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Home My WebLink AboutWI0400176_W/ CORRECTIVE ACTION UPDATE_20160324i tENR USE ONL`YY El Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event #: ANC DENR I I Environmental Monitoring Division of Waste Management - Solid Waste Reporting Form Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6). Instructions: Prepare one form for each individually monitored unit. Please type or print legibly. Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing condition, etc.). Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i). Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646. Solid Waste MonitoringData Submittal Information Name of entity submitting data (laboratory, consultant, facility owner): Municipal Engineering Services Co., PA Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: Jonathan Pfohl Phone: (919)772-5393 E-mail: jpfohl@mesco.com NC Landfill Rule: Actual sampling dates (e.g,, Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006) Surry County Closed C&D and 237 Landfill Road 86-02 .1600 May 27-29, 2015 Closed MSW Landfill -Mt. Airy Mt. Airy, NC 27030 July 20, 2015 SW-4 (VOCs) Environmental Status: (Check all that apply) ❑ Initial/Background Monitoring FX Detection Monitoring ❑X Assessment Monitoring FX_1 Corrective Action of data submitted: (Check all that apply) Groundwater monitoring data from monitoring wells Groundwater monitoring data from private water supply wells ❑X Leachate monitoring data ❑ Surface water monitoring data Methane gas monitoring data Corrective action data (specify) MNA parameters on 7 wells Other(specify) Notification attached? No. No groundwater or surface water standards were exceeded. X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. Certification To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Steven R. Gandy, Ph.D., P.E. Senior Project Manager (919) 772-5393 Facility Representative Na e (Print Title (Area Code) Telephone Number ®_ Affix NC Licensed/ Professional Geologist Seal P.O. BOX 97, Garner, NC 27529 Facility Representative Address C-0281 Date ` ��yg49fffsg®� ®® OFFSS®-0 ® /O9®� 3r®2d NC PE Firm License Number (if applicable effective May 1, 2009) Revised 6/2009 Semi Annual Water Quality Monitoring Report with Corrective Action Update Prepared for Surry County Closed C&D and Closed MSWLF, Mt. Airy Mt. Airy, North Carolina May 2015 Permit Number: 86-02 MESCO Project Number: G15024.0 Municipal Engineering Services f Compasry, PA. Garner, NC 1 Boonq NC P.O. BOX 97 Municipal Engineering Services Company, P.A Garner, NC 27529 Gamer and Boone, North Carolina License No. C-0281 TABLE OF CONTENTS SECTION Introduction................................................................................................................................................................................................................................................................................Page 1 Background Page 1 SamplingProcedures......................................................................................................................................................................................................................................................Page 2 FieldParameter Data......................................................................................................................................................................................................................................................Page 2 LaboratoryResults.............................................................................................................................................................................................................................................................Page 2 QualityControl Samples.........................................................................................................................................................................................................................................Page 3 GroundwaterSamples...................................................................................................................................................................................................................................................Page 3 SurfaceWater Samples...............................................................................................................................................................................................................................................Page 3 CorrectiveAction Update........................................................................................................................................................................................................................................Page 3 MNA Analysis (AOCs Northern, Southern and MW-11).......................................................................................................................................Page 3 Enhanced Bioremediation via Substrate Injection (AOC Southern and Northern).............................................................Page 3 MW-11 AOC Investigations...............................................................................................................................................................................................................................Page 4 Groundwater and Surface Water Characterization.............................................................................................................................................................Page 4 Findings............................................................................................................................................................................................................................................................................................. Page 5 Closing............................................................................................................................................................................................................................................................................................... Page 5 FIGURES TopographicMap with Site Location..............................................................................................................................................................................................Figure 1 Potentiometric Map of Uppermost Aquifer w/ VOCs Detected Above 2L Standards...........................................Figure 2 Total VOC Concentrations Pre/Post Injection Comparison.........................................................................................................................Figure 3 Bromide Tracer Concentrations Time Series Graph and Table..............................................................................................................Figure 4 Total Cumulative VOC Concentrations Time Series Graphs/Table................................................................................................Figure 5 TABLES Groundwater Monitoring Well Construction Table.......................................................................................................................................................Table 1 Field Observations of Monitoring Locations........................................................................................................................................................................... Table 2 FieldParameter Data Summary.................................................................................................................................................................................................................Table 3 Samplingand Analysis Summary............................................................................................................................................................................................................Table 4 Detections Above SWSL, GWP, 2L, or 2B (Appendix 1).................................................................................................................................Table 5 MNAParameter Data Summary.................................................................................................................................................................................................................Table 6 Hydrologic Properties at Monitoring Well Locations.................................................................................................................................................Table 7 APPENDICIES Laboratory Analysis Report and Chains of Custody.....................................................................................................................................Appendix A Field Sampling Parameter Data Sheet(s)......................................................................................................................................................................... Appendix B Boring Log and Well Abandonment Record(B-11R)..................................................................................................................................Appendix C License No. C-0281 CIVIL/SANITARY/ENVIRONMENTAL ENGINEERS Municipal Services SITE PLANNINGISUBDIVISIONS SOLID WASTE MANAGEMENT Engineering Company, P.A. SUBSURFACE UTILITY ENGINEERING (SUE) March 24, 2016 Ms. Jaclynne Drummond Solid Waste Section (SWS) Division of Waste Management North Carolina Department of Environmental Quality (NCDEQ) 2090 US 70 Highway Swannanoa, NC 28778 Re: Semi Annual Water Quality Monitoring Report with Corrective Action Update Surry County Closed C&D and Closed MSWLF, Mount Airy Permit No. 86-02 MESCO Project No. G15025.0 Event Date(s): May 27-29, 2015 Dear Ms. Drummond: Introduction On behalf of Surry County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this Semi -Annual Water Quality Report with Corrective Action Update for the spring 2015 event performed at the Surry \ County closed construction and demolition (C&D) and closed municipal solid waste landfill (MSWLF)-Mount \ Airy. NCDENR Solid Waste Rules 15A NCAC 13B.1632 requires that Surry County provide this report to the NC Solid Waste Section (SWS) on a semi-annual basis. This report documents the quality of the ground and surface waters during this monitoring event performed on May 27-29, 2015. Surface water point SW-4 was re -sampled on July 20, 2015 and tested for VOCs since the laboratory lost the samples originally collected on May 28, 2015. Laboratory analytical results indicate volatile organic compounds (VOCs) in concentrations in excess of SWSL and 2L Standards continue to persist in samples collected from five wells that monitor the uppermost aquifer. The surface water samples collected from the local discharge feature remain unimpacted. Corrective action to remediate VOCs in groundwater is ongoing within all three areas of concern (AOC) as defined in the Corrective Action Plan (CAP) as Northern, Southern and MW-11 with updated information presented herein. Background The Surry County closed C&D and MSWLF, permit 486-02, is located at 237 Landfill Road in Mt. Airy North Carolina. The site location topographic map is depicted in the attached Figure 1. Prior to becoming a C&D landfill the site operated as a MSW unlined sanitary landfill that consisted of two units. The northern unit was closed prior to October 1991. The southern unit is comprised of two contiguous portions. The first part stopped receiving waste prior to October 1991 and the second part stopped receiving waste prior to January 1, 1999. Both portions of the southern unit were properly closed with a low permeability cohesive cap per the Transition Plan. The top portion of the southern unit served as an exclusive C&D landfill until prior to June 1, 2008 at which time it was properly closed with another cohesive cap in accordance with the Closure Plan. For continuity, both the northern and the southern units are monitored and reported together. Water quality at this facility has been monitored at least semi-annually since 1989 with historical data available since 1994. This event was performed in accordance with the NC SWS rules/regulations as promulgated in 15A NCAC 13B and as a condition of the post -closure portion of the permit to operate. PO Box 97, Garner, North Carolina 27529 (919) 772.5393 PO Box 349. Boone, NC 28607 (828) 262-1767 As specified within 15A NCAC 13B.16320) and the SWS Environmental Monitoring Report Form and recent SWS issued memorandums this report contains sampling procedures, field and laboratory results, groundwater and surface water characterization, and findings. A table of detections compared to Standards, field data results table, groundwater flow directions/rates table, field observations of the monitoring network table, a potentiometric map of the uppermost aquifer, histograms of historical detections, statistical trend analysis, laboratory analytical reports with chains -of -custody (C-O-C) and quality assurance/quality control data. Sampling Procedures The water quality monitoring program, current as of this event date, includes sampling locations and parameters as outlined in the Water Quality Sampling and Analysis Plan (SAP) (DIN:18936) dated April 30, 2013 and approved by the SWS (DIN: 18938) on May 10, 2013. Monitoring locations are shown on the enclosed potentiometric map (Figure 2). MESCO personnel collected water samples from 20 downgradient groundwater monitoring wells (MW- 3R, MW-4, MW-6 through MW-11, MW-12S, MW-12D, MW-13 through MW-23), one background well (MW-1), four surface water locations (SW-1, SW-2, SW-3 and SW-4), and the water supply well (SCALEHOUSE) that serves the facility. Data from two surface water points (SWN-1 and SWN-2) designated in the SAP for the adjacent Subtitle D Lined MSWLF are presented because this local discharge feature is shared by both permits. Quality control measures implemented during this event included the quantification of potential artifact contaminants via equipment (EB), field (FB) and travel (TB) blanks. Samples were not analyzed from the six injection wells (IW-1), (IW-2/MW-2), (IW-3/MW-3RS), (IW-4/MW-4), (IW-5/MW-5) and (IW-6/MW-8) since they are exempt due to the presence of injectant residue which would yield unrepresentative water quality results. A summary detailing the construction of the water monitoring wells is presented on Table 1. The function and integrity of all monitoring locations were visually evaluated and no deficiencies identified as documented on Table 2. The depth to water in each well was electronically gaged prior to purging to quantify the static water level elevation. Low -flow pumping methodology or bailing was utilized to adequately purge the wells to a minimum of three times the volume of standing water in the well or until dry. Surface water samples were collected from Stoney Creek discharge feature at previously designated locations. During well purging and surface water sample collection the required field parameters were recorded. The samples were then placed into laboratory -prepared, pre -preserved containers via a new disposable polyethylene bailer. Samples were collected, kept on ice, and transported to a NC - certified laboratory under proper C-O-C protocols within the specified hold times for each analysis. Field Parameter Data Stabilized field parameters were recorded during purging which included depth to water, pH, dissolved oxygen (DO), temperature, oxidation reduction potential (ORP), specific conductance, total dissolved solids (TDS) and turbidity. The field parameter data indicates the monitored groundwater is slightly acidic, low DO, with relatively low specific conductance which is generally consistent relative to each other and congruent with data historically reported. Field parameter data recorded at the surface water locations were neutral in regard to pH and low specific conductance which is consistent with uncontaminated water. A summary of the field parameter data is presented in Table 3 and the field sampling data sheet is enclosed in Appendix B. Laboratory Results Pace Analytical Laboratory (PACE) of Huntersville and Asheville, NC performed the laboratory analysis of groundwater and surface water samples for the total recoverable constituents listed in 40 CFR Appendix I. Pace analyzed samples collected from six wells for select monitored natural attenuation (MNA) parameters. Additionally, Pace reported bromide levels in samples collected from four wells to assess migration of the tracer which was previously injected along with the remediation substrates. A sampling and analysis table summarizing the locations, constituents, and methods is presented on Table 4. Laboratory results and C-O-Cs are contained in Appendix A. 2 Water samples were analyzed to the laboratory specific Method Detection Limits (MDL), which are quantifiable at or below the current Solid Waste Section detection limits (SWSL). Table 5 summarizes constituents detected in groundwater and surface water samples that attain or were above the current SWSL, Groundwater Protection Standards (GWP), North Carolina Groundwater Standards (2L), the applicable North Carolina Surface Water Standards (213) for a class C waterbody, and Maximum Contaminant Levels (MCL) also known as "Federal Primary Drinking Water Standards". Quality Control Samples Methylene chloride was detected in quality control sample (EB); However, methylene chloride was not detected in any other samples therefore the field or laboratory induced artifact contamination is non -consequential. Groundwater Samples Total metals were not detected at levels above their respective 2L Standards. One or more VOC(s) were detected in quantifiable concentrations (> SWSL) above their respective 2L Standard in samples collected from four monitoring wells (MW-9, MW-11, NM-15 and MW-16). The majority of the monitoring locations that were found to contain VOCs included a mixture of dissolved phase aromatic hydrocarbons and chlorinated aliphatic hydrocarbons. The only constituents detected above the EPA established maximum contaminant levels (MCLs) primary "Drinking Water Standards" were vinyl chloride (MW-9, MW-16) and 1,1- dichloroethene (MW-15). A site map depicting the concentrations and estimated horizontal extent of VOCs that exceeded the 2L Standard during this event is presented on Figure 2. The on -site water supply well (SCALEHOUSE) continues to lack target detections in exceedance of current groundwater or drinking water Standards. Surface Water Samples Surface water sample SW-4 contained total copper and total zinc in levels above 2B Standards. The source of the metals as detected in SW-4 is believed to not be anthropogenic rather a product of erosion of natural deposits. Neither copper nor zinc were detected in any other surface water sample collected either upstream (SW-1, SW-2, SW-3, SWN-1) or downstream (SWN-2) of SW-4. Corrective Action Update Groundwater remediation continues to be implemented per the approved Corrective Action Plan (CAP) at the three designated areas of concern (AOC) (Northern, Southern and MW-11). A Corrective Action Evaluation Report (CAER) (DIN: 19361) was submitted on May 1, 2013 which demonstrated that the plumes continue to decrease and was approved by the the SWS on July 24, 2013 (DIN:19366). A historical summary of corrective actions performed to date are briefly presented in the following sections. MNA Analysis (AOCs Northern, Southern and MW-11) Semi-annual MNA monitoring of a subset of 12 wells for the full suite of SWS recommended parameters was initiated on May 18, 2010 and performed for four consecutive semi-annual events to establish a baseline. A revised SAP prescribing 7 wells with various targeted MNA constituents was approved by the SWS and initiated during an event performed in May 2013. MNA monitoring was performed during this event for the parameters and frequency as listed in the current SAP. MNA data presented in Table 6 continues to indicate that favorable geochemical conditions exist for continued natural attenuation. Enhanced Bioremediation via Substrate Injection (AOC Southern and Northern) Per the SWS approved Corrective Action Plan enhanced bioremediation via substrate and tracer injection was initiated in the Southern and Northern AOCs in accordance with requirements outlined in the Injection Well Permit Application and Well Permit No. WI0400176 (5/6/11) in an effort to reduce low level aliphatic and aromatic chlorinated hydrocarbons in groundwater to below the 2L Standards. An edible oil substate (EOS)-water emulsion with sodium bromide tracer was injected into four wells (IW-1, IW-2, IW-3 and IW-5) on November 2-3, 2011. Similar substrates were injected into monitoring wells MW-4/IW-4 and MW-8/IW-6 on October 24-25, 2012. Details of the injection events are provided in the Injection Event Record dated November 4, 2011 and January 10, 2013. As directed in the UIC Injection Well Permit renewed on April 15, 2013 semi-annual post -injection water quality monitoring of wells located downgradient of viable injection points (MW-3R, MW-7, MW-9, MW-12S, MW-13, MW-14, MW-15, MW-16, MW-17, MW-18, MW-19, MW-20, MW-21, MW-22, MW-23) and upgradient background well MW-1 was also performed in conjunction with this semi-annual event. Total VOC concentrations reported during this event were lower at all locations when compared to the respective moving averages of the five events preceding injection in the selected wells downgradient of the injection points (Figure 3). Evaluation of injection wells (IW-1, IW-2, IW-3, IW-4, IW-5, IW-6) continues to indicate that a considerable amount of white highly turbid (>1,000 NTU) viscous residual organic substrate and its byproducts remain in each of these wells rendering them unsuitable for representative water quality analysis. The viscosity of the water in the injection wells during this May 2014 event precludes sample collection as either a bailer will not descend or the check valve fails. IW-1 was verified to not be a viable injection well as less than 3 gallons of substrate was able to be injected into the low permeable fractured bedrock and injectant levels have remained above static conditions for over a year. For all intents and purposes IW-1 injection did not occur nor will be possible in the future. In an attempt to track migration of injectants bromide was targeted at MW-13, MW-15, MW-16 and background well MW-1. MW-16, located 86 feet downgradient of IW-3, is the only location exhibiting tracer levels which may potentially indicate injectant communication. Based on the average linear velocity rates of IW-3 and MW-16 reported since injection the injectant was expected to reach MW-16 in May 2012. Bromide concentrations at MW-16 have been variable but remain elevated compared to background levels (Figure 4). Calculations performed following injection indicates that reported levels of bromide injected was insufficient to provide clear evidence of migration within the uppermost aquifer. MW-11 AOC Investigations The CAP designated MW-11 as an area of concern due to detections of VOCs detected in exceedance of 2L Standards. MW-11 is located within the compliance boundary near the northern property line which is hydraulically upgradient of the closed northern landfill. The northern landfill closed before October 1991 which was before adoption of NC Section .1600 rules that address assessment and corrective action. VOCs have historically been detected in excess of the 2L Standard at MW-11 which include a mixture of aromatics (fuel hydrocarbons) and chlorinated hydocarbons (solvents). Over the past 3 years (6 semi-annual events) the only constituent detected in excess of 2L Standard and SWSL was 1,2-dichloropropane. The CAP prescribed that MNA and enhanced biodegredation to remediate MW-11 AOC. MNA has been performed continuously semiannually at MW-I I the past 5 years. Enhanced biodegredation has not been initiated at MW-I I AOC since hydrogeologic conditions relative to the source and property boundaries preclude it as an effective technique. MW-11 is positioned hydraulically upgradient of the source and is within the review boundary. A well was attempted to be installed at the property line 110 feet north of MW-I I on January 26, 2015 to delineate the extent of contamination. The potentiometric head at B-11R was expected to be at 25 feet (1132 ft amsl) but the boring encountered very competent rock at 9 ft and remained dry to 55 ft. (1102 ft amsl) for over 48 hours. The boring was abandonded per 2C Rules with records in Appendix C. Groundwater and Surface Water Characterization A potentiometric map constructed from water elevations taken from the uppermost aquifer which consists of both saprolite and the hydraulically connected upper portion of the fractured bedrock system is enclosed as Figure 2. Groundwater flow directions and velocity rates were calculated through modified Darcy's equation as shown on Table 7. Consistent with previous events the groundwater apparently flows in a general southeasterly direction towards the tributaries of the Ararat River. The calculated average linear velocity of groundwater indicates an approximate average of 825 ft/yr in the wells screened in regolith and 849 ft/yr in the wells screened in the bedrock. The consistent disparity in flow rates between wells is indicative of heterogeneous geologic conditions and/or a product of the limitations of the linear velocity equation when applied to anisotropic conditions which are characteristic of the geology of the Piedmont. Streams located within the facility boundaries were observed to be of moderate volume and flow with low turbidity. 4 Total metals were not detected in any sample above 21, Standards. The on -site supply well and the surface water points remain unimpacted as indicated by the lack of detections in excess of the applicable Standards. The on -site supply well is not considered potable thus bottled water is provided for consumption and "Non -Potable Water" warning signs have been erected. One or more Appendix I VOC(s) continue to be detected in quantifiable levels above the 2L Standard in samples collected from the uppermost aquifer at four locations (MW-9, MW-11, MW-15 and MW-16). All VOC concentrations remain within their own respective historically identified range. Qualitative evaluation of VOC concentrations indicate a decreasing trend over time and distance from the landfill. Total cumulative VOC concentrations during this event decreased at all locations, except for MW-7 and MW-9, when compared to their respective five event averages preceding corrective action (Figure 5). Results of statistical temporal trend analysis, using Sen's Slope Estimator at a 95% confidence level, indicate that none of the individual well's cumulative VOC concentrations have exhibited a statistically significant increase and the Southern AOC and cumulative site -wide levels continue a decreasing trend since corrective action was initiated 5 years ago. The area of the uppermost aquifer beyond the compliance boundary containing quantifiable concentrations of VOCs in exceedance of the 2L Standard during this event is estimated at 0.0 acres in the Northern AOC, 0.0 acres in the MW-I I AOC and 3.9 acres in the Southern AOC for a total facility wide area of 3.9 acres (Figure 2). This is an estimated 52% retraction of facility -wide plume area (from 8 acres to 3.9 acres) compared to when corrective action was initiated 5 years ago. Evaluation of the most current water quality data continues to support assertions drawn in previous reports. Corrective action will continue except enhanced bioodegredation will not occur at AOC MW-I I as was planned. A few VOCs persist in the upper portion of the aquifer but concentrations are decreasing over time and distance away from the landfill. The local discharge features which are all located within the property boundaries remain unimpacted. Data continues to indicate that the plumes within each AOC have stabilized and/or decreasing and there is adequate evidence that natural attenuation is actively occurring beneath the facility. Closing Water quality monitoring and corrective action continued with sampling performed again in November 2015. If you have any questions regarding this report, please contact us at (919) 772-5393 or by email at jpfohlginesco.com or sgandy@mesco.com. Sincerely, MUNICIPAL ENGINEERING SERVICES CO., P.A. Jonathan Pfohl Environmental Specialist Enclosures cc: Mr. Dennis Bledsoe Surry County &R.9y, h.D,P.E. Senior Project Manger Figures Topographic Map with Site Location Surry County Closed Unlined C&D and Closed Unlined MSWLF, Mt. Airy fl V 1000 0 1000 2000 ROAD CLASSIFICATION Primary highway, Light -duty road, hard or hard surface.. ...... improved surface....._..___.—__ Secondary highway, hard surface ........ Unimproved road.-_______--- O Interstate Route E3 U. S. Route n State Route L3 / Eananu Koaa Mount Airy, NC 28621 Lat: 36-26-30.065 Long:-80-34-15.314 Northing:983356.18 Easting:1537885.48 GORDON p,, R<R T z 0 K RUN LV C4 r 0 Surry Co Property Line • Closed Unlined C&D Landfill • Closed Unlined Sanitary Landfill O Active Lined MSW Landfill FIGURE I 237 LANDFILL ROAD N 0 W OR FORMERLY 0 WN ED B Y / / I ": JOHNNY COX 1I1;1 / I II /■ \, / I' 1, I IW-6 1 t \ 1045.19 - II: I In 11 : ,1\ l ■ RECYCLE AI1EI-- a 1/ -"A 120 - - ' % ■ + / \\ 1'�10 1100 r 109p BEFORE MSWL TOBER 9, 1991 1080 I� - II' 1 "II 1 f - 1070 ill „III - s V\:, **\ B-11 R DRY < 1102 SCALEHOUSE MW-11 (FACILITY NON -POTABLE WATER SUPPLY WELL) 1,2-Dichloropropane - 1.8 ug/I MW-11 \ 1128.45 % \ % "/ / I I lf/ % ,- ,, 1�II; ,-- / I \- \ / / / / _CO Jk,\ —— y ss/�/ �, li \\ I II `ir,,,5 Z`ALE HOUSE -' / ' % / / a I \ 1 \_1'\/ // / II \ \ it :/♦♦♦ / / i / -I- \III \\ `\ I p _ - S, I -\�♦ * /I 1 , 11 ' j III \ II �' - \`-/ \\\ I $ � ----I I III\ \\ II Y /- I 1 \❑ 11 I\\I \\ II \\ 1 --' i It I ' '<, ACTIVE \\� I ,_ ___ 1 \ 1 \ I _ I I \ \\ LCID\`\--- \ - `---- • I\I \\\ i II i I 11 `\ `I\` �`--- I '\ \ Ill I I II I I �\\ , \}�---�--'- � \ /'III / / II I i / , \\ - -- ' •-------- "-\1y \i / / III % / 1\ % / I \ \ 1 t , ,\ / , / I / / / // / / t MW-9 n-\ \\ I 1 Ill111111 1060 -- - // - y- -- ' -,, '' %I ,___r�, 1060.12 \ 11 +.�1_ _ 1� I ,y// / ,- 's /- /' ,/ ' ' MW-9 \ \ \�, \ \ \ \\\\ \ - --':7- _--r _- %I t / / II / 1 1,4-Dichlorobenzene-6.2ug/I \ \ I \ \ \ \\\\ \\I k _- -- --__ L - _-� , /,' / -� -- --\ \ \ \ -_- - -` \ \ �� \ \ / / / / It,- /' ♦ , / /' // / II 1 I ` � Benzene 2.8 ug/I \ \\\ ` _- �-- �''--I' _- - _ \ \ \ , / / /' / / Vinyl chloride - 12.3 u /I 1062.29 \ \ \ `` \ \\`\\� \ \ \ _ \ \ \ \ \ I \, _ -- _- - -_ - ,i ,, , ,- 17 - ---- ' -J--- ' 'AC ESSi ] - �r - ----- _- --- - - - -- NON\ X -,� /pia- �� 1 1 1 1 I I I 1 , i /' ♦' Ti ,'' / / ,/'. 4// / / / / ' T / /' / 1I -- ' 1108.78 SW-2 -' _--'- _ _ ` , I /'' COVERED , I I I ? 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'/ / ' / / / ; / / / /I / / / \ 1022.48 \\\ �/ \\\ - •,`\1 \\` o \\\\\,\ ,,/;, ,I ,/ / /► I I '\ ' I I MW15 SHA WNA SUMMERS \`\ K \ ,/ ly(�Px,��j�! \ - I'll�,C'y,�` \\ \ �\ . 9� ' - ,/ /' /'/ /" -_, - 1 I // /// I I I I I \ 1 \\ I \ '`__/ Benzene - 1.6 ug/I \\� �\� \ \\ ,« \\, ♦ �\ \\` '' '' - /'-,'' %'/',/-' /` / / // // /: ' I I l \\ \\ 1 \\ \\ ` ___--_' Vinyl Chloride - 1.5 ug/I \\\ \`\ \ ♦ \ ZZ \\`fie\{@�; \\`\ \\ 0 '-- / h \ 1\II\I\I \I \` \ \\ / V %\ �,\\ \ \ , �/ ^ ` �\� 9 -' �'' //'''' ''/ ' L,L�I I I tl \\ \ `\ \\ \\ `_ __''--- = 1,1-Dichloroethane - 13.6 ug/I 1 \ / \ \ _ _ \, \ \ \ 0 / / / \ \ \ \ _ \ IIII , \ \ % `\ \ \\ \, -•�-� `N '\`,\` \\\ \ `� __ /''-' / / \ - � I I \ \ ` __\ \`\ \`- _-----'_ \ \1 \ ;%,--_=\ \ `�' 95p _-,_- --'', ,-i',/ -'- \\ ,_--___-, _-- _==_____---------------- EXISTING TOPOGRAPHIC CONTOURS 1©LO i /i, / r'' l \gyp a\ -_ _-- , ---��/ ' ` ` `-___- - . . ___ ----- I /,//// , 1 tIt , \ \, ,\ \ • �_ ` ,\ , / -- - - ' _____ - �' EXISITING ROADS 1 1 ///////// I / \ `\ ♦% \�� \ , ♦♦ I _-\--- -`- \\ \\ 1 //// ////// , `\ \ \\ \'� `\ \ \\ ` `,: ` _ _ \\ ' l -'---m - - - `- //////,/// 1 ,� `-\,�\\MW_1g ;// 1 - _II -II -II -II -I • ESTIMATED WASTE LIMITS UNLINED MSW &/OR C&'D V IN - ?7"'/''' QJ ■ `,ilk;�1`; ` e .:••■■ ■••\'� , , �,, _ ��=j�"' _—___; __________________. 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III II , ,- ' -_-I I I 1 / / \ \\ \ , \ ,, // / / / / \♦ -� / / //// \ / \\ _ _ / / ;= ;/ , —1090 ------ EQUI PO TEN TI AL UPPERMOST GROUNDWATER CONTOURS \,, \ -, „ / / _ - . IIII / ,_ _ 1 / \ / ,� // / /�/ I� hic- -,� \_ ii,,,�,_ / IIII ,-, i- --_-_, i i / - -- ,/;,/ ---- : STREAM/CREEK/RIVER / / _�� —_, - // /// / / / _ Ill /i / / , /-., I .1 \/ _ , �,, / \\\\ - -// I l / ll // r<.\ / ,, / �_ - -/---1~_/ ,- �/- ,- ,- - -_-%i///, , / / ___ ACTIVE LINED _y, . I `1 / / _--- =-- :;;;;= ;;= - , , , ,--__,- ' ' '1 - " - -'/ " ' O WATER SUPPLY WELL (FACILITY CONSIDERS I T NON —POTABLE) \\\` " , �./! IIII / / /, I 111 ♦ / / r / / , ,ii'-'-''- i--i'''- i / ._ PHA � �\\\\ ( / / r l/1 / /l11/* ��, / - -i, -, -'i' / / -/ / / i ' " / l I / // // ♦♦■*/ ,-,i' i IIII-,-i-/ �/ /, / i IIII , // \ \ \`\„\\IIIII//%// /, /,,I ,,, //,/ / ♦♦ \♦♦ �, IIII , , "/ // / / / / / / / / / \ / / /-ii -// / / // / / / / / , / \II I1/1//// //ir / // I// IIII/ •1 I / ♦ -\-- i/ IIII/-IIII-i i/� ///"//// /,,,/ /',' -9s6� ` j\�� \ ,1 //�,,,/ /��„%/ /////,/// ///I/ J � ••'�• 11 ■ ■/to '/-\_-',' / / // //,,/ // / / / / / 986�'��V �1�s :i� / ,,, , /, /„ ///// / , / ■■EE.I r /' _ ,- ////'/'''-', --'=-" - ' -'-' r-- SW-3 SURFACE WATER MONITORING POINT /, / / / 1% 1 / / / / / / / / / / / / / / / / / , , / / 9e4- /,% /////IIII///l P `1 / III `\ \ ( \\--''-///////////'/ ,/ / /% / / (---_-, ,// / / I I I / I \ �__� \ / / / , / / / ,o g/ \ ,/^ I I \t \ll / \; I I / , \ \ \ \ \ \ r-i �/ /// / / / /, / , / , / , / / / / w / \\ ,\\ \;\ � --\\ \ , \ \\ 1 \ 1, 1 IIf// l/ , / r , / , r / , _------1 MW-10 MONITORING WELL \ \\ \ � - ___\`.�\ \\ �\\ \\ \ \ ` \\\ \ \ 1 f 11 1 I 1 1 / / / O / / / _ \ \ \�,\ "\\\ \ _ \ \\ \\ I t Il l l l 1 I / `'------1 IW-2 I� INJECTION WELL (NOT SAMPLED DURING THIS EVENT) - �. •\ \\ \\ \ ♦�\ \ J` `�\\\�_\ �\ -\,'-\ \\ I \%\\\ `I I I I I I 1 1 1 1 1 1 / I / ( 0� \ ' \ \ ` \\`\ `\ \ \\ \\\`\�,;,," �,� ��\ \\`\ \ \\ \\\\\ 111\1\11 I 1 I 1 I� \ ', t\ \� \, � - 1 \ \ \ ♦ ) \\ \\ \\\\\ \\ill\`\\ \- 1 `\ `\ t, \O\ \\III \1�11 1 IN \ \\ \ \ - / \ \ `\ • -' /' \\`\ \\ \\\ �\\'\ 1\I I 1 l` `-\ \`\ \, \ \\\ I I 111,�,\ \ 1 % ; 1 \ CP \ \ \ \ 1 /----_-'1 \. .- / \ \ \I\\\\\\\\, \ \, _\\ `,\1\11 t'IJ'III \\`\ ; `\ `\ `\ � �,--__N 936.43 GROUNDWATER POTENTIOMETRIC ELEVATION (AMSL) ♦ - 1 \ 11\111\\\\ t `` \\ I It\ 1 I\l \ \ \ \ \ \ l- / - '\\ \ \I\\\ \� \\ I I '`11' `\\\ \ \„'= -- *NOTE: ELEVATION NOT USED FOR CONTOURS \ ♦ e t \\ \\ \\\ \ \ '' \\ I II11 1\ 1\11 \\ \\ \ / _--, \ ♦♦ t I \\\ \\\\\\\\\\ \ , \ \PPP\ ,�\ \ \ \ I l t 11 \ \ \ \ \ \ \ `\ \\ , " 1 \\ ♦ 1 SEDIMENT BASIN ---- , \ \ ♦® t \ \\,\\�\\`\\\ \\ `- 1 \ I l l It 1 I I \\ \ \ \ ` \ \ \ // /'--\ -- ,' `♦♦ _ _ 1 r , \\ \\`` \\ \ ,-1\44WN l 1 l 1 t l � ;,1 t\ \ \\ \ \ \ \\ \ \ \✓: '/-- 1 i`♦ --------------` \ \ \ t \ \ \ \ \ \ \ \ 1 I O`\� \ , \ I\\\\\ \\ \\ \ \ \\ r \ MESON■■■♦ \\` __ ------ , r`�\\`\\\\ \ ( III\\\\\ \\ \\ \\\\ \`-=--,' i ji�EE` __`---_ ---- -- \ \\ \ 4 I__ \ 1 \\\ \ \ \ \ ----+------ -- , _\ -------------------- i \ t\ 1\y� �.- \\ 1 l ; I , \\ \ \\\0` \`-----1 1 - ---- -�-- `\` __� --_ -- -------__-/ 1 I , I , \2,_L\ ,, \\ \ , \ \ \ \\\` \, \\ \\\\\`: ---- j I \ ;-- _ \\\\ ____ ---_-_-------------- - -Ii I 1 I �\\ V \\\\\'\ \ \ \`\ \`\`\\_-_--I! SWN-4 -- ' \_ ; \_-= 6 ----------- -- - I I "' \\\`,\\\\\\\\ `\```;__;=,;1 Groundwater Levels & VOCs Detected Above 2L Standards DRY _--- \----- --= -_---- /' i \X� C._1 ; l\\ \ \\----\ May 27-28, 2015 I \. .\ \ \ \ \ \ `,, _ _ \ \ _ I ,\<, , `\`\`� � \ ` -1` \� ,: \ '\'TA \\ ; /'\ I _ _ �/ SURR Y COUN TY AREA OF CONCERN per CAP WELL # TOP OF CASING ELEVATIO N (FT AMSL) DEPTH TO WATER (FT BTOC) GROUNDWATER POTENTIOMETRIC ELEVATION (FT AMSL) BENZENE (UG/L) 1,4-DCB (UG/L) 1,2- DCA (UG/L) 1,1- DCA (UG/L) VCM (UG/L) 1,2-DCP (UG/L) AREA OF SWSL & 2L EXCEEDANCES BEYOND COMPLIANCE BOUNDARY ACRES 15A NCAC 2L Groundwater Qualit Standard 1 1 6 1 0.38 1 6 1 0.03 1 0.6 BACKGROUND MW-1 1134.35 25.57 1108.78 1 1 1 1 1 0 SOUTHERN I72 1068.86 39.91 1028.95 Not Sampled Converted to Injection Well Nov. 2011 3.9 MW-3R 1017.50 42.40 974.59* IW-3 1020.57 33.63 986.94 Not Sampled Converted to Injection Well Nov. 2011 IW-4 1026.26 38.19 988.07 Not Sampled Converted to Injection Well Oct. 2012 IW-5 1080.18 NA I NA Not Sam led Converted to Injection Well Nov. 2011 MW-12S 1025.80 13.68 1012.12 MW-12D 1027.05 0.00 >1027.05* MW-13 1008.48 27.16 981.32 0.850) MW-14 1018.80 42.08 976.72 MW-15 1075.96 53.48 1022.48 1.6 13.6 1.5 MW-16 999.54 27.41 972.13 1.4 18.7 2.5 4.9 1 3.3 MW-17 965.43 8.21 957.22 MW-18 983.00 9.87 973.13 MW-19 946.27 9.73 936.54 MW-21 965.36 6.73 958.63 MW-22 953.40 6.61 946.79 MW-23 955.31 1 7.95 947.36 NORTHERN MW-6 1067.67 22.71 1044.96 0 M W-7 1073.50 12.81 1060.69 IW-6 1088.45 43.89 1045.19* Not Sam led Converted to Injection Well Oct. 2012 MW-9 1094.07 33.95 1060.12 2.8 1 6.2 1 1 1 12.3 MW-20 1082.19 20.02 1062.29* MW-11 MW-11 1151.80 23.35 1128.45 1.8 0 = (irounawater elevation not used Tor contouring GRAPHIC SCALE 0) = "j" Qualified concentration <SWSL considered an estimate 200 0 100 200 400 800 ( IN FEET ) 1 inch = 200 ft. FIGURE 2 v D C z v o z v D m n D r m CLOSED C D LANDFILL and ................................................................................................................................................ ............. ................. ........... .......................... �, Z�, O i\, O m A.................. O N = -� v) c� z o �� - - N.. II o L ED M WLF FA ILITY C O C�,,s s RRY NTY SU COU Municipal Engineerin........... ...... 9 :::...... ...... ..... Services Company, an , P.A. :..................:.:.: ..:....................... p Y DATE BY REV. DESCRIPTION ES �, _. f*1 O m �l z CO O m o PO TEN TIOMETRI C MAP OF UPPERMOST A UIFER Q MT. AIRY N RTH AR LINA O C O I�Ct EOX 9?:GARNER IC2759 .:.:.:.:.:.:.: t:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:. ...O...OQX.49..8... t... f~,....... 2...(I�......................................... ::::::::::::::::::::::....:::::::::::..::::: :............ ::::::::::::: ..:::::::::::::::::::::::: ... 2.... 7.............................. ( M! :: o WI TH VOCS DETECTED ABOVE 2L STANDARDS ....................)......................................................... . ..... ..:.:.:.:.:.:.:.:.:.:.:.:.:.: .. 'ESE.. lJI11BET . �D28i \ \ \ \ \ \ \ \ \ \ 2 G w # / / / w § 2 o$ a q$_ G o o& 0 e& w z a 0 a 0 c- 0 0 M g c c o= m z o z 0 a _ g a m 0 S G§ _ M g S g o 2 E 6\ _/ G-4 o 6 o z 7\\ y a/ o r- o 0 E o g o $ w g o# 0 k B C) m k&_^ 00C) cyl w S m 0© C S E o R f = y _% w CD g 0 K k o « k 0 E E Q k 0& o 0 z 9 z 0 2 � o o i o q§ 0 0 4 R k 6 k\ o m \ k A 0® 0 = o / c= 0 0 o O 0 \ / / \ \ \ § / . \ 0 0 \ \ 0 2 o a* m�� O 2 0 o�_® 2 0 R E 2 CD = o 0 CD\ = o o® \ o \ c m CD c m=_ \ m z 4 z03 ® g & & \ & 7 \ 9 -< C \ � f G/\ m/ b 7 2 G 7 \%\ q / $ f 90 / 9 CD \ \ \ k \ / 2 7 � w $ f \ ƒO o ƒ = o ƒ ƒ c o ƒ ƒ ƒ § d 7 § CL CL C CL = z CL / 2 � §00 z r r 2 �� oo i2oa @ 0 I @_ c2oo z C- m n_> 0 � 2kk B�-00to ,=/CDm / O k� k 2 R Q §sA m�� 2 � Q §_C E ) @ 0 CD @ I§erg @ oom- /)§7 ©- §o/ M-i 0o EEC 7 0CD w I'a� . . � \\ .� (D m < 0 �0 /k �| CD / | � % k C \ 0 2 2 / z Figure 4 Bromide Tracer Concentrations Time Series Graph and Table February 9, 2012 — May 28, 2015 Bromide Tracer Levels in MW-16 Located 87 feet Downgradient of IW-3 which was Injected on November 2, 2011 U.JbUU 0.3000 0.2500 0.2000 E 0.1500 0.1000 0.0500 0.0000 3: U LC • U - U x: Q Date Date MW-16 2/9/2012 0.03800) 5/30/2012 0.13000) 8/20/2012 0.26000) 10/23/2012 0.28000) 5/30/2013 0.14000) 10/31 /2013 0.11000) 5/28/2014 0.22000) 10/22/2014 0.35000) 5/28/2015 0.29000) QNtK N QP (j) = The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), = May 25, 2012 Calculated date injectant expected to reach MW-16 using average flow rates of IW-3 and MW-16 (155 ft/yr) since injection occurred. Slurry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Figure 5 Total Cumulative VOC Concentrations Time Series Graphs/Table October 22, 2009 - May 28, 2015 TOTAL GUM tI LATIVL VOC CONCENTRATIONS -=S SL S-1A. 0.t. .AOO MW-11 nAOC N.nh- .AOC S.oth- aAli W.11. -PAW- 19 S."o- WN COW-129 WV1m JW1l WY19 W03-W 17 A 11"Ari %W13.LWs BgRiR31N MCITpTµ CI)MILRfry[ WLtdCP1111RRW6•+9V$] I 5."aft NWT➢ �N47 WMa AOC Well ID Oct 2009 (ug/L) May 2010 (ug/L) Oct 2010 (ug/L) May 2011 (ug/L) Oct 2011 (ug/L) Average of Preceding Five Events (ug/L) May 2015 (ug/L) Difference (ug/L) Difference N Statistical Trend Between Oct 2009 - May 2015 Background MW-1 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend IW-2 (MW-2) 105.25 207.00 207.93 159.90 79.10 151.84 79.10 NS NS NS No Trend IW-3 (MW-3RS) 202.90 127.50 127.50 144.00 127.60 145.90 127.60 NS NS NS No Trend MW-3R 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend IW-4 (MW-4) 27.00 24.20 24.20 27.60 23.50 25.30 18.10 NS NS NS No Trend IW-5 (MW-5) 35.00 46.50 46.50 47.40 34.80 42.04 34.80 NS NS NS No Trend MW-12S 0.00 0.00 0.00 0.00 5.40 1.08 0.00 -1.08 -100 No Trend MW-12D 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend MW-13 61.00 50.60 74.20 87.30 72.50 69.12 37.45 -31.67 -46 Downward MW-14 15.20 15.60 15.60 8.20 17.00 14.32 11.10 -3.22 -22 No Trend Southern MW-15 96.13 55.00 55.00 78.10 64.06 69.66 64.10 -5.56 -8 No Trend MW-16 137.90 113.60 135.70 121.20 116.30 124.94 86.00 -38.94 -31 Downward MW-17 20.34 8.40 8.85 0.00 5.77 8.67 0.00 -8.67 -100 No Trend MW-18 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend MW-19 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend MW-21 52.10 50.70 51.38 39.10 32.41 45.14 17.80 -27.34 -61 Downward MW-22 28.90 23.80 23.80 11.66 5.20 18.67 1.50 -17.17 -92 Downward MW-23 4.30 0.00 0.00 0.00 0.00 0.86 0.00 -0.86 -100 No Trend Combined Total 786.02 722.90 770.66 724.46 583.64 717.54 477.55 -239.99 -34 Downward MW-6 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend MW-7 7.40 9.40 11.20 9.70 8.80 9.30 9.70 0.40 4 No Trend IW-6 (MW-8) 22.00 23.90 16.00 12.30 12.60 17.36 12.60 NS NS NS No Trend Northern MW-9 23.50 20.40 23.20 25.80 22.90 23.16 30.30 7.14 31 No Trend MW-20 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend Combined Total 52.90 53.70 50.40 47.80 44.30 49.82 52.60 2.78 6 No Trend MW-11 MW-11 10.10 6.00 6.00 5.44 23.20 10.15 6.10 -4.05 -40 No Trend SITEWIDE Combined Total 849.02 782.60 827.06 777.70 651.14 777.50 536.25 -241.25 -31 Downward = Not sampled this event so most recent concentration shown and used In calculations * = Statistical trend analysis via Sen's Slope Estimator at a 95% Confidence Level Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Tables Table 1 Groundwater Monitoring Well Construction Table May 27-28, 2015 Monitoring Well Date Installed Diameeter Total Depth p Top of Screen Depth Screen Length g Geology of Screened Interval Top of Casing Elevation Ground Elevation Groundwater Elevat on Depth 'o Latitude Longitude (inches) (ft bgs) (ft bgs) (ft) (ft amsl) (ft amsi) (ft amsl) (ft btoc) MW-1 11/28/89 2 0 30 10 Clay 1134.35 1133.15 1108.78 25.57 36.439211 -80.568133 IW-2 (was MW-2) 11/28/89 2 70 60 10 Clay 1068.86 1068.36 1028.95 39.91 36.435833 -80.568894 MW-3R 9/27/94 2 01 86 15 Rock 1017.50 1015.00 975.10 42.40 36.434725 -80.571989 IW-3 (was MW-3RS) 5/17/01 2 52 37 15 Rock 1020.57 1018.24 986.94 33.63 36.434656 -80.571858 IW-4 (was MW-4) 8/30/94 2 55.4 40.4 15 Rock 1026.26 1025.06 988.07 38.19 36.434686 -80.569200 IW-5 (was MW-5) 8/27/94 2 63 48 15 Rock 1080.18 1077.78 <1039.50 >40.68 36.434614 -80.570436 MW-6 9/7/94 2 29.7 14.7 15 Rock 1067.67 1065.61 1044.96 22.71 36.437431 -80.571067 MW-7 8/23/94 2 23 8 15 Rock 1073.50 1071.50 1060.69 12.81 36.438439 -80.570722 IW-6 (was MW-8) 8/16/94 2 54 39 15 Rock 1088.45 1086.45 1044.56 43.89 36.439278 -80.570381 MW-9 8/22/94 2 43.8 28.8 15 Rock 1094.07 1092.07 1060.12 33.95 36.439289 -80.571508 MW-11 8/15/94 2 40 25 15 Rock 1151.80 1150.40 1128.45 23.35 36.441589 -80.569558 MW-12S 5/31/01 2 51 11 40 Rock 1025.80 1023.25 1012.12 13.68 36.435942 -80.567972 MW-12D 5/30/01 2 100 90 10 Rock 1027.05 1023.75 1027.05 0.00 36.435964 -80.567994 MW-13 5/30/06 2 35.78 20.78 15 Saprolite 1008.48 1005.75 981.32 27.16 36.435036 -80.568183 MW-14 5/30/06 2 48.03 33.03 15 Rock 1018.80 1016.11 976.72 42.08 36.434267 -80.569239 MW-15 6/22/06 2 57 42 15 Rock 1075.96 1073.23 1022.48 53.48 36.433797 -80.570467 MW-16 6/21/06 2 36.3 21.3 15 Rock 999.54 996.67 972.13 27.41 36.434536 -80.572117 MW-17 6/1/07 2 15.32 5.32 10 Rock 965.43 962.26 957.22 8.21 36.433558 -80.572517 MW-18 6/1/07 2 18.15 8.15 10 Saprolite 983.00 980.00 973.13 9.87 36.435453 -80.567050 MW-19 6/1/07 2 17.1 7.1 10 PWR 946.27 942.97 936.54 9.73 36.432231 -80.570556 MW-20 6/1/07 2 25.64 10.64 15 Rock 1082.19 1079.12 1062.17 20.02 36.439025 -80.571650 MW-21 6/1/07 2 15.41 5.41 10 Saprolite/PWR 965.36 962.22 958.63 6.73 36.434214 -80.568717 MW-22 6/1/07 2 16.04 6.04 10 Saprolite 953.40 950.23 946.79 6.61 36.432928 -80.571678 MW-23 6/1/07 2 17.1 7.1 10 Sand Silt 955.31 952.09 947.36 7.95 36.432828 -80.569156 NOTE: bgs = below ground surface amsl= above mean sea level btoc = below top of casing (PVC well casing) Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Table 2 Field Observations of Monitoring Locations May 27-28, 2015 Viable Lack of Any Locked on Tagged Concrete Location Monitoring Evidence of Arrival & Hinge/Hasp or Surface Pad Comments Location Tampering Departure Operational Labeled Appears Effective MW-1 Yes Yes Yes Yes Yes Yes IW-1 No Yes Yes Yes Yes Yes Fouled since injection 11/2/11. IW-2 (was MW-2) No Yes Yes Yes Yes Yes Fouled since injection 11/2/11. MW-3R Yes Yes Yes Yes Yes Yes IW-3 (was MW-3RS) No Yes Yes Yes Yes Yes Fouled since injection 11/2/11. IW-4 (was MW-4) No Yes Yes Yes Yes Yes Fouled since injection 10/24/12. IW-5 (was MW-5) No Yes Yes Yes Yes Yes Fouled since injection 11/2/11. Bailer would not descend MW-6 Yes Yes Yes Yes Yes Yes MW-7 Yes Yes Yes Yes Yes Yes IW-6 (was MW-8) No Yes Yes Yes Yes Yes Fouled since injection 10/24/12. MW-9 Yes Yes Yes Yes Yes Yes MW-11 Yes Yes Yes Yes Yes Yes MW-12S Yes Yes Yes Yes Yes Yes MW-12D Yes Yes Yes Yes Yes Yes Flowing artesian MW-13 Yes Yes Yes Yes Yes Yes MW-14 Yes Yes Yes Yes Yes Yes MW-15 Yes Yes Yes Yes Yes Yes MW-16 Yes Yes Yes Yes Yes Yes Red algae in purge water MW-17 Yes Yes Yes Yes Yes Yes Red algae in purge water MW-18 Yes Yes Yes Yes Yes Yes MW-19 Yes Yes Yes Yes Yes Yes MW-20 Yes Yes Yes Yes Yes Yes MW-21 Yes Yes Yes Yes Yes Yes MW-22 Yes Yes Yes Yes Yes Yes MW-23 Yes Yes Yes Yes Yes Yes SW-1 Yes Low gage height & flow SW-2 Yes Low gage height & flow SW-3 Yes Low gage height & flow SW-4 Yes Low gage height & flow SWN-1 Yes Low gage height & flow SWN-2 Yes Low gage height & flow SCALEHOUSE Yes Sample from spigot next to well which is typical Any unusual field conditions, observations, or events: Injection wells (IW-1, IW-2, IW-3, IW-4, IW-5 and IW-6) exempt from laboratory analysis as SWS approved on May 10, 2013 (DIN:18938) Stormwater control improvements performed since May 2012 event. Lubricated locks with vegetable oil spray after work at 9 wells was completed. (for specific wells see Field Sampling Data Sheet in Appendix B) Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Table 3 Field Parameter Data Summary May 27-28, 2015 Parameter Depth to Water" Water Elevation TOC Elevation Temp. ORP DO pH Specific Conductance TDS Turbidity Units ft (btoc) ft (amsl) ft (amsl) C mV mg/L SU umhos/cm mg/L Visual or NTU MW-1 25.57 1108.78 1134.35 15.1 197 2.6 6.11 310 150 17.5 IW-2 39.91 1028.95 1068.86 NR NR NR NR NR MPRM >1000 IP MW-3R 42.40 975.10 1017.50 15.3 133 1.1 7.91 220 100 23.5 IW-3 33.63 986.94 1020.57 NR NR NR NR NR NR >1000 IW-4 38.19 988.07 1026.26 NR NR NR NR NR NR >1000 IW-5 >40.68 <1039.50 1080.18 NR NR NR NR NR NR NR M W-6 22.71 1044.96 1067.67 14.2 -38 1.7 6.47 530 260 297 MW-7 12.81 1060.69 1073.50 14.9 203 1.5 5.93 320 150 23.2 IW-6 43.89 1044.56 1088.45 NR NR NR NR NR NR >1000 MW-9 33.95 1060.12 1094.07 16.1 27 0.9 6.38 470 230 14.2 MW-11 23.35 1128.45 1151.80 16.8 153 0.7 4.97 110 50 14.5 MW-12S 13.68 1012.12 1025.80 14.9 -98 1.3 5.42 250 120 19.7 MW-12D 0.00 1027.05 1027.05 14.7 201 1.3 7.31 190 80 20.1 MW-13 27.16 981.32 1008.48 14.8 19 2.1 5.38 140 60 103 MW-14 42.08 976.72 1018.80 14.7 31 2.3 5.42 130 60 18.2 M W-15 53.48 1022.48 1075.96 14.5 38 0.9 5.38 150 70 >1000 MW-16 27.41 972.13 999.54 16.2 74 0.8 5.71 510 250 Slight MW-17 8.21 957.22 965.43 14.2 67 1.1 6.19 330 160 101 MW-18 9.87 973.13 983.00 13.9 203 6.9 5.97 300 140 131 MW-19 9.73 936.54 946.27 13.5 231 3.3 5.83 50 20 Clear MW-20 20.02 1062.17 1082.19 13.9 203 1.7 5.47 60 20 Slight MW-21 6.73 958.63 965.36 14.2 173 2.2 5.43 210 100 191 MW-22 6.61 946.79 953.40 16.1 231 3.9 6.03 260 120 Clear MW-23 7.95 947.36 955.31 14.4 201 3.8 6.91 110 50 Clear Scalehouse na na na 15.1 NR NR 7.07 1120 510 Clear Minimum 0.00 936.54 946.27 13.5 -98 0.7 4.97 50 20 14.20 Average 23.88 1008.71 1034.58 14.9 118 2.1 6.06 289 135 Slight Maximum 53.48 1128.45 1151.80 16.8 231 6.9 7.91 1120 510 >1000 SW-1 - - - 14.8 NR NR 7.01 290 140 Clear SW-2 - - - 13.4 NR NR 6.97 320 150 Clear SW-3 - - - 14.9 NR NR 7.03 290 140 Clear SW-4 - - - 15.2 NR NR 7.07 310 150 Clear SWN-1 - - - 13.4 NR NR 7.13 90 40 Clear SWN-2 - - - 13.3 1 NR NR 7.17 180 80 Clear Minimum - - - 13.3 NR NR 6.97 90 40 Clear Average - - - 14.2 NR NR 7.06 247 117 Clear Maximum - - - 15.2 NR NR 7.17 320 150 Clear btoc = Below top of casing amsl = Above mean sea level na = Not available NR = No reading attempted Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Table 4 Sampling and Analysis Summary May 27-29, 2015 App. I MNA Field Parameter Tracer a IX O m c o p � O a- u, Q) Q c g o C6 m o o O w o m a)y N p .0 N U m m o U 0 c m E O O Y __ 7 5 O 0 o W Mn � X E a)o 0 2 -0 7 2 a > F (n cn U H U I= o O H U F- a H m O O 0 O (n N m O O O O O > O O ON0 a N O O m 0 COO N N N N N iv o Q _o 0 0 0 O N O WW M M M Q M LO LO W a -O -0 -6 -6 -O Q a a a a Q 5 5 Z a� FD a J J W W J W U) if LE if if FL if LL W IW-1 E x MW-1 x x x x x x x x x x x x x x x x x IW-2 E x MW-3R x x x x x x x x x x x x x x IW-3 E x IW-4 E I I x IW-5 E x MW-6 x x x x x x x x x MW-7 x x x x x x x x x x x x x x x x IW-6 E x MW-9 x x x x x x x x x x x x x x x x MW-11 x x x x x x x x x x x x x x x x MW-12S x x x x x x x x x x x x x MW-12D x x x x x x x x x x x x x MW-13 x x x x x x x x x x x x x x MW-14 x x x x x x x x x x x x x x x x MW-15 x x x x x x x x x x x x x x x x x MW-16 x x x x x x x x x x x x x x MW-17 x x x x x x x x x x x x x MW-18 x x x x x x x x x x x x x MW-19 x x x x x x x x x x x x x MW-20 x x x x x x x x x x x x MW-21 x x x x x x x x x x x x x x x x MW-22 x x x x x x x x x x x x x x MW-23 x x x x x x x x x x x x x x Scalehouse x x x x x x x x x SW-1 x x x x x x x SW-2 x x x x x x x SW-3 x x x x x x x SW-4 x x x x x x x SWN-1 x x x x x x x SWN-2 x x x x x x x EB x x FB x x TB I I x App I = Appendix I List from current 40 CFR 258 E = Exempt from sampling per SWS approved SAP [18936] Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Table 5 Detections in Water Samples above SWSL, GWP, 2L or 2B (Appendix 1) May 27-29, 2015 Sample ID Parameter Name Sample Date Result Unit MDL2 SWSL 3 21L4 2135 GWP 5 MCL 7 Preliminary Cause' MW-1 Zinc, total 5/28/15 13.6 ug/L 5 10 1000 5000 MW-6 Vanadium, total 5/27/15 10.6J ug/L 2.5 25 NE 3.5 NE MW-6 Cobalt, total 5/27/15 68.9 ug/L 2.5 10 NE 70 NE MW-7 Chlorobenzene 5/28/15 6.5 ug/L 0.23 3 50 100 MW-7 1,4-Dichlorobenzene 5/28/15 3.2 ug/L 0.33 1 6 75 MW-7 Zinc, total 5/28/15 14.3 ug/L 5 10 1000 5000 MW-7 Cobalt, total 5/28/15 77 ug/L 2.5 10 NE 70 NE MW-7 Vanadium, total 5/28/15 12AJ ug/L 2.5 25 NE 3.5 NE MW-9 cis- 1,2-Dichloroethene 5/28/15 9 ug/L 0.19 5 70 70 MW-9 Benzene 5/28/15 2.8 ug/L 0.25 1 1 5 L &/or LFG MW-9 Vanadium, total 5/28/15 11.1J ug/L 2.5 25 NE 3.5 NE MW-9 Cobalt, total 5/28/15 123 ug/L 2.5 10 NE 70 NE MW-9 Vinyl chloride 5/28/15 12.3 ug/L 0.63 1 0.03 2 L &/or LFG MW-9 1,4-Dichlorobenzene 5/28/15 6.2 ug/L 0.33 1 6 75 L &/or LFG MW-11 1,2-Dichloropropane 5/28/15 1.8 ug/L 0.27 1 0.6 5 L &/or LFG MW-11 Cobalt, total 5/28/15 12.6 ug/L 2.5 10 NE 70 NE MW-11 1,4-Dichlorobenzene 5/28/15 4.3 ug/L 0.33 1 6 75 MW-13 Vanadium, total 5/27/15 5.9J ug/L 2.5 25 NE 3.5 NE MW-13 cis- 1,2-Dichloroethene 5/27/15 26.6 ug/L 0.19 5 70 70 MW-13 1,1-Dichloroethane 5/27/15 5.1 ug/L 0.32 5 6 7 MW-13 Trichloroethene 5/27/15 1.3 ug/L 0.47 1 3 5 MW-13 Zinc, total 5/27/15 10.7 ug/L 5 10 1000 5000 MW-13 1,4-Dichlorobenzene 5/27/15 3.6 ug/L 0.33 1 6 75 MW-13 1,2-Dichloroethane 5/27/15 0.85J ug/L 0.12 1 0.4 5 L &/or LFG MW-14 1,1-Dichloroethane 5/28/15 5 ug/L 0.32 5 6 7 MW-14 cis- 1,2-Dichloroethene 5/28/15 6.1 ug/L 0.25 5 70 70 MW-15 Vinyl chloride 5/28/15 1.5 ug/L 0.62 1 0.03 2 L &/or LFG MW-15 1,4-Dichlorobenzene 5/28/15 4.3 ug/L 0.39 1 6 75 MW-15 cis- 1,2-Dichloroethene 5/28/15 40.2 ug/L 0.25 5 70 70 MW-15 Zinc, total 5/28/15 12.5 ug/L 5 10 1000 5000 MW-15 Vanadium, total 5/28/15 3.9J ug/L 2.5 25 NE 3.5 NE MW-15 Trichloroethene 5/28/15 2.9 ug/L 0.47 1 3 5 MW-15 1,1-Dichloroethane 5/28/15 13.6 ug/L 0.32 5 6 7 L &/or LFG MW-15 Benzene 5/28/15 1.6 ug/L 0.25 1 1 5 L &/or LFG Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 2 Sample Parameter Name Sample Result Unit MDL' SWSL' 2L4 26 s GWP' MCL' Preliminary $ ID Date Cause MW-16 Copper, total 5/28/15 14.1 ug/L 2.5 10 1000 1300 MW-16 1,2-Dichloropropane 5/28/15 3.3 ug/L 0.27 1 0.6 5 L &/or LFG MW-16 Vinyl chloride 5/28/15 4.9 ug/L 0.62 1 0.03 2 L &/or LFG MW-16 Thallium, total 5/28/15 8.9 ug/L 5 5.5 NE 0.28 2 MW-16 Benzene 5/28/15 1.4 ug/L 0.25 1 1 5 L &/or LFG MW-16 Zinc, total 5/28/15 16.8 ug/L 5 10 1000 5000 MW-16 1,4-Dichlorobenzene 5/28/15 18.7 ug/L 0.33 1 6 75 L &/or LFG MW-16 Vanadium, total 5/28/15 18.5J ug/L 2.5 25 NE 3.5 NE MW-16 1,2-Dichloroethane 5/28/15 2.5 ug/L 0.12 1 0.4 5 L &/or LFG MW-16 Barium, total 5/28/15 133 ug/L 2.5 100 700 1300 MW-16 Cobalt, total 5/28/15 343 ug/L 2.5 10 NE 70 NE MW-16 cis- 1,2-Dichloroethene 5/28/15 48 ug/L 0.19 5 70 70 MW-16 Chlorobenzene 5/28/15 7.2 ug/L 0.23 3 50 100 MW-17 Cobalt, total 5/28/15 26.3 ug/L 2.5 10 NE 70 NE MW-17 Vanadium, total 5/28/15 7.1J ug/L 2.5 25 NE 3.5 NE MW-20 Cobalt, total 5/28/15 17.4 ug/L 2.5 10 NE 70 NE MW-21 Trichloroethene 5/27/15 1 ug/L 0.47 1 3 5 MW-21 cis- 1,2-Dichloroethene 5/27/15 16.8 ug/L 0.25 5 70 70 MW-22 1,4-Dichlorobenzene 5/27/15 1.5 ug/L 0.39 1 6 75 MW-22 Copper, total 5/27/15 132 ug/L 2.5 10 1000 1300 MW-22 Zinc, total 5/27/15 29.3 ug/L 5 10 1000 5000 SW-2 Cobalt, total 5/28/15 22.3 ug/L 2.5 10 270 NE SW-4 Copper, total 5/28/15 13.7 ug/L 2.5 10 7 1300 N SW-4 Zinc, total 5/28/15 118 ug/L 5 10 50 5000 N EB Methylene Chloride 5/29/15 61.2 ug/L 0.97 1 4.6 5 Artifact Table contains constituents detected at or above SWSL, GWP, 2L, or 2B MDL = Method Detection Limit 3 SWSL = Solid Waste Section Reporting Limit 4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard e 2B = North Carolina 15 NCAC 2B Surface Water Quality Standard for this Specific Stream Classification 6 GWP = Groundwater Protection Standard 7 MCL = Primary Drinking Water Standard (not currently applicable for regulatory comparisons) 8 Preliminary Cause = Refers to a preliminary analysis of the cause and/or source of a detection over the respective 2L/2B Standard. A definitive source of the detection was not determined as part of this report. Preliminary cause only listed pursuant to instructions j =The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable L = Leachate LFG = Landfill Gas N = Natural originating from erosion of natural deposits. Source not anthropogenic. Artifact = False positive lab or field induced. Detected in quality control blank(s). BOLD = Concentration > 2L, 2B or MCL Standard Slurry County Closed C&D and Closed MSWLF, Mt. Airy Page 2 of 2 Table 6 MNA Parameter Data Summary May 27-28, 2015 Parameters Method MDL* Units MW-1 MW-7 MW-9 MW-11 MW-14 MW-15 MW-21 MW-12S MW-12D MW-13 MW-16 MW-17 MW-18 MW-19 MW-20 MW-22 MW-23 MW-3R 5/28/15 5/28/15 5/28/15 5/28/15 5/27/15 5/27/15 5/27/15 5/28/15 5/28/15 5/27/15 5/28/15 5/28/15 5/28/15 5/27/15 5/28/15 5/27/15 5/27/15 5/28/15 VFA - Acetic Acid AM23G NS ug/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS VFA - Butyric Acid AM23G NS ug/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS VFA - Lactic Acid AM23G NS ug/L I NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS VFA - Propionic Acid AM23G NS ug/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS VFA - Pyruvic Acid AM23G NS ug/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS Hydrogen AM20GAX NS nM NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS Methane RSK175 NS ug/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS Ethene AM20GAX NS ug/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS Ethane AM20GAX NS ug/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS CO2-Dissolved Field HACH Kit NS mg/L 80 >100 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS >100 Alkalinity SM 2320B 1000 ug/L 78800 84600 65800 20400 34000 41800 29600 89400 <1000 30500 124000 77000 8740 16300 8200 111000 NS 131000 Sulfate EPA 300.0 1000 ug/L 8090J 6420J 1810J 12000J 2730J 1760J 1670J 46200J 7420J 2920J 8470J 5390J 1500J 1770J 1060J 3640J NS 2210J Sulfide SM 4500-S2D 100 ug/L <100 <100 <100 <100 <100 <100 <100 NS NS NS NS NS NS NS NS NS NS NS Chloride SM 4500-CI-E 500 ug/L 3600 44400 49300 7030 2540 1690 28200 4220 1050 33100 38300 42600 1250 2610 13900 7310 NS 3250 TOC SM 5310B 500 ug/L 710J 4380 1560 1000 <500 827J 951J 827J <500 2950 5990 2330 <500 <500 NS 2050 NS 1260 COD SM 5220D 12500 ug/L <12500 28000 24000J <12500 <12500 <12500 <12500 NS NS NS NS NS NS NS NS NS NS NS BOD SM5210B NS ug/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS Iron, Dissolved EPA 6010 25 ug/L 29.6J <25 <25 101J 294J 6420 <25 NS NS NS NS NS NS NS NS NS NS NS Nitrate EPA 353.2 <20 ug/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS Temperature Field Instrument 0 C 15.1 14.9 16.1 16.8 14.7 14.5 14.2 14.9 14.7 14.8 16.2 14.2 13.9 13.5 13.9 16.1 14.4 15.3 ORP Field Instrument -900 mV 1 197 203 27 153 31 38 173 -98 201 19 74 67 203 231 203 231 201 133 DO Field Instrument 0 mg/L 2.6 1.5 0.9 0.7 2.3 0.9 2.2 1.3 1.3 2.1 0.8 1.1 6.9 3.3 1.7 3.9 3.8 1.1 pH Field Instrument 0 SU 6.11 5.93 6.38 4.97 5.42 5.38 5.43 5.42 7.31 5.38 5.71 6.19 5.97 5.83 5.47 6.03 6.91 7.91 Specific Conductance Field Instrument 0 us/cm 310 320 470 110 130 150 210 250 190 140 510 330 300 50 60 260 110 220 Turbidity Field Instrument 0 1 NTU 17.5 23.2 14.2 14.5 18.2 >1000 191 19.7 20.1 103 Slight 101 131 Clear Slight Clear Clear 23.5 Notes: MDL* = Lab Method Detection Limit or lowest field measurement possible. Constituents detected below quantifiable limits are shown as < MDL value. NS = Not Sampled J =The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. >100 = CO2 Concentration exceeds maximum capability of method used. Surry County Closed C&D and CLosed MSWLF, Mt. Airy Page 1 of 1 Table 7 Hydrologic Properties at Monitoring Well Locations May 27-28, 2015 Well Hydraulic Conductivity Effective Porosity Hydraulic Gradient Groundwater Average Linear Velocity Rate Flow Direction Minimum Distance From Upgradient EOW Ground Water Depth Groundwater Potentiometric Elevation Screened Interval Lithology (cm/second) (ftlday) (%) (feet/feet) (feet/year) (ft) (feet btoc) (feet amsl) MW-1 4.30E-05 0.122 15 0.051 15 S54W 0 25.57 1108.78 Clay IW-2 4.30E-05 0.122 15 0.030 9 S67E - 39.91 1028.95 Clay MW-7 8.10E-04 2.296 15 0.138 771 N60W 704 12.81 1060.69 PWR/Fractured Rock IW-6 4.40E-04 1.247 15 0.105 318 S48W - 43.89 1044.56 PWR/Fractured Rock MW-9 1.90E-04 0.539 15 0.006 7 S42E 614 33.95 1060.12 Sandy Silt MW-13 2.06E-04 0.584 23 0.066 61 S28E 1850 27.16 981.32 Saprolite MW-18 2.04E-03 5.783 15 0.143 na S31E 0 9.87 973.13 Saprolite MW-19 1.10E-03 3.118 3 0.077 2,917 S15W 2663 9.73 936.54 PWR MW-21 1.28E-03 3.628 3 0.069 3,024 S48E 2041 6.73 958.63 Saprolite/PWR MW-22 9.88E-04 2.801 15 0.140 951 S31W 2506 6.61 946.79 Saprolite MW-23 3.04E-04 0.862 15 0.083 173 S40E 2610 7.95 947.36 Sandy Silt Minimum 4.30E-05 0.122 3 0.006 7 - 0 6.61 936.54 Average 6.77E-04 1.918 14 0.082 825 - 1443 20.38 1004.26 Maximum 2.04E-03 5.783 23 0.143 3,024 - 2663 43.89 1108.78 MW-3R 2.40E-04 0.680 5 na na na 1,994 42.40 975.10 Fractured Rock IW-3 2.40E-05 0.068 5 0.248 123 S45W - 33.63 986.94 Fractured Rock IW-4 1.10E-04 0.312 5 0.193 439 S46E - 38.19 988.07 Fractured Rock IW-5 1.50E-05 0.043 5 16.349 5,075 S59E - na na Fractured Rock MW-6 1.90E-05 0.054 5 0.216 85 S77W 963 22.71 1044.96 Fractured Rock MW-11 3.10E-04 0.879 5 0.090 577 S16W 0 23.35 1128.45 Fractured Rock MW-12S na na 3 0.085 na S14E 0 13.68 1012.12 Fractured Rock MW-12D 1.30E-06 0.004 5 na na na 0 0.00 1027.05 Fractured Rock MW-14 7.45E-03 21.118 3 0.273 70,229 S75E 2098 42.08 976.72 Fractured Rock MW-15 7.21 E-05 0.204 3 0.108 268 S06E 53.48 1022.48 Fractured Rock MW-16 2.82E-05 0.080 3 0.030 29 S37W 2089 27.41 972.13 Fractured Rock MW-17 2.94E-04 0.833 3 0.062 626 S66W 2547 8.21 957.22 Rock MW-20 1.92E-04 0.544 3 0.064 423 S24E 1 692 1 20.02 1 1062.17 1 Rock Minimum 1.30E-06 0.004 3 0.030 29 - 0 0.00 957.22 - Average 1.19E-04 0.336 4 1.611 849 - �2547j 27.10 1012.78 Maximum 3.10E-04 0.879 16.349 5.075 53.48 1128.45 - NOTE: Values for hydraulic conductivity determined via slug test by GAI, MESCO, or Joyce. Hydrologic gradient from water levels recorded on May 27-28, 2015. Wells screened entirely in rock were not utilized for flow directions/gradients. Screens that traverse both rock and regolith assumed flow in regolith dominates. Hydraulic Conducitivity value and flow rate for MW-14 was considered an outlier; therefore not included in the average or maximum. na = Not available/applicable Average Linear Velocity (Q) is defined by modified Darcy's equation: _ _ K dh K= hydraulic conductivity where Q - n dl ne= effective porosity e dh= head difference dl= horizontal distance Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Appendix A Laboratory Analysis Reports Chains of Custody aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 June 12, 2015 Mr. Jonathan Pfohl Municipal Engineering Services PO Box 97 Garner, NC 27529 RE: Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory on May 29, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Godwin kevin.godwin@pacelabs.com Project Manager Enclosures Q _Kok r REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 SAMPLE SUMMARY Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Lab ID Sample ID Matrix Date Collected Date Received 92252070001 MW-12D Water 05/28/1510:15 05/29/15 13:00 92252070002 MW-12S Water 05/28/15 09:40 05/29/15 13:00 92252070003 MW-13 Water 05/27/1512:10 05/29/15 13:00 92252070004 MW-16 Water 05/28/1512:20 05/29/15 13:00 92252070005 MW-17 Water 05/28/15 08:40 05/29/15 13:00 92252070006 MW-18 Water 05/28/1511:00 05/29/15 13:00 92252070007 MW-19 Water 05/27/1513:50 05/29/15 13:00 92252070008 MW-22 Water 05/27/1515:10 05/29/15 13:00 92252070009 MW-23 Water 05/27/1516:00 05/29/15 13:00 92252070010 MW-3R Water 05/28/1511:50 05/29/15 13:00 92252070011 MW-20 Water 05/28/1515:30 05/29/15 13:00 92252070012 MW-14 Water 05/28/1514:40 05/29/15 13:00 92252070013 MW-15 Water 05/28/1513:40 05/29/15 13:00 92252070014 MW-1 Water 05/28/15 08:15 05/29/15 13:00 92252070015 MW-21 Water 05/27/1514:35 05/29/15 13:00 92252070016 MW-7 Water 05/28/15 09:10 05/29/15 13:00 92252070017 MW-9 Water 05/28/1516:15 05/29/15 13:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: SURRY CLOSED- MT AIRY (UIC) 92252070 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92252070001 MW-12D EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C SM 2320B MLS 1 PASI-A EPA 300.0 AES2 1 PASI-A SM 4500-CI-E SER 1 PASI-A SM 5310B AES2 1 PASI-A 92252070002 MW-12S EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C SM 2320B MLS 1 PASI-A EPA 300.0 AES2 1 PASI-A SM 4500-CI-E SER 1 PASI-A SM 5310B AES2 1 PASI-A 92252070003 MW-13 EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C SM 2320B MLS 1 PASI-A EPA 300.0 AES2 1 PASI-A SM 4500-CI-E SER 1 PASI-A SM 5310B AES2 1 PASI-A 92252070004 MW-16 EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C SM 2320B MLS 1 PASI-A EPA 300.0 AES2 1 PASI-A SM 4500-CI-E SER 1 PASI-A SM 5310B AES2 1 PASI-A 92252070005 MW-17 EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C SM 2320B MLS 1 PASI-A EPA 300.0 AES2 1 PASI-A SM 4500-CI-E SER 1 PASI-A SM 5310B AES2 1 PASI-A 92252070006 MW-18 EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C SM 2320B MLS 1 PASI-A EPA 300.0 AES2 1 PASI-A SM 4500-CI-E SER 1 PASI-A SM 5310B AES2 1 PASI-A 92252070007 MW-19 EPA 6010 JMW 15 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Lab ID Sample ID Method Analysts Analytes Reported Laboratory EPA 8260 GAW 51 PASI-C SM 2320B MLS 1 PASI-A EPA 300.0 AES2 1 PASI-A SM 4500-CI-E SER 1 PASI-A SM 5310B AES2 1 PASI-A 92252070008 MW-22 EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C SM 2320B MLS 1 PASI-A EPA 300.0 AES2 1 PASI-A SM 4500-CI-E SER 1 PASI-A SM 5310B AES2 1 PASI-A 92252070009 MW-23 EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C SM 2320B MLS 1 PASI-A EPA 300.0 AES2 1 PASI-A SM 4500-CI-E SER 1 PASI-A SM 5310B AES2 1 PASI-A 92252070010 MW-3R EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C SM 2320B MLS 1 PASI-A EPA 300.0 AES2 1 PASI-A SM 4500-CI-E SER 1 PASI-A SM 5310B AES2 1 PASI-A 92252070011 MW-20 EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C SM 2320B MLS 1 PASI-A EPA 300.0 AES2 1 PASI-A SM 4500-CI-E SER 1 PASI-A 92252070012 MW-14 EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C SM 2320B MLS 1 PASI-A EPA 300.0 AES2 1 PASI-A SM 4500-CI-E SER 1 PASI-A SM 5220D MAB 1 PASI-A SM 5310B AES2 1 PASI-A 92252070013 MW-15 EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Lab ID Sample ID Method Analysts Analytes Reported Laboratory SM 2320B MLS 1 PASI-A EPA 300.0 AES2 1 PASI-A SM 4500-CI-E SER 1 PASI-A SM 5220D MAB 1 PASI-A SM 5310B AES2 1 PASI-A 92252070014 MW-1 EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C SM 2320B MLS 1 PASI-A EPA 300.0 AES2 1 PASI-A SM 4500-CI-E SER 1 PASI-A SM 5220D MAB 1 PASI-A SM 5310B AES2 1 PASI-A 92252070015 MW-21 EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C SM 2320B MLS 1 PASI-A EPA 300.0 AES2 1 PASI-A SM 4500-CI-E SER 1 PASI-A SM 5220D MAB 1 PASI-A SM 5310B AES2 1 PASI-A 92252070016 MW-7 EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C SM 2320B MLS 1 PASI-A EPA 300.0 AES2 1 PASI-A SM 4500-CI-E SER 1 PASI-A SM 5220D MAB 1 PASI-A SM 5310B AES2 1 PASI-A 92252070017 MW-9 EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C SM 2320B MLS 1 PASI-A EPA 300.0 AES2 1 PASI-A SM 4500-CI-E SER 1 PASI-A SM 5220D MAB 1 PASI-A SM 5310B AES2 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-12D Lab ID: 92252070001 Collected: 05/28/15 10:15 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane cis-1,3-Dichloropropene Date: 06/12/2015 09:27 AM Analytical Method: EPA 6010 Preparation Method: EPA 3010 ND ug/L 6.0 3.8 1 06/01/15 20:15 06/04/15 19:23 7440-36-0 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:23 7440-38-2 5.8J ug/L 100 2.5 1 06/01/15 20:15 06/04/15 19:23 7440-39-3 ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:23 7440-41-7 ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:23 7440-43-9 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:23 7440-47-3 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:23 7440-48-4 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:23 7440-50-8 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:23 7439-92-1 ND ug/L 50.0 2.5 1 06/01/15 20:15 06/04/15 19:23 7440-02-0 ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:23 7782-49-2 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:23 7440-22-4 ND ug/L 5.5 5.0 1 06/01/15 20:15 06/04/15 19:23 7440-28-0 ND ug/L 25.0 2.5 1 06/01/15 20:15 06/04/15 19:23 7440-62-2 ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:23 7440-66-6 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 06/04/15 20:51 67-64-1 ND ug/L 200 1.9 1 06/04/15 20:51 107-13-1 ND ug/L 1.0 0.25 1 06/04/15 20:51 71-43-2 ND ug/L 3.0 0.17 1 06/04/15 20:51 74-97-5 ND ug/L 1.0 0.18 1 06/04/15 20:51 75-27-4 ND ug/L 3.0 0.26 1 06/04/15 20:51 75-25-2 ND ug/L 10.0 0.29 1 06/04/15 20:51 74-83-9 ND ug/L 100 0.96 1 06/04/15 20:51 78-93-3 ND ug/L 100 1.2 1 06/04/15 20:51 75-15-0 ND ug/L 1.0 0.25 1 06/04/15 20:51 56-23-5 ND ug/L 3.0 0.23 1 06/04/15 20:51 108-90-7 ND ug/L 10.0 0.54 1 06/04/15 20:51 75-00-3 ND ug/L 5.0 0.14 1 06/04/15 20:51 67-66-3 ND ug/L 1.0 0.11 1 06/04/15 20:51 74-87-3 ND ug/L 13.0 2.0 1 06/04/15 20:51 96-12-8 ND ug/L 3.0 0.21 1 06/04/15 20:51 124-48-1 ND ug/L 1.0 0.27 1 06/04/15 20:51 106-93-4 ND ug/L 10.0 0.21 1 06/04/15 20:51 74-95-3 ND ug/L 5.0 0.30 1 06/04/15 20:51 95-50-1 ND ug/L 1.0 0.33 1 06/04/15 20:51 106-46-7 ND ug/L 100 1.0 1 06/04/15 20:51 110-57-6 ND ug/L 5.0 0.32 1 06/04/15 20:51 75-34-3 ND ug/L 1.0 0.12 1 06/04/15 20:51 107-06-2 ND ug/L 5.0 0.56 1 06/04/15 20:51 75-35-4 ND ug/L 5.0 0.19 1 06/04/15 20:51 156-59-2 ND ug/L 5.0 0.49 1 06/04/15 20:51 156-60-5 ND ug/L 1.0 0.27 1 06/04/15 20:51 78-87-5 ND ug/L 1.0 0.28 1 06/04/15 20:51 142-28-9 ND ug/L 1.0 0.13 1 06/04/15 20:51 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. L2 Page 7 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-12D Lab ID: 92252070001 Collected: 05/28/15 10:15 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 531013 TOC Total Organic Carbon Date: 06/12/2015 09:27 AM Analytical Method: EPA 8260 ND ug/L 1.0 0.26 1 06/04/15 20:51 10061-02-6 ND ug/L 1.0 0.30 1 06/04/15 20:51 100-41-4 ND ug/L 50.0 0.46 1 06/04/15 20:51 591-78-6 ND ug/L 10.0 0.32 1 06/04/15 20:51 74-88-4 ND ug/L 1.0 0.97 1 06/04/15 20:51 75-09-2 ND ug/L 100 0.33 1 06/04/15 20:51 108-10-1 ND ug/L 1.0 0.26 1 06/04/15 20:51 100-42-5 ND ug/L 5.0 0.33 1 06/04/15 20:51 630-20-6 ND ug/L 3.0 0.40 1 06/04/15 20:51 79-34-5 ND ug/L 1.0 0.46 1 06/04/15 20:51 127-18-4 ND ug/L 1.0 0.26 1 06/04/15 20:51 108-88-3 ND ug/L 1.0 0.48 1 06/04/15 20:51 71-55-6 ND ug/L 1.0 0.29 1 06/04/15 20:51 79-00-5 ND ug/L 1.0 0.47 1 06/04/15 20:51 79-01-6 ND ug/L 1.0 0.20 1 06/04/15 20:51 75-69-4 ND ug/L 1.0 0.41 1 06/04/15 20:51 96-18-4 ND ug/L 50.0 0.35 1 06/04/15 20:51 108-05-4 ND ug/L 1.0 0.62 1 06/04/15 20:51 75-01-4 ND ug/L 5.0 0.66 1 06/04/15 20:51 1330-20-7 98 % 70-130 1 06/04/15 20:51 460-00-4 101 % 70-130 1 06/04/15 20:51 17060-07-0 101 % 70-130 1 06/04/15 20:51 2037-26-5 Analytical Method: SM 2320B ND ug/L 5000 1000 1 06/10/1513:29 Analytical Method: EPA 300.0 7420J ug/L 250000 1000 1 06/06/15 00:26 14808-79-8 Analytical Method: SM 4500-CI-E 1050 ug/L 1000 500 1 06/06/15 06:58 16887-00-6 Analytical Method: SM 5310B ND ug/L 1000 500 1 06/06/15 01:25 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 8 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-12S Lab ID: 92252070002 Collected: 05/28/15 09:40 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane cis-1,3-Dichloropropene Date: 06/12/2015 09:27 AM Analytical Method: EPA 6010 Preparation Method: EPA 3010 ND ug/L 6.0 3.8 1 06/01/15 20:15 06/04/15 19:26 7440-36-0 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:26 7440-38-2 20.9J ug/L 100 2.5 1 06/01/15 20:15 06/04/15 19:26 7440-39-3 ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:26 7440-41-7 ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:26 7440-43-9 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:26 7440-47-3 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:26 7440-48-4 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:26 7440-50-8 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:26 7439-92-1 ND ug/L 50.0 2.5 1 06/01/15 20:15 06/04/15 19:26 7440-02-0 ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:26 7782-49-2 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:26 7440-22-4 ND ug/L 5.5 5.0 1 06/01/15 20:15 06/04/15 19:26 7440-28-0 ND ug/L 25.0 2.5 1 06/01/15 20:15 06/04/15 19:26 7440-62-2 ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:26 7440-66-6 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 06/04/15 21:07 67-64-1 ND ug/L 200 1.9 1 06/04/15 21:07 107-13-1 ND ug/L 1.0 0.25 1 06/04/15 21:07 71-43-2 ND ug/L 3.0 0.17 1 06/04/15 21:07 74-97-5 ND ug/L 1.0 0.18 1 06/04/15 21:07 75-27-4 ND ug/L 3.0 0.26 1 06/04/15 21:07 75-25-2 ND ug/L 10.0 0.29 1 06/04/15 21:07 74-83-9 ND ug/L 100 0.96 1 06/04/15 21:07 78-93-3 ND ug/L 100 1.2 1 06/04/15 21:07 75-15-0 ND ug/L 1.0 0.25 1 06/04/15 21:07 56-23-5 ND ug/L 3.0 0.23 1 06/04/15 21:07 108-90-7 ND ug/L 10.0 0.54 1 06/04/15 21:07 75-00-3 ND ug/L 5.0 0.14 1 06/04/15 21:07 67-66-3 ND ug/L 1.0 0.11 1 06/04/15 21:07 74-87-3 ND ug/L 13.0 2.0 1 06/04/15 21:07 96-12-8 ND ug/L 3.0 0.21 1 06/04/15 21:07 124-48-1 ND ug/L 1.0 0.27 1 06/04/15 21:07 106-93-4 ND ug/L 10.0 0.21 1 06/04/15 21:07 74-95-3 ND ug/L 5.0 0.30 1 06/04/15 21:07 95-50-1 ND ug/L 1.0 0.33 1 06/04/15 21:07 106-46-7 ND ug/L 100 1.0 1 06/04/15 21:07 110-57-6 0.54J ug/L 5.0 0.32 1 06/04/15 21:07 75-34-3 ND ug/L 1.0 0.12 1 06/04/15 21:07 107-06-2 ND ug/L 5.0 0.56 1 06/04/15 21:07 75-35-4 0.31J ug/L 5.0 0.19 1 06/04/15 21:07 156-59-2 ND ug/L 5.0 0.49 1 06/04/15 21:07 156-60-5 ND ug/L 1.0 0.27 1 06/04/15 21:07 78-87-5 ND ug/L 1.0 0.28 1 06/04/15 21:07 142-28-9 ND ug/L 1.0 0.13 1 06/04/15 21:07 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. L2 Page 9 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-12S Lab ID: 92252070002 Collected: 05/28/15 09:40 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 531013 TOC Total Organic Carbon Date: 06/12/2015 09:27 AM Analytical Method: EPA 8260 ND ug/L 1.0 0.26 1 06/04/15 21:07 10061-02-6 ND ug/L 1.0 0.30 1 06/04/15 21:07 100-41-4 ND ug/L 50.0 0.46 1 06/04/15 21:07 591-78-6 ND ug/L 10.0 0.32 1 06/04/15 21:07 74-88-4 ND ug/L 1.0 0.97 1 06/04/15 21:07 75-09-2 ND ug/L 100 0.33 1 06/04/15 21:07 108-10-1 ND ug/L 1.0 0.26 1 06/04/15 21:07 100-42-5 ND ug/L 5.0 0.33 1 06/04/15 21:07 630-20-6 ND ug/L 3.0 0.40 1 06/04/15 21:07 79-34-5 ND ug/L 1.0 0.46 1 06/04/15 21:07 127-18-4 ND ug/L 1.0 0.26 1 06/04/15 21:07 108-88-3 ND ug/L 1.0 0.48 1 06/04/15 21:07 71-55-6 ND ug/L 1.0 0.29 1 06/04/15 21:07 79-00-5 ND ug/L 1.0 0.47 1 06/04/15 21:07 79-01-6 ND ug/L 1.0 0.20 1 06/04/15 21:07 75-69-4 ND ug/L 1.0 0.41 1 06/04/15 21:07 96-18-4 ND ug/L 50.0 0.35 1 06/04/15 21:07 108-05-4 ND ug/L 1.0 0.62 1 06/04/15 21:07 75-01-4 ND ug/L 5.0 0.66 1 06/04/15 21:07 1330-20-7 98 % 70-130 1 06/04/15 21:07 460-00-4 101 % 70-130 1 06/04/15 21:07 17060-07-0 101 % 70-130 1 06/04/15 21:07 2037-26-5 Analytical Method: SM 2320B 89400 ug/L 5000 1000 1 06/10/15 09:53 Analytical Method: EPA 300.0 46200J ug/L 500000 2000 2 06/06/15 00:39 14808-79-8 Analytical Method: SM 4500-CI-E 4220 ug/L 1000 500 1 06/06/15 06:59 16887-00-6 Analytical Method: SM 5310B 827J ug/L 1000 500 1 06/06/15 01:25 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-13 Lab ID: 92252070003 Collected: 05/27/15 12:10 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane cis-1,3-Dichloropropene Date: 06/12/2015 09:27 AM Analytical Method: EPA 6010 Preparation Method: EPA 3010 ND ug/L 6.0 3.8 1 06/01/15 20:15 06/04/15 19:29 7440-36-0 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:29 7440-38-2 64.3J ug/L 100 2.5 1 06/01/15 20:15 06/04/15 19:29 7440-39-3 0.52J ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:29 7440-41-7 ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:29 7440-43-9 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:29 7440-47-3 8.6J ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:29 7440-48-4 2.6J ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:29 7440-50-8 4.9J ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:29 7439-92-1 ND ug/L 50.0 2.5 1 06/01/15 20:15 06/04/15 19:29 7440-02-0 ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:29 7782-49-2 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:29 7440-22-4 ND ug/L 5.5 5.0 1 06/01/15 20:15 06/04/15 19:29 7440-28-0 5.9J ug/L 25.0 2.5 1 06/01/15 20:15 06/04/15 19:29 7440-62-2 10.7 ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:29 7440-66-6 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 06/04/15 21:24 67-64-1 ND ug/L 200 1.9 1 06/04/15 21:24 107-13-1 ND ug/L 1.0 0.25 1 06/04/15 21:24 71-43-2 ND ug/L 3.0 0.17 1 06/04/15 21:24 74-97-5 ND ug/L 1.0 0.18 1 06/04/15 21:24 75-27-4 ND ug/L 3.0 0.26 1 06/04/15 21:24 75-25-2 ND ug/L 10.0 0.29 1 06/04/15 21:24 74-83-9 ND ug/L 100 0.96 1 06/04/15 21:24 78-93-3 ND ug/L 100 1.2 1 06/04/15 21:24 75-15-0 ND ug/L 1.0 0.25 1 06/04/15 21:24 56-23-5 1.8J ug/L 3.0 0.23 1 06/04/15 21:24 108-90-7 0.66J ug/L 10.0 0.54 1 06/04/15 21:24 75-00-3 ND ug/L 5.0 0.14 1 06/04/15 21:24 67-66-3 ND ug/L 1.0 0.11 1 06/04/15 21:24 74-87-3 ND ug/L 13.0 2.0 1 06/04/15 21:24 96-12-8 ND ug/L 3.0 0.21 1 06/04/15 21:24 124-48-1 ND ug/L 1.0 0.27 1 06/04/15 21:24 106-93-4 ND ug/L 10.0 0.21 1 06/04/15 21:24 74-95-3 0.35J ug/L 5.0 0.30 1 06/04/15 21:24 95-50-1 3.6 ug/L 1.0 0.33 1 06/04/15 21:24 106-46-7 ND ug/L 100 1.0 1 06/04/15 21:24 110-57-6 5.1 ug/L 5.0 0.32 1 06/04/15 21:24 75-34-3 0.85J ug/L 1.0 0.12 1 06/04/15 21:24 107-06-2 ND ug/L 5.0 0.56 1 06/04/15 21:24 75-35-4 26.6 ug/L 5.0 0.19 1 06/04/15 21:24 156-59-2 ND ug/L 5.0 0.49 1 06/04/15 21:24 156-60-5 0.28J ug/L 1.0 0.27 1 06/04/15 21:24 78-87-5 ND ug/L 1.0 0.28 1 06/04/15 21:24 142-28-9 ND ug/L 1.0 0.13 1 06/04/15 21:24 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. L2 Page 11 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-13 Lab ID: 92252070003 Collected: 05/27/15 12:10 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 531013 TOC Total Organic Carbon Date: 06/12/2015 09:27 AM Analytical Method: EPA 8260 ND ug/L 1.0 0.26 1 06/04/15 21:24 10061-02-6 ND ug/L 1.0 0.30 1 06/04/15 21:24 100-41-4 ND ug/L 50.0 0.46 1 06/04/15 21:24 591-78-6 ND ug/L 10.0 0.32 1 06/04/15 21:24 74-88-4 ND ug/L 1.0 0.97 1 06/04/15 21:24 75-09-2 ND ug/L 100 0.33 1 06/04/15 21:24 108-10-1 ND ug/L 1.0 0.26 1 06/04/15 21:24 100-42-5 ND ug/L 5.0 0.33 1 06/04/15 21:24 630-20-6 ND ug/L 3.0 0.40 1 06/04/15 21:24 79-34-5 ND ug/L 1.0 0.46 1 06/04/15 21:24 127-18-4 ND ug/L 1.0 0.26 1 06/04/15 21:24 108-88-3 ND ug/L 1.0 0.48 1 06/04/15 21:24 71-55-6 ND ug/L 1.0 0.29 1 06/04/15 21:24 79-00-5 1.3 ug/L 1.0 0.47 1 06/04/15 21:24 79-01-6 ND ug/L 1.0 0.20 1 06/04/15 21:24 75-69-4 ND ug/L 1.0 0.41 1 06/04/15 21:24 96-18-4 ND ug/L 50.0 0.35 1 06/04/15 21:24 108-05-4 ND ug/L 1.0 0.62 1 06/04/15 21:24 75-01-4 ND ug/L 5.0 0.66 1 06/04/15 21:24 1330-20-7 96 % 70-130 1 06/04/15 21:24 460-00-4 99 % 70-130 1 06/04/15 21:24 17060-07-0 101 % 70-130 1 06/04/15 21:24 2037-26-5 Analytical Method: SM 2320B 30500 ug/L 5000 1000 1 06/08/1519:08 Analytical Method: EPA 300.0 2920J ug/L 250000 1000 1 06/06/15 00:53 14808-79-8 Analytical Method: SM 4500-CI-E 33100 ug/L 1000 500 1 06/06/15 06:59 16887-00-6 Analytical Method: SM 5310B 2950 ug/L 1000 500 1 06/06/15 01:25 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 12 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-16 Lab ID: 92252070004 Collected: 05/28/15 12:20 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane cis-1,3-Dichloropropene Date: 06/12/2015 09:27 AM Analytical Method: EPA 6010 Preparation Method: EPA 3010 ND ug/L 6.0 3.8 1 06/01/15 20:15 06/04/15 19:32 7440-36-0 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:32 7440-38-2 133 ug/L 100 2.5 1 06/01/15 20:15 06/04/15 19:32 7440-39-3 ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:32 7440-41-7 0.56J ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:32 7440-43-9 2.9J ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:32 7440-47-3 343 ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:32 7440-48-4 14.1 ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:32 7440-50-8 3.7J ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:32 7439-92-1 21.6J ug/L 50.0 2.5 1 06/01/15 20:15 06/04/15 19:32 7440-02-0 ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:32 7782-49-2 4.3J ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:32 7440-22-4 8.9 ug/L 5.5 5.0 1 06/01/15 20:15 06/04/15 19:32 7440-28-0 18.5J ug/L 25.0 2.5 1 06/01/15 20:15 06/04/15 19:32 7440-62-2 16.8 ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:32 7440-66-6 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 06/04/15 21:41 67-64-1 ND ug/L 200 1.9 1 06/04/15 21:41 107-13-1 1.4 ug/L 1.0 0.25 1 06/04/15 21:41 71-43-2 ND ug/L 3.0 0.17 1 06/04/15 21:41 74-97-5 ND ug/L 1.0 0.18 1 06/04/15 21:41 75-27-4 ND ug/L 3.0 0.26 1 06/04/15 21:41 75-25-2 ND ug/L 10.0 0.29 1 06/04/15 21:41 74-83-9 ND ug/L 100 0.96 1 06/04/15 21:41 78-93-3 ND ug/L 100 1.2 1 06/04/15 21:41 75-15-0 ND ug/L 1.0 0.25 1 06/04/15 21:41 56-23-5 7.2 ug/L 3.0 0.23 1 06/04/15 21:41 108-90-7 0.97J ug/L 10.0 0.54 1 06/04/15 21:41 75-00-3 ND ug/L 5.0 0.14 1 06/04/15 21:41 67-66-3 ND ug/L 1.0 0.11 1 06/04/15 21:41 74-87-3 ND ug/L 13.0 2.0 1 06/04/15 21:41 96-12-8 ND ug/L 3.0 0.21 1 06/04/15 21:41 124-48-1 ND ug/L 1.0 0.27 1 06/04/15 21:41 106-93-4 ND ug/L 10.0 0.21 1 06/04/15 21:41 74-95-3 1.8J ug/L 5.0 0.30 1 06/04/15 21:41 95-50-1 18.7 ug/L 1.0 0.33 1 06/04/15 21:41 106-46-7 ND ug/L 100 1.0 1 06/04/15 21:41 110-57-6 2.3J ug/L 5.0 0.32 1 06/04/15 21:41 75-34-3 2.5 ug/L 1.0 0.12 1 06/04/15 21:41 107-06-2 ND ug/L 5.0 0.56 1 06/04/15 21:41 75-35-4 48.0 ug/L 5.0 0.19 1 06/04/15 21:41 156-59-2 0.50J ug/L 5.0 0.49 1 06/04/15 21:41 156-60-5 3.3 ug/L 1.0 0.27 1 06/04/15 21:41 78-87-5 ND ug/L 1.0 0.28 1 06/04/15 21:41 142-28-9 ND ug/L 1.0 0.13 1 06/04/15 21:41 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. L2 Page 13 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-16 Lab ID: 92252070004 Collected: 05/28/15 12:20 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 531013 TOC Total Organic Carbon Date: 06/12/2015 09:27 AM Analytical Method: EPA 8260 ND ug/L 1.0 0.26 1 06/04/15 21:41 10061-02-6 ND ug/L 1.0 0.30 1 06/04/15 21:41 100-41-4 ND ug/L 50.0 0.46 1 06/04/15 21:41 591-78-6 ND ug/L 10.0 0.32 1 06/04/15 21:41 74-88-4 ND ug/L 1.0 0.97 1 06/04/15 21:41 75-09-2 ND ug/L 100 0.33 1 06/04/15 21:41 108-10-1 ND ug/L 1.0 0.26 1 06/04/15 21:41 100-42-5 ND ug/L 5.0 0.33 1 06/04/15 21:41 630-20-6 ND ug/L 3.0 0.40 1 06/04/15 21:41 79-34-5 ND ug/L 1.0 0.46 1 06/04/15 21:41 127-18-4 ND ug/L 1.0 0.26 1 06/04/15 21:41 108-88-3 ND ug/L 1.0 0.48 1 06/04/15 21:41 71-55-6 ND ug/L 1.0 0.29 1 06/04/15 21:41 79-00-5 ND ug/L 1.0 0.47 1 06/04/15 21:41 79-01-6 ND ug/L 1.0 0.20 1 06/04/15 21:41 75-69-4 ND ug/L 1.0 0.41 1 06/04/15 21:41 96-18-4 ND ug/L 50.0 0.35 1 06/04/15 21:41 108-05-4 4.9 ug/L 1.0 0.62 1 06/04/15 21:41 75-01-4 ND ug/L 5.0 0.66 1 06/04/15 21:41 1330-20-7 94 % 70-130 1 06/04/15 21:41 460-00-4 103 % 70-130 1 06/04/15 21:41 17060-07-0 101 % 70-130 1 06/04/15 21:41 2037-26-5 Analytical Method: SM 2320B 124000 ug/L 5000 1000 1 06/10/1510:05 Analytical Method: EPA 300.0 8470J ug/L 250000 1000 1 06/06/15 01:07 14808-79-8 Analytical Method: SM 4500-CI-E 38300 ug/L 1000 500 1 06/06/15 07:00 16887-00-6 Analytical Method: SM 5310B 5990 ug/L 1000 500 1 06/06/15 01:25 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 14 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-17 Lab ID: 92252070005 Collected: 05/28/15 08:40 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane cis-1,3-Dichloropropene Date: 06/12/2015 09:27 AM Analytical Method: EPA 6010 Preparation Method: EPA 3010 ND ug/L 6.0 3.8 1 06/01/15 20:15 06/04/15 19:35 7440-36-0 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:35 7440-38-2 78.2J ug/L 100 2.5 1 06/01/15 20:15 06/04/15 19:35 7440-39-3 ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:35 7440-41-7 0.92J ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:35 7440-43-9 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:35 7440-47-3 26.3 ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:35 7440-48-4 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:35 7440-50-8 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:35 7439-92-1 7.6J ug/L 50.0 2.5 1 06/01/15 20:15 06/04/15 19:35 7440-02-0 ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:35 7782-49-2 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:35 7440-22-4 ND ug/L 5.5 5.0 1 06/01/15 20:15 06/04/15 19:35 7440-28-0 7.1J ug/L 25.0 2.5 1 06/01/15 20:15 06/04/15 19:35 7440-62-2 8.1J ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:35 7440-66-6 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 06/04/15 21:58 67-64-1 ND ug/L 200 1.9 1 06/04/15 21:58 107-13-1 ND ug/L 1.0 0.25 1 06/04/15 21:58 71-43-2 ND ug/L 3.0 0.17 1 06/04/15 21:58 74-97-5 ND ug/L 1.0 0.18 1 06/04/15 21:58 75-27-4 ND ug/L 3.0 0.26 1 06/04/15 21:58 75-25-2 ND ug/L 10.0 0.29 1 06/04/15 21:58 74-83-9 ND ug/L 100 0.96 1 06/04/15 21:58 78-93-3 ND ug/L 100 1.2 1 06/04/15 21:58 75-15-0 ND ug/L 1.0 0.25 1 06/04/15 21:58 56-23-5 ND ug/L 3.0 0.23 1 06/04/15 21:58 108-90-7 ND ug/L 10.0 0.54 1 06/04/15 21:58 75-00-3 ND ug/L 5.0 0.14 1 06/04/15 21:58 67-66-3 ND ug/L 1.0 0.11 1 06/04/15 21:58 74-87-3 ND ug/L 13.0 2.0 1 06/04/15 21:58 96-12-8 ND ug/L 3.0 0.21 1 06/04/15 21:58 124-48-1 ND ug/L 1.0 0.27 1 06/04/15 21:58 106-93-4 ND ug/L 10.0 0.21 1 06/04/15 21:58 74-95-3 ND ug/L 5.0 0.30 1 06/04/15 21:58 95-50-1 0.42J ug/L 1.0 0.33 1 06/04/15 21:58 106-46-7 ND ug/L 100 1.0 1 06/04/15 21:58 110-57-6 0.46J ug/L 5.0 0.32 1 06/04/15 21:58 75-34-3 0.14J ug/L 1.0 0.12 1 06/04/15 21:58 107-06-2 ND ug/L 5.0 0.56 1 06/04/15 21:58 75-35-4 0.74J ug/L 5.0 0.19 1 06/04/15 21:58 156-59-2 ND ug/L 5.0 0.49 1 06/04/15 21:58 156-60-5 ND ug/L 1.0 0.27 1 06/04/15 21:58 78-87-5 ND ug/L 1.0 0.28 1 06/04/15 21:58 142-28-9 ND ug/L 1.0 0.13 1 06/04/15 21:58 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. L2 Page 15 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-17 Lab ID: 92252070005 Collected: 05/28/15 08:40 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 531013 TOC Total Organic Carbon Date: 06/12/2015 09:27 AM Analytical Method: EPA 8260 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 100 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 1.0 ND ug/L 5.0 97 % 70-130 104 % 70-130 102 % 70-130 Analytical Method: SM 2320B 77000 ug/L 5000 Analytical Method: EPA 300.0 5390J ug/L 250000 Analytical Method: SM 4500-CI-E 42600 ug/L 5000 Analytical Method: SM 5310B 2330 ug/L 1000 0.26 1 06/04/15 21:58 10061-02-6 0.30 1 06/04/15 21:58 100-41-4 0.46 1 06/04/15 21:58 591-78-6 0.32 1 06/04/15 21:58 74-88-4 0.97 1 06/04/15 21:58 75-09-2 0.33 1 06/04/15 21:58 108-10-1 0.26 1 06/04/15 21:58 100-42-5 0.33 1 06/04/15 21:58 630-20-6 0.40 1 06/04/15 21:58 79-34-5 0.46 1 06/04/15 21:58 127-18-4 0.26 1 06/04/15 21:58 108-88-3 0.48 1 06/04/15 21:58 71-55-6 0.29 1 06/04/15 21:58 79-00-5 0.47 1 06/04/15 21:58 79-01-6 0.20 1 06/04/15 21:58 75-69-4 0.41 1 06/04/15 21:58 96-18-4 0.35 1 06/04/15 21:58 108-05-4 0.62 1 06/04/15 21:58 75-01-4 0.66 1 06/04/15 21:58 1330-20-7 1 06/04/15 21:58 460-00-4 1 06/04/15 21:58 17060-07-0 1 06/04/15 21:58 2037-26-5 1000 1 06/10/15 10:16 1000 1 06/06/15 01:21 14808-79-8 2500 5 500 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 06/06/15 07:20 16887-00-6 M1 06/06/15 01:25 7440-44-0 Page 16 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-18 Lab ID: 92252070006 Collected: 05/28/15 11:00 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane cis-1,3-Dichloropropene Date: 06/12/2015 09:27 AM Analytical Method: EPA 6010 Preparation Method: EPA 3010 ND ug/L 6.0 3.8 1 06/01/15 20:15 06/04/15 19:47 7440-36-0 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:47 7440-38-2 13.4J ug/L 100 2.5 1 06/01/15 20:15 06/04/15 19:47 7440-39-3 ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:47 7440-41-7 ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:47 7440-43-9 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:47 7440-47-3 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:47 7440-48-4 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:47 7440-50-8 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:47 7439-92-1 ND ug/L 50.0 2.5 1 06/01/15 20:15 06/04/15 19:47 7440-02-0 ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:47 7782-49-2 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:47 7440-22-4 ND ug/L 5.5 5.0 1 06/01/15 20:15 06/04/15 19:47 7440-28-0 ND ug/L 25.0 2.5 1 06/01/15 20:15 06/04/15 19:47 7440-62-2 ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:47 7440-66-6 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 06/04/15 22:31 67-64-1 ND ug/L 200 1.9 1 06/04/15 22:31 107-13-1 ND ug/L 1.0 0.25 1 06/04/15 22:31 71-43-2 ND ug/L 3.0 0.17 1 06/04/15 22:31 74-97-5 ND ug/L 1.0 0.18 1 06/04/15 22:31 75-27-4 ND ug/L 3.0 0.26 1 06/04/15 22:31 75-25-2 ND ug/L 10.0 0.29 1 06/04/15 22:31 74-83-9 ND ug/L 100 0.96 1 06/04/15 22:31 78-93-3 ND ug/L 100 1.2 1 06/04/15 22:31 75-15-0 ND ug/L 1.0 0.25 1 06/04/15 22:31 56-23-5 ND ug/L 3.0 0.23 1 06/04/15 22:31 108-90-7 ND ug/L 10.0 0.54 1 06/04/15 22:31 75-00-3 ND ug/L 5.0 0.14 1 06/04/15 22:31 67-66-3 ND ug/L 1.0 0.11 1 06/04/15 22:31 74-87-3 ND ug/L 13.0 2.0 1 06/04/15 22:31 96-12-8 ND ug/L 3.0 0.21 1 06/04/15 22:31 124-48-1 ND ug/L 1.0 0.27 1 06/04/15 22:31 106-93-4 ND ug/L 10.0 0.21 1 06/04/15 22:31 74-95-3 ND ug/L 5.0 0.30 1 06/04/15 22:31 95-50-1 ND ug/L 1.0 0.33 1 06/04/15 22:31 106-46-7 ND ug/L 100 1.0 1 06/04/15 22:31 110-57-6 ND ug/L 5.0 0.32 1 06/04/15 22:31 75-34-3 ND ug/L 1.0 0.12 1 06/04/15 22:31 107-06-2 ND ug/L 5.0 0.56 1 06/04/15 22:31 75-35-4 ND ug/L 5.0 0.19 1 06/04/15 22:31 156-59-2 ND ug/L 5.0 0.49 1 06/04/15 22:31 156-60-5 ND ug/L 1.0 0.27 1 06/04/15 22:31 78-87-5 ND ug/L 1.0 0.28 1 06/04/15 22:31 142-28-9 ND ug/L 1.0 0.13 1 06/04/15 22:31 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. L2.M0 M1 Page 17 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-18 Lab ID: 92252070006 Collected: 05/28/15 11:00 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 531013 TOC Total Organic Carbon Date: 06/12/2015 09:27 AM Analytical Method: EPA 8260 ND ug/L 1.0 0.26 1 06/04/15 22:31 10061-02-6 ND ug/L 1.0 0.30 1 06/04/15 22:31 100-41-4 ND ug/L 50.0 0.46 1 06/04/15 22:31 591-78-6 ND ug/L 10.0 0.32 1 06/04/15 22:31 74-88-4 ND ug/L 1.0 0.97 1 06/04/15 22:31 75-09-2 ND ug/L 100 0.33 1 06/04/15 22:31 108-10-1 ND ug/L 1.0 0.26 1 06/04/15 22:31 100-42-5 ND ug/L 5.0 0.33 1 06/04/15 22:31 630-20-6 ND ug/L 3.0 0.40 1 06/04/15 22:31 79-34-5 ND ug/L 1.0 0.46 1 06/04/15 22:31 127-18-4 ND ug/L 1.0 0.26 1 06/04/15 22:31 108-88-3 ND ug/L 1.0 0.48 1 06/04/15 22:31 71-55-6 ND ug/L 1.0 0.29 1 06/04/15 22:31 79-00-5 ND ug/L 1.0 0.47 1 06/04/15 22:31 79-01-6 ND ug/L 1.0 0.20 1 06/04/15 22:31 75-69-4 ND ug/L 1.0 0.41 1 06/04/15 22:31 96-18-4 ND ug/L 50.0 0.35 1 06/04/15 22:31 108-05-4 ND ug/L 1.0 0.62 1 06/04/15 22:31 75-01-4 ND ug/L 5.0 0.66 1 06/04/15 22:31 1330-20-7 96 % 70-130 1 06/04/15 22:31 460-00-4 102 % 70-130 1 06/04/15 22:31 17060-07-0 99 % 70-130 1 06/04/15 22:31 2037-26-5 Analytical Method: SM 2320B 8740 ug/L 5000 1000 1 06/10/1510:26 Analytical Method: EPA 300.0 15001 ug/L 250000 1000 1 06/06/15 01:34 14808-79-8 Analytical Method: SM 4500-CI-E 1250 ug/L 1000 500 1 06/06/15 07:03 16887-00-6 Analytical Method: SM 5310B ND ug/L 1000 500 1 06/06/15 01:25 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 18 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-19 Lab ID: 92252070007 Collected: 05/27/15 13:50 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 3.8 1 06/01/15 20:15 06/04/15 19:50 7440-36-0 Arsenic ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:50 7440-38-2 Barium 30.5J ug/L 100 2.5 1 06/01/15 20:15 06/04/15 19:50 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:50 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:50 7440-43-9 Chromium ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:50 7440-47-3 Cobalt ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:50 7440-48-4 Copper ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:50 7440-50-8 Lead ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:50 7439-92-1 Nickel ND ug/L 50.0 2.5 1 06/01/15 20:15 06/04/15 19:50 7440-02-0 Selenium ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:50 7782-49-2 Silver ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:50 7440-22-4 Thallium ND ug/L 5.5 5.0 1 06/01/15 20:15 06/04/15 19:50 7440-28-0 Vanadium ND ug/L 25.0 2.5 1 06/01/15 20:15 06/04/15 19:50 7440-62-2 Zinc ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:50 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 2.OJ ug/L 100 1 06/10/15 17:14 67-64-1 Acrylonitrile 0.01 ug/L 200 1 06/10/15 17:14 107-13-1 Benzene 0.01 ug/L 1.0 1 06/10/15 17:14 71-43-2 Bromochloromethane 0.01 ug/L 3.0 1 06/10/15 17:14 74-97-5 Bromodichloromethane 0.01 ug/L 1.0 1 06/10/15 17:14 75-27-4 Bromoform 0.01 ug/L 3.0 1 06/10/15 17:14 75-25-2 Bromomethane 0.01 ug/L 10.0 1 06/10/15 17:14 74-83-9 2-Butanone (MEK) 0.01 ug/L 100 1 06/10/15 17:14 78-93-3 Carbon disulfide 0.01 ug/L 100 1 06/10/15 17:14 75-15-0 Carbon tetrachloride 0.01 ug/L 1.0 1 06/10/15 17:14 56-23-5 Chlorobenzene 0.01 ug/L 3.0 1 06/10/15 17:14 108-90-7 Chloroethane 0.01 ug/L 10.0 1 06/10/15 17:14 75-00-3 Chloroform 0.01 ug/L 5.0 1 06/10/15 17:14 67-66-3 Chloromethane 0.01 ug/L 1.0 1 06/10/15 17:14 74-87-3 1,2-Dibromo-3-chloropropane 0.01 ug/L 13.0 1 06/10/15 17:14 96-12-8 Dibromochloromethane 0.01 ug/L 3.0 1 06/10/15 17:14 124-48-1 1,2-Dibromoethane (EDB) 0.01 ug/L 1.0 1 06/10/15 17:14 106-93-4 Dibromomethane 0.01 ug/L 10.0 1 06/10/15 17:14 74-95-3 1,2-Dichlorobenzene 0.01 ug/L 5.0 1 06/10/15 17:14 95-50-1 1,4-Dichlorobenzene 0.01 ug/L 1.0 1 06/10/15 17:14 106-46-7 trans-1,4-Dichloro-2-butene 0.01 ug/L 100 1 06/10/15 17:14 110-57-6 1,1-Dichloroethane 1.51 ug/L 5.0 1 06/10/15 17:14 75-34-3 1,2-Dichloroethane 0.01 ug/L 1.0 1 06/10/15 17:14 107-06-2 1,1-Dichloroethene 0.01 ug/L 5.0 1 06/10/15 17:14 75-35-4 cis-1,2-Dichloroethene 2.1J ug/L 5.0 1 06/10/15 17:14 156-59-2 trans-1,2-Dichloroethene 0.01 ug/L 5.0 1 06/10/15 17:14 156-60-5 1,2-Dichloropropane 0.01 ug/L 1.0 1 06/10/15 17:14 78-87-5 1,3-Dichloropropane 0.01 ug/L 1.0 1 06/10/15 17:14 142-28-9 cis-1,3-Dichloropropene 0.01 ug/L 1.0 1 06/10/15 17:14 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 19 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-19 Lab ID: 92252070007 Collected: 05/27/15 13:50 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 531013 TOC Total Organic Carbon Date: 06/12/2015 09:27 AM Analytical Method: EPA 8260 0.01 ug/L 1.0 1 06/10/1517:14 10061-02-6 0.01 ug/L 1.0 1 06/10/1517:14 100-41-4 0.21J ug/L 50.0 1 06/10/1517:14 591-78-6 0.01 ug/L 10.0 1 06/10/1517:14 74-88-4 0.01 ug/L 1.0 1 06/10/1517:14 75-09-2 0.01 ug/L 100 1 06/10/1517:14 108-10-1 0.01 ug/L 1.0 1 06/10/1517:14 100-42-5 0.01 ug/L 5.0 1 06/10/1517:14 630-20-6 0.01 ug/L 3.0 1 06/10/1517:14 79-34-5 0.35J ug/L 1.0 1 06/10/1517:14 127-18-4 0.01 ug/L 1.0 1 06/10/1517:14 108-88-3 0.01 ug/L 1.0 1 06/10/1517:14 71-55-6 0.01 ug/L 1.0 1 06/10/1517:14 79-00-5 0.29J ug/L 1.0 1 06/10/1517:14 79-01-6 0.01 ug/L 1.0 1 06/10/1517:14 75-69-4 0.01 ug/L 1.0 1 06/10/1517:14 96-18-4 0.01 ug/L 50.0 1 06/10/1517:14 108-05-4 0.01 ug/L 1.0 1 06/10/1517:14 75-01-4 0.0000000 ug/L 5.0 1 06/10/1517:14 1330-20-7 0010J 98 % 70-130 1 06/10/1517:14 460-00-4 95 % 70-130 1 06/10/1517:14 17060-07-0 99 % 70-130 1 06/10/1517:14 2037-26-5 Analytical Method: SM 2320B 16300 ug/L 5000 1000 1 06/08/1519:18 Analytical Method: EPA 300.0 1770J ug/L 250000 1000 1 06/06/15 01:48 14808-79-8 Analytical Method: SM 4500-CI-E 2610 ug/L 1000 500 1 06/06/15 07:07 16887-00-6 Analytical Method: SM 5310B ND ug/L 1000 500 1 06/06/15 01:25 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 20 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-22 Lab ID: 92252070008 Collected: 05/27/15 15:10 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 3.8 1 06/01/15 20:15 06/04/15 19:53 7440-36-0 Arsenic ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:53 7440-38-2 Barium 59.4J ug/L 100 2.5 1 06/01/15 20:15 06/04/15 19:53 7440-39-3 Beryllium 0.911 ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:53 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:53 7440-43-9 Chromium ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:53 7440-47-3 Cobalt 4.3J ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:53 7440-48-4 Copper 132 ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:53 7440-50-8 Lead ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:53 7439-92-1 Nickel 3.3J ug/L 50.0 2.5 1 06/01/15 20:15 06/04/15 19:53 7440-02-0 Selenium ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:53 7782-49-2 Silver ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:53 7440-22-4 Thallium ND ug/L 5.5 5.0 1 06/01/15 20:15 06/04/15 19:53 7440-28-0 Vanadium 2.6J ug/L 25.0 2.5 1 06/01/15 20:15 06/04/15 19:53 7440-62-2 Zinc 29.3 ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:53 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 0.01 ug/L 100 1 06/10/15 17:50 67-64-1 Acrylonitrile 0.01 ug/L 200 1 06/10/15 17:50 107-13-1 Benzene 0.25J ug/L 1.0 1 06/10/15 17:50 71-43-2 Bromochloromethane 0.01 ug/L 3.0 1 06/10/15 17:50 74-97-5 Bromodichloromethane 0.01 ug/L 1.0 1 06/10/15 17:50 75-27-4 Bromoform 0.01 ug/L 3.0 1 06/10/15 17:50 75-25-2 Bromomethane 0.01 ug/L 10.0 1 06/10/15 17:50 74-83-9 2-Butanone (MEK) 0.01 ug/L 100 1 06/10/15 17:50 78-93-3 Carbon disulfide 0.01 ug/L 100 1 06/10/15 17:50 75-15-0 Carbon tetrachloride 0.01 ug/L 1.0 1 06/10/15 17:50 56-23-5 Chlorobenzene 0.76J ug/L 3.0 1 06/10/15 17:50 108-90-7 Chloroethane 0.01 ug/L 10.0 1 06/10/15 17:50 75-00-3 Chloroform 0.01 ug/L 5.0 1 06/10/15 17:50 67-66-3 Chloromethane 0.01 ug/L 1.0 1 06/10/15 17:50 74-87-3 1,2-Dibromo-3-chloropropane 0.01 ug/L 13.0 1 06/10/15 17:50 96-12-8 Dibromochloromethane 0.01 ug/L 3.0 1 06/10/15 17:50 124-48-1 1,2-Dibromoethane (EDB) 0.01 ug/L 1.0 1 06/10/15 17:50 106-93-4 Dibromomethane 0.01 ug/L 10.0 1 06/10/15 17:50 74-95-3 1,2-Dichlorobenzene 0.511 ug/L 5.0 1 06/10/15 17:50 95-50-1 1,4-Dichlorobenzene 1.5 ug/L 1.0 1 06/10/15 17:50 106-46-7 trans-1,4-Dichloro-2-butene 0.01 ug/L 100 1 06/10/15 17:50 110-57-6 1,1-Dichloroethane 1.1J ug/L 5.0 1 06/10/15 17:50 75-34-3 1,2-Dichloroethane 0.24J ug/L 1.0 1 06/10/15 17:50 107-06-2 1,1-Dichloroethene 0.01 ug/L 5.0 1 06/10/15 17:50 75-35-4 cis-1,2-Dichloroethene 1.0J ug/L 5.0 1 06/10/15 17:50 156-59-2 trans-1,2-Dichloroethene 0.01 ug/L 5.0 1 06/10/15 17:50 156-60-5 1,2-Dichloropropane 0.01 ug/L 1.0 1 06/10/15 17:50 78-87-5 1,3-Dichloropropane 0.01 ug/L 1.0 1 06/10/15 17:50 142-28-9 cis-1,3-Dichloropropene 0.01 ug/L 1.0 1 06/10/15 17:50 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 21 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-22 Lab ID: 92252070008 Collected: 05/27/15 15:10 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 531013 TOC Total Organic Carbon Date: 06/12/2015 09:27 AM Analytical Method: EPA 8260 0.01 ug/L 1.0 1 06/10/1517:50 10061-02-6 0.01 ug/L 1.0 1 06/10/1517:50 100-41-4 0.01 ug/L 50.0 1 06/10/1517:50 591-78-6 0.01 ug/L 10.0 1 06/10/1517:50 74-88-4 0.01 ug/L 1.0 1 06/10/1517:50 75-09-2 0.01 ug/L 100 1 06/10/1517:50 108-10-1 0.01 ug/L 1.0 1 06/10/1517:50 100-42-5 0.01 ug/L 5.0 1 06/10/1517:50 630-20-6 0.01 ug/L 3.0 1 06/10/1517:50 79-34-5 0.01 ug/L 1.0 1 06/10/1517:50 127-18-4 0.01 ug/L 1.0 1 06/10/1517:50 108-88-3 0.01 ug/L 1.0 1 06/10/1517:50 71-55-6 0.01 ug/L 1.0 1 06/10/1517:50 79-00-5 0.01 ug/L 1.0 1 06/10/1517:50 79-01-6 0.01 ug/L 1.0 1 06/10/1517:50 75-69-4 0.01 ug/L 1.0 1 06/10/1517:50 96-18-4 0.01 ug/L 50.0 1 06/10/1517:50 108-05-4 0.13J ug/L 1.0 1 06/10/1517:50 75-01-4 0.0000000 ug/L 5.0 1 06/10/1517:50 1330-20-7 0010J 98 % 70-130 1 06/10/1517:50 460-00-4 95 % 70-130 1 06/10/1517:50 17060-07-0 100 % 70-130 1 06/10/1517:50 2037-26-5 Analytical Method: SM 2320B 111000 ug/L 5000 1000 1 06/08/1519:30 Analytical Method: EPA 300.0 3640J ug/L 250000 1000 1 06/06/15 02:29 14808-79-8 Analytical Method: SM 4500-CI-E 7310 ug/L 1000 500 1 06/06/15 07:07 16887-00-6 Analytical Method: SM 5310B 2050 ug/L 1000 500 1 06/06/15 01:25 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 22 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-23 Lab ID: 92252070009 Collected: 05/27/15 16:00 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 3.8 1 06/01/15 20:15 06/04/15 19:56 7440-36-0 Arsenic ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:56 7440-38-2 Barium 37.6J ug/L 100 2.5 1 06/01/15 20:15 06/04/15 19:56 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:56 7440-41-7 Cadmium 0.58J ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:56 7440-43-9 Chromium ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:56 7440-47-3 Cobalt ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:56 7440-48-4 Copper ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:56 7440-50-8 Lead ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:56 7439-92-1 Nickel ND ug/L 50.0 2.5 1 06/01/15 20:15 06/04/15 19:56 7440-02-0 Selenium ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:56 7782-49-2 Silver ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:56 7440-22-4 Thallium ND ug/L 5.5 5.0 1 06/01/15 20:15 06/04/15 19:56 7440-28-0 Vanadium 3.2J ug/L 25.0 2.5 1 06/01/15 20:15 06/04/15 19:56 7440-62-2 Zinc ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:56 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 1.91 ug/L 100 1 06/10/15 18:08 67-64-1 Acrylonitrile 0.01 ug/L 200 1 06/10/15 18:08 107-13-1 Benzene 0.01 ug/L 1.0 1 06/10/15 18:08 71-43-2 Bromochloromethane 0.01 ug/L 3.0 1 06/10/15 18:08 74-97-5 Bromodichloromethane 0.01 ug/L 1.0 1 06/10/15 18:08 75-27-4 Bromoform 0.01 ug/L 3.0 1 06/10/15 18:08 75-25-2 Bromomethane 0.01 ug/L 10.0 1 06/10/15 18:08 74-83-9 2-Butanone (MEK) 0.01 ug/L 100 1 06/10/15 18:08 78-93-3 Carbon disulfide 0.01 ug/L 100 1 06/10/15 18:08 75-15-0 Carbon tetrachloride 0.01 ug/L 1.0 1 06/10/15 18:08 56-23-5 Chlorobenzene 0.01 ug/L 3.0 1 06/10/15 18:08 108-90-7 Chloroethane 0.01 ug/L 10.0 1 06/10/15 18:08 75-00-3 Chloroform 0.01 ug/L 5.0 1 06/10/15 18:08 67-66-3 Chloromethane 0.01 ug/L 1.0 1 06/10/15 18:08 74-87-3 1,2-Dibromo-3-chloropropane 0.01 ug/L 13.0 1 06/10/15 18:08 96-12-8 Dibromochloromethane 0.01 ug/L 3.0 1 06/10/15 18:08 124-48-1 1,2-Dibromoethane (EDB) 0.01 ug/L 1.0 1 06/10/15 18:08 106-93-4 Dibromomethane 0.01 ug/L 10.0 1 06/10/15 18:08 74-95-3 1,2-Dichlorobenzene 0.01 ug/L 5.0 1 06/10/15 18:08 95-50-1 1,4-Dichlorobenzene 0.01 ug/L 1.0 1 06/10/15 18:08 106-46-7 trans-1,4-Dichloro-2-butene 0.01 ug/L 100 1 06/10/15 18:08 110-57-6 1,1-Dichloroethane 0.71J ug/L 5.0 1 06/10/15 18:08 75-34-3 1,2-Dichloroethane 0.01 ug/L 1.0 1 06/10/15 18:08 107-06-2 1,1-Dichloroethene 0.01 ug/L 5.0 1 06/10/15 18:08 75-35-4 cis-1,2-Dichloroethene 0.86J ug/L 5.0 1 06/10/15 18:08 156-59-2 trans-1,2-Dichloroethene 0.01 ug/L 5.0 1 06/10/15 18:08 156-60-5 1,2-Dichloropropane 0.01 ug/L 1.0 1 06/10/15 18:08 78-87-5 1,3-Dichloropropane 0.01 ug/L 1.0 1 06/10/15 18:08 142-28-9 cis-1,3-Dichloropropene 0.01 ug/L 1.0 1 06/10/15 18:08 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 23 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-23 Lab ID: 92252070009 Collected: 05/27/15 16:00 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 531013 TOC Total Organic Carbon Date: 06/12/2015 09:27 AM Analytical Method: EPA 8260 0.01 ug/L 1.0 1 06/10/1518:08 10061-02-6 0.01 ug/L 1.0 1 06/10/1518:08 100-41-4 0.01 ug/L 50.0 1 06/10/1518:08 591-78-6 0.01 ug/L 10.0 1 06/10/1518:08 74-88-4 0.01 ug/L 1.0 1 06/10/1518:08 75-09-2 0.01 ug/L 100 1 06/10/1518:08 108-10-1 0.01 ug/L 1.0 1 06/10/1518:08 100-42-5 0.01 ug/L 5.0 1 06/10/1518:08 630-20-6 0.01 ug/L 3.0 1 06/10/1518:08 79-34-5 0.01 ug/L 1.0 1 06/10/1518:08 127-18-4 0.01 ug/L 1.0 1 06/10/1518:08 108-88-3 0.01 ug/L 1.0 1 06/10/1518:08 71-55-6 0.01 ug/L 1.0 1 06/10/1518:08 79-00-5 0.01 ug/L 1.0 1 06/10/1518:08 79-01-6 0.01 ug/L 1.0 1 06/10/1518:08 75-69-4 0.01 ug/L 1.0 1 06/10/1518:08 96-18-4 0.01 ug/L 50.0 1 06/10/1518:08 108-05-4 0.01 ug/L 1.0 1 06/10/1518:08 75-01-4 0.0000000 ug/L 5.0 1 06/10/1518:08 1330-20-7 0010J 100 % 70-130 1 06/10/1518:08 460-00-4 98 % 70-130 1 06/10/1518:08 17060-07-0 99 % 70-130 1 06/10/1518:08 2037-26-5 Analytical Method: SM 2320B 15000 ug/L 5000 1000 1 06/08/1519:43 Analytical Method: EPA 300.0 1520J ug/L 250000 1000 1 06/06/15 02:42 14808-79-8 Analytical Method: SM 4500-CI-E 2660 ug/L 1000 500 1 06/06/15 07:08 16887-00-6 Analytical Method: SM 5310B ND ug/L 1000 500 1 06/06/15 01:25 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 24 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-3R Lab ID: 92252070010 Collected: 05/28/15 11:50 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane cis-1,3-Dichloropropene Date: 06/12/2015 09:27 AM Analytical Method: EPA 6010 Preparation Method: EPA 3010 ND ug/L 6.0 3.8 1 06/01/15 20:15 06/04/15 19:59 7440-36-0 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:59 7440-38-2 5.2J ug/L 100 2.5 1 06/01/15 20:15 06/04/15 19:59 7440-39-3 ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:59 7440-41-7 ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:59 7440-43-9 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:59 7440-47-3 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:59 7440-48-4 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:59 7440-50-8 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:59 7439-92-1 ND ug/L 50.0 2.5 1 06/01/15 20:15 06/04/15 19:59 7440-02-0 ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:59 7782-49-2 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:59 7440-22-4 ND ug/L 5.5 5.0 1 06/01/15 20:15 06/04/15 19:59 7440-28-0 ND ug/L 25.0 2.5 1 06/01/15 20:15 06/04/15 19:59 7440-62-2 ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:59 7440-66-6 Analytical Method: EPA 8260 2.1J ug/L 100 1 06/10/1519:58 67-64-1 0.01 ug/L 200 1 06/10/1519:58 107-13-1 0.01 ug/L 1.0 1 06/10/1519:58 71-43-2 0.01 ug/L 3.0 1 06/10/1519:58 74-97-5 0.01 ug/L 1.0 1 06/10/1519:58 75-27-4 0.01 ug/L 3.0 1 06/10/1519:58 75-25-2 0.01 ug/L 10.0 1 06/10/1519:58 74-83-9 0.01 ug/L 100 1 06/10/1519:58 78-93-3 0.01 ug/L 100 1 06/10/1519:58 75-15-0 0.01 ug/L 1.0 1 06/10/1519:58 56-23-5 0.01 ug/L 3.0 1 06/10/1519:58 108-90-7 0.01 ug/L 10.0 1 06/10/1519:58 75-00-3 0.01 ug/L 5.0 1 06/10/1519:58 67-66-3 0.01 ug/L 1.0 1 06/10/1519:58 74-87-3 0.01 ug/L 13.0 1 06/10/1519:58 96-12-8 0.01 ug/L 3.0 1 06/10/1519:58 124-48-1 0.01 ug/L 1.0 1 06/10/1519:58 106-93-4 0.01 ug/L 10.0 1 06/10/1519:58 74-95-3 0.01 ug/L 5.0 1 06/10/1519:58 95-50-1 0.11J ug/L 1.0 1 06/10/1519:58 106-46-7 0.01 ug/L 100 1 06/10/1519:58 110-57-6 0.151 ug/L 5.0 1 06/10/1519:58 75-34-3 0.01 ug/L 1.0 1 06/10/1519:58 107-06-2 0.01 ug/L 5.0 1 06/10/1519:58 75-35-4 0.01 ug/L 5.0 1 06/10/1519:58 156-59-2 0.01 ug/L 5.0 1 06/10/1519:58 156-60-5 0.01 ug/L 1.0 1 06/10/1519:58 78-87-5 0.01 ug/L 1.0 1 06/10/1519:58 142-28-9 0.01 ug/L 1.0 1 06/10/1519:58 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 25 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-3R Lab ID: 92252070010 Collected: 05/28/15 11:50 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 531013 TOC Total Organic Carbon Date: 06/12/2015 09:27 AM Analytical Method: EPA 8260 0.01 ug/L 1.0 1 06/10/1519:58 10061-02-6 0.01 ug/L 1.0 1 06/10/1519:58 100-41-4 0.01 ug/L 50.0 1 06/10/1519:58 591-78-6 0.01 ug/L 10.0 1 06/10/1519:58 74-88-4 0.01 ug/L 1.0 1 06/10/1519:58 75-09-2 0.01 ug/L 100 1 06/10/1519:58 108-10-1 0.01 ug/L 1.0 1 06/10/1519:58 100-42-5 0.01 ug/L 5.0 1 06/10/1519:58 630-20-6 0.01 ug/L 3.0 1 06/10/1519:58 79-34-5 0.01 ug/L 1.0 1 06/10/1519:58 127-18-4 0.01 ug/L 1.0 1 06/10/1519:58 108-88-3 0.01 ug/L 1.0 1 06/10/1519:58 71-55-6 0.01 ug/L 1.0 1 06/10/1519:58 79-00-5 0.01 ug/L 1.0 1 06/10/1519:58 79-01-6 0.01 ug/L 1.0 1 06/10/1519:58 75-69-4 0.01 ug/L 1.0 1 06/10/1519:58 96-18-4 0.01 ug/L 50.0 1 06/10/1519:58 108-05-4 0.01 ug/L 1.0 1 06/10/1519:58 75-01-4 0.0000000 ug/L 5.0 1 06/10/1519:58 1330-20-7 0010J 97 % 70-130 1 06/10/1519:58 460-00-4 102 % 70-130 1 06/10/1519:58 17060-07-0 100 % 70-130 1 06/10/1519:58 2037-26-5 Analytical Method: SM 2320B 131000 ug/L 5000 1000 1 06/10/1510:36 Analytical Method: EPA 300.0 2210J ug/L 250000 1000 1 06/09/1518:24 14808-79-8 Analytical Method: SM 4500-CI-E 3250 ug/L 1000 500 1 06/06/15 07:09 16887-00-6 Analytical Method: SM 5310B 1260 ug/L 1000 500 1 06/06/15 01:25 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 26 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-20 Lab ID: 92252070011 Collected: 05/28/15 15:30 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 3.8 1 06/01/15 20:15 06/04/15 20:03 7440-36-0 Arsenic ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:03 7440-38-2 Barium 24.3J ug/L 100 2.5 1 06/01/15 20:15 06/04/15 20:03 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 20:03 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 20:03 7440-43-9 Chromium ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:03 7440-47-3 Cobalt 17.4 ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:03 7440-48-4 Copper ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:03 7440-50-8 Lead ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:03 7439-92-1 Nickel ND ug/L 50.0 2.5 1 06/01/15 20:15 06/04/15 20:03 7440-02-0 Selenium ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 20:03 7782-49-2 Silver ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:03 7440-22-4 Thallium ND ug/L 5.5 5.0 1 06/01/15 20:15 06/04/15 20:03 7440-28-0 Vanadium 3.2J ug/L 25.0 2.5 1 06/01/15 20:15 06/04/15 20:03 7440-62-2 Zinc 6.3J ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 20:03 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 1.7J ug/L 100 1 06/10/15 20:34 67-64-1 Acrylonitrile 0.01 ug/L 200 1 06/10/15 20:34 107-13-1 Benzene 0.01 ug/L 1.0 1 06/10/15 20:34 71-43-2 Bromochloromethane 0.01 ug/L 3.0 1 06/10/15 20:34 74-97-5 Bromodichloromethane 0.01 ug/L 1.0 1 06/10/15 20:34 75-27-4 Bromoform 0.01 ug/L 3.0 1 06/10/15 20:34 75-25-2 Bromomethane 0.01 ug/L 10.0 1 06/10/15 20:34 74-83-9 2-Butanone (MEK) 0.01 ug/L 100 1 06/10/15 20:34 78-93-3 Carbon disulfide 0.01 ug/L 100 1 06/10/15 20:34 75-15-0 Carbon tetrachloride 0.01 ug/L 1.0 1 06/10/15 20:34 56-23-5 Chlorobenzene 0.01 ug/L 3.0 1 06/10/15 20:34 108-90-7 Chloroethane 0.01 ug/L 10.0 1 06/10/15 20:34 75-00-3 Chloroform 0.01 ug/L 5.0 1 06/10/15 20:34 67-66-3 Chloromethane 0.01 ug/L 1.0 1 06/10/15 20:34 74-87-3 1,2-Dibromo-3-chloropropane 0.01 ug/L 13.0 1 06/10/15 20:34 96-12-8 Dibromochloromethane 0.01 ug/L 3.0 1 06/10/15 20:34 124-48-1 1,2-Dibromoethane (EDB) 0.01 ug/L 1.0 1 06/10/15 20:34 106-93-4 Dibromomethane 0.01 ug/L 10.0 1 06/10/15 20:34 74-95-3 1,2-Dichlorobenzene 0.01 ug/L 5.0 1 06/10/15 20:34 95-50-1 1,4-Dichlorobenzene 0.25J ug/L 1.0 1 06/10/15 20:34 106-46-7 trans-1,4-Dichloro-2-butene 0.01 ug/L 100 1 06/10/15 20:34 110-57-6 1,1-Dichloroethane 0.23J ug/L 5.0 1 06/10/15 20:34 75-34-3 1,2-Dichloroethane 0.01 ug/L 1.0 1 06/10/15 20:34 107-06-2 1,1-Dichloroethene 0.01 ug/L 5.0 1 06/10/15 20:34 75-35-4 cis-1,2-Dichloroethene 0.66J ug/L 5.0 1 06/10/15 20:34 156-59-2 trans-1,2-Dichloroethene 0.01 ug/L 5.0 1 06/10/15 20:34 156-60-5 1,2-Dichloropropane 0.01 ug/L 1.0 1 06/10/15 20:34 78-87-5 1,3-Dichloropropane 0.01 ug/L 1.0 1 06/10/15 20:34 142-28-9 cis-1,3-Dichloropropene 0.01 ug/L 1.0 1 06/10/15 20:34 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 27 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-20 Lab ID: 92252070011 Collected: 05/28/15 15:30 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene 0.01 ug/L 1.0 1 06/10/15 20:34 10061-02-6 Ethylbenzene 0.01 ug/L 1.0 1 06/10/15 20:34 100-41-4 2-Hexanone 0.01 ug/L 50.0 1 06/10/15 20:34 591-78-6 lodomethane 0.01 ug/L 10.0 1 06/10/15 20:34 74-88-4 Methylene Chloride 0.01 ug/L 1.0 1 06/10/15 20:34 75-09-2 4-Methyl-2-pentanone (MIBK) 0.01 ug/L 100 1 06/10/15 20:34 108-10-1 Styrene 0.01 ug/L 1.0 1 06/10/15 20:34 100-42-5 1,1,1,2-Tetrachloroethane 0.01 ug/L 5.0 1 06/10/15 20:34 630-20-6 1,1,2,2-Tetrachloroethane 0.01 ug/L 3.0 1 06/10/15 20:34 79-34-5 Tetrachloroethene 0.01 ug/L 1.0 1 06/10/15 20:34 127-18-4 Toluene 0.01 ug/L 1.0 1 06/10/15 20:34 108-88-3 1,1,1-Trichloroethane 0.01 ug/L 1.0 1 06/10/15 20:34 71-55-6 1,1,2-Trichloroethane 0.01 ug/L 1.0 1 06/10/15 20:34 79-00-5 Trichloroethene 0.01 ug/L 1.0 1 06/10/15 20:34 79-01-6 Trichlorofluoromethane 0.01 ug/L 1.0 1 06/10/15 20:34 75-69-4 1,2,3-Trichloropropane 0.01 ug/L 1.0 1 06/10/15 20:34 96-18-4 Vinyl acetate 0.01 ug/L 50.0 1 06/10/15 20:34 108-05-4 Vinyl chloride 0.11J ug/L 1.0 1 06/10/15 20:34 75-01-4 Xylene (Total) 0.0000000 ug/L 5.0 1 06/10/15 20:34 1330-20-7 MS 0010J Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 06/10/15 20:34 460-00-4 1,2-Dichloroethane-d4 (S) 104 % 70-130 1 06/10/15 20:34 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 06/10/15 20:34 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 8200 ug/L 5000 1000 1 06/10/15 11:06 M1 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate 1060J ug/L 250000 1000 1 06/09/1518:38 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E Chloride 13900 ug/L 1000 500 1 06/06/15 07:10 16887-00-6 Date: 06/12/2015 09:27 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 28 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-14 Lab ID: 92252070012 Collected: 05/28/15 14:40 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 3.8 1 06/01/15 20:15 06/04/15 20:06 7440-36-0 Arsenic ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:06 7440-38-2 Barium 23.6J ug/L 100 2.5 1 06/01/15 20:15 06/04/15 20:06 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 20:06 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 20:06 7440-43-9 Chromium ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:06 7440-47-3 Cobalt ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:06 7440-48-4 Copper 6.4J ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:06 7440-50-8 Lead ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:06 7439-92-1 Nickel ND ug/L 50.0 2.5 1 06/01/15 20:15 06/04/15 20:06 7440-02-0 Selenium ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 20:06 7782-49-2 Silver ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:06 7440-22-4 Thallium ND ug/L 5.5 5.0 1 06/01/15 20:15 06/04/15 20:06 7440-28-0 Vanadium ND ug/L 25.0 2.5 1 06/01/15 20:15 06/04/15 20:06 7440-62-2 Zinc ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 20:06 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 1.91 ug/L 100 1 06/10/15 19:21 67-64-1 Acrylonitrile 0.01 ug/L 200 1 06/10/15 19:21 107-13-1 Benzene 0.01 ug/L 1.0 1 06/10/15 19:21 71-43-2 Bromochloromethane 0.01 ug/L 3.0 1 06/10/15 19:21 74-97-5 Bromodichloromethane 0.01 ug/L 1.0 1 06/10/15 19:21 75-27-4 Bromoform 0.01 ug/L 3.0 1 06/10/15 19:21 75-25-2 Bromomethane 0.01 ug/L 10.0 1 06/10/15 19:21 74-83-9 2-Butanone (MEK) 0.01 ug/L 100 1 06/10/15 19:21 78-93-3 Carbon disulfide 0.01 ug/L 100 1 06/10/15 19:21 75-15-0 Carbon tetrachloride 0.01 ug/L 1.0 1 06/10/15 19:21 56-23-5 Chlorobenzene 0.01 ug/L 3.0 1 06/10/15 19:21 108-90-7 Chloroethane 0.01 ug/L 10.0 1 06/10/15 19:21 75-00-3 Chloroform 0.01 ug/L 5.0 1 06/10/15 19:21 67-66-3 Chloromethane 0.01 ug/L 1.0 1 06/10/15 19:21 74-87-3 1,2-Dibromo-3-chloropropane 0.01 ug/L 13.0 1 06/10/15 19:21 96-12-8 Dibromochloromethane 0.01 ug/L 3.0 1 06/10/15 19:21 124-48-1 1,2-Dibromoethane (EDB) 0.01 ug/L 1.0 1 06/10/15 19:21 106-93-4 Dibromomethane 0.01 ug/L 10.0 1 06/10/15 19:21 74-95-3 1,2-Dichlorobenzene 0.01 ug/L 5.0 1 06/10/15 19:21 95-50-1 1,4-Dichlorobenzene 0.34J ug/L 1.0 1 06/10/15 19:21 106-46-7 trans-1,4-Dichloro-2-butene 0.01 ug/L 100 1 06/10/15 19:21 110-57-6 1,1-Dichloroethane 5.0 ug/L 5.0 1 06/10/15 19:21 75-34-3 1,2-Dichloroethane 0.01 ug/L 1.0 1 06/10/15 19:21 107-06-2 1,1-Dichloroethene 0.01 ug/L 5.0 1 06/10/15 19:21 75-35-4 cis-1,2-Dichloroethene 6.1 ug/L 5.0 1 06/10/15 19:21 156-59-2 trans-1,2-Dichloroethene 0.01 ug/L 5.0 1 06/10/15 19:21 156-60-5 1,2-Dichloropropane 0.01 ug/L 1.0 1 06/10/15 19:21 78-87-5 1,3-Dichloropropane 0.01 ug/L 1.0 1 06/10/15 19:21 142-28-9 cis-1,3-Dichloropropene 0.01 ug/L 1.0 1 06/10/15 19:21 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 29 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-14 Lab ID: 92252070012 Collected: 05/28/15 14:40 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 5220D COD Chemical Oxygen Demand 5310B TOC Total Organic Carbon Date: 06/12/2015 09:27 AM Analytical Method: EPA 8260 0.01 ug/L 1.0 1 06/10/1519:21 10061-02-6 0.01 ug/L 1.0 1 06/10/1519:21 100-41-4 0.01 ug/L 50.0 1 06/10/1519:21 591-78-6 0.01 ug/L 10.0 1 06/10/1519:21 74-88-4 0.01 ug/L 1.0 1 06/10/1519:21 75-09-2 0.01 ug/L 100 1 06/10/1519:21 108-10-1 0.01 ug/L 1.0 1 06/10/1519:21 100-42-5 0.01 ug/L 5.0 1 06/10/1519:21 630-20-6 0.01 ug/L 3.0 1 06/10/1519:21 79-34-5 0.95J ug/L 1.0 1 06/10/1519:21 127-18-4 0.01 ug/L 1.0 1 06/10/1519:21 108-88-3 0.01 ug/L 1.0 1 06/10/1519:21 71-55-6 0.01 ug/L 1.0 1 06/10/1519:21 79-00-5 0.981 ug/L 1.0 1 06/10/1519:21 79-01-6 0.01 ug/L 1.0 1 06/10/1519:21 75-69-4 0.01 ug/L 1.0 1 06/10/1519:21 96-18-4 0.01 ug/L 50.0 1 06/10/1519:21 108-05-4 0.01 ug/L 1.0 1 06/10/1519:21 75-01-4 0.0000000 ug/L 5.0 1 06/10/1519:21 1330-20-7 0010J 99 % 70-130 1 06/10/1519:21 460-00-4 99 % 70-130 1 06/10/1519:21 17060-07-0 100 % 70-130 1 06/10/1519:21 2037-26-5 Analytical Method: SM 2320B 34000 ug/L 5000 1000 1 06/10/1511:34 Analytical Method: EPA 300.0 2730J ug/L 250000 1000 1 06/09/1518:51 14808-79-8 Analytical Method: SM 4500-CI-E 2540 ug/L 1000 500 1 06/06/15 07:11 16887-00-6 Analytical Method: SM 5220D ND ug/L 25000 12500 1 06/02/15 09:50 Analytical Method: SM 5310B ND ug/L 1000 500 1 06/06/15 01:25 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 30 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-15 Lab ID: 92252070013 Collected: 05/28/15 13:40 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 3.8 1 06/01/15 20:15 06/04/15 20:09 7440-36-0 Arsenic ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:09 7440-38-2 Barium 50.1J ug/L 100 2.5 1 06/01/15 20:15 06/04/15 20:09 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 20:09 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 20:09 7440-43-9 Chromium ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:09 7440-47-3 Cobalt 3.3J ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:09 7440-48-4 Copper ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:09 7440-50-8 Lead ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:09 7439-92-1 Nickel 3.5J ug/L 50.0 2.5 1 06/01/15 20:15 06/04/15 20:09 7440-02-0 Selenium ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 20:09 7782-49-2 Silver ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:09 7440-22-4 Thallium ND ug/L 5.5 5.0 1 06/01/15 20:15 06/04/15 20:09 7440-28-0 Vanadium 3.9J ug/L 25.0 2.5 1 06/01/15 20:15 06/04/15 20:09 7440-62-2 Zinc 12.5 ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 20:09 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 1.4J ug/L 100 1 06/10/15 18:27 67-64-1 Acrylonitrile 0.01 ug/L 200 1 06/10/15 18:27 107-13-1 Benzene 1.6 ug/L 1.0 1 06/10/15 18:27 71-43-2 Bromochloromethane 0.01 ug/L 3.0 1 06/10/15 18:27 74-97-5 Bromodichloromethane 0.01 ug/L 1.0 1 06/10/15 18:27 75-27-4 Bromoform 0.01 ug/L 3.0 1 06/10/15 18:27 75-25-2 Bromomethane 0.01 ug/L 10.0 1 06/10/15 18:27 74-83-9 2-Butanone (MEK) 0.01 ug/L 100 1 06/10/15 18:27 78-93-3 Carbon disulfide 0.01 ug/L 100 1 06/10/15 18:27 75-15-0 Carbon tetrachloride 0.01 ug/L 1.0 1 06/10/15 18:27 56-23-5 Chlorobenzene 2.8J ug/L 3.0 1 06/10/15 18:27 108-90-7 Chloroethane 0.65J ug/L 10.0 1 06/10/15 18:27 75-00-3 Chloroform 0.01 ug/L 5.0 1 06/10/15 18:27 67-66-3 Chloromethane 0.01 ug/L 1.0 1 06/10/15 18:27 74-87-3 1,2-Dibromo-3-chloropropane 0.01 ug/L 13.0 1 06/10/15 18:27 96-12-8 Dibromochloromethane 0.01 ug/L 3.0 1 06/10/15 18:27 124-48-1 1,2-Dibromoethane (EDB) 0.01 ug/L 1.0 1 06/10/15 18:27 106-93-4 Dibromomethane 0.01 ug/L 10.0 1 06/10/15 18:27 74-95-3 1,2-Dichlorobenzene 0.18J ug/L 5.0 1 06/10/15 18:27 95-50-1 1,4-Dichlorobenzene 4.3 ug/L 1.0 1 06/10/15 18:27 106-46-7 trans-1,4-Dichloro-2-butene 0.01 ug/L 100 1 06/10/15 18:27 110-57-6 1,1-Dichloroethane 13.6 ug/L 5.0 1 06/10/15 18:27 75-34-3 1,2-Dichloroethane 0.65J ug/L 1.0 1 06/10/15 18:27 107-06-2 1,1-Dichloroethene 0.01 ug/L 5.0 1 06/10/15 18:27 75-35-4 cis-1,2-Dichloroethene 40.2 ug/L 5.0 1 06/10/15 18:27 156-59-2 trans-1,2-Dichloroethene 0.35J ug/L 5.0 1 06/10/15 18:27 156-60-5 1,2-Dichloropropane 0.01 ug/L 1.0 1 06/10/15 18:27 78-87-5 1,3-Dichloropropane 0.01 ug/L 1.0 1 06/10/15 18:27 142-28-9 cis-1,3-Dichloropropene 0.01 ug/L 1.0 1 06/10/15 18:27 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 31 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-15 Lab ID: 92252070013 Collected: 05/28/15 13:40 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 5220D COD Chemical Oxygen Demand 5310B TOC Total Organic Carbon Date: 06/12/2015 09:27 AM Analytical Method: EPA 8260 0.01 ug/L 1.0 1 06/10/1518:27 10061-02-6 0.01 ug/L 1.0 1 06/10/1518:27 100-41-4 0.01 ug/L 50.0 1 06/10/1518:27 591-78-6 0.01 ug/L 10.0 1 06/10/1518:27 74-88-4 0.01 ug/L 1.0 1 06/10/1518:27 75-09-2 0.01 ug/L 100 1 06/10/1518:27 108-10-1 0.01 ug/L 1.0 1 06/10/1518:27 100-42-5 0.01 ug/L 5.0 1 06/10/1518:27 630-20-6 0.01 ug/L 3.0 1 06/10/1518:27 79-34-5 0.67J ug/L 1.0 1 06/10/1518:27 127-18-4 0.01 ug/L 1.0 1 06/10/1518:27 108-88-3 0.01 ug/L 1.0 1 06/10/1518:27 71-55-6 0.01 ug/L 1.0 1 06/10/1518:27 79-00-5 2.9 ug/L 1.0 1 06/10/1518:27 79-01-6 0.01 ug/L 1.0 1 06/10/1518:27 75-69-4 0.01 ug/L 1.0 1 06/10/1518:27 96-18-4 0.01 ug/L 50.0 1 06/10/1518:27 108-05-4 1.5 ug/L 1.0 1 06/10/1518:27 75-01-4 0.0000000 ug/L 5.0 1 06/10/1518:27 1330-20-7 0010J 99 % 70-130 1 06/10/1518:27 460-00-4 98 % 70-130 1 06/10/1518:27 17060-07-0 99 % 70-130 1 06/10/1518:27 2037-26-5 Analytical Method: SM 2320B 41800 ug/L 5000 1000 1 06/10/1511:45 Analytical Method: EPA 300.0 1760J ug/L 250000 1000 1 06/09/1519:05 14808-79-8 Analytical Method: SM 4500-CI-E 1690 ug/L 1000 500 1 06/06/15 07:11 16887-00-6 Analytical Method: SM 5220D ND ug/L 25000 12500 1 06/02/15 09:35 Analytical Method: SM 5310B 827J ug/L 1000 500 1 06/06/15 01:25 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 32 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-1 Lab ID: 92252070014 Collected: 05/28/15 08:15 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 3.8 1 06/01/15 20:15 06/04/15 20:12 7440-36-0 Arsenic ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:12 7440-38-2 Barium 68.3J ug/L 100 2.5 1 06/01/15 20:15 06/04/15 20:12 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 20:12 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 20:12 7440-43-9 Chromium ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:12 7440-47-3 Cobalt ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:12 7440-48-4 Copper ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:12 7440-50-8 Lead ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:12 7439-92-1 Nickel ND ug/L 50.0 2.5 1 06/01/15 20:15 06/04/15 20:12 7440-02-0 Selenium ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 20:12 7782-49-2 Silver ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:12 7440-22-4 Thallium ND ug/L 5.5 5.0 1 06/01/15 20:15 06/04/15 20:12 7440-28-0 Vanadium ND ug/L 25.0 2.5 1 06/01/15 20:15 06/04/15 20:12 7440-62-2 Zinc 13.6 ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 20:12 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 1.91 ug/L 100 1 06/10/15 18:45 67-64-1 Acrylonitrile 0.01 ug/L 200 1 06/10/15 18:45 107-13-1 Benzene 0.01 ug/L 1.0 1 06/10/15 18:45 71-43-2 Bromochloromethane 0.01 ug/L 3.0 1 06/10/15 18:45 74-97-5 Bromodichloromethane 0.01 ug/L 1.0 1 06/10/15 18:45 75-27-4 Bromoform 0.01 ug/L 3.0 1 06/10/15 18:45 75-25-2 Bromomethane 0.01 ug/L 10.0 1 06/10/15 18:45 74-83-9 2-Butanone (MEK) 0.01 ug/L 100 1 06/10/15 18:45 78-93-3 Carbon disulfide 0.01 ug/L 100 1 06/10/15 18:45 75-15-0 Carbon tetrachloride 0.01 ug/L 1.0 1 06/10/15 18:45 56-23-5 Chlorobenzene 0.01 ug/L 3.0 1 06/10/15 18:45 108-90-7 Chloroethane 0.01 ug/L 10.0 1 06/10/15 18:45 75-00-3 Chloroform 0.01 ug/L 5.0 1 06/10/15 18:45 67-66-3 Chloromethane 0.01 ug/L 1.0 1 06/10/15 18:45 74-87-3 1,2-Dibromo-3-chloropropane 0.01 ug/L 13.0 1 06/10/15 18:45 96-12-8 Dibromochloromethane 0.01 ug/L 3.0 1 06/10/15 18:45 124-48-1 1,2-Dibromoethane (EDB) 0.01 ug/L 1.0 1 06/10/15 18:45 106-93-4 Dibromomethane 0.01 ug/L 10.0 1 06/10/15 18:45 74-95-3 1,2-Dichlorobenzene 0.01 ug/L 5.0 1 06/10/15 18:45 95-50-1 1,4-Dichlorobenzene 0.01 ug/L 1.0 1 06/10/15 18:45 106-46-7 trans-1,4-Dichloro-2-butene 0.01 ug/L 100 1 06/10/15 18:45 110-57-6 1,1-Dichloroethane 0.01 ug/L 5.0 1 06/10/15 18:45 75-34-3 1,2-Dichloroethane 0.01 ug/L 1.0 1 06/10/15 18:45 107-06-2 1,1-Dichloroethene 0.01 ug/L 5.0 1 06/10/15 18:45 75-35-4 cis-1,2-Dichloroethene 0.01 ug/L 5.0 1 06/10/15 18:45 156-59-2 trans-1,2-Dichloroethene 0.01 ug/L 5.0 1 06/10/15 18:45 156-60-5 1,2-Dichloropropane 0.01 ug/L 1.0 1 06/10/15 18:45 78-87-5 1,3-Dichloropropane 0.01 ug/L 1.0 1 06/10/15 18:45 142-28-9 cis-1,3-Dichloropropene 0.01 ug/L 1.0 1 06/10/15 18:45 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 33 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-1 Lab ID: 92252070014 Collected: 05/28/15 08:15 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 5220D COD Chemical Oxygen Demand 5310B TOC Total Organic Carbon Date: 06/12/2015 09:27 AM Analytical Method: EPA 8260 0.01 ug/L 1.0 1 06/10/1518:45 10061-02-6 0.01 ug/L 1.0 1 06/10/1518:45 100-41-4 0.01 ug/L 50.0 1 06/10/1518:45 591-78-6 0.01 ug/L 10.0 1 06/10/1518:45 74-88-4 0.01 ug/L 1.0 1 06/10/1518:45 75-09-2 0.01 ug/L 100 1 06/10/1518:45 108-10-1 0.01 ug/L 1.0 1 06/10/1518:45 100-42-5 0.01 ug/L 5.0 1 06/10/1518:45 630-20-6 0.01 ug/L 3.0 1 06/10/1518:45 79-34-5 0.01 ug/L 1.0 1 06/10/1518:45 127-18-4 0.01 ug/L 1.0 1 06/10/1518:45 108-88-3 0.01 ug/L 1.0 1 06/10/1518:45 71-55-6 0.01 ug/L 1.0 1 06/10/1518:45 79-00-5 0.01 ug/L 1.0 1 06/10/1518:45 79-01-6 0.01 ug/L 1.0 1 06/10/1518:45 75-69-4 0.01 ug/L 1.0 1 06/10/1518:45 96-18-4 0.01 ug/L 50.0 1 06/10/1518:45 108-05-4 0.01 ug/L 1.0 1 06/10/1518:45 75-01-4 0.0000000 ug/L 5.0 1 06/10/1518:45 1330-20-7 0010J 98 % 70-130 1 06/10/1518:45 460-00-4 102 % 70-130 1 06/10/1518:45 17060-07-0 99 % 70-130 1 06/10/1518:45 2037-26-5 Analytical Method: SM 2320B 78800 ug/L 5000 1000 1 06/10/1511:55 Analytical Method: EPA 300.0 8090J ug/L 250000 1000 1 06/09/1519:19 14808-79-8 Analytical Method: SM 4500-CI-E 3600 ug/L 1000 500 1 06/06/15 07:12 16887-00-6 Analytical Method: SM 5220D ND ug/L 25000 12500 1 06/02/15 09:35 Analytical Method: SM 5310B 710J ug/L 1000 500 1 06/06/15 01:25 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 34 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-21 Lab ID: 92252070015 Collected: 05/27/15 14:35 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 3.8 1 06/01/15 20:15 06/04/15 20:15 7440-36-0 Arsenic ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:15 7440-38-2 Barium 53.9J ug/L 100 2.5 1 06/01/15 20:15 06/04/15 20:15 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 20:15 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 20:15 7440-43-9 Chromium ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:15 7440-47-3 Cobalt 4.5J ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:15 7440-48-4 Copper 3.5J ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:15 7440-50-8 Lead ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:15 7439-92-1 Nickel ND ug/L 50.0 2.5 1 06/01/15 20:15 06/04/15 20:15 7440-02-0 Selenium ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 20:15 7782-49-2 Silver ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:15 7440-22-4 Thallium ND ug/L 5.5 5.0 1 06/01/15 20:15 06/04/15 20:15 7440-28-0 Vanadium ND ug/L 25.0 2.5 1 06/01/15 20:15 06/04/15 20:15 7440-62-2 Zinc ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 20:15 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 2.5J ug/L 100 1 06/10/15 17:32 67-64-1 Acrylonitrile 0.01 ug/L 200 1 06/10/15 17:32 107-13-1 Benzene 0.01 ug/L 1.0 1 06/10/15 17:32 71-43-2 Bromochloromethane 0.01 ug/L 3.0 1 06/10/15 17:32 74-97-5 Bromodichloromethane 0.01 ug/L 1.0 1 06/10/15 17:32 75-27-4 Bromoform 0.01 ug/L 3.0 1 06/10/15 17:32 75-25-2 Bromomethane 0.01 ug/L 10.0 1 06/10/15 17:32 74-83-9 2-Butanone (MEK) 0.01 ug/L 100 1 06/10/15 17:32 78-93-3 Carbon disulfide 0.01 ug/L 100 1 06/10/15 17:32 75-15-0 Carbon tetrachloride 0.01 ug/L 1.0 1 06/10/15 17:32 56-23-5 Chlorobenzene 0.01 ug/L 3.0 1 06/10/15 17:32 108-90-7 Chloroethane 0.24J ug/L 10.0 1 06/10/15 17:32 75-00-3 Chloroform 0.01 ug/L 5.0 1 06/10/15 17:32 67-66-3 Chloromethane 0.01 ug/L 1.0 1 06/10/15 17:32 74-87-3 1,2-Dibromo-3-chloropropane 0.01 ug/L 13.0 1 06/10/15 17:32 96-12-8 Dibromochloromethane 0.01 ug/L 3.0 1 06/10/15 17:32 124-48-1 1,2-Dibromoethane (EDB) 0.01 ug/L 1.0 1 06/10/15 17:32 106-93-4 Dibromomethane 0.01 ug/L 10.0 1 06/10/15 17:32 74-95-3 1,2-Dichlorobenzene 0.01 ug/L 5.0 1 06/10/15 17:32 95-50-1 1,4-Dichlorobenzene 0.27J ug/L 1.0 1 06/10/15 17:32 106-46-7 trans-1,4-Dichloro-2-butene 0.01 ug/L 100 1 06/10/15 17:32 110-57-6 1,1-Dichloroethane 4.3J ug/L 5.0 1 06/10/15 17:32 75-34-3 1,2-Dichloroethane 0.36J ug/L 1.0 1 06/10/15 17:32 107-06-2 1,1-Dichloroethene 0.01 ug/L 5.0 1 06/10/15 17:32 75-35-4 cis-1,2-Dichloroethene 16.8 ug/L 5.0 1 06/10/15 17:32 156-59-2 trans-1,2-Dichloroethene 0.22J ug/L 5.0 1 06/10/15 17:32 156-60-5 1,2-Dichloropropane 0.31J ug/L 1.0 1 06/10/15 17:32 78-87-5 1,3-Dichloropropane 0.01 ug/L 1.0 1 06/10/15 17:32 142-28-9 cis-1,3-Dichloropropene 0.01 ug/L 1.0 1 06/10/15 17:32 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 35 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-21 Lab ID: 92252070015 Collected: 05/27/15 14:35 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 5220D COD Chemical Oxygen Demand 5310B TOC Total Organic Carbon Date: 06/12/2015 09:27 AM Analytical Method: EPA 8260 0.01 ug/L 1.0 1 06/10/1517:32 10061-02-6 0.01 ug/L 1.0 1 06/10/1517:32 100-41-4 0.01 ug/L 50.0 1 06/10/1517:32 591-78-6 0.01 ug/L 10.0 1 06/10/1517:32 74-88-4 0.01 ug/L 1.0 1 06/10/1517:32 75-09-2 0.01 ug/L 100 1 06/10/1517:32 108-10-1 0.01 ug/L 1.0 1 06/10/1517:32 100-42-5 0.01 ug/L 5.0 1 06/10/1517:32 630-20-6 0.01 ug/L 3.0 1 06/10/1517:32 79-34-5 0.14J ug/L 1.0 1 06/10/1517:32 127-18-4 0.01 ug/L 1.0 1 06/10/1517:32 108-88-3 0.01 ug/L 1.0 1 06/10/1517:32 71-55-6 0.01 ug/L 1.0 1 06/10/1517:32 79-00-5 1.0 ug/L 1.0 1 06/10/1517:32 79-01-6 0.01 ug/L 1.0 1 06/10/1517:32 75-69-4 0.01 ug/L 1.0 1 06/10/1517:32 96-18-4 0.01 ug/L 50.0 1 06/10/1517:32 108-05-4 0.01 ug/L 1.0 1 06/10/1517:32 75-01-4 0.0000000 ug/L 5.0 1 06/10/1517:32 1330-20-7 0010J 98 % 70-130 1 06/10/1517:32 460-00-4 96 % 70-130 1 06/10/1517:32 17060-07-0 98 % 70-130 1 06/10/1517:32 2037-26-5 Analytical Method: SM 2320B 29600 ug/L 5000 1000 1 06/08/1519:54 Analytical Method: EPA 300.0 1670J ug/L 250000 1000 1 06/09/1519:59 14808-79-8 Analytical Method: SM 4500-CI-E 28200 ug/L 1000 500 1 06/12/15 04:46 16887-00-6 Analytical Method: SM 5220D ND ug/L 25000 12500 1 06/02/15 09:35 Analytical Method: SM 5310B 9511 ug/L 1000 500 1 06/06/15 01:25 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 36 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-7 Lab ID: 92252070016 Collected: 05/28/15 09:10 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 3.8 1 06/01/15 20:15 06/04/15 20:27 7440-36-0 Arsenic ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:27 7440-38-2 Barium 78.1J ug/L 100 2.5 1 06/01/15 20:15 06/04/15 20:27 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 20:27 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 20:27 7440-43-9 Chromium ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:27 7440-47-3 Cobalt 77.0 ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:27 7440-48-4 Copper ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:27 7440-50-8 Lead ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:27 7439-92-1 Nickel 3.7J ug/L 50.0 2.5 1 06/01/15 20:15 06/04/15 20:27 7440-02-0 Selenium ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 20:27 7782-49-2 Silver ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:27 7440-22-4 Thallium ND ug/L 5.5 5.0 1 06/01/15 20:15 06/04/15 20:27 7440-28-0 Vanadium 12.4J ug/L 25.0 2.5 1 06/01/15 20:15 06/04/15 20:27 7440-62-2 Zinc 14.3 ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 20:27 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 2.3J ug/L 100 1 06/10/15 19:03 67-64-1 Acrylonitrile 0.01 ug/L 200 1 06/10/15 19:03 107-13-1 Benzene 0.60J ug/L 1.0 1 06/10/15 19:03 71-43-2 Bromochloromethane 0.01 ug/L 3.0 1 06/10/15 19:03 74-97-5 Bromodichloromethane 0.01 ug/L 1.0 1 06/10/15 19:03 75-27-4 Bromoform 0.01 ug/L 3.0 1 06/10/15 19:03 75-25-2 Bromomethane 0.01 ug/L 10.0 1 06/10/15 19:03 74-83-9 2-Butanone (MEK) 0.01 ug/L 100 1 06/10/15 19:03 78-93-3 Carbon disulfide 0.01 ug/L 100 1 06/10/15 19:03 75-15-0 Carbon tetrachloride 0.01 ug/L 1.0 1 06/10/15 19:03 56-23-5 Chlorobenzene 6.5 ug/L 3.0 1 06/10/15 19:03 108-90-7 Chloroethane 0.01 ug/L 10.0 1 06/10/15 19:03 75-00-3 Chloroform 0.01 ug/L 5.0 1 06/10/15 19:03 67-66-3 Chloromethane 0.01 ug/L 1.0 1 06/10/15 19:03 74-87-3 1,2-Dibromo-3-chloropropane 0.01 ug/L 13.0 1 06/10/15 19:03 96-12-8 Dibromochloromethane 0.01 ug/L 3.0 1 06/10/15 19:03 124-48-1 1,2-Dibromoethane (EDB) 0.01 ug/L 1.0 1 06/10/15 19:03 106-93-4 Dibromomethane 0.01 ug/L 10.0 1 06/10/15 19:03 74-95-3 1,2-Dichlorobenzene 0.30J ug/L 5.0 1 06/10/15 19:03 95-50-1 1,4-Dichlorobenzene 3.2 ug/L 1.0 1 06/10/15 19:03 106-46-7 trans-1,4-Dichloro-2-butene 0.01 ug/L 100 1 06/10/15 19:03 110-57-6 1,1-Dichloroethane 0.01 ug/L 5.0 1 06/10/15 19:03 75-34-3 1,2-Dichloroethane 0.01 ug/L 1.0 1 06/10/15 19:03 107-06-2 1,1-Dichloroethene 0.01 ug/L 5.0 1 06/10/15 19:03 75-35-4 cis-1,2-Dichloroethene 0.39J ug/L 5.0 1 06/10/15 19:03 156-59-2 trans-1,2-Dichloroethene 0.01 ug/L 5.0 1 06/10/15 19:03 156-60-5 1,2-Dichloropropane 0.01 ug/L 1.0 1 06/10/15 19:03 78-87-5 1,3-Dichloropropane 0.01 ug/L 1.0 1 06/10/15 19:03 142-28-9 cis-1,3-Dichloropropene 0.01 ug/L 1.0 1 06/10/15 19:03 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 37 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-7 Lab ID: 92252070016 Collected: 05/28/15 09:10 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 5220D COD Chemical Oxygen Demand 5310B TOC Total Organic Carbon Date: 06/12/2015 09:27 AM Analytical Method: EPA 8260 0.01 ug/L 1.0 1 06/10/1519:03 10061-02-6 0.01 ug/L 1.0 1 06/10/1519:03 100-41-4 0.01 ug/L 50.0 1 06/10/1519:03 591-78-6 0.01 ug/L 10.0 1 06/10/1519:03 74-88-4 0.01 ug/L 1.0 1 06/10/1519:03 75-09-2 0.01 ug/L 100 1 06/10/1519:03 108-10-1 0.01 ug/L 1.0 1 06/10/1519:03 100-42-5 0.01 ug/L 5.0 1 06/10/1519:03 630-20-6 0.01 ug/L 3.0 1 06/10/1519:03 79-34-5 0.01 ug/L 1.0 1 06/10/1519:03 127-18-4 0.01 ug/L 1.0 1 06/10/1519:03 108-88-3 0.01 ug/L 1.0 1 06/10/1519:03 71-55-6 0.01 ug/L 1.0 1 06/10/1519:03 79-00-5 0.01 ug/L 1.0 1 06/10/1519:03 79-01-6 0.01 ug/L 1.0 1 06/10/1519:03 75-69-4 0.01 ug/L 1.0 1 06/10/1519:03 96-18-4 0.01 ug/L 50.0 1 06/10/1519:03 108-05-4 0.01 ug/L 1.0 1 06/10/1519:03 75-01-4 0.0000000 ug/L 5.0 1 06/10/1519:03 1330-20-7 0010J 99 % 70-130 1 06/10/1519:03 460-00-4 100 % 70-130 1 06/10/1519:03 17060-07-0 100 % 70-130 1 06/10/1519:03 2037-26-5 Analytical Method: SM 2320B 84600 ug/L 5000 1000 1 06/10/1512:05 Analytical Method: EPA 300.0 6420J ug/L 250000 1000 1 06/09/15 20:13 14808-79-8 Analytical Method: SM 4500-CI-E 44400 ug/L 5000 2500 5 06/09/15 07:14 16887-00-6 Analytical Method: SM 5220D 28000 ug/L 25000 12500 1 06/02/15 09:35 Analytical Method: SM 5310B 4380 ug/L 1000 500 1 06/06/15 01:25 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 38 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-9 Lab ID: 92252070017 Collected: 05/28/15 16:15 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 3.8 1 06/01/15 20:15 06/04/15 20:30 7440-36-0 Arsenic ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:30 7440-38-2 Barium 52.OJ ug/L 100 2.5 1 06/01/15 20:15 06/04/15 20:30 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 20:30 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 20:30 7440-43-9 Chromium ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:30 7440-47-3 Cobalt 123 ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:30 7440-48-4 Copper 3.9J ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:30 7440-50-8 Lead 3.OJ ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:30 7439-92-1 Nickel 3.8J ug/L 50.0 2.5 1 06/01/15 20:15 06/04/15 20:30 7440-02-0 Selenium ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 20:30 7782-49-2 Silver ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 20:30 7440-22-4 Thallium ND ug/L 5.5 5.0 1 06/01/15 20:15 06/04/15 20:30 7440-28-0 Vanadium 11.1J ug/L 25.0 2.5 1 06/01/15 20:15 06/04/15 20:30 7440-62-2 Zinc ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 20:30 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 1.91 ug/L 100 1 06/10/15 19:40 67-64-1 Acrylonitrile 0.01 ug/L 200 1 06/10/15 19:40 107-13-1 Benzene 2.8 ug/L 1.0 1 06/10/15 19:40 71-43-2 Bromochloromethane 0.01 ug/L 3.0 1 06/10/15 19:40 74-97-5 Bromodichloromethane 0.01 ug/L 1.0 1 06/10/15 19:40 75-27-4 Bromoform 0.01 ug/L 3.0 1 06/10/15 19:40 75-25-2 Bromomethane 0.01 ug/L 10.0 1 06/10/15 19:40 74-83-9 2-Butanone (MEK) 0.01 ug/L 100 1 06/10/15 19:40 78-93-3 Carbon disulfide 0.01 ug/L 100 1 06/10/15 19:40 75-15-0 Carbon tetrachloride 0.01 ug/L 1.0 1 06/10/15 19:40 56-23-5 Chlorobenzene 2.4J ug/L 3.0 1 06/10/15 19:40 108-90-7 Chloroethane 2.4J ug/L 10.0 1 06/10/15 19:40 75-00-3 Chloroform 0.01 ug/L 5.0 1 06/10/15 19:40 67-66-3 Chloromethane 0.01 ug/L 1.0 1 06/10/15 19:40 74-87-3 1,2-Dibromo-3-chloropropane 0.01 ug/L 13.0 1 06/10/15 19:40 96-12-8 Dibromochloromethane 0.01 ug/L 3.0 1 06/10/15 19:40 124-48-1 1,2-Dibromoethane (EDB) 0.01 ug/L 1.0 1 06/10/15 19:40 106-93-4 Dibromomethane 0.01 ug/L 10.0 1 06/10/15 19:40 74-95-3 1,2-Dichlorobenzene 1.6J ug/L 5.0 1 06/10/15 19:40 95-50-1 1,4-Dichlorobenzene 6.2 ug/L 1.0 1 06/10/15 19:40 106-46-7 trans-1,4-Dichloro-2-butene 0.01 ug/L 100 1 06/10/15 19:40 110-57-6 1,1-Dichloroethane 2.7J ug/L 5.0 1 06/10/15 19:40 75-34-3 1,2-Dichloroethane 0.21J ug/L 1.0 1 06/10/15 19:40 107-06-2 1,1-Dichloroethene 0.01 ug/L 5.0 1 06/10/15 19:40 75-35-4 cis-1,2-Dichloroethene 9.0 ug/L 5.0 1 06/10/15 19:40 156-59-2 trans-1,2-Dichloroethene 0.21J ug/L 5.0 1 06/10/15 19:40 156-60-5 1,2-Dichloropropane 0.01 ug/L 1.0 1 06/10/15 19:40 78-87-5 1,3-Dichloropropane 0.01 ug/L 1.0 1 06/10/15 19:40 142-28-9 cis-1,3-Dichloropropene 0.01 ug/L 1.0 1 06/10/15 19:40 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 39 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Sample: MW-9 Lab ID: 92252070017 Collected: 05/28/15 16:15 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 5220D COD Chemical Oxygen Demand 5310B TOC Total Organic Carbon Date: 06/12/2015 09:27 AM Analytical Method: EPA 8260 0.01 ug/L 1.0 1 06/10/1519:40 10061-02-6 0.01 ug/L 1.0 1 06/10/1519:40 100-41-4 0.01 ug/L 50.0 1 06/10/1519:40 591-78-6 0.01 ug/L 10.0 1 06/10/1519:40 74-88-4 0.01 ug/L 1.0 1 06/10/1519:40 75-09-2 0.01 ug/L 100 1 06/10/1519:40 108-10-1 0.01 ug/L 1.0 1 06/10/1519:40 100-42-5 0.01 ug/L 5.0 1 06/10/1519:40 630-20-6 0.01 ug/L 3.0 1 06/10/1519:40 79-34-5 0.01 ug/L 1.0 1 06/10/1519:40 127-18-4 0.12J ug/L 1.0 1 06/10/1519:40 108-88-3 0.01 ug/L 1.0 1 06/10/1519:40 71-55-6 0.01 ug/L 1.0 1 06/10/1519:40 79-00-5 0.01 ug/L 1.0 1 06/10/1519:40 79-01-6 0.01 ug/L 1.0 1 06/10/1519:40 75-69-4 0.01 ug/L 1.0 1 06/10/1519:40 96-18-4 0.01 ug/L 50.0 1 06/10/1519:40 108-05-4 12.3 ug/L 1.0 1 06/10/1519:40 75-01-4 0.0000000 ug/L 5.0 1 06/10/1519:40 1330-20-7 0010J 97 % 70-130 1 06/10/1519:40 460-00-4 100 % 70-130 1 06/10/1519:40 17060-07-0 98 % 70-130 1 06/10/1519:40 2037-26-5 Analytical Method: SM 2320B 65800 ug/L 5000 1000 1 06/10/1512:17 Analytical Method: EPA 300.0 18101 ug/L 250000 1000 1 06/09/15 20:27 14808-79-8 Analytical Method: SM 4500-CI-E 49300 ug/L 5000 2500 5 06/09/15 07:15 16887-00-6 Analytical Method: SM 5220D 24000J ug/L 25000 12500 1 06/02/15 09:35 Analytical Method: SM 5310B 1560 ug/L 1000 500 1 06/06/15 01:25 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 40 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 QC Batch: MPRP/18587 Analysis Method: EPA6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET NC Groundwater Associated Lab Samples: 92252070001, 92252070002, 92252070003, 92252070004, 92252070005, 92252070006, 92252070007, 92252070008,92252070009,92252070010,92252070011,92252070012,92252070013,92252070014, 92252070015,92252070016,92252070017 METHOD BLANK: 1472278 Matrix: Water Associated Lab Samples: 92252070001, 92252070002, 92252070003, 92252070004, 92252070005, 92252070006, 92252070007, 92252070008,92252070009,92252070010,92252070011,92252070012,92252070013,92252070014, 92252070015,92252070016,92252070017 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Antimony ug/L ND 6.0 06/04/1518:53 Arsenic ug/L ND 10.0 06/04/1518:53 Barium ug/L ND 100 06/04/1518:53 Beryllium ug/L ND 1.0 06/04/1518:53 Cadmium ug/L ND 1.0 06/04/1518:53 Chromium ug/L ND 10.0 06/04/1518:53 Cobalt ug/L ND 10.0 06/04/1518:53 Copper ug/L ND 10.0 06/04/1518:53 Lead ug/L ND 10.0 06/04/1518:53 Nickel ug/L ND 50.0 06/04/1518:53 Selenium ug/L ND 10.0 06/04/1518:53 Silver ug/L ND 10.0 06/04/1518:53 Thallium ug/L ND 5.5 06/04/1518:53 Vanadium ug/L ND 25.0 06/04/1518:53 Zinc ug/L ND 10.0 06/04/1518:53 LABORATORY CONTROL SAMPLE: Parameter 1472279 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Antimony ug/L 500 480 96 80-120 Arsenic ug/L 500 465 93 80-120 Barium ug/L 500 458 92 80-120 Beryllium ug/L 500 462 92 80-120 Cadmium ug/L 500 460 92 80-120 Chromium ug/L 500 456 91 80-120 Cobalt ug/L 500 459 92 80-120 Copper ug/L 500 451 90 80-120 Lead ug/L 500 456 91 80-120 Nickel ug/L 500 460 92 80-120 Selenium ug/L 500 439 88 80-120 Silver ug/L 250 228 91 80-120 Thallium ug/L 500 466 93 80-120 Vanadium ug/L 500 444 89 80-120 Zinc ug/L 500 460 92 80-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 41 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: SURRY CLOSED- MT AIRY (UIC) 92252070 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1472280 1472281 MS MSD 92252055001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 512 478 102 96 75-125 7 25 Arsenic ug/L ND 500 500 494 459 99 92 75-125 7 25 Barium ug/L 32.1J 500 500 518 485 97 91 75-125 7 25 Beryllium ug/L ND 500 500 492 457 98 91 75-125 7 25 Cadmium ug/L ND 500 500 490 456 98 91 75-125 7 25 Chromium ug/L ND 500 500 488 449 97 90 75-125 8 25 Cobalt ug/L 12.6 500 500 501 463 98 90 75-125 8 25 Copper ug/L ND 500 500 482 446 96 89 75-125 8 25 Lead ug/L ND 500 500 484 447 97 89 75-125 8 25 Nickel ug/L ND 500 500 490 452 98 90 75-125 8 25 Selenium ug/L ND 500 500 466 434 93 86 75-125 7 25 Silver ug/L ND 250 250 244 226 97 91 75-125 7 25 Thallium ug/L ND 500 500 493 458 99 92 75-125 7 25 Vanadium ug/L ND 500 500 482 442 96 88 75-125 9 25 Zinc ug/L 6.3J 500 500 496 457 98 90 75-125 8 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 42 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 QC Batch: MSV/32002 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92252070001, 92252070002, 92252070003, 92252070004, 92252070005, 92252070006 METHOD BLANK: 1475797 Matrix: Water Associated Lab Samples: 92252070001, 92252070002, 92252070003, 92252070004, 92252070005, 92252070006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/04/15 16:39 1,1,1-Trichloroethane ug/L ND 1.0 06/04/15 16:39 1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/04/15 16:39 1,1,2-Trichloroethane ug/L ND 1.0 06/04/15 16:39 1,1-Dichloroethane ug/L ND 5.0 06/04/15 16:39 1,1-Dichloroethene ug/L ND 5.0 06/04/15 16:39 1,2,3-Trichloropropane ug/L ND 1.0 06/04/15 16:39 1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/04/15 16:39 1,2-Dibromoethane (EDB) ug/L ND 1.0 06/04/15 16:39 1,2-Dichlorobenzene ug/L ND 5.0 06/04/15 16:39 1,2-Dichloroethane ug/L ND 1.0 06/04/15 16:39 1,2-Dichloropropane ug/L ND 1.0 06/04/15 16:39 1,3-Dichloropropane ug/L ND 1.0 06/04/15 16:39 1,4-Dichlorobenzene ug/L ND 1.0 06/04/15 16:39 2-Butanone (MEK) ug/L ND 100 06/04/15 16:39 2-Hexanone ug/L ND 50.0 06/04/15 16:39 4-Methyl-2-pentanone (MIBK) ug/L ND 100 06/04/15 16:39 Acetone ug/L ND 100 06/04/15 16:39 Acrylonitrile ug/L ND 200 06/04/15 16:39 Benzene ug/L ND 1.0 06/04/15 16:39 Bromochloromethane ug/L ND 3.0 06/04/15 16:39 Bromodichloromethane ug/L ND 1.0 06/04/15 16:39 Bromoform ug/L ND 3.0 06/04/15 16:39 Bromomethane ug/L ND 10.0 06/04/15 16:39 Carbon disulfide ug/L ND 100 06/04/15 16:39 Carbon tetrachloride ug/L ND 1.0 06/04/15 16:39 Chlorobenzene ug/L ND 3.0 06/04/15 16:39 Chloroethane ug/L ND 10.0 06/04/15 16:39 Chloroform ug/L ND 5.0 06/04/15 16:39 Chloromethane ug/L ND 1.0 06/04/15 16:39 cis-1,2-Dichloroethene ug/L ND 5.0 06/04/15 16:39 cis-1,3-Dichloropropene ug/L ND 1.0 06/04/15 16:39 Dibromochloromethane ug/L ND 3.0 06/04/15 16:39 Dibromomethane ug/L ND 10.0 06/04/15 16:39 Ethylbenzene ug/L ND 1.0 06/04/15 16:39 lodomethane ug/L ND 10.0 06/04/15 16:39 Methylene Chloride ug/L ND 1.0 06/04/15 16:39 Styrene ug/L ND 1.0 06/04/15 16:39 Tetrachloroethene ug/L ND 1.0 06/04/15 16:39 Toluene ug/L ND 1.0 06/04/15 16:39 trans-1,2-Dichloroethene ug/L ND 5.0 06/04/15 16:39 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 43 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 METHOD BLANK: 1475797 Matrix: Water Associated Lab Samples: 92252070001, 92252070002, 92252070003, 92252070004, 92252070005, 92252070006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers trans- 1,3-Dichloropropene ug/L ND 1.0 06/04/15 16:39 trans-1,4-Dichloro-2-butene ug/L ND 100 06/04/15 16:39 Trichloroethene ug/L ND 1.0 06/04/15 16:39 Trichlorofluoromethane ug/L ND 1.0 06/04/15 16:39 Vinyl acetate ug/L ND 50.0 06/04/15 16:39 Vinyl chloride ug/L ND 1.0 06/04/15 16:39 Xylene (Total) ug/L ND 5.0 06/04/15 16:39 1,2-Dichloroethane-d4 (S) % 98 70-130 06/04/15 16:39 4-Bromofluorobenzene (S) % 99 70-130 06/04/15 16:39 Toluene-d8 (S) % 100 70-130 06/04/15 16:39 LABORATORY CONTROL SAMPLE: Parameter 1475798 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 51.6 103 80-125 1,1,1-Trichloroethane ug/L 50 47.9 96 71-129 1,1,2,2-Tetrachloroethane ug/L 50 51.8 104 79-124 1,1,2-Trichloroethane ug/L 50 50.1 100 85-125 1,1-Dichloroethane ug/L 50 48.4 97 73-126 1,1-Dichloroethene ug/L 50 48.3 97 66-135 1,2,3-Trichloropropane ug/L 50 53.1 106 75-130 1,2-Dibromo-3-chloropropane ug/L 50 49.4 99 71-133 1,2-Dibromoethane (EDB) ug/L 50 53.4 107 83-124 1,2-Dichlorobenzene ug/L 50 57.7 115 80-133 1,2-Dichloroethane ug/L 50 48.6 97 67-128 1,2-Dichloropropane ug/L 50 49.8 100 75-132 1,3-Dichloropropane ug/L 50 54.0 108 76-131 1,4-Dichlorobenzene ug/L 50 55.6 111 78-130 2-Butanone (MEK) ug/L 100 99.91 100 61-144 2-Hexanone ug/L 100 109 109 68-143 4-Methyl-2-pentanone (MIBK) ug/L 100 99AJ 99 72-135 Acetone ug/L 100 105 105 48-146 Acrylonitrile ug/L 250 241 96 40-160 Benzene ug/L 50 51.0 102 80-125 Bromochloromethane ug/L 50 50.0 100 71-125 Bromodichloromethane ug/L 50 43.7 87 78-124 Bromoform ug/L 50 33.9 68 71-128 LO Bromomethane ug/L 50 62.3 125 40-160 Carbon disulfide ug/L 50 41.7J 83 50-160 Carbon tetrachloride ug/L 50 47.1 94 69-131 Chlorobenzene ug/L 50 54.0 108 81-122 Chloroethane ug/L 50 46.2 92 39-148 Chloroform ug/L 50 45.3 91 73-127 Chloromethane ug/L 50 50.7 101 44-146 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 44 of 72 Pace Analytical Services, Inc. aceAnalXical� 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 LABORATORY CONTROL SAMPLE: Parameter 1475798 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers cis-1,2-Dichloroethene ug/L 50 50.5 101 74-124 cis-1,3-Dichloropropene ug/L 50 49.7 99 72-132 Dibromochloromethane ug/L 50 42.8 86 78-125 Dibromomethane ug/L 50 50.3 101 82-120 Ethylbenzene ug/L 50 53.3 107 79-121 lodomethane ug/L 100 113 113 39-154 Methylene Chloride ug/L 50 55.0 110 64-133 Styrene ug/L 50 57.1 114 84-126 Tetrachloroethene ug/L 50 55.0 110 78-122 Toluene ug/L 50 49.9 100 80-121 trans-1,2-Dichloroethene ug/L 50 49.0 98 71-127 trans- 1,3-Dichloropropene ug/L 50 50.9 102 69-141 trans-1,4-Dichloro-2-butene ug/L 50 41.OJ 82 40-160 Trichloroethene ug/L 50 48.6 97 78-122 Trichlorofluoromethane ug/L 50 50.1 100 53-137 Vinyl acetate ug/L 100 106 106 40-160 Vinyl chloride ug/L 50 54.5 109 58-137 Xylene (Total) ug/L 150 161 107 81-126 1,2-Dichloroethane-d4 (S) % 96 70-130 4-Bromofluorobenzene (S) % 102 70-130 Toluene-d8 (S) % 100 70-130 MATRIX SPIKE SAMPLE: Parameter 1475800 Units 92252070006 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 15.2 76 70-130 1,1,1-Trichloroethane ug/L ND 20 17.7 88 70-130 1,1,2,2-Tetrachloroethane ug/L ND 20 16.6 83 70-130 1,1,2-Trichloroethane ug/L ND 20 17.4 87 70-130 1,1-Dichloroethane ug/L ND 20 18.5 92 70-130 1,1-Dichloroethene ug/L ND 20 19.3 97 70-166 1,2,3-Trichloropropane ug/L ND 20 16.8 84 70-130 1,2-Dibromo-3-chloropropane ug/L ND 20 15.0 75 70-130 1,2-Dibromoethane (EDB) ug/L ND 20 17.1 85 70-130 1,2-Dichlorobenzene ug/L ND 20 18.5 92 70-130 1,2-Dichloroethane ug/L ND 20 17.8 89 70-130 1,2-Dichloropropane ug/L ND 20 18.1 90 70-130 1,3-Dichloropropane ug/L ND 20 17.5 88 70-130 1,4-Dichlorobenzene ug/L ND 20 17.4 87 70-130 2-Butanone (MEK) ug/L ND 40 37.9J 95 70-130 2-Hexanone ug/L ND 40 35.9J 90 70-130 4-Methyl-2-pentanone (MIBK) ug/L ND 40 35.5J 89 70-130 Acetone ug/L ND 40 37.OJ 89 70-130 Acrylonitrile ug/L ND 100 85.7J 86 70-130 Benzene ug/L ND 20 18.7 94 70-148 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 45 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 MATRIX SPIKE SAMPLE: 1475800 92252070006 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Bromochloromethane ug/L ND 20 18.9 95 70-130 Bromodichloromethane ug/L ND 20 14.0 70 70-130 Bromoform ug/L ND 20 11.8 59 70-130 MO Bromomethane ug/L ND 20 18.8 94 70-130 Carbon disulfide ug/L ND 20 15.6J 78 70-130 Carbon tetrachloride ug/L ND 20 15.6 78 70-130 Chlorobenzene ug/L ND 20 18.6 93 70-146 Chloroethane ug/L ND 20 19.7 98 70-130 Chloroform ug/L ND 20 16.3 81 70-130 Chloromethane ug/L ND 20 21.8 109 70-130 cis-1,2-Dichloroethene ug/L ND 20 18.9 95 70-130 cis-1,3-Dichloropropene ug/L ND 20 15.9 79 70-130 Dibromochloromethane ug/L ND 20 11.5 58 70-130 M1 Dibromomethane ug/L ND 20 17.4 87 70-130 Ethylbenzene ug/L ND 20 18.2 91 70-130 lodomethane ug/L ND 40 41.3 103 70-130 Methylene Chloride ug/L ND 20 19.8 99 70-130 Styrene ug/L ND 20 18.8 94 70-130 Tetrachloroethene ug/L ND 20 18.5 92 70-130 Toluene ug/L ND 20 18.0 90 70-155 trans-1,2-Dichloroethene ug/L ND 20 19.1 96 70-130 trans- 1,3-Dichloropropene ug/L ND 20 15.4 77 70-130 trans-1,4-Dichloro-2-butene ug/L ND 20 14.2J 71 70-130 Trichloroethene ug/L ND 20 18.4 92 69-151 Trichlorofluoromethane ug/L ND 20 19.5 97 70-130 Vinyl acetate ug/L ND 40 33.2J 83 70-130 Vinyl chloride ug/L ND 20 19.7 98 70-130 1,2-Dichloroethane-d4 (S) % 101 70-130 4-Bromofluorobenzene (S) % 98 70-130 Toluene-d8 (S) % 99 70-130 SAMPLE DUPLICATE: 1475799 92252070005 Dup Max Parameter Units Result Result RPD RPD Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND ND 30 1,1,1-Trichloroethane ug/L ND ND 30 1,1,2,2-Tetrachloroethane ug/L ND ND 30 1,1,2-Trichloroethane ug/L ND ND 30 1,1-Dichloroethane ug/L 0.46J 0.46J 30 1,1-Dichloroethene ug/L ND ND 30 1,2,3-Trichloropropane ug/L ND ND 30 1,2-Dibromo-3-chloropropane ug/L ND ND 30 1,2-Dibromoethane (EDB) ug/L ND ND 30 1,2-Dichlorobenzene ug/L ND ND 30 1,2-Dichloroethane ug/L 0.14J 0.13J 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 46 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 SAMPLE DUPLICATE: 1475799 Parameter Units 92252070005 Result Dup Result 1,2-Dichloropropane ug/L ND ND 1,3-Dichloropropane ug/L ND ND 1,4-Dichlorobenzene ug/L 0.42J 0.44J 2-Butanone (MEK) ug/L ND ND 2-Hexanone ug/L ND ND 4-Methyl-2-pentanone (MIBK) ug/L ND ND Acetone ug/L ND ND Acrylonitrile ug/L ND ND Benzene ug/L ND ND Bromochloromethane ug/L ND ND Bromodichloromethane ug/L ND ND Bromoform ug/L ND ND Bromomethane ug/L ND ND Carbon disulfide ug/L ND ND Carbon tetrachloride ug/L ND ND Chlorobenzene ug/L ND ND Chloroethane ug/L ND ND Chloroform ug/L ND ND Chloromethane ug/L ND ND cis-1,2-Dichloroethene ug/L 0.74J 0.72J cis-1,3-Dichloropropene ug/L ND ND Dibromochloromethane ug/L ND ND Dibromomethane ug/L ND ND Ethylbenzene ug/L ND ND lodomethane ug/L ND ND Methylene Chloride ug/L ND ND Styrene ug/L ND ND Tetrachloroethene ug/L ND ND Toluene ug/L ND ND trans-1,2-Dichloroethene ug/L ND ND trans- 1,3-Dichloropropene ug/L ND ND trans-1,4-Dichloro-2-butene ug/L ND ND Trichloroethene ug/L ND ND Trichlorofluoromethane ug/L ND ND Vinyl acetate ug/L ND ND Vinyl chloride ug/L ND ND Xylene (Total) ug/L ND ND 1,2-Dichloroethane-d4 (S) % 104 104 4-Bromofluorobenzene (S) % 97 97 Toluene-d8(S) % 102 102 Max RPD RPD Qualifiers 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 47 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 QC Batch: MSV/32080 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92252070007,92252070008,92252070009,92252070010,92252070011,92252070012,92252070013, 92252070014,92252070015,92252070016,92252070017 METHOD BLANK: 1481289 Matrix: Water Associated Lab Samples: 92252070007,92252070008,92252070009,92252070010,92252070011,92252070012,92252070013, 92252070014,92252070015,92252070016,92252070017 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L 0.01 5.0 06/10/15 12:42 1,1,1-Trichloroethane ug/L 0.01 1.0 06/10/15 12:42 1,1,2,2-Tetrachloroethane ug/L 0.01 3.0 06/10/15 12:42 1,1,2-Trichloroethane ug/L 0.01 1.0 06/10/15 12:42 1,1-Dichloroethane ug/L 0.01 5.0 06/10/15 12:42 1,1-Dichloroethene ug/L 0.01 5.0 06/10/15 12:42 1,2,3-Trichloropropane ug/L 0.01 1.0 06/10/15 12:42 1,2-Dibromo-3-chloropropane ug/L 0.01 13.0 06/10/15 12:42 1,2-Dibromoethane (EDB) ug/L 0.01 1.0 06/10/15 12:42 1,2-Dichlorobenzene ug/L 0.01 5.0 06/10/15 12:42 1,2-Dichloroethane ug/L 0.01 1.0 06/10/15 12:42 1,2-Dichloropropane ug/L 0.01 1.0 06/10/15 12:42 1,3-Dichloropropane ug/L 0.01 1.0 06/10/15 12:42 1,4-Dichlorobenzene ug/L 0.01 1.0 06/10/15 12:42 2-Butanone (MEK) ug/L 0.01 100 06/10/15 12:42 2-Hexanone ug/L 0.01 50.0 06/10/15 12:42 4-Methyl-2-pentanone (MIBK) ug/L 0.01 100 06/10/15 12:42 Acetone ug/L 1.2J 100 06/10/15 12:42 Acrylonitrile ug/L 0.01 200 06/10/15 12:42 Benzene ug/L 0.01 1.0 06/10/15 12:42 Bromochloromethane ug/L 0.01 3.0 06/10/15 12:42 Bromodichloromethane ug/L 0.01 1.0 06/10/15 12:42 Bromoform ug/L 0.01 3.0 06/10/15 12:42 Bromomethane ug/L 0.01 10.0 06/10/15 12:42 Carbon disulfide ug/L 0.01 100 06/10/15 12:42 Carbon tetrachloride ug/L 0.01 1.0 06/10/15 12:42 Chlorobenzene ug/L 0.01 3.0 06/10/15 12:42 Chloroethane ug/L 0.01 10.0 06/10/15 12:42 Chloroform ug/L 0.01 5.0 06/10/15 12:42 Chloromethane ug/L 0.01 1.0 06/10/15 12:42 cis-1,2-Dichloroethene ug/L 0.01 5.0 06/10/15 12:42 cis-1,3-Dichloropropene ug/L 0.01 1.0 06/10/15 12:42 Dibromochloromethane ug/L 0.01 3.0 06/10/15 12:42 Dibromomethane ug/L 0.01 10.0 06/10/15 12:42 Ethylbenzene ug/L 0.01 1.0 06/10/15 12:42 lodomethane ug/L 0.01 10.0 06/10/15 12:42 Methylene Chloride ug/L 0.01 1.0 06/10/15 12:42 Styrene ug/L 0.01 1.0 06/10/15 12:42 Tetrachloroethene ug/L 0.01 1.0 06/10/15 12:42 Toluene ug/L 0.01 1.0 06/10/15 12:42 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 48 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 METHOD BLANK: 1481289 Matrix: Water Associated Lab Samples: 92252070007,92252070008,92252070009,92252070010,92252070011,92252070012,92252070013, 92252070014,92252070015,92252070016,92252070017 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers trans-1,2-Dichloroethene ug/L 0.01 5.0 06/10/15 12:42 trans- 1,3-Dichloropropene ug/L 0.01 1.0 06/10/15 12:42 trans-1,4-Dichloro-2-butene ug/L 0.01 100 06/10/15 12:42 Trichloroethene ug/L 0.01 1.0 06/10/15 12:42 Trichlorofluoromethane ug/L 0.01 1.0 06/10/15 12:42 Vinyl acetate ug/L 0.01 50.0 06/10/15 12:42 Vinyl chloride ug/L 0.01 1.0 06/10/15 12:42 Xylene (Total) ug/L 0.0000000001 5.0 06/10/15 12:42 1,2-Dichloroethane-d4 (S) % 99 70-130 06/10/15 12:42 4-Bromofluorobenzene (S) % 100 70-130 06/10/15 12:42 Toluene-d8 (S) % 99 70-130 06/10/15 12:42 LABORATORY CONTROL SAMPLE: Parameter 1481290 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 55.3 111 80-125 1,1,1-Trichloroethane ug/L 50 55.5 111 71-129 1,1,2,2-Tetrachloroethane ug/L 50 54.4 109 79-124 1,1,2-Trichloroethane ug/L 50 55.7 111 85-125 1,1-Dichloroethane ug/L 50 56.0 112 73-126 1,1-Dichloroethene ug/L 50 50.8 102 66-135 1,2,3-Trichloropropane ug/L 50 55.4 111 75-130 1,2-Dibromo-3-chloropropane ug/L 50 62.1 124 71-133 1,2-Dibromoethane (EDB) ug/L 50 54.9 110 83-124 1,2-Dichlorobenzene ug/L 50 56.3 113 80-133 1,2-Dichloroethane ug/L 50 54.6 109 67-128 1,2-Dichloropropane ug/L 50 57.8 116 75-132 1,3-Dichloropropane ug/L 50 56.1 112 76-131 1,4-Dichlorobenzene ug/L 50 55.0 110 78-130 2-Butanone (MEK) ug/L 100 110 110 61-144 2-Hexanone ug/L 100 125 125 68-143 4-Methyl-2-pentanone (MIBK) ug/L 100 113 113 72-135 Acetone ug/L 100 111 111 48-146 Acrylonitrile ug/L 250 267 107 40-160 Benzene ug/L 50 58.3 117 80-125 Bromochloromethane ug/L 50 57.9 116 71-125 Bromodichloromethane ug/L 50 52.1 104 78-124 Bromoform ug/L 50 50.9 102 71-128 Bromomethane ug/L 50 57.6 115 40-160 Carbon disulfide ug/L 50 54.9J 110 50-160 Carbon tetrachloride ug/L 50 57.5 115 69-131 Chlorobenzene ug/L 50 55.9 112 81-122 Chloroethane ug/L 50 46.2 92 39-148 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 49 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 LABORATORY CONTROL SAMPLE: 1481290 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloroform ug/L 50 50.1 100 73-127 Chloromethane ug/L 50 50.6 101 44-146 cis-1,2-Dichloroethene ug/L 50 56.3 113 74-124 cis-1,3-Dichloropropene ug/L 50 58.2 116 72-132 Dibromochloromethane ug/L 50 49.9 100 78-125 Dibromomethane ug/L 50 57.2 114 82-120 Ethylbenzene ug/L 50 55.2 110 79-121 lodomethane ug/L 100 106 106 39-154 Methylene Chloride ug/L 50 53.8 108 64-133 Styrene ug/L 50 57.1 114 84-126 Tetrachloroethene ug/L 50 52.9 106 78-122 Toluene ug/L 50 56.0 112 80-121 trans-1,2-Dichloroethene ug/L 50 55.5 111 71-127 trans- 1,3-Dichloropropene ug/L 50 60.0 120 69-141 trans-1,4-Dichloro-2-butene ug/L 50 60.OJ 120 40-160 Trichloroethene ug/L 50 55.2 110 78-122 Trichlorofluoromethane ug/L 50 52.2 104 53-137 Vinyl acetate ug/L 100 114 114 40-160 Vinyl chloride ug/L 50 54.4 109 58-137 Xylene (Total) ug/L 150 173 115 81-126 1,2-Dichloroethane-d4 (S) % 95 70-130 4-Bromofluorobenzene (S) % 98 70-130 Toluene-d8 (S) % 100 70-130 MATRIX SPIKE SAMPLE: 1481292 92252070011 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 0.01 20 21.3 107 70-130 1,1,1-Trichloroethane ug/L 0.01 20 24.1 120 70-130 1,1,2,2-Tetrachloroethane ug/L 0.01 20 22.8 114 70-130 1,1,2-Trichloroethane ug/L 0.01 20 22.6 113 70-130 1,1-Dichloroethane ug/L 0.23J 20 24.8 123 70-130 1,1-Dichloroethene ug/L 0.01 20 22.6 113 70-166 1,2,3-Trichloropropane ug/L 0.01 20 24.0 120 70-130 1,2-Dibromo-3-chloropropane ug/L 0.01 20 23.8 119 70-130 1,2-Dibromoethane (EDB) ug/L 0.01 20 23.6 118 70-130 1,2-Dichlorobenzene ug/L 0.01 20 23.4 117 70-130 1,2-Dichloroethane ug/L 0.01 20 23.0 115 70-130 1,2-Dichloropropane ug/L 0.01 20 23.6 118 70-130 1,3-Dichloropropane ug/L 0.01 20 24.3 122 70-130 1,4-Dichlorobenzene ug/L 0.25J 20 23.4 116 70-130 2-Butanone (MEK) ug/L 0.01 40 48.6J 121 70-130 2-Hexanone ug/L 0.01 40 50.0 125 70-130 4-Methyl-2-pentanone (MIBK) ug/L 0.01 40 47.7J 119 70-130 Acetone ug/L 1.7J 40 47AJ 114 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 50 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 MATRIX SPIKE SAMPLE: Parameter 1481292 Units 92252070011 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers Acrylonitrile ug/L 0.01 100 121J 121 70-130 Benzene ug/L 0.01 20 24.4 122 70-148 Bromochloromethane ug/L 0.01 20 24.6 123 70-130 Bromodichloromethane ug/L 0.01 20 20.9 105 70-130 Bromoform ug/L 0.01 20 17.6 88 70-130 Bromomethane ug/L 0.01 20 21.0 105 70-130 Carbon disulfide ug/L 0.01 20 22.6J 113 70-130 Carbon tetrachloride ug/L 0.01 20 23.2 116 70-130 Chlorobenzene ug/L 0.01 20 24.5 122 70-146 Chloroethane ug/L 0.01 20 21.5 108 70-130 Chloroform ug/L 0.01 20 21.7 109 70-130 Chloromethane ug/L 0.01 20 22.2 111 70-130 cis-1,2-Dichloroethene ug/L 0.66J 20 25.6 125 70-130 cis-1,3-Dichloropropene ug/L 0.01 20 22.8 114 70-130 Dibromochloromethane ug/L 0.01 20 18.2 91 70-130 Dibromomethane ug/L 0.01 20 23.0 115 70-130 Ethylbenzene ug/L 0.01 20 24.8 124 70-130 lodomethane ug/L 0.01 40 34.2 86 70-130 Methylene Chloride ug/L 0.01 20 24.9 124 70-130 Styrene ug/L 0.01 20 25.1 126 70-130 Tetrachloroethene ug/L 0.01 20 23.4 117 70-130 Toluene ug/L 0.01 20 23.7 118 70-155 trans-1,2-Dichloroethene ug/L 0.01 20 24.4 122 70-130 trans- 1,3-Dichloropropene ug/L 0.01 20 22.6 113 70-130 trans-1,4-Dichloro-2-butene ug/L 0.01 20 23.9J 120 70-130 Trichloroethene ug/L 0.01 20 23.1 115 69-151 Trichlorofluoromethane ug/L 0.01 20 22.7 113 70-130 Vinyl acetate ug/L 0.01 40 43.2J 108 70-130 Vinyl chloride ug/L 0.111 20 23.7 118 70-130 1,2-Dichloroethane-d4 (S) % 102 70-130 4-Bromofluorobenzene (S) % 99 70-130 Toluene-d8 (S) % 98 70-130 SAMPLE DUPLICATE: 1481291 92252070010 Dup Max Parameter Units Result Result RPD RPD Qualifiers 1,1,1,2-Tetrachloroethane ug/L 0.01 0.01 30 1,1,1-Trichloroethane ug/L 0.01 0.01 30 1,1,2,2-Tetrachloroethane ug/L 0.01 0.01 30 1,1,2-Trichloroethane ug/L 0.01 0.01 30 1,1-Dichloroethane ug/L 0.15J 0.01 30 1,1-Dichloroethene ug/L 0.01 0.01 30 1,2,3-Trichloropropane ug/L 0.01 0.01 30 1,2-Dibromo-3-chloropropane ug/L 0.01 0.01 30 1,2-Dibromoethane (EDB) ug/L 0.01 0.01 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 51 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 SAMPLE DUPLICATE: 144291 Parameter Units 92252070010 Result Dup Result 1,2-Dichlorobenzene ug/L O.OJ O.OJ 1,2-Dichloroethane ug/L O.OJ O.OJ 1,2-Dichloropropane ug/L O.OJ O.OJ 1,3-Dichloropropane ug/L O.OJ O.OJ 1,4-Dichlorobenzene ug/L 0.11J O.OJ 2-Butanone (MEK) ug/L O.OJ O.OJ 2-Hexanone ug/L O.OJ O.OJ 4-Methyl-2-pentanone (MIBK) ug/L O.OJ O.OJ Acetone ug/L 2.1 J 1.91 Acrylonitrile ug/L O.OJ O.OJ Benzene ug/L O.OJ O.OJ Bromochloromethane ug/L O.OJ O.OJ Bromodichloromethane ug/L O.OJ O.OJ Bromoform ug/L O.OJ O.OJ Bromomethane ug/L O.OJ O.OJ Carbon disulfide ug/L O.OJ O.OJ Carbon tetrachloride ug/L O.OJ O.OJ Chlorobenzene ug/L O.OJ O.OJ Chloroethane ug/L O.OJ O.OJ Chloroform ug/L O.OJ O.OJ Chloromethane ug/L O.OJ O.OJ cis-1,2-Dichloroethene ug/L O.OJ O.OJ cis-1,3-Dichloropropene ug/L O.OJ O.OJ Dibromochloromethane ug/L O.OJ O.OJ Dibromomethane ug/L O.OJ O.OJ Ethylbenzene ug/L O.OJ O.OJ lodomethane ug/L O.OJ O.OJ Methylene Chloride ug/L O.OJ O.OJ Styrene ug/L O.OJ O.OJ Tetrachloroethene ug/L O.OJ O.OJ Toluene ug/L O.OJ O.OJ trans-1,2-Dichloroethene ug/L O.OJ O.OJ trans- 1,3-Dichloropropene ug/L O.OJ O.OJ trans-1,4-Dichloro-2-butene ug/L O.OJ O.OJ Trichloroethene ug/L O.OJ O.OJ Trichlorofluoromethane ug/L O.OJ O.OJ Vinyl acetate ug/L O.OJ O.OJ Vinyl chloride ug/L O.OJ O.OJ Xylene (Total) ug/L 0.000000000 0.0000000001 10J 1,2-Dichloroethane-d4 (S) % 102 102 4-Bromofluorobenzene (S) % 97 100 Toluene-d8(S) % 100 98 Max RPD RPD Qualifiers 0 4 1 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 52 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 QC Batch: WET/37952 Analysis Method: SM 2320B QC Batch Method: SM 2320B Analysis Description: 2320E Alkalinity Associated Lab Samples: 92252070003, 92252070007, 92252070008, 92252070009, 92252070015 METHOD BLANK: 1478318 Matrix: Water Associated Lab Samples: 92252070003, 92252070007, 92252070008, 92252070009, 92252070015 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Alkalinity, Total as CaCO3 ug/L ND 5000 06/08/15 17:50 LABORATORY CONTROL SAMPLE: 1478319 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 47400 95 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1478320 1478321 MS MSD 92251906010 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 39.6 mg/L 50000 50000 86500 84100 94 89 90-110 3 4 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1478322 1478323 MS MSD 92252474001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 192 mg/L 50000 50000 218000 220000 53 58 90-110 1 4 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 53 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 QC Batch: WET/37973 Analysis Method: SM 2320B QC Batch Method: SM 2320B Analysis Description: 2320E Alkalinity Associated Lab Samples: 92252070001, 92252070002, 92252070004, 92252070005, 92252070006, 92252070010, 92252070011, 92252070012,92252070013,92252070014,92252070016,92252070017 METHOD BLANK: 1479236 Matrix: Water Associated Lab Samples: 92252070001, 92252070002, 92252070004, 92252070005, 92252070006, 92252070010, 92252070011, 92252070012,92252070013,92252070014,92252070016,92252070017 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Alkalinity, Total as CaCO3 ug/L ND 5000 06/09/15 19:18 LABORATORY CONTROL SAMPLE: 1479237 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 47600 95 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1479238 1479239 MS MSD 92253094001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 27.5 mg/L 50000 50000 76500 77700 98 101 90-110 2 4 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1479240 1479241 MS MSD 92252070011 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 8200 50000 50000 500000 509000 983 1001 90-110 2 4 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 54 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 QC Batch: WETA/23162 Analysis Method: EPA 300.0 QC Batch Method: EPA 300.0 Analysis Description: 300.0 IC Anions Associated Lab Samples: 92252070001, 92252070002, 92252070003, 92252070004, 92252070005, 92252070006, 92252070007, 92252070008,92252070009 METHOD BLANK: 1475158 Matrix: Water Associated Lab Samples: 92252070001, 92252070002, 92252070003, 92252070004, 92252070005, 92252070006, 92252070007, 92252070008,92252070009 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfate ug/L ND 250000 06/05/1519:41 LABORATORY CONTROL SAMPLE: 1475159 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate ug/L 20000 20000J 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1475160 1475161 MS MSD 92252271001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L ND 20000 20000 20300J 20300J 102 102 90-110 0 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1475162 1475163 MS MSD 92252055001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 12000J 20000 20000 33100J 33200J 106 106 90-110 0 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 55 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 QC Batch: WETA/23216 Analysis Method: EPA 300.0 QC Batch Method: EPA 300.0 Analysis Description: 300.0 IC Anions Associated Lab Samples: 92252070010, 92252070011, 92252070012, 92252070013, 92252070014, 92252070015, 92252070016, 92252070017 METHOD BLANK: 1479613 Matrix: Water Associated Lab Samples: 92252070010, 92252070011, 92252070012, 92252070013, 92252070014, 92252070015, 92252070016, 92252070017 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfate ug/L ND 250000 06/09/1515:16 LABORATORY CONTROL SAMPLE: 1479614 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate ug/L 20000 19600J 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1479615 1479616 MS MSD 92252593001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 5.9 mg/L 20000 20000 25500J 25400J 98 97 90-110 0 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1479617 1479618 MS MSD 92252070014 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 80901 20000 20000 28400J 28600J 102 102 90-110 1 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 56 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 QC Batch: WETA/23157 Analysis Method: SM 4500-CI-E QC Batch Method: SM 4500-CI-E Analysis Description: 4500 Chloride Associated Lab Samples: 92252070001, 92252070002, 92252070003, 92252070004, 92252070005, 92252070006, 92252070007, 92252070008,92252070009,92252070010,92252070011,92252070012,92252070013,92252070014 METHOD BLANK: 1474756 Matrix: Water Associated Lab Samples: 92252070001, 92252070002, 92252070003, 92252070004, 92252070005, 92252070006, 92252070007, 92252070008,92252070009,92252070010,92252070011,92252070012,92252070013,92252070014 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride ug/L ND 1000 06/06/15 06:48 LABORATORY CONTROL SAMPLE: 1474757 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride ug/L 20000 19800 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1474758 1474759 MS MSD 92252474003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 5.0 mg/L 20000 20000 23900 23700 95 93 90-110 1 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1474760 1474761 MS MSD 92252070005 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 42600 20000 20000 61400 64900 94 111 90-110 6 10 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 57 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 QC Batch: WETA/23195 Analysis Method: SM 4500-CI-E QC Batch Method: SM 4500-CI-E Analysis Description: 4500 Chloride Associated Lab Samples: 92252070016, 92252070017 METHOD BLANK: 1478839 Matrix: Water Associated Lab Samples: 92252070016, 92252070017 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride ug/L ND 1000 06/09/15 05:13 LABORATORY CONTROL SAMPLE: 1478840 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride ug/L 20000 20400 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1478841 1478842 MS MSD 92253008001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 65.7 mg/L 20000 20000 98300 86100 163 102 90-110 13 10 M1,R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1479013 1479014 MS MSD 92252368001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 12.7 mg/L 20000 20000 34100 34000 107 106 90-110 0 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 58 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 QC Batch: WETA/23242 Analysis Method: SM 4500-CI-E QC Batch Method: SM 4500-CI-E Analysis Description: 4500 Chloride Associated Lab Samples: 92252070015 METHOD BLANK: 1481788 Matrix: Water Associated Lab Samples: 92252070015 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride ug/L ND 1000 06/12/15 04:44 LABORATORY CONTROL SAMPLE: 1481789 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride ug/L 20000 20200 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1481790 1481791 MS MSD 92252070015 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 28200 20000 20000 49300 47300 106 96 90-110 4 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1481792 1481793 MS MSD 92253609001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 3.5 mg/L 20000 20000 23100 23600 98 100 90-110 2 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 59 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 QC Batch: WETA/23115 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92252070012 METHOD BLANK: 1471738 Matrix: Water Associated Lab Samples: 92252070012 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand ug/L ND 25000 06/02/15 09:50 LABORATORY CONTROL SAMPLE: 1471739 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand ug/L 750000 785000 105 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1471740 1471741 MS MSD 92251288003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chemical Oxygen Demand ug/L ND 750000 750000 778000 778000 103 103 90-110 0 3 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1471742 1471743 MS MSD 92251814001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chemical Oxygen Demand ug/L ND 750000 750000 756000 756000 101 101 90-110 0 3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 60 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 QC Batch: WETA/23116 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92252070013, 92252070014, 92252070015, 92252070016, 92252070017 METHOD BLANK: 1471818 Matrix: Water Associated Lab Samples: 92252070013, 92252070014, 92252070015, 92252070016, 92252070017 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand ug/L ND 25000 06/02/15 09:35 LABORATORY CONTROL SAMPLE: 1471819 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand ug/L 750000 787000 105 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1471820 1471821 MS MSD 92252070013 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chemical Oxygen Demand ug/L ND 750000 750000 808000 808000 107 107 90-110 0 3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 61 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 QC Batch: WETA/23179 Analysis Method: SM 5310B QC Batch Method: SM 5310B Analysis Description: 5310E TOC Associated Lab Samples: 92252070001, 92252070002, 92252070003, 92252070004, 92252070005, 92252070006, 92252070007, 92252070008, 92252070009, 92252070010, 92252070012, 92252070013, 92252070014, 92252070015, 92252070016,92252070017 METHOD BLANK: 1476921 Matrix: Water Associated Lab Samples: 92252070001, 92252070002, 92252070003, 92252070004, 92252070005, 92252070006, 92252070007, 92252070008, 92252070009, 92252070010, 92252070012, 92252070013, 92252070014, 92252070015, 92252070016,92252070017 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon ug/L ND 1000 06/06/15 01:25 LABORATORY CONTROL SAMPLE: 1476922 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carbon ug/L 25000 24200 97 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1476923 1476924 MS MSD 92252070001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Total Organic Carbon ug/L ND 25000 25000 24800 24700 97 97 90-110 0 5 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1476925 1476926 MS MSD 92252070012 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Total Organic Carbon ug/L ND 25000 25000 25100 25100 99 99 90-110 0 5 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 62 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALIFIERS Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits. L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated samples may be biased low. MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. MS Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the calculated result. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 63 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: SURRY CLOSED- MT AIRY (UIC) 92252070 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92252070001 MW-12D EPA 3010 MPRP/18587 EPA6010 ICP/16673 92252070002 MW-12S EPA 3010 MPRP/18587 EPA6010 ICP/16673 92252070003 MW-13 EPA 3010 MPRP/18587 EPA6010 ICP/16673 92252070004 MW-16 EPA 3010 MPRP/18587 EPA6010 ICP/16673 92252070005 MW-17 EPA 3010 MPRP/18587 EPA6010 ICP/16673 92252070006 MW-18 EPA 3010 MPRP/18587 EPA6010 ICP/16673 92252070007 MW-19 EPA 3010 MPRP/18587 EPA6010 ICP/16673 92252070008 MW-22 EPA 3010 MPRP/18587 EPA6010 ICP/16673 92252070009 MW-23 EPA 3010 MPRP/18587 EPA6010 ICP/16673 92252070010 MW-3R EPA 3010 MPRP/18587 EPA6010 ICP/16673 92252070011 MW-20 EPA 3010 MPRP/18587 EPA6010 ICP/16673 92252070012 MW-14 EPA 3010 MPRP/18587 EPA6010 ICP/16673 92252070013 MW-15 EPA 3010 MPRP/18587 EPA6010 ICP/16673 92252070014 MW-1 EPA 3010 MPRP/18587 EPA6010 ICP/16673 92252070015 MW-21 EPA 3010 MPRP/18587 EPA6010 ICP/16673 92252070016 MW-7 EPA 3010 MPRP/18587 EPA6010 ICP/16673 92252070017 MW-9 EPA 3010 MPRP/18587 EPA6010 ICP/16673 92252070001 MW-12D EPA 8260 MSV/32002 92252070002 MW-12S EPA 8260 MSV/32002 92252070003 MW-13 EPA 8260 MSV/32002 92252070004 MW-16 EPA 8260 MSV/32002 92252070005 MW-17 EPA 8260 MSV/32002 92252070006 MW-18 EPA 8260 MSV/32002 92252070007 MW-19 EPA 8260 MSV/32080 92252070008 MW-22 EPA 8260 MSV/32080 92252070009 MW-23 EPA 8260 MSV/32080 92252070010 MW-3R EPA 8260 MSV/32080 92252070011 MW-20 EPA 8260 MSV/32080 92252070012 MW-14 EPA 8260 MSV/32080 92252070013 MW-15 EPA 8260 MSV/32080 92252070014 MW-1 EPA 8260 MSV/32080 92252070015 MW-21 EPA 8260 MSV/32080 92252070016 MW-7 EPA 8260 MSV/32080 92252070017 MW-9 EPA 8260 MSV/32080 92252070001 MW-12D SM 2320B WET/37973 92252070002 MW-12S SM 2320B WET/37973 92252070003 MW-13 SM 2320B WET/37952 92252070004 MW-16 SM 2320B WET/37973 92252070005 MW-17 SM 2320B WET/37973 92252070006 MW-18 SM 2320B WET/37973 92252070007 MW-19 SM 2320B WET/37952 92252070008 MW-22 SM 2320B WET/37952 92252070009 MW-23 SM 2320B WET/37952 92252070010 MW-3R SM 2320B WET/37973 92252070011 MW-20 SM 2320B WET/37973 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 64 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Lab ID Sample ID QC Batch Method QC Batch 92252070012 MW-14 SM 2320B WET/37973 92252070013 MW-15 SM 2320B WET/37973 92252070014 MW-1 SM 2320B WET/37973 92252070015 MW-21 SM 2320B WET/37952 92252070016 MW-7 SM 2320B WET/37973 92252070017 MW-9 SM 2320B WET/37973 92252070001 MW-12D EPA 300.0 WETA/23162 92252070002 MW-12S EPA 300.0 WETA/23162 92252070003 MW-13 EPA 300.0 WETA/23162 92252070004 MW-16 EPA 300.0 WETA/23162 92252070005 MW-17 EPA 300.0 WETA/23162 92252070006 MW-18 EPA 300.0 WETA/23162 92252070007 MW-19 EPA 300.0 WETA/23162 92252070008 MW-22 EPA 300.0 WETA/23162 92252070009 MW-23 EPA 300.0 WETA/23162 92252070010 MW-3R EPA 300.0 WETA/23216 92252070011 MW-20 EPA 300.0 WETA/23216 92252070012 MW-14 EPA 300.0 WETA/23216 92252070013 MW-15 EPA 300.0 WETA/23216 92252070014 MW-1 EPA 300.0 WETA/23216 92252070015 MW-21 EPA 300.0 WETA/23216 92252070016 MW-7 EPA 300.0 WETA/23216 92252070017 MW-9 EPA 300.0 WETA/23216 92252070001 MW-12D SM 4500-CI-E WETA/23157 92252070002 MW-12S SM 4500-CI-E WETA/23157 92252070003 MW-13 SM 4500-CI-E WETA/23157 92252070004 MW-16 SM 4500-CI-E WETA/23157 92252070005 MW-17 SM 4500-CI-E WETA/23157 92252070006 MW-18 SM 4500-CI-E WETA/23157 92252070007 MW-19 SM 4500-CI-E WETA/23157 92252070008 MW-22 SM 4500-CI-E WETA/23157 92252070009 MW-23 SM 4500-CI-E WETA/23157 92252070010 MW-3R SM 4500-CI-E WETA/23157 92252070011 MW-20 SM 4500-CI-E WETA/23157 92252070012 MW-14 SM 4500-CI-E WETA/23157 92252070013 MW-15 SM 4500-CI-E WETA/23157 92252070014 MW-1 SM 4500-CI-E WETA/23157 92252070015 MW-21 SM 4500-CI-E WETA/23242 92252070016 MW-7 SM 4500-CI-E WETA/23195 92252070017 MW-9 SM 4500-CI-E WETA/23195 92252070012 MW-14 SM 5220D WETA/23115 92252070013 MW-15 SM 5220D WETA/23116 92252070014 MW-1 SM 5220D WETA/23116 92252070015 MW-21 SM 5220D WETA/23116 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 09:27 AM without the written consent of Pace Analytical Services, Inc.. Analytical Analytical Method Batch Page 65 of 72 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: SURRY CLOSED- MT AIRY (UIC) Pace Project No.: 92252070 Lab ID Sample ID QC Batch Method QC Batch 92252070016 MW-7 SM 5220D WETA/23116 92252070017 MW-9 SM 5220D WETA/23116 92252070001 MW-12D SM 5310B WETA/23179 92252070002 MW-12S SM 5310B WETA/23179 92252070003 MW-13 SM 5310B WETA/23179 92252070004 MW-16 SM 5310B WETA/23179 92252070005 MW-17 SM 5310B WETA/23179 92252070006 MW-18 SM 5310B WETA/23179 92252070007 MW-19 SM 5310B WETA/23179 92252070008 MW-22 SM 5310B WETA/23179 92252070009 MW-23 SM 5310B WETA/23179 92252070010 MW-3R SM 5310B WETA/23179 92252070012 MW-14 SM 5310B WETA/23179 92252070013 MW-15 SM 5310B WETA/23179 92252070014 MW-1 SM 5310B WETA/23179 92252070015 MW-21 SM 5310B WETA/23179 92252070016 MW-7 SM 5310B WETA/23179 92252070017 MW-9 SM 5310B WETA/23179 Date: 06/12/2015 09:27 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Analytical Method Analytical Batch Page 66 of 72 lJocument Number: F-CWR-CS-0034AVA R Issuing Authority: Pare HirntarGvilla rlrralitrr Office Client IVame. Uh!.C'CF'� IL21C��i/)C-0ln. • Page 2of2isfor Internal Use only Courier: ❑Fed Ex ❑ UPS❑ LISPS❑ Client❑ ornmercial❑ Pace Other { A'- ::� �. Custody Seal on Cooler/Box Present: ❑ yes no Seals intact: ❑ no v yes ❑ Packing Material: ❑ Bubble V❑p ❑ (gGNone ❑ Other rhermometer Used: IR Gun T1401 Type of Ice. &d / Blue None Samples on ice, cooling process has begun romp Correction Factor T` 401 No Correction •C 'orrecked Cooler Temp.:contents;_ Ideological Tissue is Frozen: Yes No�N Date and Initial of per o�} x fining /�} Temp should be above freezing to VC Comments: ,hWh'of Custody Present: s Yes DNo ❑NIA 1. ,hairs of Custody Filled Out: 0 e ONO ❑NIA 2. ,pain of Custody Relinquished: " Ye U ❑N!A 3. Sampler Name & Signature on COC: Yes('❑No ❑NIA 4. Samples Arrived within Hold Time: 14yes ❑No NIA 6, Short mold Time Analysis (<72hr): ❑Yes 13No NIA 6. lush Turn Around Time Requested: Dyes - Nk ❑NIA 7. Sufflcient Volume: OYe ` No ❑NIA $, ,orrect Containers Used: 0 ❑No t7NlA 9, -Pace Containers Used: Y 5 ❑No ❑NIA containers Intact: Yes ONO ❑NI 10. =altered volume received for Dissolved tests Dyes ONO ZN!A 112. 11. ;ample Labels match COC: ❑Yes No ❑NIA IVY L,�i -Includes dateltime/iD/Analysis Matrix: W .y kil containers needing preservation have been checked, Yes ❑No ❑N!A 13, VI containers needing preservation are found to be in Dyes 'No ❑NIA :ompliance with EPA recommendation. meeptions: VOA, coliform, TOO, O&G, VVl-DRO (water) 0 eynNo Samples checked for dechlorination: Yes ❑N ❑NIA 14. leadspace in VOA Vials(>6mm): ❑Yes dNo DNI.r 15. rrip Blank Present: Dyes ❑No ` Ivry 16. rrip Blank Custody Seals Present Dyes ❑No NIA 'ace -Trip -Blank -Lot #-(if-purchased):--.-- - - - - - 'alient Notification/ Resolution: / Field Data Required? Y 1 N Person Contacted: u.�� W-cam _L0LDate rime: Comments) Resolution: �,�+ t riff _l air r a _f4 its S,•.� �y C s� _p`.� �, _ 7 v. KG. Y SCURF Review: Date: 5 29 SRF Review:' Date: s' 10 0 Note: Whenever therer a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le out of hold, incorrect preservative, out of temp, incorrect containers) WO#:92252070 11111111111111111111111 92252070 Page 67 of 72 -1ceAnalyticaf Section A Required Client Information: Company: Municipal Engineer Address68 Shipwash Drive Garner, NC 27529 Email: Phone: Reouested Due Date: SAMPLE ID One Character per box. (A-Z, 0-9 / r -) Sample Ids must be uniqu F 1 MW-12D 2 tlAAu9�s r V, ' 1 3 MW-13 4 MW-14 5 MW-15 6 MW-16 7 MW-17 $ MW-18 9 MW-19 10 MW-1 11 MW-2D N CHAIN -OF -CUSTODY 1 Analytical Request Document 00 The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. CIDa, 1I d Section B Section C Required Project Information: Invoice Information: Page: t Of 2 ,Report To: Jonathan Pfohl Attention: Project Name: Surry Closed -Mt Airy (UZ Project #: MATRIX CODE � a o COLLECT Drinking Water DW a �j WMtar V17 Waste Walvr Product WW P ? > a Ur SNYSOd ow SL OL �_ START Wipe WP w Arc Other e AR CT Ts O U x C. � ¢ a N DATE TIME [ WT slap ww C wa.nI. WY six~s Cj'Al VVT sja 1d tC VJT 5 5 aI`fG WT Ths 4S WT si - is !a c WT Sjadfis s'iG wT s/aar`+s r! c c WT zlits 1ts� WT slasils :' WT 5jd3ls WT ADDITIONAL COMMENTS REIJNqutsHED SY! AFMUATION fFJy�'Sc� Pace Quote: Pace Project Manager: kevin.godwin pacelabs.com, Pace Profile #: Requested Ar a Z Preservatives > Q U W ro O Q n ENO f72 a W eJ o a z w a m 1 U o ° °T- a O s S 's z N z t 2 m Q a < a ¢ 6 co O O TIME ran a a Y 0 6 DATE TIME w1f S i FLIER NAME AND SIGNATURE PRINT Name of SAMPLER: SIGNATURE of SAMPLER: ACCEPTED BY r AFFILIATION Signed: State I Location 1� --d C� G' 66`''i DATE TIME SAMPLE CONDITIONS .2- 5 �CaL m /�acewia�ytl%a+r Section A Required Client Informationt Company: Municipal Engineering Sen Address: 68 Shipwash Drive Garner, NC 27529 Email: Phone: Fax Requested Due Date: SAMPLE ID One Character per box. (A-Z, 0.9 1, -) Sample Ids must be unique W t- 13 MW-22 14 MW-23 15 MW-3R 16 MW-7 17 MW-9 18 19 20 21 22 23 Section 8 Required Project Information: Report TO: ,Jonathan Pfohl Copy To: Purchase Order #: Project Name: Surry Closed-Mi MATRIX CODE DrinkOng water DW m a a OU U I Waler WT Wy[G WaIGr wW b a PrOd�c P z,vsalid SL V, od OL START wipe WA A1r AR a w 4 Clhar CT U 7-- TS y N s DATE T WT wT :fad u 4,45 N CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately- a m Section C a Invoice Information: Page ; 2 Of 2 Attention: Company Name: Address: Regulatory Agency Pace Quote: IC) Pace Project Manager: kevin.godwin pacelabs.oem, State / Location Pace Profile #'. = rIGJCIVGtIVCJ V J 0 OU N END ¢ d � w F UZ a r = U, U 0 M C O c N z U m L Q a 2 y O O TTIME a * S x 2 x z z z E) ¢ ¢ ¢ F U ADDITIONAL COMMENTS ItELINCUISHED BY I AFFILIATION DATE TIME f _ s asf S L ACCEPTED BY I AFFILIATION DATE I TIME n ?" FL s� •� ,� iz SAMPLE CONDITIONS iPLER NAME AND SIGNATURE 0 PRINT Name of SAMPLER:0r.0 m SIGNATURE of SA DATE Signed- u Z 2. o z E o Z lJocument Number: F-CWR-CS-0034AVA R Issuing Authority: Pare HirntarGvilla rlrralitrr Office Client IVame. Uh!.C'CF'� IL21C��i/)C-0ln. • Page 2of2isfor Internal Use only Courier: ❑Fed Ex ❑ UPS❑ LISPS❑ Client❑ ornmercial❑ Pace Other { A'- ::� �. Custody Seal on Cooler/Box Present: ❑ yes no Seals intact: ❑ no v yes ❑ Packing Material: ❑ Bubble V❑p ❑ (gGNone ❑ Other rhermometer Used: IR Gun T1401 Type of Ice. &d / Blue None Samples on ice, cooling process has begun romp Correction Factor T` 401 No Correction •C 'orrecked Cooler Temp.:contents;_ Ideological Tissue is Frozen: Yes No�N Date and Initial of per o�} x fining /�} Temp should be above freezing to VC Comments: ,hWh'of Custody Present: s Yes DNo ❑NIA 1. ,hairs of Custody Filled Out: 0 e ONO ❑NIA 2. ,pain of Custody Relinquished: " Ye U ❑N!A 3. Sampler Name & Signature on COC: Yes('❑No ❑NIA 4. Samples Arrived within Hold Time: 14yes ❑No NIA 6, Short mold Time Analysis (<72hr): ❑Yes 13No NIA 6. lush Turn Around Time Requested: Dyes - Nk ❑NIA 7. Sufflcient Volume: OYe ` No ❑NIA $, ,orrect Containers Used: 0 ❑No t7NlA 9, -Pace Containers Used: Y 5 ❑No ❑NIA containers Intact: Yes ONO ❑NI 10. =altered volume received for Dissolved tests Dyes ONO ZN!A 112. 11. ;ample Labels match COC: ❑Yes No ❑NIA IVY L,�i -Includes dateltime/iD/Analysis Matrix: W .y kil containers needing preservation have been checked, Yes ❑No ❑N!A 13, VI containers needing preservation are found to be in Dyes 'No ❑NIA :ompliance with EPA recommendation. meeptions: VOA, coliform, TOO, O&G, VVl-DRO (water) 0 eynNo Samples checked for dechlorination: Yes ❑N ❑NIA 14. leadspace in VOA Vials(>6mm): ❑Yes dNo DNI.r 15. rrip Blank Present: Dyes ❑No ` Ivry 16. rrip Blank Custody Seals Present Dyes ❑No NIA 'ace -Trip -Blank -Lot #-(if-purchased):--.-- - - - - - 'alient Notification/ Resolution: / Field Data Required? Y 1 N Person Contacted: u.�� W-cam _L0LDate rime: Comments) Resolution: �,�+ t riff _l air r a _f4 its S,•.� �y C s� _p`.� �, _ 7 v. KG. Y SCURF Review: Date: 5 29 SRF Review:' Date: s' 10 0 Note: Whenever therer a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le out of hold, incorrect preservative, out of temp, incorrect containers) WO#:92252070 11111111111111111111111 92252070 Page 70 of 72 -1ceAnalyticaf Section A Required Client Information: Company: Municipal Engineer Address68 Shipwash Drive Garner, NC 27529 Email: Phone: Reouested Due Date: SAMPLE ID One Character per box. (A-Z, 0-9 / r -) Sample Ids must be uniqu F 1 MW-12D 2 tlAAu9�s r V, ' 1 3 MW-13 4 MW-14 5 MW-15 6 MW-16 7 MW-17 $ MW-18 9 MW-19 10 MW-1 11 MW-2D N CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. a 1I CIDD- Section B Section C Required Project Information: Invoice Information: Page: t Of 2 ,Report To: Jonathan Pfohl Attention: Project Name: Surry Closed -Mt Airy (UZ Project #: MATRIX CODE � a o COLLECT Drinking Water DW a �j WMtar V17 Waste Walvr Product WW P ? > a Ur SNYSOd ow SL OL �_ START Wipe WP w Arc Other e AR CT Ts O U x C. � ¢ a N DATE TIME [ WT slap ww C wa.nI. WY six~s Cj'Al VVT sja 1d tC VJT 5 5 aI`fG WT Ths 4S WT si - is !a c WT Sjadfis s'iG wT s/aar`+s r! c c WT zlits 1ts� WT slasils :' WT 5jd3ls WT ADDITIONAL COMMENTS REIJNqutsHED SY! AFMUATION fFJy�'Sc� Pace Quote: Pace Project Manager: kevin.godwin pacelabs.com, Pace Profile #: Requested Ar a Z Preservatives > Q U W ro O Q n ENO f72 a W eJ o a z w a m 1 U o ° °T- a O s S 's z N z t 2 m Q a < a ¢ 6 co O O TIME ran a a Y 0 6 DATE TIME w1f S i FLIER NAME AND SIGNATURE PRINT Name of SAMPLER: SIGNATURE of SAMPLER: ACCEPTED BY r AFFILIATION Signed: State I Location 1� --d C� G' 66`''i DATE TIME SAMPLE CONDITIONS .2- 5 �CaL m /�acewia�ytl%a+r Section A Required Client Informationt Company: Municipal Engineering Sen Address: 68 Shipwash Drive Garner, NC 27529 Email: Phone: Fax Requested Due Date: SAMPLE ID One Character per box. (A-Z, 0.9 1, -) Sample Ids must be unique W t- 13 MW-22 14 MW-23 15 MW-3R 16 MW-7 17 MW-9 18 19 20 21 22 23 Section 8 Required Project Information: Report TO: ,Jonathan Pfohl Copy To: Purchase Order #: Project Name: Surry Closed-Mi MATRIX CODE DrinkOng water DW m a a OU U I Waler WT Wy[G WaIGr wW b a PrOd�c P z,vsalid SL V, od OL START wipe WA A1r AR a w 4 Clhar CT U 7-- TS y N s DATE T WT wT :fad u 4,45 N CHAIN -OF -CUSTODY 1 Analytical Request Document CN The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately- a m Section C a Invoice Information: Page ; 2 Of 2 Attention: Company Name: Address: Regulatory Agency Pace Quote: IC) Pace Project Manager: kevin.godwin pacelabs.oem, State / Location Pace Profile #'. = rIGJCIVGtIVCJ V J 0 OU N END ¢ d � w F UZ a r = >� c U TTIME 0 M C O c N z U m L Q a 2 y O O a * S x 2 x z z z E) ¢ ¢ ¢ F U ADDITIONAL COMMENTS ItELINCUISHED BY I AFFILIATION DATE TIME f _ s asf S L ACCEPTED BY I AFFILIATION DATE I TIME n ?" FL s� •� ,� iz SAMPLE CONDITIONS iPLER NAME AND SIGNATURE 0 PRINT Name of SAMPLER:0r.0 m SIGNATURE of SA DATE Signed- u Z 2. o z E o Z aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 June 12, 2015 Mr. Jonathan Pfohl Municipal Engineering Services PO Box 97 Garner, NC 27529 RE: Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory on May 29, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Godwin kevin.godwin@pacelabs.com Project Manager Enclosures Q _Kok r REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 SAMPLE SUMMARY Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 Lab ID Sample ID Matrix Date Collected Date Received 92252055001 MW-11 Water 05/28/1517:00 05/29/15 13:00 92252055002 MW-14 Water 05/28/1514:40 05/29/15 13:00 92252055003 MW-15 Water 05/28/1513:40 05/29/15 13:00 92252055004 MW-1 Water 05/28/15 08:15 05/29/15 13:00 92252055005 MW-21 Water 05/27/1514:35 05/29/15 13:00 92252055006 MW-6 Water 05/27/1511:35 05/29/15 13:00 92252055007 MW-7 Water 05/28/15 09:10 05/29/15 13:00 92252055008 MW-9 Water 05/28/1516:15 05/29/15 13:00 92252055009 SCALEHOUSE Water 05/28/1517:00 05/29/15 13:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: Surry Closed -Mt Airy (AM) 92252055 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92252055001 MW-11 EPA 6010 JMW 15 PASI-A EPA 6010 JMW 1 PASI-A EPA 8260 GAW 51 PASI-C SM 2320B MLS 1 PASI-A SM 4500-S2D MAB 1 PASI-A EPA 300.0 AES2 1 PASI-A SM 4500-CI-E SER 1 PASI-A SM 5220D MAB 1 PASI-A SM 5310B AES2 1 PASI-A 92252055002 MW-14 EPA 6010 JMW 1 PASI-A SM 4500-S2D MAB 1 PASI-A 92252055003 MW-15 EPA 6010 JMW 1 PASI-A SM 4500-S2D MAB 1 PASI-A 92252055004 MW-1 EPA 6010 JMW 1 PASI-A SM 4500-S2D MAB 1 PASI-A 92252055005 MW-21 SM 4500-S2D MAB 1 PASI-A 92252055006 MW-6 EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C 92252055007 MW-7 EPA 6010 JMW 1 PASI-A SM 4500-S2D MAB 1 PASI-A 92252055008 MW-9 SM 4500-S2D MAB 1 PASI-A 92252055009 SCALEHOUSE EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 Sample: MW-11 Lab ID: 92252055001 Collected: 05/28/15 17:00 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 3.8 1 06/01/15 20:15 06/04/15 19:08 7440-36-0 Arsenic ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:08 7440-38-2 Barium 32.1J ug/L 100 2.5 1 06/01/15 20:15 06/04/15 19:08 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:08 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:08 7440-43-9 Chromium ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:08 7440-47-3 Cobalt 12.6 ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:08 7440-48-4 Copper ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:08 7440-50-8 Lead ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:08 7439-92-1 Nickel ND ug/L 50.0 2.5 1 06/01/15 20:15 06/04/15 19:08 7440-02-0 Selenium ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:08 7782-49-2 Silver ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:08 7440-22-4 Thallium ND ug/L 5.5 5.0 1 06/01/15 20:15 06/04/15 19:08 7440-28-0 Vanadium ND ug/L 25.0 2.5 1 06/01/15 20:15 06/04/15 19:08 7440-62-2 Zinc 6.3J ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:08 7440-66-6 6010 MET ICP, Dissolved Analytical Method: EPA 6010 Preparation Method: EPA 3010 Iron, Dissolved 101 ug/L 50.0 25.0 1 06/02/15 23:46 06/04/15 20:42 7439-89-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 06/04/15 20:00 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 06/04/15 20:00 107-13-1 Benzene 0.82J ug/L 1.0 0.25 1 06/04/15 20:00 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 06/04/15 20:00 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 06/04/15 20:00 75-27-4 Bromoform ND ug/L 3.0 0.26 1 06/04/15 20:00 75-25-2 L2 Bromomethane 0.71J ug/L 10.0 0.29 1 06/04/15 20:00 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 06/04/15 20:00 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 06/04/15 20:00 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 06/04/15 20:00 56-23-5 Chlorobenzene 1.2J ug/L 3.0 0.23 1 06/04/15 20:00 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 06/04/15 20:00 75-00-3 Chloroform ND ug/L 5.0 0.14 1 06/04/15 20:00 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 06/04/15 20:00 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 06/04/15 20:00 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 06/04/15 20:00 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 06/04/15 20:00 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 06/04/15 20:00 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 06/04/15 20:00 95-50-1 1,4-Dichlorobenzene 4.3 ug/L 1.0 0.33 1 06/04/15 20:00 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/04/15 20:00 110-57-6 1,1-Dichloroethane 0.85J ug/L 5.0 0.32 1 06/04/15 20:00 75-34-3 1,2-Dichloroethane 0.32J ug/L 1.0 0.12 1 06/04/15 20:00 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/04/15 20:00 75-35-4 cis-1,2-Dichloroethene 2.3J ug/L 5.0 0.19 1 06/04/15 20:00 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/04/15 20:00 156-60-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 07:48 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 Sample: MW-11 Lab ID: 92252055001 Collected: 05/28/15 17:00 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 1,2-Dichloropropane 1.8 ug/L 1.0 0.27 1 06/04/15 20:00 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 06/04/15 20:00 142-28-9 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/04/15 20:00 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/15 20:00 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/15 20:00 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/04/15 20:00 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/15 20:00 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/15 20:00 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/15 20:00 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/04/15 20:00 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/15 20:00 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/15 20:00 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/15 20:00 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/15 20:00 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/15 20:00 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/15 20:00 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/15 20:00 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/15 20:00 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/15 20:00 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/15 20:00 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/15 20:00 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/15 20:00 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 06/04/15 20:00 460-00-4 1,2-Dichloroethane-d4 (S) 100 % 70-130 1 06/04/15 20:00 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 06/04/15 20:00 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 20400 ug/L 5000 1000 1 06/09/15 20:33 4500S2D Sulfide Water Analytical Method: SM 4500-S2D Sulfide ND ug/L 1000 100 1 06/02/1516:10 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate 12000J ug/L 250000 1000 1 06/05/15 23:45 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E Chloride 7030 ug/L 1000 500 1 06/06/15 06:57 16887-00-6 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand ND ug/L 25000 12500 1 06/02/15 09:50 531013 TOC Analytical Method: SM 5310B Total Organic Carbon 1000 ug/L 1000 500 1 06/05/15 19:36 7440-44-0 Date: 06/12/2015 07:48 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 Sample: MW-14 Lab ID: 92252055002 Collected: 05/28/15 14:40 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP, Dissolved Analytical Method: EPA 6010 Preparation Method: EPA 3010 Iron, Dissolved 294 ug/L 50.0 25.0 1 06/02/15 23:46 06/04/15 20:51 7439-89-6 4500S2D Sulfide Water Analytical Method: SM 4500-S21D Sulfide ND ug/L 1000 100 1 06/02/1516:10 18496-25-8 Date: 06/12/2015 07:48 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 7 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 Sample: MW-15 Lab ID: 92252055003 Collected: 05/28/15 13:40 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP, Dissolved Analytical Method: EPA 6010 Preparation Method: EPA 3010 Iron, Dissolved 6420 ug/L 50.0 25.0 1 06/02/15 23:46 06/04/15 20:54 7439-89-6 4500S2D Sulfide Water Analytical Method: SM 4500-S21D Sulfide ND ug/L 1000 100 1 06/02/1516:10 18496-25-8 Date: 06/12/2015 07:48 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 8 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 Sample: MW-1 Lab ID: 92252055004 Collected: 05/28/15 08:15 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP, Dissolved Analytical Method: EPA 6010 Preparation Method: EPA 3010 Iron, Dissolved 29.6J ug/L 50.0 25.0 1 06/02/15 23:46 06/04/15 21:06 7439-89-6 4500S2D Sulfide Water Analytical Method: SM 4500-S21D Sulfide ND ug/L 1000 100 1 06/02/1516:30 18496-25-8 Date: 06/12/2015 07:48 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 9 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 Sample: MW-21 Lab ID: 92252055005 Collected: 05/27/15 14:35 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 4500S21) Sulfide Water Analytical Method: SM 4500-S21D Sulfide ND ug/L 1000 100 1 06/02/1516:10 18496-25-8 Date: 06/12/2015 07:48 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 Sample: MW-6 Lab ID: 92252055006 Collected: 05/27/15 11:35 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane cis-1,3-Dichloropropene Date: 06/12/2015 07:48 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010 ND ug/L 6.0 3.8 1 06/01/15 20:15 06/04/15 19:16 7440-36-0 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:16 7440-38-2 85.6J ug/L 100 2.5 1 06/01/15 20:15 06/04/15 19:16 7440-39-3 ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:16 7440-41-7 ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:16 7440-43-9 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:16 7440-47-3 68.9 ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:16 7440-48-4 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:16 7440-50-8 3.2J ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:16 7439-92-1 2.8J ug/L 50.0 2.5 1 06/01/15 20:15 06/04/15 19:16 7440-02-0 ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:16 7782-49-2 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:16 7440-22-4 ND ug/L 5.5 5.0 1 06/01/15 20:15 06/04/15 19:16 7440-28-0 10.6J ug/L 25.0 2.5 1 06/01/15 20:15 06/04/15 19:16 7440-62-2 ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:16 7440-66-6 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 06/04/15 20:17 67-64-1 ND ug/L 200 1.9 1 06/04/15 20:17 107-13-1 ND ug/L 1.0 0.25 1 06/04/15 20:17 71-43-2 ND ug/L 3.0 0.17 1 06/04/15 20:17 74-97-5 ND ug/L 1.0 0.18 1 06/04/15 20:17 75-27-4 ND ug/L 3.0 0.26 1 06/04/15 20:17 75-25-2 ND ug/L 10.0 0.29 1 06/04/15 20:17 74-83-9 ND ug/L 100 0.96 1 06/04/15 20:17 78-93-3 ND ug/L 100 1.2 1 06/04/15 20:17 75-15-0 ND ug/L 1.0 0.25 1 06/04/15 20:17 56-23-5 ND ug/L 3.0 0.23 1 06/04/15 20:17 108-90-7 ND ug/L 10.0 0.54 1 06/04/15 20:17 75-00-3 ND ug/L 5.0 0.14 1 06/04/15 20:17 67-66-3 ND ug/L 1.0 0.11 1 06/04/15 20:17 74-87-3 ND ug/L 13.0 2.0 1 06/04/15 20:17 96-12-8 ND ug/L 3.0 0.21 1 06/04/15 20:17 124-48-1 ND ug/L 1.0 0.27 1 06/04/15 20:17 106-93-4 ND ug/L 10.0 0.21 1 06/04/15 20:17 74-95-3 ND ug/L 5.0 0.30 1 06/04/15 20:17 95-50-1 ND ug/L 1.0 0.33 1 06/04/15 20:17 106-46-7 ND ug/L 100 1.0 1 06/04/15 20:17 110-57-6 ND ug/L 5.0 0.32 1 06/04/15 20:17 75-34-3 ND ug/L 1.0 0.12 1 06/04/15 20:17 107-06-2 ND ug/L 5.0 0.56 1 06/04/15 20:17 75-35-4 ND ug/L 5.0 0.19 1 06/04/15 20:17 156-59-2 ND ug/L 5.0 0.49 1 06/04/15 20:17 156-60-5 ND ug/L 1.0 0.27 1 06/04/15 20:17 78-87-5 ND ug/L 1.0 0.28 1 06/04/15 20:17 142-28-9 ND ug/L 1.0 0.13 1 06/04/15 20:17 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. L2 Page 11 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 Sample: MW-6 Lab ID: 92252055006 Collected: 05/27/15 11:35 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/15 20:17 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/15 20:17 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/04/15 20:17 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/15 20:17 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/15 20:17 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/15 20:17 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/04/15 20:17 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/15 20:17 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/15 20:17 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/15 20:17 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/15 20:17 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/15 20:17 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/15 20:17 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/15 20:17 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/15 20:17 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/15 20:17 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/15 20:17 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/15 20:17 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/15 20:17 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 06/04/15 20:17 460-00-4 1,2-Dichloroethane-d4 (S) 102 % 70-130 1 06/04/15 20:17 17060-07-0 Toluene-d8 (S) 101 % 70-130 1 06/04/15 20:17 2037-26-5 Date: 06/12/2015 07:48 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 12 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 Sample: MW-7 Lab ID: 92252055007 Collected: 05/28/15 09:10 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP, Dissolved Analytical Method: EPA 6010 Preparation Method: EPA 3010 Iron, Dissolved ND ug/L 50.0 25.0 1 06/02/15 23:46 06/04/15 21:09 7439-89-6 4500S2D Sulfide Water Analytical Method: SM 4500-S21D Sulfide ND ug/L 1000 100 1 06/02/1516:30 18496-25-8 Date: 06/12/2015 07:48 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 13 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 Sample: MW-9 Lab ID: 92252055008 Collected: 05/28/15 16:15 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 4500S21) Sulfide Water Analytical Method: SM 4500-S21D Sulfide ND ug/L 1000 100 1 06/02/1516:30 18496-25-8 Date: 06/12/2015 07:48 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 14 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 Sample: SCALEHOUSE Lab ID: 92252055009 Collected: 05/28/15 17:00 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane cis-1,3-Dichloropropene Date: 06/12/2015 07:48 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010 ND ug/L 6.0 3.8 1 06/01/15 20:15 06/04/15 19:20 7440-36-0 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:20 7440-38-2 10.91 ug/L 100 2.5 1 06/01/15 20:15 06/04/15 19:20 7440-39-3 ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:20 7440-41-7 ND ug/L 1.0 0.50 1 06/01/15 20:15 06/04/15 19:20 7440-43-9 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:20 7440-47-3 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:20 7440-48-4 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:20 7440-50-8 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:20 7439-92-1 ND ug/L 50.0 2.5 1 06/01/15 20:15 06/04/15 19:20 7440-02-0 ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:20 7782-49-2 ND ug/L 10.0 2.5 1 06/01/15 20:15 06/04/15 19:20 7440-22-4 ND ug/L 5.5 5.0 1 06/01/15 20:15 06/04/15 19:20 7440-28-0 ND ug/L 25.0 2.5 1 06/01/15 20:15 06/04/15 19:20 7440-62-2 ND ug/L 10.0 5.0 1 06/01/15 20:15 06/04/15 19:20 7440-66-6 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 06/04/15 20:34 67-64-1 ND ug/L 200 1.9 1 06/04/15 20:34 107-13-1 ND ug/L 1.0 0.25 1 06/04/15 20:34 71-43-2 ND ug/L 3.0 0.17 1 06/04/15 20:34 74-97-5 ND ug/L 1.0 0.18 1 06/04/15 20:34 75-27-4 ND ug/L 3.0 0.26 1 06/04/15 20:34 75-25-2 ND ug/L 10.0 0.29 1 06/04/15 20:34 74-83-9 ND ug/L 100 0.96 1 06/04/15 20:34 78-93-3 ND ug/L 100 1.2 1 06/04/15 20:34 75-15-0 ND ug/L 1.0 0.25 1 06/04/15 20:34 56-23-5 ND ug/L 3.0 0.23 1 06/04/15 20:34 108-90-7 ND ug/L 10.0 0.54 1 06/04/15 20:34 75-00-3 ND ug/L 5.0 0.14 1 06/04/15 20:34 67-66-3 0.14J ug/L 1.0 0.11 1 06/04/15 20:34 74-87-3 ND ug/L 13.0 2.0 1 06/04/15 20:34 96-12-8 ND ug/L 3.0 0.21 1 06/04/15 20:34 124-48-1 ND ug/L 1.0 0.27 1 06/04/15 20:34 106-93-4 ND ug/L 10.0 0.21 1 06/04/15 20:34 74-95-3 ND ug/L 5.0 0.30 1 06/04/15 20:34 95-50-1 ND ug/L 1.0 0.33 1 06/04/15 20:34 106-46-7 ND ug/L 100 1.0 1 06/04/15 20:34 110-57-6 ND ug/L 5.0 0.32 1 06/04/15 20:34 75-34-3 ND ug/L 1.0 0.12 1 06/04/15 20:34 107-06-2 ND ug/L 5.0 0.56 1 06/04/15 20:34 75-35-4 0.22J ug/L 5.0 0.19 1 06/04/15 20:34 156-59-2 ND ug/L 5.0 0.49 1 06/04/15 20:34 156-60-5 ND ug/L 1.0 0.27 1 06/04/15 20:34 78-87-5 ND ug/L 1.0 0.28 1 06/04/15 20:34 142-28-9 ND ug/L 1.0 0.13 1 06/04/15 20:34 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. L2 Page 15 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 Sample: SCALEHOUSE Lab ID: 92252055009 Collected: 05/28/15 17:00 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/15 20:34 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/15 20:34 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/04/15 20:34 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/15 20:34 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/15 20:34 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/15 20:34 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/04/15 20:34 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/15 20:34 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/15 20:34 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/15 20:34 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/15 20:34 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/15 20:34 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/15 20:34 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/15 20:34 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/15 20:34 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/15 20:34 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/15 20:34 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/15 20:34 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/15 20:34 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 06/04/15 20:34 460-00-4 1,2-Dichloroethane-d4 (S) 102 % 70-130 1 06/04/15 20:34 17060-07-0 Toluene-d8 (S) 101 % 70-130 1 06/04/15 20:34 2037-26-5 Date: 06/12/2015 07:48 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 16 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 QC Batch: MPRP/18587 Analysis Method: EPA6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET NC Groundwater Associated Lab Samples: 92252055001, 92252055006, 92252055009 METHOD BLANK: 1472278 Matrix: Water Associated Lab Samples: 92252055001, 92252055006, 92252055009 Blank Reporting Parameter Units Result Limit Antimony ug/L N D Arsenic ug/L ND Barium ug/L ND Beryllium ug/L ND Cadmium ug/L ND Chromium ug/L ND Cobalt ug/L ND Copper ug/L ND Lead ug/L ND Nickel ug/L ND Selenium ug/L ND Silver ug/L ND Thallium ug/L ND Vanadium ug/L ND Zinc ug/L ND Analyzed 6.0 06/04/1518:53 10.0 06/04/1518:53 100 06/04/1518:53 1.0 06/04/1518:53 1.0 06/04/1518:53 10.0 06/04/1518:53 10.0 06/04/1518:53 10.0 06/04/1518:53 10.0 06/04/1518:53 50.0 06/04/1518:53 10.0 06/04/1518:53 10.0 06/04/1518:53 5.5 06/04/1518:53 25.0 06/04/1518:53 10.0 06/04/1518:53 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 1472279 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 500 480 96 80-120 Arsenic ug/L 500 465 93 80-120 Barium ug/L 500 458 92 80-120 Beryllium ug/L 500 462 92 80-120 Cadmium ug/L 500 460 92 80-120 Chromium ug/L 500 456 91 80-120 Cobalt ug/L 500 459 92 80-120 Copper ug/L 500 451 90 80-120 Lead ug/L 500 456 91 80-120 Nickel ug/L 500 460 92 80-120 Selenium ug/L 500 439 88 80-120 Silver ug/L 250 228 91 80-120 Thallium ug/L 500 466 93 80-120 Vanadium ug/L 500 444 89 80-120 Zinc ug/L 500 460 92 80-120 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 07:48 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: Surry Closed -Mt Airy (AM) 92252055 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1472280 1472281 MS MSD 92252055001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 512 478 102 96 75-125 7 25 Arsenic ug/L ND 500 500 494 459 99 92 75-125 7 25 Barium ug/L 32.1J 500 500 518 485 97 91 75-125 7 25 Beryllium ug/L ND 500 500 492 457 98 91 75-125 7 25 Cadmium ug/L ND 500 500 490 456 98 91 75-125 7 25 Chromium ug/L ND 500 500 488 449 97 90 75-125 8 25 Cobalt ug/L 12.6 500 500 501 463 98 90 75-125 8 25 Copper ug/L ND 500 500 482 446 96 89 75-125 8 25 Lead ug/L ND 500 500 484 447 97 89 75-125 8 25 Nickel ug/L ND 500 500 490 452 98 90 75-125 8 25 Selenium ug/L ND 500 500 466 434 93 86 75-125 7 25 Silver ug/L ND 250 250 244 226 97 91 75-125 7 25 Thallium ug/L ND 500 500 493 458 99 92 75-125 7 25 Vanadium ug/L ND 500 500 482 442 96 88 75-125 9 25 Zinc ug/L 6.3J 500 500 496 457 98 90 75-125 8 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 07:48 PM without the written consent of Pace Analytical Services, Inc.. Page 18 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 QC Batch: MPRP/18597 Analysis Method: EPA6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET Filtered Diss. Associated Lab Samples: 92252055001, 92252055002, 92252055003, 92252055004, 92252055007 METHOD BLANK: 1473333 Matrix: Water Associated Lab Samples: 92252055001, 92252055002, 92252055003, 92252055004, 92252055007 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Iron, Dissolved ug/L ND 50.0 06/04/15 20:36 LABORATORY CONTROL SAMPLE: 1473334 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Iron, Dissolved ug/L 5000 4650 93 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1473335 1473336 MS MSD 92252055001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Iron, Dissolved ug/L 101 5000 5000 4640 4840 91 95 75-125 4 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 07:48 PM without the written consent of Pace Analytical Services, Inc.. Page 19 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 QC Batch: MSV/32002 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92252055001, 92252055006, 92252055009 METHOD BLANK: 1475797 Matrix: Associated Lab Samples: 92252055001, 92252055006, 92252055009 Blank Parameter Units Result Water Reporting Limit Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/04/15 16:39 1,1,1-Trichloroethane ug/L ND 1.0 06/04/15 16:39 1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/04/15 16:39 1,1,2-Trichloroethane ug/L ND 1.0 06/04/15 16:39 1,1-Dichloroethane ug/L ND 5.0 06/04/15 16:39 1,1-Dichloroethene ug/L ND 5.0 06/04/15 16:39 1,2,3-Trichloropropane ug/L ND 1.0 06/04/15 16:39 1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/04/15 16:39 1,2-Dibromoethane (EDB) ug/L ND 1.0 06/04/15 16:39 1,2-Dichlorobenzene ug/L ND 5.0 06/04/15 16:39 1,2-Dichloroethane ug/L ND 1.0 06/04/15 16:39 1,2-Dichloropropane ug/L ND 1.0 06/04/15 16:39 1,3-Dichloropropane ug/L ND 1.0 06/04/15 16:39 1,4-Dichlorobenzene ug/L ND 1.0 06/04/15 16:39 2-Butanone (MEK) ug/L ND 100 06/04/15 16:39 2-Hexanone ug/L ND 50.0 06/04/15 16:39 4-Methyl-2-pentanone (MIBK) ug/L ND 100 06/04/15 16:39 Acetone ug/L ND 100 06/04/15 16:39 Acrylonitrile ug/L ND 200 06/04/15 16:39 Benzene ug/L ND 1.0 06/04/15 16:39 Bromochloromethane ug/L ND 3.0 06/04/15 16:39 Bromodichloromethane ug/L ND 1.0 06/04/15 16:39 Bromoform ug/L ND 3.0 06/04/15 16:39 Bromomethane ug/L ND 10.0 06/04/15 16:39 Carbon disulfide ug/L ND 100 06/04/15 16:39 Carbon tetrachloride ug/L ND 1.0 06/04/15 16:39 Chlorobenzene ug/L ND 3.0 06/04/15 16:39 Chloroethane ug/L ND 10.0 06/04/15 16:39 Chloroform ug/L ND 5.0 06/04/15 16:39 Chloromethane ug/L ND 1.0 06/04/15 16:39 cis-1,2-Dichloroethene ug/L ND 5.0 06/04/15 16:39 cis-1,3-Dichloropropene ug/L ND 1.0 06/04/15 16:39 Dibromochloromethane ug/L ND 3.0 06/04/15 16:39 Dibromomethane ug/L ND 10.0 06/04/15 16:39 Ethylbenzene ug/L ND 1.0 06/04/15 16:39 lodomethane ug/L ND 10.0 06/04/15 16:39 Methylene Chloride ug/L ND 1.0 06/04/15 16:39 Styrene ug/L ND 1.0 06/04/15 16:39 Tetrachloroethene ug/L ND 1.0 06/04/15 16:39 Toluene ug/L ND 1.0 06/04/15 16:39 trans-1,2-Dichloroethene ug/L ND 5.0 06/04/15 16:39 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 07:48 PM without the written consent of Pace Analytical Services, Inc.. Page 20 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 METHOD BLANK: 1475797 Matrix: Associated Lab Samples: 92252055001, 92252055006, 92252055009 Blank Parameter Units Result Water Reporting Limit Analyzed Qualifiers trans- 1,3-Dichloropropene ug/L ND 1.0 06/04/15 16:39 trans-1,4-Dichloro-2-butene ug/L ND 100 06/04/15 16:39 Trichloroethene ug/L ND 1.0 06/04/15 16:39 Trichlorofluoromethane ug/L ND 1.0 06/04/15 16:39 Vinyl acetate ug/L ND 50.0 06/04/15 16:39 Vinyl chloride ug/L ND 1.0 06/04/15 16:39 Xylene (Total) ug/L ND 5.0 06/04/15 16:39 1,2-Dichloroethane-d4 (S) % 98 70-130 06/04/15 16:39 4-Bromofluorobenzene (S) % 99 70-130 06/04/15 16:39 Toluene-d8 (S) % 100 70-130 06/04/15 16:39 LABORATORY CONTROL SAMPLE: Parameter 1475798 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 51.6 103 80-125 1,1,1-Trichloroethane ug/L 50 47.9 96 71-129 1,1,2,2-Tetrachloroethane ug/L 50 51.8 104 79-124 1,1,2-Trichloroethane ug/L 50 50.1 100 85-125 1,1-Dichloroethane ug/L 50 48.4 97 73-126 1,1-Dichloroethene ug/L 50 48.3 97 66-135 1,2,3-Trichloropropane ug/L 50 53.1 106 75-130 1,2-Dibromo-3-chloropropane ug/L 50 49.4 99 71-133 1,2-Dibromoethane (EDB) ug/L 50 53.4 107 83-124 1,2-Dichlorobenzene ug/L 50 57.7 115 80-133 1,2-Dichloroethane ug/L 50 48.6 97 67-128 1,2-Dichloropropane ug/L 50 49.8 100 75-132 1,3-Dichloropropane ug/L 50 54.0 108 76-131 1,4-Dichlorobenzene ug/L 50 55.6 111 78-130 2-Butanone (MEK) ug/L 100 99.91 100 61-144 2-Hexanone ug/L 100 109 109 68-143 4-Methyl-2-pentanone (MIBK) ug/L 100 99AJ 99 72-135 Acetone ug/L 100 105 105 48-146 Acrylonitrile ug/L 250 241 96 40-160 Benzene ug/L 50 51.0 102 80-125 Bromochloromethane ug/L 50 50.0 100 71-125 Bromodichloromethane ug/L 50 43.7 87 78-124 Bromoform ug/L 50 33.9 68 71-128 LO Bromomethane ug/L 50 62.3 125 40-160 Carbon disulfide ug/L 50 41.7J 83 50-160 Carbon tetrachloride ug/L 50 47.1 94 69-131 Chlorobenzene ug/L 50 54.0 108 81-122 Chloroethane ug/L 50 46.2 92 39-148 Chloroform ug/L 50 45.3 91 73-127 Chloromethane ug/L 50 50.7 101 44-146 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 07:48 PM without the written consent of Pace Analytical Services, Inc.. Page 21 of 35 Pace Analytical Services, Inc. aceAnalXical� 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 LABORATORY CONTROL SAMPLE: Parameter 1475798 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers cis-1,2-Dichloroethene ug/L 50 50.5 101 74-124 cis-1,3-Dichloropropene ug/L 50 49.7 99 72-132 Dibromochloromethane ug/L 50 42.8 86 78-125 Dibromomethane ug/L 50 50.3 101 82-120 Ethylbenzene ug/L 50 53.3 107 79-121 lodomethane ug/L 100 113 113 39-154 Methylene Chloride ug/L 50 55.0 110 64-133 Styrene ug/L 50 57.1 114 84-126 Tetrachloroethene ug/L 50 55.0 110 78-122 Toluene ug/L 50 49.9 100 80-121 trans-1,2-Dichloroethene ug/L 50 49.0 98 71-127 trans- 1,3-Dichloropropene ug/L 50 50.9 102 69-141 trans-1,4-Dichloro-2-butene ug/L 50 41.OJ 82 40-160 Trichloroethene ug/L 50 48.6 97 78-122 Trichlorofluoromethane ug/L 50 50.1 100 53-137 Vinyl acetate ug/L 100 106 106 40-160 Vinyl chloride ug/L 50 54.5 109 58-137 Xylene (Total) ug/L 150 161 107 81-126 1,2-Dichloroethane-d4 (S) % 96 70-130 4-Bromofluorobenzene (S) % 102 70-130 Toluene-d8 (S) % 100 70-130 MATRIX SPIKE SAMPLE: Parameter 1475800 Units 92252070006 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 15.2 76 70-130 1,1,1-Trichloroethane ug/L ND 20 17.7 88 70-130 1,1,2,2-Tetrachloroethane ug/L ND 20 16.6 83 70-130 1,1,2-Trichloroethane ug/L ND 20 17.4 87 70-130 1,1-Dichloroethane ug/L ND 20 18.5 92 70-130 1,1-Dichloroethene ug/L ND 20 19.3 97 70-166 1,2,3-Trichloropropane ug/L ND 20 16.8 84 70-130 1,2-Dibromo-3-chloropropane ug/L ND 20 15.0 75 70-130 1,2-Dibromoethane (EDB) ug/L ND 20 17.1 85 70-130 1,2-Dichlorobenzene ug/L ND 20 18.5 92 70-130 1,2-Dichloroethane ug/L ND 20 17.8 89 70-130 1,2-Dichloropropane ug/L ND 20 18.1 90 70-130 1,3-Dichloropropane ug/L ND 20 17.5 88 70-130 1,4-Dichlorobenzene ug/L ND 20 17.4 87 70-130 2-Butanone (MEK) ug/L ND 40 37.9J 95 70-130 2-Hexanone ug/L ND 40 35.9J 90 70-130 4-Methyl-2-pentanone (MIBK) ug/L ND 40 35.5J 89 70-130 Acetone ug/L ND 40 37.OJ 89 70-130 Acrylonitrile ug/L ND 100 85.7J 86 70-130 Benzene ug/L ND 20 18.7 94 70-148 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 07:48 PM without the written consent of Pace Analytical Services, Inc.. Page 22 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 MATRIX SPIKE SAMPLE: 1475800 92252070006 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Bromochloromethane ug/L ND 20 18.9 95 70-130 Bromodichloromethane ug/L ND 20 14.0 70 70-130 Bromoform ug/L ND 20 11.8 59 70-130 MO Bromomethane ug/L ND 20 18.8 94 70-130 Carbon disulfide ug/L ND 20 15.6J 78 70-130 Carbon tetrachloride ug/L ND 20 15.6 78 70-130 Chlorobenzene ug/L ND 20 18.6 93 70-146 Chloroethane ug/L ND 20 19.7 98 70-130 Chloroform ug/L ND 20 16.3 81 70-130 Chloromethane ug/L ND 20 21.8 109 70-130 cis-1,2-Dichloroethene ug/L ND 20 18.9 95 70-130 cis-1,3-Dichloropropene ug/L ND 20 15.9 79 70-130 Dibromochloromethane ug/L ND 20 11.5 58 70-130 M1 Dibromomethane ug/L ND 20 17.4 87 70-130 Ethylbenzene ug/L ND 20 18.2 91 70-130 lodomethane ug/L ND 40 41.3 103 70-130 Methylene Chloride ug/L ND 20 19.8 99 70-130 Styrene ug/L ND 20 18.8 94 70-130 Tetrachloroethene ug/L ND 20 18.5 92 70-130 Toluene ug/L ND 20 18.0 90 70-155 trans-1,2-Dichloroethene ug/L ND 20 19.1 96 70-130 trans- 1,3-Dichloropropene ug/L ND 20 15.4 77 70-130 trans-1,4-Dichloro-2-butene ug/L ND 20 14.2J 71 70-130 Trichloroethene ug/L ND 20 18.4 92 69-151 Trichlorofluoromethane ug/L ND 20 19.5 97 70-130 Vinyl acetate ug/L ND 40 33.2J 83 70-130 Vinyl chloride ug/L ND 20 19.7 98 70-130 1,2-Dichloroethane-d4 (S) % 101 70-130 4-Bromofluorobenzene (S) % 98 70-130 Toluene-d8 (S) % 99 70-130 SAMPLE DUPLICATE: 1475799 92252070005 Dup Max Parameter Units Result Result RPD RPD Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND ND 30 1,1,1-Trichloroethane ug/L ND ND 30 1,1,2,2-Tetrachloroethane ug/L ND ND 30 1,1,2-Trichloroethane ug/L ND ND 30 1,1-Dichloroethane ug/L 0.46J 0.46J 30 1,1-Dichloroethene ug/L ND ND 30 1,2,3-Trichloropropane ug/L ND ND 30 1,2-Dibromo-3-chloropropane ug/L ND ND 30 1,2-Dibromoethane (EDB) ug/L ND ND 30 1,2-Dichlorobenzene ug/L ND ND 30 1,2-Dichloroethane ug/L 0.14J 0.13J 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 07:48 PM without the written consent of Pace Analytical Services, Inc.. Page 23 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 SAMPLE DUPLICATE: 1475799 Parameter Units 92252070005 Result Dup Result 1,2-Dichloropropane ug/L ND ND 1,3-Dichloropropane ug/L ND ND 1,4-Dichlorobenzene ug/L 0.42J 0.44J 2-Butanone (MEK) ug/L ND ND 2-Hexanone ug/L ND ND 4-Methyl-2-pentanone (MIBK) ug/L ND ND Acetone ug/L ND ND Acrylonitrile ug/L ND ND Benzene ug/L ND ND Bromochloromethane ug/L ND ND Bromodichloromethane ug/L ND ND Bromoform ug/L ND ND Bromomethane ug/L ND ND Carbon disulfide ug/L ND ND Carbon tetrachloride ug/L ND ND Chlorobenzene ug/L ND ND Chloroethane ug/L ND ND Chloroform ug/L ND ND Chloromethane ug/L ND ND cis-1,2-Dichloroethene ug/L 0.74J 0.72J cis-1,3-Dichloropropene ug/L ND ND Dibromochloromethane ug/L ND ND Dibromomethane ug/L ND ND Ethylbenzene ug/L ND ND lodomethane ug/L ND ND Methylene Chloride ug/L ND ND Styrene ug/L ND ND Tetrachloroethene ug/L ND ND Toluene ug/L ND ND trans-1,2-Dichloroethene ug/L ND ND trans- 1,3-Dichloropropene ug/L ND ND trans-1,4-Dichloro-2-butene ug/L ND ND Trichloroethene ug/L ND ND Trichlorofluoromethane ug/L ND ND Vinyl acetate ug/L ND ND Vinyl chloride ug/L ND ND Xylene (Total) ug/L ND ND 1,2-Dichloroethane-d4 (S) % 104 104 4-Bromofluorobenzene (S) % 97 97 Toluene-d8(S) % 102 102 Max RPD RPD Qualifiers 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 07:48 PM without the written consent of Pace Analytical Services, Inc.. Page 24 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 QC Batch: WET/37973 Analysis Method: SM 2320B QC Batch Method: SM 2320B Analysis Description: 2320E Alkalinity Associated Lab Samples: 92252055001 METHOD BLANK: 1479236 Matrix: Water Associated Lab Samples: 92252055001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Alkalinity, Total as CaCO3 ug/L ND 5000 06/09/15 19:18 LABORATORY CONTROL SAMPLE: 1479237 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 47600 95 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1479238 1479239 MS MSD 92253094001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 27.5 mg/L 50000 50000 76500 77700 98 101 90-110 2 4 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1479240 1479241 MS MSD 92252070011 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 8200 50000 50000 500000 509000 983 1001 90-110 2 4 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 07:48 PM without the written consent of Pace Analytical Services, Inc.. Page 25 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 QC Batch: WET/37807 Analysis Method: SM 4500-S2D QC Batch Method: SM 4500-S2D Analysis Description: 4500S2D Sulfide Water Associated Lab Samples: 92252055001, 92252055002, 92252055003, 92252055005 METHOD BLANK: 1472297 Matrix: Water Associated Lab Samples: 92252055001, 92252055002, 92252055003, 92252055005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfide ug/L ND 1000 06/02/1516:10 LABORATORY CONTROL SAMPLE: 1472298 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 526J 105 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1472299 1472300 MS MSD 92251903001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 523J 523J 105 105 90-110 0 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1472301 1472302 MS MSD 92251926005 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 511J 511J 102 102 90-110 0 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 07:48 PM without the written consent of Pace Analytical Services, Inc.. Page 26 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 QC Batch: WET/37808 Analysis Method: SM 4500-S2D QC Batch Method: SM 4500-S2D Analysis Description: 4500S2D Sulfide Water Associated Lab Samples: 92252055004, 92252055007, 92252055008 METHOD BLANK: 1472306 Matrix: Water Associated Lab Samples: 92252055004, 92252055007, 92252055008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfide ug/L ND 1000 06/02/1516:30 LABORATORY CONTROL SAMPLE: 1472307 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 522J 104 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1472308 1472309 MS MSD 92252055004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 549J 549J 110 110 90-110 0 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 07:48 PM without the written consent of Pace Analytical Services, Inc.. Page 27 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 QC Batch: WETA/23162 Analysis Method: EPA 300.0 QC Batch Method: EPA 300.0 Analysis Description: 300.0 IC Anions Associated Lab Samples: 92252055001 METHOD BLANK: 1475158 Matrix: Water Associated Lab Samples: 92252055001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfate ug/L ND 250000 06/05/1519:41 LABORATORY CONTROL SAMPLE: 1475159 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate ug/L 20000 20000J 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1475160 1475161 MS MSD 92252271001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L ND 20000 20000 20300J 20300J 102 102 90-110 0 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1475162 1475163 MS MSD 92252055001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 12000J 20000 20000 33100J 33200J 106 106 90-110 0 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 07:48 PM without the written consent of Pace Analytical Services, Inc.. Page 28 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 QC Batch: WETA/23157 Analysis Method: SM 4500-CI-E QC Batch Method: SM 4500-CI-E Analysis Description: 4500 Chloride Associated Lab Samples: 92252055001 METHOD BLANK: 1474756 Matrix: Water Associated Lab Samples: 92252055001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride ug/L ND 1000 06/06/15 06:48 LABORATORY CONTROL SAMPLE: 1474757 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride ug/L 20000 19800 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1474758 1474759 MS MSD 92252474003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 5.0 mg/L 20000 20000 23900 23700 95 93 90-110 1 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1474760 1474761 MS MSD 92252070005 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 42600 20000 20000 61400 64900 94 111 90-110 6 10 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 07:48 PM without the written consent of Pace Analytical Services, Inc.. Page 29 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 QC Batch: WETA/23115 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92252055001 METHOD BLANK: 1471738 Matrix: Water Associated Lab Samples: 92252055001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand ug/L ND 25000 06/02/15 09:50 LABORATORY CONTROL SAMPLE: 1471739 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand ug/L 750000 785000 105 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1471740 1471741 MS MSD 92251288003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chemical Oxygen Demand ug/L ND 750000 750000 778000 778000 103 103 90-110 0 3 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1471742 1471743 MS MSD 92251814001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chemical Oxygen Demand ug/L ND 750000 750000 756000 756000 101 101 90-110 0 3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 07:48 PM without the written consent of Pace Analytical Services, Inc.. Page 30 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 QC Batch: WETA/23178 Analysis Method: SM 5310B QC Batch Method: SM 5310B Analysis Description: 5310E TOC Associated Lab Samples: 92252055001 METHOD BLANK: 1476913 Matrix: Water Associated Lab Samples: 92252055001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon ug/L ND 1000 06/05/15 19:36 LABORATORY CONTROL SAMPLE: 1476914 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carbon ug/L 25000 24000 96 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1476915 1476916 MS MSD 92252673001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Total Organic Carbon ug/L 1.8 mg/L 25000 25000 26500 26500 99 99 90-110 0 5 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1476917 1476918 MS MSD 92251906009 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Total Organic Carbon ug/L 2.0 mg/L 25000 25000 26600 26600 98 98 90-110 0 5 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 07:48 PM without the written consent of Pace Analytical Services, Inc.. Page 31 of 35 Pace Analytical Services, Inc. aceAnalXical� 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 www.pacelabs.com (704)875-9092 QUALIFIERS Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits. L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated samples may be biased low. MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2015 07:48 PM without the written consent of Pace Analytical Services, Inc.. Page 32 of 35 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Surry Closed -Mt Airy (AM) Pace Project No.: 92252055 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92252055001 MW-11 EPA 3010 MPRP/18587 EPA6010 92252055006 MW-6 EPA 3010 MPRP/18587 EPA6010 92252055009 SCALEHOUSE EPA 3010 MPRP/18587 EPA6010 92252055001 MW-11 EPA 3010 MPRP/18597 EPA6010 92252055002 MW-14 EPA 3010 MPRP/18597 EPA6010 92252055003 MW-15 EPA 3010 MPRP/18597 EPA6010 92252055004 MW-1 EPA 3010 MPRP/18597 EPA6010 92252055007 MW-7 EPA 3010 MPRP/18597 EPA6010 92252055001 MW-11 EPA 8260 MSV/32002 92252055006 MW-6 EPA 8260 MSV/32002 92252055009 SCALEHOUSE EPA 8260 MSV/32002 92252055001 MW-11 SM 2320B WET/37973 92252055001 MW-11 SM 4500-S2D WET/37807 92252055002 MW-14 SM 4500-S2D WET/37807 92252055003 MW-15 SM 4500-S2D WET/37807 92252055004 MW-1 SM 4500-S2D WET/37808 92252055005 MW-21 SM 4500-S2D WET/37807 92252055007 MW-7 SM 4500-S2D WET/37808 92252055008 MW-9 SM 4500-S2D WET/37808 92252055001 MW-11 EPA 300.0 WETA/23162 92252055001 MW-11 SM 4500-CI-E WETA/23157 92252055001 MW-11 SM 5220D WETA/23115 92252055001 MW-11 SM 5310B WETA/23178 Date: 06/12/2015 07:48 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Analytical Batch ICP/16673 ICP/16673 ICP/16673 ICP/16681 ICP/16681 ICP/16681 ICP/16681 ICP/16681 Page 33 of 35 j A qacuoAnalylioal I condition Upon Recei, Document Number: F-CHR-CS-003-rev.16 Client Name: w Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Cllent❑Commercial❑ j Co L� df_ce Other Custody Seal on CoolerlBOX Present: ❑ yes no Seals intact: ❑ yes ❑ no Rpgmvlzi Packing Material: ❑ Bubble V❑p ❑ ggubbl�ads ❑ None ❑ Other C. . Thermometer Used: IR Gun T1401 f Type of Ice: (W�t Blue None ❑.Samples on ice, cooling process has begun Pa e 1 of 2* Issuing Authority: Pace Huntersville Qualitv Office " Page 2 of 2 is for internal Use Only temp Correction Factor T1401r No Correction corrected Cooler Temp.: ' :1 °C biological Tissue is Froaen: Yes No //=contents:aj l! Qf pe s n exa Ining �f t - ,) ` � , tempshould be above freezing to 6°C Comments; '_hain'of-Custody Present: Ye�❑No ❑NIA 1, lhain of Custody Filled Out: Dyes No ❑NIA 2, chain of Custody Relinquished: - Ye No ❑NIA 3. Sampler Name & Signature on COC: 13 e ❑No ❑NIA 4. samples Arrived within Hold Time: ' Yes ❑N NIA 5. Short Hold Time Analysis (<72hr): ❑Yes ❑NIA 6. Rush Turn Around Time Requested: ❑Yes KI I' -❑NIA 7. Sufficient Volume: ❑Y No 1-1N1A $ ' Ar' ` AO A4 til iUr) h{:S.SU+1ft aq _n lorrect Containers Used: ❑No ©NIA Containers Used: ©-Pace zesdNo ❑NIA containers Intact: ❑No ❑NIA 10, =iltered volume received for Dissolved tests Yes ❑N ONIA 1 t, Sample Labels match COC: ❑Yes No ❑IVA ++ 4 l 12. 06 1. At o; [t�vLti -Includes dateltime/ID/Analysis Matrix: \V�� %II containers needing preservation have been checked. , Yes ❑No ON1A 13. 11l containers needing preservation are found to be in []Yes 13N' ❑NIA :ompliance with EPA recommendation. .xcepSions: VOA, coliromi, TOC, O&G, Vvl-DRO (water) // ©�r ❑No samples checked for dechlorination: Yes ON ❑NIA 14. -leadspace in VOA Vials(>6mm): ❑Yes dNo ON 15. rrip Blank Present: []Yes ❑No 16, rrip Blank Custody Seals Present ❑Yes ❑No NIA 'ace-Trip..BlankLot #-(if-purchased):------- — -- -. --- --- - --- - -- ;lient Notification/ Resolution: Field Data Required? Y 1 N Person Contacted: ��,rzc, 6C61, Daterrime: -�•12-? r Comments/ Resolution: _ f�� `72 "�- r �,-�. �=s•� , p.ss o jwd `� i!�. �1 SCURF Review: Date: 1 SRF Review: IDate: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le out of hold, incorrect preservative, out of temp, incorrect containers) W0:9225205 11111111111111111111111 92252055 11` Page 34 of 35 CHAIN -OF -CUSTODY 1 Analytical Request Document ac°Analyficaf The Chain -of -Custody is a LEGAL DOCUMENT, All relevant fields must be completed accurately. section A Section B Section C Required Client information: Required Project Information: Invoice Information: Pa e : 1 Of 1 Company: Municipai Engineering Services Report To: Jonathan i'fohl Attention: Address: 68 Shipwash Drive Copy To: Company Name: Gamer, NO 27629 Address: Regulatory A en Email: Purchase Order #, Pace Quote: EEq Phone: Fax Proi Name: Sury Closed -Mt Airy (AM) Pace Project Manager: kevin.godwin pacelabs-com, State 1 location Requested Due Dale: Project #: Pace Profile #: Requested Analysis Pilterod !N Z aATRcx cone o COLLECTED z Preservatives Orinking Wotor DW b .- water WT 3 m m LL Waste Waver wW Product P SAMPLE ID Saivsoid 5i� v ~ CD Z Oil oy o c? S7gRT END S One Character per box. W.P. wP w (A-Zr 0-91, •) Aa AR o 0. F m w 21 o o ¢ J /- [ Sample Ids must be unique a:era Tss x z ,~„ a w a p u Z m a p = p i o m C b v ro /� r�)'�� 7 2 l -(( H 4 a co O 0 O N 'c Q 4 4 U p o N 'o m w DATE TIME 6ATE TIME w # z z o a ¢ c� rii a= 1 MW-11 W7 "*Is Sv X X X X X X X O 2 MW-14 W7 ]'f9t 1i� X X 7i 3 MVV-15 WT ;tLSi'5 i $ X X Qi J 4 Mw-t WT S1)21[S I a'•IS x x oG 5 1 MW-21 Wr �J �ilalfts •�'K IX X X � 6 MW-6 WT zloiiii 7Il.5 X x 7 MW-7 Wr s dgfn `# • 10 X X o d% a MW-9 WT 5�aihs 's t; X X c/ 0 6 9 Scalehouse WT X X U� 10 11 12 ADDITIONAL COMMENTS LINQIIISHED BY I AFFILIATION DATE TIME ACCEPTED BY I AFF[L1ATlON DATE TIME SAMPLECONDITIONS SAMPLER NAME AND SIGNATURE _ c 0 m a PRINT Name of SAMPLER: ` � � I- z 1 a m$ Z U } w Z rn = } SIGNATURE of SAMPLER: ' DATE Signed: IT1a311 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 June 11, 2015 Mr. Jonathan Pfohl Municipal Engineering Services PO Box 97 Garner, NC 27529 RE: Project: SURRY CLOSED MT AIRY (AM) Pace Project No.: 92252473 Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory on June 02, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Godwin kevin.godwin@pacelabs.com Project Manager Enclosures Q _Kok r REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 11 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 Project: SURRY CLOSED MT AIRY (AM) Pace Project No.: 92252473 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 11 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 SAMPLE SUMMARY Project: SURRY CLOSED MT AIRY (AM) Pace Project No.: 92252473 Lab ID Sample ID Matrix Date Collected Date Received 92252473001 92252473002 MW-9 MW-21 Water Water 05/28/1516:15 05/28/1514:35 06/02/1516:30 06/02/1516:30 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 11 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: SURRY CLOSED MT AIRY (AM) Pace Project No.: 92252473 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92252473001 MW-9 EPA 6010 JMW 1 PASI-A 92252473002 MW-21 EPA 6010 JMW 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 11 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED MT AIRY (AM) Pace Project No.: 92252473 Sample: MW-9 Lab ID: 92252473001 Collected: 05/28/15 16:15 Received: 06/02/15 16:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP, Dissolved Analytical Method: EPA 6010 Preparation Method: EPA 3010 Iron, Dissolved ND ug/L 50.0 25.0 1 06/09/15 17:42 06/10/15 22:03 7439-89-6 Date: 06/11/2015 02:06 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 11 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED MT AIRY (AM) Pace Project No.: 92252473 Sample: MW-21 Lab ID: 92252473002 Collected: 05/28/15 14:35 Received: 06/02/15 16:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP, Dissolved Analytical Method: EPA 6010 Preparation Method: EPA 3010 Iron, Dissolved ND ug/L 50.0 25.0 1 06/09/15 17:42 06/10/15 22:06 7439-89-6 Date: 06/11/2015 02:06 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 11 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED MT AIRY (AM) Pace Project No.: 92252473 QC Batch: MPRP/18653 Analysis Method: EPA6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET Filtered Diss. Associated Lab Samples: 92252473001, 92252473002 METHOD BLANK: 1479142 Matrix: Water Associated Lab Samples: 92252473001, 92252473002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Iron, Dissolved ug/L ND 50.0 06/10/15 21:39 LABORATORY CONTROL SAMPLE: 1479143 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Iron, Dissolved ug/L 5000 4570 91 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1479144 1479145 MS MSD 92252092004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Iron, Dissolved ug/L 832 5000 5000 4980 4830 83 80 75-125 3 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11/2015 02:06 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 11 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALIFIERS Project: SURRY CLOSED MT AIRY (AM) Pace Project No.: 92252473 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11/2015 02:06 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: SURRY CLOSED MT AIRY (AM) Pace Project No.: 92252473 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92252473001 MW-9 EPA 3010 MPRP/18653 EPA 6010 92252473002 MW-21 EPA 3010 MPRP/18653 EPA 6010 Date: 06/11/2015 02:06 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Analytical Batch ICP/16734 ICP/16734 Page 9 of 11 malytfow i w11uiiicrit rvaruc. Condition Upon Recei Document Number: F-CHR-CS-003-rev.16 LJVGurr]CnL rtCvib"'U. 1Vr[7y 10, CUR Page 1 of 2* Issuing Authority: Pace Huntersvilie Qualitv Office Client Name: " Page 2 of 2 is for Internal Use Only Courier: ❑ Fed Ex ❑ UPS[] USPS❑ Client❑ Commercial❑"' Pace Other Custody Seal on Cooler/Box Present: ❑ yes ❑-no Seals intact: ❑ yes ❑ no Packing Material: ❑ Bubble VDP ❑ Bubble Bags [ }' None ❑ Other Thermometer Used: IR Gun T1401 Type of Ice:/W)e Blue None ,{ Sampies on ice, cooling process has begun Temp Correction Factor T1401 No Correction Corrected Cooler Temp.: °C Temp should be above freezing to 6'C Biological Tissue is Frozen: Yes No NIA Date and Initial of {erso "n, contents: Y t Comments: Chain of Custody Present: gYes ❑No ❑NIA 1, Chain of Custody Filled Out: 1)Y�s ONO ❑NIA 2. Chain of Custody Relinquished: ❑Yes 11No ❑NIA 3. Sampler Name & Signature on COC: D7 LINO ❑NIA 4. Samples Arrived within Hold Time: 6Yes ONO ❑NIA g, Short Hold Time Analysis (<72hr): Dyes ©vdo ❑NIA 6. Rush Turn Around Time Requested: ❑Yes ❑ f6 ❑NIA 7. Sufficient Volume: 12 es ❑No ❑N/A 8. Correct Containers Used: -Pace Containers Used: Eyes ONO byes' ❑No ❑NrA ❑NrA g. Containers Intact: (]Yes LINO El N/A 10. Filtered volume received for Dissolved tests Dyes ❑No ❑NIA 11. Sample Labels match COC: -Includes date/time/ID/Analysis Matrix: -Dyes ❑No ❑N1A 12. All containers needing preservation have been checked. All containers needing preservation are found to be in compliance with EPA recommendation. exceptions: VOA, conform, TOC, O&G, VJI-DRO (water) ❑Yes ONO ❑yes ONO Dyes ❑No ' N/A pN1A 13. Samples checked for dechlorination: ❑Yes ONO ❑Nlk 14. Headspace in VOA Vials ( >6mm): Dyes ❑No ❑ 16. Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # (if purchased): Dyes ONO Dyes LINO ❑NIA ❑NIA 16, Client Notification/ Resolution: Field Data Required? Y 1 N Person Contacted: DatelTime: Comments/ Resolution: SCURF Review: /a'> Date: 1 r 5 SRF Review: Date: L 5 Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers) WO#:92252473 H111IIIOIIIIIIOIn Page 10 of 11 aceAr>aljRical CHAIN -OF -CUSTODY 1 Analytical Request Document 0) The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. m d aecuon A Section B Section C Required Client Information: Required Project information: Invoice Information: Pa 8 . 1 Of 1 Company: Municipal Engineering Services Report To: Jonathan Pfohl Attention: Municipal Engineering Services Address: P.O. Box 97 Copy To: Company Name: Garner, NC 27529 Address: Regulatory Agency Email To: jpfohl(oimesco.com Purchase Order No. Pace Quote Reference: Phone: 919-772-5393 Pax: Client Project iD: Surry Closed -Mt. Airy (AM) Pace Project Manager: Kevin Godwin State I Location Requested Due DaterTAT: 10 Day (Default) lContalner Order Number: Pace Profile #: North Carolina Requested Analysis Filtered [YIN) 2 d a COLLECTED Preservatives N N N N Y N N N N MATRIX COPE g 0 un Dking Wter aDW m U Z O Water WT W 3 U ~ tc W.tar WW P SAMPLE ID n m 0Prod= smvwud s� START END ii rn One Character per box. QJ Wife OL r it Q (A,Z, 0.9 f, -) Arc AR a N Sample Ids must be unique other oT w U w m # Tiasuc TS X w z O w M O C 1 to a Q a 4 o T' •/�� ' ' z Q N DATE TIME DATE TIME ¢ z 2 z z O O O o > > x 1 WT G 2 WT G 3 MW9 WT G sazlif U, 'S x l 4 VVT G 5 WT G 6 WT G 7 MW-21 Wr G I,h`i/ 5�ar , o �� x 8 Wr G 9 WT G 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS �' [ ✓ 3� �1 1 �1 v Irk: I n �'� �,�t 1� J �✓ SAMPLER NAME AND SIGNATURE d m PRINT Name of SAMPLER: Jonathan Pfohl U c _-, m y DATE Sined: SIGNATURE of SAMPLER:.; } G a 2 Lu } o E z r ` Ut_'of 0 o 3 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 June 24, 2015 Mr. Jonathan Pfohl Municipal Engineering Services PO Box 97 Garner, NC 27529 RE: Project: SURRY SWs Pace Project No.: 92252037 Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory on May 29, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Godwin kevin.godwin@pacelabs.com Project Manager Enclosures Q _Kok r REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 Project: SURRY SWs Pace Project No.: 92252037 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 SAMPLE SUMMARY Project: SURRY SWs Pace Project No.: 92252037 Lab ID Sample ID Matrix Date Collected Date Received 92252037001 SW-1 Water 05/28/1511:10 05/29/1513:00 92252037002 SW-2 Water 05/28/1515:35 05/29/1513:00 92252037003 SW-3 Water 05/28/15 20:50 05/29/15 13:00 92252037004 SW-4 Water 05/28/1518:10 05/29/1513:00 92252037005 SW -A Water 05/28/1517:35 05/29/1513:00 92252037006 SW-13 Water 05/28/1517:50 05/29/1513:00 92252037007 SWN-1 Water 05/28/1517:20 05/29/1513:00 92252037008 SWN-2 Water 05/28/1516:20 05/29/1513:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: SURRY SWs 92252037 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92252037001 SW-1 EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C 92252037002 SW-2 EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C 92252037003 SW-3 EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C 92252037004 SW-4 EPA 6010 JMW 15 PASI-A 92252037005 SW -A EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C 92252037006 SW-B EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C 92252037007 SWN-1 EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C 92252037008 SWN-2 EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY SWs Pace Project No.: 92252037 Sample: SW-1 Lab ID: 92252037001 Collected: 05/28/15 11:10 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane cis-1,3-Dichloropropene Date: 06/24/2015 09:12 AM Analytical Method: EPA 6010 Preparation Method: EPA 3010 ND ug/L 6.0 3.8 1 06/02/15 23:30 06/04/15 23:16 7440-36-0 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:16 7440-38-2 20.3J ug/L 100 2.5 1 06/02/15 23:30 06/04/15 23:16 7440-39-3 ND ug/L 1.0 0.50 1 06/02/15 23:30 06/04/15 23:16 7440-41-7 ND ug/L 1.0 0.50 1 06/02/15 23:30 06/04/15 23:16 7440-43-9 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:16 7440-47-3 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:16 7440-48-4 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:16 7440-50-8 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:16 7439-92-1 ND ug/L 50.0 2.5 1 06/02/15 23:30 06/04/15 23:16 7440-02-0 ND ug/L 10.0 5.0 1 06/02/15 23:30 06/04/15 23:16 7782-49-2 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:16 7440-22-4 ND ug/L 5.5 5.0 1 06/02/15 23:30 06/04/15 23:16 7440-28-0 ND ug/L 25.0 2.5 1 06/02/15 23:30 06/04/15 23:16 7440-62-2 ND ug/L 10.0 5.0 1 06/02/15 23:30 06/04/15 23:16 7440-66-6 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 06/04/1517:46 67-64-1 ND ug/L 200 1.9 1 06/04/1517:46 107-13-1 ND ug/L 1.0 0.25 1 06/04/1517:46 71-43-2 ND ug/L 3.0 0.17 1 06/04/1517:46 74-97-5 ND ug/L 1.0 0.18 1 06/04/1517:46 75-27-4 ND ug/L 3.0 0.26 1 06/04/1517:46 75-25-2 0.78J ug/L 10.0 0.29 1 06/04/1517:46 74-83-9 ND ug/L 100 0.96 1 06/04/1517:46 78-93-3 ND ug/L 100 1.2 1 06/04/1517:46 75-15-0 ND ug/L 1.0 0.25 1 06/04/1517:46 56-23-5 ND ug/L 3.0 0.23 1 06/04/1517:46 108-90-7 ND ug/L 10.0 0.54 1 06/04/1517:46 75-00-3 ND ug/L 5.0 0.14 1 06/04/1517:46 67-66-3 ND ug/L 1.0 0.11 1 06/04/1517:46 74-87-3 ND ug/L 13.0 2.0 1 06/04/1517:46 96-12-8 ND ug/L 3.0 0.21 1 06/04/1517:46 124-48-1 ND ug/L 1.0 0.27 1 06/04/1517:46 106-93-4 ND ug/L 10.0 0.21 1 06/04/1517:46 74-95-3 ND ug/L 5.0 0.30 1 06/04/1517:46 95-50-1 ND ug/L 1.0 0.33 1 06/04/1517:46 106-46-7 ND ug/L 100 1.0 1 06/04/1517:46 110-57-6 ND ug/L 5.0 0.32 1 06/04/1517:46 75-34-3 ND ug/L 1.0 0.12 1 06/04/1517:46 107-06-2 ND ug/L 5.0 0.56 1 06/04/1517:46 75-35-4 ND ug/L 5.0 0.19 1 06/04/1517:46 156-59-2 ND ug/L 5.0 0.49 1 06/04/1517:46 156-60-5 ND ug/L 1.0 0.27 1 06/04/1517:46 78-87-5 ND ug/L 1.0 0.28 1 06/04/1517:46 142-28-9 ND ug/L 1.0 0.13 1 06/04/1517:46 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. L2 Page 5 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY SWs Pace Project No.: 92252037 Sample: SW-1 Lab ID: 92252037001 Collected: 05/28/15 11:10 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/15 17:46 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/15 17:46 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/04/15 17:46 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/15 17:46 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/15 17:46 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/15 17:46 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/04/15 17:46 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/15 17:46 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/15 17:46 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/15 17:46 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/15 17:46 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/15 17:46 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/15 17:46 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/15 17:46 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/15 17:46 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/15 17:46 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/15 17:46 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/15 17:46 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/15 17:46 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 06/04/15 17:46 460-00-4 1,2-Dichloroethane-d4 (S) 98 % 70-130 1 06/04/15 17:46 17060-07-0 Toluene-d8 (S) 101 % 70-130 1 06/04/15 17:46 2037-26-5 Date: 06/24/2015 09:12 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY SWs Pace Project No.: 92252037 Sample: SW-2 Lab ID: 92252037002 Collected: 05/28/15 15:35 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane cis-1,3-Dichloropropene Date: 06/24/2015 09:12 AM Analytical Method: EPA 6010 Preparation Method: EPA 3010 ND ug/L 6.0 3.8 1 06/02/15 23:30 06/04/15 23:19 7440-36-0 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:19 7440-38-2 15.6J ug/L 100 2.5 1 06/02/15 23:30 06/04/15 23:19 7440-39-3 ND ug/L 1.0 0.50 1 06/02/15 23:30 06/04/15 23:19 7440-41-7 ND ug/L 1.0 0.50 1 06/02/15 23:30 06/04/15 23:19 7440-43-9 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:19 7440-47-3 22.3 ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:19 7440-48-4 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:19 7440-50-8 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:19 7439-92-1 ND ug/L 50.0 2.5 1 06/02/15 23:30 06/04/15 23:19 7440-02-0 ND ug/L 10.0 5.0 1 06/02/15 23:30 06/04/15 23:19 7782-49-2 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:19 7440-22-4 ND ug/L 5.5 5.0 1 06/02/15 23:30 06/04/15 23:19 7440-28-0 ND ug/L 25.0 2.5 1 06/02/15 23:30 06/04/15 23:19 7440-62-2 ND ug/L 10.0 5.0 1 06/02/15 23:30 06/04/15 23:19 7440-66-6 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 06/04/1518:03 67-64-1 ND ug/L 200 1.9 1 06/04/1518:03 107-13-1 ND ug/L 1.0 0.25 1 06/04/1518:03 71-43-2 ND ug/L 3.0 0.17 1 06/04/1518:03 74-97-5 ND ug/L 1.0 0.18 1 06/04/1518:03 75-27-4 ND ug/L 3.0 0.26 1 06/04/1518:03 75-25-2 ND ug/L 10.0 0.29 1 06/04/1518:03 74-83-9 ND ug/L 100 0.96 1 06/04/1518:03 78-93-3 ND ug/L 100 1.2 1 06/04/1518:03 75-15-0 ND ug/L 1.0 0.25 1 06/04/1518:03 56-23-5 ND ug/L 3.0 0.23 1 06/04/1518:03 108-90-7 ND ug/L 10.0 0.54 1 06/04/1518:03 75-00-3 ND ug/L 5.0 0.14 1 06/04/1518:03 67-66-3 ND ug/L 1.0 0.11 1 06/04/1518:03 74-87-3 ND ug/L 13.0 2.0 1 06/04/1518:03 96-12-8 ND ug/L 3.0 0.21 1 06/04/1518:03 124-48-1 ND ug/L 1.0 0.27 1 06/04/1518:03 106-93-4 ND ug/L 10.0 0.21 1 06/04/1518:03 74-95-3 ND ug/L 5.0 0.30 1 06/04/1518:03 95-50-1 ND ug/L 1.0 0.33 1 06/04/1518:03 106-46-7 ND ug/L 100 1.0 1 06/04/1518:03 110-57-6 ND ug/L 5.0 0.32 1 06/04/1518:03 75-34-3 ND ug/L 1.0 0.12 1 06/04/1518:03 107-06-2 ND ug/L 5.0 0.56 1 06/04/1518:03 75-35-4 0.76J ug/L 5.0 0.19 1 06/04/1518:03 156-59-2 ND ug/L 5.0 0.49 1 06/04/1518:03 156-60-5 ND ug/L 1.0 0.27 1 06/04/1518:03 78-87-5 ND ug/L 1.0 0.28 1 06/04/1518:03 142-28-9 ND ug/L 1.0 0.13 1 06/04/1518:03 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. L2 Page 7 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY SWs Pace Project No.: 92252037 Sample: SW-2 Lab ID: 92252037002 Collected: 05/28/15 15:35 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/15 18:03 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/15 18:03 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/04/15 18:03 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/15 18:03 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/15 18:03 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/15 18:03 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/04/15 18:03 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/15 18:03 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/15 18:03 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/15 18:03 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/15 18:03 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/15 18:03 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/15 18:03 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/15 18:03 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/15 18:03 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/15 18:03 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/15 18:03 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/15 18:03 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/15 18:03 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 06/04/15 18:03 460-00-4 1,2-Dichloroethane-d4 (S) 102 % 70-130 1 06/04/15 18:03 17060-07-0 Toluene-d8 (S) 101 % 70-130 1 06/04/15 18:03 2037-26-5 Date: 06/24/2015 09:12 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 8 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY SWs Pace Project No.: 92252037 Sample: SW-3 Lab ID: 92252037003 Collected: 05/28/15 20:50 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane cis-1,3-Dichloropropene Date: 06/24/2015 09:12 AM Analytical Method: EPA 6010 Preparation Method: EPA 3010 ND ug/L 6.0 3.8 1 06/02/15 23:30 06/04/15 23:23 7440-36-0 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:23 7440-38-2 21.OJ ug/L 100 2.5 1 06/02/15 23:30 06/04/15 23:23 7440-39-3 ND ug/L 1.0 0.50 1 06/02/15 23:30 06/04/15 23:23 7440-41-7 ND ug/L 1.0 0.50 1 06/02/15 23:30 06/04/15 23:23 7440-43-9 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:23 7440-47-3 8.81 ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:23 7440-48-4 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:23 7440-50-8 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:23 7439-92-1 ND ug/L 50.0 2.5 1 06/02/15 23:30 06/04/15 23:23 7440-02-0 ND ug/L 10.0 5.0 1 06/02/15 23:30 06/04/15 23:23 7782-49-2 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:23 7440-22-4 ND ug/L 5.5 5.0 1 06/02/15 23:30 06/04/15 23:23 7440-28-0 2.6J ug/L 25.0 2.5 1 06/02/15 23:30 06/04/15 23:23 7440-62-2 ND ug/L 10.0 5.0 1 06/02/15 23:30 06/04/15 23:23 7440-66-6 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 06/04/1518:19 67-64-1 ND ug/L 200 1.9 1 06/04/1518:19 107-13-1 ND ug/L 1.0 0.25 1 06/04/1518:19 71-43-2 ND ug/L 3.0 0.17 1 06/04/1518:19 74-97-5 ND ug/L 1.0 0.18 1 06/04/1518:19 75-27-4 ND ug/L 3.0 0.26 1 06/04/1518:19 75-25-2 0.79J ug/L 10.0 0.29 1 06/04/1518:19 74-83-9 ND ug/L 100 0.96 1 06/04/1518:19 78-93-3 ND ug/L 100 1.2 1 06/04/1518:19 75-15-0 ND ug/L 1.0 0.25 1 06/04/1518:19 56-23-5 ND ug/L 3.0 0.23 1 06/04/1518:19 108-90-7 ND ug/L 10.0 0.54 1 06/04/1518:19 75-00-3 ND ug/L 5.0 0.14 1 06/04/1518:19 67-66-3 ND ug/L 1.0 0.11 1 06/04/1518:19 74-87-3 ND ug/L 13.0 2.0 1 06/04/1518:19 96-12-8 ND ug/L 3.0 0.21 1 06/04/1518:19 124-48-1 ND ug/L 1.0 0.27 1 06/04/1518:19 106-93-4 ND ug/L 10.0 0.21 1 06/04/1518:19 74-95-3 ND ug/L 5.0 0.30 1 06/04/1518:19 95-50-1 ND ug/L 1.0 0.33 1 06/04/1518:19 106-46-7 ND ug/L 100 1.0 1 06/04/1518:19 110-57-6 ND ug/L 5.0 0.32 1 06/04/1518:19 75-34-3 ND ug/L 1.0 0.12 1 06/04/1518:19 107-06-2 ND ug/L 5.0 0.56 1 06/04/1518:19 75-35-4 ND ug/L 5.0 0.19 1 06/04/1518:19 156-59-2 ND ug/L 5.0 0.49 1 06/04/1518:19 156-60-5 ND ug/L 1.0 0.27 1 06/04/1518:19 78-87-5 ND ug/L 1.0 0.28 1 06/04/1518:19 142-28-9 ND ug/L 1.0 0.13 1 06/04/1518:19 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. L2 Page 9 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY SWs Pace Project No.: 92252037 Sample: SW-3 Lab ID: 92252037003 Collected: 05/28/15 20:50 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/15 18:19 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/15 18:19 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/04/15 18:19 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/15 18:19 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/15 18:19 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/15 18:19 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/04/15 18:19 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/15 18:19 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/15 18:19 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/15 18:19 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/15 18:19 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/15 18:19 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/15 18:19 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/15 18:19 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/15 18:19 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/15 18:19 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/15 18:19 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/15 18:19 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/15 18:19 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 06/04/15 18:19 460-00-4 1,2-Dichloroethane-d4 (S) 98 % 70-130 1 06/04/15 18:19 17060-07-0 Toluene-d8 (S) 103 % 70-130 1 06/04/15 18:19 2037-26-5 Date: 06/24/2015 09:12 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY SWs Pace Project No.: 92252037 Sample: SW-4 Lab ID: 92252037004 Collected: 05/28/15 18:10 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 3.8 1 06/02/15 23:30 06/04/15 23:26 7440-36-0 Arsenic ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:26 7440-38-2 Barium 4.4J ug/L 100 2.5 1 06/02/15 23:30 06/04/15 23:26 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 06/02/15 23:30 06/04/15 23:26 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 06/02/15 23:30 06/04/15 23:26 7440-43-9 Chromium ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:26 7440-47-3 Cobalt ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:26 7440-48-4 Copper 13.7 ug/L 10.0 2.5 1 06/02/15 23:30 06/05/15 16:27 7440-50-8 Lead ND ug/L 10.0 2.5 1 06/02/15 23:30 06/05/15 16:27 7439-92-1 Nickel 3.7J ug/L 50.0 2.5 1 06/02/15 23:30 06/04/15 23:26 7440-02-0 Selenium ND ug/L 10.0 5.0 1 06/02/15 23:30 06/04/15 23:26 7782-49-2 Silver ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:26 7440-22-4 Thallium ND ug/L 5.5 5.0 1 06/02/15 23:30 06/04/15 23:26 7440-28-0 Vanadium ND ug/L 25.0 2.5 1 06/02/15 23:30 06/04/15 23:26 7440-62-2 Zinc 118 ug/L 10.0 5.0 1 06/02/15 23:30 06/05/15 16:27 7440-66-6 Date: 06/24/2015 09:12 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 11 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY SWs Pace Project No.: 92252037 Sample: SW -A Lab ID: 92252037005 Collected: 05/28/15 17:35 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane cis-1,3-Dichloropropene Date: 06/24/2015 09:12 AM Analytical Method: EPA 6010 Preparation Method: EPA 3010 ND ug/L 6.0 3.8 1 06/02/15 23:30 06/04/15 23:29 7440-36-0 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:29 7440-38-2 12.9J ug/L 100 2.5 1 06/02/15 23:30 06/04/15 23:29 7440-39-3 ND ug/L 1.0 0.50 1 06/02/15 23:30 06/04/15 23:29 7440-41-7 ND ug/L 1.0 0.50 1 06/02/15 23:30 06/04/15 23:29 7440-43-9 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:29 7440-47-3 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:29 7440-48-4 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:29 7440-50-8 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:29 7439-92-1 ND ug/L 50.0 2.5 1 06/02/15 23:30 06/04/15 23:29 7440-02-0 ND ug/L 10.0 5.0 1 06/02/15 23:30 06/04/15 23:29 7782-49-2 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:29 7440-22-4 ND ug/L 5.5 5.0 1 06/02/15 23:30 06/04/15 23:29 7440-28-0 ND ug/L 25.0 2.5 1 06/02/15 23:30 06/04/15 23:29 7440-62-2 ND ug/L 10.0 5.0 1 06/02/15 23:30 06/04/15 23:29 7440-66-6 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 06/04/1518:36 67-64-1 ND ug/L 200 1.9 1 06/04/1518:36 107-13-1 ND ug/L 1.0 0.25 1 06/04/1518:36 71-43-2 ND ug/L 3.0 0.17 1 06/04/1518:36 74-97-5 ND ug/L 1.0 0.18 1 06/04/1518:36 75-27-4 ND ug/L 3.0 0.26 1 06/04/1518:36 75-25-2 ND ug/L 10.0 0.29 1 06/04/1518:36 74-83-9 ND ug/L 100 0.96 1 06/04/1518:36 78-93-3 ND ug/L 100 1.2 1 06/04/1518:36 75-15-0 ND ug/L 1.0 0.25 1 06/04/1518:36 56-23-5 ND ug/L 3.0 0.23 1 06/04/1518:36 108-90-7 ND ug/L 10.0 0.54 1 06/04/1518:36 75-00-3 ND ug/L 5.0 0.14 1 06/04/1518:36 67-66-3 ND ug/L 1.0 0.11 1 06/04/1518:36 74-87-3 ND ug/L 13.0 2.0 1 06/04/1518:36 96-12-8 ND ug/L 3.0 0.21 1 06/04/1518:36 124-48-1 ND ug/L 1.0 0.27 1 06/04/1518:36 106-93-4 ND ug/L 10.0 0.21 1 06/04/1518:36 74-95-3 ND ug/L 5.0 0.30 1 06/04/1518:36 95-50-1 ND ug/L 1.0 0.33 1 06/04/1518:36 106-46-7 ND ug/L 100 1.0 1 06/04/1518:36 110-57-6 ND ug/L 5.0 0.32 1 06/04/1518:36 75-34-3 ND ug/L 1.0 0.12 1 06/04/1518:36 107-06-2 ND ug/L 5.0 0.56 1 06/04/1518:36 75-35-4 ND ug/L 5.0 0.19 1 06/04/1518:36 156-59-2 ND ug/L 5.0 0.49 1 06/04/1518:36 156-60-5 ND ug/L 1.0 0.27 1 06/04/1518:36 78-87-5 ND ug/L 1.0 0.28 1 06/04/1518:36 142-28-9 ND ug/L 1.0 0.13 1 06/04/1518:36 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. L2 Page 12 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY SWs Pace Project No.: 92252037 Sample: SW -A Lab ID: 92252037005 Collected: 05/28/15 17:35 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/15 18:36 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/15 18:36 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/04/15 18:36 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/15 18:36 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/15 18:36 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/15 18:36 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/04/15 18:36 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/15 18:36 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/15 18:36 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/15 18:36 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/15 18:36 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/15 18:36 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/15 18:36 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/15 18:36 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/15 18:36 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/15 18:36 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/15 18:36 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/15 18:36 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/15 18:36 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 06/04/15 18:36 460-00-4 1,2-Dichloroethane-d4 (S) 101 % 70-130 1 06/04/15 18:36 17060-07-0 Toluene-d8 (S) 101 % 70-130 1 06/04/15 18:36 2037-26-5 Date: 06/24/2015 09:12 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 13 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY SWs Pace Project No.: 92252037 Sample: SW-B Lab ID: 92252037006 Collected: 05/28/15 17:50 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane cis-1,3-Dichloropropene Date: 06/24/2015 09:12 AM Analytical Method: EPA 6010 Preparation Method: EPA 3010 ND ug/L 6.0 3.8 1 06/02/15 23:30 06/04/15 23:32 7440-36-0 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:32 7440-38-2 13.6J ug/L 100 2.5 1 06/02/15 23:30 06/04/15 23:32 7440-39-3 ND ug/L 1.0 0.50 1 06/02/15 23:30 06/04/15 23:32 7440-41-7 ND ug/L 1.0 0.50 1 06/02/15 23:30 06/04/15 23:32 7440-43-9 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:32 7440-47-3 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:32 7440-48-4 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:32 7440-50-8 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:32 7439-92-1 ND ug/L 50.0 2.5 1 06/02/15 23:30 06/04/15 23:32 7440-02-0 ND ug/L 10.0 5.0 1 06/02/15 23:30 06/04/15 23:32 7782-49-2 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:32 7440-22-4 ND ug/L 5.5 5.0 1 06/02/15 23:30 06/04/15 23:32 7440-28-0 ND ug/L 25.0 2.5 1 06/02/15 23:30 06/04/15 23:32 7440-62-2 ND ug/L 10.0 5.0 1 06/02/15 23:30 06/04/15 23:32 7440-66-6 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 06/04/1518:53 67-64-1 ND ug/L 200 1.9 1 06/04/1518:53 107-13-1 ND ug/L 1.0 0.25 1 06/04/1518:53 71-43-2 ND ug/L 3.0 0.17 1 06/04/1518:53 74-97-5 ND ug/L 1.0 0.18 1 06/04/1518:53 75-27-4 ND ug/L 3.0 0.26 1 06/04/1518:53 75-25-2 ND ug/L 10.0 0.29 1 06/04/1518:53 74-83-9 ND ug/L 100 0.96 1 06/04/1518:53 78-93-3 ND ug/L 100 1.2 1 06/04/1518:53 75-15-0 ND ug/L 1.0 0.25 1 06/04/1518:53 56-23-5 ND ug/L 3.0 0.23 1 06/04/1518:53 108-90-7 ND ug/L 10.0 0.54 1 06/04/1518:53 75-00-3 ND ug/L 5.0 0.14 1 06/04/1518:53 67-66-3 ND ug/L 1.0 0.11 1 06/04/1518:53 74-87-3 ND ug/L 13.0 2.0 1 06/04/1518:53 96-12-8 ND ug/L 3.0 0.21 1 06/04/1518:53 124-48-1 ND ug/L 1.0 0.27 1 06/04/1518:53 106-93-4 ND ug/L 10.0 0.21 1 06/04/1518:53 74-95-3 ND ug/L 5.0 0.30 1 06/04/1518:53 95-50-1 ND ug/L 1.0 0.33 1 06/04/1518:53 106-46-7 ND ug/L 100 1.0 1 06/04/1518:53 110-57-6 ND ug/L 5.0 0.32 1 06/04/1518:53 75-34-3 ND ug/L 1.0 0.12 1 06/04/1518:53 107-06-2 ND ug/L 5.0 0.56 1 06/04/1518:53 75-35-4 ND ug/L 5.0 0.19 1 06/04/1518:53 156-59-2 ND ug/L 5.0 0.49 1 06/04/1518:53 156-60-5 ND ug/L 1.0 0.27 1 06/04/1518:53 78-87-5 ND ug/L 1.0 0.28 1 06/04/1518:53 142-28-9 ND ug/L 1.0 0.13 1 06/04/1518:53 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. L2 Page 14 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY SWs Pace Project No.: 92252037 Sample: SW-B Lab ID: 92252037006 Collected: 05/28/15 17:50 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/15 18:53 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/15 18:53 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/04/15 18:53 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/15 18:53 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/15 18:53 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/15 18:53 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/04/15 18:53 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/15 18:53 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/15 18:53 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/15 18:53 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/15 18:53 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/15 18:53 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/15 18:53 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/15 18:53 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/15 18:53 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/15 18:53 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/15 18:53 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/15 18:53 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/15 18:53 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 06/04/15 18:53 460-00-4 1,2-Dichloroethane-d4 (S) 102 % 70-130 1 06/04/15 18:53 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 06/04/15 18:53 2037-26-5 Date: 06/24/2015 09:12 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 15 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY SWs Pace Project No.: 92252037 Sample: SWN-1 Lab ID: 92252037007 Collected: 05/28/15 17:20 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane cis-1,3-Dichloropropene Date: 06/24/2015 09:12 AM Analytical Method: EPA 6010 Preparation Method: EPA 3010 ND ug/L 6.0 3.8 1 06/02/15 23:30 06/04/15 23:44 7440-36-0 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:44 7440-38-2 13.1J ug/L 100 2.5 1 06/02/15 23:30 06/04/15 23:44 7440-39-3 ND ug/L 1.0 0.50 1 06/02/15 23:30 06/04/15 23:44 7440-41-7 ND ug/L 1.0 0.50 1 06/02/15 23:30 06/04/15 23:44 7440-43-9 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:44 7440-47-3 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:44 7440-48-4 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:44 7440-50-8 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:44 7439-92-1 ND ug/L 50.0 2.5 1 06/02/15 23:30 06/04/15 23:44 7440-02-0 ND ug/L 10.0 5.0 1 06/02/15 23:30 06/04/15 23:44 7782-49-2 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:44 7440-22-4 ND ug/L 5.5 5.0 1 06/02/15 23:30 06/04/15 23:44 7440-28-0 ND ug/L 25.0 2.5 1 06/02/15 23:30 06/04/15 23:44 7440-62-2 ND ug/L 10.0 5.0 1 06/02/15 23:30 06/04/15 23:44 7440-66-6 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 06/04/1519:10 67-64-1 ND ug/L 200 1.9 1 06/04/1519:10 107-13-1 ND ug/L 1.0 0.25 1 06/04/1519:10 71-43-2 ND ug/L 3.0 0.17 1 06/04/1519:10 74-97-5 ND ug/L 1.0 0.18 1 06/04/1519:10 75-27-4 ND ug/L 3.0 0.26 1 06/04/1519:10 75-25-2 ND ug/L 10.0 0.29 1 06/04/1519:10 74-83-9 ND ug/L 100 0.96 1 06/04/1519:10 78-93-3 ND ug/L 100 1.2 1 06/04/1519:10 75-15-0 ND ug/L 1.0 0.25 1 06/04/1519:10 56-23-5 ND ug/L 3.0 0.23 1 06/04/1519:10 108-90-7 ND ug/L 10.0 0.54 1 06/04/1519:10 75-00-3 ND ug/L 5.0 0.14 1 06/04/1519:10 67-66-3 ND ug/L 1.0 0.11 1 06/04/1519:10 74-87-3 ND ug/L 13.0 2.0 1 06/04/1519:10 96-12-8 ND ug/L 3.0 0.21 1 06/04/1519:10 124-48-1 ND ug/L 1.0 0.27 1 06/04/1519:10 106-93-4 ND ug/L 10.0 0.21 1 06/04/1519:10 74-95-3 ND ug/L 5.0 0.30 1 06/04/1519:10 95-50-1 ND ug/L 1.0 0.33 1 06/04/1519:10 106-46-7 ND ug/L 100 1.0 1 06/04/1519:10 110-57-6 ND ug/L 5.0 0.32 1 06/04/1519:10 75-34-3 ND ug/L 1.0 0.12 1 06/04/1519:10 107-06-2 ND ug/L 5.0 0.56 1 06/04/1519:10 75-35-4 ND ug/L 5.0 0.19 1 06/04/1519:10 156-59-2 ND ug/L 5.0 0.49 1 06/04/1519:10 156-60-5 ND ug/L 1.0 0.27 1 06/04/1519:10 78-87-5 ND ug/L 1.0 0.28 1 06/04/1519:10 142-28-9 ND ug/L 1.0 0.13 1 06/04/1519:10 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. L2 Page 16 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY SWs Pace Project No.: 92252037 Sample: SWN-1 Lab ID: 92252037007 Collected: 05/28/15 17:20 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/15 19:10 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/15 19:10 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/04/15 19:10 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/15 19:10 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/15 19:10 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/15 19:10 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/04/15 19:10 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/15 19:10 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/15 19:10 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/15 19:10 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/15 19:10 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/15 19:10 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/15 19:10 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/15 19:10 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/15 19:10 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/15 19:10 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/15 19:10 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/15 19:10 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/15 19:10 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 06/04/15 19:10 460-00-4 1,2-Dichloroethane-d4 (S) 101 % 70-130 1 06/04/15 19:10 17060-07-0 Toluene-d8 (S) 101 % 70-130 1 06/04/15 19:10 2037-26-5 Date: 06/24/2015 09:12 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 17 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY SWs Pace Project No.: 92252037 Sample: SWN-2 Lab ID: 92252037008 Collected: 05/28/15 16:20 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane cis-1,3-Dichloropropene Date: 06/24/2015 09:12 AM Analytical Method: EPA 6010 Preparation Method: EPA 3010 ND ug/L 6.0 3.8 1 06/02/15 23:30 06/04/15 23:47 7440-36-0 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:47 7440-38-2 12.7J ug/L 100 2.5 1 06/02/15 23:30 06/04/15 23:47 7440-39-3 ND ug/L 1.0 0.50 1 06/02/15 23:30 06/04/15 23:47 7440-41-7 ND ug/L 1.0 0.50 1 06/02/15 23:30 06/04/15 23:47 7440-43-9 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:47 7440-47-3 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:47 7440-48-4 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:47 7440-50-8 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:47 7439-92-1 ND ug/L 50.0 2.5 1 06/02/15 23:30 06/04/15 23:47 7440-02-0 ND ug/L 10.0 5.0 1 06/02/15 23:30 06/04/15 23:47 7782-49-2 ND ug/L 10.0 2.5 1 06/02/15 23:30 06/04/15 23:47 7440-22-4 ND ug/L 5.5 5.0 1 06/02/15 23:30 06/04/15 23:47 7440-28-0 ND ug/L 25.0 2.5 1 06/02/15 23:30 06/04/15 23:47 7440-62-2 ND ug/L 10.0 5.0 1 06/02/15 23:30 06/04/15 23:47 7440-66-6 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 06/04/1519:27 67-64-1 ND ug/L 200 1.9 1 06/04/1519:27 107-13-1 ND ug/L 1.0 0.25 1 06/04/1519:27 71-43-2 ND ug/L 3.0 0.17 1 06/04/1519:27 74-97-5 ND ug/L 1.0 0.18 1 06/04/1519:27 75-27-4 ND ug/L 3.0 0.26 1 06/04/1519:27 75-25-2 ND ug/L 10.0 0.29 1 06/04/1519:27 74-83-9 ND ug/L 100 0.96 1 06/04/1519:27 78-93-3 ND ug/L 100 1.2 1 06/04/1519:27 75-15-0 ND ug/L 1.0 0.25 1 06/04/1519:27 56-23-5 ND ug/L 3.0 0.23 1 06/04/1519:27 108-90-7 ND ug/L 10.0 0.54 1 06/04/1519:27 75-00-3 ND ug/L 5.0 0.14 1 06/04/1519:27 67-66-3 ND ug/L 1.0 0.11 1 06/04/1519:27 74-87-3 ND ug/L 13.0 2.0 1 06/04/1519:27 96-12-8 ND ug/L 3.0 0.21 1 06/04/1519:27 124-48-1 ND ug/L 1.0 0.27 1 06/04/1519:27 106-93-4 ND ug/L 10.0 0.21 1 06/04/1519:27 74-95-3 ND ug/L 5.0 0.30 1 06/04/1519:27 95-50-1 ND ug/L 1.0 0.33 1 06/04/1519:27 106-46-7 ND ug/L 100 1.0 1 06/04/1519:27 110-57-6 ND ug/L 5.0 0.32 1 06/04/1519:27 75-34-3 ND ug/L 1.0 0.12 1 06/04/1519:27 107-06-2 ND ug/L 5.0 0.56 1 06/04/1519:27 75-35-4 ND ug/L 5.0 0.19 1 06/04/1519:27 156-59-2 ND ug/L 5.0 0.49 1 06/04/1519:27 156-60-5 ND ug/L 1.0 0.27 1 06/04/1519:27 78-87-5 ND ug/L 1.0 0.28 1 06/04/1519:27 142-28-9 ND ug/L 1.0 0.13 1 06/04/1519:27 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. L2 Page 18 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY SWs Pace Project No.: 92252037 Sample: SWN-2 Lab ID: 92252037008 Collected: 05/28/15 16:20 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/15 19:27 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/15 19:27 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/04/15 19:27 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/15 19:27 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/15 19:27 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/15 19:27 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/04/15 19:27 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/15 19:27 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/15 19:27 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/15 19:27 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/15 19:27 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/15 19:27 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/15 19:27 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/15 19:27 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/15 19:27 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/15 19:27 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/15 19:27 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/15 19:27 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/15 19:27 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 06/04/15 19:27 460-00-4 1,2-Dichloroethane-d4 (S) 97 % 70-130 1 06/04/15 19:27 17060-07-0 Toluene-d8 (S) 101 % 70-130 1 06/04/15 19:27 2037-26-5 Date: 06/24/2015 09:12 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 19 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY SWs Pace Project No.: 92252037 QC Batch: MPRP/18601 Analysis Method: EPA6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET NC Groundwater Associated Lab Samples: 92252037001, 92252037002, 92252037003, 92252037004, 92252037005, 92252037006, 92252037007, 92252037008 METHOD BLANK: 1473363 Matrix: Water Associated Lab Samples: 92252037001, 92252037002, 92252037003, 92252037004, 92252037005, 92252037006, 92252037007, 92252037008 Parameter Blank Units Result Antimony ug/L Arsenic ug/L Barium ug/L Beryllium ug/L Cadmium ug/L Chromium ug/L Cobalt ug/L Copper ug/L Lead ug/L Nickel ug/L Selenium ug/L Silver ug/L Thallium ug/L Vanadium ug/L Zinc ug/L Reporting Limit Analyzed Qualifiers ND 6.0 06/04/15 22:53 ND 10.0 06/04/15 22:53 ND 100 06/04/15 22:53 ND 1.0 06/04/15 22:53 ND 1.0 06/04/15 22:53 ND 10.0 06/04/15 22:53 ND 10.0 06/04/15 22:53 ND 10.0 06/05/1516:24 ND 10.0 06/05/1516:24 ND 50.0 06/04/15 22:53 ND 10.0 06/04/15 22:53 ND 10.0 06/04/15 22:53 ND 5.5 06/04/15 22:53 ND 25.0 06/04/15 22:53 ND 10.0 06/05/1516:24 LABORATORY CONTROL SAMPLE: Parameter 1473364 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 500 472 94 80-120 Arsenic ug/L 500 458 92 80-120 Barium ug/L 500 459 92 80-120 Beryllium ug/L 500 460 92 80-120 Cadmium ug/L 500 457 91 80-120 Chromium ug/L 500 458 92 80-120 Cobalt ug/L 500 461 92 80-120 Copper ug/L 500 458 92 80-120 Lead ug/L 500 455 91 80-120 Nickel ug/L 500 458 92 80-120 Selenium ug/L 500 434 87 80-120 Silver ug/L 250 224 90 80-120 Thallium ug/L 500 460 92 80-120 Vanadium ug/L 500 451 90 80-120 Zinc ug/L 500 453 91 80-120 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/24/2015 09:12 AM without the written consent of Pace Analytical Services, Inc.. Page 20 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY SWs Pace Project No.: 92252037 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1473365 1473366 MS MSD 92252036001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 464 514 93 103 75-125 10 25 Arsenic ug/L ND 500 500 452 499 90 100 75-125 10 25 Barium ug/L 144 500 500 597 644 91 100 75-125 8 25 Beryllium ug/L ND 500 500 457 503 91 101 75-125 10 25 Cadmium ug/L ND 500 500 449 496 90 99 75-125 10 25 Chromium ug/L 5.2 500 500 458 501 90 99 75-125 9 25 Cobalt ug/L ND 500 500 448 492 90 98 75-125 10 25 Copper ug/L 8.7 500 500 508 507 100 100 75-125 0 25 Lead ug/L ND 500 500 444 485 89 97 75-125 9 25 Nickel ug/L ND 500 500 446 490 89 98 75-125 9 25 Selenium ug/L ND 500 500 429 477 85 95 75-125 11 25 Silver ug/L ND 250 250 220 243 88 97 75-125 10 25 Thallium ug/L ND 500 500 446 493 89 98 75-125 10 25 Vanadium ug/L 4.OJ 500 500 448 491 89 97 75-125 9 25 Zinc ug/L 11.4 500 500 478 495 93 97 75-125 3 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/24/2015 09:12 AM without the written consent of Pace Analytical Services, Inc.. Page 21 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY SWs Pace Project No.: 92252037 QC Batch: MSV/32002 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92252037001, 92252037002, 92252037003, 92252037005, 92252037006, 92252037007, 92252037008 METHOD BLANK: 1475797 Matrix: Water Associated Lab Samples: 92252037001, 92252037002, 92252037003, 92252037005, 92252037006, 92252037007, 92252037008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/04/15 16:39 1,1,1-Trichloroethane ug/L ND 1.0 06/04/15 16:39 1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/04/15 16:39 1,1,2-Trichloroethane ug/L ND 1.0 06/04/15 16:39 1,1-Dichloroethane ug/L ND 5.0 06/04/15 16:39 1,1-Dichloroethene ug/L ND 5.0 06/04/15 16:39 1,2,3-Trichloropropane ug/L ND 1.0 06/04/15 16:39 1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/04/15 16:39 1,2-Dibromoethane (EDB) ug/L ND 1.0 06/04/15 16:39 1,2-Dichlorobenzene ug/L ND 5.0 06/04/15 16:39 1,2-Dichloroethane ug/L ND 1.0 06/04/15 16:39 1,2-Dichloropropane ug/L ND 1.0 06/04/15 16:39 1,3-Dichloropropane ug/L ND 1.0 06/04/15 16:39 1,4-Dichlorobenzene ug/L ND 1.0 06/04/15 16:39 2-Butanone (MEK) ug/L ND 100 06/04/15 16:39 2-Hexanone ug/L ND 50.0 06/04/15 16:39 4-Methyl-2-pentanone (MIBK) ug/L ND 100 06/04/15 16:39 Acetone ug/L ND 100 06/04/15 16:39 Acrylonitrile ug/L ND 200 06/04/15 16:39 Benzene ug/L ND 1.0 06/04/15 16:39 Bromochloromethane ug/L ND 3.0 06/04/15 16:39 Bromodichloromethane ug/L ND 1.0 06/04/15 16:39 Bromoform ug/L ND 3.0 06/04/15 16:39 Bromomethane ug/L ND 10.0 06/04/15 16:39 Carbon disulfide ug/L ND 100 06/04/15 16:39 Carbon tetrachloride ug/L ND 1.0 06/04/15 16:39 Chlorobenzene ug/L ND 3.0 06/04/15 16:39 Chloroethane ug/L ND 10.0 06/04/15 16:39 Chloroform ug/L ND 5.0 06/04/15 16:39 Chloromethane ug/L ND 1.0 06/04/15 16:39 cis-1,2-Dichloroethene ug/L ND 5.0 06/04/15 16:39 cis-1,3-Dichloropropene ug/L ND 1.0 06/04/15 16:39 Dibromochloromethane ug/L ND 3.0 06/04/15 16:39 Dibromomethane ug/L ND 10.0 06/04/15 16:39 Ethylbenzene ug/L ND 1.0 06/04/15 16:39 lodomethane ug/L ND 10.0 06/04/15 16:39 Methylene Chloride ug/L ND 1.0 06/04/15 16:39 Styrene ug/L ND 1.0 06/04/15 16:39 Tetrachloroethene ug/L ND 1.0 06/04/15 16:39 Toluene ug/L ND 1.0 06/04/15 16:39 trans-1,2-Dichloroethene ug/L ND 5.0 06/04/15 16:39 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/24/2015 09:12 AM without the written consent of Pace Analytical Services, Inc.. Page 22 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY SWs Pace Project No.: 92252037 METHOD BLANK: 1475797 Matrix: Water Associated Lab Samples: 92252037001, 92252037002, 92252037003, 92252037005, 92252037006, 92252037007, 92252037008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers trans- 1,3-Dichloropropene ug/L ND 1.0 06/04/15 16:39 trans-1,4-Dichloro-2-butene ug/L ND 100 06/04/15 16:39 Trichloroethene ug/L ND 1.0 06/04/15 16:39 Trichlorofluoromethane ug/L ND 1.0 06/04/15 16:39 Vinyl acetate ug/L ND 50.0 06/04/15 16:39 Vinyl chloride ug/L ND 1.0 06/04/15 16:39 Xylene (Total) ug/L ND 5.0 06/04/15 16:39 1,2-Dichloroethane-d4 (S) % 98 70-130 06/04/15 16:39 4-Bromofluorobenzene (S) % 99 70-130 06/04/15 16:39 Toluene-d8 (S) % 100 70-130 06/04/15 16:39 LABORATORY CONTROL SAMPLE: Parameter 1475798 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 51.6 103 80-125 1,1,1-Trichloroethane ug/L 50 47.9 96 71-129 1,1,2,2-Tetrachloroethane ug/L 50 51.8 104 79-124 1,1,2-Trichloroethane ug/L 50 50.1 100 85-125 1,1-Dichloroethane ug/L 50 48.4 97 73-126 1,1-Dichloroethene ug/L 50 48.3 97 66-135 1,2,3-Trichloropropane ug/L 50 53.1 106 75-130 1,2-Dibromo-3-chloropropane ug/L 50 49.4 99 71-133 1,2-Dibromoethane (EDB) ug/L 50 53.4 107 83-124 1,2-Dichlorobenzene ug/L 50 57.7 115 80-133 1,2-Dichloroethane ug/L 50 48.6 97 67-128 1,2-Dichloropropane ug/L 50 49.8 100 75-132 1,3-Dichloropropane ug/L 50 54.0 108 76-131 1,4-Dichlorobenzene ug/L 50 55.6 111 78-130 2-Butanone (MEK) ug/L 100 99.91 100 61-144 2-Hexanone ug/L 100 109 109 68-143 4-Methyl-2-pentanone (MIBK) ug/L 100 99AJ 99 72-135 Acetone ug/L 100 105 105 48-146 Acrylonitrile ug/L 250 241 96 40-160 Benzene ug/L 50 51.0 102 80-125 Bromochloromethane ug/L 50 50.0 100 71-125 Bromodichloromethane ug/L 50 43.7 87 78-124 Bromoform ug/L 50 33.9 68 71-128 LO Bromomethane ug/L 50 62.3 125 40-160 Carbon disulfide ug/L 50 41.7J 83 50-160 Carbon tetrachloride ug/L 50 47.1 94 69-131 Chlorobenzene ug/L 50 54.0 108 81-122 Chloroethane ug/L 50 46.2 92 39-148 Chloroform ug/L 50 45.3 91 73-127 Chloromethane ug/L 50 50.7 101 44-146 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/24/2015 09:12 AM without the written consent of Pace Analytical Services, Inc.. Page 23 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY SWs Pace Project No.: 92252037 LABORATORY CONTROL SAMPLE: Parameter 1475798 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers cis-1,2-Dichloroethene ug/L 50 50.5 101 74-124 cis-1,3-Dichloropropene ug/L 50 49.7 99 72-132 Dibromochloromethane ug/L 50 42.8 86 78-125 Dibromomethane ug/L 50 50.3 101 82-120 Ethylbenzene ug/L 50 53.3 107 79-121 lodomethane ug/L 100 113 113 39-154 Methylene Chloride ug/L 50 55.0 110 64-133 Styrene ug/L 50 57.1 114 84-126 Tetrachloroethene ug/L 50 55.0 110 78-122 Toluene ug/L 50 49.9 100 80-121 trans-1,2-Dichloroethene ug/L 50 49.0 98 71-127 trans- 1,3-Dichloropropene ug/L 50 50.9 102 69-141 trans-1,4-Dichloro-2-butene ug/L 50 41.OJ 82 40-160 Trichloroethene ug/L 50 48.6 97 78-122 Trichlorofluoromethane ug/L 50 50.1 100 53-137 Vinyl acetate ug/L 100 106 106 40-160 Vinyl chloride ug/L 50 54.5 109 58-137 Xylene (Total) ug/L 150 161 107 81-126 1,2-Dichloroethane-d4 (S) % 96 70-130 4-Bromofluorobenzene (S) % 102 70-130 Toluene-d8 (S) % 100 70-130 MATRIX SPIKE SAMPLE: Parameter 1475800 Units 92252070006 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 15.2 76 70-130 1,1,1-Trichloroethane ug/L ND 20 17.7 88 70-130 1,1,2,2-Tetrachloroethane ug/L ND 20 16.6 83 70-130 1,1,2-Trichloroethane ug/L ND 20 17.4 87 70-130 1,1-Dichloroethane ug/L ND 20 18.5 92 70-130 1,1-Dichloroethene ug/L ND 20 19.3 97 70-166 1,2,3-Trichloropropane ug/L ND 20 16.8 84 70-130 1,2-Dibromo-3-chloropropane ug/L ND 20 15.0 75 70-130 1,2-Dibromoethane (EDB) ug/L ND 20 17.1 85 70-130 1,2-Dichlorobenzene ug/L ND 20 18.5 92 70-130 1,2-Dichloroethane ug/L ND 20 17.8 89 70-130 1,2-Dichloropropane ug/L ND 20 18.1 90 70-130 1,3-Dichloropropane ug/L ND 20 17.5 88 70-130 1,4-Dichlorobenzene ug/L ND 20 17.4 87 70-130 2-Butanone (MEK) ug/L ND 40 37.9J 95 70-130 2-Hexanone ug/L ND 40 35.9J 90 70-130 4-Methyl-2-pentanone (MIBK) ug/L ND 40 35.5J 89 70-130 Acetone ug/L ND 40 37.OJ 89 70-130 Acrylonitrile ug/L ND 100 85.7J 86 70-130 Benzene ug/L ND 20 18.7 94 70-148 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/24/2015 09:12 AM without the written consent of Pace Analytical Services, Inc.. Page 24 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY SWs Pace Project No.: 92252037 MATRIX SPIKE SAMPLE: 1475800 92252070006 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Bromochloromethane ug/L ND 20 18.9 95 70-130 Bromodichloromethane ug/L ND 20 14.0 70 70-130 Bromoform ug/L ND 20 11.8 59 70-130 MO Bromomethane ug/L ND 20 18.8 94 70-130 Carbon disulfide ug/L ND 20 15.6J 78 70-130 Carbon tetrachloride ug/L ND 20 15.6 78 70-130 Chlorobenzene ug/L ND 20 18.6 93 70-146 Chloroethane ug/L ND 20 19.7 98 70-130 Chloroform ug/L ND 20 16.3 81 70-130 Chloromethane ug/L ND 20 21.8 109 70-130 cis-1,2-Dichloroethene ug/L ND 20 18.9 95 70-130 cis-1,3-Dichloropropene ug/L ND 20 15.9 79 70-130 Dibromochloromethane ug/L ND 20 11.5 58 70-130 M1 Dibromomethane ug/L ND 20 17.4 87 70-130 Ethylbenzene ug/L ND 20 18.2 91 70-130 lodomethane ug/L ND 40 41.3 103 70-130 Methylene Chloride ug/L ND 20 19.8 99 70-130 Styrene ug/L ND 20 18.8 94 70-130 Tetrachloroethene ug/L ND 20 18.5 92 70-130 Toluene ug/L ND 20 18.0 90 70-155 trans-1,2-Dichloroethene ug/L ND 20 19.1 96 70-130 trans- 1,3-Dichloropropene ug/L ND 20 15.4 77 70-130 trans-1,4-Dichloro-2-butene ug/L ND 20 14.2J 71 70-130 Trichloroethene ug/L ND 20 18.4 92 69-151 Trichlorofluoromethane ug/L ND 20 19.5 97 70-130 Vinyl acetate ug/L ND 40 33.2J 83 70-130 Vinyl chloride ug/L ND 20 19.7 98 70-130 1,2-Dichloroethane-d4 (S) % 101 70-130 4-Bromofluorobenzene (S) % 98 70-130 Toluene-d8 (S) % 99 70-130 SAMPLE DUPLICATE: 1475799 92252070005 Dup Max Parameter Units Result Result RPD RPD Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND ND 30 1,1,1-Trichloroethane ug/L ND ND 30 1,1,2,2-Tetrachloroethane ug/L ND ND 30 1,1,2-Trichloroethane ug/L ND ND 30 1,1-Dichloroethane ug/L 0.46J 0.46J 30 1,1-Dichloroethene ug/L ND ND 30 1,2,3-Trichloropropane ug/L ND ND 30 1,2-Dibromo-3-chloropropane ug/L ND ND 30 1,2-Dibromoethane (EDB) ug/L ND ND 30 1,2-Dichlorobenzene ug/L ND ND 30 1,2-Dichloroethane ug/L 0.14J 0.13J 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/24/2015 09:12 AM without the written consent of Pace Analytical Services, Inc.. Page 25 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY SWs Pace Project No.: 92252037 SAMPLE DUPLICATE: 1475799 Parameter Units 92252070005 Result Dup Result 1,2-Dichloropropane ug/L ND ND 1,3-Dichloropropane ug/L ND ND 1,4-Dichlorobenzene ug/L 0.42J 0.44J 2-Butanone (MEK) ug/L ND ND 2-Hexanone ug/L ND ND 4-Methyl-2-pentanone (MIBK) ug/L ND ND Acetone ug/L ND ND Acrylonitrile ug/L ND ND Benzene ug/L ND ND Bromochloromethane ug/L ND ND Bromodichloromethane ug/L ND ND Bromoform ug/L ND ND Bromomethane ug/L ND ND Carbon disulfide ug/L ND ND Carbon tetrachloride ug/L ND ND Chlorobenzene ug/L ND ND Chloroethane ug/L ND ND Chloroform ug/L ND ND Chloromethane ug/L ND ND cis-1,2-Dichloroethene ug/L 0.74J 0.72J cis-1,3-Dichloropropene ug/L ND ND Dibromochloromethane ug/L ND ND Dibromomethane ug/L ND ND Ethylbenzene ug/L ND ND lodomethane ug/L ND ND Methylene Chloride ug/L ND ND Styrene ug/L ND ND Tetrachloroethene ug/L ND ND Toluene ug/L ND ND trans-1,2-Dichloroethene ug/L ND ND trans- 1,3-Dichloropropene ug/L ND ND trans-1,4-Dichloro-2-butene ug/L ND ND Trichloroethene ug/L ND ND Trichlorofluoromethane ug/L ND ND Vinyl acetate ug/L ND ND Vinyl chloride ug/L ND ND Xylene (Total) ug/L ND ND 1,2-Dichloroethane-d4 (S) % 104 104 4-Bromofluorobenzene (S) % 97 97 Toluene-d8(S) % 102 102 Max RPD RPD Qualifiers 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/24/2015 09:12 AM without the written consent of Pace Analytical Services, Inc.. Page 26 of 30 Pace Analytical Services, Inc. aceAnalXical� 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 www.pacelabs.com (704)875-9092 QUALIFIERS Project: SURRY SWs Pace Project No.: 92252037 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits. L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated samples may be biased low. MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/24/2015 09:12 AM without the written consent of Pace Analytical Services, Inc.. Page 27 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: SURRY SWs Pace Project No.: 92252037 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92252037001 SW-1 EPA 3010 MPRP/18601 EPA 6010 92252037002 SW-2 EPA 3010 MPRP/18601 EPA 6010 92252037003 SW-3 EPA 3010 MPRP/18601 EPA 6010 92252037004 SW-4 EPA 3010 MPRP/18601 EPA 6010 92252037005 SW -A EPA 3010 MPRP/18601 EPA 6010 92252037006 SW-13 EPA 3010 MPRP/18601 EPA 6010 92252037007 SWN-1 EPA 3010 MPRP/18601 EPA 6010 92252037008 SWN-2 EPA 3010 MPRP/18601 EPA 6010 92252037001 SW-1 EPA 8260 MSV/32002 92252037002 SW-2 EPA 8260 MSV/32002 92252037003 SW-3 EPA 8260 MSV/32002 92252037005 SW -A EPA 8260 MSV/32002 92252037006 SW-13 EPA 8260 MSV/32002 92252037007 SWN-1 EPA 8260 MSV/32002 92252037008 SWN-2 EPA 8260 MSV/32002 Date: 06/24/2015 09:12 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Analytical Batch ICP/16683 ICP/16683 ICP/16683 ICP/16683 ICP/16683 ICP/16683 ICP/16683 ICP/16683 Page 28 of 30 /�Iff�ee�fnalytical" l 1e l�oncallion Upon Recei Document Number: F-CHR-CS-003-rov.16 Pa e 1 of 2'" Issuing Authority: Pace Huntersville Quality Office Client Name:y+ ►. ) c i u—,'ri o ' Page 2 of is for Internal Use Only Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Client❑ C merciai Pace Other Custody Seal on CoolerlBox Present: ❑ yes W no Seals intact: ❑yes ❑ no rp"i 3 y Packing Material: ❑ Bubble V❑p ❑ Bubble Bags None ❑ Other thermometer Used: IR Gun T1401 Type of Ice: Wet Blue None aeample, on ice, cooling process has begun remp Correction Factor T1401 No Correction dorrected Cooler TerrSp.: -C -- Biological Tissue is Frozen: Yes No MIA Date and Initi s f arson xa a ' rem should be above freezing to 6°C p 9 Comments: contents: 'Ihiain of Custody Present: es ONO ❑NIA 1. chain of Custody Filled Out: es El No ❑NIA 2, chain of Custody Relinquished: es ❑No ❑NIA 3. Sampler Name & Signature on COG: res PNo ❑NIA 4. Samples Arrived within Hold Time: es ❑No ❑NIA 5. Short Hold Time Analysis (<72hr): ❑Yes XN1 ❑NIA 6, Rush Turn Around Time Requested: ❑Yes 40 ❑NIA 7, Sufficient Volume: es ©No ❑NIA 8. 'orrect Containers Used: l[7>K, El No El N/A 9. -Pace Containers Used: s El No ❑NIA ;ontainers Intact: es ❑No ❑NI 10. -iltere'd volume received for Dissolved tests ❑r ON o ria IA 11. Sample Labels match COC: Yes No El NIA 12. -Includes dateltime/lD/Analysis Matrix: k1l containers needing preservation have been checked. es ©No ❑NIA 13. kil containers needing preservation are found to be in es ❑No ❑NIA :ompliance with EPA recommendation. exceptions: VOA, coliform, TOC, 0&G, WI-DRO (water) ❑Yes (.]No Samples checked for dechforination: es ❑No ❑NIAFL,i 4. leadspace in VOA Vials (>6mm): ❑Yes No .. 5.rf rrip Blank Present: Oyes ❑No NIA 16. rrip Blank Custody Seals Present ©Yes ❑No NIA "ace -Trip -Blank Lot #-(if-purchased):- "ifent Notiticationl Resolution: Field Data Required? Y 1 N Person Contacted: Via., ti �-{n„ &0 Dateffime: Comments/Resolution:. �M ,`.?�o1.p�� Tt4 r� �,� �_.�q So z ncc�'��.;{ r^,;rz Sc.-`Lee, SCURF Review: IDate: I 5 P511 SRF Review: ` ! �� Date: Note: Whenever there i discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers) Place label here Wa:92252037 1111111111111111111111 _ 92252037 Page 29 of 30 /51 CHAIN -OF -CUSTODY 1 Analytical Request Document . The Chain -of -Custody is a LEGAL DOCUMENT, All relevant fields must be completed accurately. Section A Section B Section C Required Client Information: Required Project Information: Invoice Information: Page - 1 Of 1 Company: Municipal Engineering Services Report To: Jonathan Pfohl Attention, Address: 68 Shipwash Drive Copy To: Company Name: Gamer, NC 27529 Address: Regulatory Agency Email: Purchase Order 9: Pace Quote: Phone; JFax Project Name: Surry SWs Pace Project Manager kevin.godwin pacelabs,com, State 1 Location Requested Due Date: Project #: Pace Profile #: Requested Analysis Filtered YIN rnallxFx cone 0 COLLECTED z Preservatives r o, any w,rar ow U 4 r Water WT W-t. Ware, P,adi P SAMPLE ID solisL rY g } on O> START END X M One Character per box. wlp= WIP (A-Z, 0.91, -) ar AA Otter OT o U w F = m M O U Sample Ids must be unique T;;;,,r, Ts u J 0 c O e C a C W rr r r - t U 0 m C to cn O S O in ro L Q I^ s DATE TIME DATE TIME N z z= z z 6 5 O ¢ a 1 sw-t WT X X J� 2 SW-2 wT 3=35 I X X U a2 3 SW-3 WT 3-5Z I X X �U &'11C 4 sw-4 WT X X 5 SW -A VVT sf� S X X 6 SW-B vv r x x V 7 SWN-1 WT X X 8 SWN-2 WT �'�� X X l 9 Sldba.3 wr X x 10 11 12 ADDITIONAL COMMENTS RE�INQUISNED BY I AFFILIATION DATE TIME ACCEPTED BY I AFFIUAT10N DATE TIME SAMPLE CONDITIONS 1. /l SAMPLER NAME AND SIGNATURE c PRINT Name of SAMPLER: r'r U � SIGNATURE of SAMPLE DATE Signed: m� 3 Is nUr cr v� aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 July 28, 2015 Mr. Jonathan Pfohl Municipal Engineering Services PO Box 97 Garner, NC 27529 RE: Project: SURRY CO MSWLF Pace Project No.: 92260076 Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory on July 23, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Godwin kevin.godwin@pacelabs.com Project Manager Enclosures Q _Kok r REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 13 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 CERTIFICATIONS Project: SURRY CO MSWLF Pace Project No.: 92260076 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 Virginia/VELAP Certification #: 460221 South Carolina Certification #: 99006001 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 13 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 Project: SURRY CO MSWLF Pace Project No.: 92260076 Lab ID Sample ID 92260076001 SW-4 SAMPLE SUMMARY Matrix Date Collected Date Received Water 07/20/1517:00 07/23/1513:05 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 13 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: SURRY CO MSWLF Pace Project No.: 92260076 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92260076001 SW-4 EPA 8260 SNP 51 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 13 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CO MSWLF Pace Project No.: 92260076 Sample: SW-4 Lab ID: 92260076001 Collected: 07/20/15 17:00 Received: 07/23/15 13:05 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 24.2J ug/L 100 10.0 1 07/28/15 09:27 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 07/28/15 09:27 107-13-1 Benzene ND ug/L 1.0 0.25 1 07/28/15 09:27 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 07/28/15 09:27 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 07/28/15 09:27 75-27-4 Bromoform ND ug/L 3.0 0.26 1 07/28/15 09:27 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 07/28/15 09:27 74-83-9 2-Butanone (MEK) 13.OJ ug/L 100 0.96 1 07/28/15 09:27 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 07/28/15 09:27 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 07/28/15 09:27 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 07/28/15 09:27 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 07/28/15 09:27 75-00-3 Chloroform ND ug/L 5.0 0.14 1 07/28/15 09:27 67-66-3 Chloromethane 0.15J ug/L 1.0 0.11 1 07/28/15 09:27 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 07/28/15 09:27 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 07/28/15 09:27 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 07/28/15 09:27 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 07/28/15 09:27 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 07/28/15 09:27 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 07/28/15 09:27 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 07/28/15 09:27 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 07/28/15 09:27 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 07/28/15 09:27 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 07/28/15 09:27 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 07/28/15 09:27 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 07/28/15 09:27 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 07/28/15 09:27 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 07/28/15 09:27 142-28-9 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 07/28/15 09:27 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 07/28/15 09:27 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 07/28/15 09:27 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 07/28/15 09:27 591-78-6 lodomethane ND ug/L 10.0 0.32 1 07/28/15 09:27 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 07/28/15 09:27 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 07/28/15 09:27 108-10-1 Styrene ND ug/L 1.0 0.26 1 07/28/15 09:27 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 07/28/15 09:27 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 07/28/15 09:27 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 07/28/15 09:27 127-18-4 Toluene ND ug/L 1.0 0.26 1 07/28/15 09:27 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 07/28/15 09:27 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 07/28/15 09:27 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 07/28/15 09:27 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 07/28/15 09:27 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 07/28/15 09:27 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 07/28/15 09:27 108-05-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/28/2015 06:14 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 13 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CO MSWLF Pace Project No.: 92260076 Sample: SW-4 Lab ID: 92260076001 Collected: 07/20/15 17:00 Received: 07/23/15 13:05 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Vinyl chloride ND ug/L 1.0 0.62 1 07/28/15 09:27 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 07/28/15 09:27 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 103 % 70-130 1 07/28/15 09:27 460-00-4 1,2-Dichloroethane-d4 (S) 108 % 70-130 1 07/28/15 09:27 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 07/28/15 09:27 2037-26-5 Date: 07/28/2015 06:14 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 13 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CO MSWLF Pace Project No.: 92260076 QC Batch: MSV/32722 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92260076001 METHOD BLANK: 1519232 Associated Lab Samples: 92260076001 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 07/28/15 04:10 1,1,1-Trichloroethane ug/L ND 1.0 07/28/15 04:10 1,1,2,2-Tetrachloroethane ug/L ND 3.0 07/28/15 04:10 1,1,2-Trichloroethane ug/L ND 1.0 07/28/15 04:10 1,1-Dichloroethane ug/L ND 5.0 07/28/15 04:10 1,1-Dichloroethene ug/L ND 5.0 07/28/15 04:10 1,2,3-Trichloropropane ug/L ND 1.0 07/28/15 04:10 1,2-Dibromo-3-chloropropane ug/L ND 13.0 07/28/15 04:10 1,2-Dibromoethane (EDB) ug/L ND 1.0 07/28/15 04:10 1,2-Dichlorobenzene ug/L ND 5.0 07/28/15 04:10 1,2-Dichloroethane ug/L ND 1.0 07/28/15 04:10 1,2-Dichloropropane ug/L ND 1.0 07/28/15 04:10 1,3-Dichloropropane ug/L ND 1.0 07/28/15 04:10 1,4-Dichlorobenzene ug/L ND 1.0 07/28/15 04:10 2-Butanone (MEK) ug/L ND 100 07/28/15 04:10 2-Hexanone ug/L ND 50.0 07/28/15 04:10 4-Methyl-2-pentanone (MIBK) ug/L ND 100 07/28/15 04:10 Acetone ug/L ND 100 07/28/15 04:10 Acrylonitrile ug/L ND 200 07/28/15 04:10 Benzene ug/L ND 1.0 07/28/15 04:10 Bromochloromethane ug/L ND 3.0 07/28/15 04:10 Bromodichloromethane ug/L ND 1.0 07/28/15 04:10 Bromoform ug/L ND 3.0 07/28/15 04:10 Bromomethane ug/L ND 10.0 07/28/15 04:10 Carbon disulfide ug/L ND 100 07/28/15 04:10 Carbon tetrachloride ug/L ND 1.0 07/28/15 04:10 Chlorobenzene ug/L ND 3.0 07/28/15 04:10 Chloroethane ug/L ND 10.0 07/28/15 04:10 Chloroform ug/L ND 5.0 07/28/15 04:10 Chloromethane ug/L ND 1.0 07/28/15 04:10 cis-1,2-Dichloroethene ug/L ND 5.0 07/28/15 04:10 cis-1,3-Dichloropropene ug/L ND 1.0 07/28/15 04:10 Dibromochloromethane ug/L ND 3.0 07/28/15 04:10 Dibromomethane ug/L ND 10.0 07/28/15 04:10 Ethylbenzene ug/L ND 1.0 07/28/15 04:10 lodomethane ug/L ND 10.0 07/28/15 04:10 Methylene Chloride ug/L ND 1.0 07/28/15 04:10 Styrene ug/L ND 1.0 07/28/15 04:10 Tetrachloroethene ug/L ND 1.0 07/28/15 04:10 Toluene ug/L ND 1.0 07/28/15 04:10 trans-1,2-Dichloroethene ug/L ND 5.0 07/28/15 04:10 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/28/2015 06:14 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 13 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CO MSWLF Pace Project No.: 92260076 METHOD BLANK: 1519232 Associated Lab Samples: 92260076001 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed trans- 1,3-Dichloropropene ug/L ND 1.0 07/28/15 04:10 trans-1,4-Dichloro-2-butene ug/L ND 100 07/28/15 04:10 Trichloroethene ug/L ND 1.0 07/28/15 04:10 Trichlorofluoromethane ug/L ND 1.0 07/28/15 04:10 Vinyl acetate ug/L ND 50.0 07/28/15 04:10 Vinyl chloride ug/L ND 1.0 07/28/15 04:10 Xylene (Total) ug/L ND 5.0 07/28/15 04:10 1,2-Dichloroethane-d4 (S) % 105 70-130 07/28/15 04:10 4-Bromofluorobenzene (S) % 100 70-130 07/28/15 04:10 Toluene-d8 (S) % 99 70-130 07/28/15 04:10 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 1519233 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 50.4 101 80-125 1,1,1-Trichloroethane ug/L 50 52.1 104 71-129 1,1,2,2-Tetrachloroethane ug/L 50 54.4 109 79-124 1,1,2-Trichloroethane ug/L 50 52.3 105 85-125 1,1-Dichloroethane ug/L 50 48.7 97 73-126 1,1-Dichloroethene ug/L 50 51.1 102 66-135 1,2,3-Trichloropropane ug/L 50 55.1 110 75-130 1,2-Dibromo-3-chloropropane ug/L 50 52.1 104 71-133 1,2-Dibromoethane (EDB) ug/L 50 53.2 106 83-124 1,2-Dichlorobenzene ug/L 50 54.0 108 80-133 1,2-Dichloroethane ug/L 50 48.7 97 67-128 1,2-Dichloropropane ug/L 50 50.1 100 75-132 1,3-Dichloropropane ug/L 50 52.1 104 76-131 1,4-Dichlorobenzene ug/L 50 52.5 105 78-130 2-Butanone (MEK) ug/L 100 100 100 61-144 2-Hexanone ug/L 100 108 108 68-143 4-Methyl-2-pentanone (MIBK) ug/L 100 110 110 72-135 Acetone ug/L 100 101 101 48-146 Acrylonitrile ug/L 250 239 96 40-160 Benzene ug/L 50 51.5 103 80-125 Bromochloromethane ug/L 50 54.3 109 71-125 Bromodichloromethane ug/L 50 54.5 109 78-124 Bromoform ug/L 50 49.4 99 71-128 Bromomethane ug/L 50 43.5 87 40-160 Carbon disulfide ug/L 50 45.8J 92 50-160 Carbon tetrachloride ug/L 50 54.7 109 69-131 Chlorobenzene ug/L 50 51.0 102 81-122 Chloroethane ug/L 50 46.0 92 39-148 Chloroform ug/L 50 51.7 103 73-127 Chloromethane ug/L 50 43.7 87 44-146 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/28/2015 06:14 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 13 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CO MSWLF Pace Project No.: 92260076 LABORATORY CONTROL SAMPLE: Parameter 1519233 Units Spike Conc. LCS Result LCS % Rec % Rec Limits cis-1,2-Dichloroethene ug/L 50 50.1 100 74-124 cis-1,3-Dichloropropene ug/L 50 51.4 103 72-132 Dibromochloromethane ug/L 50 52.6 105 78-125 Dibromomethane ug/L 50 55.2 110 82-120 Ethylbenzene ug/L 50 51.4 103 79-121 lodomethane ug/L 100 89.1 89 39-154 Methylene Chloride ug/L 50 51.0 102 64-133 Styrene ug/L 50 50.8 102 84-126 Tetrachloroethene ug/L 50 50.3 101 78-122 Toluene ug/L 50 52.8 106 80-121 trans-1,2-Dichloroethene ug/L 50 47.9 96 71-127 trans- 1,3-Dichloropropene ug/L 50 51.0 102 69-141 trans-1,4-Dichloro-2-butene ug/L 50 53.1J 106 40-160 Trichloroethene ug/L 50 49.4 99 78-122 Trichlorofluoromethane ug/L 50 50.8 102 53-137 Vinyl acetate ug/L 100 99.2 99 40-160 Vinyl chloride ug/L 50 46.3 93 58-137 Xylene (Total) ug/L 150 152 101 81-126 1,2-Dichloroethane-d4 (S) % 100 70-130 4-Bromofluorobenzene (S) % 102 70-130 Toluene-d8 (S) % 100 70-130 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/28/2015 06:14 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 13 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALIFIERS Project: SURRY CO MSWLF Pace Project No.: 92260076 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. LABORATORIES PASI-C Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/28/2015 06:14 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 13 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: SURRY CO MSWLF Pace Project No.: 92260076 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92260076001 SW-4 EPA 8260 MSV/32722 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/28/2015 06:14 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 13 I-JUGUIIIt' IIL INaIIW. IJUGUInUIIL RtlVibUU. IVIdy 10, w 10 1PzCeRr�<?fytiCala Sample Condition Upon Receipt (SCUR) Page 1 of 2* Document Number: Issuing Authority: F-CHR-CS-003-rev.16 Pace Huntersville Quality Office Client Name: Page 2 of 2 is for Internal Use Only Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Clienteno fY mercial❑ 1?ar Other Y y� Custody Seal on Cooler/Cox Present: El yes Seals intact: ❑ yes ❑ no Packing Material: ❑ Bubble V❑p ET Bubble Bags ❑ None ❑ Other Thermometer Used: IR Gun 140 Type of Ice: et Blue None Samples on ice, cooling process has begun •rmmn 1'_nrrarfinn FmIfnr T1441 Nn Correction Corrected Cooler Temp.:`' ° Biological Tissue is Frozen: Yes No IA Date and Initials of -person a nr; C contents: � 7" �� Temp should be above freezing to 6°C Comments: Chain of Custody Present: Yeb No ❑NIA 1. Chain of Custody Filled Out: Ye No ❑NIA 2. Chain of Custody Relinquished: Yes No ❑NIA 3. Sampler Name & Signature on COC: es s' ❑NIA 4. Samples Arrived within Hold Time: ❑ es ONO NIA 5. Short Hold Time Analysis (<72hr): ❑Yes ❑ o NIA 6. Bush Turn Around Time Requested: Dyes No ❑NIA 7. Sufficient Volume: Yes ❑No ❑NIA 8. No ❑NIA Correct Containers Used: �Y�es;210--ElNiA -Pace Containers Used: 9. Containers Intact: Yes ONO IINIA 10 Filtered volume received for Dissolved tests Dyes ❑No 11. Sample Labels match COC: �Elyes No ❑NIA -Includes datettime/iD/Analysis Matrix: 12. All containers needing preservation have been checked. Dyes LINO NIA All containers needing preservation are found to be in Dyes ❑ IA compliance with EPA recommendation. exceptions: VOA, collform, TOC, O&G, Wf-DRO (water) Dyes ❑No ),I, - Samples checked for dechlorination: ❑Yes ❑No I 4. Headspace in VOA Vials( >6mm): Dyes ❑No ©NI $. Trip Blank Present: ❑Yes ONO IINIA Trip Blank Custody Seals Present ❑Yes DNo ❑NIA Pace -Trip Blank -Lot # if purchased): 46. - - Client Notification! Resolution: Field Data Required? Y I N Person Contacted: Comments/ Resolution: Date[Time: SCURF Review;4adfls:crepancy /" Date: -? z3 S SRF Review; Date: 2 `' 1-5 Note: Whenever then affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers) ,26()07 6 1i l{ll�l� Imi0?6 92260 ,c,uel available) Page 12 of 13 Amilylill CHAIN -OF -CUSTODY 1 Analytical Request The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields Document must be completed Iccurately. Section A Section B Section C Required Client Information: Required Project Information: Invoice information: Pa e : 1 Of I Company: Municipal Engineering Services Report To: Jonathan Pfohl Attention. Municipal En2ineering Services Address: P.O. BOX 97 Copy To: Company Name: Gamer, NC 27529 Address: Regulatory Agency Email To: jpfohl{oimeseo.Com Purchase Order No. , `j �. ; , (�- !�/i j l � i= Pace Quote Reference: Phone: 919-772-5393 1 Fax: Client Project ID:.1cej[Btl-ee8rd (fie) Pace Project Manager. Kevin Godwin State ! Location Requested Due DatelTAT: 10 Day (Default) Container Order Number: Pace Profile #: North Carolina Requested Anaf sis Filtered Y1N _ a Z MP.7RiX CODE - COLLECTED z Preservatives N N N N N N N N N N N N onnNmg Water DW m O Watm wr Waste Watar WW 3 a w Pi P SAMPLE ID o;rsoa 1p 9 START END p to N F o� One Character per box. W.Po VIP W 4a i N (A-Z. 0-9 f . -) A!, AR Othl Or Sample Ids must be unique rs�uo rs 0 O x r T11TETI1E w o �' a Ory ¢ ! a • l f n GATE TIME y? z z z i O 0 1 Wr G ^1ilf.\ ��n �i 4 3 3 x ' 3 4 5 6 7 8 9 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY 1 AFFILIATION DATE TIME CCEPTED BY I ILIATION DATE TIME SAMPLE CONDITIONS 1•.%�5wi+.�l �:v� �� /� /�----�I+�I'4d"LJ-- ! Y'/,l J�/, �:v It/� ��i , �•+� o— V _ SAMPLER NAME AND SIGNATURE m m -6 U ¢ in y 2 c PRINT Name of SAMPLER: ti Jonathan Pfohl .-. � �-, } o o E z _ SIGNATURE of SAMPLER: \ � DATE Signed: — ' , %� {` J 1L aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 June 08, 2015 Mr. Jonathan Pfohl Municipal Engineering Services PO Box 97 Garner, NC 27529 RE: Project: SURRY CLOSED MT AIRY (BROMIDE) Pace Project No.: 92252477 Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory between May 29, 2015 and June 02, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Godwin kevin.godwin@pacelabs.com Project Manager Enclosures Q _Kok r REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 13 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 CERTIFICATIONS Project: SURRY CLOSED MT AIRY (BROMIDE) Pace Project No.: 92252477 Ormond Beach Certification IDs 8 East Tower Circle, Ormond Beach, FL 32174 Montana Certification #: Cert 0074 Alabama Certification #: 41320 Nebraska Certification: NE-OS-28-14 Connecticut Certification M PH-0216 Nevada Certification: FL NELAC Reciprocity Delaware Certification: FL NELAC Reciprocity New Hampshire Certification #: 2958 Florida Certification #: E83079 New Jersey Certification #: FL765 Georgia Certification #: 955 New York Certification #: 11608 Guam Certification: FL NELAC Reciprocity North Carolina Environmental Certificate #: 667 Hawaii Certification: FL NELAC Reciprocity Pennsylvania Certification #: 68-00547 Illinois Certification #: 200068 Puerto Rico Certification M FLO1264 Indiana Certification: FL NELAC Reciprocity South Carolina Certification: #96042001 Kansas Certification #: E-10383 Tennessee Certification #: TN02974 Kentucky Certification #: 90050 Texas Certification: FL NELAC Reciprocity Louisiana Certification #: FL NELAC Reciprocity US Virgin Islands Certification: FL NELAC Reciprocity Louisiana Environmental Certificate M 05007 Virginia Environmental Certification #: 460165 Maryland Certification: #346 Washington Certification #: C955 Massachusetts Certification #: M-FL1264 West Virginia Certification #: 9962C Michigan Certification #: 9911 Wisconsin Certification #: 399079670 Mississippi Certification: FL NELAC Reciprocity Wyoming (EPA Region 8): FL NELAC Reciprocity Missouri Certification #: 236 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 13 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 SAMPLE SUMMARY Project: SURRY CLOSED MT AIRY (BROMIDE) Pace Project No.: 92252477 Lab ID Sample ID Matrix Date Collected Date Received 92252477001 MW-1 Water 05/28/15 08:15 06/02/15 16:30 92252477002 MW-13 Water 05/27/1512:10 06/02/1516:30 92252477003 MW-15 Water 05/28/1513:40 06/02/1516:30 92252477004 MW-16 Water 05/28/1512:20 05/29/1513:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 13 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: SURRY CLOSED MT AIRY (BROMIDE) 92252477 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92252477001 MW-1 EPA 300.0 AIS 1 PASI-O 92252477002 MW-13 EPA 300.0 AIS 1 PASI-O 92252477003 MW-15 EPA 300.0 AIS 1 PASI-O 92252477004 MW-16 EPA 300.0 AIS 1 PASI-O REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 13 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED MT AIRY (BROMIDE) Pace Project No.: 92252477 Sample: MW-1 Lab ID: 92252477001 Collected: 05/28/15 08:15 Received: 06/02/15 16:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Bromide ND mg/L 0.10 0.069 1 06/07/15 20:35 24959-67-9 Date: 06/08/2015 03:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 13 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED MT AIRY (BROMIDE) Pace Project No.: 92252477 Sample: MW-13 Lab ID: 92252477002 Collected: 05/27/15 12:10 Received: 06/02/15 16:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Bromide 0.26 mg/L 0.10 0.069 1 06/07/15 20:57 24959-67-9 Date: 06/08/2015 03:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 13 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED MT AIRY (BROMIDE) Pace Project No.: 92252477 Sample: MW-15 Lab ID: 92252477003 Collected: 05/28/15 13:40 Received: 06/02/15 16:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Bromide ND mg/L 0.10 0.069 1 06/07/15 21:18 24959-67-9 Date: 06/08/2015 03:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 7 of 13 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED MT AIRY (BROMIDE) Pace Project No.: 92252477 Sample: MW-16 Lab ID: 92252477004 Collected: 05/28/15 12:20 Received: 05/29/15 13:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Bromide 0.29 mg/L 0.10 0.069 1 06/07/15 21:39 24959-67-9 Date: 06/08/2015 03:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 8 of 13 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED MT AIRY (BROMIDE) Pace Project No.: 92252477 QC Batch: WETA/47072 Analysis Method: EPA 300.0 QC Batch Method: EPA 300.0 Analysis Description: 300.0 IC Anions Associated Lab Samples: 92252477001, 92252477002, 92252477003, 92252477004 METHOD BLANK: 1235309 Matrix: Water Associated Lab Samples: Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Bromide mg/L ND 0.10 06/07/1514:10 LABORATORY CONTROL SAMPLE: 1235310 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Bromide mg/L 10 9.8 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1235311 1235312 MS MSD 35191456001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Bromide mg/L 0.12 10 10 9.7 9.7 96 96 90-110 0 20 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1235313 1235314 MS MSD 35191619002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Bromide mg/L 0.069U 10 10 9.5 9.4 95 94 90-110 1 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/08/2015 03:30 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 13 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALIFIERS Project: SURRY CLOSED MT AIRY (BROMIDE) Pace Project No.: 92252477 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. LABORATORIES PASI-O Pace Analytical Services - Ormond Beach REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/08/2015 03:30 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 13 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: SURRY CLOSED MT AIRY (BROMIDE) Pace Project No.: 92252477 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92252477001 MW-1 EPA 300.0 WETA/47072 92252477002 MW-13 EPA 300.0 WETA/47072 92252477003 MW-15 EPA 300.0 WETA/47072 92252477004 MW-16 EPA 300.0 WETA/47072 Date: 06/08/2015 03:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Analytical Batch Page 11 of 13 � x'tceAlr��lyPrr,�l uocument Name: le Condition Upon Recei Document Number: F-CHR-CS-003-rev.16 uocument Keviseo: may its, zu io UR Page 1 of 2* Issuing Authority: Pace Huntersville Qualitv Office Client Name:�� * Page 2 of 2 is for Internal Use Only Courier. ❑ Fed Ex ❑ UPS❑ LISPS❑ Client❑ CommercilofEf- Pace Other Custody Seal on Cooler/Box Present; ❑ yes ©-o"no Seals intact: ❑ yes ❑ no Packing Material: ❑ Bubble V❑p ❑ Bubble Bags [Z'--None ❑ Other Thermometer Used: IR Gun T1401 Type of Ice: (�Ve Blue None ]'Samples on ice, cooling process has begun Temp Correction Factor T1401 No Correction l- Corrected Cooler Tent •C Biological Tissue is Frozen: Yes No NIA Date and Initials of person examining p" contents: - Ternp should be above freezing to 6'C Comments: Chain of Custody Present: PYKII ON, ❑NIA 1. Chain of Custody Filled Out: ❑ A ONO ❑NIA 2, Chain of Custody Relinquished: es ❑No ❑NIA 3. Sampler Name & Signature on COC: ON, ❑NIA 4, d�es Samples Arrived within Hold Time: JaQ ON, El NIA 5. Short Hold Time Analysis (<72hr): ❑Y6s ONO ❑NIA 6, Rush Turn Around Time Requested: ❑Yes EfNo ❑NIA 7• Sufficient Volume: ❑Tres ON, ❑NIA Correct Containers Used: tlYes ONO ❑NIA 9. -Pace Containers Used: Yes ONO ❑NIA Containers Intact: Yes ONO ❑NIA 10. Filtered volume received for Dissolved tests Dyes ❑No NIA 11. Sample Labels match COC: YCs ONO ❑NIA 12. -Includes date/time/ID/Analysis Matrix: All containers needing preservation have been checked. ❑Yes ❑No !A 13. All containers needing preservation are found to be in Oyes ONO I-)f4A compliance with EPA recommendation. exceptions: VOA, coliform, TOC, 0&G, W-DRO (water) Dyes ❑No Samples checked for dechlorination: Dyes ❑No Q A 14. Headspace in VOA Vials (>6mm): Dyes ONO ❑NfA 15. Trip Blank Present: Oyes ONO ❑NlI� 16. Trip Blank Custody Seals Present Dyer. ONO ❑NIA Pace Trip Blank Lot # (if purchased): Client Notification/ Resolution: Field Data Required? Y 1 N 7! Person Contacted: ) ' �, % [� } �' aterrime: L- - f Comments/Resolution: -o b C S-c i"l--) SCURF Review: 11) Date: WO# v p22` SRF Review: —} Date: /5 "77 41?2- Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR I Certification Office ( i.e out of hold, incorrect preservative, out of temp, 92252477 incorrect containers) Page 12 of 13 ace4naljdfcal CHAIN -OF -CUSTODY 1 Analytical Request Document - The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. d Section A Section B Section C Required Client Information: Required Project Information: Invoice Information: Pa ge : t Of 1 company: Municipal ngineering Services Report To: Jonathan Pfohl Attentlom Municipal Engineering Services Address: P.O. Box 97 Copy To: Company Name: Garner, NC 27529 Address: Regulatory Agency Email To: ipfohl cDmesco.com Purchase Order No, Pace quote Reference: Phone: 919-772-5393 JFax Client Project ID: Surry Closed -Mt. Airy (Bromide) Pace Project Manager. Kevin Godwin State 1 Location Requested! Due Date/TAT: 10 Day (Default) lContairter Order Number; Pace Profile #: - — North Carolina Requested Analysis Filtered (YIN) z_ v a COLLECTED Preservatives Y MATRIX CODE 8 0 o Drinking Wotor eW - U z O ..to, VVT c S t;7 WW. wotm ww SAMPLE ID Product a � START END w J " somsoha sL One Character per box. o'u c� u t y F Alpo wi (A-Z, 0.9 1, -) Air AR — �' z to Sample Ids must be unique other oT u, uj } i m of Tissue 7S U x y o c Cc 0 M H u ¢ a ¢ a ¢ r1 O m c to N z z U _ m w v c Q E E o [i N DATE TIME DATE TIME N m = 2 2 z z z O m 1 MW-1 vJr G r 2 MW_93 VYT GI$ 3 MW-15 WT G x cb 4 MW-16 — 'IGbr ( 'VJ i VV7 G 1 1 x S • me 6 n t� :� 7 9 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY / AFFILIATION DATE TIME ACCEPTED BY! AFFILIATION DATE TIME SAMPLE CONDITIONS Na- SAMPLER NAME AND SIGNATURE m u m az �ti PRINT Name of SAMPLER: Jo than , fohl 2 Lu } � � 'aE �� Z .} SIGNATURE of SAMPLER: ! DATE Signed: �tr,� 171 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 June 15, 2015 Mr. Jonathan Pfohl Municipal Engineering Services PO Box 97 Garner, NC 27529 RE: Project: SURRY BLANKS Pace Project No.: 92252475 Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory on June 02, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Godwin kevin.godwin@pacelabs.com Project Manager Enclosures Q _Kok r REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 20 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 Project: SURRY BLANKS Pace Project No.: 92252475 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 20 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 SAMPLE SUMMARY Project: SURRY BLANKS Pace Project No.: 92252475 Lab ID Sample ID Matrix Date Collected Date Received 92252475001 EB Water 05/29/1517:55 06/02/1516:30 92252475002 FB Water 05/29/1518:00 06/02/1516:30 92252475003 TB Water 05/29/15 00:00 06/02/15 16:30 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 20 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: SURRY BLANKS 92252475 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92252475001 EB EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C 92252475002 FB EPA 6010 JMW 15 PASI-A EPA 8260 GAW 51 PASI-C 92252475003 TB EPA 8260 GAW 51 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 20 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY BLANKS Pace Project No.: 92252475 Sample: EB Lab ID: 92252475001 Collected: 05/29/15 17:55 Received: 06/02/15 16:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 3.8 1 06/03/1517:15 06/04/1518:28 7440-36-0 Arsenic ND ug/L 10.0 2.5 1 06/03/1517:15 06/04/1518:28 7440-38-2 Barium ND ug/L 100 2.5 1 06/03/1517:15 06/04/1518:28 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 06/03/1517:15 06/04/1518:28 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 06/03/1517:15 06/04/1518:28 7440-43-9 Chromium ND ug/L 10.0 2.5 1 06/03/1517:15 06/04/1518:28 7440-47-3 Cobalt ND ug/L 10.0 2.5 1 06/03/1517:15 06/04/1518:28 7440-48-4 Copper ND ug/L 10.0 2.5 1 06/03/1517:15 06/04/1518:28 7440-50-8 Lead ND ug/L 10.0 2.5 1 06/03/1517:15 06/04/1518:28 7439-92-1 Nickel ND ug/L 50.0 2.5 1 06/03/1517:15 06/04/1518:28 7440-02-0 Selenium ND ug/L 10.0 5.0 1 06/03/1517:15 06/04/1518:28 7782-49-2 Silver ND ug/L 10.0 2.5 1 06/03/1517:15 06/04/1518:28 7440-22-4 Thallium ND ug/L 5.5 5.0 1 06/03/1517:15 06/04/1518:28 7440-28-0 Vanadium ND ug/L 25.0 2.5 1 06/03/1517:15 06/04/1518:28 7440-62-2 Zinc ND ug/L 10.0 5.0 1 06/03/1517:15 06/04/1518:28 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 06/12/15 16:47 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 06/12/15 16:47 107-13-1 Benzene ND ug/L 1.0 0.25 1 06/12/15 16:47 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 06/12/15 16:47 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 06/12/15 16:47 75-27-4 Bromoform ND ug/L 3.0 0.26 1 06/12/15 16:47 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 06/12/15 16:47 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 06/12/15 16:47 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 06/12/15 16:47 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 06/12/15 16:47 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 06/12/15 16:47 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 06/12/15 16:47 75-00-3 Chloroform ND ug/L 5.0 0.14 1 06/12/15 16:47 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 06/12/15 16:47 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 06/12/15 16:47 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 06/12/15 16:47 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 06/12/15 16:47 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 06/12/15 16:47 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 06/12/15 16:47 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 06/12/15 16:47 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/12/15 16:47 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 06/12/15 16:47 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 06/12/15 16:47 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/12/15 16:47 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 06/12/15 16:47 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/12/15 16:47 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 06/12/15 16:47 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 06/12/15 16:47 142-28-9 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/12/15 16:47 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/15/2015 02:46 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 20 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY BLANKS Pace Project No.: 92252475 Sample: EB Lab ID: 92252475001 Collected: 05/29/15 17:55 Received: 06/02/15 16:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/12/15 16:47 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/12/15 16:47 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/12/15 16:47 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/12/15 16:47 74-88-4 Methylene Chloride 61.2 ug/L 1.0 0.97 1 06/12/15 16:47 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/12/15 16:47 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/12/15 16:47 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/12/15 16:47 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/12/15 16:47 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/12/15 16:47 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/12/15 16:47 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/12/15 16:47 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/12/15 16:47 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/12/15 16:47 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/12/15 16:47 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/12/15 16:47 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/12/15 16:47 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/12/15 16:47 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/12/15 16:47 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 92 % 70-130 1 06/12/15 16:47 460-00-4 1,2-Dichloroethane-d4 (S) 93 % 70-130 1 06/12/15 16:47 17060-07-0 Toluene-d8 (S) 99 % 70-130 1 06/12/15 16:47 2037-26-5 Date: 06/15/2015 02:46 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 20 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY BLANKS Pace Project No.: 92252475 Sample: FB Lab ID: 92252475002 Collected: 05/29/15 18:00 Received: 06/02/15 16:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 3.8 1 06/03/1517:15 06/04/1518:31 7440-36-0 Arsenic ND ug/L 10.0 2.5 1 06/03/1517:15 06/04/1518:31 7440-38-2 Barium ND ug/L 100 2.5 1 06/03/1517:15 06/04/1518:31 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 06/03/1517:15 06/04/1518:31 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 06/03/1517:15 06/04/1518:31 7440-43-9 Chromium ND ug/L 10.0 2.5 1 06/03/1517:15 06/04/1518:31 7440-47-3 Cobalt ND ug/L 10.0 2.5 1 06/03/1517:15 06/04/1518:31 7440-48-4 Copper ND ug/L 10.0 2.5 1 06/03/1517:15 06/04/1518:31 7440-50-8 Lead ND ug/L 10.0 2.5 1 06/03/1517:15 06/04/1518:31 7439-92-1 Nickel ND ug/L 50.0 2.5 1 06/03/1517:15 06/04/1518:31 7440-02-0 Selenium ND ug/L 10.0 5.0 1 06/03/1517:15 06/04/1518:31 7782-49-2 Silver ND ug/L 10.0 2.5 1 06/03/1517:15 06/04/1518:31 7440-22-4 Thallium ND ug/L 5.5 5.0 1 06/03/1517:15 06/04/1518:31 7440-28-0 Vanadium ND ug/L 25.0 2.5 1 06/03/1517:15 06/04/1518:31 7440-62-2 Zinc ND ug/L 10.0 5.0 1 06/03/1517:15 06/04/1518:31 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 06/12/15 17:03 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 06/12/15 17:03 107-13-1 Benzene ND ug/L 1.0 0.25 1 06/12/15 17:03 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 06/12/15 17:03 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 06/12/15 17:03 75-27-4 Bromoform ND ug/L 3.0 0.26 1 06/12/15 17:03 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 06/12/15 17:03 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 06/12/15 17:03 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 06/12/15 17:03 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 06/12/15 17:03 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 06/12/15 17:03 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 06/12/15 17:03 75-00-3 Chloroform ND ug/L 5.0 0.14 1 06/12/15 17:03 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 06/12/15 17:03 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 06/12/15 17:03 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 06/12/15 17:03 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 06/12/15 17:03 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 06/12/15 17:03 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 06/12/15 17:03 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 06/12/15 17:03 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/12/15 17:03 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 06/12/15 17:03 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 06/12/15 17:03 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/12/15 17:03 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 06/12/15 17:03 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/12/15 17:03 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 06/12/15 17:03 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 06/12/15 17:03 142-28-9 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/12/15 17:03 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/15/2015 02:46 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 20 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY BLANKS Pace Project No.: 92252475 Sample: FB Lab ID: 92252475002 Collected: 05/29/15 18:00 Received: 06/02/15 16:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/12/15 17:03 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/12/15 17:03 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/12/15 17:03 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/12/15 17:03 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/12/15 17:03 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/12/15 17:03 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/12/15 17:03 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/12/15 17:03 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/12/15 17:03 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/12/15 17:03 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/12/15 17:03 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/12/15 17:03 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/12/15 17:03 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/12/15 17:03 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/12/15 17:03 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/12/15 17:03 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/12/15 17:03 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/12/15 17:03 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/12/15 17:03 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 90 % 70-130 1 06/12/15 17:03 460-00-4 1,2-Dichloroethane-d4 (S) 87 % 70-130 1 06/12/15 17:03 17060-07-0 Toluene-d8 (S) 99 % 70-130 1 06/12/15 17:03 2037-26-5 Date: 06/15/2015 02:46 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 8 of 20 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY BLANKS Pace Project No.: 92252475 Sample: TB Lab ID: 92252475003 Collected: 05/29/15 00:00 Received: 06/02/15 16:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 06/12/15 17:19 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 06/12/15 17:19 107-13-1 Benzene ND ug/L 1.0 0.25 1 06/12/15 17:19 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 06/12/15 17:19 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 06/12/15 17:19 75-27-4 Bromoform ND ug/L 3.0 0.26 1 06/12/15 17:19 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 06/12/15 17:19 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 06/12/15 17:19 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 06/12/15 17:19 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 06/12/15 17:19 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 06/12/15 17:19 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 06/12/15 17:19 75-00-3 Chloroform ND ug/L 5.0 0.14 1 06/12/15 17:19 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 06/12/15 17:19 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 06/12/15 17:19 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 06/12/15 17:19 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 06/12/15 17:19 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 06/12/15 17:19 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 06/12/15 17:19 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 06/12/15 17:19 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/12/15 17:19 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 06/12/15 17:19 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 06/12/15 17:19 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/12/15 17:19 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 06/12/15 17:19 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/12/15 17:19 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 06/12/15 17:19 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 06/12/15 17:19 142-28-9 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/12/15 17:19 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/12/15 17:19 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/12/15 17:19 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/12/15 17:19 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/12/15 17:19 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/12/15 17:19 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/12/15 17:19 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/12/15 17:19 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/12/15 17:19 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/12/15 17:19 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/12/15 17:19 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/12/15 17:19 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/12/15 17:19 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/12/15 17:19 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/12/15 17:19 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/12/15 17:19 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/12/15 17:19 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/12/15 17:19 108-05-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/15/2015 02:46 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 20 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY BLANKS Pace Project No.: 92252475 Sample: TB Lab ID: 92252475003 Collected: 05/29/15 00:00 Received: 06/02/15 16:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Vinyl chloride ND ug/L 1.0 0.62 1 06/12/15 17:19 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/12/15 17:19 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 89 % 70-130 1 06/12/15 17:19 460-00-4 1,2-Dichloroethane-d4 (S) 87 % 70-130 1 06/12/15 17:19 17060-07-0 Toluene-d8 (S) 97 % 70-130 1 06/12/15 17:19 2037-26-5 Date: 06/15/2015 02:46 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 20 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BLANKS Pace Project No.: 92252475 QC Batch: MPRP/18607 Analysis Method: EPA6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET NC Groundwater Associated Lab Samples: 92252475001, 92252475002 METHOD BLANK: 1474278 Associated Lab Samples: 92252475001, 92252475002 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed Antimony ug/L ND 6.0 06/04/1517:08 Arsenic ug/L ND 10.0 06/04/1517:08 Barium ug/L ND 100 06/04/1517:08 Beryllium ug/L ND 1.0 06/04/1517:08 Cadmium ug/L ND 1.0 06/04/1517:08 Chromium ug/L ND 10.0 06/04/1517:08 Cobalt ug/L ND 10.0 06/04/1517:08 Copper ug/L ND 10.0 06/04/1517:08 Lead ug/L ND 10.0 06/04/1517:08 Nickel ug/L ND 50.0 06/04/1517:08 Selenium ug/L ND 10.0 06/04/1517:08 Silver ug/L ND 10.0 06/04/1517:08 Thallium ug/L ND 5.5 06/04/1517:08 Vanadium ug/L ND 25.0 06/04/1517:08 Zinc ug/L ND 10.0 06/04/1517:08 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 1474279 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 500 479 96 80-120 Arsenic ug/L 500 456 91 80-120 Barium ug/L 500 448 90 80-120 Beryllium ug/L 500 450 90 80-120 Cadmium ug/L 500 454 91 80-120 Chromium ug/L 500 440 88 80-120 Cobalt ug/L 500 451 90 80-120 Copper ug/L 500 440 88 80-120 Lead ug/L 500 447 89 80-120 Nickel ug/L 500 451 90 80-120 Selenium ug/L 500 432 86 80-120 Silver ug/L 250 224 90 80-120 Thallium ug/L 500 460 92 80-120 Vanadium ug/L 500 435 87 80-120 Zinc ug/L 500 449 90 80-120 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/15/2015 02:46 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 20 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: SURRY BLANKS 92252475 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1474280 1474281 MS MSD 92251954001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 478 483 95 96 75-125 1 25 Arsenic ug/L ND 500 500 458 461 91 92 75-125 1 25 Barium ug/L 48.4 500 500 498 504 90 91 75-125 1 25 Beryllium ug/L ND 500 500 456 461 91 92 75-125 1 25 Cadmium ug/L ND 500 500 453 458 91 92 75-125 1 25 Chromium ug/L ND 500 500 443 447 89 89 75-125 1 25 Cobalt ug/L ND 500 500 446 450 89 90 75-125 1 25 Copper ug/L 11.6 500 500 450 454 88 89 75-125 1 25 Lead ug/L ND 500 500 441 447 88 89 75-125 1 25 Nickel ug/L 2.7J 500 500 448 452 89 90 75-125 1 25 Selenium ug/L ND 500 500 429 431 85 86 75-125 0 25 Silver ug/L ND 250 250 223 225 89 90 75-125 1 25 Thallium ug/L ND 500 500 451 456 90 91 75-125 1 25 Vanadium ug/L ND 500 500 438 445 87 89 75-125 2 25 Zinc ug/L 28.6 500 500 473 477 89 90 75-125 1 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/15/2015 02:46 PM without the written consent of Pace Analytical Services, Inc.. Page 12 of 20 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BLANKS Pace Project No.: 92252475 QC Batch: MSV/32119 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92252475001, 92252475002, 92252475003 METHOD BLANK: 1484008 Matrix: Associated Lab Samples: 92252475001, 92252475002, 92252475003 Blank Parameter Units Result Water Reporting Limit Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/12/15 14:41 1,1,1-Trichloroethane ug/L ND 1.0 06/12/15 14:41 1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/12/15 14:41 1,1,2-Trichloroethane ug/L ND 1.0 06/12/15 14:41 1,1-Dichloroethane ug/L ND 5.0 06/12/15 14:41 1,1-Dichloroethene ug/L ND 5.0 06/12/15 14:41 1,2,3-Trichloropropane ug/L ND 1.0 06/12/15 14:41 1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/12/15 14:41 1,2-Dibromoethane (EDB) ug/L ND 1.0 06/12/15 14:41 1,2-Dichlorobenzene ug/L ND 5.0 06/12/15 14:41 1,2-Dichloroethane ug/L ND 1.0 06/12/15 14:41 1,2-Dichloropropane ug/L ND 1.0 06/12/15 14:41 1,3-Dichloropropane ug/L ND 1.0 06/12/15 14:41 1,4-Dichlorobenzene ug/L ND 1.0 06/12/15 14:41 2-Butanone (MEK) ug/L ND 100 06/12/15 14:41 2-Hexanone ug/L ND 50.0 06/12/15 14:41 4-Methyl-2-pentanone (MIBK) ug/L ND 100 06/12/15 14:41 Acetone ug/L ND 100 06/12/15 14:41 Acrylonitrile ug/L ND 200 06/12/15 14:41 Benzene ug/L ND 1.0 06/12/15 14:41 Bromochloromethane ug/L ND 3.0 06/12/15 14:41 Bromodichloromethane ug/L ND 1.0 06/12/15 14:41 Bromoform ug/L ND 3.0 06/12/15 14:41 Bromomethane ug/L ND 10.0 06/12/15 14:41 Carbon disulfide ug/L ND 100 06/12/15 14:41 Carbon tetrachloride ug/L ND 1.0 06/12/15 14:41 Chlorobenzene ug/L ND 3.0 06/12/15 14:41 Chloroethane ug/L ND 10.0 06/12/15 14:41 Chloroform ug/L ND 5.0 06/12/15 14:41 Chloromethane ug/L ND 1.0 06/12/15 14:41 cis-1,2-Dichloroethene ug/L ND 5.0 06/12/15 14:41 cis-1,3-Dichloropropene ug/L ND 1.0 06/12/15 14:41 Dibromochloromethane ug/L ND 3.0 06/12/15 14:41 Dibromomethane ug/L ND 10.0 06/12/15 14:41 Ethylbenzene ug/L ND 1.0 06/12/15 14:41 lodomethane ug/L ND 10.0 06/12/15 14:41 Methylene Chloride ug/L ND 1.0 06/12/15 14:41 Styrene ug/L ND 1.0 06/12/15 14:41 Tetrachloroethene ug/L ND 1.0 06/12/15 14:41 Toluene ug/L ND 1.0 06/12/15 14:41 trans-1,2-Dichloroethene ug/L ND 5.0 06/12/15 14:41 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/15/2015 02:46 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 20 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BLANKS Pace Project No.: 92252475 METHOD BLANK: 1484008 Matrix: Associated Lab Samples: 92252475001, 92252475002, 92252475003 Blank Parameter Units Result Water Reporting Limit Analyzed trans- 1,3-Dichloropropene ug/L ND 1.0 06/12/15 14:41 trans-1,4-Dichloro-2-butene ug/L ND 100 06/12/15 14:41 Trichloroethene ug/L ND 1.0 06/12/15 14:41 Trichlorofluoromethane ug/L ND 1.0 06/12/15 14:41 Vinyl acetate ug/L ND 50.0 06/12/15 14:41 Vinyl chloride ug/L ND 1.0 06/12/15 14:41 Xylene (Total) ug/L ND 5.0 06/12/15 14:41 1,2-Dichloroethane-d4 (S) % 91 70-130 06/12/15 14:41 4-Bromofluorobenzene (S) % 91 70-130 06/12/15 14:41 Toluene-d8 (S) % 98 70-130 06/12/15 14:41 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 1484009 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 54.8 110 80-125 1,1,1-Trichloroethane ug/L 50 61.0 122 71-129 1,1,2,2-Tetrachloroethane ug/L 50 53.7 107 79-124 1,1,2-Trichloroethane ug/L 50 53.2 106 85-125 1,1-Dichloroethane ug/L 50 57.4 115 73-126 1,1-Dichloroethene ug/L 50 57.0 114 66-135 1,2,3-Trichloropropane ug/L 50 52.3 105 75-130 1,2-Dibromo-3-chloropropane ug/L 50 51.5 103 71-133 1,2-Dibromoethane (EDB) ug/L 50 55.1 110 83-124 1,2-Dichlorobenzene ug/L 50 54.4 109 80-133 1,2-Dichloroethane ug/L 50 54.6 109 67-128 1,2-Dichloropropane ug/L 50 55.8 112 75-132 1,3-Dichloropropane ug/L 50 54.3 109 76-131 1,4-Dichlorobenzene ug/L 50 54.1 108 78-130 2-Butanone (MEK) ug/L 100 113 113 61-144 2-Hexanone ug/L 100 100 100 68-143 4-Methyl-2-pentanone (MIBK) ug/L 100 103 103 72-135 Acetone ug/L 100 115 115 48-146 Acrylonitrile ug/L 250 291 116 40-160 Benzene ug/L 50 56.9 114 80-125 Bromochloromethane ug/L 50 60.6 121 71-125 Bromodichloromethane ug/L 50 51.1 102 78-124 Bromoform ug/L 50 49.6 99 71-128 Bromomethane ug/L 50 54.1 108 40-160 Carbon disulfide ug/L 50 53.6J 107 50-160 Carbon tetrachloride ug/L 50 58.5 117 69-131 Chlorobenzene ug/L 50 54.3 109 81-122 Chloroethane ug/L 50 45.6 91 39-148 Chloroform ug/L 50 52.3 105 73-127 Chloromethane ug/L 50 51.2 102 44-146 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/15/2015 02:46 PM without the written consent of Pace Analytical Services, Inc.. Page 14 of 20 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BLANKS Pace Project No.: 92252475 LABORATORY CONTROL SAMPLE: Parameter 1484009 Units Spike Conc. LCS Result LCS % Rec % Rec Limits cis-1,2-Dichloroethene ug/L 50 61.5 123 74-124 cis-1,3-Dichloropropene ug/L 50 54.9 110 72-132 Dibromochloromethane ug/L 50 48.3 97 78-125 Dibromomethane ug/L 50 53.5 107 82-120 Ethylbenzene ug/L 50 53.6 107 79-121 lodomethane ug/L 100 104 104 39-154 Methylene Chloride ug/L 50 63.2 126 64-133 Styrene ug/L 50 55.2 110 84-126 Tetrachloroethene ug/L 50 55.2 110 78-122 Toluene ug/L 50 54.4 109 80-121 trans-1,2-Dichloroethene ug/L 50 58.6 117 71-127 trans- 1,3-Dichloropropene ug/L 50 55.6 111 69-141 trans-1,4-Dichloro-2-butene ug/L 50 55.1J 110 40-160 Trichloroethene ug/L 50 53.3 107 78-122 Trichlorofluoromethane ug/L 50 49.2 98 53-137 Vinyl acetate ug/L 100 110 110 40-160 Vinyl chloride ug/L 50 55.2 110 58-137 Xylene (Total) ug/L 150 160 107 81-126 1,2-Dichloroethane-d4 (S) % 108 70-130 4-Bromofluorobenzene (S) % 95 70-130 Toluene-d8(S) % 101 70-130 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1484010 MS 92252725003 Spike Parameter Units Result Conc. MSD Spike Conc. 1484011 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits Max RPD RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 21.4 23.0 107 115 70-130 7 30 1,1,1-Trichloroethane ug/L ND 20 20 23.9 26.1 119 131 70-130 9 30 M1 1,1,2,2-Tetrachloroethane ug/L ND 20 20 19.9 20.8 100 104 70-130 4 30 1,1,2-Trichloroethane ug/L ND 20 20 21.8 22.7 109 114 70-130 4 30 1,1-Dichloroethane ug/L 0.40J 20 20 23.6 24.4 116 120 70-130 4 30 1,1-Dichloroethene ug/L ND 20 20 25.8 27.0 129 135 70-166 4 30 1,2,3-Trichloropropane ug/L ND 20 20 21.2 21.3 106 106 70-130 0 30 1,2-Dibromo-3- ug/L ND 20 20 18.4 20.5 92 102 70-130 10 30 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 20 20 22.5 23.8 113 119 70-130 6 30 1,2-Dichlorobenzene ug/L ND 20 20 23.1 23.7 115 118 70-130 3 30 1,2-Dichloroethane ug/L 0.80J 20 20 20.1 20.8 96 100 70-130 3 30 1,2-Dichloropropane ug/L 0.74J 20 20 24.8 25.3 120 123 70-130 2 30 1,3-Dichloropropane ug/L ND 20 20 21.8 23.0 109 115 70-130 5 30 1,4-Dichlorobenzene ug/L 3.1 20 20 26.6 26.7 117 118 70-130 0 30 2-Butanone (MEK) ug/L ND 40 40 38.OJ 40AJ 95 101 70-130 6 30 2-Hexanone ug/L ND 40 40 40.2J 43.OJ 101 107 70-130 7 30 4-Methyl-2-pentanone ug/L ND 40 40 39.9J 43.1J 100 108 70-130 8 30 (MIBK) Acetone ug/L ND 40 40 41.6J 44.8J 95 103 70-130 7 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result Date: 06/15/2015 02:46 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 15 of 20 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BLANKS Pace Project No.: 92252475 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1484010 1484011 MS MSD 92252725003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Acrylonitrile ug/L ND 100 100 1091 114J 108 113 70-130 5 30 Benzene ug/L 0.83J 20 20 25.1 26.8 121 130 70-148 7 30 Bromochloromethane ug/L ND 20 20 25.0 26.2 125 131 70-130 5 30 M1 Bromodichloromethane ug/L ND 20 20 20.9 21.0 104 105 70-130 1 30 Bromoform ug/L ND 20 20 17.7 18.8 89 94 70-130 6 30 Bromomethane ug/L ND 20 20 24.4 21.9 122 109 70-130 11 30 Carbon disulfide ug/L ND 20 20 25.7J 25.2J 128 126 70-130 2 30 Carbon tetrachloride ug/L ND 20 20 24.9 26.1 125 130 70-130 5 30 Chlorobenzene ug/L 2.9 20 20 26.3 27.2 117 121 70-146 3 30 Chloroethane ug/L ND 20 20 26.2 27.5 131 138 70-130 5 30 M1 Chloroform ug/L ND 20 20 21.3 22.2 106 111 70-130 4 30 Chloromethane ug/L 0.22J 20 20 22.3 23.1 110 115 70-130 4 30 cis-1,2-Dichloroethene ug/L 5.6 20 20 29.4 31.4 119 129 70-130 7 30 cis-1,3-Dichloropropene ug/L ND 20 20 23.3 24.2 117 121 70-130 4 30 Dibromochloromethane ug/L ND 20 20 18.5 19.6 93 98 70-130 6 30 Dibromomethane ug/L ND 20 20 22.5 22.7 112 114 70-130 1 30 Ethylbenzene ug/L ND 20 20 22.3 23.4 112 117 70-130 5 30 lodomethane ug/L ND 40 40 33.7 42.2 84 105 70-130 22 30 Methylene Chloride ug/L ND 20 20 20.6 21.7 103 109 70-130 5 30 Styrene ug/L ND 20 20 23.1 23.6 116 118 70-130 2 30 Tetrachloroethene ug/L ND 20 20 24.6 25.8 123 129 70-130 5 30 Toluene ug/L ND 20 20 23.1 23.7 115 119 70-155 3 30 trans-1,2-Dichloroethene ug/L ND 20 20 23.6 24.6 118 123 70-130 4 30 trans-1,3-Dichloropropene ug/L ND 20 20 20.9 22.1 105 110 70-130 5 30 trans-1,4-Dichloro-2-butene ug/L ND 20 20 19.6J 20.3J 98 102 70-130 4 30 Trichloroethene ug/L ND 20 20 24.9 26.1 123 129 69-151 5 30 Trichlorofluoromethane ug/L ND 20 20 24.5 24.9 122 124 70-130 2 30 Vinyl acetate ug/L ND 40 40 36.6J 37.5J 92 94 70-130 2 30 Vinyl chloride ug/L 1.2 20 20 27.4 29.0 131 139 70-130 6 30 M1 1,2-Dichloroethane-d4 (S) % 89 96 70-130 4-Bromofluorobenzene (S) % 93 93 70-130 Toluene-d8 (S) % 98 98 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/15/2015 02:46 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 20 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALIFIERS Project: SURRY BLANKS Pace Project No.: 92252475 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/15/2015 02:46 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 20 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: SURRY BLANKS Pace Project No.: 92252475 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92252475001 EB EPA3010 MPRP/18607 EPA6010 ICP/16689 92252475002 FB EPA 3010 MPRP/18607 EPA 6010 ICP/16689 92252475001 EB EPA 8260 MSV/32119 92252475002 FB EPA 8260 MSV/32119 92252475003 TB EPA 8260 MSV/32119 Date: 06/15/2015 02:46 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 18 of 20 ��'Iceklalyfical' LJVI+UIIICIIL IVGIIIC: Condition Upon Recei Document Number: F-CHR-CS-003-rev.16 uucuinent mervlsuu. May Io, cU is Page 1 of 2* Issuing Authority: Pace Huntersville Qualitv Office Client Name: Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Client❑ Commercial Pace Other_ Custody Seal on Cooler/Box Present: ❑ yes ❑ /o Seals intact; ❑ yes * Page 2 of 2 is for Internal Use Only ❑ no Packing Material: ❑ Bubble V❑p ❑ Bubble Bags E/i None Other Thermometer Used: IR Gun T1401 Type of fee: Blue None ❑ 5popies on ice, cooling process has begun Temp Correction Factor T1401 No Correction Corrected Cooler Temp.: a •C Biological Tissue is Frozen: Yes No NIA Date and Initial Qf, e s n x r fining contents: � Temp should be above freezing to 6°C Comments: Chain of Custody Present: " Yes ❑No ❑NIA 1. Chain of Custody Filled Out: p es ❑No ❑NIA 2, Chain of Custody Relinquished: r! El No El NIA 3. Sampler Name & Signature on COC: Yes ❑No DNIA 4, Samples Arrived within Hold Time: Yes ❑No DNIA 5. Short Hold Time Analysis (<72hr): Dyes PNo ❑NIA 6. Rush Turn Around Time Requested: Dyes dNo ❑NIA 7. Sufficient Volume: M res ❑No ❑NIA 8. Correct Containers Used: ❑Yes El No ❑NIA 9, -Pace Containers Used: Qies ❑No ❑NIA Containers Intact: Yes ❑No 0 !A 10. Filtered volume received for Dissolved tests Yes ❑No F El NIA 11. Sample Labels match COC: MYes 0 No El NIA 12.�� -Includes dateltime/iD/Analysis Matrix: All containers needing preservation have been checked. 0 es ONO ❑NIA 13. All containers needing preservation are found to be in ❑❑No ❑NIA compliance with EPA recommendation. exceptions: VOA, coliform, TOC, O&G, WI-DRO (water) Dyes ❑No Samples checked for dechlorination: Dyes ❑No.. LJNiA 14. Headspace in VOA Vials ( >6mm): ❑Yes ONo P2 1K 15. Trip Blank Present: Dyes ❑No ❑WA 16. Trip Blank Custody Seals Present ❑Yes ❑No ❑NIA Pace Trip Blank Lot # (if purchased): Client Notification) Resolution: Field Data Required? Y / N Person Contacted: Oate/Time: Comments/ Resolution: SCURF Review: . 1' r i j') Date: SRF Review: �{i� �� Dater �l.S Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( 1.e out of hold, incorrect preservative, out of temp, incorrect containers) WO#�92252475 1111111111111111111111 92262475 Page 19 of 20 aCe.4n3fytica! Section A Required Client Information: Company: Municipal En Address: P.O. Box 97 Gamer, NC 27529 Email To: jpfoh�mesco Phone: 919-772-5393 Requested Due Date[TAT: 10 LU LU 2 3 4 5 6 7 8 9 10 11 12 Section B Required Project Information: Project iD: Slurry ner Order Number: O N O O N CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. IL Section C Invoice Information: Pa E ' t Of 1 Quote Reference: Project Manager: Kevin Gal Profile #: I Requested Analysis Filtered Z — a COLLECTED Preservatives N N MA7RIR CODE g ZE D-k.ng Water DW U Watcr wr Wocly Water WW s U C U SAMPLE ID R = m a S°msaud a START END O N One Character per box. oilOL F ne Sample Ids must be unique other OT o a i T$U. TS 0 X O a 0 c t6 Q H .J Ei!m i on t `m w DATE TWE DATE TIME N s � z 2 z z i7 wr G I S:s,' "A 4 wT I G I 64Z ?,�V 4 T ADDITIONAL COMMENTS SYIAFFILIATION DATE TIME ACCEPTED BY 1 AFFILIATION Gc- DATE TIME State ! Location North Carolina SAMPLE CONDITIONS SAMPLER NAME AND SIGNATURE m o 2 c PRINT Name of SAMPLER: JpRathin Efohl 8_ SIGNATURE of SAMPLER: I DATE Signed: Z $ — o E Appendix B Field Sampling Parameter Data Sheet(s) Field Sampling Data Sheet Project: Surry Co Closed C&D and Closed MSWLF-Mt. Ai Samplers: J_ Pfohl Page_1_of 1 Sampling Parameters Water Quality Parameters (Stabilized) Monitoring Point Sample Date Sample Time Depth to Water (STOP) Static Lab Parameters to be analyzed for Volume Purged (Gal) Sample Type Goes Dry During Purge Total Depth Measured as expected Total Depth Expected CO2 (mg/0 DO (mg/L) iORP pH Temp. © Specific Cond. (us/cm TDS (m9/L) 3 ~ CH4 Gas Vapors M_W-1 UIC 40 Q,, IW-2 , ��! WLR & T - - - 68.08 MW-3R UIC 100 IW-3 WLR & T - - - 52 IW-4J.LZ WLR & T - - - 57 IW-5 �J�F I WLR&T - - - 5 64 MW-6 x�.l AM ln, �4 31v MW-7 k UIC 25 IW-6 _ WLR & T - - - 56 MW-93,5 UIC�� z� y 46 MW-11 AM --- 40 -o v7_ MW-12D rt..: AM "� ,. ',1-00 - 7. 0 v ,s IMW-12S a UIC r `1. v 51 MW-13 " UIC 35.78 - =,; ri f' MW-14 UIC 48.03 - a MW-15 - UIC i 56.98 MW-16 UIC �� ; a .i, 1-!`e- dk�� x e��t 36.28 - - MW-17 UIC(3�zt��E'.,- 15.32 MW-18 UIC _� '� 1 I 18.15 - t �,t , I '- MW-19 UIC ��,� y,w 17.1 - MW-20G UIC L Y 25.64 MW-21 UIC, 15.41 MW-22 UIC (�', �' 16.04 - 3,9 °t . MW-23 UIC P,l _ 17.1 SCALEHOU E AM '� a=i` >' _� 222 SS B=Stainless Steel Baler, D B=Disposable Baler, P=Low flow Pump, PD=Purged Dry VT=Very Turbid, MT=Moderately Turbid, ST=Slightly Turbid, C=Clear NR=No Reading Attempted, NS=No Sample Obtained r `'� Field Sampling Data Sheet 2 <_ M Ncinal Project: Surry Co Closed C&D over Closed MSWLF & Active Subtitle D Lined- Mt. Airy (Shared Surface Waters) Samplers: J. Pfohl Page _1_of 1 Sampling Parameters Water Quality Parameters (Stabilized) Monitoring Point Sample Date Sample Time Visual Flow Rate Lab Parameters to be analyzed forPurge Visual Guage Ht. Sample p Type Goes Dr y During Total Depth Measured as expected Comments ,\ ` Q°F pH Temp- ©p' Specific Cond. ( us/cm TDS m /L ( g ) -6 ~ CH4 Gas Vapors p (ppm) SW-1 s- Z ' f :I b :.,I I s , ° - - l ,` ` tJ s, - SW-2 SW-4a- 4 I , SWN-1 �3,L's- SWN-2 't' I ? - - ; ,' r"_j `E - SWN-3- SWN-4 rq- SW-A Downstream r 4 X SW-B I G Downstream MW-6Rt�,� L SS B=Stainless Steel Baler, D B=Disposable Baler, P=Low flow Pump, PD=Purged Dry VT=Very Turbid, MT=Moderately Turbid, ST=Slightly Turbid, C=Clear NR=No Reading Attempted, NS=No Sample Obtained Appendix C Boring Log of B-11R Well Abandonment Record for B-11R LOG OF BORING: B-11 R (Planned MW-11 R) Surry Co. Closed MSWLF (AOC MW-11) Project No. G14120.6 Drilling contractor: Bluestone Date started: 1/26/2015 Surface elevation: 1157 (aprx.) Drill rig & method: 6" OD DTH no SPT Date ended: 1/26/2015 Top of pipe elevation: na Logged by: J Pfohl Completion depth: 55.00 ft Depth to water (TOB): Dry>55' Stickup height: N/A Depth to water (24hrs): Dry�:55' a o a co a o E — > U) E Cz Description of Material & Remarks Well Diagram U) m m 0 5 10 15 20 25 30 35 40 45 50 55 Planned to be MW-11 R to delineate contamination detected in MW-11 which is located �110 feet south and downgradient. SAPROLITE; Silty Sand, Reddish Brown, moderately dense, dry. ----------------------------------------------------- WEATHERED ROCK; Slightly weathered gray rock, dry. BEDROCK; Very dense gray competent rock, no fractures noticed, dry. Boring remained dry >48 hrs. so was abandoned per 2C Rules on 1 /29/15. U U 0 0 a 2 C7 0 0 c m L 0 7 7---------------------------------------------------- Boring terminated at 55.0 feet Municipal Engineering Services Company, P.A. Operation/Construction Managers Civil/Sanitary Engineers Environmental Studies Page 1 of 1 PO Box 97, Garner, North Carolina 27529 (919) 772-5393PO Box 349, Boone, North Carolina 28607 (828) 262-1767 WELL ABANDONMENT RECORD This form can be used for single or multiple wells 1. Well Contractor Information: John Thompson Well Contractor Name (or well owner personally abandoning well on his/her property) 3579-A NC Well Contractor Certification Number Bluestone Environmental, LLC Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, Injection, etc,) iflmown 3. Well use (check well use): []Agricultural ❑Geothermal (Heating/Cooling Supply) ❑ Industrial/Com mere is I ❑Municipal/Public ❑Residential Water Supply (single) ❑Residential Water Supply (shared) Non -Water Supply Well: IDNIonitorine Dry boring planned to be MW ❑Recovery ❑Aquifer Recharge ❑Aquifer Storage and Recovery ❑Aquifer Test ❑Experimental Technology ❑Geothermal (Closed Loop) ❑Geothermal (Heating/Cooling 4. Date well(s) abandoned: 1 /29/15 ❑Groundwater Remediation ❑Salinity Barrier ❑Stormwater Drainage ❑Subsidence Control ❑Tracer ❑Other (explain under 7g) 5a. Well location: Surry Co. Closed MSWLF Facility/Owner Name Facility ID# (if applicable) 237 Landfill Rd. Mount Airy, NC 27030 Physical Address, City, and Zip Surry County 593700691273 Parcel Identification No. (PIN) 5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) 36.441742 N 80.569848 rttoN LY: WELL ABANDONMENT DETAILS 7a. Number of wells being abandoned: 1 For multiple injection or non-waler supply wells ONLY with the same construction✓abandonment, you can submit one form. 7b. Approximate volume of water remaining in well(s): 2 dry (gal.) FOR WATER SUPPLY WELLS ONLY: 7c. Type of disinfectant used: 7d, Amount of disinfectant used: 7e. Sealing materials used (check all that apply): ❑ Neat Cement Grout ❑ Bentonite Chips or Pellets ❑ Sand Cement Grout ❑ Dry Clay 0 Concrete Grout ❑ Drill Cuttings ❑ Specialty Grout ❑ Gravel 171 Bentonite Slurry ❑ Other (explain under 7g) 7f, For each material selected above, provide amount of materials used: Bentonite Slurry (3-55') 150 Ibs bent. with 65 gal. water Concrete (0-3) 80 Ibs concrete with 3/4 gal. water 7g. Provide a brief description of the abandonment procedure: Intended to be monitoring well MW-11 R but open boring dry >48 hrs. Tremie grouted bentonite slurry from 55' - 3' BGS. No settlement -12 hrs. Concrete slurry gravity from 0-3'. 8. Certification: ,� _ 2/15/15 ign ue of ertifi,qAKVeII contractor or Well Owner Date By signing this fornn, 1 hereby certify that the tmell(s) was (were) abandoned in accordance with 1 SA NCAC 02C .0100 or 2C.0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 9. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well W abandonment details. You may also attach additional pages if necessary. CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED SUBMITTAL INSTRUCTIONS Attach well construction record(s) ifavailoble. For multiple injection or non-waler supply ,veils ONLY,vah the sane constructionlabandonnuml, you can submit one fbrm'. 10a For All Wells: Submit this form within 30 days of completion of well 6a. Well ID#: B-11 R (planned MW-11 R) 6b. Total well depth: Boring 55 (ft.) 6c. Borehole diameter: 6 (in.) 6d. Water level below ground surface: Dry (ft.) abandonment to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 lob. For Iniection Wells: In addition to sending the form to the address in 10a above, also submit one copy of this form within 30 days of completion of well abandonment to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 None Installed 10e. For Water Supply & Iniection Wells: In addition to sending the form to 6e. Outer casing length (if known): (ft.) the address(es) above, also submit one copy of this form within 30 days of completion of well abandonment to the county health department of the county 6f. Inner casing/tubing length (if known): None installed (ft.) where abandoned. 6g. Screen length (if known): None Installed (ft.) Form GW-30 North Carolina Department of Environment and Natural Resources — Division ofWater Resources Revised August 2013