 2-Naxonone NC u94 500 0.48 1 MIW122211 591.7" Iodamalhime NO VW% 10-0 0.32 1 07M311222-01 74.1112 Memyt.ne Chtonde NO u91L 1-0 0-07 1 02/13112 22.01 75-oi 2 4-M461yt-2-p.0lanon4 [0,4181q NO u91L 100 0.33 1 0211112 22:01 101.10.1 SiyrMa NO V91L 1.0 0.25 1 D21131122; 01 100.42.5 1,1,1,2-Talnthloro.ln6ne NOuyL S.0 0.33 1 OW1311222'01 630.20.E f,1,2, 2.7auacheaoer,.ne NO uyL 1.0 D,40 f 021131122ZA1 79-34A Teb-hi.r..dr- NO uWL 1.0 0.41 1 02117M222:01 127.16.4 Toluene NO uyL 1.e 0.2E 1 02M ul2 INK 10112E-3 1.1,1•Trkthlua►hana 140 VyL 1.0 0-49 1 owl Ill 22201 71.55.E 1,1,2•Tdchloxoadtlne NO u91L to 0.29 1 owl 11222.411 76-00-5 Td.1riao.1ho- NO ugk 1.0 0.47 1 02M 31122201 7F01-S TdchlmdAuoro.a.tn.na ND uo1L 11 020 1 02y111222.01 7S42,.4 l,2.17dchiwWapane NO Wk 1.D 0.41 1 =1511222:01 96.114 LFlyl Imam NO uyL WD 0.35 1 021111222,01 101-0Sd V" chloflde NO u91L 1-0 OAR I 02113117 22:0% 75,0$ 4 Xy14 no{ToraO NO uyL 5.0 0-69 1 02M U1222'.01 1330.20.7 Sfllrolafn 443r¢m.0.130b.112... lS) 95 % 70.130 1 02113112 22131 460,M4 DIbr0m 11uof¢mem4n. IS} 107 % 70-M 1 02M 311222A1 186021.7 12-0wnloyaa0una d4(8) 105% 704" I Owl 11222-01 17060-074 Towwo-1161S1 93 % 70-130 1 0211371222A1 2077-245 23I0S AkalkNq mdvueal MaX1¢d: SM 232DO A1Nalnhr, Tolel.a Ca003 low VWL 5000 5000 I 02MM2121W S2100 BOO, 6 dAy Malyllcal M41hod: SM 52$08 BOO, 5 day 1934 uGeL 2000 2000 1 D2111r12 17.30 O21612 17:20 30DA IC An1.n. 21 Day. MAlybcmV M.Nod: EPA 300.0 SWilm NO u91L 2500m0 5000 1 02=12 1511 14106.79.8 4900 Cill9rl0a An4fy11C41 Madmd- SM 4590-p•E Chlafkas NO uyL 5000 5000 1 02l20l12 p9:a5 1166740 E 13108 TOC Ansly" Ma11od: SM 5310B Taal 4roar4c Carbon 8360 uyL 1000 1DOD T 9=112 20]11 74404CC 134 Data: D2128,201209. 66 AM REP ORT OF LABORATORY A NA LYSI S Pa0a 22 at Osta: 02181`201209:55 AM REPORT OF LABORATORY ANALYSIS Pao•7baf3d 1'N. r.pen Msl fbr 0. tiofcde d. m-01. n Ul- rN. e.L Ne4 wl b. npmd,e.tl. -aA n 61 mil-A"y W,,-.m.0 P.w Mary-., S.n.e.t Mc ,H0-m.-..evn..nlor P.-Rtiryec.l e•m.r.-xc r. A.rryeeal 7.rvrn1 Ne. P.n AiWyuearlerWe.r, rn[. P..a AnMyrk.lHrvie.l, In[. �CeAna�yCiCr7l• 77E.NM..IPyRv.d-r+[NR z77sn .,m.a. 9WKpe : 5.t.1p7 Et.n. Nc 2r7m6 Vh W. NG 2111 4 iN+nrrw ii N: 26071 13381 -*21 Ia26i274.v1f6 iyu[167519= QUALITY CONTROL DATA pmpit l SURRY CLOSED LF Pace Pinked No 92511055 QC9.1c11: MPRP19913 Anmllal.Malhna. EPA 6010 QC 51.leh Meftd. EPA 3050 Anaiy.0 D1.01pl10n: 6010 MET NC Glnwu1wK14r Au odA10 LmG SmFrk*% 1W 11951001.9215195tM2,921119St003, 92111951004.92511951605, p2111951000. 92111951007, 92111"loon , 92151 p 51009 METHOO OLAW 7Z2691 A11140daled Lab Sampin: Pcraml.M+ Mavl.: Miff 0211111101. 921t}935002, 92111951003, 921H95f 004, 92111951005, 921119S1996, 62111951007, 92t11951006. 92it195t099 T110nk Rm"Jing unna Result Unin AnalyLed "lifiv4 Anumorry uyL NO 50 412f101200'32 Amenic uyL ND 70.0 9211&1200:32 amount 9914. NO In 0211 &12 00:32 6ervcwl 1,9L ND 1.0 02r1&1200.32 C.dnuuon uOIL ND 10 OVIN1200:32 CI1r0mlum uprL ND 10 9 0211 &12 OQ 32 COW uyL NO 100 0711601200:32 Cmpat upL N0 10 0 02)1 W12 W 32 Lsm9 Yp+L NO 10.0 0711&1700.32 Nlcael W41L ND 50.0 02/16112 m 32 S.kanmm uptL NO 10-9 0201 IN Da 32 S4nr npoL ND 10.0 0711 &12 G0.72 Tnn6um ugrL NO Ss 02119r12 W.12 Yanamum OWL NO 25.0 0711&I10012. 7Jnc AWL NO 10.0 0211 &12 09 32 LABORATORY CONTROL SAMPLE- P.rameteF ?USOZ Un9111 sp. COML LICE Ruuil LCS $ Roe V. Roc Limit Oualrnmm An9mwy uyL S00 649 96 W-120 An id. ..WL 500 4" tip 00.129 .rm L1m uyL SGG 449 96 A0.120 17eyuum iyL 500 71a 103 60.120 LAdm4un ugY So* 506 102 60-170 Cn2emum uyL KID S97 too 60-120 Conk 11p4 590 499 100 90•t20 CGppet yprL am 4" 37 60420 Lead uyL 500 500 100 90-120 Nickel 1IptL 590 504 101 60.120 Selankrm uWL 500 407 97 60.120 sur.F IryL 250 261 100 50321) 71r6mk. op+L 590 413 95 60420 Van.04mr IiyL 500 4IG 99 60-120 bn1 uyL S00 504 101 00.720 /n�aa .1 ..,,J n +q P.m Auloul 6.[r144a, Inc P4u An.rY9ni a.ryr..m, i" i.e. A-lyd"I 6wHws, Me. ' ceAIQ10icai 20 f[r weave Re[e-fidA m61"..aaDr oeoo.we.r+w aW.+ov 1 - Even. NC 27200 A.h..1am. NC i000. w.ynrrm.. Hu 20VA OW)627.01121 (m2a1754-?'?4 I tw 4675 9n02 QUALITY CONTROL DATA Prujecr: Pace PrOJad No-: SORRY CLOSED LF 9211 t951 MATRIX SPICE 6 MATRIX SPIKE DUPLICATE. 122s93 722594 MS u50 R2111951KI Spike Spike us MBd1 MS MSD %AK mu P.rameler unll. R.m11 Cone. C.M. Rnult R.eull %Rac 'A Ri,e U1wM RPO RPD dun Antimony uyL ND 500 S90 495 492 99 Vol 7S,125 1 25 Ananio uyl NO 500 500 S06 102 101 100 75.125 1 2S EI-mim uyL 1l6 S00 500 690 194 97 oil 75-125 1 29 B"um upY NO S00 S09 515 512 103 102 75-123 1 23 C.dm:um ,+pr1 NO 500 S00 606 502 102 500 75.125 1 25 Cnromum ugtL 7,2J 500 S90 517 609 102 100 75-125 2 25 CoEmit uyL alu S00 S00 610 600 100 p9 M-125 1 29 Copper uyL 6.51 500 500 503 497 99 96 7S425 1 25. Lead 101L NO SGG SW 501 494 99 lie M126 1 27 Nickn ug+L 5.3J 500 509 S07 S00 190 99 73.126 1 25 Solomm uyL N9 500 so 505 495 101 AS 75.125 2 25 She, ugrL ND 250 250 253 250 1P1 1p9 75.12s 1 25 TTa&um uyL 7.7 500 500 472 476 93 64 75.125 1 25 Yanamum uyL 112j $00 SO S06 502 100 99 76.125 1 25 21.0 uyL 31.7 500 1400 sm us 509 L6 7S•l75 2 25 Ditto: 021207201 a OS16 AM REPORT OF LABORATORY ANALYSIS P.ge 24 or39 De It. 0u29f2012 00.56 AM REPO RT OF LA 90 RATORY ANALYSI S P.pe 2S e130 T+n i.Wrl.mr mlar. PourW..4e.pinrW Try reepn MM-tN i.pro -d...[.M n kA +14.w.1 w4 wgn.o.+.m O+P.0 In4ly.r.11 9nM. �� Mewd w. •Wmi, ewn..M.r P.n morkc l S.- Inc Pau Analytltsl fi Wtal, In c- Pow Awlyrkrr e4FAAMZ• rot. Pau Analy6ea, dervlar, Inc. g/.p ��'1�f r� Pace A nmlydeer llrrrus, Inc,. Pr er A nil vuem 9 rrvlt.s, Inc. Plea A nalyou l9rrWrer, rnt L�LL AMIy[iCal r X15 Earr te.rmP,. APetl - S,Ar h ZM Rlwnraa 0• SWO. 1 Wr S, ,PO p5a4 />r lUr 1�+R� '�175 Elfl MeeOPw RwO. 9,n. h 7i73 RivtriAt Dr 95{7D Y Y Ass svw lop �__.�� Edrn, RC M24a A1exr,F NC 16XH M.nr r.w. HC 74o7e wwear.rfr a+n Ed.n NC 777ee Aygriw MC jeep. nwrrAAr N11*11e {3]6y�-0QI, y07SiZ5t-IrT6 f7w y57 SW02 + i5 W234071 I 4 aze1 2x-1116 y7w>a75-000. QUALITY CONTROL DATA PYP1acl- SORRY CLOSED LP Psca pf*L1 No.: 021,1061 OC Belch: MSV716174 Aneyelm Mmlhad: EPA 9260 OC Balpn Mrttwd: EPA 12M An."hl 17mmtt1ptlan- 6260 MSV Lew Lwal LendAl Aeaodelyd Lob Sampler, 0111061001. ONIIOS1D02, 901H051 D01. 11211101004. 021 T19S1005. 02111051006. 02TI 1 OS 1007. 92111951 ON, 02111951009 METNODBLAWC 721246 Motflk: vwler Aeavdeled Loh 8empyea: 92115 W 5401, 9Z H 5951 DOZ, 92111851003, /21 f t 051004, 92111951905, 92 }! 1931006, 921119S1067, 0211 vim Im. 9I111951 ON Parlmeler U.N. 61ank Result Repenaeq LIMA Analysed Ouelmere f,1,3,2•TetraWPrcetl,anr 11Wt ND 5L DWY1211,54 7ncHvrvetlrmr -WL. HO 1-0 Owl Utz 1154 1,1�,2.7.6aciawart,.na uyL NO 3.0 ON13n213:66 1,1,2-Trialora41hana vg1L NO 14 Owl Yi2 13-59 1,1.Oklduwtlane vyL ND 5,6 02113f121 S;66 +,1.O1 hlvroevrna i4rL ND 5.0 OVIU1213,56 +,2,}7rlthkmprvpane uy L ND 1.0 OZr1311213:56 1,24Ohrvmo-lctWwaVmpane ugYL NO 13.0 W71Y121315 +,2-DlG0maethen. fEDR1 uyL ND 1,5 6' WIZ 13.46 1,2-DWNao6anaena ayL NO S.D aim 2133/ 1,2-Dkhrero lhwe UyL NO I.MV12 f318 1,2-01d+levopropene uyL ND I'0 Owl Y1211.51 I,3•DaAbr vplopana uyL NO 1-0 D2113A2 f3A6 5-4.phwwmnenlena uyL NO 1.0 02N371213M 2•Bulenona IfAEK] vVL NO 100 OWY12 11M &Haaanona uyL ND SO-0 owl W1213,65 "edryl-2ymnl—(AIr6Ky uyL ND 100 02rWI1336 aar". uyL NO 100 02r1Y1Z 13-31 Acrow*fle uyL NO 200 OWIW1213:69 Barrarrra uyL N❑ 14 0211311213:56 &omohlarvmamene uyL NO 1.0 021f Y1213'56 @gnvdlchlvrvmemane uyL N➢ 1-1)O7l1311Z 13AO &omoform uyL NO 1.0 0&1Y1213.16 6r0mam lhfi r uyL NO 10.0 0Y1YI2733S cubo dAtA uyL NO SOS 42113f12131 Cathm 14trWIPAIda uyL NO " D2n 3L121369CMwwnwe uyL ND 3d 021Y213 Chlprwtunr uyL NO . 10003!I13.51 CNmvrm uyL NO 6O22 CI,10—khans uyL NO 1.0 01113112131,51 we Np1L NO 4.0 O2l131121331 .3.Ochhwcelnana d1-1,3-Olthlwppreprne uyL NO 1-0 021+if, 21329 OAtomocnWron+elnena uyL NO 3 0 D2+WIZ 13:5/ Old'.mvmad,ane UVL ND t0.0 =131,2115: EmytWnxmr uyL NO 1.0 owl Y1213:5 Ieltlor 01A. uyL NO $0,0 DZ71 U121336 Methylen a Clrlontle uyL NO 1-0 OVIV121336 Wl a uyL NO IA 02MY1213:56 TO-10 rv.mane uyL NO 1.0 42113112133E Takr.ne uyL NO 10 0211 Y1213-56 crane-1,2-Dlchlwva thane uyL NO 5.0 0211311213:59 Dela: 01129120209.56AM RE PORT OF LA BO RATO RY A NA LY&S 1Ne rep.n ahal rw1 ti ie wodww r.0 r r.,rww yre h.ryyn wnsrnt pl Pa.. Mairi,ui 4rv,ua iri Papa 26 v139 CUALITY CONTROL DATA prtyect: SORRY CLOSEO LF PmwN*c[No-- 92111MI METHOD BLANK: 121246 Metsm Nkler Aee9det►d LeO Sirnplee: 921110S10D1, 921119510D2, 92511951003, 0211195100i, 921i1951005, /Ii110S1006, 02ft1951O07, 9251195100E, 921l195l069 81-k Rapartal0 Parameter tmos Reau6 Lhni Analysed Olntmen Danm-1,3-D d,rvrepropena uyL NO 1A WII 3112 f3;m trene•1,4-Dkmua•2•tutana uyL NO 100 MIU1211:56 TdarrloraeOhena uyL ND 10 92r1 Y121336 711hbm4uaevmelhene uyL NO S (IO21t3152 +366 vinyl ecetale uyL ND 50-0 O2113112 13:51 VVM d,larlde uyL NO 10 OVIU1213:56 Vane R tmq uyL NO 5.4 OZ71Y1213:56 12-Deh*-th.n.-d4 [5) % to 74-ISD 02113112133 i•&nmdluordheDlene (S) % O9 Ty130 OZ7111121I'S6 DevomoAuprornadlena 0)% 107 70430 02HY1213:56 Tclua nad6{6j % 91 70-130 OZ01V 1213,59 LABORATORY CONTROL SAMPLE: Palemalor 724247 llnme Spike tone. LCS RnWt LCS %Rec %Rec Lltwu O"Mefa 1,1,1,2-YatraNaprveditine uyL SD 505 }111 7MI'36 1,1,}-Trknlnroalhana vyL SD Ill-1 112 70�130 1,I,2,2•TetacMcroehhens uyL SD 46 317 10-131 I I'2-Trknloroet,an. uyL 5o 47-4 05 70•s713 +,1-pkhlmroetn.nr lryL S0 41-0 66 70.116 -Dlwu 1,1araoe.q,ene uyL 50 13-4 70.132 1,2>TRcp uyL O 14.3 - 69 79.30 12.O*iromm6e3 yL 7&13d 1,R-Dltrthan a (EDB) WL SO 49.1 90 X.10 1,2-tAdoe be—na pyL 56 41.11 93 70.110 1,2-Dlchrulcethanm rlIVL SO .1 111 MI30 1,2•Dchiproprdpan4 uyL SO i6,6 07 70.150 !,3-0IL•hlar oprupene uWL 50 S3./ ids 70. 30 1 ,4X7Ydeno6wuane uyL 50 46.E 93 70.130 2-Bulanan. (MFK) uyL 100 45.51 16 70.145 241eeanons uyL 100 1" 102 10.144 4-Merhyl-2penunana LAMB%} vyL 100 0/7J 89 M1 0 Acetans uyL 100 19-01 60 50.17S A=Y1M1Traa uyL 254 238 95 76.143p Beniena uyL SO 46.2 92 7D43D Ommvchi... —then. uyL 50 50.6 10 7D4 30 9remvdichlvlvmedlene uyL SO St.i i9a 70.130 &omarurm uyL 50 55-7 111 MI" O.umvmeurene yg& SO 49.6 99 54.110 Carte On hmursde uyL 50 47-0,7 94 7D-131 Carton le0atnlOrldr vDrL SD 5o.6 I11 70-117 CnloroGen7ene uyL 56 16.6 9] 70.s]4 CNaldelpene uyL 50 43.2 46 SO-,14 Cllvrolprm uyL 50 $.S 100 70.130 De ta: 02f2W701209: 54 AM REPORT OF LABORATORY ANALYSTS TNI r.ywr V,.l rq, W ragvdwd- alc.p h HY. wiwu, by riPrn oen..nr cl P.ta Arr l7Lul earre.a ,nt Pa/e 27 of 39 P4n Analy9r4r eery NeN Inn Pi [s AI W ylesel 4ervlass, Ina. P.p Analyllral eaMne, IM- p p�� q} GCAnaIyflGaia 205 E.y AN.en. Re4d -aNu A 3225 R,"-d. a ➢e99 o rr wa 6w1. +00 + y�.yr4hhsYr. 9d He 272e4 Ashswl4. NC; 79404 eanMmH.. NG 2W7a 17Se1473.1e1+ (S2W54Jtte I7w fA;'.Y90P7 QUALITY CONTROL DATA Prolae t: BURRY CLOSED LP Ae- pt61e91 No : 9211t95t LAWRATORY CONTROL SAMPLE 721247 SPA. LCS LCS % Rea Pee Artletor LION C.- Re;We %R" LPMs tlk4kPam Gnlwam.thene �yL 7p 424 65 64.17E pFl )ANchlpfOelhMe uA SA 43.0 p6 76T31 C1e-r,3-0 ItItlaprePefy UWL 50 52.2 104 70-00 plprafnacwprvnie9+en4 V§fL 50 52 0 105 70•530 Dlhty —th.ne YWL 50 50 T 100 10.131 ElhyltM[ene "m to 40 9 94 70-130 [odolnelh4n. Usk 100 101 191 49.160 Melhylan. Chlpnde UA 50 51.5 10 03-In Shreve uafL 59 41.5 99 70.130 T.V—hi".thene VWL 50 So.0 100 70.17E Toluene VDIL 50 460 92 70.13E 10hn4. 1,2•Dlrfilar.e4eane 0yL 50 439 06 70•130 17aro•I,]- DIthl9royrppen! 4L 5o 52-9 104 74132 it IA-D CI+N110-2-Iwtdhe 9yL 50 53.61 107 79.141 Trtcrylpra49eane VVL 50 462 96 70-130 inchi m a 6!vrna— 09eL 50 54.9 110 S2.133 1Anye 4ca+Al4 uyL 1 OE 65 9 66 66.157 Nnyl chloride VL 59 43.1 !M 60.130 XTlrhe lToptl} uyL :5G 145 97 M130 1,2•D1cl+leraemana-d41S) K toll 70.13D 4-ar maWarohonarne{Sl % $02 10.130 CNxaUr.Rut[omemrna lsl % }pt 70.130 Toluene-aa 18} 9y too M130 MATRIX SPIKE A MATRIX SPIKE DUPLICATE- 7212441 7ZT249 Ms MSD 9211195t0o1 Splke Speke MS MSD MS M8D %Rec Mel P6Mmeter Units Room Cont. Cond- loml-1 Rawrt %Rec %Rec UroOe RPO RPD 9ue1 1.+• DlgNur oath one oWL NO 50 5o 539 '.2.9 $Do I% 70-168 2 M� 941+tene uIWL ND 50 5 53.5 53.0 To7 +Do 70.148 1 30 Chlvrahenrene ug+L NO 5o SO So.O g00 12 }00 100 10.146 1 30 Tolwane uWl- NO 50 5D 494 404 99 99 70.155 0 30 7e1oh m.thwei uyL NO 50 50 522 51.0 104 102 oil- 161 2 70 1,2 DiCerorae014ne-d4{Sj % 104 104 70-IN 4•B+Wnp 94aahenlM4t31 % 97 99 70.130 Dlhrom Awolrom4111yn! {SI % 105 104 70.130 Toplene•do (sy 5G 9p 96 70.130 P.4. AMIyUW JI'Maek Int. P.t. AnelyN.16aMen, Ina P44o APM}eIW16.Mw., Ink CE�l1�%kCai. DS E4M Ms4aaa Real • 3�N A 2225 R nnUa a 9epo x.. ar H.. p— 1Cq � .wm.ke�.Prn Eden. NC 21`261 .W.mwnw »WN. NC 27604 M. NC Iwlm 13Xx3 4921 14I61274-7176 [7(r1o15.9p97 QUALITY CONTROL DATA Pnpect. SORRY CLOSED LF Pru pmocl No.. a2111951 QC Belch. VIETf+9753 AnaryNi Melhad; SM23208 OC B4Ich Mopoel SM 23296 Amlyow Deeaeplom 23200 Atha rally 0kal0dele1P Leh 52 npkr: 92111951001, W II1951902, 92111951 EDS,/2111951 PO4, 9211 T951 OOS, 92111951006, 92511951 W. 9211$ 651001. 921 %I WOOD METHOD BLANK' 723565 Makle. ftIv Aelredaled Lab 54 mpre.: 0211195 Too 1, 021TIWOOZ, §2111Ill 1003. 02111061 ON. 412 111 05100S. 92i 11951006, 92111051007, 22115 05100 . 02111951 we 61-k Repwurg Peremelm Untie Reeull Ll7ret AnOV1e4 Ouek6el4 AlkerOlTy, Total rt. CaC07 UWL ND 59E0 02)17112 12-00 LABORATORY CONTROL SAMPLE' 7235M SpRa LCS LIDS % Rec P.r.merer Un+Ie Cunt. 9.111,01 %Rec Lr+lals Ouae6ere AlhoWlly, Total eT CeCO3 UWL SDOoO 50900 ID2 90.110 SAMPLE DUPLICATE 723557 92112$16003 Dup Mek Pwameiar UM. Rerun Rawl! RPD RPD Due99en Akeenuy. Total a. C.CD3 woil, 3340 man, 3000000 11 20 SAMPLE DUPLICATE: 723566 92111951008 0wP Max Perame9er Llnae R.WR Reerpl APO RPD Okel"m Alkalimty. Total ee CaCO3 uO+L 57499 57400 0 20 Data: OZIWOIl do "AM REPORT OF LA13DRATORY ANALYSIS Page 210139 Dole: DV2&2012 09-56 AM REPORT OF LABORATORY ANALYSIS Page 20 at 39 TM rapert Nrx eai 4l +epvd�[4p ax[4p[ N lV iM npert Nrl m1t iM iapeWeaa- exx:apl ae M. oinvA wr.Mn—OM Of Prw Ma,feeal San—, I� Wvl IM aP tenaare PI Pace A+rFryy 6e-O4. Nk PacA Anal vocal 15 rvl.::, Inc, pe.: A.ytl::l l.rM.:r, Irv. Pon A Aly0cal "Pill" r, Ine, ceAnalytical 2d3 E.x r....a+w Reed • S„n.A 2225 R,-,-1A 01. load.,---y A-. Sum too NNC 2"04 Wm1:rw N:. NC 7e07% 133e>eY]-BLx7 taxe]25a•7176 [roaI675iIg7 QUALITY CONTROL DATA Pr.).n SURRY CLOSED LF p.ca Prvlocl No.: 92111951 OC R.Ich: WETI1"n An.yu: Method: SM 52106 OC Belch Method: SM 5250E Anelysla Dascrlpllm: 52f 0S 000, 5 day A.Annned Leh sampNr p2111951002, 92111951001, 9211195100A, 92717951005, 9211193t000, 92771951005 METHOD BLANK' 72095a Motile, Watar A..odr.d Lab Semple.: 92111951002, 9211195105]. 92111951D0{, 921t1951905, 927t1951005, 5211195,004 Blank Repadln0 Per.m.r.r Lmlla Raµll Limit A"y=ad OuaYean am. soory LWL NO 2000 02011V171547 LABORATORY CONTROL SAMPLE 720M Sprks LCS LCS % Rec Par.m.ler Una. Cone. Rd" %Rae Lkn11. Ouao on SOD, 5 CLAY 14L 794000 134WO fill ae-115 94.05 SAMPLEOUPLICATE- 72fOW 921110510015 Duo "no p.r.mel.r Was RA -It R.euk RPD RPD 0vae9ero SOO, Sday uyL ND MD 20 54,65 �acelvqfyflcaiA see: Ana"tA 9Nyle.r, Inc Peer A"slyEeal a.Mc At, Inc. Pen A.Nyd.:l l:Mu:, Inr. 206 Eru W.dw qme-Eu�laA 7xY_RmrAtl: lk lead lkr Aw Sur 100 Ewn. NC 7771e Aah.. . NC 7alyla Mu W-A.. NC 2107e I]]e1e75•e921 M?.k?sa-717e 1704197s-om QUALITY CONTROL DATA Proper SORRY CLOSED LF Pat. pr*,t No: 92111951 QC R.1ch: WET110d77 Anayets Method: SM 5210R QC 6.10 Me51od: SM 52105 Ana"Iii Doic 1pdon: 5210E SOD, S day Assadstad Ls6 So mpl.4' 92111961001. 2211101007. 92111051 ON METHOD BLANK-' 77100e Mobn WNaI Aaeddatod Lab Samples: 92111951001, 921119Sf007, 921170.51009 61ank Reporting Paramsnr UnAs ResuN LWWt ARdyt.d OwaAen RODS day uyl ND 2WO 02)1&121730 LABORATORY CONTROL SAMPt.E: 7210US Spike LCS LCS % Roc P"amCHr ynlo Com. Ru1A1 %PAC UFNN Oue996rl SOD, 5 d y uyL 1990" 150000 79 eM115 04 SAMPLE DUPLICATE: 721009 1211194NDI Qup Mel prsmetw UPks Result Reoull RPD RPO OusOm 600. S doy Ppy1 e 6 myL 7040 A9 20 BA D.T.: 07l70012 09'54 AM REPORT OF LABORATORY ANALYSIS Page so- er]9 Dole0212,11 don DO: 56 AM REPORT OF LABORATORY ANALYSIS P•9e 31 ar 39 Tom. . r .r no u m aced. A 0 n A 1. — .:tart.har nil EA �yeer.ew.:. cop e. nAl — Y. N. ea+t-- t tr p— A,ulybe S.— .1 P.0 wuiyuui S. mu. Inc a Pa.: Analydul Eovl:ea, Inv peen Analytical aarvfaaa, Inc. Pau Analytcal a:rrleey, Inr- I aceRnalyt+'ai 206 E.N M..u— Read - 9"4. A 22M PI —Ad. Or. WW KlneeyA.. I" 1m .. . p yam, Eesn NC T73da Aeh.Wls. HC 2l6P 1{,rnler.ne.. HGM7e r336id732 21 la2ep64a177 17041e1F9002 QUALITY CONTROL DATA P,upct SVRRY CLOSED LF Pace Prejeci Nv.: 92111951 CC batch. WETA111561 Aneysls Metrvn& EPA300.0 CC 9eich MmOod. EPA 300 0 Anslyds Desuipeow 300-0 IC Amlans Aaevcieted Lab Samples: 9211 f 95f 061, Di 11 I P611102, D2 t 1 S 957003, 0211 f 951004, 9217 f 951 OOS METHOD BLANK: 723524 Malrh; Water Aseodmleu Lab Se mp et- 112111451001, 9211S951O02, 92111951000. 92111951 DO4, 921119l4003 stank Repunlnp Parameter LJnk. Rmsuk uni AnaeyLed Q.Wan Sulfate uyL RD 25MO 02f20112 5515 LABORATORY Cl)NTROL SAMPLE. 723525 Stake LCS LCS % Rex Peremeler unNs Conc. Re.ult % Rec Lklllls QualiOsFs WfAl. , WL 20000 16500J 94 9Fi10 MATRI9 SPIKE SAMPLE: 721529 921116330% SO- MB MS l4 Rea Peramelar llnns ReeLAI Conc. ReaulL % Rec LImf1A Quakkera S4llsle 4L 12.5 MOIL 20000 33200J 104 90-110 MATRIX SPIKE SAMPLE- 72032E 9201 EU4001 Splk. MS MS %Rec Persmal.r Llnn. Robot Conc. Reautl % Rec Ll"No ausakers Surfele uyL III$ mprL 20000 1510000J 604 90-f19 M6 SAMPLEOUPLICATY 723527 92111607006 DNP MIN Parameter IJnfy Re.ull R..Wl Rai) RPO OnaNPpA SWlale uyL 12-6 m0'L 124DDJ 1 20 8A MPLE DUPLICATE: 773529 92111WO91 Oup Moo Peramstar Unit* Result Result RPD RPO QUINDM Shdiele AWL gill MOIL OD7000J 1 20 Date. QZ2WO 1209:56PM REPORT OF LABORATORY ANALYSIS pop 32 d109 IN. revel Yiu Wart E. r.p.,P—a. —pl n I. -0—i Hie"m n p k at Pap AmFp a rrnee Pao: A-tOW 6mlc:r, in c- Pace A-MYGNai Ifervlul, 'me- Pau Analymmi asrviars, Inc. ' y acekvlytical • l05 EsN Mard9w — • —1. n WS RbsrYd. Ix. ae00 %Weer Ar: Su1. 100 Fd NC 7729E Ashneh- NC 25004 H�nrr.a:- INC tame [�. 1523-eazi ra2ai7S4-717e 1704XIM90Q2 QUALITY CONTROL DATA Prafert: SVRRY CLOSED Lf PA9C PfpJePl Ho-: 92111851 OC 5etch: WETAft15e2 AmNad Malhvd: EPA300.0 CC 9aich Method; EPA 300.0 Analysls Osser"on: 300.0 rC Minn. PAadcatetl Lae 5tarrhp4e: 92t t t 951006, 92111 BS f907, P211 f 851006, 92 f 1 f DS 100fl METHOD BLANK: 7243" Meth; Hater AuedslsdLWSampNar 92ff1D5f006, 9211f95f007, 9214195100a. 92111951009 Blank Repurllnp Parameter crud Ream Umh Analyzed Otars.M Wrote upL NO 2W000 ON22J121436 LABORATORY CONTROL 45AM PLE' U4395 Eoke LCS LCS % Rea Parameter Uplis Conc. Result % Rev Llmtr Qualonors Sutf*W upfL 20DOO 100W 94 D0.110 MATRIX SPIKE SAMPLE: 724396 02111957906 Spike MS MS %Rec l ar.M.L.1 Unlis RuWI CC". Re.WI x Rev Lhdd Oualirefa Sv1la[e upfL 331001 moo 465M 77 90-t1O Ml MATRIX SPIKE SAMPLE: 724194 921t2413001 Spice MS MS %Rec Parameter Ur As Result Cam, Rewll qL Rec LI-t. Quefa.,a SWIMe uyfL 1$3 mprL 200(M r113000J 149 RD-110 M6 SAMPLE DUPLICATE: 724397 92 11195 1 we Cup M.r Parameter Llne>t III Re.ul! RP❑ RPD QualiAera 5011110 uprL 131GOJ 3320P1 0 20 SAMPLe VWLICATE; 724309 92t 124IWOI "UP Maur Parameter Llnha ReRPf Real'. Rpa RPD Ou.119er. shdl.le uyL 153 we& 159000J 4 20 CeI.. 02u2anu12 09.56AFrl REPORT OF LABORATORY ANALYSIS TNa np9n ae.a -.q W eepiytli.e.e, .—In n MI. wlnwi pi. ovary. --nr of P.. Mf}Tea, S*M .. I - Pep. 33 of 3O 1 Pen AmyUul aerw.ee, in[. P...Anetyd.al Wit—. Im F.o. AnNy6u1 9mHaef, NC 1O5E..t Llaedow Rud -SuNA 7323 Rh.rr:d.D, MO KbuyA-9W I0O • J 1[• r� EWn. NC 772as AheW, NC WODA NC 7901e (lmNr 15971 162B1254.7176 fm4)u54D97 QUALITY CONTROL DATA P.1mer SORRY CLOSED LF PSN Project No.: P2111"1 OC 89" WETA111580 An.". Method: SM 4500-cFE OC Basch Method: SM 4500•CI•E AnWslc O-gi0an: 4500 CnMdde Associated Lab 3emoks: 92111i51001, 92111;5f 11. 92111951005, 9211195s DD4. 92111951005, 92111951009, P2111951007, 92111957001, 22t1195f 000 METHOD DLAe9C 774235 Mawr: 7Aloter Associated Lob Sempksr WI11951001, 921H951D02. 92111951003.92i11951004. 92m951005, 92111951009. 92111951007, 9i111961006. 92111951009 91enk Rkpdrdnp Pmamet.r Unla ROOl41 Unk Ans"od Oua66ers Chloride DO& N❑ 5000 02i2011209:38 LABORATORY CONTROL SAMPLE: 724236 Spike LCS LCS %Rev Paramder Witt Con. Re-11 %Rec Llmits Ouollfiers chtwoa UYL 20000 20400 102 90•It0 MATRIX $PIKE SAMPLE m Pammor CNdnde 724217 Units uO'L 92MI151001 Reason NO Spike Corm. 20HO MS Result 2MO MS %Rec 102 %Roe Writer Oue9Anre 75•125 SAMPLE DUPLICATE. 7242A 12111951Dp2 Dup Me. Pmammar Units Rewlt Rauh RPO RPO Cudimers CNerlds upR NO NO 24) Dare: WMV2012 D9:55 AM REPO AT OF LA SORA70 RY A NALYS IS Pepe 14 a 39 Tiir r.Pcn.h.c not W mpPdu ad, ranµ In M. -hoi.itihs wnaen —t al Pea AmIVbcmI Semde In Zltical Pee. Andvtmd a4rvlwr, rne. peck AeMy9.4r Skrvi rN. Ina. Pap An.ryrlvel amlwl, Ina.I/^ :a0 EK Alndow RR.d - &i1. A 2725 F?—aie. b 9a69 KP y m: 9uea 100 �J Ed— NC 27Y6a Aih-* NC 7B9n1 rYwreMe. NC 2507a 113e)MI192r LMI1154•ii7e 170y5754M2 QUALITY CONTROL DATA Project: SURRY CLOSED LF P.Co Project ND.: 92111951 OC Botch: WETAr II W Ansyalk Method: SM 53108 OC 9euh McCmd: $M 5319n Ans"K Desulpddn! 5110E TOC A ... Idt.d L110 Samples: 2211105$001, 9211115 1002. 52111951005, 42111951004, 92111"1005, 921E195E 006 METHOD BLANK 723516 MaWk: Mier Asspdaled Leh Samptec: 9211f9Sf 00f, 92715951002. 92111951007. 925i1951004, 921159510p5, 9211195i006 Blink Rewkg Parameter Untio Rewk Limit Anelyled qualifier. TerAl Ctgank Carbon vWL ND 1000 0212W1216,44 LABORATORY CONTROL SAMPLE: T23SI9 Spi" LCS LCS %Fiat P6romet6r U111H Cdnu. ResWt %Roc IJlnts Oua4hms TOW Organic Carbotl uprL 25000 23600 95 90.110 MATRI%SPIKE SAMPLE 72352G 22111633001 Spike MS MS %Roc Par omator unme Rosum Conc. Recuil %Rec Limllo Oucllen Tow Otganie Cam on uprL 4.1 mph. 25000 26000 97 76-125 MATRIX SPIKE SAMPLE 723522 112111605011 spike MS M9 % Rep Pvemetu 11naa R.w1I Co". Recruit % Rec U!"Aa OIIe9hea Total Otpm is Carbon uWL 4.2 mWL 25000 25600 66 75-125 SAMPLE DUPLICATE. 723521 92111931002 Dup Mar Panmaler Links Resuh fessull RPO RPD DualOars T"I OrgWc Carbon uyrL NO NO 20 $AMPLE OUPLICATE: 721523 9211t633052 Dup M" Psremetar LANE ReaWi Re*A RPO RPO O9A66kn T0111 Orporic Ce rbw up'L 6.2 fnA 15120 1 20 0e1e: 11712&7012 P9 58 AM REPORT OF LA 9D RATO RY ANALYSIS Pag635 0139 T per .pen .he. n.rW npmduc.tl.-.pt. kA. wffl ]ha W do WWt Or P.C. Ano"W 8err . IW .ryNn . Pa[. Anal P4.a AIWvdaal f. Ins y9.a1 .rnur. Inc, ti pace Analyw pl eacy,ves. Inc. aceA�lytrcala nOE,n M..pee R6e0 • S aN r 2225 R1Nr." Or "OO K—y aw 4W. lip Aaraftmom Se.,- r. 2T2e6 Ain llle-NC Zmlt Holm' ll., NC WIN r]?e"M-0021 ie2sp",7176 f7D11a7&g0N7 QUALITY CONTROL DATA Proptl. BURRY CLOSED LF Pace Plo+ecL No.. 92111951 OC R.tth: WEI Vf1$99 Aney7n µethvd- 8M W0$ OC Batch Malhed SM 63f0a Aneym. DeaelpW! WOO TOG AasoGared Lab Samples: 92711961007, 925fi9S1006, 9Z7tS451009 METHOD BLANK: 72S365 matrai: VAIef Ramumaled Lab Se njolaa. 92? 1195 1007, 92111151f105, 92111951009 Men Re"".0 pworn.14r LJnb Rew1i LI14! Analyzed Queaaers Tplal Organic Carbon u911. NO I000 0273r12 19:52 LABORATORY CONTROL SAMPLE: 725366 LCS LC3 %Rec Parameter Link. tkcd Conc Filawl %Rec 0nals Quardlera Total Ory6mc Carom uyL Z5000 23100 92 %6110 MATRIX SPIKE SAMPLE: 725361 92T71957007 Spike MS MS %Rap Pramlelel UP,IA R69u11 LOnC. Rawl, %Rec Llmna Question T.t.r GID.Wc CArben 3160 25000 252.00 66 7!1�125 iAATR17I SP11KE SAMPLE 72SASI 9211=4003 Spike MS MS %Roe Pramefer llnaA Reatdl Conc. Result %Rec Llrldla QuaMAere Total 9r0aa,c Gorgon NprL 8-7 rngfL 25000 27400 75 M125 SAMPLE DVPLICATE 725366 92111951mil 1w0, Max Parameter tan" R.-Il 11 a 11 Ron RPD Q.elker. Total ofglmlc Carbon ug& f07% t000 3 20 SAMPLE DUPLICATE' 725370 92112304004 Duo Mu PAramelaf units Reeurt Relun RPO RPO Quallroms Tole, Otganlc Cmrbw up1L NO NO 2Q a Pa.. Anslypea, 6m11vni ln.. Pam. Anal OW New....Inc. ace 4natytr'cal xis E.A M..den Read - S In A 7.25 a- .d. a Ed.n, NC Mae R.heW.. HC 9eep4 ,:3]6j6z3ae21 1626r25M•T1YO QUALIFIERS Pau Anal yawl e.rYlce., Inc. omb KNr YAva b w iW iylVray.re NC 2R036 11041675-Wp7 Propla SURAY CLOSED LF Pape Preyxi No-: 921$1951 DEFINITIONS DF - 00.m*m Fador, It Iepvtfd, reprasent% Me TAclw applied Ia The reported dmta due to diehgas In soh.ple preperslldn, diruilon or the simple rdlquol, or mplalure content. NO - Nd Deleted a1 or aday. adjwled reporen0 Imll J - Fr6mated Concen"Ilm .None Ilea adJualed malhod delulme Ymll end bela.v the a dju.led,.porNnU „mlr MDL -Adjusted Mdthad DeLmikim LJmn. S - Sun 008t► 12 U,phemyrhydraz,ns (627011alad analy1a) denmil to Azagenaene, Con.l.lenl *in EPA guldail unroindad dale are dspieyad and have Neer road to calculate %rotor ory and RPQ slum. LGSIo) - Laboralry Crurol Sample (Dupllcale) MS(Oi • Maw Spike (Dup6csta) OUP - Sample Dupkale RPO - R.I.IN. P.fc MA Dirfrence NC • Not CAW solo. Sal - %wo Gel - Gem-I)p U - Indestas the compo.rnd was ertslyzed for. Nut pot dolacted. N-NNroeodipnenylan.na decPmpb.ea and cannot be .ep.r.fed from OlpNarrylamMe Iralnp Method 6270- The result rapmt.d fo, e edl anayfe to a cambrmod 9omanNMRUpn. Add p,ea.rv.U.n maynol b, appropriate for 2.OhWoeihylylrryl elhm, Styrene, and Vlnyr chlonda, Pace An.ly9ee4 Ma TNI smulled. Conhle your Pan PM f1N Pie ❑Udenl llm of acorednAd mnmV 103. LABORATORIES PASLA Pun Arm"cal Services • AeheWlls PASI-C Pace Analytical Services - Charfone ANALYTE QUALIFIERS 8 4 The OWcaedglutamic acW standard elusun edad the range 6f 196 plus or m30,5 mpti B5 BOO seed Wank lvaa uut.,de sec.ptenee aitema Reported scuds were eccepled eased an 0... 4k1g qu.ary cone al Ind"tafs. M I MAlrl[ aPlkO 0e6e.sry no se dad QC Hmiµ- aalch ecceP1 ad based on lur"Lory c 1011 l Ample MCS) ruaveiy. mo Mdtriz apds and Main% Joel dYpACAe r6 eovory ndl. a alu Bled ape, !. w bon ornim due la .ample ddWion. Dale. 0212IV2012 09:56 AM REPORT OF LABORATORY ANALYSIS Pepe 36 of 16 Dale: 02f26R01209:56 AM REPORT OF LABORATORY ANALYSIS Ynde ]7.1 39 rhea rr van Yr.r nv1 t»..prptl,�.tl ..upL.r Mi -N. •.Ma e,.4 .ot be nla�6 J. • P1 n rill reerarl are womm a 01 of Pas. Anely.cal ]Laneg he a fe t the xr1.Nn ceee.nt dr Pad A .ly el S.rric.t Ix, LG /'Yf ki �4¢l a Po00 Amlyeaat e.rvlO.t, lnt- 3W Beet M.arpew Re.e • S-la A A.O. Aw1VIhW fer VIM, IM 2225 ft—W. Or Ptu APaly9ul aaevle.a, MO. SWO K--I AW Sun 1C0 f y yM U.n NG 2i2M Aµ4t - HC 2"m Nn —o.. NC 2a07e � (]]5]523d921 (e2eg51.717a {l6lpi5.a0e2 QUALITY CONTROL DATA CROSS REFERENCE TABLE P"41A BURRY CA 0 S E0 LF P.ca nrojw No.: $21,1951 Analytical Lin ID Satmpla 10 QC Batch A14thod OC SM0 AAP.loc.I M.+n.d Batch 921119610d1 WWI EPA3010 MPRP19913 EPA601a ICFI140 97111961602 MWaR EPA3010 MPRPr99T3 EPA 5010 ICPM140 12111111000 "I'"I'll"M- EPA 3010 MPRP199+1 EPA Be 10 ICOM1411 6211116100 Mw•16 EPAS010 MPRPIM913 EPA 6p 10 1CPA140 02111l IMS MW11 EPA3610 MPRPA913 EPA6a10 ICPS140 S3111661006 MW125 EPA3010 MPRPl9913 EPA6010 ICP19140 l2111617007 MW120 EPA3010 MPRPIR913 EPA6010 ICP79140 lafl 1l41006 MW-13 EPA0010 MPRP19911 EPA6610 ICP1lT40 12111l4190e MW-fa EPA3010 MPRP19913 EPA60T0 ICP19140 f211tl11tgt MW-1 EPA0260 MSVIIlT74 l2177la1 p02 NAy-3R EPA 6260 MSYFS 6174 *211116105 MW-1! EPA 6260 MSV]16174 l2171111004 "I'll" EPA 6250 MSylll+ie 62111!l1006 Mw•1! EPA e260 MSVIISI14 112,116l100, MW123 EPA9250 MSV71111174 -1119101 EPA 420 SYl7 2711l6f0ee Mw.77 EPA 6200 MSV716174 :21111,1a0, Mw-ll EPA8260 molvi16174 f2111661001 MW-1 SM 23205 VVETM11753 921t1l61002 mw-3R SM23208 WET04753 92111661003 VW-fi SM 23HO VVETO0753 $1111091004 MVIL. SM 2320E WE7119751 4211119100e MVV-1! SM23200 WETI19753 42111961601 MYV•126 SM 232n VATI+97113 92111951 o0i MWA 20 SM 232ag VVET11975a 9211116160e MW-I3 SM 2320B WETI19751 021111610*0 Mw-16 SM 23205 WETIIl753 921111061001 +IVY-1 Sµ 5210E WE7114677 SM 52106 WET1196al MR SM5210B t WET116701002 &4W4 SM 210E 1EET ON,,SM521aB 7792111l861003 969 /22111Z 4 PAW-19 SM5210B 1lyETl+%75 SM 52+pg VYET119679 IM11931006 MWt1 97A 52108 V4711%75 SM 32la8 VVE77596]9 l2111151006 MW-12S SM 521 a8 VATIIO675 SM 52108 WETA9679 92111961607 Mw-12D SM 521DS 1NETI1%77 SM 5210H VVE 11"Al "111951008 MN7-10 SM 5210E WEC71l075 SM 521H WET119079 92111le1o0! Mw•la am S2100 VXV19677 Sµ52108 WETMUS1 l I111l61007 AIW.1 EPA300.0 VVETN11561 925111610a2 Mw-]R EPA ]000 VJETN11S61 121$1161003 MWf5 EPA 30o.0 WETAM561 121111110" Mw-1a EPA=100 VETN"Mil 92111l11006 MVV-+a EPA300,0 Y&TNTl"ll 92111l6100t Mw-128 01W-12U EPA300A WETN11S62 l21111l61a07 EPA 300.0 WE7A111902 921t1"1006 MW-13 EPA 300.0 WETN11562 oat. 0WU2 012 09 56 AM REPORT OF LAHORATO RY ANALYSIS Page 31 01 39 Trye sport whet npiq nmaduc.d, .-pt. M- .dfNad aaa x�Aa�itina✓�101 Y.c. Aar.aryOY S.rrpt. aw Paaa A-"W lne Pace AnHytlM 3-1cu, IM '� a�i Pi 11! fAl �Cr[�Ia 01-1—. 706 E.M w-d— wd Sw A 22M 01—1 lda IN - E4an NC 272U Aan . NC 2MW4 i (3WXu3-w2- (62 OM-717a QUALITY CONTROL DATA CROSS REFERENCE TABLE Project SURRY CLOSED LF Pace Ptoj.a No: 02111"1 Pd. Amlydul 5t 14ee. Ise. L2 �]Kx,ee7A . S..1W nun —.. !aS 73o7e Lab 10 Seanpla to CC Batch Nmhbd 0C BA1eh AnalyBeal Mothed 12111951001 NW-11 EPA 300.0 V&MVI1662 92111281601 MW-1 SM 1SX-cl-E VVETN11560 0111961002 MWaR SM 4500-CI-E WETNI1560 S2111661007 Mw-is SM 4500•CI•E WETNT136a 92110l1664 11W16 SM 1500•CHE Y4ETN11360 92 IMI"$ MW1! SM a500•CI•E YVE7N1f 560 52117l61006 61W+28 SM 45no-cl-E WUN1140 121t1961007 Mw-12a SAt 4S001Cl•E WETN11560 t2111f61001 MW-13 S44500•0•E VOETNI1599 121111161009 MW.15 SM4500.CI-E WETN111560 12111167091 M%M SM 53108 MTN11560 l2111HIM MW-7R SM 55508 TN VVE11560 62111l61003 MWds SM 5310E WETAMW l2111161004 MW16 SM ",asWETN11560 12111 MDes Mw-7! SM 531 no V9CTN+}560 92111!l1006 Mw•12S SM 5310E MTN 11560 02111091007 INVV-120 W 53115 VIETN11599 921179a1006 MW-7] SM 531pg WETN+T599 92171961006 MW-16 SM 33tas VVETAW 594 Cble 0212612012 09 56 AM REPORT OF LABORATORY ANALYSIS Tb 1.P n..1-11w n pr.d,ew... q% b e . n—I N.-ft....... top— "I ruin St NWol. I- ■nowumi B" Page 35 of 39 �0 2� x b .T � Document Name: Oooument Revised: January 30. 2012 / racraaryrcal Sam lia Conditlon U on Recel t (SCUR) Page 1 of 2 Document Number: Issuing Aulhority: F-CHR•CS•03-rar,08 Pace Hurtersville Quality Office Client Name: 2Lk2l . Project # q -Zjl 1 gS' Where Racelved: D-Knteraviile ❑ Asheville ❑ Eden Courier. 0 Fed Ex ❑ UPS❑ USP50 Cllenl❑ Commeraka(!� Pace Other 00110fial,4•a';F--:;" ; Custody Seal an Coblerl6vx AnaanF' ❑yea off nd Seely intact: ❑yes ❑ no Packing Material: ❑ Bubble Wrap MA& -a Sags ❑ None ❑ Other Thermameter Used; IR Gun 7111,T1 M Type of ice: al Blue None 0 Samples on Ica. wokV procaas has be9w una-u., r.,.ro.r,.., r� ehr.nrr74•r^ f;koloplcal Tlsauo Is Froan: Yrr Ne wA data a Itl r nlnp Corrected Cooler Tamp.; C conteMe: Temp should be above heez" to G'C Comments: Chaln of Cu slody Present' Ova. DNv DNA I- C haln of Cu olody Filled Out: Yer DNa DNA 2, Vial n of Cu slodyRBli+l ulahad- es 114. ❑NA & Sam Wer Name d Signature on COC: Yu Ow DwA 4- Sam pies Arrived wilnfn Hold Time: Yas D. DNA 5, Short Hold Time Mal ys Is <thr: •s ON. DNA 6. R u a h Turn Around 11 me Roque i led: Dvav No Ow, 1, Sufficient Volume: ;K.s Owe DwA 8, Correct Containers Used: E4. ow, 9- drr�s -Pace Containers Used; Lx.. ON. ©NA Conlalnem Infect: •r One OHuA S0. Filtered volume received for Dissolved lesis Mo. ONe wA 11. Sample Labels match CCC: as DNe ONA 12. -Includes dateltlmeAOlAne ale Matrix: All cordslnars ne.", pn sllwi have been V"mkod. n ❑Ne ONA 11, AN p IaNen naedina Araaamadan are found to De In ❑qar ❑Ne ❑NIA compYanCe vulh EPA recommmdazl r xeaoh— VOA, willow, TQC. OLD. WI•pRd ter) ❑Yss ONo iNum .rw rama4nd Sam 1es checked Tor dechlorina llon: IMP DNo DNA 16- Heads ea In VOA Vials limm : aver ❑ OfaA 15. T4 Blank Present: 0Yn Droo 0 78. Up Blank Cuatody Seals Present aver Drra Pace Trip 81 enk Lot iY if purchased : CItonI NotIflcat ant Resolution: Field Oats RequkeV Y ! N Person Contacted: DalaMme: Comments! Resolution: SCURF Revlew: 0 0 tvH 2 In ZI SRF Barlow: oat.: I tO L Note: M'ganevar they a dlswepancy aeatiag Norlh CwdW w c vllance samples, a copy of o,la form YAP be sent to 11A Noah r S EHNR CenHlu lion Office I 1.4 ml of hold. kftMrKt presanadw, out or temp, k)ooa F mmakmral Environmental Coriservatidn Labonitorles, Inc. � 1� �� +G—��J 101-A W.o I.d. 1.d..tr .I [ours eNk [arT NS ]]91I Y M...,- f19...1.]v.0 FAA! 111.447.55ts ..rwW..nt.46..eom .vivo. eneo.. h.. cam Friday, February 24, 2012 Munklpal Engineering Servlces (ML)001] Attn: ]onathan Pfohl P.O. Box 97 Gamer, NC 27529 RE: Laboratory Results for Project Number, Cnone], Project NamelDesci 5uPry Co. Closed LF ENCO WoAorder(s)i C201511 Oear ]onathan Pfohl, Enclosed Is a copy of your laboratory report for test samples received oy our laboratory on Friday, February 10. 2012. unless otherwise noted in an attached project narrative, all samples were received in acceptable Condition and processed In accordance with the referenced methodViDrocedures. Results for these procedures appty only to the samples as suomined. The anatytical results Cnntalned In this report art In Compl lance With NEtAC standards, except as noted In the project narrative. This report shall not be reproduced except In full, without the written approval of the Laboratory. Thus report contains only those anaNses performed by Environmental Consorvadon Laboratories. unless otherwise noted, all arkis"m were performed at ENCO Cary- Data from outside organiza37ons will be reported under separate cover, I you have any questions or require further Information, please do riot hesitate to contact me - Sincerely, CLLSUI� Chuck smim Project Manager Endosure(s) Enrn9 sm Pml IAb Vol mom&3 q1 Sam$Wol 07111)f17 09:20 MealrWi o;110,�11 1ai15 Held Dm 1Tlm,l.] T P,.P DAralTlrn[•; "0,.. D.. iTrep: EPA 3N.11 ovnril G:12 r, 12 0:5, Vnonu 22.9r U..110, MIN-=P. lab to; Crauit�l lampt.M 02folit111.. 0 1ra..lr.dr o27107i214.7s Par.m.e.r Mid o.e.✓T9m.(.j. Pro o...rru-t) M.ir.h oa.ltlm.[.) MWe ... IE Wt) panpli2 W11 WIM12 7212 u..s3q. MWua ub W. t LS11-Q2 .. di cxloi ;2 171au R.air.C. olrser l2 ]ails Pry M.lrw. EPA 300A 0�ANi2 02fI1112 000 1,2111112 22 n EA.nr SP: ..lIW17D W. ID. 0015U504 .1,m •01071f011I 00:15 %%-lv dr 07/10117 ILis P.r,m,M, M•10 D,..rT...(1) Pro 0.a1TIm.(.i A...Iyw. 0.4 1TMn.l.I EPA 200-0 D31MI12 02/21/11 W.a+ 2,r1:r20.r 2:5E IMMIID. 03W-1,7 ubto, C101711.09 s.mpi.n: 021011113.Ss a.rar,re: 61110r1714i15 • ,m. .r IIeW ow1Tv.,[.j .. .. Pry Da6lTlrn,[.) Anair.lA w1.17x...(.} 071m) Dzav1l PP:51 201110]I t1:12 cu..r 2D: Mw-is man Mi CID 1511-00 un,$", a2lov)12 ls,00 1t,uw,d: o]I]o; 31 s.:1s Mad Da W--[1) Pry Dow 1nm.[d[ M.Ir1r O.Ri1�me(.; ^_L'.a•['�i •• 63,o"MI 92;7:ril M:�' I121; Io 17 21:29 -en-t m: Mw•15 ta. Pot C701M t-07 5—Pl.1: 07100nii ]@oo A .Nr.d: 027101 i2 i4:5s P.r,— Muw D-a Tln.,(-). _ . Pr.p o.a1TMmj.) —rip Dow lT il) -A i r mpyll oWVQ W57 7R112111: 00:18 drmrtai nw-71 labsDl C201511-0a s.M . 0211GAZ 09.50 n4c61,..d: o113art: sans P.ram.S.r M.W 0.keTFlr A(.) Pro 10.s1TI—..) A .lyn D...Jnr (.) EFA)Wa 03109112 OL.ulS 09'39 2J2L'201100: 35 Ex.5e un MW-ts tan rpm C201591-01 4-mplod. 02/01117 17di0 a...lr.a. 07 1or1i i4:u m,4r mid Da.1Tbm(.) MID a.,'?".) M.lyw1 W nlf7lw.[.j EP, ILM.0 03100W 02altil 0937 712Lm12 00-31 I1W mr,1-rrdw..f Inge. m rhn r"a, — wlinF.hu l+ge r• 15 1'nae : nr l5 c E N, 0 61nejO. KW-12A L.Yep1 CHISIX-py "W'. R.f.IR 11.y 01 Mpi MRL NC 7WIL 01ft ...nllld Nt1.. tl.crn,Dr 0014 1 l 501. 0.$:, NE 14q t")M.G C1.n1M MW-17 1a61G: C201511.OS Meryl. Ruulb !bp p1 ntK MR!_ NC 1w , un,b M.—d N.W -,a ] S 00:s ou �E i 1PA Wo cl . t to: New-18 lib 10, "*151"7 An.lrV R..rlb .I.p p. M8L MRL NC7WLL Yn R, M.M.d new 6� . o.o rA 1 ] i7• o 5. r{ m [L CPA 3o0.o ENEO P..PrspH.N: MW1 L tl srnplq ID; C;o 151 e-oe R—O—d: ]l. L:�: l.' �n li Meh'1x: Ground Wn1e. Eempldd: o71 eot12 09=20 Work Ow- P-JJ t Sun Co. 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"-M 1 W 51.0t I l cf +. 5 PW 14 of 15 v.ww..nwl.h,.aam The analyze was detected In the associated method blank - The sample was anayzed at dilutlon. The reported value is bch~ the 13b0ratory method detection Iknit �MDL] and the tobaatory method tepoMW furlt (MRL), aftnted for actual Sample preps radon data and moisture clnteryt, when[ I1pplotwe. The analy[e was analyzed for but not detected to the levet shown, adjusted for actual sample preparation data and mdlstvre content, where applicable. The Cc)r4WuerlM 16"ted for tftd anah'te IS art eSbMted value ADMe the Ca ItFat" range Of the Instrllrner,L Thk value k conpdered an estimate. Method Rep"rig Limit. The MAL is roughly equlratent td the practical puanutho n WMt (POL] and Is bafld on the low point of the mRbraum Curve. whm appllcable, sample Preoaration factor. drlutlon fAWr, and. In the Cafe Of soa Samples, mosture content. The Spike recovery was Outside acceptance 11m4M for the MS and,(Or Mstr due to fnalm, interference. Thd LCS SnW r LCSD were wnhln acceptance II is slowing that the labwaxory 1s In control and the data is acc"ble. EIVCa xvn�.,neal�6,-mm P.P 15415 May 30, 2012 Quarterly Water Quality Monitoring Report Prepared for Surry County Closed C&D and Closed MSWLF, Mt. Airy Mt. Airy, North Carolina May 2012 UIC Permit Number:WI0400176 SWS Facility Permit Number: 86-02 MESCO Project Number: G12032,0 Submitted: October 16, 2012 Municipal � Engiaeeripg c� nc l .e..wwr P.O. Box 97 Municipal l:nguieenrig Services Company, P. A Camcr aryl f3oanc, Nonb Carolina Garner, NC ?7529 License No. C-0281 TABLE OF CONTENTS SECTION Sampling 2 Field Parameter Data�^ Page 2 Laboratory Results-,.--.---.---- Fage 2 Groundwater Samples -------------- ------- m___.__._m_......_....mFage 2 Groundwater . _.._.....,._Page 3 . 3 Closing..-_ T ._......-_.Page 3 FIGURES Topographic Map with Site Location,____ W.__..._.. _Figure I Potentiotnetric Map of Uppermost Aquifer wl VOCs Detected Above 2L Standards— ... .W... .,..._..,..__ _,Figure 2 rime Series Graph of Total Cumulative VOC Concentrations-,----- _, __, . _.................... _..._...._.__..,._,_.,,, Figure 3 TABLES Sampling and Analysis Summary ..... .� W.. .......W... W._.W.._ . _ ... .. ..._.__...- Table 1 Detections that Attain or are Above SWSL or 2L Standard (Appendix I) W,.-..Table 2 Indicator Parameter Data Summary ,...,_......... ... .............. „ Table 3 Field Parameter Data Summary .............................. _.... ............ ........... __.._.._..._..W_W_W.,W....._ _____,w._W.W..._ _.....W..W..w_W_w .._..W_Table 4 Hydrologic Properties at Monitoring Wells _.. _._.._..__.._.___.._._..___.._ _.._...__ ..__... _ ._....---Table 5 APPENDICIES Laboratory Analysis Report and Chains of Custody_—,.-,.-------- - Appendix A License No C-0287 CIVILISANlTARYIENVIRONMENTAL ENGINEERS SOLID WASTE MANAGEMENT Municipal Engineering Services Company, P.A. SITE PLANNING ISUBDIVISIONS SUBSURFACE UTILITY ENGINEERING SUE) October 16, 20I2 Mr. Thomas Slusser, P.G. Aquifer protection Section -Underground Injection Control Program Division of Water Quality ]North Carolina Department of Environment and Natural Resources 1636 Mail Service Center Raleigh, NC 27699-1636 Re: Quarterly Water IQuallo, Monitoring Report Sorry County Closed C&D and Closed MSWLF, Mt. Airy 237 Landfill Road Mount Airy, NC 27030 SWS Permit No. 86-02 UIC Permit No. W10400I76 MESCO Project No. G 12032.0 Dear Mr. Slusser: Introduction On behalf of Sorry County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this Quarterly Hater Quality Monitoring Report for the Spring 2012 event performed at the Sorry County closed construction and demolition (C&D) and closed municipal solid waste landfill (MSWLF)-Mount Airy. The Injection ;Pell Permit Application and Well Permit No. W10400176 (5/6/11) requires that Sorry County provide this report to the underground Injection Control (UIC) program on a quarterly basis. This report documents the quality of the groundwater during this monitoring event performed on May 30, 2012. Laboratory analytical results indicate volatile organic compounds (VOCs) attributed to landfill activities continue to persist within three wells that monitor the uppermost aquifer downgradient of three injection points. 1-lowever, total VOC concentrations have decreased in two of the three locations compared to the baseline established during the five events prior to the November 2011 injection event. Background The Sorry County closed C&D and MSWLF, permit #86-03, is located at 237 Landfill Road in Mt. Airy North Carolina. The site location topographic map is depicted in the attached Figure I. Prior to becoming a C&❑ landfill the subject area operated as a MSW unlined sanitary landfill that stopped receiving waste prior to January 1, 1999. The MSWLF was closed with a low permeability cohesive cap per the. Transition Plan. The top portion of the southern unit served as an exclusive C&❑ landfill until prior to June 1, 2008 at which time it was properly closed with another cohesive cap in accordance to the Closure Plan. Per the NC Solid Waste Section (SWS) approved Corrective Action Plan enhanced bioremediation via substrate and tracer injection was initiated in accordance with requirements outlined in the Injection fk'ell Permit Application and We]I Permit No. W10400176 (5/6/11). EOS05981342 plus 1x16 oz EOS® Vitamin BI2 supplement and sodium bromide tracer were injected into four wells on November 2-3. 2011 in an effort to reduce low level aliphatic and aromatic chlorinated hydrocarbons in groundv+titer to belowbrth Carolina Groundwater Standards (2L Standards). kjections were perfdtttted through �?, � and 1 W-5 anT'details are provided in the Injection Evert Record dated Noven ibcr 4, 2010, PC) Bcx 9' GAmar. North Carolina 27529 772 7343 PO Bc,x 349 Boone NC 26607 (MI 262• ;767 Water quality at this facility has been monitored at least semi-annually since 1989 with historical data available since 1994. This is the second quarterly post injection report and the premier post injection report was submitted to the UIC and SWS on July 25, 2012. This report contains sampling procedures, field and laboratory results, groundwater and surface water characterization, and findings. A table of detections compared to Standards, field data results table, groundwater flow directions/rates table, a potentiometric map of the uppermost aquifer, indicator parameter data table and laboratory analytical data results are also enclosed. Sampling Procedure MESCO personnel performed this sampling event following the parameters, frequency and well locations established by the UIC. This event was performed in conjunction with the required SWS semi-annual water quality monitoring event; therefore additional information than required by the UIC may be reported. Groundwater samples were collected and analyzed from nine wells which includes MW-3R, MW-12S, MW-12D, MW-13, MW-15, MW-16, MW-18, MW-19 and upgradient background well MW-1. Additionally, water within the injection wells were measured and visually evaluated in an effort to determine the amount of residual organic substrate remaining in the wells which may help evaluate the viability of these wells to be used for future water quality analysis. Monitoring locations are depicted on Figure 2. Sampling was performed per the protocols outlined in the SWS approved Groundwater and Surface Water Sampling and Analysis Plan which was submitted with the Corrective .4clion Plan (CAP) revision 2 dated December 10, 2010. The depth to water in each well was electronically gaged prior to purging to quantify the static water level elevation. Low -flow pumping methodology or hailing was utilized to adequately purge the wells a minimum of three well volumes or until dry. During purging the stabilized field parameters were recorded. The samples were then placed into laboratory -prepared, pre -preserved containers via a new disposable polyethylene bailer. Samples were kept on ice, and transported to a NC -certified laboratory under proper chain of custody (C-O-Q protocols. Field Parameter Data Field parameters recorded included pH, specific conductance, temperature, dissolved oxygen (DO), oxidation reduction potential (ORP), total dissolved solids (TES) and turbidity. A summary of the field parameter data is presented in Table 4. Laboratory Results Pace Analytical Laboratories (PACE) of Huntersville and Asheville, NC performed the majority of the laboratory analysis. Groundwater samples were analyzed for all the parameters requested by the UIC which includes VOCs and total metals listed in Appendix 11 of 40 CFR 258, alkalinity, sulfate, chloride, total organic carbon and biochemical oxygen demand. Environmental Conservation Laboratories (ENCO) of Cary, NC analyzed the samples for the bromide tracer. A sampling and analysis table summarizing the locations, target parameters and laboratory methods is presented as Table 1. Water samples were reported at the laboratory specific Method Detection Limits (MDL), which are quantifiable at or below the current Solid Waste Section Limits (SWSL). Laboratory results and C-O-Cs are presented in Appendix A. Groundwater Samples The only total metal exceedance was an unprecedented concentration of cadmium detected in MW-12D. The wells with VOCs detected in quantifiable concentrations in exceedance of their respective 2L Standard during this event include MW-15 (I,1-dichloroethane, TCE, PCE, benzene) and MW-16 (benzene, 1,4-dichlorobenzene, 1.2- dichlorapropane, 1,1-dichloroethane, vinyl chloride). Table 2 summarizes Appendix I constituents detected in the water samples in concentrations above the current SWSL or North Carolina Groundwater Standards (2L). Table 3 summarizes indicator parameters quantified by the laboratory. A site map depicting the spatial distribution of VOC concentrations detected above the 2L Standard during this event is presented on Figure 2. Groundwater Characterization A patentiometric map of the uppermost aquifer created from static groundwater elevations recorded during the May 2012 event is included as Figure 2. Groundwater flow rates and directions were calculated via modified ❑arcy's equation and are included in Table 5. Groundwater flows in the unconfined and upper bedrock water -bearing zones in a general southwesterly direction away from the waste limits. Calculated groundwater velocities were variable but consistent compared to historical observations. Findings The quarterly laboratory results indicate that low level dissolved phase VOCs consisting of chlorinated hydrocarbons and aromatics continue to be detected in groundwater samples collected from MW-13, MW-15 and MW-16 which are located within the relevant compliance boundary. Contamination continues to not be identified in samples collected from the other six wells sampled during this event. All VOCs detected in concentrations above the 2L Standard during this event remain within their own respective historically identified range. The total cumulative VOC concentrations detected in the nine wells monitored during this event decreased by 31% (267 ugll to 184 ugll) compared to the moving average of the five events that proceeded the injections (Figure 3). Specifically total cumulative VOC concentrations decreased 45% in MW-16, 44% in MW-13 and increased 8% in MW-15 compared to their own respective five event moving average (Figure 3). Evaluation of the injection wells (IW-1, IW-2, IW-3, IW-5) continues to indicate that a considerable amount of residual organic substrate remain in each of these wells rendering them unsuitable for representative water quality analysis. The viscosity of the water in the injection wells during this May 2012 event precludes sample collection as either a bailer would not descend or the check valve failed. As previously speculated It was confirmed that injection into IW-1 was unsuccessful as no more than 3 gallons of substrate was introduced to the fractured bedrock aquifer at lW-1. The depth to substrate as measured in IW-I had only subsided a total of approximately 22 feet in 210 days (E2" Iday) and had yet to reach the 50 foot pre -injection static level. Bromide tracer was only detected in low non -quantifiable ` j-qualified" concentrations in MW-16. Closing Corrective action to remediate the VOCs as detected in groundwater is expected to continue. The third post injection quarterly water quality monitoring was performed on August 20. 2012 and (lie report will be submitted to UIC and SWS upon completion, If you have any questions regarding this report, please contact us at (919) 772- 5393 or by email at ipfohllfinesco_com or nidurwav@mesco.com. Sincerely, MUNICIPAL ENGINEERING SERVICES CO., P.A. Jonathan Pfohl Environmental Specialist Enclosures cc: Mr. Dennis Bledsoe Surry County Ms. ]aclynne Drummond SWS-Compliance Branch Figures Topographic Map with Site Location Surry County Subtitle D Lined MSLF, Phases 1 & 2 Surry County Closed C&D and Closed MSWLF, Mt. Airy 1 ' .; / ,•,2ph .,.. � - � Y ram' --'_•: c'.•', 'r r .. "... L.1 •`'�-� •i.' ;-.mil ::.. _-;_ � !I , .. -.- - .,' Closed _ Landfill. y .a Subtitle D - rV. ` - �': fix✓`:._. .,�Y� . a . l t.l 't''+s. t - _ r•' -- - _ ' . '' r, - r _-1L3'^.- t yam': "c . ROAD CLAssir;CATION 237 Landfill Road P►imary highway, Light -duty road, hard or hard surface improved surface Mount Airy, NC 28621 Secondary highway, hard surface . Unimproved road La#:36-26-30A65 �.� - � Long:-8f]-34-15.314 Interstate Route (�:3 U. S. Route (D slate Route Northing:983356.18� ^� 1 MILS Easting:1537885.48 FIGURE 1 wai- NOW OR FORMERLY O WNEO $ Y JOHNNY COX lls�q�vmm. 0 in B: I OWNED BY SURRY COUN TY NOW OR FORMERLY OWNED B SHA WNA SUMMERS / rx+saNO FOPOGRAPwc CONTOURS VJMTINO R0AVS 1 - -- ESMATED WASTE LMTS UAJNM USW *ICR CAA — LAVER UwTS OF SU&ME D Lwm Msr+r 1 7 -.- ---- CYTENT OF a'0+E9rE aAY aOSVRE UPON CLOSEO USW ANO CM(! ,A PROPERTY LWE EXTRAPOLAM FMW SURVEY AND Gi5 COUPUANC£ BOUNDARY (2.50' FROM EOW a 50' FROMPROPERTY UrjQ EXTENT OT VW2) DFTE1CTW ABOVE 2L S7ANDA7a WE %O CaVPUMCi aOUNQAl R+ AREAS PREWOUSLY M lECTED EOUIPOMNPAL UPPERMOST CROENDWAMR CONTOURS WA iER SAPPLr Hitt SW-1AL SURFACE WATER UOMTOPWC, PANT Uwe 15) UONTIORINC WELL hW c) W ECNON WELL IASI OROUNOWAIER POTEArROUETRM CLEVA; (A&M) -NOTE aEVATIGN NOT USED rOR COV �J SE�T aAsw --.....,�.......w. roc. o.,..�...... a .r..w OWNED BY SURRY COUNTY FIGURE 2 f r a CLOSED C&D LANDFILL and v' p • •55 -• - -- CLOSED MSWLF FACILITY MuniClpa� /Engineerin 4 Ica1 i POIENiiQOElRlCYAPOFLPPERUMTAgUfi77 SlJRRYCpLI1VTY 'P Se�Lce� f �a��.P.A. + 11111I 4LCS L+ETECIE4 A9OW 3 SIAM MS MT. AIRY, NORTH CAROLINA - >dwr.r.t cmn Figure 3 Total Cumulative VOC Concentrations PrelPost Injection Comparison October 22, 2009 - May 31, 2012 Toni Ca mdadve VOC Concer}vallons - SWSL or 2L Standard watt-WN Time -Sr rks Grwh a� ' No salviv Date LI •MYv-16 4r*M1'-13 •FMA15 aA1lAC Wals .FAhcM hAM.T7I] MW1-MVY-3R •MN-18 •W.19 � z Well ID Oct 2009 (ug/L) May 2010 (ug/L) Oct 2010 (ug/L) May 2011 (ug/L) Oct 2011 (ug/L) Five Event' Moving Average of Five Events Preceding Injection (ug/L) May 2012 (ug,L) Difference (uglL) Difference (%) MW-1 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 MW 3R 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 MW-12S 0.00 0.00 0.00 0.00 5.40 1.08 0.00 -1.08 -100.00 MW-12D 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 MW-13 61.00 50.60 74.20 87.30 72.50 69.12 38.41 -30.71 44.43 MW-15 96.13 63.89 55.00 78.10 64.06 71.44 76.83 5.39 7.55 MW-16 137.90 113.60 135.70 121.20 116.30 124.94 68.60 -56.34 45.09 MW-18 0.00 ❑.00 0.00 0.00 am 0.00 0.00 0.00 0.00 MW-19 0.00 0.00 0.00 0.00 0.00 O.00 0.00 0.00 0.00 Combined Total 295.03 228. 264.90 286.60 258.26 266.58 183.84 -82.74 -31.04 Surry County Closed C&D and Closed MSINLF, Mt- Airy Page 1 of 1 Tables Table 1 Sampling and Analysis Summary May 30, 2012 A . II MNA Tracer n d I a E m u7 z o m m -o v' U w m U ❑ E �c > F- ¢ U F- m CO d a m a r u, 0 a CV [o Q C.1 M O 4 CU O Q O CD CD W ¢ "' Q s a m IVIM x x x x x x x MW-3R x x x x x x x MW-12S x x x x x x x x MW-12❑ x x x x x x x MW-13 x x x x x x x x MW-14 x x x x x x x x MW-15 x x x x x x x x M W-'16 x x x x x x x x MW-18 x x x x x x x MW-19 x x x x x x x App I = from current 40 CFR 258 Surry Countv Closed C&d and Closed MSWLF. ML Airy Pace 1 of 1 Table 2 Detections in Water Samples above SWSL, GWP or 2L Standard (Appendix 1) May 30, 2012 Sample ID Parameter Name t Sample Result Unit MDL 2 SWSL' 2L 4 2B s GWp' Exceedance _ Date Amount MW-12D Cadmium 5130112 2.5 ug/L 1 1 1.75 0.75 MW-13 1,2-Dichloroethane 5130112 0.811 ug/L 0.12 1 0.38 0.43 MW-13 Trichloroethene 5/30/12 1.1 ug1L 0.47 1 3 MW-13 1,1-Dichloroethane 5/30/12 7.6 ug/L 0.32 5 70 MW-13 cis-1,2-Dichloroethene 5/30112 26.9 ug/L 0.19 5 70 MW-13 1,4-Dichlorobenzene 5/30/12 2 ug/L 0.33 1 6 MW-15 Tetrachloroethene 5130112 1.5 uglL 0.46 1 0.7 0.8 MW-15 Benzene 5130112 2.3 ug1L 0.25 1 1 1.3 MWAS Trichloroethene 5130112 4.6 ug1L 0.47 1 3 1.6 MW-15 1,2-Dichloroethane 5130112 0.73 j uglL OA2 1 0.38 0.35 MW-15 1,1-Dichloroethane 5/30/12 23.1 ug1L 0.32 5 70 MW-15 1,4-Dichlorobenzene 5130/12 4 ug/L 0.33 1 6 MW-15 cis-1,2-Dichloroethane 5130/12 40.6 ug/L 0.19 5 70 MW-16 Benzene 5/30112 1.2 uglL 0.25 1 1 MW-16 1,2-Dichloroethane 5/30112 1.8 uglL 0.12 1 0.38 MW-16 1,2-Dichloropropane 5/30112 3.6 ugli- 0.27 1 0.51 MW-16 Vinyl chloride 5130112 3.9 u911- 0.62 1 0.03 MW-16 1,4-Dichlorobenzene 5130/12 13.6 ug1L 0.33 1 6 MW-16 Chlorobenzene 5/30/12 4.3 uglL 0.23 3 50 MW-16 cis-1,2-Dichloroethene 5/30112 38.7 uglL 0.19 5 70 MW-16 Cobalt 5130/12 58.8 ug/L 5 10 MW-16 Trichloroethene 5130/12 1.5 ug/L 0.47 1 3 TB Methylene Chloride 611112 3.2 ug/L 0.97 1 4.6 T Table contains Appendix I con shtuents detected in wells designated by UIC at levels at or above SWSL. GWP, 2L, or 2B MDL = Method Detection Limit 1SWSL = Solid Waste Section Reporting Limit 2L = North Carolina 15A NCAC 2L Groundwater Ruahty Standard 2S = North Carolina 15 NCAC 26 Surface Water Quality Standard for this Specific Stream Classification "GWP = Groundwater Protection Standard j =The reported value is between the laboratory method detecllon limit (MDL) and the laboratory method reporting limit (MRL) adjusted for actual sample preparation data and moisture content, where applicable BOLD = Concentration > 2L Standard 70 0.2 1.42 3.09 3.87 7.6 5urry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Table 3 Indicator Parameter data Summary May 30, 2012 - Parameters - Method MUL' Units MW-1 MW-3R MW-12S MW-12D MW-13 MW-16 MW-16 MW-18 MW-19 5130M 5130112 5/30112 5130/12 5/30112 5/30112 5/30/12 5130112 5/30112 Alkalinity SM 23208 1000 ug/L 69800 94fi00 76800 79800 57700 5/30/12 114000 7250 16500 Sulfate EPA 300A 2000 ug/L 7710 4960 44900 8540 2680 54500 5000 <2000 2190 Chloride SM 4500-CI-E 1000 1 u IL 3560 2780 4650 1110 34200 <0,00 L 18800 1400 2510 TOC SM 5310B 1000 ug1L <1000 <1000 15200 <1000 2430 <1000 3220 <1000 <1000 BO❑ SM5210B 2000 u IL <2000 4000 <2000 7200 <2000 <2000 <2000 c2000 <2000 Temperature Field Instrument 0 C 14.4 15.7 13.7 13.9 14.7 14.7 14.5 14.2 14.1 ORP Field Instrument -900 mV 167.0 121 -778 68 281 31.0 55 196 307 DO Field Instrument 0 mg1L 2.9 0.6 2.5 3.6 0.7 1 0.9 7.9 3.8 pH Field Instrument 0 SU 6.0 7.54 7.33 7.03 5.83 5.9 6.1 5.85 5.58 Bromide (Tracer) EP_A_300.0 _ Field Instrument O,029_ mg/L NS NS <0.029 NS <0.029 <0.029 0.13 NS NS _ Sp. Conductance 6 us/cm 300 260 170 500 200 130 300 13 0 Depth to Water Field Instrument 0.00 ftbtoe 22.48 40.13 13.37 0.00 25.09 52.95 25.47 5.91 10.77 Water Elevatian Calculation 0.00 Ftamsl 1111.87 977.37 1012.10 1027.05 983.39 1023.01 1 974.07 977-09 935.5 Notes: MDL• = Lab Method detection limit or lowest field measurement possible. Constituents detected below quantifiable limits are shown as a M D L value- Surry County Closed C&D and Closed MSWLF, loft. Airy Page 1 of 1 Table 4 Field Parameter Data Summary May 30. 2012 Depth to Water TCC Parameter Water` Elevation Elevation Temp Units ft [btoc] ft (amsi) ft (amal) C lW-1 22.63 na na NR MVV-i 22.48 1111-87 1134.35 14.4 IW-2 39.92 1068.86 1068-86 NR MW-3R 40.13 977.37 1017.50 15.7 IW-3 NR na 1020.57 NR IW-5 40.61 1039-57 108018 NR M W-125 13.70 1012.10 1025.80 13.7 MW-12D 0.00 1027-05 1027.05 13.9 MW-14 34.41 984.39 1018,80 14.5 MW-15 52.95 1023-01 1075-96 14.7 MW-16 25.47 974-07 999.54 14.5 Minimum 0.00 974-07 999.54 13.7 Average 29.9E 1024-25 1046-86 14.5 Maximum 52.95 1111.87 1134,35 15.7 bloc = Below top of casing amsl = Above mean sea level na = NO available NR = No reading attempted Specific ORP 00 pH Conductance TDS Turbidity w mV _ mglL SU umhoslcm mg/L Visual or NTU NR NR NR NR NR >1000 167 2-9 5.9E 300 150 14.8 NR NR NR NR NR >1000 121 0,6 7.54 260 130 Clear NR NR NR NR NR >1000 NR NR NR NR NR >1000 -778 2.5 7.33 170 85 325 fib 16 7.03 500 250 114 132 2.4 5.39 81 40 18.2 31 0.8 5.93 130 60 205 55 0.9 6.10 300 150 Clear -778 0-6 5.39 81 40 14.80 -29 2-0 6.47 249 124 135.4 167 3-6 7.54 500 250 325 Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Table 5 Hydrologic Properties at Monitoring Well Locations May 30, 2012 Groundwater Average Groundwater Hydraulic Effective Hydraulic Linear Groundwater Potentiometric Monitoring Conductivity Porosity Gradient Velocity Rate Flow Depth Elevation _ Well (cmisecond) (%) cfeellfeety (feetfyear) Direction {feet btoc) Meet amsl) MW-1 4,30E-05 15 0.522 155 S42W 22.48 1111,87 IW-2 4.30E-05 15 0.154 46 S43E 39.92 1028.94 MW-13 2.06E-04 23 0.295 273 S27E 25.09 983.39 MW-18 2.04E-03 15 0.093 na S29W 5.91 977.09 MW-19 1.10E-03 3 0.094 3,576 S12W 10.77 935.50 Minimum 4.30E-05 3 0.093 46 - 5.91 935.5 Average 6.86E-04 14 0.232 1,012 - 20.83 1007-36 Maximum 2.04E-03 23 0.522 3,576 - 39.92 1111.87 MW-313 2.40E-04 5 na - na - - naM 40.13 977.37 IW-3 2.40E-05 5 0.215 107 S41W 31.10 989.47 1W-5 1.50E-05 5 0.066 20 SO4W 40.61 1039-57 MW-12S na 3 0.232 na S09W 13.70 1012A0 MW-12D 1.30E-06 5 na na na 0-00 1027.05 MW-15 7.21E-05 3 0.193 480 S03W 52.95 1023.01 MW-16 2.82E-05 3 0.200 194 S42W _25.47 974.07 Minimum 1.30E-06 3 0.066 20 - 0-00 974 07 Average 6.34E-05 4 0.181 200 - 29.14 1006,09 Maximum 2.40E-04 5 0 232 480 - 52.95 1039.57 NOTE: Values for hydraulic conductivity determined via slug test by GAI, MESCO, or Joyce. Hydrologic gradient From water levels recorded on May 30, 2012. Welts screened entirely in rock were not utilized for flow directions/gradients. Screens that traverse both rock and regolith assumed flow in regolith dominates. na = Not availabWappticabie Average Linear Velocity (Q) is defined by modified ❑arcy's equation: K A K= hydraulic conductivity where Q = - - . --- ne= effective porosity n dl dh= head difference dr horizontal distance Screened Interval Lithology Clay Clay Saprolite Saprolite PWR Fractured Rock Fractured Rock Fractured Rock Fractured flock Fractured Rock Fractured Rock Fractured Rock Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Appendix A Laboratory Analysis Reports Chains of Custody Appendix A Laboratory Analysis Reports Chains of Custody /__-PaceAnalytic��� June 14. 2012 Pon AmalAm.l Nrrl.A/, me - Pon A Mlyeeal i.rvld N. Me. PAe. AnMWWl 6.n16.1. 4" X15 EW M.deer Road -6WI.A am 14", .v ggmx "A U4100 Edw W-277le AlnrN.. NC ;NM H-W= HC]eG71 19.761ED-ml iR211 4,717e MOWS W17 Mr. Jonathan PfoN Municipal Engineering Services PC BOX 97 Garner. NC 27629 RE Praje& SORRY CLOSED - MT AIRY (UIC) Pace Project No.: 92119680 Dear Mr. Pfohh Enclosed are the analytical results for sample(s) received by the laboratory on May 91. 2012. The results relate only to the samples included in this report. Results reported herein conform to the most current T N I slandards and the laboratory's Quality Assurance Manual, where appilcable, unless otherwise noted in She body of the report. Analyses were performed at the Pace Analytical Services iacation indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning Ihis report, please feel free to contact rn e. 'Sincerely, Kevin Godwin kevin.godwinapaceiabs. co m Project Manager Er,dowres REPORT OF LABORATORY ANALYSIS TN. r.MH wN -1W r.pr.AceO..edpl P Alro . vn►,-. M. wHp.n eonwtl or P.e. ANImml s.neel. Inc.. Page 1 or 55 • Pau Amly6..1 MM.ar, Ine. Pa.. AI,m"" A—l.a., In[. Pa.. Ar.YWui 6.M[rr, I- AnNytica! 209 Eut M..d.w Rew - Sua. A 2ZM Rm..We Or MW K wr Ay. &w. 100 - Ed-. NC 772M Aeµraa, MC 20M HMI. WA NC 24g16 + f736)6234N21 16261254.7$76 r7p4)6mgm CERTIFICATIONS Pmjnt SUR RY CLOSED - MT AIRY(LIIC) Pin pmj.d Na.: V2119080 Pa" AnY 96.M 6aryl[n, I— Pr n. A-typ[n aPrrla.4, lne. P... AnYylp.l leryln.i r... 2a CaC6"lyticaI 205Enl Maeeaw Read -Sr A =5 Ftw' . Rena KM"Ayt $Wtl 100 Ed.. NC 272M AY�.ya.. NC 20" Hw —A . NC 26078 f73e]62]-em1 le2el754-111e f?;m1675.1-m SAMPLESUMMARY pmjoc1: SGRRY CLOSED - MT AIRY (L11C} Pace P,q.d NP.: 92119650 Charbtt. CanlRaallan IOe Lab 10 Slrhpla 10 Matrix pale Collected An. Recalrad 960P Khcey Aye Ste 100. Hwl Pm Ale, NC 26076 CorinecbelA Cuum-09. 0. PR-0104 Nvrlh Cerolne Ddn king V*ter Cartiacetbn 6: 37706 PkrndafNELAP Cani&6tipn [: E67627 92119a80001 a1 W-1 WSW 0513Pf12 10;15 M1112 13;40 North Caroaru Pleld SeMces Cerokoll- R 5342 Kanluay I/ST Ceruicttlon!' 54 North Cued"VVaatawal.r C.ra6c-sm- R- 12 LG isiana OHH Onnklrq Waw Is LA 100031 921n1a80002 MV&3R W4Nar 0=11012 16:05 CM1112 13:40 South CvoHna CHelcaalon t, 09o09o01 Mal Wgiris C u61ct8 on R�. 357 92nn9660003 MW-125 VAIK OWW1213�35 OM111215:Aa Soolh Ca1CAn! o"Wo water Cart. !: 99006003 WgIMANELAP Cart 11"Don R: 460144 VaVnl4 OWPkNO Waltr CaA86allon 1.00213 92119680004 NLW .120 V*iw 06720l12 12-.H W31112 13A0 62111680006 MW13 mtw 0513af1217A0 a373111213:40 ma A 1225 tl woldo Or., 2225 Rlyaraldepr.,Prhevlla, NC 26604 3oum CuolNt Cartictllun/.99050001 92111660008 MW-16 YIIl1lf OS130713 Si;40 0513111213:40 F londtfNE1.AP Ca roles bon 0. E67646 Nr pu+I0 Carta ncAfbn ■ 00072 92n1106000T MWA1 Y9aoar MWI211;00 OU3111213:40 Met. eaeutaln Carolcall" a; µ.NC 030 Nord1 Car011no aN klnp VV.1ar Caro nca6on l: 37712 Welt WgINa C. mfl-tnn a: 158 WUL—NELAP Certincwen a: 450147 92119660006 MW-16 WNWOU30112 IC05 OY3tf12 la 40 NPM C.rdine W.w."mw Cerble.tinn 9: 40 - 92119609009 MWn5 WRur 05736tl1218,05 M111213:40 REPORT OF LABORATORY ANALYSIS TP:A" nn SIR not ea to meuud ....Pt h ILA, .I"""-Imn—.nt.r Pa- An.If" 5— imp Papc 2 er 55 REPORT OF LASORATO RY A N ALYS IS rh,. r. pan Ylrt nai M r.pmd�c.d-..c.PI n Mi. Pope 3 of 55 f Par,. ANlri+cci S.rvic.., •n{. Psw Amlyli"I J< Wv4, IAc. Pa[. Analytlul S.ttl[aa, IA[. C8AI471ytrC�1 • 2p� Ea.t Afa.c1. Aaa. - Sw+aA 7273 R y.ray. pl 0e0D.1R AH JA. 1 W HC 7116N Aan.r116. NC VC 2501e ;]Y.•H;] E9.': 1e2A1234•]1 ]e 1D1 j6's9C9< SAMPLE ANALYTE COUNT Praject: 5 L1RRY G1,013 Ell - M i AIRY I LII'C j PReo Prpycl No.: 92119680 P.c. An.fyPe.i 6..rle.a, Ine. P... A.u1yn[.i 7.ttf.a., ine. Pm.. An 1l 11ca1 earvl..a. Inc. ' - aG8Jg173�j�fCd� [ pas �a,1+A..mw BP.Y • Swy A 2m a.,.,a.,. 7t oe66 • =-r A.. sw. ,m AW.wP NC I.. H.,nrm+. Nc 2807e IlSe)023-092+ r121]254.71 le [ M4476 900 SAMPLE ANALYTE COUNT P,ol.61: SIJRRY CLOSED - MT AIRY WICI PALS N.po 1 No. 92119660 Analyl.s An.I)lea Lab ID S.mp I. I Method Analyse R.Pall.d 1a 6A r.lory Lab ID S.mµ1. ID M.Shed A—iy41a A.pen.d Fape-Wr, 1211ei10001 A.W1 EPA 6017 JDA +6 PASI•A EPA N)0.0 SAE 1 PASI-A EPA 7470 SI48 I PASI-A SM 450041 E JDA 1 PASI-A EPA 8266 NICK 68 PASI-C SM 5710E SAE 1 PASI-A SM 23209 AES 1 PASI•A 92146660066 MWAS EPA6010 JDA f6 PASI-A SM 52108 50H 4 PASI-A EPA 7470 SHB 1 PA51-A EPA 000.0 EWS 1 PASI-A EPA 6260 MCK 68 PAS1-C SM 4500-0-E JDAL 1 PASI-A SM 20208 AES 1 PASI-A 5M S91 D8 SAE 1 PASI-A SM 5210B 90h 1 P'A51.A 92t156e0002 MW2R EPA 8010 JDA 16 PASI-A ♦rPA 000.0 SAE 1 PAS1-A EPA 7470 SHE 1 PASI-A W 4500.CI E JDA 1 PASI-A EPA 8260 MCK 86 PASI-C $M 53T06 $AE 1 PA$1-A SM 29208 AES f PASI.A 421111"0007 MW-16 EPA.6010 JDA 10 PA51-A SM 521 OB SDH 1 PASI.A EPA 7470 SHB T PASI-A E PA 300.lj EW9 1 PASI•A EPA 6260 MCK 6S PAS!-C SM 4500-CI-E JDA 1 PA51-A SM 2720E AES i PAS1-A SM 5216B SAE I PA51-A Ski 5217E SOH 1 PASI•A 921T9660003 MW-129 EPA 60T0 JDA 16 PASI-A EPA 300.9 SAE f PASI•A EPA 7477 $H6 I PASI-A SM 4500•CI,E JOA 1 PASI-A EPA 6250 MCK fib PASI•C $M 531013 SAE 1 PASI-A SM 23208 AES I PAaj•A 621196e000A MW19 EPA6010 JDA 16 PA$I•A $M 521 OB SD51 I PASI•A EPA 1470 SHB I PASI-A EPA 300.D EWS I PASI•A EPA8260 MCK 6! PAW-C SM 450D-il-E JDA 1 PA61•A SM 2720E AES 1 PASI-A SM 531 p6 SAE 1 PASI-A SM 5210E SDH 1 PASi-.A Will e00b4 MW120 EPA 6610 JDA 16 PASI.A EPA 3 00. 0 SAE I PAS[ -A EPA 1470 S116 I PASI.A SM 450aCf-E JDA 1 PASI-A EPA 3260 MCK 86 PASI.0 SM 6310E SAE t PASI-A AM Z020E AES I PASf.A $21166841009 MW16 EPA 6010 JDA 16 PASI-A 5M 521 a WA I PASI-A EPA 7410 SH8 f PASI-A EPA 3006 SAE 1 PASI-A EPA 6260 MCK 66 PASI-; SM 4500-CI.E JDA I PASI-A SM 23206 AES t PAS1-A SM 53109 SAE I PASI-A 9M 52109 SDH 1 PAIM-A 9211966D006 klv%l2 EPA 61210 JDA 15 PASI,A EPA 300.0 SAE t PAS1-A EPA 7470 SH8 1 PASI.A W 45K-CI-E JDA t PASI-A EPA INN MCK 66 PASI-C SM 51109 SAE 1 PA84-A SM 21208 AES 1 PASI-A SM 6210E SDH i PASL•A REPORT OF LABORATORY ANALYSIS P.pe 4 AI SS REPORT OF LA 50 RATORY ANALYSIS PeOe 5 c155 TI,.,.M6 N.. tat oe •.d.d.[ ...-rA n h . ,... hpon.n.l ncl Oe nMd—d. —pt n Mi -M tl+.+.TArn moan, ePP.. AA,g , Sa.rs.a MP., fn* wnfrn mount of P.m A-Wh . S.—. In[ ace 4r►alyti�ale Pop Anelytle el !orrice., rn.. 7D Eo rl Meed w Ao r� - 6uii ■ Pape Alwype419ery1u4, Ma. Peer Anaiyecer d-lpr, rn.. 7i A..e br POW Kince7 A e Sulr'OD aceMalyticala A." Aeelpi4a164frrl.r, Me. ]W Faa! Y..dow Real - 5u A P.er An.lyae.l 6."Ide., Ina 77I5 RN*-c. [ r eae. AnN7ea11 aampl. lni SWO KN g M SWN 100 Ear.. NC 2729E A.h-OW. RC 26604 Nuroere.pe NC 20D75 1 are Eden. MC 2779E A h".. NC 241804 NuM.tNM- NC 2401a j 376mm7 -21 (62a)354-Ir In [7D41015 m7 ija 67y eP I le;p]2,54. yl 10 1784p75.OM ANALYTICAL RESULTS ANALYTICAL RESULTS Prp19cL 5t1RRY CLOSED - MT A1RY [111C) Prol-C 5l1RRY CLOS€D - MT AIRY IWC) Pace PF.".4 NO 6211 a66D Pa.. Prppd NO 9211 MAG Sample: 7AYY-1 Let' 10: 121"46606! CoMoNd: 03170f1210;15 Received: 05+7171213-A0 Matrbl: M10 S.rnW9: MYWS WOO: 1211f6S0001 Cokzt-d: OS03W 121015 Recelved: OWfV 12 13 40 Metrl.: Nhter Reperl Report Peromolem Rewha U-115 urrm MDL OF Prepared Ar19ly:64 CAS NO. Cud Parameter. R.-N. Vnm LImN MOL OF Prepared Analyzed CAS No. Omit, 6D 10 ICP ilwmdwm&r An4lyllcal Memod: EPA 6010 PreporaEan MOod[ EPA 3010 12" M8V Law Level L4mdflll Anatyeoal Medlod- EPA 8250 Ar Qmony NO uYL 6.0 5.0 1 W0111210-DO D&W12 00,50 7440.364 0ana•5 -4•OlvNorv2•butene NO upL 100 1.0 l 0MV12 19.19 116•57.6 Aveenlc MD uWL 10-D 5.0 1 D6A141210-00 05MV12 105 7440.34.2 Olchloro&IWoromamane NO upL 5.0 021 1 0610Yt2 t6.29 75-71.8 17.rlum 22-" uDrL 100 6,0 1 MM101210DD 0610y120010 7440.30.3 I,1-P.nloroa0+sne NO MWL 5.0 0.12 1 0610Y12 4.29 75.34.1 B-IWM NO "A 1.0 1.0 1 061 0101210021 'DO 061120050 744041.7 12-Olehloroeth6na MD uWL 10 0-12 1 M03112 tl126 n0. 107.2 Cadet. ND ug4 1 0 1.0 1 06A111210'00 06=1200:50 7440.41.9 1,1-Cekwoothene NO ugR S.0 0-56 1 DMW$2 962E 7S-3S4 Chromium NO ug4 10.0 5.0 $ 06r011$ZID00 06WI20010 744047.1 ae•1,2.Okhlvroetnena NO ugh 5-0 0-t9 1 OM311219:29 164-59-2 Cobell NO ug4 10.0 5.0 1 DWIF$2 $D:00 06f02112001a 7440.44.4 trans-1,2-Dlchlom.00- NO WWL 5.0 0.49 t 06NOU121929 156.60•5 Copp.( ND uWL 19.0 !,0 1 0"1112100 06107f12 00-60 7440-50-6 12-RicMwoprodan. NO WV& 1.0 027 1 06A31121939 7647.5 Lead MDug4 10.0 5.0 1 0610111210:00 0MV1200-50 741D-92.1 1,3•RloMoropropane NO11pL 1.0 0.21 1 OSA31121920 142-24.O Nickel NO VO& 50.0 5.0 1 0=11210,00 061D2fi2 D010 7440-92.6 22-0101mopmpeno NO uWL 15.0 0.0 1 060Y12 1919 W-20.7 Selenium NO upL 1DO 10.0 1 OM111210'00 D6r0Nt2 DD'5D 176249,2 1 J-OkhlwcProy.ne ND uWL 5,0 0-42 1 MU121929 553.56.0 541mf ND uOL 10.0 5.0 1 OM11121000 0610211200-50 7440.22-4 61-1,3-OlCh104 OW ppane NO upL to 0.13 1 O"W121029 10061-01.5 ThalNum ND ugA 5.5 5.4 1 M1112 tO:OO 067L12112 00:50 7440.75-0 tran4-t,)-DmNof.ptv0ene NO uWL 1.0 025 1 OBr0Yt2 19:29 IONI-02-6 lln HD UgI4 100 5-0 1 06MV1210.00 D61D711200:50 7440,31.5 C"tenaene NO u04 1.0 0.30 1 06EY12191D t00.41.4 V."sum MO uWL 25-6 50 1 OMIJ12 10.00 DCu02112 00:51) 7440.42.2 E0+14 molhaoryl9lo NO uPt 10.0 020 1 DWU12 1929 97-63.2 Zeu HD upL 10.0 10-0 1 OW101210A0 0610211200'50 7440.6E-0 Neaechlw 11-buladkne NO ug4 10.0 0.71 t D6v03r12 1929 87-W3 2-Na.anone NO upR 50.0 0.4E t 96103/12 19:29 591.78.8 7470 Mercury Analy9cal #lathbd: EPA 7470 Prepandon Method: EPA 7470 radpmadlene NO ugrL 10-9 0.32 5 DBM311210:20 74.0&4 Mercury NO upL 020 0.10 $ 061011t7 12'l0 ftf=1211:56 7470.97.E IFOOutand N0 WfL 100 35.0 1 06AY1219:29 76.63.1 Me DlacryionlONe NO ugrL 100 1193 1 DW311219!29 126.9E-7 4260 MSV Law Leval L.ndfltl An9lydcal Melt od: EPA4269 Mearytane Chlmium Np ug16 1.9 0.97 1 DdClr12 1929 7S4W2 A-1- ND ug& 100 22 1 D6f9Y1211121D 67.64.1 Me" m9th cryl6l. NO uA 34.0 2.0 1 GNOW1219;76 WeZA AcelonITA. NO ug& 55.0 22 1 OWY12 t929 75-016 4•Me6ryl.2•penunan a IMIBKy NO upL 100 033 1 06r0Y12 1" 10&10.1 A.cmietn NO udL SSA ILO 1 DOIDY1270!19 107.02.E Nephlhelane NO MWL 10.0 1 .24 1 06mul21921 01.2" Acrylon8rilt NO 4& 200 1.9 1 M3112 t9:29 16T-9Y1 pmplonh7de RD uprL 1W 3.9 1 UGMY12 19,11 107-12.0 Adlyl cW.Ktla NO upL 10.0 1.5 1 DEmv121929 ID7.050 styrene ND ug4 1.0 0.26 1 0610Y12 $929 10042.5 Benxena ND uWL 5-0 O25 1 0610Y12 19:29 7141.2 1,1,%2-T911achlerae lhana N0 UA 5.0 0.33 1 06103012 19-29 630.2D-6 DromocN-.lhene NO UA 3.0 0.ti7 I 06N3112 1929 74.97.5 1, 1,2.2.7etrachlorce lha me NO uWL 3.0 0.40 1 O6N3112 IS-29 76.34.E &pmadlMloromelnane NO ug4 1.0 0,1E 1 MOM 1029 75.27.4 T4togWWQelhana ND u0% 1.11 0-4E 1 D61D3012 1629 127-16.4 Broawloan NO upL 1.0 On 1 OW03412 I"$ 75.25.2 Tpluane Hp VA fA 010 1 D6103153 192E 10E-06-3 9+omomelhone ND ugk t0.0 029 t OBAY12 1929 7441.9 12,4-TAchlNooenxane NO ugtL 10.0 0]6 1 06JOI121029 120.62.1 2-8ulanme(M EK) NR upL $00 0.96 1 06f0Y12 19-211 7114113 1,1,1-Tdehldmtlh4ne NO u74 t-O 0AE 1 0mulz 1929 71.35.4 Cerhan dlaulede 40 ugrL $Do 12 1 D"V121929 75-15-0 15,2-Trlchl-edhane NO uglL 1.0 926 t 06 W12 1910 79.07.5 Carbon tv"d4vld. NO VOL 1-0 024 1 OBAYt2 Ii29 56.233 hRhl6roauten. NO uWL 1,0 0.47 1 DBAY121916 79.01-6 Chhtoboflme NO LgR& 3-0 0.23 1 OE70Y52 %0:29 $08,10.7 Trsdllaroeuorome0+4na NO upL 1.0 D20 I MN$2 10211 75•E9A ChWrpethane NOupL 100 0.54 1 0GOY1259:29 T&09-3 121-Trichlompr9pen. NO uQL fA D11 S DSA311219]9 W$14 Chloromrm NO upl 5-O 0,14 1 061OY111929 67.6E-3 Vk1y1 aDelete NO upL 56.0 0.35 1 0WO3f121979 109-25-4 Chloram*lhmo NO uWL 1.0 0.11 1 061011121929 7467.0 I.W cNulda NO VA 1.0 Ok2 1 05MV12 19-20 75.01.4 Chlor m". NO uIXL 20.0 0.27 1 0=311211,19 12E-09.4 Xylenai7olell NO wafL 5.0 0-6E 1 06"12 09-19 1310.20.7 SZ-DIbr.-ichlmopropan6 NO ug0. 13.0 21 1 O"W1219Z26 06.124 Sunopate. 4-&omoluwabanaane (S) 102 % 70-130 I O6M%l $021 4604X" DluomprnaxameNane NO uok 3.0 0.21 5 06r9Y12 19-29 124-04.7 OiYromaeMorpmelh.na I51 Itl % 70.130 1 0610Y12 111'29 146E-53.7 1,2.01tll maemene (EDO) NO ugh $.0 0.27 1 00431,219-20 106.97.4 1,2.DieNorO.Ih.n. t14181 leg % 70410 f 0610Y121920 17OW474 Olbrompmeaw. NO uWL 10.0 9.21 1 0"W1211:22 74-95.3 Toluene-d6 (S) 96 % 70-130 OWV1719:29 2P746-5 12-pichla6ban2ane NO upL 5.9 0-30 1 OWN 12 $9:29 9550-1 1,3-D1ctilambe0aene ND WA 5-0 0-24 1 061DY12 1029 541.73•1 1,4.O4hlorc6eea..n4 NO uWL 1.0 0.31 1 W02112 19!29 106-4&7 Del. 0615412012 D1-26 PM REPORT OF LABORATORY ANALYSIS Pape 6 of 55 Dale: OW$4f2012 01:16 PM REPORT QF LABORATORY ANALYSIS PRO 7 o155 iNa reed ehe4 mr a noreauna eee.pi a. rw- TN. r.perl wN -p be..p,*c-d • Pt a" -r" er.Mlea Pen 1 V Pap Arnq►o9r %w . W Mn.-"-- opnrenr or Pec ArWy- 5- 1- P4ee Ae4lyHaal6ervbe., Ine. RA r.Ae "cal Servl u., Iac P... APAlyeeefaHYlip,lrrc I.G7'11 MI �'rA'✓r X4 E..r PA.. dew H.4tl-eda.A :72s Rry.rye. Ur ONO l4e.rwr A. aWe 100 [dAn. NC 172me A4marA., ryC 29aw INuwr.Me, hC 7807E 131mA73.097• i475I75A-71=® 1i➢11a7S9GW ANALYTICAL RESULTS PrOiscl: SUR RY CLOSED - MT AIRY IUICI pmae Pcyw No. 92,19880 Sample: MW.I La610: 62119660001 Ca11. C1ed: HOC? $2 1g:15 Ra[ely ed: OW3111213;4D Me61r; w4jor Ad"n Pae4metws Rmptis Unlb Uml MOL Of pr.pa7eE A1141001 CASNO. guar 73208 AIkapnity An.lylm.IM.(hed SM232W Al aMWI, Tow as CaCI11 69900 uglL Il)00 62105 600, 9 day MAIV1Ks1 Method: SNk 521 OR 1100, 5 dmy NO wWL 2000 309.0 Ic An10" 79 Daye An.lyncml M-TIhad EPA M O swtw 77101 uPwt 250000 4S90 ChPand. Analyleral Me41pd' 5M 4500•C4E Chlmkde 3160 4fL 1000 131 O6 TOC A-441"I McOmA SM 5110E Total Orpenle Calton NO VOL 4000 fool) 1 MU6017 18'4D 7009 1 0190111209!S5 0610501209A5 7000 1 06fg 111R 19A9 14809-79.8 tua I 0612021339 15487-004 1D09 1 061IN121702 7440.44-0 Qal.: Omf PAmou 01.16 Pm REPORT OF LABORATORY ANALYSIS I.* I.-,t .n.N np1 W f.pveuvd. .rc.pl n f4 x1.mM Cie r.mAn .xne.ru nl P4u Malrial dervt.. me P.O. a ar 55 P... Ar oq.I me rWaes, IM. v.e. h.aydeal 4.rvlu e, Ine. P... Anal ytl[rl e.rvi.u. Ine aceArra�ytiCal, 206 e w m.e gnmb -SPne A 7775 ANt .d. d n0ov Myc.v Aw 5vb , W Ed". N1: 772ae AN.wI., NC 784Mc 7e77a faMA271m071 4a2ipsA-?"7 17041E7541m ANALYTICAL RESULTS Project: BURRY CLOSED • MT AIRY (UPC) PaWe Project Ne.: 821196a0 SampW MW-3R Lab& 921IS680002 Coh"Wid OSr10f121505 R-f-d OS13$021310 Meul. Waint "twit Palarnaule Rewde untm Limll MDL OF Preperad Anelyred CAS N.. D1a1 I"o PCP l)rvundwrt.r AneryOsal Method: EPA Solo Prep.nUar, Me01o0: EPA 3010 Amtlmbny NOuyL 601 5.0 1 0610111210'O0 O6g211261:09 7440-M4 Aware NO 6WI 1 a.0 5.0 1 001112 1OAO 06MV 12 61:06 7440.34.2 S"wm NO VWL 100 6A 1 OW11210mo 06102112 KOS 7440-IS-3 Beryllium ND upyL 1.0 1.0 1 OSM111210A0 0 OVQ 01:06 7440-41.7 C.drmium NO uWL 1.0 1.0 1 OSMI1121000 061p211201:05 744041.9 Chfnmlum NO ug4 1a,0 5.0 1 OOM 111210.00 06IOW201:06 744647.3 raborl RD uWL 1a0 5D 1 OSM 111210:00 O&OZ$201:06 744"-4 Copper NO uyL 10.0 5.9 1 OW11210:00 DEW $201'06 7440-50.6 Lead RD upR fP.O 5.9 1 06/01117 10A0 06/07/12 D1 A6 7439-92.1 14ICkAl NO ugx 50.0 5.0 1 0810111210:00 D61=Q 01;05 1440.02-0 selenwm NO uWL 10.0 10.0 1 0610111210.00 0610211201;06 778249.2 $Myer ND yg1L 10.0 SD 1 MCII1710:00 0154M$201 :Oa 7440-2Z4 Ti1Merlrn NO UWL 5.5 54 1 06MV1210:90 0610211201:05 7440.29.0 iln NO mat 100 SA 1 O"IM210.00 06W1201,06 7440.11-5 Ven.olum RL7 up4 25.0 SD 1 CBMI11210:00 WD711201 :06 7440-92-2 2xrc NO upfL 10.0 10.9 1 0"s1121a-00 940OV120110 144044.4 7470 Mercury Anelytleel Malhod: EPA 747a Preyer46wr Method: EPA 7470 Metcu,y NO VOL 0.20 0.10 1 116i W1212:10 DBNL12 11311 743€874I 3289 MSV Low L.Ve1 Lend}ill Analocal Method; EPA 9260 Acelwe NO upfl log 2.2 I O"W1219:45 47-04.1 Acelonlpee NO 1JWL IWO 2.2 I 0816L1219:45 75-OS-a AP+6P.ln NO ugfL 53.0 1.6 I COMU12 19145 107d2.8 Aclywnhrlla ND ugrL 2DO 1.0 1 O$MWI219A5 107.1}4 ARV cnland. NO uq% 10.0 15 1 O&OU12 IS --AS 107-054 6enemn. ND uprl 10 0.25 1 0810311219.45 71.43.2 Emmachlcramethane NO uVL 7.9 0.17 1 06f9311219:45 74.97-5 Bmmudddomme9lene NO ugll 10 0.19 1 COX3112 11:46 7$27-4 gtermobfm NO ugrl 3.0 0.26 t 06 V1219:45 75.25.2 efomammihme NO up1L 10.0 0-29 t 060311219:45 74.53-9 2-11uunone (MEH) NO uyL 106 0.96 1 060311219i9 76.9161 Carbon d-15de NO ug& 10U 12 1 0&0311219-0 15-194l) Carbon mra&Aarlds NO ugrL 1.0 0-25 1 OSMIl12 19;45 56.23.5, Chlorohemuhe NO ugh 3.0 0.13 P 06M111219:45 109.96-7 Cnloroelhmne NO uWL t0.0 0.54 I OW01112 to:45 71-00.1 Ch1w.P.rm NO ugrL 5.0 0.14 1 O"WI219.45 67468.1 cp blOmelhane NO UOIL 1.0 all 1 OGM3112 19:45 74.97.3 CNeroprene NO ug1L 2C.0 0-27 1 06MV1219:45 126.99.6 i,2•ObrOmo63-chlpf opropme NO uyL t3,0 24 P OSM311219:45 W12.6 plbramvrhlaromelhene ND uyL lA 07l 1 ORMU1219A6 124460 1 -0Wromwtheme (609) NO up+L 1.0 0.27 1 UMV12 10.46 106.93.4 Dlbromomethane NO uWL tUA 0.21 1 OOr031171945 74.95.1 1;2•OIcwwGb"1cne NO K& 5.0 0.30 1 OOM311719:45 95-So-I 15-01ch1u06en,we NO UA 5.0 0.24 I 0603117 19:45 541.i3.1 t,4-01dhI0reb4Aj*ma NO u9+L 1 0 0.13 1 08fO1rr7 r9'A5 I6S-d&1 Dole: owl 4001101:35 PM REPORT OF LABORATORY ANALY5i5 Page 0156 IN.,.pen r .e rbt h ,.Pf ducad...Pell n uli W"V! b,. wPlrn -- pf Pe_. AneW& S-. I- P.n A.el ypa.l e...aeae, Me. Pat$Anoly1ml atryleee, Me- P.n Anelyea.l NMrn, In.. ace 4rralytiCai• 305 Ease Me.dew Real - sYll/A am A"usw. Or MM A -I, W.. S� Ion jr rw.l rem Edon, NC 27M AaheA14, NC 25004 Nunw,.A , NC 2607E ? 43361623-M, 1626175e-7176 [7Oel6i}p097 ANALYTICAL RESULTS prWecl: SURRY CLOSED. MT AIRY MCI pue Pny.cl No.: 92t19650 Sample' 6obm Lot) 101 92119660002 Co6.clad: OSf36t2r5:05 RevaN.d: 0513u121140 M4trix:V0nier Report Penmetem RmLt. Unil. Umlt MDL OF Prepared Ano"od CAS No. Ou6 6200 M6V Law Love) Lmol111 M.10%l Method: EPA 620 utna•1,4-0Iddoro-2-butane NO u91L $00 S.O 1 OCVOYI2 59:16 1f0.57$ Dlchloto di luarmhemen a NO ujVL 5.0 021 1 MON t2 I9:45 75-71.6 I,I.Orchrurv. m.ne ND u91L 5.0 9.32 I 06M3117 IWAS 7$-34.3 lA•Dldlmoenane ND W1 1-0 0.12 S 06102f1219:45 107.06.2 1,!•OKhlwoathene NO uyL 5.0 0.5E 1 OMY1219:45 75.35-i d.-1.2-Dlchlomelhene NO u9A 5.0 0.19 s 06101rf 219:49 156.51-2 tnn.-1,2-Di0Narcaura na NO OWL .10 0.49 1 MU,219:45 1$6.50-5 12•DrcM-prop.n. NO ua& 1.0 0-77 1 0wm:z 19-44 7a-07-5 1,3•D$cN&w09ent NO u0L 1.0 016 1 06r03172 19;45 142.26.9 21.01crZa rapene RD uyL 159 0.13 1 O6/OU12 M45 694.20-7 1,1.61dhtarop/ep.n. ND uWL S,0 0-19 1 06f03112 TORS 5R3.56-6 de-1,3.01cmteprop en. NO u0A 1-0 0.11 1 05r0Y 12 1945 100614" trans-1.3.0iddompropena NO U9A 1-0 02S 1 OVM2 fF45 10061-02.5 Elhy6en2.ne ND LPA 1.0 0-30 1 0WV$21945 S00.41.4 Eriyl l Mmua w. NO uyt 10.0 020 1 0"3012 MAS 97-453.2 kuaddar o• 1,3-o,peAen0 NO u04 10-0 0.71 1 M3112 IMS 67.6E-3 2.14e1MD-0 NO UW1 50-0 0.4E 1 MM3r 121045 551.7E-6 lodameth.ne ND ug& 19.0 0.32 1 MY1219:45 14.664 I.oEuten of ND uyl 100 35-0 t M311212:45 ?A-Wl M&I"A 4Vego NO u1PL 100 0.93 } OM311219:45 124.96.1 Mo6lyiene CtiWida NO 0OA. 1.0 0,97 1 06MY1219:45 75.06.2 L49ytnuNaWl.le NO OWL 30.0 7.0 1 9"W1219:45 60.623 a 1f.67y1•2 p.n0 none (MISIC) NO wq& 10a 0.33 1 06MY12 19:45 T06.10.1 Nephehomos NO uyL 10.0 024 1 D6103r 12 $9:15 21.20.3 Fimplonike. ND tot, 150 3.9 1 06AY12 $9:45 107-12-D Syrelre NO uA 1.0 0-26 1 Mutt t6;45 10042.5 f ,I,s,2-TaV4chloroe9r.n. ND ua -0 013 1 D610Yf2 1;:AS 630.20.E 1,12,2-TaOachlww9�.n. NO OWL 3.0 0.4o 1 061OL12 s045 71iL3 -5 Tatadtlw .11h n6 NO OWL 1.0 0.40 1 M31121945 IVA" TaWen. NO UO& 1.0 026 1 00.NY12194S 10 463 12,4-TdRNoro6aruena NO up1L 10,0 0.35 1 0610311219;4S 12042.1 1,1.1.7rkMoreamene NO Opt 1A 0.4E 1 amulI 19:45 7136.E 1,12•TfthA"o.than. ND U9A f.0 1129 1 O MU1219Y5 ?1;-MS TrIchlocollhwe ND ugk $4 0-47 1 0603112 19:45 7941-6 7rlduw0w.m.4h.ne ND Oak 1.0 010 1 o610YI2 19:45 75-014 1,2.3-Tnchlor.wcp4 a NO uA 1.0 0-41 1 06M.V12 11JAS W10.4 YhN Acelele NO 49A 50-0 9-06 1 oafOVI2 19 0 106-0S4 Vrryt chlande NO uyL s.0 0-62 1 00NIM lll45 75.O1•4 XVIona (T";) NO up7L 6-0 0.66 1 O6/OY12 IS 45 1330.20.7 Su.roQafa4 4-&0nolvombenlene ( S] 99 % 70.]30 I 06/02/12 I9A6 ■60.011.4 D,NWnp SupOmethene iSy 105 % 70.130 1 OOMU1219:45 16a"3.7 1 2-DWhiweMMn►-dA (5) 104 SL 70.130 1 0610311219145 17060-w-o TOWen4-06(51 t0O % M130 f 06 3112194S 2037.26.5 Del. 0611 Ar29s 205: J6 pm REPORT OF LABORATORY ANA LYSI5 P49610 of 65 7%e npen ehe= -k a repnk ..d, nectar n M- wly.eutp.. w11rn eena.nl M Pe4 ArrlylMal SeMne, Inc P... Awyreel Serrle.e, Me. r.ee Aryry9rei Hrvleei, ine. ft. Anal yAul 1.rvteae, we ZAnaiylical' 7" Een M..dw R.ea - E- A 2225 Rhe,e ee MW nhe.1 Ave 1u 400 Eden, NC 27705 W,wll.. NC 2M04 1eM,Nrnte. NC 2607E 13761.73-0971 1175 R", 7� !7w j67Se0V! ANALYTICAL RESULTS PnlaaL BURRY CLOSED • MT AJRY IUIC1 pace pmpd No . 9211966C Semplo: WW-3R L66111: 92119960002 Colletled: 05170e1215n5 A..M-d- OSR1r1213:40 MokU-NhW Repon paramalan RetWt6 Units Umd MOL DF Pf.pefad A.".d CAS No Qual 23299 Alkallnity Mel7pcel ls.rhpd: SM 23208 AaaFnity, Total to CaCO3 94600 u9fL 1000 Iwo 1 06106112 16:49 62108 600. 5 day AAM".21 M.Ihod: SM 92109 ODD, 5 cloy ND Opt 2000 20110 1 0"101209-55 06AM120945 306.E IC Anlans 21 Clay. Mdy0r41 Mehod! EPA 300A sulfate 4940J wWL 2500d0 7000 1 MOV1220.02 1460E-19-6 4500 Chia ride An.lyl"l Met"& SM 4504 0-E Chlorid. 2760 wgrL 1D00 r000 1 MM120906 16667.00.E 63100 TOC AnNy6t.r Melva d: SM 531 OS Tolel Or9an4c Cuban NO OWL 1000 sa90 1 0MV12 f7:24 7440.Ii-0 Dole: O6r10012 01:36 PM REPORT OF LABORATORY ANALYSIS P.Ot I pi35 fe.e rePert ena not aP,edlr+d...netN M hat, w nwl 9a a.lpeniRneenld Pen Aalye .9.MPn,I- • Pax: Anal yV<.I eerrmu, Inr. Ride And lyll ul feryle.., Inc. Pace AnNyOul SoNlue, ne. �511� r ice L'�f1+K1� fC[�1 h•1 Ea r•.I.edpw Reed • 5wdN A 2225 A-r.a. Or vow V-" Me Sum 100 . µJ, Ec.n rcc 777ee ..,1.. rr0 2e6W rwnelieu.i. m0 :K1re t33eW341971 .Sia 176 No ifi.10759792 ANALYTICAL RESULTS Prolecl SURRY CLOSED • MT AIAV MCI Paee aletect Ne. 9211 9680 $Ample- W,%III5 Lah Ry 3I111989005 Cvaetled 051301,21715 R.Perxed. 05131112+340 Meirir Vde+ef patarnemll Re.ut. uml. R.pvd Ll mil MOL OF Prepared Analyaed CA$ No pu.1 60101CA 0Mp dw.t., Analytical Method. EPA 0050 Pfeper eu¢n Mellrod. EPA 3010 Andmaay NO ayt- fi-t 6.0 1 DEMI117 to 00 0&Oy1201.1a 7440-MA Af.enlc NO ug& 10.0 5-0 1 ON0111210'(10 UMW 12 a) 10 7440-31-2 9.r14m 20-44 Ila& 100 SO 1 0410111210:00 06+02l12 at 10 7440.39-3 9atydrum NO uyL 1.0 10 I 0610in21000 ONO2ff20,10 7440-41.7 CewWvm NO u1PL 1-0 10 1 06101l1210:00 06/0211201:10 7i40J3.0 Lnmm..m muyL 190 50 1 0Sr0111210:150 06102r 1201•.+O 744047-1 C¢t.m ND uyL 100 SO 1 0610t1171000 ON0711201.10 7440.49A Capoer NO nyL IOR 50 1 06MI+1710'OO 08A2H2 O1'10 7440-50-8 Lead Np uyL 10.0 5.0 1 06ra,N2 +0,00 0610211201:f0 7439.92.1 Nk441 t10 uyL S0.0 50 1 ONO 1"216-00 WOW 20,-10 7440-02-0 Sol lmurO ND 11WL 10.0 19.0 1 06l91112 10.00 06+02112 01:10 7792-49.2 SINsr NO uyL 10.0 50 I 0610i+121000 06r02+1201.IO 144a-224 ThdYum NO uyL 55 54 1 OLM,+17 I009 061ON120110 14.2E-0 T. ND uyL 100 6.0 I Od161+t2 10:00 3114 I2 01:1 a 74404, , Ve-ode-rn NO uOR 25.0 5.0 I 06101n210.0o OT 1111It 7Ai0-62.2 IIn¢ NO ayL $0.0 100 I 06+011121000 f)afaV1Z01.10 7440$6.6 7470 M.rcury Anerytkal medal EPA 7470 Prepa1e60n Merhud EPA 7470 Mercury NO uglL 020 0.t0 I M1+12 t2 10 O6N2112 12'01 7439.97-6 62a0 M5V Low I,nrN Land rut A-.ryllp.l Method EPA 8260 Aciton. NO uyL IN 2.2 1 061v3l,220OD 67'N-1 Acetutotlle NO uyL 55.0 2.2 1 06A3112 20'00 75.05-8 A,91- ND uWL 530 16 1 0=31,22000 ,07•02.1 A,Cryknlhxe NO uyL 200 1 9 1 0N0311Z 20;00 107-11-1 AIN- ch1¢ndr NO uyL 10.0 d t 061031,2 2v:00 107-0} 1 R.nxne NO dgA. 1.0 0.25 f ZVI"220"00 71.43.2 9rnm¢¢tuvrpnled�ene NO vOIL 3.0 0.17 1 061031t220:00 74-97-5 &¢mvb[hl¢romeM.- NO WVL 1.0 016 1 Od1W1122000 ]5-27-4 &pin¢hrm NO uyL 3.0 0.20 t 06MV1220:00 75,25-2 9rom¢methene NO v0L ,0.0 0.29 1 06r0Y,220.00 74-a3•P 2-Bu1en¢rte lME1i) NQ 4WL 10a 0.9E 1 0e10311220.00 Te-03-3 Careen dlevlllde NO uyL f00 1.7 t 064311; 20:00 75-15-0 Cerfivn 1ev.cnlwree NO 4g4 $.a 0.2S t 0WON1220:00 56-23-5 LhlOrapen7ena NO vyL 3-0 023 1 (I&MVIZ 20 cctoe-00 1 Chlvrwdi.n. NO -t- ,0.0 0-14 , a010311220:00 75-00.3 Gfit¢roror•n NO uyL y.0 014 1 06W31122a:00 67-56-3 Ghlelenwlnella NO uA 1-0 9.11 1 6".1z 20:00 74-e7-1 ChWroprrne NO WWL 20.0 027 1 0"W1220.00 126-911-8 1,2-O,6r¢mc-]-chwmprvpene NO u01L 11 a Z.5 1 0610W 2.00 96.12-e Qip.omoc+�lorom.mane NO uyL 3.0 0.71 1 06r03l 1270'00 174-4&1 t ,2•parvmveth.ne JEpS] NO vWIL 1.0 0.77 1 OG+0311220'00 106-934 DO-nn.m.Eh.ne NO uyL +0.0 0.21 1 OGr03+1220.00 74-95.3 12-Okhtorohenxelle NO uyL 5 0 0 30 1 011M3112 20 a0 95.50 I 1,3-O+cnlorohenxene NO u4L 50 024 1 05+03r122000 541.731t 1 ,4 prctt¢rnhntieu. NO uyL I. 033 1 0611IW220-00 105d6-7 Dale; ON 1 er20120f:30 PM REPORT OF LABORATO RY A NA LYSJ S Papa 12 0155 Tn. anon Met per ca reprne.W. dceeyt., the. . 1nc, i"wxbn -M M P.m APdlracal Serves, Inc • Paw Millypeal arty, en, Me. Pace Anal71ial AdMtot, Ina. Pre. Anal ylle,I ""-, lne. - aceMalyfical 7 E..t 4.edca Now • S.'"A 7273 p.'urlda tr wm Katar Me 3.4 I W Mar PA,- E Edon. NL i179a AdA w. PIC MM M+N.rwwa i;G i807a . 376167]891t +628y2S,-7r76 41P418f iawl ANALYTICAL RESULTS Pro}rcF SURRY CLOSED - MT AIRY {UIC) P nce 1-10Jen No 92 T 196M S.mpl.: MW-125 LoblM 92119680003 Codeetd. DY30,121335 Recelrrd: 0SOM21340 Me0'4 1Ne+er Rrpvn Peremelan Reauh4 IJn.n L.mll MOL OF PrepereR Anely+trd CAS No. QuAl 0260 MSV Low Loy4l Laneflll And"col Me hod EPA Bat) Iran.-l4-DcNo+¢-2-0vrene ND uyL 100 10 , 06r0311220.00 r10-57-S Dichlom dlllumomath.ne 01O 4yL 5.0 021 1 06Po 31122.0-00 75.71.E 11-Okv0rae Inane NQ YQIL. 50 0.12 1 afiN3112 N." 15 04.1 1,7•Prchlorvrinan NO uyL 1.0 0.12 1 06102/12 Mac t07-06-2 1,7 DicfilNo than: ND OWL 50 0.56 I 06+OL12 20-00 75 35.4 01-1:-0icnl0rwlhenI 9.SSJ UWL S.o 0.19 1 a6rOb1220-00 156-59.2 Unne•1,2-Dlr7xoroe91ene NO OWL 5 0 0 49 1 06r03112 20. 00 166-60-5 1 2-DchWrayOp.ne NO uyL 'OWL 1.0 0T7 1 O6r010 2 20 DO 70-8R5 1,]•Dlchyrpprppene NO 1.0 0.211 1 0810311220 a0 142.2E-9 2,2-0lcnloreprepene NO uyL 15.0 0.11 1 06103H22a:00 Sw-20-7 1.1-01c hr¢,oWa$wn, NO uyL SO 111 1 06f0311220:00 563-55-6 W-1-0-CAc7d¢roPf ep._ NQ'A 10 013 1 MMW 122000 t00fi+-01-5 tene-1 ]-IXcnlvr¢prvp... NO uyL , 0 076 1 06+03+12 20:06 10061-02 6 EelylOen:ene NO uyL 1.0 on1 (IV03+127000 tW-41-4 E01yI mathauylHe NO uyL 10.1 0.20 1 0MIJ, 2 70:00 97-fl3-2 He.ecnloro•i-3•Auledien. NO u01L ..a 0.71 1 061031122000 67.60•] 7-Hrrmpnr NO uyL 500 0.4E 1 MMW,22600 591 78.E ted0metnene NO atprL 10 0 0.32 4 40+OU 12 20:00 74.60-4 I.gWtAnp} NO u9+L 100 15.0 1 051017}720:00 76-80-+ Me0lacrylenlWlr NOUWL 100 0.93 1 06.ro11t220.00 126-94-7 Methyl A.. Chr¢rlde NO atyL 10 097 4 OVOID 1220:00 76-09-Z M.thyl mHeeu yleta ND +1yL 30-0 2.0 1 amul2 20.cc 60 62.0 4•Methyl-Z•pentenene lMt9rc) NO uyL 100 0.33 1 081031172900 t66•+0-1 NapnN.lone NO uyL 101 024 1 OM311220:00 91.20.3 Propicnlrnle NO 1egIL 150 3E 1 "4311220:00 107.12-0 Styrene NO uyL 1.0 020 1 41"W1220:00 100-e2.5 1 .1.f.2•Taaedllwve011ne NO uyl, 5.0 0.11 1 Main 220;v0 630-20-0 7-Tatef,71lorbe0lane NO ug+L 3.0 0.40 1 0"311220.00 79.34.5 Fetr.clOpr oelnene NO AWL 10 049 + 0610N1220 as 127.1E-e TGlyene NO 4p+L 1 0 0.26 1 0619 N1720 09 100 09-d },2!-7ricnlofobenierve NO vd1L 110 0.35 1 06101rt22900 120.62-+ r 1,1.7nahl¢rp.lh.n. NO uyL 1 O 0.43 1 ONO 31+720.00 71-57 6 2-Tdchlvrvelhene NO'DA, 1.0 0-79 1 0610111270'OO 79•a0-6 Trkhhra th.ne NO ug1L 1.0 047 1 061 ""21 0.90 79-011 YnchlAwBu¢ro me+hene NO ug+L 1 0 9111 1 tl6lOSr122<70tl 7y-69J I.2,]•Trichtwownip"a NO nA 1.0 011 f OfiAN122004D 96•,$.a V"o Tit mli NO uyL 50.0 0.05 1 06MV12 20.90 ;a Who chlwlde NO uyL 1.0 0.52 1 OM-4 06N311220.00 5-- 1-4 %ylene lTerell NO ug'L 6.0 0W 1 g6r0]1t 2200tl 151020.7 S W-11M I- 4•Sramo04o1vhen7enet3l 100% 70.130 1 06103r 122000 460.09-4 plvr orno el10f9meil14na;S1 1 1.% 70•r30 1 0610N122000 1858.53-7 1.2-Dichleroath... 44 f5) ,02 % 7a130 1 06101r12 20'Oa I7080-07,0 Toluene -de 191 141 -A 70-f]0 1 06m 311270 to 2037-26.5 061.: Me I V2012 01'30 pM REPORT OF LABORATORYANALYSJS te...ep0rt r,.. mta r.c� -Pt W Pap. 13 or 55 • Pan A"y9tH aer4cea• Ma. Pae. AnafydeH a.rvlmi, Ise. PAA. Agelydnl aceAnalytical =u5 E.0 Alaefr Re.d - Gu A RM R. A.A. � gem. -, Ar. SW. 10a -1-a-M- Eden. NC 2728E Aah.rn., NO 260D4 rA..lerwlre. he 26076 ' f3361e73d9i1 1e26175�Te 76 l7w]ei}9092 ANALYTICAL RESULTS Pro"I SURRY CLOSED - MT AIRY IUI C} Pam Pr*jw No OZ1196BO sampN: M5Y.126 Lab 10! 9211900003 C09acted; OSYJ0I2 13:35 RecM9ad; 050111213:40 Msft; M* Report parunelm Re.uaa Un to 1.11111 MOL OF Preprad Melyzad CAB No- Ou.1 23200 AILalknhy Anarywo, Method. SM 23208 A1k.ln lly-TmW a4 CiCO3 76600 uyL 1000 1000 1 06106r12 14:40 02$08 BDD• 5 day A..lyllcal Me6wd: SM 52108 800- 5 day NO uyL 2000 2000 1 06M 111209:515 04106112 02:45 3110.0 tC Aw... 26 DAIS Analyllcal Method- EPA 300.0 Sulf.1e 44100J uyL 1250000 10000 5 NAW1215,143 1146ob79-0 4WD CTrrond. An s"w Method: SM 4500-CA•E Chavr.n. e65a nplL $000 1000 1 06WN1200:10 16667-D04 53106 TOO Anmllhlcal Melhod: SM 55108 Tela1 Orpanlr. Carbon 15200 uyL 1004 Iwo t CWIV12 17:45 744OL44-0 Dale: OW14l201. 01`36 PM REPORT OF LA SO RATO RY ANA LYS tS Pap. 14 v155 TN. r.port Net Mfn rypryd,c.d, erupt n M. aaeww aas ae.n.n een.a.a of Pam AfrpaeW D.r..nw 1no Pau. 4-1 y11..1 saw pas_ Mk. Pa.. AriAryllcal a�eAe1r,,�aiyyti5�1yaMl • d.�,. NC 2e6 6. Pep AMA, yesa 16eMn.,". a%- E.0 NAM&; Fo.d - 21.uA WW..� AyS,.N1PS Ae,..rh HI: 2a404 rw4n... Nc 7m079 I gwN23-0921 1e26j734.717e 01)4W5.9 7 ANALYTICAL RESULTS Proje9l: SVRRY CLOSED - MT AIRY(UICI Peae +'ro)ae No.; 9I119650 sarnpl6t M*120 Lah IO; 92111669604 Cowed! OS0012120 A.ddYed: 05131O Z 13:40 100k: Vlm1w Report Flrarnatem Rawls Unlia LHnll MDL OF Plapv.d Analysed CAS ND- 4wd 60101OP Or Ctwalrr A atytkal Maftp J EPA 6010 F§aparaam Me01od; EPA 3010 Anumony NO uyL 6.0 5A 1 OB1mw$1 10.00 06W211201'11 7440.36-0 Menlo NO up+L $0.0 5.4 1 OWII1210:00 06MV1201:11 7440-36.2 BvIum 9.AJ 4pA 100 6.0 1 06701112 f0A0 0610N120t:11 744"7 Beryllium NO uyL 1,0 1,0 1 00101210L0 06f07J129TA'4 7440-41.7 Cmdrmum 2.6 uyL 5A I 1 DOM 111210;00 DWW120113 744043.0 Chfvinkim N'D,.WL 10-0 50 1 am 111210-00 13"V1201,13 744047.3 CvhaR NO uyL 10.0 SO 1 0MV12101 0 060D211201-11 1""" Copper ND u%,L 10-0 5-0 1 0MV1210.90 O010211201:13 744MO.11 Le.d NO uyL 10-0 6-0 1 OMI112 10,00 00@y12 all 7439A2-1 Nickel HD uyL 50-0 S.0 1 04J0111210.00 06R21120113 7440-02.0 Seleruum NO vyL 10.0 IO.o I OMV12 10 00 Oof02112 DI A3 776249.2 S-1- NO uyL lop S.o 1 Oer01112 10;00 06r47112 D1:13 7440.2I-4 Th.lrum ND uyL 5.5 5.A I D=111210:00 DOWQ 01-13 7440.24.0 T1n NO uyL 100 5.0 1 QW1112 I DWOV120113 7440.11-5 Venaraum NO uyL 25.0 5.0 1 OMIO1210:00 06W7112 01-13 7440412.2 2aP: NO u0r1 10,0 10.0 1 o"V1210A0 0610211201:13 744G-668 7470 Mercury AmNAkml Ma shod: EPA 7470 Pfepafa6pn Method: EPA 7470 MA-ry NO uyL 020 0.10 1 DWGIA?. I Z-IU 06103f12 M04 743D-97.6 9260 M8V Low Lay e 1 Landfill AnWkal Me Clad EPA 11260 Acewm ND uyL 100 2.2 I 06103112 20:16 67•64.1 Amtwitrile ND uyk S5.0 22 1 46Af3112 20:16 75DO.a A-:- NO uyL 51.0 1.8 1 0"-VI220:16 107.02-1 Aaylvn.lrlle ND uyL 209 1,0 1 WOW Ia 20-141 107.13.1 Ally] chwrld. ND uyL 10.0 1.6 1 OWN12 lolls 107.03.1 Benzene No uyL 1.0 035 1 D&ADW122IX 16 71.41-2 6rvmoduommHhane ND upf- 3.4 0.17 1 HOW 12 20: 16 7A-97.5 Bromoachroromethane NO Up1L 1.0 0.16 1 061OW122016 76.27.4 8ramehrm NO u0R 3.0 0.26 1 0610311220:Is MMI BrvPwm.tllene NO uyL 10,0 0,20 1 0610VI220:16 74.63-9 Y-Sutanme (MEK) NO a.yL 100 0.96 1 08+03112 20:1a 78-93.3 Cal4on dudllde ND uyL 100 1I 1 06MV122014 M1510 Cofbon l e0d Wd9nde NO uyL 1A 025 1 061031f220;15 56.23-5 Cht0rp6enzene NO uyL 3.0 023 1 O6W311220.10 1D6-91F7 Chw.vein... RD uyL 10.0 OS4 1 0"W1220.10 75.00.3 Chlv.vwnn ND uyL 6-0 0.14 1 06MV12 20:16 87.66•3 Cnlv.vme0l... ND Ugrt- 1.0 0-11 1 0MV122016 7447.3 Chlofoprane NO uyL 200 027 1 WOW1229:115 126.99.9 1,2.Olhromo•3•rhloroprpp.ne NO uyL 43.0 2.5 1 061010 1220: t6 96.12.6 pWrvmvchlvrom.rhen4 NO uyL 1.0 0.21 1 OMU1220:16 124.48.1 12-❑Ihromoeplane;ED6j NO uyL 1.0 027 1 MMUII 2D:15 104,934 Obromomemeno ND uyL 10,0 02f 1 MV371220:16 74.953 t I•Dkhlvrah.n;en. NO uyL 5.0 0.30 1 00=1220:16 9550.1 1 3-Dkllwryhen2Me NO uyL 5.0 024 1 OSMU12 20:16 541.73-1 1,4-0Ichlorodenzane NO vy1 1-0 OA0 1 OMU1220:111 IWAs-7 Dale: M$Vzp120t:36 PM REPORT OF LA50RATORY ANALYSIS A.D.15.1.% TN. sport wW net a r.p..dupd...-* n hP. .,Mt ew M en Dement al pan Mala1W 6..Awa. Ire /� �,,, ,,.�+ P,.. An.rytletl farW... •Imo. Pa..■"ya,.r a- �..nc. 1 a�iPi l4f k'lil,rQl a AS EaN 4, allow ReW - 6,A n 7T15 R�.r.W.4+ 1 . ...r e..o..a. Ella.. Re V705 AahoM RC 2N*4 [2,yM22-101 1677I754.7t79 AN ALrn CAL RE S VLTS Pr D}ect SORRY CLOSED MT AIRY {NCI P.ce Prole CT No 921191600 Pac. AnYyllcrr SvNi e4., Ino- 9pOD✓Jn[•,Ar. 6�,.,0 ffllP.p aceArralytical' Analyl..al SrlHcr., Int. PILO AO&IYOW %DSmattM.rd.eA.W-�A 9rrvlpa, Iny- =5rn..,. o1 H-W-A. NC ZOOM j - ,.e,-„rya,,, Eden. NC 272a6 Aah.W NC 3W04 1?Daut7 S7137 l37®1677-sitf le2ep5.•71 76 ANALYTICAL RESULTS Prolecf SORRY CLOSED • MTAIAY (LHC1 Paca PmMci No 92119660 Sample; MW,120 L4010; 971196e0004 C911501ad DSI2WQ I;t:00 Reealyed. OWI11213:40 MOVW V9116r sample, MWORD Report pare9,rlera Assn 11. undo unw MOL DF Prepared A"24d CAS No. Oust P.ramal.r. S2t0 MSV Low L.wal Lond1111 Ana"mi Method: EPA 0260 2220it A1W.W. by tr/na-1,/-pp,Iw9-2-puree. NO VWL i00 1 0 1 0610YI2 20:16 110-5T•6 A1k.Y,dy, ToI.1 .1 G.001 Dlchlurod1guorom alMna NO uOrL S•O 0-21 1 0616311220:10 7541.1 1,1 •pichler0etnane No ugrL 5.D 032 1 06 W1210.16 75.3A-3 52109900, allay 1 x-Dkwor..rhan. NO uWL 1.D 0.12 1 011103112 4:141 107-06-2 gap, S day 1,1-04ch19reath.np ND V^ 50 0.56 1 D6*311220-16 75.35.4 dr1.2-,DkJhWree9,ene ND up1. 5.0 0,1E I 06W 12 29: 16 156-W2 200.D IC Anton. 26 Day. Deer1.2,CICh1N a.thane ND uWL S.O 4*1 1 0610011220.1E 1%40.5 Sulfate 2.04cmneO:Cpm.. NO uQ& 16 0.27 1 06WI220.16 79-27.6 1,3-plehleroprapane ND uyi I.D 0.2lt 1 061D711220:,6 142.20-9 46D0 Chloride 12.OICNwoprop.nr NO up4 150 Ilia 1 061 W 220.16 S94.20.7 ClHendr I,t-plcNoro-propene RD uWL 5.0 GA9 1 DROD+1220:14 563•Sa-6 do- 1,3•dohlDreprop an, NO up1L 1.0 0., 1 06103+f1201, 10061.01.5 611011 TOC (f"-1, 3•0,chiatarepene NO uWL 1.0 0.26 1 061031T220: 115 TOMI-02.6 e1hVit neon. NO uyL 1.0 030 1 06n13r1220:16 100-/14 Tel.l Organl c C orb" �Ihyr melnaaylare NO uA ID0 0.20 1 OB wl1 20-la 974112 tioucWvu- 1, 3•humdwrla NO "Ok 10.0 0.71 1 Mao 2D:1a 67.66.3 244.Nw9e. NO mg& Wo 0.4E , M3022716 59f-704 Iad9me01pne ND "WI, 10.0 0.32 1 OW31122016 74-664 I.Owlend ND uprL IDO 350 1 0610311220: 16 M134 Me6,. ayA 9ruNl. NO uyL 109 021 1 0MV12 20:110 1264 -7 Me9glana Ch1WId. NO uWL 111 0.97 1 0643112 2016 7S49.2 Methyl msIhmW4te NO uWL 30.0 2.0 t 0MU1220:16 60.62.6 4-M.my12-p-ean .1M1614} NO uWL too 0.33 1 06103A220; 16 108-ID-1 Nephe,.lene NO uq& 100 024 1 Mail 91.20.3 Pr9p69nwo. NO up,L ISO 36 1 0 WIZ 20;16 1D7-12-0 Spyranr RD.0& 10 0.2E 1 MWI220:16 100-42.1 9.1,1,2•TatrapMmeenaml NO u{9L 6.0 0.13 1 D6f031122D:16 an-20-6 I.1,2,2 Terawer 0ea,ane ND uoii 3.0 040 1 OSM311220:16 79.34.E T.vw+,lwe.tft-. NO VgA 4.0 0.46 1 06r0312 20:16 127. " Toluene NO 4VL 1.0 0.26 1 0&4=1220: 16 10646.3 f �,4-Tdchtw9D.nzenr ND uDrL f00 0.35 1 06 W1220-16 120-62-t r f,,.Tncngr9etnane NO 4WL 1.0 0.4E 1 0"3012 20-16 71.55.0 } 2•Tnd,4,od6,ena NO uWL 1A 020 1 Oei"1220-16 79-60-5 Tndda0.9,ene NO uWL 10 047 1 OWW12 20:16 M01-0 TilchlaoM.pometnan. ND uWL 1-0 0.70 1 06+0311220:1m 75-0" 1 ,2,3-TnvilP.Oprap.ne ND ,Ip4 10 041 1 DNDY1220: 16 96.5E-4 V-0 ace tote NO upR 50-0 0.35 1 WOW12 20:16 106-05.4 y110 chi.kl. NO ugiL 10 0-42 1 06r03112 2016 75.01.4 Arlene(Total) ND 1A 5.0 0.66 1 061DIJ1220:16 1119-2C`i sum,rp.ra. 4-& 0.,01u&.ban ran. i Sl 102 45 70.110 I 0&D31124.10 460- 04 DtNa-flu ....Ih-t51 101 % 70.130 1 DOMIO1220:16 lama-5S-7 1,2.0vhrw..tn4 ne•d4 i S] 9e % 10.110 1 D61OW%22016 17D60-D7-0 191--,da 151 90 % 70.110 1 06103et2 20:10 2937.261S WM. OW 14+i01201.3E PM REPORT OF LABORATORY ANALYSIS Tm,.Mft .hap ne10. npredudd--W n rm. _Pwn r,e wAwn --1 or Paco Ana,p 5.n- w Pape 16 0155 D.Ia 06, 14l2017 01:36 PM Pau Anary9gt 1-1-, Mc. 4pa000...y$wo S.n1a0 Newwft INC 2W74 176r Hp754W2 LAD1C; 921776a0004 CoNectrd O51]p1121200 R.cdlwe 0Sr31112 $a A0 M.ua. Hm[ar Ra9or1 Reaulla [Jr4l. Llrwt MOL DF p,epwed Analysed CAS No AnatVOW Melhdd: SM 23209 798DO up1L 1000 $000 I 0a1061t2 16;AO Anaiyllcal M.064: SM 52109 7200 upfL 20M 2D00 1 M111209:65 06AW12 OW46 AnalyOnt Method SPA 300-D 6640J ugiL 25D000 200D 1 ONW1101:11 1410W" An plyllcal Malhod SM 4500-CI•E 111G up1L 1000 100E 1 06yE6y120 111 10147-0" APNyUCel Method SM 53106 ND u0n 1000 1090 1 OVIV121715 7440.44.0 REPORT OF LABORATORY ANALYSIS rN. r.pm Ma,-t"npmdwe. -pi n Na "n M,MIMn wnaenl of Po- Amt" Sor , Ire. L-M A.D. 17 .1 SE aceAnalytical • PAC*Amlynal S.Maar, Ine. X5 E.H M..dw Road • 6u'a A Paw Anawn..l 71rr14w,1ne- Awe AA.Iyoeal 7eMwa, Ine- 2225 R re aW O 96M K-" M,a. auL 100 //r73� //,.❑ (I,,,, f qL G171 1r[�i • Pan Anal yllerl aervlen, Ine l 5 Ea., M..M. Ro.d • lw4 A Paw a,utydul eaMlu., lati 2235 R"a " Or Pace An.tyeul MrWaa, Ine- aeac,u,rwrw.e sw. +m E.- NC V" ANrraa. NC 2MO4 M~wffia, NC 25MO � yxJ�yy Eu.n kC Ririe NC 7e6W Nu�rn+ra, MC Ie07a + I t3m),623-m l 162a1254-71 TO j104l675a092 1330]023 002 te7e1�64-7+1e IyO+wT sco92 ANALYTICAL RESULTS ANALYTICAL RESULTS Prolsol: BURRY CLOSED - AFT AIRY (UIC) Project: SORRY CLOSED - MT AIRY (U1C) Pace Project No.: 92119a10 Pau ProJ.ct No. 92119610 sample: Mw-13 Lob ID: 271111a00ai Copecled: OV40) 17 17.130 R4ecrred 0503111273:40 Me01p. WNer Sample: mvLI3 Lab 10t 92f 10930006 Collected: 0615011217:09 Recurred: 05MIi 1213'49 MPut. ttw Report Repon Paramelen Ra.ults UMIa Ltmll MOL OF Prepared Analy2ed CAS No. Dual Parrnelers Reaulta UNIa UnPI MOL OF P-apered Analysed CAS No- coal 0101 CP Oremndwata, Arts"l M.lh.d: EPA Got Or op. noon M.thud: CPA 3010 0240 M%V Low Love LandIN1 Anal0cal Maenad. EPA 1260 Ar(-"y NO mail. 6.0 50 7 OW0117210;00 NMI CIA 740415-0 be„a• 1,4.Olduorv-2mutene NO ug1L 100 1.0 t 06m311220:]2 110-!,74 A2P4ac NO uaiL 1D.0 3.0 1 06M 117210:00 06702112 CIA 7440.36.2 DlchNxOdAuoramelhana N0'a 5.9 021 1 0MV11220-32 75.71-0 Sulam 67AJ u9�L +0a 5.0 1 WO1112 f0A0 o6M2112 D1-10 744 o-11.3 I,f.pchttroaftrno m u9rL 5,0 OZ2 1 060Ul2 20:32 1�34.3 Swyibwm ND 4prL 1.11 1.0 1 06101112.10A0 MIII1201:11 7440d1.7 I R•DluNorvad".0 DAI'l tKVL 1.0 0.12 1 06W1220:32 107-*2 Cadmwm NO UyL 1.9 7-0 t 05M 111210A0 Dow 201;16 7440.4 -9 1,I4xdW:oalMne NO Uor- !.D am 1 MV122032 75-35-4 Chromium NO udL 10.0 SA 1 05MVI2 ICM 06FM 1201:11, 7440411 de- 1,2.OlchlorwNenP 26.1 W0 1A 0.19 1 DSW7 220;32 1W-59.2 Tr9bed 9.3J UQrL 10-0 44 I 0610111210-00 0002112*11If 7440.40.4 Dane-1,2AI9Nv1valhma NO WWI. 5.0 OAS 1 0"VI220:32 716.60.E Coppar ND uWL 10,0 aR 1 06MV1210!00 OBWII01:16 7440-50.8 720I9Notopgpene NO PWL 1.0 0.21 1 06M31S22DW 71-MS Load NO uWL 10.0 5.0 1 06M1r1210:Dd MOVI20i-16 743492.1 1,5-flkhlorapropene ND uyL 1.1 0.21 1 0670311220:32 142.21-9 N1001. NO Pail 50.0 5.0 } 06 I 2 f0-OD 06MV 2O1;16 7140-02.0 2)-01N+loraprdgane ND uprL 16.0 0.13 I 06m311220:32 594.20.7 Saranlum NO uWL 10.0 70-D } MI"1000 061021120, 15 776249.2 1.1.O1ch1ar opropene ND -WL SA CAD } 06mul220; 32 563.56.6 SWr NO uyL ID.O 1,0 1 011011 I tD:OD OBM711201:1: 1440-22J a..sa•OlchlnryproP.ne NO molt 1.0 0.11 1 ClIms/1270: 32 IOo6t-01.6 Thnlum ND mO& 5.5 64 1 01M117210:00 o6A1211201:11 7440-26-0 tr.ne-1,3-01 wlempropane ND ugiL 79 0.26 } a610311220:32 100E f.D-6 Tin NO mat too R.0 I 06A11S270;00 MV1201:76 7440.31-5 EAybonure NO u911. 1.11 1.30 1 O"VII220:32 IOD41-4 Vsnadum ND m94 25.0 5.0 1 06ml17210: 0 Dow 201:16 7440-R-2 Ethyl molhavylale ND uprL 1D0 020 } 0=31220;32 17-03-2 FInc ND WWI, 10.0 I0.0 1 06m 11$210:00 OM 12 01:16 7440414 NerPd,Iora 1.Ybulediene ND We& 10.0 011 1 0"102 R0.72 67-06-3 2-Ne2anene ND P9rL 50.9 CALL 4 0110l 20-32 W-71.6 747O M►rcury An elylkN Method: EPA TIRO P/►penlon MMOod: EPA 7470 Iodvmhw+ el NO LIPL ICA 0.32 1 011 2 XM 74.1E-4 Mercury NO uait 020 0.10 1 0=111212-10 06m711211:01 7439•iT4 I.Pbuunw ND uyL }00 35.9 1 OM311220:32 7943.1 AIeN.cryonlvd. NQ uVL ISO 0-93 1 DSMU122k32 121111W7 UP MSV Law Level t-mdnll Andynpal L16ihod! EPA 6260 Methylene Clda,lde NO uDOL 1A 0.97 1 06M1rt2 M0:32 7501.2 Aulrne NO UA 100 22 1 061DY1220:32 6744.1 Al eolyl memacryre le NO u9rL 30-0 2.0 1 06M3r}2 20:32 $042-6 Acol-leN. NO myL BSA 22 1 D6M311220:32 754" 4.IAe%vl, 2•pa nla r oa . [M16K} NO uaiL 100 on1 DW20122022 106-10-1 Aawdan ND Usk 51.0 "a 7 06m31t220;32 107-D2.6 NephthaTene NO VA 10.0 a-24 1 MV$220:32 91.20-3 Av,y-Itlle N0 u$#L 200 1.9 1 OSM31122032 107-11,1 ProplmWll0 N0 up1L ISO 3,6 I 116MY122D32 IPY-12-0 AM chloride NO u91L 10.0 1A 1 CM31122032 707-0&1 Styrene AID mail 1.0 D.25 I 06M311220:32 100-42•5 9.42ene NO u91L 1.0 OZS 1 M31:220:32 i1-03.2 1,1,1.2-Te treOnlarveltene NO 6.0 D.51 I DWI` 22Ir:32 1b. odgar. rrvl.n. ND u0'L ],a 0-11 1 0&V3112 70:72 7i•17.5 1,12,2•Tevarhlor.etnana mgCt NO uaiL 3.0 0.40 1 730-20-5 06m31122012 7:.34.5 8=,fiPhturvmethene ND � 110 Clio 7 06M311229:32 7F27.4 hvachlade6tene NO UOr1. 1.0 0.46 1 061Wr1220:32 l27-la•l 9mmv10rm ND WWI 3.0 0-26 1 06W 12 20:32 75.25.2 To4orld ND UA 1-0 a,"1 06POW12 20;32 106-66-3 SmmomeP�ane NO WWI 10.0 0.21 1 01Ay722D;32 14-10.9 12,4-Tnchlwohan2ene DAN u9% ICAO 0-35 1 DWN1,22032 12022.1 2 MAknane iMEK1 NO uaiL 100 D.W 1 060311220:32 71-03 3 1,1,1-rrkhyrP.lh.na N0 vWL 10 0,4E 1 01l2 20:32 71.55-6 C.rhan deul6d. NO Wail. 100 12 1 06MVII220'32 75.154 5,1,2-TA0ltbroe9tane NO up1L 1 0 021 1 Olin 22032 N00.6 Crtgn Uhr.Qhlorrds NO us4 1.0 0.25 1 mull W23-5 O�e^a 1.t uaiL 1.0 0.47 1 OWIP1270:12 79-014 Cnloroban2ene 2.1J Ug4 SA 023 1 06MU122D;32 100-i9.7 TrIchlonluolvme9hans NO uaiL 1.0 0.20 1 9614U722O:72 75.6W Chlaro e6lene NO u9rL 10.0 0,$4 1 O&V31122072 75-OD-1 I,2,3.TrkhloropoPene NO uyL 1.0 0.41 1 06A3r T22732 wl" Chloro bum NO u91L 0A 0-14 1 06M311220:32 67.66.3 V"eeelete ND uyL 50.0 Us 1 MU1220:32 10s-05.4 Chiwomalhane ND wail 1.0 0.11 7 O"W1270:72 74.67.3 Wryl chloride NO -0& 1.0 0.62 1 06M311220;32 7&01-4 ChlrvPranu NO uDIL 20.0 027 1 06W12 20:32 12 -MR Ky1en4 [TotaO NO usrL 5-0 0.6E 1 01A]1112032 1330.20.7 12-D4xvmo- iWwopi Opr,e NO , Wl 1310 23 1 06r0U 12 20:32 i6-124 Sumapana 4-&amaluoroben2ene IS) 99 % T4130 1 06m]77290.]2 460-0&4 DrlMom.chluomeTana NO uA 310 021 1 06M3172 "M T24d1.7 LHbromn6urernalh.ne ( S) f02% 70-130 1 06iV111220'.32 1666.53-7 1]-OlMomoamene {EDB) N9 mail. 1.0 027 1 o610LS228:32 SDa-97J 1,2-0kNrJ8lShene-04 l5} f07 % 7Q130 I Dibro1nomelb-I, ND u9R 10.0 021 1 ON U722012 74-DE-3 Toluene•d115} 99% 70.170 1 06m3rf229-32 2037.26.5 DLW1220'32 207.21-5 12DW4w*h6,t.-a 0.60J uyL 5.0 0.30 1 oa10311i 20:32 96•SO.I 1r]-OlohkroP.n2ene No uyl 5.0 024 1 WOU122032 541.73.1 1,i- Worabar"I 2.0 Wail-7.0 0.33 1 06MU1220:32 1DR4R-7 own.116174R07201:36 PM REPORT OF LABORATORY ANALYSIS Face 16 o156 Data- 06, 1412 D12 01.31 P14 REPORT OF LABORATORY ANALYSIS Pepe 19 or 55 The nW"w16e repreeuP.d, -p1 in M. TN. r.me e 0 nt:t be •.p­"', • im r, An .rN ft yAtMn Ppn.enl 0 13- ht,a"rat IWW"k Inc wfq - M onto aen.rnt Pr Pepe A,nlprel 1.,NPe. M Paw Aryryrisn 5tnlan,t- Pea. AMrypar 6ar100e, lna P.-mkyt i 1.nlwf, Ina. ceAnalykca!r MS Ea5' awwaf Rate• L.eu A 2225 w,uW. Af OW K".y Ma. Lrp tp6 Ed . NC 2726E Atm. w 4c mw f..+mhloe- NC 2Wia 07602 -m- t62512541176 170415754M ANALYTICAL RESULTS PrpJecl. 6URRY CL a9E0 - MT 0W f 1116j P... Prppd No. 97119660 S.mple- Wvi-13 Lab t0: I21111460006 Co"cled 050011211:00 Ruwwod- OS031112 13-40 MaVLV YAW Reped pmr.m.tere R4swis Lhft LJmlt MOL OF Pfeppred Anpmzed CAB No. Ou41 2120E All slimly, An.M"I Me wmle SM 212OB AkaWly. Tole] es C.CO3 07700 uyL 1000 1000 1 0W08l12 16,4E I2109 BCD, 6 day MelyOpd MethodSM 52109 800 5 "1 NO ulyL 20W 2000 1 OSAtf12 14.41 OWO6012 11:t6 000-0 IC An -an. 21 Days AAMN1 Cat MOelad EPA 100 0 Suifste. 2EE01 uyL 250000 2000 1 U 09012 0115 14606.71-6 aa06 Chmnd. A&,NW.1 Me [hod. SM 4W,C7-E Chladdd 74200 u01L 1000 1000 1 061OW12 o"I 16667-00-6 67 too TUC AnNprcal mmtoOl: SM 5110E Talel 4l4 omctc Copal 14M uyl 1000 1000 1 MUM 16107 7440.44-0 Dale. 0W 14r201201.36 PM RE PORT OF LA BORATORY A N A LYSiS rr Mean y.M rvr I r.,f tlise! eraf�l n M .+near e. rnVn ranr,enr ¢i Ptw MYrWcY 9.mw. ke Pepe 20 vl 55 aceAnatytica!' eaee ArW ypaal S.MC[a, lea. :V7 EaY M.elbw Rase - Sod. A Fa.. AnatyCul eami"k Inc. pate A"""I a6mul. Ina. 2225 Rlnred. " M MO Kt -my Are. Swe 400 NC 2726. AN.^R NC 7.404 Ilun0,-A., 11c ;so?. i I [17.p2Ym92r (.7e125F117. 1701�875.90e2 ANALYTICAL RESULTS Prml.cc SORRY CLOSED - MT At RY 1171C1 Pape Pro" No. 92119660 Samplr. NW-16 Lab IO: 921111660006 CvRecutd. OSf70f 1217r40 Rec.rred 0$11111213.t0 Mepd: AwN 1:r.wl per.melem Results unit& 41nu1 *DL OF pmpeted Analyzed CAS Ne. Qual 60101Cp 4roundwnar Analyllcal Mad,nd: EPA 6010 Pre"N oth" McWhod1 EPA 3010 Anampny NO uyL 6o SA I OW111210CIO O&WJ120120 7440.36.0 Ar..mw NO uyL loci 5.0 I 06f61112 10 0O OWOVQ 01:20 74403E-2 Bmhum 46-IJ uyL IN 5.0 1 OMIO12 MOO 0610211201-20 7440.31P•3 8"Wm ND u94 1.0 1.0 1 06101n710-00 06J6p1S20120 7440-41.7 Cadmium NO uyL 1A 1.0 1 06f0111210.90 06100l120120 7440,43-9 Chromium NO YpIL 10.0 5.0 1 0"1012 10 00 O&OVI2 0120 7441117.3 Cmhell 56.E uyL 10.0 S.0 1 O&O1f12 f000 06mZ 1201:20 7440484 Copper NO ugt 10.0 S.O I OW0111210.00 OEWIZ 0120 7440-60-0 LeW NO uyL 1&0 S.4 1 OEr6111210.00 06N&120120 743942.1 Nkkel NO ugeL 5011 5.0 1 0610V12 I0.00 06WI20120 7440-02.0 Selenlum NO uOfi. 10-0 10-0 I OWM1012 10% OWOv120120 1762- 0-2 $Aver NO vjVL 10O S.O I 004111210-N 06421120$10 7440-22-4 Th.lkum NO upt 5.5 5.4 1 OWP111210:00 0WWi1120$20 7440-266 Tin No 4A 100 S.0 1 061OIA2 to:" 06WI20120 74"1.5 .ve"drum NO u1yL 25-0 3.0 1 0641112 10.00 OWOV120120 744042.2 214c NA uyL 100 10.0 1 OW01f17 f000 OSX27120520 7440-066 7470 MefWry Ai.lylcal Melhod: EPA 7470 Frep-11- MCNod' EPA 1470 mercury ND udL 0.20 010 t ORIO12 12:tO 06A21121709 743P-976 a zoo Msv Low Level Lan11111 An Aly wml Ma11wd EPA 112110 Acetone NO uyL IOO 22 1 MOM 230:47 67.64.1 A4.w19blle NO LWL 55.4 22 1 OMU1220.47 75.05.E Aaolalh NO uyL 600 1.0 1 MM311220-41 101-02-5 A:ryrpn[bp. NO uyL 200 1.9 1 0MV12 20.47 107.13-1 AJV,11artde NO 4WL $40 1.5 1 06IO3N720-47 107.05.1 8enxene 12 uyL 1.0 US 1 MU12 20-47 71.43.2 Bremmcllrarenleth.F. NO uyL O E 017 1 06f0N12 20 47 74.117.5 evdmparhlnramemma NO uyL 1.0 11.18 1 O&43f 12 20.4 7 TS-27-4 8mmooem NO uyL 1,0 0 2e t 0MV12 20 47 75.26.2 arom¢meslm No yyL 10.0 029 1 0010VI220A7 74-63-9 2-8 tmr% ne lME KI NO uyL 100 0.96 I 06fO3fl220-47 76.113.3 C.tban d1.u16de NO uyL 100 1: 1 O"W 1220-47 73.151E Celben lab.dr�brWe k0 uyL 1.0 0.25 1 0643f 12 205Q23.5 Chlmohenamne " uyL 3A 0.73 1 o"3412 20'47 106.904 Chmloclhan. RD uyL 10.0 0-54 1 OW0311220-47 75.003 ChJQF0farm NO uyL 5.0 0.14 1 061031L229:47 Q-06.1 ChWmmeh.n. ND Not 1-0 0.11 I Dam 1220:67 7467.3 Chlpreprane NO uyL 20.0 0.27 1 OWU12 20:47 126A6.6 12.Oeupm0� 3•d0urpw opena NO uyL 13A 2,5 L 0643f 122947 M-12.9 DRwomachbramclhmm NO uyL 3.0 021 1 Od43f122IY47 12445-1 12-OBremeelhana(EOB) NO uyL 10 027 1 0603f1220147 106.934 plbrpmemeElane NO uyL 10.0 O21 1 O&OW1220:47 74.95.3 12411chlo, obonma IAJ uyL 5.0 0-30 1 MON1220:47 E1-50.1 1,1.01ch rcloom ne NO uyL 5.0 0.24 1 06 W12 29:47 W43.1 1,4•Dkh1afohenx&ne 13.4 VA 10 0.33 t 0616L12 "AT 106.46.1 Dale: OW 14r;o t 201: 36 PM REP 0 RT OF LABORATORY A NALYS IS Pepe 210155 1% fap.n"MIhe wpnmt-md. -ptn Y. WNWt"rrnllM wnr at Fen A-Ivea 5er.lu.. uc • Pea AnMylhlJ 6erMw$, u,c P41e A nrybcal swryt. Ins. Paw A-oiyucll sera loom. zee. x0a Eae1 Nte.anw Real - 3wr A aceAnalytical 22M Rr,.nWa a 91W �.1 A e Sw I . Ede.., nC 2725E Ay'rrM. NC 70104 x.nrr.•,ue pC gap @ j33a167]-5971 137at254.7176 j7041s75.9077 ANALYTICAL RESULTS PToper WRRY CLOSED - NIT AIRY;UIC] Pace Prvptl Na.: 921196SO Sample- MAl-16 La610t W12690M Codootad PUM1217:40 ReveNed: 05 IIIZ13:40 efatna-lALller Report pwameien fiaeua4 Ilnh. umll MOL OF prepred Analyzed CAS No. Oual 1260 MSY Low Lw.l Land1111 Analytical Method' EPA 6260 prw 1,44N hk4e-2-Wene NO u01L I 1.0 1 0&03112 n 47 HOSTS f%eTlurodlnuvromemene NO 'WL S 0 0.21 1 cc"12 W-1" 7S•it-d I, I - DICNacelnane 3.0.1 uprL 5.0 032 1 Olsen t220-47 75-34-3 1]-OrJitprvemer+e 1JI is f 10 Q.A2 I Dsft 1220:47 tO745.2 1.1•Dkhlof0ethene NO WA 5.0 0.5E 1 Deft 122D'47 M3" c11.1.2-Dltldofpethene 31,7 "pi,5.0 0.19 1 0"311220'47 1N-M2 vane-1,2-DichlOroMhane NO uyL .1 0.. 1 0510Y1220,47 15540.5 1 �•Olr hrelepopina 3.6 uplL 1.0 n.27 1 DM31122047 i5.87-5 I ,343kiuoropopana ND -D'� 1.0 Ole 1 66IO3N220:47 142.28.9 2,2431oh1cropopana ND -OIL 15.0 0.13 1 M31122047 594.20.7 1,1.D/ctep vprapene NO.2k 5.0 049 1 G&MV1220A7 563-53-0 do-1,3-01ddvrerap ene ND uu1L 1.0 013 t M311229-47 1000141.5 mm 1,3-0h;l4wopnpene ND uyL 1.0 025 1 Os-'W1220;47 1000-023 E"tonzana NO udl 1.11 0.30 1 067DY12 2OA7 100-414 Elul m thmowvlele NO wA 10.0 0.20 1 f07f 0512201"t 67.53$ Ne.awora 1,16uudNn4 NO uyt 100 0.71 1 0E103f1220,47 2•Nexenane NO upt 50.0 i .Aa 1 064311220:47 501.76.E lodomao+ene NO uA 10.0 0.32 1 OSf0Y1221W 74.60�4 I4ceut4nat NO vg& too 35-0 1 MMU1220A7 76.63A Me116M10M6114 NO vWL 100 0.90 1 MMU12 2047 126.66.7 Methylene Chlwlde NO up0. 1.0 & 1 06NY1220'47 7549.2 Melhyl meM.cfyleN NO-0tL 30.0 .71 2.0 1 Q%AW1220A7 10.624 i-Me5y:-2�wunone(WSK! NO u9t i00 0zl3 1 0E10Y12200 ID6.10-1 Naphllolene ND ug?L 10.0 0.24 1 0"v1270:47 01-20-3 Pfophrn6f9a NO up'L IN 111 1 WOW220,47 $07.12-0 Sry'4ne NO ulpL 10 035 1 06f931122D;47 $00-42-5 1,1,t,2•TetreMlwa.atone NO uyL S-O D.3] 1 061DY 1724:47 670-20.6 1,1,2,2-Taeadappe9'Ine NO"Wi. 30 D.40 1 9msM3/f720:47 71.24-5 Tevadilww6+4ne NO uyL 1.0 0.45 I MM311t20'47 127.1E-4 TWuene NO uo4 1.0 0.25 1 D"Wil22D;47 1014E-3 1 ,2,4-Tnchiorahanxena 0.671 uql $0.0 035 1 0610Y220L47 12042.1 1,1, 1 •TnMlorvHnan4 ND-pR 1.o 0-►6 1 OW311220:47 7135.E 1,1,2-Ttl4ntwdalhwe NO -ufL 1.0 029 1 0MV12 20-47 79.004 Td9hloreathene 1.6 uyL 1-0 047 1 O6NY 1220A7 79414 Trich oca%mom 4hoca NO uyL 1-0 030 1 0610Y 12 20:4 7 75.69.4 1�,3.7rkhklapropene NO uWL 1.0 0.41 1 06103M220:47 96.1E-4 Ytnyl acafale NO uyl 50.0 0.35 1 OWW12 20,A1 10645.4 Y" eNorw. .1.0 upL 1.0 ON 1 DWY12 20:47 75414 %ylane (Tcla ll NO uA 5.0 0.5E I 0610Y1220:41 1330-20•1 4-&ompluorvhenrene fSl 100 % 70.130 1 OW311220%7 460.0 plpromv6uervmaNane (Sj 109 % 70.130 1 D6f0311220.-47 196E-53.7 1�-Olwwo.then4•d4 (Sy 105 % 76130 1 0E1 M220:47 17D60-073 Taluene•ds is) 06 % 70.130 1 0610Y12 n 47 2037.26.5 Dole. 0m1V201201 xPM REPORT OF LABORATORY ANALYSIS p4pa220155 TNo'"M Y,el net be aped- exwpl n V. .4r'eu1 P. rwabn -m of Pew Av "* 5.n *. R1c �, 1^' 4 eaee Anel rellf lerv'gl, M. pace Analyve14 lm-leee, 1" Pe.e Annydcal savlgR M4. GBAn3 IYPl 7D E11' Me.evw R300 • SLr". 72Z Rpenele Or 9e00 ...iA .. SwF 100 ,l' Eden NC 7178s A.H wwe NG 7Taw F4MInri1.. NC 2�17! + [3]6>td73-097' {67atY54.71 >B y7[r117g9(pj I ANALYTICAL RESULTS Dr.je t SVRRY CLOSED • MT AIRY (L1101 Paco Protect No.' 62119660 Sample: MW11 4hI0t 121111118000111 Collected. DWW1217-40 R.cervad: DW111213-40 Meeb Warm, PramMan n20g AIN rllnlly AIN4 unary, Tow a4 C.CO3 Iz109 BOO, S day 800, 5 day 300-0 IC Anlene 21 Day. suliat4 4s0D ChlOnde Dhlonda $3108 T0C Total OrOr'Ic Carbon Oat.- 0W1412012 01'35 PM Reppd Resulrl units urw MOL OF Prepared Analyzed CAS No. Oum Anelylkal Method: SM 2320EI 114M ug& 'ODO 1000 1 DrYM11215.40 AnaryllCel Malhvd: SM 52100 NA uyl 2000 2000 1 MV1214:41 06A6112 11:15 AhW10.1 LIe51od: EPA 300.0 SWIJ uIVL 25mo 0000 I 06N9112 01.3E 54306.79.E 00e101W Method: SM 450 -0-E ' 195D0 ugIL 1000 1000 1 oismill209:12 16ee7-00-0 M9lylkal Melwd: SM 501 D8 32M uWL 1000 1000 1 W211211:10 7441144.0 REPORT OF LABORATORY ANALYSIS TNa nerd small need rapmd,read, 4xb04 11 M. ooip' 91a •r19ea _m of Pew A ma"d 60,40". M Papa 23 of 55 P.0 Anelyllsal a.rym.., In.- no, Ae.1141u16gw.P• Me P.O. Andy6ea16em. 0. We. P... AnYyawl &-rv...• m. P- ANlyleo 5e r1...- lme p- Ampym.1 4-1.- a e. PaceAnatytical • 205 E!V WAWA/ Rood - 5' I A ms n.l 04 4eaa r,-" �w. S.0'60 I - BC�/�Ii3� rCa� , 3 Fasr M.- - Sun. A 22M Z. .O paw I�e.r Ar. H- 1d0 ..wa..P.rr .r. Eu- NC 27200 Aar,..... NC 2510- Flumrlydr.. NC 25015 1 - .w nrwn. Vm Cd-. 1.0 272a6 Ayevue. lc 7aev. rMnr.w+. 4L lady: 1176021d67+ {ax pm-7+74 17N d75-9QR 173516234662+ 1e 7e 1.64-71 to [704475e ANALYTICAL RESULTS Propel SURRY CLOSED - MT AIRY IUI C) P ece Prelecl Na 92119660 Sampl.: 1AV7.18 Labib- 42119660001 CWIaclad: 05 WI211E0 R.eeNGd 651111213.40 Main& lAulel R.pdn Parem.Irre R... It. IMFlo Limes MDL Di W.pered A44.1n.d CA9 Na. DY.1 6010 ICP 0-dw.l.r mu-v A-. '. R.r-u 64rytllum Cadmk m Ohrom"M Cebell Cvpger Lead N.CkN Selemum SINer ThYYum Tln Ve-h- Zme 7470 Monuly Mdroury 8260 M5V Law LAvel Land loll Aczl n* ACaI.n15114 Aaw.1n Auylannr9e aryl d,4nda Bm24na 9rvmvmloraneth.ne &nMCl1 l.rOme6tene arvmvlvrm &dmeme914ne 2 ffia- ne M KI Cuhvn disu15d. Car Gar 1.611x14o.10. ChIP Wwz4ne Chmroothena CNvrpbRn Chlorvm.6l.ne ehlgrdprene 12.Our emo-]-cnuroprepane Dlaremodilapmethena 1,2-D4ramplmen. JE66) D1br6m9Nen.nr 1;24Okhbmba z"a I,]-Okhiorchen2rne I'4 D Mamt-- ene Will: W41209 073E PM Anelyp5el Me+had: EPA 9010 Pre p.frtlon M4thAd' EPA 3011) ND -A 60 SO 1 05M 111210'00 OSW12OT237440.34.0 NO uA 100 50 1 06+0111210:011 061021120123 7440.3E-2 I Uli up1 IN 5.0 7 OaA 1;$210:00 0641,1201.23 7440.394 NO OWL P.O 1.0 1 051010210:00 ONOW120f 23 1440.41.7 NO OWL 1 0 1.0 1 O&OV1210:09 OMWI20123 744043.1 NO upl 100 S.0 1 W0111210!00 OM211211t23 7H047-3 NO uSL I0-0 5.0 1 05M 111210.00 OSMVI20123 744041.4 NO Volk Ion SA 1 OWII. 210,00 0MV120123 7440.54E NO upL 10.0 5.0 1 0=111210:00 O6f02rl20523 74191-92.1 NO uWL 50.0 50 1 Dam Ih7 10:00 D"Vi20123 7440-02-0 NO uprL 104) 10.0 1 CMII1210:00 0610211201.123 7782-49.2 NO uolk 109 5A 1 0610111210:00 OUVI2 O1523 7440.22.4 NO Volt $.5 5.4 1 ONO 111210:00 O&VV1201.23 744044.4 NO up4 100 5.0 1 DUC111210:(10 06JWI20123 7440-314 NO uWL 3S 0 so 1 MMII12 10.0 06r02112 0123 7440.62-2 NO uWL 100 10.0 1 06.01117 la 0o 06MV120121 7440-66-6 AnelylW l Ma6red EPA 7470 Praparauen Malhad. EPA 7470 NO uVL 0.20 0-10 1 014111212:10 0510211212:17 7439.97.E AnalVOc.l Method. Et2Aa260 NO u0A 100 22 1 064311221 �03 57.54.1 NO upfL 530 22 1 0610311227-c" 75-0514 NO upL 53.0 111 1 06f0311221 L03 10142.9 NO uo1L 200 1.9 1 06103N221p3 101.13•t NO uIVL 10.0 1s 1 OSM311221:03 10145-1 NO VOA 1.0 0.25 1 0"311221:03 7T-43.2 NO up'L 3.0 0.17 1 D510311221-03 74.97.E NO VOA t.0 0.16 1 05103r1221.03 75.27.4 NO VA 30 026 1 06f031122"3 75.23-2 ND uWL 10.0 029 1 0WOV122103 74.63-9 No upL 160 004 1 061D311211103 14N3.3 NO VA 100 12 1 06M31122103 75-t5,0 NO uy4 1-0 026 1 0a103J 1221-03 W23-6 NO upL a 021 1 06143f122"3 109.O17 NO ij r 10.0 0.54 1 06/03112 21-03 75.00.) NO uWL 5-0 Old 1 0610311221.03 67.6E-3 NO u4tI, 10 01$ 1 OWV122103 74.47-3 NO uy 200 a17 1 OVOW1221103 1241-49.8 NO uyL 130 2.3 1 O6f W22103 96-724 NO OWL 3-0 021 1 0610L12 21:a3 12A•48.1 NO u4fL 1.0 0127 1 0MV12 21.D3 106.534 ND VOIL 10.0 0.21 1 DOW 12 21-03 7419S-3 NO VOA 5.0 030 1 D61DW1221:03 95-Wi NO u0A 5.0 0 24 1 OW3012 21 01 541-73.1 NO uWA 1.0 0.33 I QGM3172 21:03 1064r.7 REPORT OF LABORATORY ANALYSIS iNe llpert.n.l -1 W npe0is.d-.-p1 n AO w.IpW M -lln twnoeml 60 $- N A. r" 5..-. M ANALYTICAL RESULTS P,.Jacl• BURRY CLOSED • MT AIRY (WIC) Pere Project Ng.: 92119680 8a plv MW-16 Lab IO. 62119680467 Ca6aned- 05r3011211.00 Aecelved: 05r31A1 1340 V.V,. Wel.r Rapen Pma 61" Raau11. Unre UrNI VOL OF Pr.pa,ed Anol"4 CAS No 0u10 6260 MSV Law L.r.l L.ndllll Anely1k P Mothvd- EPA 8250 It", 1,4-01fir9ro•241pene NO u0fl IO0 1 0 1 DN0311221:93 110.57$ D1dlWradlWPremelhene ND uWL 5.0 021 1 OM311221:03 75-71.6 i 7-DkhIv*GIlua . NO u01L 50 0.32 $ 0610311221V3 75-34.3 12-010wotoelhano NO 41L 1.0 0.12 1 081031122113 107.06.2 1.1-OkhlW0@BwPe NO VWL 5.0 0s6 t WON1221:03 75454 cm- 1,2•Dichtoloelnane NO r.O+L 5.0 0.10 1 oem111221.01 158-50.2 Jn ,I r2.D chlor p.9tene NO up'L 14 0.40 1 0"3112 2t:03 13a-00•5 s,2-0IWdaoprsp.ne NO u01L 10 027 1 06;6311221:03 74,81.5 1,3-❑k31lor9prOpane NO uOfL 1-0 0-26 1 05MV122T:03 142.26.9 22.010bift rdpene NO 401L 15.E 0.13 1 061031f 221:03 594.20.7 1,1-Dlehkroyfvpene NO uWL 5.0 0-49 1 OMUI22tA3 563.56$ ,A-f 3-0Ip7dvrvprppene NO uWL 1 0 0.13 1 ON0311221.03 10061.01.5 van.-1,340idlefepl6p4n6 NO ugiL 1.0 0.29 1 061031122103 10061-02-0 Em03em4ene NO uyL 1.0 0-30 1 0610311221:03 10041.4 Ethyl melnacryl.t. NO VyL 10.9 0-20 1 O6r031122t V3 47.63.2 taetechloro-1,1w11adlane NO OWL 10.0 0-71 1 0610111221:03 67L6.3 2-Hkx. and NO OWL 50.0 046 1 OM3112 21:03 501.78.6 Indamethene NO VOA. 10.0 0.32 1 CBMU1221:03 74•46.4 120butandl NO upl 100 35.0 1 0610311221A3 76-a34 MemauylWwwa NO uyfl 100 0.93 1 06MU 1221 (13 126A6.7 ue""a CNorlde ND VO'L 1.0 097 1 081p3112 ?1 -0 75.09-2 Methyl merh.ez&I. NO VWL 30.0 2.0 1 0643112 2103 80.62.6 {JAe01y14•p.nlenate (MIRK) NO UgA 100 0 33 1 06103112 21:03 106-lo-I Naphthalene NO OWL 40.0 024 1 060V 122113 91.20.3 P10pmnHffld NO upL 150 1.6 1 olleaV122103 107.12-0 6lyren. NO uolL 1.0 626 1 0WOU122103 10O.42.5 1,1,1,2-ie4acr4prvanen. NO uOIL E.0 0-31 1 06W1221:03 6304G-a 1,1,2, 2-T.Oechloroew.ne NO uWL 30 0 40 i o6103112 21:03 79.34-5 Tanchl rneet.ne NO VWL 10 ace 1 Oa163f 12 41 03 127.16,4 Talr.ane NO uSL 1.0 0.26 1 004W1221:03 106.8E-3 12,{•TripllpreGen2me W W. tO0 035 1 0MV12;1:03 U0.42.1 1,1,1-hrchkeoa6tane NO UWL 10 044 1 O6 V122143 71.65.E 1,12-TndtlomolhaAe NO.@L 10 029 1 OSOCW1221:03 79.00.5 Tkmmoelhame NO uyl 10 0.47 1 O61D3112210 7"t-6 irtd1101e6upr6maOlane NO uWL $.a 0.20 1 OaPM1221;03 75.69.4 12.7-Trlchleluplopehe NO LPL 1.0 0.41 1 DSMU1221-03 W, %W .Mlat. NO up4 50.0 0.3E 1 06103r 1221:03 106.OS4 VYlyl eluorld. NO uWL 1.0 6.02 1 D61OU12 21 03 7541.4 %ylene ffwp1J NO ug1L 5.0 0.6E 1 DUO 311221-03 1330.20.7 9uf70yana A-&Pmoluoroben4en a ISI 100 % 70.130 1 08103r 12 21 D3 460-Mi OiWvmvAuarorpelhane 13) 1DO % 70-"(1 1 08/03112 21 03 1a611-51.7 12.01ChlerOelh2na44 tR) 1D3 R 70.130 1 06/03112 21'03 77060-07.0 Toluen e•d61S) 44 % 70-t30 r DOY1221 D3 2037-26-5 Pap 24 of Dale: 060$4r205201:36 PM REPORT OF LABORATORY ANALYS13 rl.. capon NN rot be r4pmGfcW. epup! n 1� w4wur er umeln ppml 04 ✓ .p M.I�ndl S.r�. sic peye 75 P1 63 �2ceAnalyticaf* Fa[. AnW ygeW 6.rvle. r. lrw- Rau Anafyd.al her mxm. 1m.. Pa n. Analyd..l e9rcl9a., In¢. 206 Errt M9sWww Road - 6wr A 2225 RM..W. Or. 9ed0wnea7 Avg sun 1w ..ar �yyr a„ Ear+. NC 2126E A h.A., NC 20604 M"'".. NC 2101e 1176j623-Mi (825PWIM 110416'S40B2 ANALYTICAL RESULTS ProJ.ct: SURRY CLOSED - MT AIRY (UIC) pace Pmpd No.: 92119B60 8arnpl.- MW-16 Leb IO: 92119860007 CU..t.d- D513WI1 11:00 RsC4dVad: OW311121140 M6tW if ater Repo14 P-rumen Rerun6 Units Lin* MDL OF Prepared Analyzed CAS No. 0u11 71202 A I k.l In lly Anaiyml µshod: SM 23208 Alkaknl[r To Ial as C. CO3 7260 upL 1000 62toB aOO, 5 dry Analyiwal Meshed. SM 521 OB BUD, 5 day NO upL NQ11 300.0 C Anlon6 29 04ys AwOcal Motnod: EPA 300.0 Sulfate ND uyL 250000 4500 Chlond. AA.IyOoal Method: SM 06 C1-E Chlunde 1400 vyL 1D00 6310E TOC An.lyilcal Melhe d. SM $31 OB Tor.1 O.Onn,. Carbon NO uWL 1000 1000 1 OWON12 1E:40 2000 1 D6fO1f1209:55 OE10611209;45 2000 1 0WVW12 01:62 14606.79.E 1000 1 08N6112 0912 16867-0045 100E I 0&12112 $15211 744044-0 62 Nil. W14�2012013� PM REPORT OF LABORATORY ANALYSIS Page 26 .I 55 TM fep."tinenetN fael.A .9ewpi n KA .IhmnM 91it16A mwW 0 P60a Ans" 16.yyirae. Inc Paer A naly9Cn 6erYleer, is- Pa6. A Mal runt e9rN4.6, 1n6. PauAmLytleflHrvlur,ln<- ❑❑pp��,,��II ++ -ace1171Al lri[�1' 20e Earl Mndew R.6e • lr A 7Tj5 Rrv.rW9 Pr. p6pp urc9�Aw Su4 +W � Eorn NC 272E! AanaMa, NC 2eecm Hun�r.n1.. WC 7evya j 336Nd73 097t let 04a1 M 17p4lm 9097 ANALYTICAL RESULTS Pt.J6ct: SURRY CLOSED -MT AIRY(UIC) Pace ProJed No.: 92119680 Bamplr. 1AW19 Lab IO: 62119E60006 Co6ecled: 05/30112 14-a6 ReceNed• 06A1f 12 13:40 Ma"i Nhtar Rapoft Param.len Results uMb Urni him OE Preperad Analyzed CAS 00. 0"1 6010 ICP Oro tfwater AnalyLcal MRIhod: EPA 501 D Ptobra0nn Method; EPA 3010 ,gnU-ony ND uyL 6.0 5.0 1 OW11210-00 06VN 120117 7440-39-0 Araamc NO ugA 10.a 5.0 1 OWV1210:00 0W0211201117 6arlum 35.7J upL 100 5-0 1 ;""11-2 VA"1210�00 OLWJ120127 440-39.1 aarylNum NO uy4 1-0 1.0 1 QWV12 191DO OEM 12 CI:27 74404t•7 Csdrf9um NO gIL 1.0 1.9 1 0610111110,00 06f971120127 744043.9 Chromium NO uyL 10,0 5.0 1 0Bl A210;00 06MV12a1:27 744047.3 C.ba l ND uyL 10.0 5.0 1 OWO 1121"0 06A2l120127 7440.41i copps. NO UWL 10.E 5.4 1 OW112 1000 W=12 0117 7440-504 Law! NO UQ& 10A 5.0 1 OM11121"0 06POW20127 7439.92.1 NId�N NO WrL 50-0 5.0 1 ONI1210,09 OW0211201:21 1440-Q4 Selenium NO uyL 10-0 10.0 1 0610111210-00 06r021120127 778249.2 Sil-r ND vD+L 10-0 5.0 1 04AIM21090 O64171'120127 7e40-V-4 Thsipum NO uyL 5-5 5-1 1 061011210-00 011MV1201IT 7440.2E-0 Tln NO k, L 100 5.0 1 MV1210: 0 0em27120127 7440.41-5 Veneta- NO uyL 25-0 S.0 1 in"IA2 Iin:O 01WOVI20 t'27 7440-62.2 bmc NO upO. 100 10.0 1 MIN210'00 06=1261:27 7440.66-6 7470 M rwlry Amdydcel Metnod EPA 7470 Pr epve9cn M.t%k EPA 7470 Merwry ND VOL 020 0.10 1 06MIF$2 $2:10 0W02J12 1720 7439.974 a2E0 M8V Low Level 1.andN11 AnSOCOr MoMod: EPA 62E0 Acelone NO ugfL 100 22 1 06MV2 023 6744.1 Acelonlhlle NO vgfL SS.O 22 1 OBl05f120313 76.0E-0 Aanlaln NO upfL $3.0 1.1 1 OWY$20323 107-02.6 Am"Iris NO uplL 200 19 1 06 W1201'23 107.13.1 Ally chloride NO up', 10.0 1.5 1 DO W120323 107.06.1 8-n - NO upL 1.0 0.25 1 0=51120323 71-43.1 131owcnlorom inane ND uyL 1.0 0.17 1 0610Sf129373 14-91-5 &omo4cnlor9m9ifla" NO uyL 1,0 0,1E 1 OWW120323 7S-27.4 &amo10fm NO uyL 3.0 026 1 06f0511203-23 75.25.2 &omomenena NO vy1 10.0 029 1 DIUD51120323 74-61-9 2•5ulen.ne iMEKI ND ug1L 100 0.96 1 0610502 0123 76.93.3 Carbon ashAds NO uyL 100 12 1 06105M 21*23 75.154 Cafbon Ie6adlroride ND uyL 1.0 0.25 1 04MWI2 0323 56-23-$ Lnlafobeazene NO uyL 3.0 0.23 1 061061120323 106.90-7 Cmat"ufans NO upL 10.0 0.54 1 I WOMW12 03;23 75-0 3 Chloralorm NO upL 5.0 0,14 1 08NS1120323 67.6E-3 Chiaromethwo NO ug1L 1.0 0.1t 1 6E1051120123 74-97.3 ChiorOprene NO ugR 20.0 027 1 0WNI203:23 125.99.6 1,2•0Eromo•3•CM.roQr.psns NO uyL 13-0 25 1 06AS7120323 96.12-6 Dlbromoch1womethene NO uyL 3.0 0.21 1 06AW120323 12446.1 1 2-OR3toM0eY1a6a (E061 NO uWL 1.0 027 1 06AW 12 0323 106.934 QibrP rnethane NO uyL 10,0 0.21 1 D& W$203,23 74.95.3 12. Okhlw.banesne NO uyL 5,0 0.30 1 0610511a 023 95-W1 113.01mtorpbsnzen6 NO uyL 5.0 024 1 0"W120 21 641-73-1 1,4.DkhWrohenzene ND ug1L 1-0 0.33 1 09705l120323 106.4E-7 Dale: 06+5412012 01;36 PM REPORT OF LABORATORY ANALYSIS Page 27 of 55 M. r.pw1 N.r -q hm r.pfe4rrt erprpin M. w ftw 9ra "Mn.eaa.nt of Pap A WO w B.M.aA Inc tl ❑��} i j PooAn■ylwrl efrWrrl, I". P... An,ryuc.i f.rrtu r, In I aCBAr JytrC3+• 206E,et M..d ReW-SWt.A 2V Rmumdm 01 {136=3 AR21 'amj s4-lire ANALYTICAL RESULTS Propld: 5LRRY CLOSED - MT AIRY (VIO) PrCe Prut.cr Na. 92119550 Pee. AnYyewt furl-e, In �p �/�� A.-AMtyMc t 1arvlass, Irlr. pie. AnNy9-1 WroIN1. kte. WOO N yA". Srw 100 �apmpic81 • Ms Featy etdmw Read - Svee A 2226 R\...m.Or wr.Mw+3m. VC 2k071 Ldw..M 2721e Ammer**. Nc 21104 (1pllixlS•f0px Ir jaaa1 2541921 jarm O-7m ANALYTICAL RESULTS Pmoct: SVRRY CLOSES - MT AIRY (VIC) P.CO Prvleet No.921196ao Sample; MW-It Pfrermlers 1.0 IL1: 4211566000E Resuef VnM Gslected: 0SIM 12 14:05 R.CHyed: 05131112 13:40 MmbN: VYMter Report tlrnll MOL or Prepeled Ans"Ci CAS No ❑uml 62e0 M11V Low Lfyel LWWIII Ao OW41 M.tho j: EPA E260 'r , 1.4•Oichlwo•2bulen. NO oWL 100 1-0 1 O6l051T203:23 110.57-4 O.M., pdfl v "eln.ne NO uo1L 5.0 021 1 06MU$2 07'27 7571.E 1,1-Olchlay.ln.nr I.6J uVL 5,0 032 1 04VOV1203,23 75.34.3 1,2.Okhlprselnfne NO uofL to 0.12 1 06105132 0313 1074*2 1."Ichivr-then. NO uS(L 5.0 0.0E 1 W0-Vt2 03:23 75.35.4 cn-1,2.OoL.t"thfm 10i uyn. 5.0 O.A 1 06MU120323 155-N-2 tr W 1.7-C.chlmvelh. NO ug1L 5A 0.49 1 Q`MVI20323 156-M.5 5,2-71chlwvpr.prne NO uoh 1.0 027 1 06+OS1t20313 7"7.5 1.7.Okhloroplopfne NO uy1 1.0 0.21 1 06105112 0323 142.25.11 2;•OIchI.awopfn. NO u21, I5.0 Ala 1 015," 20323 594-20.7 1,1-0109-wopau6 NO ug& 5.0 0.49 1 091OV1203:23 561.56.E df• 1.3.01chtat oprsp.m NO uIVL 10 0.$3 1 061051120773 t000t-01-5 v.na.t,]-OIChlvroprapene NO OWL 1.0 029 1 0610S1120313 1ONI-02-1 Eft1bencene NA up'r. 1.0 0.30 1 OMP1203'23 10041-4 Ethyl mflheuytela NO ja 10.0 0.20 I 06W12 0033 97-612 H.eeWvro-t.]-Mul.dfvne NO uo1L 10.0 0.71 I 0610511203:23 67-MI 2-H..--. NO uprL 500 645 1 0610511203,23 691.7645 IOdomea.ena NO ugfl 10-0 O SP I 061p5112 03-23 74.66A ewMmmve NO OWL 100 35-0 1 0865012 03-23 7e-611 Mvthecrylonl0ll. NO upR too 0.95 1 0611511203-23 126.96.7 M.Ihpfns ✓ wwm. NO up1L 1-0 0.07 1 06O5112 03:23 75494 Methp mflhmapfm NO uolL 30-0 I-0 1 06105/12 0317 M624 4-Me9g4-2�.nt, wn. tMI3K) NO vyL 105 033 1 WS012 03,23 109.10-1 hf4phtmlfnf NO uVL 10.0 024 1 OWWO12 0323 01-20-5 Proplpnlb6e NO uprL 150 36 1 0610611203T3 10 -12.0 Styrene NO v01L 1-0 02E 1 06NN120323 10042.5 1, T,I,2•T%tmhrw0fat Sol NO u006 S,0 0-2s 1 QE705l120323 630.20-6 1.1,2.2-TW mWor"th A.0 NO up1L 3-a 4140 1 OE1051111032.3 72.14-5 TebaChls7wslans NO OWL 1.0 0.46 1 06105112 03-23 121.15-4 TaPudma NO uA I a ll.26 1 061051t2 023 106.6E-3 1 ,2,4•Tnehwobon2M. NO u9R 10.9 0.35 I D15*51120323 12042.1 l,l,t-Trwh=srihmm NO WL 1-0 0-4a 1 0616511203:23 71.5u 1,1.2-TnchlON61h So. NO uplL I O 29 1 961 & 2 0313 79.00.5 Trlchtwom*lenf NO uyL 10 047 1 061051110323 72-01-0 TrklNereAllorOmsClMe NO uprL 1 0 0.20 1 0E105112 03:23 73.69-4 1 ,2,]•TriCllfornprepvtf %0 UWL 10 0.41 t 0610571203:2.1 *11.4 1.w .C.t.10 NO uglL 50-0 0.35 1 06103112 03-23 106-06.4 VMOCNWM. NO'WL 1-0 002 1 OWO5M20323 75.01.4 Xpenf {Tots¢ NO uQfL 5-0 0.6E 1 0010502 03:23 1330-20-7r SWrep.lee Aaamo l.mbenrene(5) 467 % 70-130 1 061051520373 450.00.4 Lrhro puwnmmlh.nf(5) 101 % 70-130 1 061051120320 1a66,434 17-OlrJdixvflhana•d4{SI IV % 14.130 1 06l051T203:23 17060.07.0 T0lueae•d6 (S) 109 94 70-110 1 09/05/12 03.23 2017.26.5 Mat.: 00114020 1201:36 PM REPORT OF LABORATORY ANALYSIS P.u. 26 crs5 7l..mm"sho net M Impre6u-f, m al n AA. -r-A IM vnlrre MP,am 0 $- - why w Sa""I. hk P.ss Analyawl *.Mess, me. WOO t46e6x An. Fur 1OO Md Swdd.. NC'NOlk sample: MW-19 LabID: 9211*660006 C.Hectsa- 0573N 12 14:15S R.ea ved: 091111T2 $140 MAMIk: Vyltul Report Parsmelem Results LMNk Limit MOL OF Plepsrea Amiyxe6 CAS No- Ouk1 N208 Atkallnky Arlalylkol M.Otvd: SM 2320E Atk.Lnity, Tow 6f Ca CO3 1*a00Ga Iwo 1000 I Ofmtl2If, :40 62108 200, 6 day Ah elyticel Method: SM 52109 EQO, S dey NO utpL 2000 2WO I 0&01112 09 45 06+06117 09:44 30O.01C An1vn. 26 O.ye Analylkal McNmd- EPA 500.0 SuIMI. 2120J uglL 230000 lava I 067801120233 1460I MS 4600 Chlvndf AhmMical Method. SM 4500•CI-E Chl.dde 261a vWL 1000 $000 1 M010?2 0923 166*7.X 8 E1108 TOC Anmlylkal Method. SM 5310E Tvtml Oromhl0 G.rhon NO uo7L 1000 1000 1 Mit2lt2 16.4t 744014.Q D.I. 06014a012 01.3E PM REPORT 4F LABORATORY ANALYSIS Tr.t re.Ml .h v -1 e. mgvd4a. M-e1 n A. Mrftl"wrlrlmt scot of Pace Aomrleert SuYkam. In[ Poo* 29 a155 • Pau Arvdyo.al a.Mt.r, In¢. Pea. An*"W 1pile.f, In¢, Pate AnNy9ui 8-loo r• In[- '/,^/^/^■ � P... AnYyNal SaMa.r, In.. Poe&Anri7dleal IMI"s, I- Pave Analy0cal aamb m. lne. aceAr�alytical 205 Ea.1 N.dw R¢.d - 5-. A 2225 R--la G 9eW X.�c.y an. 5- 100 �I .., Qyjf faa� 2w E..t Morro +r R¢ad - 5. A 2226 Rlra .41 90W % , Iw. 5w 1 W �ayyr� Edon, NC 2129E ANe ft RC 7eao4 .nr14W., NC 2907E y m. id.n- NC 172M AM."* Iw 2660. Mmwwl NC MO1e @3e16n-mu, [62e)754•+1 YO [704*759092 P36f623E921 (9291251.717e ryeJ4i5.9pQ7 ANALYTICAL RESULTS ANALYTICAL RESULTS Prolecl SORRY CLOSED - MT AIRY (U IC) Pr9jec7: SURRY CLOSED - MT AIRY (UIC) Pace PrvJecf No.. 02119680 Pece Project No-; 927T9660 Sr11pN: MW16 Ldb1D: 12111680009 Collected. 05730/12 +6;05 RecaNad: OSMIJ1213:40 Maw; Valar SAMPia: MW-16 Lab ID: H119460001 C49ectad: DSr3011216:05 Re Ived 05Yu I j 12 114D Mob- Haler Report Repoli P.ram.10. R. W4 Lh11ta LIPkK RNOL OF Pnpand Analyzed CAS No. Quel P-Melera Rewlt. Urdu Lima MOL OF Prep.ed Analyzed CAS No Ouu 00111 ICP 0roundwaur Pnalylwal MethodEPA 6010 Preppauan McOm L EPA 3010 6260 M6V Law Lowl LandNO Ans"cal M91hod: EPA 6260 AnpmOy ND uVL 6.0 5.0 1 Mill 210, 00 06M211201:307440•3&0 tr.n.-1,4-01Woro-2-0ulene NO JOWL IDO 1.0 t WJ3,1221-34 1101-57-8 Amme NO UWL Iola 5.0 1 001 Ill210;10 0SWI201:30 7440.3E-7 dmloloNEuwomethene N13 JOWL 6.0 021 1 0"W:221:34 75.71-9 9.ium 36-61 JOWL too S.D 1 D6M11121 D:0D 06M2712 01;30 7446.393 t I•DICHW-1hene 13,1 up4 5.0 032 1 06MY22174 75.143 BelynWm NO Vt 1,O 1.0 1 06M111210:00 W02112 ot:30 744041.7 12-Okfi:w. [h.nA 0,73d JOWL 1-0 0-12 1 06M31f221-34 lo7-062 Cedmlum NO JOWL 1.0 lA 1 06M11121D;pD 0Nr02r+205:30 7440.43-9 1,1-Dichlwneihene ND Vat 5-0 0.56 1 OWOW1221:34 75-354 Chr.m¢rm NO JOWL 10.0 5.0 1 06M1 f1210'OD 06M211201: XI 7440473 d.-1.2-Dkhloroelnene a6.4 u0% S.0 0.11 I 0610Y 1221:34 156.59-2 Cohmll NO uWL $0.0 5.0 t o6N11t2 WAD 06M211201;30 7440-4" u.n..1,2.p1d11vraama n e NO JOWL 50 0.49 1 Domw1221;74 156450.6 Copper NO uWL 10.0 5,0 1 0amil$1 0;00 0&=1201:30 744D404 1,2-DMNwopropene NO u9R 110 0.27 1 OSM311221:34 71147.5 Lead NO VA 11.1 5.0 5 Ill"I'21DA0 ISM;2 D1:30 1411112.1 1,1-OlcNwopl.pen. NO u91L 1-0 D.24 I 06RY 1221:34 142.26.9 rLcllef RD VOL SO,D 5.0 1 06M11121O-DD 06r02z1201:70 744D.02-0 2.2.0+ hlwopmp.na NO u9A. 16.0 O.tD 1 D6Mldi221:14 59440.7 3 1nlum NO upR f0.a Iola 1 ISM 1112 f0A0 06002H2 O1:30 776249.2 1,1-01ch1oroprop.n4 NO ugrL 5.0 D. 7 06MY1221;34 543-5" SIN. NO u91L to it So 1 OOMII1210:00 06102J 1201;30 Za.22i ue-1,3.01ehloropropene NO JOWL i,p 0." 1 am, 22,134 f0061-013 ThelNum ND JOWL 5.5 5A 1 06M111210.00 06AM1201:3a 7440-21-0 vane•1.3-DlWoaopapene NO uWL 1.p 0,$0 1 05MM122,;34 f006]-02-5 Tin ND JOWL 10D 5-0 I G6rOs7121DAD 06M01f201;30 7410•Sl-5 Ethybanz.n. NO uWL 1.0 0.39 1 01 1221A4 100414 vamch.rm NO JOWL 25-0 5-0 1 a"7112 10±H D&O 2 01:30 744042.2 Ethyl MMncrylele NR uW4 1 D.0 0.20 1 DWW$Z 2]:34 17d0.2 21nc NO JOWL 10.0 10.0 I OW1112 IM 06M211I 01:30 7440464 Hexachiwr 1,34E tadl.na NO nWl 10.0 0.71 1 D MWIZ 21:34 47.4E-3 244.xwn o NO uDeL 50.0 0.4E I 0"W1,2 21:334 S91.7e-5 7474 Marcu ry Afiaff41Ce1 Method: EPA 7470 P1ap.alon Method EPA 717p lodamelhme ND JOWL 10.0 0.32 I OW03z122f-34 74.564 Mercury No ua& 0-20 DAD i NMI IR:10 059211212'12 743W-4 Nowl.nN No uWL 100 35.0 1 OBIOY 1221-34 M8361 Mellatrylorl*V0 ND upt 100 0.93 I 064341221:364 720.98.7 0200 MSY Low L6rel LwidlW AnmWifl Method: EPA 3260 Me thylarb ChMnde NO JOWL 1 A 0.87 i OW30 127;34 75-00.2 Ac.lw, NO VOL 100 2.2 f 0610Y12 I1;34 41-"-1 Me thyl metnecrylate ND uWL 30.E 2.0 J. O6M011221:34 8042.6 AC9torobI4 NO uarL 55.0 2I + 0493112 I1:34 754" 4-M4thyI.2�enl.npn4 (M191q No JOWL Too 0.33 i DEM3112 21 34 +01lM-3 A-wP NO JOWL 53.0 1.6 + 06,0E 1221:34 107-014 Naphth.l.n. NO JOWL 10.0 Q-T4 i D61OL5221:34 91-20-3 AerylonJoNo NO uWL, 20o 1-9 1 D6MY12 21:34 tOT•13-1 Pr000n109e NO JOWL 130 1-6 1 MY12 21:34 507.12.0 AIM ehlende NO JOWL 10.0 1.5 1 06N3r12 21134 $07.05-1 Styrene NO uVL 1S 025 1 MM311271.34 100-42-5 Banana 2.3 upn- +-D tl35 1 OBMY122134 7l-4]•2 1.1.1,2-Te9.Wwoaoien. NO JOWL i-0 0.33 I DISAW 22,.'l 63D-20-6 SromocnlmemeNene ND JOWL 3.0 1.17 1 DIRMW s22s:34 74-p7-,5 1,5,2,2-Tatrerl4.oelh.nv NO JOWL S.Q 0-4o I 06MY1221�34 79.34.5 Brvmadlpll-ovnmh.ne No.04, 110 036 1 061031+224:34 76.274 Tetr.dllwoeplen. 1.6 JOWL 7,0 D.44 1 D49371221;14 +27.144 Sf9m0fe1m NO u9n, 3,0 0.26 1 06MY122$54 75.25.2 Toluene No JOWL I.0 D2E 1 omwil2211 10"& fkom9me914r14 HD u9AL 1D.0 D30 1 06MY1221134 744" 1,24.Trlchloroeepiane ND JOWL 50.0 0.35 1 C&SWI221:34 12042.1 2-But6none WENT NO up1L 10p 0-9fl i 06107112 21:34 7E•9Y3 1.1.1-TrkhiwP.then, ND VWL 1,0 0.4E 7 OL40V 2 21:Se T1-533 Carhop d.dld. ND JOWL 100 12 1 06703ry2 21:34 75-15-0 1,12-Ttichl.oeln@no ND JOWL 1.0 029 1 O6MY72 21'34 79-00.5 Ce10on Ie1r.WwMe No JOWL $.0 0-25 7 06MV12 21:34 56-255 Tr h!w"th.ne oA JOWL 1,0 0-47 1 away 1Ili 131 79•ol•a Cnlombenrene 2," JOWL 3.0 0.23 1 o6M3f1221:34 196.90-7 Tdchlwo6uar om4mene NO jr.JO 1-0 020 1 OBMYl221:34 75414 Chwroethane NO JOWL 10-9 9.54 1 DEM01f1221:34 75.00.3 1,2.3-Trlchl.eprop-0 NO JOWL 1-0 0,41 1 o6M3f7221-34 "A" CMorolwm NO VWL 5,a 0-14 1 06M314 21:34 6746.3 Ynyi.c.lefe NO JOWL 60-0 0-35 1 o"W12 21 34 106-05-4 ChiDm"ih.n. NO uyi 1.0 0-11 1 MM311221:34 74-91.3 vinyl NO JOWL 1A 0,62 t D6ML 1221;34 75-014 Chlofopre ND upk 20.0 D17 1 041D31+I 21;34 IM10 6 Xylene IT0100 NJ) JOWL 5.0 o.66 7 MM3112 21:54 1330-20.7 12,Dbtomo-3• ddwapropone tic ug& 13.0 2-5 1 OW311221.14 96.12.E S-y.f.. 4.8roltu9uuoaanzene [SJ 9E % TD•430 1 06MY1221 �4 46p-0pJ Or6r.nachlaramelh.na No JOWL 3.0 021 I 069Y1225:34 1244E-1 Oihrpmo9voromelhene [Si 107 % 7D•130 1 06MY1221�3a 1666.53.7 +,2-Obl'amP.th.nr IEoB] ND JOWL 1.0 D.27 I D610Y122t:34 f06.93.4 12-Olpllvroem.na-04{s) $071E 70. 1 0693r1227;34 17060.07.0 DlNom Ihan9 NO uWL 10.0 0.21 1 061(3f12204 74.95-5 Toeu.n a-d6IS) lot % 70-130 1 MY12 It:74 2077.2E-5 1,2-Dlchloro6anzar+a NO u0fL SA 0,30 1 OSM311221,34 95.50.1 1,3•Dlehlmod"n- NO uWL 5.O 0.24 t 06 x1221;3A 641.73-1 I+•Olchtwobwz4ne 44 ug& 1.0 0-33 1 06MW 1221:U 106-46-7 0418, De mol201.34 pM REPO RT OF LABORATORY ANALYSIS Page 3D 9f 15 D.I.: 0611412012 DIM PM REPORT OF LA BORATC RY ANALYSIS Pape 31 a155 T1ir "Pal MA pat at r pledrsae, -pi n %A. TNe r.p¢d ch.1 np1 M n .d-d..a c.Pt n ILA. .laleur el. waan e...r1tof V-An 4*W E.Mpe. I- ew..1 T. w t1 eanwnl.l k.re .uw:yvr,JO S•rvlp. I- a Pau AnYytleal SaWcom, Mr. Pace AmalyVerl laMC4A 1nr- Pau Aa.lyaerl a.lylw., Inn. ceMalytrCa! 20a Eau k%.auw Road - Swe A 2225 RN.rad. Or. 060016neq Aae. 9ullm Weie4ar �„ Ed— HC 27266 AaneHle, NC 2660, 1"%fwAe, NC 26076 (13Eha238021 (42k175441Te (V4075� ANALYTICAL. RESULTS Propel, $URRY CLOSED - MT AIRY MCI Psas Ploprt No.: 9711%60 9..mMr: ag7.1a Lab 10: a2119660006 CamaMed! 05 W1216:05 ReClIwed: 9513,11213-40 Marlx Wine, Report Pummelefm fc.10. Hold Li" MUL DF Prepared An.ryaad GAS Hp ❑UN 2376E Alkallnny Anmryllem Molnod: Sµ 2120E Alkmmndy, Tolml as CoCO3 54700 �pk 1000 IIW 1 06MI2 16.40 $2100 BOO, 5 day AnAlytlG•e1 M-mad' SM 52108 Bon. 8d.y No nWL 2000 2000 1 OWII121a:41 00fW12 WAS 309.0IC Anlcnm 22 Pays Anatyt0ml Monad: EPA 1661 Sabers NO VA 250000 2000 1 061MI202:46 14606.79.E AS00 Chloride Analyllcml Method: SM 4500•CFE C1.10na. IMW port 1000 1000 r "MI209-25 16aa7.00-6 33100 TOC Analyl—I M.1hotr SM %31 OS Toler Oly.mc C mrhn n ND ugeL Ian* 1000 1 06r1221218:51 744044-0 aceRna�trcale Palm Anmfocm aaMrer, try. �7 Earl Mader Remo l A Pao#Anelyaai meyYiM4, Inc. ?ri Pnenw Dr A... An.lyarc l Serylpr, Inn. 9699 Rv,orr 9wr. 100 Ed.n,NC2I766 Ash—rrL:Nii }WnWWW..NC2Bara [03e3a77d97h 162p254•7176 7041a754m? QUALITY CONTROL DATA ProlerL SURAY CLOSED - W AIRY IUC! Para ProJect Nc . 92119680 13C natch. MERPJ4263 An.",. klelned- EPA 7470 CC Batch MWad: EPA 7470 An.lyns Defnlpmon: 7470 Mercury Assorial ad LAO Somplem. 92, 19650001. 92 t I S660002, 621196a0001, 92110680004. 921196CM5, 92 SI 0660006. 9211966OD07, 9211%a0006, 92i19660009 METHOD EL1WK 7714S1 Malnx: Veatar Aemodated Lab Samplek: 9211%60001, 1[2 11 06000w. 92119a60003, 911t%m0004, 02119aaOW5, 02118660006, 92119660007, 92119560o01, R2119660002 Blank R4wwo P... el., UIh4a Reuel Lrm11 AnerYsed DWktlels Memlry uprL NO 0.20 mto 1 r 1211199 LABORATORY CONTROL SAMPLE. 771492 Splke LCS LCS %Rec Pat.meler vnma COW RtWll -A Re LJrr6l. quellfem Mercwy uyL 2-5 22 a9 0420 MATRIX SPIKE a k1ATR1%SPIKE DUPLICATE: 771493 771494 Ms MSO 921t9644002 Sake Splits ms MSO MS MSO %Rat Mm. Pevameter unitm Result Cone- Cane, R4WR Rawl( %R4a %Red Unwirm RPD RPD Owl mercwy volt 0.103 2-5 25 1.5 1.6 59 5e 75.125 7 25 kl1 bake: 061fAg01201�36 PM R E POR T OF LA BORATORY A NALY Si S Pape]4 n155 Dole 06r14f20f20116PM R E P ORT 0 F LASORATO RY A NA LYS t S P.0a 31 Pf 75 w. .[c^ N.1 n . •.proeyr.d.. N ^'J1. TNn r.Pon Ymr net me n�d-Ad .. aP$ M rK —,-ten _—, .r P.-• Lr— 3.,—, iT -1-1 M. -ma rvn .t I.. Arr11 1 ln—. rr. rn Pa.r4rni51.ECau..M, H4Cda,lMy P.A-40 ul Asm,"1. "1 Pau Anal ytul a.NI c.., n.. ERA u 'tical 295 R....M0, OKG ,A. $Out0 C272" a . H 2MW --w—m Nc 2m76 + I]7ai923 ae]+ [152A1234.717e IrD.la7'ra DUALITY CONTROL DATA Proraet. SDRRY CLOSED - MT AIRY {UIC) Pace Pwlaol No.: 12179660 QC Balch; MPRPI10772 Anaiyaie Moumd: EPA 6070 OC Belch MWwd: EPA 3010 AnaryaN Dncdplon: 6010 MET NC Orouedrratmr Aaaccaled Leh Ssenwee: 927196600D7,921+9660002, 92119660007, 92st9660004,927+9860005, 9277968D006, 92119660007, 1121 IN mom, 92119660009 METNODSLANN 771426 Matrix: nhnr A46-Im.d Lan So mpkIj: 071596600D I, post 9660002, 92119e60003. 921196e0DO4, 0211"be"$. 92119650006, "I IM60D07. 921 t1860006, 90119660001 Blank Reponing PYemeter unea Raeull LIm11 Andpod Oua99srs Ardlmony uyL ND 45.0 Oelo2112 00-30 AEaerlc uyL ND 10.0 D6102A2 t4 D2 Barium W24 ND IDD o610215206:36 6aryalum uyL ND SA MM2112 DD3a Cadmium uyL ND 1.0 IDINO 12 D0;36 Chromium uyL NO 10.0 06102/12 00,36 Coball uyL ND IO,D Oed071120D;35 Copper uyL ND IDA o&V2r1200:36 Lead uyL NO 7D.0 05MV12 DO:35 Nkkel uyL ND 50.0 0610211200136 Selenium uyL ND 1D,0 06AIy1200139 Sorer uyL ND 10,0 o6R2j1200.36 Thawm uyL No 5.5 06102112 DI Tun uyL NO 100 HIDE 1200136 V-040m uyL ND 25.0 Oemo o1200:36 Z,c uyL NO 10.0 WM2152 00:35 LABORATORY CONTROL SAMPLE' 771427 parmeep7ar Mlle Antimony uDfL Am— uyL 5.rw vyl Beryllum uyL Cadmium uyL Chromium uyL Coba6 uyL Copper uyL Load uyL N.cke1 ug4 Seionum uyL Sher uyL Thallhlm uyL Tk+ uyL Vmnpoh uyL 5nc uyL Spike LCS LCS % Rea Cone. RasiAl %Ree umlpl o+ul6an SOO 469 94 90-120 Soo 445 97 50-120 500 474 95 W120 500 470 94 90.12D 500 473 15 60•i20 500 409 94 60-120 500 464 94 SO420 5m 476 95 20-120 SOO 469 94 10.129 Soo 470 94 00.120 5O0 466 93 W120 250 239 95 - W12D 500 459 92 W,20 500 460 13 6D.120 500 475 15 50.120 500 461 92 60-120 Dale: 06r140701201.36 PM R EP O RT OF LABORATO RY A NA LYSI S p.0e 34 or 55 ywa npm wt-1anp k—d, .ilPwh U. N+A rip—Nncs tar P.m After" 6aafts. lc P.m A maryd.al e. rri.ff, Inc. 9— A miy9.al lamicef,+Re. P..a An.ly6.a15.Mae, MR alyti' a�eAria)yficai 30� E.. W.dp Row • SuP.A 77Y Rnfr.d. Or eaD6 6 s.7 W. SuN 1DD . .�n. mf Ed.n. NL 272Ag MWR.. NL 2aea4 .Miwllaii., NC 26p7p I33eia212G]+ Ipia126{.711a 170410764012 QUALITY CONTROL DATA Prq.ci BURRY CLOSED -k1T AIRY ILNC] Pao. Prmpm No.: 921196e0 MATRIX SPIKE SAMPLE' 771414 92119670QDI Spike MS MS %Rea Pmram lef Unim RnWI Corr. ReaWl %Rae 1-1mim O uall" AnummW uyL NO Soo 472 94 75.M Amordc uyL NO 500 463 99 75-125 Barium uyL T1.1J Soo 4" 94 75125 Baryllpm uyL NO 50D 473 95 75.125 0- 1 ., m uyL NO 500 407 93 75.125 Chromium uyL ND Soo 469 94 7!l- 75 Caha6 uyL NO 590 464 9] 75-125 C.Pppr uyL NO 500 461 Be 75.125 Lepl uyL NO 600 451 Be M126 Nickel up+l No SOO 463 97 75-125 Salena2m uyL ND 500 456 12 7S•126 Sorer uyL NO 250 239 075.125 Thmlllum uyL ND 50044 59 is-'25 Tin uyL NO 500 470 94 75.125 YallooN uyL NO AN 477 96 75.125 tune uyL ND SOB 401 91 75.125 SAMPLE DUPLICATE: 771429 9211MOMT 0.0 Yaa P.rrlmelar U,,Af Result RmIt RPD RFD Duammo Atwn y uyL NO NO 25 Ara.Na uyL NO NO 25 Raruum uyL Z2 2J 21.11 4 25 Berowm uyL NO NO 25 Cadmium uyL ND ND 25 ChrorNum uyL NO NO 25 Fohme uyL ND NO 25 Capper uyl NO NO 25 Lead qVL NO ND 25 Nrksr uyL NO NO 25 S.lanlum uyL ND ND 25 Sorer uyL N❑ ND 25 Tlnlnum uyL NO NO a Tin uyL ND NO 25 Vmnmdwm uyL ND NO 25 23na uyL ND IND 25 Dan: 0611412012 61:36 PM REPORT OF LABORATORY ANALY5IS T74. rewn.n.r -1 be rep.oanud,.awpl h PA, .t"C . "ftY ean. N p— Ar I"CAl 50-1, IN. Page 35 010 • Paps MWypoal l "-. pit- Peer AntlAo? auvlg4, 06 Paw AnelylNel4 "v " I- a�eRrr��ytrcal 205 Fort kl..do. Rees. Swn A n" AA-r Ov UM K-p, w. Su1e 100 yX18�, li5en. NC 2Tlea AAe ev6r. NC 2a5W Nynnrenle. NL Se0'+6 [33a1673lm- 425N5e-n 741 i20a1e759092 OLIALITY CONTROL DATA Pr Df-1 SORRY CLOSED - MT AI RY (ul r. Pen proles[ No. 92119560 or Own MSV718311 ArtmPeps Method: EDA8766 9C 94teh Method: EPA a260 AneN115 0490lp0on- MO MSV Low Level Gndaa A4.9d4red I. eh Same ka 921t96a0001, 92f79Be0002, 927199e0D0], 92110660004, 921196e000S, 9211IM0009, 921196a0007. 921196ao009 ME7NODBLANR722444 Melee MI., A4ap1A416d LAC Semple.. 921196a0001, 92119660002. 92119660003, 92119660004,92119660005-9211968000a, 92119680007, 92119a10009 Blank Repertn0 PuRmeter Chen R45u11 L1rNl Analyzed O.Wers 1,1,t.2• Toy a drlbrootnVl4 upL NO 50 06f0Y1213: 30 1.1,1-Tncnlolo:oiene dyL ND I WOW 21330 1.1.2-2•Te LF001-rpelhane VyL ND 3.0 O6r0Y1713.30 1, 1.2•Tnchlvmalh an a Vyl NO 1.0 061pN5113:30 I, f.plWproetnanr uyL 1}D 50 06103rl213.30 1,1•Dkhlproetnene NyL NO 5.0 OB1VY1213l 30 1.t-Okdllwoptopena uyL NO 5.0 0"3J1213-30 1,2,3-7ncrvaoprlrp4ne �y'L ND 1.0 96f0Y l213. 30 1,2,4-TncN& ban24n¢ uyL NO to .0 Uemw1215:30 1,2-Dlhromo•]-d+lproprp114na uyL NO 13.0 Oar0S17211.30 1,2-Dlblomoelhfib. (Cos) ri^ NO 1 0 M311213:30 I,;-Oltlllvroh4n2ane uyL ND 5.o 06103h213-10 1,2-RrpllCraelh4ne uyL NO 10 06PoY1213-10 1,-Olchlwopropana uyL NO 1.0 OEM N;213-30 1,3 Dlcniwaben=ene uyL NO 50 owad213-30 T-1•Dlcrvweptopana VWL ND t 0 06AY12IS-]0 1,4-Dlohtwobsn:ene uyL NO 1.0 ofimul213-30 2.2-DI ww-Pmpone uyL NO 150 06AY1213-30 2•Butanone (MElt1 uyL NR too 06103M 13-30 2•Nexenene uyL NO 50p D6AY12 T3130 4-Melnp•2-pemanpn. (MI BIt3 uWL ND }00 D6103f12 30 AWO" uyL NO 1 m MOM 13:30 Ac gw';btle vWL ND SSO 0610N12 t3:30 A"WAtn uyL NO 11.0 0a431121110 A,VIOD bile V;fL NO 200 06103112 13:30 A4yl chlww. uyL NO 10 ❑ Da1031t2 13 30 Benyene upL NO T 0 0643111 13 10 Brumodamamelnene uyL NO 30 0"311211:30 6rornoasnrvnmalnRnr uyL NO 1.0 DelOL12 t31D 6romvlolm VyL ND 30 oa10]712 f7:]p BrSmom.alene upL NO 10.0 OSMU1213:30 Calhun dlaldade uyL NO ly0 0emul2 13.30 Coition letrochlatde ZL NO IA M 112 1] U Chlarv0en0me uyL NO 10 0a10Y12 f1:30 Cnrorp0i14no 41, NO 10.0 06A311211: ]0 Chlurelorm uyL NO 5.0 0610Y12 71:30 ChlAremelheno uyL NO 1.0 M34121130 CNorpptene uyL NO 2015 (19muf213:30 cl:-f,2•DlChlorceln On r uyrL NO SO Oe16Y121113D 114-1,1•Qi¢hlntoprvpene uyL ND 1.0 O64.V 213:30 Di6rom chlor omelhai +.y1L NO 30 7ElAL:211:30 Data- OW1412012 01:36 PM REPORT OF LABORATORY ANALYSIS Page 3e o155 Lle:npcn:nrl nsrty # Y .-,. n" .1, Nt 1n• ~ aon$w al P:ca M rjtml Se+'nwe lbx Pee: ASYyt[aAl■e.OLc"Une.RIWyK2225 lql, Ina. Pl tr•n:lytiul Srrvleee, Inr. - aceAr�lytrcal • 303 6H FN.dew Rvla • Sinn A 227E RNe.We Or 9800 u+ncer lwe 3wi. +pn Eden, NC 02M aMerN:. NC 2fa04 N.rn4rwnt Nc 2W15 t17610TIA921 45]5yt54-7175 47D415Ti9 QUALITY CONTROL DATA "of". SORRY CLOSED • MT NRY (171C1 Pas: Projecl No-: 92111610 METHOD BLANK: 772444 Mott- waw A4.edHed Leh Sem01e.' 921196aDO01, R2119ae0002, 9211 HBD003, 921106a0004, 021194 0005. 921196a000S, 921196a0007- 921196a9007 Blank RoporN P"Orner:r 110aa 1104u6 Lint Analysed DueLMra f3mromamem.ns uyL ND 1p.0 064311213:30 77ip11w0diAydomelh4ne uy1L NO 5.D 0ar0011211.30 Earyl matnaa-&p uyL ND 10.0 O6AL1313:30 E1hylhenrano vWL NO 1.0 0a4Y127110 Nlxachlwn• 1,3 hu14dene VyL ND 100 O61 M273.30 14,"Malha" uyL NO TO.O 061030213: 30 leohulen¢I uyL NO 100 0&OY1211-]0 lAelnacryl0ndnle uyL ND 109 0a10Y1213�10 Methyl mealapry[eu uyL NO 10.0 06M31t27110 Methylene ChlCnde vWL NO 10 06rol'o 213:10 Noobv A.ne uyL NO 10.0 a"Y721'IN o'.0 nlll44 uyL NEI 456 061031Q 0:50 Slyrenm uyL NO 1.0 06AY1211:30 Totr4eNor041hen. uyL NO 1.0 O610Y72 73:30 TCkuna uyL NO 10 OBr0Y1213: 30 tran4-1.2-0IaNeloedlen. uyL ND 5A 0a1051121)'30 3rana-1,l-Olcnlorovr opene VpL NO 1.0 06r0Y1213.30 krone•l,i-dCNlprv2•bVleno uyL ND 100 06MN121130 Tnhroelhenem14n MyL NO 62113-30 Tdwouwp uyL ND .0O 1623-30 vinyl awtele uyL NO 50.0 D610YI2 13-10 Vinyl ch"a uyL NO 1.0 OW3112 1IN nyleno (101411 on NO SA De4112 13,30 y,24),hItnm1h .. 15) 1L $01 70.730 Oa4Yt21330 44komoauomben2ene (s3 1L 100 76.11D Dal0Yt2 1] 10 Dbromplucvo nalhene (Sl % 107 7D430 064Y}2 t3:30 Tolwne•da(5) % 101 70.130 06NY121240 LABORATORY CONTROL SAMPLE: 772443 Spilka LCS LOS %R" Peram4tal untie Cone Runt %Rae urtYu am"&$ 1,t,1,2•Tetrachlnree7hane upL $0 57.4 103 79-120 1,1, 1 •Trlclew"6ane uyL SO 5Is 104 70.130 I chwraethana tiWL 56 51-4 193 70-130 I2,2•Tatra S,t,2-TdvhleroelhRn4 uy1L 50 U 110 70-120 t,t-Dlchlot0e111an: NOrL 10 45.5 92 79-120 1,1-DICMw04014n5 upL So 61.6 103 70-132 t,1-Olchlmopropen: YpIL 50 ea.e 96 ill- 30 1.2,3-Tr,01* opropana uyR SO 54.7 ID9 70.170 1.a,4. Ichl 01:,en4en. uyL So 51-0 f02 10-134 1,2•Dihr0-'1-chlaroPMPwe uyL 50 53-0 L06 74110 lZ-Dibt.rn..1hkn4(EDB) U L 50 S1.S T03 70-130 1.2.OIchl&ob*U0na u00L 50 46.2 i8 70-130 1.2-Dietnlotoe0lens upL 50 514 103 70.130 Ur 061144012 01'36 PM REPO RT OF LABORATORY ANALYSIS Pope 3T 01 SS The repan eh.l net be n0.d-d,.teeµ n V- y.Wl Ahr pMW. -nrenl a1 Pee. Ane+rhgl $4ry�plr. kc ^.1//. P.ea Anal3ne al eerrl.4e, Ms, Pass A"yeemr.enHme a, Me. Pat. A-to.rl .tryl[ef, la[. • pttt AnPlraa.l ea..ttte, Inr. rya. Ar Iye[.t 6a/t ,, In, Pan Anelyeeal aerHne,1- r RLsRr�alyti�ale �3 Errr M[.mw Aeea - 5� U A 2225 RMwWa IN ON 1[- Aw 5i 1pp ■__ aceAnarytioi �'+E.rt Alea6ew ReW - Sra JV 2725 Rrewaltl. Or. W00 PM�eeY+Me 6uL 10p ... e..m.w. Eda1. NC 272a4 Asneow KC 2e604 H�nev.y4e. NC 26676 .r..yr.raram E.. 47L 2+2ea AY.e.6a. NC 26a04 Hy a*,,Na. NC M10 I j] 0234421 tPXP5�7174 y7wHisvpe2 ' i33d]a23A11Y1 (elaj2347176 716+0754yp7 QUALITY CONTROL DATA QUALITY CONTROL DATA Prajeel SURRY CLOSED - MT AIRY (LhCj Pr*cr, BURRY CLOSED - MT AIRY (u1C) P.ca Prvjepl Na-: 921i966p Paco Arvlaei Nv-: 92119660 LABORATORY CONTROL SAMPLE: 772445 LABORATORY CONTROL SAMPLE: 772445, Soho. LCS L . % Rac Spike LOS LCS % Rea PanmHfr umts Cane. Remult %Rev um1U Duamm Parmmale+ links Canc Result %Rac Lnft OuaR6er► 1,2-olddmvprvpanP up1L 50 11.4 103 70-130 Onyi @"let* uy L IOU 102 1132 W157 1,3-Okhlvrvhenaene LVL 50 16.5 97 74130 YAnyl chloride uyL 50 60-6 $02 60.130 1,]-D14mwvp wGRp -WL SO 50-4 101 70.130 Xylem [7apq uwl 15D 147 96 7W130 1,4.01d+krRp.n:env uyL 60 is-3 97 70.130 i,2.OldNoroemene-d41s} % Po 70.770 2,2•o1d11ereprvp.na uyL 50 49.5 99 66-746 +-BramoAuorvbenxena 102 TO.176 2.9ut.nvn4 (MEK) uyL 100 119 119 70.145 DR-emveW--ehane 19} % 104 70-130 2+Ie...W6 uyL 100 106 109 70-144 Toluene•da {SI % 101 70.110 4-Moth:.2•parl..(MIBR] upl. 106 1i5 "1 76740 Acetone uyL 100 P29 129 64176 Aesionialle uyL S00 $23 105 7 .. MATRIX SPIKE S MATRIX SPIKE DUPLICATE: 772446 772441 Acvleln uyL 250 252 101 70-130 MS MSO Aeryt-lue. uyL 250 265 "1 4 70.1] 91aatimm Spika SPlee MS MSo PAS MSO %Rev mu AIM chloride ZL 60 42.0 URa.ult Cwc. Cow. Reaull Result %Rea %Ric Unit RPO RPO Cual 9enlene uyL 50 49.1 98 70.1 SO uyL N0 5a 50 63,a 63.7 1p7 191r 17 '3D OPamocraore4vamana OWL SO 51.1 $w 70. 30 gantrachlprwNene uyL NO 50 SO 6a 97 70.145 "Ill": 9 30 8romodichkra tpl 1a uyL 60 61,It 10 TO.Im CrIlarBenxana 50.5 61.6 uyL NO 50 Sp,6 6I,3 101 115 70-f46 19 36 Br=mm uyL SO 63.6 107 70-136 Tauenbanxan. TWuenv % 49.1 57,Is raWL NO 50 9S 116 51 1S 30 9rvmvme7rane OWL 50 62-7 105 54.130 Tdchhrwalarta uyL NO 50 SD 53.1 63.6 m 126 sa- la 30 Carbon dlwllde uyL 50 56.QA 112 70.131 1 1128'. % f0a 1p6 m;%I 70.130 C.lbvn teCachlpridm OWL 50 55.7 11! 70.f32 11m0ethaNr.ne(-114 +-0rpm011u0f.6an7.n6{Sj % 211Will fop 102 70.130 ClOvraeentene uyL 50 49.5 99 70.130 D6x.ms-dd rOmetlrana{Sj % $05 105 70.130 CNeraeN.ne vplL 50 60.0 170 64.174 L9 Tptuena-0a 1S! % 97 96 70.170 Cnlprofum uyL 50 41.9 I00 70-130 Chlervm.dienm uyL 50 614 103 44.13D Cnlnroprena uyL 50 56.9 114 70430 d2-iM�hlapeNen. uyL 50 61.4 163 74131 pa-1,3-Dlcnupprppen► uyL s0 5]-6 107 70.130 06romecMolp .thane uyL 50 52.4 I" 70.100 pAramvmethene uyL 50 53.7 107 70.i31 Orcnlvrvdfluprvmethmne uyL 30 40-5 61 56.130 Ethyl-1h.cryl.i. uyL 50 62.1 1. 10.120 Ealyll"MOIna UA 50 50.0 100 70.130 Eea><aehlvra-I,3.6uudlene uyL 5o 56.1 112 70.130 Ivpomethane uyL 100 at.a at 49.160 .abulanol uyL 100p 1070 107 70.130 MHnacrylan4ulra uyL 500 S5S 111 70.130 Methyl ma0iauyleta uyL SO 569 1. 701-130 McOlylen. CNande uyL 50 56-6 ilJ 13.130 t0ph91alene uyL 50 50.9 102 70.138 Prppianwhle uyL 300 564 113 70-130 Styrene uyL 50 49.9 100 70-130 T.beWp4pedwne OWL 50 49.5 99 79-120 Toluene OWL S0 49.0 90 70420 u.m-1,2•IXchwra►n.n a uyL 50 SO.5 105 70.13D pan.-1,3.0cm:pmpen4 uyL 59 113.! 106 min tram-1,4•Dchluv•2 b,,I- OWL SQ 57A) 114 70.141 Tnchlorae91en. uyL 50 52.7 !05 M130 TnGhlorpiluoromathane uyL 50 54.5 i09 a2-133 D.m. DWI 441)t201:35 FPA REPORT OF LABORATORY ANA LYS 13 Pape a 016S oil. 0&14r20i2 01'30 PIM REPORT OF LABORATORY ANALYSIS Pape 39 a1 S5 rIn report rrye igtN ngoacas, taztpl n A/, TN. Mn 0M1mfi rota. r.pM"id. -04 Pn U vA.raW N w.�n eonwN er Pau N Intel Swb. tne- wawo a,e -ft, --k.r Pan Awyr Semce. m • P.HRnYytffa, aaMe.a, M[. Pa.. A nakvul ",krica., ICI• Pau ■nairdul 64nfa1, Ir1[. y1 Rom ��Rl 20.0 f aat Ma.Cuw Read - 5„�n A 2225 RNmrsomm Dr 9e00 idoomf m: Sup. tDO Leen- Ne 77700 Am$,%. NG 20moe I4N.rrhg NC 0e078 1116)621d921 152SP54.7, 70 I7W 10754m QUALITY CONTROL DATA Prol.ul SURRY CLO$ED - MT AIRY tUIC) Pale Pf.rd No: 92TIf1660 OC Batch: W.V119324 AneF7.la M.tha9 EPAS200 CC Balch Af200d. EPA6260 AANIV" D.mmiphon: 6260 MSV Law Level L.n01 Amovied L.b Semple.: 92119680006 METHOOBLANK772763 me". mler Aeea[Mlee L.h Samptel- 9211WSQD i Blanli Repwlml? Pafamern Lfnae Rawl u" AAIWzed ouGmen tr.filWrvam.n. uyL NO 1.0 0"511203:08 1,l,1•Tnthiwflmtllln. uyL NO 1 0 ONO 5112 as'08 1,1,2,2-Tmemcniorae111.nr dy1 NO 3.G 061a611203:96 1,1,2•Tacmamsth An. NyL NO 1.0 0"W1203:06 1,1-p6xnlalvr04- WWI.NO 5.0 06f05f1203,08 I,t-IXrnweeethd ne uyL NO 5,a timill 1 2 05:08 1,$-Oknlmoprovane uyL ND 5.0 OBf06f 12 03.06 1,2,}TflWvropfnp.ruf uyL NO 1.0 MIV1203:08 1.2,a•TYC6ef p9mnlrne uyL ND 10.0 06MV:213.00 1.2.Omram013-FhlpfapfaPena uyL HD 11.0 0Ims12 03:at 1,2•GMomommn. MOB) WWI. NO 1.0 0",Ul2 03:08 en 1,2•Dmhhlnrcoiene uyL ND 5.0 0N05ft20300 02,01chimoolh ne uyL NO 4.0 0df05f1203A8 5,i-0Idavrppropans uyL No 1.0 0610511203.06 1,]-0IWwflamtmr,r ffWL NO 5D 0Na5f1203A6 1,3 DIpNvfowapens uyL ND 1 0 06105f 1201A6 $A-0Icllly�benxe.lr uyL Np 1.0 0"SM203:03 2,7-Ok*Jm*pr4pene uyL ND 150 08A5f 1203.08 2•BWortanm IMEK) WWI- NO 100 OB10Sn2 01.08 2•KONene uyL ND 50.0 O=V12 03:08 a6mot 1.2•Pamanons (MIBK) uyL NO 100 081D6112 0308 Agkne udL NO 11006105112 63 08 AcetoritNr uyL ND SSA ONaSf1203: 06 Amvlaln uyL NO 33.0 MM5l1273:05 Ac,om1tr9. uyL NO 20O D610N 120309 At"allrmMe uyL ND 10.0 a6108f 1203�06 8enxenm uyL NO 10 O&DW1203A8 8rvmvmmfomemane uyL ND 1 0 O81d9f12 03.L8 Brem9dohlod 0 romimm.e uyL ND 1.0 06m,4112 D3A8 t,c_ Hm uyL ND 1.0 0W65112 a3:06 Bromomalhmne LK9L ND 10.0 06f051f203-06 Cnbv dwlid. Vt NO 100 06f0571203.01 Cvtl" tat,och,10 ma uyL NO 1.0 am!tlf 2 a3:00 ghlwrweneane uyL No 1.0 09A511203:06 CNwvemane 4WL NO 100 06f0511203-08 cm-r- uyL NO 50 06mv 1203 D8 chlo ...mmn4 uyL No 1.0 ONOS+12 a1 a6 L7rlvrvprena uyL NO 20.0 OM5112 03-00 or-1,2-LNchlorv.In.na uprl Nq 5.0 0b05f1203-06 n..1,3-DldflwpOropene uyL NO 1.0 0N6L1203.L8 Of9fPRwdlloiommatmn. uyL NO 300610NI2 O3 a8 Ofhro mammmane uyl. ND tO.O 0610311201.06 D,chimoa6uornnwman. uyL NO 5.0 a8 "] p 03-08 EM 1r: DGI 14120120 t: 36 PM REPORT OF LABORATORY ANALYSIS Tlf.-. -v,,m not he mP -d.m 0fe hW wFWl1,m-m1 arP1.Mm 08-arlfntl[e,'4 -A. Inc. 13400 40 Of SS Pala A nmlytk al H.M r, In[ Pa La Amfytla lewylaat, Ine- P.- A.0yeeal6meWavl,lnc pp ❑/�/^1p]/ n7� / I = �C Analytica�r Fgj X5 f.11 Wren. Roma � 5r[Im F 7275 R,rmrmtla ar erro0 Kiruel A+r Sfffl lOo . Aa' a nm Eden. NL l7]a6 ANafW. NL 786a4 Hen -I. NC 2IM78 [3761673d9:+ fe]8171f 11Y6 1Y6awrs9dff: QUALITY CONTROL DATA P,viect, SURRY OLDS F11-MT AI RY 1VICI Pees pmled No 1 i2119680 METHOD BLANK. 772763 Mepn vww Amcilaled Lab Semplec 9211HOOODO Pa[.meler Un4m Blank A ... dI Repod1 q Ulm An.lya.d Ouawm" E:to mem"late nVL ND MOO OM611201:06 Errylhenrons uyL NO L0 0B1051, 211"08 H.meN9ra-1,3-0uladlarn uyL NO 15.0 06ra511203:06 ledome"oriI uyL NO $0.0 06f03112413:00 1.6"10,101 uyL NO 100 06A611201.06 MeihecrylMPM14 uyL NO 100 a"&,20308 M.Ihyl m.1h.mP.1e u94 NO Wo asmst 2 03:06 MeNod- Chloode uyL NO 1.0 0"517203.08 Nmphthefmne uyL NO 10.0 0SM511203.06 Prvplanlnmd uyL NO 00r0 150 511203:08 SlyremA LIWL NO I.0 06A5/120308 TevacNproelnrne uyL NO I,0 =511203.00 T.W.- uyL NU 1.0 06 Vn(13.06 LYcm..eefenr uyL NO 5.D 08106f120308 trana.l3-DCNVZprepenk uyL NO 1.0 0610Y I20306 irma-1,4•I71CN1arP.2.9u1ene uyL ND 190 06f05N203:06 TnehWmalhma uyL NO 1,0 0MWI203:06 THcnlwolueromaI9904e uq)L NO 1.0 OMW 1203.08 Hrlyl .f:tl.1r uyL NO 55.0 GOM6112 03'08 NnyA dwoNdr uyL No 1.0 0"9112 O3A0 Koar a (Talmll uyL ND 5.5 08f05112 0108 1,2•DIChlerpeNfane-a4{5) % 102 70.130 08f05+12 pDA5 4.81amo0utlroa.n2ene (SJ h 10] 10.1]0 06r03112 Dfw6m06Y0rOme6lenr ($I % 105 03106 70-130 061051 2 p3:08 7W.8no-dS (5) % 90 70.130 a"V 12 03.06 Lf,BOMIrDRY OONTROL SAMPLE. 772764 Spike LCS LCS AL R9e Pmrommor UnNt, Cvrfe. R"YI %Ree Ufwo Qu.I16rf. 1, 1,1,2•TMdlMrf1 m61 so m uyL 50 69.2 190 70.110 1,1, I-Trichlvme wo uyL 50 a3,7 07 79A 50 1,11} Tm0moVor0 mdl one uyL 504 99 70.130 1,f,2-TfichlweeFena NyL 50 52.9 1D6 10•1 Ut ],1.O,d+lo+ne9fene uyL 50 0.6 es 70.135 1,1-0,morn491e n4 „y4 50 a5.0 90 70.132 1,1•IXr:Wwvpropene 4yL 5a 45.5 91 701-130 1,2,3•Tflehkfnyc0anr uyL 50 53.2 t06 70.130 1,2,i-Ydrhkfedenxene uyL 50 47.6 95 70.136 I ,2•LLiife6,tr•].d1lofOprapmnr uyL 50 so, f01 70.130 1,2-DWomPalhena(EDE) ufyL 0 51-1 102 M130 1,2-EkHmahenlrne uyL 30 461 92 7D1130 1,2-ptdYvfm.ih.ne uyL 50 499 94 70-130 1,2•Dlchlorepeopene uyL 50 48.6 09 70410 1,3-plcnlorvh epune uyL 50 45.9 92 70.130 1,3•01c oroytoomne uyL 50 49.2 9a M130 0614: D6fI412D12 013E PM REPORT OF LABOR ATORY ANALYSI S Pope 41 of Ss Iti. mean NM wl tlm nVcdudd, mrcmaln till. w, Tefr P,m yF,yn ewanN of Frea Maiyeni 5an.em irc p4n RnNyeul 14rvlaZ Inc. P... An41ydw1 ear 1-k Me. Pam Ams"cal 114NIO1, Inc. aceArialytical • V6 E44 a ndpw Rp4d • SC.4 A 27M I'l-on "o-. J eIIW Ktm.1 Mr Su4 1IX} 1 ... pl wniam EMn. HG T7 x88 Arp4yH4, RC 7510/ lunlrm 14, NC y10T4 iIU1033 on, IaT6175+7170 {714J6T59 QUALITY CONTROL DATA ProjeeL SURRY CLOSED - MT AIRY IVICI Pece Plojed No.: 9215%a0 LABORATORY CONTROL DAM PLE, 772794 Sp91a LCS LCS %Rac Paramaler Unite ewe. Rawlt % Rec Llmtra 01 t ,4.Olrhembanrina 09& 56 48-1 92 M130 2,2.pldilornpfopane up+L 50 37A 75 56.145 7-SWRrlena IME%} uyL 100 96.9J 99 70-145 2-Haaanona uyL 100 161 104 70-144 4.M41rry1.2•panlenane IAMBN1 uyL 100 103 101 70.$40 Acel"' upfL 100 116 11a W175 AcatuMafle ZL 500 4" 100 70-139 A —WA uyL 250 219 e4 70430 Acrplmlvae uyR 250 261 101 70.143 AM rinorldA uyL so 33,7 67 10-130 LO seniena uyL 50 40.6 Re r0-13e Stpmpdrleram4lhnn a -0& 50 u-9 90 T0.13o eromodlchlorame 0l.ne upfL So 47-6 95 To-130 Ro term uyL 50 52-2 104 70.130 Sromom*Zane uglL % 41.3 a7 W30 Carbon paullde LIVL 50 50AJ 101 70.131 Garuwl latrachl.rlde uyL 50 49.a 100 70-132 L1llorawnawe uyL 50 47.2 04 70-130 G1rp1ea51en1 uyL SO w-7 129 64.114 I'ti fum uyL 50 u.z Sa 70.130 C7eprwna0lane uprL 50 461 93 54-130 ctbxav ne uyL 0 40.5 99 7o-130 ela-1.2.Okhlim edune uyL 50 45-7 91 70-131 .1 q ,]-0IphlpoproparM 1pIL 50 a72 W 7o- 17 0 0OnrameW 16lana uyL s0 19.6 190 70-130 OErarmma571M uyL 50 50,0 160 7W 131 D1hlorod4u m 0Une uyL 50 31.0 a2 50- 130 E0171 MMOMYkA0 uyL 60 46.4 97 70-130 E01rt6ennm H9& so 47,0 96 10.130 HafacNoryl,3-huudlana np�L SO 40.4 99 70.13G lodamaMne uyL 100 79-is eo 49L160 fa961Nmol uyL 1000 1040 104 M130 MelluwMonerea 491L 500 419 96 70.130 Me"molhocryleu uyL s0 64.7 f09 7LL130 MaNane Chlwda uyL 50 50.0 100 al- $30 NWthaane -A 50 45.7 07 7G I ProplorM6ae VWL 500 520 l04 70-139 Slyr, uyL 50 46.5 97 74130 TakeW'...ane uyL 50 46,5 93 74130 Tduena upfL s4 A6-6 93 70.130 trane•1,2-Dl4nloroafirne uprL 54 14-6 90 T0.130 1anr 1,]-0lchfdopropena upR $0 41.5 99 T0.172 lane-I.A-Dlcmara-r-0uten. 01^ 50 4SAJ 92 70. Al TflchImoelhene u9& 50 49.4 99 70-130 Trichkmeaumu.n.chana uyL 50 40.1 92 62.133 " acatala uyL 1p0 as.0 85 6a-157 VInyt cnbrlde uyL 5d 43-6 e7 %-130 Xvlwt �Totall "WL 1so 139 93 70.130 , P..,r AL"rY..l 64niu r, tome tlsa A... AnNrl 9-1—, In.. Poo"AnYype41 eanrtaa, Inc. aceAr�aJyticaJ 705 E.N xrrre.w Palrt • surt. A 7333 Fq . lc. Or 9e0➢ IWr l 8� $m : FtNC 27E1e A.n.rll., MC 26104 t Iknove4. NC 21076 I11d1e23-09J1 1e2III2WI70 (744y( sv= QUALITY CONTROL DATA Protect BURRY CLOSED - MT MRY {UIC) Pace Pralsm No.: 921$0660 LABORATORY CONTROL SAMPLE: 772764 Spike LCS Les %Reg p1rlmRler Vnla 0-0 RmtA % Rev LIMN Oue9aen 5,2-0Icl4orwihene•d4 IS) % e9 7o-130 4-5rwwl4orohanxawe (61 % 103 70-130 Obnmo Mlolamee,ana ISI 95 7o-5]0 Toluane•de is) on 09 10-110 04%- O&W2012 01.3e PM REPORT OF LABORATORY ANALYSIS Pepe 42 of ss Omit 06r1u2012 01:34 PM REPORT OF LA 90RATORY ANALYSIS Pa0e 43 of 55 TNk mpRM N.1 ml p. qpn -"'4rdp1 n al. Tla nprrtW lralW nyro vd..awd I1%0. Mequl aN prlrwn t n"m el Pad Analy►ml 64— ft. Mh.ut pN "— rar...n[er F.pr Atir19[al9 —Al, Nn P.w An.lypW aerrlen, lna. P.w A-10-t Seale'1, me. Pa.. AnYyenl S.rvkef, Ina. ,001r�afa 2W4enkl..dewRe.e-Su,NA 225Rw.WW vep6Auw7Aw 6u41W C4M1. RC 21710 A wls. NC 2850e Hu-ft No 711075 (3767A73d9}, 1a75rrse•y1 Te 1704A7ra097 QUALITY CONTROL DATA PraJect BURRY CLOSED - MT AIRY (LRCI PA" Peojecl No 9211 DOW 4C Seth: VVETf21It0 Anelyals Method: SM 2376E OC Eolcn Method: SM 2720E MatylM DaavgMMr 23205Aik.9Nfy Asseaered Lab So-eprsa 22119960001, 92119660002, 12119660003, W119660004.92 t?p600005, 92 11 9680M. 02 ti 9666007, W I I%60066, 92119660009 METHOD BLANK: 773669 Mobil: YYYur Ass6Cal ad lab S. mp4al. RV% 9650001. 12119680Od2, 921$MR0607, 92119669604, 9211 M80005, 921196AD005, 9211"I=7, 92t19660006, 92119680009 E14nk Rep-un9 P06M.ter Unae Relot Llmll Analyie4 Colinas Agaknlry, Total et CeCO3 uyL NO 1000 0846712 16:a0 LABORATORY CON 7 ROL SAMPLE: 773870 BOON LCS LCS %Rec Perimeter Un9a Came. RaaWl %Rec Uml1a 001kAele A1ka9nlry, ToW u CoCO3 4(L 50000 46400 07 96.510 MATRIX SPIKE SRMPL€773A72 92113710001 $011'a MS MS %Rae PNemelef (M-Le Re.HI Con.. Rnurt %R.e Uneh OUANAees Alkok y, TWO as CeCO3 uyrL 15A mprl 50060 51400 91 MATRIX SPIKE SAMPLE: 773674 92119679005 Sp.ko MS MS %Rot Panmalar ulfus Reeull CPnP. Rewir % Rec Llrrie< Qua9eers AIAallrtlry, T81a1 as CAC03 vyL 39.1 MWL 50000 80W 92 SAMPLE DUPUCATF 773871 9211/710001 Dole Mel Pe4rr1M5r VAAa R1111691 AMA RPO RPO 040thlre AWWWry, TQW a6 CaCO3 vyL 1S.9 MQVL 15600 2 20 SAMPLE DUPLICATE T73673 921$W79005 Dup Mar P.remaler unite A.sal Feawr RPO RPD Oue9ken AlkWnly, Telal as C.= u9rL 791 myl 3L900 20 20 Dal. 000140201261.39 PM REPORT OF LA SOR ATORY A NA LYSIS PA9s 44 at 55 T.,. r.Nrl MN -I as repradu d, -pt n kAI .,eu .u..--n-.nr c1 Pic. Anr,p m-%-. iz Pat. AoWy11ta15 NLt.e. 1% Pate ANIy11r.I A""', I Ie t P a,. An.yaNt AeN1Ml, k.. //gy,pp .]....J + aLL iil �[Ti rCa+' :QS E. M..&* Mo 1 . 6uir. • 222S Fir. W..1 Yl b KVe.� Are sv I W Aanerae NC 2NO, -y r.yak NC 7A174 i I13518238v: le25 R"-11 m (70e16T}vw2 QUALITY CONTROL DATA ProJ.cl: BURRY CLOSED • MT AIRY SUICI P.W PrPJed Na-- 92119666 OC Balch: WET021056 AnsNels Method: SM 5210E OC Snch Method' 8M 5210E M.h.ls Daeerlpc- 52165 EQD• 5 day A.aOd.I ad LO S"V'49: 9211 9630061, 02119660002, 112119660003, 22T1 %AOOOL, 9211968D007- B2I I moODa METHOD BLANK, 7710D M.W.- Wale, Aesodelad Lob Sarnpraa: 92119656001, 92119600002, 9211%8000}, 4251 %6000A, 92119660007, g211966p0O6 Blank Reparlke9 P.r.meler VnA. Realel Lirtet An.lyled puak(- E00,5 low LIWL ND 2000 0610611209:45 LABORATORY CONTROL SAMPLE 771471 Spike LCS LCS % Rot Paremelee Unme Cone. POEM -A Rat LIwite Ouslinare 600, S day uyL 199WO 178000 90 114.115 SAMPLE DUPLICATE. 771472 9211 in 000e Oup Max Peromaler Wile Raalet RewN RPO RPp Ouall6en 900, 5 dry uyrL ND NO 20 O.1e: 06714I101201,36PM REPORT Or LABORATORY ANALYSIS P.6. 45 at 55 -... ro.r vae n 1 h .Pr.di.e.d.. Pl NI, ..Mu1 m. - Nn mn l or Pr_ . AmN%am S.Wwe. im P.- Rnadym j Zane.., In[. Pala Amlyeeel 6 Ink Ink ■ew Analy6en Urowk Ina, aCBAmlytiCala 206 fan M..Ccw Re.d -S.ftA YM Rm, Em DF. WWK rM. 8w 100 Eden_ wC ZTM Aenw6e, NC law .w 4wwmk NC 7a076 + IOOe16nd92r {6741234Tt 76 fr0'a1676.9092 QUALITY CONTROL DATA Raoul: SVRRY CLOSED • MT AIRY {WIC) Pua Pr.bc[ No.. 921/9660 CC Balm: WETr21062 Analysis Method: SM 52108 OC Belch Ma6wd SM S2i06 Anmyah D..alpll l: 52108 BCD, S day Awed.l.d L.b 9empka: 92119660005. 92119660006, 9211use 0009 METHOD BLANK. 771713 Matrix: Nhlor A.eodaled Leo Sarnpie.: 921196600M. 971191SUOM, 02119660009 Blank Repormg Pusmeler Une. R010 LI.NI A.Wyiad OuesAers BOO, 5 day MpL NO 2009 0670N12 11:10 LABORATORY CONTROL SAMPLE: 771714 Spore LCS LCS % "CC Poram.l.. {Jn A. CMG. A-00 %Roc LIrN4 quallAars SOD. 5 d.y vIVL 196000 176000 66 Wll $ SAMPLEDUPLICATE: 7717" 421196owl NP Mak Paw"Mr UnAA R.adll Rawri RPO RPO OummIlm BOD, S dov uglL 163 mWL 160000 0 20 • Paee A ral ytlseV.e.rla.., Ink PEE. ANlySyl %a Iaee, Ina. Pew Analytical 6.,vk-. Inc. ra q�,� ry 7'V aG'[.lUlytfYal 205 E. Waorw Awd • SUia. A 2276 Rrnrelea 0.. 9600 Ke 1 Are Sur. 100 .w Pc.reCl vr* Ed ­NC 717e6 AshvAl , NC 25Nr4 HLn%" d NC 26776 {0061625 M21 ta163764.71 T4 f70a16759092 QUALITY CONTROL DATA Prole Cr: SURRY CLOSED • MT AIRY (VC) Pace Pwj.c1 No.. 92T19660 CC Barcm: VVETJV122M A6.4*1 Method: EPA MO 0 CC 9alch Method: EPA 300.0 An. [role D.ar:ipuon: 300.0 IC Anion. AfsOaNled Lab Sanwita: 9711 H11000 I.02119660002, 92119610N3 METHOD BLANK- 771367 Motm: Wow As"alad Lan So mpl.a: 92119660001. 92119660002, 921196a0003 semi' R4penn9 Pa.maler Dne. Reaue Limn Aneiyx.d Dv.Lfi.n 50rote .%9L NO 250000 Ou01li213.42 LABORATORY CONTROL SAMPLE: 771366 SPik. LCS LCS %Roc Parsmaar Wn6e Cone. Result %Rac LN1ats OwsAels Sulwo M94- 20000 19900i 96 90-110 MATRIX SPIKE SAMPLE: 771391 92tI R'S"on Spxa WS MS %Rac .r Paemel UnMe Rem9l Cone- Rpaaf %Roc Llrlara 0ve14ere SWfua UWL ND 20000 23M 120 90410 Ml MATRIX SPIKE SAMPLE: 771474 9211984400P. sole. MS MS % Rao P.r..n.ter U." R-Ult Cont. R..ur1 % R.G Urnly Ouae6ef. Wiple 19A. NO 70000 ND 0 9o-110 M1 SAMPLEDUPWCATE: 771392 92119644%9 DUp Max Puameler Une. R.eWI RmAt RPO RPO qu.9Aera Su mto uWL ND NO 20 SAMPLE DUPLICATE: 771415 92T1W4002 OUP Ms. Pwanatu Vella Res.er Resin. FWD RPO C.-MW. SWIM. MWL NO NO 20 O.la: MO V2012 0 1. 36 PM REPORT OP LABORATORY ANALYSIS Pope 4e of SS Odle: 06f1412012 51:36 PM REPORT OF LABORATORY ANALYSIS P.R. 47 .155 Tire mWvt MY rqr ba rapmeMc.u. exwpl n W. Tlra npatNN Pn he row". d...wp1h N, .e the rr.leae wne.erat Paw Awaw S.novE. Inc. nIV%,A iM WMl.A dMW4 el Paw Afdhr r 0-0dok I- P..e Aeelydnl 6"t.a, 1-96.6 Analymal 6.i kmt. Me.Pee. Anetyoeel eeNlwa, Ine. �C 0AnaViwll 207 L4H Mnae+ Reea - S 1. 2225 Ruanae 0.. HW Ke Ame ". 100 - �' 1�d.n. NC 27M AW-114,. NC 2a104 l4unle-1.. NC 7a07a ra36a29aPn (a2at25F7tra tre41mrs4av4 QUALITY CONTROL DATA Plokcl SURRY CLOSED - MT AIRY (UIC) Pan Prated No.. 92119660 Oc emcll WETA112262 Analyers M"cd! EPA 300-0 OC Balch Malnod: EPA 300.0 Analysis Deeulpson: 300.0 IC Anyone Pssadolen Lab Semp1e6 122, 19660004, 92,10 8000S, 9211%6OW6, 02 11 961110OV.11121 I wa0006. 92, t 9660009 METMOO BLANK- 775510 Mawr Wrlw Au■del6a Lab Saner■e! ➢21f%50004-92119aA0005,➢i 119660005,92119660007, 921l96a0006, 9211 %60009 Blank Reporlrl0 Parameter U.N. A-0t Lure! Analymi Ouaet.ra Sulfala uyL NO 250000 06106112 22:W LABORATORY CONTROL SAMPLE: 775511 Spice (.CS LCS SL Rec Pmam■ter Untie COAL. Ra.utl % Rau Lu7rh OuallSer. Swwo Pyw 20000 19000J 95 K-110 MATRIX SPIKE SAMPLE 775512 92120272001 aWk6 MS MS SL Rot Paameler Units Rewit Celle• R0e161 %Ray: Limit Qwl#us S.ntale uglL 556 mpti 20DM 733000J a7•y 60-110 Me MATRIX SPIKE SAMPLE: 775516 4121UISSI005 spike MS MS %Rac Puem.tan U.N. Result Cont. A-W, %Rec Lush. Oualien Sulaltm uprL NO 20000 2t20oJ 67 90-I10 SAMPLE DUPLICATE 715615 9]120272001 Dup Ma, Pet.meta. Urma R..Wt RmA RPO RPD Qum116a•s Sutrale uWL 556 MWII, 663000J 1 20 SAMPLE DUPLICATE: 7M$5 92119661095 Due Max Pw miser Lima Ramut Rerllt RPO RPO Out N6■rs Sldlgre uWL NO NO 20 Emit; QWIAQ012 01:9 PM REPORT OF LABORATORY ANALYSIS page 46 of 55 TN. r m o,.l rcl ....M n Nu. reer.A"N M. wn..nl cr Pgce A lysc SeM a Inc Pen Anvylle.r 5en9e.s, Ise. Poe. Ana ly6Hl 5GNIW1. Me. Pan Anelyltea! m.rvleat, Ine ceAnalytrCa�• 20Eavw.aa.Aa.O•S rA 22-arvurf.N 9&q•^uVRra 5..rp100 Ede... NC 27266 AM.eye., r1C 769m4 unrnrN. NC 25tl,5 .: 3y6yn0,21 It761R54.'1 ,e I70a I57 -VWa 0UAL17Y CONTROL DATA Noil6ct: SURRY CLOSED -MT AIRY(UtC) Pau Prgecl No.. 82119660 OC Balch: MTAOU75 Analyze. Melhed Sat 4500-Ct-E OC Balch Method: SM 4500-Cl.0 Ane"m O.aelptim: 4600 Chloride Associated Lall S6mpNs' 9211961WO2, 92119660003, 92119560004, IR 11 a6e0005, 0211%60006 METNOOBLMAL 775427 M"r NhIw Auaci sled tab so most: 9211➢660➢92, 921195a0005. 9211954NO4, 921 i 96e0005, 92119666W Blank Repar(Ing Pommel- Unlls R■eult LI-C Mdy2ed Oua6Aen CMPrlde uprL NO 1000 0670e01206-55 LABORATORY CONTROL SAMPLE: 775U26 Spice LCS LCS % Rec Pummau, Unit. Cone. Result -A Rau Umlle Oum6Aan CModdr vatL 20000 mop f01 90-110 MATRIX SPIKE SAMPLE- 775429 0119761091 Bpi" MS MS %Rac Parameter utom Ras�l1 Cores. RauAl %Rac Llydk Questing chf.ode ugrL 234 mOA. 20M 291000 67 75.125 SAMPLE OUPOCATE. 775430 62120033001 NP Map Parameter Unit. Reedy Result RPO RPD Qustilm CMOrlda Yell 6730 mglL 73t0600 ➢ 20 Dale: Owl 41201201:2S PM REPORT OF LABORATORY ANA LYS 15 Pepe 49.155 TN. r.W"wta rov u—O. e.wm.. Ar .n l er • Man —.-.1 Paco A.N166mi 5--- mtc a ps" A014rh el 6arbae., km. P46e Ar.alyd cal 6.Mmer, lna Paam Analya"I slarYlCee. me- aCeAnalytical Xd E.Y a .tl Remo • & YA 2225 R.semoo dr 9600 Kftfy A". SUM IOV ..v,at< burn Eden- NC I7166 �e . NC 2e604 HwwraAla, NC 2e075 i (3.M)a23419z1 la2af2'dF7174 4704p75-900P QUALITY CONTROL DATA Prooel: SCURRY CLOSED - MT AIRY tUIC} Peca prpj7P1 Ne,: 92119580 OC E51!ch WETNI2275 Am",, Metned SM 4500•Ct-E OC Smich Ma6wd; SM 4500,CI,E Anafyalm Oesvtp0en; 4500 Chloride Aasodaled Lab Somples: 9211%6W07, 9211tf6a0006, 9211966D009 METHOOBLANK: 775431 Matrix: VAler A..W.I.d Lob SarryMe: 92119080007, 92119660006. 92119660009 Blank Rep0ru10 Paramler Will Re.0 LIrw' Analyzed 4uml6are CNPndo uprL NO 1000 OMW12 0012 LABORATORY CONTR✓JL SAMPLE: 775402 Spike LCS LCS % Rec Parmatsr Unes Canc ResWl %Roc twill Oua6Den CMorlds VIL 200W 20200 101 20-110 MATRIX SPIKE SAMPLE 775434 92119644002 Saka MS MS %Rec Pupmeler un4e Reeyll Conk. R.,Vlt %R.P LIirIN OumAAer. Chlorde uVL 2100 20000 22400 101 76-125 SAMPLE DUPLICATE 775433 92119644007 C1uP Mee Puemelar Unfi R..ud Re.uh RPD RPD Ovallaen Clmnnde uplL 210D 2100 0 20 r� �t,,,, r�.g a Pace Analyeerl amMees, In' Pat. An.1ytldI Bard 00%, Inc. Puree Analyded lenime. lnm. pcA 1Qlyt7yul 705 E V MeeGew Reetl - Svu 11 2]36 Rw "'D' " gm Kk Av A.f. 3aw to f aRearacaramta.r Eden K 777" AW2.6aq 14C NOW -Iu r mx aa, RC 2w7ft 1 (3311)6734n, (6261254-717m (Tuwl -iaw 1 QUALITY CONTROL DATA Project; SORRY CLOSED • M7 AIRY (I11C) Pace Project No.: 9211%60 OC Be" WETN12113 AnOpi. Method: 5M 450010-E OC Bmlch Mattwel SM 4500-CI•E Pnaryen De.Wp6on: 450D Gtlfwlde Assodsled Lab Samples: 92119660001 METHODBLANK: 777104 Maw: Vwlar Admcdalad Lob Smrrpleo. 92119660001 Blank Reportitp Pnrameler uml. Revell uR41 Analged Ou"florm CNorlde ug& NO 1000 DW57l1211:66 LABORATCWCONTROLSAMPLE 777155 Spike LCS LCS % Rec Pusmew LMRe Cono. Ramat %Rat Ll.rah Quablle Chloride WIL 290M 20200 $01 90-110 MATRIX SPIKE SAMPLE; 7771E6 921196a0001 Spike MS MS 6S ROD Parama(ar UnRs Rnult Done. RnrAl %ReC um+a OvAhfim Chiwldo uwL 3WI =09 23M 1pt 75-125 SAMPLE DLPLICATE. 777157 92Q0629001 Opp Alex Parmmeler LIn11e RemWt Re.1111 RPD RPD OHea6an CNorkle uWL 56.3 milli. A6600 0 20 Owl: Owl42012 0t:16 PM REPORT OF L.AS0RATO RY ANALYSIS Page 50 0155 Dew OW1412012 01,36 PM REPORT OF LABORATORY ANALYSIS Pape 51 0r 55 71e rea.rr Wet ..1" np—e O...wp ea TM mmn enra ml ee nNe wd. sxemq n 1J. rv1%re.a Ci. wll`n een.ent of Paem AnHrLa1 ienneae rr,e _".q N. wnrbn —.nl of P.- Anarfynmr &@W *.. aK • aRmr".al e.mvi r.., role Pao. A n.Irw.w ante.., Ine Par. An mry%et S.rvlv.m, Inc. �+a n�1� 2m. Z. 0-.arx Rc rs - S.N.A I735 Hlwn�w I7. DLL M+rti1 ✓'�a� 9MW V— y Ar. SW. IDO I:r mn Id.., NC 7779a Ar '4Nr SIC 7l604 1WAIeNc 7a019 ? ti7a]821d971 ra761754-7176 17041e7S9097 QUALITY CONTROL DATA Pmrgwl BURRY CLOSED - MT AIRY NI CI Paee Propel No.. 92i19680 OC Sarch WETA112104 Ana rv.l. mmr m SM 5110R OC Balch Medrod: SM 50108 An.Iyale 003CAP6eM1: 50108 TOC Aa4ori.led Lao 5ampfe. 97tI I M 0001, vI1 LIP 002. 92119660007, 92119660004, 921196806 0065, 921t sello , $2119680007, 92119660006, S211609660009 METf1013 BiANK: 776S67 M.trh: WAlem AAsonaled Lab SafAples: 921 t9660001, 02119690002. %1119660005- 02119660004, 921194"005. S2119660006, 0211966mw, 5211 WWII . 0211' 6moo9 Slam Repaling P.ramd.r VnII. R—IT Ij h Analyzed queleem Total Orgenlc Carbon uy+L NO 1000 06M V 12 16:04 LABORATORY CON71101. SAMPLE: 77656] SPI" LCS LCS 5k Rae pwo,"lam UrIns Cana, Result %Rea LIm6f Ou011wo Tool Omoo we Carbon uWL 25000 24500 gh 9b110 MATRIILSPIKE SAMPLE' 178584 92119680001 Spike MS 6!S %Roc Pvamliel Unas Rew11 cove. Rm" % RAc LNNIa OuY6H. Total Oroonlc C"- rIp1L NO 25f100 25400 lob 7'3-125 k1ATR A SPIKE SAMPLE 776566 921t9665002 Splk. MS MS %Am. pang"far Was ReeNl Lena. Reµdr %R.a Lltnlfa OuNAaua TOW Orgrv. carom uWL 1300 m➢+L 2.%m 1240000 -234 75.125 me SAMPLE Ol7PIXATE: 776695 92t19860002 [)up Max P.r.m.ler Unlls Result RMNII RPO RPO Gummmmr4 TOW Organic Carbon uWl ND N6 20 SAMPLE 0VP1JCATE 776643 9Z119904001 Dup Me. P.r.,n.1.r Vnas Result RsaWt RPO RPC 0whkan Two. Omgarwc cmbaA ug+L 9 0 mglL _ 12D00 29 Z(I m J P.e. APuoYtleal aemasv, I- Pan A.0ydwl iavVlen, kola. 2L2 IGr7� 705 Ew U..-. Nv.a-%� I.A =5Aqu4da0r. ...r u� Edon. nc 2775e AahMN. NC7ea04 I (306p234971 162e1754.71m QUALIFIERS Prolem SURRY CLOSED - MT AI RY WIC) Pace Fralvct Na. 9211MD P roe Anslytlea! aaMeea, Inc 9AOu nww:ar Ara. sale I HwnNrnw. NC 28070 nwla7s9arn DEFINITIONS OF . Lllubm Factor, If reported, repro a.nfa the hctw applied to Ine re"ned dole due 10 ahenpee m aernels pr4ptua9on, dluom or f ample erlqu06 w maaama content. NO - Not Oaiaeed at w .bw. adolled moorting lmll J • Es9mamal n omnu%mn above the vcWwI4d me clod detecilon Amll and below Oss .dloaled lapordng Nrna. MDL - Agwad MefhOd Delectim Ural. PRL • Pace Repunlna Lana. RL - Renaming GmN- S - tluffogole 1.2 Dlpnenylhydresbla {4270 Na1lti anaryte} tie Cahlp0ler to Ala benec n E. C"Nigmnr IL4111 EPA guldelin-4, unfounded data afe tilsPI eyed .old Ine Ve been rrr Ed to Calw1mle %fa[overy Intl RP13 vol u es. LCS{D}-L. wmwry Cantrol Sample(Dupacal.i IASIDI • Matrix Spike I[rupilcals] DVP • Sampla Oup6cale RPD - Ralo*c Pwcml Diftrance INC - Nol CalcWable. 50 - &I Ice Get - Cleail U - Indc.le. (he eampound w.a analysed far, but not d0eatad. aFNNrmadlphenylamin/ deoarnpaau eed tanrwli 11a eepara led Sam Olp]ne11y1.mMI LNdg MMhod 5270. Tho,.suit mapegod fm each wSly te IN 4 cembaned [ane'tmIAan And pre Demotion may not be eppropdate ter 2-C1n1e✓0eihyh.nyl eons, Sty —a, end ylnyl rhfwwo. Plc* Anafyuc l I. TNr Iroadled. Contest your Pace PM for the wn.nr Gat at acaedllod an@" TNI - TTI NELAC Ina Carle LABORATORIES PAS, -A Pace Annot0N 5amw w - AeheYNN PAS -C P... Malyl I Sera.. - Charlod. ANALYTE QUALIFIERS m Oxygen ws.ge a Less than 2.0 for .a odyoons set The repwled slue A on eelom.led lee. IhAn Value end Is calculwea V Ne doudon ueing 0.. mo.r .maunl of.amp). D8 The rdHlve I)em om dfortnam IRPO) lwwasn [me as rrple and supple dupecale escee0md ImcwAlwy contra Nrnlh. LO AAm" recov Dry In Ine laboratory control sompla 1LCS} "a cmWde GC ll+nlle. M1 11,114lhx ap.ke reennry exceeded OC Ilmnlls. Bergh accepled hawed aR lalwrarory eamma serryile {L CS) reeoYmuy M4 Made V ike and Meuw spike duplrcal. rat:DVery "I EVEluo ed abalmr O tfal Nrr1KI due la so mPl4 dllud0n. Dole 001I417012 01'-'�15 AM REPORT OF LABORATORY ANALYSIS Page 52 e1 55 Dale' 0601417012 Ot'36 PM REPORT OF LABORATORY ANALYSIS P.U. 63 e1 5$ T7.. r.pon.na —I"n}wq, ...c.pf mr 1d TM rlmn rn rr ml ✓r rnpm pa .er:epf h ko wil—I ttr w mn mneenl al pate Arulrvul $—, w WI —I rh. reilen cnaa.ar 94 ftc An.iluvel 9erl.re. Y 04aa Analyfaal 5a 16al• IPe- Pace An.lynrn 1 Icea, W, Pose An.1V0oal e.rl4ell, Inc. Pau Rn.lygeal %mcaa, In.- Pa[. PnNyll ul 15—lea, Inc P.ca A04hM041 ¢.,ilea, In{, �I .� al.e7'li ral yf r�Rl' 206 fam ANacww RaW-6,ateA 2225 RN.neGG GOOD KWA"A". Sv1. I (I ,,,, ' acQ. P111aVical' AS i.rt W.dow Rm-6uMA 2225-1",wo Of 987E Kw"V Ave. 3W I - ... .w.a m. Ed-. NC 272M AMa�e.4- oK ?WW K-Wr .4- RC 2007e " �,.`y,K.... yn i:ean, Nc iT7le AaK.rM. NC W" NYnWa,M.. NC 2107e • [336WSd921 IeMA4.71711 I704IO7sl07V 11]4I411aa21 [e2el -r1Ye 1701]97SV000 QUALITY CONTROL DATA CROS5 REFERENCE TABLE 0UALMY CONTROL DATA CROSS REFERENCE TABLE Plooct SURRY CLOSED - MTAIRY IUD) "act: BURRY CLOSED - MT AIRY 111I Cj Piece P voct No; 92175660 Pea Project No 0211g600 AmrA"l AmiAcal LAID ID 5ampla ID OC BHch Mottled OC Bitch Anal Acid Method Batch LID ID S.mpl. 10 0C 9.tch M.1hod OC Balch Amlyllcal 10.4hnd Blotch f241fN0001 MYWI EPP-3010 MPRWID71I FPAIWO ICP19954 W1!l6000! MWt! SM 52108 WETIV062 SIA52109 WET121005 1211f68060P MW+1R EPA3010 A41PRWIVIZ EPA8010 tCPM54 f211166000t MW-1 EPA 300.E VVETN12230 1211961lO03 MW-126 EPA3010 MPRP770712 EPAGOIG ICpt"54 fI11 +66D00O MW3R EPA 100.E 4VEPN12270 0211098DO04 MW.120 EPA 3010 MPRPIIC712 EPA6010 ICPtg654 137T MMWYV.-11265 EPASD..0 MTAV1223D MISSIONS MW13 PA370110 EPA3010 MPRP110712 EP010 CP964 ICPI654 4V-1! MPRPt072 EPA0I0 1101 250004 M12111580006 W-10 EPA WETN 12282 '21,MOOT MW-1 EPA300 MPRP10712 EPA OOD ICFW54 82113"006 MW-3 3300.0 EPA 00.0 VOETN12262 9211fONO, 5mll EPAD 10 MPRPIO712 EPAZO10 ICPM54 2211l0 EPA WETN112282 021166000% m*fi EPA010 mpflP10712 PA 6r0 ICP79034 V 3300.0 EPA000 WETN2282+0 4glx;711111711+99fi1600e0e0000006000003{823 MW18 EPA 300.0 WETNI22 lf192l5t7tle64080006006 MMWW1-0R EPA747E MERP7426EPA77E ERC102 92111900009 MW16 EPA300-0 WETN22827111719fFa0001D00117 EPA77O PAERP14263EPA747 MERC1482 12111600 M7470 ERP1413EPA7410 MERCA162 02110630001 MW+ SM 4500•CI•E WEN12313 4 W12D EPA 1470 3EtPA747E ERPM2 MERC48 MW3R SMM{500-CI-E VETN12275l2190160 MW-13 E47D MERPM283 EPA 147E MERC14112 W-128 S4500•CA-E WETN2275 M EPPAA 7470 MERP14263EPA 1470 MERCt41e2 12t596+0064 MW-f7O SM 45p0-CI-E YlETN12;75 121t9480007 MW-16 EPA7470 MERPH263 EPA 747E MERCf4162 :11798000D4 MW-13 SM 450D-Cl-E Y&IJW 2775 02113"0000 MW-19 EPA 7470 MERP14263 EPA 7470 MER[14192 127r9660606 MW-16 SM 450D-CFE 1WETN12279 92111540000 MWte EPA7470 MERPi4263 EPA7470 MFRV4162 f2r71860007 MW-16 SM 45MCI-E WSTN12276 92111660004 MW-1 EPAd200 M6V778311 17111+6000. MW-79 SM 450E-CUF VWTN 52276 $11116a0e0Y MWaR EPA e260 M8V11:311, 12110660009 11W.16 SM 450E-CIE. YyETNSI276 9I119630001 MW128 EPA6260 1SWI131, 0211%l0004 MW-12D EPA 626E MSV119311 $3111060001 MW-i SM 53108 WEW$2304 1I1196eODD5 A1W-11 EPAe250 115"1", 9x116i60007 MVY.19 51115310E VYETAA=4 92119600006 MIN-76 EW16260 MSV71l31, lI 17 e600003 MW-123 SM 53108 VYCW,2304 e 2rie690007 MW16 EPA 6260 M8VlIl311 92115080004 MYV-120 sM 13108 Y&TN 12304 0209{60006 MW-13 Bm5310B WETN12304 l2119660006 MW-1f EPA9260 MSVr18324 11211811110006 MWAS Sm 53100 WETOJI2304 9211968000! MW16 EPA A280 MSVII2511 12111540007 MW-16 SM 531 DB WETA412304 M1f660006 MW.19 SM EA me VVUN12304 7$119660007 Mri-1 SM 27206 YYETR 111E 1I11f660009 MW-16 SM 53f09 WETN123M +$11 G65VOD3 MWJR SM 21WO" V4ET2I17t0 9I 11l6+0003 A1W-125 SM 232DB WLTR7710 1211150NO6 KOV-120 SM 2370E WET12rr10 12ri9680064 A1Wtl SM 2320B AET12111D f25t9O+D066 PAW-139 9M 23206 119ETW110 62 illso'001 MW-18 SM23Z06 WETf21710 9277+GO DOOM MW10 SM23206 WET2111 l24MAWO9 MW-16 SA12320B VVETF2111: 9211+68 MW.1 SM S378 WETQiM SM 521006 VVEYt2710057 MW.3R SM 5108 1VET21056 579x1160002 9211960003 Myy-1a SM 5210 WETy2158 SM208 WT105700 W.2 11 T056 SM 5200 WETR057 1f211f4090 9211966000E MW-13 SM 52709 WETR7062 SM 5210E WM21065 +2T19600006 0OW-16 SA1 521OR VVETf2l062 SM 521OB WETA! 066 68000E MW-16 SM 521t06 ET4t0a S52109 WET111057 1790e MW-17 SM57OR 5 WET72056 SM 206 WCTl207 Dole; 06714t2012 01.36 PM REPORT OF LA 00 RATORY ANALYS IS Page 54 9156 D.I.: DWI 4110t201:36 Pot REPORT OF LABORATORY ANALYSIS PAyc 55 ora5 TNa nper[ Mal o- ta. r.prpdrwn. erupt n hal, f Nl r+Wp W ncl a ,.p pdu d. n pl.,". me-1 no �[+we PI.— Anallml I:.—, •nc *. t04 .ne.n —k or Pop. Anoly" 54,*** lrc � x�,11���■■�©asse000s� J_>I rMEER t _� ►■■■osasooaos ���� ■!� t��l'j«• REUNION • 111111111111� 111111111111® WOMEN 10401". .10�■■■■■■■■■■■■�_©r ���■■■©as©soli©s© 1 •4 ' �©�©h1 ■■�© 1i7������ _ Sam le Condltlon V an Racai pt 3CUR 1 1 ail Document Number. Issuing Authority: F-CHR-CS-03-nay.0? Pace Humerov"s QmPfty Office Client Name- r dl itc�, Project# 221r9(,Y() W he re Roca ived Hunterevllh ❑ Asheville [],-EEden Couden ❑ Fed Ex ❑ UPS❑ USPB❑ CIIONE] CommerdePan Mer — BEEMENEEMI Custody Seal on Coolon9ox Present: ❑ yea � no Seats Inteci: ❑ yea ❑ na ISMOMMENN Pecking µoIsdal: ❑ Bubbl(Q_1�jrap [ Bubbfd Bdge ❑ N ❑ Other Thermomaler Wadi tR Gun�I]1QY T1103 Type of loe� Blue None 4 Semplas on in, M" pn a hn bown �_ _.._..i.. s..,.. 1 e1 • Ain r`niwnn- T1. a9• Ain I`..r n.-nnn CorreeledCaalerTamP.: C 3 0 Two should ae ehura X.adnp to WC BiologI"I Tlssus le Fan: Y.. ka0w�i Commence: oar..na Ins P.n .mWinp eantenr: chain of Cu Presdnl: r 01. ❑. 1. Chain of Gwstwt Filled Out r OPJo OwA 2. Chain of CuibDdy RglinqulModlz XY, ONe 0" 3- Sampler Name 6 slgftolwa on COC ❑NU OwA 4. samples Arrived vllhln Hold Time: rn Q* PwA S. Short HOJd Time An to r72hr : OYr IAM QVA S. Rush Tum Around Ttme udslod: PYr oft ONIA 7. SuMGent Volume: yr ON. OwA e- covaLt Camalnsra Used- -Pace Conlainars Used' �Yr f11Na ❑" Yr Ha OwA g. Contalnem Inlad: Orr ON. ❑PNA 10, FlPoared volume mcelvad for Olasohrdd lasts Ovr ON. wA 11- Sample Labels match Chi: -Includes dauiNrnellttlftalysfa MA x1 , ��'.. 1pX. OWA �' r 12. Ne TP"- a S ar AN COMMM nuettg pfeae -Wa- rove seen ehocw. Aa wntahani nes&V prerervallon w found to ee In oompllanca vA EPA nimmmndauon' ... voA, oxok-'Tmoac.wWkp u OPen OwA r� . ON. OwA Ore. ❑+ 13, irw M. Samples Vwcksd far dochlull"Ilon: OYr Otis wA 14, Heads ocs in VOA Hass "mm : Orr ;eh. OwA is. TA) Blank Present Trip Blank Custody Seals Present Pace Trip Blank Lal #Y tl Purchased : Orr ON. � DYr QNo '6P 18. Client HetHisationt Roe oludon: Fkld I}ale Requhetl7 Y 1 H Person Contacidd: OalaMme: Cammpntaf RaaduLcn: SCURF Review: -47 pow 1 S 31 SRF Review: odte: Now wh.new a dlsmwwa y aifdgkq NUM na rooe cudlmpNaffame.., a d tpmi l hr+enr u m. NO" Cet lullan Office I La out of hdd, lft o el prgONPI&C pet of lamp, kCdVfed COIAWMl Environmental Conservation Labe ratpript, Inc. ■r►�� 193-4 Wn .kl wq..W.k [earl F A r■ S � � ■ � [art hr 11511 + ��\� Ph— 919-d0D3090 F"! 919,d97.l SiS www,enccl.a..eom www..n[al.lfa.tem Thursday. hme 14, B012 Municipal En line ing Services (MU091) Attn: JDrlathan PION P.O. Box 97 Gamer, NC 275n RE: Laboratory Results for Project Number: G11024.Ciosed, Project N7tniejoesc: Surry Co. Closed MSWLF - Mt. Airy ENCO WOrkorder(s): C206089 Dear ]onathan Ptohl, Endosed is a copy or your laboratory report for test samples received by our laboratory on Friday. Tune 1, 2012- Un;eSs otherwise noted in an atfaoed project narrative, all samples were r"ved In eCteptablt; wnpltlon and prMeSSW in amordanoe with the refeenged methodstprowures. Resins for these procedures apply only to the samples as submitted. The analytical resvlLs conWlned in this report are In oompliance with NELAC Standards, except as noted In the vroject narrative. This report shall not be reproduced except In Full, without the wrlttm approval of Ute Laboratory- Thls report Con Wlns Only those analyses performed try Environmental Conse vatlon Laboratnnas, unless otherwise noted, all analyses. were performed at ENCO Cary. Data Rom outside Ortlanl2atkons will 6e reported under separate corer. If you have any questions or require further Information, please do not hesitate m contact me Smoerely. Chuck Smith Project Manager Enclosures) C16.l 70r Mw421 _ - lab W. C109019 I Umpkda U130111 ]7dS A...rvd1 09/01731 lawv H.Id n.lal}".l M1ro 0.4/TF.Mt.7 M.."O.prnm.faj 061221i2 ON17y11 9713C 671UNH .631 Ca.ntlor NW-13 L.y 10: ClOooN"I a..Pld: Dap0yl2 L7:00 X.ulrw: Oalal711 11:10 P...w.pr Meld Da"fIr ..t.l Pr.P O.dlTlm.(.i A..",. e.pllim.t.j EPA 3[0.0 0417y12 ac: l2,r:7 v? ]r WS717012 17dH [ndAl iD1 9ny-ld lab lD, Cl0WOa . Umpidr 06101111 L"O A.Wr d: 09 DI+SS ilrl0 P.r.m.l.r Hold O.1.: lull.!.) 4, V 0.l.1?1—(.) ,rralr.l. ba l.rilm.l.J Ev. 3W0 mi lq.r',: •?6,171:7 11::� pl.nT r0: MWIS Lae 10: moa019-04 0503O151 rNDS . k—wd: 0a10if 1113:30 .af.m.ea. Held OLI.IiInP[.1 ... n.p 0 evT. W!.f!t _ .aftJ r.t.l DwLaol2 Ol!De 9r17120i211:d2 Cant l6i 9tWla LE ID: C10"a9-09 a.m d: 091]0r12 1714D pt"w1w, 06/01111 SSi10 P.r.m.l.r H.Id Dd1.7T"n..1 P,.P D—t Tlm.l.! d,..r, i. D. 1.7 r1,n.{.j r=. ].v: L,,. r: I 11 f I2,:: 11i.35 Eli 7,rm2 1155 T!,. Inl.l euml.er orr.6e. m 1hu rereri, —k6rS V . irg. i. i wer2oril OF www..ncol a b. -o NORTH CAROLINA SWS SAMPLE OETEMON 5U MMARY PIw.f37h MW•le ' L.4 TO: CIDO59.03 M.Irp p..ue. F1.1 OF MOL MAL Ara SLL Yn14 .e 0" H.Yr .19a]de.O 13 1 I 0.00 0." rE. TrVL Z� fENk' yyn� .nw�ebs.cn n+ D."Ml,uml KW.12S ANALYTICAL RESULTS L.h S.mple TR-CN0E 401 Mc-iY+d: OWO 1i L213: 30 M.W.: G—d Wafer 5—ol.,d:05)37.:17 1.1 35 Work Ordar•. C2MM Pro3.cl: Sv Co. Closed MSWLF • MI. Nry S.mplod ov: ?Wa[INn PfeA Claulul Chemistry Parameters • • MCI W— f rJNC 5911 Amwzk rcas Mm...t...e 6asW4 Dab uwb 91 SM IV— BC 4HLSL Mswhaa &Uhmod Lx eoe.. ate. v .yL t a RI + • F.. IW a owwu 14 r! Cea n+. w—"v w.yen...«...e. e... rL..— --. ...w.v...N P.v 4 ud 1! ENCO www.anmlehr.mm Oeavlpu—: MW11 Loh Sample 1L: C206089.O2 Reeelred: 06j01A2 11:30 He hixi inwnd Wa1M• sampled t 0VIW 12 17: 00 work Order: C206089 Projo t: Swry Co. Cbsed M$WLF - w M $w pled by; ]a .L r MN Clasaiea l C).Wn la" Parame[rrs -I'MM CAI? ►sNQlAI" SYlJ an.1.s rr.c w�.e..1 AaaWh bap help L[ HILL !SILL 1SL.iSYSL Z1alhpd exwreed Aa Mp1ss hm... RMHN..f a en v ^Wv > evi • fo [.a x,r�,+.. �x. a �:.nv r[a Laaeipgen: RW-N Leo Sam pla 1L, C2060"-Ol Relrhe: Gnxrd Wale Sampled: 060111210' 00 PrOj9d: kKM CO. Cloned MSMI - MI. Alry lamplad by: ]O1aIIMe ftm Claeelcai Chem Potry ParrmeLen ^ FrYU G�•:ner'LsT anrryTe Mt S9lI WWw,e W.ha._ liealwd: 06/011u 11:1O WwF Ordv: C2060A9 Aaapl4 y3a0 Vella Of Ma Mu xcsws MALhAA aealrxad BI M2W4 ,_ ter.. nrvnN . w.. wm 4W MM..r",—^yr ._.Cu..[NA rW nOve nw.�..M�^u.r+rYar..r.r +[ae rrxsy...+rnry.�p rn.�ee.r wh,. Nge 5 of I I Not 6 v[ I I Da.e]1PU-t MW-15 Lab Sam PI a IO: C206090-01 Mahe: Greed Wa[b Sampl.d: OS130/12 15 05 Pmj.d: Scary Co. G—d MRYLS • Mr- Airy S.mplad ay:3—th.n MM Ica Www.ancolahs.wm RKdwd: OW01)SI 13:30 Werk Order: C2061M Classical Ch.mtstry Parameters . CACC G.p -nPIV+'rnSlhY S91J ApYrte fCaS i.umibrl saapllA Dap Malta D[ MML MAL NCSM Anduld as man 1i..14 .111 - E.mf V -1 t ..." 1. FfA]w. -,,NU V..; M wwW..n wl.h..wm Oa.crlpd— MW15 Lah Sampl. ID: C206DB9.05 R. W w10 en 1112 13:30 PAA {tw Gra•.W waw SanPrad; 0Vl9i 12 17:40 Wwy OFd\F1 QD50e9 Prpjodt S ry Co- CIOWd M$WLF - Mt. AhI 5ampied ly: )MALN M1 P(ON Classical Ch am iatry parametars an.WM Fe tY�wlrrl ar.IMC. [2"Af4 i•.] HtlWia FJad 0Nh ilI tlLl NSL HC$wc. MIL" ennased ex NLtaA r>. 3W- nN132 tru ..n rM• �...� �.r�....,r...,....hr.. r...�...r »,..va..vr..r...r.-r .. •a•M..... w ire nr..1..n.. rry em. wnl.. mews sr e�Ym.wFr, . m..... �,.rro...y r ra Npe?ur;I Page Av![I ENC� www.en [ale La.rrn 4aaMgl [7ua !a Pu atom - Quality Control OUA ITY CONTROL ^—. _ El 8" 2FfX& • AV AWP D tunk(Ia La004-CLK1I Tne•e:: xr: z':F1) o7.)s ••. r--=':•cr i:. 7'::: ;. t•. I - .. spllu aturea %m t: RPp f _+tn•he _ _RaruR_ _nay _ RRL wil. navel AMOL riRIC umw Rip U.11 "alas - U U LGS(IF LI004-W Ne d: Dy1I1201i 17:A+r+Fyntl' 16f l L•F71I 15:i'. f spk. sews. MRtp An ti w Rnelt a oafs. Irnrw Lwr R—It wlr raga R>b umn Nara. MRI. Malts. ipla a( IF I)W4,MS 1 I nepure :6: 1 L..17 v7 A MAVxn: W1 LiuIi 16:19 acwee: c2"C li t•91 SPIN. 54— A%uc RPn "Ayla ROOF aiaf MRL Vitus Law R..ult w1c: L1RJa RPh U-It Mua. km PN*. res to-1m Malrta SRI4a Dea ( 271300e • Map 1) kmarad: W12M 12 07A a —VW! Wl771e1I IW.]S Saurn: C106091-H span fto" "mc RPO M e. Ruul[ t HRL unlu Lars Ruu1t XRIC 1Jmlta It" LhAIL W.I.. .. Npr 9 nr'I Pyr 100111 www-el. oolaha.wm The anafyte was detected In the assoclated meHt is blank - The sample Was anaOCO at dgWon. The reported value Is between the laboratory method detectbn Ilim (MIL) and the Ial oratory method reporting IgtQ (MRI-% adjusted for actual sample preWaW dais and rncist n! [onteny where appadable, The ana" was anaFyFed for but not debwed to the level shown, adjusted for mclual sample prepatfiWm data and mWsture conten4 where appllmble. The P9rKenhBpDn ln*AtW for this analyte 15 as estattated value abuv Me calibration mope of the 1Ftsm"nl. Thk va41e Is considered an e56n1ate• Metttpd Reporting LVnR- The MR M roughly equivalent to d1e practical quantaadon lknit (PQL) and Is based on the km pant of the cal&atkm MINP, WI$M apolfb*, sample ptep8n1tkDn FaCtdr, dlluty7e Factor, and, In the me of salt samples, mDistu re content. r/wW,gymla6�,mm -emu. m rn.ii.1ii August 20, 2012 Quarterly Water Quality Monitoring Report Prepared for 5urry County Closed C&D and Closed MSWLF, Mt. Airy Submitted: December 21, 2012 P.O. Box 97 Gamer, NC 27529 License No. C-0281 Mt. Airy, North Carolina August 2012 UIC Permit Number:WI0400176 SWS Facility Permit Number: U-02 MESCU Project Number: G12432.0 Municipal Eaginteriog c..r..r rx a[ Municipal Engineering Services Compazry, P A Gwwr and Boone, Noith Carolina TABLE OF CONTENTS SECTION Introduction Page 1 Background _Page I Sampling Procedure_---_.�, 2 � � -- _--Page Field Parameter Data _---- _�-----� ---_-_______Page 2 Laboratory Results_ _ _ Page 2 Groundwater Samples_ _Page 2 Groundwater Characterization W _Page 3 Findings Page 3 Closing _ Page 3 FIGURES Topographic Map with Site Location Figure i Potentiometric Map of Uppermost Aquifer wl VOCs Detected Above 2L Standards Figure 2 Time Series Graph of Total Cumulative VOC Concentrations ......Figure 3 Time Series Graph of Bromide Tracer Concentrations _ _Figure 4 TABLES Sampling and Analysis Summary. Detections that Attain or are Above S WSL or 2L (Appendix 1) Indicator Parameter Data Summary Hydrologic Properties at Monitoring Wells APPENDICIES Laboratory Analysis Report and Chains of Custody Table 1 Table 2 -.-—Table 3 Table 4 Appendix A License No. C-0281 CIVILISANITARY IENVIRONMENTAL ENGINEERS SOLID WASTE MANAGEMENT Municipal Engineering Services Company, P.Q. SfrE PLANNING I SUBDIVISIONS SUBSURFACE UTILITY ENGINEERING {SUET December 21, 2012 Mr. Thomas Slusser, P.G. Aquifer Protection Section -Underground Injection Control Program Division of Water Quality Notch Carolina Department of Environment and Natural Resources 1636 Mail Service Center Raleigh, NC 27699-1636 Re: Quarterly Water Quality Monitoring Report Sorry County Closed C&D and Closed MSWLF, Mt. Airy 237 Landfill Road Mount Airy, NC 27030 SWS Permit No. 86-02 UIC Permit No. WI0400176 MESCO Project No. G 12032.0 Dear Mr. Slusser: Introduction \ Municipal Engineering Services Company, PA (MESCO), on behalf of Surry County, appreciates the opportunity to \ present this brief Quarterly A'ater Quality Report that details a water quality monitoring event performed at the Surry County CIosed C&D and Closed Unlined Municipal Solid Waste Landfill (MSWLF) Facility (Permit # 86-02) on August 20, 2011 The Injection Well Permit Application and Well Permit No. W10400176 (5/6/11) requires that Sorry County provide this report to the Underground Injection Control {UIC} program on a quarterly basis. This report documents the quality of the groundwater during this monitoring event performed on August 20, 2012. Laboratory analytical results indicate volatile organic compounds (VOCs) attributed to landfill activities continue to persist within three wells that monitor the uppermost aquifer downgradient of three injection points. However, total VOC concentrations compared to their respective baseline averages established during the five events prior to the November 2011 injection have decreased inmost locations. Background The Surry County closed C&D and MSWLF, permit #86-02, is located at 237 Landfill Road in Mt. Airy North Carolina. The site location topographic map is depicted in the attached Figure 1. Prior to becoming a C&D landfill the subject area operated as a MSW unlined sanitary landfill that stopped receiving waste prior to January I , 1999. The MSWLF was closed with a low permeability cohesive cap per the Transition Ilan. The top portion of the southern unit served as an exclusive C&D landfill until prior to June 1, 2008 at which time it was properly closed with another cohesive cap in accordance with the Closure flan. Per the NC Solid Waste Section (SWS) approved Corrective .Action Plan, enhanced bioremediation via substrate and tracer injection was initiated in accordance with requirements outlined in the Injection If'ell Permit.Application and Well Permit No. WI0400176 (5161II). EOSOD598B42 plus Ix16 ox EOSID Vitamin B12 supplement and sodium bromide tracer were injected into four wells on November 2-3, 2011 in an effort to reduce low level aliphatic and aromatic chlorinated hydrocarbons in groundwater to below the North Carolina Groundwater Standards (2L Standards). Injections were performed through IW-I, IW-2, IW-3 and 1 W-5 and details are provided in the Injection Event Record dated November 4, 2010. PO Box 97, Gamer, North Carolina 27629 (9'9)772.5393 PO Box 349, Boone, MC 2A607 (828)262.5767 Water quality at this facility has been monitored at least semi-annually since 1989 with historical data available since 1994. As directed by the UIC, quarterly post injection water quality monitoring was performed on February 9, 2012 and May 30, 2012 with reports previously submitted to the [TIC and SWS. This report contains sampling procedures, field and laboratory results, groundwater and surface water characterization, and findings. A potentiometric map of the uppermost aquifer, time -series graphs of select constituents, a table of detections compared to Standards, field data results table, groundwater flow directions/rates table, indicator parameter data table and laboratory analytical data results are also enclosed. Sampling Procedure MESCO personnel performed this sampling event following the parameters, frequency and well locations established by the UIC. Groundwater samples were collected and analyzed from nine wells which includes MW-3R, MW-12S, MW-12D, MW-13, MW-15, MW-16, MW-18, MW-19 and upgradient background well MW-I. Additionally, water within the injection wells were measured and visually evaluated in an effort to determine the amount of residual organic substrate remaining in the wells which may help evaluate the viability of these wells to be used for future water quality analysis. Monitoring locations are depicted on Figure 2. Sampling was performed per the protocols outlined in the SWS approved Groundwater and Surface Water Sampling and Analysis Plan which was submitted with the Corrective Action Plan (CAP) revision 2 dated December 10, 2010. The depth to water in each well was electronically gaged prior to purging to quantify the static water level elevation. Low -flow pumping methodology or bailing was utilized to adequately purge the wells a minimum of three well volumes or until dry. During purging the stabilized field parameters were recorded. The samples were then placed into laboratory -prepared, pre -preserved containers via a new disposable polyethylene bailer. Samples were kept on ice, and transported to a NC -certified laboratory under proper chain of custody (C-O-C) protocols. Field Parameter Data Field parameters recorded included pH, specific conductance, temperature, dissolved oxygen (DO), oxidation reduction potential (ORP), total dissolved solids (TDS) and visual turbidity. A summary of the field parameter data is presented in Table 3. Laboratory Results Pace Analytical laboratories (PACE) of Huntersville and Asheville, NC performed the majority of the laboratory analysis. Groundwater samples were analyzed for all the parameters requested by the UIC which includes constituents listed in Appendix 1 of 40 CFR 258, alkalinity, sulfate, chloride, total organic carbon and biochemical oxygen demand. Environmental Conservation Laboratories (ENCO) of Cary, NC analyzed the samples for the tracer bromide. A sampling and analysis table summarizing the locations, target parameters and laboratory methods is presented as Table 1. Water samples were reported at the laboratory specific Method Detection Limits (MDL), which are quantifiable at or below the current Solid Waste Section Limits (SWSL). Laboratory results and C-O-Cs are presented in Appendix A. Groundwater Samples Total cadmium was detected in levels above the 2L Standard in MW-18. The wells with Appendix I VOCs detected in concentrations above the SWSL and in exceedance of their respective 2L Standard during this event include MW-15 (vinyl chloride, TCE, PCE, benzene) and MW-16 (1,4-dichlrobenzene, 1,2-dichloropropane, 1,2- dichlroethane, benzene, vinyl chloride). Table 2 summarizes Appendix I constituents detected in the water samples in concentrations above the current SWSL or North Carolina Groundwater Standards (2L). Table 3 summarizes indicator parameters quantified by the laboratory. A site map depicting the spatial distribution of VOC concentrations detected above the 2L Standard during this event is presented on Figure Z_ Groundwater Characterization A potentiometric map of the uppermost aquifer created from static groundwater elevations recorded during the August 2012 event is included as Figure 2. Groundwater flow rates and directions were calculated via modified Darcy's equation and are included in Table 4. Groundwater flows in the unconfined and upper bedrock water - bearing zones in a general southwesterly direction away from the waste limits. Calculated groundwater velocities were variable but consistent compared to historical observations. Findings The quarterly laboratory results indicate that low level dissolved phase VOCs consisting primarily of chlorinated hydrocarbons continue to be detected in groundwater samples collected from MW-I3, MW-15 and MW-I6 which are located within 250 feet of the waste boundary. No contamination continues to be identified in samples collected from the other six wells sampled during this event. All VOCs detected in concentrations above the 2L Standard during this event remain within their own respective historically identified range. Total cumulative VOC concentrations compared to their own respective five event averages decreased in MW-12S (-1449/0), MW-13 (-39%), MW-16 (-22%) and increased in MW-15 (30%) for a total cumulative reduction of 13% (Figure 3), Evaluation of the injection wells (IW-i, IW-2, fW-3, IW-5) continues to indicate that a considerable amount of residual organic substrate remain in each of these wells rendering them unsuitable for representative water quality analysis. The viscosity of the water in the injection wells precludes sample collection as either a bailer would not descend or the check valve failed. Bromide tracer was only detected in low non -quantifiable `j-qualified" concentrations in MW-12S, NM-13 and MW-16 during this event. Bromide concentrations have exhibited an apparent increasing trend in MW-16 (Figure 4). Closing Corrective action to remediate the VOCs as detected in groundwater is expected to continue. The fourth post injection quarterly water quality monitoring was performed in October 2412 and the report will be submitted to UIC and SWS upon completion. if you have any questions or comments regarding this report, please contact us at (919) 772-5393 or by email at jpfohl(a)mesco.com. Sincerely, MUNICIPAL ENGINEERING SERVICES CO., P.A. �q .0 Jonathan Koh Environmental Specialist Enclosures cc: Mr. Dennis Bledsoe Suny County Ms. Jaclynne Drummond SWS-Compliance Branch Figures Topographic Map With Site Location Surry County Closed C&D and Closed MSWLF, Mt. Airy N 4� -fir L 41 7. - ... • �� .. - ' J i i •v;.. +. �,, •ram 1 i •: ' t t, . •Z ate' l,` soy 1 i Landfill ••�� � •.-,',y��, •ram- �\ yp! -- ��'•-i�, .. .1 ` c-'-. . y ?, �'• ROAD CLASSIFICATION 1 o 1 MILE Primary highway, tight -duty road, hard or hard surface improved surface ..� Secondary highway, hard surface - .- _ Unimproved road --_> - FIGURE 1 t� Interstate Route "ID U. S. Route 0 State Route SCALEHOUSE ATER SIIPALY WLLL A1R-,5 NOW OR FORMERLY OWNED er JOHNN Y COX nWd 4 - % IIIY-l� � ® 5 5W-2 - - S OWNED BY SORRY COUNTY jib _ _.. • 'y ... r z 1 � i ri Mw•�rwe�st't°'. Fj MIA uw �•:l 14 ,s NOW OR FORMERLY OWNED BY rro ww r • SHA WNA SUMMERS ` f EMS TRIG ROADS tip' +' _.._.._ ESTWATED WASTE:-JWTS tArC+MEP usW &IOR CAD LW8E wins I, -,U&nr a llHfD osftr -•-•-•-•-•-•- EXTprr Or COMMIE CLAY OLMOC LVON CLOSM MSW AND CbD ky� uwaR i er' PPIFERTY LrrE EXTRAPOLAtm FROM SURVEY AND CIS •s �. �� �- —•-W-. rOWPrArrca eoi,e,Ouer (rso' FROM eCw w w' rnaw PRUPEtrrr urrQ <Z3t�— EXTENT Or wc(a) outcrm Asow 2L stANOARO 6El w DowPumct Bm*omr .�[iN1YE IiFII'.... W AREAS PREVIOUSLY W.[CiCO . ' Im- FOLWOTERRAC OPPSMOST GROLWOWAT[R CONYWRS .yyL 1a S1 f{F!p - 5TREAWtt2EEK/RIYER WAM? %X'PLY WE1L sw.A� SLOPACE WATER YONITARIMC POW -9� r' J• ,,,� YW19® Y6WITORWC WELL _9•LA IX•1 A1W0 NWXCTMN WEii GROUNDWATER POTENM]CIETRIC ELEYA MAN (., A� �.. MOT{EiEYA Ii(JH Ar6t USID FOR COM7IX1R5 SEOAIEN7 BA-VN OWNED BY SORRY COUNTY 'au[ :rnLf. FIGURE 2 E r { CLOSER C&D LANDFILL and CLOSED MSWLF FACILITY Municipal �� E�gineerin N r 9 e ^ ry �4 SGRfiY COUNTY srrvrces ��-' Company, PJL ti P0ANWt-MC wp of UPPER61%7 AOLFER _ + WTH rocs ACZCFW AWv f a SrAMMMS MT AIRY, NORTH CAROLINA �,o.�+m l •° "' 'Q. K`: Figure 3 Total Cumulative VOC Concentrations Pre/Post Injection Comparison October 22, 2009 - August 20, 2012 Total Cunulativt VOC Concentrations �= SML or ZL Standard 300 Mutd-Waa Tkn Seq%s GtV1q 250 150 00 Su n r � Sa VIDD" Lij •WX 16 uMY-13 -WY 15 -M UC YYOK -MN-1IS MAI I2D -RAW-1 ,WM3R ww.. 18 BMW-18 � Z Well ID Oct 2009 (ug1L) May 2010 (ug/L) Oct 2010 (ug1L) May 2011 (ug/L) Oct 2011 (ug/L) Average of; Five Events Preceding August Injection 2012 (uglL) (uglL) I I Difference J (ug1L) Difference MW-1 0.00 0.00 0.00 0.00 0A0 0.00 OM 0.00 0.00 MWl-3R a00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 MW-12S 0.00 0.00 0.00 0.00 5.40 1.08 O.QO -1.08 -100.00 MW 12D 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 MW-13 61.00 50.60 74.20 87.30 72.50 69.12 42.18 -26.94 -38.97 MW-15 96.13 63,89 55.00 78.10 64.06 71.44 93.08 21.64 30.29 MW-16 137.90'113.60 135.70 121.2a 116.30 124.94 97.70 -27.24 -21.82 M W-18 OM 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0,00 M W 19 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 Combined Total 295.03 228.09 264.90 286.60 258.26 266.58 232.96 -33.62 -12.61 Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Figure 4 Time Series Graph of Bromide Tracer Concentrations February 9, 2012 — August 20, 2012 Bromide Tracer 0.3 0.25 0.2 J _ 3 0.15 0.1 0.05 If 0 61;11 Date MW-1 (Background) • MW-12S o NW-13 O MW-15 • MW-16 Non -detects shown as i4 detection level Date MW-1 (Background well) MW-12S MW-13 MW-15 MW-16 2/9/2012 ND <0.024 0.034 0} 0.240 0) 0.0240) U38 0) 5/30/2012 ND <0.029 N❑ <0.029 ND <0.029 N❑ <0.029 0.130 0) 8/20/2012 ND r0,029 0.0390) _ 0.2000) ND <0.029 0.2600) 0) = The reported value is between the laboratory method detection limit (MIL) and the laboratory method reporting limit (MRQ. Surry County Closed C&D and Closed MSWLF, Mk. Airy Page 1 of 1 Tables Table 1 Sampling and Analysis Summary August 20, 2012 ADD. I MNA Tracer a m a E m a `" 0 C V ° x [] a C) °m o rr Q V) L) m` Q a m c u, m Co to M m - 0 a w w rn p °'' g rq `r' �' cW o �' J -0 @ ¢ a a LO ZUL Q a MW-1 x x x x x x x x MW-3R x x x x x x x MW-123 x x x x x x x x MW-12D x x x x x x x MW-13 x x x x x x x x MW15 x x x x x x x x MW16 x x x x x x x x MW-18 x x x x x x x MW-19 x x x x I x x x App I = from current 40 CFR 258 Surry Countv Closed C&D and Closed MSWLF. Mt. Airy Page 1 of 1 Table 2 Detections in Water Samples above SWSL, GWP or 2L Standard (Appendix 1) August 20, 2012 Sample 1D Parameter Name + Sample Result Unit MDLz SWSL' 20 2B 5 GWP; Exceedance Date Amount MW-1 Cadmium, total 8/20/12 1.2 uglL 1 i 1.75 --� MW-1 Zinc, total 8120112 21.4 ug1L 10 10 1050 MW-13 1,1-Dichloroethane 8120/12 8.7 uglL 0.32 5 70 MW-13 Trichloroethene 8120112 1.3 uglL 0.47 1 3 MW-13 Cobalt, total 8120112 13 uglL 5 10 70 MW-13 cis- 1,2-Dichloroethene 8120112 29.4 uglL 0.19 5 70 MW-13 1,4-Dichlorobenzene 8/20112 2 uglL 0.33 1 6 MW-13 1,2-Dichloroethane 8120112 0.78 j ug1L 0.12 1 0.38 o.4 MW-15 1,1-Dichloroethane 8/20112 28.1 ug1L 0.32 5 70 MW-15 1,4-Dichlorobenzene 8/20112 4.5 uglL 0.33 1 5 MW-15 Vinyl chloride 8120112 1.8 ugfL 0.62 1 0.03 1.77 MW-15 1,2-Dichloroethane 8120112 0.88 j ug1L 0.12 1 0.38 0.5 MW-15 cis-1,2-Dichloroethene 8/20112 48 uglL 0.19 5 70 MW-15 Trichloroethene 8120/12 4.6 ug1L 0.47 1 3 1-6 MW-15 Tetrachloroethene 8120112 1.8 ug1L 0.46 1 0.7 1.1 MWA S Benzene 8120112 3.4 uglL 0.25 1 1 2-4 MW-16 Cobalt, total 8/20/12 307 uglL 5 10 70 237 MW-16 Benzene 8/20112 1.9 uglL 0.25 1 1 0.9 MW-16 Vinyt chloride 8120112 5.2 ugfL 0.62 1 0.03 5.17 MW-16 Zinc, total 8/20/12 12A uglL 10 10 1050 MW-16 Trichloroethene 8120112 1.7 ug1L 0.47 1 3 MW-16 1,2-Dichloropropane 8120112 5.4 ug1L 0.27 1 0.6 4.8 MW-16 1,2-Dichloroethane 8120112 2.9 ug1L 0.12 1 0.38 2.52 MW-16 1,4-Dichlorobenzene 8120112 19.4 ugfL 0.33 1 6 13.4 MW-16 cis-1,2-Dichloroethene 8i20112 55.1 ug1L 0,19 5 70 MW-16 Chlorobenaene 8/20112 6.1 ug1L 0.23 3 50 MW-18 Cadmium, total 8120112 2.5 uglL 1 1 1.76 0.75 T Table contains Appendix I constituents detected in wells designated by LIIC at levels at or above SWSL, GWP, 2L, at 28 = MDL = Method Detection Limit ' SWSL = Solid Waste Section Reporting Limit { 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard ' 28 = North Carolina 15 NCAC 2B Surface Water Quality Standard for this Specific Stream Classification GWP = Groundwater Prote0on Standard l =The reported value is between the laboratory method detection limit (MDL) and The laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable BOLD = Concentration > 2L Standard Surry County Closed C&D and Closed MSWLF, Mt. Atry Page 1 of 1 Table 3 Indicator Parameter Data Summary August 20, 2012 Parameters Method MDL* Units MW-1 MW-3R MW-12S MW-12[D MW-13 MW-15 MW-16 MW-18 NW-19 8/20/12 8120/12 SM112 W20112 8/20/12 8120/12 8/20112 8120112 8120112 Alkalinity SM 2320B 1000 uglL 52200 90000 123000 65000 53400 1/18107 136000 8020 12000 Sulfate EPA 300.0 2000 ug1L 7160 4790 43200 6650 2690 <2000 <2000 <2000 <2000 Chloride SM 4500-CI-E 1000 ug/L 3770 2960 4860 <1000 29100 <1000 36600 <1000 2360 TOC SM 53108 1000 ug/L 2990 19000 1 34200 2540 8360 9620 12300 1900 2470 BOO SM52108 2000 ug/L <2000 <2000 <2000 3100 <2000 3200 <200Q <2000 <2000 Temperature Field Instrument 0 C 14.6 15.9 138 13.9 14.2 14.8 14.7 14.5 14.4 ORP Field Instrument -900 mV 163.0 118 61 -101 207 19.0 38 193 281 DO Field Instrument ❑ mg/L 3.1 0.5 3.2 1.8 0.7 1 0.9 7.5 3.5 pH Feld Instrument 0 SU 5.98 7.52 7.19 7.33 5.88 5.98 6.13 5.91 5.62 Bromide (Tracer) EPA 300.0 0.029 mg1L �0.029 NS 0.039 NS 0.200 <0.029 0,260 NS NS Sp. Conductance Field Instrument 0 us/cm 310 250 610 180 210 110 310 10 0 Depth to Water Field Instrument 0.00 ftbtoc 22.63 42.29 13.61 0.00 26.36 51.14 26.98 9.48 9.32 Water Elevation Calculation 0.00 Ftamsl 1111.72 975.21 1012.19 1027.05 982.12 1024.82 972.56 973.52 936.95 Notes_ MDL' = Lab Method Detection Limit or lowest field measurement possible. Constituents detected below quantifiable limits are shown as c MAL value. NS = Not Sampled since not required during this specific event Surry County Closed C&D and Closed MSWLF. Mt. Airy Page 1 of S Table 4 Hydrologic Properties at Monitoring Well Locations August 20, 2012 Groundwater - Average Groundwater Hydraulic Effective Hydraulic Linear Groundwater Potentiometric Monitoring Conductivity Porosity Gradient Velocity Rate Flow Depth Elevation Screened Interval Well (cmisecond) (%) (feetifeet) (feetlyear) Direction (feet btoc) (feet amsi) Lithology MW-1 4.30E-05 15 0.510 151 515W 22.63 1111.72 Clay IW-2 4.30E-05 15 na na na na na Clay MW-13 2.06E-04 23 0.177 164 S25E 26.36 982.12 Saprolite MW-18 2.04E-03 15 na na na 9.48 na Saproiite MW-19 i.10E-03 3 0.085 3.214 S15W 9.32 936.95 PWR Minimum 4.30E-05 3 0.085 151 - 9.32 936.95 - Average 6.86E-04 14 0257 1,176 - 16.95 1010.26 - Maximum 2,04E-03 23 0.510 3,214 - 26.36 1111.72 - MVII-3R 2.40E-04 5 na na na 42.29 975.21 Fractured Rock IVV-3 2.40E-05 5 0.192 95 S29W 33.47 987.10 Fractured Rock lW-5 1.50E-05 5 na na na na na Fractured Rock MW-12S na 3 0.254 na 521 E 13.61 1012A 9 Fractured Rock MW-12D 1.30E-06 5 na na na 0.00 1027.05 Fractured Rock MW-15 7.21E-05 3 0.309 768 S05W 51.14 1024.82 Fractured Rock MW-16 2.82E-05 3 0.178 173 S39W 26.98 972.56 Fractured Rock Minimum 1.30E-06 3 0.178 95 - 0.00 972.56 - Average 6.34E-05 4 0.233 346 - 27.92 999.82 - Maximum 2.40E-04 5 0.309 768 - 51.14 1027.05 - NOTE: Values for hydraulic conductivity determined via slug test by GAI. MESCO. or Joyce. Hydrologic gradient from water levels recorded on August 20. 2012_ Wells screened entirely in rock were not utilized for flow directionslgradients. Screens that traverse both rock and regolith assumed flow in regollh dominates. na = Not avaifablelapplicable Average Linear Velocity (Q) is defined by the equation: K d r1 K= hydraulic conductivity where 0 - - - - ne= effective porosity f7 r dl dh= head difference dF- horizontal distance Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Appendix A Laboratory Analysis Reports Chains of Custody Pace Anarynul &—I n., M. Pa44 AnaryuwN 9♦ 1i.e. I.., Pan A-IVNul fervlaes, l". 4 Poo Aratyoor 5.Mcee. Mw. Fee. A.elyum l.nlnr, Mr. Plate Ansl youl Ban l[ %, Me. acekWyhcal ms r.. curve. ne.d-sw.A 222sa .rw. nr taco KMcer �. ew.1pp ceAna�ytfca� sr se.tw.m. . sw.a x27s R.reM. s.y1q ^riK•M r Pr. Etl.n NC 2'+7ae NPa.ur. NC M&M K.—A.. NC 7 7! II �,,,.,,r,..�.,„, Eeen, MC 7129E ,wurel., 4C xaeoe Ic.n..P... +tC mole IMIPM W Iniay7la-7111 tlrKbr S90➢2 + jW)o"401 fe2.054-71M r701]5764W2 September 05, 2012 Mr. Jonathan Pfohl Municipal Engineering Services PO Bax 97 Garner, NC 27529 RE: Project: SORRY CLOSED LF Pace Project No-: 9212a71G Dear Mr, Pfahl: Enclosed are the analytical results for sample(s) recelved by the laboratory on August 21, 2012- The results relate only to the samples included in lhls report- Results reported herein conform to the mast current TN standards and the laboratory's ❑ualIlyAssuran ce Manual, where applicable, unless otherwise noted In the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample anelyte page for analysis unless otherwise footnoted. If yaw have any quesllons concerning this report, please feel free to contact me Sincerely, Kewn Godwin kevl n. g Dow I n@ pacel a b s. cam Project Manager Encld.urn 4.1111� REPORT OF LABORATORY ANALYS]S rnn repen Nao nab W eoPMdO 0 ..�.PI. Ni wr-W M+.rrMn Den 1 PI P ew MIrMeN I--- in[. P opt I of 19 PM)act: SORRY CLOSED LF Pws Protect No.: 92128710 Chwrl;aue Cert+Hcallnn IDS MC Kin c.y Ave Ste 100, Muntenvl4e- NC 2078 Npn1 Crown. Drinting V*tm, CerhRGtl.n /- 1770E North C:rotlna Fl.ld Sonrnw GrSBcW on / 5142 North Carolina V%BI4wwlu Certillution •: 12 South Car011nw Certllcallen III; 99000O01 Aeheyllt. C.rtl7kallon los t225 R—mde N , Ash"ne, NC 28104 FWd7NELAP C4relcawoe 1: E87548 Muw4ehuranS C. 011Cw40n 1: M-NC030 NorM Greene LYlnldng water C4riscallon W. 37712 CERTIFICATIONS Frond. NELAP Certhkptlon /; EMU Kentucky VST C.Alkatw /: 54 wool vir a corl/c.lan /; W VlrglnlaillELAp CeruBeeton C 45DUI No"th cor 0101 wa4teyn1er conleePon 1; 4a South C ,cunt C4MnUn / M30001 Mot Vagina co VAcalm 1: 354 IV VnIP ELAPerawo. cdon ■. 4111U2 REPORT0F LA B 0 P ATORY ANALYSI S 7wr.WO her-1W -.4,t ar0 wit• N. WWWny "M Pr P"s, 11000l SeMu.. Im. P.ge 2 ul Nr Paw AnNI.l b.MN1, I— P.�. An.Iytls.j a.rrlcy., I., P... APMy".:l6m1n1, I— P.ee Ammi ylH.l leMPn, Inc. Pal. A"kV06.l d9iHHi, WC P... A -".I 6.Me.1, Ina, ■ ' Il�tr�' 71N FPN �M.d¢r' ReW .'&.0 A Ii]5 Rrv..W. Ilr. i/OG %jai M.. SW. 1CA a�eRnalytrcal %�'+F. �r M..tlgw R .A - 5� M A 22M RNu Cr OWO K—v A.: 5. 4 100 ���`E ftl.n HC 77id9 +W.rP�. H� 20001 HHnwya;. NC 7A0+1 � Pry iO.R. nC 27200 AN wld1. Nc 3d501 N.nArM.. NL U078 [530Id23d921 I020254-717d i7O4j sow 1196j675a-wit jljM24,7179 1704IA15-0007 SAMPLE SUMMARY SAMPLE ANALYTE COUNT Prolccl. SJRRY :LOSE❑ LF SJRRY CLOSED LF P.co Pral.ct No 921267t0 Pacr Pr6j@Ct No. 92/26710 Lah id Sa pt. 10 Mama Dale Colloctod Wo Rocairad A—Iyr.1 Lob ID Samp1.10 142thod A"IVSL. R.p.A d I..ab—mory W24710001 MW-1 ftlw QW011208 OS 0112$11215:00 32121710002 MV 7N vow usneeI21400 OWV121M. 02126110001 MW-1 EPA SOIO JMW 15 PASI-A %21067I0002 MW425 Vftt.r Obr20112 D9:00 M14216-,00 EPA NOD KJM 52 PASI-C b21241710004 MW120 W-10, 0lfJ011206'SS OW111716,00 6IM WOO SUW I PASI-A 921267,10006 MWA) Willer 0SRWI2 13:35 06721112 IOUO SM 52109 JOH 1 PASI A 011297 109011 MW 16 Wow OWZN12 1200 06721712 WOO EPA 300.0 AES t PAS1 A 92129710007 MW16 Waller 0N20112 II.00 OWIn2 16:00 SM i50"IC E DUN I PASI•A 92121710000 MW-10 yhw 0&7W1200:30 61W2171216:00 SM S3103 AES I PASI-A 3212171000 MW19 Wal.r OMW1219:15 W6+2111216;00 9212VIO"2 MW-SR EPAS010 JMW IS PASI-A EPA S260 NJM $7 PASI-C SM 2320E SMW I PASI•A am $2100 Jam 1 PASI-A EPA 300.0 AES 1 PASI•A SM e504CI-E PMN I PASI-A SM S3100 AES 1 PASI-A 62129710001 MW.12s EPAS010 JMW 15 PASI.A EPA 6260 KJM 52 PAS1.0 S7d$3200 SMW 1 PASI-A SA1 52108 JSH 1 PA5 -A EPA 300.0 AES I PAS! -A SM e500-t.E DUN 1 PASI-A SM 53102 AES 1 PASI-A 92126710004 MW120 EPA6010 JUW 15 PASI-A EPA6200 1WM 52 PASI�C SM 2320E SMW I PASI-A SM 521OR JS}1 1 PAS! -A EPA300.0 AES 1 PAS1-A SM 4500.00E DUN t PASI-A SM 5310H AES I PAST -A $2128710009 mW10 EPA 6010 JMW 15 PAU,A EPA6260 Kim 52 PAS1-C SM 23205 SMW I PASI-A SM 52100 JSH 1 PASI-A EPA300.0 AES 1 PASI-A SM 45MCI•E DMN 1 PASI-A SM 63108 AES I PASI-A 52126i10006 MW1F EPA6010 JMW 16 PASI-A EPA 6260 KJM 52 PASFC REPORT OF LABORATORY A NA LYSI S Paw P119 REPORT OF LABORATORY ANALYSIS Pogo i dI 39 TN..rm. eh" nel M aP• —d. -.pl n W. iN...p¢n MO nal 5..W d—...e.P1 n ". wPr Hftn p¢n..nl ¢I P— An ,�W S.n+Pr. k. .nhmA Nr win rnnwnl.1 P.[.+ 'y9eM 94mwc w • P.ce A-M 7Ikp S:r ftet, lee. 0... Arlalyunl S4rvl.e 1, H1e P.e. A elydnl A.rv1.e., In!• �c�1J7f fply♦!ll�'[3� M5 E.9 M..dee Rc.p - 5M1. n 7M Rr.mq. a MA9 au..a1 Ay. SWe Ida Eden. NC 77:M AAnww.. NC ZM4 HunMf.va4. f cG M71 =76MMQ,e 1 162e r54.71 r6 170-Ars-ow SAMPLE ANALYTE CIO UNT prelnl- SUR RY CLOSEO Lf PI.-Pr910pi N. 9212a710 Anelyle . Lab IQ Sample l0 M.Ihod AMJYala Reported Laboratory SM 2320 SMW 1 PASI•A SM WOO JB+i 1 SASI-A EPA 300.0 AES I Pr151-A SM 4500-C1-E DMY 1 PMI-A am 5310B AES 1 PASI-A 92126710007 MVY.16 EPA 6010 JMY9 IS PASI-A EPA 8260 KJM 52 PASI-C SM MOB SMW 1 PASI-A SM S21PB JBN 1 PASI-A EPA 300.0 AES 1 PASI-A SM 4500-0-g DMN 1 PASI-A BM 531OB AES 1 PASI-A 9213171c006 MW-11 £PA6Q10 JMW 16 PA61-A EFL 4260 KJM 52 PASI-C 5M 232M SMW 1 PA41-A 54 521" Jea I PASI•A EPA 300.0 AES 1 PASI.A SM 4500-CI-E Dryl" 1 PASI.A SM 5308 AES 1 PASI-A 19126710009 MW-11 EPA 6011) JMW 15 PASI-A EPA 6260 RJM 52 .PASI-C SM 23206 SMW I PASI-A SM 5210B JBM 1 PASI-A EPA 300.0 AES 1 PASI-A SM 4500.CI-E OMN I PASI-A SM 53108 AES I PASI-A REPORT OF LABORATORY ANA LYSI S Ifx ricon-a rplb r.pvEk.d..."M n W. *p-n e4"M,P MMPlu Al rrC S.n - page 5 .139 A.pAwYpeal eerrlen, Mc. Pee. A.Myll4.1 Sarrr.al, Me. P44. A> IyfM.I 1. 1l %, Inc. 2eAfWylical' 7M Ent wee.. Refd • I.N A 7225 %r..•rae Ci 9adb K "" S . Ed-. Ed, 4C 272M AehMl., NC 1S 1edn.rPMrr hG 2awo IM)W4921 1871 PS. I178 f 7d 187' WM ANALYTICAL RESULTS Pr9Jeet: SVRRY CLOSCO 4F Pace Protect No. 9212/710 S.MP19' MWA Lalslo: 921267160MI Cabbed: 0MV1206:00 Received: 6M2111215:01 AIas4:VVa1er Re purl P4fbme1el. Reeu114 L"Is LI M MDL Q7: Pr40ered Arr.lYJ:ed CAS N.. Odal M9 Mia 0r9undwaler Aneyd I Method. £PA 6010 Pfepeledun M*M6: EPA 0010 An1momg NO uWL 60 5.0 1 6S12&t2IM. 084M12 DA3 7440.36-0 Monk NO uyL 10.0 S.0 1 0S4&12 ILOO ONQ&i2 V.IS 7440.36-2 Berlum 66.6J uyL 100 5.0 1 OV2511211-00 0Ef2G12 21:13 7440-59-3 5 'ry IMM NO UWL 5-0 1.0 1 0"1&5111-00 0M2N12 21:13 744041.7 Cadmium 13 u0+i 1,O 1.0 1 QBOZN12 II= 00",a 211a 7440J3-9 Chromwm NO ug& 10.0 5.0 1 0612511211.00 064N122113 7440.47.3 Ceblq NO uprL 10.0 5.0 1 ON25r12 06126f 12 71,13 7440-4 4 copper NO uyL 10.0 5.0 } 20 OSIJ&1211 DO OWM2 21:13 7440•50.8 Lead ta* ugrL 10.0 5.0 t OW511211,00 M2611221y3 7430-12-1 Nlcl01 No uQ& 50.0 5.0 1 ON2511211:" 064M1221=13 7440-02-0 $ellwm NO ugfL 10.0 10.0 1 CUM 2 11 -00 ON2&1221,13 77U-A!?.2 Slyer NO uWL 16.0 5.0 1 0646f1211-00 CMZN12 Z1:13 7440-V4 7hellurn NO 00& 55 5.A 1 BMW Ia%1'00 062N1221,13 7440-21.4 Vanedum NO uWL 25.0 5.0 t 0612W$211-00 0646f1271:11 7440-02-2 211c 21.4 uga 10.0 4.0 t 08MM211;OD 062N122113 74eO-664 1260 MSV Low Level Landllll Anerytro%l Malho d. EPA 6260 Acetone NO uDfL 100 2.2 1 064611200:31 U44.1 Acrylom0lle NO ugOL 2M 1.6 t 0M25H2 O0:31 107.13-1 Benzene No oWL 10 0.25 1 M2611200.31 71.4" Br.mephl.r Ih... No 64L 30 0.17 } CON1200:31 14-97.5 aromadTchlorgmemau NO ugk t.0 0.16 1 064611200:31 75-27.4 Bromoferm NO ugfL 3.0 0.26 1 ON26f1200:31 75.25.2 Bro rrat me NO ugfL 10.0 0.29 1 OMNI:! 74•83.9 2 Bvgn.ne (MEK} NO ugfL tD0 0.98 1 064&1200'31 76.934 0%roan dtlul6de No ug+L too 12 1 0M3&12 W-31 M-15.0 Carbon l.t,.. lwld. NO uWL 1.0 0,26 1 0MV 12 00.31 56-23.5 Chlorobenzene NO upfL 3.0 0.23 1 CUM12 0011 $08,941-7 CM.-(,- NO uyL 10.0 044 t M25012 00:31 75-00.) Chlorolofm NO uWL M 0,14 1 OM29120011 61•56.3 ChWr.melhene NO uWL 19 0.11 1 M=12 00:31 74.11-3 1 2•>}�Lrorno-3-ohNroprppnne NG apL 13.0 2.5 } 6N25f12 00:31 16.12.6 OIM9mpchlpromed+.n. NO uyL 3,0 0.21 t 084&1200:31 124.46.1 1 �•Qwromoetl»ne IEOBI NO ugrL 11 627 1 OM2&I200, 31 10S-9Y4 plhr9mprnelhene NO ugrL 10-0 0.21 t 0695112 M31 24.95-3 12•04chswabanzano NO upL 5.0 0.30 I 06251120011 55.50.1 1,4.OkNorobanxeCa No ug1L 1.0 013 1 0&25112 OCX 106a6.7 bane-1,4-Dichlor9.2-0ulahe NO u01L 100 1,0 1 0M2M1200:31 110-67-0 1, 1•Qkhloroethane ND uyL 5.0 0-11 1 012511200:31 75.34.3 1 ,2.Olcmorache ne NO uWL 1.4 0,12 1 0091290'31 lo7-06.2 1.1-Orhlaroelhe no NO ,VL 5.9 0-56 1 054&120041 M.38.4 da• 12•0IMloroalhana No ugfL S.0 0,10 1 0612&120011 156.59.2 lran.•1,2-DI ehlornelhene NO upfL S.Q 0.49 1 OIY2511200:31 IMAO8 5 12 Zicmcropf9psno NO uWL 1.0 0-27 1 0612511200.31 78.97.5 1,3•Dlphl9r9pr9Pene NR 4VL 1.0 0.29 1 OMNI 142-24-9 ae-I 3-Di.NwaVrapene NO ug:L 1.0 0.13 1 0112611200;31 INGI-01-S We 091051201209:17AM REPORT OF LABORATORY ANALYSIS Pe9669139 rn. riven trier not w rea.00r-.a. except n na. wNeul W4 Mn coneont of P. A Iye l e%fr.oe.. Mc Aavm Anil yuval !omen, lna. P.ee Annyeleae SaM-, rne- Pau A�.lytlul O. rrleH, Vne. P.D. Amkydnr a.,wv.a, Inm. P..r Annyn en fervlwr, Ina. P4.0 Avtlyp.al SaMgr, Ma. i'E1IV fQ1 �' Va 205 Eon MmeWw Rard-SwMA 2225 Rr.enele Dr "M KOctr A.. $ure$M ,�;a1ce)AR'?)ytia. 705 E.N Atvnpr RPra• SuavA 2223RN..W.7r 9"N+ vAye Suer 100 Eorn, "C 2r265 Mn.Mm, NC 3006a leew ., NC 2w76 '-PFeYa- Edwl. NC 27M Aan.vri.. HL 3e604 Iw-%-Aa, NC 31075 L)077d071 MI)023-Ml o2z)n�7170 I701Y759062 ANALYTICAL RESULTS ANALYTICAL RESULTS Prolvct: SORRY CLOSED LF Project BLII4RY CLOSED LF P- Probe! No.: C2$26710 pap project No. 9212i710 Lmpia! UVWA Lab 10: /212J7112001 Collected; NMI 120600 paealrad: 012111216:00 Movu Mi" Sampw MW-SR Lou IO: 9212117 s0902 Collected 0W2011214-40 RaeeW40' 062 111916: D9 MWIX 1N.1e+ Rap." Repo" Par.metrro A4..Iw urJta Llmle MIX OF Praaered Anerrled CAS No. OU21 Puomatera Re awn utwN Llnw MDL DF Propwd Malytetl CAS No. dual 11200 M4V Low Leral Lsndlnl Anoirucer Maifod EPA 6260 9010I CP Oreundw.tvr Analyllcd Molihod; EPA 5010 Prap4w6an Method: EPA 3010 3rattIA-3 DIOA-pfop.na NO ugx 1.0 026 1 OKW 1200;31 10061.0245 ArOmony NO uyL 6.0 5.0 1 0a25f12 s1:00 DIINW1221111 7446,36.0 Elhyber.eelrm NO uOrL 1.0 0.30 1 DIMU1200-01 10041.4 Aravnw NO upL 10.0 5.0 1 0a2591211 00 101141 1221 15 7440-16.2 I-Mer.none NO ugfL 50.0 0.46 T O& T200:31 Sol-7" B4rl4m S,1J upL 100 15.0 t 062511211A0 OL02WI225:18 7440-39.1 lodomelhene NO ug1L 70.0 0.32 1 OWN 12 ODS1 74-664 9eryl0um NO WA 1.0 1.0 1 0625l1211-00 9V260 1221:16 744041.7 Malhylanv Chlwlde NO UWL 1.0 091 1 01426f1200;31 73-09-2 Cadrnlurn NO UWL 1.9 1A 1 MV12 T1:00 06R611221A6 744043.11 4•AladtVk4-peMnnone IMIBr.I ND vg& $00 0.33 1 06R911200;31 105.10.1 Cnromlum NO -vt 10-9 5A 1 OVZW12 SSOO Oin&1221:16 7440-47.3 styrene ND upL 1.0 0.20 1 OWNIZO0:31 100-42.5 Cobut NO upL 10-0 5-0 1 06126152IVOO 95R6f122116 144049.4 ,,1,1,2-Te-hi,-11hane NO up1L 5.0 0-33 1 062Sr1200:31 630-203 Copper NO uWL 10.D 5.0 1 ORQW7211A0 OKRA?1221�16 7440.40.E 1,1,22•T6eecnlarcv dune NO UA 3-0 0.40 1 MIMI200:3t M34.5 Levi NO vyL 10-0 5.0 1 0E2671211:00 DE2L1221!1a 7419-92.1 74bachwattiren. NO ugx 1-0 0.40 1 011511206:31 127.164 Nlckd NO uVL 50.0 5.0 1 062571211-M OW6,1221:16 7440-02-0 Towne NO MOIL 1-0 026 1 PM1200:11 101.1E-3 541an1um NO ug1L 10.0 10-0 1 OMNI211100 61114&t221:16 778246.2 i 1,s.Trknlwvalhene NO uDk 1.0 DAI 1 OWN 1200:31 71.55.E 5dyer NO u01L 1010 50 s CI2511211.00 D6r1a15721:16 74411-224 i �,2.7nchlorvuhane NO MOIL 1.D 0.29 1 DIR5112 00-31 79491.5 TWAT rrt NO u01L 5.6 5.4 s OW2511211AO OMQ 21:i6 7uO-26-0 TA:hlorurhen. NO U94 1.0 0.47 1 D62111200:01 79.01.8 Venadum NO VVDIL 25,0 5.7 $ O6f2511271OO 01121U5221,16 744042-2 1lkh1w0uer6meth.n. NO uyL 1.0 0.20 1 Da26n;i 00:31 7519-4 Zinc NO UWL 10.0 WO 1 MW1211:09 0112115221;A 7440.504 12,3•TdcNwpropana NO upL 1,0 0.41 1 Oea"2001.31 96.164 Vl"o .card. NO upC 60.0 0.35 t Da2L12 0031 10e-0564 e2w 11019v Low Lera1 t--dnll AneMkd Meinod: EPA 9260 W,ie Wrld. NO upt IS 052 1 06125+1200;3i 75-01-4 Acetone NO upL $00 22 1 DUM12 WAIL 674&1 Xyl- [Tr.9 NO up'L 5.0 0.66 1 OWW12 00'31 1330-20.7 Ae"hil16a NO uyi 200 1.9 1 OWS112 00'47 107.13.1 Sun00410a e-SrOmoAvvr66vn2ene [3) 99 % 70-130 1 0&2Wli20O;31 4aO-00.4 8en2ene NO uwt 1.0 026 1 012511200;47 7143.2 Dlhroma&-rvm.th an. 15) 121 % 70-130 1 062511200:31 186645 -? lk-cmerem ih- gwmodlcNwomedwe NO ueiL NO ug1L 3-0 1.0 0-17 0-1E 1 1 Dl2521200:47 74.97-5 OW5+tZ 00:47 76-77.4 12-Dlchwrvemvne44(Sl 124% 70-In 1 06n4EN Z 00:3117060-07-0 9rvmomrm NO ugfL 3-0 070 1 OW101200:477&25.2 Tatum. 161% 102 % 70.130 1 O6r2611200:3$ 2037.264 Bromoma4l.na ND uyi 10.0 ON 1 06125)1200,47 74.63.9 23208 A6ea9n Ny Anslykal Ma61od; SM 23209 2-Buts l * 1M Ex] NO ug1L 100 0.1E 1 OW"2 00,47 71-9311 Carbon dlaullde HD upL ISO t2 1 011251120047 75.15.0 A1e.44N. Total a. C.CO3 $2204 ugn- 5000 $000 1 OMNI2 16i1 C.rObn tovauN.1do NO ug1L 1,D 0-25 1 0&2&12 00;47 56.23.5 a Mon San, i day Arta"Gol Maatod! SM 52109 Chloroban2en6 NO ugfL 3.0 023 1 062Sf12 00:47 100.9a7 Chloroa6wna NO uwL 1010 0.54 1 014511200AT 75404 800.5 day NO upL 2000 2000 1 062211204:00 DE2711208:30 ChlaeDrurm NO u911 E-0 0.14 1 OaQ5f1200-47 674116-5 340.0 IC An1oMa 29 Daya Pndyekal McOlad: EPA 30OA Chloro"Iten. NO ug& 1-0 D.11 t 06125012 07a7 74.87.3 1.2•Dlhromo•]-chlwoprapane NO ugR 13.0 2.5 t O6r&1200:47 W12.1 $M11.la 116DJ uWL 250000 20" 1 ON30112 0127 T46D6.79 8 pilfamvahlorametllvr14 NO MOIL 1.0 O21 t 06R 5112 001.47 12446.1 12.Olhromvelhulr(E DB) NO upL 1.0 0.27 1 OE251 t200:47 106.034 4 a6p Chlerlde Anafylkal Maenad: SM 4500•G-E ps(If0momethvne NO UA TOA 021 1 06725l1200:47 74-95-3 Chlvrld. 3770 Mgt 1000 1000 1 PWWJf221-21 16667-00.6 1,2.OIeblorob"rane NO upL 5.0 0.30 1 06121W1200:41 w50-f I.4-Te"Wohsnra'd NO upL 1.0 033 I 084511200:47 106.4E-7 53100 TOC Analytlo.I M4QIad:SM 53109 Irene-1, 4,OIcPdo-241uemne NO upL 1D9 1.0 1 06R511200:47 110.5741 Total OrOurlc C arbor, 210 uA 1000 IWO 1 06R3112 ITAP 744044.0 1,10kNaroe6une NO upL 5.0 0-32 1 062Sf 12 D0:47 75-34.3 1 j•Olclllvraalnona ND upl 14 0.12 1 011R5f 12 00:47 107-06-2 S,I Dlcnlvroethanm NO US& 5-4 0.56 1 0625112 001.47 M354 da-1,2-DluidoroelHane NO MOIL 5.0 0.111 1 06/25112 0047 166.59.2 (Iona-1.2-f7lworoammna NO uOfL 5,0 DA9 1 0L2111209:47 156-W5 1,2-nkhloroprep4ne ND upL 1.0 D21 1 nA11511200'47 76.67-$ I,a-UNor Mop an e NO uU+L I.0 0.21 1 oMV. 00!47 142.2E-9 da•1-3•DrcnloNprop6n a NO uo& 1.0 0.1) 1 Oa251t200:47 1owl -0I-5 Dal.: D9l05ro12 09. 11 Au REPORT OF LABORATORY ANA Lv SJS Pape 7 0139 D.N: 0970a2012 09: 11 AM REPORT OF LABORATORY ANALYSIS Pace 6 of 39 Trwr ewM.1 lwt a..pmeveau I. c.Pnr,n tar.rmpa".h.1-I L. .Pm7d,ie.d...dP M 1v. wtP 0.we cor m.M Of Pmw A -rev" Servvw.. irK .1-111- Tyr, canm.M of P... F Iru- S.M... Ina Pea. An41Yftsl eawl we, Ma. Pale A-Iyn[�l e.W.... me Pan A-wyOr.l amrw r, M. Paw An.1 VOW 6enrrr.r. Inv. Awe Andyo w eerrtaaa, Me. P.e1 Anaryrinr nPrvlw., W. 23ceAnalpical' 205 E.sr M.edaw pa.tl - 6NN A 2225 Al . W. Or OeGO.asrr Ar. sum Ix riL'BAR� IC3�� 7s>.s Eall M..dprr R I - S 1.A 22H Rk~P 9r Ae00 KIn er. Sew 1w -eweib ee. EMe. Tlr, i7216 AN.H'. K 2ee04 1n1A .yew, HC 2trdle Ed.n, NC V26e AIMW, MC 26104 Hunl.,ewr.. HC 2e07a I,M]6234921 ie2612S Ivn (1. p7S•Bn12 17]IIOT]aP7r N163254.75 Ell ila a75•oau2 ANALYTICAL RESULTS pe ).c1: BURRY CLOSED LF Nee Pr11scl No-: 92120PIC S.mai.: I11NA3R ilwvm left La6f0! 52126710002 Results On" Cols Wed: 06720U 1214:00 Report Llmll MOL OF Received: 0112111216:W MOrb.: Water Pwpamd Anelyeed CAB No Oual 62N NSV Low Level Landfill Anslylital Me1hAd. EPA 12aO Ilaels•},]•pctduopran.ne NO OW4 1.0 0.241 1 OL7515200.47 lnoet42-4 Ehyb.nl.na No OWL 1.0 0.30 I 01251t200:47 1004Ii 2•Huan.na NO uWL $0 0 0 411 1 0623752 00:47 591.79-5 Ipd4m.Fane NO I.WL 19.9 0.32 1 06MS11.7 0OA7 1446-4 Mehoane CNOMW ND OWL 1.0 0.97 1 OW55Q 00.47 75.09-2 4•A1.1rn4.2-Aenlllwna lMl BKj NO OWL too 033 1 0M251I2 o0:47 106.10.1 Slyrsne No 44 1.0 0,23 1 0612S112 ODA1 10042-5 1,1,5,2•TalraWo1ca11 en. No upk S.0 031 1 OM2511200'47 630.20.E t.1,3,t :eOsihkrovllene No L4L 30 0.40 1 00251I2 PrOA7 76-u-21 T.trechlanelnena No OA 10 0.46 5 002511200:47 127-t6.4 TOlu4na NO uWL 1.0 0.26 1 Oer7511200:47 1oa-81-3 1 ,",' LTrl wwoarhone NO uyL 1.0 0.4E 1 OWS11200AIr 71,55.6 1,,2•TrIchWoetlene NO OA 1.0 0.29 1 0525112 W;4'1 79.0.5 TTIgl1owa7lene No VA 1.0 047 1 CUM 200:47 79-0.6 TrEGtllpraeualPmelnena ND OWL 10 0.20 1 01250200:47 7549-4 12,3-'rt1011Proprepena NO OWL 1 0 Oat 1 WWI 00:47 96.194 Vinyl acetate 14D qgx 50.0 035 1 OWS1120047 IQa-0S4 V" cil vrlda No u1o7L 1.11 0.67 1 0625112 WAT 75,01.4 xyr.ne fr to NO uyL 5.0 066 1 O12511200:47' 1330.20,7 Suerdyafea 4.9ram 1luw G0an2ena I91 9a Ti 7E/.130 0625112 WAT ►60.00.4 G16remo1W0r0M*thWe 181 t+6% 70•t30 1 1.231120047 116&5314 I ZU6nW1 PMl+0e-d41 S) 12$ % 70•t3o 1 062511a 00:47 t7060-07-0 Tolunna -dB (S) $03 % 70-130 1 OMI200:47 2037.26.5 20206 Alkalinity Anelyurai Malnod- Ski 212DO Atkeenrly, 7alel ee CaCO3 90dp0 uuk 5000 1000 I ON26112 1.!I. 62106 000, 1 dey Aneytical MethodSM 521 OB ROD.5 day ND uWL 2000 loot r 0622l5204:00 OW2711201.30 3 PO.O IC Anka 21 Daye AnWvl-1 IA.tw d: EPA 3W 0 5u11.4 47re0J hill& 75000o .No I ON3W12011T 14101.79-4 46M CbWmd. AnW4CaI Method. SM A500•Ct•E Ch"46 2990 wWL foot IDOD I O910N7221-25 15667-00-0 $4105 roc Amio llcsI mmnod' am 4310E 7ulM C?%-c Conan I►000 UWL 1000 1000 r 01.N1217'31 744044.0 Mf pkta:0m0W2012 0011 AM REPORT OF LABORATORY ANALYSIS Papa 9n139 rN6'. en 00 not be re Pq ed,...pt h IJ .*..1 N.+.naen C-I.M 44 Pep An.ly" 6.r U.. I - ANALYTICAL RESULTS Pr011cl. BURRY CLOSED LF P.ea Plated No. 62121710 sample! MW-126 Lab ID,, 12126711IN2 Cokecled. 06440IT2 09:00 RHAlred: DIIW 1216:00 Mft1w YE111er Report Puml.len Rndle u7 Ll"I MOL OF prapMed Ar1lIW" GAS No- Duel 1.010 1CP 4rountlwalPr Anslylical Method. EPA 6010 Pr.pwmWrP Metod: EPA NI0 Andmony ND OWL 6.0 6D 1 062511211110 04y2611221-20 7446-3114 kuw NO uA 10-0 5.0 1 05251t251.00 ollaw122110 7440-36.2 62nOM 16.01 uWL 100 50 1 0126152 woo 0 W 12 21.20 7440.36-} (WvdMm NO upk 1.0 1.0 1 0125t2 tt.00 OWN122120 744041.7 Cadmium NO OWL 1.0 1.0 1 0112M12 11.00 O&W2 2120 744043.9 Chromium NO uWL 10.0 S,0 1 OM251121100 O612Mf221:20 7440•c7.3 Cohery NO up1L 10,0 5.0 1 OM511Z 11:00 062)f12 2120 W0441 4 Copper NO OWL 10-0 5.0 1 0625112 Ii.00 0N2&122120 744O.X4 Lead NO 'A ".0 5.0 1 062511211.00 0612W122110 700.62.1 Nickel NO OWL 39D 6.0 t 0625112 I1-00 062.N I121;20 1440-02-0 Salanlum No uprL 10.0 10.0 1 O62N121190 MV122120 77424t-2 Silver NO 4& 10,0 S,0 1 OWUI; 11 EO W12M12 21:20 7440.224 ThmhOm NO uP4 5.5 5.4 1 OU25M 211:00 012E11221:20 7440.2E-0 vhnatk m No uWL 25.0 5.0 t t15r25N211.00 QWW t22120 744042.2 Inc NO u04 10.0 10.0 1 CW%1121100 DaQW1221:20 74404" 4210 M9V Lew Level Le.dfui Anelyhni rJelhoa: EPA 12110 AcMane 7.241rp'L 100 2.2 1 O62S11201.03 67.641 AMiunllme NO uWL .00 10 I OW&T20103 10743.1 Seneene ND uWL 1 0 0 25 1 06QIV12 0V03 7+.43.2 Sr9mnd4n0me01ene NO wWL 3.0 017 1 01125l1201:07 74-67.5 SrangdlChlPremelh.ne No uWL 1.0 0.1a 1 062411201:03 75.27.4 Sromogrm NO ugIL 3.0 0.26 1 OIr1.Sl12 01.01 7&2&2 9romomebena ND OOIL 10.0 0.29 1 Oa12SI1201.03 74.63.9 2-11ul.npne (MEK) ND uWL I09 0.96 1 DW*T2 01 03 71-93-3 Canon divulAda tap OOrL 100 12 1 9KNt2 OtO3 75.154 Camon I9eochlorlde NO OpyL 1-0 0.25 1 06126112 01:03 50.234 Chiaw6entene NO uprL 3.0 0.23 1 011251}201!03 t01.90-7 ChWroen.ne NO uWL 10.0 0.54 I O12MiZ 01 OS 75-DO-3 Ch1w.ft- NO uj0L 50 0.14 1 0y25I 1201 DS 57•66•1 Chia -than. NO uplL 10 Vi 1 t112W 1201.03 7A-97-1 t 2-ppamv.l•G+IvrPPrppen. RD up& I3A 2.5 1 0125112 a1,03 W124 QGSt1610ch1ofamathena NO utyL 3.0 1121 t 012L 1201 L03 12446.1 I,2.Omramoelhene(EOBI NO OWL 1-0 0.27 1 062Nt201:03 10943.4 ubtomarnwrwe NO UOL I" 0.21 1 0112611201:03 74.95-3 1 ,3.Dkhlorohentane NO u0L 5-0 0.}0 t ON2W 1201'01 95.50.1 I.4.Dlchlvr00entene NO uplL 1.0 03} ! 0125I120191 106-047 laern-t 4.plchlor 2-hldene NO L%IL 100 1,0 1 0112315201A3 119.574 1,1 •olchlaraelnane ND Og& 5-0 0.32 1 0612W201.03 7S-3 -3 1 2-prehloreemene NO upti. I-0 0.12 1 OW2V 2 01 03 107-D&Z r,1-Okhloro.dnne ND vOrl 5-0 0.5E t 01r2SI 120103 7&35-4 t,e•I,2-D1cMnvel4me 1,11,1 401L 10 0.19 I O621W1201!03 15636.2 Prom. NO NO u6r1 5-0 049 1 00511201:03 1544*5 1,2-OKKwopmpane NO ,.j& 1.0 0.27 1 061251201:03 7&67.5 +,]AI[hrmapropans NO uqi 1-0 0.25 1 o64N1201A3 142-21.1 oe•1,]-Dlcidornptvpene NO uWL 1.0 013 I ON2511201.0} vXMI-01-5 Data, OW05201209:17AM REP ORTOFLABORATORYANALYSIS Page 10of39 Tr. wiled Onµ net Ae ispr w..anpl n el. rw N. will rnn L or Pen Arrlyeev&enp im a�eAna�ytica� r Pael Anaeytl.0 aarvlear, en.• 7O5 E.M ria.daw Rem - a,rd • Paa4 Analydial a-rweea, live- 7775 Rlr-r-E. n, P.e. F.rlydr.l Smwpr, 1-- P6p0'< v Aaa ew- Ipp a�Qlil ra��ra!' A-.- An.fydr rl 2-Ac.., I.r. X' pa.r h.dVrr Re.e - SWIM F Pew F„a1yPCal simpol. Ma. Pau A-Iymed 6m ima, IN. �I%S A-9.0, 0000K vl pee. sues I d Ed-n. NC 277pe F.h-rN- NC Teaaa XunM,Mia. XC 760Tp ' x,neaaer m* Edmn- NC ITI66 FN-uN-. le0 2eaW I..,Y+eraa, NG 7paTa + I lit'erm73-092, 1673123L1,76 r70r1m7SIHM 1]Sajez2dP1, [eI81Ma-717p 064pT3.9d92 ANALYTICAL RESULTS ANALYTICAL RESULTS Prolecl: SORRY CLOSED LF PrGMCL: SORRY CLOSED LF Pace i4.00 M.: IP212671D P.ee Prpjap NO.: 971767t0 !ample: 61VF122 Lse ID: 9212e710003 CP6.clmd: Oa2011299--fld Rfiedwdd D82111214:00 Ma961;M in Sarnpl.: MW120 LAID! 921I6710064 Cvlk ded. 0620112 IM35 Re cEmmil 0171r 1710.00 M.mh VATer ROW Reppn pwmmmre Resuh. LhBs uIrm MDL DF Preprl►d An. to.I CAB No. Duel Pvmmstem R.ruh6 Onbe Llrrit MOL OF Preptaed Ansiyaed CAB No Oua1 126a MAV Low Level LwAllll A.."-i 4e6,pd: EPA 060 Sol MIS Oroundwstar AnatynuI Method; EPA 60t0 PrepmrmGan Melhud: EPA 3010 usrn-t,]•Dkt4oraprOpMs NO uWL 1.0 026 t 06Q511201:03 10061-01d An6mmy No uyL 8 D 5.0 1 062SM 11:00 064611221. R] 744"-a Elnylb4namna ND ugrL 1.0 0.30 1 OMNI 201 d13100414 Amon- NO uyL MO 5.0 t OWS/12$1.00 06261122$ 237440-34.2 2-H*'a me NO vyL 50.0 046 1 0676112 01-03 5914" B.Num E.7J uyL 100 5.0 S =WI2 11.90 OMM2 2123 7440.31.3 I0d0m.Cune ND uyL 191-0 0-n 1 0411M1201.03 74.0.4 Baryllarm NO uyL 1.0 1.0 1 COV12II:D9 04112811221'23 744641.7 M6myte0. CN0r166 NO uyL 1-0 D.97 1 0WNQ 01;03 75-09-2 C.*rk- NO uplL }.O 1.0 1 Oaf25112 II to 06RNi2 2123 744043-9 4-Mo"-2-panempN%*(06118K) NO uDti 1OD 0.31 1 01,251120113 100-190 Chromium NO uyL 10.0 5-0 1 OWN1211.00 OW4012212a 74aa-47.3 Styran6 NO uQ& it 0.29 t OW511201'03 100-42.5 t04411 NO-M& Ina SA 1 OWN 1211:00 01,71V 12 21.23 7440-46.4 11,1,2-7atzhimnounane No uyL 6.0 0.33 1 062511201.03 61O-Ia4 Copper HD uyL IO.o 5.9 1 0625M 11;00 PKIIII221;23 7"040.8 1.12,2•TemacNarpaelans ND uyL 3.0 OL40 t OSR51120 M 79.34.5 Lead NO uyL MO S.0 1 06Y,(5152 O.LOO Oa2611221,23 7439.92.1 Tehschlsroalnen- ND uyL IA 0.45 1 OMWI201195 127-1a4 Nlpy.l NO uyL 50.0 5.0 t 06250211.00 GUM 22t.23 7440.02-0 Tearm► NO uyL 1.0 0-26 1 OW511201,03 10".3 Selertlum NO uyL 100 IOD 1 OWNIZ II= 06461122%73 "4249-2 1,1,1-Tr1rnWrnemena NO uyL fA OAa 1 08751120"3 71-5" S.Iya• NO vyL t8.0 5.0 1 0WV12 wOO 0WVl22$ 21 7440.224 1-1,2-Tnddpr0eei.ne ND ugfL 1-0 a.29 1 aanVI201-03 79-013-S Thmthum NO uwt 5.5 5.4 1 062511211-00 OL21VI22123 7440-284 Tnahleraethsne ND uyL 1-0 0.47 1 OKV12 01:01 79-DI.6 vAnauum NO u01L 25.0 6.0 i 06fJ5.11211-00 GOMM Mts 7440Q.2 T11ChI-Agarpm-1h4nm NO uyL 1-0 D.20 1 061751I201:03 75-6>t-4 the NO uyL 10.0 10-0 1 0e12611211-H OWNI;!1123 744CM-6 1,2.y-Tr[[hlwppr0p.ne NO uyL 1.0 0.41 1 06261S2 0113 96-16-4 NO "0& 60.0 0,35 1 owulI01'03 10"W4 624D 1d94 Law uv.I LandlHl Msty6cml Me mod; EPA MOVnN+cel.r. M1nyr LAIN Wa NO uyL 1.0 0.62 1 062912 a1'03 75.014 Acton. NO uyL 100 22 t OSWI201:19 67-04.1 %ylene(ToUO NO uyL 50 0.66 1 OWU120S:O3 1330-20.7 Actyianhrll► 40 ugq, 200 1.0 1 66=1205:16 107.13.1 Sewruparea Bantwe ND uyL 1-0 025 1 OMNI?01; 10 71.42-2 4-Bremasumeb-n..ne(8) 97 % M-130 1 061251120"3 460-00-4 OrOmv�laromelh... NO uyL 3-6 0.17 1 OWN12al: 14 74-97-5 dhrem011..newnethen- ISj 114% 70-t30 1 QW91201-03 IMB-53.7 S+vmOdlchwromethrna ND uyL 1.0 0.18 1 OWW12 Gill 75-27-4 I2-DwNwo.lhsna44 13) 119 % 7(030 1 0a11511215"3 1705047-0 I3'0"wrm ND 4911- 3-0 O26 1 I)SIM12 D1:10 7636-2 talume-de IS) IN % iQ 13a 1 0645r 12 D1-0D 2037-26a BrOnwrnae,sns ND uyL 10.0 029 t OWN 1241:1a 74.04 21m Alaalkllry An&W.I M.tnud. SM 2170E 2-8viAnm. IMEKI NO uyL Ina 0.96 1 06=112 01-1a 76.9E-3 C41bm dleulede " WA 100 S2 1 0645112 01:18 75.15-0 Ar"", Te1.1 a6 CaCO3 123000 uyL SDO0 1000 I D51Ia112 16,05 CamwI letrad,rande NO uyL 1.0 12.25 1 9N25112 al; Ia 56.735 62108 BOA, i dsy Anerylkrl Methad: SM 52i08 CXNromenzane NO uyL 3.O 0.23 1 OWN12 Ol:la 109.90.7 Cnyraa6,ene NO uyL 10.0 D.54 1 062311201-115 75-00-1 BOD, Sday NO UqR 2000 2000 1 OSQVI70470 DW?;l205'30 Chla'010- ND UyL 5.9 0.14 t OWS01201311 6746.3 ChlOremel,.ne NO uyL SA 0.1I t OWN12 a1:1a 7467.E 760.07C An10na 260sys MnyllOal MadMd EPA ]DO.O 12.Oyrvltlo-]-cnwroproprne ND uyL 13.0 2.5 1 062511201:16 W12.4 wbid 4320ai uyL 500000 4000 2 0OW121Vail 14696.7941 Duamochlat"41hwe ND UgR 3.0 0.21 1 O 2511201:18 124i6.1 12-Dbeempelhens iEOBI NO uyL 1-0 0.27 1 OWN12 01:1106.93.4 4600 Ch10Ads Ansykal Method' SM 4500•0FE D1brd""6%sns NO vyL 1D 0 021 1 06r&l2 01:1: 74. 5-1 Chbndt a6ma uyL IODO IOU t o9107J122126 16867.00E 1,2•prNy0pen2ene NO uyL 5.0 0,30 1 OL254 t201:10 9S•50.1 1,4.OkMervbrnTm- ND uyL 1.0 0.33 I 062511201:16 106�6-7 $2100 TOC Analyl["k014lhod: SM 531OE lrr,a-I,4•DIWxO.2•bulene NO uyL 100 1,0 1 OWS1129f:16 110-57E Tp1.l C gank C.rb- ]42Dp uyL 1000 1000 I OIftL52 17:5i 7440-4iA 1.I-OkNuoslh:: NO 41L 6,0 0.32 1 OWS112 all:18 7i-1i-3 12-0khlprveN.nr NO uyL I.0 0.12 1 0625+12 OS-16 107.042 1,1-❑kmwemthmne NO uyL 5.0 Om 1 06RSr1201.111 7S•35.4 ele-1,2-010d.Oelhmne NO uyL 5.0 0,10 1 Oa12S112 D1:Ia 1554)9.2 Irmn6-t.2-04chloroemene NO uyL S.O 0.49 1 062601201-11 t69E0-5 12-picnl0r0pr0pane NO uyL 10 0.27 1 OW&I2011a 76.97.5 1,3-Dkhl6rgtrvpans NO uyL 1.0 0.21 1 M311201!$1 142n711-9 ds•1 3-Didd0t0pr000n. NO uyL 10 013 1 OWN1201:16 IMI-01.5 Owe 09 OV7017 DO: 11 AM REPORT OF LABORATORY ANALYSIS Pape 11 0139 Owe: 09105/2512 09.17 AM REPORT OF LABORATORY ANA LYS IS Page 12 6136 Tm n0w1 Met iwe Im ,.PP ed. erupt n M, ttra rapen ✓iat mi w lapmdurad. -cape In rye. wlegytM M1Qwn wn-ant pl Pau A,ylyeral Sr rvr.e Inc - t-I M -imm a-n.- 1 el Pee- Amlyea-i S-nnn.. Ine AlCe A.1a1 y+16M aaMeta, Ina P... A- vu..1 Sarrrna, Ine. P.c. An..yric,i s.nic.,, ine • Osee A"yae.l anw eat, Me. Ale. A"yaear =troe.r, lne P.w. An4yae41 a.rvi4.m. ne. n' : aceAna� �4aIa 206 E.ml hw-=p Road . S. 7725 Rnrnd.0 gap xv.;.r n.. „it : 4 p,,�+ �❑ Yf fp! �1 Pl I 196 E.n4t.dat Rew - SWH A I22s Rht .q. 3r GM N.nc.l A. W. too .w a+ Egan NC 272ea Mn"W nG 26av4 Hun4l.na.. K 7007p .•' P.a ueaY➢. oem Ed.n NC 27204 M ..n. He 2W /N. W.. NC 2au15 r33am2a-Dual i621u�4.7175 i7wH}YSWY 1336ia774W71 1426954 7175 17p4}a1591322 ANALYTICAL RESULTS ANALYTICAL RESULTS PMACI. SIIRRY CLOSED LF PraJact Sl1RRY CLOSED Lit Paw hqW Nu, 92121110 Pau Pr0j.d No. DPW 10 7amph: MW-120 Laeltl: a21ZOII0004 Cva-led. 0e20A206:3i Recowed. OS12f11219.00 Maine Vaiv Sa P1a: MW,13 L.tr ID: %31 II71 DOD Cnllectid: Qa2D+121135 R.odv-d. 9e211121U. 00 MAWS Mia, Repot Rapoil Pa.Rm4Nra ROWAN l/nW Umi1 Am DF Prapmred An4lvmd CAS No ❑..1 P.M-1.n R.wa. fln+h limit MOL Dr P=ryar/d AAAWld CAS N. ❑wN 8Y60 MSV Low laver Lan+IrrO Analylleal Method: EPA 9260 6010 ICA 0roundwml.r Aso"cal Method: EPA 4501➢ Prapa+lovn Method. EPA 1010 naha.+,3•pldilarOo0pene Np rapt 10 026 1 DW511201:18 10061-02.45 Anelndny NO pWL 0.0 50 1 OW2511211-00 082811221:29 744045.0 Elnykeniene NO uWL 19 0.30 1 oaf2S11201. to 100-41-4 Ai -le ND up4 f6.o SA 1 OW2511211U6 08R611221:7:6 744078.2 2-HamsnOna No uofL 500 0.48 1 OW2511209;10 S9r-76.6 lidrwm 87.3J 1ipR 10O SO 1 Oa2511211-DO UWW 1221215 7440.39.3 rpdomathmna NO uofL 10.0 0.31 1 08R5112 al:ta 74.88.4 OWYOum NO ug& 1 0 1.0 1 ON2511211 Da 0eRN12 21T6 7440-41-7 W"rane Crderld. kp uWL 1.0 0.97 1 O825f12 01 1S 75.09.2 Cedmum NO uWL 1.0 1-0 I OU4511211 00 Oar2art2 2126 7440�3.9 4-Me1ryl-2-p4ntenone(MdEIK) Np UgIL 100 0-15 1 4W25112 as.+8 101.10.1 Chronlum No uWL 10.0 50 1 Ov2N1211.00 0,M12 21.29 744W7.3 Sgrran. N , "U,-1 0 025 1 084VI2 O1:16 109.42-6 CcLmil 114 .0k 10.0 5.0 1 M7S112 11-90 Muir 2 21:If 7440.48.4 1,f,1,2.Tetrarhlveoeplan. NO Vok 50 cm 1 0&257+201-16 630,70.9 Znppar "D uyL f0.0 5.0 1 06f2N1211 A0 W2N1221�26 7440.50.a 1,1 �,2-TekadapraaIN NO uWL 3O p.40 1 canWI201:ta 70,34-1 Lead k0 u01L 10.0 50 1 D&US11211.00 06 W221123 7430-92.1 TaY.ca.la.veth... No UA 1.0 Q-46 1 1 6WIWI2 01,1a 127.154 Mcli el No DrL 50.0 S 0 1 06fd5f12 11.K DW2a712 41;I 744C, 2 0 rplyene ND uWL 10 026 1 0"W1201;10 106.ea-3 p.l.nMm NO N04 10.0 100 1 W250211:09 OW&i22126 7762.49.2 1,IT.+ TnonlvrvaO.ane No uWL 10 (IA4 1 ON2511201;16 71.65.E 59yer NU uWL 10.9 6-9 1 06I25112111)0 OLT&i22126 7440-22-4 11,2-Tlichlwoed+ene ND uWL io 029 1 pa4S112011a 7Y.00.5 Thmbum NO uWL S.5 5-4 1 OAg5fl211.00 MV122146 7440-2a-0 iriU+ler pathane N0 VOL +.0 0-47 1 0&i511201=1a 79.0+.6 Venmdv+ NO UWL 25.0 5.0 1 Do W1211 DO OWN 122125 7440-62-2 TrlChlwpSupramamane No Von-10 020 I 46f25f1201:1a 75-60F4 ih+ NO uWL 10.0 10.0 1 0625112 W00 09W1221:28 744066-6 t 2,3-TmeplaOWr pena ND uWL 1.0 041 1 oa2W12 01.1a Will-m %F-0 actrale NO 4WL Soo 9.35 1 Oa25112 DI. IA IQa.u6-1 Level Me V Low L.l L.nd}III AnWyBCe+ 14aa.dd: EPA 6250 Vnyl Ohlor.de NO uWL-0 0.62 1 pe2S112 pt:la 75.01.4 A.cetnve NO up4 1QO 23 I aIr141t2 p1.34 6741.1 f,+lin. ITnull ND up1L 1.0 o.86 1 96MN 20f-18 1330.204 Arylu.+nrn. NO uWL 20O 1.0 1 0112N t201 .34 107.13-1 Surropales 9anaeve NO uWL 1.0 423 1 082511201:34 71.4Y2 4-&o0•v5uvr DO-lens(5) 18 A 10-1317 l 0625/1201 18 A60.00a &omoenla+nmelhene 00 vQ& 3.0 0.17 l W25r1201:34 74-97.5 Do, ormRvvromelnan4SBl tit % 74139 1 Oa2511205:7e 1666•S3-7 OrvmpdWarpmeth4ne 40 uyL 1.0 D.fa I am" 20134 75-27.4 12•Dichlorveth6he-d4 {5) 121 % 70.139 l as gromoforfn kD uWl 1.0 Q,2 0S261}2001,34 75-252 ivlu.na-d6 for 103 025122 8romomawan4 uy 0.0 6.2 WAN 2;34 7h639% 23208 Ar116Wnily Amal"alµ40104-SM 23206 2.8udnpn. fMEKI NO Vpk 10O 0.9E 1 DNZW729134 76-93-3 Ceraan Aiaullde NO uWL 100 12 1 Qa125152 Oil U 75-15-0 AluWVL Taw am C.CO3 66000 UWL $000 1000 l O62Sf1216:12 Ca rhlx.lalraehledlda NO uWt Io Q.26 I 9a23f52 0134 56.23.5 521 DR ROO. 5 day An41vkal Method. SM 521 OR Chnlo6anaans 14+J ugil 3.0 0.23 1 ON25152 01:34 104.90-7 C14. *l..na No VOL 10.0 0.54 I OI2a112 01:34 n 00-3 500. 5 day 3100 u01L 2090 2000 1 0N22f 12 94:00 0a27112 06:30 Chloroform NO Vg& 5.0 o$4 1 ON2W2 01:34 GT-W3 300.0 IC Anion. 214aya A -".I MaMnd EPA N000 Cxklonlf%-e 0 u 1 N250 1200134 14.61-3 5cnopna lorar Np uWl 130 . 082&t3,34 9G+2•a1"Ibromo- Su1Nle 6660u ..WL 250000 Woo I Oar30r12 02.31 14e0e-79.0 Diwnm efiloron,oth na No -WL 3.0 0.21 1 DLQ501201 34 724-4&1 l,2•Drramae9+ane MORI No QA 10 0.21 I 0N2S11201;34 10"3.4 4500 Chlondr Ans"cal Ma9+o0: 3M 4%0-Cl.E plorowr mp+mna NO uv- S-0 IS Q.21 I 0SJM,2 01.34 74-P5-3 ChWda NO uWL 1000 1000 r UMM1211j30 11540.9041 12•plchtuaeatronm 0J uWL .68 5.0 0.30 1 0KIP12 DI 34 05-50-1 1.1•Dufilar ebeniane 2A uQ& U 0.33 1 O12N12 01 S4 f06.46-7 $3108 Too AnelyLtei M►m.o Sm 3110a Irena.t 4•Dllmdlrr2•trulan! ND up11 100 1 0 t Oari'Y12 01 34 110.57-0 Tortl ❑r0an10 CPO- 2640 uWl 1009 1p09 S o"W214'11 7440.44.0 1, 1-0Khrorvmthanm 6.7 uWL 5.0 0.32 + DWW 211:3A 75-54.3 1,2-D60,19M than4 0.741 uA 1.0 0.12 1 0112S1}201:34 107.06.4 +,1-Orehl6r6tutene NO uWL S0 0.56 + 0828r1201.34 75.35.4 da•1,2-DlcNocualhenm 21.4 uWL 1.0 0.10 1 O&M ;! 01.34 155.51.2 (I...•1,2-DclWWpalhene No.0& 5.0 Q.49 I Ohl I201-34 5564*-S 1,2-okN:oMpane NO uWL 1.0 027 1 0NYW1201:34 7F67.5 1,1•pkhloropio an e NO uWL 1.9 0.211 1 OWW 2 01:34 142-MO da•1.3131Worppropena NO uWL 10 0.r3 I Wzv12pl:34 10061.01.5 n.1a.091ow2012go. 17AN R EPORT 0 F LA13 0 RATO RY A NA LYSIS Pop 130r39 Data. 99ru54101209:1?AM REPORT0FLA80RATORYANALYSIS P4pet46130 Tart r.M, IA" W- �vae�<n. naol...a tlnr.wn ww n Ve i.wesae. t,.. Wa M- r. ' W r n eaewel nr.ert An.iy4ni Sa Tyra., 1M wnpat 0. w4 ten el Pad Atil 141.N $.nAq.. 2ceApaVicaf' 1-1-, Inv. Par 6 AN ly7laar S"I"1, env Pau Anatydul Sa ml re r, Inr. Pra Annypul UM en• Me. Pa.. ArJlyucal f.rvlur, Ine- Pa.. AhMy1Na16.rvrdu,MC. 2"E..t M.Aevw Re.d-SWuA 222d RnrrW. dr. 9m lOnea7 A.va S�.ra l0c qn r� RLQ maj 1 `W�A 3Q5 E. NrrWwrloW -SuelA 2228flN.rrd. i/f Pala i4 rAe.. Suer 1W 1' yy Egan, NC 271M Mhwn., NC 20W, ii-b A., NC P6076 +ry: Edon. NC 27M A.hhM, NC 29004 HunWr l.. NC 76074 f Ple]623der7 iaXPA4-7176 (raeer75-9092 1 fmlG23Emi r62612347176 (70ryy754m ANALYTICAL RESULTS ANALYTICAL RESULTS P *.L SURRY CLOSED LF PM)acl: SURRY CLOSED LF Pace Pt*d No.. 621207/0 Pope PrcHn Na.: 0212e71a San.p14: M%V-13 Lab 10: 1212171000E Calacted: 0l2011213:35 Rataived' 092111214,00 Mello-y6tat Sample: mW-11 Lab ID: 12126710,M Co6eclad, 0612M272,00 Rocalrad: 01121 f1216:00 k141k VAUF Repen R.pen Farwnatay Reaaaa urm UrNI MOL OF Prepwad Mafyred CAS Na. Ouw Paramaten Resume Lkxd Llmll MDL OF Arepwed Ana"d CAS N.. Oual 6216 YSV Low Lawol LwmVill Malytical M.emd EPA $200 401E ICP Oro-dwaler Anaty0sa7 Memod: EPA 6010 Pr.pAratipn Math.& EPA 301p tlam•1.34)lcNaopMpana NO up+L 1.0 096 1 041WQ 01:34 W061-02-0 An4mony NO UA 1.0 5.0 1 0612511211,01 01211122E-30 74:..0 Et11y01enrana ND UO& 1.0 0.30 I MWI201144 1,00.41.4 Ar.tervc NO uWL fa.a 5.0 1 a61m,211 AO ORMI221!30 740.36d 2-H.aanone ND uglL 50-0 0,4E I 0V2511201 '3591.7E-6 9whlln 39.3J vWL 100 6.0 1 M91211,00 OSW$221;50 7440.393 lodom4%ma NO uWL 10.0 0.32 1 06/25/12 01 ad "4'"A BervAum NO uQ& 1 0 1 S 1 Q6g5112 11 6a OWN,? 21:30 744q-41.7 M*lhylan. CNarld. NO uA I,0 0.17 1 064L51120%14 75-OW7. cmdomum NO uyL 1.0 19 1 d2 O5112 It;00 06261122%30 744043-9 4-M.my1-2-pamm�one (MISK) NO uWL too O.SQ 7 0825112 at94 106.10.1 Cheomkrm NO ug1L 10.0 5.0 1 OMNI211M o6aV1221:30 744047.3 Srylene NO uyL 1.0 026 1 064571201:34 IDO42-5 Cabell 9.7J up1L 10.0 SR 1 MOP 211 AO M811221,30 74404114 f ,1,1,2-T.eaGllawelan. ND v S,Q 0-33 1 0142Sf1201:34 53040-6 Copper NO uWL t0A 5.Q 1 06r2521211;00 Oer21n221:30 714♦>-9p•6 1,1,2,2•Tatrachto- un one NO ug& 3.0 0.40 1 D62R1201:54 79.34.5 Lead NO uWL to.0 S.D 1 OWN1211 00 0e29fl221'30 7430.92.1 Tatrad�broe6rene NO ugeL 1.0 0-45 1 06125E1201-34 127.184 Nkkel NO ua& 50.0 50 1 =25U 11.00 062111221130 7440-H-0 Taluen. NO ug1L 1,0 026 1 D612&1201:3A 10¢d6-3 Sel"mm ND ug& 79.0 100 1 06Ru1211.00 01RN122T311 7762a" 1,1, 1•Trkheya6mm. NO uWL 1.0 0.41 1 a8231 t2 at 14 71.55.6 Slevor ND -WL 10.0 5.0 1 o6Rvv1211:00 WWI 221:30 7440.22Hf 1,f.11rn uo61hana NO 4& 7.O Dit I o6r26r1201:34 71•D0.5 71%dlum NO up4 S3 6.4 1 06f7"711 00 OU21V1221:30 744620-0 7rlchlawrhana 1.3 K& f -0 0.47 ! OU2511201:34 mol-a Vanadium ND uWL 25.q 5.0 1 0612511211:00 O6r2611221:3a 744M-2 TrlehlorolpoFam.man. NO uyL La 020 1 061201:34 75.69.4 R51 Ilnc NO uWL 10.0 10.0 1 OWS4211;00 062e11221,0 74400-9 12.1-Tnchlwepropane NO uWL 1-0 0.41 1 OWN,291:34 9616.E Vinyl AC.t.18 ND uWL 50.0 Q_u + OW25M2 0114 10605-4 8260 MSV Love L"O Landfill McMkal M.IhedEPA 8260 Velyl chla de NO uWl 1.0 OA2 1 CLOW12 0114 M014 Acalona NO N& 100 22 1 0MU12 01-50 97-64.1 Xyl.ne [Ta1aq ND uWL 1.11 O!6 1 OWW 12 01:34 133620.7 A1ae0l1e Cry NO UA 200 1 9 1 01126112 01:SD 107.13.1 3uf "Alan Earlrena 14 uDL f,0 a26 1 a62611201,50 71.43.2 4•Bmmofuao6anrm119) 11 11 70.i70 1 052L12 Q134 460-00-. 8r¢rr�ocNorometnana NO uyl 1 0 0.17 + 0625r17 OI:SQ 7i-97.5 [MbrnmR 6uwoM.lh.n. la} 11 ] % 70.130 I a6 V 2 01:14 16a6.53.7 6ramaAChlorernetleAna NO uyL I.0 0.15 I 0125112 01:50 7s.27 a 12.D1thcac.lhan6•w f9y 121 % 70-110 1 06125M20134 17060-07LO 8romofirm WD VWL 0.2E 1 0&*5M201:50 75-25-2 Te1u.n.J6(S) 104% 70.110 1 Ol4251t201:34 2Q37.25.5 9ramamadlana NO uWL 1010 0.21 1 05425f120110 74-134 23208 Allulln7ly An erytkal M.th.d SM 21206 2.Oulanofl. (MEK) ND uyt 100 Q96 I oordvt2 01;50 71.13-3 Carhnn d-Mda ND vWL 100 12 f 03251T2 at:" 76-15-0 A1ka4nity. Toler as CaCO 3 13A00 uWv $ 00 1000 1 own 12 W16 C lfaan latrachlorlde ND UA $.a 0.25 1 am 1201;50 W233 12108 000, 1 d.y Anelyucel Ma61od: SM 52108 Chrorapenren4 2.6J ug& 10 0.21 I. OM12 0110 1Q640.7 Chlereedlane NO uOit 10.0 0154 1 06251720110 75•OC.3 000-5vey ND �g& 2000 2000 1 DUZV120400 OU2711206:30 Chloroform NO vgrL Sp 0,14 1 05Y251120110 67.6E-3 CNoromeTane ND uVL 1.0 0.11 1 0625112 0730 74.373 ]OOA 1C Anlom 26 Pay Mafylkal Ma6ro d: EPA ]OQ 0 12•DOromo•3•cnloropropan. NO uy 13-0 2.5 1 OR271120,-6a 9612.E Wool.2190J uWL 250000 2000 1 OW301120249 f41Q671?4 Dlbrom chlnromelhena NO uWL 3,D 021 1 06R511201;50 12445.E 12.Oleromoefdme(EOSj NO UWL 1-0 0.27 1 OWW1201.50 7q6-03-4 4600 Clrhnd. Malylkal Mfh aed: SM A500-C1•E plhram6maarane NO uy+L 100 021 1 OSYL5112 Q1;Sp 74-90.3 Ch%F*o 2616a uWL 1000 1000 1 ORM4012 79:32 t6667.00-0 1,2'OI<Nmotonadne NO uWL $.a 0.30 1 OM511201:50 15-50.1 ,,Olchlordhmxena 4.6 uWL 1.0 0.33 1 Oe251124130 106J67 13109 TOC Analyucal Memod! SM 53WS trans, 1. 4•Dlchlwo•2.6utone 40 upd. 100 1,a I Oe2S112 D110 710-57-6 Taim Ol game Cub- 6060 uWl t000 7g00 I 06i271121621 744644-q 1,I-DK+tlaoe0lane 28,1 uWL 6.0 0.32 1 0542611201-50 M34.3 12-Drenlwae lhena 6.e6J u1yL {,0 0.12 1 01R6f12 g1:S9 19706.2 1,1-prcNwoeOrena NO ugx 54 00 1 06f2511201:50 71r35.4 W-12-Dlchl.roelhena UA ug& 54 0,19 1 0625:11201 So f58-SS1-2 tML• 1.2. Okhlor0-U'_r NO vg& 5-0 0.48 1 aans 12 01,50 156-60 5, 1 ,2Archloroprop.ne NO uWL T.0 017 1 a1f26r12011D 7667-5 13.Olrluoropro0anc NO uWL 1-0 0.28 1 0442E 7201:50 142369 df• 1.3.0I4Mr0f0pr0p ana NO uyL 1.4 0-13 1 D625112 at10 1006141-5 Oak. 00105201209:17AM REPORT OF LABORATORY ANALYSIS Paoa 15 of 39 Data: 09r051201200 T ?AM REPORT OF LABORATORY ANA LYS IS Papa 16 of 39 Tree r.P.n Ad nee M npreauutl,.-Pt N M. YN. r.p.n N.1 MI W lopfodue.d-.-rapt n M. .004e . o.ne.M.r Fava A-Lni..l tH rvlw.. inp . w�v,W y . wnlrn -, W P -A AN P'y Sa- nc Poo. A nmiyemm1 l.Mey, inp, PA.- A"Ppv l7ery lte/. tAc Par. Aomirk.l a.ryfMl, in. )72 rL"ar tiO NH Wood. nom.3„% A Z226 RNv Or ➢omn, rA.1 sito!dC rn �yy�mra. Fo". NC 2176E A.w-NG 7a8W Ir.nyrmW4. NC 2oo76 i334162-892, 1261231-1174 4T 147SapfC- ANALYTICAL RESULTS Pasted SURRY CLOSED U Alc. PlvJeot Nv.- 02123710 sample: MW-18 Lab lM 921211710006 CvEaded: 04=112 12-00 Recetyed: OKIM21000 Map4: ',*tar Report Pmemelerl Reaulm urem Llmi MOIL OF Pt4owed AnoNloo CAS No. oue1 anal AIRY Low Li- 1 Land Nil Melytlm Mvel9d. EPA6250 I,-.- 1,3-plprler9prup.ne NO uoi 1.0 0 26 1 M5012 01 50 10061-02-6 E"lbentene NO U*fL 1.0 0.30 1 OIRV120t60 19041.4 2-Ma.anone NO uyL ".a D 46 1 NuzW12 01 50 591 •T6.6 1 Wonnlmm�r NO UOR $0.4 0.37 r 08025J42017M 74.E" MNhylene Ch,mL'la NO ugh 1 0 0.97 1 0625f 12 01-50 75.01F2 A -Me HW1,2•Pi h tonane(MIpK) ND UWL 100 031 1 Mu DIM 109.10.1 Styrmnl NO 4& 1,0 0.2e 1 QUM$201:50 10042.E 1,1,1,2-Tetreanldr➢ellanm ND uyL 5,0 OM 1 0VW1201:50 630.20.6 1, T,2.2•TrtracMorvothane NO UWL 1.0 04O I aW511201:60 7934.E A91Ctll47ea61rnr 1A ugh 1.0 a 48 1 MU12 01:50 127.14.4 T➢lyana NO uyL 1.0 026 1 06J25t1201;50 105,4&3 1,}, I-TIIchlgoeElwlr NO Lag 1.9 046 1 aW 25f 12 DI:50 Ms" 1,12-TaclhlamotinE NO ugfL 1.0 020 1 OeY16f12 O1:5c 19-00,5 Trliuormm9lmne 4,6 ug4 110 0.47 1 062511201150 7s-01.5 hlndvrelumomeglana NO voL 1.0 020 1 a6R5l1201-50 75.6g-4 }2yTn5M1le.ipr➢pmna NO uOR 1.9 0.41 1 062L1201:50 W?4-4 Vlnyl acedle NO uyL 00,0 0.35 1 0623l12 01.50 108.054 Vlnyl chloride 14 MOIL 1.0 0.62 I MV12 01:59 75.01.4 xylrne (Talon NO UWL 1.0 ON r OE12Sf12 01:60 1320.2p.7 5u p.feo 4.flrmnar➢0100en tan: (9) s1 41 70.130 I 682Sf12 DI 50 Ailc 4 plhrnmeEuoromvlhmne l Sl 1104. TO.150 1 06f23f1201:50 1069-53-7 r2-I}Iohl¢roethenr-d4 (5) 117 % W30 1 MRSf1201-50 17060474 Taluane-da(sl 103% 70-130 r OWN 120r:60 2031.26.5 2Me AhA4,l Oy AI1elylleal Melhad. SEI mia AJkfmniry, To 111 as C00O3 31100 uyL 5000 1000 I 0613WI21)-ifi WOO 080, E ay M00-1 M.hmd Sµ 5210E 600.5day 320 u04 2900 .004 1 OW2211204100 MV1208.10 300,0 tC Ankm id Dayi Anmlylleal Mo6md EPA 300 0 sulror. fop uyL 250009 2000 1 030011201.02 14108.7241 4500 Chferlde Anpy-moi Moviod: SM 45a&CLE cMwMr NO uaq, IOU loop 1 09M I12 ISM 16667-004 63108 Too Analocal Mmoa: SPA 5110E I" otgmc Gatimn $620 uyL ion 1000 1 OU23712 1909 7440-AALO Do% OWO520t7OR 17AM REPORT OF LA130RATORY ANALYSIS rr.a rmpy- W.41 net a �eprodup40. eecxp x. M. ntrgyr he -M, -I ¢f P.e. A.-v e.- IK Pagm 17.119 Pan AnYyamNafMen, Ine. Pace Artllyll up SMIMNlie. F.I. Anil r➢A a4ry1taf, inc. 3CBAf�3�ffC3i� E.N W roP. Rsmd Sud A 7275 RN.4Ne Dt 9500 Y 1IW4 9 w. 1 W + _ � ec . NC 277Be Au me. NC 208U HunNnr.. NC 3801! 113M3av11 MA)254,7176 i704117390➢2 ANALYTICAL RESULTS P,cy.aj: SURRY CLOSED LF Pace Project Na.: 92126710 9mmplr: MM1 Lob 10: 12128110007 Cvkelmd; 0111=12 TIM Reeslr6d' QW2Tf12 16:00 Mr11p: Misr Repdd Pmrmrnera+r P..kd1m L)" Urril µDL OF Plep000d Mopr"d CAR kv. Our 60101 Cp Qraun dwaler Anmlyifwl M.lhe d: EPA 6010 PFopormilan M elhod; EPA 3010 Antimony NO uWL fi ll 6.0 1 01125A2 WOO 96=1221:33 744036.0 Ameme ND uyt Ica 5.0 1 06 UT2 11:00 MW 12 M33 7440.3E-2 6afrum 940 uyL IOo 6.0 1 OWN1211.00 06202 21:33 7440393 6mry61➢m NO ugh 10 1 a 1 0623r1211:00 oarmi221:13 7444.4i•7 Cetr.km NO uyL 1.0 1.0 1 062571211,00 0WMI221:13 14a443.9 C.hfomk.m ND ug1L 10.0 5.0 1 06291211:00 OWW 1221.33 7440473 rebmll 267 up1L loo 53I 1 Oe, WIZII1W OYW&I221:33 7440-46-4 Copper ND uyL 1019 6.0 1 08261T2 WOO OW20f 1221:32 7440.50.E Lied NO ugtL 10.0 $4 1 o5aWR 11:00 MiW1211:33 741942-1 Nickel tO,SJ uok 60.0 6.0 1 0625J12 t1:00 0626f1221:33 7440.02-0 6e11r11um NO uyL 10.E 10.0 1 06A50211.00 O&Wl22113 i762.49.2 Slyer NO ugh 10A 5.0 1 ON2WI2 tt.00 MU1221 33 7440-22.4 TnrlEum NO upfL 6.6 5.e 1 0625J1211:00 06761122133 7440.2E-0 1lenmdum NO ugh 25.0 6.0 1 0625ri2 55:00 MW12 21-13 7440-62.2 Zino I" uglL Ica 10.1) i 08rjL12 T1'00 962611221 31 744041641 82M0 MSY Low Lmyel LmndM Anmlyrcal Method: EPA 3260 Acrione No uglL 10D 22 1 D61ZSf1202;06 6744-1. A�ylonN.ile NO uglL 200 1.0 1 Mort 107.1M 5enxene 1.9 u9tL 1 0 0.25 1 OMWI202;06 71.43-2 8romedll9romelnana ND ug+L 3-0 0,17 t 0625f120205 74.97.5 BromodlsMmomdhlne NO ugh 1-0 0.1E I 0626f1202-06 75-27.4 6nmelofm NO uyL 30 0.26 1 O&M,202:06 73.2E-2 &omomethmnm No ugfL 10.E 020 T MWI202:06 7443.9 2.6utm,,m-(MEK) NO ugrL 100 0-95 1 WWI 202A6 16-93-3 Carbon dlautlde NO ugh too 12 1 M6 ul242-011 75. 1" Cmroon 4umetgu4h NO uglL 1.0 025 i OWN1202-M 56-23.5 Chlo.obmxerte 6.1 uWL 1-a 021 1 062671202-00 10&947 Chlwo.thone NO uA 10O 0.54 1 06125712W06 7690-3 ChWroprm NO ugh 50 0-14 I. 0617WI7 W 06 67415.3 CJIIpromeYl.ne No ugh 1.0 0.11 1 06125f1202.06 74-07.3 12•DWuamo• 14tHlOfGutaodn. NO ugh 13.0 2.5 1 0625J I70106 96-}2-8 Diornm9ehtor9mmthanm ND uvl- 3p 02T I 0625J12(1208 124-48-1 1,2-0r✓omoe plena(E DW No ugh 1.0 027 1 o625t 1202 u5 106. Ej4 Ll1brem9mr1h4" NO ugfL 10.0 921 1 M25M W:Od 74-95 3 1 ,2A6h1arOban7ene UJ ugh 5-0 0-30 1 06J25+120206 D$so-I 1,O,Mhoroban cone 1E.4 ugfL 1.0 0.33 1 08rd51t2 d2;b6 106-48.7 cane-1,4 DIoMoro-2-0menm NO uWL tall to i 08rM1202:09 110-S7-0 1,1-01chlor0NMna MJuSfL 5-0 0.32 1 OE2Sf120206 75-34.3 12.OIch1womthane 2A uyL 1-0 0.12 1 MMI202:06 107,06-2 1,1-DichlwoelNanE 49 uyL 510 9.56 1 OWSf 120210E 7€364 c1}1,2-olGi¢roalh.na 16.1 uyL S.0 0.19 1 06251I202-M Ise-W2 rrinr, i,2d11Clum. ethen a No uyL 5.4 0.49 1 DR&M$2 a206 M-00-5 1 .2-Dleh1waprvpane 6A uyL 1 0 a21 t 0a251T2 g2 06 76-67-5 13-flkrAuoprapane NO uyL 1.0 025 1 66291202-06 142.2&0 ,i - 1,3•01chloroprop An& NO uyL $.0 0.11 i OV2WI2 02:00 loge 1-01.5 Dm1e. OWOo20120117 AM R EPO RT O F LA SO RATORY ANA LMS P.D. IR039 Tare mWq N.1 rwr ul i.F. 4� -P1 .n h. erne. --I of Peu Ar jfa 64nna1. NIc Ce14fl ffC�l • Pia An4tyee.r R.rvk n, rnc. Ms East AYadew Raaa • twz. P.O. Ana".131-4- , t- 7774 A-. W4IJr. Pee4 A"V%-k aeWlin, Ina. a600 KpmM7 Are. SWS 1W ace Ana)yficale Pale Aw yekal Rem.., Inr., 205 Ent Maaaew Fe.e - 5uua • Pe.e AmIya Cal i4WINK IMF Pap Ar,aIvMal aaMe.., W. :� RHrsE. 1v peaD K,"l . "$ 100 Eaan. NC 7726E Ar1Mr, NC 46604 IWnKrr.ra. NC 2Mr7a - ..r Per.r(y wv Eean, NC 771ee Aylavrie, NC 26904 HwWwn., NC M010 f316162344121 (e2fix4-717a 1701 M11&eG7i 133e1423d1K'1 (116) '35+717a 170W)1&4M ANALYTICAL RESULTS ANALYTICAL RESULTS Protect: SORRY CLOEEO LF Project: SORRY CLOSED LF Pear Pr*dt No.; 021267W Pace PrMjecl No.- P2121710 sample: MVV-16 LablD,, 92129110M Conctaa o120112 11.00 Recsared! 062111216:00 We ur: Voter Sample: MW15 L6110' 12126710001 Welled' 062011Z 09:30 RecoNed: 004711121100 M6➢r}s' %AhW Repott Repan P-nalara Reeu{fa IJN14 Um6 )AOL of Prepared Ans"d QAS No OUR; P►remoten Resu6e uhim L1m6 MOL CIF pme06mid Arts"itd tAs No. Owl 1210 M0V Low Loyal LsndRll Analylkal MaOnd: EPA 1260 11010 rCF arcundweter Analylcal Method: EPA6010 Preparation Method' EPA 3010 Irene-1,3-Dlehloroprepane HD OWL t-0 026 1 0=5J1202-DO tOO61-0241 Antimony NO ugk 1.0 S0 I QSa 51121100 OSa6f122146 7440.344 E1lynan3ane NO uWL 1.9 0130 1 OWV1202:W t00414 Arsenic NoUWIL 10,0 SA I DWU1211AO 062vil221.45 7440.3a-2 2-el6rsnone NO up1L $0.9 0.46 1 OS12L 12 02:06 591.76E sedum SO.?J uWL 100 5.0 1 0945112 t1.00 OMW22$;0 7440-397 Iaderhatlen4 NO FOR. 10-0 0-32 1 OWN12 02:06 74.65-4 BUY&M MD upIL 1.0 1.0 % UII*W$211-GO C&MY12 ZIAII 744041-7 Mampene chlo tde RD 4h 1-0 0.17 1 0025112 02:06 75-0&2 Cadmium 21 up4. 1 O 1.0 t OWS112 11.00 01126r12 21.4E 744043-9 4.4Ae".2•pinunwo(M18K) NA 41 100 0,33 1 MU120216 106.10-1 Chromium ND vyL 10.0 5.0 1 ON29121100 oW&I221-41 7440.47.3 Swans NO uyL 1.0 0.2E 1 OS251120200 10042.5 Ce1,4$ ND VA 10.0 5.0 1 W25,0211:09 OWN1221;41 7440-{14 1,1,1.2-Ta6edJwoenane NO uDfL 5.0 0.33 1 OWU1202:06 630.20.E topper NO uOfL 10.0 5.0 1 MWI2IIAD 002611225;46 7440.60.E 1,1,2,2-Ta"Oh! eilane ND ua& 3.0 0.40 t 0625f1202'06 79.34.6 Laed NO %JwL 10-0 5-0 1 06awl! 11:00 062511221-46 7459.12.1 7elndih.oelhene NO.0& 1.0 0.46 1 06RSfl202:06 127.18.4 NIc141 ND uWL 50-0 S.0 1 Wsil21110 06a6f1221-44 7440-02-0 Tausn6 ND ugyL 1.0 029 1 O6R511z W.04 106.6E-3 Selenium NO uyfL 100 10.0 1 MU12 Won OWN1221:46 771249.2 TnAporn4914ne ND NO& 1.0 0.49 1 06n25fl2 MIA 71.5" SNWer NO Lg& Ito 5.0 1 09415021t,60 062&1221:49 7440.224 1,1.2-Trldllafo.inene NO - IL 14 029 1 0&12W 1202,00 79.00.5 TMWum NO uyL E,S $A 1 00511211A0 06aN 12210 744041.0 TrkM-**II 12 vyL 19 OA7 I OWN12 02-H 79-01-6 V4nadiw NO uyt 25.0 S-9 1 06 WI 1,00 0U26r 12 2 1:4 0 744M-2 Trtdrloroeuaromelhane NO uyL 1.0 020 1 0LIM 1202A8 75-694 214c NO uWL 10.0 10-0 1 Oa*W$211- 0 0=W,7 VAR 7440a6-E 1.2.1•TrkNomopropone MD UWL 1.0 0.41 1 06aSr 1202-06 W164 virm eceute NO upfL 50-0 0-SA 1 01R5r4 029E 106-0S4 126E M5V Low Loyal Landfill AA001nal Me 01ad EPA 6260 V"A odwlds SA 4& t-0 0.42 1 0512511202;057"14 Acetone 4,7J upY 1DO 22 1 091511702,21 67.64-I %Mena 17oea0 NO UWL 6-0 0.66 1 OWU$2 02'OS 1310-20.7 A910-11n1e No upt 200 1 9 1 o1125112 02R1 107.11.1 Eu,mottee Benime NO upL 1.0 0.25 t ca/35r 1202-21 7143-2 4-lremofuurohm4.na lsy 0741 70-130 t 062511202:06 460.004 2lrornoworem4riene No upR 30 0.17 t OS25+120221 7{•97.5 f3lomemoauorom.m an4 fs) 113% Milo 1 O6rj511202;06 164643-7 91an1adnaoromemane ND u011. 1.0 011 1 0E1251120221 7'ti-274 1�-RlcNuw�nene-d4 [S} 115% 70-130 1 OWW120206 17`0150-07-0 13mmoramm NO uprL 3-0 "a 1 05125l5202:21 M2&2 Takrene-d61S) 104 % 70-130 1 0416112 2037.2E-5 B, m Mslren. N0u0IL 10.0 0,22 1 O6R50120221 7441.0 23208 Alkallnny Anmli kal Ma61ad SM 23209 2-6urenona (MExt No UA 100 0-96 1 012502 0221 75-93-5 Ceraon d1wid1 ND UC& 160 12 1 "QUI202'11 75-15-0 AAa►nOy, Told as C&C01 134000 Ua 5000 ION 1 06/301/2 1324 Calk. teaachlae144 ND u1+L 10 0-25 1 D6a5ft2 W21 56-23-5 a21011 BOD. E dew AnsWllul Method. SM 521 oS Chlorad.n7.lne NO 4WL 3.D 0.23 1 CLOW12 027A 106.90-7 Chlareethene ND 4VL 10.0 D.54 1 o&23f12 D221 7S00-y HOD-5 tiny NO uO+L 20H 2000 1 0122M204LOO 00a71120CM Chlorararm No uyL 5.0 0.14 1 ONZ51120221 07.66.3 Cnkrom.riana NO Vg!L 1,0 0.0 1 OL25112 OL21 74.87.3 300A IC Anton. 36 Day. Analytical Mmh.q; EPA 3000 t,2.OiWomo-1,cNaropmapam NO uWL 13,0 2,5 1 C172511202:21 94.12.1 SLOW* NO uWL 25D000 2000 1 0613W}203:16 14805-792 mm-ochlamamemane ND uWL 3.0 0-21 1 01f250292:21 124J6.1 1z-0mromoelhene(E081 00-A 110 027 1 062W202]1 106.034 4WO Chloride Anelmcel Method: SM 4500-C1-E owamomelhane NO dWL Inc 0-21 1 0625112 W;21 7495.1 Chromlda 36i00 uy1 two 1000 t OM1120:31 iS667-00.6 1,Z-okfilorabenxane No up4 5-0 O,x 1 0AQSf120241 16-S&I 1,4-Dknlorahenaens NO uprL 1-0 9.13 1 OWSM202-21 10640.7 63108 Too Anatytmai 1416Mod: SM 51108 Uana-t•4-Dlcnluru•2.6utene NO uA 100 1-0 1 Oafm 12 02121 tlo.574 Tae1[OrOanlr:Luhan 77300 uy1 1p00 ION 0023r121921 744044-0 1,1-oEnyroad+ane NO UWL !,0 0.32 1 0125r120221 75-34-3 17.-D.cMu &man* NO uii?L 1.0 0.12 A 0625112 02.21 $07-06.2 1,1-olcn1o1a4N4na NO 4tL 5.0 0.5E 1 06126112 0221 15-3s-d pa-t,Z-01c3+lvrae6lene No uprL 510 0.10 1 D1a91120271 556-50.2 tans-1,20 chMmethene NO uyL 5.0 0.49 1 01f1LA2 U21 $5640-5 12.OkMoA quopane NO FOAL t.0 027 1 062611202-.21 71.67.5 1,3•DlcMaroprcpena ND uyt t.0 0-26 1 002511202:21 142-H-li de- 1,3.01cnloropropena No uWL 1,0 0-13 1 OV25112 02:2 1. 10061-0A-5 Data M054101201.17AM REP0RT0FLA6ORATORYANALYSiS Page 190439 Cold 091052D1200:t7AM REPO RT0FLABORATORYANALYSIS Paps20Dr34 Ttiarlwn r.a! n.l a nproducatl a nW n All TlN rpen NY net" nproWeoa. *-A%In NI .moue 1,a erFan [ naanr or Pee. Arrlraral 5.ry . me we.ewM..lrwn PanMntaf P.oa An ".W S.M.% ft Pa.* A-lyaeal er.ew5v.ln.. ra. Ae. yal.w ernin., lee vac. Arta yowl born., trice acel V fd� r� ar • 235 Len m..tl Ae o -. Au,eR 73I5 A-W. Or JWD wrc.y Are. Srr IDo ww a•Ieaer n.. [W .NC 272M ANwM eft11e0. nu.wrnr. NC 7e019 R 11)13�u4931 iE2l1354-11 ]a 17,71475.10m ANALYTICAL RESULTS PropelSVARY CLOSED Lf pAc. ara)e i No . MV26710 sample: MYY-16 L►WD: e21367I0006 Couaotd 041Z0+120630 Rrcalved• OW111215:00 Mfltlx. Nhter R.pon pm-Ows Rveullt v" 01 Mpl OF Prtperad AnN-Ymd CAS No Quid 4240 MSV Low L4riI Landfill An mylrcwl Moth.d EPAUK Pane-13-Dichlordptapent NO uyL 10 026 1 05WIz 0221 1p08t_074 E61yloen2ene NO UWL to 030 1 MW1202-71 IOD414 2�i.aanpna NO uyL 10.0 0 4a 1 0051I2 0271 591.763 H1vIna1rlan. NO uyL 1Do 032 1 01R511202-2 74.4E-4 ""one CNorlda NO uyL i 0 1137 1 OLIN 12 0221 7S-0¢-2 4-Me9lyl-2yemenon. IMMIK) ND uorL 100 0 33 1 06Ri112 0221 101.10.1 sweat frM vorL 1 0 G 26 S 061i5112 02] I 100.47.5 t,1,I,z.Te9kdllWoellMnr NO ClyL 50 033 1 Dow 2022 630.20.E I,1,F,2•bgeehPproeOlene NO uyL 30 OA0 1 OSWI20221 79.34.5 Tetechlwse0tene NO uyL 10 046 1 DAQW120221 127.1a.4 Toluene NO uyL 10 026 1 UF2251120231 t06-0a•3 1,t.1-Tny11e.0e1narr NO uyL 10 OAS I OWN 202.27 i$-55-0 1,1 7-TnMdoroealanr ND vyL 1 C 0,29 1 0617Wt2 0221 79.00.5 T+Nhlmo.0ene 00 uyL 10 0.a7 1 06f2if120221 79.01.6 Tr"C WOC616"ffi.hi NO uyL 10 0.70 1 WIWI20221 75-M" t ],'d-Tnchlmoprap.ne NO uyL 1 0 0.41 1 Od23d12 0241 9&18 4 VVry14.0141. NO uyL 50 0 015 1 OWY12 02-21 106.051.4 Wo cnlwad. NO uW�L I.0 0 6F 1 OMW12 022 75-01.4 Kylvna;Talal) NA uyL 5 A 0.66 1 0643112 0221 1330.20.7 4.8rvmaMrorooen Lane)5) 9e x 70.130 1 0445112 Q21 W-00.4 17ip70+rW4Nerpmemane i5l .11% 70-13a 1 O6/f51120271 146E-53-7 t2-01[Nmomh$na-d4 (5} 119 14 70.130 1 0612V IF 02-21 17060-07-0 Toluene -do d51 4041E 70.110 1 UNW202R1 2037.2115 23708 AlkAttnity AnAyllcal Momod: SM D20B Alkawry, To tw at CarQ3 ON uyL 5000 1000 1 DS W 12 13-34 62100 BOV. 5 tlay Anmy1w.I M.Ihud: SM 521 OB BOD. S day NO uyl 2000 2000 1 06=11204.00 OaWiU 0630 300.0 IC AM- 26 O.ye Analylleal Me91vd. EPA 300 0 5ulfel. NO uyL 730000 2009 I 013W1203;30 14608.79.E ANO Chloride Anagllgl "11100' SA 4500•0.E Chloride NO uyL low INC t 0=4112 1914 18667-00.6 40198 TOC AAWVWel M.rhed: SM 51108 Total Ofpeme Cnhon IND uWL INN I000 i 06123112 1935 744044.0 Date-09r05r.0t2Oil: 1IAM RE PORT OF LA BO RATOR Y A NA LYS 15 1. no.n~ mi pe mpmd-1.*.c. pi in .M0 ere anfY wn/enr of Pao. AM,"-, E.r ., r- Pao$ 21 a 39 P Pm me Amdyllcel eaMae.• Mr. Pace An.lydaWAnal ur wat., 1n.- P... ytn4l Berate.., k" aceJ4naly�ical m6 E.N M..mRe.d - Sw A 22M RN.r fk 06DOt{wc.r R 1m Eem. NC V a. A�..y.la, NO Za$04 Ihnalmd. NC ]a07e r3mp7_-ae21 d$2$11se-7tm r7 y515awi ANALYTICAL RESULTS Rq.et SURRY CLOG EO LF Fete PFWCA No $2126710 sample: 36W-19 Lett ID: 971Z4710009 Col"" Col" 061,101 f7 50:16 Rtnlwd: OW 111216'00 Ma116e-VYRter Report parameter. R..WI. 11n11a Ldwl MDL OF Prepued A.1aym lo CAB N.. Q.W 40101 CP Omn dwater AnmlylLcal Melhod- EPA 6010 Pr.PRre4on Melrmd: EPA 3010 Anllmony ND uyL CID 3.0 1 OWN12 WOO 0612871211:61 7440.15.0 Apaenlc NO UVL 10.0 5.0 1 06125712 55;00 08J2471211-61 7440.36.2 Bertum $e.1J u01L f00 5.0 i 011/!8li7 ii.00 OSYFt712214-31 7440.193 B. Lum NO uyL 1-0 1.0 1 13251521100 0612N1221.51 7440.44.7 CB*Wwm ND uyL 1-0 .1 1 Wd W" 15:00 O4>Z0.r121, 11 7440.43.9 Chromkim NO uyL 1910 5.0 $ OG25712 $5:00 067N122111 7+4W73 CD6nI! NO u4+1 10.4 3.0 1 081251iz 1It 00 0872MI3 F1-51 144"" Copper NO uyL 10.0 5.a 1 06R5112 11.00 06128712 21.11 7440.50-6 Lead NO uyL 10-0 5.0 1 0&2u6 21$ Do WWI 7439.92.1 Nldlel NO UWL Soo .50 } 062611a 11.00 06426112 2 1 -51 7440-02-0 Seim- Np uyL IOil 10.0 1 L16r(575211:Op 0041VI221-a1 771240.2 Sayre NO UWL 10.0 5.0 1 08125l52 $1.00 MIWI221:51 7440-22-4 Tneleum NO uyL 55 SA 1 06+25l t2":00 064N1221:51 7440.26.0 Vanadlum NO uyL a S.0 1 087Z57121Ito 0612611221:11 74J0-62-2 Zinc ND UWL 10.0 10.0 1 OW26ft 111,00 081R871221:51 74AD-04 6240 M6V Low Level Lec1d1111 AnmylN:al Mee10d: EPA 4260 Atsume NO UWL f00 23 1 067157120237 E7.64.1 AnylorRlrlle NO U91L 200 I.9 1 ooa&fl202:37 107.13•I Ben2ene ND uyL 13) 0.25 1 0612511202: 37 71.43.2 BrumelJ,ImOmemenr NO 4yl 20 0.11 1 06r:W 2o237 74_21.5 &6rrMmchl6ramt7yne NO uyL 1,0 0.19 1 OflaWl20237 7627.4 Bromorolm NO uyL 1.0 026 1 C&f2W1202:37 75.25.2 13--on.1n... NO UWL 10.0 0.29 I 06125f11 W-37 7443.9 2 El.lenpe. fmEK) NO uyL IN 0.94 1 OSr251120237 76.93.3 Carhort liwlid. ND uyL too 12 1 06Y;6112 D"7 75.15.0 Cvt mn f.oavl .Fid. NO uyl 1.0 023 t OVAU12 02'17 56-23.5 Chioroaenrene NO uyL 3.0 D.23 1 CGOW1202-37 106.M7 Chl. -than. NO uofL f0.0 0.54 1 ON25112 0237 7500.3 Chdvralv+m ND VWL 5 C 0.14 1 OWW12 0217 67-W3 C111010 elnene NO uyL "I Cell I 06l2671202; 37 74.67.3 12-Ditr0mo- 3-4hioropf open. NO uyL .1.1 2.1 I 042571302:37 8612.E tilhromarnlPrometnarN ND uyL 3A 0.21 1 087250202:37 124.461 1,2-Oe*vm0. mane (EOB) NO uyL 1.11 021 I 06f2511202.37 106.13.4 Th6r6md-olh-4 NO uyL f0.0 0-2, ! o111251120237 74-95-3 52-plchlofohent.ne NO uyL 4.0 0.30 I 0512N1202,37 9550.1 1,4-Dichladh4n tone NO uyL 19 0.33 I CKU 2 02;37 I08.44.7 vefn•i,4-WcrNo ro•2L6uNne NO uyL 100 1-0 1 08rW202:37, 110.57-5 pl illprOelNne 3,aJ ug& y,0 0.32 1 057,5052 09-37 754W I �•DInJNmaacUne NO uyL $.a 0-12 1 DWV1202.37 101-06-2 1 1-MCN0r9ethe.e NO uyL 5.9 0.56 1 C&2512 O2:37 75-35.4 .Wl.2-0Iehdotmenlant 3.1.1 uyL 5.0 0.10 1 06715l12023i 154-59-2 Irani- T,2•01ch:oroathone NO upfL 5,0 042 1 06r25f1202:37 168-00.5 5,2-DICHb6prvpane NO -at 1.0 0.27 1 OE2ift20277 76•E7.5 1,2-DIC opropena NO llyt I ' 1 0.2E 1 1W25f1202-17 f42.H4 ah1.1.3•Plchlompropena NO uyL 1.0 013 1 CUM1202:37 10061.01.5 Dela: ON0512012 09; 17 AM REPORT OF LABORATORY ANALYSIS Page 22 of 39 Tla ripen n.. net G D-R-d. rend n M. MTdd"-men .easel of P_ 0­1" s.rrur.e trice Pea ArWyleal aaMesr, IrK --a-eat a..weaa, Ise. PA"ApOyNsi Son,"r, Iee- 2CBArk?�ytiCd�' 205 Feet la..p R[se • Sw A 27C AN.ratl. 0r 9m00 Km s A.e ark l W Ed.n. NC r7ee A.herr- NC 2mw NunMraW.. HC y6076 [ 1-pW1 (m16)254.7, 7p 170•}679-9092 ANALrnCAL RESULTS pf*CL SLIRRY CLOSEO Li Pkea PFaod Me- 92126710 6smpwi kRV-16 Lad t0; 97126710009 Culkged: 00,70112 10:10 Rscelwd: 0621112 T6:00 them: wiler Report p"ITIOPIN Result. LkWm umq MOL OF ptaprusd Am"d CAS No. Opal 620 M6V Low Level Landfill Ahatyncsl Memad: EPA 5260 vseto•1.3•okhlaoptopana NO uyL 1.0 0.20 I 067511202-37 10061-02-0 F"answa NO uIVL 1.0 0.30 1 06y25r12 02;37 $0041.4 2-hlessnone NO LWL 500 049 1 0tI V1202:37 SRI.754 tmdems&W. NO uyL 10.0 0132 1 08l15A202:37 74.664 MtNcoo Chwele NO uyL 1.0 D.97 1 0612511202:37 7&OR2 44w1apryl•2•psn9mn9 &a WSK1 NO uyL Ica an 1 01142611202:37 166-70-1 Wine NO uyL 1.0 0-26 1 OWN1202,17 10042•5 1,1,f,2-TsNaclsorwb sne NO vyL salt 037 f O7d23r 1202-137 E30.20-6 ,2 1,1,2-TeVeCNerp9lheP4 NO uWL 3.0 DAD f OWW12 O2:37 M34-5 Totmehl-M.na NO uWL 1.0 0.46 1 QaWW1202:07 127.$44 Tokwa NO uyL 19 025 1 00RS11202:37 108.013 1,1,1-Tdahl.pothsne NO upR 1-0 0.46 1 OWNf202137 71.55.6 1,1,2-TdcMorpalhane ND I WL 1-0 DA 1 0625112 02,37 70-00•5 Trk211noHhena NO uyL 110 4.47 1 O6r25112 OZ37 7"14 Trkhlaalluo•omalhane NO uyL 1 0 0.20 1 06251120237 7"94 12,3,Tr6Wk..prppena NO uyL 1.0 0.41 1 08125112 OZ37 Wtd.4 ,ow -tom NO uyL 90.0 0.35 1 DMS012 0217 106-05.4 Vinyl d+lwea NO uyL 1.0 0.62 1 OM12 0Z:37 75.01.4 xylsns (Total) NO U94- 5.0 D-66 1 OWN12 02:37 137o-20.7 Sym w.k. 4 Br emoluWobao2ene (S) 102 % 701-130 1 06261T2 02 37 460.00-4 Clot- avnromamana(31 121 % 10.130 1 O62W1202:37 1866.53.7 1,2-01enWropinsne•d4 (9} In % 70-f00 1 0l2511202;37 17060.07-0 Tw.-.-da (S) 104 % 70-130 1 OWN1202,37 2D37.26-6 2320E AIkahnRy AnsloicM Maaiod. SM 23208 Atka Nnuy-7wel so Ce CO] 12690 UWL 5000 1090 1 a"W12 13r39 62100 SOD, 6 dey An.Mlool Method: SM 52108 BOO, 5 day NO uyL 2000 20" 1 OW2112 0400 0627fQ 06:30 300A IC Anrons 29 Days AnahM1ltai Molhod: EPA 300.0 SWl.1. NO uWL 2S0000 2000 1 06/30/12 04:38 14601-794 49M Chwrlda Anovacei Method: SM 4&00-CI•E Chiond4 2360 uyL 1000 1p60 1 49ur3471219;74 1646T•006 631 DB Toe Ansyilul Method. SM 5310E Tom Orgonlc Carpem 2470 vyL 1000 IWO I 082311211140 744044-0 Cal. 0910"012LID. 17 AM REPORT OF LABORATORY ANALYSIS Page 23 of 39 tutopenr .-met a,spoc-e a 0nM .y~Th. w, [anent er Pa[. Mr ly.[.I S.mrie rz Aae. Aopyd4Y SeMm. k1[. P440 Atil ypur a.rvl[ep. In[. pate ♦ -.OVIW/l Soni"1, R .. ' -- a✓r elV ra ��.��' 705 Ea.14..00w Read •SWI*A 1225 R'rr... Or. gwo Malay A : Uft 100 Eden, Me 272U A.n.Ye. uC N004 rwnl.7 1- NC 7?118 rmlffl77aatr 100,25a-?, M f70116759092 DUALITY CONTROL DATA Project: SORRY CLOSED U P4ta k*ct No.: 921267 f 0 QC Baxn: MPRP011346 Ana"ll. Me01ud: EPASOIO Or 0pleh Mathed EPA3010 Ansysk Onntpaen: 6410 MET MC Crovndwatsr ANOG+.ted L ph Sample a: 9212671000f , 921267 f 0002, S2 f 26770005, 921267 tpp04. 921267f 0045. 921267104p6. 92126710007, 021217 t9001, 92128710009 METNOOSLANK; A21447 Mppla: V1MImr Aseoc12144 Len Sahpiaa n128710001. 02121710002, 9212a 710003, 02121710004. 9212971000S, 9212171 0006, 02120710007, 92128710006,92126710009 Blank Rsportlnp Ppr.metar Llnaa Result LiftA Pft"d OU60.rs Arbmany AIL NO 9-0 OWSJ1221:05 ksooic uyL NO 40.0 08R611221-DS 8enom vyL 510 100 Oa128H22VO5 8mrylllum uyL MO 1.0 CMIV1221:06 Gadmwm vyL MCI III 06261T2 21.05 Chrpmwm uWL No 10A 0629112 2145 Cobalt uyL NO 10.0 062611221'05 Copper uyL No 10.0 OW1022T.05 Load uyL NO to,* 006riz1$0 Nlcasi wen NO sto d6reN122"s Selenium ug+L NO 10-0 06R8r1221-.06 91.er uyL NO 10.0 CW.Soi221105 Thallium uWL NO Ls Mom 21,05 Vanadium vprL NO 26.0 9412601221:05 21nc uyL No 10.0 MV12 27 05 LABORATORY CC04TROL SAMPLE' P4Tamat.1 621646 unna 501ae Cant. LCS RaiMl LCS %Rae %A.. Llmlla DUSnaara AnOm" uyL Soo 465 93 60.120 Amce t, uyL 500 475 93 BIL120 Betkuro uWL Soo 470 95 60.120 BorvCum WL 500 487 97 M120 Cadmkim uWL 500 4116 97 60420 ct"num uWL 500 483 97 M120 Coha6 uyL SOO 410 96 60.120 Capper uyL w4 44 45 W170 Lead uWL 500 461 66 60.120 N"44 uyL 50C 48D 06 64120 Selenium uOfL SOD 471 94 6b120 Sayer uyL 250 24T 96 60-120 Thsawm vyL 500 466 94 60.120 Vansdvrll well. 540 494 67 60.T20 Zlno uWL 500 401 96 60-T20 0.14: IIWW612 M. AM REPORT OF LABORATORY ANALYSIS Pape 24 mr18 7te1 raven rum-- N r.a du c.a 91 r. Ns .1houk iM wain [eal.nt ar Psa A Nowt Senses.. rot Fact Aruey,lrel aerel[y, Inc Pate Amlyy eal Servleae, InO. Pau RPNy1ka, aervleee F,c, ace 4nalytrca! 205 Eeel Mamda+ Wed - &-4 A 2225 pnewde pr 26%xu ea7A a 6.. 100 ewwyrraeame Ed- IrL 272M AW,.wle. NG 26p04 H-W-1-e. NO 2a018 [D55la2]d921 1a26l754-7i76 r764le7S9W2 QUALITY CONTROL DATA pf"cl 5VRRY CLOSED LF Pace pro" No. 92T28710 MATRIX SPIKE d MAT RU( SPIKE DUPLICATE: 621641 021850 MS 490 92T28809001 Spike Spike MS MED MS MSD %Rac Ida. Pvemeter umtb Reeufl Cenc. cc" RomIt Resvil %Ric %Rec W"ft RPp RPO Duel Andm j 4yL NO Son 500 456 477 92 95 7"25 4 25 Amae c L.WL NO 500 500 466 481 93 97 73.126 4 25 Be,wm t•yL 16.1 50D 500 413 305 93 R8 7fr125 4 25 5"mWm 4WL NO 500 500 460 494 06 96 75-125 3 25 Ceemlum 4g1L NA SW SOD A79 494 95 99 75-125 3 2S Chmmum uA NO 500 500 476 491 95 08 75-125 3 25 rMfli , D+L 10 5DD 500 481 502 95 96 M125 4 25 Covow ug7L NO 500 500 a "A 94 49 751126 5 25 Lead I,gk ND 500 500 473 402 95 as 751-12S 4 25 M."I "VL ND 500 500 A75 40 95 98 75.125 4 25 Setenlum uyL N9 500 500 463 07 93 97 75.125 5 25 &Myer 4yL NO 250 R50 237 244 95 96 75-1Z5 3 25 Tnmlavm uyL NO SDO w 456 461 91 96 75.125 5 25 Ypn+rA4m uyL NO 5DD 500 470 498 a6 100 M126 4 x5 Lln[ uyL NO 500 000 474 481 94 97 75-125 3 7S a�77'J+',y P.ve ArWylkel Hale H, tnc. Pave AaagYul ■eeldse, Hw. Pau AnN ydral aehleee, ine. acGllr Ra yticaI a 2D3 Eesl MaeW,., RneY • e�,a .• 72?S RNw+tle Df. PL'001(iz.r Ara 3,na tpp 1 ewwhxabat cdn [d.n. NG 2720E A m-ft. NO z"" 29029 mQjf 73.6921 0261,2547176 I7M )6f S Yl9: QUALITY CONTROL DATA ProAct SORRY CLOSED LF Pa.v PrPl+q No . 92t26710 4Ca+1ch: MSUR0180 An@"Melha4: EPA826D QG welch McWad: EPA 6260 An@"m Dasulplgn; e204 MGY Lvw L-1 Lend62 AeeOdafed Lah Semplee: 92128710001. 92121710002. 02128710003, 921267I000a-92126710005-1121267W006, 92 W10007, 921215710008. 92129710009 METHOD BLANK: 621155 Malrlx: Mter AavGalmd Lab SmnVmv! 92128710001, 9212911 D002, 92126710003, 92128710004,92126710095. 9212671 WOE. 92171710007, ul2871 UWE, R2126?10000 Blank Reparong perameler OMPIS Rtlmull Llmlf Anslynd Dual Bera 1,1,1.2-To Rchkry eth a" upfl NO 5.0 0825112 DO." 1,1,1-Tllct oraothwo uyL ND 1.0 MV12 DO: 00 1,i,2,2-Tph+chlpreelhene uyL N❑ 3.0 w2W1200-go 1,1,24ricnromai ne uyL ND 1-0 08125f 1200,00 1,1•Dkhlvroeihane uyL NO 5,0 D6r23112 am 1,14)Iolmos Menm uyL NO 5-0 MN1200.00 1,2,3-Trrgtl0ntpr0pane uglL ND 1.0 06r28112 D0.00 1,2•f516rvmv3-rlJvrpprppene uyL ND 11A DWW1200.00 1,2•DMb Melhene SED51 uyL NO 1.0 D8I & ;! D0:00 1,2•Dlchlarollen2en0 uyL NO 6.0 0612W12 D0:00 1,2-CkN. eon— uyL ND 1.0 0$f2511200:D0 1,2•DkNvrvprvpane uyL ND I.p O6/l511200.00 1,3•DIc111vrvpropene vyL NO 1 A 08R6112 00.D0 1,i•Dlchlmdbrn7.e0e up4 ND 1.0 06Yu 12 D0:00 2•Bulerene fmEKi uprL NO t00 0612511200.00 2•Hexanvne uyL NO 50.0 0812 W 1200:00 4ddmmyl- pe tW fi (M18K) vyL NO. 100 08023f 12 00:00 Acelme uyL ND 1 DO 06725112 D0:00 Acrle9n1hea uyL NO 200 08125712 DO. DO Benzene uyL NO 1.0 0a125112 DO.00 Rrom9cld9+vmelnane uyL NO 3.0 O6r25f 12 DO. DO St0M0dICh40f0m04h0M4 uyL NO 1.0 06R5112 DO: DO l3r.m.fatm uprL NO 3.0 08/25112 00-00 N umamelhene uyL NO 10.0 OWN 1200-40 Cutw dleu044e uyL NO 100 OMBJ120000 Cubm 1al.eoNwwl uyL NO 1.0 O&25012 00:09 Chl.f.blo.ena uyL NO 3.0 M501200:D6 CnlOrpelhdn4 uyL NO 10.0 06y15H2 O0. DD Chlorcklm upri ND &P OaRWi2 DO:DD r,W9Fgrnelhene uyL ND 1.0 082'i4120000 de-1,bOl9hfprpeehane uyL No 5.0 0812 W1200. DO de-1,3•Dfr5lioraprppene upfL NO 1.0 D6g5112 QO.-DO DEreme.hlnrameDtan+ uyL ND 1.0 OW25f120000 obnmomelhfne Ityl ND 10.0 0646I1200,00 EIhylb%r De uyL NO 1.0 OWN 1200:00 Iedamamene uyL NO 10.0 00R511200:00 Mafiylana Chlprlde uyL ND 1.0 OW2511200A0 Styrene uyL NO 14 06026f1200:00 t.0.hro,oChene uyL NO 1.0 OW2511200:00 Toluene uyL NO 1.0 0846r120040 vane-1,2-Dichkrve6lvne uyL NO S.D 0672511200:00 Nis: 00 =01209!17AM REPORT0FLA9ORATORYANALYSIS Pogo 25ef39 D4IeO9r05720120917AM REPORT OF LABORATORY ANALYSIS pigs 26nf39 TM r.perl mhal n M mpradwad- oopt n K4 11[a f.pan Y+el mtu ,.xeept h aS NtfraKM wfflan[avent of Pap F+ lym[al Sur, 1nr_ neln "w uma ., P.. Analyse+, 6.eNue- Inc Pas. A,nalylle.l aaM er6, le[. P... Rnafye ul aarvrr.., Me. Pa.. Ae4i y6ul aahlr.6, al., Ce'RA*icalr 265 E..r L...mw R.1a •Sun. A =5 RnN11e. a, 9000 r..cay Aw Oro. 100 Ed . ou 2Z AN..YI., Nc 26991 H ,wv9., NO 26076 pY5]e2349j1 t626U54-7t76 (701)175.9092 QUALITY CONTROL DATA P .j.d. BURRY CLOSED LP Paea prp(.d N9.1 P2524710 METr4OO BLANK: 625155 Ma61a 1Mter A..Odalad Lan San%Aov 92126?10001.92121710002, 921247 $ D003. 92126710004. 92121710N5, 9217511 ODOG. 9212a710007, 921261113006, IIZU971 OM Slank Repord"g Parameter Unit. Roam LirrA Analyzed OuaN6m 06na•1,}deMarvprop.ne uyL No 1.0 o6 M200-00 eena•I,4-Dlddw0.2•eUlona -WL NO $00 OWU1200.00 Trldllarv.&h . uyL ND 1 0 OMV12 D090 7rk411eroluw.m zh.rva uyL NO I. A 06251$2 00:00 ~ecalare UA NO 50-0 OV25112 OD:09 WM uyL NO 1.0 0RQVI200:00 xyNna(T,t.l) rvyL ND 10 06Y2811200:00 1,2-DkN.o.Iho_a(S) % 119 70.130 OaRir1200:00 4•Brama4uorooen7.na (S) % 07 70.130 Oa W12 00,00 fflGomefuuomam.na(S) % 1%4 70.130 06R141200:00 TOtuan.4113) 194 70.130 06/25112 00-09 LABORATORY C ONTROL SAMPLE: a21I56 awke LCS LCS % Roe Parem.wr unae Cam R430 % Re, Umlte Ou.ahm 1,1,1,x•T.lnduwe.dune uyL so 467 93 70-130 1,1,1-Tnddom lh- uyL 50 46,0 se 70.134 0.an 1,1,2,2-Tdnechlwaer uyL 50 46.0 92 70. 130 1,1,2•Ttiridor9 M." uyL 50 48,1 67 70.150 1,14710da-than. u91L So so.6 la 70.130 1,1.OIallo[wdr.n. uyL 50 43.7 a7 M132 1,2,3-TrlWvrvprvp.ne uyL i0 41.3 97 70.130 1247Mrvmo-}chlwopropme uyL 50 42.0 9a 70.130 1��Wrvenoemane(E DBI uyL 50 50.7 tol 70.130 1,2-DIaM�oLannna u9rL 50 44A 69 MI. 1,2d7td11vrvedl.na yyL s0 49,7 99 70-t30 I,2.Okhlerepraw4 uaiL 50 49.1 Pa MOO 1,3.Oktpr deraep.n. uyL 50 50-11 102 70-130 1,4•DkhbrO6.e2.n. uyL Sa 44.2 &6 mm 2­01~6na(MEK) uyL f00 96-7J 19 70.145 2-Norman. uyL 100 lol 104 74141 4M.Nyl•2•perlranonc (MISK) uyL 100 07-BJ 66 70.110 Aealena UyL 100 a92J 119 50.175 Aaylon&la uyL 250 230 ex M143 Baniene ayL so 51.5 103 MI'A &omoGFJwomalhane uyL 50 45.1 92 711Ald BromOgchbrvmrlhan. uyL 50 48.9 66 70-130 Ocarn.vrm WWL 51) i1.2 102 70-130 Br9m9m69rena uyL s0 29.0 se 84130 cwlt, n dl.ulldo uOrL 50 42.ai 66 70-131 Ca.twl t.eachtarldd uyL s0 50.0 100 70.131 Gr4oroEenzane 1qR So 47.6 95 7C-130 CldMerlh.nr 69A 5o i3.i 17 64.134 Cldorwyrm uprL 50 47.4 95 70-130 Post And1A[.I Nrvlars, Ins. Pie[ AOAYOIN SWAM, 414, Pau AnalpuV Ntrlwa, In.. _ aceArk7lytrcal 2V5 e.W fw.ae. n..d . Snla A sus Fl&wde or Data wn[.r A"sr,N ion Ed_, NL Irm A.N[NII., NO 2660a nune.rWA.. No M7e 1336]6234621 f62alx34-7176 170-W&4 72 QUALITY CONTROL DATA P,01w SLURRY CLOSED LF Pace prvloct NO.: 92128110 LABORATORY CONTROL SAMPLE 821156 Spls. LCS LCS %RAO Patamelet unla Cane. Readl %Rec ulrid D.u9Nrs G19PT6ma7ferye too& so 40,1 a0 54.130 de-1,2•Dkhtoraa0fana uyL 50 47.5 65 7pd 31 d.-1,3 D d k up 9pene uWL 50 4:2 96 M130 Dmramachlwomrdiene u94- 50 4-1 67 70.130 DleFDmamalow. vyL 50 456 93 70-T31 ENylbonsan. VOL 50 4110 96 70.130 lodamrthan[ vWL 100 64.3 64 49.160 Me"anc CNOnda uyL 56 42.0 a5 63-130 SMme uyL 50 i6.9 9a 70.130 Te6adaoroothena 1.WL s0 40.0 9a 70.130 Toluene uyL 50 46.4 93 70•t30 9arIA-f,x-pGllyoeFane uyL 50 46.0 90 70.130 none-1,3-Olchlordpropene uyL So 49-1 06 70-13x tram- 1,4-DdilwO-2-butane UWL 50 40AJ 97 70-141 Trkhbruvlh- u9rL 50 46.7 07 70.130 Trkhrow4uwcmHhene uyL 50 38.t 72 62.131 Vi" 2"1110 vyL too 96.4 91 60-157 Vinyl ollwnd4 U91L 50 41,1 63 1i130 XI- lr teq uyL 15p !i] 91 70.130 1,2-Dldrlorvrulcnaaf4 (6) % 95 70.130 4•Bromotlwo6.nzerl. (S) % 105 76130 D16roma6uoramnnanc (S) % 98 70-130 Teruo ne-da(5) % 96 TQ130 MATRIX SPIKE&MATRIX SPIKE OUPUCATE: 621$57 625166 his MaO 02124710042 Splea Spl%o MS MSD NIS Mao %RAG Max PAr.melw Urul. R.&UH Cane. cant. Raeull R*KA % Re, SL Rec Wn is RPO RPO Oual 1,1-dcMoroemene u0R NO So S0 5S1 $8.4 111 113 70.168 1 30 Sdnzarv. uyL ND 50 50 46A 6a.a 96 114 70.140 17 30 CNcrotl.nzrn. uyL NO 50 50 54.1 10.3 too 121 70-146 11 30 Totu.rla uyL NO So so 57A 92.6 116 fib 70•Ias 56 30 TrlchloTOaatene u9rL NO 50 50 56.5 63,3 t13 127 M151 11 30 1,2•L1Kew*oIhan.-d4 (S) % 126 116 7"30 4-Brvmvlluarahana4n4(S) % 100 96 700.130 Dlhromolum methanr (S) % 117 $00 M130 Tnluane-41 (S} % 10 $00 M130 0410, 09rO Sr30120917 AM REPORT OF LABORATORY ANALYSIS Pa0e 27 at 39 Dale 00 OW612 09:17 AM REPORT OF LABORATORY ANALYSIS Pap 26 of 39 T1w n Ao .l not d .p-al ..r_. p.n nrl Tl npon NK0 eel. nr,ed ". r p1 F Ni m Fwt N. w,lYa eenunt or P- mtiyhc.l S.ryr[A., inc an.,rA.11n. wn conl.nl of Pad MryV 36ry­. Int Pan AwAylkp Smin., I.n P.Pe Analya ul a.rvlear, .na Pan An.1y9.af 5errin r, M[. aceRnalyticaf [ 236 [-I Maaean ROM - %.P a 2225 Rwe*rtle low xnal Jw. Suk 1Ca Ea.n NC 2i2ea Awarlia. NC 7NO Mrnwm l NC 71076 r776AZ34wl 14 1254-7t'la 1704Ie7SWY. 0 JALITY CONTROL DATA Pr91.cl: WRRY CLOSED LF Pace Pr9faC4 NP.: 92126710 OC Balch WETf2219S AnatpA Memo& SA123208 Or, BWIVh Melhoo: SM 2320B AnV41" Desa4p4W. 23206 NkeWly Aa.901alsd Lab Samples: 92126710[r01. 921767 i 0002. 9212a 710003. 9212a7 Y 0004, 92125710005 METHOD BLANK II 2n3s MaP1a: Valor Au"aled Lao So ,"s: WI28710001, 9212671000I, 92126710041, 92126710004, 92 t21710005 Bleat R.Porllnp Paromeler WiLa 94150 LWA AOafysed Ql "Hera NWIWre, Total so CaCO3 1 WL NO 5000 06126112 1300 LABORATORY CONTROL SPLE 622639 Spike LCS LCS % Re. PR/melor Won! Carla. R./WI %Rea urIie 040pan No". Total as Ca003 yWL 50006 46500 97 90.110 MATRIX SPIKE SAMPLE 622645 W126696001 Splka M5 M8 7L Ra0 Porsmetar Un42 Res411 Cone. Ra.411 %Rea LIMN CU441.ra AlkaunAy, Tow a CoCO3 v0lL 63 7 mgfL S0000 104000 a1 MATRIX SPIKE SAMPLE a22641 92129DOW01 Spite M5 MS %Rot PPramalar Unn Reath Can[. Ref41t %R.e LImYN OuA164r1 013k44n1ry, T01AI do CaCO3 ugfL 56000 t06000 61 SAMPLE DUPLICATE GJ "6 921215155001 04P MAa Pvamata, Unee Ra.yAl Reeu11 RPD RPD 4ualidey aµAWTV, Told as C.!.03 ygti 175 mplL 18100D 4 20 SAMPLE DUPLICATE: 622646 9212a69a003 D4p M4a pa[amat.. UP6e ResWr Rn4K RPD RPD quefiher. A3kn6p,N. To[A1 as CaCO3 YpL 41.0 myfL 35a0o 13 20 Cole 09ro512012 011 17AM REPORT OF LABORATORY ANALYSIS Pap29 0139 wi n. •.ppa,oP...det n M w aiw[ er[ wri4.n nn.mi.1 P.0 M.itTCN S.mn. i�r. �,aceAnNyAXI Pae/ lln4lynW Pae/ Analyaul ma -lass. Ina Pon. Ahay6n1 anr.k41. Nw. -Ea.1Mama RPaa-SWaA 2725"""a a. aEOp .[iic.7AM. �..,[./�e.h.— Ed.n. RC 2r766 RW,-n4la. hC 7eW4 iSONnt. n .wnkr/ea[, hIC '.a076 rxfW]-012t fe2eI75[•.174 4inap7[ram QUALITY CONTROL DATA PropcIt SURRY CLOSED LF Psu Plpl4u Na-: 92126719 OC Balch: V1ET122VA A -"Is Method. SM 23200 OC B.toh Method: SM 232061 Ano"Li Oncrlpom 23208 ApNU01y AuodHeo Laa Ssmpko: 92125759006, 92126710007, 92126710006, @212a71009p METHOD BLANK. 624700 M.bh: W.1" Assadoloa Lab Solrmlet: 9212671c90a, 921267t9067, p21267t0006, 92526T10009 Shni RPp-1hp Pat.m.hr Unb Ramp Llrw Mahrred Ou166.0 Alwitwty, T91AI as CeCO3 1•9+L NO 5000 ON3cf12 12:31 LABORATORY CONTROL SAMPLE: 624701 Spin. LCS LCS % ROG Paramalar Lima Cana Result 1A R44 LIR91. [3ua96na ANaNnlly, Tclsl as CaDO3 uyL Sac00 43300 91 90-110 MATRIX SPIRE SAMPLE! 82012 92129379002 Splks MS MS % Rot Pararr..lu Unm Renpt CPrIA. Rawl %Rea Uwa OusA6ars AIkaIIrwry, T9kl n CaCC3 uglL 59.5 mgfL 50000 101000 64 SAMPLE DUPLICATE: 624711 92129379001 D. p Max Pafam/N. 11n4. Rawls Re." RP'D RPO 13YaN6efa Alaa9f4ly, Twat as CaCO3 401L 34.9 mDq- 350ilo a 20 Cate 0&OSr2012 09.17 W REPORT OF LABORATORY ANALYSES Page 30 or 39 7rb nPon NN -11. ramaduraa. WW M aA, .o—t Y..n dy I of bap Ar..Perar Somas.. M[ "Awjydret Words", In•. Pa[. An."mal a.rvlwa, lne. P.w Anmydeal 5enllwr, Ine. aCeAnalytiCal' 2D5Ism ll.a Rew-lu6•A 2225RNurh 98701OnwyM. sw1.1o0 Eden. NC 272M Ak.40e. NC 2a604 Huew-A . NO 3007A [7361623-M I 1526125.-TM [m. 1676 wm QUALITY CONTROL DATA Prow: BURRY CLOSED LF Pam PIajw No.: 921287 t D OC match WEi122120 Ana" Memod: SM S210B OC U" Mamod SM 52108 Maryut Oesclptl9n: 52108 SOD, 5 day Maodaled Lad Samples: 02121710001,92121710002,P2126710003.921287100M,42121710005,92129710000,9212E710007, 92121710001, 921217tW09 METHOD BLANK' VMS? Matr4: Water Assodated Lab SampMs: 8212871000?. 921267 1 W02, 921267 1 X03. 92120710004. 9212871 C005, 02126710006, 92 T2871 M07, 0190711*Bad,12128710049 Blank RapwOnO Pu mvmF Units ResuO Urr11 Anotgod Oualmers SOD. S Dar uwL NO 2000 O8f27112 0610 LABORATORY CONTROL SAMPLE: 819002 Spike LCS LCS %Rac P.—Rw V3 ka Conc Rerutl %Flat Uffm Ouellowe BOO, S dry uy+L 19SOW 196000 95 94.5.115.4 SAMPLE DUPLICATE: 1119091 92121504001 Dup Mae Pummater UnaM Rawdi Reed. RPO APO Owllmirs BOO, 5 day uVL 5.6 m fL 5400 4 20 ❑are 09;0`_. Dl2 79 17 AM REPORT OF LABORATORY ANALYSIS Pays 1t of 19 7 �..Pod and rut a mp�_ e.cept w Na. wheat Nm r n t[nunt er Paw AmiAml Se m. lnt a Paw A"ya[.r i•Men, In[. P.[. Alwlydwl ieryNn, 1_ Pace AKalyarar Xe cma, We. Ana2W Eaer Meal[- A- cenaVica! R..4 • SuNeA 2225 RN-41ds. 11M Kbtey Aw. E. 100 w.y�rYR, i1,e Ed.n. NC 2I786 Am.vY., NC 26SU Hwa mawo., NC M70 IS1e1521a9x1 te2a12u7175 [7w167�-rcga gUAL1TY CONTROL DATA P+gw1: BURRY CLOSED LF Pau Pryecr No : 921267H1 OC Balch: WETAr13072 Maysh Mmhod: EPA ZOO 0 OC Balch Molhod: EPA 100.0 Aneysla Oeuxlptlon: 300.0 IC Arwwe Aaaociatod Lab Samples: 42121710001, 9212171*01", 9212$713003.1121297100%, 92s211?IbW S. 42120:0006. 02121710007, 92121710008 METHOD OLANK: 924 f93 Mailm, mlu Assaculed Lab Samplaa: 92126710001, 42f28710002, 92126710003. SP2129710004,9212871 MOS. 9212971 WOO. 429287IOM7, 92126710008 SLIM Repettily ParamHeF Unke Result Llmm Anayxad Ouakmm Sulue uprL NO 250000 01Yy.9/12 mie LABORATORY CONTROL SAMPLE: 824r64 Split. LCS L" %Rec ParamNu UnKs. Conc Re.ult %Rec Limo O.Alowts Surhls uWL 2000@ :6506J 91 90-110 MATRIX SPKES AMPLE., 624TSS IF2128400007 Spike MS MS %Re Pa7ememof Units Reeull Conc. Result %Rec Lkvwtl Ouel6sm SWfeie uWL 1090 myrL 20000 I I50000J 436 90-110 M6 MATRIX SPIKE SAMPLE: 024187 92129601026 SPIk6 MS MS %Rec Pelsmeur Unle Re" Conc. Read! %Re c U11ie, Oueslera SWlale u9rL 5.1 mgrL ?WW 217 DOJ 63 90-110 SAMPLE DUPLICATE: 824186 92129400007 C"P Max Puameler Un1Is Raeum Resudl RPD RPD 4uaaAeF4 Sulfate PWL 1090 MO& tt50000J 5 20 SAMPLE DUPLICATE 024156 92120091026 Oup Ma[ Palamater U0114 Re.u11 Reeull RPO RPO Ouellmm BLOW& udL 5 1 MOL 51801 5 20 Der.• 0910572012 09:17 AM REPORT OF LABORATORY ANALYSIS Pey. 32 ar 39 Tm i.�n.n.l note. ­o . e '. r 1W rrTeul Te w mn e.nxnt 0 Plc. A lrat.l E.rvk.. Inc Pau Ammar eervl.er- MS Paa4 Analypael 8enlo.e. me Per. Anrryyr,.l aerwl"i, IM. W5 E.N moom. Pl a•5Wb1A 2225 A—w Dr %061D0 +yikMtrt �. Ba..l, 11C 2,ma A MANP .:C mod .AA1lalpar- NC 2W76 (AuyGn ml fe N25 -il rd a0d)l lm QUALITY CONTROL DATA PrPJecl. SORRY CLOSED LF Pece PrPJen Na.. Q126710 OC Bexh- YVETNI3074 ABay.l. Melhud EPA 300.0 OC Balch M.thed: EPA 30.0 Maryut Deamodw 300.0 1C Amens AaeeG.tad Lad S.rrrple/. 921217100D9 METHODBLAN%- 924248 Matrix: YSNIu Arradalld Lab 5emplaa: 92%23710009 Blank 7tAwlnp Panmelrr units Revell uma Analyr<aa malfteh SlAlale OWL NO 250000 Oal30r120410 LABORATORY COWROi DAMPLE. 8742e9 SJrke LC5 LCS %Rac Panmeler Uln - Ccrc. Revell %Reo Lunn 9Nd19er. SuPlow WVL 20Oo0 $11 Doi 95 20,119 MATRIX SPINE &AMPLE. 174250 92128710009 SPAR MS A19 %Rat PwAmelpl Llnite Ae1pn Cenc. R—. j 'A Roe Llmiu OualAara 9ldlala uyfL NO 20HO 20001 99 00.110 SAMPLE DUPLICATE 124251 9712071D009 Oup Mod Peea frmer unae Raallll Rasull RPD RPD gO.BAera Sulhle upfL NO NO 20 Data. Well5rd01209-17 AM REPORT OF LABORATORY ANALYSIS Peke 33 rf 39 . •evrn .n.a,„�u..Prre�.d...=.n a nr ..rra.a P.. ynrgn raewnl el P... Aw y— S.nnye I- I 2eAn*ical' P." Arwyul lrrHe.a. iB1. P.c. Anliyye.l Spryly 1. Me. Pa- AI VOW artily., IM. K'S EHI Mr.da.. Read -- A — Raw-. a.— Ae` 1 Mr eu9a 40D Eden- NC 272H A.n.ra.. NC De51fe F %,walr, NC 2BO71 PNA:1-001 4MAJ 3441m iml M7spm QUALITY CONTROL DATA Plotecl- SORRY CLOSED LF Pace ptopm No: 9212/710 CC Baich: YYETA113109 Anrry411 Me11106 SM e5O0�FE OL Balms Malhad: SM e50DLFE An41yu1 Oeeeripdon. 4500 CNWd. A.wdated Lab Somolee: P212971p001.92$2871DO02, 02,207T0003 METHOD BLANK: 826815 Mruk Amw Amsodwad Lab Sempkfl: 92129710001. 97 IZ0710002. 92,17871 DUDS 111ank Repwbnp Pwameler unlla Rrw11 Llmll An Jylld 0u0e0ul rwoode OWL "D 1DOD 0"211220:19 LABORATORY CONTRDL SAMPLE. 02E8141 Spike LCS LCS -A Roil P.rrmrler Uhec Cone. RnJI %Reo Llmlll gummnm Chlallda OWL 2000D 70000 100 90.110 MATRIX SPIRE SAMPLE 82la17 92i29380001 SPlke MS MS %Rat Paremaler Una* Rerrdl CPrw- Rudl %Rae Llmlle Dnaeaen C.tgmda UWL 7190 "L 20000 7060000 -470 15-125 M5 SAMPLE OUPLICATE' 928918 92$29390001 DuP Mae Perpmelrr Un4. R.cuD Revel RPO RPD Chnllm ChkrNle uA I'll VD mWL 711200M 1 20 Dale. 09105120IZ 09 17 AM RI: PORT OF LABORATORY ANALYSIS Pepe U BI 3p Tlrr rye.n.r dl nr19a aped—d. r.gpin All. .ftw e1. xn , —1.1 Pw Arrq.rr Srn.ur. Inc •Jr�^J/� „� f Paer aFylydael 6rl.r/el, Ins. Paar anmrytlW aervlum, Inr. Pa¢e AnMyYOar Aan,tml, lrt�, p ` 3 Pa.r A,,004411a,Me/1, I.t. Ham Ane.y W a P—. 61r. Pace A-WVOPal 6er"no. Mt. .T RLre/V ki ��i�f a 2P5 E.r Ma. Ra.d - S..0 A � $1wrufa tl, cwa xM�ny M 1, 100 - '��'iGAnaVi al m ro5 Ea.r A1./daw Re.e - s„dm A = RMaiait. d 9e00 e.,rer A... Aw $m ! m„r,yKay y Eden, NC 177ee Aam.rM, MC 7E6W 1W W-Ae, HC 2e076 - ..Jpp- i Eden. W 7i29e Am"A., NC 208U f4n,t•iw1h. NC 290711 rMD 023-0921 lA2e]?_Wl 7e r704W S9LIB2 n75)52341 71 t92ljYw47e CM4167s*m QUALITY CONTROL DATA pt4poc7. SORRY CLOSED LF Pau Prge¢t Nn.: 92/26710 CC Batch: MIETAd13111 AnalyN. MaDrod! SM 4500-CI-E CC Barth M.Vwd: SM 4500-CI-E M."I. D.ar+quon. 4506 CNoddt Waeei.lre Lmh B4RgM6' 921267100D4, 92126110005, 9212575p000, 92126710907, 92126710005, 92126710009 METHO6 BLANK: 627413 Miff, Alm" Aoondmted Let, SornPlea: 92171710004. @2126710005, 92t26770005. 9212A710007. 92126710005, 92126750009 Blmnk RepodYlO Pvemour Unaa Result LYNI Analyzed Oumosm CNmlds uWL ND 1000 ON0411219.29 LABORATORYCONTROL,SAMPLE- a27434 Spike LCS LOB %Rao Pwmmetsr Unit Cana. Rmh % Rea LImM Ductile" CN¢tldm ugA. 2DODD 20100 100 94110 MATRIX SPIKE 6AMPLE! 627435 92129710004 Spike NS MS %Rat Parmeter m Unit en Result Do. RsauR %Rec Llmlls Oum9llmk Chlende uyL NO 20000 2000D toy 75-125 SAMPLE OUPUCATE: t1274315 Pars —tot Chtortde 92526710004 DIP Ma. Unix Result Result RPO RPD Gammon ugA NO HD 20 QUALITY CONTROL DATA Project SURRY CLOSED LF P.e. Prelecl No.. WWII) CC Batch: WETNUDD1 AnmryWs Mmud: wSM 5310B DO Balch Method: SM 53i08 An "Is D.aalpiicn: 571011 TOC Aasoolmlad Loh 5emple. :212:714DO01, 92125710002, 92125710003, 9212A710904, 921211710005, 921267t0008, 921IA 110007, 212i7DOOe, 01227/0009 METKOD BUINK A$9722 Mmtrlt: Wate A. ... at.d Lob Se rr g4s. 9217571 OK1, 0212117100D2, 92126710%3, 92129710004. 02129710005, 02521171 OW5, 9212$750007, 10,21287 1 000a. 92126710009 Blank R"Fling Paramelmr Units Rmm Llmh Analysed Ou411gem Totrl DFpsnl¢ Carbon uwL NO 1000 O523712 1429 LASORATORY CONTROL SAMPLE: 519723 BPIka LCS LCS % Rec Parameter unils conc. R"Urt Rem. Unit 0u00em T911I OrOonl¢ DiFboe uyL 25000 23300 95 90.110 MATRIX SPIKE SAMPLE "9727 921257t0003 SQIke MS MS %Rec Ptrmmelm unlam Result Car.:. Rs.ull %Rec LRNk Oua6Amn Total Cagaric CmrW ug7L 19000 250% MOO 34 75-725 MI MATRIX SPIKE SAMPLE- 619757 92127e03ml? 4IM MS MS %Rae Parameru Unl4 Rm.ull Cone. R—tt % Rec ti ft OumaAary T¢e.l Drg.N. Cerb- up9. 2 3 mplL 25000 27100 99 75.125 SAMPLE DUPLICATE: 619725 92*2e710001 Dup Ms. ParameteF U¢Aa R*Wt Rowit RPD RICO Oua96mn Total Orgmr4c Carbon 4L 2990 2940 2 20 SAMPLE DUPLICATE: e1975d 971;760.1014 DuP Mar Pmr.meler Vnes Re.ult Result RPp ROD Gua9een Total O,0amc C.rh on ug,L 1 I mOIL 1090 0 20 Dow Ow0512012 09 17 Am REPORT OF LABORATORY ANALYSIS Pegs 35u139 Omi. 09705r:012 D9:17 ATM REPORT OF LABORATORY ANALYSIS PogirN 9F39 Tl.m W. that net Erb nA,.d—d...at1 n adl. T . npo,t Y,am W b. ne.,¢oure4....,I ii hM. rM rout lbe wnll.n —1 or P.cr A-ry/e.l S.rrn... I- wtw e,. e.a..n(ye4at ae pet. err rrat.l en,C4R 1eC Zac, Arialytical" +^". yp.Yeaan P ..j SUF RY CLOSED LF Pape PtgeciNa.. 92126710 Prre Arrrtjfl at 9enfrea, Inc. AS �aai kar addw RyAd - Hyee A Fen . Na 77760 4316l607-e975 QUALIFfERS Ran Anam,vlc ! larvlees, I"C. P.n Anal lrh.rl?.rvrer r, Ind. nN Rry.r Or v6hp Iwc.r A.. 2r2 •%W A.h.ylr. HC 74doe x.rr�l.r.hAe K. e0TE @311751•Thie 1TL4;6T'rHpd7. DEFINETIDNS DF - O+ugdn Fadlrw, II repdtlsd repruent. Ne IeG or .pplred 1a the xe pPrlee Oele We [o ehep6el w se male leapt allm. Motion et the sample mWquat, or rnpla9Pe Cpnlenl. ND - Not De[acted at or rypy6 P dJumhed lapwOrrl lmh. J - Eaflmated can[an646on Above the *"led method dolodien llm6 and b@ID* the adryaled rapprgn0 lint MDL 0.opalad M1mod Oataptlan Umn. PRL - Pace A epoOlm q Llml[. RL • Reps*dnQ Limit. S - Sure o6.le + 2.Oghenylhydrayne (6270 ested enak+e) decampoles to Aaab4h4zame Con.nlen[ -th EPA, vutdellne., .-vended deta are 011dp44yed and hara Lean u.ed to crlNldte %(egg-ry end RPD V41uee LCS{Ol - Lalmraloty Control Semple 1Ou01ce[r) MSMO Matra S01 [Duird"1 I OUP - S rm1dE Dup11c ere RPD-R.I.W. Pd,e 1 Qlf.r en. NC - NW C.ICul.hre 5G - 59lda Gd - Cis nn.ue U - 1nyulaa the epmpound was Malye4d fa, but Mt detaclee. N-NMoOga1I0errylamane daCo+npwes end uerndl he .ecaraled from DVhemytemhe unnq Method 1210, The Pawl repealed Per seen WoNte Is a combm.d dpnssMr.11on. Awe prom Rvedan may rol As epptapn ale for 2-Cnlervdmybnnyl ethet, Slypan a, d %W CNondr Pace An.lykp el Pa TNI @W.,11ed. CA 4.1 ymR P.C. PM Ppr Ohs torte nl flit of eGan..,&led r+yyle.. TNI The NELAC PwIlule LABORATORIES PAS1yq Pace MelylleN SorWv -Ash eyiq. PASI-C Pot Analytlaal Ber-WWas - Cho tone ANALYTE QUAUytERS µh Mauer 14)rk4 recdydry eew.ded QC 161m14, BpCh eeeeptsd her ed do lepdr.lar7 C*nlrvl sorcVlo (LC$) r.eayery k% Malrrr safka end Me eix spike dupllule recovery not avW"d saalpel control fifth; OPe 10 urnpla diMki;n. Dole: 09105R012 09:17 AM REPORT OF LABORATORY ANALYSIS Page 27 0139 has"M4 NM net 0. rsro"od...w 4 n %A. helwhn l,..n4re canf.at ee P.em ^mlyqul 9.mdf. +rc Pau Fn.I yPPN f.Men,lm. Pen A"PY10 M /w.lref, Ies. Pose Aulyndsl "Hlder, Ind. 1 ��'eAaiytlC2l a 2DS E.M kM.,b Redd - &e4 F ZM Rirer.M. Ot. HeW rtxK.IAw tir.N 1W eeh.dheMrnf Ed.n NS 2f26d Ass yft Ho now Mumm-10.. NC 26DTe p16h MAWh [e41754-71 is V04141i QUALITY CONTROL DATA CROSS REFERENCE TAN LE Pf.j@.L SLURRY CLOSEO LF Pau Pup.1 No.: 92126710 Andlyllwl uD 10 Sample 10 OC Batch Method GO Sa1ch Anelyti CAP Method Bahia[ 121 26710001 PA-1 EPA 3010 MPRPf11346 EPA60h0 ICP110403 92h2111 go. Mw-0R EPA 30t0 MPRPI11346 EPA 6DI0 ICp110,03 fi526710003 Mw-125 EPA 301a MPRP11174S EPA6010 ICP110403 92$26710004 Mw-120 EPA 3010 MPRP111346 FM 60 to 1CP110403 92129710005 Mw-11 EPA3010 MPRP711346 EPA6010 1CP110{03 921267100% Mw-16 EPA3Lf0 MPRPI11346 EPA6010 1CP1104a3 92126710007 Mw•16 EPA3010 MPRPY11346 EPA6010 1CP11o4G3 12126710u06 MW-11 EPA 30 $0 MPRPh1346 EPA60f0 ICP110403 921x677 DOD Mw-19 EPA 10S0 MPRP711346 EPA 60fO ICP010403 92124710001 Mw-1 EPA 626D MSVaD160 92U1710002 Mw-3R EPA 6260 MSVf2ol60 h 6 MSVf2016D :21 t2104 226700 Mw-120 EPAIRa MSV120160 9i2e7100D w13 EPA 6260 MSVRDi60 92126710006 Mw-16 EPA 626O MSw2D 16O 121281101107 Mw-16 EPA,6260 PASV0201:0 121x671D066 Mw-19 EPA 6260 MSVRD160 92126710009 Mw-19 EPA 6260 MEV20160 12131711)D61 Mw-1 SM 23208 WETf2 M MNr-]R SM 23208 WET122195 :9rix671DOD2 212671.1002 klw•125 5M 2320P1 YYET122115 1i126110004 Mw-10 6M 23208 WETf22195 92126710006 Mw-IS SM 232013 w122115 S2126710006 Mw-15 6M 23209 WEVM314 12tx6110D07 Mw-1e SM 2320E WET722234 9ri26710DOD Mw-76 9M 23209 YYETlii234 92126710900 Mw-19 5M 252011 wETIM34 122671001 Mw-1 SPA 511 oil wET221SM S2IDG WET02212:ZT26110 D02 Mw•7 SM UPas YV12126SM 52119 wEn212 9212111003 SM 21 126 1 VETr22h28 1 YJET42126 2710{ $2110o Mw•12D 208 SM 5Do WETl26 SM 52108 AS=228 9i5241100006 Mw-13 VIM 52110E NT2t 26 SM 2108 AITf227f21 211 Mw-1 SM 620 WETf222. SM 62f08 1IT1000, WET2i2 9267D07 w6 SM52108 WCTl22iam 20B WETf22126 92121TINO Mw-16 SM 52100 WE=1126 BM 52 TOB WETf22129 92121710009 Mw•1 6M510B WETM20 SM 521OB VVETQ2 20 1212g10001 WI EPA 300-0 wETAf13072 9212171DODx Mw-3R EPA 100.0 WETAIIS012 92126710003 Mw-125 EPA 300-0 WETA113on 04 21710004 1212 hfW-12O EPA 300-0 wETAf13072 92T211 0606 Mw-13 EPA3NO.O wETA)13072 95121710006 MW4a KPA300.0 WETN 13072 921i6710007 Mw-fi EPA300.0 WETAM3073 121217, 0004 Mw-16 EPA 300.0 YYE1Al13072 12128710000 Mw-19 EPA 300.0 wETA113074 Dote DWVd,i01209:17AM REPORT OF LABORATORY ANALYSIS pile. 166130 The nM, rh.1-4+ op —se. ...or n M, ml Ashe wnlErn d 1vP Pac. McIy+IW BtMcH. IfK [���yy�,, yyyy +yl+�'r• JJPeM_e.._, Paw AiW ytlu!larvlwr, lns- ]OS Eamm"W.Fl C-SUUA P.w MWygal6.Mw.,Ine. 2725 OWV14. 01 Paw Analylull.rvlur, lna, 99W KYr r,Wa S�t00 pa EdW NC 7TI6! ANWMM. NC 76604 t.�wma.. NC V" !wr MIMA23dml fRAPM-7176 I70ajer3.v099 QUALITY CONTROL DATA CROSS REFERENCE TABLE P,Qjnt: SORRY CLOSED LF P.p P,*d No : F2126710 ACal 1..6 0awnpSemple10 OC Beech Method QC Batch Analytlul M.tlwd Botch l2126710901 MW1 SM {SW-Ci-E YVETNI310: /2126710002 MW.1R SM A -CI'E VVETN1310 92126710003 MW-129 SM 4500-CFE YVETA11310 H126710001 MW120 SM 1500•C!•E VYErN13111 1272R 10001 MW!3 SM a3g0•CV•E V*TN11111 l2126710006 MW" SM iS00-CFE VMTN13111 12120710007 RW.11 SM 45K-CFE Y&TN11111 f2121710006 MW-11 SM 4500•C!-E VYETN13111 f2l2671 M MW-i! SM 4500-CFE YVETN11111 ■1129710001 WK-1 SM 53108 VrETN130g1 f2121T10002 MW 7R SM 53106 VVETNt 3001 12123710603 MW-1m am 131 OB VVETN13001 071217100" MW-12D RM 5310B VVETN17001 l2122710091 MW43 BM53106 VVETP2001 22, 217,00" MW16 91d 5310E WEW 300, 121L171600T MW-11 SM 3110E WETN 13001 lit 21R 10006 MW-1! SM 51, WETOV,3001 921217106" MW-lf S. 53108 WETAf13001 D.ra 091MO12 09:17 AM REPORT DF LA 6O RATORY ANALYSIS Pape 39 v139 TN.1.W rh.E rot a mpmdmW..><¢.pi h nr. wheal n. rnlrn ow....r er v.e. An.lyapl S.rrle.� Hx.. Document Name, Document Reylsed. May 7, 2012 � Y i• Sample Condition Upon Rec4lpt (5CUR) Palle 1 of 2 'Document Number_I —lsauing AuthoritY.. ^q-- ant W hBra Received: of Huntvramlle ❑ Ashov do ❑ Eden CouFfar. 0 F►d Em [] UPS❑ U&PSO Chn0 rcl ;Po" ❑they Custody goal on CoalarMax lirsoen4 Q yea F��J/no Same intact: C1 y06 ) no _ Pscklnp Minted d: © Bubble Wra aubbis begs © No 9"ri Car Thsmwmstar U.ad: iR tlun 3101 T3142 Types of kin:Blus NoneTomo Correction Factor ism: No Correcton T1 Correctlon Corroded cooler Tomp.t— 1,7� C eiolo*ol Tine we to Frown: Y.r Nor win oat..nd 1,n1 conunta: � T"P sh.-V it move lea" to a'C Comments; Chein of Cuwdy Prevent: N. OVA 1. Chein of Custody raied put; 2f., 0No Q—A 2. Chain of Cw%tody Rep Is -hod! of., O>re OWa 3• Sam ter Hama 6 SPgrialure on COG M N,r 13WA 4. Sam lea Arvind wi7irn Hold 71n ! af. PW QWA 6- 3hort Hold Tkn6 Ana le .72hr ; RK., On. Ckm E. Rush Turn Around nmoRequested; Ov.. C)" 7. &umcleniV"mo: . ON. ONO is. cormrtconla]nm Lead: n U. OWA -Pace contalnom lined; 2e.r Ow OWA 9• Gontainors Intael: 01. CiNa Nhk 10. Finered ytiluma racelvwd rdr Di6aprved last% Oy- ON. WA 11. Sampfa Labels match CDC; ❑yw er,. OWA -Includes daterllmaRlNMe is Wmtrfx: boy Ifr..l fJ 1(.jC7 �.F,�, ;7/i 5�' /0— 5 as c nl.lrma n..dhe pna odbm hays lain d-*.& . ❑m ❑" AI ow. -I Mta Hooding pronrvotion are found W ne n cmaWares won P7+A racommandailm . ❑Nor Dim yens "I.-T=ova, MORO I-W, MY- ❑ft t j, ruiwrrwe.wen.d Sampling Chocked IaF decf u rlauonOn! Clue 214A 14 Hoods mInVOAV7nia a6nnim: ❑y. . UWA 36. Tnp Wank Prosant Ov. [IN. 2<A Tr'P Biondi Custody Seale Prevan! ❑r. ONa A Pace Trip Blank Ldt 0 If pu rehooad : A8- Client Not!"C60"i Resolution: Flard Dols R4*(Wvd7 Y 1 N Person Coll egad' DatdTimc Comm enw R4aaluGon: Environmental Conservation Laboratories, Inc. ta:-Aw.eerreni. tnewtrl.l Cawt nary mr, Ir5 t t phony. eta.467AM FAR; ai9.407.35t5 Monday, Se✓7temher 10, 2012 Municipal Engineering Services (M0001) Attni )onathan Prohl P.C. Box 97 Gamer, NC 27529 — Y `L www.evcvre h,.[un� RE: Laboratory Results for Project Number: G11024,Closed, Project Name/Desc: Sorry Co, Closed MSWLf - Mt, Airy ENCD Workorder(s): C209796 Dear knethan Prohl, Enclosed is a copy or your laboratory report for test samples re cehred Dy our laboratory on Thursday, August 23, 7012. Unless otherwl se noted in an attached prcject narrative, all Sam pies were received In acceptable. condition and processed In accordance with the relerence l nteihods/procedures. Results for these precedLires apply only to the samples as submitted. The anaytical results contained In this teport are In comp! lance with NELAC standards, exmt as noted to the pmje ct narrative. 1l is Teport shell not be reproduced except in Tull, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. unless arherwlse noted, air anayses wen preformed at ENCD Cary. ISata from outside "anlzatlons will be reported under separate cover. If you have any questkins or require furtW lnrormatbn, please do not hesitate to Contact mn Sincerely, cu-��A Chuck Smith Project Manager / 8 2z Z SCURF Rerla l boa: 8 S7tF Review• bee; Enclosure(s)e(s) Now: Whonevor a dhrcroponcy offoo N Narlh Ceralm romplonc, mein. a C t tafarm wll be sent io to Nosh Cuelino DEHNR Cwuncaflon elnca ( Ise vA of rwi4 Inperrett pteservetrvs, out as I.mp, 4—"d ".WnN ) TIK total —1- of Peet in Zhu lgcn, mclknN rho p°ee It I I C9.nl lol MW-1 L.b 10: a 0979"1 S.myM; 0611P117 06N0 0..9.hndr 0l731113 A0;7p P...mwr New v.1.17....1.y Fr.p o.a mnw[.) JnN)91a H.M1Tla..[q PA ?aip a9l.ilf2 "In'11 P626 91SPO1273-31 Mm Sbr 4W-11. Lb E0: C70971-"3 I—pl.d; .0a/5p11t2 09100 9yyh.dl O9171113 1b:1P • LR..1 Im _ MW-11_ _ _ _ _ lab Ipr U01,76"S 1.rnpH . "IN)11 UAS _piy7_]) S] ip_:l_P__ P.r.mwr Hold Tlm.(.[ McITH. p. l.;""(.) a-t IN MW15 lab TM C709796-0i S.W041N W1201111300 PA-WWd: 06/13/12 1410 r.ma r ".Id O.blTlm.[.] Prp O.WTIm.E.) A..Ipl. 0.7.1T1m.(.) 99,P,l l C9>711111 M:28 91SIM12 W-12 CINdl fpl MW16 Lab Ip; CM79"5 a..n Ml M6 20112 ISIOP R 1 .dr M125111 1O1JP Hpld o..,rrlre.A•1 ... P"v o.rlrx.rKa1 .. A..1]r.6 n.l.lnm.(.) ves x:•W -- I..-. DIAW13 W-36 9AM12 w.3o �co xww.enmlabl-mm C11.nlla: MW-17. labiol Cjo9H6-w An.lyM R..uly Fl.p 11F MpL MAL N[iWIL Vnil. N.IA.d N.la. 6 sm6e p.039 ] 00A 0SO If myL EF. 1001 pkm ipl HW1! Lab 10; C309796.03 M dy1. R..91s A p OF MOL MILL NC11WSL OrAw M.Mdd N.b.. emn,de Q,)0 3 I OA 700A !]WITH: M1ySS L bIm L70P796.0] M.I7i� R—Ift Fl.p pl MHL MRL MC%W V.N. M.lb.6 N.l q•c+�x 1.26 1 L •1.02, 0 K. N6 -9A EPA ] .D D*KrlpUm: MW I Matron GrO m WAfv Ploj6dL S." Co CW.W MSWLF - M. A­ CIa..IU I Ch$M Iacry P&ratneten FACJ Cary aWOT d—.,v JW SPIJ AMMUD lCASXumbul M . ISM 1.-n q ANALMCAL evcul rc l.8 S—pl.10: U09M-01 F- . P1.6: 0l110112 06-90 Sam pl.d 0ji I Pf:- IP www..nrnl.p r.cvm 0..aI—d: W23117 1030 Work or6.1: CM7% ARAWY tl o =U au xo. asc MIAM, U-t , A...,.aq at MOA. on. u •yn vvr. v.w k J.o MM.l] n.0 — I- w.•+. m.n, — N .�. w� n �K.�...r �...nMr. u�. tiL •w M •erM.N � Lr. 1'.444 d ii www.en cvleh.n,.0 On.rlprlen: MW-17-. l.h S.mpl. 1p: r.i n9 ra-0! R—I-d: 00/17/12 1O m4t,px: Gmw o W.tC S.Lnpi.6: GSA e:.l1: �/i.•rl Work Ord— C2"?% P.e}WS: Starr Co. CW W MSLW - M{. ANY 5—pIz By. i •'kN Glawfwrl Chem ktry Parrmatari ' fdCil l7.Y Ltwyd a,Wifr1+1C S9!] A.AlxN.1LdS.dYalhtl La.Il. Ea uwu ul m" KaL mr- wasw AWSM4 iR Holm ...m,.. p..ar•.ral• .... L ^y, I nd. ow w rrn ,m. nmv L, A.n — �Lf nr.n ....n w M m MM a 1.[a.M h N. L,Iwuen..b +r eM a r.r+N+r n rM Pale 5 v[ l I 0eeCripSlan: MW-17 Leh Ewnple 1A: C2p97"-07 rmxld M.U-1- Gw.[v Sampled: OOf 10.r 1; [1']5 Scary Pruj6d: to CINM MSW1F • ML Alry S.mpred ow; 1.'10H Lla lc.l chem ktry P.nrR.bory A..LLaea fcu M�ha[! ElVC0 www. nronlabr.eom Retay.d: 091731l7 m:;o Work Order: M9795 Azi.us t1e0 uuu lz MAL !SILL lSLSSYSL C.1h" BeWPd 1k MISS Dwalpd— MN-l5 Lab S.mpl. L0: CZ1979d-I4 K.W.: cra,.d w.fr Sampled: G11201i2 12: 00 Py*]*O! Spry Co. Ck.d1 MM9 - Mt. Airy Semplyq Ityl J. PI.M Cia..lcel Ch.fnktry Ppltim.tan ^ -E/1CP [ry rerVNrlM+rlhC ;P11 MwAa IEl. xw.Ler1 .nna. ltaHFu-rl ^ ENIC0 wWw-enpMeba.mm R.O.WM= 01473119 10,;o Work Order. C2D9M 6AAWL >Ja 41p14 G[ tlOL wai ML�]ffSL �epd 8e.4�d 6l hL}A. o Ala V iwp2 ! oury o 1C xe era [oo.o wear, ll oo.!- [ce rya earn new a.ry �va aw�r4 u r«uwa F sa i..arrw. w nu. e,.r a. r..�rw•� yfJ ien ..pen l.4r•r �lr +. in..a.�.Y rr �w.y.e ey via �ay.rrl,.M ^nr �! M np�awrar n �W Pep b.!lI Pa pp 7nf I Cv.Apl-kn MW-16 L.. Sam PI. IOl Ci09296-05 R.WR: GaW WHIM S.mpl.d: 0IV20112 l2:00 Praj NO: Swry Co. ClaSed MSWLF • F1f Airy Stiff Plod 6Y: 7- PION Ci..alul ChdMIt y P.ram:.t.r. e.4441r� ....N.. ra"Ill+r•11 e Wk, ca www..R l.o..eam Recals.d: 08J2]eQ i0 10 Wark Ord-: C209M R.m4eL fly¢ IL= LE MGL MU Me SWSL h1.sk.d 8—.h Ei ham -A 1 Polo ... .. na 10e0 "nwij 00:1. Cr Mrcrrv..n m4ehN.eor� Classical Chomlotrr P.ram.ter. • efV Control ❑URLITS'_COHIROL Beck .Wfd1O - NO PREP _ Al..k {pf04010-ELIq} ..a9:0-;N1. 0 947i V01] I' l? SpINR Se ft MRIC RM M R..91t MRL U.Ita L.r.1 A —IL WRFC Urnld Apo Llmie IMS (0I04010-M1) Pmp.md: 09iPa2012 08'.6 tiWytt0: 09IM2011 0-n SPIN. SeurC. MFAC RIM AR. b to lr . rug MRC U.P. L—W R-.I% %RIC Limits RPO U.rt M.[r e.W.w. � t .5a q1 I n f00 w ffP M.lrlx SPI N e ( ]10.R10 • MS] ] R w-O: 09MR012 00:45 Mlypud; "M42012 10r l5 Se r< G]0 027-01MI .p0t. ft. %RIIC RM 'An.irl. A...lt PI.v i.Rt U.I. Lows! RbWt MA11C U&m Rro Llmlt Ih1n M4y1. Spl�. o.p Ptaeu10•M5772 Rd. OYf011]012 OS M*w 0910WN1210:31 s.a.u� Clu9.]fbLR[y SPIN. Surd HRlC RPP fM.IYkN R.sNlt ppo MAIL4.Ip L. l Rpult 19R1C_ U.". R/0 Lilt II.W llx I—— . .iR...+nh......,..P h t. ­n•....— mar•-, N. iMb "wM Page 8 or I I P., 9 of I I B U E MRL E,hiC� w�wr.en hfl efrf. eo nr The analyte was detected in the OSSOClated method blank. The sample was Anatyted at dilution. The reported value Is between tit lapbratory method detection Iwrk (M❑L) and the la bpfatory method reportlnq limit (MRL), adjusted for amat Sample preparation data and molstum content, where applicil We. The analyte was ana"ed for but not detected to the level shown, adjusted for actual sample preparation data and rrwisture Conaenl where appllCable• Tne Co'centratlbn Irdt[a[ed t9r thisanafyte Is an estimated value above the Ca Ltxatlon range of the hlstru-crit, This value is Considered an estirmie. Method Reporting LYnit. The MRL Is roughly equivalent to the practkal quantltabon k m1[ {PQL) and Is based on the low pant of the cailbr tion curve, when ai)OCAbk, sample pfeparatmn factor, dilutlon facor, and, In the case of soli samples, moisture COMent- E U f4aa lu of 11 Pape 11 F 11 �JVC� ..vw.anmle6a.mm MEN I oil ■ SEEN loss Olson mass MOMMM me% son ■ Eli NONE UNCOMMON MOMMUM1111 I 110090 1 NUNN IN LEE 111111 October 23--24, 2012 Quarterly Water Quality Monitoring Report Prepared far Surry County Closed C&D and Closed MSWLF, Mt. Airy Mt. Airy, North Carolina October 2012 UfC Permit Number:Wi0400176 SWS Facility Permit Number: W02 MESCO Project Number: 612032.0 Submitted: January 31, 2013 Emtntnic�i�pwc-,, f r- Mc F.O. Box 97 Municipal Engineering Scrvices Company, P.A. Gamer, NC 27529 Gamer and ems, Norm Carolina License No. C-0281 TABLE OF CONTENTS SECTION Introduction . _._.._ .�.... _ 1 _-Page Back round_-_-_^_- __- - g - _ - --- - � Page 1 Sampling Procedure 2 _ _W _ . _.--_-._-------Page Field Parameter Data 2 .._ w_W .._W_..Page Laboratory F�esults _ _ ..._...._.._.._._. _..... _..__._.._.._...w..._._� ............ .......w...­­-_.--Page 2 Groundwater Samples_ _ . _..._ ..w� ._..._�,..._._... _.._.__._.._ _ �,..w _.Page 2 Groundwater Characteri�atian _.._.... _...._ _.._._.w._ _...._ ._.W. ....- ..Page 3 Findings �.._.-._...__ _._.� .___.._. _ ..W.._..w___W.�. _ - Page 3 Page 3 FIGURES Topographic Map with Site Location_ _ Figure I Potentiometric Map of Uppermost Aquifer wl VOCs Detected Above 2L Standards .......... _-___-_-_Figure 2 Time Series Graph of Total Cumulative VDC Concentrations___-.___.__.,_-..-_............... Figure 3 TABLES Sampling and Analysis Summary Table 1 Detections that Attain or are Above SWSL or 2L Standard {Appendix I} m_ m_ Table 2 Indicator Parameter Data Summary -------- __...... -................. ............. ... ........... ........................... .... ......... ._..._..._................. Table 3 Field Parameter Data Summary Hydrologic Properties at Monitoring Wells APPENDICIES Table 4 .....Table S Laboratory Analysis Report and Chains of Custody„..--_-,,,,,,, ---------_-W__W------------ _ W--------- Appendix A License No. C-0261 CWILISANITARY IENVIRONMENTAL ENGINEERS SOLID WASTE MANAGEMENT Municipal Engineering Services Company, P.A. SITE PLANNINGISUBD(VISIONS SUBSURFACE UTILITY ENGINEERING (SUE) t January 31, 20I3 Mr. Thomas Slusser, P.G. Aquifer Protection Section -Underground Injection Control Program Division of Water Quality North Carolina Department of Environment and Natural Resources 1636 Mail Service Center Raleigh, NC 27699-1636 Re: Quarterly Water Qualify Monitoring Report Surry County Closed C&D and Closed MSWLF, Mt. Airy 237 Landfill Road Mount Airy, NC 27030 Event Date(s) October 23-24, 2012 SWS Permit No. 86-02 UIC Permit No. W I0400176 MESCO Project No. G 12032.0 Dear Mr. Slusser: Introduction Municipal Engineering Services Company, PA (MESCO), on behalf of Surry County, appreciates the opportunity to present this brief Quarterly Water Quali4, Report that details a water quality monitoring event performed at the Surry County Closed C&D and Closed Unlined Municipal Solid Waste Landfill (MSWLF) Facility (Permit # 86-02) on October 23-24, 2012. The Injection 11Wl Permit Application and Well Permit No. W10400176 (51611 1) requires that Surry County provide this report to the Underground Injection Control (UIC) program on a quarterly basis. Laboratory analytical results indicate volatile organic compounds (VOCs) attributed to landfill activities continue to persist within three wells that monitor the uppermost aquifer downgradient of three injection points. However, tot a] VOC concentrations compared to their respective baseline averages established during the five events prior to the November 2011 injection have decreased inmost locations. Background The Surry County closed C&D and MSWLF, permit #86-02, is located at 237 Landfill Road in Mt. Airy North Carolina. The site location topographic map is depicted in the attached Figure 1. Prior to becoming a C&D landfill the subject area operated as a MSW unlined sanitary landfill that stopped receiving waste prior to January L. 1999. The MSWLF was closed with a low permeability cohesive cap per the Transition Plan. The top portion of the southern unit served as an exclusive C&D landfill until prior to June 1, 2008 at which time it was properly closed with another cohesive cap in accordance with the Closure Plan. Per the NC Solid Waste Section (SWS) approved Corrective Action Plan, enhanced bioremediation via substrate and tracer injection was initiated in accordance with requirements outlined in the Injection Well Permit Application and Well Permit No, WI0400176 (516/11 . E SW598B42 lus Ix16 oz EOSOD Vitamin B12 supplement and sodium bromide tracer were injected into er 7-3, ZUrM an effort to reduce low level aliphatic and aromatic chlorinated hydrocarbons in gr ."Carolina Groundwater Standards (2L Standards). Injections were performed thrn - , details are provided in the Injection Event Record dated November 4, 20ld- PO Box 97. Gamer. Noah Carolina 27529 (919i 772-5393 PO Box 3a9. Boons, NC 286f17 (828) 262.1T57 Water quality at this facility has been monitored at least semi-annually since 1989 with historical data available since 1994. This is the fourth quarterly post -injection water quality monitoring event with previous events performed on February 9, 2012. May 30, 2012 and August 20, 2012. Reports of previous events have been already submitted to the UIC and SWS. This report contains sampling procedures, field and laboratory results, groundwater and surface water characterization, and findings. A potentiometric map of the uppermost aquifer, time -series graphs of select constituents, a table of detections compared to Standards, field data results table. groundwater flow directions/rates table, indicator parameter data table and laboratory analytical data results are also enclosed. Sampling Procedure MESCO personnel performed this sampling event following the parameters and frequency approved by the UIC. Monitored locations were consistent with those approved by the UIC with the exception of points planned to be established downgradient of IW-1. Since injection into IW-I was unsuccessful downgradient points [MW-17. MW- 22 and Stoney Creek surface water (SW-4)] have not been monitored on a quarterly basis per the UIC permit. However, these points have continued assessment monitoring on a semi-annual hasis under authority of the SWS. Groundwater samples were collected and analyzed from nine wells which includes MW-3R, MW-125, MW-12D, MW-13, MW-15, MW-16, MW-18, MW-19 and upgradient background well MW-I. Additionally, water within the injection wells were measured and visually evaluated in an effort to determine the amount of residual organic substrate remaining in the wells which may help evaluate the viability of these wells to be used for future water quality analysis. Monitoring locations are depicted on Figure 2. Sampling was performed per the protocols outlined in the SWS approved Groundwater and Surface Water Sampling and Analysis Plan which was submitted with the Corrective Action Plan (CAP) revision 2 dated December 10, 2010. The depth to water in each well was electronically gaged prior to purging to quantify the static water level elevation. Low -flow pumping methodology or bailing was utilized to adequately purge Elie wells a minimum of three well volumes or until dry. During purging the stabilized field parameters were recorded. The samples were then placed into laboratory -prepared, pre -preserved containers via a new disposable polyethylene bailer. Samples were kept on ice, and transported within hold -times to a NC -certified laboratory under proper chain of custody (C-O-C) protocols. Field Parameter Data Field parameters recorded included pH, specific conductance, temperature, dissolved oxygen (DO), oxidation reduction potential (ORP), total dissolved solids JDS) and visual turbidity. A summary of the field parameter data since injection is presented in Table 3. Laboratory Results Pace Analytical Laboratories (PACE) of Huntersville and Asheville, NC performed the majority of the laboratory analysis. Groundwater samples were analyzed for all the parameters requested by the UIC which includes constituents listed in Appendix I of 40 CFR 258, alkalinity, sulfate, chloride, total organic carbon and biochemical oxygen demand. Environmental Conservation Laboratories (ENCO) of Cary, NC analyzed select samples for the bromide tracer. A sampling and analysis table summarizing the locations, target parameters and laboratory methods is presented as Table 1. Water samples were reported at the laboratory specific Method Detection Limits (MDL), which are quantifiable at or below the current Solid Waste Section Limits (SWSL). Laboratory results and C-O-Cs are presented in Appendix A. Groundwater Samples The wells with Appendix I VOCs detected in concentrations in exceedance of their respective 2L Standard during this event include MW-13 (1.2-DCA), MW-15 (PCE, TCE, l,i-DCA and vinyl chloride) and MW-16 (1,4- dichlorobenzene, 1,2-dichloropropane, 1.2-dichlroethane, benzene, vinyl chloride). Table 2 summarizes Appendix constituents detected in the water samples in concentrations above the current SWSL or North Carolina Groundwater Standards (2L). Table 3 summarizes indicator parameters quantified by the laboratory. A site map depicting the spatial distribution of VOC concentrations detected above the 2L Standard during this event is presented on Figure 2. Groundwater Characterization A potentiometric map of the uppermost aquifer created from static groundwater elevations recorded during the October 2012 event is included as Figure 2. Groundwater flow rates and directions were calculated via modified Darcy's equation and are included in Table 4. Groundwater flows in the unconfined and upper bedrock water - bearing zones in a general southwesterly direction away from the waste limits. Calculated groundwater velocities were variable but consistent compared to historical observations. Findings The quarterly laboratory results indicate that low level dissolved phase VOCs consisting primarily of chlorinated hydrocarbons continue to be detected in groundwater samples collected from MW-13, MW-15 and MW-16 which are located within 250 feet of the waste boundary. No contamination continues to be identified in samples collected from the other six wells sampled during this event. All VOCs detected in concentrations above the 2L Standard during this event remain within their own respective historically identified range. Total cumulative VOC concentrations compared to their own respective five event averages decreased in MW-12S (-100%), MW-13 (-35%), MW-16 (-25%) and increased in MW-15 (2%) for a total cumulative reduction of 21% (Figure 3). Evaluation of the injection wells ([W-1, IW-2, IW-3, IW-5) continues to indicate that a considerable amount of residual organic substrate remain in each of these wells rendering them unsuitable for representative water quality analysis. The viscosity of the water in the injection wells precludes sample collection as either a bailer would not descend or the check valve failed. Bromide tracer was only detected in low non -quantifiable ` j-qualified" concentrations in MW-12S, MW-13 and MW-16 during this event. Bromide concentrations have exhibited an apparent increasing trend in MW-16 (Figure 4). Closing Corrective action to remediate the VOCs as detected in groundwater is expected to continue. Monitoring of MW- 3R, MW-12S, MW-12D, MW-13, MW-15, MW-16, MW-18 and MW-19 is planned to change to a semi-annual basis with the next event scheduled for May 20I3 as proposed in the approved lnjeclion Well Per mir : fpplicaiiorr. If you have any questions or comments regarding this report. please contact us at (919) 772-5393 or by email at jpfohl umesco_com. Sincerely, MUNICIPAL ENGINEERING SERVICES CO., P.A. �q l Jonathan Pfoh[ Environmental Specialist Enclosures cc: Mr. Dennis Bledsoe Surry County Ms.laclynne Drummond (Electronic Copy Only) SWS-Compliance Branch Ms. Sherri Knight (Electronic Copy Only) UIC Ms. Shuying Wang (Electronic Copy Only) UIC Figures Topographic Map with Site Location Surry County Closed C&D and Closed MSWLF, Mt. Airy hard surface improved surface Secondary highway, hard surface Unimproved road --z�=— Interstate Route t—) U. S. Route 0 State Route FIGURE I NOW OR FORMER[. Y I OWNED 8Y JOHNN Y COX �� to ova+ sw-2 � YW7 0 ®js 0 SCALEe M59 �ATFJL SUPPLY WELL rw•� OWNED BY SURRY COUNTY n Msr� A? T e.w -ti m.Ps T. NOW OR FORMERLY OWNED BY SHA WNA SUMMERS lmw-2�3 EA75TNu0 TOPOGRAPHIC Ga410l/RS EMS TWC ROADS E57MATED WASTE Wn ON VJM WSW &ICR C&D f -_------------ L*0? LWTS OF SJaIRE 0 LINED YSNIF ....._..._.. EXTENT OF COHE9YE CLAY CLOSURE UPON CLOSED NSW AND CAD i PROPERTY LME EXTRAPOLATED FRaV SLJRWr AND CIS »....,..,.__ CO"PWANCE BOUNDARY (250• FROM EDW of SO' FROM PROPERTY LWE} EXTENT OF VM,? OE7ECTEO ABOVE SWSL & 2L STANOARO SEYONO COMPLIANCE 7fN10� EWPOTENTfAL UPPERMOST GMANOWATER CONTOURS STREAM/CREEKIWVER WATER SUPPLY NEU SW-3 SURFACE WATER L-OWY WNC POINT ~v is Afawtopwcl NELL W40 +N.ECTION WELL I" GROUNDWATER POTENTRDUE7RIC a"A; MSQ WOTE ELEVA TOi NOT USED FOR VON SEDWIENT OA9N OWNED 8Y SURRY COUNTY }} FIGURE 2 i -- - CLOSED C&D LANDFILL and ° • - .� .. CLOSED MS WLF FACILITY Municipal �] [ Englneerrn i ; Services �' Company. P-A- • SURRY COUNTY f' e l _ POTENIILNICifdrC MAP UP "HOST AMWER j 01" rocs DETEiED AROW a STANou W MT. AIRY, NORTH CAROLINA Figure 3 Total Cumulative VOC Concentrations PrelPost Injection Comparison October 22, 2009 - October 24, 2012 TOSai Cumu[Ave VOC ConcenVadons a- SWSL or X Standard Well ID Oct 2009 (ug/L) May 2010 I (ug►L) Oct 2010 (ugIL) May 2011 I (ugIL) Average of Five Events Preceding Oct 2011 Injection Oct 2012 (uglL) (u9IL) (uglL) 0.00 0.00 0.00 Difference (ug L) Difference N MVIt-1 0.00 0.00 0.00 0.00 0.00 0 MW-3R 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 MW 125 0.00 0.00 0.00 0.00 5.40 1.08 0.00 -11.08 -100 MW-12D 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 MW-13 61.00 50.60 74.20 87.30 72.50 69.12 44.70 24.42 -35 MW-15 96.13 63.89 55.00 78.10 64.06 71.44 72.60 1.16 2 MW-16 137.90 113.60 135.70 121.20 116.30 124.94 93.70 -31.24 -25 MW-18 0.00 1 0.00 0.00 0.00 0,00 0.00 0.00 0.00 0 MW 19 0.00 0,00 0.00 0.00 0.00 0.00 0.00 0.00 0 Combined Total 295.03 228,09 264.90 286.60 258.26 266.58 211.00 -55.58 -21 Surry County Closed C&❑ and Closed MSWLF, Mt. Airy Page 1 of 1 Tables Table 1 Sampling and Analysis Summary October 23-24, 2012 A i Indicator Parameters Tracer a� i n E m �n o E @ c m N U D m m 3 a E U 0 ❑ 0 E 0 Ckf> r Q U) p Q m Q LY p CD O m U c0 0 N 4 p �t O CD CDd ED W M U} v � w � C4 O ch M M -0 - Q m Q IL n Ln a- MW-1 x x x x x x x x MW-3R x x x x x x x MW 12S x x x x x x x x MW 12D x x x x x x x MW-13 x x x x x x x x MW-15 x x x x x x x x MW-16 x x x x x x x x _ MW18 x x x x x x x MW-19 x x x x x x x App I = from current 40 CFR 258 Sumr Cauntv Closed C&D and Closed MSWLF. Mt. Airy Pane 1 of 1 Table 2 Detections in Water Sarnples above SWSL, GWP, 2L or 28 (Appendix I) October 23-24, 2012 Sample ID Parameter Name Sample Result Unit MDL2 SWSL' 2L4 Exceedance Date Amount MW-1 Zinc, total 10/23/12 10 uglL 10 10 1050 MW-12S Cobalt, total 10/24/12 10.8 uglL 5 10 MW-12S Zinc, total 10/24/12 13.1 uglL 10 10 1050 MW-13 1,2-Dichloroethane 10/24112 1 ug1L 0.12 1 0.38 0.62 MW-13 Trichloroethene 10/24/12 1.6 uglL 0.47 1 3 MW-13 Zinc, total 10/24/12 16.4 uglL 10 10 1050 MW-13 11-Dichloroethane 10/24112 8.5 ug1L 0.32 5 70 MW-13 1,4-Dichlorobenzene 10/24112 4.3 ug1L 0.33 1 6 MW-13 cis-1,2-Dichloroethane 10/24/12 29.3 ug1L 0,19 5 70 MW-15 Trichloroethene 10123/12 4 ug1L 0.47 1 3 1 MW-15 1,1-Dichloroethane 10/23/12 17-1 ug1L 0.32 5 6 11.1 MW-15 Benzene 10123/12 2A ug1L 0.25 1 1 1.4 MW-15 Tetrachloroethene 10123/12 1.2 uglL 0.46 1 0.7 0-5 MW-15 Vinyl chloride 10123/12 1.4 uglL 0.62 1 0.03 1.37 MW-15 Vanadium, total 10123/12 7.5 j uglL 5 25 4 MW-15 Zinc, total 10123/12 19.1 uglL 10 10 1050 MW-15 cis- 1,2-Dichloroethene 10123/12 34.3 uglL 0.19 5 70 MW-15 1,4-Dichlorobenzene 10123/12 4 uglL 0,33 1 6 MW-16 Benzene 10123/12 1.8 ug1L 0.25 1 1 0.8 MW-16 1,4-Dichlorobenzene 10123/12 20.6 ug1L 0.33 1 6 14.6 MW-16 1,2-Dichloropropane 10/23/12 5.1 uglL 0.27 1 0.6 4.5 MW-16 1,2-Dichloroethane 10/23112 2.8 ug1L 0.12 1 0.38 2.42 MW-16 Vinyl chloride 10/23112 5.7 uglL 0.62 1 0.03 5.67 MW-16 Zinc, total 10/23/12 13.6 uglL 10 10 1050 MW-16 Chlorobenzene 10/23/12 6.8 uglL 0.23 3 50 MW-16 Trichloroethene 10/23/12 1.3 ug/L 0.47 1 3 MW-16 Cobalt, total 10/23/12 247 uglL 5 10 MW 16 cis-1,2-Dichloroethane 10/23/12 49.6 ug1L 0.19 5 70 I Table contains Appendix I constituents detected at or above SWSL, GWP, 2L, or 2B i MDL = Method Detection Limit 3 SWSL = Solid Waste Section Reporting Limit 4 2L = North Carolina ISA NCAC 2L Groundwater [Quality Standard BOLD = Concentration a 2L. or 26 Standard Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Table 3 Indicator Parameter Data Summary February 9 - October 24, 2012 A"inft Suaala Chtonde lDC HOE) Yetnpopture DRP DO PH 9ratn+6e jTmoj Specift Conduclants Depth to water Walar Elevation Me01m SM 2=6 EPA 3009 SM 4500-Ci- sM 5aloa SM62100 FwIu Instromen F1114 Inslrunlenl FWd 4lstrunent pidid Instrumanl EPA 300.E Field Instrument Feld Inslrw m Cakulalmn LIDL' low 2000 1000 1060 21100 0.0 A00 0.0 0.00 0.024 0 0-00 0.00 lM95 uglL 1 UgIL kpW1 4L C MV Z21W nyltus7cm FuAoc pt" 2110M 57400 63M c5000 2930 420DO 14.4 120 2,4 6.63 c11-021 300 25-70 1103.55 M002 69800 7710 3560 c1000 <2000 74.4 167 2.9 5,96 Ns 360 22.45 1111.37 81211f 52200 7tae 17711 2990 <2000 14.11. Ida 3.1 5.98 19.029 31a 22.63 1111.72 MV9-1 IWWI2 24M 7450 4340 3070 <2000 16.4 207 &1 8,73 m.029 300 22,05 1105.30 h6n 24WO 6330 35b0 2030 c2000 14.4 128 24 5.96 c.a24 300 22-48 1105a0 Avg. 51000 7185 3890 2997 r2000 15.0 1$a S0 5.38 s424 303 24,87 1109.119 L4cc jam- Me 4340 30T0 0000 IM 207 3.1 5.83 e,024 310 29M 1111.87 VAIIZ 123000 eSaS0 E5000 3820 0000 15.1 do R.3 7.08 e0A24 270 41.65 975.85 Won 2 94NOO 4950 2780 r1000 0000 1S.7 121 0.6 7.54 NS 250 40.13 977,37 a72911 2 90090 4780 2Bb0 19000 0000 15.9 lie 0.5 732 NS 250 4229 W521 MNLM IW3n2 1040M S850 1110 2410 0000 15.2 132 01 8.12 NS 3110 42-54 274-M Mkt 90000 4790 2780 2410 r2000 15.1 IM 0.5 7.08 NS 250 40,13 974.90 Avg. 102900 520E 2950 Sale :2uou c21100 15.7 115 1.1 7.57 NS 270 41 AS 975,85 Max, 123000 Saba 3110 I N00 15.9 132 2.3 8,12 NS 300 4254 977.37 2AF12 lama 33100 5b10 34M c2600 15.1 125 50 6.69 0.634 SBO 11.10 1012.70 540112 76M 449M 4650 16200 13.7 -773 2.5 7.33 _Z0A29 170 _ 1137 1012.to MV02S grM12 12MM 43200 4880 34200 12000 <2000 13.8 51 3.2 7.12 0.039 Ste 1341 1012.19 10124112 77200 36000 3200 4380 1S.8 -62 1S 7.30 10.029 190 16.71 1009.09 Mn. 78800 33106 3200 3450 c2000 d000 13.7 •776 1.3 a.a9 -•029 170 IS.10 ION-09 A - 90500 393M 4630 14310 14-a -163 3A 7.16 0.C37 33S 1429 1011.52 Max. 123M 44800 Belo 34200 cADO 15.8 126 5.0 7.33 0.039 610 10.71 1012,70 2110012 81200 7220 e5000 37110 4440 15A -62 1A 7-19 40.024 ISO 0.00 1027.05 5n30l12 70M 8S40 1110 -low 7200 13.9 BB 316 7.03 NS 500 0.00 1027.05 110IF12 65000 66SO 41000 2540 3tOp 13.9 -101 1.6 Im NS 580 am 1027.06 MWI20 16R4712 67760 7430 1270 2100 aa06 152 138 49 5.9 NS 370 O.W fa27-OS Mn. 65000 6550 1110 2100 s2000 13.9 -101 1.1 6,59 NS 1S0 0A0 1027A5 Avg., 73425 7460 1190 2807 c2000 14.a 11 2.8 TA NS 300 0.00 1027.05 MUj 81200 0540 12M 3780 0000 15A 138 4.8 7.33 NS 500 0.00 1927.05 219ft 574W di000 U400 10700 .2000 13.8 363 0.7 533 0240 220 MSG 981,92 5r3W1 57700 2660 342M 2430 42000 141 2151 0.7 5,a3 w.029 200 2SA9 933.39 M SA 2 55700 21b0 33090 14700 QM00 13.9 301 0-9 M 0240 250 26.85 ea1.a3 MW-13 1012411 53400 2690 29100 E360 2000 14.2 207 0.7 5A5 0200 210 25.35 952.12 MInJ 53400 2180 20100 2430 0000 13.6 207 0.7 5.33 c,029 200 25,09 981.83 Aty. 58050 2517 32675 W48 <2000 1a.2 288 0.8 5.67 0227 223 26.17 SUM Mix 57700 2690 34400 14700 0000 1a.7 363 0.9 5.89 0.240 260 26.65 965.39 2AII2 48700 c5000 -Sow 11100 24a0 142 -92 23 7.03 c0.024 2B0 52.17 1022.79 5Wl 41059 5450 c2000 11000 400a 14,7 31 0.0 S,93 eO_m 130 52-95 1023.01 6R011 39100 s2000 41000 8520 3200 14.6 19 119 5.96 e0_029 110 51_14 1024-62 MW15 fo0t35 4am 2320 23W 10600 0450 16.3 162 0-1 5.51 W-029 so $0-7Z 1025.24 Mh 39100 me 2150 W20 -20M 14.2 -92 0.1 5.91 401024 90 50,72 192Aa7 Avg, 442N 78410 23M 10440 -2000 15.0 30 1.0 e.14 40,024 140 57.75 1024,22 Max. 46700 54500 23% 11100 4000 15.1 192 2z 7.03 eA29 260 52.95 1025,24 219n12 NOW 7170 lam 14200 0000 14.3 44 4-4 S,711 093E 429 26.a5 972.69 SW2 1140M 5000 Ism 3220 0000 14.5 55 0.9 0.10 11.130 304 25A7 974-07 Br20n12 736000 c20M 36500 123M 42000 14.7 38 0.8 6.13 0166 310 26,95 972.55 1 IV-16 10r"12 142000 Q000 43300 19900 0000 15A W 9.6 5,03 0250 360 27.1a 97L36 Mn 99600 sow lam 3220 .2= 14-S 38 as 3.78 0.038 300 25A7 9-IZ36 Avg 1212906 GO" 27225 12405 -20M 14.7 55 1.7 alai 0.177 353 26.57 972.97 Marc 142000 7110 43300 19900 c1000 15.1 81 4A 6.13 "SO 420 27.18 974.117 10600 <5000 c5000 6350 8830 1$2 305 4.6 6.42 c0.024 0 9.01 973-99 Nall? 5n3W 2 7250 0000 1400 c1000 4000 142 IIE 7-9 5-65 N$ 13 591 977-09 812W121 8020 c2000 I -I000 19W c2000 14.5 193 7.5 5.91 NS f0 BAa 973,52 MW 14 lGa&R2 6470 c2om c10011 1140 c2000 151 288 4.6 0.42 NS a 914 973.70 mini 72K QppO 14017 1140 c2000 14.2 193 49 5.85 NS 0 5.91 073.52 R a635 000o law 3797 0000 14.9 2415 52 6.15 NS a 9.41 974.69 vax.i 10800 c2000 14M a3E0 c2000 117 305 7,9 5.42 NS 13 9.49 977,09 2n10112 11900 e5000 c5000 2530 0000 15.e 309 4.1 5.62 49.024 10 9.41 B36.a6 SW12 12000 Q= 23SO 2470 c2000 1i.4 281 3.5 5.02 Ns 0 922 636.95 B12WI2 141500 2190 2610 s1000 .2000 14.1 s07 31 5.58 NS 0 19,77 935.50 W*19 l0✓•23112 - 2830 4000 2310 2780 e2000 15A 372 43 Slat NS 20 9S3 036.74 _ W 2930 12WO 2310 2470 12000 14.1 281 3.S 5.58 c0924 9 9.32 935,50 A 10a33 2190 2393 2593 0000 14-7 317 3-9 5.66 ea m 8 9.76 936.51 _ Max. 15500 279tl 2510 27ao I Qzm M4 372 4.3 5-51 M-O24 20 10.77 836.95 N01es; MOL' a Lowest Lab S4elnnd Deledew I"or lowest Held rnessmernem posa4lfe. Cnnsa ue11t5 dweewd below quami8able r4n8s are shown as c M0L wloa. NS = Not Sampled For Surry County Closed Can and Closed MSWLF. Mt. Airy Page 1 of 1 Table 4 Field Parameter Data Summary October 23-24, 2012 Parameter Depth to Water Water TOC Elevation Elevation Temp. ORP DO pH Specific Conductance TDS Turbidity_ Units ft (btoc)l ft (amsi) ft (amsi) C mV mg►L SU umhoslcm mg/L. Visual or NTU IW--1 13.55 na T na NR NR NR NR NR NR >1000 MW 1 29.05 1105.3 1134.35 16.4 207 3.1 6.73 300 140 15.3 IW-2 44A4 1024.42 1068.86 NR NR NR NR NR NR >1000 MW-3R 42.54 974.96 1017.50 15.g 132 0.9 8A2 300 140 Clear I W-3 33.98 986.59 1020.57 NR N R N R NR N R N R >1000 IW-5 40.95 1039.23 1080,18 NR NR NR NR NR NR >1000 MW-12S 16.71 1009.09 1025,80 15.8 -62 1.5 7.30 190 90 Slight MW-12D 0.00 1027,05 1027.05 15.2 138 4.8 6.89 370 180 Clear MW-14 41.65 977.15 1018.80 14.8 163 2.3 5.43 110 50 20.6 MW-15 50.72 1025.24 1075.96 16.3 162 0.1 5.61 90 40 78.8 MW-16 27.18 972.36 99R54 15.1 81 0.6 6M 380 160 Slight MW-17 10.38 955.05 965.43 16.0 43 2.1 6.16 300 140 Clear MW-18 9.24 973.76 983.00 15.7 288 4.6 6.42 0 0 Clear _MW-19 9.53 936.74 946.27 15A 372 4.3 5.81 20 0 Slight_ Minimum 0.00 972.36 999.54 14.8 -62 0.1 5.43 90 40 15.3 Average 30.98 1014,14 1046.86 15.6 117 1.9 6.59 249 114 38.2 Maximum 50.72 1105.30 1134.35 16.4 207 4.8 8.12 380 180 78.8 bloc = Below top of rasing amsl = Above mean sea level na = Not available NR = No reading attempted Surry County Closed C&❑ and Closed MSWLF, Mt. Airy Page 1 of 1 Table 5 Hydrologic Properties at Monitoring Well Locations October 23-24, 2012 Groundwater Average Groundwater Hydraulic Effective Hydraulic Linear Groundwater Potentiometric Conductivity Porosity Gradient Velocity Rate Depth Elevation Monitoring (%) (feettfeet) (feet/year) Flow (feet btoc) (feet amsl) _ Well _ jemisecondj _ Direction MW 1 4.30E-05 15 0.081 24 S27W 29.05 1105.30 IW-2 4-30E-05 15 0.149 44 S42E 44.44 1024.42 MW-13 2.06E-04 23 0.100 93 S31E 26.65 981.83 MW-18 2.04E-03 15 0.126 na S25W 9.24 973.76 MW-19 1.10E-03 3 0.081 3,081 S13W 9.53 936.74 Minimum 4.30E-05 3 _ - 0.081 24 - 9.24 936.74 Average 6-86E-04 14 0.107 811 - 23.78 1004.41 Maximum - 2-04E-03 23 0-149 3.081 - 44.44 1105-3 MW-3R 2.40E-04 5 na na na 42.54 974.96 IW-3 2.40E-05 5 0.243 121 S41 W 33.98 986.59 lW-5 4.50E-05 5 0.116 36 S30W 40-95 1039.23 MW-12S na 3 0.060 na S09W 16.71 1009,09 MW-12D 1.30E-06 5 na na na 0A0 1027.05 MW 15 7-21 E-05 3 0.122 304 S06E %72 1025.24 MW-16 2.82E-05 3 0.257 250 S42W 27A8 972.36 Minimum 1-30E-06 3 0.060 36 - 0.00 972.36 Average 6.34E-05 4 0.160 178 - 30.30 1004.93 Maximum 2.40E-04 5 0-257 304 - 50.72 1039.23 NOTE Values for hydraulic conductivity determined via slug test by GAI, MESCO, or Joyce. Hydrologic gradient from water levels recorded on October 23-24, 2012. Wells screened entirely in rock were not utilized for flow directions/gradients. Screens that traverse both rack and regolith assumed flow in regolllh dominates. na = Not available/applicable Average Linear Velocity (Q) is defined by modified oarcy's equation: K A K= hydraulic conductivity where 0 - - • - ne= effective porosity Ul dim head difference dl= horizontal distance Screened Interval Lithology Clay Clay Saprolite Saprolite PWR Fractured Rock Fractured Rock Fractured Rock Fractured Rock Fractured Rock Fractured Rock Fractured Rock Suny County Closed C&D and Closed MSWLF, Mt- Airy Page 4 of 1 Appendix A Laboratory Analysis Reports Chains of Custody . Pace")ytrcal' November 09. 2012 P.0 Aryryne.l B.frfen, fn.. .W E..f M.— Rc.d . 3w`r. A Ee.n NL 27yA6 r136ri218011 Mr. Jonathan Pfohl Municipal Engineering Services PO Sox 97 Garner, INC 27529 REProject: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92136379 Pia. Aftmvo l6.rYlen, M. P.w A..Ivm.+ 5--co., line. a M.C. A-wyee.4 6.fWe..- kli P.C. ArWYook 5wry.- W. P.- A.Nytim S---. M. 2T.5 RNff W G Pa61i n-.C.r A.. 5— +00 p7� pA,�,� yy Pt�GrQly�ri l mo E..i M..vavf +feae %.: A 22Z Fl. n or vB:q ...yy nn. Sw. W A.n.wi.• NC 2Wk- H-NX. " NC 26076 fyy�y Ea.a NC T766 Awwfl. NC 79" fn,ny..... NC MIS1om)Me-7i In i70,%75-0 2 immZ!AY]f t626%25+7+75 l7owmem CERTIFICATIONS Piolect BURRY CLOSED -MT AIRY WICI Pace Propct No.. 92+16379 LirarI0S1� G m}lctlton Ids 9800 Kiri ey Ave. Ste t00. Hunt vrerfiv- HC 28076 Flwldw%EIAP CA rli6Gfeon s E87627 Nvh Cn:m DA'Wnp vvetd ccmft a5an f 3T7p6 keoWt ky UST Certlflr _ F 0 Norm C.roNn. Field 5afvice. Crr7.c.em �: 534i We.t W pins Certi6caeon f 357 NarN Cmr:n. w""Ater CerpSCa[Iwr f: t� vrginr.lyELAP Cerohc.11an A. 460,22+ sa m caralnA cem6 scan f ND05MI AiAo wilt- Ce-5nentiorr, tp. 2225 Fbve-s'de Of • h.rtvft. INC 2nm Norm CAraen, Wm.tew.ter C.reec.00n f .0 Rai, .1NE LAP Cmm&-mn ■: E67CA8 South C—W. C. l-0 f 9H300t}t ?A s"chuA m Certftfl- 0. A4NC036 Nh11 vitoma C.rYky9on 356 room cm..a c mWng YVAIW Cnrgec.cnn r V7+2 vif,;ml%IVE LAP Cer Me llon 0 e60222 Deaf Mr Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory between 0dober 24, 2012 and October 25, 2012. The results relate only to the samples included in This report Results reported her eir. Conform to the most current TN standards and the laboratory's Quakily Assurance Manual, where applicable, unless otherwise noted to the body ol the report Analyses were performed at the Pace Analytical Services location indicated on the sample an alyte page for anatys+s unless otherwise footnoted. it you have any questions COncernjng this report, please feel free to contact me Sincerely, Kevin Godwin kevi n. godw i nLM. pace) a b s. com Project Manager Enup.ur.A REPORT OF LABORATORY ANALYSIS 1 r-.. �.pcn.nu roi a r. PfP3we ..�.rn n ti i ve.�P�l N vn�tl.n t�1 Pf P.ef An.ysnl 6uraef •.. Peen + of 49 REPORT OF LABORATORY ANALYSIS He"Wn Y•..-wi h. , duwf­Ptnfw 0"W"x ft-c-4.l P.. A-ly.ui S.— rv. P.ue 2 ur 45 IV 6 PAM Ar Yftfil 94M[n, Inc. P.sa Analreeal 6WIM., Ind- Pan Anafytlad 6arvlen, M.. J 246 E.m Meamrw Road � !i f A 2ns Rrvrrda Or Y600 K—,Ara Sww tpp + •..Mt'ar.•ea�aWln Ewen NC 772B6 Mh.y6. NG 2664i Nnl.mrh. NC 29079 + !136y521dB2r 18�1234-TIiB (7[MrBT'+91R2 SAMPLE SUMMARY Prokcl. SORRY CLASED-MT. AIRY MCI Pace Project No.: 1036379 Lab ID Sanpla tD Matrix Was Ccgkm d Date Rocoyed 62138311001 MW-1 Mter 10r2VI217'00 IW40121675 92136379002 MW.7R Water 1W2311206-35 IWV1216:36 02130379007 MW18 WM1dr ICQ311210:45 1=41121635 92116179D04 MW-12S vv tar IOQ01215�0 Icv2v1214j0 8213W179006 MW-12D Ware, 101201214!34 10461121420 821363790D6 M1N-13 Wa14r 1012471211:00 104571214:29 9211617W007 MW-19 W.Ier 1=4J121200 lorP51121470 9213937900a MW-19 41ra!ee 101411217:00 1025f121420 REPORT OF LABORATORY 4ANALYSI5 I lva r.MH Yl.r ml W f.prodwed..xc491 n hAI w6wu1"-Ir6n vy,aant of Pete Au 10S.—k Iw Pogo 3 0149 Pau F6M yWNl 64rvlen.lne. PA.6 AMIyeN1 aerylnl, Ine, �f [��. P. YI1 H11 �1.• WA Eau Mda&w Rome -3uid A 2225 Rrr.r+G dr „ry wrw_r w+i Ewr.. NC Yl:�6W Abler+le, NC 2696A ❑161673-ml RI2ey16W7r76 SAMPLE ANALYTE COUNT Pr.I.Cl St1RRY CLOSED -MT. AIRY (UIC) Pa c e Pojeo No.. 92116379 P.q A6alyee.l Werylq �, 16L 9� t(.nc.r M. S--% 103 >•unl..w�u. Nr: 2a176 1704f6Tbaati2 Analyl- Lab fD Semple ID M61hod kwlyats Rep.cb d Laborarery 9213637Wo01 MWi EPA6010 J4dW 15 PASI,A EPA4240 KJM 52 PASI.0 SM 23200 KCS I PASI-A SM 52100 LMD I PASI-A EPA 300.0 AES I PAST -A SM 4500-CI-E DMN 1 PASIA SM 5310E AES 1 PAS -A 9213617W002 A1W3R EPA6010 JMW 15 PASI-A EPAW26O KJM 52 PASI-C SM 23208 KCS 1 PASI-A SM 52108 LMD 1 PASI-A EPA 3000 AES I PASI.A SMA5ODZI-E OMN I PASI-A SM 5310E AES 1 PASI-A 92136379001 Mw-is EPA 6010 JMW 15 PASI-A EPA6260 KJM 66 PASI-C SM 83ZDS KCS 1 PASI-A SM 52108 LMD 1 PASI•A EPA 300.0 AEG 1 AASI-A SM 4500LC1-E DMN I PASI-A SJA 53100 AES i PASI-A l213637HU MAL12S EPAR10 JMW 15 PASKA EPA 5260 KJM 52 PASI-C SM23205 KCS $ PASI•A SM 52108 JSH 1 PASI-A EPA30D.0 AES i PASI-A SM 4500-0,E DMN i PASI-A SM 63100 AES f PASi-A 92131079005 WhI.120 EPA SO10 JMW 15 PASI-A EPA 6260 KJM 52 PASI-C SM 23209 KCS s PASI•A SM 52160 JDH s PASI,A EPA100.0 AES t PASI-A SM 4500.C1-E DMN 1 PASI-A SM 53100 AES 1 PAS1-A W211W179o06 MWTS EPA6D10 JMW 15 PASI-A EPA 62611 KJM 6W PASI•c REPORT OF LABORATORY ANALYSIS Page 4a+49 Tna r.pfrt NAA nei W t.Vroducw,.�uPl m full +NP lPw .nripin wnwnl el Pace Analytical ServN:ee. i� Pau Analye[w &ww[.{.1M P4 C4 An.l1M416.fe141,'m a�'E ytl�t • 205 Ea., M..eew Re.e - 5.et. A 2Z. R,v . tl. .�o4nesW ee�. Ed.n Nc i77e6 A.n.,die K 7NK4 p36)n71492, 14 78125a-7, 75 SAMPLE ANALYTE COUNT Pra}ecL SURRY CLOSED-M i. WRY (u1C) Pace prgecl No: 92136379 pan An4lyuur S{nl u., Ine. w.nynwee. NC 7811e r�oaie�s-east Analyms Lab l0 8ampio 10 LSaHla6 Anely." Reported J-Ab..wry S023208 KCS I PAST -A W 52105 J9rt I PASI•A EPA 3% 0 AES I PAS( -A SM 4500•CFE OMN I PAS( -A SIA 5310s AES i PA51•A 12116179007 MW-18 EPA6010 JMW 15 PAS( -A EPA 6260 KJM 52 PASI-C SM 23206 KCS 1 PASH-A SM 521013 JUK 1 PASi-A EPA 300 a ASS 1 PASIJL SM 4500-CI-E DMN 1 PASI-A SM 531 Q8 AES 1 PASI A 97119375008 MIN-19 EPA6010 JrBW 15 PAS4,A EPA 6260 KJM 52 PMA-C Sµ 23706 KCS t PASi-A SM 52105 J811 t PASI-A EPA31109 AES 1 PASi-A SM 45004i-E OMN I PAST -A SM 5310E AES 1 PASI-A REPORT OF LABORATORY ANALYSIS P.B. 5.149 rA{,epen M"rot w;GMd ae, . 0 n tun ..abut t. MmUP c. -1 of P.. AMynca S-ry ..Inc Pau Anal, Ine- 1-A n4lc[I ee.yl0e[. Ie4 Plp Rn�l 11111,1, IP[. aceRnalyticalR MS Eeel W.W.W.RPw - Swl{ R y.2225 Ai..rea. w ue0v • nr1 S 10p NC 27.Ta A.n.H.. Wr 20W4--Wre,�M. i4L M28 OW473-MT 1e20'2WI76 17041e'IS-9W7 ANALYTICAL RESULTS pmiect SURRY CLOSED -MT AIRY ILrIC) Pen Project N. 02136379 Semple; MW-1 LWQl 92136VII001 rpkded. IW23112 17.00 Recuyed: IOR4f 12 16'33 MaVuV*m t Report Peremerere Reevps Uruu Um6 MDL OF Pepwed Analyzed CAS No Q11e1 60101QP 6ro9ndwrier Mssyr k l Meylud: EPA 6010 Pmpara9en µelhW EPA3010 Andma,y NO uA 6.0 SA 1 1026f1216,55 111011129107 744036.0 Awmc NO uyL 10.0 6.0 1 1WS012 Ia:ss Iimil1201p7 740,311,2 aarlum 56AJ ZL 100 SA 1 1W251121ej5 111011I201.67 7440it-3 Elw^m NO aDL 1 0 10 1 100511216'S5 211 .0 -1440..1., Cedwoum NO uplL 1.0 S.a 1 10061121a:56 HtD 291 o7 7440i3-9 Chmmlum NO u01L 1p0 50 1 1W2511216.55 1110101201.07 7440473 Cobalt NO uWL100 6-0 1 104611216'.35 11101f120197 7H04B4 Copper NO uyl 13.0 50 1 10Q51121a15 1110111201.07 1.11-W. Leed NO uy1L too 6-0 1 IOQ5112 fai5 11101f12010? 743W92.1 Nickel NO u01L SOA 50 1 f0Q6f12 la SS 111010 12 01.,D7 744"2k Selenium NO uWL 10.0 10-0 1 100912 1a;" 1110111201 47 776249.2 SINe1 NO up 10.0 i.0 S IMU12 "15 1110111291-97 7440,22.4 Thaloum NO uWL 5.6 3.4 S IWS112 t535 11101/12 01 p7 7440.7E-0 V4nemum NO u0R 25.0 6p 1 lww$2 16155 1110111215107 744042.2 1- 10-0aWL 10.0 10-0 1 10Q50216:55 f1101ft20101 7440466 8210 M5V Low Lerel Laed7Rl An-"P IAalhad EPA MO Acelon. NO up1L 100 10.0 1 1110,1712 17-32 67-64-1 AerymniIrae NO 401L 200 is 1 11/03112 1732 107-13-1 8anxene NO uWL 10 0.25 I 1110311217:32 7143.2 gromochlor.melh... NO uWL 1.0 0.17 1 11 M112 17;32 74.W-5 Eiromodkehto-1h.ne NO u01L $.0 0.18 1 I110311217:32 75-27J em"IDOM NO 11pIL 30 026 1 11 W$2 I7:32 75.25.2 Promernetl,ane NO u01L 100 0-29 1 11f03112 1732 74-a19 2-autanone z,) NO 4;L I 0.96 1 II103Jt2 17:32 7a43.3 C:'b n M.'A8 N13 u0rl In 12 1 111n 21732 MIS-d Carbon 101mciuprld. NO 41L 10 0.25 1 I1f03f12 1732 56-n-5 Chlnropeniene NO uyL 3.0 oil 1 WtIw1217:12 iM-9D-7 Chbr601han4 NO U VL 10.0 0.54 1 11+'03+12 1732 21-Oa1 Chlerefwm NO UVL 5.0 0.14 1 WOV1217:32 67-46.3 Cnl.feme1h-6 NO u91L 1 0 0.51 1 111031:2 I1;32 74-67-3 12.Olbt mo-3-chlarapropane NO ugtL 130 2.5 1 1,M312 1722 26.12.6 Dbno rjklme elhane NO LVL a(]0.21 1 111d31I2 17:12 I2446.1 t,2-DINomulhane (coal NO uWL 10 077 1 1110311217:32 100.93.4 OlbfomOmetherM NO wA 1110 0.21 1 IT1031121732 74-95-3 1,i-0lohiwaben;ens NO uyfL 5.0 0.30 1 1470W1217,32 plr50.l 1,4-13 ewwobanxan. NO u9fL t.0 0.33 1 1"011217,32 IW46.7 ImwIA-DichWre-2bulene NO u0(L 100 1.0 1 "low 1217:32 I10.57-a 1,1-0khlw.ebune NO vGOL 5.0 0.32 1 11103112 1712 76-343 1.2.01pllly rh4ne NO uOrL 1 0 0.12 1 1$=1217:32 107�06.2 11-01'NOF ethene NO v0R 5.0 0.56 1 11+0311217'12 153" da-1,2-Dawroamene NO ugVL 5.0 0.11, 1 1110311217:32 156.59.2 ua {-1,2-GllnreeAene NO uWIL 5.0 0.49 1 111031121712 1564WO 12.010h,0r0prapane NO uWL 1 0 027 1 II1=I21TM MV-5 1,3-0WA. r.pr.pane NO -WL 1.9 0.2a 1 1fA331121732 142.2&9 de-1,3.O0,loroprow. NO vprL la 0.Q I "low 12 17:32 1005$41.5 D.I. 1110wzD120326 pM REPORT OF LABORATORY ANALYStS P*O-6 of0 rm;.-it N.I ratM ...Mr. U. H.O.w1h. y,.rl1{n wnwnl0 Pw. A7ulyeeel S.ma., ire Pam An.l ytlul 11-kes,Iee. Pace Anailytical 6Hrlcee, Ina. Pam An.tye.ar 3.rvlm r,.... � 5 Earl M..&. Read - 5.A 2M Fr- N D. V0, [irr:.x R'r. SMW ,0D Ed.n W 272" A.n.W.. LIC 25" M.nbr11 NC 2907a LW234wl tMM7-4•r17e 170e1a7&Ppv2 ANALYTICAL RESULTS Project: WRRY CLOS FQ-MT. AIRY (UIC) Pace pr*CI No.: 92136779 Sample: MVM Lob 4D: 92136376001 Collecled: 1W2W 12 17 D0 Recelvad; IMOT 2 M 35 Mrelr. waler Rep" Pemnittam Rewlte units LInr1 MDL OF Prepared Ane7yzed CAB No. Qual 8200 M8V Low Level Lmndfr4 Anmlyncal Meth. d- EPA a760 hens-1,3-pl.filnrdpropene NO ug1L 1.0 Edrydb.u.nr NO uyL 1.0 2•1-Inanone ND up+L 50.0 Pdvmethmne NO UWL 10,0 mothyl.rl. ChrWIdd ND u0R 1.0 4•Mell,04-penlonmia (MPSK) NO'WL 100 Styrene ND .pfL 1-0 1,1, 1.2-Teuachlemazme ND LO+L 5.0 I,1.2, 2-TalmhLomwhapm NO uy+L 3.D Teuachloroetllen. ND uc1L 1.0 Tot.++ane ND ug+L I➢ I,1, 1• Tnciiiwoell.ane ND 4WL I�0 1,1,2-Trm4Aor,mthene ND ugfL 1.0 Tr]ddoro l ..a NO uwt. 1.0 TrionlWoNi.fdrndlhkn. NO IIIWL 10 1,2,3-inrjllara9rmpene ND 1+yt 1.11 Vinyl ecelele ND up4 50.0 V" chloride NO Ulan- 1.0 xyPene [TwaP ND ugx 5.0 sur7npafa4 4 RI0M09u0ra1ben lone l9] 96 % 70.130 pibromveuwomerher.a iB1 100 % 70-730 1,2-grclumoelmane-dl{6) 109 14 70-130 Toluene-d6 15j 100 % TO-130 2320E AIk.Ilnny Al1ayllf.Al M.9fod: SM 232013 Alk.Wmy, Toter se C.0O3 24800 UP& 500D 6210EI BOD, 5 day Anmlykel Mahod. SM 52108 90D, 5 day ND ugoL 2000 100-O IC Anion. 26 Day. Ana"ml Method- EPA 300 0 $ultlle 740d up'L ;t. 4 500 Chloride AnsWul hlemod: SM 4500-CFE Chloride 47+10 uplL 1009 6310E TOC Anetylleal Maawd! SM 511 OB Toll Organic C.b.n 3070 up+L ION 026 1 11f03+12 1732 10061.02-5 0.30 1 11103112 17t32 IDD•41.4 0.46 1 1VOSr1217;37 W-7" 0,32 1 1WW121712 74.89-4 0-67 1 1VD311217-12 75.09-I 0-3] 1 111D3112 17:37 1D6-m-1 (126 1 11103112 1702 1 DD-42.5 0.31 1 11l0341211;32 630.20-e 0.40 1 1110311217:12 79.343 0.46 1 11103712 17•.32 127.18-4 0,26 1 111031%2 17152 106411.3 0.48 I "IM217:32 71•s54 0.29 1 111030217:32 7A00.5 0.47 1 110037t217'32 72-M41 0.20 1 111OW1217:32 75,69.4 044 I 11 f0311257:32 96-19-4 D.36 1 11+OU12 T7W T06-Wit 0.67 I 11+03l12 t7'32 75-014 0.6d 1 11MV121732 133D•20.7 1 11 MW1217:32 400.00.4 1 li f03l17 17:32 1668-53.7 1 11103112 17,32 17060-074 1 IT103+1217'32 2037.26.5 IODD I 1110211212'W 2000 1 16r2W1202:00 1012WI220:10 BA 2000 1 I1M A2 21;41i 14806.79-0 ION 1 11+06112 21:12 16667.004 1000 1 1119411202. TO 7440Ja_0 Dal. 11109f2D12 03:76 pm REPORT OF LABORATORY ANALYSIS TRr My n d,N not W r.Prodi.ced. -im in IWI. .ftw Pr wniNn r:.na.et 0 Paw Arµrre[a+ giorviW. I- Page 7 .i 49 Pa.. Arulytl.ar a.Mm., Inc. Pam ArWyMul6.rvr.a� Ina Pee. A,.mlyri S.rvl.aa, Inc. aceArraly[ical• 25E.N WrdvwAaad-SYMA 2725Anw.d.0, 0W0I,-VAre S, IOD Ed-. NC 211aa Arnewle, NC 28W 11�nbr.ri. Na 2alll6 133616234M 4626125,,7176 17M 197"m ANALYTICAL RESULTS Project; SURRY CLOSED -MT AIRY SUICI Pea Projec! No.. 92t36379 21-0-. M9y4R Leh ID: 92136379002 Cdtleead. f0+2311706'3$ ReceWed VV24+1216.15 Metrn Mir, Roden Per.melers R... I. vntti Llmm MOL OF Prepared Anaryz.d CAS No. ❑vat "I0 PCP Gmundwaler A4)mlyl,c91 Melhod! EPAOOtO Prep or melon Method: EPA 3010 Antimony NO uuJL 6.0 5.0 1 10MP5 216:55 Icc t11719-35 7440-36.Q Amenic NO up4 100 5.10 1 1ef25112 I6:55 1p135p21975 7440342 aarwm NO uyL 100 50 1 1W511216;56 1613111719:15 7440.39.3 Beryrllum NO .9.1 1.0 T O 1 Icf251121N55 IMU12 19.35 74e6-41.7 Cadrraum NO uA III 1.A 1 f07j5+1216.16 1014"1I 19:]$ 74a D-43-9 Chromium NONugli- III 5-0 1 1W61T21635 1WD1121935 744(W-3 Cobaft ND up+L 10.0 5.4 1 1012Wt216;55 10f3V12 19-35 744D46-4 Copper NO VOL 191 5.0 1 1072NO218:55 10+Stry21935 744"01 Lead ND u¢L 10.0 5.0 1 10V26712IS; 55 19031l12 19.35 7430.92.1 Nickel NO.O4 500 5.0 1 1WN12 Ia.$5 10A1+12 t9y5 7440.02-0 3elenlum ND uGeL 10.0 100 T 10)2WI218:55 10131+12 7635 7762-49.2 Silrel NO up+L 10.0 1.0 7 70f25f121a:5: 10+111721935 744V14 T"Llium ND uWL 5.5 5.4 1 tW250 216:1 111/31/12 19�35 741.4 V.nhd.+ ND uS?L 26.0 5.0 1 10Y2Sf1276:56 1On",21p:s5 7440-62-2 Zinc ND u9+L 10.0 T9.0 1 IW251121a:55 1013711219:75 7440d6-0 6260 MSV Low Level LmmMP Analylkal iri EPA MO Acclone NO uO+L IDo to.0 1 I1M311217-50 U-34.1 Ac y cOrde NO uVL 200 1.9 1 11+03l12 1710 107.13-I Benzene NO LdL t 0 1125 1 11 MU1217-50 71-43-2 BromaeWmamethane NO uVL 3.0 I. Ir 1 11103ry217-50 74.97.5 Brom 6dma,ometlmne NO up1L t.0 0.18 1 11 MU1217-30 75-27.4 9rOroVl.rm ND ug+L 3.0 02a 1 IIMZ01217.50 75-21&-2 9rvm.medlene NO VWL 10.0 0.29 I 11 AV 1217:50 74-1341 2-8urmna-{MEKj NO uprL 100 096 1 11 M3+121750 75-93-3 Caton Oiwl Ode ND uyL 100 1 1 1NO3ry217.50 75•IS-0 C4rten lerecMarlde NO ug& 10 02 .25 1 IV03f7217:50 56M-5 C♦tl.rp6mnxene ND uA 310 023 1 1IM301217:50 101.90-7 Chl.roerhene NO upR 100 0-54 I 11f03+12 17�60 75-OD-3 ChWrolorm NO uyl 5-0 0-14 1 1V03112 17.30 a7.6o-7 Chlorometh4ne ND uyL fA 0-11 f 1u631121rso- 74.87-3 I2-Qhr.m.-3-CIII-Propmn0 ND u9iL 11-0 7IA I 11l0311217:50 98-12-6 Dibt ln.chl.fom.%dn* L40 u61 3-0 0.21 1 11103f1217:60 124d -1 I,I-Oarom.eth.,e IED81 ND uWL 1 D 027 1 111111 $217'SO 106.93J D irrit"methm-m ND ug& 10.0 D.21 1 11M"2 17 50 74.95-3 12-DlchlProben2ene NO up+L 5.0 0.30 1 I1l031121'7:50 95-50-1 1,4•DicMorvbenaena ND up+L 1.0 0.33 1 11103it217:50 M-48.7 liana-1,l-pichWro-7-4ul.ne NO uipt 100 1.0 1 1u03n217:4S0 110-67-5 P,T•DlCNorollDtena ND ujVL S.0 0.37 1 I1 MUJI1 17:5: 76.34.3 1,2.0Ic lwmlhene NO LVL 1.0 0.12 } i1'O3W1217.60 107.05.2 M-01cNmmelhene NO u0+1 5.0 0.5a 1 11 1031121730 75-15-4 V40-1,2-DirhParae0lene NO u01L 50 0.19 f 11MU1217750 INAPIP.2 Paly-1,2-dchloroetrene ND uWL 5.0 0,49 1 malf,21740 166.003 1$OlcMoroprepana ND uy L0 027 1 1 M3112 1710 76.67.5 1,3i]IcMarvpropane ND uWL 1.0 026 1 1TN3112 17150 142-!-9 cia-1,10ichint propene ND upR 1.0 0.13 1 MOW 121730 tan 01.5 Otte: ItlO9120T2 Q32s PM REPORT OF LABORATORY ANALYSIS page of 49 ♦ a,rport NaY nerd tiu�nd,.cn..ycepr n fwl .ne.oa1 the .r,iatn w,,..M P1 Pay:. A-11h[ar S41- i•e P 0 Anyy0Ael 9eMeW I-- Pie. A"y9ur g.rvlwf, Me. PA" AnA1=1 m.mic.., Inc �3/7gy1pp �■� /L��� /.'� PLG"'^J'�' i06 E..l M..dew Rew-6.W.A l2NSRw.r---Or 911001i�rc.y Ai• Svt. IM • .1n. iewlr y. Ed NG 212ea Afn.r.l. NL 7m9M .nriwow. NC M75 ]39pm m2c NMI 254-7176 f704)07 5 9", ANALYTICAL RESULTS pfbl4et: SORRY CLGBEO•MT-AI RY PCj PaEa pl*Ct Na-. 42136379 SNnpia; MW3R Lab 10: 12136376002 Collactad. IW2311208: 35 Re Ivvd: IDQ4r1216.35 Moira. ftler +lewd paAmetefe Rewlte unlis LJmK MOL OF Mepred Analyzed CAB No OIu1 9260 MSV Law Lewi La4ldfdl Anal 6r 1 08e11-dEPA 6280 &Arra-1.3-OkillaWOM 40l NO 4q+L 10 026 I ltm311217:50 10001-024 Elhylben¢ene NO uyL 1,0 0.35 1 1VO112 17:50 100-41-4 2-me-Hoot NO uyL 50,0 046 1 1f10p11217:50 591-78-6 lodunimaiene NO uyL 10-0 0.22 1 1VOW 1217:50 74-W4 m mylens Cnlonde NO uyL 1.0 0,97 1 limn217:50 7S-094 4-4-0, 4-P-4inone (MIRK) NO uyL 100 1.13 1 IVIXI 12 17;50 10 -10.1 Blyrane NO uprL 10 0.26 1 IV031t21?'So 10042.5 1,1.1 9•TfuAcnloroemane NO uyL 5.0 0.2s 1 1110]112 II" e30-20-6 1,1,2-]-7ev ednmuelnane NO uglL 3.0 9.49 1 fuo2lsx 17:5a 7934.5 Te".1wellhene NO uyL 1 0 CIAO 1 1V03A2 t750 IV-10-4 Toluene NO uyL 1.0 026 1 1V03112 17;50 10140.3 1,1.1. Trlchimosthene NO uyL 1-0 044 1 1VOW1217;50 71-55A 1,i,2• Tricnlmoff6we NO OWL 1.0 029 S 1110311Y f7:S0 79-00-5 TrkhlwvHhme NO uyL 1,0 OA7 1 IN03112115" 79.014 TrkhlWolluvrdm.INrM+e NO P92 1,0 0-20 1 1111.1217:50 7'.F60.4 1,2.3- iflcltraroprepen. NO.0rL 10 CAI 1 11102A21730 WI" V5ty1 a0mlald NO MCA. 60.0 0.35 1 11103712 1?r3o 106-05-4 Vinyl chloride No uyL 1.0 0152 1 11103/12 17;50 7 -01.4 Kylene IT01.1) NO uyL 5.0 066 t tI owl 217:50 133040-7 Surrogelea 4.9rom llumb""ne IS) 97 % 70-110 1 11 fowl 217:J0 460-00.4 Dit-mo8udmhmThana [S) t22 % m 30 1 11 ION121710 1"1653.7 ii-0Ichlor0alhane-d415I SOt % 70.13p 1 S1m11121740 17050-07-0 Toluene-J6IS) 99 % 7LF130 1 1110311217: 50 2037.26-5 23 Z0R AMmifinify Analytwal Mehod SM 2120B AlmOtty, Toth as CaCOS 10400p uyL 5000 400 1 1IM2112 12:0 6210E EGO, S day Analyllcal M41hod. SM 5210E BOD. S,Iay NO uyL 200o 2000 1 IWAM20200 1LV291122010 94 300.0 IG AM- 28 D.y. APa1ylml Melnod' EPA 3W 0 $yl We 6660J uyL 250000 2000 1 11101/12 22R9 14805-79-0 4504 Cldorlde AnmWxml Me71o4 SM 4500-C1-C Chlorlde 2110 uyL 1000 I000 1 11106If221;12 16287.00-6 63106 70C MaWncal Method. SM 53109 Tuwl Organic Carbon 2410 uyL 1p00 Ii700 1 MW120224 744044-0 0.1.: 1110W20I2 03:29 PAN REPORT OF LABORATORY ANALYSIS �.o.�„i e•..r n,�^•,>^.. i c r w_.,..:tr ..r: se ..re. • . Pepe 9 of 49 PA n. A � ydW 6AMq.,Mc P.- An.17I1W S.rrIg4, Inc P.w Anfiyawla.rWwf, le¢ �CG /'111� � I• ]06 EA.I M..tlnw a.. - 6vr. • �"25 Rr.ni.d. h• 9R%1 v-w.v an 5r.w tgg e.w i.r.tru me Cd.n ryC 77;58 A.n.yn. ryC 7een4 i�wrrw•If Irk 7+r1]e 137 IM-11971 157111754.7170 i7 W M7 S2R e ANALYTICAL. RESULTS ProleCL SORRY CLOSED -PAT AIRY (l1lrl Pale Pro)ecl No. 92 M370 5wple: VW41 ub In: 112136379003 Cone tied. 1W w 1210.45 Reeelred: 10*4012 M:15 mean bihter R+rp t Peremele.e R.auINC LWIN umll MOL OF Prepared Anll"Ild CAS No. OuN solo iCP Groundwater Anal ual Method EPA 4010 PrepW WNkn Melhvd: EPA 30W "mvny NO uyL 6.0 5.0 1 1W502Ia 55 f07311f219.35 7440-W-0 Armerdc NO uwt spa 5.4 t IDIZ51TI T6:55 %=1112 19.30 7440-3&Z I3.m_ 41.3J uyL f00 50 1 102Wf2 W55 1N31021438 741G393 geryll.rm NO uyL 1.0 1.0 1 1W261T216S5 1W31021038 744041.7 Cadmium NO uVL t a 1 0 1 1DQUII 1155 1W3VIZ 19-38 744043-9 ehm-. NO uyL 100 5.0 1 1025M215:55 1N3111210:3S 744047.3 Cohmh 24T OWL 10.9 5.0 1 1W2511210:55 IW II1219:39 ?"044-4 Ceppm NO uyL 100 5.0 1 1111251121 SAS IW3111219:35 7440-50-8 Lana 5,1J uyL ICA 5.0 1 1W241121 SAS 103111210:30 700.92.1 Nickel "'INJ PyL 50.0 5.0 1 1046H210:55 IW3 T1121018 744042-0 Selenium NO uyL 10.0 10.0 1 IDOW1210.55 1W311I219:36 776249.2 &No? NO uyL 10-0 5-0 1 10f2WI2 18-55 1W3 t112110.36 7440-224 ThNYum NO up4 5.5 5.4 1 10/25112 16;55 1p13t11219.36 74ap-IS-0 Vrnedium NO OWL 25.0 5.0 1 t025112 i6.55 10131/12 19.38 7440452 2 I4nc 12.9 uyL 10..0 10.0 1 IWSIQ 16.55 }N1111210.38 7440-6" 8260 M5V Low Laeel Landfill Analyhral McNoe. EPA 8260 .acetone NO uyL 100 10.0 1 41m3y12 ?4'" W-M.1 Aceronrrme NO OWL 55.4 22 I 11101712 18A9 MCI" Acl Weln NO uWl 53.9 1-6 1 lu wl214:09 f07-0" AcryldnHnle 10 uyL 200 19 I 1S103t12 f8:09 f07.13- 1 Allyl cNonw NO uyL 10.0 1.5 1 1TIOU12 t6:09 107.05-1 genrene la OWL 1.0 025 1 1110311218'00 71.43-2 &omnthlaomemane NO OWL 3.0 0.17 1 111OW12 $91.09 7+97.5 &vmodlddvromethane NO vWl. 1.0 0,7a 1 1VCV I216.09 75214 Wmm�lmrm NO uyL 3.0 0.2E 1 1110311216:09 751-25-2 Bromometn"a NO uyL 1CA 029 1 %ImU1210.09 74-63-9 2-Rul.nvne )MEN) NO uOiL 100 0.96 1 1 T43112 16:09 76.93.3 Carbon dlwltde ND uyL t00 12 7 f7mw 216.09 75-15-0 on CarbWrachtold4 NO YO.R. T.0 0.25 1 11 foul 21aE9 56-23.5 CnlorebW2erle 6JI uyL 3.0 0.23 I I WOV12 16:09 105.90.7 Clilor.0thme NO uyL 100 17.54 1 11 mUlz 10.09 75-03.3 Chl4rale" NO uyL 5.0 014 1 $1 M301216:09 67-W-3 Chlolemelhane NO uyL $.a CAI t $I IQW1216'09 74-67.3 CNoroprenm NO uyL 20.0 027 1 i$ WJ1216i79 126-99411 1,2-AiWomo•SGJoraptvpana NO OWL 13.0 2.5 1 111031121699 96,12-6 ph1affkGhhrPmeth.ne No uyL 3.0 121 1 111'OW121649 124411A 1,2.011mmmaelnene IEbHy NO OWL 1-0 927 f .13W12 16.09 106.93-4 Olbromome0lmne NO uyL 10 p a 21 1 11103/12 16fl9 74J95-3 7,2-okhlarvhen2erK ZAJ uyL 50 0A$ 1 I low, 21 a 09 95.5W1 1,30i; loreb-Aene 0]9J uyL 50 024 1 11003112$ll 09 541 73-1 lA-Oki, oben2ene 20.1 uyL 10 033 1 11IW71216:09 19646.7 iranm•1-4-0lWerg•2-bulene No uyL 100 1,0 1 1NIO1121 -0: 1f0-074 D1ChldrodiAuoromelnane kD uyL 6.0 0121 1 11m3H21a-0751714 1,1-Olchltlraelh.ne 4-1J upn. 5 p 0.32 1 114W1216U9 75-34.3 12-Dlehloruemene 2.1 uyL 1 0 0.12 + t1103J12 t609 10706.2 {Tale 11MI2612 03:20 PM REPORT OF LABORATORY ANALYSIS Pape 10 ON 40 ,*Nrt fnex rrel a ,*Mdu d .[wyl of l wnnvN"iM .0'.....1 P-0 A Inr 3Wm Ire • pace Arwyaul aeryleca, IAC- Paaa AmlMoel Sark e, ln . p �„ n� r .• ace �l7�C1! u15 DeZNC eM„� H2M,uM..wRad-SmA EdN.?729e AhaWr 13361633d921 1a2a1254.7175 ANALYTICAL RESULTS proled: SORRY CLOSEOMT. AIRY (UIC) Pica pM)e% Na. 92IM379 Pen Analytical cervical, rne- 9eoo R,r�.yAY. sur. +od 1W�1etw�4. NC 2DD7A I704075.9092 Sample: MW-14 Lab ID; 92531IM003 Collacled: A07237121045 RacHva0: IW12.$635 MANN vWtar R.PQA Parulretan Rawl% Unlls L1rml MOL OF Praparad Aneiysed CAS No. Oual a280 MSY Low Level, Landfill Anaivhcel Mamod. EPA 6260 1,1-0rchklfaemene NO ugrL 50 054 1 1110311216.09 75.35.4 da-7,2-DkYdnroeNene 41.1NgIL 50 0.19 1 1170N1216V10 55659-2 gam-1,2•Dlchloroe0len. 0.611 Ugfi 5.0 040 1 111o3N2 19.01) 55fi-60-5 1.2-WcHoraprvp.ne 5-1 uyL 1.0 027 1 11IOU1216:09 78•117.5 1,3•DlcNuopapena ND ugfL 1.9 0-2a 1 11MV1216A9 t42.2A-9 2R•OdcYrlugNapane NO Vly 15.0 0-13 1 117ASI12 16:09 594-20.7 1.1•pChIG1opr0pene NO LVL 6,0 0-49 1 11 f0111218:09 963-58-0 da-1,3 pltl lamp open. NO uWL 1-0 0-13 1 1IIOU12 16:09 f0051.01.5 OM7a•!,3•DIGhIOfAplvpena NO LWL 1.4 41" 1 T1703A 218:09 $00151-02-9 E0glban2arle NO VL 1-0 0-30 1 1110311216'fl9 10041.4 E"t malhaeF&IO NO u0rL 10-0 020 1 11MU1216:09 e7.61.2 Naxacnlarwl,3.dlladane NO ugrL 10.0 0-71 1 11f031lz W09 67.66.3 24-leranone NO uyL 50.0 046 1 11 f0311z T9.01) 591-76-e lodanremane NO VL 10-0 0-32 1 11/03112 75:09 74-1164 I.amtenor NO ugfL 10D 35.0 1 11003172 t6'00 76•as11 Methomyrenlmle NO ugL 100 0.93 1 11f031125699 126-9e-7 Me#rOene Chroflda NO ug4 1.9 OM 1 11/03112 T6:09 75-0 -2 Mamyt molhor yf.l. NO ugrL 30.0 2.0 1 1IM3112 is % SO.624 4-Metrryl-2-panunone IMIBKI NO uWL Ion 033 1 1V03112 ISO 109.10.1 Naphiholena NO ug& 1130 024 1 11 M311216.-09 Yl•20-3 Proplmdnle NO uglL 150 1.6 1 11MU12 T6:09 IW-17.0 Sryrena NO uWL 14 0.26 t IIOOW12 MlWi 100425 1.1.1,2-T.Ln.arlvava61ene NO09fL 5.0 0.31 1 111071219:09 630.20•6 1,1,2.,2-T.bacnlnrpeOlene NO u-WL 3.0 0.40 1 1IM3112 Moo 79-34.5 Teaschlot-tham NO UWL 1.0 0.46 1 11 MU12 IS:09 127.14.4 Toluene NO uWL 1.0 0.26 1 11 f6311i 11149 foe-04-7 1.2.4-7drlrlorphertiena 0.73J ug1L 10.0 0.35 1 11103712 19.09 120.12.1 1,1,14,1chloroothana NO dgiL I a 0.46 1 IIMV12 16:09 71-55$ 1.1.2-W-hlorvelho" ND ugY 1.0 0-29 1 11 M3112 Ia:09 7940-s Trlchioroadrene 13 ug+L TA 047 I 111037121a99 M01.6 Trlch1w06u01 n melhan a NO UPI 1.0 0)0 1 111031121a 49 76•S24 1 ra,3-Tdchloroprvvene ND.0& 10 041 1 11f03112 IS fl9 96•}a-4 Vinyl acetele NO uWL 50.0 0-35 1 11003/12 18:0il IO -05-4 V4yl chloride 6.7 ug . 1-0 0.82 1 111OM2 1a:09 7!,014 Xylem fTvle11 NO tjA 5.0 0,a6 1 11 f0311214109 I330-20-7 8urrngaree, 4-8r OmpAuorouanaene(S) 9B % 7D-13D 1 IJODW121699 46DA0.4 Dlbromolluorvmelhene (S) 103 % W130 1 11f63f12 1698 llwa-53.7 1,2-Dichlvroe7hanr-M ISI 105 % 70-130 1 111030121111M 17060-07-0 Yvluene�78{5) 100 % 70-110 1 111D3M2 18�09 2037.26.5 23208 Alkelimly Anehmcal µalhod: SM 21208 Alkellnlly, Tolel so CaCO3 14N000 ygfL 5000 IWO t 11@2f 12 1210 92108 BOD, 6 day Analyilcel Method: SM 52108 800,5day NO u0A 2000 2000 1 10,251t202:00 10CWI220!10 B2, Ba Pete IVM(112 D.T 26 pM REPORT OF LABORATORY ANALYSIS Page II of 40 I r.e report Nax rat ka mpmeueae, erupt A kw. M eioul the ynlrrn conMn101 P.c. "lyecal S mvv. rn< • Pan Anal0"I aarrlcas, Ins. Psw Analytical Se Icvm, Ins Paca Analyllesl S-l".. Inc. aceAraalytrcal 2 �'1 Meamy Rued • guiyA 222s Rk..esle D+ da06 k- " $ W 1 W Ea-. NC 272ee AY dlt. NC 2aW4 NNrq.rwae NG 2e016 (23e)m6101 jflA 5a.7116 r7'J11$]}pce7 ANALYTICAL RESULTS Proyecl SORRY CLOSE D-IAT AIRY MCI Pace Projacl Na. 92136379 Sample: MW-16 LaIM: 92134579003 Collecled 1023P21045 Recelved, IORi1121615 k1e61r.Vloler Repod Parameters R-WIls Urrla Llmd MDL OF Prepared "Lyted CAS No. Oust 300.0IC An"- 2a 0eye AmIlV%-1 Method: EPA NO 0 Sultile NO ugrL Mono 2000 1 1110202 12:0 1406.79.6 4500 Chlonde A1ulymcal Method. SM 4500-0-E Chlonde 433" Ng'L 1000 1000 r 51106fi221:17 766a7-9Q-0 53108 TOC Anelybcal Method: SM 53108 Total Orginlc Carbon IBM ugrL 10D6 IOQO I 1T7040120236 7440.44-0 Oate. I IIOS 20T2 014$ PM REPORT OF LARORATORY ANALYSIS TRa report ellell not no r. -ed. -eo1 n tuli, -".. 0- Mnrtyn -.1 W Peca A-1vi , S.rvk... Inc Page 12 ni 45 Paar Rrufygeal earvlaas, Ine. P.- Amlynval oar 1-. Ine Para Aealyara! aafaltal, rrw. . Z&Wpical' a eau w.m.. ana3-sewn _m r<.. ."., 0800 � ,A.. s,.*,m .wowwr me Esrn, "c 77206 A---- f;G 26604 H-%r..,ra NC 20075 rl]a16230"1 r57B17s -7178 i7p. A7!1-am ANALYTICAL RESULTS Prpleal: SORRY CLOSEO MT. AIRY ILIICI Pete Pm$ed No. 92138379 Bample: MIN•133 La1710: 92139079004 CRllecsed. 10f2411215.00 Recolved 10475N214:20 Menlr: Wales Repan Pmfhmetam fiewall. unit. omit MOIL OF pfepetad Amlhftad CAS Ng Quml 6010ICP 0mundwuah An ytical Me mod: EPA 6010 Preparatm Mamod: EPA 3010 AnWrMmy NO uyL 60 6.D 1 1012611218:511 1W3111218.04 7440.3l-0 Araaruc NO.OpL 100 51) 1 102N1216-58 11101121670 744033Q Ilarlum 20-6J uyL tw 5.0 } 1WWI218;50 101301216;D4 744439.3 BeryMam NO nyL 1 0 Lo 1 10r2611218:i0 IDe3111218:04 7440i1.7 Cednnum NO uyL }.0 1 0 1 16R611218:13 1Or3571218W 744043-9 C hromwm NO ..A 10.0 5.0 1 10r261121850 1013111218'04 7440.47-] Cabaat 1e-6 uyL 10.0 6.0 1 1OR811218:50 10laV1218:04 7440J5i Copper N13 uyL 10.0 5.0 1 1012WI216:50 1IN3111218:04 7440-5" Ltma NO u0'L 11.1 1.1 1 10 111218:50 103 111218'04 7439.92.1 hYcaal 6.2J uyL 50.0 0.0 1 101261121850 101311121804 744042-0 Sol.... ND u1?1 10.0 hnD 1 10rzen21l'50 1Of31112112-04 770"ll-2 saver NO vWL 10.0 5.0 1 1CVZWi216: 50 1013iM2 1004 7440.22.4 7b,0urn NO uyL 5.5 5.4 1 1LV2N1210:50 105411216:04 7440.2a-0 w,lndlum NO uyL 25 0 5.0 1 1WWI 2 48SO 10121112 18:04 7440-52.2 ilne IaA uyL 10.0 10.0 1 161461121610 1On$01218.04 7440-M-6 62SO MSV Low Live LandflH Analvi"? Mafhod- EPA 8260 A-1w. ND ug1L SDa Taa 1 1110311211127 674M-1 Aclylonrirlle NO uyL 200 1 9 1 11)03112 1877 107.13.1 Benzene NO uyL 1 0 025 } 1110N121427 7$-43.2 9r0moch1or6m4Napa NO uyL 3-0 0.17 1 1WWI 21a 17 14-91.5 Brumodlchloremathdho NO uyL IA 0.16 t 11103f121827 75-27-4 Bfomelplm NO uyL 3.0 026 1 11103f12 1827 75.25.2 arpmpmarhene NO uyL 10 n 029 1 111D3112 1827 74,$3-9 2-13wl anme (MEN) NO uyL 109 0.26 t 11101f12 11127 M93-3 Cmrann dNulldd NO uyL ion 12 1 111031121827 7545.o Cm-bm Iek.pdw ldo NO uyL 1.D 025 1 11103f12 18.27 5&-n-5 Chlomb-2-11 NO uyL 3.0 023 1 WO142 1827 108-90-7 Ohlcroethmne NO uyL 10.9 054 1 111030121327 75.00.3 Chlotobfm ND uyL 5.0 0.14 f 11103fT2 la.27 67-55,2 Chlocamelhoma NO uyL 1 n VI 1 11103A21527 74-87.3 12-EHI p-3-.h1-prppane NO uyL 13 D 25 1 I1003n2 1527 95-12-0 OibramarAfmomeEhane NO uyL 10 021 1 11WA21927 124-4&1 1,2.0-b omoelhene[E081 NO uyL 1 D 0.27 1 11103AZ 1121 10e-93-4 OH7romome0lmna NO uyL 10-D 0.21 1 111037T2 T621 14-95-3 1,2.OUNotabenzene NO uyL 1.0 C." 1 IVOUT2 Ia27 95.50.1 1 ,4.Okhivrnoanzane NO uyL 1.0 0.31 1 1110302 }6:27 IC646.7 trans-1,4.D1nh10rp-2-h41e na NO uyL tan 1.0 1 11003/12 1527 110-5741 1,}-Dlcfaoroeu.ane 024J uyL 5.0 1132 1 110031121127 75-34-3 1,2•Dlchluoeloaee NO uyL 1 0 012 1 IV03112 1927 107.M2 I,}•DlcNoroethene NO uyL S.D 056 1 11MV121927 75.35.4 CAI-1,2-OmhlDroefhene 1.1J upL S-0 010 t 71fONf21921 155.59.2 trans-1,2-NOMrmemana NO uyL 5.D 040 f 1110LT216:27 1W 604 1 ,2alcNuePrpp.ne NO uyL 1 a 027 h 1110302 1827 78-47-5 1,3-OkMoroprapene ND UWL 1.1) 025 1 110031%2 1627 142-25-9 da-1,3.O.rntorppropena NO uyL 1.0 013 1 I11OA2 I627 IDoe 1.01-5 Dow: IU09r205201:26 PM REPORT OF LABORATORY ANALYSIS Papa 13 01 49 wle l au vmn.n eama.mt er Y.ee Amloml Sm-os, Inc P.ea Aetlylle415ary.en, Pon ;CA Vol. A"YOQI>t.ral.lt. Inc. Paes "0var4l mamaat. lar- aceh7al+yftal' 70a Eaa MPPOw Rv W-LLAMA 2725 gy..asM seo0n x.r A.e Sw 1p0 nw...xrr..a mm Edam. Nc 272ee Aa.hoM o. NC 15004 numw�wxa. NC 28070 Ima)8n,a921 Ia2ap7 7t78 t70416*54XQ2 ANALYTICAL RESULTS Project SORRY CLO8ED•MT. AIRY pc Pace Projed Nu.. 92136370 Se Pla= MW-123 LaL10: 1121363791104 Colleeled: 102411215:00 IRacelved 10251121420 Manly Water Reporl P.rmmetere Romho Untie Llmn MOIL OF prepared Analyzed CAS No. Dual 8260 MSV Low Love Lrnolml Analyeeal MMoo: E¢A 8260 Irarta•1,3.01chrofaprupana NO LWL T.0 0.26 1 1170yryx 1027 10"1•D24 E"tE z nm NO �UIL 10 0.10 1 11MW121d27 100-414 2-HeyanoM NO uyL 500 0." 1 114031121:27 591-7a5 ladome0lane NO uyL tn.c 032 I 11 f03112127 74.18-4 Me"". Clllcride NO uyL 1.0 0.97 1 17 W121:27 75-09.2 4-McVryl4-pe.tsmme{MIBIQ ND uWL SOD 0.. 1 11My12127 106.10.1 6lyrene NO uyL 1.9 a.21 } ItMW1214.27 100-42.5 1,1, 1.2•T.kr.cf k .eM-. NO u9rL 50 033 1 1110WQ la27 03D•204 1.1,x,2.70.6iLhk u6414 M NO uyL AD 0.40 1 111DJ1121027 79.34.D T.Machtoroelnena No vyL 1.0 0." 1 11m211121"? 127.164 Teluena NO uyL To 03! 1 11l03112 1027 106.86.3 t 1,1 •Tntlllottrmtrmne NO ayL ) a 0-49 1 11113L121827 71-05-0 T.I,Z-Trlchlno mdhmne ND uyL to 0.20 t 11M112182? 711-00-5 TfIchl0foelnana NO dyL 1.0 0.47, 1 111D3ry21112? 7941-6 Trrchlmaauammimmne NO uyL T-0 0-10 1 1tlb311216.27 75.69-4 $2,3-Tr1eh1arppmpmne NO uyL 1.0 0.41 1 1T1011121827 96-184 V.0 ace tale NO uyL 50 n D.15 1 111D3112 1527 186A6-4 Vto 01-de NO u91L 10 0.82 1 11=121027 75,01.4 %ylene (Tortl) NO uyL 5n 0.66 1 fu03012 la27 11130•20-7 Sunnparn 4-Br0mo4uorohentene(6) 9B % 70.139 t 111ON21427 45D•001-4 Ohf oma9ud umelnone(S) 101 % 70-130 1 111031121427 1""" 12.Oknlaurhane•d4 {S1 ICA % 70.110 1 111DWI2 Is 27 17080-07-0 Toluene -dB I5) Ion % 70-130 1 11OD30121827 2037,21.6 232M AlkalMay Anmhri m Momad. SM 2120B AAahnlly, lolol me CaCO3 772M uyL 5000 1000 1 11102/12 10:41 S2108 BDD, 3 day A..hllfcel MethodSM 32108 BOO 5 any NO uyL 2100 2000 1 10281120045 10=1211:10 82, B4 3DO-0 IC Anions. Za days Anmlylkel Method: r$W 3Dn-D SLO414 36000.1 uyL 25DDOD 2000 t 11102FI20207 14608.79.E 450D Chl.nda AneN7 I Metmal Sal 4500-C -E Chlondm 12H uyL 1000 loaf] 1 111D6r12111:37 11567-01145 83108 TOC Anotytkml Malhod SM 53108 Wei Organ.0 Cal tWn 436D uyL 1aD0 loon t 1100711,10055 7440-44-0 04ty 111a9r2012 03 26 pM REPORT OF LASORATO RY ANALYSIS Page 14 p149 Try. open an" opt be ropi -oat..-Pt. "I. W SWln aha Wfllbn Oryl W Or PaCa ANHryecal W.Ywaa. Inc ' Pa Ar yL[.r 6mMN .Im. pave Amiyucor Servlul, Inc. Poe- A-149cal 9mP11.es, Im. p ,.� f f ace iV k Iylar 205 E..t IM.a RcW - 6.n.w 2M3 Rxo va. 0, oeD6. o, A,. R.I. I .. .w rd eu u n Etlen W 2723e M1 ...rdi.. NC 78e04 H­%r .I. NC 25a29 133610234p7, 46161754-7176 17D416754067 ANALYTICAL RESULTS Propel SUR1iY CLOSED -MT. AIRY (LAC) Pace PmMct N0: 92136379 Sample: MYW120 Lab 10t 92134379005 Calloeted; IW2111214:30 Recawed• IOaSr 4214: 20 Matrn.'Am lar Rapon PNmmelvo gmrm Ueda Urref MDL OF Prepared Analyzed CAS No. Qnel SDI ICP 13-dwd.r AnW-csl Method. EPA6010 Preparation Method EPA1010 AndR nY NO DyL 6.0 5.0 1 1Of25112 Ia:60 1W31112 TSW 7440-39-0 Ameme NO uyL too 5.0 1 10126121a:50 111011121613 74AD-36-2 8a,iwn, 6AJ uyL I00 $.0 1 l(V26112 18:50 10)311T2 1827 7440-39-3 Baryllum NO uyL 1.0 1.0 1 1012WI2 1650 IMM12 Ta.07 744041.7 Codmlum NO uyL 1.0 1.0 1 10126112 16;5D =M2 W07 740-43.9 Chrommm ND uyL 10.0 5A 1 1Of25112 19:50 ID13VIZ 16;07 744D47.3 C94eh NO UVIL 10.0 5.0 1 10126112 16:50 IW3111216;07 7440-40-4 Copper NO uyL 10.0 6.0 1 1GY2&1218:50 t0*V1216:07 744M(I-a Lead NO uyL TOO 5.0 T 1OR6112 T8,50 10131 it 21S:07 7439.92.1 Nrck.l NO uglL Soo 5-0 1 10R6f121a;50 t=10211 07 7440-02-0 Serenium NO uyL 10.0 10.0 1 1WW12 IS,S0 1013VIZ 16:07 778249.2 Sllyer NO u01L 10 D 5-0 1 104&17 111:50 1 W31112 19:07 7440-224 Thallium NO uyL 5.5 5.4 1 1O(MI2 IA,SD 1 W311121907 7440.2a•0 VanArAum N13 Dg'L 25.0 50 1 I(WV121&:NO IW3111216:07 744042.2 Z.,c NO uyL 10.0 lO D 1 1OW12 16:60 iN11112 1607 7440-M-6 1260 MSV Low Level LAndRI, Andy[kal Method EPA MD Acelw,e NO uWL 100 10.0 1 11103i 1216:465 6744.1 AcrVMNtrde ND uyL 200 1 9 t 15f)3112 Ia:46 1p7.13.1 Beneena ND ugR 1.0 0.25 1 IVD3112 1a.46 7143.2 &0m9cNor0mamane NO DyL 3.0 D.?7 1 11/03012 IS'45 7497-5 Bre"dMoro-olhana NO.10. 1.0 Dle 1 IlsOV121645 76.27.4 e,9,Po" NO uyL 3.0 0.26 1 11MI12 la;45 75-25.2 Eh.-melhana NO uyL 10.0 029 1 11f031T2 ISAS 7443.9 2-Sulmnona (MEK) NO uyL $90 0.95 1 11103/12 M45 7a-93-3 Carbon IRau16d. NO ua 100 12 1 111031T216,45 73.I&O Carbon tehacmmofs NO uyL 1,0 0.25 1 11 M311219;45 56.23.5 Chtwobehrene NO ugrL 3.0 023 1 11003112 M45 106.90-7 Chl.F"lhen. ND UWL 10.0 0.54 1 1100311215AS. 75-00-3 Ch,9,olmm NO ug1L 5.0 014 1 110031121 a:45 67.66-3 Chlo,omelhene NO dyL 10 0.11 1 111DWI2 16:45 74-a7.3 1,2-DAromo-}chWrOpopmna NO uyL 13.0 2.5 1 11 f0311216:46 W12-8 DibromochIa d h.ne ND uglL 3.0 0.21 1 11 fOWlZ T6,45 1244.0A 12.OL,umaawna 1EDBI ND u9m. 1 D 0.27 1 11/03112 tBAS 108-074 OiWomom m... NO vWL 100 0.21 I TIM311Z W45 74-65-3 l2.OlcMuohen7ena ND VL 5.0 0.30 1 11 M311216A5 95-50-1 t,i DkMnobenlene ND OWL I.9 0.33 1 It fowl 216>45 106J4F7 trade -I A-Dicho,a-2-bulene NO uyL 100 1.0 1 111W112 WAS 110.57.E 1.1•Dlchkwoelharl a NO uyL SA a.32 1 Tf Mill 10-45 mi4-3 1,2-Dkldor9m h .. NO uWL 1.0 0.12 1 11 IOU1216-45 I07.06-2 1,1-DlahWoalhena NO uyL SO 0.56 1 t1f0111216A5 '15-35-4 de-1.2•01CNoroethnne NO ug& 5.0 0.19 1 11103ry2 faAS 156-0-2 trem•1;2-plchloroethene NO uyL 6-D 0.49 1 IiMW1216:45 156-6M 12•Dichl9ropropane NO ug14 1.0 0.27 1 11MV1216,45 76.67.5 1,3•Dichloroptopmn. NO uyL 1.0 D.29 1 IIMW121aAS f42-2" Cti-1,1-OId,IM9propen. NO ugrL 1 D 0.13 1 1IM11213:45 f0061-111-5 0016: 11A)m2o 1202:0 pM REPORT OF LAW RATORY ANALYSIS Page 15014R TN. r.per th.l,wl b.,.pwd-d...copt n ka .In eve wons. -..,I ur Pace An.Iy9_.I Snrx.w ,nc Pau An.iyaks, a.MPn, im P... Anllyaea, aervlcaa, Inc- Pau AnYy9a.19erylpea, lm. aceAr�aJytical' 70a Ea.i Meadow Road &K4A 7175 RH..d. ❑, s6oD K nT Ave 5 6. 1p0 €d.n ryC 27M ASN... NC 2E, Hu WY Ns NC MM (3WWz36971 1A7ai254.117a M541975.9m ANALYTICAL RESULTS Prapm BURRY CLOSED•MT. WRY IUIC) Pace Prooct No.. 92136379 Sample: MW-1ID LablD1 U136379001 C9aecm: IKAF 1214'30 Received 10r25ry71420 Matrix Water param616M p.tuKe Unit. Report Llml MOL OF Prepared A..Iyaad CAS Nn. UL d M0 MSV Low Level Landfill Ana,ytcal M601od: EPA 0260 ganrt,1-pitnlorhpropane ND uyL 1.1) 0.26 1 1110J1215AS W91-02-0 Ethylbentene MD uyL 1.0 0.30 1 11103/121 a'AS IN-414 2•Hekmrinna NO ugii 511.0 046 1 11/0V12 MIS %I-76-S tadomalhene NO vWL 10.0 0.32 1 T1103f1216:45 74.H-4 Methylene Chlo,ida NO ug4 1.0 D.97 1 111031121aA5 7S-D9.2 4.Ma0h4-2-penlan9na(MI BKJ NO uolL 100 D.33 1 ITMW1216A5 IDa-f O-T Styrene NO uyL IV 0.2E 1 IMA2 IRAS 1D0y2-5 1,1,1,2-Te0oct0o, oeth one 40 ugrL 6.0 0.33 1 1T1031121845 630.204 t,12,2•Tedachlw net. one NO ug1L 1.0 0.40 1 11AV12 fa:;5 79-34.5 T.aagll.raethene ND ug1L 1.0 DAIS 1 111D31121 a A6 127-15-4 Toluene NO ug1L 1.0 026 1 1VVWI21a AS Ipa-96.3 1.1,1-Trlchromethene NO uyL 1.0 0.40 7 11103n2 IN 45 71-55•a T,1,2•1`rehleroemanC NO VL IV 029 1 1U0311216:45 79.00.5 Trkhlarcedwne NO uyL to 047 1 11103/121 SAS 79.0t-6 TrichI.F.1u0ome11une ND uyL to OJA I IIM311216:45 754694 12,3•TrlChi9rtyrvpelte NO uyL IA 0.41 1 11003112111:4S 96•la4 Vinyl .c tatc NO uyL S0,0 036 1 tVO117 t6:45 l03-0S4 V-0 cMwlde NO uyL 1.0 0.62 1 IIMWl219.45 75.014 XYiene 1Tdail NO uyL SA 0.86 1 11103r12 10,45 11130-20-7 Sumogaen 4- Bmmolumaba0xene(S) 919 h 70.110 I 11101121946 460-00.4 ❑ibroma6uw0methena(3) 101 % 70.130 1 11 W121SA5 1969.51.7 1 ,i•Dkhbraetltene•d4 (5) 103 % 70,130 1 IVOW1218.45 17060.07-0 ToNena-db(S) 100 % 70-13il I IVD31121aAO 2037-26.5 23200 Alkallnlry Anelytlpel Method: SM MOB Alka6mity, Tole, n CaCO3 67700 uA 5000 1000 1 11102M2 19:67 621n6 806, 6 day Analytical Method. SM 5210B ROD.5 d.v NO ugli- 2000 200D I 1872611200;46 10=0122110 82.04 000.0 IC Anlans 2e Day. Analytical Metmel EPA300.0 $uINt6 7430J uyL 2S000O 2DOD 1 111027120220 14608•793 4500 Chl9 rid. Anldyllaal Meltwd. SM 4500-Ct•E Chlonde 1170 ug1L 1000 1000 1 117061I21939 15a67.00.6 5310EI TOC Analyllcal MsOwd 8M 53106 Tole Organic Carbon 21DO uyL 1000 $000 1 114711201.09 744044-G Data: 111097Z812 03:26 PM REPORT OF LABORATORY ANALYSIS TNa nowt shoo ant he npad„c.d.., eep A full. ynewD Ore Krnrn conemM mi Paw A,uiyncal Sw­s 1rc Pape la of 49 a Pan AnNypprl 6rr.irr., Inu Pep ArWygg1 c 4ervae9.lnr Paw Aminful 18Mve9, Ina. w .05Et VR" 2RNN 1600ryrAnSWNrD7ceAnayical Ed- NC 2778E AW -d*. NC 2WO4 no-r 40. NC 2507a imai,623-692r 1676t2WI76 VW87541)92 ANALYTICAL RESULTS ptopvl: SVRXY CLOSED-M7. AIRY fUICj Peca ProjectNo.. 92136379 sample; MW13 Leh ID: 9217957408E colleoled 1D124 r72 n.u0 Received IWW1214.211 M.klr. VAtar Report P-rnerrrn Re811[5 uwl. 6"1 MOL OF Prepared Anelyaed CAS No Gu.l 50101CP Ornundvnen An"Jeol McThpd EPA6010 ProPMAMM Method: EPA 3010 Antimony NO uyL 5.0 S,0 1 IoR611218.50 1VD70 1220.01 7440.39-0 Areanlc NO uyL 10.0 5.0 1 1007&1218:50 11113711220p1 7440-38-Z B.rmm 411J uyL 700 5.0 1 IWIV1218:50 11007112 20:01 7440.39.3 Oeryawm NO 41 L 1.9 19 7 1p72E112 16:69 n+01117 20:01 7"o-41.7 C.dmum NO uyL 10 1,0 1 10128112218:50 111071T22D.01 744043.9 Chrp 4m NO uyL 100 5.0 1 1012V 2 18 50 11 f07r12 20.01 74"7.3 Coka9 ND uyL 1D.0 SA 1 1624112155D 17;0?1122011 7440•i&4 Capper NO ugh 10.0 SA 1 1012E712 14:5t1 }11077122Da1 74a0.50-6 Lead 1vD ug1L 1D.0 5-D 1 f028r12 i5:5D T110711220 u7 743W 2-1 NRkol NO uyL 5D.0 5.0 1 1WMI2 T6;50 71M711221) aT 7440-02-0 Sol "lum NO uyL 1D.D 10.o 1 II'2817218:50 1110711220,.01 7782-49.2 50ear NO uyL 10.0 SA 1 1026112 t5:513 111071122007 7440-22.4 Thailem NO uyL 51 5.4 1 1612611218;50 1N071122001 N40-28-0 Vanadium NO uyL 25.0 6.0 I low,21650 171571122001 744042-7 Ih,o 1i-4 uyL to(] 10 D I 1049F12 10 SO 11/07112 20.01 7440-56-6 8280 MSV Low Lovet Landfill Analyhval lhelhod: EPAE760 AM= NO uWl. too 1D.0 1 1110311219103 6744•1 Ara onle lie NO uyL $5.0 22 1 1100//72 11113 75-OS6 Auown NO uyL 53 D 1.E 1 11.3112 19:03 10742.8 APryi-&W. ND uyL 200 t 9 1 11 M3112 1903 107.13-1 AO ohipride NO uyL 109 1-5 1 1IMU12 T9;03 107451 9rnzene 0.11IJ uyL 1.0 0.25 1 11/03112 7:03 71.43.2 Eromachldom6planQ NO uqR 3.0 OA7 1 111031121::03 74-97.5 BramodcNorameDlane NO uyL I,0 0.5E 1 111ON1219V3 M214 &omelolm NO uyL 3.0 D2E 1 WOV121903 15.25.2 Eeamomelnen0 NO u01L 1 11 0 020 1 11103dl21903 74.83-9 2.8u[enon6 EMEKI NO uyL 1W 0-96 1 T1MN12 I 76.93-3 Cerhun maul5de NO uyL 100 12 1 111W 21903 M15-0 Carlton telrochlvr[de NO uyL 1-0 0.25 } 11/03112 19.03 W21.5 Chlory en -e 2, Ili uyL 3-0 0.23 1 11103112 19.D3 10840.7 Chl. oethane NO uyL 10.0 0.6E 1 111D31721903 75-o0.3 Chloroform NO uyL 5.0 0-14 1 11 nW219;03 61-86.3 Chlo-rfi.ne NO uyL 1.0 011 1 11f0311219:03 74.67.3 Chlornprena NO u9L 20,0 0.27 1 71 M3012 t903 126-99-8 12-Dixvmo-3-ohlpropropnnp NO uyL 13.0 2.5 1 1110311219V3 96-124 Oibtn,nprhi.r omilhmw NO uyL 3.0 1321 1 1$10310 219 03 $244141 1,2-DiNQmoelhoRt IEDEI NO vyt 1.0 D.27 1 171ow 12 19 03 tOS-93.4 ❑H.pmememen. NO uyL f0.0 0.21 1 11163r121903 74-953 1,2•DicNaeben2ene DATJ uyL 5.0 0." 1 111OW 12 19.03 96.50.1 1,3-Dwhlwoomxene NO uyL 5.0 0.2E 1 11103112 I8.0] 541-73.1 1,4.0xMoroeenulw 4.3 uyL 19 11= t 7110311219.03 104i6.7 I+me•1 A-DichWto-2.4u1ene NO uWL 100 1.0 1 111011121801 110.574 DIPJllorpaeuaromelhene NO u9WL 50 O2t t 1110111;21901 75-714 1,1 OKNu9elhQne 8,8 Wilt 111 0-11 1 11M3021003 75.34.3 1 2•Dlchtorvemone 1,0 uyL 1 0 0I 12 1 11f0N1 21103 10746.2 Dote IIeo91$012 o326 plc REPORT OF LAE30RATORY ANALYSIS i^y rrport µ.N sal G ypydurad..yr.pt r�. e1ev: o wMrn eae..n1 er P- A-IebE So= 11 Pape 17 at 19 Pact ArWydul 6ervie". I". Pew Amlydpl 6aerien, kle Pose AnNytle.lsrvlee.•1- aceArlarytrcal • We E.ar P..dw Aea r . A 7M Rrr.l M 9ePp Net MA 9W . SR Em... NC 2719E weerne. NC 7SWJ nunu,. A.. NC 2I07e 130et923 W21 {eS pu-7.7e IM407541002 ANALYTICAL RESULTS Pwlecl: SORRY CLOSED -MT. A1RY 1UICd Paco Project No. S2136370 Semple: MW-12 Las 1D: 92734271109E Collected: 10 4112If 0o Received: 10251121420 Mom: Nina, Report Par.meehr. R45-115 Unka Grtyt MOL OF Pnp4n0 Amlysed CAS Na. 01W USO 41SV Low Loved LandlHl A ,oytical Mathad EPA 4260 1,1-0kMproelhene NO uyL 5.0 0.59 1 71 f0311218V3 75.35-4 Qu-1,2-dthtoroelnrne 21.) uyL So 0.19 t 111031121903 IW59-2 0e1r-1.7-Clrchlvrveplene NO uyL $.0 0.42 7 tf1031121903 IN40.5 12-DhnlmepropenQ NO uyL 1.0 027 1 11M3112 f9.03 7"7.5 1,1•Drdllmemo ne NO uyL 1 D 029 1 riION 219.01 142.28,9 22-Pkhlaropropme NO uyL 15-0 0.13 1 1NO3r121903 594-20- 1,1.Dkhleeopropme NO uyL 5.0 9.i9 1 1tM31121M 583-06-5 oa•1.0•Dlctiaropropane NO u[yl 1 D D 13 1 11103112 79 D3 10067-01-5 tl ea9.1-0-OIoNQfopMpene NO uyL 1.0 035 1 W9311218;03 19051.02.E Emyleantene NO uyL 1 0 0.30 1 f110311218;03 10041.4 Ethyl metho"Ale NO uyL la 0.20 1 11r0L 521903 97.43-2 HeKecmvro-t,}llutatll.m NO vWL too 0.71 1 11103112 1"3 67.SS-3 2•FlrkanonQ NO uqR so .9 0.40 1 1110/112 1903 591.78.E Iod-lh- NO ugrL 10.0 0.32 1 7110311210:01 74.84-4 Ieouurand NO uyL 709 35.0 1 11 MN121903 7E-0311 I ftV l0414114 NO uyL lGo 0-93 7 111031121:03 126.96•T Malhylane ChlmW4 NO uyL lk 097 1 117001121901 75.09.2 µ.alp melh.v VI" NO u0.1- 30-D 20 1 1wOvi2 19 u3 au-024 4•fAe",2-pentanom(MlElp NO uai 100 0.33 1 111Wli21903 106-10.1 NAp"plena NO uyL 10-0 0,24 1 11/00172 1903 41.2q-3 PropionkrOe NO uyL ISO 3.8 1 1110112 1903 107AZ4 "tam NO uyL 1 0 026 1 111031121"3 10042-5 1,1,1,2-TaO.EhlwpeFana ND uA s.p 0-33 1 11103012. t9:01 $30$64 1,12.2-TeDaeliar aortas. NO uyL SA 0.40 1 1110111219;01 79-34.5 Tetrecnieroelhone NO uyL 1.0 0.46 1 5i103r121003 127.18.E Toluene NO uyL 1.0 0.26 I 1110311219:03 100.0.11 1,2,4-Tnchlordoeneena ND uyL $0.0 D.15 I 1110Y 219.03 720.82.1 1.1A1 TricNuro oth am NO vyL 1.0 0.48 1 111OU121903 71-554 T,1.2-Trichlw"Ohp" NO uyL 111 D29 1 11 lu311219d] 79.00.s Tnehlurvethene 1-E uyL 1.0 0.47 1 1 NL1219d1 79-01.6 ;11 Trish. aAuomm.[nene NO uyL 10 0.20 1 711030 21903 I54*4 t,7,3-Tr1chlwpprvpene NO uyL 1.0 9.41 1 IIMU121903 9&1" V"ecelot6 NO uyL 50-0 0-35 i 111OV1219.03 108-05.4 Nnp oMonde NO uyL 10 062 1 111631127943 75.01.E ]tylene ITunill ND uyL 60 0.56 1 11M311219:D3 1330.20.7 8u"ORtaa 4-EregwluoubmJenr{sj 96 710-.no 1103121 D03 Eo-00 O1HlromoWoremcmane (5j 79c 03 30 11101121901 .53.7 1 ISSOr 2.O4nHoraeinn•L% S] tNt 3 t z903 1060.07-0 To1uene-dB I5I 99 A 70.130 1 111031121903 2037.26-5 73209 Alkalinity AnHvi"I Method. SM 2320E A 5;allnlly. 10141 a. Go= 87700 uyL 5000 1000 1 1V!12d 1220:14 811 oB BOD, a day Aho"Mt Malhod. SM 5710E 1300.5 dey NO uyL 2000 2000 1 1041J7; 00.Al tOnWI221 ID "94 [Nip 11+992012 03.26 pM REPORT OF LABORATORY ANALYSIS P.O. 16 of 49 TN. sport .M1.r np1 a rvprvQ g. ra ray n MI. x�4rW1 Or. �f.n-mNn[Or �1�1 Aiel rLpl S.rvip. ire[ • paw An.l ylle.l a.rvle.., Tee. >.a. AmlVdca1 aervlea., 1"S. PA"An.l00 l.ryl..s, M4� Paee Anal rdu u. ...I ins. .... af ydc.18"car, 1n' P.- A.Wyu-rs..wu., Me .24ceAI�Iical :�= Ea rr M..rx+1r R..� S..,s n 2Df. R". Pr 9&.y7 Y - µ. 5u. M0 '��� � � `�I• 3p5 Ean kl..0ow R. u - Srw A MTS Fnv.de Dr sem K+esr Me Sir km .w [fW^�Km Ei.n NC iT29E AN.ra. YL MN }M 1M HC 2a314 ..- a�ifcarafil �n Eq.n NC 2r7aa Aan.yr:. NC :a6p4 H.,nYrpn. Hf-7Wie f3]fi1E738H21 [82e1754 7170 (rV74)al'r9L972 I1�6p2]-0p!1 }daelr4-grin f7D41a15-9ne: ANALYTICAL RESULTS ANALYTICAL RESULTS F%*.t MRRY CtOSEO-MIT AIRY (111C) Pr0)eC1 BURRY CLOSED -MT AIRY IVIC) Pace Projad No . 021/6379 Pan Pfoleot No.. 9213637D 9amper, MW11 Lab*: M36371006 Colle teed- 19f24012 t100 Roomed: I012M214:20 M*UU Water Sam*; VW-11 Lab ID: 92136079007 Cellecled: iW41121200 Racaroed1072SM214:20 Maui. Mlef R.P.n R.Pvn pwam.Iwa Rewb. umbl UrrYl IADL DF Prepared Ans"o CAS No, Owd Paremalem Raub Ur16a Llrret MOL OF Preo4red An.N7.d CAS 40 Oum 300A IC Anlona H Gay. Anehucal afath.d: EPA 390.0 60101CP ammo vmsr Alnefy60al M4010d: EPA 0010 Pr.pudba. Method: EPA ]0 TO SNhte 216a.] UWL MWO 2000 1 11f071122152 14W-7" M1 AnEmmY NO uyL 6.0 5.0 1 10fM2 1610 1IM711220; 10 7440-36-0 Anode NO uyL 100 SO 1 Ip12W 12 I6150 I1f07r12ID:V0 74aD-36.2 41M C1dorlde A..Nb.d Meln.d SM0Do-p-E Buklm 16, si UWL 100 50 7 fOr16n216:Is I11D7lt220't0 7440-39-3 1•hi-go MM uyL 1000 Iwo 1 11KWI219;39 16667.DO4 gWY%m NO uyL t 0 10 1 TW6l12 I6.'50 110071122010 7440-1t-7 C.&Nwh NO uyL 1.0 1.0 1 lWIW12 t6:50 11,0711220:10 744043.9 $S t08 TOC Anahueal klomod: SM 53108 C.hromhim NO uWL 10.0 5,0 1 t0+20112 t0;50 11107e12 20:10 744047-1 IMM OrOenlc Cra.n 14706 UWL IDOO f000 t 1IWIIZ 0119 7440.44.0 cobalt NO uyL 10.0 5.0 1 10/26712 16:50 11107112.0;10 7440-4E4 Copper NO uyL t0.0 5.0 1 1Or26112 16:50 1110711220'10 7440.50.E Lend NO uyL 10.0 5.D t V) W12 $050 1110701220.10 7439.92.1 mckel NO uyL 50.0 6 0 t IDr16112 5640 1 VG7112 20 10 7440-02-0 Selenium NO UpfL 100 10.0 1 102E+1216:50 1 IP07012 20:10 7712.0.2 $liver NO uyL 10.0 5A 1 1W2Wt216:3D It107+1220:10 7440-224 ThalWm NO uyL 5.5 5.4 1 10126/1218.50 1IMM220:10 7440-2" VanaAlum NO uyL 25.0 6p 1 IMM12 fa.50 10/022010 74a042.2 2.1 NO uVL 10.0 10.0 1 16Y16r1216:rig 1VD711220:10 7440.66.E 9260 MEV Low L"al Lwdflll AnmMwal Method EPA 6260 Acatone ND idyl 100 10.0 I of 1p31t2022 6744-t Aawdonllule NO ug,'L 2D0 I le 1 11MV12 1922 107.13-I 9.utm4 NO Ly:L t0 025 1 11 POU12 ID22 7143.2 SmO chtwam*m4nt NO 1 VL 3.0 0-17 1 11MV12 1922 74-97-5 8rom.}ONuoromem.ne ND UWL 1.0 0.1E 1 11103112 I a 22 7"r27.4 8r.rnototm NO uyL 3.0 On 1 IVOV12 M22 75.25.2 Stcmum.th.n. NO uyL 10.0 on IVOW12 $9:22 74-634 2-9u1a.o.e(MEN) NO uyL 11" 095 1 11 M3112 ii122 7&93.3 Cafbm Disulfide NO uyL 100 12 1 11003112 1922 7415-0 Cerhon leaechron¢e NO uyL 1.0 025 1 lV03112 t022 58.21.5 LhWfnbenxana NO uyL 3,0 0.21 1 11 W121922 tmgl9 -7 Cnfofaemane NO uyL $15.0 0.54 1 MOk121922 75-00-3 ChWorolerm NO ug7L 5.0 0.14 1 $1 MW1219-22 67.66-3 ChWromel,am NO uyL 1 0 01t I 111031121922 74.67.3 t,2,Dkwomo-3 ehl.lopropm no NO uyL 13.0 25 1 $1 Amf121022 9W12.0 Oydl anwcnbromefhane NO uyL 1.0 021 1 11701/12 t922 12445-1 I-2.plbtomoedeme(EDB) ND uyL 1 0 0.27 1 61110WI21922 106.934 D&ta melnane NC3 uyL $0.0 0.2t 1 IM34121922 74.9 3 12.Olemmobamm�a NO uyL 50 0.3D 1 11 M3112 t9:22 6ar50.1 1.4.01cNwab6 rene NO UWL 1.0 0.13 1 1110312 t922 106.467 9ane•1,4•Di{Y40r0-Ifiaune ND uWL 100 1,0 1 111031121022 150-57-5 I,1.OknloroeNene NO Up'L 5.0 0.32 1 t11031I21922 75.34.3 12.OI woolhane NO uyL 1.0 012 1 111D3f121922 107-06-2 1 1.0Ich1woethene NO uyfL 6.0 0.5E 1 111011121:22 75 75-4 cW120 4moethene NO LWL 5.0 0.19 1 11103712 522 156.504 Yana-1,2.OIchloroeNen. NO uyL 5.0 0.40 t 111031121932 15630,-5 1,2-DICNnpprapane NO uyL 1.0 0,27 1 VIMV121922 76.67.E 1,)-Dlcwwovopane NO uyL 1.0 026 I 11 MW121922 192.2" vis-1,3.OrchWrvprepepe NO UWL 1.0 0.13 1 11 Min 21022 1ml-0I-5 Owe' 11!09f�012 03 76 PM REPORT Or LA EVORATORY ANAtYSSS Pmgo 19 D1 49 Pale. 111012012 03:26 PM RE FORT Of LABORATORY ANALYSIS Pap. 20.149 TN- Ron Wo-1 d ..zab1 n kW. TINS r.fgn.m.l.al bo fopfodu-0-Mnr,n. wer.ul Yr w twr mn..eS 0 oaf:. Alrlredf S.r- Inc whouf.N "10*m Coe..hf of p.Re An 1".el E-6 Im zw • PAca Amty9aal 8en�leH, I— Pace A MOVO M e.rrlo.t, Int Pane Anay6ul an+'lua, I" aceArialytical ^-* La i V.- 30ead • Suit. A ]= Rirerl.N ih 9800 M. A- 5 R 1 W ww ]r.4u pe Edan. f1L 272" kenerfY NC MD. MunrnrA.. NC 281171 ima"49j1 r626]254]175 1>a 197S9LB7 ANALYTICAL RESULTS Pro)ece SORRY CLOSED -MT WRY (UIC) Pace Pr9Jed No. 92136719 5ampta-1IWyy16 Lab tO: 92136379007 Cokcfed IMr241121200 Receiyed I0/25N214:20 MR": Miff Report Parernelert fimulls Unite Ldrxt VOL OF Prapafed AuMaIynd CAS No. Dual K64 Al By Low Lard Laudfitl Anaryncal M.M.d EPA 626Q vent l,3 Okhlompropen0 NO uWL I O 026 1 WON1219:22 IOM-02-6 Ethy6enxena NO 10 030 1 11103f121932 11004$ 4 2•rfexarione NO uWL 50-0 046 1 11 003fl2 1IT 22 591494 lodomizlhene ND up'L 102 0.32 1 11 f031t21922 7468A Metl,ylene chloride NO uWL 1-0 0.97 t IV0302 111:22 75494 4-Methyl-7-nen lAnone IMI BK) ND uA 100 0.33 1 11 f03A219:22 106-10-1 S.ryrenn NO ud4. 1 0 026 I 11 M3112 14'22 10042.5 11 ,R•TaYAd,loloPQ..n. t4v u91L S.O 013 1 11 f0771219:22 630-206 f.1,2,2•T" d'iern.1n, a NO uWL all) 0-00 1 i1103r1219;22 7" -5 Tebrecnlotoetlrene NO u0+1 1.0 0.46 1 11 MW12 to;22 127.18-4 Toluene NO uWL 1.0 020 1 11 n1311219M 10636-] 17rlchloroMhane ND uWL 1.0 04a 1 11f031121122 71-55-9 5,1,2-TridlWmelhane NO ugre 1 0 021 1 11 M34121922 79-W5 Tr4A:wooMene fd0 uWL 1.0 047 I 11fO3f121922 79.91-6 TriDh wallderometMane NO u94. 1 0 0.20 I 1 M31121922 75.69-4 1.1.3-Tr1d,1wP0rapene NO ug L I A 0.41 1 11103a12 19.22 91-10-4 vrryl "Jail. NO uWL 50.0 0.35 1 11101112 1:22 108.054 V" chloride NO U94 1.0 0.62 1 11MN12122 75.O14 Xylene(Tma1) NO uWL 6.0 0. 1 IIf031121922 1390-20-7 Surmalf4a 4•Srbmoiuemk?061411e [8I 97 % 70.1 ]6 1 11=012 11�2 460.0-4 Olbroma6udon1ellme[91 101 % 70-100 1 11IDN121822 1968.53.7 I Z-OkhlorpelVurne-d4 (s} 103 % 70-130 1 11OD3012 1922 1706Q-07.0 Toluene-18 IS) 101 N 70-130 1 W01021922 2037.26.5 20205All allnify AnaYyllcal Med,od- SM 2320B A1kolnity. 7afal at C@003 5A70 uWL 5000 1000 1 It M21122022 62108 SOD, 5 day Annlyticnl mothod. SM 52108 B00 5 day NO uWL MIT 20Q0 1 1 orMl2 OQ:45 10130f 12 21 10 52, BA 300.0 tC Ammn. 14 Day. Andytieel Matted EPA 300,0 S'-W. ND uWL 750000 2000 t 1110W,22233 14808-79-8 4500 Chloride Anasoini Meliod; SM 450041-E G,lonae NO uWL 1000 loan 1 11MV11219.40 16667-15M 53108 TOC Wlalylleel Meylbd; SM 53108 701ai Orgnnl•- Coition 1140 uWL tOQll 1000 1 11M70121906 7440�44.0 / „�1 f Paq Ae,Yyneal 9aMean lne. I.- A rnryeaal afrvrwe, Inc P.- Anaryllcar e.rvleas, lne. ceAnalylical' 7?'f.. kl.amwPe.d-SerA 22251tiw Or oW1 .-rAre S.N I a.,rbinelDr Fden NL 171. f -s roc 76a04 Hyr -d NC ;9076 (lle)6r3-w, (e761zu 7, M rlw IArSawu ANALYTICAL RESULTS Preece SURRY CLOBEO-M 7. AIRY{UIC} Pace Pr00.1 No., 1213079 Sample: KW-19 Lab10: 82136079001 Collecten 10+2411217:00 RecNyed IWW1214:20 Mavis : Vhw RepoA Parameiert Reaulb LIn114 Umir MDL OF Prepared A,alytyld CAS No. tlwl W,a 1CP Oro drrnar Annlyllcal lili EPA SOT 0 NopAn16W161a1nod EPA 3010 Amlmeay NO uWL 60 SO 1 SOrA.'721160 11107r1220.17 7440.36-0 Arse- NO upR 100 5.0 1 1012W$216:50 11107112 20 17 7440,38.2 Barium 14,11 uWL 100 6.0 1 1OW1216SO IW07n220:17 7440.30.3 8erylwm NO uWL t d In I IWMIZ 10.10 1IM711220111 7440-41.7 cndmum NO uWL I 0 1.0 1 1OaWl!21950 11107 f122017 744041.9 Chromium NO uWL Ina SA 1 1WZN1716:50 111WA220:17 744047.5 cebap NO uWL 101 5.11 1 102W1218S0 11107h 210:11 744.4 Coppef NO uWL Too 5.0 1 1012W 2 16:50 11A17112 20:17 i440 50.6 Lend NO uWL 10-0 S,0 1 10 111216:58 1IM711220A7 7439.92.1 Nlckdl NO u0R 10.fl 5.0 1 1W WI218S0 111Q711220:17 W -012-0 Selenium NO uWL 10.0 10.0 1 1012611215:50 111DV1220:17 7782AP-2 Sorel NO uWL 10O S0 1 IOMNIZ 10:30 11MV122017 7440.224 Thallum NO uWL 5,5 S.4 1 fOn&1216-50 11f0711220.17 7440.22" ,A-odlum NO uWL 26.0 5.0 1 ,4 W1218�50 1141'220;17 744" -2 Zinc NO uWL $0.0 loop 1 WO M12 is 50 11 WA220:17 74404" 4260 MSV Lew Level Landllll Anelypeei Meplod: EPA 5260 Aceland NO uWL 100 10.0 1 11 f0ula 19:4Q 6780.1 ACrylenimic NO uW1 2Q0 19 I 11 MW 219.40 107-13-1 Benzene NO uWL 1.0 025 1 1N0111211.40 71i12 11, m-1,lorometn4ne NO uWL 3.0 0.17 I I1oW12 "An 74.97.5 Sl9modi h"_m.9,a he NO uWL 1.0 0.1B I 11NW1219:4g Y6.27-4 Sromolorin NO u0t1 3.0 026 1 1104WIZ IISA0 75.25.2 Er0mamenane NO at 100 0.21 1 T1f0011219.40 74.03r-g 2•13uwlirrp WEK} NO v%fL 100 096 1 1f1031l It M40 75.93.3 Carbon CA sulfide NO uWL 100 1.2 , 11103r1219�1O 7 c4fhon writ im Ida NO uWL T.0 0.25 2$" 1 11163ry219A0 w 3-5 Chbraimrmane NO uWL 3.0 0.23 1 1I1W11219.40 IWS&7 rhr.raeihane NO uWL 100 0.54 1 IIM711219AC 75.00.3 Chloroform NO uWL 50 0.14 1 IIXW1211.A0 67-W3 Cnlor0inenane NO uWL 1 Q Oil 1 ITM121:40 74a7-3 1,2.Odxomo•3•ctaorowopane NO uWL 130 2-5 1 1 oWI21:40 9642.1 Olhromochi,romelhane NO uWL 30 0-21 1 1VOW1219:40 12448.1 I,2-Olbremoethnne iEOS) RO uWL 1 0 C27 I 11M2f1210:40 105.8]-4 Oibromom th.ne NO uWL 10 a 021 I ll=n219:f0 14-95-0 12.Oeh!wo60nzend NO uWL 5.0 0-30 1 1IMIA219:A0 95.50.1 1,4.O1chamben2en a NO uWL I 0 0.33 1 1:W3 21940 106d6-7 tlenx-1 6-Dlchlmo-2bulene ND uWL 70a 1.0 1 11 in 219,4Q 11"7-6 1,1.OkhtoraalnAne NO uWL 50 0.12 1 lVI)V%21940 75.34-3 i,2-ONhlor0e6+ane NO uWL 1,0 0.12 1 11100/12 19:40 107-V'2 1,1-01[Mofoallwne NO uWL 510 0,54 1 11103N21$:40 75 W4 w-12.OIWorxttwrvn II AJ uWL 5,0 0.19 I 11f03112 f9:40 i563W2 bane-]�.-Olda9roe61ene NO uWL 50 Q41 1 IIMU12 IP40 155.6" 1.2.Okhloropropene NO uWL 1.0 0.27 1 111011121940 76.67-5 1,3�IeNorepr0pane NO vg& I.0 0.2a 1 11 MU121gr00 142.28.9 cIS•I,1-0Wdoropopene NO uWL 1.0 5.11 1 111Q7h219A IMI 414 Ogle: l Imo 12 oa 26 PM RE PORT OF LA B O RATORY AN ALY SI S pogo 210140 Oafs: W09120120326PM RE P ORT O F LA BORATOR'Y ANALYS IS Pogo n0140 This remg Y 01 note. viwvdi d :FDI n Ira riv-W,1 N.Y wth. •tyrrdwfd- e.ce Pl n NI. M7�Gur A. zrria wnfe.H 4I Pap MOPWS4n+p1. Jr.. wr7eul pie -10t to .1 .0 1'.. Anse r�M s.me.e. is Paw wsWyOW 9".w, J. Pa44 Ae W-w ". IcaR 1n Pace An.Iyual a.rv4n, I— , Pam AnWyu,.l 6erWen, Alw. Pam Amlydal Sai I"- P.- A-tyfial earvlar• 1- PLG�71tQm�WIM 205 Eaii w RM Aow - Su aal kl 2225 rtwa. Or WOO -'-q A. 1uw 1W � aceanatyti�at l09 E.q Va.60. Row bWtr A 2225 Fl a . pr 9e00 Mmwr Ara SNH -Cu rrnl amm Ed.r. "C 7M. Ad -A a NC 70" >+�+.N.�r. kC 79G J ... .11�f✓reaYCt m9 Ewn HC ai2ea A-aa0A M.. NC 2 �r,nt.raH{r, HG 20M (3N)Wj"QI (478)25�4.7179 (7w)S'1 Sfi(19-7 (]M*27E971 15�61254-71 75 IMAWI-44M ANALYTICAL RIESUITS AUALITY CONTROL DATA Frolsc+. SU RRY CLOSEO•M T. AIRY (UIC] Pr0leol SORRY CLOSED -MT. AIRY 01ICj Pace Prolect No.: 92136379 Paco PivJecl No.: 92134379 9amPW MWII Lab 10: 02131937HOO CoAlectsd: 1O124712 T7:00 Remlyad; 10Q5l1214.20 MatrOv YL%w OC Batch: MPRPIt1813 Anmrymin Metnud EPA9010 Report CC Satan Method, EPA 1010 An."m D-lpti- 6910 MET NG Gro..dwater pmam.Aara R-.1% unit. Llmil MUL OF Propal6d Ane"d CA$ No. Ouml Associated Lah Se mpleA: 02136379001 62110 MSV Low L4y4i LwmMU Ayraytket Method- EPA 6250 METHOD BLANKa60114 Millis Water hens-U-O'c avraprapene NO uWL 1.0 0.26 1 11/03112 19-40 10051.02-0 Asmociated Lea Samples' 92136179001 E0ly O"We ND rpR 1.0 0.30 1 1110311219A0 1OD41.4 Blank Reporting 241eranone NO uyL 50.0 0.40 1 11 Mail 21SAO 591-78-0 Para7neier Units ReauO Urnil Analyzed quaa5ar. lodomedleaa NO bWL 10.0 0.12 t 1110311219:40 74.81114 Nlelnylene Chlvnde NO uWL 1.0 0.97 1 1V011219.40 75.W2 RndinonY uWL NO a9 71165H2 O0:04 4-Mamyl-?�enr4npnalMl9K} N4 uWL 100 0133 t 11103M7 f9:40 101-10-1 RneNc uWL NO 10.0 1110t11200:04 Styrene NO uWL 1.0 0.26 1 1110311219:40 10042-5 8adum uWL NO 100 1110111200.44 1,1,12-TetramWmethene NO uWL 5.0 033 t 11003M219AC 00.20.6 Seryti' m uWL NO 1.0 1KIM200-04 1,7 NO uWL 3.0 0-40 1 11 r4311219.A0 7lF34-S Cadmlum uWL NO 1-0 1110111240:04 Tetra-Not"thena NO uWL 1.0 OAA t IV03A219A0 127.18.4 CMomlum uorL NO 14.0 11101r1240:04 Towene NO uWL 1.0 0.26 1 111031121SAO 1oe-08-3 Cobalt uWL NO +0.0 116111200:04 1 i,i-TrtchWoetlra.r. NO uWL 10 0.40 T 11703M219;s0 7t-55-6 Copper uWL NO 10.0 111011f240�04 A NO uWL 1.0 020 1 1110311219,40 15Oit-5 Levi uWL NO TOA 11m1112 13404 .1,2•Frld+Imoemana TirrrkcnAlloAxrwoauaw,.noem NO 1.0 0 1 112 71F013 NSeiclkeeltl� uWL NO 50.0 $1 M111200:04 eMane NO �yL 10 0-20 t IIM112lipAO 75-60.4 um uWL ND 70,0 1110111200:04 �,STnchkmplopene NO uWL 1-4 0.4T t 1110311219A0 9&114 Shyer uWL NO 70.5 1110 Tanadim uWL NO til200'04 5.0 1170111200-04 Vinyl aCelata Vinyl chlW We NO uWL 500 NO WL 10 0.35 0.62 1 1 1110311219-40 108-05.4 1Uo3112 IS AG 75A14 vanadium uWL NO 25.0 11l0111200�04 %ylena ITwat) NO uWL 5.0 0-0 1 IVOW1219Ao 1330-20.7 2lI1C uWL ND Io.O II M 111290:04 Sumverea 4-&ammluorohenzene{S1 971% 70.13C T 111Wry219�40 4904504 Olh•om011u orometmmna IS} TO$ % 70-130 T 11103112191.40 1668.53-7 LABORATORY ppNTRpL -RAM PLE: 000135 1 2-0knkroe0utne 04 (SI f06 % 70.130 7 11103r 121SAO 1706007-0 Spike LCS LCS °S, Rep Tolyene-da(S) 99 % 70.730 T 1110311219:AU 2037-2a-5 ParaA11a1a1 Llna. CenE. Refull XRec Li'Nla Dllakrium 2320E Alkalinity AAP"ul Mated: SM 23M Anbmmny uWL 500 512 102 613020 Arsaiac uWL 500 508 102 80.120 Alkeanrry-Total 14 CaCO3 19"1 uWL 5000 1000 1 r1102112202a Ratlum uWL 500 506 f01 80.120 Seryffi m uWL 500 510 T02 ao-120 62108 BOO. S day Ar.eNllcal Method SM 521OR Cadmium uWL sod 609 T02 $0.120 BOD. S day NO uWL 2000 2000 1 T025112 OoAS I0130r7227.10 82.84 Chwa vum uWL 500 518 104 601-120 Cobalt uWL 500 502 TOO 80-12o 300A IC Anions 28 Day. Anmyucal Method: EPA 300.0 Capper uWL 500 514 103 80•+20 SLobile NO up4 250000 2000 1 1710711222:4$6 14aOo-79.5 Lead uWL Soo 503 101 80-t30 Nickel uWL $00 311 102 80.120 4500 Chlande A.O,*al Method! SM 4500•CI-E Sefenwm uWL Soo 507 1 of 80.120 Chloride 2btp uWL 1000 7000 1 11/08112 19:41 16687.00-6 S4ver uWL 250 754 1W 80-T20 Tryallkun uWL 500 483 97 00170 a31 OR TOO Anafyllcal Method! SM 53108 Vanadium uWL Soo 514 103 60-120 Lne uWL Soo 511 102 80.120 Total Otpan+o Carbon 2790 uWL 1000 1000 1 17/07712 IS 31 744044-0 MATRIX SPIKE SAMPL i M0357 S213a105418 Spoke MS MS %Rec Pnameler Unll4 Re.ull Conc R"W1 %RSt IJIriM OLAlSars Anamony uWL NO 500 515 103 75-12S Arsenic up,L NO 500 506 lot 75A25 Date: 1110940 12 03:28 PM REPORT OFLABORATORYANAL.YSIS Pape23ot49 Dille: 11109A201201:26PM RFPORTOFLABORATORYANALYSIS Paoe24nf49 IN. I.pan an.Y N. M nprodup.d..9-J A n kJl. . rapert M.R -1 M+.Mro ad. .-to n 1A. M�l ar. w mm con.rnlor Paw Arv+nficsi S wa uK vna-, eh. vvan -.N pr Pau Aryllyp.l 34-.. Irw. Pau Anelytlul per —, no. P... Andyt" 1ervleee, inc. Pev. AnAlypoar a.rv—, In., aceArraJyticale MEem M..eew Reed-6wrA ray Rne—Dr Seta aM.y Are Ste. 100 (dM Nc 7176a A.Mevrie HG i6aW HunNrfNe- NG P8076 • 17701e239991 [e79)754'7178 (704 167 -mv QUALITY CO NTRO L DATA Prp)ect SORRY CLOSED -MT -AIRY l=) Pace Propel No.: 92136379 MATRIX SPIKE SAMPLE a60357 92106t95016 Stake MS M$ %Rec Fe —el., IJnAe Rosin Gpnc. Report %Rec UnWS OuaYaen 840unn uyL 172 509 572 100 75-TZ5 BelYRum uyL NO 5% 507 101 75.125 Cadrnium uyL NO fl00 4" 100 75-125 Chromium uyL Np 500 511 law 75-t25 Cabm uyL NO S00 495 69 75-125 Capper ugrL ND 1.00 515 103 75.125 Leal uyL ND 5DO 491 96 M•125 k&Ael uyL NO %a 501 100 i5-f25 Selenium uyL NO 500 500 100 75.125 Silver 'WL NO 250 .2 101 15.125 ThelllNm uWL NO 300 466 90 76-125 Vanadum uyL RD 1100 514 102 75.12S 90C IIyL NO 500 SOT 100 75-125 SAMPLE OLIPUCATE 86035! S2136T95011 Do Max Paremeley Vnee RAWII ROSA RPD RPO Oual9lelp Am" uyL ND NO 25 AtIoNc ZL RD NO 25 Ber:um uyL 175 177 t 25 BlrYlllum uyL NO NO 25 Cadmium uyL ND NO 25 Cluomlum vyL NO NO 25 Cehsa uyL NO NO 25 Copper uWL NO NO 25 Lied WWL NO NO 25 N1GNOL 4914 NO 71.1 25 SWMnl-m uyL NO NO 25 Silver uyL NO ND 28 ThekWm uyL NO ND 26 Vl mbum uyL NO ND 25 2JRr, 4L 2a.5 30.0 5 26 Dale lm)W2012 00!20 PM REPORT OF LABORATORY ANALYSIS TM1 r.pprl nrr -tae nyvM . —pt n MI. wheal ale Willem eenwnt nr aeee Amly.ul Ssrvsas, Inc P.Q. 25 el 0 peu A.Wyever eervle.e. ine. Pep. Anolydwr Ge ImL Ina Pau Anelydtmi VON—e, Im- aceArralyhcal AS EAe! Meedew Re.a wiN A 2735 Rwh.q.6 990D r�r Are 8�L 100 Ed., NC 272M 0> .Mi.. NC;.p Hinq•v.ue_NC26070 l376 e23-M, 182a13U-7176 C704 1515-009: OUALITY CONTROL 17ATA Prelpee SORRY CLOSET -AIRY (UIC) Pace Project No 92136379 OC 9.Ich MPRP111614 An.lyms Memod. EPA 6010 OC Seth M.thbd' EPA3010 Ana"m Deanipparn 9010 MET NC Ol oundwaler A."umad Leh Saaplaa: 92136379002, 92T36379003 METHOD BLANK. 660361 Mahar: MI& Amacimed Lah so mpinp: 92I39379002, 92136379003 Slink Repmtlna P.r.meb.r u i. R..ul! Und A.Wyted uvap6em Aryam ny uyL ND 6.0 10R1,121a:1a Amens. uyL ND 10.a 1011r112161e Benum uyL NO f90 10At1121a 7a Re010m upfL NO 1.0 10731112 Ta:1a CamlMum up4 NO 1.0 1W31112 fa'I Chromlum uyL NO 10.0 IW3V12 fa:16 Coha6 uyL NO 10.9 1073111216:16 copper uyL NO 10.0 10731 A218:1a Lead uyL NO 10-0 10,11,121816 RmAvi uyL ND 500 .1112 r6:1d SaLanklm uyL NO 100 104111219:r6 Sher uyL NO 10a 11,111121r5 Thealum uOIL NO 5,5 1=11121:'S Vanadium uyL No 25.0 1MV12 IIIIA: Lnc uyL NO 10.0 10r3111214:1 LABORATORY CONTROL SAMPLE: U0362 $peke LCS LGS %Rec Paeamalar Lh1ap Con. Reeull %Rac Lilrah Ouff"lora A.IpT" uOrL 5" 511 on 60420 Ameme uyL 500 522 104 6o-120 Barlum uyL 500 sill 104 MI20 Beryllium uyL 500 521 104 64120 C"irmum uyL 5" S23 105 64r20 Chromium uyL 500 523 106 60-120 C.b.9 uyL 500 523 105 M120 Copper uyL 500 529 196 6¢120 Lead uyL 500 524 105 W120 Nickel uyL 500 527 105 60-120 Selenium uyL 500 526 106 60.120 SAysr uyL I50 2a0 104 60.120 Th.uium ZL S00 520 10a av-+26 Venedium uyL S00 524S r05 a0-129 Inc uyL S00 526 105 80420 MATRIX SPIKE SAMPLE: 060363 02135714016 Splice M6 MS -ARec Parameter 0"llr R-01 orn. Rnu11 X Rep Llri lm uusm— AnSmony vWL ND 500 532 T136 75-125 Arterkc uyL NO 500 525 705 75.125 Dote +I)M012 03:26 PM REPORT OF L.ABO RATO RY ANALYSIS Pepe 26 er 49 IN. r.ppj V,M nvt b. ..r..pr n It, weeal ere wnae-ic—t&Do. A 11» So —.Ire PaxarWy.I.ml 6erWen, lnc. Pax Annyueel 11-1—. Ine. Pma Anava"I amrylemm, 1— �] a Paa Ar1m1y7![el aarvleaf, lne- PAC*A"IV""l SU Ito 1, Mc pmea An y9al aarvrx., lne- aceMalytical• 705 Em.1 V.. daw 4e • $ ilr 7XJ5 R . udr D WW nlnc.y A.e SLAY 199 Pacem,3j cal 235 E.N rA..tlow RmW - sYlr A 2225 R.m..dm G Noun 1 ndy A— S.. 1w �„` •v..a, nN1 ee.n. Nc x'n_aa AM.rn. NC 3eeo1 n�nelnnNs. Nc 7907e ,o„ Edo. NC 27M A.n.Vn. NC ZNWA ft�tw—.. INC 21107D i ]391a2]A52+ fe29125A-71 TB {7011d7"m 031114712&Wt 179126+7176 17wiV.14m QUALITY CONTROL DATA QUALITY CONTROL DATA Ar6lecr. SORRY CLOSED -MT. AIRY IUICI Pruject SURRY CLOSED -MT. AIRY (UPC) Pecs Pr6jecl No.. 92136370 Pace P+tyact No.: 92134379 MATRIX SPINE SAMPLE 6E0363 CC Bitch MPRP111829 Analyses Melh6d EPA6010 92134714DIO 8plke MS AAS % Rau OC Balch Method: EPA3010 AnaNaes Omcrlpo0p7 out MET NC Gtounawpler Pmrerrnler Unite Reaull Cone, Raowl %Rec U!"Its Ouak6an Assedeled Lab Samples 92139379004, 92118179005 Bmrwm uyL 142 500 657 103 7S•125 Beryium uyL NO 500 520 104 75.125 METNOO BLANK M"M Mo71a lhhtor Cadmium uyL NO 500 524 105 75.125 AmaZiolad Lob Samples: 92138379004, 92i]6379005 Chromium uyL NO 500 525 105 75•123 Ri-k Repomn6 Cobme uyL NO 5011 524 109 75-12S parameler Unito ReLuh LIHC Analy2ed Ouekaere Copper uyL NO Soo 532 106 751-125 Lead uyL NO 500 $18 103 75.125 Pntlmony uyL ND 60 1071111216�44 tfthw uyL NO 690 525 105 75•f25 Anenec uyL NO 10.0 10031112 IS•44 Sdienklm NyL NO SOO 525 105 75.125 BedYm uyL NO 100 1OWA216;44 Shyer uyL NO 250 260 104 75A25 Bdtylllum uyL NO 1.0 10alA2113A4 ThImum uyL ND He S19 102 75-M Cadmlum NyL ND IA 1Mal Ill 216;44 Vanedum uyL NO 500 534 106 76.125 Chr6mNlm uyL NO 100 $W3111215:44 Zinc uyL NO 500 530 105 715-125 C00 uyL NO 10.0 10Yl 111215.44 Coppei uyL NO 10-0 1WI111215:44 Lead uyL NO 10.4 191S 11/21544 SAMPLE DUPLICATE MMA Nkkel uyL NO 500 1OKI 1/121544 Sehnlum 11yL NO 100 10131/12 16'44 92133714017 Duo Mee 311yor uprL NO IOa 10/31112 IS 44 Pef4md[er Wile ReamReaua RPO RPO QYNldmre: Thdllum uyL NO 5-5 1W ,12 16-44 Antimony uyL NO NO 25 Vanadum uyL NO 250 101311121644 Promo uyL NO ND 25 Zinc uyL NO 10-1) IW3111216,44 Sedum ug& 30-4 ]0$I 1 25 BeryOum uyL NO NO 25 Cadmlum uyL NO NO 25 LABORATORY CONTROL SAMPLE: a61302 011FOM141Y uyL NO NO 25 Spike LCS LCS %Rec Codex uyL NO NO 2S Patommef uhu c4mc. Reaull V. Rae IJMts 0-10.ne Copper uyL NO NO 25 Leed nyL NO NO 25 Anamony uyL 500 494 99 6tF120 Nickel uyL NO NO 25 AiIianVO uyL 500 ►a3 97 60•120 SaImu l uyL NO NO 25 Sedum uyL S00 479 96 60120 S&dr uyL NO NO 25 Berynklm uyL $00 194 97 M120 Thamlom uyL NO NO 2S Cadmium uyL Soo 464 97 W120 Venadu. uyL ND NO 25 Cnmwum uyL 500 AST 96 80-120 Inc uyL NO NO 25 COba9 uyL 500 403 97 60-120 Coppw uyL $00 490 98 80420 Lead uyL Soo W 98 80-120 Nlcitel uyL 500 488 97 M120 Seienlum uyL San 907 97 5DA20 Bayer uyL 250 243 97 60.120 7haluln uyL 500 479 6a 60420 Vanadium uyL Soo 4116 97 60.120 inc uyL Soo 402 95 6O.120 MATRIX SPOKE SAMPLE 661303 9213E350012 Spiia MS MS % Roc Parmmeter Units R"UR com ReWM %Rec [Jmlu Oum"A.'s Rmlmony uyL NO S00 513 103 75-126 Amermc 11yL NO SOD 515 102 75.125 Dale: 11109f1012 032a PM REPORT OF LABORATORY ANALYSIS Poga 27 of 49 Omt.: IVD59012 0125 PM REPORT OF LABORATORY ANALYSIS P.Or 20 nl 49 Tram mnon.nml nel bd nproducad. m.cmpi - kAI D . r.p.6.H.N -1 be nomd-ad....pi In lull. wh—I m. -mm cm..ntm Para AM lv c.l S.rvixi f>G wftui 81m wiAln.On..rn Or Pow A"Iyypl S.W"F. Im. Paw Aamlygcal aer IMs. ME• Pace Analyee.l aarvlwe, Me. Pau Malymul Umlma, im- . � ' `�JA W5 Eeei V-.Wo Raw • S., A 2= n"w o• 9" K—k A.. Sr.w f ail Ee.n %K 177a8 Amlraru. INC 28904 re,�1.*er,.e N.2e074 (ax1G23a9:1 1112617544170 (iW I975.90@T QUALITY CONTROL DATA Frolecl. SORRY CLCSED-MT. AIRY Il1rCl Fan Project No.: 92136319 MATRIX SPIKE SAMPLE- 661303 92}X=)12 SPAR Ms MS %Rec Pusmater Onile Remelt CmP R-11 1G Rec U[ ft 0v6k6ua Bmnum uyL S9 7J 500 575 97 7&125 Berylllum uyL 30 Soo 390 99 75-125 Cadmmum uyL NO 509 512 102 75-126 Chm mum ayL 7.9J sail 510 100 75125 CahaK uyL NO 509 514 102 75.125 Copper uyL No 60o 417 102 75.125 Land uyL 1531 SOO 511 101 7&125 NKke1 uyL NO 500 516 103 75.125 Salem m uyL NO Sao 511 102 75.125 $Aver uyL NCI 250 251 100 7S-125 Thr@Ml m uyL No silo 496 100 75, 25 VAnadwm uyL 9Am 500 615 101 M125 Zino ugrt 245 500 532 101 75.125 SAMPLE DLIPLICATi: 661104 021MS54013 Dup AAes PuRm"r VMKa Revel! Revell RPO RFD Ouail6ma An9mony uyL ND NO 25 A—WQ uyL ND NO 25 swum 4y+L U.IJ 53.41 1 27 Elmll-um ug7L 11 NO 25 Ca4mkrm ug'L NO NO 25 Chlomum uyL NO N❑ 25 Cnham uyL NO NO 25 Copper uyL NO ND 25 Lead uyL NO NO 25 Nickel uyL NO NO 25 Selenklm uyL NO 4D 25 9Ayer uyL NO NO 25 Thalllum uyL NO NO 25 Vanadium uyL NO NO 25 2arc uyL NO ND 25 P.a Ar1Yym.4l 5mrvlee., M.. P... A"ydal a.rvla., Ins Pau An.Iydeel 8ervrma, me 1. aceAMlyfrcal • 7M Eaml A.aauw R¢ad S it A 2 75 aanHtl.4 Rape x x.l W. dm. N[ V.1m Ae 6. 41.. NC ZO4 H„ne^ 9 NC 3 r5 17aapz]-Wl 1e7e M4-Ilya iT011erbBw7 QUALITY CONTROL DATA Fref": SORRY CLDSP 04 T. AIRY Il11Cl Pace Project Ns : 92136179 CC Baich- MPRP111530 A"Iyal. Mmihod: VA6010 CC Batoh M61hod EPA 3010 An -yam Daov" n: eon MET W 01006w41ar /Wpdalatl Leh 5emppta. 92i36379(g6, 92136379007, 92I06378006 METHOD BLANK. M1306 Met" NAIw Aa odaled LW Snaglam: 92136379006, 92136379007, S213637MM 9lank Repoednp Panmeler u me Asum L1mll Anmtvmd Ousla4n. Anhmon7 uyL NO 6.0 11 r071t2 A6:64 Anerlic uyL NO 10.0 111971A219:54 Banum uyL NO 190 111071t219:54 El"kwm uyL NO 1.0 110071A219:54 Cadmium uyL ND 1.0 11 M711219:54 C hrorq,lm WWI. NO 10.0 1110711219;54 Co6aa uyL NO $0.0 1100711211?54 Copper uyL NO IDA 11 M711219.54 Lead uyL NO $00 11 M711219'ri4 41.60 uyL NO 50.0 1110711219:54 Se]enk.m uyL NO 10.0 11r07,1219:54 S9Per uyL ND 10.0 t110711219:54 Tllplllum uyL HD SA 1lion,219 % Vanedllua uyL NO 25.0 11107112195a $AC uyL NO 10.0 t11071121954 LABORATORY CONTROL SAMPLE. 861309 Far meter Onka Andmwv uyL Afa We 4L Barium uyL BeryWum uyL CadmNjm uyL Ghromium uyL Cduatt uyL Copps uyL Lead uyL Nickel uyL SNenwm uyL Sher uyL Th.IR4r11 uyL Venedium uyL Zinc uyL $Pike LCS LOS %Rae Cone. Rmaull K Rec Llama Oumkllan NO 505 191 913-1 is NO 497 Be 60.120 NO 496 99 N A24 silo ",1 104 19.120 500 506 10t 60-120 600 602 too 50.120 50 495 99 60.120 sail 497 99 SO-12O SOO 505 101 mm No 491 99 M120 NO 506 lot U-120 250 255 102 89.120 500 40 99 90.120 No 496 99 Se-120 500 501 100 N-120 MATRIX SPIKE SAMPLE 861310 82136379006 5P ke MS Mg % Rao Parmmele, Vnra R-11 Conn. Raaull 45 Rec Ln.416 dusmmM Andmvw uyL NO 590 512 102 M$m Amm. uOIL ND 500 506 101 n 125 DO";11109R51241315PM REPORT OF LABORATORY ANALYSIS 1.4p29uf49 Cal. IImmi'l03:26PM REPORT OF LABORATORY ANALYSIS page 30er42 Thm r.p..! 0.4 _( r.Pativemd, ..0 n U. Trw Mprrrj .NPI net G leprr dual, m P4 n M. e.erwnM. eft. �.mel.l Ps. mKrlrgp.r San P. i/ wvM m eedrn mnaenl9} Paw Amikeaw Desk. I- /� �/7� /� Pap Anaryaeal aarrleae, Me. P4.. AT."6 &l 7arel ini. Ine. • a4GA pical• 205 c.al W.per A.", S...A 22Rmr 0, Ed-. NL 21M AA I-sA. l.0 2?AW I13 jd62 l 7e P'.)w 9URRY CLOflEO-MT. AIRY 111]C) Paw P,oj.c1 V. W06379 MATRIX $PIKE SAMPLE: as 610 Per.mete, Until: HarlUm uyL Berg/ium uyi Cadmium dy1 Chromium uglL Cobalt vWL Copper uyL Lead uyL Nwker uyL Salanlum uyL sm-, uyL Tuallwm 491E Venedlum uyL 71M: uyL QUALITY CONTROL ❑ATA P.- An4ylkal y.rvrn., lae. PAC. Analytle.l eatdc4.-Me. Pa m A eatytlul aaCrl m h. Mc 9A7G ��, �• 6,.:� ,°� 3C8AridiytiCB� • p� Ean M. ed.w ho.a. 54 A -ma,4N.. NC 2B07e y. E", NO I'M A.n.rM. r:C 2BKu (704475-am + 1370102]2821 rq]e 1754.1, �a QUALITY CONTROL DATA P,.Jncl SORRY CLOSED -MT AlW lVIC) Pace Prolect No 9ZI36370 92136319006 Raault Sp1ke twit. MS R,r.ulr Ms 'ARec %Rat Lmin 13u0aeela 41.7J 5110 540 1pp 73-T25 NO 500 523 105 75.125 NO 500 507 101 75425 NO SOB 5DO 102 75-125 NO 500 502 99 75.125 pill00 51T 101 75-125 ND 500 SO4 100 75.125 ND 500 494 99 75.121 NO 506 SD6 101 75-125 NO 250 257 i0D 75-t25 NO 500 491 9A 75.125 NO SDO 505 101 75.125 to 4 500 S20 101 75-125 SAMPLE OUPLtCATE 661 V t 92136379007 O.P PaC.mAr4i LMPf Rer4t ReWry And.ony OWL NO NO Ane1.c uyL NO NO B.num uyL 1 a SJ 18-21 Boryelum uyL NO ND Cadmium uyL ND ND cnrpmlum uyL NO NO Cobalt uyL NO NO Copper uVL NO NO Lead u91L NO ND Nlckel uyL NO NO Seem uyL NO NO Silver uyL NO N17 Theleum uWIL ND N❑ Ver.Adlun, uyL NO NCI Zinc uyL i'D NO RICO Data 1110920 2 032e PM REPORT OF LA00RATORY ANALYSIS Try. Hpp Ad nor" r.gve%4e .awcr n 11,11 .11­1pia-Man-unt or Pau Anarrypl Saivwra. In[. 2 Max ftPp Oualleere 25 25 2s xs 25 25 25 25 25 25 25 25 25 25 25 P.ye 31 of a9 Paw Amoye.ar S. ."i, I—aCco K. p.A: 5�.r,x n�nrran.4 NE 2907e 17Nt575_m9 OC Batch M3V2P904 An.IV14 Malhod. EPA6260 OC Batch Method. EPA 6260 An.",, Oeacm9un V60 MSY Lm Level Lenaea A4wenled Lab Samp1e.92}38379001-92136]7900:,921]6379003.4217617300+.42,36379005- 92176379006. 92136379007. 92T36379D0l METHOD BLANK 065911 1A.11n Wate, A4--to lLab Somple5 92135379p01, 9213B379002-921163790D3, 92136379004. 92136379005. 92136379008• 92136379007. 921aG7.7s00e 8ran1 R.P.Mn9 PAraln.Ier Units Rewr L1nyl Anatylad O.AeAers 5111l1,,,,,12211 NO 14:45 I110114Tchl01oethah. 1.1, OWL ND I(1 246 uyL NO 3.0 107+2 45 11141,1,2,2 ,-0.,,2i1p]•.--117TCo'nhnrdlcllledPwfihrrlflpubvareprroovmrppegapdreneeinwepnxn 1uu1yL 14 1.0 11103n2AS ND 1 0 114-1'2 4u9L I,1.Okh. h yL NO S.0 IT' 1 2 .15 uyL NO S.I$ V121445 ge4e nne. VL NO 10 11u03e 1214�45 91L NO 103112 2 445 100 11031, 1,2•dhrume,.}cmeluptepane uyL NO 13.11 111031121111 1 ,2.0bromvaNgHe I E DO j uyL NO 1-0 11 OD]1121445 1,2.OICN.tobe It up1L ND 5D 1110311214:45 t ,2-0len+oroerhene OWL NO 10 1, m31121145 1,2-Chchlnoprnpenr ,.yL NO 1 0 11'03 1 i4 45 1-3-Dlthlwobaru cr,e OWL NO 5 0 11v03112 14 45 1•3-1),chlnvp,.pane yyL NO 11.11. 111031121445 1.4.Nehlnrebenxene uyL NO 10 11+02,12,445 22.0Ia111orop10peno ug+L NO ISO I11011121445 2-Rutenp {MEK) OWL ND 100 1110]r12 14 45 2-Heeanvno uyL NO 50.0 11/031121445 4 [MIRK] uyL RO 100 11/05112 14A5 Acetone uyL ND 100 1110311214:45 Rcelarlbrle uyL ND 550 1T 00301214:45 0a01.1n uyL NO 51.0 11PoL1214:45 Acrylonmlle uyL NO 200 11/0311214 Y5 Ally) chlwide v91L NO 10.0 11r07112 14'41 Bene.ne uWL NO 10 11 ro3[121445 8=610mmethane uyL NO 30 '11D31121445 Bromoq,cnkrpmNnene uyL NO $ 0 11103/12 14 45 9rvm0orm uyL NO 30 1110111214'AS Bromvmeman. uyL NO 10.0 11103r121A 45 &, 4-41de OWL NO 1110711215: 45 1005:45Cubon lgn.cnlp OWL NO 1 0 11107/12 14 45 Cnlorobanxene Owl -HD 3 0/1/03112 14 45 Chiplpelfian! uyL NO too 1110?112 14 45 Cfivl o ltolru 11yL NO 50 1110112144S Cripa, -,-mega uyL NO 1 0 1 TM3112 14.45 Chl,,pp,cne uyL NO 20.0 11/03112144: d.•1,2-DlOhlar0elhene uyL ND 5.0 11i0]l1214.45 ds•1.3•Dlehlprdprppene u91L NO 1.0 t1103+12 1445 plprvmvcNoromeDl.l,v u91L NO 30 1t103"21445 Dale. 1t109r2012 03.20 PM REPORT OF LA80RATORY ANALYSIS rt.. r.pen W., -, W ,apleu,cad.. A1. •­ Wlewut eq. m, rh c IwN of Pme Analybcal 541rK.,4. Inc PApe 12 w 4o • Paw Anelyseal s.rrisn, lnc. P... Analyurel e.Mwt tnR Par. anelyltea! 0-1cea. Mr. /�,,,, acPr 1V 1Ul �ca� :J6 to" M..ae. Nnw. Erna -25 R-" 5, mm x.wr A: S.Y •00 Ld4�. NG:7I64 Ffh.vM »G 211A04 n+i�Ynn1.. NC ]ta17a 133A16i5dW i [e7ejZLFr17G i7d �%S 9dAQ QUALITY CONTROL DATA Prepcl BURRY CLOSED -MT AIRY PIC) fan Protect Tiu . 92136379 METHOD BLANK $65911 Maptr. YYatar A1fOCIa1e4 LaC $m roles: 97 t 00379001, 82 t 36378p02. 92136379p03, 92136379004, 92I36370003. 0213637DOO6- 9213fi3 T90p7. 92130379005 &One Reputing Paramelu Ur1As ReevN L("I Aneryzmd Ou00ere Oalrornomemene uyL NO 10.0 11103M 14.45 OK31Io1P4AA+Mtam.lhmna uyL NO 5.0 I1103n: 14 45 E01y1 n!ltnmvylata uyl ND 15.0 11MV121445 E6lytherueee uWL ND 10 11100121445 Me[achlrt.-1,3.pul molavv u0R NO t0A IVDW1214-45 Ip o-thane 41- NO 10.0 1110Y12 14:15 IaaeytantP uyL NO 140 11103112 fA.45 Ma1NmwvWA41. uyL NO $09 11111111,14:11 M41t1y1 meslverylm le uyL NO 35.0 11 MW,214:4o W ih,ylene C-Wrlde uyL NO 1-0 1110102 $4 45 Naptllnalen. nyL 0.401 109 11l0311214:45 P'OPIO ND'k. uyL NO ISO I1=1214,45 Stytane uyL NO t 0 11f03112 I 45 Taunullornemene uWL NO 10 IIm:W1214.45 Toluene u91L NO 1.0 1VOW1214t45 uera t•2 OwNwoev"t uyL NO 50 11 M301214-45 fr:m-1.3-0101mop. opens uyL ND 1.4 1:4W11214-45 pans t,4.01d11ma-2-hutvne uy L NO 100 110311214-45 Tnchi."Ilena uyL NO 1.0 1110471214A5 Tnthl6rekuummelnane uyL NO 1.0 111p31171A A5 Wo 00etne uyL NO 50.0 11103r12 14:45 Y1ny1 chwrWe uyL NO tB 11 W";? 14:A5 XV4". (Tuh11) qWL NO 5.0 11/01/12 $4.45 1,2athlWo Ikrane-d4 (Si % ID5 70430 f5 MAZ 14:45 44 B+ om0 rlyarpp4naMe iS) '.k 96 70.130 "W"1141 010tmn00116mmethane{s) x t02 Min 11143r1214.45 Toluane•.1a IS} t O1 70030 1 V43r12 14 45 LABORATORY CONTROL SAMPLE 4165912 SPLe LCS LCS % Rat Pe1.m.90r LmM CO4c. RmIt %R4c limps Ouamors s .1,1-2•Tetrmchbtoetnme uyL 50 50.1 i41 70.130 1.1.1-TmNotasthaaa uyL 50 502 104 70-130 1.1.Z 2•Tetre�+W-lh-e upL 50 49.1 96 10-134 1,1 Z-1'nch+n+oethabe uyL 50 496 99 70.134 1,1-O-uhrwocmmne uyL 50 491 95 70.130 11 lachWrmrrhene uyL 50 492 96 70.132 11-OKh1 moptopene uyL 50 49.3 99 Milo 1 ?,) T1 OwmpwD.ne uyL 50 Gal 96 70.130 1,2,4, Tn4MOroaanrene uyL s6 53.4 toe mlu 12•D47mtww3-ch0,r0p.Dp.n. 1iWL 50 59.2 112 70-130 1,2.00omoe11ane(WD) uyL 50 50a 102 70-130 I,2.)mhkreba na uyL 50 51.9 104 70-130 1.20d11M0e41ant INYL 50 40.2 95 7M130 Oate 11108R012032sPAN REPORT OF LABORATORY ANALYSIS Th.-.eo•t.h.t rot a npnf­.,.,I v M rwt-i Mo W n oar of Pecr An lv" S.Mge. IK Para Anaty5E.16almo.., - Pete Aamtylleal ll.ryl.a.• Mr, Seer "Wyo., S-4-4, Mr. aceAfiarytrcal • M Ew Wear Rwa - Sv • 222b Rn L+ coda n r.r me S4* 1u0 T„r c+.un+c+n Eerr Nc S12aa Ai .". INC 2OW4 NwwiwM NC 7A4/A IUA1e738aY1 [AW154-71fa i744IA7s on QUALITY CONTROL DATA Pr m BURRY CLDSED-MT AIRY (NIL) Pace Project Na 92136379 LABORATORY CONTROL SAMPLE: 985912 SPl%e LCS LCB % Rao Pxsmeter ur16s Co'e. R"LQt %Rat Llrrsh OuarNer 1,2-Oid".I repana uyL 50 50 S 101 70•130 1.3.01cNar96a"ane uyL 50 521 104 70.130 1-3-DIcNNOID'apane uWL 50 505 101 70-00 1 44N.Mmr.bwn , K uyL 50 51 1 102 70.130 22-Dicw"eprppane uyL $0 47.5 95 5*145 2-Butanons WEX) uyL 100 DO 61 9t 70445 2-14vaanune uyL 10D TOG IDs 74.144 4•Mellryl4{+enunona fMIBKI uyL Too 106 $06 70-140 A+xlone uyL t40 al.OJ 67 54.175 Aeemm". uyL 500 496 100 70.130 ln Aumh uyL 1� 251 103 70-130 Acryluldnla nyL 250 251 101 70-143 Allyl crowlde uyL 50 49.1 55 70.130 Bentepa uyL 511 51 a IQ min Bromocnloromch5ne up& 50 506 101. 70A30 BrenlD"L.rnrnethona uyL 54 5T 7 M 70.130 Brorhoform uyL 50 51.7 103 70.104 efomamemane uyL 50 63 5 197 $4-130 CBMW draWkde uyL 50 420d 56 M131 Cerhan lehanh*lde .2fL 50 51.9 104 M132 ChWlaoanrone uyL 54 512 102 70.130 Chtmethane OWL 50 At 86 64-134 CNw0arm uyL 50 501 100 70-130 Ch$mmethmn. uyL 50 59.9 120 $4,120 CNOrtNxane uyL 50 61.5 No 70.130 de-1-2•DichluotHhana upL 50 45-0 95 70.131 pr-1,34)lchowo apane uyL so 517 103 74-130 Dihrerabcpt.o Whana uyL 50 51 a IQ 70•t30 W tampmeMane uyL 54 50.2 100 10.131 OidlWron6uwornelhanv uyL 50 ".1 132 5643013 Ethyl mafhmcrywe uyL 50 55.6 111 70.130 Elhy$ew- uyL 50 Al 104 Min I4arecNua-1,idAWlerw• uyL 50 So 111 m= rodmmethane uyL 100 94.4 95 49-160 hbhutanal uyL low t110 111 70.130 MathO 0111lle uyL 5" 501 100 70.130 Me5lyl melhavytelr uyL 54 306 102 70-130 Methylene Chlorine uyL w 47.9 96 SlAn Naphatalene uyL 50 52-9 toe mim pmoomlle uyL 500 511 02 70-130 Styrene uyL 50 62.A IDS moo Tett"woethane uyL 50 s0.7 101 7OL130 Tduana uyL 50 50.6 101 70-130 (Farwt,2•DuO wcm-e uyL 50 414 97 71)4n trarre-l.}Qdtdpraprppene uyL 50 51.7 103 70.T32 aaml•1,4dchWra•2•e+rt.ne uyL 50 61.61 123 MW Tnph1mamw: uyL 50 40.7 90 Min 7Rchloml- Dmemana uWL 50 54.4 109 Q, 133 Pmpe 330149 Qate: 11+09120120320 PM REPORT OF LABORATORY ANALYSIS inr r.p1h YrN not t •.wotln[�0 .rraq w rw n141wrl1M waaan cene4n! nr P4o. A..•n�na+S.rvd1 Mc Pop 34 of 49 Pea A"yged "Mum, Me- Pna Pee. AhpW 7mlu., Ins. u PaAnrlyoul Boni"., Ills. r, 3 1a 209 Feet kleedaw Roes • SuneA 2m Rr W. Or. 9a001h_W m: SWIG 1L0 , yr fd4 . INC. 212BB ASHSo W. WC 9Beal HuaNfe.11. NC 20078 f336IB21d921 Ian PW7170 17041675-IKW QUALITY CONTROL DATA Pro)kct: SORRY CLOSE&MT. AIRY IuIC) Pew Pra)ed No- 92138379 LABORATORY CONTROL SAM PLE: 865912 Spl It. LCS LCS 9. Rae Panmuer uRtIm Cana. Raalrll % Rot Limb Ouallmors Vi o somidia tp7L 100 103 101 Bf 157 Valyl chlarlde Np'L 50 55.1 110 M130 XNena {ra" VOL 150 154 102 70.130 1.2-twollo moll.wd415} % 99 70-130 i-Brom0lualobanzerle IS) % 98 76130 Dbrum Nuommlane IS) % 99 70-130 Toluene -de SS} % $00 70L-130 MATRIX SPIKE &MATRIX SPI KE OUPIICATE M5955 866914 MS MSO 92138379001 Spike Spike MS MSO MS MSC %Rec M" Perameiel LI Nle Reeull Conc. Cwc, Reeull Rawls %Rec % Rea urn" APO RPO Oual 1, 1•ClchkM.mene uplL NO 50 50 54.6 58-6 109 112 iQ 166 4 3ff Ekmrsne upt NO 50 80 46-9 48-4 94 97 70.148 ] 30 ChIer b.neene uWL NO 50 50 54-3 66-9 109 112 M146 3 30 Tuuena uWl NO s8 50 54.4 66-2. 109 113 70 t55 ] 30 Tnchimethene ug& NO 50 60 64A 56.1 199 1Ti W15T 3 30 1,2-0uhlwnelhmnmd4 M) % 107 107 70.130 4-BFam.Bunlaben4aw (S) % 94 95 70 130 D@rom il" metnma(SI % 104 168 7o-130 Tawv*e-de M) % 100 98 70.130 Pace ArWycicaP SmIu1, In., Pau Analy9oe18. vP"e, Me. Pau Anmy""I ■enlul, lna. dL8i4lE3�yflCdl� 2CS E.m".&w Rew - fw,NA ;!m Fl,--i" P, VOW A,",Ay.. Suns 100 e.rx a+rnrEt et.. Ed— NC 2778a Aanave., NC 26804 HRnyfal�Ae. NC 2e07a I33m)929da71 (829)pS�717e 17011e7S9097 QUALITY CONTROL DATA Pv0JecL S11RRY CLDSED-M .. AIRY IuIC) Pecs Plojed No. 92138379 OC S.ml, VQFT722975 APwysls Malhpd- SM 2320B OC 8atcn Method. SM 232OR Aneryats Deamnptw 2320BAlkemrly A.aociar.d Lan E+mplee: 92138379001, 92118379092, 92136379803 METHOUBLANK: 664755 M89I0: mil, Asa.olated Lon SAmples. 92 T 36179M 1. 9213S379002, 92136179003 Blanit Repariing Perameter IMXa Re N Llrnr Andyzed t.Wors Alkokmrty. Tote as CaCO3 tIWL NC 5000 11107J12 1014 LABORATORY CONTROL SAMPLE: 864759 SPlke LCS LCS 16 Rec uetamaier Crud- Came. Reeull 95 Re, ulrwB Oua98em Alkaknny, Totid as Co COI upfL 60000 50800 102 90-110 MATRIX SPIKE SAMPLE: M4761 92135714p19 Splk9 A43 MS %Rec Parameter Lk11U Re 01 C.nc Reeull %Res -1mkL 4ua98ef. Aerslin9y, Tote 4. CmCOy IIjyL 43.9 mgt 50000 90400 93 MATRIX SPIKE SAMPLE: 884783 92135714020 Spike MS MS ARec Pmametef unite Reeull Cwc. Reeull %Rec Llmis QusIllem Alkekmmy, Total no Cocoa upfL 95.8 MWL 50000 82300 -27 SAMPLE Ol1PLICATE: 864760 92135716910 No Ma. Parameter un8a Resell Remo RPD RPO oommmem ABiapnity. Totel a. C00O3 upfL 43.9 rng)L 43400 1 20 SAMPLE OLIPUCATE'. M762 92135714029 Oup M" Parameter un0A Restdi Result RPC RPC Ou@NNm Alkalinity, Tole) no C.CQ3 ur3fL 37.8 mylL 37900 0 20 Dale- I1f09Q012 03-26 PM REPORT OF LABORATORY ANALYSIS Papa 05 0149 Data. i 1 IMIll 291:28 PM REPO RT OF LABORATORY ANALYSIS Page 38 0,1413 IN. nped.har mtd nMdL—d- -Pt W. Tw r.pom shall fp1 M 4,04eca4. 4xcepl. eAl. WWe A the Homan eeneeml.l Pe.a Amlyowl 9.nma'e. lrc vAaIaM1IM x.NYn eaneenl at Pau AFulytl"1 service. Inc • Paw A.Wvw.l Sarvlves. Ina. P...A.Wvg .l 8arrlwa, Ina Paa. Arltlylleel avyla.a, IN- �}�.,.11 /n. 1 Ce�lytica1 200 x.et Wed— R-W • S.nwA 32TD RwerYd. 11 UK* er..[.r Ay. 3. 10 IM . fd.n. NC 272M MKwo.. NC 28806 nMwtwa.- NC 28078 1036108334021 ianlmR 717% t70{W754KW QUALITY CONTROL DATA Prvpck Si1RRY CLOSEJIMT. AIRY Ilfl41 Pau ProJecl Nv.. 9213037g QG Belch: WET2299a A-p"s Meulad: SM 73208 OC Belch Method: SM 23205 Anayea De.ulpovn: 237QO Atka imy Aas=sted Lab Samples: 921 ]6379001, 9273G 379005. 92t36379008, 9213W79007, g2136379008 METMOD BLANK. 865587 Maklx NM1R A.wcialed Lab Samples 9217537900{, 02179379005, 021763700M, 02138379C07, 92136779005 Btank Reporting Parameler Unaa Reaull Umll APayced OuaYOem Alk0r*. Total se ClIC03 UWL HD 500D 1I107112 1S 56 LABORATORY CONTRO L SAMPLE. 16555E Splka LCS LCS 7c Res paremoler un9a Cone Result 9L Rec LIRQ% QuolllLom Alkallnity, Total es GC03 v0L 50DOO 46500 01 90.110 MATRIX SPIKE SAMPLE 665590 92136280005 Splke MS MS %Rec Parameler Und. R..u11 Cone. ReaWl %Rec L1rNtffi cumbnere ArkaknRy, Talal ■a CaCO3 uWL 87 5 n WL 50ON 130000 85 MATRIX SPIKE SAMPLE 005592 92MI79005 Splke IRS AIS %Rec Psremewr tme% Result Conc. Reau11 Si Roc Limits DuaNSers Akollnly, Total n CsCO3 uWL 57700 5OHO 111000 57 SAMPLE DUPLICATE 865589 92135i80005 DW Mae Pa..M.te, Une9 Resin ReaYp RPD RPD OuaNBam AlkaAnity. Total ae CaCO3 Pp'L 67 5 myrL 87200 9 20 SAMPLE OUPUCATE: 866MI 9213A379005 D.P Mo. Aerameter unns Rewtt Result RPD RPD Ousom Mooney. Tatty ea C00O3 uWL 87TOO 67700 0 20 a Pam AnAye.at Amkoe. Inc. Paa. Anelytlut Arvin., tna P. Go AnalyRaal 9.ryl..r, IN. eA ytcar ac �]1i 2p3 F.., M .&d R0a6 • �. A !I%t Ri.arWa Pr 9�p rcv�tir AW SYw 1p0 . rod., NC 71166 AcnaWn. NC 25004 N,..1 A. NL 2w10 {31g15n4WT 026aW7170 00.4als4n92 QUALITY CONTROL DATA proleci OUR RY CLOSED -MT. AIRY (ulC) Pace P.v1eLt No: 071 M379 13C 0etch. 1NEr422882 Anatyw. Method: SM 52108 QC Belch Medved SM 521D9 Aneyaa DasarioB S210R BOO, 5 day Aawcleled Lab Samples: R138VOW1, 02136379NZ. 92138379D03 METHCDBLANK: 959520 M401x: YWtar Aaeetleled Lob Samples. 92136379001, 921363791YD2, 92178379003 Bla" Reponhl; parameter Un9s ROMA Ums Ad.lynfl Quam.re BOD, 6 day cWL NO 200D IWW122D'1D LABORATORY CONTROL SAMPLE. 859529 Spike LCS LCS % R9c PArAmetar Unite Cone Result %R.e UwAt% QueRSera ROD, 5 dsy 4& 198000 327000 105 84.5.115 a E14 SAMPLEDUPLICATE 859530 92130379002 DuP Pvamefer ands Resul Result RPD DOD. 5 day uyL NO NO Mai RPO Dualmers YO Dete: Iu09r201R 03:26 Phi REPORT OF LABORATORY ANALYSIS Pape 37 u149 Del-: IIMWZ012 01 a PM REPORT OF LABORATORY ANALYSIS Pape x el49 T M,.PuR .na wi.,cep n Mi, 'r s r.Pprt We- rot a M1A A.M" the wtim. -I PI Pace A -Vl Sam Inc •ff v p,. e n --I el Pew Analy.ul S.n . I- Pan Annyntil eeMn1, Inc. Pau Amlya eal l.rvrnl, Inc. Pact Anely lcsI aarclra.. Inc. aceArial icaf • 7n5 E.M M..m Ao.e • S,.1. A 22?3 Rr..n tk 9a0O 1[near Ar. sw lW l[d,1n NL 77789 ,w..rdM a0 NC 264 ran%,w 11C 2851a r33o A23.e92, ISMJ154-1176 004191 "2 QUALITY CONTROL DATA Molact SURRY CLOSES -MT. AIRY ILMC1 PAce Amour Na. 92136379 OTC Balch YVETIZ2390 AnarysK Method. Sid 52108 OC 94tch Method. SM 52108 Anwyit Deam"on: 5219B BOO, 5 day Aeaoda(md Lao Sarllpks. 92116379004, 92 13617000. 92136379006, 92136379007, 92136379006 METHOD BLANK 66a19 Mbell: uwkr As.ouat*d Lb Sernpk.. g2176379064, 42136379005, 92t76379006. 92136374D07-92139779006 BIMM Reportng PunnaNt Un4a Rasta U,ne An4lysea r2u41,144m 600.5 day uWL NO 2000 1OW 1221 10 Be LABORATORY CONTROL SAMPLE a60460 Who LCS LOS % Rec POramder Un9O Cone. Re ;t % Reo L1mi18 Ouansm BOO. 9 daY uWL 196D00 240000 1T2 64,5.115,4 84 SAMPLE DUPLICATE: 96001 9213a1T9O0a Dup MA. pwomm, IJMa Rerult Rteutt RPO RPO 4ualih- 800.5 day uWL ND NO 20 B2.94 26A,wocai r Pen AnalytleN Urylcel, I- Peet An.ly6ul aan+ret, Ine. PA" AealynCal WOE*$, Inc. 705 Ea.t Meeeaw Rew - Son. A 2755 R—a DI 990b K—V Aw Suk 100 ,rr,wy my Ea.n NC 2i2B4 R.hwra. NC 7aa0a lk.ntin�er, yC iarlia nse>92sas2, te2alxs47+1e iiwwisg6s2 ❑UALITY CONTROL DATA Ptapp SORRY CLOSEO•MT. AERY ILIICI Pace Propcl No. 9213837D OCBatch, YVETNI39M Anstyais Method! EPA30D.0 CC Batch Me6wd: EPA300-D Anstrsla Da tpOm: 300.0 IC Anions A c atad Lab Sampks: 92176379p01, 92176379002, 92176379003, 42136379004, 92136379003 METHOOBLANK: 66411E MOldy MW A4.adaled Leb Sample%: 42i16179001, 921M379602,92178379003. 421163790p4. 92138779005 Bland Reportng Paremeler Un4f Renal Lj-t Anety=ed Ojuae64n Su"16 4L NO 25M $11011121946 LABORATORY CONTROL SAMPLE: 894419 Spike LOS LCS %Rec Parametai Units Cono. Result %ROC UmkL OuallOers Sull.to oWL 20000 16600.E 91 9O.1111 MATRIX SPIKE SAMPLE 664420 927362350t6 Sptc MSMS %R.. Peremeler Unrta Reeptt Cu.,c Re-ft %Rec LJnen 0-bpr S 101. uyt 6.2 myR 2000D 266001 102 90-110 MATRt%SPIKE SAMPLE 664422 9713679N06 Spike MS MS %Ree Pmemelt,r Units Refull Con. Rea,Yl %Rec LIr1Y1s OuaYalr: SWWe uprL 3290J 20000 26600.1 117 9D tt6 Mt SAMPLE OUPUCATE: 464421 1121352301115 Dup Ms. POram6tar Units Revell Raku6 RPO RAC 0ua11114n Sulfate ugfL 6.2 mgA. 63401 3 20 SAMPLEOUPLICATE Il"AV 92136192DD6 Oup Mes Parameter Wk. A—ri Reaun RPO RPO 9u0i6.5 Bulkk ug+L 3260J 334OJ 2 20 Only IIM9RO12 31-29 PM REPORT OF LABORATORY ANALYSIS P�PL 3,; ai 49 De10 11 rD9r2O12 03.26 PM REPORT OF LABORATORY ANALYSIS Pape 40 o149 TN.•.poe -0 netw r.W14-Ad .xe.m n kn. 1--per! sh.s — t ,apree,aa3 e 0 w f.I. Are,out era -,Mn ownl.d of Aap Argecar ti—. I- • Mwl e.. nm- cve.an, of Pme Ansiy9cri S—Ims Inc • Pate AnYyewl 54Men. In6. Pate AWd Plcol 6arrle.e, 4— Pao. Anarydael Sonrwe, We. //,, yy�^^r k7yrrlaaj 3 E w Uaeevw Ra.d 12,2 A 2= R—. dew p6g0 NnpT a... 6uY 506 f 133n)623a1T:+ [e26m4.717a 170.11e74m092 QUALITY CONTROL DATA Projacl: SURRY CLOSED -MT. AIRY IUICI PAM PF0180 NO.: 92136179 OG llo-h- VVETNI3450 Ar *%* Method EPA300.0 OC Omen MO*Dd: EPA 300.0 Analye4 Deaaiplkm 3W.0 r6Anlma Aa.06.1fid Leh Samplaa: 9R 1363190M, 92138319007. R2135379MM METHOD OLANK. 666373 Motu Mhlw AesONaled Loh Sompls4: 92136379008. 92136379c07, 92136170W1 simI Reperlhp Ppameler Lrnms Recut! umt Analyxcd Oueemers su"Afe 'W4. ND 25000o 11(07022125 LABORATORY CONTROL SAMPLE 565374 Spike LCS LCS K Re. Pwameesr unmo Conc. RHO %Rat Llmll 011N16ws SulfM. "WL 20000 18moi 93 W110 MATRIX SPIKE SAMPLF 665375 927163790% SPur. Ms MS %Roc P. b—tor Imes Result tp C ReSyl: V. LA111a (1uaiaere Sulf to uOrL 2160J 20000 30 w 1a0 90lt0 Mt MATRIX SPIKE SAMPLE 665177 92136WOM Spike MS MB X Rac .f Pammv Unlle RMO Gene- R"WI %Rae LN1oh Ou.kmero $Wool- uWL 114000J 20000 229000J 573 wl" M6 SAMPLE DVPLICATE. 665376 92136179006 Cup Me. Par -MOW r]nrla Re4.11 Reaull RPO RP13 quakaen SWIlm u4'L 21604 2170) 0 20 SAMPLE OUPLICATE 465376 92136561003 Du Mee Pw4me101 ]lode Ree.Il R.,um RPD RPO OvehRmu. SWlel. u91L 1140pp.1 "60001 1 20 e MMeea, Nr- Paq Rnwyllgl iarYMH, N.R Pew AnYypeel eenlen, aAe. ' a%�. Ii77d✓' ��.�1 28 EeY Warr. Aqd - &A. A 2m ff".." Or 9600 K" r.w Sim. Im E. . K 27ZM A h-ft. NC 26604 11u %—me. NC 2mle 01364n-mi 169 mA,7176 rTuK7'r9pe2 QUALITY CONTROL DATA Nqp i, SuRRY CLOSERM7. AIRY fuic) Pace Prnycd Hu. 92136379 OC 86r0n y48fA113661 Anary" Memod SM 4500-CFE OC 8atc4 Me61od: SM 45MCFE AnalrsY Dasplp6 n, 45W Cmadds Aaeaciared Lob Saaplas: 37213N 19gp1, 9213637006Q, 92r0637900] METHOD SLAW B67243 Mobbr: Y5111or Aaeddaled Lao Salrpka: 92136379D01. 927363760p2- 9Q136319g0] &onk Rappnlnp Poromalef Lines Rewk Link An*sm l ourAllm CNndde uWL NO 000 17A3671721'06 LABORATCRY CONTROL SAMPLE 867244 spike LCS LCS %Ree Paramolsr units Cone Re.ud %Red Um14 4uallam Chlcrde uprl 20000 19M 100 90-110 MATRIX SPIKE SAMPLE: B67245 02135714026 9plks MS Ms % Rat Paramelar Unna ReMurl t C— Rae % Rae LJn41a tlualN.ra Chlarlda iWL 2.5 myR 20o00 21900 97 751-125 SAMPLE DUPLICATE: W7246 92135714026 Dup Max Paramelar Unbs Reaull Reeun RPO RPO Ouakmen Mends uyL 2.5 mgoL 2160 15 20 Dole: 1UMO12 03:26 PM REPORT OF LABORATORY ANALYSIS No. 41 .149 Dow ,I rp912012 03 26 PM REPORT OF LABORATORY ANALYSIS Page 42 or 49 TM noon Ynm �1 M •Pnd­qO....W n M- T> LTen od ream mi e. �.pad�d e.a.yi - rw .f—Oa —be- womnl el Pecs A-,, Y S—., ire MMuI M y.xMn (norm of Pia S — u,e • Pa.. A.Oydoal"rVID", kM,. Pka. Amlomel lk lafa. Ina. P.- Analytical 6.Nle.., In.. aceMalytica! 205 L.al M..rb. Fcw - S _A 22Z Reseal Dr mw N.rc.! Ave Sun 100 wy r Egan. NC 7?iBb AalwrM. NC 28MM NC 20075 1336167d 971 i99e}aSa.711a 1AM*IS-Dm ❑UALITY CONTROL DATA kop.k Sl1RRY CLOSED -MT. JURY (UIC) Pac. Pr9AR No : 9213WO qC Hatch 11YETAIIVO1 Am". MNnod• SM 450D�CI•E QC Batch M611md SM 4500•0•E AP@Wm Dnvlplm: 4500 Chionde Asscdammd LsbSample: 9217&379004, 92y76379005, 92136379D06, 82138379W7, 92t36379008 METHOOBLAW 169t94 Motu : VAIM Aanedmd Lsb $--whoa: H2136379004, 92t76779005, 921]6379006. 921 ]6379007. 92136179006 Blank Reportil9 Paremalal tanks RIUK L rdt Analyzed DuaYOem Crania UyL NO 1000 StA3N1219:11 LABORATORY CONTROL SAMPLE 819195 Spike LCS LCS % Rec Pars-mm LMIa Cone. Remull % Re, Umlp Oum111m ChtwiltA uyL 20M 20M too 90.110 MATRIX SPIKE SAMPLE: 869196 92138210ODS SpIW MS lab %fiat PYe.f.r m Unit. Cane. R-11 I7 aaua 'ARae LMws Ouaeem chrPMe uWL 50.6 n WL 7D000 702 0 % 73125 SAMPLE Ol7PUCATE 56910T 921362600015 cup MAR Panmelar VOL, Rnuu Rasun RPD RPD Qualifiers Claarlda upfL 60.8 MWL 50200 1 20 Date 11f0912012 0326 PM REPO RT OF LABORATORY ANALYSIS Page 43 of A T" r*Wq fnm. mi W mWadi f..c.pt p M. -*we e.. �cmWI cf P_Ar If"S.-Oo.•� Pau Anal yucel AaMce., Ina. Pace AnaWml S. rcoi. Ine. P.- Ama?Vd-P 6.Nkn- Ina r q nn,,,,,,,, ff l ' acellf7[YlA'c 1, 295 EaN W.dlw Raad -SionA 2=Ri..rw. D+ OW wry A- Sun iW .• NC 272M A mtvft NC 21a04 NC 21071 I]a619 5M, zdi2b. ?t7a 4tNM754m QUALITY CONTROL DATA Protect: SORRY CLOSEO-MT. AIRY (UIC) Paw Pfnl40 NP.: 92IM37R pC fetich: YVETNIM62 Anm"m Matl+od: SM 531013 OC Batch Method: SM 53105 Analysis 0"mPldn: 5310E TOC A.96d4ted Lab Sa PIft! 9;138379001, 9219137900;, 9213E379WS METHOD BLANK 666W2 M801e V1a1er Amdmt" Lab Samplee! 92176379001, 92138379002. 92136779W3 Blank Raperlhp Parameter Un1e Rewli Omit Analysed Ouaalm Total Orgerk CaFbw vi ND 1000 1110l122148 LABORATORY CONTROL SAMPLE: 16600] Spike LCS LCS % Rea Peremeter U." Canc. ROVAI %Rec Units Cuntlm Tatrlr 0%0-c Carbon uyL 25000 25700 101 W-110 MATRIX SPIKE SAMPLE 1560IIA 97135714015 Spike MIS M9 %R.c Parameter (Inge Resull m1 Cc. RUO %RAC LIMM Owl1m Trial Orpwc Carbm uWL 0.5 mgx to" 31500 1B 76-12S MATRIX SPIKE SAMPLE' 665001 92135714026 Spike MS MS %Rea Paramaler unlls RemAl Com. RHLA % Reo L]mlla Owbgm Tpul Organk Grhon uWL 9.3 mpR 25000 33200 w M125 SAMPLE OLIPUCATE, 866006 02135714017 Dup Mex Parameter undo Reswi Result ROD RPD UuAllliwa Total Organic Carbon uWL 11-0 MWIL 10800 2 20 SAMPLE DUPLICATE 966007 92133714027 Oup Mar Panmeler Unls Reelm Result RPD RPD 11ulklim Total O.ganla Car w l uWL 4.6 mglL 4470 1 20 Dalr 1110 12012 0s.26 PM REPORT OF LABORATORY ANALYSIS Page44 Pr 49 me rapers " mr wnpfr euud...004..V w IFWUr 010r e..n can.ml if P.0 Ar ,leal SaMeaR fee • Paw An AyWa164nia". Inn. P.c4 ATwN" EIMH 60e. Ina P4ce Andlka yl 6empa, Inc. L'lIp L 1 ( l ' I i Fade Moss Rea & %A 2025 Awi da Pr 9e00 N—, A 5u $w . ; Eden. INC 27" Aana . NC 2111604 H-wr os. he 2BDra • 1336)52? , AM25 N?a 17041675-0 OUALfTY CONTROL DATA Plo*c7: SURRY CLOSED -MT AIRY (L11C) Pace Prated No.: 92t36179 DC Belch: %f*TArT3872 Ana"m McOwd: SM 53198 QC So" Me6wd: SM SHOW Amaral%0.4np9rin 53105 TOC Anodded Lab Se"Ies 92136379004. 92736379095, 92136379008 METHODBLMK. 868667 1MIi 1AIIIIla1 Assedaled Lob Semples 12219579004. 9Q t 34179005. 92 T 36379006 51-1, Reporing Promekr Linea Resup Umk Analyzed Qua90ma Total Orpme Carbui uyL ND 7p00 IIMO121526 LABORATORY CONTROL SAMPLE: 6MM11 Spike LCS LCS %Rec pueme7el Un111 CorK. Result %Rat Llmk. 13u09asrs Tales OTgrde Garhon -WL 25o00 24000 99 90-110 MATRIX SPIKE SAMPLE 65886o 92136192006 Spke MS MS ea Ree P,ramayal Unm Resin Gene. RINN, 95 Ree Lie.q 044aii a Told OManrc Carbon uyL 67N 25000 29100 90 75.125 MATRIX SPIKE SAMPLE' 666091 92136198005 Spike MS MS V, Rec Premeler Unlh Reawl Cant f?.SLd, % Rec LI-11 OuMAen Tplsl Ogmm carbon u04 28 3 rr WL 26000 S7700 94 7�12fi SAMPLE DUPLICATE; ON4190 92736192009 Cup Mee Perameler UnKI Reaem Rek4K I RPD aus9pan Tmw DrpRHc Green vWL low 103M 3 20 SAMPLE OUADCATE; 608692 92136398o05 Oup Me. Perameler Limo Result Resup RPD RPD Qus91Nn 1`641 organic carhnrt d1 33.3 MWL 32900 1 20 De7e fi101f201201ZePM REPORT0F LASORATO RY A NA LYS IS Pagi450149 Tt., rEwn snr­IN r.e.v ....0n1, .VOA N. nn1Yne &EM 0 Pad' Neal dal Servaea. 'n[ PEW Analxa6el &"—. IAR. Psee A-10-1 p.rrk.e, IN, PEWArulylleal INAMN-a, lrye. zw 105 E.duo.dS Road S A iS7.3 Rh. as 0e Ya00 tonal Aw S_ Tw Eaen NC 272H AY . NC 2110M IVnyrae,K.. NC 200M • r3M03d9,11 ITpala759w QUALITY CONTROL DATA Proleek BURRY CLOSED -MT. AIRY (UIC) Pau Project No. 92/36379 OC Belch. VVET0103665 Aeellall Mdhpd: SM 53108 Qc Belch Metwis SM 53109 An" Dacr"m 5110B TOC Assarloled Lot? Samples: 92136379007, 92t26319M METHOD BLANK 86773A MAIIIi VN96r AeaocWmd Lab Semplee 10 36379007, 92138371=6 Blaek RepoMg Ppamet6l Unh Reseal LI+Ap ARIAyzed Quallim Teal Organic Carbon uyL NO 1000 t110711216:36 LABORATORY CONTROL SAMPLE a8T737 90" LCS LCS % Rao Perameler Umh Conc- Rasull '4 Rac LirNh QuaMlns Told Orgiimc Carbon uyL 2fi0D0 25060 1DD 904110 MATRIX SPIKE !AMPLE = 667Y36 92i36179007 SPRA, MS MS %Rec Piummeler Urnns R►WAI Conc. Result %Rec U"M Qualm Total 0r0pnlc Carbal uyL 1140 25000 26800 103 76-125 MATRIX SPIKE SAMPLE: III 92136111MIZ 5p91e MS MS %Rec ParaM.ler Una ROOM Conc- Reauk 49 Re, Lklaka 0wnlera 7o111 Organic Carbon 9p9L 5 6 we& 2ww 31700 104 7S12S &AMPLE DUPLICATE: 6677111 02136170006 Dap Max Pramelal Unaa Resu11 Recall RIPEN RPD Dua Am Total Organic Carbon uyL V110 2710 2 20 SAMPLE DUPLICATE: 687741 92137066001 NOW Mo. Perameler Unlis Recap Re" RPD I Quoiri Trial D106nIC Celb6il uyL 3.5 myL 3520 0 20 9816 11+09401203:26PM REPO RT OF LABORATO RY A NA LYS I S Page 40 ar 49 Tn. r.wn .n.. -1 G..'.Pn+dw.a..•.C. ^ M. rnII 1h.. nEa rpra4nl .I PAd Meraervy S. ,.o ez PAM Analye[ardM aft. IM. Pa[. A-IVM r s—ileac, I"yri �'B i(1 �Yf2t• 205 E.N Wit o Ro[d So4A Ar sid. p• •MP4e+ee Pea Ed- NC 27M A:2.5 v�aW,e. NC 2e0u4 11]dy1m-e .1 t47a105.-71+e QUALIFIERS fimi. 1. SURAY CLOSED -MT A1PY IU:CI Pew areJed No . 92I3637A DEFINITIONS Pau Anatytlal Stroh" M[. 09oo.-[r Are s— 1l +Ae.lerern. NC 2907d 17010754M DF DM+ton Fec{vr- d tenons tl, rapt ea enh the featw eppl+nd',p the �epp,led dala due lv ch engga ,n 14mpH PlepArM.on, rNl�nPn PI 1h. fampl. aaµ+pl, of mpyNly CMIe+11 NO Not D.lected at er nbpve 14,91ed rewbnq U-It J • E6smate4 Coneenpgllpn above the edlusled rnethod detection Il mn and below Ine edh+eled reporting IImA MDL Adlusla4 Mvthod 011acbOn L•mn PAL • Pecs Reporting Llmr RL • Repenlnq Llmr S - &•negate I,2-0+phenylhydrarine 162701Ialed enalylo decompoaen to Arobenrene Cm Lllonr w1th EPA pyldetmes, 4nrpunded 9rle are R6p5eyed and harre been 45ed 10 calewlete %recovery and RPD wdu.a L C3[R} Lgbarelvry Cvnlrel Srmpk IDPphealel M SIO) • Me ala 9pll.a JDuPl+cele) DL1P - Sample D4pllcate RPD ReIM" Percent 0i7I.1ence NC Not alculahle SO - Silk. Get Chan-LJp V - IndeArea n. --,p and we. enNyred fa, brrl na1 det.Cled hl-N6roaodglhenyle mine deepmpp6ee and cannot pe 10pealed hom piphenyrerme 4amq M.Inv4 6270 The ree4d teRo+ted for each an style Is a cvmhlned convenvn9on Add pre 4—flon me not he eppropnale for 2-Chl-wos thyhrnyl ether. Styrene and Vinyl chloride Pace Anehrycal A. 4cued10d Contact your Pope PM hr the 6urrenr bat of .,1F.dIj.d AnAlylas. TNI • The NELAC IneaWle LABQRATORIES PASI.A Pece Analviwol Senlees A4hey9le PASt-C P.qq Anelypcel Sarvrcee Cha4otte ANA LYTE OUALIFIEAS e2 Otypen -mg. meal than 2 0 for All ddullone set The repo, led vaam M en esllmalea lees than Value and It CAILUA1ed far the mlutwn usng The m_T amount eT ae mole B4 The OW ... lglutemlC grid.'. exceeded the range of 191 plus w minus 30.5 mg',. Li Anetyre racavmry in the Iabvrslory conaol sample {LC5j exceeded OC Amhm. Anetyte pretence below tepofEng lanlll 6r ""V Bled setup"' Results unaflsde4 by ingn We. Mf Melne soils recarery sac ee de000 I,miq Be1M a[[epre6960e0 On IAtl Orelpxy Canlrel {emote [LCS1[emrely w Metrtl apaq and MAMA lgll.t 4upllcele rewvary net eval401ed against Control Il mile due 14 /MPple Mullion. RT RFD value Was Waide con0ot I" Pie !v unearleul ly al r-Wirl W a new The PR 004e: 11109t=2 0:26 PM REPORT OF LABORATO RV ANALYSIS PAge 47 of 49 Tree room m., no1 a rso—. ". ey[eP1 n tV,. _W on —We --(Of Paw A-gtc d unoce4. 4c Pa{. An•lYWAA SeM[a. Inc. Pee. Aalytlur Eerrla4 "I Pau A.Nyuul 9.Mees, Ine. ace ytrcat • l76 E4H Meaeer vetl - 6, . e A 2225 RNusae gWG.eur Ar. 5r tCO Eden N_ 7770 aen.W,. NC 7E604 rwnrrvv,Te. Ne 2w7t []369I3-49V npg)25e•7, 78 (7wj175-D E2 QUALITY CONTROL DATA CROSS REFERENCE TABLE ProJecl SIJRRY CLOSED•MT. AIRY ILl•GI P.C. Pr.j-1 No. 112T35379 Arts v,4-I Lac 10 Semple 10 CC Basch Method QC Brtet+ Amlyucal Mathad Baw, 9213079001 MW-1 EPA 3010 MPRPl11a11 EPA 601tl ICPr1oe20 02135379002 MW3R EPA 1010 MPRP111814 EPA6010 ICPrr06T9 9213E379903 MW16 EPA 3010 MPRP111 e14 EPA6010 ICP110119 9711336]37900054 MW-t12S EPA 1010 MPRP11164 EPA60T0 ICPl10e11 2790 MW-20 EPA 300 MPRP711029 EPA 600 [CPO 031 9I1 ]6374005 Mri-1] EPAMtg MPRPA$830 EPA6oTg ICP11o834 .16179001 MW-T6 EPA1010 MPRP !130 EPAE010 VCPA0614 9211a37900a MW-19 EPA1010 MPRP11IS30 EPA60111 ICP110634 9013677900t MW-1 EPA0240 MSV2o964 92115379002 MW-SR EPA52E0 MSVl20964 921]6179003 MW16 EPA 67V MSVr20964 S2136379004 MW-12S EPA 0280 MSVr20964 Y2116179009 MW120 EPA 62150 MSW20964 9$136379006 MW-13 EPA6260 MSVYa09S4 62106]79007 MW.ta EPA e260 MSV20964 971797790a6 MriWS9 EPA 0260 MSV20964 9Y13677900t M-t SM 232013 WET122975 9213937900Y MW3R SM 2120E WET122975 9217677000] MW-16 9M 2320E SVETl22975 92176379004 MW-129 SM 2120B VJETl22994 97116379006 MW-12D SM 23206 YJETf22094 9I136379006 MIV-13 5M 232p8 WET122994 9217677700t MW-1a SM 2320E WETF22094 92135370006 MW.19 SM 2320E WETF22994 92135319001 MW-1 SM 52t OB VOETF4862 SM 5210B WF-Fr22e63 6213 MW.7R Ski 5210B WET22462 SM 52108 VVF2663 921760790002 SM 52100 VVET72882 SM 521OB Wra B3 36079004 MW12S SM 521oB WET22696 SM 55 VYVVEETi2222e99997211 120 M 21 WET22SM 5 8 PA 20 SM50 103037g6 eSM 52U VYETR259999211][37 2 M 52108 yE7286 9M 52t0B VyET22P999 9213637900 W-19 5210E WFT51,1510E MTAt9 94176]79091 MW-1 EPA3000 VJETA413514 92t36779002 MWSR EPA 300.0 WETW13614 421]5379003 MW-16 EPA 300.0 VVETA113834 92135779004 Mri-125 IS 300.0 WETPJ13614 421365790p5 MW.120 EPA 300.0 WETAJ13614 72116179005 MW-13 EPA 300.0 WETAIt 3650 02139179697 MW1E EPA 3tl0.0 WETAOX:0 52136174606 MV4-11f EPA 3000 WETAr1'A 0 92136]7900t MW.1 SM 4500•CI•E VVETAr136e1 aI1 S63790oI MW-SR 51A 4500-C1-E WETAr196e1 921310W03 PAW-14 SM 4500•CI.E WE TN136e1 OAIe 11+092o 12 0126 PM REPORT OF LABORATORY ANALYSIS Pmge 46 pr49 Tht •epcn -a -1 ea nMr&C.- except n w. wToul the u.rnan a7aaerrt o} Paw AnNyeW Serve[aa rz 11"y"al:aryls.., I— peer An ".4w 9-10.6. 1" N.. APWyawl GNI.I. km BCBI'S! IQ1 JC2I • an E��� Wye Re0 - S� A 2225 apn.q. Ar gWa K ,A- Sue, M Ed- NC 7 M AN,aVM he 28W4 HY W—I., NL alm 1336I673EP71 (97612SWIM 476-167590a2 QUALITY CONTROL DATA CROSS REFERENCE TABLE PfojKL Pau Prow No. SORRY CLOSED49T Alm (VIC) 92136376 AmMiul Lah ID Bam* ID OC MOO A1oed CC Balch AnNyuul Malhod Batch 92136379006 MW-12S SM 4SD4-CI-E WETAd+]74l Ut 36379006 MW-1W SM 4500•C+-E WETAf137Df 9213{779006 MW-13 SM 45WCI•E WETAM 1745 7213677l00] MW-16 SM 4SDDACI-E IAETNI7701 6210G379006 MW-19 SM 4500-aE WETAI+3701 37136370001 MW-1 SM 53+0B WETW+31W 92136379003 mw31t sM 53+0 WETAI+M2 12136376M MW-14 SN+53148 WE7W+36E2 W3637l0p4 MW123 SM 53508 YYETA113672 627363760o6 MW-12O SM 53508 WETN+3672 92136379006 MW-13 SM 5310E WETN53872 62176379007 MW-111 SM 53100 WETA113695 9213637H011 MW-li SM 531 DO WON 13695 C Eau. IIo0912012 0120 PM REPORT OF LABORATORY ANALYSIS PApa 49 of 41; f •w1 W+.;md� Ul whMCa ,an. of Pry Ag1ry 1S-- P;{ 1 I ;+��.��:_; ■■■■ooaaoaso .�;�e1111111111111® _� - ,`� I,111111ANun© `s6j �'1��■■■■aa■■aeaa�©� y I Document Name: Sam le Cend1Uan U on RecW SCUR Document ": May 7, 20T2 Revie1 of 2 Document Number: laauing Au#"ty. 1III FCHR-CS-M-mv.07 Pace HunterailHe Quality 0" Ci- nt Name ln wills Project # 9�i 3y9 When RaoelYad: ❑Terra ❑ AshevHle ❑ n I Courtar. ❑ Fed Ex ❑ UPS❑ USPSO Cann❑ march Pece Other Cwtody Zfael en Coalarieox Pruerrt: ❑ yen no Sena irieect ❑ yes 0 no Pecking Mete rltt: ❑ Bubbte Wrap �ubbta Bag% [] Norm © oiler Thermomvier Ueed:IP. Gun 10 T1102 Type of la: I� Blue None on tu, woo pw�W rns I— bdl T.ma [:rvrwHlnn Ger-1nr _ TIAM- Nn Cnrrantim T1 S N.f`n "e-L4m Biological Tleeus Is From: ru m WA aNa us of pan ammkung Carraoted Caolsr Temp.: C e;if Tamp snasd ba above 1 e6 r p to rc Cornmerta: LX Choln ofC Present Ya. ❑N. OWA 1- Chair of Custody Flied out . ON. O" 2, Chakr of Cu Ree uiahad: . ON. OVA 3. S er Name A IN neWrs on COC: r ON. ON,A A, Sam Arrlvod wkhin Hold Tlme: Y qN. owA b- Short NOW Time Analysis cT] ON. OWA S, Rush Turn Arouse Tim* Requested; OrN W UWA 7. 9otllclentVdume:An'&_� QN. OwA B. Cornice Containers Used: Ja�r... Orr. Own -Pace Contskrars Used, ArN ON. ❑WA S. Conhonefe Inwd: .. OW. OWA 10. Fihered volume received kw M&WIvad last! OvN ON. r6WA 11- Semple Libels munch CDC: [7rr Ot . Oka 4=udae datWrnaAD1Anvl la %wrr- 1 l.i N caowwk era vm*M w h.- Men oMtMwr. .. ON. QNIA Ae =Wnm neetsp presame ers k.wrd W be k1 pia Ok. U WA cbff4A ce dN EPA urammendaaon. VQ& .NbmA roc. nse. W FCAo Or.. ON. I saew w _ Sam a decked for dad1kRiMSon7 101r, ON. DWA 14. In VOA Vlds 7emm Ons Vic aw 15. Trip monk Present' Ov. OW. O TAp Blank Custody Santa Preaem QYn OW. QWA Pace Trip Blank Lot 0 0 Ruwhr - Mont Notlflesdonl Resolution Flow DWI Racruwd7 r r x Person CordacrM! DatarTlma: Cmnmentd Reedulkn: SCURF Rsnlew: ow: I k 7Y 1' SRF ReNlsw: bras! riolt Nfirrrrer 1 a dlaaperrvy rlfeClMQ Nunn CareYnA C'.mP�+Pe umpw, s Dopy roan u1k her sent m Pe Name area 00WR CaAllpanon O@o t i a out of k.et Inmonsct yeswW,@. ma of W.p. Yrorwrad co.lei"ftl C r � t.. Room € 11010€ ALag # P� � Sk ii111�1111111© i L.111MIMI 11-10 1111WMEM: � © E . SEMMES It 940HEMEAM all. I' i�.■■■■■■M■■■MM�. ■�■■ev0000rie�_ ' ■■■■■■■■■■■■ ■■■■■y■■■■■■■ MMMMMMMMMM :■■■■■MM"Mas��© M■■O©©MEMMIR r' Nl�■■�■■■■�■■■■�©MEMEMMOZOMM a ■MEN ■■■■■■...■■■�.©f ■■USE ■■■r©� r:: �11-owl Client Name: IMPT6:roegh9 Project# Rx l3y37 / Where Received: �Hunta.rsville ❑ Ashewga ❑ Eden Courier. ❑ Fed Ea ❑ uP50 USPsO C1lent❑ C rani Pa Other Custody &&& on Couladaox Preardl ❑ yea no Beale lr'w;L ❑ yse ❑ no Peehlnp Natarf al: ❑ Bubblbbls Baps ❑ None Other Thermometer Used: IR T7102 Type a1 In:�.Blve None %,65 mplae on M. molrV prates. has begun Tame Cnmrmon Fectu T7 `101, No Cnrredinn 11702- Nn C.M'aniinn Carrseud Gaoler Temp.,�I C Ternp andrlc gs,eaw 6'.s>tine m a'C Blalaglwl Tissue Is FFoxen: Y.. e. WA Ganrnerhe: law end Inf iR P.pery my�p vontamea Y7/ 'r••.r A Chain of Cua Pneaant: qno QN1A 1. Cheln of Cuslady Filled Out n QNc QNIA y, Chal n of Cusiody RailoquehooL, .. ON. ONA 3. Sa rrpivr Name d signature on CGC: ON. 0" 4. So miplus Anhrad wllhin Hold Tlrnu- ON. OWA 5. Short Nald Time Anal is s72h K. QNo ONO& S, Rush Turn Around Time Re ueata d: Gvrr ONA 7. Suf iewfli Volume: ON. QW. 8. Correct Containers Und: -Pape ror4ainere Und- �.. Ow QW1, T5 IN. OWA 9. Containers intact ❑Na ❑" 10 Flaerad votLLnme racelved for Olmohnd taste OYw Oro A 71- Sample Laboa mach COG! -Includes dsloRknollplAn w Matrtr.• Oy. yo CN.oa d 12- • ` t- Sa1rV e 1ry o i, N, ox"iP rs ^Mla'W ;,~esrwn haw Dean caste, AA cordeinum reading pregervaddn am Found to 6A hm cormWarxr wah ERA reppmmar4rilo-. • voA ewbrm, Toe. cad, sum-0Ro _w M ON. ❑NA :)ND QNA My" ON. 13. 1`1A1 mA.e mwpNYq Sam tesdwAadfordschlonnation: fiye�-- OYFr 0No 'OfuA 14. Head spa In VOA Nab I s6m ' 41. & ❑NIA 15. Trip Blank Preaen Trip Blank Custody Seale Prowl Pace Trp 81ank Lot a 0 pumbasod): RYw ON. rA OYn DN. *A 10. Clierd Notlficatioil Raeofudon: FIrD tine Requl w? Y 1 N person Contacted: DmIo Irry ComrneniQ Reeoluticn: Environmental Conservation Laboratories, Inc. 1e7-A W.edv iF h Ind.w d Court gory Pic, 27511 Ph—: atf.447.3ea0 FAx, MA67.3515 Friday, November 9, 2012 Municipal Engineering Services (MUp01) Attn: Jonathan Prohl P.0- Box 97 Garner, NC 27529 RE: laboratory Results for Project Number, GL1024XAosed, Project Name/neac: Surry Co. Closed MSWIF - Dramlde ENCQ Warkorder(s): C212317 Dear Jonathan Kohl, Enclosed Is a ropy of your laboratory report for test Samples received by our laboratory on Friday, tJt[aber 26, 2012- Unless otherwise Rated In an attached project narrative, all samples were received In acceptable condition and processed In accordance with me FeterenW methodsdprocedures- Results for these pnCedures apply Only W the samples as submltted- Tie andlytical results contained In this report are in rpm pllince wrtlm NELAC Standards, except as noted in the project narrative. This report shall not be mproduted except in full, without the written approval or the Laboratory. This report Contains onty chose analyses perlorn lid by Environmental Conservation Lablorirttirl,es. Unless otherwise noted, all analyses were performed at ENCO Cary. data from outside organizations wig be reported under Separate cover. If you have any questions or require further Information, please do not rlesnate [a contact me Sincerely, CLLSUI� Chuck Smith Project Manager SCURF ReviewL.L caw: o SRF RGYIeW: Osh: to C s EnUsurefsl o WED; whanayeF Ih n a dlarapanoy arrsctlnp No* Carolina compliance rampim, A copy Gr. worn vAfl he WE to the Noun CEHNR CeraftAl*n Olam t I.a oA of hold, [noomv (xom etrye. out$4"p. 4mconect canlalm ran I he hrl.I -her arm nr 1hrr rep-n, mclvNnF Ihir rage a It w .v-xAaba-L wwTv.en cclaba. cam 6r.ae lo: MW-L MLIM•D Lb IN 02123MM &.MA & 10/31112 Sh00 R.a.M.d� 10)24)i2 avidn P.rrmeter H.ld D.I.(iimr(r) Peep hap rTlm.]F] 4ugalr Dees; Ttm.(r] --- -11 -.- . .1... i1! Ll.'0U11 .•1'1° :111170:; cu.,ID- MWi Lab 01.230-02 Smpl d: 10122r1217M Rmt"d1 10/24/11 0i:40 TPrrrm - Mold DaL.lTimafa) Pr.p Dag.lThlla[a) Malry,la twMMme[r) [;A ".: :I:: S:Ii 1Lp 1112 14:33 1111(1D12 14:33 cm-1 ID: MW-12% Lab Iy: CII017-Ql _ _U .pg.&. 50/24/12 M-00 7l.PaMd: 1012ya OS:W arem. r hold brief Tlme[aj a,.p MhllTlnl.(a) An.IrFIL D.d(Dme(.) 1. 3W.L 1a!!::'--! 1110L112 M;ap i:lti70t7 t5.a6 .gNn[LD: MW1] 1+61D: L2123L)-04 C 701241 L; 11:00 A.e.lwd: 1D124f i2 o9:R0_ _ rime r M.W D.tel Tlm.(,] Prep Mdlilme(a} An.lTrlr D.lrl it me[L] ESA _76 L1:21111 L110412 ISM li1t17017 :S - I P1.al loL MY-55 Lab M; C2 Mt?- S paanplW: 10/23112 LIM R-W.Wl 1D125112 09:40 P.remew IIoM DRe1TFrw[.] P,.p D.L.ITh2X(.) analF.iL DabalTlm.[L] 111201L7 i1P71l17 15:L6 1111170f7 15:1s GWd101 MM•if WI IDi C]F7717-0f %aPlpl.ii 10123/12 ILWA$ R lW.W: 10/20/12 O9Ay P.FMes*x TleW ael.IThne(r} Pr DedlTlme(,y A A ,6 M.1 TImO.) — EPA 3L00 111Nf12 11191/12 15:33 1:i L.rU :... r�uccv www.etteni elaa.cn ni en"t ID: MWY7 Lah ID: C212317-D4 ae.kv. Re.. 16 FI.g DF MDL MRL MC SWSL UMB M.IMC M.lef N—L.'4 "Cif =.5: '4 -Si.epa3 ., 6M1Di MW-16 1.b ]D: C712317-M M MIN FI.g DF MDL MRL x[ I.SL -1. M.iN.d Xov, Lx-4i 5 78 l 1 007'i i 51' A a UL .Pa 3W ] ClE_1VCO wvrw..nml.bs.wm O..crlptlon: MW-1 MSIM5O Lab S.mpl. IO: 1.712317-01 PA.Wl d: LOIMlL2 09:40 M.Wk: Crowd Wat& Sampl.d: 1 O12111217-00 work Ord.r: C212317 Pre}. : Sorry Ca. Ch." M90LF - Sm o* Sampi.d By: 3. M&W Cl"ou m i eh.m wry Pan moths Balk--fd4-tlACMkW gawu. Fjy umb al MDL MiD. ft"A" dLku0 ibabuad Is mats, •iYl tir nYYr ..W Y w wyY •r �w w.�.r Y• YY�..r�.r ... �+i nrvr I�r ryr•.W.M . ��r 'w 1 ••f 12 ENS CG www".nml.h..m�+ O.a.71pu—: MW4 Lb S.mpl. ID: C212117-01 IL.C.{Y.d: JWl &Ji209.40 Matrl%1 Onvq Wain Sa W d: 10l27lU 17:D0 W.rk Ord- C212317 P-J. M S1k.y C. QH d MSWLF - O.nndd. S.mpl.d By: I. ft" Claaalml Chem Im" PapaSahars ' fAi776y nYfkd.d7fe lhC 54!! ►o.1lLICatambw A.udu aW WIY 0L ML an ncmm tlatbad aaapsad 6e maims _. 13_ q1 9m tit a ...1 .. r. "aA f ".1el) 1 a1 w f.. .rM �Y. �Yro v. x.qY wn.vne Ir .�. Kwnwr. 1•e •r. n^T e..rr••4xti.1� Wyylptlen: MW-125 Leh Sample 10; C712317-03 M.trla: Ga—d W4tn Sampled: 1012V 17 15:00 Pr.1.e: SM Co. C1o..d M5WLF 9romw S.mplad lr: 3. PM Clowlal ChemlKry Palam.tem ... sxn 6,l, n„n,w+rse SAC f4U wnr.1.—Aah....m Received: 10 M12 09:40 Work Ordw C212317 aaLr4 Oka Hold mE ML au MI' sw5t dalhad do.load v MmY ..n ..y1 1 eon ..w rr U. — a �! 4 u .. — O..Cdptl—: NW13 L.h Semple 1D: C212317-04 MatHx1 G—i W.I. $.mplydt 1(04412 11:00 Pm)-t Sum Co- Closed MMF • &a.nNe Sampled my:). P(Wy Gawlwl Chem"Pammetan P"rq—fAv—IYW{AC i911 ....rd rc.s a..ebild .XIM4� I=N.e47•e1 - www-.nea7ah.-mm Received: 1g1I6J12 09: 40 WWN OMv: C1 I Z)17 SMAN an Hdd CE M" tl8L EI MnL M,1 ia.pani at Yale ..1. w1 ! rod. nV lief flu if 1r � ilr,Ne+rww.+X lerw.u�e�u.rrxdga. ira.te'r...!Fl.r un w ryrerwW rJ 1. ,1 .—m .--u--w w— -.M—e wr.e Peke n �r! ]] I'.ke 7..I 1: rrww.encal.kcwm p.acrlpllrn: MW-15 Lob B.mpl. IP1 C 712I 17.O5 R.cslwd: 10126f1209:.0 Matr9c rro wid Water Sampl.d: LW23112 12:00 Werk Ordrf C212117 Prnj.et: 5-ry Co. Cbxd MSWLF B pnide S.mpl.d ay: 1. Vry N Cl.sslcal Chem&" ParamaGn VOLv Ch`cWKV-4w P'K "I; AsshmL-LLUAsmWrl am&= an Q= O! im ML6 2S.Ih.d de.m.k E! 212101 —r—nnl- can N -1 1 00f. afC• M "IMO IIAVR II:I. ■R 11. rr+r nYY. n.le W r+ek r •rww. YI tm .ilnalae..r1 ^w err r �>• n M I'.gcRnf Q www.rloelak..00m OrcrlptIon: MW16 L.D Sampi. ID: Ci12117-06 R—OWOe: IOf26f1209:40 Mauls: C+c. V wales Sampled, 10123/32 WAS Week nrdWt C2 t2317 Pr.). : Sir Co. U.-d MSWIF 9nn.dr S.Mpl.d Op I Phis CFaeslcal Chem Wtry Pa r.metem - E1N'U Gry:r-rh.+>x+Nrr fAC 5Y11 4ufrd tra. k..hw E...0 Das Umb ar MM HILL. Mizhu tl.6aed a..hwd lb maim r,..L. nxx..7•.1• ..1. -1 i ooze .1. Nr +.loon unw un — maI r.Yr �r.11e MM m m. r.Nr r IrN+a m trr kerwrar. w n+r .'rI r rN.r � n ti 1'rpr R of I ] ENC w.lrw,en pP[a 6e. cam WaLt7i COP2TRVL oas.lul n,emterry Peremet er. - q�euey I:ontra[ RII y; 223027 - NO A?fP W.ek ("SM22-RLYI) .ao 5 :.off ,Yd: 11I0172e1a 12:16 spla. U. .11 R Reo Rlr Raul! MP.l. Unlfs Lewl A-ult Yp1lG Uwfft Rm LMIH Netm UM[2330n 27�1) Reiland iAaoym! iljd[1M1212i 33 99*0 1fa %mc RPO IWufL MRL Unit• L.wt Itteul! %RIC U.16 pP []Mt New 2 w 1 A IN Melnx SpIM• t22]ov2 ]-n52y Prepared a "Iyrm: 117 "I1 pn-yi 5•we•: CI12 a 1�-tlt 7p" Temp w'"' RPo Mehl. [tewtt Flea MRL Vnff. LeM R-09 %RIC WOW RFD Well hel.e wM•w f 0 P W q I. u e)I. ":, b Ilu M•tne SPIk. D-P[vPW2'1-2ei02] p.epe•ed a aneryxed: I tIV NL2 W:" S.um: C21.xx1-or mp1b w— %me ■IC •aerYM Re It Rea NPIL wd" [reel RMWt wee LbNg "C' U Wt ".w vrmU� r. IN v 21­ w lin . r W f MRL )-at T'agp I I Pr 12 FJV0:10 www.en m[a6s.00m The anafyte was detected In the associated nwbod blank. The sample was anaiyxed at dilution. The reported value is between the laboratory method detection Ica (MIL) and the latk7tatory method reporting iknk (MRL), adjusted for actual sample PreoaraTOW data arid ma6ture [omentr where appllca ble. The analyze was analyzed for bit not detected to the keel shm", adjusted for actual sample preparation data and moisture Wntent, where apphLaNe. The concentration Indicated for this analyte s an estirmted value above the calitaation range of the uistmment- T%value is considered an estimate, Method ReWIng Limn, TM MRL is roughly equivalent to the practlraf quantbOw Iph1C (PQ1,1 and is based on the low point of the callhration CO", when a0kabk, sample preparation factor, dilution factor, and, in the case Of Wl san)pfes, moicturfl content. Resull 6 estanated due to paSnne resI in the assocated method blarkk, �.s ��[�'s ENMRON ENTA!N$ COEwAnoN LABORATORIES CHAII-OF-MTO0Y W-CORO w *AncaFabsAom �...e. �. c=� w my car.iex.• le w:ae•. .,;.e„x... ..n s.n= .raw.,, nrRrnsa Mm�,.xw rye � a �- - •- _— ' �i� _^�570. lark �l"L 'DES 4 Riif `t �-3P wwrti � w rw.•,�wr f +� ' i .. ur�.lw