WI0400176_Monitoring (Report)_20141201

Rogers, Michael
From: Jonathan Pfohl [e-mail]
Sent: Monday. December 01, 2014 5:47 PM
To: Rogers, Michael
Subject: Re W10400175
Dear Mr. Rogers,
Below is a dropbox link to the Semi Annual Water Quality Monitoring Report for the latest event performed at
the Surry Co. Closed MSWLF and Closed CDLF-Mt. Airy in May 2014 per UIC #WI0400176.
https:llwww.dropbox.comislr9dga6dd7rr3lwc/Sorry%2OCo.%20C Iosed°/n?4M S WLF%20and°/a? OClosed%2 DC
DLF%20Renort%20%28 W I0400176_May20l4%29�pdf?dI=
This file will be available for download via dropbox til at least December 15, 2414 after which time it may be
removed.
Hard copies were sent to the UIC Raleigh office and the facility.
Monitoring has/will continue on a semi-annual basis in conjunction with routine monitoring per the SWS with
the most recent event performed in October 2014. The October reports will be submitted upon completion.
If you have any yuestionslconcems please contact us anytime.
Thanks,
Jonathan
On Mon, Dec 1, 2014 at 3:44 PM, Rogers, Michael <michael.ro ers ncdenr. ova wrote:
Greetings -
Please send a copy of the May 2014 Semi -Annual Water Quality Monitoring Report for the above permit to my
attention. Thanks.
Michael Rogers, P.G. (NC & FL)
Hydrogeologist P.
12101 CAN 1VWC .�1 _
Water Quality Regional Operations Section
1636 Mail Service Center
Raleigh, NC 27699

Direct No. 919-807-6406
http:llportal. ncdenr.org]web/wq/gps/gmTro/reporting-forms
NOTE: Per Executive Order No. 150, all e-marls sent to and froln this account are subject to the North
Carolina Public Records Law and may be disclosed to third parties.

Semi -Annual Water Quality Monitoring Report
Prepared far
Surry County Closed C&D and Closed MSWLF, Mt. Airy
Mt. Airy, North Carolina
May 2014
5ubinitted: October 1, 2014
P.O. Box 97
Garner, NC 27529
License No. C-0281
UIC Permit Number:WI0400176
SWS Facility Permit Number: 8"2
MESCO Project Number: G14032.0
MU12idpalJ�'
Municipal biginerring Services Cniupm . P A
Carver and Boone, Wrlh Carolina

TABLE OF CONTENTS
SECTION
Introduction _ — ---
......-------------------- _ _.... _ Page I
Background....... _..­.. ...... ..� _ _ _ _._ _____.._.—___..._.......�
r._.._..__�.._._..__..__ Page I
Sampling Procedure_.. _ ..____.-__... __..___.. .._ _ __._._...
__... �_._.... _ __.......Page 2
Field Parameter Data._._m ... _ Y_ .__...
...._._.. _ _...... .. ._._. Page 2
Laboratory Results-_-
Page 2
--__---__..,,,_,m._.._,_,_._..___
._. _- — .
Groundwater Samples _.__.._
�.� _ .Page 3
Groundwater Characterization _....__..__....____
-..__._._ ___--Page 3
3
Closinp-..----------------------------------- -
........ . Pajae 4
I at let 14 V
Topographic Map with Site Location..-.- ..�-.-._ ..-. µ __..._ m..._...._..... ._..._..........._......_.._..._......_...____.._..___.._..._.... _Figure 1
Potentiometric Map of Uppermost Aquifer wl VOCs Detected Above 2L Standards„ , __,,,,,Figure 2
Total Cumulative VOC Concentrations Pre/Post Injection Comparison -W _ Figure 3
Bromide Tracer Concentrations Time Series Graph and Table . _ , „ _ _ -Figure 4
TABLES
Sampling and Analysis Summary _...._._.__._..........
........m
Detections that Attain or are Above SWSL or 2L Standard
Field Parameter Data Summary.--- ..............
............_ ..____w......
Hydrologic Properties at Monitoring Wells _W _ .................
MNA Parameter Data Summary.._,_,,,_,___ __„_„_
APPENDIX
Table I
Table 2
_Table 3
,Table 4
Table 5
Laboratory Analysis Report and Chains of — -_-_- __--_-_- ---------- - _ - _Appendix A

License No Cr728'
October 1, 2014
Mr. Thomas Slusser, P.G.
Aquifer Protection Section -Underground Injection Control Program
Division of Water Quality
North Carolina Department of Environment and Natural Resources
1636 Mail Service Center
Raleigh, NC 27699-1636
Re: Semi -Annual Water Quality Monitoring Report
Surry County Closed C&D and Closed MSWLF, Mt. Airy
237 Landfill Road
Mount Airy, NC 27030
SWS Perm it No. 86-02
UIC Permit No. W10400176
MESCO Project No. G 14032A
Event Date(s) May 27-29, 2014
Dear Mr. Slusser:
Introduction
Municipal Engineering Services Company, PA (MESCO), on behalf of Surry County, appreciates the opportunity to
present this brief Semi -Annual Water Quality Report that details a water quality monitoring event performed at the
Surry County Closed C&D and Closed Unlined Municipal Solid Waste Landfill (MSWLF) Facility (Permit # 86-02)
on May 27-29, 2014. The Injection Well Pernilt Application and Well Permit No. W10400176 (4/15/13) requires
that Surry County provide this report to the Underground Injection Control (UIC) program on a semi-annual basis.
Laboratory analytical results indicate volatile organic compounds (VOCs) attributed to landfill activities continue to
persist in Ievels above 2L Standards at seven wells that monitor the uppermost aquifer downgradient of five
injection points. However, total VOC concentrations have decreased at all locations compared to their respective
baseline averages established during the five events prior to the first injection event performed in November 2011.
Background
The Surry County closed C&D and MSWLF, permit #86-02, is located at 237 Landfill Road in Mt Airy North
Carolina. The site location topographic map is depicted in the attached Figure I. Prior to becoming a C&D landfill
the subject area operated as a MSW unlined sanitary landfill that stopped receiving waste prior to January 1, 1999,
The MSWLF was closed with a low permeability cohesive sail cap per the Transition Plan. The top portion of the
southern unit served as an exclusive C&D landfill until prior to June I, 2008 at which time it was properly closed
with another cohesive soil cap in accordance with the Closure Plan.
Per the SWS approved Corrective Aclion Plan enhanced bioremediation via substrate and tracer injection was
initiated in the Southern and Northern ADCs in accordance with requirements outlined in the Injection Well Permit
Application and Well Permit No. W10400176 (5/6/11) with the goal to reduce low level aliphatic and aromatic
chlorinated hydrocarbons in groundwater to below 2L Standards.
On November 2-3, 2011 an EOS-water emulsion with sodium bromide tracer was injected into three we]Is ( IW-2.
IW-3 and I W-5). Injection was attempted. into IW-I during this same event but due to the tightness of the formation
an insignificant amount (< 3 gallons of slurry) entered the uppermost aquifer- For a]I intents and purposes 1W-I
injection did not occur nor ever will be able to in the future. Monitoring of wells downgradient of this location will
continue to be monitored semi-annually as required by the NC Solid Waste Section (SWS). Any observed changes
in geochemistry downgradient of IWA is not attributed to the unsuccessful injection event. Details of the premier
injection event are provided in the Injection Event Record dated November 4, 2010.
P 7 5nx 97 G;jrmi r. Norl}i Carol?"o 27529 i919} 7j2.5393 PO Box 30. Boone NC 2"07 1,8281 262 ' -C_'

On October 24-25, 2012 similar substrates were injected into monitoring wells MW-411W4 and MW-81IW-6 in
fulfillment of Phase 2 of Corrective Action. Details of the second injection events is provided in the Injection Event
Record submitted January 10, 2013.
The UIC Injection Well Permit was renewed on April 15, 2013 which reduced monitoring frequency from
quarterly to semi-annually and the prescribed constituents listed in the approved application was also reduced
and vague_
Water quality at this facility has been monitored at least semi-annually since 1989 with historical data available
since 1994. This is the seventh post -injection water quality monitoring event with previous events performed on
February 9, 2012, May 30, 2012, August 20, 2012, October 23, 2012, May 29, 2013, October 29,2014. Previous
event reports have already been submitted to the UIC and SWS.
This report contains sampling procedures, field and laboratory results, groundwater characterization, and findings.
A potentiometric map of the uppermost aquifer, time -series graphs of select constituents, a table of detections
compared to Standards, field data results table, groundwater flow directions/rates table and laboratory analytical
data results are also enclosed.
Sampling Procedure
MESCO personnel performed this sampling event targeting the parameters outlined in the Water Quality ,Sampling
and Analysis Plan (SAP) (DIN.18936) dated April 30, 2013 and approved by the SWS (DIN: 18938) on May 10,
2013. Monitored locations were consistent with the renewed Well Permit (4/15/13).
Groundwater samples were collected and analyzed from fourteen wells which includes MW-3R, MW-7, MW-9,
MW-125, MW-13, MW-14, MW-16, MW-17, MW-18, MW-19, MW-20, MW-22, MW-23 and upgradient
background well MW-1. Additionally, water within all six injection wells were measured and visually evaluated in
an effort to determine the amount of residual organic substrate remaining in the wells which may help evaluate the
viability of these wells to be used for future water quality analysis. Monitoring locations are depicted on Figure 2.
Sampling was performed per the protocols outlined in the SWS approved Groundwater and Surface Water Sampling
and Analysis Plan which was submitted with the Convective Action Plan (CAP) revision 2 dated December 10, 2010.
The depth to water in each well was electronically gaged prior to purging to quantify the static water level elevation.
Low -flow pumping methodology or bailing was utilized to adequately purge the wells a minimum of three well
volumes or until dry. During purging the stabilized field parameters were recorded. The samples were then placed
into laboratory -prepared, pre -preserved containers via a new disposable polyethylene bailer. Samples were kept on
ice, and transported within hold -times to a NC -certified laboratory under proper chain of custody (C-O-C) protocols.
Field Parameter Data
Field parameters recorded included depth to water, pH, specific conductance, temperature, dissolved oxygen (DO),
oxidation reduction potential (ORP), total dissolved solids (TDS) and turbidity. A summary of the field parameter
data since injection is presented in Table 3.
Laboratory Results
Pace Analytical Laboratories (PACE) of Huntersville and Asheville, NC performed the majority of the laboratory
analysis. Groundwater samples were analyzed for all the parameters requested by the SWS which includes
constituents listed in Appendix 1 of 40 CFR 258 plus select monitored natural attenuation parameters (MNA) at
select locations. Environmental Conservation Laboratories (ENCO) of Cary, NC analyzed select samples for the
bromide tracer. A sampling and analysis table summarizing the locations, target parameters and laboratory methods
is presented as Table 1. Water samples were reported at the laboratory specific Method Detection Limits (MDL),
which are quantifiable at or below the current Solid Waste Section Limits (SWSL). Laboratory results and C-O-Cs
are presented in Appendix A.
2

Groundwater Samples
The wells with Appendix 1 VOCs detected in concentrations in exceedance of their respective 2L Standard during
this event include MW-9 (14-dichlorobenzene, benzene, vinyl chloride), MW-13 (1,2-DCA), MW-14 (PCE), MW-
15 (PCE. TCE, 1,2-DCA, 1,1-DCA, benzene, vinyl chloride), MW-16 (1,4-dichlorobenzene, 1,2-DCP, 1,2-DCA,
benzene, vinyl chloride), M W-21 (1,2-DCA, L I-DCA) and M W-22 (1,2-DCA). Although oat regulatory applicable
the only constituents detected above the EPA established maximum contaminant levels (MCLs) or primary
"Drinking Water Standards" were vinyl chloride (MW-9, MW-16) and 1,1-dichloroethene (MW-15). Table 2
summarizes constituents detected in groundwater samples in concentrations above the current SWSL or North
Carolina Groundwater Standards (2L). MNA data presented in Table 5 continues to indicate that favorable
geochem icaI conditions exist for continued natural attenuation,
A site map depicting the concentrations and estimated horizontal extent of VOCs that exceeded the 2L Standard
during this event is presented on Figure 2.
Groundwater Characterization
A potentiometric map of the uppermost aquifer created from static groundwater elevations recorded during the May
2014 event is included as Figure 2. Groundwater flow rates and directions were calculated via modified Darcy's
equation and are included in Table 4. Groundwater flows in the unconfined and upper bedrock water -bearing zones
in a general southwesterly direction away from the waste limits. Calculated groundwater velocities were variable
but consistent compared to historical observations.
Findings
The laboratory results indicate that dissolved phase VOCs consisting primarily of chlorinated hydrocarbons continue
to be detected in groundwater samples collected from seven wells. All VOCs detected in concentrations above the
2L Standard during this event remain within their own respective historically identified range. Total cumulative
VOC concentrations were lower during this event compared to their own respective five event averages established
prior to injection in all locations as shown on Figure 3.
Evaluation of the injection wells (I W-1, 1 W-2, IW-3. IW-4, I W-5 and l W-6) continues to indicate that a considerable
amount of residual organic substrate retrain in each of these wells rendering there unsuitable for representative
water quality analysis. The viscosity of the water in the injection wells precludes sample collection as either a
bailer would not descend or the check valve Failed.
In an attempt to track migration of injectants bromide was targeted at MW-3R, MW-13, MW-14, MW-15, MW-16,
MW-21 and background well MW-I. MW-16, located 86 feet downgradient of IW-3, is the only location
exhibiting tracer levels which may potentially indicate injectant communication. [cased on the average linear
velocity rates of IW-3 and MW-16 reported since injection the injectant was expected to reach MW-16 in May 2012.
Bromide concentrations exhibited a consistent increasing trend in MW-16 the first year following injection then has
decreased the last year (Figure 4). Calculations performed following injection indicates that reported levels of
bromide injected was insufficient to provide clear evidence of migration within the uppermost aquifer.

Closing
Water quality monitoring is planned to continue with the next event scheduled for October 2014. No further
injections are planned at this time but if they do Permii conditions will be met including giving the UIC advance
notice prior to installation or injection of any additional well(s).
If you have any questions or comments regarding this report, please contact us at [phone] or by email at
infohl(@mesco.com.
Sincerely,
MUNICIPAL ENGINEERING SERVICES CO., P.A.
�Qj�
Jonathan Pfohl
Environmental Specialist
Enclosures
cc: Mr. Dennis Bledsoe
Surry County
Ms. Jaclynne Drummond (Electronic Copy Only)
SWS-Compliance Branch
Ms. Shuying Wang (Electronic Copy Only)
UIC

Topographic Map with Site Location
Surry County Closed Unlined C&D and Closed Unlined MSWLF, Mt. Airy
1' lti1 j�
J.
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of 5 •'r"�. _' y, is r' _ X7- - - �� ��• - : - - .. .�}� �}
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'21
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_ ._. �. `�. .ram -�.� 't�•�_ ._ — f.
237 Landfill Road ROAD CLASSIFICATION
Primary highway, Light -duty road, hard or
Mount Airy, NC 28621 hard surface.__ _ .. improved surface . .
Lat:36-26-30.065 Secondary highway,
Long:-80-34-15.314 hard surface - Unimproved road.
Northing:983356.18 0 Interstate Route C3 U. S. Route 0 State Route
Easting:1537885.4$
Closed L!nliltefi C'&17 Lctttdli[I
Closed Unlined Sanitary Landfill
1 0 1 MILE
_ FIGURE 1

237 LANDFILL ROAD / 1130":;
NOW OR FORMERLY
OWNED BY
JOHNNY COX
IW-6
1047.47
mw-s
1 4-Dichlorohenzene - 6.6 ugA
Benzene - 3.3 ugA
Vinyl Chloride - 10.8 ugA
MIN-6 -
1045.29
MW-3R
976.55*
MW-'I 6 IW-3 ,
973.85 989.62
MW-16
1,2-Zhroropropane - 3.2 ugA
1.4-Dlchkorobenzene - 15-0 ugA
1,2-01Chlorog[nane - 2A ugA
Benzene- 1-8 ugA
Vinyl Chlodde - 8-7 ugA
M W-20
1062.78
SW-2
MW-7-
1061.69
957.04 !
MW-17
1
(1 345 F' UPSTREAM}
QP.,, N
as now a .
RECYCLE AREA
ll IN
I,ouK#*# I
S `R
T/VE
- L ID
MS WLF CLO FORE J
+ ER 9, 1991 j
°° r
t
EM3TiNG
e wn
rkl
1
LDVEREe
TIRES .
++ f
l .
f+I
CLOSED C&D OVER CLOSED MSW
STOPPED RECEIVING C&D BEFORE JUNE 1, 2008
STOPPED RECEIVING MSW BY JANUARY 1,1999
l ACTIVE GCCS /
.tw-5

Semi -Annual Water Quality Monitoring Report
Prepared far
Surry County Closed C&D and Closed MSWLF, Mt. Airy
Mt. Airy, North Carolina
Submitted: October 22, 2013
P.O, Box 97
Garner, NC 27529
License No. C-028I
RECEwEnEN owo
May 2013 f r
Aquifer Protection Section
UIC Permit Number:W10400176
SWS Facility Permit Number: 86-02
MESCo Project Number: G13032.0
Municipal Eagiaeeriag
co..�.rA
Gnwar, NC r �aA KC
Municipal Engineering Sen�ices Company, P.A
Garner and Boone, Nonh Carolina

TABLE OF CONTENTS
SECTION
Introduction--
_ ,._,______Page I
Background �..�
___ ___Page I
Sampling Procedure...._...._.m.m.m.._._...... _ .... ..... . ............... _... _
Page 2
Field Parameter Data.._
�._ .._Page 2
Laboratory Results.
_..__ _ —.—,Page 2
Groundwater Samples
,...._....Page 3
Groundwater Characterization
_ Page 3
Findings
Page 3
_
_ _
Closing
_ _ .. Page 4
FIGURES
Topographic Map with Site Location _....... _ _W Figure 1
Potentiometric Map of Uppermost Aquifer wl VOCs Detected Above 2L Standards_, _.,._. ..,_.Figure 2
Total Cumulative VOC Concentrations Pre/Post Injection Comparison.— _ _ . figure 3
Bromide Tracer Concentrations Time Series Graph and Table ._ _ ._ Figure 4
TABLES
Sampling and Analysis Summary,.
Table 1
Detections that Attain or are Above SWSL or 2L Standard
Table 2
Indicator Parameter Data Summary ______Y------- �T _, T_µ — -------------------
3
Field Parameter Data Summary
__.. Ta61e 4
Hydrologic Properties at Monitoring Wells.___.. -_._.._,.._..
.Table 5
APPENDICIES
Laboratory Analysis Report and Chains of Custody.
ppendix A

License No. C-0281
CIVILISANITARYIENVIRONMENTAL ENGINEERS
Municipal
Services
SITE PLANNINGISUBDIVISIONS
Mr. Thomas Slusser, P.G.
Aquifer Protection Section -Underground Injection Control Program
Division of Water Quality
North Carolina Department of Environment and Natural Resources
1636 Mail Service Center
Raleigh, NC 27699-1636
Re: Semi -Annual Water Quality Monitoring Report
Surry County Closed C&D and Closed MSWLF, Mt. Airy
237 Landfill Road
Mount Airy, NC 27030
S W S Permit No. 86-02
UIC Permit No. WI0400176
MESCO Project No. G 13032.0
Event Date(s) May 29-30, 2013
Dear Mr, Slusser:
Introduction
SOLID WASTE MANAGEMENT
Engineering
Company, P.A.
SUBSURFACE UTILITY ENGINEERING (SUE)
October 22, 2013
Municipal Engineering Services Company, PA (MESCO), on behalf of Surry County, appreciates the opportunity to
present this brief Semi -Annual Water Quality Report that details a water quality monitoring event performed at the
Surry County Closed C&D and Closed Unlined Municipal Solid Waste Landfill (MSWLF) Facility (Permit # 86-02)
on May 29-30, 2013. The Injection Well Permit Application and Well Permit No. W10400176 (4/15/13) requires
that Surry County provide this report to the Underground Injection Control (UIC) program on a semi-annual basis.
Laboratory analytical results indicate volatile organic compounds (VOCs) attributed to landfill activities continue to
persist in levels above 2L Standards at six wells that monitor the uppermost aquifer downgradient of five injection
points. However, total VOC concentrations compared to their respective baseline averages established during the
five events prior to the first injection event performed in November 2011 injection have decreased in most
locations.
Background
The Surry County closed C&D and MSWLF, permit #86-02, is located at 237 Landfill Road in Mt, Airy North
Carolina. The site location topographic map is depicted in the attached Figure 1. Prior to becoming a C&D landfill
the subject area operated as a MSW unlined sanitary landfill that stopped receiving waste prior to January 1, 1999.
The MSWLF was closed with a low permeability cohesive cap per the Transition Plan. The top portion of the
southern unit served as an exclusive C&D landfill until prior to June 1, 2008 at which time it was properly closed
with another cohesive cap in accordance with the Closure Plan.
Per the SWS approved Corrective Action Plan enhanced bioremediation via substrate and tracer injection was
initiated in the Southern and Northern AOCs in accordance with requirements outlined in the Injection Well Permit
Application and Well Permit No. WI0400176 (5/6/11) in an effort to reduce low level aliphatic and aromatic
chlorinated hydrocarbons in groundwater to below the 2L Standards.
On November 2-3, 2011 an EOS-water emulsion with sodium bromide tracer was injected into three wells ( IW-2,
1W-3 and IW-5). Injection was attempted into lW-1 during this same event but due to the tightness of the formation
an insignificant amount (c 3 gallons of slurry) entered the uppermost aquifer. For all intents and purposes lW-I
injection did not occur nor ever will be able to in the future. Monitoring of wells downgradient of this location will
continue to be monitored semi-annually as required by the NC Solid Waste Section. Any observed changes in
geochemistry downgradient of IWA is not attributed to the unsuccessful injection event. Details of the premier
injection event are provided in the Injection Event Record dated November 4, 2010.
PO Box 97, Garner, North Carolina 27629 [phone]
PO Box 349, Boone, NC 28607 [phone]

On October 24-25, 2012 similar substrates were injected into monitoring wells MW-41IW-4 and MW-811W-6 in
fulfillment of Phase 2 of Corrective Action. Details of the second injection events is provided in the Injection Event
Record submitted January 10. 2013.
The UIC Injection Well Permit was renewed on April 15, 2013 which reduced monitoring frequency from
quarterly to semi-annually and the prescribed constituents listed in the approved application was also reduced
and vague. 7
Water quality at this facility has been monitored at least semi-annually since 1989 with historical data available
since 1994. This is the fifth post -injection water quality monitoring event with previous events performed on
February 9, 2012, May 30, 2012, August 20, 2012 and October 23, 2012. Previous event reports have been already
submitted to the UIC and SWS.
This report contains sampling procedures, field and laboratory results, groundwater and surface water
characterization, and findings. A potentiometric map of the uppermost aquifer, time -series graphs of select
constituents, a table of detections compared to Standards, field data results table, groundwater flow directions/rates
table, indicator parameter data table and laboratory analytical data results are also enclosed.
Sampling Procedure
MESCO personnel performed this sampling event following the expansive list of parameters approved in the
original Well Permit (5/6/11). Monitored locations were consistent with those approved in the renewed Well Permit
(4115113).
Groundwater samples were collected and analyzed from fourteen wells which includes MW-3R, MW-7, MW-9,
MW-12S, MW-13, MW-14, MW-16, MW-17, MW-18, MW-19, MW-20, MW-22, MW-23 and upgradient
background well MWA. Additionally, water within all six injection wells were measured and visually evaluated in
an effort to determine the amount of residual organic substrate remaining in the wells which may help evaluate the
viability of these wells to be used for future water quality analysis. Monitoring locations are depicted on Figure 2.
Sampling was performed per the protocols outlined in the SWS approved Groundwater and Surface Water Sampling
and Analysis Plan which was submitted with the Corrective Action Plan (CAP) revision 2 dated December 10, 2010.
The depth to water in each well was electronically gaged prior to purging to quantify the static water level elevation.
Low -flow pumping methodology or bailing was utilized to adequately purge the wells a minimum of three well
volumes or until dry. During purging the stabilized field parameters were recorded. The samples were then placed
into laboratory -prepared, pre -preserved containers via a new disposable polyethylene bailer. Samples were kept on
ice, and transported within hold -times to a NC -certified laboratory under proper chain of custody (C-O-C) protocols.
Field Parameter Data
Field parameters recorded included depth to water, pH, specific conductance, temperature, dissolved oxygen (DO),
oxidation reduction potential (ORP), total dissolved solids (TDS) and turbidity. A summary of the field parameter
data since injection is presented in Table 3.
Laboratory Results
Pace Analytical Laboratories (PACE) of Huntersville and Asheville, NC performed the majority of the laboratory
analysis. Groundwater samples were analyzed for all the parameters requested by the original UIC Permit which
includes constituents listed in Appendix I of 40 CFR 258, alkalinity, sulfate, chloride, total organic carbon and
biochemical oxygen demand. Environmental Conservation Laboratories (ENCO) of Cary, NC analyzed select
samples for the bromide tracer. A sampling and analysis table summarizing the locations, target parameters and
laboratory methods is presented as Table 1. Water samples were reported at the laboratory specific Method
Detection Limits (MDL), which are quantifiable at or below the current Solid Waste Section Limits (SWSL).
Laboratory results and C-O-Cs are presented in Appendix A.

Groundwater Samples
The wells with Appendix I VQCs detected in concentrations in exceedance of their respective 2L Standard during
this event include MW-9 (1,4-dichlorobenzene, benzene, vinyl chloride), MW-13 (1,2-DCA), MW-14 (PCE), MW-
15 (PCE, TCE, 1,2-DCA, benzene, vinyl chloride), MW-16 (1,4-dichlorobenzene, 1,2-dichloropropane, 1,2-
dichlroethane, benzene, vinyl chloride), MW-17 (vinyl chloride), MW-21 (1,2-DCA) and MW-22 (1,2-DCA).
Table 2 summarizes Appendix I constituents detected in the water samples in concentrations above the current
SWSL or North Carolina Groundwater Standards (2Q. Table 3 summarizes indicator parameters quantified by the
laboratory.
A site map depicting the spatial distribution of VOC concentrations detected above the 2L Standard during this
event is presented on Figure 2.
Groundwater Characterization
A potentiometric map of the uppennost aquifer created from static groundwater elevations recorded during the May
2013 event is included as Figure 2. Groundwater flow rates and directions were calculated via modified Darcy's
equation and are included in Table 4. Groundwater flows in the unconfined and upper bedrock water -bearing zones
in a general southwesterly direction away from the waste limits. Calculated groundwater velocities were variable
but consistent compared to historical observations.
Findings
The Iaboratory results indicate that low level dissolved phase VOCs consisting primarilyof chlorinated hydrocarbons
continue to be detected in groundwater samples collected from seven wells. All VDCs detected in concentrations
above the 2L Standard during this event remain within their own respective historically identified range. Total
cumulative VOC concentrations decreased during this event compared to their own respective five event averages
established prior to injection in all locations except for MW-15 as shown on Figure 3.
Evaluation of the injection wells (IW-I, IW-2, IW-3, 1W-5) continues to indicate that a considerable amount of
residual organic substrate remain in each of these wells rendering them unsuitable for representative water quality
analysis. The viscosity of the water in the injection wells precludes sample collection as either a bailer would not
descend or the check valve failed.
The bromide tracer was detected in low non -quantifiable ``j-qualified" concentrations in MW-7, MW-14, MW-16
and MW-21 during this event but neither levels nor trends were significant. MW-16, located 86 feet downgradient
of IW-3, is the only location exhibiting tracer levels which may potentially indicate injectant communication. Based
on the average linear velocity rates of lW-3 and MW-16 reported since injection the injectant was expected to reach
MW-16 on May 25, 2012. Bromide concentrations exhibited a consistent increasing trend in MW-16 the first year
following injection then decreased the last six months (Figure 4). Calculations performed following injection
Indicates that levels of bromide that was injected was insufficient to ever provide clear evidence of communication
within the uppermost aquifer.

Closing
Water quality monitoring is planned to continue with the next event scheduled for late October or early November
2013. No further injections are planned at this time but if they do Permit conditions will be met including giving the
UIC advance notice prior to installation or injection of any additional well(s).
If you have any questions or comments regarding this report, please contact us at [phone] or by email at
jpfoh [e-mail].
Sincerely,
MUNI CA AL ENGINEERING SERVICES CO., P.A.
J �na han Pfohl
En it r}i rental Specialist
Enclosures
cc; Mr. Dennis Bledsoe
Surry County
Ms. Jaclynne Drummond (Electronic Copy Only)
SWS-Compliance Branch
Ms. Shuying Wang (Electronic Copy Only)
UIC
4

Figures

Topographic Map with Site Location
Surry County Subtitle D Lined MSLF, Phases 1 & 2
Surry County Closed C&D and Closed MSWLF, Mt. Airy
1�
Per
X.
fir, � � :� ��.� •� - . ,l ', �s.y
Y"� -• � + '.a• yr. • � �Y�:
•�-, .lam + :. '
. Yam..
Aft
z •:r � �� La
-�
Subtitie ❑
i r•
� � a
~ROAE] CLASSIFICATION
237 Landfill Road Primary highway, Light -duty road, hard or
hard surface improved surface
Mount Airy, NC 28621 Secondary highway,
Lat:36-26-30.055 hard surface _ Unimproved road ----------
Long: -80-34-15.314 01 Interstate Route 0 U" S. Route 0 State Route
Northing:983356.18 ? a 1 MILE
Easting:1537885.48 FIGURE 1

I
rJIAV OR FORMERL Y
0 WN>ED 8 Y
JOHNNY COX
AM
e
i
MW-afi +
wn se• l
l
! 1
r 1
1
_ 7
f 1
1 1 7
a,
Swell , (i W Fr LwSTR7) l {
SCA.LEHOUSE
IFACiL NOM•POTA.BLE WATER SUPPLY WELL)
1
+
+
1
- 1
1
' ' fffwf
- � 1
1
j 0 WNED 9 Y
SURRY' CQUN TY
polo
1
i
1
� 1
fr.'axrsrm7rs�r� 1
i
1
1
7
1
fl111yy' p�
1
7
1 ....
M�rlr
NOW OR FORMERLY OWNED 6 Y
SHA WNA SUMMERS
�� —
1 —
w ; - EN EMSr ROPOCRAPrIrC CCWTOUR°.
�+ YM TNJG Ri.AU$
- ESTULATED WASTE L0 5 VNLOAIEV M5W &/OR f:RV
LIW[Fi [Mr5 OF SUBYTLE D LA ED H$wLF
iVf"T or CGwE5r4F a-ky Cl OSf1RE UPON GYOSED u5w AND C,"
LAB W PROPERTY LfNE Ek MAMA TEO FROM SURVEY AHD 6f5
1 - / COMPL]ANLE RWND.ARY (25C' FROM EOM J, SC7' FROM PROPERTY LeW]
E%TENT �W ypq5j DETECTED ABL UE $WSL .f iL STAND,IRD BE1"OM1'O LI]i/PLIANP[ BWM1'i'a^'
� 1
AcwLmm 1090- EOWPOTENRA. VPPERUOST SRUL'NDWATER (.WOVRS
!•
} — 5TREAV/C1?47EK/RAER
_- WATER SUPPLY WELL;FACUTY CONSIDERS IT NON -POTABLE)
• am 5VRFAa WATER UOMTpi1NG PONT
W" HO.M7,A1NG MILL
wIck:T 0h WELL
f].11 C-RpIJNPWATER POTENTf011ETRFC ELEVAAON (AOa)
_--- - NOTE ELr VAT?LV4 NOT V5ED FOR Ca'+TCNjF?5
5EDf11VrF 64-91N MIPA�PIArWa�O11 E.tw1ANwi1Mi�
ow
A - .. er •! n IIOu �l+a�il .�.11 lwf FKW ennl�ls
RNA IpW
- wee
— _ OWNED By
SURRY COUNT
1 y
I
GRAPHIC FC.ALF. - -
,�_,I.R FIGURE 2
}" CLOSED C&D LANDFILL and
CLOSED MSWLF FACILITY muservk pa! Eng)neering
SURRY COUNTY 8°^`k''+ �..�' C—Parr'. P.A.
P0tiNRMVW VAP OF VPPER"t AQWM .n. ptnelwa acvs .Y IGtI«III.R KC Ian
1 WIN V005 DE -WO a )WOW a S AWARDS MT. AIRY, NORTH CAROLINA ►�1�+ a.11l..�..

Figure 3
Total Cumulative VOC Concentrations Pre/Post Injection Comparison
October 22, 2009 - May 30, 2013
Wells Downgradient of Injection Points (Total Cumulative VCC Concentrations as PQL or SWSL)
:00 ... _. __ IYMiRliMei Titne$erles Gre�h _ _
ISO-
,u7
�
:W :0 _ .LU •Z
r
M
o-- �o - ------- -w
ell
c
�o
Sm" Ada
-WV-16 -M*19 •Allhl-23 --. W-21 & W U MN -MIN W15 -MW-19 PA*19
Average of
first Five
Corrective
Oct May Oct May Oct Action May Statistical Trend'
2009 2010 2010 2011 2011 Events 2013 Difference Difference Between Oct
Well ID (ug/L) (uglL) (ug/L) (ug/L) (ug/L) (ugfL) (ug1L) (ug/L) (°Iaj 2009-May 2013
INJECTION WELL (IW-1 ) UNSUCCESSFUL INJECTION SO DOWN GRADIENT WELLS NOT SHOWN
INJECTION WELL (IW-2) MONITORED DOWNGRADIENT BY MW-12S, MW-13 & MWA8
MW-12S
0.00 0.00 0.00 0.00 5.40 1.08 0.00 •1.08 •100
No Trend
MW-13
61.00 50-60 74.20 87.30 72.50 69.12 29.17 -39-95 -58
No Trend
MW-18
0.00 0.00 0.00 0.00 0,00 0.00 0,00 0.00 0
No Trend
INJECTION WELL (IW-3) MONITORED DOWNGRADIENT BY MW-3R & MW-16
MW-3R
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0_
No Trend
MW-16
_ _
137.90 113-60135.70121.20116.30 124.94 76.50 -48.44 -39
Downward
INJECTION WELL (IW-4) MONITORED DOWNGRADIENT BY MW-14, MW-21 & MW-23
MW-14
15.20 15.60 15.60 8.20 17.00 14.32 7.50 ;.8; 48
No Trend
MW-21
52.10 50.70 51.38 39.10 32A1 45.14 36.82 3.3? -.18
Downward
MW-23
4.30 0-00 0.00 0.00 0.00 0.86 0.00 1 { -100
No Trend
INJECTION WELL (IW-5) MONITORED DOWNGRADIENT BY MW-15 & MWA9
MW-15
96.13 63.89 55.00 78,10 64.06 71 A4 81 A 8 9.74 14
No Trend
MW-19
_ _
0.00 0-00 0.00 0.00 0.00 0.00 0.00 0.00 0
No Trend
INJECTION WELL (IW-6) NOT SHOWN AS NO WELLS DOWNGRADIENT WITHIN ZONE OF INFLUENCE
Statistical Trend analysis via Sen's Slope Estimator at a 95% confidence level
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1

Figure 4
Bromide Tracer Concentrations Time Series Graph and Table
February 9, 2012 -- May 30, 2013
Bromide Tracer Levels in MW-16
Located 87 feet ❑owngradient of IW-3 Injected on November 2, 2011
0.3000
0,2500
0.2000
0.1500
0.1000
0.0500
0.0000
Date
Date MW-16
219I2012
0.0380 U)
5/30/2012
0.13000)
8/20/2012
0.2600 Uy
10/23/2012
0.2800
5/30/2013
0.1400 U7
q
(f} = The reported Value is between the laboratory method detection limit (MOL) and the laboratory method reporting limit (MRL),
= May 25, 2012 Calculated date injectant expected to reach MW-16 using average flow rates of IW-3 and MW-16 (155 fVyr) since injection occurred.
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1

Tables

W
N+
O
rD
m
y
C1
iA
W
N
W
V
�
Reason Not Sampled
x
x
k
x
iC
1-1-1
x
xxx
x
x
1-1
1
x
x
Lab EPA 8260B
OCs
Total Metals
X
x
x
x
x
x
x
1-1-1-
x
x
x
x
x
x
x
x
Lab EPA 60OW 00q
x
x
x
x
Lab EPA 8280E
VoCs (App II)
IT
Lab EPA 80001700o
atal Metals (App 11)
Lab SW8151A
Herbicides -Chlorinated App 11
Lab EPA 827QD
Semivolatile Organics (SVOCs) App II
Lab EPA 8081E
Pesticides App 11
Lab EPA 9014
Total Cyanide
11
Lab SM18 4500-S D
Sulfide
M23G
VFA
M20GAX
Hydrogen
M20GAK
Methane/EthenelEthane
Field Hach Kit
Dissolved CO2
x
x
x
x
x
x
x
x
x
x
x
x,x
x
x
x
EPA310.2
Alkalinity
x
x
x
x
x
x
*
x
x
x
x
x
k
x
x
x
EPA 30Q,0
Sulfate
Lab SM18 4500-SS D
Sulfide
i
x
x
x
x
x
x
x
x
xxx
x
x
x
x
x
EPA 300.0
Chloride
a
x
1.1
x
xxxx
x
xxx
xk
x
x
x
ISM 5310B
TOC
X
xk
xxx
x
x
xxx
xx
x
x
x
ISM 5220D
CQD
x
x
x
x
x
x
-.
x
x
x
x
x
x
x
x
x
SM5210B
SOD
X
x
x
x
x
x
Lab EPA 6010
Iron, total
Lab EPA 9014
Nitrate
x
x
x
x
x
x
-.
x
x
x
x
x
x
x
x
x
Field Meter
Dissolved Oxygen (DO)
IX
xxx
x
x
x
x
x
xxx
x
x
x
x
Field Meter
Oxidation Reduction Potential (ORP)
21
ro
-.
x
x
x
x
x
x
x
x
x
x
x
x
k
x
x
Field Meter
Temperature
v
x
x
x
x
x
x
x
xxx
x
x
x
x
x
x
Field Meter
Conductivity
x
x
x
x
xxxxxx
xk
x
x
x
Field Meter
Total Dissolved Salida (TDS)
m%
f
x
x%
X
Xx%+-x-.
x
x
k
%
xfield
Meter
pHxx
x
x
x
x
x
x
xxxx
xxxx
x
x
Field Meter or Visual
Turbdity
X
x
x
x
Lab EPA 82608
VOCs (App II)
Lab EPA 05000/7000
Total Metals (App II)
Lab SW8151A
Herbicides -Chlorinated App II
Lab EPA 82701)
Semivolatile Organics (SVOCs) App II
n
No
Lab EPA 80818
Pesticides App II
Lab EPA 9014
Total Cyanide
Lab SM18 4500-S D
Sulfide
x
H
x
x
EPA 300A
Bromide
�

Table 2
Detections in Water Samples above SWS or 2L Standard
May 29 - June 1, 2013
Sample 1D
Parameter Name
Sample
Date
Result
Unit
MOL"
SWSL 3
2L•
Exceedance
Amount
MW-7
1,4-Dichlorobenzene
5130113
- 3.2
uglL
0.33
1
6
MW-7
Cobalt, total
5130113
60.5
uglL
5
10
MW-7
Chlorobenzene
5130/13
5.8
uglL
0.23
3
50
MW-9
1,4-Dichlorobenzene
6130113
a
uglL
0.33
1
6
2
VW-9
Benzene
5130113
3.4
uglL
0.25
1
1
2.4
MW-9
Vinyl chloride
5130113
7.6
ug1L
0.62
1
0.03
7,57
MW-9
Copper, total
5/30113
15
ug1L
5
10
1000
MW-9
Cobalt, total
5/30113
188
uglL
5
10
MW-13
1,2-Dichloroethane
5130113
0.57 j
ug1L
0.12
1
0.4
0.17
MW-13
cis-12-Dichloroethene
5130113
21.3
uglL
0.19
5
70
MW-13
Trichloroethene
5/30/13
1.2
uglL
4A7
1
3
MW-13
1,1-Dichloroethane
5/30113
6.1
uglL
0.32
5
70
MW-14
Tetrachloroethene
5/30113
1.2
ug1L
0.46
1
0.7
0.5
MW-14
cis-1,2-Dichloroethane
5/30113
6.3
uglL
0.19
5
70
MW-15
1,2-Dichloroethane
5129113
0.68 j
ug1L
0.12
1
0.4
0.28
MW-15
Trichloroethene
5/29113
3.4
uglL
0.47
1
3
0.4
MW-15
Tetrachloroethene
5129113
1.1
uglL
0.46
1
0.7
0.4
MW-15
Vinyl chloride
5129113
1.6
ug1L
0.62
1
0.03
1.57
MW-15
Benzene
5/29113
3.8
uglL
0.25
1
1
2.8
MW-15
1,1-Dichloroethane
5/29/13
31.3
ug1L
0.32
5
70
MW-15
cis-12-Dichloroethene
5129/13
35.6
uglL
0.19
5
70
MW-15
1,4-Dichiorobenzene
5/29/13
3.7
uglL
0.33
1
6
MW-16
Benzene
5129113
1.5
ug1L
0.25
1
1
0,5
MW-16
1,2-Dichloroethane
5129113
2
ug1L
0.12
1
0.4
1.6
MW-16
1,2-Dichloropropane
5129113
3
ug1L
0.27
1
0.6
2.4
MW-16
Vinyl chloride
5129113
4.6
ug1L
0.62
1
0.03
4.57
MW-16
1,4-Dichlorohenzene
5129/13
16.6
ug1L
0.33
1
6
10.6
MW-16
Cobalt, total
5129113
171
uglL
5
10
101
MW-16
Zinc, total
5129113
11.9
uglL
10
10
1000
MW-16
Chlorobenzene
5/29/13
5A
uglL
0.23
3
50
MW-16
Trichloroethene
5/29/13
1.4
uglL
0.47
1
3
MW-16
cis-12-Dichloroethane
5129/13
42
ug1L
0.19
5
70
MW-17
Vinyl chloride
5130113
0.83 j
ug1L
0.62
1
0.03
0.8
MW-17
Cobalt, total
5130/13
46
ug1L
5
10
MW-17
1.4-Dichlorobenzene
513D113
2.6
uglL
0.33
1
6
MW-18 Thallium, total 5129/13 7.5 ug1L 5.5 5.5 7.22
MW-19 Zinc, total 5/29/13 14.1 uglL 10 1 ❑ 1000
5urry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 2

Sample ID
Parameter Name,
Sample
Result
Unit
IVIDL 2
SWSL 3
2L•
Exceedance
Date
Amount
_
MW-20
Zinc, total
5/30113
10.1
ug/L
10
10
1000
MW-20
Cobalt, total
5130113
17.3
ug/L
5
10
MW-21
1,2-Dichloroethane
5130113
0.52 j
ug1L
0.12
1
0.4
0.12
MW-21
1,1-Dichloroethane
5130113
8.3
ug/L
0.32
5
70
MW-21
1,4-Dichlorobenzene
5/30113
1.3
ug/L
0.33
1
6
MW-21
cis-1,2-Dichloroethene
5/30/13
25
ug/L
0.19
5
70
MW 21
Trichloroethene
5/30/13
1.7
ug/L
0.47
1
3
MW-22
1,2-Dichloroethane
5/30113
0.42 j
ug/L
0.12
1
0.4
0.02
MW-22
Cobalt, total
5130/13
105
ug/L
5
10
35
MW-22
Barium, total
5/30/13
107
ug/L
5
100
700
MW 22
1,4-Dichlorobenzene
5130113
3.4
uglL
0.33
1
6
MW-23
Cadmium, total
5129113
1.2
ug/L
1
1
2
' Table contains Appendix 1 constituents detected at or above SWSL or 2L
2 MDL = Method Delection Limit
'SINSL = Solid Wash Section Reporting Limit
`2L = North Carolina ISA NCAC 2L Groundwater Quality Standard
t =The reported value is behveen the laboratory method detection limit(MDL) and the laboralory method reporting limit {MRQ.
adjusted for actual sample preparation data and moisture content where applicable. {Value maybe considered estimatedy
BOLD = Concentration �- 2L Standard
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 2 of 2

Table 3
Indicator Parameter Data Summary
May 29-30, 2013
--
Parameters Method 11ADE" Units
Background
IVY-1
IW-2
MW-1
MW-17
MW-19
MW-22
MW42S
MW-13
MW18
5129113
5130113
5129/13
5I30113
5129113
5130113
5/29113
Alkalinity SM 2320B
1000
ug/L
81700
136000
20500
147000
726M
67700
10000
Sulfate
EPA 300.0
2000
ug/L
7400
5400
2080
3320
412002
3390
<2000
Sulfide
SM 4500-S20
100
NS
NS
NS
NS
NS
NS
NS
'Chloe
SM 4500-CI-E
1000
_29A
uglL
4070
37800
2850
6450
3220
29900
1430
TOC
SM 53108
1000
ug/L
3770
8180
3140
15300
3010
13200
1540
COD
SM 5220D
25000
u IL
<25000
NS
NS
NS
NS
NS
NS
BOD ISM5210B
2000
ug/L
2400
<2000
<2000
36DO
10700
<2000
68400
Iron, total
IEPA6010
50
ug/l-
330
NS
NS
NS
NS
NS
NS
Bromide (Tracer) JEPA
300.0
0.029
uglL
NS
NS
NS
NS
NS
NS
NS
Background)
IW-3
IW-4
Parameters
Method
MDL•
Units
MW-1
MW-3R
MW-16
MW-14
NW-21
MW-23
5/29113
5129113
5/29/13
6/30/13
5130113
5129113
Alkalinity
SM 2320B
1000
ug/L
817DO
18500
185000
39100
42300
143000
Sulfate
EPA 300.0
20QO
ug/L
7400
<2000
9880
3080
23013
3710
Sulfide
SM 4500-S2❑
100
ug/L
NS
NS
NS
NS
NS
NS
Chloride
SM 454Q-CI-E
1000
ug/L
4070
3460
27800
4630
26800
3150
TOC
SM 53108
1000
u IL
3770
1440
19800
6940
13900
4120
COD
SM 5220D
25000
ug/L
<25o0Q
NS
NS
<25000
<25000
NS
BO❑
SM52109
2000
ug/L
2400
�,2000
12000
<2000
9600
<2000
Iron, total
EPA 6010
50
u IL
330
NS
NS
92.9
169
NS
Bromide (Tracer)
EPA 300.0
0,029
7gA-
NS
NS
0.14
0.08
0.11
N5
Background
IW-5
lW-6
Parameters
Method
MDL"
Units
MW-1
MW-15
MW-19
MW-7
MW-S
I MW-20
5/29/13
5129I13
5/29/13
5/30/13
5130113
5130113
Alkalinity
SM 23208
1000
ug/L
81700
57600
20500
90800
120000
19700
Sulfate
EPA 300.0
2000
ug1L
7400
<2000
2080
7990
2430
t2000
Sulfide
SM 4500-S2D
100
uglL
NS
NS
NS
NS
NS
NS
Chloride
5M 4500-CI-E
1000
u 1L
4070
1900
2850
38300
66100
9250
TOC
5M 53106
1000
ug/L
3770
6190
3140
15000
9510
5120
COD
SM 5220D
25000
1L
<25000
a25000
NS
33000
35000
NS
SOD
SM5210B
2000
ug/L
2400
<2000
�2000
-2000
4300
<2000
Iron, total
EPA 6010
50
ug/L
330
3390
NS
<50
45700
NS
•Bromide (Tracer)
EPA 300.0
0.029
ug/L
NS
CO29
NS
0.44
NS
NS
Notes:
MDL' = Lab Method Detection Limit or lowest field measurement possible. Constituents detected below quantifiable limits are shown as < MDL value-
' Indicates dilution factor used
NS = Not Sampled
Surry County Closed C&D and CLosed lMSWLF, ML Airy Page 1 of 1

Table 4
Field Parameter Data Summary
May 29-30, 2013
Depth to
Water
TDC
Specific
Parameter
Water
Elevation
Elevation
Temp.
❑RP
DO
pH
Conductance
T13S
Turbidity
Units_
ft (btoc)
tt [amslj
ft (amsl)
C
_mV_
m_g/L
SU
umhoslcm
mg/L
Visual or NTU
Upgradient Background Well MW-1
MW-1
24.32
1110,03
1134.35
14.5
193
2.8
5,99
290
140
16.5
Injection IW-1
(Unsuccessful Infection.
Little to
no Injection occurred)
IW-1
13,55
na
na
NR
NR
NR
NR
NR
NR
>1000
MW-17
8,19
957.24
965.43
13.9
81
1,5
6.19
210
100
Clear
MW-19
9.64
936.63
946.27
14.1
288
3.1
5.99
0
0
Slight
MW-22
5,14
948.26
953.40
14.3
224
4.7
6,99
10
0
Clear
Minimum
5.14
936.63
946.27
13.9
81
1.5
5.99
0
0
Clear
Average
7.66
947.38
955,03
14.1
198
3.1
6.39
73
33
Clear
Maximum
9.64
957.24
955.43
14.3
288
4.7
6.99
210
100
Slight
Injection IW-2
IW-2
39.63
1029.23
1068.86
NR
NR
NR
NR
NR
NR
>1000
MW-12S
13.41
1012.39
1025A0
13.5
62
3.8
7.01
510
250
Clear
MWA3
25.38
983,10
1008.48
14,5
221
0.7
5.86
150
70
106
MW-16
8.91
974.09
983.00
14.3
193
6.5
5.64
10
0
--Clear_
MInlmum
8.91
974.09
983.00
13.5
62
0.7
5.84
10
0
Clear
Average
15.9
989.86
1005.76
14.1
159
3.7
6.24
223
107
Clear
Maximum
25.38
1012.39
1025.8
14.5
221
6.5
7.01
510
250
Slight
Injection iW-3
IW-3
30,22
990.35
1020.57
NR
NR
NR
NR
NR
NR
n1000
MW-3R
40.95
976,55
1017.50
15.5
121
0.5
7.68
210
100
Clear
MW-16 Y
24.59
974.95
999.54
_ 14.1
62
0.7
6.12
300
140
Slight
Minimum
24.59
974.95
909.54
14.1
62
0.5
6.12
210
100
Clear
Average
31.92
980.62
1012.54
14.8
92
0.6
6.90
255
120
Clear
Maximum
40,95
990.35
1020.57
15.5
121
0.7
7.66
300
140
Slight
Injection IW-4
IW-4
34,24
992,02
1026.26
NR
NR
NR
NR
NR
NR
>1000
MW-14
35.39
983.41
1018.80
1C3
131
2.1
5A7
80
30
20X
MW-21
5.62
959.74
965.36
14.5
209
2.2
5.49
160
70
193
MW--23
7.23
948.08
955.31
14.3
201
4.5
6,99
10
0
Slight
Minimum
5.62
948.08
955.31
14.3
131
2.1
5.47
10
0
Clear
Average
16.08
963.74
979.82
14.4
180
2.9
5.98
83
33
Clear
Maximum
35.39
983.41
1018.8
14.5
209
4.5
6.99
160
70
Slight
Injection IW-5
IW-5
40.34
1039.84
1080.18
NR
NR
NR
NR
NR
NR
NR
MW-15
51.69
1024.27
1075.96
14.5
28
0.9
5.99
120
50
75.8
RAW-19
9.64
936.63
946.27
14.1
288
3.1
5.99
0
0
Slight
Minimum
9.64
936,63
946.27
14.1
28
0,9
5.99
0
0
78.8�
Average
30,67
980.45
1011.12
14.3
158
2.0
5.99
60
25
78.8
Maximum
51.69
1024.27
1075.96
14.5
288
3.1
5.99
120
50
78.8
Injection IW-6
IW-6
41.30
1047.15
1088.45
NR
NR
NR
NR
NR
NR
780
MW-7
11.82
1 D61.68
1073.50
14.9
201
2.8
5.82
300
140
38.9
MW-9
33.17
1060.90
1094.07
15.9
31
2.8
6.38
290
140
12.7
MW-20
19.42
1062.77
1082.19
14.5
203
1,1
5.51
0
0
183
Minimum
11,82
1060.90
1073.50
14.5
31
1.t
5.51
0
0
13
Average
21A7
1061.78
1083.25
15.1
145
2.2
5.90
197
93
78
Maximum
33.17
1062.77
1094.07
15.9
203
2.8
6.38
300
140
183
bloc = Below top o1 casing
amsl = Above mean sea level
na = Not available
NR = No reading attempled
Surry County Closed C&❑ and Closed MSWLF, Mt. Airy Page 1 of 1

Table 5
Hydrologic Properties at Monitoring Well Locations
May 29-30, 2013
Groundwater
Average
Hydraulic Effective Hydraulic Linear
Conductivity Porosity Gradient Velocity Rate
Monitoring
Well (cmisecond)
MW 1
4.30E-05
IW-2
4.30E-05
MW-7
8.10E-04
IW6
4.40E-04
MW-9
1.90E-04
MW-13
2.06E-04
MW-18
2.04E-03
MW-19
1.10E-03
MW-21
1.28E-03
M W 22
9.88E-04
MW-23
3,04E-04
Minimum
4.30E-05
Average
6.77E-04
Maximum
2.04E-03
MW 3R
IW 3
I W-4
IW-5
MW-B
MW-11
MW-125
MW-12D
MW 14
MW-15
MW-16
MW 17
M W-20
Minimum
Average
Maximum
NOTi
(%) (feetlfeet)
15
15
15
15
15
23
15
3
3
15
15
3
14
23
1.003
0.026
0.063
0.127
0.032
0.093
0.119
0.037
0.052
0.143
0.116
0.026
0.165
1-003
(feet/year)
297
8
352
385
42
87
na
1,397
2,296
974
243
6
608
2.296
Groundwater
Flow
Direction
Groundwater
Depth
(feet bloc)
Potentiometric
Elevation
(feet amsl)
Screened Interval
Lithology
S33W
24.32
1110.03
Clay
S73E
39.63
1029.23
Clay
N87W
11.82
1061.68
PWR/Fractured Rock
S34W
41.30
1047.15
PWRIFractured Rock
S34W
33.17
1060.90
Sandy Silt
S26E
25.38
983.10
Saprolite
S25W
8.91
974-09
Saprolite
S13VV
9.64
936.63
PWR
S55E
5.62
959.74
Saprolite/PWR
S27W
5,14
948.26
Saprolite
S32E
7.23
948.08
Sandy Silt
-
5.14
936.63
-
-
19,29
1005.35
-
-
41.3
1110.03
-
2.40E-04
5
na
na
na
40.95
976.55
2.40E-05
5
0.205
102
942W
30.22
990.35
1.10E-04
5
0.137
313
S43E
34.24
992.02
1.50E-05
5
0.147
46
S64W
40.34
1039.84
1.90E-05
5
0.194
76
S80W
22.28
1045.39
3.10E-04
5
0.036
228
S31W
21,22
1130.58
na
3
0.142
na
S19W
13,41
1012.39
1.30E-06
5
na
na
na
0.00
1027.05
7.45E-03
3
0.121
31.202
S69E
35.39
983.41
7.21 E-05
3
0.214
532
S01 W
51.69
1024.27
2.82E-05
3
0.198
193
S43W
24.59
974.95
2.94E-04
3
0,092
928
S67W
8.19
957.24
1.92E-04
3
0.202
1,341
S05W
19.42
1062,77
1.30E-06
3
0,036
46
-
0,00
957.24
7.30E-04
4
0.154
418
-
26.30
1016.68
7.45E-03
5
0.214
1,341
-
51.69
1130.58
Values for hydraulic conductivity determined via slug test by GAI, MESC0, or Joyce.
Hydrologic gradient from water levels recorded on May 29-30, 2013.
Wells screened entirety in rock were not utilized for flow directions/gradients.
Screens that traverse both rock and regolith assumed flaw In regolith dominates.
Flow rate for MW-14 was considered an ouiller; therefore not included In the average or maximum
na = Not ovailablelapplicable
Average Linear Velocity (Q) is defined by modified 0arcy's equation:
IC= hydraulic conductivity
where Q = _ Ane= effective porosity
n e d1 dh= head difference
dr horizontal distance
Fractured Rock
Fractured Rock
Fractured Rock
Fractured Rock
Fractured Rock
Fractured Rock
Fractured Rock
Fractured Rock
Fractured Rock
Fractured Rock
Fractured Rock
Rods
Rock
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1

F
Appendix A
Laboratory Analysis Reports
Chains of Custody

f Aaea RnaylNW a.r.lan, h,4
P.[. FM1ary.tr Mr.kn,in.
F...."VW[rI e.rvle.a, I-,
Pau �nHr11[.I SarN[a.- InI. Fat. A
gyw4m 4.Mq 1. lnr_
- aceA+►alytrcala Tf E.x hU.d Read - e,rr. a
2Y R..a.W. r
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7Z73 R r a G. C[
Edan-n[ 772aa
A .y HC Xa
[ ,Viwnr MC M70
r � Edon. HE
Nc.. ,w
13300234w,
ceser25+r1 re
rlply'IS9Cg7
r]]Eip'.3RY;r
re �alvs. Lila
CERTIFICATIONS
June 28, 2013
Pr*"I. Svey C7wad•Att O&Y (UiC)
Pu. Pro" No.. S215053
Mr- Jonathan Pfohl
Munidpal Engineering Services
PO Box 97
Garner, NC 27529
RE: Project; Surry Closed -Mt Airy(UIC)
Pace Project No.: 92159a53
Dear Mr. Pfohl:
Enclosed are the analylical results for sample(s) received by the laboratory between May 30, 2013
and May 31, 2013. The results relate only to the samples included in this report- Results reported
herein conform to the most current TNI standards and the laboralory's Quality Assurance Manval,
where applicable, unless othervelse noted in the body a} the report -
Analyses were performed at the Pace Analy4cal Services location indicated on the Sample analyla
page for analyses unless otherwise footnoted.
if you have any questions concerning this report, please teal Ire to canlact me
Sincerely,
Kevin Godwin
[e-mail]
Pfc]eCt Manager
Enepowraa
REPORT OF LABORATORY ANALYSIS
}iYr ra�I[ NY nelu l.p..K"d, ar[aPr hQP hJt.
xra,eWlNia rwarn rJna..W.rP.0 AM,Yw Sw .[n[
P.ge 1 .117
ch. 10ft C"Iffic.rwa lo.
211W Kin-Y Aye. Sr[ IOil, Apt O—ov 1., PIC 28070
With Cvdna D inbM NNilf C.r6Acalw 9' 11701
N.r Norm C.eMa NW 5ery4e2. C.AA—Von f: 5342
Nwm Cardin W"W.aNr CarYAcalwo 6, 12
5-6 C.,.m, C.rOAcanon I: "OD6001
A.h. 111. Gr11xe.11.n 10,
2225 RIV-god. Dr.. Aah.yNa, Nc 26104
F].ndLWELAP C.rditc. Y_ is E17e4
e
MauadWaarra Cu6Acm%o 6 M-NCO30
Norm Camera D In up Vapor 0"0-10vn a 37712
Pwr1d0NELAP Card6c.ii- Ee7627
Ke KP&Y ust c.M0.ar4_ a 64
M.1 Vlydra. Cer6ee.Am a: 167
VLgIn1.ArELAP Cu0c.0.n ■: 460221
Math Cwo6n. w..iawoW Crraa[allen ■ 46
Scan Crww,. C.64c.dui r: Wo3o001
Mot Va60e6 Car6A."*" 1: 156
W yMr46/IIELM C asAAcalnn +' 460222
REPORT OF LABORATORY ANALYSIS
T»r u W N Year M.I M n W.dn[ad .anPi h M,
.w r,m.i na wniyr. avna[M or P.e[AMI?W4, S.rwn[ i[,[
Pa er � n.ryll[.10.aayra. r, ins
-Alp ,wa bw io7
Hr.�,...r HC 7rn7iC
I trot. i!. yu7
Aape 2 ni 77

Paw A"ysa.51.r.1ur, Ine.
P.sa Andydw S"ce., In e-
Pa.. An dyu:18....... 1—
Pau An.I yeeel 4eMee., Ine. Pat. Anelyar.r 1 .mi"1, In e-
Per. A.My11nI i.Me.., Ine.
�p p,.,r
•�
70G E. Ahebrn RnJ • Su4A
7717 R�r.rW. Or
PM1n knc.r+W. S. ,LV
�{..,.
aceN k7
rca�
1b6 E.M WaOee d - J M A mm F..•�
Fh
iEr]Q rUc.r
�•re S.. 1w
�
yyr ca.
Ed— NC 27M
Aap.y6e- HC 205a
H.—A kC 1e0r6
_
e�
Egan NC 222M AY•.wia NC
2NOa
H.,Me."c
NC Hole
13W)623HI921
(m)2511,,F
[r'JI NIs pp9r
1
1336)6134A21 1&Ml2'54•1I75
[104j6]5•809:
SAMPLE
SUMMARY
SAMPLE ANALYTE COUNT
p"i-t
Scary C19N6MI
Aty [VK:)
Project
S—y Cl —d-M1
Amy (Old)
Paw P,.Jee1 N..
9215965b
Pec. Pr i.C1 No
921S903
LAb 10
9A p1. 10
M.Wx
0.1. Call—Nd
0.1. R-4—d
ArrA1yt.
Lab D
Sampl. IA
M.Ihnd
Analyflt
R.porled
L•Lcr.l Pry
521516A3001
M19.1
Waur
O5RW1313-35
0513011317.25
32119653002
MW-0A
Wa1.r
05021f13159:W
OW3011317:25
12154153001
MW.1
EPA6010
SHI
IS
PAS1-A
92159663003
MW129
We ter
0N24n310:4i
0513011317:25
EPAa200
MCK
52
PASI-C
1210863006
Mri•77
N,yrK
O5R911] 12:00
OSp011] 1735
SM 2320B
AES2
I
PASI-A
12I65a63006
MW19
Yyeler
8y2611315'05
OS w31725
SM 5ZI08
MOW
I
PA$1-A
92f64553007
MWAS
vVes,
owaf1311"
057301I317;26
EPA 300.0
SAE
I
PASI•A
32164663006
MW-16
Vykles
05RW1S09:40
DSflWI] 1726
SM 4WO CI-E
OMN
I
PAST -A
12169163009
MW120
VNIIM
050290010: 11S
05rMA31726
9M Si 109
SAE
I
PASI.A
02162153010
MW-Ii
0J.1.1
057291T31415
052302131725
121616i3002
MWLIR
EPA 601❑
SH1
T5
PAs!-A
32169667011
MWti
W.ler
OSR9d13 1415
0531)1131725
EPA 626O
MCK
S$
PALM-1'.
92169167912
MW7
5A\ler
0513N13 to:44D
064fn3 1423
9M 2320E
AE32
I
PAST -A
52161960013
MW9
W.ler
06170r13 11:w
OSr3M1314:23
SM 52100
UDW
T
PASI•A
42159e63014
MW-17
W.Nr
05nafl306:00
M$t!314:23
EPA 3000
SAE
I
PAST -A
921691e7014
M W-14
MMmr
ON30113 12.05
03/31113 14M
SM 450OLCI E
OMN
V
PASI-A
12110113011
MW17
V41W
mild
0531n3 M:23
SM 53100
SAE
I
PAS4-A
a2111651017
MW-20
Wa1cr
OW3011110,00
0Y31n3 IC23
1215""003
MW12s
EPA0010
sHt
15
PASt-A
102191113011
MW-21
We ter
05130f1314: 30
05131n31410
EPA 62b0
MCK
52
PAS!-C
921611VOIS
MW-22
mLer
OSf70n3 a9'.20
05f111171423
SM 23208
AES2
1
PASI-A
8M52108
MOW
I
PAS! -A
EPA 300.0
SAE
I
PAS! -A
SM 4500-0FE
GMN
1
PASI•A
SM 53109
SAE
1
"-A
12114153006
MW 23
EPA 6010
SHI
15
PAS -A
EPA 6260
MCK
92
PAS-O
SM 2320B
AES2
I
PASI•A
SM 52108
MOW
1
PASI-A
EPA 300.0
SAE
1
PA$I-A
SM 4500-C1•E
OMN
1
PASI•A
SM 53108
SAE
1
PASI-A
12169663005
MWI6
EPA 9010
SHI
15
PASI-A
EPA 1$M
MCK
32
PASI•C
SSR23200
AES2
1
PASI-A
SM 52108
MC1W
T
PA% -A
EPA 500.0
SAE
T
PASI.A
SM 4500RCHE
OIAN
1
PASI-A
SM S3109
SAE
1
VAS -A
921MIS3007
MW-15
EPA 6010
SHI
IS
PASI-A
EPA"("
MCK
52
PASI.0
REPORT OF LABORATORY ANALYSIS
REPORT OF LABORATORY ANALYSIS
1 rx. r.p.rt N.A-1 w,.Prodv_w..r[.W y
N11
Tr•r 1. KO ehN Her ne Iepod—d. expeln W.
w,.qH e,. x.pYn cvna.nl
of P.w Atilryr.r 5. rv�o.r Irti
Pmge 3 of 17
-t-1".nman eanwn! of Pace Amlltie.I Sa, N r. Ine
P1ya 4 A 77

aGeAr�lytfcal
P.0 Rnryaeal a.rvlul, IN- Pat. Anr]Mu, 9.Mw%III P.M. An.1y11ut 1.Mu., Ine.
2M E..t Mwda.' Row • SW. A 222E Na.IW. ar 9a00 KP[ar Aw 1W. 100
E Wn, NC 2 i7aa A h.,%. NC 28104 Hwau.rN-11C 26D71
jlmpo 3-aVl f8211214.7171 (MOS7'+-9062
PIG).cl SL" Got.d 41 Ary (UPCI
Pan Plogacl No. 9215485)
Lab 10 sampM ID
931SM63M MW.16
12$59153000 MW-120
921 so I53D I MW19
*2155643011 MW-16
92161665012 MW7
IZI M63013 A1100-1
SAMPLE ANALYTE COUNT
Malhad
SLI 7320E
SM $2100
EPA 300.0
SM 4500.0 E
SM 5310E
EPA6010
EPA1260
SAI 232013
SM 52106
EPA 3M.0
SM+50B-G•E
SM 53108
EPA 5010
EPA 8260
SM 23208
SM 52ios
EPA 000.0
SM 4500•CFE
Sµ S310B
EPA6010
SA123208
SM 52108
EPA 300.0
SM 4SO C4,E
SM 5310E
EPA0260
EPA0010
EPA 5260
SM 23206
SM 52108
EPA )00.0
SM 4500-CIE
SM 53108
EPA6010
EPA V60
SM 2320B
SM 52106
REPORT OF LABORATORY ANALYSIS
Ilw I.(grtNN rot G npretlue.0 .r.uPln hr,
.1anw M Iwbnuxr 1 W Pau MWyw l 14moa., lac
Ans"s
Rnaly.ta
Rapari.d
Lahm.tery
AES2
I
PASI-A
MDW
1
PASI-A
SAE
1
PASI•A
OMN
1
PASI-A
SAE
1
PASI•A
JMyd
15
PASI-A
AICK
52
PASI-C
AES2
1
PASI-A
MOW
1
PASI•A
SAE
1
PASI-A
DMN
I
P"-A
SAE
1
PASI-A
JMW
15
PASI•A
MCK
52
PASI C
AES2
1
PASJA
MDW
1
PASI A
5AE
I
PASI-A
DMN
I
PASI A
SAE
I
PASI A
JMW
1s
PASI.A
AES2
I
PASI-A
MOW
1
PASt•A
SAE
I
PAST -A
DMN
1
PASI-A
SAE
t
PASI-A
MCK
67
PASI-C
JDA
15
PASI-A
MCK
52
PASI-C
AES2
I
PASI•A
MDW
1
PASI -A
SAE
1
PA%,A
DMN
I
PA-V-A
SAE
1
PASI.A
JDA
15
PASI.A
AACK
52
PASI-C
AES2
1
PA&,AA
MDW
1
PASI A
P.G. 5 Pr 77
f
aceAWlylical
Pao AnMya64114Me41,Im P4.4 ANlyae4l a.rvral, Ine. Ma.. A.." " a """ In..
Wb E.MNI..M. R.w-&"A 2226 A.ra. Dr. Dwo Kr.c.r Ar.. 5J Ica
Ed.n NC 272H Ae.Ow NC MD4 1.wrMrM.. MC 2r170
1ualfi�l I1261254-T176 l761]6>'}9110:
5 A M PL E ANA LYTE COU NT
pm*l S—V Cw.*o-M1 At j (L)IC4
Pace PrnJaol No. 92,5053
AIIAlyl4.
LA! 10
SaIrpls ID
M.Ihpd
Analy.11
R.P6rt.6
La6erMory
EPA 300 0
SAE
1
PASI A
SM 4500-Cl E
DAIN
1
PAp A
SM SMs
SAE
1
PASI-A
911H8136fa
MMI43
EPASa10
JDA
15
PAW -A
EPA62H
MCK
52
PASI•C
SM 2320E
AES2
1
PAW A
Sm 521(iB
MDW
I
PAS! -A
EPA )09.0
SAE
I
PASI.A
SM 4500-CI-E
9MN
1
PA91•A
S1A 5)toe
SAE
1
PASt-A
12161860016
YW 14
EPA 6010
.13A
15
PASI-A
EPA 6250
MCK
52
PASI•C
am MD8
AESZ
I
PAN -A
9M 521011
MDW
I
PASI.A
EPA 3000
SAE
4
PASI-A
SM 4500.UE
DMN
f
pABI-A
SM 53105
SAE
1
PM -A
921"863016
MW47
VASCO
JDA
IS
PAVIA
EPA 628D
MCK
52
PASI-C
SM 2320E
AES2
I
PASI•A
SM 5210B
m01V
I
PASI-A
EPA 300.0
SAE
I
PASI A
5A145D0.CI-E
OMN
I
PASI-A
SA153109
SAE
I
PASI•A
13166160017
AiW.20
SPASM
JDA
15
PA& -A
EPA1250
MCK
52
PAIN•C
SM 2320B
AES2
I
PAST -A
5MS210B
MDW
t
PASWk
EPA 3M.0
SAE
I
PASI-A
SM OWCI E
DMN
1
PASI.A
SM 63100
SAE
1
PASI.A
1 ZISH5301a
MWP
EPA 1D 10
JDA
is
PAST -A
EPA 6260
MCK
52
PAS1•C
SM 2320E
AE32
I
PASI•A
SM 5210B
MDW
I
PASI-A
EPA 300 D
SAE
1
PASI-A
SM 4500-CI-E
0MN
I
PASI-A
REPORT OF LABORATO RY A NALYSiS
04 r-A*M -f d -1 b. pod Yd- nnp 0 nA.
MR-1... mifth ean. ar Pan M rYca1 S.Ir..I.. Nr:
P.D. 6 d 71

• Paw Anal yd..l 1:1..• �.. P... Anery.l.l banle.., rnr.
A4.. An=:t A.hlw., Ln[
1
Pee. An&V9..l !.Hera, lne.
P.•.
Aeelp.W &"-., W. Pate A.Nlrkal a.r.-. IM
.'25 E..I lh.r w Avae - S. • 224 R .nq.
aceRrraJytical
C•
9K)p .wr.. w. ir4r Ipp
I A ^
aCCi�flalyhcar
Ias E..r M.ep.w R..a . S.r A
2273 Fl.-.k%0. OW x.c.. Mr S•w +Dn
D-
..
E., Nc 2r7ea Mn.ril.. rrc axa4
f•nl•i r.Na. NC amia
��
ee.n. ruc 772p6
A.n.we. W 26ao4 n..,r.a.N. r.c 7eore
i I1751M-wl j4 kM4 ilia
+
IrW)Slsfrf97
Py11e216e11
1626 n4.717e r";§Ir Vm7
SAMPLE ANALYTE COUNT
ANALYTICAL RESULTS
ProNol- a1.ry cla..e-rMAry a;u>cl
alran.l S-y Clbd-Mf"y
JUICJ
Pad. Pt*y No.: 921598S3
F." pmoul Nw P216903
Anslyl•s
aanlpl.: MVJ-1
L.6171: 931ae4183091 C.fte.d 05✓2➢11313:35
R-!wed: 05A0f1317;25 M.trAr %&I.
L.64 3"k a3 M•Ihod
Anslyses
R4por%d L468n1ary
86pelt
pwo- l.r.
R•-A. L#els L-4
MIX
D:
Prep.r.d Anrff2rd CAS No Ou.l
yM 53108
SAE
1 PAS -A
921a9613019 MW-22 EPA6010
JDA
15 PASI-A
4010 MET ICP, 3029C
AnNryc•1 Me mod: EPA 9010 Pfepora600 Me"
SM
3030C
EPA 6200
MCK
S2 PASI•C
Aadm.n7
ND u9R
0.9
Sp
1
W31113 MAD 06N3f1322:57 7440-35-0
SM 2329E
AES2
1 FASFA
A,,-
No -a&
10.0
100
1
M111110:40 CM311322:57 7419-38.7
barium
22-6J aryl-
100
$0
1
W31n31040 06 IN122-57 7441!`3¢7
SM 5210E
MDW
1 PASI-A
80ryu.m
ND upA-
1-0
1.0
1
96RIIV1 +Q:40 Q6f0Y1322-" 7/40JI.7
EPA 300.0
SAE
1 PAS1•A
Cadmium
ND u9t
10
1.0
1
OSfb11+3 tD;0 06r0Y1322;Si 7A{p-A3.9
OM 4500-CI-E
OMN
1 PASI-A
Chwmlum
NO u0A
100
51
1
0S41flS 10:40 0610Y13 22:57 7440.47.3
Cobsk
NO ug&
100
5.0
1
MR1310'40 06MV 1322:57 7440.4a4
SM S3108
SAE
I PASI-A
Capper
NO ug1L
100
5.0
1
05131013 10:40 05'A7Y177237 7440.50.E
Lead
NO u911.
10.0
SA
1
0":1113 f0:40 96V3113 22:57 7439.92.1
Ml kel
NO w-
Wo
S.0
1
06r31f11 f0:40 0=315322:57 144p42-0
Selenbml
ND v94
10-0
10.0
I
OSf31nS 10A0 0510Y1S 22:5i 77a2J9.2
S9yer
ND n&
100
S0
I
W351131040 96f0Y13225 7AW724
Thmleum
ND u91L
115
S
3,5
1
9N31f1S 10:e0 08f0Y1322:57 7440-26.0
1h."um
ND.9t
Ma6.0
1
06f I.f0Ao 06103;532257 1410-82.2
7 h.
NO uglL
10.0
$0.0
1
M1113 10:40 OMY1322:57 7440-054
9260 MEV Low 1rr.1 Land1111
An.Ny l fAsmod-
EPAa2110
A-1-
NO uq+L
100
10.0
1
069&13 06:16 07-04.1
AayleN[r6e
NO .QIL
200
1.9
1
o&wd13 oa:16 107.11.1
8en2enr
NO u91L
1.0
0-25
1
05Na71306�16 7143-2
6r.meoNorom.lh.ne
Nb KA
S.0
0.17
1
Qw511306:16 7447.5
Ek.m.dl Arofom.lh.ne
NO uWi
1.0
0-14
1
OWDIV+S 05:15 76-27.4
at.mnfolm
ND u9+l
30
026
1
06*91305:1: M25.2
8rnrn.m.1hon.
NO ug&
Ica
0.29
1
Dwyl306:174.63-9
2-eufan0ne {ME KI
ND up4
100
0."
1
0505l1305I Z 3.3
Celbon dsWAd.
NO 'A
f00
12
1
0619Sv130o'is iS-15-0
Caflap• ohlonde
Mrn
ND up4
fA
0.25
1
0&05r1306:1a W23.5
Chlorpb.h2en.
ND 1191L
3-0
0.23
1
06r05113067141 198-PO-7
Chlawe6rene
NO upol
10-0
0.34
I
o6f05713o4:1a 7S-0D-3
Cfilprobrm
NO uok
5-0
0.14
1
0"511546 fe 57-68.3
C.I1Wremolho..
NO uq+L
1.0
0.11
1
0&05/13061e r407-;
1,2-D6.omo-}chbroprepme
NO L.&-
13A
2.S
V
ua10L 1105 10 06-12-8
Dwremoohwrwnemane
NO ugA-
3,p
021
1
0&0L13051e 124-45-1
!?-DAxomornena MDR)
NO uWL
1 0
027
1
06/05113 Qe.f e f 06 93 4
Dlbromem alma
NO uA
+0.0
021
1
0&O013 oll$e 74-95-3
1Z-OiWgobe.tM•
NO uplL
S.0
O.SQ
1
p&o5/u ee�le 95-50-1
1,4-bld9orsbm2•n.
Nb upJL
1,0
0-31
1
D&051130616 106-45-7
Ir&ns4 4•DkNoro-2...N .
NO 4&
100
$A
1
0620511] 06�16 1s0-57-6
1 t-01pM•ro.INne
NO ugh
5.0
0.32
1
M511306:15 75.34.3
1�-Oichlor.dh.ne
ND u91i
1.0
0.+2
1
05N'rNS06:1a Ip?-w2
1.1-Okhlvreelhene
ND uA
S-9
0.53
1
0510Sr1306:1a 75.35.4
rh-1R-OiWoroethene
ND upli
$.0
0.19
1
96706f1306:16 I36-S9.2
m tr 12•Dler4w.s0..n0
NO uvk
SQ
0.49
I
o6rOS113081a 15640•5
1,2-ow"-Qpmp:n
ND udwt
10
0.27
1
05r0'YIS D6.16 76-a7.5
1,]-0kh aropropan•
NO up�L
1.0
026
1
a610& 1oe:1a 142-2S-P
a.-1,S�d6oropopena
NDg94
1.0
Q.13
I
uGK)9306:fe soo61-01-5
REPORT OF LABORATORY ANALYSIS
REPORT OF LABORATORY ANALYSIS
r 1..raNn.h...,w 1wnV.ewced..' p.-MI.
TN... r..f m1 e...vo d. -.aka
mrn M w"M eenw.l •I Pow An.lye o 6rn+wr. Inc
Pg. 7 a117
Dsle: OSf282013 10 49 AM
vn. w . ns1 --1 Pr
P.. A7u'~ S- uw Pope 6 al 77

2cmnaMtcal'
P.a Amy".1 PNvkn, Me.
P...
A n.ly6e.l l.rrlerr, M[. P.c. Ae.Iy0e411.ry1.e4,1",
2e3 E.. W.dn. 7aed • a w.
xm n.....rd. w 6e00+1,.c4r.re .r,14 1ou
1�
F.Pn. Nt 27244
Ao1 "., Nc 2aag4 Ix.,r,arre Nc 10076
(SUIS224921
1a761254-7176 1104AM-Bari
ANALYTICAL RESULTS
Prpjael' SWWr Coasts
MIAkyIUIc)
P_ pm)&N N.: 921S9aS1
9Mnpla: mvi-1
Lab 10: 12161163001 Caft-lad (ISr791,111.15
Rec4,red 0513011 1725 Malfiv lMt/r
Repon
pot.mele+a
Reins uMh tIm1
MOL
OF
Prep-d Anety2e6 GAB Nd. Duel
1210 MSV Lew Urn Landfill
Annygtn M.Owd EPA 6260
Idan.•1.3.OwlPlapop.n0
NOuOk 1.0
026
,
ON051000-12 1006141E_9
Elhylh.n2ene
NO-Ok 1.0
0.10
1
06MIJ i3 ON: II $90-41.4
2 H6..rwne
NO u911 5o.0
040
1
0610511306:te SRI.764
o .-ghov.
ND ug& to.0
D32
1
06A611a O1: 11 to -a"
Menylene CAtonq.
NO u0& t.0
097
1
661051, 106:14 75,09.2
4 Me61N-2-penNnen.(M181p
NO uyL too
0.)7
I
MMNI104:19 IU-1011
strand
NO ugk $.(1
0.26
1
05mSI1306:Is 10042•5
1,2•TekacNarP.al.h.
NO PgA s0
O33
,
06r¢y1a 06:,i 070-20%
2•Tetrod"a.tr,ane
N0 uyl 1.0
1:..1)
,
060311306r1: 79.14•S
Tetr.chla9e11erla
NO ug4 10
0 48
1
OWW13 D6:16 127.16.4
Toluene
NO uDeL 1 D
a211
1
ORMW13 DRAII 101-60-3
i t,1-YrldMwaalh m.
NO up4 1.0
0.46
1
05m&I101:16 7145-0
1,1 2-Tnchlw0adlane
NO up,l 1.0
0.29
t
06166113 as a6 79-00.S
Tr,ydpgelhen.
NO uV& 1.0
0.47
t
06@L1301:11 72,01-6
TNCMuPAuor9m.lhple
NO ugk 1.0
0.2❑
1
D6105113 05 10 15-69 4
1,2,3•TIIcNwWopme
40 ugA IO
(I41
1
0610511309.19 9616-4
WO Icnale
ND uOA $01)
015
1
06*U00911 $08,05-4
V1.0 cNmld.
NO upA I0
0.62
1
O&OW1301:$1 75-0t-4
1(yl.ne (TM.4
NO u9A 5.0
Dos
1
OM05+13 00:f 0 1330-20-7
sweamte.
4 8t0rna6M b4Meana IS]
06 % 70 130
1
0"W1I Do 16 460404
DWrgmgWoromelhan. IB}
106 % 70-t10
1
0610511306: 16 1161-SS-1
I L2 OkMra.elh.ne-do I91
100 % 70-130
1
0"W,30916 170d"74
Tulu... �6is)
go % 76110
,
06105f1308: 16 2037,A S
73201 Alk.knky
ArWy41 M.6,od. SM 232013
Ar...n6y, Torn e. C.COS
111700 uyL 50OU
1000
1
OOf04113 14.57
6i.105 000. 6 day
An"Ical M.rhpd 5M 52100
00D. 5 Joy
2400 u9'L 2000
7000
t
DV31113 00 36 06104113 11:40
300.04C Anion. 21 I1.y.
Analylkal M.lhod EPA 300.0
Sint.[.
74004 ug1L 250000
2iw
I
06MA03 24:20 141144- .6
Ono Chlande
M.IT,Inl MelhgdSm 4500d3-E
Cloorlde
4076 pA 10D0
1000
1
004111132"a 16167-0016
631mB toc
An.IVI1c.l Malhod 5M S3,0B
T.W CrOan,c Ca L-
3710 u0�1 low
low
1
OGIOU13 17:39 7440a4 0
REPORT OF LABORATORY ANALYSIS
iN. mp'. .w W..l.edrod-..caps n ar.
D.I.. DW20*013 10 49 AM .44.nd n. r,.n1.. nm-1 el P.. hrl,lcal a.1vk... 4.e
Pape 9 61 77
• P.e. Ann mgm 3=64, Jm-
Pic. AIWIV661 s"k-, m.
PA.. An.lyhe4l aerrk... MC.
! ace Ar+atytical 2[6 64 M. a - Ft m • RA. A
72" a Rlyer.ld. O,
nrOD Fear 6 . 6u. , OD
.
ES.n-NC 772ee
Ae vM. NL 7L.l1i
k-y .,O.. He Zma
f33awmaw,
[026j75 J$m
17041175 sm
ANALYTICAL RESLLTS
Pn*.L Burry Cloud -MI Alry {Iflr•.}
Pace Rood N9-. 02159653
66plprac MVW3R
LAh iD: 12111113DOZ
Co6ecled
0U79113
D9',0
ReselredDS13001117'25 Mega VA br
Repen
Puam.[.n
Reaull. Units
L,mll
MOL
OF
NNOW.d Analysed CAS No- 41r.r
6 01 0 MET ICP, 3030C
Artoko" Mattlad EPA 6010 prop. r06on Method: SM
5010C
Anhmony
NO ug&
0 D
5.0
1
OW31113 10-45 OSMY1323.00 7440.35.0
An.me
NO UR&
t0.0
too
1
OW311131040 OGMU13 23.00 7440-36-2
Barium
NOVA
,e0
S.a
I
05f3 t11310:40 OWN 1323-DO 744049.0
leryaaem
NO ug4
10
10
1
01,3111310:40 0MV1323.00 144041.7
Ca*nw
N0 00A
1 0
1 0
1
06J31113 %040 WON 13 23 00 74404M
Chromium
NO uyL
too
5.0
1
06131113}DA0 961031i323:00 744047.3
Cobalt
NOugiI
10.0
6.0
1
=101310:40 OWN 1323:00 7440.404
Capper
NA WO&
to.0
5.0
1
Wd(31111 f0:49 OWOWQ 23'OO 7440.504
Lead
NO uQ&
10.0
5.0
1
Owl fl310:40 O61DWt3211" 7431-92-1
Nickel
NO uOfL
50.0
S.D
1
D613lit 3 10:40 O& ON13 21:00 7440-02-0
Serenlym
NO ap4
lop
10.0
1
Wa10a 1040 OMN1323.00 7712.49.2
SINV
NO ug&
10.0
S.o
I
MIN 110'40 D603M121.00 7440-224
Thrrum
NO uUJL
55
5.5
a
05r31113 10.40 06103f13 23:00 7440.26.0
V-0,04m
NO -(Pt
2S 0
5.0
1
0Y3111310:40 D"W13 23:00 7440 62.E
Inc
NO uglL
IO D
10.0
1
OSR11n310:40 0610Y1323:00 7440.66-6
6260 MSSI LoW L.ral S..n6I&
An.lylkal 1A.0%ad. EPA O26D
A..I-.
NO ugIL
106
10.0
1
0"U13 0634 9744.1
Amlomilme
NO n0A
20D
19
1
0SMS; 1306'34 101.13A
84n2ene
NO NO+L
1 0
0.26
1
091091306:34 7143-2
B[gmg N .gmelhan.
NO UA
30
0.17
1
0607150110434 74-1?7-5
&omOdldderel„e D,4ne
NO Lqk
1.0
0.16
1
WOW I]0434 76-27.4
B[omobmm
NO uyL
] u
0.20
1
06*U13 06:34 75-2541
&ama m.6la„4
RD uyl
t00
029
1
0610511301:34 74-13.9
243u14na,e [ME1(]
NO UA
100
0.26
1
D6pS1t3 01:34 76.03-3
Conlon m.Wkm
ND PAIL
Io6
12
1
0610511308.34 76.05-0
C.rbo Iebaehldlne
NO u A
to
029
1
WON13 06,34 55.21.5
Chrorolxnxene
ND VA
3.0
023
1
iWOW1301:34 1D1-10.7
CW.ro.yrene
NO 49&
10.0
0.54
t
OWN 01!34 75-00.3
Chlotolvm
NOuOA
5.0
0.14
}
D61DS71306:34 674&3
ChIPlom.n.ne
NO uA
10
0.11
1
06A5113 01:34 74,67.3
1,2-09reme 3-c"rep.ep.ne
NO wvL
13 ❑
25
1
0d?@Wl3 G6.34 9E-12.9
alheom m'Womalhons
NO uqA
30
5.21
1
D600511306:D4 124.46.1
I;2-Dkram.e04ane(ED51
ND u0A
10
0.27
1
D610511306:34 10&93.4
916r9monumene
NO u0A
10.0
0.21
1
06105113 06:34 14.9$-3
I,2-pich7PrpMnxene
ND -R&
50
0.30
1
0640511306: 34 OS50.1
IA-OicNwo6anxene
NO u0A
1 0
0.33
1
00N51130634 106.4e-7
Dam- 1,4-0Idllnro•2•bulene
NO u0A
100
1.D
1
06f0511306: 34 r10d7-0
},147kh19eo4ClAne
NO uOIL
5.0
032
1
0BA511306.34 7"4.3
1A-Okhhugem.n.
No 40&
1.0
0.12
1
0"SI130634 tar-09-2
1,1-Okmotuouery
NO uwt
$.0
0.55
1
MWI300-34 75,35.4
a.-},2•pdhwr0ethene
NO VA
70
0-19
4
06f0&1y 0434 156-51-2
11 arIvSR•dddawalherl.
NO uOiL
5.0
RAN
1
06mvI's 03 14 1S6.60.5
1,2-D6,WWgprop.ne
NO upIL
10
027
1
WOW 0614 T641-5
1,3-DkWW.W.p.n6
NO ug&
I.D
0.26
1
064W130014 142.21-9
rx.t•3.Oiehlwoprnp.r..
NO DyL
I o
oil
1
06M&I104:14 low 1-01.5
REPORT OF LA BORATORY
ANALYSIS
One. 05/26/20)3 10:49 AM
w2-1 IN. wft [en..nr m P.
Molrnral 6e 6. 1w Pepe }0 e177

■ P. AnNyd..t
�'��bl�.'i11/i` �• aNA P.. Ar.le.el aervlcak l- P." An.lyec.
on.
MSW- 5,
NrvINI, In..
T725 RNMMM Of. 96001rr.u7 Ar. e,/r ion
.w.rlr�..lea.aN Edr. NL 27]ae ANere., NL 2aa0a N..yl.r.e. HL 3607e
1 [yll pan-M, {l711761.71711 f104167&ooui
+ ANALYTICAL RESULTS
prvjecl: Sorry Ce.eeuM1 Aay {ulCj
Pece Pr.Iad Ne.. 9215"53
aempt.; MW3R Lab 10! 12169112002 C.Pode d: 05,R9113Oil :1a R..W-d: 0531Y1317:2S Mwft Vaeiar
Reperl
Prema44n
iinNlla Lr116
Llmll
MDL
OF
prepared +Nelyted CAS No 0.0
8250 MSV Low Laval Lrldflli
AnelyewI Mawd: EPA 6200
1r erM-t,l•prJrbrapropene
NO uA
1 0
0.26
1
064311] 06:34 10061-02-6
E0lyovnzene
NO uA
1.0
0.30
1
06ro5f1306.34 IM41.4
2-me.ahvne
NO va1L
Soo
0.4E
1
OONSl13 08-34 531.76.E
I.d... Mon.
NO uok
100
0.32
1
061P6l1700:34 74• "
Me Mylehe CNvride
ND ug11,
1.0
0.97
1
06l0W 13 Oa34 76-09-2
4.M.W-2-penlenme (MIBR1
NO uOIL
100
0.53
I
06I05r 1108'34 f06-f0-1
9fyL.N
NO up+L
"1
0.2E
1
ON0S1$306:34 1Q0-42.5
1,1,1.2.7�g4cMoroenan6
NO ua+L
S.0
0.31
1
Oe10615] 04:34 610.20.E
2,7-T.Y..Naoealane
NO n&
30
0.40
1
06+O51 0614 10.34.5
Tetrachl.-Ih r..
NO Ma+L
1.0
O.ie
1
06105f11 06'34 127-16-4
Tvluane
NO uWA
1.0
02a
1
06PO5f130934 1D!-l6.3
I,},I•Tr1d11we.al.na
Np uyL
1.0
a4a
i
06AW1106:34 71.55-0
1,t2-Tndllwv.Mans
NO uWL
1.0
029
1
06AW130#134 7F045
Trkhlwe ""
NO "A
1.0
0.47
1
06AW130634 79-0Id
Tru:hluvauvrPm.lhane
NO MOIL
1.0
020
1
06AS113061.34 76-69J
13,]•Tllcnloroprvpena
NO uqk
1.0
DAI
1
06iGW130634 00-164
Vinyl acewla
NO upl
$4.0
Q.36
t
06A61130634 f06-0&1
vinyl enlalde
NO -A1.0
0.62
1
06AW170634 7a-01.4
xyleru (T.L.g
NO u011
SA
0.6E
1
OM13 06;14 1330-20-7
Surrvya[aa
4-8rom d4 .benrene [Sj
97 %
70-00
1
OWM3 0634 460.00.4
dGomolWorvrn.mula{51
1a5 %
7p.120
1
06Aa11306154 1680.03-7
12.!]klAvroalhane•d{(S)
100 %
70.130
1
0W0a11306:54 17009-07.0
T91uen" f31
102 %
10.130
1
DaAWS3 06:14 2037.20-5
2320E Alkoanay Anlllyucai Me6w4: SM 232W
AlMangy, TPtpl ee CPCO3 law uA 5000 1000 1 Owl 1$:05
6210E 000, 9 day A-tyacel Minh. d: SM 52f 08
500, 5 d.y 00 uyi 20H 2000 1 OSP31113 00:36 06A4113 1640 82
300.0IC Anbm 26 Days Anelyticel M.Mod: RPA 100-0
Sulfite 3710 VWL 2004M 20M 1 061o5113 11.2a 14106.79.6
4600 Chloride Anelylkel Method: SM 4500-CLE
Chlwld. 3490uaq 1000 1800 I 06111A32027 16667-00.6
93100 TOC Aneiyvicel MPNod: SM 531 Q6
T.W OrU-I. Cerben 4120 uari t000 1000 I 06A5l531751 7440.44-0
REPORT OF LABORATORY ANALYSES
rvs ,.pars w.r nose. �p,owe:.e. ..=wl � rJl
O61e: 06+26+2011 10'49 AM .n..ew M. wnb.n eena..X v*Pea A.rrpeel Senwe.. M1c P.u. f 1 0177
P.a41In4yHeV O.Mae4, In& P.c. An.lydaV A.rvlc{., InY_
aceAnapicai r W5 E..I MeeW W head - su e. A 3273 R ef.ye
.ww pw>Jw. m. E.
kC Trye6 Ar...nn N[ 26MM
(2 )473E921 16T6N'JA-71 re
ANALYTICAL RESULTS
PrplecL &dry Gloved-M1 AYy (VICE
P.ce Proleq No.: 9215965/
Paw AnelylN.l Nmw., ]r.e.
e0001Wleer Me SJI.1�
Iraprs eaa
6empla: MW-123
Lab Ilk: 9219"83003
Ccol oWd: OWMI3 10:4a
Received' OS!'JOM 3 17-25 Man: Valor
R.W
Pwbmelen
Rommi Moir
LImB
MOL
OF
Prepared Anaycad CAS No. Dud
1910 MET ICA 3630C
Melylkol M4Med. EPA 6010 F r*PanWn
MMlwd: SM
3030C
AAtlmmy
NO ug&
60
$.0
1
OU3101310:40 06A311321.03 7440.34-0
An.rdc
NO ugA'
10.0
10-0
1
05I3111310:40 OWN 1323:03 7440-1a•2
00.1um
}7,6J uWL
100
1.0
1
1111:1:1 f0:40 06A311321.03 1440-39-3
94ry6um
NO u9+1
1 0
1,0
1
OW31113 f 0:40 OWN 3 2303 744011.7
Cednw+m
NO MAIL
1.11
10
I
01M 111310:40 MM311321:03 7440-419
Ch.-4-
NO uaA
10,0
a P
I
M."3 f 040 06A3113 2191 744047.3
CobAO
43J upfL
10.0
5.0
I
OW311131040 PaA3r1S 2SA3 744046.4
COME
NO "gA
10.0
6.0
I
OS11111310:40 OW03r1128L3 7440-0-8
Le.d
NO uW1
10,0
5.0
1
OW31113 10:40 MM31132103 7439.92.1
Nka41
NO uyi
50.0
SA
1
63r7fl13 IOAO 0!l0371373.03 7440.02.0
Selenium
NO uA
f0.0
10.0
}
051]11!] 1040 0&0]71323I03 71762.49.2
SArer
NA up4
f0A
5.0
L
0017111'1'10:40 0aA311323.1 7449-22-4
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NO uA
S,S
S3
1
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I41nad1Mm
NO vQ&
25-0
50
1
DI,* 13 10" 06A311123.01 741Ot2-2
n.P
NO ua4
10.0
109
1
054n f 7 10:40 OW3113 23.03 744046.6
1260 MBV Low Level LendfBl
Ably" al Mallmd' EPA6260
Ac61Ma
NO Lj0'L
100
11
1
06A51" %:A: 041-1
Ruylp.01r6e
NO UqA
200
1.9
1
06+O5i 13064107.13.1
Seflm6
NO uqA
lA
0.25
1
05A571109:4: 11J}2
9lamod11w0m0Meha
NO uqA
3.0
0.17
I
06AS+116a17Mg7-S
Br emodldAOrvin6Men.
ND U91L
1.0
0.1E
I
b6A51130649 TS-27.4
8ram0brm
NO ug1L
3.0
02a
1
OBIVS11306-49 75.26-4
&umemeilene
NO uWL
10.0
0;9
}
OBASf1306:►9 7441-9
2-BuL.-.(M EX)
NO ug&
too
0.06
}
nSAW1]081.4 76.93-3
CedxndlelA6d.
NO uWL
foci
I]
1
06A511300-42 75.16.0
Ca rbon tatractgaelda
NO UA
"1
025
}
c4fm 10414a W215
Chla-b-tane
NO uyL
111
0.23
}
0W0311] 06:40 706.90.7
Cnler60th"
NO uo&
10.0
0 -54
1
08l1, 0649 75-0 3
OS1
Chk..Iu-
NO uOIl
SO
U4
1
060Sf 1184.40 67-06-3
C1ltafome6lan.
NO vaR
1.0
0.11
1
0810.�t3 MA: 11.67.3
13-D9aomo- 3-chlw.rap. ne
NO ua,L
11-0
2.a
I
061M 13 QBA 9}12.6
tft m .hWom.lh.na
NO uO&
3.0
0.21
1
067O51f3014: 124-46-1
1,2.0pramvelhene IE061
NO uOIL
1-0
027
1
0610Sr13 01'A 1P6-63-4
OIN-0 edlene
NO uo&
10.0
0.21
1
M501300,40 74-95.3
1,2-D1chlorvbenrene
NO uq+L
5.0
0.30
1
76ASf1306:49 95.5a•1
1,4-0khrorvbahrane
NO upt
1.0
0.33
I
6BASf130149 10a•46.7
1.04•pehlvro-2-bul.ne
NO 00A
too
1.0
I
0$,ft.3 Qa:aq 110-514
I,I-Olcdoroeth.ns
P.S3J ugeL
5.0
132
I
06A51130649 M914-3
1,2-0khlorO.than.
NOugIL
1.0
0.12
1
OWN 30a49 107.084
1,1-004.04 the rH
NO up+L
S.0
0-56
1
75.35-4
da-1.2•dchlvladhene
076J uVL
5.17
0.19
1
610OWU$306A9
06E 13064q 156-59.2
tralla•1?•DkNarae01en6
NO uaA
S.0
CAS
1
06AWt3a 4: 1S6.a0-B
124NCN Omopena
NO %&
1.0
027
1
OW05f1S 06:47"7.0
1,1-OkMoropropene
NO'Q&
1A
0.2a
1
0610�1201149 142.26•a
de-I,Y01Walvpvpene
NO4
ua
1.0
0.11
1
06fpW130649 10061.01,t
Dow DW202013 10'49 AM
R EPO R T 0 F LABORATORY A NA LYSI S
Th...w,1. j not b. npnMura�l-..c•0 H kA.
xf amyl N. wH, ean.e.l 0 Paw Afylrewl B.r . Ix
Peas 12 6177

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9.W Ntc.y A.. 1u,.1 W
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A....- Nc 2160.
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1311)gm-W71
lexy254.1t7M
1704)AT54M
ANALY'niCAL RESULTS
p,vlrcr Burry Gta4 d-Mt Ally [V1CI
Pate Rolac1 No- 92159/53
Srmpla; MWA25 Lab ID: 02161663013 Collected OW1113 $0;45 Received: 05130,1317:25 Mott(- 1M141e,
Repr
Pa,amelerl Holder LYa6 Li,N1 MOL OF Prepared Aettyted CAS Na Oual
w.. AnN yl.al 1.rwt.., In.. Pa.. Annyuwl a. yle.., ter-
P.-Angytle.l NM 1r1ca., 1
aceAnaA4ical
ms P.m W.ao. R.� • sk"w A
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C 211
A4hwd. ND.
Ilp,yrW . W 20078
t
13YAzC -a9i1
1e2117V-7479
gnw1e,56097
ANALYTICAL RESULTS
P,.Kel. Sway Wol.d-Mt
Ary (VIC)
Pace P.l n No.. 9Z159153
Sample; MW23
Lab ID: 12156663009 C.M. ct.d 05i191 t3 12:00
R--ild. DOn011317:25 M.vh: "Ill,
Aepa-1
parr M.t.rr
Rek.K1 Vnin Umtt MOL OF
p,.pued
Analyred CAS NO Oue1
1269 MSV Law Loyal Lrrdtlll
A-4-kr1 Method EPA 625D
ROW MET ICP, 3030C
Malyllc.l Ma 9+od EPA 0010 Pteparal0n
Memo d. SM 303X
11am 1,3�Jlciaerpprrpen.
NO h"
I O
026
1
064511306.49 1OW6 02.E
An Mwv
NO ugh-
60
5.0
1 DV3111310:40 D61031132304 7440,36.0
Edhylh.nrene
ND aryl
1.0
0.30
1
D6165113 D0-49 IM41.4
IVaaNc
NO 400.
19Q
10.0
1 0513111310'40 D&ON132306 7440-36-2
2 Heea'hene
ND Y04
50a
046
1
Hew 1304A9 601.78.6
Bulum
30AJ ury1
100
5.0
1 OW11310-40 CM211323:08 7440-3"
Iodpnl.DhAft.
NO uyi
10.0
032
t
DSM61130149 74-6"
8.,^.
NO ug-
10
1-0
1 OW391131040 D610311323.00 7440.01.7
M.Mvtm. CMorM.
NO ug1L
1.0
0.97
t
OV05113 Oa-49 75-00.2
L.dmwm
12 ug ,
to
10
1 05171/13 10 40 0"V13 23 a6 7H6i3-9
a McD1y1-2-penlrnme lMl ex]
NO ug&
100
0.33
1
05/05113 01:49 we, 10,1
Chf n kI m
NO ug1L
10 6
5.0
1 05,31113 10:40 01103tt3 23:00 7440.47-3
Stylrnr
NO ug•i
131
026
1
DMW1301-49 100,42.5
Cob.91
NO u21L
106
SO
1 D5 U131040 061 VO 2306 7445aAA
1,1, 1.7-TvtlaWvoahm.
NO-uA
S.0
0.35
1
MMU1301:4Y 030.21t0
Ptpp.1
NO ug1L
10.0
3.4
1 OSl]171770:40 06143tt]2]:06 Tf10.50�
I,h,7.2-TevacMueal.nle
NO �sk
3.0
0.40
1
06195M1 00140 7",5
irad
NO 4&
10.0
SA
1 Mill WAD 09OStt3 21. D6 7439-W-t
Te4rthloruelhble
NO n&
1.0
0.4E
1
0610511306:42 127-1"
NIVW
NO 401E
501)
5.4
1 0511111310:41) 0&031112305 7440-M0
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NO ug+L
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0.26
1
06N611309.49 101.66.3
S.I►rnum
NO ug1L
100
10.0
1 M lil310:40 O"Wl52300 174249-2
1.1,1-Trlmlyretllan.
NO vg&
t0
0.46
1
061M1130949 71.55.E
SiTyer
NO uq&
10.0
5.0
1 OW3111310:40 0610M 1323-DO 7440-22-4
1? 7 TurtlI-11+arla
NO uryi
10
022
1
061M11308.40 7/-00-5
ThNaum
NO ug4
55
5.5
1 06131113 10:40 0&43113 23.49 7440-21•0
TrlcnWloaetane
NO 11g4
1.0
0.47
1
0d'0511308:49 79.014
Vfnadlum
NO uWL
25.0
5D
1 M1311131040 06@31112306 7440.02.2
irrhln oluoromedhanr
NO opt
10
0.70
1
OB105r 1308:49 75-694
Inc
NO ,A
TOO
100
1 OW3101310.40 0"101123.015 744D-W-B
1.2.3 TnohlvtppOpuh.
NO vgA-
1.0
0.11
1
05m6t 1104 0 91-11-4
Vnyl ..elate
NO uWL
60-0
0-35
1
DEJOW .10E-i9 100.OS-4
1260 MBV Low Level Land11N
MmyticaI Method. EPA 926D
Vnyl eNwid.
NO 491E
I-D
0.52
1
0110w; 3 61-49 70,01-4
Acel9ne
NO UO&
100
10.0
1 O"SH3 00,05 67-64A
Xylend [Tdt.f
NO Yg&
5.0
0.1E
1
06105113 01:19 1330-2D-7
Ac l-While
NO uglL
200
to
5 Dam 13 09(15 107-0-1
36froliaha
9.nran.
NO ug&
la
025
1 DN061130105 71-43.2
4 Sromoluvra6m2ene (5)
102 %
70A30
1
0610511301:41 460-90.4
Bro.Iwcldoremelhrn.
NO ug1L
0.0
0.17
1 0"501300 as 74-973
Olbrnmuwwomainane l5)
412 %
70-130
1
061 W1 01:49 T666.53-7
gremedwerwn.lhrn.
NO ug&
1.0
0.1E
1 DLVUI30905 75-27-4
1,2 RlGllwvelnu,e•ei IS)
103 %
70.130
I
0&0511300.40 17000.07.0
8lomoh.m
NO uWL
3.0
0.2E
1 D"511309.05 75.25.2
Tdvene-da (51
91) %
70-130
1
O&O5J 1301:41 ZD37-26-5
Brcmomethma
NO ug&
10.0
0.29
t 0610WI309'.05 7443-S
3320H AJO.linity
Mlilyll l Me111od. SM 232DR
2-Wan.n.(MEN}
NO kg&
100
091
1 0610Y130905 76.93.3
Carbwh'K.VKde
NO uOR.
too
1.2
1 ubmsf1109.05 71.150
P1e611nity, Total at C►CO3
72500 uWL
Woo
1000
1
06N4113 1t 07
Carbon t.1-Nwlde
NO ug4
1.0
02S
1 061051I0 09:05 SS-23.5
52100 BOO, 1 dry
Anmyucrl Method.
SM &2Ifla
Ch*.bentene
NO v04
10
023
1 o"WI S 09-05 16a-90-1
Chtorve0-
NO ug0.
10.0
0.54
1 Wow" 09:05, 76-00-3
E00.5day
10700 ughL
2000
2000
1 p if00014 061041t511-46
Chlvrolwm
NO ugA,
5.0
0-14
1 06rOS1I109:05 5746.1
Chm'."Iban.
NO 191E
1.0
0.11
1 D61Dw$109:05 74.67.1
SD0.01C Anlva.t 76 Oryt
AnNHlctl M.Nad. FPA 300.0
t2 Dkh,-u-3-Wc,np,.pme
NO Z-
130
25
1 D61OS1 T309:05 96.124
SWIal.
41200J uU&
500000
40Do
2
D61W131141 $41011-11&1
Zabror+WdllerPmee+ant
NO ug1L
3.4
021
1 DWO51110905 Q949.1
1,2-Diu..-man.(EDE
NO ug&
1.4
D27
1 06)05r1309.05 1D6.134
4600 CNatld.
Anelyl.cal M.9h.d: SL1 450D CFE
OIW-m.t h.n.
NO ug1L
10.0
0.21
1 0&0511109:05 74-05.3
CIIIerWa
3230 udL
10p0
1000
1
06tt11132029 16167.006
1,2-Oldit.rah.ntene
NO ugk
4.0
0,50
1 0610511a 09-05 MOO
1,4 iNchluroben0uha
NO vglt
1.0
0.13
1 O&05r1309-05 10546-7
9316D TOC
Anrtyllcal M.Dhdd. 5M 53100
Iran.-1,4 Olddoro•2 bulene
No ugh[
100
15
1 0610511309:05 110.976
Tula Ol genlc Cam.
3010 ugrL
1000
IOOO
I
06105tt316;05 744"4
1? 4)ICNa oetrbn.
0,37J uWL
5.0
0.32
1 OQNSr1309-05 15.34.3
1 ,2 IDlcrnv,oelm-
NO ugk
1.0
0-12
1 OW0511300:04 107.06-2
1,1-(]Ichlprpelha:ne
NO uD4
5.0
am
t 0610$1130905 75,351-4
d.-1,2-Ochlvrvetlene
0.71JugL
5.0
019
t 6WWI3DO. DIS T56-511-2
N►m•12.OIrNwo.lhane
NO ug&
&0
OA9
1 061 "30905 t56.605
1 ,2-01CIhleraprvpene
NO ug1L
1 D
0.27
1 O6A5117 D9.05 76-07-6
1,3-OlplJoroprppene
NO uglL
1.0
02D
1 061M,11309.05 142-29-9
tlPl,]-OIrJXvroprvp...
NO ug&
10
0.13
1 461(1y 13 D9 D5 t0061-01-5
REPORT OF LABORATORY
ANALYS13
REPORT OF LABORATORY
ANALYSIS
T u =ewed.tro...up1 61
. ..mn.n.1 - a +vvevc.a ....w.h e,..
Dole: 0112lfd413 10:49 AM
...raw N�...h.lYn r.+�xM .r P.- W Wr" S.=. hrc
page 13 9171
[)pie M12612011 10 40 AM
h..r.ad 1n. w.rn.•• can..m
or n.c. M Iyr S.-'.
I- P.D. t4 9177

P.- Ar Vbm.l a4M[ar, Ma- P... AeelyLa41 aewi..a, Ina
Paw AnNyum aervinr, Inr-
aceAlrWy[icala
Whf et)A.4 ftmd - a .A
2??a iti&a om0.
9600 R, Ar 5W 100
.-
. ur
Eden. NC 2126E
ANeHM. NC 26W4
Hunirrwlre- NC W076
{1Mi162S-6921
ra2d)754-117e
[RAPIS- tl92
ANALYTICAL RESULTS
pm*t: Sorry Cieaed-Mr My (UIQ
Paa ProNol No: H215965}
Eawil": MW23
LAID 10: 9216916300E Cdliaclmd: QW2911312:DO
RLealYad: DA13M131725 M.1.4 YNtdt
Reporl
Parameter.
ResuKa um b LWMN MDL OF
PXepMad
Analyzed CAS No (lull
9264 M3V Low Level Landfill
Anarylkei Me9wd: EPA 626D
Irani• 1, 3.O+dlloroprnpene
ND VON.
10
0.20
1 00=1109.05 10061.02.6
E6lyban ne
NO v04
10
O,3r1
1 OSM5113 Calls 1DD.41-4
2-Maranon.
ND uyi
50.0
0-46
1 01370511399.05 591-70-0
iodunw1hane
NO uu�L
10.0
912
t O6ASr1a WAS 74 "
Mathylane CNwlde
NO uyi
1-0
D-07
1 DM0511309 as 75-09.2
4-Ma0iyt-2-p..W one tWaK)
NO Von-
100
0.31
1 06N511a 0905 106-10-1
Styrene
NO uWt
to
021
1 O6 WI109:05 IOW42-5
1,2-Tekdehlwneth ne
NO uO&
5A
0-33
1 OFW511309:06 630.20.E
1.1,2.T-Tebachlorae Ilene
NO ug&
3,0
DAD
1 06195713 D9A5 7W34-5
tabadhk o.th ne
NO ugM1
1,0
0.4E
1 06M6113 09:05 127.1E4
Toluene
NO ug1L
1-11
0.2E
1 DM0M 1309135 t06�3
+,1 $.Tridllmaetnana
NO uyL
1.0
0.40
1 OWNI309A5 7135.E
1,1,2-YnEhbroemarle
NO u91L
1.0
0.2E
1 06PoY13 Do 05 7940.5
irldltuoeNane
NO uG&
1.0
0,47
1 06A3111 09:05 79-0t-6
7AdlhxeLuvremeihane
NO n&
I,0
0.20
1 ofilmld 09-05 7""
1.2,3•Trkhlwoplopane
NO uqh
1.0
1)0
1 OfieW 1309A5 96.18-4
vino o"tel.
NO uWL
50.0
0.31
1 O6ASr 13 M.P: TWUS4
Vk.A N lomd4
NO .14
1.0
11.
1 OW0613 09U5 me 1.4
Xyienm (Tolall
NO uWL
S.a
0,6E
1 061D5113 09:05 1530-20-2
Surmparaa
4.8romalluo.4eenWe (S7
>M %
70-130
1 06103113 01g0 AGO -OD -A
ClhrpmalWoremeihana 13)
102 %
10-130
1 0610617309 D5 1681-53-7
1,2-Okhlaraelhane�4 15>'
95 %
70-"0
1 06N5113 09 06 17060-01-0
Tohrene-d6131
100 %
70-00
1 061051Ia 0905 2037.26.5
73200 A1kalMlty AnalyWal MLewd. SM 23208
Alkol Ilty, Total e1 CoM3 11600 ulpt 5DOO $m 1 D6N4113 11:50
6210E 800, 1 day Anelyncal Mo6w4- OM 52108
BUD, Sday NO uV& 2DO6 2000 1 OW11130036 06104133111 0
300-0 IC Anions 26 Days Anolywol ►Xalh.d- EPA 300.0
S1rHate NO og& 250HO 2000 1 061 uQ 16:22 14606.79.E
4a00 CNPrtd. Anaryu�an Method: SM 4500-C1-E
Chlagda 3IN upR 1000 100 1 DYWI320:20 153674*6
HI as TOC AnaWol Melhod SM 5316B
total Organl. C.rb.. t440 uA 1D00 IQ" I 0"Wil IIIA9 744044-0
REPORT OF LABORATORY ANALYSIS
T ti..-A NN -IN re0rvdi.c.d.....M n M.
Dale: 0M W2013 1049 AM Pace A Vli 1 9emw.. t�
P. Xe AnatydNr atr.l.n, Me. Pan An[Iyllmal Lauren, Ma P. a. A-ynul IW We•M..
(�Z
Ana�ytica� a W5 Ea w.m. Ro-d • auN A 7225 Rkrad.0, WW Km-yAre 5.+. Ipl
xwyuYea can Ed-. NC 212M iu&I.WW. we 2aeDm 1a,nsrwA.. MG 2201E
1nCA23.6921 (WAR54-7176 t7041L159t60
ANALYTICAL RESULTS
ProlacL Su1ry CIo..WMt Airy (UIC)
Pmu Pr91ad No- 92159653
.ample: MW-15 LabrD: 62161660004 Ce1Icc3ed: OU201131s:05 Remycd: OS11Nt3+1:25 Ma7rl.:VARer
Repo"
Pnrnme14rl Raatdis LIN11 LrmR MOL Or Prepared An aly2ed CAS No- Owl
6010 MET ;CP. }OOC
An@WAI Mm1hod! EPA6010 Ptepatalla6 M61h00: SM 30MC
1H6mony
NO UA
6.0
5,0
1 MV1310:40 OMY1321:10 7440.3E-0
AmW-
NO uOrL
1010
VOA
I OW31113 10:40 OWWI123!10 7440.36.2
Barium
26.7J Vg&
$00
SA
1 0M3111310'40 DWY112310 7440.30,3
Bary9erm
NO u04
1.0
IA
1 OW) 111310-40 0610111323,10 7440.41.7
Gadmlum
NO VWL
1.0
1.0
1 OS13111310:40 06/031132310 744043.9
Chm hl
NO uyL
10.0
SA
1 Of In310.40 0110311323:f0 7440�47.3
Cohm6
7.3J UA
10.0
5JI
1 06131013 1O41) 06MU13 "Ad 7440-40-4
Copper
NO VA
10A
5.0
1 05 V13 to:40 0610}713231a 7440-541•8
Lead
NO uyi
10-0
5-0
1 OW31 ft310:40 OM 511323:10 7438-92.1
Ml Iel
NO uOAL
50-0
SA
1 061311531D%0 05MV1327:10 74404n-C
Selenllrm
NO u9R
10-0
10-0
1 Wa I0310:40 0MV1323:10 7782a9.2
SINer
NO up,L
10.0
50
1 OW31FI110;40 00MV I323:10 744042-4
TnalXwn
NO VA
IJA
5-5
1 M10310AG 0610311323: 10 7440-2a-0
Vanadum
NO uq4
25.0
5-0
1 054111310:40 WWI 23:1D 7440.62.2
zm[
NO u9&
10-0
10k
1 MI 1111040 060OW1323 10 744D404
6260 M5V Low Level Landfill
Analylkal Modwd: EPA 8200
APelnne
NO u9,L
1DD
100
1 Od06tl309-1 E7.94.5
A4rXlpmnac
ND v9A.
200
1-9
1 %A751130911 107-t3-1
8en2.ne
1-& OOL
1-0
025
1 06M5r1309'21 71.43.2
BfG1110eh1D+eme barN
NO uck
3.0
0,17
1 0610511302:21 74,07-5
8romadddwoma9une
NO uOk
to
0,1E
1 061071130'21 75-2114
8FO-001m
NO uqA
3,0
0.2E
1 DOASfl3 09:21 75-25.2
8rempmalh.n.
NO up1L
10A
0.21
1 ONO51130921 74-03.9
2-Butmnona(MEK)
NO u01L
10D
0.96
1 DBMN130921 7663-3
Carbon d.W6dc
ND u1A.
100
12
1 MM5113 W21 75-15-0
Cmr4a+ IoCaChlm Ida
NO uD&
1-0
0.25
1 06l071130921 5643-5
Chlprdb..r...
2-21 uOfL
3A
0.23
1 064YJt30921 101-DO-7
Chlow.th.ne
0,67J u911
t0.0
0.54
1 oM051130921 75.00.3
Chlarn form
NO uglL
5.0
0.14
1 ON0511309:11 67411-3
CNmomari.na
NO uq+L
1.0
03$
1 06M51130021 74.67.1
I x•Obramo•3-chiorapeopanc
NO nk
13,0
2.6
1 0510511309'21 96.12-6
DhNomoehJcicmelhana
NO ug1L
3.0
021
1 OGAWI30921 124.4E-1
1,2-D16nomoa6rmne IEDB}
ND uqh
1.0
0.27
! OBA511349T1 10B-p]J
Dlvornomalhsn
NO 4&
IO,D
0.71
I 06/ W 309:21 74.95.3
1,2-D+chir benzene
NO OR&
$.a
0.30
1 0"W13 09,21 16-SoO
1,4-OirNmoben2ene
1,7 uplL
1.0
0,33
1 01'mi30221 $06.40.7
tr-arla-7,4-Okhlprp-2-bu[ene
NO uA
100
1.0
1 Waif 13 D1.21 $10.57.5
1,1.Olchlaoelhane
31.2 UpA.
5.0
0-32
t 96M50I 109!21 75-34a
12-UicMwp.dune
0-663 uO(L
l A
0,12
t 061"13 W21 107.06.2
1,}•Ok:hloroslhena
2.6J WA
5.0
0.5E
1 0610611309:21 75-354
do-1,2.Okhlm oa then a
36,9 uA
5,0
0,10
1 06*U$a 09:21 1S6-4S1-2
Iran.-1,I-OIP7dPr p elh ene
DAN OWL
6,0
0,41
1 DMY1309.21 1%-60.5
1 ,24)kldoropropane
NO uOR
$.a
027
1 061050309:21 71•E7.5
1 ,3-0IEtaorpprepane
NO OWL
1.0
026
1 01N51130921 142.28E
da-1,340iddorrgaapene
NO up6.
1L
0-13
1 pa1D511304:21 X0061.01.5
REPORT OF LABORATORY ANALYSIS
Ttra rerun W,0 -1p r.P"-d. crept r, rW.
Pape 150177 Do% OM26120131 OA 9 AM w..wA a1. wMYncm..marPau,a..rXec.ls.mc.e.I-
P.O. 19.117

•
P...Nn
Pace 4.0ye.ar X.-A.
A.Mylealw1-
aGpAnalytical
2m 1.1 Mc.d Row arxl.A
2xx6 nw.nw dr
9e0o Milear Axe. alw. 100
.
E4. NC 27M
a}h.vH., NC 7S6W
Hu�rgnl.- NC ]W7e
jmojan m9
r628y264-7174
I7"Amo002
ANALYTICAL RESI3LTS
Pre3ecl Svrry Clav sd Ml Aay NU C}
Pew P,cOd No.. 0211,9853
smmp1.: MIN-16 W 6 m: 02181881001 Cc6matad: 0512WI115-05 Racclyed: QSIS0113 1725 Mack: Nhkr
ROPM1
Pummeten RA4uI1. L"kt LW MDL OF Prepmred Anelyaed C119 No- O11e1
8210 M5V Law Level Land NN
nape•1,1 Drcntarapropsna
EOhyGuniene
2 HeA
7Gdemethme
Me lhyl.n. Chlwld.
4-Melljy1-2-pmWmne (MISK)
Styrene
1,1,1-0 Teaewwaenml.e
1,1.2,x-TelreeMoroetliane
Telreehloroethene
Toluene
1 i-1-rrlanl�eent.n.
1,t.2-Trlonlmeem.na
Trad,lm-khm
Trkhloro0uolometlnn.
1),3•hlmluapr9pen4
V" mcelare
VYryl CN&M.
Xy,ene (TWA4
Sur7mpah.
a•BranwWwetwltene Ig1
[1lhomoWprpmWune 1S1
1,2-171cmmomrhanm 44 15]
Tnkie Nll (SI
23200 Alk.Lnity
Nhmmraify, TiaW as CaC01
12108 BOO, 6 day
ROD. 5 day
390,0 Ic Anions 28 Omy.
Sv1M1e
4 a00 Ch/ kW
Chlnmda
43100 101C
Tale, Or panic Cae6an
AfWplval McMod: EPA 0260
ND u011
1.0
0.26 t
MOW I109:21 IMI-024
ND v01L
1.0
0.10 1
06m5f 130911 500-•11.4
ND vUIL
M-0
0.46 1
D"lie 130P.21 SOT-75.6
ND utpt
10-0
0.32 t
D51050T3 W21 74-864
ND u011
1.0
097 1
0610W t)0921 75.09.2
NO ugOl_
100
033 t
p6J06ft309:21 IQS-Wl
ND v04
1-0
010 1
06/05/13 0921 10042.5
ND veft
a-O
0.31 1
WOW,I OR21 83111W A
NO v01i
3.0
0.40 7
oOJo5113 v7:21 71.34.5
1.1 u01i
1.0
0,46 1
06/05/13 oil 21 127.16.4
NO vt?L
10
026 1
o&OL130221 108-6a1
ND upR
1-0
0.41 1
06JOU,309:21 71.0-5
NO u01L
1.0
0.29 1
061051130921 70.W5
3-4 u01L
1.0
0-47 1
05xsr13 C921 79431.6
NO u01L
to
0.20 1
D"W 13 09 21 75411-4
NO u0R
1.0
041 1
(mm 3 Oliji 961a-4
ND ugL
50.0
035 1
064WI10921 101-05.4
1.4 eyL
1.0
0.67 I
DGMWI30921 7641.4
ND u(piL
so
0.6E 1
061051130921 1330.20.7
971i 70.}30
7 04N511309]1 460-00.4
97 TS 7D•1110
I 06705f13 as 21 1666.63.7
99 14 70.130
1 04M" 3 0921 17060-07• D
103 % 70.130
1 Oolnt3 09:21 2037.26•5
Analylkal Method. SM 2120R
67600 u91L 5000
low
1 08104113 t2:OD
AnaNIWAa Mamad: SM 521 OB
NO Opt =l
WOO
1 OU3111300:06 WWI IS 40
ArmMkol Mm61od: EPA 100.9
NO upR 250000
2000
1 08J05113 Wu 1480E-79-11
An 41.d M.1hedSM 4500-CiE
1100 "WL 1000
1WD
1 =1101320130 15967-00.6
AA."mi Me Mod. SM 50100
11796 eOk 2000
2D00
2 0"W1308.18 744044-0
REPORT OF LABORATORY ANALYSIS
rH. rapoH thee -1 M ferroduieA, ..Leal n kA
D.L. 06J2812.013 W49 AM .new,1 lh ..m.n eun.anr.r P.e. Am1vWel rho Asti 1x. Pao. 17 al 77
PAC:
aAnN Weal aeMen, Ir
Pave Analytical IIA.wea r, rnv-
Pa e. AMlylie.l
acemalytiml•
]ME..Ir a --ROW •eW.A
�73Rr. w. Or
100M of Are 6,A IM
__.
Edan-NG 172ea
Aaha.w-ac 78a04
arc 7101e
P3 pl euh
fffim)mi 7h re
17641S7e 911BS
ANALYTICAL RESULTS
F .Ject. saf y closed -MI RW I111C]
Pact Propd No 9215/051
samplel MYV•19 La6ND. 02119863007 Colk-cled 0517WIl 11:25 R.CMVed: OWW317:25 Ma1r1. V4$.r
Report
Aaremmlen Reeuea MIt6 Ufrdt PAM OF pr"Wo An*zmA CAs No. Oumi
a 0In MET ICY, 3030C
AnIM-Ir
Aim.mc
erwm
ewyswm
Cedmlum
Cht-Wum
COUSIN
COPp•r
Lead
Mchal
stiank m
S4yer
TWA-
lAl1md um
zi-
1210 MEW Lew L...1 Lmnd1N1
Acelvnm
Acr wwvllm
Benzene
Rromochra=(hmne
&omed chlommem.ne
RfOm ham
Bromorr141hane
x-aInanona 1MEKI
C.Ihon O.WFde
C.hbon 1.1t.dl1olide
Ghldro6en1ene
ChW1oe0Man
Ch1Pra4Orm
Chlere mehme
1,2-0elramm• 1 •arwrep. ePenr
W6rom chimomethane
1,24 Wamee thane(EDBI
DWlomemelhmne
12-0WilaFo6anxene
f ,4 •dchror Pkmnimne
U W -! ,4-Olchloro-0-0ylen e
I,1•Dktdwodthalx
1,2431.Nm oeMh
1,1-UtcNoroelhene
cH-1,2-Dldhlaroedhenm
Iran.-1,2-Otdhlareem.na
1 2•Dkhlo.aprvpene
t,3-Drehloropmp.ne
.6F 1,1.OIdAoroptopm
(h,e: 0612anill a 10:49 AM
An mlylltal Mc1wd: EPA MID Prapmr soon Mmlhal SM 3Q30C
NO ugA.
6.O
6.0
1
05/31113 10:40 0"311323:13 7440 X-C
ND vOIL
100
10.0
1
ONVI13 11140 06N3113 23:13 7440.30.2
612J u01L
10D
6A
1
OSR}11310'4O 06f0311323-13 7440-39-3
ND upti
10
1-0
1
CW3t11310.40 OWp31132):13 7440-41-7
NO u0A
1 D
1-0
1
0673111310:40 06JWW 131113 7440-43.9
ND u0&
IO.D
5.0
1
05131J1110:411 O"V 1313:11 7440-47-3
6.4J 091L
ID.O
50
1
M111310:40 OWW1323-13 74404a J.
NO Ia01L
I0.0
4.0
1
O613III 110:40 06f03J13 23-13 744D-SO4
NO p01L
10.0
5-0
1
OW311131014D 06r03r1323-13 7439.02.1
NO W1L
S0D
5.0
1
DS131,13104D 06mu,:123-13 7440-02-0
NO UWL
100
In
1
05731J1311140 OsMVI323-13 7762-49.2
N13 Ilp1L
10.0
5.0
1
040111310:40 0610:01231a 7440.22-4
NO Ia04
5.6
5.6
1
OUM11310:40 OW3r 1323r17 7440-28.0
3.7.1 VWL
25.0
6.0
1
ON31113 10:40 06N3113 23.13 7440,62-2
14.1 uDfL
10.0
100
1
OW11113 10-40 MMU13 23.13 7446-H 9
Andy6cml McAod: EPA 12aO
NO u0a-
190
10.0
I
06A75113 09:37 6744.1
NO uQR
200
1.11
I
OAIOSfl3 W137 107-I3.1
ND"OL
10
025
1
08JOjf 13 D737 71.43-2
NO ZL
3.6
0.17
,
06fn$309.37 74.227-5
NO uOR
1.0
11.18
1
06105rt111L37 75274
NO UO&
3.0
026
1
0610S1t309:37 75.262
ND u07L
10.0
(129
1
06A51t3 W'37 7443-9
ND u02L
f OD
0.96
t
06N5013 00:37 7693.3
NO ug&
111D
1.2
1
O6w7 100:W 75,1E4
ND ugA-
1.D
026
1
OBNyt309:37 5623.5
ND Ip1L
3.0
0.23
1
06f Ia09:37 106.90.7
NO u9JL
10.0
0.54
1
OBN91309]7 75063
ND ugA.
5-0
034
1
06J061130917 67.4.3
NO uWL
"I
I'll
ll
1
DSWI3 OO:37 74•97.3
NO Ia01L
11.0
2.5
1
Dams$1309:37 16.12-8
NO uplL
3.0
0.21
1
06/01/13 00:31 124-4a-I
Nb uO✓<
1.0
0.27
1
0613 0917 106 93-4
NSJ
NO ugA
f0.0
0.21
1
06NG1300,37 74-95-3
NO u0A-
S.0
00.30
1
D6aF ,5 D1'37 9540-1
NO uDJL
1 0
0.31
1
udmu1309.31 106-46-7
ND u01L
100
1 0
I
OR105113o9:37 1f0.57.8
2.11 uWL
5.0
0.32
I
bowl 30217 MN-5
ND uWL
1.0
0,12
1
ON051130927 107.0E-2
ND u06,
5.0
0-56
I
GUMI309-37 75-35.4
2.1J uyi
6.0
0.19
1
WWI300-37 1s"04
NO uOA.
5.0
0.411
1
WWI 309:17 16640.E
NO Up&
"1
027
t
0610511309-37 7a•87.5
NO v01L
1.0
0-28
1
o6706r 1109:17 142-2&1?
NO vD1L
1-0
0-1,
1
WWI) 09:37 10061.01.E
REPORT OF LABORATORY A NALYS IS
IH. r.pnn wM nor w,.P,"m ad.. pu
w ah
raeflea Wwnbn cementer Pe- M AIV a 8.= IRt.
Pmpe l a of 77

p.e. An41 yeas, SeMcea• Wc. P... Anmlya..1 EWIn1• Inc. PN[a An4tydaat e.NkGi I. Ina-
aceAnalytrcat•
�5Em•IAeaAyRP.tl-S.
22%P.-W.Or
9d.10kinP.7 A.a $u1.+00
..
Eam. wl 22TSa
Aererne. Nc 7ee0.
Vt„nwr.rd.. NC 76D16
1336A73d421
1a2m1E44-7175
fl W la mwaz
ANALYTICAL RESULTS
ProJeel: 9urry Ctoeed•Ml Amy lu,ci
pa" project Ne-: A213ge53
EamlpNm: mw-10
LahlD: 112181663007 CaAscted: MVI311:25
Rawly4d; 0513011317:25
MM1k Vkler
ROPa11
Paremalara
Romdta l.mdis UnID MOL DF
Prepared A..ty,rd
CAS No. Duel
6380 MSV Low Loral LmndT16
Anm"y l lh": EPA6260
vane• 0 D,cw-owepe"
NO "&
1.0
0.2E
1 OVON13 09-17 $0011-02.6
Ethybea30ne
NO OA
1.0
Vill
1 D6-DW301;37 100-414
2-Ho.anone
ND vuA.
50.11
0,4E
1 mu13 O 37 %1.76.5
odamalhmna
NO rg2L
10.0
02
t HfON1309:37 74�5i
Ma1+yl one CNwwfe
NO uWA-
1.0
0.97
5 mmw 110:37 76-09.2
4•M.lh,i-2•pa npmnone IMI Bky
ND UA
$D0
0-33
1 06A1503 09:37 106.10.1
Styrene
NO UA
IA
026
1 061050309,37 10042.5
t 1,1,7.T.b acnlvrae Gene
ND vg+L
5A
0.33
1 0NI)513509;37 60Q-20-e
t,1,2,2•T.ked+leree thane
NO ug -
SA
0.40
1 0NOW 309,37 79.3a-S
Te tr.chloroelpena
ND upiL
1-0
0.46
1 0610511309.37 127.18-4
7dlumne
NO vg2
IA
0.25
I ONON,1037 10644.3
i �,1-7d+3.lorde9.me
ND ugl-
L0
0.4E
I OOM6d1309;37 71.55.6
I.1,2-7rlkhknnalhmna
NO.0A
1-0
020
1 OBMSH309-37 79.00.5
Trkhloroeth.ne
ND WA
1.0
0.47
1 O"VI3 as 31 76.05.6
illchlaraAwpam.11ane
MCIvgfL
lA
121
1 D&D5f170137 7""
t,2,3-Trtcnbreprapana
NO uA
1.0
0.4I
1 M051 309:31 56.1E-4
V*A 2 el.16
NO UA
60.0
0.35
1 06MV13 00:37 I05.0&4
V.0 cNollde
NO uQ&
I.0
0.02
1 O61OSI53 00:37 7S•01.4
Xylane tTWmp
NO upA
5-0
0.46
1 06/ON,3 09.37 1310-204
S,lo-paema
4-&etno Aupe6en4ene lSl
91 x
76130
1 0610511309:37 460•QO.4
O,MOmvauwame0.mne l S}
107 %
70.134
I OS10511309;17 1666.53-7
1,2.OlcntaEoettyne•d4 (S)
103 %
70.130
1 OMNI109,37 17060-07-0
T*14R1-46151
101 %
70AM
1 O6A51130937 2037.26.E
23308 Alkellnlly Anelytled A111hod; SM MOB
Almalnlly, T91N ee CaC01 20100 ug1L 5000 1ODD I 00M4113 12-11
6210E BOO, 5 day Ansly"I Mm9,md; 69 6210E
9OD, S day NO ugR 2000 2400 1 0513111300.3B 06+041f 3 16;44
3 DO.O IC Anlenm 25 Daym Allalytkal Mm"7 EPA 300.0
6W1.1. 2060J uyL 250000 2m 1 MAM13 WAR 1450E-79•8
4300 Chlewd. Ano"mi Method: SM 4NQ-12-E
Chlondr 2150 uglL i000 ION I 061I1n32011 16667.06E
6110E IOC Anahlloal Mnhdd: 5k1 53IN
Tote, Organic Carbon 3140 00t 1000 1000 1 Oct=" 11-56 7440i4-0
lace
P,.e Aivly9¢w eeMv.t, Inc.
w... An "-15-1-, Inc.
pas. Anatyuaat lwtses, Ine.
Analyfica�
A
D773 RNxW. Dr
gam 1[Rti� Ar.. SW 1C/3
NC 7179e
AN.r11a, NC 24MP1
rpmy mae nC mm
i130M73d92+
Iar p7S1•Tt �
ITW M15.>IO117
ANALYTICAL RESULTS
Prejasi: S.Fy CIo.a6Ml Aky (UPE)
Pecs Project No.! 9215051
Smmp1.: 119156
L.e 10r 32159153001
CW*u.d ON1911300 Aa
R-k-d: 05tl30I1317.25 Metre.MI.-
Report
Pop ... le.
Remul[e Lrwbl
1Lre1
MDL
OF
Prepared Anaty.ed CAS NP. clum
6010 fAFT ICP• 1030C
Analytical Method: EPOk WID Pr"Fa99n Me010d: SM
3D30C
A.11 n y
NO ugfL
0-0
5-0
1
Or 013 10:40 0&*W 13 23,51 7440.36.0
Anshle
NO ugIL
10-0
10.0
1
0613VI3 10-40 "Mull 7440.39.2
13WNM
11.5J UWL
100
5.0
1
OS "13 10-40 D%4)N 123:!1 7410.3F3
Baryllk-
ND bp&
1-0
1.0
1
0E13111] 10 4 0610311121:5, 7440i1.7
Catlmmlm
NO wk
1.0
1.0
I
MAf113 10-40 D6 v 323:i1 7440.4"
Chmmm.m
NO VA
10,0
5.0
1
=III310:40 0610511323t51 7440.41.3
ro"m
NO P94
10,1
1.1
I
0"""1310,40 "NONil323:51 7440-06-4
Copper
ND uyi
10,0
5.0
I
0E71fy13 10.40 Oe1O511323;51 744E-50-5
Lead
ND uA
10.0
S.O
t
ON`31y13 1OA0 o6msfla 23151 7439.92.1
Nickel
NO uwt
50.0
5.0
I
MISIH310:40 O&M 1321:61 7440-Q2-0
Selmnlvm
ND uOt
10.0
10A
I
Malta $0:40 041061132161 778249.2
51Nw
ND upo-
10.9
5.9
1
MI 310:40 06f0611321,$1 744O-i2i
th.INum
7s v¢L
S•5
S-5
1
Min 310:40 0)WVWt321:S1 7440.25-0
V.nmdum
NO I,w%
25.0
5.0
1
MIM310:40 05+0511321:" 1440-02-2
Ilnc
NO uGlL
10.4
10.0
1
OWII1310Y0 06M511323-51 7440-66-6
6166 MSV Law L.yeI L-Win
Analylk:al M.Mad: EPA6260
Acetone
NO uQ&
1DO
10 0
1
08/01013 09153 07-0i-1
Auylordtrlkr
NO uA
100
1,0
1
06A515106:53 101.13.1
Ben:en0
NO wwL
1.0
O25
1
06 N$3609:53 7143.2
&emod»eremNhmne
NO uyL
S.0
0.17
I
06MS14301:53 74.97.5
&emodchlerommNene
NO u0R
1.0
0-11
I
D&ON,109; 51 IS- 7�4
1 ,,z,rm
NO uryi
3.0
0.26
}
0"NI309'53 75-25.2
Bto "1h Ohs
ND Ypd-
$0.0
0.29
1
0&0511309-53 74.63•g
2-Bul.none tMEKI
NO ug4-
$DO
0-6!
1
DMW 13 0053 "-93.3
Cm10on AIsW6ds
NO ugh.
500
12
1
06MN1109:53 75.15A
Cmrd9n lemmdd9nd.
NO upiL
1.0
0.25
1
Oem51130D:" 56-234
010;oemn....
ND upR
3.0
0-23
1
OW0511309.5] ID&DO'-7
ch.*a, no
NO UgI
10.0
O.64
1
05T611300:53 73-00.3
Chlera53rm
NO ugIL
5-0
0.14
1
OLRW1309-53 57-06.3
C110mmethmne
NO ugk
1.D
0.11
1
ONION 1309:53 74a7-3
1,2-DiNrvrrla-}ohlOrelrop...
NO uSA
13.0
2.S
1
WaN571309:111 96.12.6
deram5clddromemane
NO ug&
3-0
0.2$
1
OBM611309,53 124.46.1
1$DtPM"O1mna 1.111
NO upli
14
027
1
OIL= 3 09;53 106.93.4
D41rom mMene
NO uWL
$0.0
0.21
1
09MV0 Q9;53 14.953
t j-01pNoto6enyens
NO uyi
5.0
0-30
I
D110511309,93 95•561
i,4-D1cMwohenrans
NO UA
1.0
Om
I
061051110013 106.40.7
Dena-1,4•DrWaro•2-0u14na
NO tlyi
too
IA
I
11WMUI309.53 110-57•6
t-1-0kMwaathane
NO VA
5.0
0.32
1
06m6113 09:53 75.34-3
1.2-0khlorurlllane
ND uUlL
1-0
0A2
1
OBMSn309:E1 107-ad-2
1,1•i7lchlvroeNmne
NO vU&
5.0
4.5E
1
06r0Y 1300-53 7635.4
uim•1,2•Dlrnlwo.IMne
NO ug&
5.9
D.19
I
Oemw 3 A 53 $56.59.2
tTmnm-1,2-DlcMoroathene
ND wyL
iD
0.49
I
OWOSr13 tNB:63 156.64.E
I,-0khkropt*p*n:
NO U91L
1.D
0.27
1
DO=3 D93S 7d-07.5
I,D-Dlchl... prop.n
NO up1L
I.D
0.;e1
t
06PDU 0951 142-2&11
do- 1,3-01,i11orapropen.
ND uOi
1.0
0-13
1
06f05p1300:51 1OWILOI-5
REPORT OF LABORATORY ANALYSIS REPORT OF LABORATORY ANALYSIS
Two raped WW net be r.Pmd..d. -.W In W. rtw r.Me N.t rwl l" r.pm .d.. 0 n 1u1.
Dew MN013 10'49 AM Mo-t th. wmvl. a.rN. r.t Pen Aa Ir" Ser*os. Kc. Page 19 VI 71 ❑O.: 06170913 10.49 A3.1 .ae Me ware. mn..m xP.-A, Ivkw 9.pwy.. Inc Pepin 20 of 77

P.-A...Iyd.., 3-1.4.-N.. Pa n. A ivlyq[rl M If Ou, 1....
aceRrra�ytisa� • SOS E..t M..d.w n.e Su.. A 2225 PN.nd. h
2i28e Aa -ft. NC 2WO
{SWAG 3- 71 jgmj 5F1I Ta
ANALYTICAL RESULTS
Pra{.0 il-,y Llvaed M1 A}y 1UrC1
Pex. pwjJ No 921 690 53
Slrnpl.: MLW II
L.b1D: 1211215MON
CWkc1.d
Re part
Pnemeler.
Remllt VA Jta
LOW
6260 646V Lx.w I-.r.l Landflb
Analyi"l Method. EPA 6760
tram- I.I. Ok11lv.aprnpene
NO ugrt
1.0
Hnybmuam
NO u(VL
1.0
2-H6.e *ne
NO WL
100
iwomelhan.
ND Z,
10 0
M.1fyl.na Cldmld.
NO uOeL
I 0
4•Malhyl•7•panlanona (MIm
NO upll
100
54rene
NO vy?L
1.0
I,5.1,2-7ra.ehlafo.lt.Im
NO ugA
56
1,1,2,2-T1tr1c1Jw "Ch...
NO uO+L
1.0
Tatrochlofeether}a
NO uU&
1.0
T.&an.
NO yOfL
I.0
},1.1• Trkhlprq.m- a
NO LM;k
I.0
1 �,2-Trki+lorasmalre
NO u94
10
'rhkfna9,ana
NO 6A
1.0
Trkhkro6uofam"ne
NO upt
1.0
f 2,}Trlchkraprppane
NO -lyt
I I,
VW:"IW4
NO uDk
60.0
V,W p4mm.
ND uW1
1.0
%ykne ITbWM
NO pQIL
5.0
S-H.fea
4airempivaro5enlsnr [S)
99 %
70-130
[am Omv 6umem.rh.ne[SI
102 %
70.In
1 r.-115chlvr..M.ne-04 [SI
102 %
76.130
Takfene•dE tSI
e6 %
70-100
2320E Alkalktlly APIOVIIG41 Me" SM 2020B
PJk.W4, Tokr .. CaCO3 16W uGfL 5000
62105 BOO, 6 Ely AnalyOcaV Ma4wd- SM 52100
BGD. S day 11400 ugfL 2000
306.0 iC Ardenl 21 Day. Anluytkal Me6.Od: EPA 300 0
SW4ra NO NAIL 250000
Alpo chk.lda An.W.1 Meth.d; 54 4500-CEE
Chk,W* 1430 up4 loop
931(18 TOG An.Yl.@A Malhod: SM 5310E
Teml C,gardc Carbon 1640 uWL 1000
P...An.ry4cer lr rrlo.r, Me. JO Pan An.4ytl[al a 1.•.Ie.r, M[. Pa e r Ana1y11 w16erv.se., Ina.
9a001un..rAw ate. lra aceAnalytrca�r 205 E..+M.. Wn Re.�
N-6-di.NC 21I1:e f/ wr 4>:wer sr. Ed.e. NC 21768 Aalnr,ll. NC 766p[
t1p1]6?&a= 1 (M0234921 1+17617Y+-I+]6
ANALYTICAL RESULTS
P.pNcL $Ivry CS-d-MI Atry (UEI
Pace Plepcl No.. I7169455
OW2011300:40 R.ceWmd: OWNIVI31126 M.IPU "%IMF
MOIL OF Pre;'Wed moketed CAS Np. Qudi
0 26
1 96eQW11 09.51 1DOW •02-6
0.30
1 06mm 13 09.5) 100-41.4
9.46
f IWO5r+309:i3 01-10-6
0.32
5 06)05113 09 53 743E-4
0.07
1 DEM5d" 09:53 7y-09-2
031
1 Domm 1100-63 IWIC-1
0.26
1 06MU 11 01:53 10042- 5
0.33
r 2a o6m&1301-53 63W6
0.40
1 06m5A306:53 7934.5
0.4E
m 69mm1309:53 t27-le•4
p.26
1 06m&1] 09:53 105-66-�
0.46
1 OOlOSr1169:51 71.36.E
1.22
1 O6mm13 0961 74.00-5
047
1 b6mula 00:S3 70.01.E
p.70
1 09pm1100;53 1""
0.4t
1 0"u,309;53 9E-16.4
0610m1309:53 t06.05.4
0.67
1 0610511309:J3 75-01-4
0.6E
1 06705f1309:53 1130.204
1 06N513 0953 460-00-a
1 OW051:3 09:53 IE66.53.7
1 06005113 09: s 3 17060-07-0
+ 06105f 13 09:52 2017,2E-6 5O
1000
1 06104l13 m2-22
20H
1 0511v 130036 OSIOvi31640
2000
1 06m57m 3 10:03 14601.79.E
1 WO
I 0&11113 1037 18167-00-0
16r10
1 06KW 3 10=10 14404"
REPORT OF LABORATORY ANALYSIS
TN.r.pe11,eh.11-ttre np d-d.r.uptn AN.
Dafe 0ma12013 10:49 AM +.noP1 h..xry cPn..n1 cr P.c. AeuIp- 5rrv.ma IK Pape 21 11! 17
P.-Ahal"Iesp 6m;m, Irk.
MW Kuj Ay swr ten
Hunr.plla INC 7m76
{1M1ammpg
6ampla: MV&120
PNerrlatere
Lab 10: 921SWIM
Rdums LAYLL
Co6.cWd: 0517011310!15
Raped
Llrr4 MDL OF
RviceW.d: ON31YI317;25 Mark: Mler
Prapafed Anslyzad CAS N.. QW.1
401E MET rCP, 3030C
An.ly4cd Merced EPA6010 Prepafa9un H.Pmd SM 3030G
An6mp y
NO up1L
60
5.0
1
05131113 WAS WWII 00nt 7440.3E 0
Araeruc
NO mg&
10.0
}0.0
1
0503IN11DAQ 0610m13 O0:01 7440.11-7
BMlum
6.6J uWL
100
6.0
1
M1143 10'40 O61OW IO6:01 7440-144
Beryllkm
NO
1.0
1
O'Yd1113 f0:40 OE10611'-(11 74a0�5.7
C.dmlum
NO vW
10
I.O
t
05r111t3 f0.40 Oe*W 100:01 7440.4 -0
Chlarnilm
NO uyl
10.0
5.0
t
05131f1310:40 06r061300A1 7440-473
Ccbe1
NO.%&
10.0
5.0
1
OU3111310-40 0610&1300.01 7440.4E-4
Cupp..
NO UP&
10.0
5,0
1
050311" 10Y0 O&WI,100,01 7440.50.E
Lead
NO 19&
10-0
6.41
1
0513TI1310:40 OSIM1300.01 74U-y2-1
HkkM
NO up1L
10.0
6-0
1
0513l7m310-40 06r0ml300.01 7449-024
SNaleum
NO ugIL
10.E
10-0
1
m111310-40 WWI 300*1 7711149.2
Sleaf
NO u9+L
10-0
5-0
1
Om3H13 10-00 D&MI1 00-01 7440-22-4
Thallum
74 uWL
5.5
5-5
1
0513111310:40 Om0611300.01 7440-26-0
V...dlvm
NO uG&
-.10
5-0
1
OS73t713 1040 06m&13 W 01 744"2-2
Zbc
NO ugfL
10.0
10-0
1
M111310'40 OUM1300'01 744036-6
a2i0 MS V Low Lrrrl Landlnl
AnaM.ca1 fJ amp d. EPA 1250
A-1-
NO uA
100
10-0
I
06XV1131006 67.64.1
,.crylvn'lllle
Nil ug4
.0
IA
I
06m611110.06 107.1Y1
Benz...
NO UQA
1 0
075
1
OSr
O&'l3 +0.01 714362
Brpmaxhmrpmeamn.
NO upIL
3.0
017
1
06m&n 10:66 74-97-s
Brvmvmx,1.,0m.IhAH
NO uA
1.0
016
1
O&05119 }On1 75.274
Br.mvlvrm
NA p04
10
02(p
1
OCOW13 t0:06 7S-26.2
Brormmellene
NO UWI
100
029
1
QSfmI31001 74.63-9
2•Buu~m (ME%]
NO e01
I00
0) %
1
OSAW I3 10:06 76.03-3
Carbon dauride
NO 1f0A.
100
1.7
+
OBlOSJ+3 10:06 75.1E-0
Cnben leb9cm.14e
NO I QiL
t 0
025
t
06MV13 F0;06 56.23.5
Chblvbentenr
ND ugIL
3.0
023
5
0&OSf 1310O{ f0&W7
01.welhrne
NO ug1L
10.0
0.54
1
06KW13 10'00 15410-3
Chlm.k-
NO u9&
5-0
0.14
1
06005l53 10:04 0746-1
Cltkfcm.M.-
No WA-
1.0
0.11
1
a41my131066 11-67-3
1,2-Ol.romo-l-mlurvp.upene
NO vgk
13.0
215
1
06mmm310"0E W n-6
Oibremochlw-Lemma
NO u01L
3.0
0.21
1
bef0611310.011 124.48•I
1,2-Dilr-lh-n EDBj
NO ugJL
ill
0.27
1
66m51121100: IOWE3.4
ONOmomem.ne
NO LHyt
10A
0.21
1
0"W1 "I 06 74.05-3
1 2-Dkhlv,vhenxane
NO uDL
1A
0.30
1
mmsill f0:00 9}50-1
+,4•Eluhlorvtrmxeu.
NO uWL
1,0
0.31
1
06mSl1110.06 ID&46.7
P.r+.-1,4-pidJvrv-2 hulene
ND uUIL
100
1-0
1
06m5110 10.0E I10.57.9
f,l-OkMnpe[hanr
ND-WIL
6,0
0.32
1
05msr13 In (is 763C3
12.OkNmoslhane
NO.0&
1.0
,.12
1
p"511110:06 f07-W2
S,t•OkMwoelhene
NO ug&
5.9
0.5E
I
WWI IO:OE 73-35-4
cY-+,2-bld+brv.+n.nr
NO uyL
5.0
0.19
1
06f0Sf1110:941 154-W2
u.r1a•1,t•pcnb,oa0+ena
NO ..p4.
5.0
0.49
1
06m&1110.08 136 W,6
m�-0Ivl4urpprop.ne
NO -ok
10
0.27
+
OSMUIa IO.ff1 76-a7.5
m,1.Ok111oraprvp.ne
NO I.pfL
10
026
1
DEMU1310.01 714212✓}1
cis. 1,3-dehloropropene
NO uV&
10
0-13
1
061135112 10A1 IONI-01-5
REPORT OF LA 80RATO RY
A NALYSIS
tm.... m
fh4 "k
r.rx.ducM, neap) w
uk
Dail: 06 N20t]t0:49AM
fN .l. xT41.. ru....rv1r'w
iyn11re.1 S.rv.oa.. W P.Oa 22 of 77

e
P.cr A-1ly ., a.rvic.
P.er
A 1ygc.1 merv,..4, ,n¢ F... An k'll..l a.ryld,, I—
. aceAnalytical
205 f..i Heravw Rvry - Sv ,r R
1215 RN. rd. f r 96DD vurlwa aw. l60
NC 26". 1un14few., Nc 7s31a
S 310102] U.
18281254.7170 1704 piS0007
ANALYTICAL RESULTS
P,Q*ct Surly Cloud-M1 A"(V!C!
Pau Pf*cl No-! 92159651
Empty: MY4420
Lab 10- 12186863007 Co9ectad: OSl W" 10:15
Raeelwari OW10151172S Mmuhl: yyater
Rep"
Pwame4mm
Reeutla Llrnla Limn
MDL
OF
Pfmpmed Analynd CAB No- Oust
0260 MTV Low Le w L-dflM
Analydcel MelllodEPA 826D
truk.l,]•OlcNuopropena
NO ua 1-0
026
1
069511110:a8 10081-02-9
EOryldenren.
NO tQ& I.O
0130
1
061051121" 10041.4
2-H... n
NO ug,L 50-0
0.46
1
0045fl310:05 591.7E+6
odomemane
NO ugi& 10-0
0.32
1
061051131,C" 74-66-4
Mea,ylene CNvrlde
NO ug& 1.0
0A7
1
O6f0&13 10.04 75-09.2
4-Methyl-2-p_l me (MlaX)
NO n & I"
D.33
1
O&W 13 Im 106.10.1
Styrdnm
NO WL 1-0
0.26
1
0MV13 10�6 10642-8
f,1,1,2-T.ilmchlofoedlane
NO ZL 6.0
0.13
1
0610WI3 lOIO6 53O-20-0
1,1,2.2-Tetrmchlxod4hmne
upl
NO L 1.0
0.40
1
06"13 WN 79-34-5
Totmchlwoemene
NO uglL 1.0
0.46
1
06iFOW 131096 t27.16.4
Toluene
NO uWL 1.0
D.24
I
05m5f13 10A6 t06.66.3
t,t-l-TnmMmoeth.nm
NO ugft I 1
0-4d
1
0111DW 1006 T1-55-6
t,t. 2•Tdchlwoelhene
NO uR& 1.0
0.29
!
O6A5f 1214�0a I9-00-5
Trkhlmwlhmne
NO ugfL 1.0
0-47
I
06f0L12 f0'06 79-01.6
Trr¢hlwoh.momeu+ea.
ND .0& 1.0
020
1
06N'Y13 101" 754a.4
t2,3-TdcMwoprapenm
NO wt 1.0
0.41
i
0&0&1310:06 W14-4
Vinyl acetate
NO ug& 50.0
0.35
1
06105f11 f0�06 108.05.4
Vinyl chloride
NO tall 10
082
t
$"NJa 10:06 75A1.4
Aylene;Totdq
NO uyA. 5 a
D 86
t
o6NW11 10;oa 1130.2Q7
SunwarH
4-Bramwuarahenrena(51
99 % 7D-1311
1
O&W1310V6 44Q-00-4
O tw.avAuwome%m IS)
10s % 70-too-
t
061 W 310:a6 IDW51.7
1,2-{f1elJweeln.ne-d4 (SI
fot % 10.110
1
064511316.0E 17060.07.0
TuL4ene-d8 (S]
101 % 70-130
1
064&1319:00 i037-24-5
2320E A*%Ii-tty
Analylkal Method: SM 2120E
Ar"Nsimy, Total It CmCO3
S6060 uy1L 50d0
1000
1
OWNI13 t5:19
621PB DOD, 6 day
Anmlylkal Melrwd: Sm 52108
BOO.5 der
ND uglL 2000
2000
1
05a 1113011:36 DGMI13 18'40
300,0 IC ANvr+r 2e D.y4
An.y..1 M.0l 1: EPA 100.0
$ulfare
8Z801 uWL 250DOO
2000
1
0M 1110:44 14000 79-6
4 NO Chlond.
fvnfyl of M.lhad: SM 45040,E
cNa,M¢
4470 up'L 3000
3000
1
p611111320:34 16067 00-0
6310E TOC
AhWl..l Mat+vd: SM 53106
Twrd 0r9en1c C.ihvn
2470 uWL ION
ION
I
064W1320:00 7440.44.0
P.a. An lvo4 a1 m:ndcoi, lne,
P... AmayeW 44r.1q 4, Ma
P.. Anm,yP¢.f aervlp 4, Ine-
ceAnalyticale
l3EmnMeeawR¢rf yw.A
r221Fl wsdmdt
9600 ..�.
71766
Affl rA.. NC 200M
,1~-al.. NC awTo
r1
f
(3361a73a921
i6741254.1176
[7wtero-aw7
ANALYTICAL RESULTS
P,*.I: Sorry Claeed•M4Aky (VC)
Pame Prated N6-: 9215S653
sample: MHh16
L*I, ID: P71 Il W3010
Co4rcfed- OW2911314:If.
Facm4 d: 05d10/1317:25 Ma4tr: Wmlmr
R.p.d
paremeten
A.w144 UNIX
Urnit
MDL
OF
Pupued Anatyred CAS No, dual
6010 MET ICP, 3030C
Andlytical Method: EPA 5010 Prepna6vn
Melh9d: SM
3630C
MVmvny
NO ug&
60
5.D
1
05n 14310:40 O&Wl30004 7440.16-0
ArdeNc
NO upL
10.6
10-0
1
M1103 $0'40 OWDW130004 7446a6a
BIMum
66,IJ 4&
100
S0
1
u6111 r1310;40 O6f0611300:04 7440-39a
Beryllium
NO ua&
1.0
1-0
1
OW31A3 W40 OB10W1100.04 74404; 7
Cadmium
NO ug4
1.0
1-0
1
O5n1All to O&M 300W 7440�-9
0tvamium
NO ugA
10.0
SE
1
0011131 DA0 06106113 WD4 744 D47.3
Cahm6
171 up4
10-0
5-0
1
=111310;40 QBIM1100:04 744OJai
Ccppaf
NO uplL
1O.D
SA
1
051311131CA O6fOW1300.04 7440.50-0
Lml
NO u94
10.0
SO
1
usaIAa 113:411 06f06143 DO:04 74311L 92-1
Nickel
6-44 wl#L
50.0
5.0
1
OD70111110:40 O&OW 1100!04 744042.0
Satenmum
NO u911.
10.0
10.0
1
05131113 10:40 D6106113 00:04 7742.0.2
Saw.,
NO ug0.
10.0
5.0
1
0513TI1310:460 O&Wn00:04 7440-224
Thallium
NO u91L
5.5
SA
I
06At11310.aO 06/06/11 0004 7440-2a-0
Vmn4dium
NO u9fL
250
5.0
1
M111310.4D D610N11 W'04 744D-07-2
Zinc
14.5 uO+L
10.0
50.D
1
05AN1310:40 D6706f 1100:04 7440.04
23208 Alpalkmy
Aneyhcai Mmtho d- SM 2320EI
AlkeWhF.Ta1at.. C41CO3
189M up'L
Soon
ID00
1
asnul3 $5'30
62109 100, 4 day
Anelydul Method: SM 52108
BOD.5 day
12000 upL
2000
20H
1
05111f 13 00:36 OB10411 1 16:4a B2
369A iC Anions 26 Oeye
AnehltlPal Mathed: EPA 340.0
wt.le
a68aJ up4
2500H
2000
1
1)6O511319.57 146U1149-8
46D0 Chloride
Andyned Method: SM 4500-aE
Chlerlde
27400 uyL
1000
1000
1
067111t120=16 15067-DD-a
S31OB TOC
An alylleal Method: 9M 5310B
Tolm Organic Cal ban
154DO ugR
1000
1000
1
0=5113 2010 7440-44 0
REPORT OF LABORATORY ANALYSIS REPORT OF LABORATORY ANALYSIS
*N. r.Pmn wr na, e...P�ar.a..,c.o<,. ey ih,4 nperl Nq net a nproe�eel. m.a4q .h M,
Oala 0612812013 10 49 AM whorl the wft. tvn 1 of Peee A-10e S.nWn. Inc page 73 .1 77 Date: DW26201110' 4%AM w4wu, h. "ml -.-I of P- Ar yecel Sen0cme, tre Page 24 at 77

Pac. Rnrple.r 5.rvrc.., In[. P.-A.Mrydc.t e.rvru., Mc.
2ceAnalyfical' ' E..1 .r..e..r Row
r ye,�yM rnn E&.. NQ iryae Aw.rn. NC 2mW4
rllelon ho I ram P74417a
ANALYTICAL RESULTS
Prulact 6wry Clowd-MI Wry (VICI
Pau Nood Na.. 9Z1591153
P.-A.Myllwl Nnln., Ina. 10
Pion Anslytloal 6errle•r, Inc- Pic. AnMyllpl 6a0lw 1, In•.
OW rarc•y 4: SwW 1W I 2eAmlyfical' xwr.. 4..onr Row - sw. A xrn nR. w. n.
H-wmlA.. NC 21076 ,wrnac.�ea un� Fdan. NC U21i Afh.w4- rJC 79a94
f711r)a76-0m {3361673-0021 ia2e1254. 717a
r
ANALYTICAL RESULtS
Propet Surry Cbwd-MI AMY IUICI
Pica Pt*d No,: 92159553
SWF401 MyY-46
P.remeten
La610: 0214HSJO71
Re.u11e UNIi
Coll.eled OW011314:IS Rdoahred: 0613W13 17 25 Maori.: Wilor
Rapod
LirRR MDL OF Named mewed CAS No. flo01
12116 618V Low L•r•I L-01111
Ral.lypcM M.Yrmd EPA 1750
Acelone
NO up4
to
10.0
1
0114111111523 67.64.1
A,.WmNia
NO ulm
55.0
7.2
1
OW11113 Is21 75-0S-a
Auulellr
NO uplL
530
1.6
1
0WIP131523 117.02.6
AcrymMI'da
NO Np4
200
1.9
1
OWH1131523 107.13.1
Mel chloride
NO "A
10A
1.5
1
061111I31523 107-05-1
Benznl.
is U4IL
1.0
0.25
1
OWIle131523 7143-2
lk-cranerne0...
NO UWL
3.0
B.17
1
Oar111131523 74-07-5
9romoacMwometlrAne
ND up4
1.0
O.la
1
OW I Ifil 1523 15.274
Bral twm
NO Upli
3.0
u]6
1
UVW13 1523 7S25-2
Oramometwe
NO up4
100
020
1
IM1111131523 7"34
2Auta.one (MEK)
NO "WL
100
0.66
1
OW1103 1521 75.93-3
C.r0wlaw kL
NO up4
100
I]
1
4Wl III 11523 7545-0
C.rdon reuaworlde
NO up4
1-0
0.25
1
9NIIII 11521 5111-23-6
Chwro6eneala
8A up4
3.1)
023
I
06/11113 1523 10 ,00•7
Chlaroelhene
NO ui1L
10.0
0.54
1
W11131623 75.00.3
Chkmororm
NO 05k
5.O
0.$4
1
DOM 1113 $521 6746.3
Chlwarna0len•
NO uU&
1.0
0.11
1
96/11113 }523 74-87.1
Chlwrrpr.ne
NO uqr,
20.0
0.27
1
06111111523 12 -1 -1
ONlromochkromelNarla
NO.0&
3.0
0.21
1
WINI1ll 1523 124.41.1
12.O4rcmoedl.n.(EDO)
NO 4d1l
1.0
0,27
1
WIV131523 106.93-4
Dlbremem.lh.ne
ND uy/L
r0.0
021
1
DI0III 11623 74.95-3
1,2-Dlcnlorohaniane
1.95 UVL
5.0
0.30
1
Out $M31523 MO.$
1,3.OkiYwoOenzene
0.32J u41L
6.0
0.24
1
061111" 1523 541.73�1
1,4•bk mu b.nze
16.4 uyL
1.0
0.33
1
OVIII13 1523 IM49.7
ttatl.•1.4-Dldamd-241 to ul
NO upli
IN
1.0
1
OWIV13 1523 110.57.8
O1Altoreu6Uoromepuna
NO UNjk
5.0
021
1
OWIU13 1623 7541-6
I,1-0Ichld...lhane
2-mi uWL
6.0
0.12
1
OWIOn 1523 78.34.3
!,i•OIGIduo.11l.n.
2.0 4WL
1.0
0.12
1
Owl 11131523 1074a-2
1,1-0iCNwoethene
NO uU&
6.0
0.56
1
owl 1)131s23 75.35.4
W-I�-Oknwree then*
47-41 uyL
6.0
0.12
1
OWII0131523 IN-59.2
Pw-12-0Ichlwoem.ne
NO up4
5.0
MAIN
1
OM1103 1513 IN- WS
1,2.OIe1Aer.prupene
3A uWt,
Ml
1127
1
OWN 1/131523 76.17-5
1,9-0kMaPpropane
NO UA
1.0
028
1
OWN 10131523 142.29-9
22-Dkhlanpropane
NO Ui4
15.0
0.11
1
41VI1M31S23 M-20.1
11.tIKnlwwl+opnna
NO up4
6.0
0-42
1
ml V1315:23 563-W15
n1-r 3-0,chloropropene
NO "A
1.0
0.11
1
OW111131521 10061-01.5
Iran.•1,] Ochloruprnpane
NO o04
1.0
02e
1
Witt) 1623 1006i-0'!•6
E111A enr.ne
NO U94
10
0.30
1
O61i1717 1523 1W-41-4
Ethyl melheuyl.le
NO Upt
10.0
020
1
OB111113 1521 0-61.2
Ms..cldnr.• 1, 3•tm.dlan a
NO uq&
10.0
9.71
I
Do? I1113#523 67-01-3
2-11•4anw.
NO U01L
50.0
0.45
1
M111131523 591-7a-4
odomelhana
NO -ill
101)
0.32
1
WIIIn 1521 74-06J
Imb4t-1
ND ug&
100
35.0
1
06fIIll 1521 71411.1
M49recrytmtp1Na
NO OgA
100
0.93
1
051111131623 126-Ob7
Alethyt.n. Chloride
NO utllL
1.0
0.97
1
OW11111523 75-09.2
Ma 1hy1matnavylafe
NO u0A
30.0
2.0
1
OWN III 31523 80-02-0
REPORT OF LABORATORY
ANALYSIS
rnr. report
.n.e rw1 he nWoM d...c.prn NA.
Date: OCII1201 S 10:45 AM
'1a 1 r A. lAn een.anr of
Pme Ana lVocal S.nr.... Mc.
Pipe 26 of 77
Pom AnolVaul suNe.s, In&
vem runaq A.• iw 106
Run.rM4. NL a1071
110i167s-f077
Sample: MW18
puireelefe
LAb ID! 12161663011
Rouft UNIa
Cdl.cled-
RePOn
Llml
0502VI114.15
MOIL DF
R•cN od: INW301017.25 M4b4r: Wa9N
Prap.nd AnaW" CAS Na. gt1aV
a260 M5V Luw Lewl L-0141
A.Wh.W Meihnd EPA IMil
4•MaNN-2 Penunnne 1M10K1
NO UDR
f00
0.33
1
MI10131523 04-lu-1
Nophth.l•ne
NO Uyi
10.0
0.24
1
Mo 11/131523 ?1.20.3
PropleMRIO
NO Up4
$50
3.5
1
0601111115-23 107.12.0
9aerane
NO UPL
SA
026
1
OWIII" Ifi 23 10042,S
1,1,12-Teeachtuw. th...
ND up1
5A
0.33
t
OWIV13 1523 N4-2"
I. 1.2,2•Te is Chlmaa llahe
ND ug&
3.0
0.40
1
06711/13 iila 70-31.5
Te tr.rhlwaeMme
ND upiL
10
0.46
1
OWITY131523 127. Ia.A
Toluene
ND uu4
1.0
026
f
M$11131523 104 W3
t 7,4-Tnahlorattenrene
0.63J Ug�!-
10.0
1:1.16
t
0611r113 IS23 170-62-1
1-I,I-Trldrinroelh.ne
ND UOR.
1.0
814a
I
00r111131523 71.554
},1,2•TriahlwaaNarle
NC ui1
10
019
1
06A 11131522 7a-00-5
Trkhtoroethene
%A uQ&
1.0
047
1
Ho I11131523 79-01.6
hldlWroalwrom.lh.n.
ND Ui1L
1.4
020
1
a&I I7131523 7549.4
1,2,3•Trldhlwop open*
NO uu4
1.0
0.41
1
0611111 l 1513 96 1 4
YY1M.-W.
NO vuM1
50.0
0.35
1
DUI 1113 15 23 108.65.4
VF.Il chloride
4.4 Uyt
1.0
6152
1
O6r111131523 7154$ 4
xyl aria (Talalj
NO u1j1L
5.0
0.60
1
08r511131523 1330-2114
S-g.r.a
4-Beamoluwobenrsn. (S)
95 %
M130
1
OW111131523 AW00.4
plhromoeuoromelh.ne (S)
90 %
ml"
1
O6r11113 IS:73 Ia61-S3.7
12•DkAla+aalhae.•d4 IS)
95 %
7a130
1
081110131523 17060-07-0
Toluene•d6151
IN %
70.130
1
06715113 1523 2437.2a-5
REPORT OF LABORATORY ANALYSIS
rlw r•p•h eh.l n•1 b. npndue.d. •.apt n A41,
O.Ie: UMV251116:49 AM rdrmlN.r ..ilrn.4rlwnlcl Pp. "'ICIA S.rwe.., I.
Poi! 26 84 11

p.ee A"yN N.eme.a, 1- P.ee An.lyucsi Iwvlee., Me. P... An dyN., 1.nrlve., Ine
2ace Awlytical • 206 E.M l -k- Read - SAwrb A 2225 RW. a 9100 arcer Are. 6.1. 100
11M +IMMH, NC MO
i I3a0102]41911 10241254.7170 1704187S9
ANALYTICAL RESULTS
Prplecl: Sorry 0 ..d Mt AJry Iu ICI
pace. Pr vjecl Nv. 9215$153
Sample= 1AW-7 Lab ID: 921111 93011 C;.0 l.d: W IWI310:40 Recelrad: 00101314-21 M.trh: Wolat
Pulmelcre
Re"I1e LYE
Raw
Urr I
MDL
OF
Prepafed AnWynd CAS No. Oval
4010 F1 E7 rCP, 3036C
Analylk:.1 Me 1+vd: EPA%I D Prep.ream
Method: SM 3010C
Mkmmy
NO UA
6.0
5.0
1
OW04113 17:40 06MV1304:44 144036.0
Ar..Na
NO upL
MO
10A
I
OW4113 U;40 05MIWI104A4 744036.2
eerlum
71.IJ uyL
100
50
1
D&WIS 1T;40 0MVI104,44 74403I.3
8er71Wm
NO upL
1.0
1-0
1
01A411317'40 0610811313'.26 744041-1
Ca d.r um
ND WL
1-0
1.0
1
05A41S317AO 064W304A4 7440-43-9
L hrwakim
NO nph
10.0
6.0
1
04WI1 17:40 O6JO8r1304A4 744947-3
Cp6aq
Ga-1 ug+L
10.0
E.a
1
08"1317'40 06fow I304,44 7440484
Copper
NO ugk
10.0
6.0
1
060041131Tr40 061W1304:44 7440.50-0
Lead
NO upi
10,11
1,11
1
0"411311:10 NMW 11 D4:44 7430-92.1
Nkgel
NO -gJL
80.0
5.0
1
06A4111 17 i0 06J06113 04A4 7440-02.0
5=rom.m
NO ugk
IDA
1D,1)
1
OWHII317:40 OSJ0611304:44 77824942
Sorer
NO O A
11,0
50
1
06"1317AQ 0 MWQ 04;44 7440-22-4
Th.11um
NO ugA
S.a
5.5
S
0610411311,40 p6NN1104:44 1440.21-0
+nneN•.m
NO upi
25.0
50
T
0620411117,40 OSJ06J1304,." 7440A2-2
LY.c
NO up+L
10.0
10.0
1
05"Af 13 f7:40 06r00J1304A4 7440.604
1260 MSV Low Law a1 Lar10111
M.II Ikal Method: EPA 6200
Aeetonv
NO poi
100
10.0
1
owl 111315,29 6744-1
A.rylonlrrlle
ND u0R
200
1.9
1
0EI111111a39 107.1]-1
84nrdna
0.71J uWL
1.0
0.25
1
Owl I1:31,570 7143.2
g.omocrdwomelhene
NO n;L
1.0
0.17
1
=1111313:39 74.97.5
&pmpdcYwwnelhane
NOuyt
IA
0.1E
I
D811111]13;30 75274
Elm -farm
NO tQ&
3.0
026
1
01111f13 S331 73.252
Brompwehene
NO 10,4
$0.0
0.29
1
0611111311:31 74-03-9
2•Bu11nm.(MHKI
NO I&
100
0.96
1
611
01ha M39 7"3.3
C:Ab d.W6d4
NO uWL
100
12
1
0 "ll115;30 7s-13-a
Crhan+ehacldodde
NO agIL
t.0
0.25
1
0E1111131311 a6-2a-5
Chimt) plena
12 PWL
1.0
0.23
1
DW"113 1530 108-90.7
CAlorp e11ar1e
NO opt
10,0
0.14
1
M:,11133I 75410.1
C1Ycr'form
NO opt
S-0
0.14
1
ON 13151S:3, 07-60-1
Chhrvme.flane
NO upL
1 0
011
1
W10131539 7447-3
12-D41'mwl-cnlnraprvpane
NO u9&
11.0
ZJ
1
owl V1315:39 II&QLa
Owrpmadhr v+n.9l.ne
NO upi
5-0
0.21
1
ON1I113 11�39 124d61
1,2-Dft-hra IEOBj
ND u0&
10
027
1
061111i 315'at f05-93.4
DUramamellane
NO uWL
10.0
0.21
1
0WIM3 15;39 74.95.3
1)-plcMpro6enxma
0.31J UOL
5.0
0.30
1
DWI, Ill 15;30 Ia-a0.1
1,4-Olcliorpbenxene
1.2 >aUIL
1.0
0,33
1
"11Ma 15;38 $064E-7
u.rwDlw2-bubo
NO ugJL
100
1.0
1
M4111115:3I 110.57.E
1,1,)kNwpelhene
ND u9+L
5.0
0.32
1
NMI 11316139 76.34.3
1,2-DkhlwoeNena
NO L4;&
1.0
a.12
1
Mill 315:39 107-M2
1,1-D0.4Ymvelhene
ND uN&
5.0
a."
1
66111113153: 75.35-4
a.-1.2-dwwwh.n.
DAIJ -g&
S.0
0,19
1
0611411511l9 156.59.2
uma-1,2-Dk1Yu'e.plene
NO uWL
S.0
0-If
1
D61111151539 151-00.6
1,2.Okhkrvprpp.n.
NO nA-
1.8
021
1
01 IM31S:30 7647-5
O lc hlwopropa ne
NO vok
10
021
1
o6J111131sill 142.284
c1. 1.1 Dichluruprapvnv
NO uy4
1 0
0.13
1
oW1511315'JI IOO6I-0i•5
REPORT
OF LABORATORY ANALYS15
1Nr..
can �w pal a np.oeuc.e..r=.M
n h,..
D.I.. WZ(201110 49 AM
x.v.v..1 m. rriwn o.n..nr nr R.-
A•u lye i Se•.ia..1k
p4ge 27 el 17
lase RnNytl4al a.rvlee., lne. P.ee An.type.l aervlpr, Mv.
P... AA.lyeeel 6errlra3- Mv.
I aceMalytical•
2M E It M..dor Rv.d G.%A
2225 R-Id. Or
"M Mwc.r Ar. Suer 100
' w„•��a
Ed n, NC 277Aa
ANVA.. NC 21a04
IMmV•MI.. Ne 7107a
+
[3161aY3a971
1626]234-7179
170e a17y9097
ANALYTICAL RESULTS
P101arL
Sorry Cloned-M1 Alry (UICI
Pace Plulecl No.
92f5g653
S.mplr: MW-7
Loh ID_ 91151893011 Celle R.d. DLIM113 1D 40
Recurred: OS311I314:23
M.64 ypeler
paramaler. ResW1e UrAm L1m1t MDL OF Propar4d Analy3ed CAS No Oual
1290 MEY Low Lar.I Lan1111I A-lydcd M.1h.d: EPA IlM
Irana-1,3-Old*FoPrvpana
NO uWL
to
026 1
owl Ill] 15:11 IONI-02.6
Ehykunrene
NO ugR
1.0
0 30 1
Owl1113 15110 100.41.4
2•Reanone
NI, ugIL
100
9-01
QVIII113 15:39 591-1"
IedoiffAM a
No ZL
l8.0
0.32 1
OWI"I 1531 74.11h4
Mehylene CIa4Nlde
71D uq+L
1.D
0.07 1
OEJ11113 I Sa 71-09-2
4 #4.1ry1-2ymW+me IMIBK)
ND uglL
IDD
a.33 1
oNlllt3 1531 106-10,4
Srylrna
NO 1ay2L
VD
0.29 1
OWM$3 t5'39 100.42-5
1,1,I,2-TetFSCl0 QV1hIne
NO ug1L
5.0
0.31 1
O6l11113153E 630.20.E
1,1,2,2-Leh4eNwo.6.ane
ND 4;L
SA
D.40 1
06111f111 S:39 79.34-a
Totmotdorvoth one
NO ugIL
I
0.4E 1
06/11113 15;39 127.16.4
Tcluena
NO ugJL
I,u
0-2 I
DwIlM s-39 1Da-66-3
1,1,1-TaciAwpgh4n4
NO ug&
4.0
0.4E I
06N'I","19 "I$"
2•Tr1clAvrwlh4ne
NO ug1.
}.0
0.29 +
01111JIS II'm 79-06-5
7rkhlorv.henr
NO uok
IA
0.47 1
DW,111315-19 79A1-0
Ttkh1ere6uele'r.h.n.
NO .I&
1.0
02a +
D8JIWO 16.19 7540-4
+,V-T,1cWWeprahene
NO vg&
1.0
0 41 1
0EJ1111311:19 Sd-164
Vinyl acelate
ND upL
10.0
0-35 1
owl I11515'31 106.05-4
Vnyl chiwlda
t4O upi
1.0
CA2 1
owl"', I630 ia-01.4
%ylene ROIeD
NO ygri
5-0
0 E6 5
0611111I I539 1330.zo-7
SunaOahs
4ArompAuao6enxen. I51
99 %
711-130
1
191111111163: 45""
D0l amldwomelhanc IS}
91 %
70.130
1
OW11113 15:3158E-51.7
12-OW waalhene-04 (S)
94 %
10.M
1
06111 J13 15�39 17o80.07 0
Teklene-d1 M
Ill %
70•1S0
1
Wilm 1511" 2037.2E-5
2120E Alkaloft Analyllnrl MaCwd: am 2320B
Alkrinlry- 7we1 as Ca=l 96900 Do 5000 Iwo 1 D&SM3 11:3a
12tO8 HOD, 5 day AnrhOcal Mm%pd: SM 52108
DOD,5 day NO upi Me 2000 1 0MV1301:10 084061319-15 62
100,0 I[ An10nr 21 O.y, APaly6cal Me hod: EPA 300.0
supra 7990J uDL 250006 "W 1 08l05113201,39 1460E-7I.6 Mt
46M Chlend. Malylk.l Irlelhed: SM 4500-CI-E
Chwrld. 11100 ugrL 2000 2000 2 ON51N520A7 taa67-00.8
153100 TDC Ari elylkal µelhod SM 53l00
ToW Organic Cwt;w I WN uyL 1000 1000 t Wd0Y13 20:30 7440-44.0
REPORT OF LABORATORY ANALYSIS
7r.r r.pen .NO rg1'...vvou»d...c.p1 � eli
D.te- 08l261/013 10:49 Ala w.houl p...,n11an c .....top p- M.ygl aerv�o... I-
P.qc 20 W 17

P4EP AW .W
.y P.AalyePPi
ar1.P, M..P
Rve
2225 Ru.DraceAnaiytical
Cs.
Eon42M
AV.RC 749W
f]3a1a]341G7f
II]A)764-111a
ANALYTICAL RESULTS
Pr01a 1 Swry Clo..a-Ml
A)ry (UG)
Pace Propd No. 9215965.1
P.- A"yan4 arrvinr, Me. Prc4 Anal y"..l'WAw ,. Me. P444 Amlyryael 9"dn,,n..
Ya60 Klr..r Art S�IPIw I pV4 i',11�1� �c�J�a SOS EaN WaMw load-Su'.R 2M R-W
11uwi rye 7s01a r .wv .f.cs yA Earn W. ]7715 A+R ... NC 2ae01
I iM jar �pW] f3? ywl ail f (.]el+'SK-r f 7a
ANALYTICAL RESULTS
Pr61.c1Swty CHied-MI Ally (UIC)
Pan ProJed No.: 92159153
Sample I1W9
Pumnal4re
LaL 10: 121 Sill MI
t mAl UFO%
C.Umd: 13WO,311:?D
R+pvn
UrrjI MDL OF
RsceJyad 05f311139423 MAW.: W6MI
Prepared Andyrad CAS Np- 0"1
dot MET IGP, 3030C
An.lyl1e41 M.P.4 EPA6010 Fhep...
1 n M.thod: SM
3030C
Antimony
NO uOJL
60
50
1
06*01317;40 061p6Jt304;49 7440-36-D
AIy.,,m
Hp MOIL
Intl
one
1
06f0411317,40 06R16f9304:48 74411-39-2
Sedum
63.3J ugvL
100
SE
1
06"1217'40 06JQN 91 04A: 7440.39.3
0 ryolum
NO VIP&
LO
,4
5
p6f041131r-40 OGIaN,.313211440�1.7
C+dn4um
ND upR
10
10
1
DOMQ1317;40 N?OPT304.0 744E-43.9
CN-um
NO MOR
Ion
5.0
1
06A14J13 17-4o O6mvi 3 04 41 7440-47.3
CGI>A
as uOIL
10 0
S 0
1
161141:3 ,1-40 11.13.-41 1:04AJ
Copper
11.0 MOIL
I o 0
5.0
1
OGM403 17-40 MON13 04:41 740-50-6
Lead
ND MOIL
100
50
1
1"411317=10 0610611304:411111,91-1
NIck.I
NO u4JL
50.0
so
1
o6Jo4J! 3 ! 740 06JON93 04:46 7440•0?•0
6aleMum
NO u41L
100
10.0
1
OW041317;10 WmWI3144a 71U-40,2
Silver
ND UuOL
on
1.0
,
0M1317. 0 06+06J93.AS 7440-224
Thallum
ND FOIL
5.5
S S
1
06A4f13 I7-10 It"1111 04:46 7440-2S-0
VA -bum
ND u07L
Is.,,
5.Q
,
061D4f13174D 06JON9]04V6 7N962.2
2efc
NO ug1L
1Da
10.0
,
001Q4f 1317:40 0910N5Q 04:46 71444964E
1210 MSV Low Lrrel Land9111
Andyncal Mmhod: EPA 11290
Acelen.
NO llp&
t00
too
1
W1113 Isis 57-64.1
A"Pomtrl.
NO L*t
200
1.9
1
0611911315155 107.13-1
Bmama
3.A UWL
T.0
0.25
1
0611T1131535 71.4}2
BfumoWoevmednne
NO Myt
3.0
0.11
1
061,11,31515 74-17.5
9, d hNwmelhene
ND npJL
} a
0.9E
1
ml III is 71-27.4
erornokrm
NO I*&
i.o
0.2E
1
ON1111315-55 16.25-2
BrOnti mvlana
ND OWL
10.0
0.2E
1
will", 1515 114""
2-eal4rlone IMEKI
NO u06
100
0.96
I
OW1113 I1:55 76.13.3
C+dell 115AAd4
NO u04
too
12
1
06f111, 3 IS 15 75.15-0
C+rhon l.ln World+
NO upR
1-0
025
1
o6f11I1315.55 5S23•5
Chlarot,m n.
2-IJ u01L
S-a
023
1
46n1J131151 10S9o-7
ChI.rne91+n4
NO u01L
too
0.64
1
ow 1111315:55 75-00.3
Chke 0.rnf
NO uy1
5.0
0-14
1
owl"171S:SS 67.6E-3
Chl.M_6ian.
NO uUA-
1.4
0.,1
1
Q6111(13 IS:55 74.67.3
12 DIG.m¢]-wowrrbp.ne
NO uA
,2.o
25
I
Om11113 15:55 96.12.E
Df6rorn mwa--O n.
No u411
1.0
071
I
DWI ft3 ISAS 124.4a•1
1'2-0br.mo6nl4h. IEDa]
f4D MOIL
13)
0.27
1
06JIIAI 15:55 10& !64
pkromapfall+ne
No up1L
10.E
011
1
0&l1J93 93:51 14•E1-1
1,2-OR7anr v6en:.ne
2.4J u01L
S.4
034
1
Om 111131551 N.50.1
1,4-D-10wvbene.ne
IA uyL
1-D
o.33
}
OW1119375:55 1054E-7
flans-1 ,4-Dldi4l o-28MIanP
NO uqR
f00
$A
S
o141lJ1355:55 110.57-6
1,9•DkNwo4pune
2.7J IPpR
6.0
0.33
T
46J113 9S:SS 7534.3
1 ,$.D$Na4alnane
NO MOIL
1.0
0.12
1
Dew"".15;55 ,07.01.2
1,9-0ICMorpapMnd
NO MOIL
5.0
0.5E
1
OW9111315:55 75-354
da-1�•Did9wa+lnena
4.6J uWL
50
0.}1
1
06111.11315-*+S 1SSS10
Or - 1,2404.Hweeihene
NO 4A
5.0
010
1
DN9711115.66 151540-S
1]-DIV w prow
NO uDiL
1.0
027
1
ON11J131555 7147.5
113-owru opropape
NO eyL
I.0
0.2E
1
out 11131535 142-21-9
wa•1,]•Dlallm vpropPn.
NO 4g4-
1.0
0.13
1
06111113 15-5S 9o061.01-1
REPORT OF LABORATORY
ANALYSIS
Tlw RW
env nw o."Pra at..l.epin
ho.
Oefe: 06J2"13 10 49 AM
wh Vw -ft. w..Md or P.
A6PIy+01 U+ . rc Papa 20 at 77
tar Analytic4l a4rWur, Mo.
9a0D KMur 6w S� 1GO
HnfI.Ip mt b 014
11IMPIS9aa2
S4mp1e MW4
P.ramal.n
Lo IO: SV69163013
Resins Ls41a
Collened W5011] 1120
Rap."
UIM MOL OF
R.pelvad 051+13142] Ma1Jly V%06?
Propmed AmOVzad CAS Nu Oual
d 260 MSV Low L.T.I Landfill
MAy" WOlad: EPA 6760
1,.nti-1,3•Ulchlaapinpene
ND Vail
1 0
❑ 26
T
Sul 10131565 10061.02.E
Edryb.niene
NO MOIL
1 0
a 30
1
Du"113153S 100.41-4
2•Na.+ba.a
ND Molt
50.0
0 46
1
4&91J13 15 SS 591.1a-5
I.dome9nrn
NO uWI
100
002
1
00111N3 MO 74-59-1
M.alNenr cl6pnp.
NO Vk
1 0
0 a7
1
0611013 I 7a•01.2
4-MvIhvI 2-Psfll+ntme(M10K]
NO uoR
IN
033
1
witila IS-55 106-10-1
5yren.
NO MOIL
1 0
0.2E
1
W"11315;65 100,12-5
T.U.09-.ben.
14D ugR
5.0
013
1
0611111315-51 930 2"
1,1,2,2•TeIrp-mop v411ana
No uOJL
3.0
040
1
OWUI1315-55 79.34.5
Tev*wm'Deaun+
No uok
1 n
046
1
oWtI113 ISM 127.16.4
Tolland
NO 4&
1 0
0.26
T
46/11113 9315 I"Ia6.3
1.1,1-TrKWcrneman4
NO volt
1 D
0+6
t
06R111315.JS 71-554
1,17-7rldfluvetlf ene
NO ug1L
10
029
1
Owl 11131515 Tlt-D 5
Tlxhlwosmene
ND us&
1.0
0 47
1
00J„ 19] ISM 70-014
Trlchrwa6uvlom.INMv
ND u4l.
1.0
o.20
1
0611111115.35 154"
1,27-Trlchbroprppana
NO ug;L
,0
041
1
0111111315:55 p6.9S4
Vino aufN+
NO u01L
so.0
0.1
aI1113 MIS 106.aS-+
wil cr4wWe
7-6 uWL
1.0
092
1
00111113 ISM ?"1-4
?Lv" a ITclaq
ND u6'L
SA
one
1
o6J I111315755 1330-20-7
aufrngat"
4'a'W011rarep.n]ene (S]
97 �.
70-130
1
WW1315:6: 400.OD-4
O16rbmola.fbmelhpne IS}
9a %
10-110
1
Will, 315$ 156E43-7
1,2-Ok:fdarerthene-d4 IS]
9+ %
74150
/
0E M1315:65 47010.07.0
TmW v-40 I51
66 %
70.130
1
06/1111311 5S 2037-"11
2320B Alkah" AnOOOMP M+Owd: SM 2320e
Adkohmly-TOW 4a C4CO3 1200D0 U01L Soap 10% 1 p1J19113MOO
12100 eOD, 6 a4y Answer Met"d: BM S214e
BOD-5r&y 4300 uwt 20W 200a I 06ml 13a110 06MV1319.13 w
300.0 IC Ad— 21 O.V. AAWkal Ms6fod: EPA 300.0
S...... 2430J US& 250000 ?0N0 , a6v05J,321AS 14001-79.1
460E Ch]onde AIIAy1nI Maenad: SM 45WCI-E
CI,Wde 66100 uWL 4000 4000 4 061111I3 WAR 16a07-00 6
1310E TUC AnaA eml M.1had SM WOO
Told Ulyenk C m4m, 161E US& ION ,nDO 1 0160591320:40'144044-0
REPORT OF LABORATORY ANALYSIS
TH. r.pN, eh.k ml t np.du PwP
Cole W212013 1D:49 AM wenw".ef , ri.I 1 el Feu Nxl61ra1 5.mfaP err.
P+g. 1D m 77

•
AFe. FMI7He.1 a.eylee{, Ina, P.0 An{hdl{ah 1NYNM, M{.
1 aceRrraiy[ical
7O6 E.er N..dow Ro.d • E e. A 7725 ftNa ape 0.
....ier.4d.r.
Eden. NC 277" A*wl*4-NC 2411OA
1
133a15nA6r21 (626}25M7176
ANALYTICAL RESULTS
PruJect S.C.eeed-MI
Aiy (UIC)
Pace Pmoecl No 92t59853
Sample; MW-13
P.,melen
4010 MET ICP, 3030C
Ammar
Areenk
Oml4R1
Beryllym
Cedrrum
Chl9r.4um
CuheK
Co"Op
Lead
Nlck4l
S.Ianlum
gayer
thmHum
1 n.dum
zinc
SUM MOW Low La l L..d}lll
Aeeton{
AcrylonahYe
Eeneene
0.onwdlkcometlen.
&omodldw... -th-
11-0.1m
Br.mame6h.ne
2-54tanone (M£K)
Carhop deu16d6
Carhop Iet-N .ld.
Chkroh-gene
Chwraaln.n.
Chtmo(mtm
Chloromeriana
t 2-00bl omo- 3-cMwWropme
O+h.6mochklome01a1e
1,2.ON.trmde9ranA MOB)
DNxom6mekhenr
l2-OWd.oaen2en.
1 �.0lchlwatar+[ene
bane-1,4-DIGJoro-2-hula ne
l,s-Olchl6eaeavna
,.2-pcNoroeor ne
1,1-DIchl6r oelhe ne
d.-12-Dkhlnroelhene
Iran!•1,2 Okllfarcel hene
12-Oita. opropene
1,3-0104 ropropene
G.-1,3-Dlchfolopeopen.
Paw AnelyvkN 6.rvle.e, Me.
9edO rmc.T Mn s�.n,95
F}#4.rai.. NC 7607E
17w1e7s /ou
Lab 10-. 12161113014 C.I.dted: O5l30rI3 111:00 Receeyed 0" 1113 1433 Makin: IANar
Rapan
H-Al. LF114 Lima ML DF Prepend A .dp d CAS NO. OUeI
Ana"ul Method: EPA 6010 Pnpnalm Malted! 3M 3030C
NO DA
6.0
5.0
1 OSM411317,40 061081i304:52 7440.3E-0
NO ugk
10.0
IDA
1 OW01317.40 06ANf304:52 7440.3E-2
61,62 UOIL
IO0
5.0
1 0=4113 17-40 06R15113 94:52 7440.39.3
NO uWL
!.0
1.0
} 06f0411311-49 061p61}3 13:42 7440.41.7
f40 uQ&
I.0
IA
} 0611W 317:40 0WON1304:52 11 40424
NO upt
10.0
5.0
1 09004A3ITA0 0No80104:92 74404h3
Lai uprL
10.0
5.0
1 08100317:4g OW0811304:92 7440.04
NO uq4
10.0
5.0
1 OWUR317:40 OMS1130432 7440.50.6
ND u0A
10.0
5.0
1 06104I13 17:4D QUOU130452 1439.124
NO uQA,
50.0
50
1 OW01317:41) OWOWI304:62 7440.02-0
NO ugx
109
10.9
1 06,0411317 40 0660VI30452 778249.2
ND uWt
10-0
54
1 ON0411317:40 ONONI304:52 740-224
NO uOA
5-5
5.5
1 0504f1317'40 061061130432 7440.21-0
NO d04
2s 0
5.0
1 05,0463 11A0 06106r 130412. 7440-02-2
HD ug&
10.0
10.0
1 06A74f11 $740 06406113 04,W 7440-063
Analylkal Meted: EPA 0280
NO 40R
100
$0.0
1 06JI1111 $CIO 57-44.1
NO uRk
200
1.0
1 Owl 111a16:10 107.13.1
NO UA
1A
0.25
1 0611111S W10 71.43-2
NO UA
3-0
0.17
1 OW1111314:10 74.27.5
NO UWL
1.0
0.18
1 0Wf111315:10 75-274
NO n1L
3.0
026
1 OW$1113+E:fo 75-2&2
NO up4
10.0
0Z9
1 Wsm:i 1E:10 74-a"
NO uO&
100
0."
1 oW$V1316:10 76.13.1
NO np4
Son
12
1 OWIV1315:10 75.15-0
NO ugk
1-0
Cal
1 0&11113 10:10 56.23-5
OMJ up4
3.0
0.23
1 0W1111315:10 106-i0.7
NO u04
10.0
0.54
1 OW1111316:1a 75-00-3
NO 4p4
5.0
0-14
1 0&1 VI310:1a 6738.5
NO uWL
1-0
9-11
1 Owl 1016:10 74-67.3
ND v9R
13.0
2.s
1 OWIVN ICID 66.12•e
NO u01L
3.0
02I
1 OWI1r13 I6:10 $244"
NO u0A
1.0
027
1 06111113 I6:10 $06-934
NO ug&
10.0
021
1 06111113 15:I0 74.25-3
NO dglL
5.0
0.30
1 0W14fA 16:10 15-50.1
0-794 uWL
1.0
0.73
1 WTI r1519:10 106.45.7
ND uWL
$Do
1.0
1 06r+N1315:15 IIO.57.6
RI uWL
6.0
0.32
1 Oer11H3fe:10 76.34-]
0.k7J uprL
1.0
0-12
t OWIV1315:19 107.08•2
NO upii
6.0
0.5E
I o6H+9316110 75.35-4
21.3 uck
5.0
0.111
1 OWNH315:I0 lW59-2
NO up4•
5-0
0.41
1 0611111316110 156-60.5
NO uU&
1-0
0.27
1 OW1II131610 75.0715
NO UA
1-0
0.20
1 OW11113 1010 142.2E-9
NO NPR
1.0
0,13
1 uNl l R31&10 luml-dt-5
REPORT OF LABORATORY ANALYSIS
r lee r.We .n.. nor M nplpd. d-.ec.pt h ".
Date 0W2512013 10'49 AM .ene.n a,e -man caneent 0r Pace Aeellleal &4 &_ Inc- pe0e 51 01 77
Paw AMlylkd 6.Men, Me- P... AnNyd-l6.rrre.., 1" Pe4{ An.ly04m 4eeyµ46. kht
ace Amlytical 206 Ee.[ wedaw Raee -Foal 222a PN.ree. 9800 wne.y Ay. 6u1. 100
Pic- NO 27206 Aeh.AM NC 28804 FAeh•r.dh, NO 21078
f I30BJAM41021 (ake12SF 1119 I70ya75407
ANALYTICAL RESULTS
pre).cl; Swry Clo{. d•klr Aty(UPC)
Pew prood No.: 92159553
$"pl.t MW.13 Leh 10: 121e9113014 CQkvterd: 05WI304:00 Re Ivvd: 03nV1314:23 Makk. ri►lrr
Reporl
Puemelen Rmeulle VNI. LIml1 MOL OF Prepwad Analyzed CAB No Owl
9260 MSV Low Lay.] L4ndnt
Anary0cal M.trod: EPA 0200
I'd- k 1 Oldrloropcopene
NO upll
1 0
Elhyheneene
NO u01L
1.0
2•Heeenwl4
NO Uph
SOA
Icdnme,hene
NO Ngk
too
kletlylen. Chloride
NO -A
IA
4-Me1hy1-2-penkmone [MIBKI
NO K&
100
w rena
NO uyL
1,0
1,1, 1,2•[e-mail]1an
ND up6•
5,0
1,I,22-Tekad4ouoanane
NO up%
3,0
Tekechkwee,h4ne
NO uo&
IA
Toluene
NO UB&
to
$.I'l46WIl thane
ND uqk
1.0
1-1,2-TrlchI-4llr►n.
NO u0&
14
Trkhlam.eh►n.
12 upiL
1-0
Trkhkrmlue.omethen.
NO ugA-
1-0
I r9.3-TnehM,cW0pen.
ND .511E
1 0
v"A acelare
NO u911
50.0
vhryl cN.1d.
NO UgA
1.0
Xyl.n. 1T01.0
ND uv-
So
Fwrop4na
4.BromvluarPhenl4ne 151
86 %
70•!30
OlarumaeuoeomaOrene [3]
97 %
10-130
12-D dN-th&n.-M [SI
93 %
70-130
Tolu►ne•rk[3)
100 %
70-110
2326E Al"Imily
A"kAkal Me shod: SM 2320e
Alke lnity. T014M e1 CMCC 3
$7700 upL
Soot
03100 BOO, 5 day
A."Icol Meft P: SM 52109
600, 5 day
NO UP&
2000
300.0 IC AM- 28 Days
Anatylk.l Method: EPA 300-0
Sultow
1310J ugIL
250000
4S00 Chlerld.
Analyl"l Method. SM 4500•C4-£
ChWnde
29100 ug+L
IOOO
6310E TOC
Ane1y1k.1 Method: SM 5310EI
To Lai Otg.nk C!then 13200 ut'L logo
026 1
OW 1111310 11) 10061-02 fi
11.30 1
ONI1r131010 +00-41J
0.449 1
ON111316:f0 191.7"
032 I
0E111NS 1s10 11.614
0.97 I
DIV 316-10 75.W2
0.33 1
ON11f 13 10:10 101-10.1
0.26 1
OW 11H 3 16:19 100.42.5
0-3.1 1
OWII11316:10 e3O.20-6
0.40 1
CUP 1nr 16:10 79-34-S
0-46 I
ONI l r43 is to 127- 58-i
0.2E 1
ON11117 tE:10 106.50-3
0.48 1
Owl 111310!to 71.55-6
039 1
mlv$pl Ieiio 79-00-5
0-47 1
0N111N 111M) 79.01.E
0.20 1
OWIIA315:f0 7549.4
0.41 1
UN11f1311:10 W184
035 1
06l I17+3 IS 10 108-054
0.62 1
061IIII316:10 75-01.4
0.6E I
MI III ICI 1339.20.7
I
06/11113 15110 450.00.4
1
0 W 1+ f 13 15:10 1 U &a j-?
1
0 W 11113 15:10 1706OA7-0
1
0611v13 is 10 2037-25-5
1000 1
0611143 12112
2000 1
OWIM30110 05103 Q IS;15 62
2000 1
06MY112+12 14006-7 9-e
I*" 1
06111A ] 20 52 16917-00-E
I000 I
0610511120.60 740.+4-0
REPORT OF LABORATORY ANALYSIS
7%...p.n h.4 -1 Me eepl dy d..ewpt n N4.
De re: 060291201/ 10:44 AM e"6 A Py+RAYn penee6l OF Pace Fri.ly.kal servo... kc
P.O. 32 .1 77

i Pau PEe. A.lyar.l aarvlu 1, ee.
aeAna44icai 7e6 E.N rsr.yNw AeW SInN • 17]7 RrrerµN Le
Ilw. e.><.ril m. Err. HL 7i71M AJlerae. HC tae0r
Isle>sap null re7elasa. f r 1e
ANALYTICAL RESULTS
PINee1 Swly CWaed MI Aky ([11C]
Pace Ndlrel NO.. 92130852
1 Vicl.eFWn4yrlr Srl er., e AN IHc....
wYxcAs- IeAna)yiical
3775 Rrr.Ne ih
rwnlerrN.. HC 26G1A .Ir1.�.lala mr. Eden "c 2rlaa Acn w.c, lat: la6W
176liais ana: i37e1e7e-ea71 I17.}25.1-irie
ANALYTICAL RESL3LT$
! rvjecl: Burry CW..cl-MI A►y (1110)
P.c. ProJeq Pro : 9215965]
Bample- MW-14
Lob 0: 97159663016
CWle dod: 05110lI) I2:05
RecMod: MI1111413 M9aq' Wilier
Report
Peremelen
Re Nfltr LAJle.
Llml[
WL
DF
Plepued A11WV 0 CA$No. 001
6010 MET ICP, 10300
Ah.lyllcal Merced EPA6010 Prepstomn
]4e91ad: SM
3030C
An6many
ND vy+L
6.0
5.0
1
0IM401317;40 05rONS305.05 7440-3"
A ..ok
NO ugll
rD.O
10-C
I
WWI 17:441 D&DN}3 05'05 7440-35-2
B.N..
24,2J ugrL
100
SO
1
06f04113 17 10 ONON13 05105 7440.39.3
Beryflkfm
ND ugVL
I D
7.0
1
OW0401117-40 OMO103 12:45 7440-41.1
Cadmum
ND uok
1.0
1 ❑
I
06164113 17:44 O&OV13 04.05 744043-0
Ch,. bm
ND ug&
10.0
5D
1
OWDW 1317'40 00ON1306.06 7440.47.3
Co4.11
ND 4o+L
10.0
5.0
1
o6f04l 13 17;40 O&W13 05:05 7440-40-4
Copps
ND uglL
1D.0
5 0
1
ON04113 17:4D 061011113 05'05 1444504
Leak
NO uglL
$0.0
$0
1
0610411317:40 0610N1305:05 7430.9b1
Nlciet
ND ug&
60.0
5.0
1
0&04I1317140 OEMBF1305:05 744047-9
P,el.wW
ND Dp&
VIA
Ion
I
0NOH13 f 7:45 09MV13 05:05 7762.49-2
SAW.
ND 4&
$0.0
60
1
06104f 13 r7:10 ovilvi3 (15:06 7440-224
Thatoum
ND uWL
55
$.5
1
06W317:40 65NN 1105:05 7440-I6-0
Vanadlwh
NO ugk
250
50
1
06+0415317:40 OWN, 305:05 7440-Q4
Znc
NO Dolt
10.0
10❑
1
06414M 317.:A0 OWN 1305'05 744D-66-6
126D MBV Low Level Lannfill
Anrfylrcd M.lhe d: EPA 92$0
Acelom
NO uyl
too
t0.0
1
0=511114V V-64.1
AmlorArae
NO uQ&
200
1.0
1
0~314:0 107-Ml
84nm a
NO uglt
1.0
0.26
1
0 MWO 14:0$ 71-43.2
&Pmectdwonemene
NO"A
3.0
0.17
1
OMU1314:01 74.427.5
Drvmvt06hwr onleulene
ND uglt
1.0
0.16
1
MMU13 Kos 7S•27.4
Oromolarm
NO uglt
3.0
0.2E
1
090511314101 7"5.2
6kornnrhe6leh.
NO ug&
10.0
0.29
1
06p0511314:01 74.0"
2•8utanem(MEK)
ND Dolt
$00
096
1
0610311114;01 76.01.3
Carbon 6ru14de
ND dg4
too
12
1
0&ON 13 14:01 75.15-0
Car5orr latrerfdarlde
ND NW,
1.0
0.25
1
DW%fl314:01 Will-5
Chlmobmxne
NO ugA-
3.0
023
1
060ON131401 Ica-00.7
Chlptermene
ND ug1
10.0
0-54
1
O6r05113 14:01 7540.3
Chlorobrm
NO ug+1
5.0
0 14
[
064511314:01 5740.3
ChWr......
ND uu?L
1.0
0.11
1
0&oirl314r01 7447.2
1,2-Ddrrnma-}eMerapr-pane
ND ug1L
13.o
2.9
1
owo&13 14d1 96.12.E
OibromodNoromelhrlr
NO.0k
3.0
0-21
1
0&0511314-01 124.46-1
1,2-Oar.rrwa0une iED9]
NO uQ&
1-0
a"
1
06105r13 14.61 10"3-4
Lebrwnvm mo-
NO l*&
19.D
071
1
06r0N1314A1 74.954
1,2-0khlorobencene
ND ugA,
5.0
0-30
t
06105f1314.41 16.50.1
l 4-DKNuro6mlfrne
NO ulA
10
033
S
OWN 13 141)1 10646-7
Irr1.-1,44IN20 m-2-bul.ne
ND ug&
too
10
1
06*501114-DI 110•574
I,}•DkrJe.orin4r.e
6-OJ u91L
5.0
9.32
1
ONONQ 14,01 W34.1
1.2-131cMoroelh-.
NO uOrL
1.0
0.52
1
0610N1314L01 107.05.2
l,}•Dl Norwllrana
NO uglL
15.1)
054
1
OMNI114.01 71-15-4
W-I.2-0rdeweemene
9,3 ugh
5.0
0.10
1
064NI.114:01 1S&SR2
Gam-1,RGddwoeN...
NO ugfL
5.0
040
1
0WGW13 14:0I t56.60,5
t,2-Dkt4 rdprcd.er
NO ngk
tag
027
1
QSV&12 14:01 76-07.5
1,]•Dlohbwpprpyaee
NO idyl
TA
0.2E
1
06106/13 14:01 142-22.9
at. 1, 1- DlcWaropr.pen a
NO uDk
1.0
0.13
1
OWN, 314;01 10061-61.5
REPORT DF LA 00 RATORY ANALYSIS
1M r.v„1 D,w.�a a repeevaw e.erpr an M
Date: 06121IG 0 1110. 49 AM wne..r .,. r..nrn[en..n1 er Pc[. MA11ru1 s.rrw4 u.e. Page 31 o1 77
Para RnNynnr a.rvlw r, Ins.
lr��i cf^rai Are SDN IT[1
M.�rMr 1rC :? fe
I rn+>ersriw
S.rnpt•: MY044
Lab ID- 12169E6301S
Cd9eded: ON`3011312.05
Reoelvd: ON3111314.23 Mebbr: if114fef
Reporl
Perametell
Rs.At. Lk1it.
LIMI
MDL
OF
Prepwed Arko d CA$No 0.01
1260 M5V Low Level LandflX
Anelyl"l Me uwd. EPA 6260
v.m-1.3-pdeo.eprop.ne
NO DOA,
1 0
026
1
OWN1314;01 10061-024
Ed}y .-...
NO u011-
1-0
OAD
1
OWN 13 14:01 10"1.4
2•Heaan9nr
NO uQ&
500
hie
t
09rON 1314:01 Sol 79.E
Ie60l lh.M1e
NO ug+L
10.0
0.]2
1
OEM&I11441 744E-4
M.Orylarl. Chlaad.
NO ugrL
1 6
017
1
Da45113 14:01 75-W2
4•1A.Gy, 2 yen4n.r1. JWSKI
NO ugfL
100
0.33
1
06AWI314.01 IWTO-1
51yl.m
NO .0A-
1.0
020
f
06/05113 14,01 100-42-6
1,1,1k .b.d'y-Ih.n.
W; uq&
60
013
1
DaMV1314:01 630-20-6
1.1,2.2-Rlto.W.o.al.nr
NO ugil
30
040
1
MY1314:01 7934.5
Telr.dllwo.lhene
11 uglL
1 D
0.40
1
OWW1314:01 12?44.4
ToNme
NO ug+L
10
026
1
66/051f314:01 10-61.3
1,1,1-Trklllwoethrin.
ND u%VL
10
049
1
O6r05f1314.01 71-S"
1,1,2-Tvkhkroem.ne
ND ugm-
10
0.29
1
091W 13 1401 70-00.5
Torhlor"s,"m
D.AA1 ugrL
1 0
p47
1
061W 0 t4'9f 76A1.6
inchlwowommelhine
NO uCfL
10
670
1
09MV 131401 75,"4
12.34,kchlmapreyene
NO �v.
10
041
1
0E10136013 14:Ot 9&tS-4
V"fc. late
ND ugt
50.0
0.15
1
06105e$31401 106.0514
V" cm .w.
ND ug&
1.0
6.52
1
M*W1114:01 75.01.4
Xyllnl J49.1j
ND uglL
5.0
0.66
1
DaMN1114:01 OW20.7
si r ogafea
4.5F m Werobene.ne 19]
100 %
7O.130
1
06A7N13 14.01 460.00.4
Dbtordo6uarameMn. l9j
105 %
70130
1
DNON13 IC01 1669 53.7
1,2-01d+atooll a-44 [$]
90 %
70-130
1
OMN1314:01 $706007.0
TcgLw a-aM
107%
70.130
1
06f0511114.01 2DV-265
211203 Alkal"
Mlybcel Method. SM 212oB
Alkali". TeW al C&CO3
36100 uck
5000
IOOo
I
0N111[3 [243
62100 600, 6 day
AnaryAcll tyre lnod: SM 52108
800, 5 day
NO uurL
2D00
200D
1
OBMI11361 to 0610N1310-15 82
300A K Anlom 26 Oayl
AnstAkol Aletnod: EPA 300.0
swills
309o3 ufyL
2S0000
2000
1
09M71321AE $406-79.6
4100 World.
Me1yl..1 MethodSM 4500-fyE
CAWrlde
me uWL
loco
1000
I
061 I ft320.53 16a67-0o•6
6319E Toe
Anelybcal M.awd: SM 53IM
Told Orgent. Car hvn 9340 u011 1000 1000 t 06rD5r1321 SS 7440-44-0
0411. OW2672013 to:40 Aµ
REPORT OF LABORATORY ANALYSIS
I Ira renae NY -1 a np•eeuud...rapa rn U.
yr.Iaur art. -R PrrNnr or Pea Mop" S.rvw. r�
Page 34 of 77

PA.e A-wyw.l iarvleer, Ina P.c. Anilylierr 6.rv1.•a, Ina. P.a AnMyoae1 e4Mc1l, lna.
2eAmlytical' MIF at Me." R.aO • swaA 2225 RN..ad• f:. OWkee.Y Ar• s A. 100
w�w„ Ed.e. NC 2i735 A ,M.r . NC 2"N Hun+e,e a NC 26071
130e)e77a97+ fA]Al2s1-111A ['�6I IATSDaPJ
ANALYTICAL RESULTS
N.JW: 8ur.y cloe.a MI Aky PJ1cl
P.- P,.Jad No.: 9215WA53
6.mpl.: Mw-tl
L.b iD: 52191813016 CaMded: O6Wt3 06;13
Reolfvrd: 650I113 14:21 MMEr. NkNr
Rap it
P.ramele"
Rdlull. WN tkA
MOL
OF
Propelled "old CAS NO. ✓Duel
4010 MET ICP, Woe
A--W1IFt M.ihOd EPA6010 Prapelrdon Method! 8M
SOSOC
Ar,11, ny
NO uWL
6.0
to
1
0"40317:40 061CW1305-0d 1440.76-0
Ar.anl.
I,
NO
10.0
f0.0
1
0510411317740 06fo6117 oS:06
feria.
46.ZJ uyL
100
5.8
1
064411317:40 66Am30506 7410-19-3
B.rplwm
NO uq&
IA
1.0
1
064411317AII 0610W13 13141 744041.7
C.dmlum
ND up1L
I A
1.0
1
"AwI:$ 17>40 0"013 0691 7440-43-9
Chf•mA,re
NO up+i
to.0
5.0
1
OM01317,40 06A1143 0501 744047.1
CobAN
46,0 ap+L
1010
5.0
1
0504113 17:40 WWI 05:01 7440464
Copper
NO upA
t0.0
5.0
1
06AW13 17:40 06f06113 05-01 7440.50.E
Leal
NO ug1L
10.0
5.0
1
00"1317AU 0646r1305:01 743p•02.1
Nwkar
7.6J ugfL
so,0
5.0
1
06111013 17:40 0146113 0606 1440.02-0
Selenium
NO ug1L
10.0
10.0
1
0=411317:40 061661f36S:06 7762.49.2
sllaer
NO "A
10.0
5.0
1
OSAW13 11;40 WDUI3 06:06 7440.n-4
Th.rWm
NO up4
0.,1
6J
1
DWOQ 11117;40 06461t30506 7440-Z6-0
V.nadlum
NO -A
25A
SA
1
OB@U13 17:40 6141r13 05:00 744042.2
Inc
NO ug&
IOA
10.0
4
01A4J1317;40 054111305:08 T140-w 6
6110 M8V Lew y..awl Lrldfill
A.WyOoar Me nod: EPA 9260
Acetone
NO -a&
f00
10.0
1
06r1s/131AZ11 61•&1.1
"IQFlrle
Np upR
200
1.9
1
OW111121626 f07.13.1
Senlone
0.61J'Ok
1-0
025
1
OEM11131020 7143.2
BromoGelerom.pl.ne
ND ugk
1.4
0.11
1
06111113102E 74-91-6
0roreoddFAW...lh.n.
ND UgA-
1.0
0.1E
1
0.1103162E 75.274
&emoto m
NO vgk
3.0
026
1
06111113 162E 75.26.2
&omem•Ih.n.
NO ug1L
$0,0
0 a
1
0//11113 1624 74.63"
2-6utelrl•ne 111I
NO ugA.
IDo
OJ6
1
06f11112 162E 76-93-3
Carbon N. eMdd
NO wgk
lDo
12
1
ON, 1'131626 i5.15-0
Care. IeeAchlvrldc
ND ugA,
1,0
0.25
1
owl IM31616 56.23-5
Ch"Obencene
2.1J AWL
3,0
0.23
1
W11031625 f06.90.7
Chlanoo114ne
NO ugIL
10,0
0.54
1
OEIt1113 $026 7500.3
C-hkl.fW.
NO uWL
6,1
OA4
}
OW111131676 678E-2
Chkromeri.n.
NO uWL
1.0
0,11
1
oN1111] =5 74d7-]
1Z-Oevamo->-ChlDrop Op. n•
ND u0&
13.0
2.5
1
0611I7131126 96-f2.1
Dwromomloroln.nene
ND ug&
3.0
021
1
06111113163E 124-46.1
12•LMxom6erian a M4
NO up&
1-0
037
}
OW 0131.2. 106-13.4
Olbromvmeurane
No ZL
11-0
011
1
MIJ15162e 74-OS-I
I ZDkNWbb1,nlW6
1.1J uUVL
5.0
0-30
1
OW11n3163E WWI
I,4•DkhWubme6no
2A Np4
LO
0-33
1
OW111131:26 104-4617
Oitwl,4.pid+t9re-Z-0ulen.
NO ugfl,
100
10
1
16r1111] 1611 1f0-VA
1,1-0kMw0.11rn.
0.67J up4
&0
0132
1
OW111131626 7513,11
1.2-0k,N m1Ka
037J uOIL
1.0
0.12
1
06111113162E 107-t>&1
I.1.OkNweelhene
NO up1L
5-0
0.5E
1
on111316:26 M35.4
til•t,2•LMchler9.Shene
Z-ZJ -A
S-O
6.19
1
61TI11}9 1626 136.39.2
411n4-12.pr0N....Man.
NO z&
5.0
3A
1
OW11143 163E 166.60.5
12.Okhbropn.pene
NO u0&
I.0
027
1
01011113 162E 76-07-5
1,3-01d0orepeop.ne
ND -A
1.0
026
1
OW11113 $926 142.284
d.-1,3-0Idawopropana
NO uplL
I'D
0.13
1
06/11113 162E 10061.01.5
REPORT
OF LABORATORY
ANALYSIS
,Ne 1•Pmt Nell r M nmwc.d, •.caw n
#A.
Data! OWN2013 10 46 AM
■P eal w aten..nea.a el
Pon Frmiyleal AMae,
Im P.qe 36 0 71
P. oa Anel yauV AetMe." ne. I". Amlydul leMaar, Ina.
ace
AmMical" xnr.ow•svnA msn..rd.e
FMrR IeC 7Y766 A�..rlla, NC 26604
IMOD234MI I61504 717E
ANALYTICAL RESULTS
Rofad: &.1"CIO-d-Mt Aky JUIC)
p.c• Proj.G Na.: 9216pa53
Semple: MALL? Lob Id: 121814 53011 Calla dad. 051301110645 Received: 0517
Pelee A.Mys", 6."keol, I",
DEOo Kve•y Aw Snt. 100
HunYnml.. NC 7877E
[7041ai'r9[IPI
Report
Aalemelelt
Re1u11. Unite
Gmk
MOL
OF
Prep.red Analyred CAS No. Oull
1190 M611 Low Lee.l L.1011
A.9tr kal McIAod. EPA 6260
Ir•m• 1,3-Olchlwoyropene
NO dyi
10
6.2e
1
OW1 V 13 162E 10061.02.E
F-1lyhmiwl.
NO up4
1.0
0.30
1
010111111:21 1W414
2-H.x.nena
NO ug1L
ED.0
0.4E
1
OW11113126 S91.794
lodomellene
ND ZL
10.0
0.32
1
o6111113162E 74.11"
MaNylene ChlMnde
NO uqA
1.0
0.07
1
06f Iill 31046 7"91.2
4-M.W-2-p.MI on. 1MI61C1
NO 091E
100
0.33
1
06111031626 IM10.4
Styl4ne
NO ugk
1.0
0.26
1
O6,11431926 10042.5
1,1,1,2-Teuaddor0e$m•
NO ugfl.
6.0
0.31
1
OW11143 1526 S30.246
1,1,2, 2-TAVacl4mc nne
ND *&
1.0
0.40
1
owl 11134625 79.94.5
T ..Mwoelhene
ND upli
1.0
9.4E
1
0W1In31626 127.114
Tnlume
ND uWL
1.0
0.2E
1
9 liM31626 106.66.3
Tkhlwoelhlne
HD 091E
L0
0.41
I
001111151E26 T1.5S-6
2-inriilw6.01ane
NO u91L
t.0
0.29
1
061111f11626 71-pyi
T,kt,INosms-4
NO 001E
1.0
0.47
1
owl Ill 2 1626 76-01-9
irkMwoluerormthma
NO up1L
1.0
0.20
1
001 411111610 75-00-4
I ,Z.}nlWaoplopene
NO up4.
IA
0.41
1
OW $1131526 95.1 SA
IAny1 ■-Lela
Np uWt
50.0
0.35
1
O61I4113 1626 105.054
UL1yl CrAwlde
0J3J up1L
1.0
0.62
I
Wit Vll316-16 76-0I.4
XMn• eftotefl
NO "A
5.0
0.66
1
06113162E 1330-20-7
SurrApllae
4-Brom•luwobmxm.{51
96 %
70.130
1
66AIA3:626 460.OD-4
Olx6maMreromethrl• (sj
97 %
70.570
1
OW11113 626 iatlm' 1.7
12-0kNwoeth•ne-0415}
91 %
70.130
1
OWII031626 110641-07-0
Teluene•tl6 1S1
91 'J.
76.130
1
06111111 162E 2037.20-5
2710EI Alk%IJnn Analytical Molh4d: SM 23208
Al"IINly, Total •a C.0O3 136000 ugll_ 5000 1000 1 0//11113 12:34
6210E BOO, 6 day An►Iylleel Method: 5M 52109
BOO, 5 day ND uj0L HOD 2000 1 06101/13 01'}0 OW06113 12:15 B?
300.0 IC An 2E Days An elylket McOlod. EPA 300.0
Sahara 1400J v6VL 250000 20M 1 OU9132227 1460E-799
4600 Chlond. Analytical Moth. d: 5M 4600.0-E
Chlwld• 37100 uWL 2000 2o00 2 WIV13 ZL54 16167-oo-s M1
13109 TOC A pI[Vtx.I M.Ihod: SM SS1 DB
Total Or park Cerbcn 6110 uWL 2000 119K 3 06471110901 744044-0
Ow. 06FIIV2 DI 3 I0:40 AM
REPORT OF LABORATORY ANA LYSI[S
TN.+.P.rl "r M ner•d,icae..,dw n el.
.0m, eM ♦ hon ­1 OF Pace Auly6 s.mn. nC
P.O. 36 or 77

�/I/J' •
•
I.- A"v al l.M..a, rne.
306 E.0 M..de•r I.W - 61 A
V.-
An.Vyll[N a.rvlue, Ine� P.w AA.lyy0.1 a.7Y1.At, Me.
2725 AM (1, "M. :A'.. SW. M
�
aceAr�alytrcal •
P.r. *"Y0 0 6rnle.., 9M..
2M EW A4.W+ Rws .3w. A
Pare Anrlydral 1. -. dne.
2m Rn�rr:d. lie
P... A.Myw.r Mryrwr, I—
9eCn rxrwl Arr r- rpp
� �
Ewn He n7ee
W,.w MC 7leW Hwrr..yl.. fK 7A(Ile
' pm � -
EO+�. FN= 71:9!
A ye, 11C 7e6p1
.w„tie. NC 2e076
,+
034110 a-ewr
[emj -Wl i6 I1aHN+ 17
r3as.,er l.a c)i
14M)m 1rm
jt-w+ ,
ANALYTICAL RESULTS
ANALY-MAL
RESULTS
Pr9lecr: swrl, C461 ed•Ml AVY (WI
P,.*l Skrry CW..d-M11ury
100)
Pace Falecl NO.: 92159953
Pace PrvleCt W 9215053
sample MYe-20
LA 10: i21 SOSS3017 ' v.Ucl4d.: OW3011I I000
Racslyed: 0513111314:23 Malik: V*bel
S.mple: MW20
L11h ID: $2161413017 CnMd9ed: 093011a It.00 Reeelvrd 05131113 1623 M.M. V&w
Report
Repoli
paramews
R.wln
L4ala G116I
MDL
OF
Pr►pelad Ammy21d CAS No Ouel
Pvamal.w
RaWto Lk#b LIr1111
MOL
DF Prapar.d
Allaly3ed CAB N. ID-1
9010 MET [CP, 3030C
A.WytWal Me l,ed: EPA 6011] Prep.ralm 1Aelhod SM
3030C
9360 MSV Low L-I i-dillt
Aneloul Meswd: EPA 8260
AnUmbly
NO ugh
60
50
1
060411311740 O6+ON1305:12 7440-Wo
trowt 3-0.N... pwpene
NO wg& I 0
on
1
O6Af11310t42 10051 V4
Am..-
NO WA
10.0
10.0
1
Ddr Q0 1MO WWII 05:12 1440-36-2
@rhyeenrene
HD ug1L 1 0
0.30
1
OWIV1310:42 10041-4
©.r-
11.71 ug&
1oO
5,0
1
WW1 317t40 0670e1R305: 12 744o-39-1
2•04eenan4
NO idyl 500
0.46
1
ON11FI715:42 511 76.E
Berym-
NO uA
1.0
1 0
1
WWI 1PAD oe7ON13 13:62 744041-7
lddantalhvre
HD ug& 10.0
0.32
1
061111R3 16.82 74-894
C.Jmrum
NO u011
1 0
1.0
1
Demo 13 17:40 0N0N13 05:12 7440-41-9
M.thylm,a CAlalde
N13 1r9A 1 0
0147
1
061111ta W-42 75-0-2
Chromu,m
NO ug1L
10.0
5.0
1
HOW 0E06113 OS:12 7440.41-3
{MI Bp
NO ugfL 100
0.31
1
ON1110 t6:42 106-WI
cpnan
17.3 OOA
10.0
6.0
1
D60HI317'40 06W13 05:R2 7440-48i
Sryr4na
NO ug1L I 0
0.2E
1
0611103 161.12 100-42-S
Copper
ND uQ&
10.0
60
1
Dem4113 17:40 o61oe113 0 ,t2 7440-50-4
1,1,1,2 TrhaWcro•F.hd
NO v91i 5.0
0.33
1
owl Ist 31 e:42 630-ma
L-I
Np ug4,
$0.0
6.0
1
06A401,1 11;40 960e113 OS;12 7439.92.7
1,l,2,2-Tek4chlorwa,rne
NO u91L 3 E
(140
1
DWI 19314:42 79-34-5
Nickel
NO ulpt
500
5A
1
O6MV131?AD 0610611305:12 7440.02.E
Tmr.chkxo th-
NO ug1L 1 D
9.4d
1
0511111316:42 127-Ts•4
Ge1er4um
NO ug&
300
10.0
1
0604113 17AD 069N13 06 12 7782-40.2
TPIu..4
NO uV& I 0
0.2E
1
6W11113 Is:42 106 H-3
Slyer
NO ageL
100
50
)
0667V1317A0 ft;QW$305;R2 1440.22.4
111-TrIp,I9luem.ne
NO ugrt I
048
1
DWI 111316.42 71-55•S
Tlimlkum
NO uqk
35
SE
1
061040131?An 0&0e11305:027440-26.0
1,1,2-Tnp,lwoeillrie
NO uGIL 10
029
1
D61T 1013 16.4 2 79-00.5
V-.,)-
ND u9A.
25.0
50
1
060H13 1? Q o6+0e11105,12 744042.2
Trlpnitrr-M-.
NO WOOL 1 0
0.47
1
DN7111316`42 79 Ill 4
imc
10A 4orL
100
IOA
1
OW6410 0:40 06l0N5305:12. 7440404
Trkhl..R... -ts-
NO "& 1.0
0.2E
1
DGR 111316:42 7530.4
I),3•TrkehIw0prepen4
NOUVL 10
DAI
1
OWW13is:42 96-16-4
s3s0M1V44+vL.r414andlNl
Anaylc.lM.dwdEMe260
VYlyl r-W.
ND .2k 6o ❑
0.35
1
O61T01316:42 TDA-05.4
Ac.lene
NO uglL
100
Ina
1
Owl $11315.2 87341
VmV ewwwe
NO UD4 1 0
D.62
1
DNTR71315 42 15-01-4
AcryWA10111
ND MWL
20D
19
1
owl IM316742 107.11.1
X01ne{T91a)
ND ugl. 5.0
0.86
1
OW91316:42 $330-20-7
BOO-.
NO ug&
1.0
025
1
0611111316-A2 7143,2
Sweegalea
&vmvchlerameth-
Np ug&
3.0
0.17
1
owl 11131E-42 74,17.E
4.&drndluaeeevee0a IS)
07 % M130
1
ON111131s:42 460-00-4
BlomodlChlwpmeUlef4
NO ug&
1.0
0.16
1
owl 111315.42 75.27i
DIGamPaumvmelneee IS)
94 % 74130
1
0NR111319 42 166E-53-1
8,0-torm
ND ugR
3.0
0.26
1
0N1V1318.2 75.25.2
1koiwl rvaer4ne-d4 (S)
93 % 70-130
1
061111531E 42 1706"7.0
B,.--Ih-.
NO at
10.0
02%
1
ON11113161.42 74-93-0
Tok,"l d6(5)
100 % In 130
1
OW11M 10:42 2037,24-S
2 Bul.ncne 1MEN}
NO ug&
1Do
0."1
0&11113 16:42 7&03-3
23208 Alkohn"
Anely I Methoe. GM ]3200
C r,t.-&0.10dr
NO uryi
l00
12
1
0611111316A2 76.1"
Carhm leti-Nwlde
HD uOIL
1.0
0.25
1
06111113 16:42 W23.5
AArsaey, 70tw a4 tacos
0700 ulyL 5000
t000
1
ON11113 12:45
Chwldhrnxdll.
NO u0Y
3.0
0.23
1
06111113 10,42 106-10.7
stifle 500, 9 day
A-lylrcrl M.dlnd SM 521 De
Chw1aa91ana
NO ugA-
10.0
DIN
1
0WI1113 15.42 75•DD-3
L11rar9Wrm
NO VA
5.0
0,14
1
08111/13 1842 e7A6-3
BOO, 5 day
NO upAL 2000
2000
1 0616111301:10
06A3113 19 IS Dx
ehwlameeharte
NO uyL
1.0
0.11
1
0W111R3 1e:42 7447-1
1-2.Oeynma-l-eldMupevper,n
ND ug1L
130
2.5
1
06/11/53 Ie:A2 9er 12.1
300A M AnbiO 24 Days
AAWNcel MD alnd. EPA 3000
oThremd d,rerem.alane
ND ugA-
3.0
0.21
1
0E1l1112 teA2 124ie•1
5W141e
ND ugiL 23D000
2000
t
OBAW 11122.40 1480E-748
1.2 Olervmaoth r (EM
NO aq&
1.0
077
1
0NI1113 ta:42 IO6-93-4
Olhr9mememane
HO -u&
10-0
0-21
1
DWI IM316:47 74-1S-3
4100 ckladda
MMyllced Method SM 450E-CFE
12-Dkhh>rp6enlMa
NO vVIL
5-0
0.30
1
0&1Ina f6A2 MD.1
chwwa
1260 uWA low
low
1
0N1L53 2231 168e7.00-0
1,4 D1ch1-b-2enc
ND uq+L
10
013
1
06111113 W42 106-48-7
rr.ns 14-Didrlaro 7 eolen.
NO u%L
100
1.0
1
o6Htll3 15:42 110.57.E
6310E TOc
Anatyllral Ma01ee: SM 5310E
1.1-ORmwoerhene
ND WQA
50
0-32
1
0601119 WG 7534.1
1,7-DlcMoroeln.ne
NO uyi
1.0
0.12
4
OWI III 316,42 107-06.2
TW Orgarlle Cuba,,
9120 uDIL low
ION
1
08RIV02234 7440-410
!,1-plwvr orrhene
NO.0&
S.0
0.6E
R
DUII11318%2 75-354
p.• 1,2•Dld,iPlpe n
ND ug$
F0
Us
T
DN1111310:42 556-5>-2
tr4nr-1,2-pchrmned
ND ug.-L
3.0
041
1
ON 111f 016:42 R56-W-5
I3•CucYuu nprop.ne
ND ua&
1.0
D.21
1
DWI 111316r42 71-717•S
1,3-6lchlwoprayv.
ND ug&
1.0
0.2E
1
Dull 1101642 142.21A
d4.1.3 Ckd,rpinprvlwne
NO uVL
1.0
0 is
1
Wi 111316,42 10061-01-0
REPORT Of LA BORATORY
ANALYS IS
REPORT OF LABORATORY
ANALYSIS
TN. roped h.1 w W nryed,c.J. -,u n
hA.
Tlee,.perl.hY r l he,ehlnM,c.d.. pl In M.
De lf: 0628R013 10:49 AM
.1e..,d a,e wmre roieerinr
P.. h 1,w.l 5.1rb. r'c Page 37 e171
Dale: 06128R20tI 10.40 AA1
wnml..h eenrn -I el
per. M,.lgrap f.wnae. Irt
Pag. 39 01 77

�,=Anapical'
Pan Aneryaad M-A.n, Ina.
P...An.lruurle.mc.e,In.Per.
An.lydul a.r.14.., hie.
y113 6... M..&. R..d , 5 A
1273 Rv.nN. O,
U-Wo NA- .vr 5ulb 1DD
! -'
Ese.- kC 272M
A+nMlr. NC 1a1104
iMn\r4w.. NC 7a076
+
I3]61623-092s
te7e;Z54.717e
t704j67sa01x
ANALYTICAL RESULTS
proem: SWN plaaad-MIAiry WE)
Pace Porrect No-: 02159653
samPic MW-Z1 Loh 10: 31161093014 C Ilmol.d: 95130143 1410 R4nlred: OSP5111314:21 Ma►h9:'Wer
Repdrt
pelemelm Reoullr M11 LIm6 MOL OF Propr.d Analyzed W No. puel
Maio ME7 ICP, 3(p10C
AnO.nony
Ade.r4c
Snail
B4ryAlum
C4dmWm
Ctlrvmlum
Loh.11
Copprr
Le.d
Nldiet
Sereruum
Vvw
Thelium
Vanadum
zm.
1261) MSY Low Love L.ndf01
A-q
AuysmirM
Benzene
BrvmocNoromelh4na
Brvmodrhlvrume9lana
&ornolvrm
Brom methyl
2-Sulenen. tMExl
C.rb- denude
Comm letrechlorlde
Chlorobenaene
Chloroelh.ne
Chwrvbrm
OQ1Wfurrl.Mena
1,2•DbrOmO•}C140rOprOpaeO
OlEromornirRom.6fana
12.00er9moefime (E061
0l6romnmr1hane
12-0lohraroirer12en4
1 ,4.OICrdplOirentMe
Irane•14.p1chler.•7.61nen.
1,1-0"v-thane
1,2-D1cWOfuelMrH
1.1-UlcniordelMne
W 1,2•ptNoroe then e
u.ne-l2-dworaemene
1,2.0khkrtopraP•ne
1,1.Okhlarepropenr
rls-1.S•OiWllarovrovena
AAmy6ce1 Malhod: EPA 601 Q Proparoilon MoMod: SM )NBC
NO up2
6.0
$A
1 OW013 HAD QGN61t3 05:IS 7440.3E-0
NO Np4
10.0
10A
I o6J0411117:40 06AB1110616 744046.2
42.2J NIL
too
6-0
1 OM411317,40 061WJ130515 7440.51.3
NO ugk
1.0
5-0
1 0CM4013 $740 0600611111:55 7440-41.7
NO Nm-
1.0
1.0
1 0610403 17:40 0SX811305;15 7440-A .4
No ugA-
10.0
5.0
1 061041$117;40 OUIV130515 7440-47.3
NO uq+L
Mo
54
1 0=4413 1740 OW00113 0S:15 7440.46-4
NO uqA
Io-0
50
1 OW0411317:40 0610af 1305:Is 7440.50-0
NO ugn-
19.0
5A
1 OW0411317AC 06/06113 MIS 743E-12-1
NO nail
50.0
5.0
1 ORM4113 llim Qwm13 US,$6 7440.02-0
NO NA
10.0
10.0
1 0=411317:40 06Na113 MIS 776249.7
NO uWL
10.0
5.0
1 06A41317:40 DUO&130515 7440.22.4
NO uQ&
5.5
6.5
t 06104f 1317AO 06Ne"05:15 7440.26.0
NO up&
260
6.0
t maw13 17,40 DWM13 MIS 7440462.2
NO up4_
10.0
100
1 06*411317.40 0SAW"05;15 7440-06.8
Analytical Melhad: EPA8260
NO ugJL
IQO
10.0
1 OW1111S 163e 67-04_1
NO LA
200
1A
1 08111111 ASI W-13.1
N0 ,gk
$.0
1125
1 0e1I1131059 71i3.2
NE) uyi
3.0
0A7
1 OWIIIt316:59 74-97.5
NO upi
1.0
BAB
I 0WW13 ISM 7S-77.4
NO NIL
3.0
026
1 m111316,66 ?"15.2
NO N&
100
0.29
1 Oen 1111163E 71.61-P
NO up A-
100
0-66
1 owil".16em 1`143-3
NO iiA
100
12
1 owl 1A31a Sa mI S•0
NO uA
1.1)
026
1 051111131" 56.23.E
0.12J NA.
3 0
0.21
1 owl 1113 16-5a 106.90.7
NO uy4.
10-0
0.54
1 0611114316:Se 75-W3
No uok
5.0
014
I 06111J53 565E 67-6-3
ND N&
1.0
DO
1 061111t1 1659 74-67.1
NO NA,
13,0
2-6
1 MUM IBM 00.12.E
NO NIL
3.9
021
1 Mill116.55 $2445.1
ND uUJL
1,0
0.27
1 Mill 3163E 104.93-4
ND uOJL
to ,0
021
1 9M111131638 74.05.3
NO up4
S,0
0.3a
1 Oelltl13163a W50-1
1,3 uyL
1-C
0-33
1 WIII13 IBM 106-064
NO CIA
100
SA
1 06J1111316Sa 11D•57-0
"ugiL
5-0
0-32
1 08P1fi1318;6a 75.34-1
0,82J upL
1,0
0.12
1 061111131e64 107-W2
NO VC&
6-0
0,6E
1 Owl IFQ 10:56 75-35.4
28A NA-
5.0
O.tP
1 94111n3 16:51 fWW2
NO ug1L
5.0
0.49
1 owl I013 165E 156.MS
0,31J uA
1.0
027
1 06111111 t6:56 76-07.3
NO ug?L
1.0
0.26
1 Owl In31636 142-2e-0
NO ugh-
IA
0113
1 p61111111B3a 10081-01.5
REPORT OF LABORATOKYANALYStS
Tlea nW end nrla npnducrd, es" LN NM -
DM.. OW2812011 10:49 AM .4»ad the wdem avr.awd yr Pan Amkry{yl 8.h:a.. k%. Pape 39 01 77
Paw Ankype rl S.m-, rne. P.C.An4lypn1 84"Inni. M C
LL1�11 fCi 71/Ql iM E..1 M..diw Ro.e . o". A 11l Rh«We p
rrwPf.4re+mr 90.n, Nc 27m A.n.r . Nr- 23MM
iD3616n-0P2r (am)2S4-ir76
ANALYTICAL RESULTS
Prgavt Surry Ckeed-Mt Airy IOICI
pave P"cl Nd-: 9215P853
Pap RnNypeel bervlr. r, rne-
a iOnc,iy A„e Sw km
rri, W-A NC 28078
I1 IM-0002
sample: MW21
Pafamelan
Leta 10: 921 SOU301JI
Rawer MIS
ColledM- 0N30113 14:30
Rl Pcid
LM* MOL OF
Hruntl d: W3111b 1423 M.4k: NAkler
Prepared Anwrod CAS No. Qua1
6260 MSY Low Lovel LxldfNl
Analyllwl Melded: EPA 6260
inm•1-S-picnrnrepropene
NO ug1L
10
926
1
WWII r6:56 10061-02-6
E61Ybenrene
NO NIL
1-0
0-:$0
1
WII" IBM 109-41-4
2-Hr.rnon.
NO uglL
50.0
0.4e
1
OVIII1316,58 501.766
todome0l.ne
NO qQ&
10.0
0.32
1
96111J1316.5a 746E-4
M.Wyl-cNond.
NO uA
1,0
0.97
1
66111113 ism 75-00.2
4-Melhyl-2�enl.nvne(MI015)
NO uA
100
0.33
1
OWIII13Is," 105.10-1
6lynne
NO N&
1.0
0.26
1
0N11113 1631 1ODA2.5
1,1,t,2•Tairaohlvrvalh.n.
NO uq4
5.0
0.37
f
061111$3 10 58 630-20-a
1,12,2-Trinmmu.11eno
NO ug&
3.0
0.40
1
MOM la:S6 M34-5
Toaaditnalwo
NO up&
1.0
0.46
t
Ow IIha 16:511 127.1E-4
Teluwa
NO ugk-
Co
016
1
06111f13 IBM 1"45-1
1,1,1.7rlchlneealane
NO uqn_
1.0
BAB
1
D8111113 1538 71-55-6
1,1-Tnchimoe9lme
NO uOIL
10
029
1
MnI113165a 79L p5
Trlltllproelhen.
1.7 uglL
1.9
9.47
I
0WI$113163a 19-014
Trlchlwa4wnme1hen.
NO ug&
110
0.20
1
ON11113 Ia58 75.89.4
1.7.1-Td4hl.Pvp.Pv4^r
NO N&
1.0
0.4t
1
06411131411. 96.16.4
Vlnyl acelale
NO N&
50.0
0.35
1
Owl I?1S 16:56 106.95.4
Vlnyl tmfid0
NO ugVL
1.0
0.62
1
061111151e36 y"l-4
Arlene ITom)
NO N&
0.0
0-66
1
0601183 18-58 1330.20-7
Su Wint..
4•13rOMIuMbon"" (5)
S7 %
70430
1
D611111516:6S 450.00.4
DIErp ko emelhane (6)
1DO %
M130
1
DIV"11316:Sa 168653-1
1,2-pirhloroeplene•d4 t5l
94 %
70-13D
1
Owl $113163a 17060.07-0
Toluene-da(S)
P6 %
70-130
1
0611511/ 1154 2037-26-5
232013 Alkellnlly Analyucal Minn. dSM 2320B
Alke Rniry, Tolel me C.CO3 42300 ug& 5000 1000 1 WIM31314
62109 SOD, 6 day Anelyucel Me lhvd SM $2108
600.5dev 9600 PIL 2000 2000 1 061011301:16 Vium 311:15 97
3DO-0 IC Anions 26 Oeys An kiii me moo EPA 10D O
Sulrele 23001 NA- 250000 2000 1 OSMU1322:54 14408-N9.6
4600 ChloAd. An mMkal M.Ihed: SM 4500•0•E
Chlodde 248K uVL 10o0 1000 1 OWIW1322:31 t6667-00-6
13108 TOC Analrikel Method. SM 53111E
rate) Or g.mc C.r ban 13600 uplL 1000 ION I 0610511322;44 7440.444
Dole: 06126r2e13 10-44 AM
REPORT OF LA 80 RATO RY A NALYSIS
Me r.Pwl .h.f ml M mgmk-vd. -pt n e!
.9-4 p,e..rlVnW "m of Peer/wly➢ lB.�n M[
Pago 40 of 77

•
P... An.1yu... am..•., .n..
P.C. An.yYt.l 1.+rleya, I..c. P... An.lyneal Hnkn, Ine.
a
PAN An kri" 1.I.4. I. In..
Pan An.lytlNi. lxr4c.., 4nm.
P.- AAdydca13.n1..L Ma
(�r� ��}�t}�/� /. y+
�l�G/V rR±I ��LQ1
NS EA.1 W.dtw
RoW - SW. A
22i5 R..W IN Y000 Nxty1 Aw SW t0)
G�G /-Y R[ ILKII
Me EaY Mt.tlew ReW -.S�Nr A
]725 R.*Wa 0,
9W.1 rxrwt AW S44 Il'q
£~. NC 2776E
MMra.. NC MI Pr 1ufn4rwN.. NC 71076
y�,
Ea.n. NC 2T2e6
A4n.Am. W 26W4
NC Ma l
f
r
l3]d]973-6C21
0211154a1re 4751167&OM
I
13]6M2]diYl1
pmrJO4-717e
ITP11e75iW7
ANALYTICAL
RESULTS
ANALYTICAL RESULTS
wr11.9e: slurs Clv.ed Mt Ary IL11C1
1$pl.9l: s,,..y CI9a.d A!r Ary 141C}
P.9a 1$9JH%No.' 92169153
Pan Pr9pc1 NO.: R159153
Samoa: MW41
Lab 10: 11119013019 C.kdad- Otr101130940
Rocely.d. CV3101314:Z3 MWk-Y9Mu
lemplo: MW22
tab IV: 10211941134111 Coleclod: 057301130920 Ral:e4yed: 0513111314:23 MW&: V6W
R.pml
Rep6d
pummel..
Ra.ue. L1rNe Q vi
MOL
OF
p.ep.rod Malyled CAB No- OWN[
Param.tar.
Re.Wt. U-Ieg LI-t
MOL OF AlapMad
Anaey2ad CAS No- oua
6010 MET ICP, 36304C
Al4901c61 Moc
ad. EPA 6010 PF bpuallon
µamvd SN1
3030C
9260 M5V Law Laval Land}III
An Nyllcal M.Ihod: EPA 6260
AnNKwny
NO u04-
0.0
5.0
t
061N4213 17;/O 067061I3 05-16 7140-36-0
(1 r 7,3.01dacr6P.epene
ND U1VL 10
0.2E 1
W71711317-14 10061.02-6
AmNe
NO uyL
10.0
100
1
06r04A317:40 47E WQ 05:1a 7440-W2
E1hy15en2anW
NO ug4L 1.0
030 1
DN1141311:14 100-41.4
9arwm
107 ugrL
100
6.0
1
0610411317:40 0610N5105-5a 749-39.3
2-N.laO.Rla
NO ug1L 50-0
0.46 1
ON11113 17; 14 595 71-6
6aryllNm
NO u0&
1.0
1.0
1
D5RW1317:4m WWII 1351 744D41-1
4e60-1hon.
NO NA- 400
037 I
Wr1103 07.14 74664
Cadn4um
NO 1041L
1.0
1.0
1
WIW13 l740 DOOM$105:11 744043.9
A4r41111 CIN6rld.
NO -Q& 1 0
9.97 1
WI111317'14 75439.2
Chromium
NO vylL
10.0
5.0
1
W104743 07:40 MASI"05:11 7440.47.3
44m#W,2•pa nu Nana IMI Ex}
NO uWL 109
0.33 1
MIM3 57;14 IQA' W$
Ceaa11
101 ugfL
10.0
6.0
1
W704111 t7'40 OE70111305: 117440461
swone
NO u04, 10
0.26 1
W1111311'14 l00-425
C 6,Pa.
NO uq&
$0.0
5.0
1
0=601317:40 06f0611305: 16 7440.50-6
...
NO u01 50
0.33 I
DIV I V1317: 14 63020-e
L.M
NO ugk
10.0
5.0
1
WrOV13 t7:40 CBMIV13 (15;11 7431-12-1
1,I,2,2-T.bachlw.elh...
NO uWL 30
0.40 1
6611111317'14 79.34.3
Moe'
NO uWL
60.0
5.0
1
OL0411] 17:40 08MVI1(15'16 7440-02-0
T.bacM-1h.R.
NO ADA, 1 0
041 1
1%11111317 14 127.1E-4
S.IMIRm
NO ug4,
10.0
10.0
1
06a7031740 O"VII05:10 771249.2
Taluena
NO uWl 1 0
0.26 1
06H IA01714 f0E-1B•3
smv[
NO uA
10.0
E.0
1
041/4113 IT;40 ONOM110 A6 7440-12.4
I,t,l-T.1ohlPlp.dl.ne
NO u0& 1.0
0.46 1
0611111317:14 71.55.6
rhdbvm
NO uA
5.5
5.5
1
OM1131TAO 061 WI3 03:0 1440-21-0
1,1,2-Tdohlamoe h-
NO u0ll It
0.29 1
06111/13 1714 7040.5
Yaneaum
NO u0A
25.0
5A
1
01MV1317,40 W10613 05; 41 7440.624
imlchlotuntan4
NO ug4- 1.0
0.47 1
00411" 17:14 7941E
ZINC
NO uyL
1010
10.0
1
OSAW1317,40 011?W1360-11 7440.6E-1
TdchW.Onvl9.a.Ih4a.4
NO ug4 $.0
0.20 !
661111131 FA4 1i-504
1,2,3-Trl.hIMW-pole
NO u91L 1 0
OAl 1
WI V13 17'14 Will-4
6240 r6SY Law L.Y.V Ln+d H11
/U14ry11CN Mashed:
EPA 1260
Vhyl.-ml.
NO v9k 50.0
035 1
0611111317'14 1W454
A-tw.e
NO ug4
460
10.0
1
Owl 111317'14 67454.4
Vinyl Chle.Ida
NO 119rl 1.0
0 62 1
Owl In317:14 75.01.4
Apylwrtlrll6
NO ugIL
200
1.0
1
W tI71317,19 S07-S3-1
xWe.. (W.0
NO uO•L 5 0
1!,66 1
Owl U1317:14 1330-20.7
Ee"ene
0.31J 1tg7L
1.0
0,25
1
Owl 111317:14 71-03.2
sdo"NNS
6.umnphrprarue9l.na
NO uWL
111
0.11
1
Owl 111317'14 74-97.5
4-Pmsn.n luw Pbmx.n. ts)
% % 70-130
1
06 W13 17'16 4WO0.4
IN-ddNRrem.lh...
NO u011
1.0
0.1E
1
WNt11317:14 75.274
(SIefMlaRUM",$0W.I%
99 % 70-I30
1
W1111317'14 IWL-53-7
Emmolalm
NO -gll
1.0
0.26
1
wl111317:14 75-25-2
I,2P6chlp10e1h.ne d4 Is)
95 % 70.130
1
owl 11131714 11060-07.0
0'o mellana
NO u A,
t0.0
0.20
1
Wr10317-14 7493-9
T.I da N-CE(5)
99 % 70-150
1
061111131734 2037.2E-5
2.9uta a IMCKI
NO uWx
700
OA6
1
O IWI317-14 7"11.3
I32DB Alkali"
An.MK•r McM.oa- 3M 2720E
Carbon b.ulld.
NO upii
100
1.2
1
ON11113 17,14 7515.0
Camas letoolla4d.
NO .&L
to
0.23
I
ON11113 17:14 36.23.E
Nkms y, Tot.r a. Carol
147000 uyL 5000
1000 I
ON111I3 1149
ChIDMbM 6ne
IAJ VVL
3.0
".)
1
Owl III 317'1A 101-WI
62 SOO 900, 6 d.y
A -MI -I Me sled SM 52100
chl.r6am4N.
NO jai
100
0.54
1
66r11n317'14 75ae-3
CIII.P.k.m
NO ugrL
5.0
014
4
06111013 ITI■ 67410.3
800-5 day
3100 uyi 2000
2000 1 05mtll3 01'1O
06A15113 10 55 92
C1d.wm NL-S,
NO uV&
I-0
0 11
1
Mllf1117'14 7407.1
1i-Otrvmv.3•Ch4me Opa..
NOuWL
130
25
4
W1111317:H 96.12.6
300AIcAnions 210.ya
N,r yllcim4*tm6dCPA 7000
OINr Mloedora..lemN..
NO u110L
3.0
0.21
t
Wftl11a 17:14 124-4E-1
3,01.1&
33201 ugrL 2SO000
2000 I
0603113 23 07 1460a-19 a
1,2-O6romwe..n. (EI791
NO u01L
1.0
0.27
1
Wf1511a 17:14 10&13-4
06KOmomeman4
NO VA
$0.0
0.21
1
W71111317:14 74-95.3
AM ChlPm4d.
Anelyncal Meawd SM 4500-C1-E
1,2-MPAQ. ohm z.ne
0.11J upl,'
5.0
O30
1
OIVIIII317; 14 9&34!
Ch40114e
646E uQ& 1000
1000 1
064130132237 1661700E
1,4-olcNm.b-:an.
3A uWL
1.0
0.33
1
06r1111317:14 106.4114
NaOa-1,#•dWo.0 2 tn.t.na
NO uyL
10O
1 0
1
06H111317:14 110.57.E
$3100 TOG
A..y W.1 M.Ihod SM 571011
l.147kh1u9.fi4vhlorv6lh.dnne
1.7J upM1
5.00
0.12
1I
0611111317:14 7&34.2
Toles Ory.nlc Car hon
11300 .OIL fm00
ION1
06+0511] 23�N 7440i4-0
17ne
OA7J u0&
1
0.12
O1Y1111317;14 107-WZ
1,1-dcMorvel114na
NO u0M1
Sy
0.56
1
Owl" 1311:14 75.35.4
d1-1,2-pdaoroelhone
314 VOL
30
0-11
1
ON111131714 IWW2
Im.h.-1,24X m610a11ana
NO u04
60
0.12
1
wilp.317:14 IN-00-5
1,2 O1d+raeoprop..le
NO ug0L
10
0127
1
0&11153 171141 71.67.E
1 7-ON:Id6reprep...
NO uglL
1.0
021
1
06111f1317;14 lQ40.9
ck 1 3 OkN-f..p.n.
NO ugh
1.0
0.13
1
m6111rt317•.ti IOW t-01-I
REPORT OF LABORATORY
ANALYSIS
REPORT OF LABORATORY ANALYSIS
Oaf. 0612612013 to 49 AM
w.ro.,.ar.r.r4n c61.Ianl o F.-A wKmal sw.v.. 1- Papa 416177
ON Ia. ON26l201310A 9 AM
w1-tth.rn.4n m.nwrtar0-
a....r.ca. S.rvr.I. N.c
PeO. 42 nr 11

•
Pace Apo
vgcoEll:nAsara,
.R1.
P.A..ryp7.l S
P15n .
Ak.Mworc..,1
2e E
.• srBAnd��� R
T25 Ry.nxq (N
A0n
i.Av
.�
WM
A — NC
2.a,1
1m07ePC
.
= pM2
Salelns7, l0
1704I67'F9W7
QUALITY CONTROL DATA
Prajeol. 9urry Cldbed-M1
APy (VIC)
P6w ProJe41 Hp.: 92159633
OC Batch: M✓5RP117449
An.tole Me1h.4
EPA 5010
pC Ratea Ml11104: SM 9=
A.eyele Ileeenphon
6010 MET 3070C
Aa.ad.ted Lah S.mplee: 12l39637001, 92159953002, 82139353003, 92559853005- 97139653009, 92139653007
METHOD BLANK 904386
Ma4'hr: mtsf
Aewdared Lad $e wife 92159853001, 92159553002, 92139653003, 92159933003. 92159653009, 92139853007
Blank RepwMlg
Pelem.pr
unee
R.e,M LMN1
I woyced QM0111 .
An6mmy
uyL
NO
8-0 0"311321:39
Are.,4c
•,y1
NO
10-0 00,0N1321;39
Bsrk,m
•,91L
NO
f00 0o/0N1321;39
Berywk,m
nWL
NO
1-0 WIO711321'39
C6dmNm
uyL
NO
1.0 05+0311321'39
ChrpmNm
uyL
NO
10-0 OM311321:39
COW
uyL
NO
10.0 0610311321:34
Copper
uyL
NO
10.0 0610311371:39
4e.d
IL
NO
10.0 0010311321139
Nickel
uyL
NO
50.0 0154v 32;n
Selmu.
uyL
NO
10-0 06A 1371'39
51",
aprL
NO
10.0 05MV132139
Th...
uyL
NO
5.5 0N0311321:39
V ...ill.m
uyL
NO
25.0 06A31113 21:39
2krc
uyL
NO
100 0610311321.39
LABORATORY CONTROL SAMME:
Peruneler
964307
untie
Spike
Canc.
LCS
Ruwt
Les
%Rec
%Rea
lkNs Oveeksm
Ankmo y
,.yL
500
503
101
80.120
A,44w.
pyL
Soo
504
101
60-120
El -Wm
pWL
50o
eu
98
61, 20
9arywin
uprL
500
521
101
90-120
Cedmlum
uyL
800
515
103
60-120
au.mlum
uyL
Soo
505
tot
80-120
Cotten
uyL
Soo
Soo
$01
80.120
Copper
uyL
500
467
0
600.120
Lewd
uyl
5.00
502
100
80.120
Nickel
uyL
50o
509
tin
a0-120
Selenium
uyL
500
563
113
so- '20
Slyef
uyL
250
260
704
800.420
Themum
uyL
No
4"
99
60.In
voinssunt
nGIL
$00
469
96
W$20
zinc
ug'L
sw
537
111
0420
MATRIX $PIKE A MATRIX SPIKE DUPOCATE' 064US
9114369
MS
MSO
92TM51DQI
SO"
Spike
MS
MSO MS MSD
%Rao
May
Pwremelm Uric f{e.Ai
Cone.
Con..
Rkkuk
Result %Rec %Rae
Umis
RPO RPO Oval
�
A,Nknmy uyL NO
500
SOo
497
501 0S Iw
75-In
1 20
REPORT OF LABORATORY ANALYSIS
Tra. ,apes ehtl ,wl tr. ,eprPdund...[ep:. PA.
Date. 08128R013 10:49 AM ».ho,n n. ,mn.n µ.lor v.e. ,v,.+rw r s.r,�.. r,� Page 43 of 71
P... A",.."beMc.l, lea
P... An.lyga4 6e.r1..e- I,—
Peu eneryaeel eerv,ee., Me-
se
aceAwlyticala
2O5 E..t Me.dow Ro.d • 9, A
7725 , ,.d. 0r
NM K , =100
Eden NC 2>70m
An Mr, N 2W4
IM1 ,e NG 261
+
(a3ek[7a-o92,
Ipw 126e-i1/s
LAM P67590p7
QUALITY CONTROL DATA
Plojecl:
Pap pr9JeR No.:
Sorry c7uwe4MI My [111C]
921591153
MATRIX SPIKE 8 MATRIX SPIKE OUPLICATE•
984399
984389
MS
MSO
9215051001
Spike
Spike
MS
MSO
MS
MSO
%flee
Mae
Paramele, Ibis
Ruuk
conc.
Cone.
R—un
A.. M
°.► Re.
% Rec
lkrar
RPfl
RPO Cl-1
A,eam.
uyL
NO
100
500
164
502
9$
100
M125
2
20
9erlum
uyL
22.23
500
"a
497
504
95
96
7S•123
1
20
9e,ymum
uok
NO
500
500
507
514
101
101
7}123
1
20
C.dmwm
uyL
12
500
500
4"
504
100
loV
75.I"
t
20
Cheomum
uyL
NA
500
500
495
501
99
100
7&125
1
30
Coww4
uyL
NO
Sp0
500
491
a99
98
00
7b125
1
20
Lipper
uyL
N❑
590
500
463
469
92
64
15-125
1
20
teed
uyL
MO
500
500
466
489
97
97
75-12S
1
20
HIck.1
uyL
N❑
500
500
493
40
90
100
75.125
1
20
9elenNm
uyL
NO
500
500
S35
523
107
100
73.125
0
20
Serer
uyL
NO
250
260
258
257
102
103
min
1
20
Th.b.
uyL
NO
50o
S00
479
4"
95
"
'15, 125
1
20
V.n.dh,m
vyL
NO
500
me
483
449
96
90
M125
1
29
Tint
vyL
NO
S00
500
SIT
517
106
106
M125
0
20
REPORT OF LABORATORY ANALYSIS
TN.,.pod M.1 nor 6. nPrnduc.d-..opt h ell.
Dille ' p612N2013 10 49 AM r. nm.t w�. w N, e.n..et or R. Amiylcal 6.wb., h•c
P.P. 44 pt 77

.Aq AMIVMuIVW..., Ma.
IL..AnA.y4./l a.ryla., M[.
P.- AnW,6a.l S—P.., Ins.
1
aceAnalytica!•
xs EaN wawwtr..6-Gw1.A
2223 K,.at. Dd
1kAQ .[n.. rR.. Sr.. sW
.
I—m.
aa.n, htC T+2ea
A pqw. NO 26a04
.1un.a..yd., HC 7a076
130a]173a921
Io-AP54-71m
(70416754m
QUALITY CONTROL
DATA
"I". 9uoy Ck1..d-IAt
AhY (IIIC)
Pon Prood N.. 921S1053
OCRAWAL MPRPm13447
Arr.Y.k. Method
EPA6010
-
OC Batch Me" SM 3030C
Arury.l. D—ipkm:
SDI MET 30)OC
Aaaoelaled Lab Sample. W15985
Well. 92159657009, 92 t 59653010
METHOD BLANK. 164390
Mahn Val.,
Aayodaled Lob Samp4a 8215915D006.
S2159M 53009, 021511653010
Blank R600nln0
P6.meler
tine.
Re.u6 LWA
Analyzed OuMMn
AnOthb"
OWL
ND
60 051DLI 123:36
ks"D
OWL
NO
100 0010511323,36
860tm
Ir.
ND
100 Oefoul323,35
B.Mlulm
NWL
NO
t D 00MI 1123,36
C.d .n
uWL
NO
I ❑ OS1061132332
Chmmlum
upL
ND
100 06lOSl132ZZ36
Cope:
upl
ND
100 0641t11525:36
Lop➢e.
upL
NO
10.0 WON11315:55
Lead
4L
NO
10.0 06r0y13 23,36
Mcke1
UOrL
NO
50.0 OWW 123i36
SAW,*.
RAIL
NO
10.9 D6MA:127:36
Sauer
u91L
HO
100 06MM323.36
TA.alum
uyL
ND
55 66my1323:36
wnedum
OWL
ND
25A 01f051t321:31
Le[
LIWL
NO
$0.0 W00511121-M
LABORATORY CONTROL SAMPLE
P6am.l.r
964391
unl.
Spite
Cope.
LCS
Re.M
LCS
%Rai
%Rae
LLrft 0Iu16.n
AnommV
uWL
500
St6
tD3
60.120
A.a.ry1:
LWL
500
510
104
00-120
Sar.tm
ug+L
50D
601
100
60-120
Bary6lum
LVL
$W
533
107
60-120
Gdmkun
uWL
500
514
103
10-120
Clw.mum
OWL
5O0
SOO
IBe
60.120
em"
UVL
Sdt]
50%
too
10.720
Cupp.
PA
Soo
452
96
10.120
Lead
uyL
!,DO
50
102
10.120
N1ck41
-OA
500
514
101
60.120
sm-l.m
ugrL
SOD
$27
105
M120
Saner
uWL
250
25a
tin
60.120
ThaNlum
4g4-
Soo
502
too
60-120
Ven.dlum
ugrL
SOD
494
99
Win
Lac
LWL
500
55S
111
60.120
MATRIX SPIKE 6 MATRIX SPIKE "LICATE 014392 M4393
MS MSU
92159653006 SpiHo Spike HAS MSD MS MSD % Rat Mat
P.1.meler unity Rea101 Cent. Cant Rendl ReRAI %Rot %Roe Li"% RPD RPD Dual
AnkmmW uVL ND 500 Soo 316 503 103 100 75-126 3 20
REPORT OF LABORATORY ANALYSIS
TN...pW ■..t -x h. r.Pr^ .e. —jA n M.
O.I.. ON2W2013 $0:49 AM .1h.1 M w.ar.n ca...n1.r PK. Arvllu[O % . a 1. Pape A o177
[ Pa[. Anmelymal Se.rl[.a, 1nC-
Pace AMtyu"l 6"Ifte. rn 0-
PA6 An.lrrhal Son—[. Im.
t..1 A..m. Pe.n . $— A
acel4nalytrr a�
2227 RNr.w Or
ae901Nre.r .. 9uiu 10D
j ........y..m Elan. Nc 212l6
A.hAW4. NC 7ea0A
larwrww. NC 20070
' 1]36k6�-0ft7.
[a.N175A-71 �6
(Y6VH7�+909:
QUALITY CONTROL DATA
Pm)vd
Sumry Vased-Ml A4Y (ur-)
Pea Roiled No.
92159653
MATRIX SPIKE 6 MATRIX SPIKE DUPLICATE:
9643912
964393
MS
M"
92159I43DOI
stoke
Stoke
HIS
MSo
MS
MSD
%Rac
Kit
Peram.ler Llale
Result
i 6.We
Cone.
Ruun
RooWI
%Roc
%Rec
LJmkh
RPD
RPD Dual
AneNe
u97L
ND
no
500
517
505
In
101
73.123
2
20
8.61m
U9+L
11.51
500
500
51D
501
too
N
16.125
2
20
BOVA—
OWL
T16
SOO
SW
532
5111
too
101
75-125
3
20
Cadrnum
..WL
HD
Soo
Soo
SDI
496
101
99
7fr125
2
20
CMolwum
up&
NO
Soo
Soo
491
440
90
96
15-125
2
20
C.b.a
6W'L
ND
500
SOD
501
490
100
96
75.12!
2
20
Copp.
uA
ND
SOD
Soo
SOD
467
99
96
TS'25
3
2D
Lead
1.WL
No
500
5Im
501
401
101
"
7'F425
2
20
Nickel
.OR.
ND
Soo
Soo
512
S03
102
301
736 2$
2
20
S.lanlum
uWL
NO
SO
500
579
566
Ito
113
76•t2S
2
20
Suter
UWL
NO
260
256
256
251
102
10D
75. 125
2
20
Them.
Zl-
7.5
Soo
500
501
492
99
07
73•l2S
2
70
vwbdW
uOrL
ND
SOD
SOD
496
A17
99
97
75125
2
A
Lnc
ualt
NO
5%
500
544
613
107
$211
MI"
2
20
REPORT OF LABORATORY ANALYSIS
rN...Aen Chas-1 e. r.pr.du<w. —0 n W
Date: ONp61291 ] 16:411 AM .0-11a-'W', aan..nt.r pare Anawy Iian k IR
Pepe 41 or 77

Pie. Anal yucel e.Mee., Inc. Paw An.tyaerl se-k..• Inc.
aceAndlytfcal a Zu Ern Mint.1i - &n[e A 7275 R.nnw Or
I �� EWn. ML 71Z9p A amm.. NC 714W
i]]ap23419]1 4620l154-1116
DUALITY CONTROL DATA
Propel- Sorry Cle.ed-Mt AYy(UIC)
P4Ca Pl ojaet Na
92158653
P.- A.Myn"I 9.mlue, Mr. Pen AruJyde.r a.mi-. Me. P... Ae.".d 9-FL... Me
pew K-r Are &W. 1 W acelm)ytical 205 E.N Nar- ROM - S1N1r A 2245 ttr. ra. d.
IAnr1rA.. NG 2wTh J .ww�aYO.� F.., NG 2720 Ad1.r{rr. NG 20604
1700875i L1Jdn,sws [phone]
QUALITY CONTROL DATA
Prejac* Sw y Cbnd-MI Ny lU1C}
Peace Project Na.! 9215"53
OC Balch: MPRP113465 An,."k. Method: EPA 0010
QC Ulch M.9wd: SM 1030C M.1y.la Dnulpbw: $010 MET 30MC
A ...Wad Lab Sam0..: 921596510, 2. 92159853011. *152653014, 92159a55015, OZ559653018. 9715985301732f5965301b,
92159653010
METHOD BLANK 98e294
Meats: V5ltar
Ae.oclaled Lab So mpiae:
P2158553012, 92156e53053, 921596530t4, 62t59833015, 92159853018, 92159651017, 97159651016.
P2156651019
Bl.nk
RkpMN1p
Paramour
Units
R-30
Limll "$ad Qua66e1.
".Wq
t101L
NO
6.6 OWOW1303:44
Ar.eKe
uy L
NO
t0.0 OWOW1303:µ
6.11um
-WL
NO
100 OOM I30144
8 vol-
uyL
NO
1.0 0610611312�r
Cadmium
u01L
NO
1.4 08MIWI30144
Chrprnl-
uOL
NO
TO 0610W1303-44
Cayak
uyL
NO
10.0 0&E611303-44
Capper
uyL
N❑
10.0 06MWq 03;µ
Laaa
uyL
NO
10.0 OWOW 30 -44
NN.k.1
u01L
NO
50.0 M060'13 03-44
Selemk,m
u0rL
ND
10.0 06Y0601303: 44
SSraf
uyL
NO
10.0 08r0a113 03'"
Thellum
uyL
NO
5.5 06M8H303,44
V.nadlum
uyL
ND
26.0 0W04IM303-"
Zinc
ryL
ND
10.0 0suo1) 03,44
LABORATORY CONTROL SAMPLE:
Param..ur
966266
We
Spike
co".
LCS
R..14t
LCS
%Re.
%Rae
UIRs O0016.1e
AnO--Y
uyL
500
494
69
60420
A1.4ria
NyL
500
490
9a
a0.1211
Swum
uyL
5OO
471
94
60.520
B.ry6um
uyL
SDO
S0l
102
80-120
Cadmium
uyL
590
491
98
80-120
CRraRlh,M
uyL
500
460
84
80-120
C.b.N
OWL
S00
410
94
a0-120
Copper
uyL
500
477
96
a0-120
Lead
uyL
500
460
96
90.120
W1e1
uyL
sD0
447
97
60.120
Sel.nlum
uyL
500
"I
115
e0.170
86re1
uyL
750
N3
97
80•f20
T114OWM
uyL
500515
95
So- 129
V.n.dum
uyL
5o0
471
96
$0.120
inc
uyL
500
531
106
e0-120
REPORT OF LABORATORY ANALYSIS
f.. r.Wft W.r -11y reFm - .. c.p In MI
Del.: 05r26rf0131049 AM wv-i" en.n mn"N 01 Pec. ArrlyuW uevr e. Ins
P.0a 47 of 77
Aa 0e AAOIyU al $-I0a r, Me.
gmK+rceY Ave Sow No
.Ap,rrwd. MC 763I1
I:w>srsacw2
MATRIX SPIKE d MATRIX SPINE DUPLICATE'
966296
006M
MS
M50
92151946001
Spike
Spike
M5
MSD
MS
MSO
%Roe
Mn
PaYameler
LWIA
Rae4At
Cane
Cane.
RO W,
Reeu6
%Rae
%Rea
Urrift
RPD
RPO Ouel
ArKlmany
uyL
NO
590
500
501
466
101
91
75.125
3
20 Y
An fgt
uyL
NO
500
500
Sti
602
102
100
M125
2
20
Sedum
uyL
104
500
500
574
W
14
61
75•f25
2
20
Serylwm
uyL
NO
500
$00
500
466
f00
9e
7""
2
2a
C.dmlum
uyL
NO
500
S0o
476
466
65
91
75.125
7
?D
ChromWm
uyL
N❑
500
500
462
"1
62
60
75•f25
2
20
CabeX
uyL
S3.t
500
500
515
506
92
60
75-125
2
20
Capper
uyL
ND
500
500
507
414
101
96
IS•126
3
20
Leed
uyL
Na
504
500
i7p
461
94
92
7a+125
11
2
20
Nkkat
uyL
NO
500
500
476
46e
66
94
125
2
20
59Ienklm
uyL
11.3
500
500
519
506
102
66
75, 126
3
20
SWb
uyL
ND
250
250
75.3
70.5
29
11
IS-175
7
26 M1
Ttulkuln
uyL
ND
SOO
500
472
407
64
92
75.123
2
20
V.n.dlum
uyL
ND
50D
Soo
478
464
65
93
N>•125
3
20
Zinc
uyL
NO
500
500
504
494
100
96
76.125
2
20
REPORT OF LABORATORY ANALYSIS
tNr r.Pnn Y.N ner ba lapeeduK.d, e.eepr n M,
Dow 06128Ye013 10!49 06M .,.Awl M when cnl..enr Nf Pau An.lyxal SdMcae. Int.
Pe0. 40 of 77

PAZ A"ok al e.nieu, Inc- PA.. An "cal Mnkn, In.-
- aceAnalyticai • 205 Ea k M.aeor See. A 2rn R.nnp.
r .w:Ne..rl.lraP Eden. NL 21---M AN.Ne. MC 7A9f11
i3361e:7-i971 1e 2*25..7, 10
QUALITY CONTROL DATA
ProJrtl:
5mry CW,.d-MI Amy IVtG!
Pat. P10*1 N0.
92159653
UC Be":
M51/23197 Ma2y.ld Mdlhed: EPA 6260
OC 8a1ch Me"
EPA 6260 Amiy" D►eugAw 6Mo MEV Low Loral LdndPA
Anea.tad Lab Sampler 92159653p01.92l39653002. 9213%53003, 9253%53003, 92159853006
METHOD BLANK. 94616 i
keelnl: lom W
Aeavyaled L+b Sen4ka. 921 S%5300f, 92t59653002, 9215965]tl07, 9215%63005,
9215965]006
B1anF
Raporiin9
P.1 k1ne1rf
un9a
Newry
LkA1 Anldyxad
2-letrecNorpaeeana
nyL
NO
5.0 0610CJ1303:52
f,l,f-TnR4o.0a1hena
uyL
NO
10 Oe1051t303:52
1,1,z,2-TitraPhlurn.dlrn.
uyL
NA
1,0 WON 11 61:S2
1,1,2-Tfld,largpn.na
OWL
NO
I,610 0 0511303M
1. 1-T1kaJaeeurend
YyL
No
5.0 W051130132
1,1-auuoro. n.nr
"WL
NO
6.0 AMU, 303:52
1,2,]-TnoN«opeopenr
WWL
NO
1.0 Gd1 M303:52
IA-Dw10mo 0-Ciompfepa/le
uyL
NO
130 06105N30357
1,2•Dm9n.oelnarw }EDB)
uyL
NO
I A OdfuV 3a377
1 r2471cfil0rdreneene
IrWL
NO
50 00A5113 03.52
%2-01dwwoa0ner
bWL
NO
t.0 WIWIa 03:52
1,2--Dwidopoer
WL
NO
10 0500w 11003:511
1DIX
oy
NO
10 ofilw 3:32
1,1khlmQbepnxn,e
uWL
NO
10 WOW$36152
2•861tan9na IMEK)
UWL
ND
100 0e105113 03:52
-Ne.mme
UWL
140
50.0 WWI
4•Mem0•2 p.nlanala lNIIBKI
uyL
ND
I DO WWI 03:52
Atelwl.
uyL
NB
100 fX.M'.11130152
Aayla,roM
uyL
NO
200 061W 303:52
B.nxene
uyL
NO
I.0 06 521153 52
&wn0w0rnn,el�ene
uWL
NO
3.0 gem* 01.52
&omorl.hrontmeln.nr
uyL
NO
so DOW) 03:52
&Pm.nnn
uyL
NO
30 OWN130152
%womathane
uWL
NO
10.0 0616571303,52
Cdrb- dl.ullde
uyL
NO
100 06106113 03'52
Carvm, rcuau,tww.
UWL
ND
1.0 OW51130115Z
LlirnrpWntenf
VL
ND
3.0 05 sf1k30a 52
Chrmpelhr+a
uWL
NO
t00 Wow 1303'S2
Chl.f.T.rm
uWL
NO
50 94fM51130152
CNw ameda„e
ayL
ND
I.0 11"S'1303-52
w-5.2-Dlcnlvroed,ena
uWL
ND
S.0 odr03f110]-32
4.•I.3. D+d,lpraprawr,.
uyL
NO
ID 06+0511301:52
D6lumochlwnmaeiene
uWL
No
30 OTrD51110352
ONNamontelik"o
uyL
NO
10-0 D400511103;52
Qenylpen7ane
uyL
NO
IA O6M51t301:52
lodom.11 r
dWL
NO
I o o WWI
M.lhylene Chloritle
uWL
NO
I.0 "llow1303:52
Styrene
UWL
ND
1.0 06fo511303:52
ievachloroednnr
uWL
ND
1.0 OW511303:52
TO....
UWL
NO
10 06ffisl303.12
ken.-1,2 Dcftloroendne
uyL
NO
50 06f95r1303:52
e ane.11,3 Ot-N-propene
pyC
NO
1.0 p"w 303-62
Iran.-1,4-1XWm0 2.9uwane
"WL
NO
100 0firo5+1303-52
REPORT 0F LABORATORY ANALYSIS
Ta. nporl Np nelq r.ryPNro,4 e.o.p n M
Otte OW242013 10'49 AM r.arwn n. W+ �n el Pi- Aru,7rc.1 5.,wv... [rc
Oweken
P.e. An.lyd..l e.nl..s, in.. Pf ee Anal ytlaal eefT'le.., lne. P.ca A neriel"I 6eM4.., Ina.
MM n - Ava Sw. 100 aceA�aiyfical� - L..1 w.m.Ilp,o • 1„e. A -I- 01 T ad. or
Mn.• .. WC mle " ia. r: d..•. NL 7729e A04W0. NC 2e6W
1m�W15-9psf7 [pe,6U-m, 1:6p3+•717e,
OUALITY CONTROL DATA
p(ge.f. Suny Cbae"t Airy IVIC)
Pd9e prppd Np.. 921524151
METHOO BLANK: 9a5367
Malnx: Watn
Adwetel" Leh 5amplee
92157653001, 2215"53002.
921596S 3001, 921505105. 0215%53006
Stank
R.Owtlnp
Peramelef
un"
Rrdpll
Lirm Analyzed Ouakkn.
Trlp,rarvrlhM,r
vyL
ND
6f03f
1.0 01190V
Tr kNbrv4geremefllrne
uyL
NO
I.0 W105+1303.52
WtooNwo
uyL
ND
300 061051130352
4lnyl oN.-Id.
uyL
ND
1.0 0610511303:52
%ylend ROulO
uyL
ND
5.0 OM511303:52
1,2-pdJvroatnan�d4(9)
TL
03
10-1T0 06A15h30152
1•&9m9IIwTopenxarla l9l
%
98
70',X 0"Sn300:52
Onremekueremaeu-IS)
%
105
7fr130 ON0711101.5"
TOWarN+16 (5)
%
10}
70-130 06MS11301:52
P... Aeatyu.rl6 M""re0.
pag0 K1=Ara. Gi 100
HimW.ra.. IIC 7e675
410435754M
LABORATORY CONTROL SAMPLE.
Pvemel4r
966366
urKn
Splk.
Cu.
LC6nt
Reaulf
LC.
%Rac
%Rat
unaI. Oudekele
1,1, 1,2-TatrbLWuto en end
uWL
50
46.4
91
70-110
1,1,1•Tnallor"twe
uyL
50
451
94
10.130
1,4,2,2•TagaoMwoeNene
110-
50
46
9fi
70-130
1,t,2-'rfl hl oerhane
uyL
50
50-9
102
70-I30
I,fi]kilkroemAne
vWL
50
476
95
To, so
},1•Dlddorvelhe ne
uplL
5o
40 0
60
70-112
I.2>Tdcmo,ogropene
uOfL
50
43.9
fib
70. 130
12.CWx m0-3•u,la 0pr0p.nv
uyL
60
466
97
70.130
1,2-DNmom-11h. a IEPB)
uyL
50
19.1
99
70.130
1�•Olddorob4nx.n.
uyL
60
40.4
99
70AU
1,2.9k5dprw9lanr
uyL
50
438
6e
70.170
1,2-Dkldnepropene
uyL
50
4411
9e
70.130
1,]-Dkillprppfapso.
uyL
so
46 3
93
70-170
T11NJnrvb.nxene
uyL
50
46.1
9i
7W 130
245uhnene [MEK)
uyL
100
104
104
70.145
2440a -,
uyL
!00
105
lod
M144
A-Methyl-29-tan0ne IMIBK)
uWL
Ip0
101
101
10,440
Acelwu
uyL
$00
102
102
50.175
Acrrlonitr0.
uWL
2w
2410
101
70-t43
B-Tope
uyL
0
41.5
99
70.130
El m chforameth n.
"A
50
521
104
70.130
9ramOdld,lplem.Nane
uyL
50
41.1
95
70.130
Bromoform
uWL
50
617
101
7d13U
8.0 ..we..
IWL
5o
541
106
54.130
Carom dieWide
Vi.
so
47.0J
94
10.131
Carbon l.ved,lwld.
uWL
50
43-6
ee
10-112
CMoroEanx4ne
-WL
50
46.2
95
70-110
CNW -lhene
uyL
50
50.0
100
54 134
Chlomp. m
uyL
50
47-6
96
70-130
CN.rr th. a
'WL
50
117
95
64 170
pa-I,Z-Olrnlueemene
uyL
50
$1.2
102
mi31
da•1,]-DIdlloropropene
uWL
50
47,6
66
70-130
REPORT OF LABORATORY ANALYSIS
T1Y. r.pprt N.1 not to [.gndunW, ..c.pl n Y
Pdq. 49 .171 Wla: 06126201a 10.40 AM w,rwn M e m.n [anuM el P- A-1,11 l 5.nra.. 1.
Pa00 50 eT 11

J P.-A-P,� laeyNaa, I- Pee. A n.lyaaal aanNea, M..
�,dl'L ical 205 F.W uesmw Rasa , A = R-w 0f
�^^""''JJ • EA- NC 2TAa AhaHN. NC 1950e
03MM 971 1620=4-7T 75
QUALITY CONTROL DATA
Propel Sulry Ck.ad•Mt My (u1C)
Pace Poo" No.. 921511953
P.G. Analrtleal 14M..e. Ine
P.-
A.My".1 aervrae., Me Paee AnslytlaY
a s, Me.
9600 MA.ery Iw. 6ulb}aa
ceArralyticala 7QS 1.e[MaWex Rene-S.xNA
T775 Aw. 01
Ikrrltran4.. Nc HoTe
_
Eden. NC 212a6
Aenmh. NC 7a6Da
M017541w
l]38P52 -8021
(6261254- /a
QUALITY CONTROL DATA
Pfoprc1: Swry Cka.d•MI A" (Ur-)
Pmcm Prppd Na.: 92159051
LABORATORY CONTROL 9MIPLE' MMIM
Splks
LCS
LCS
% Rat
Pvmmatrr
Unllm
Cana.
RemWl
% Rea
tlmlu
Oyal4an
dlbroMbgllara klw.
uyL
s9
49-1
91
70-130
OlbroMmolwa
uyL
5a
48-7
97
70.131
E91y1bsn:an.
uyL
50
4a.a
07
MIM
Iodpm.lA4n4
upR
I00
72.3
72
494110
M.alrlen. ClHMd.
uyL
50
52.4
105
63.130
Ste-
uyL
50
fax
010-110
T.b.armara.lhenm
uprL
So
11.6
95
70- 13a
,rw.. ne
yo&
50
486
96
M130
amnm•1,2 OIdJortrmMna
uyL
50
so
102
M SO
9an..1,3-pWnoprvp.ne
yyL
SO
47 3
95
70.13x
r.n.-1•e-deMora-2 bulane
t1wL
50
54 9]
lie
70-141
Trlrnlp.ova+sna
apt
50
f6 3
93
min
Tnch/pr.Auwom.dl.na
UOL
50
49.5
97
6,x.13]
VMyl.cet.le
vg&
100
lot
105
a6.1S7
Nrry1 chlond.
uyL
SO
662
112
a9.130
xyiene lr wl
not150
144
96
70-13d
1 2-picNvr uavran.-d4 (SI
%
99
ia179
4&rom.�nprObmnxmnm (S1
%
96
70.130
fibroma nuaroM49gIT4(5)
%
99
M130
TOP- a-aa (a)
%
100
10-120
MATRIX SPIKE 6 MATRIX 5PIKf OUPUCATE
96B349
$04390
MS
M30
IF2159 BUM
Splk.
soul.
MS
MSn
MS MSO
%Rae
0,14.
p..ammlar
Un"
Rawl
Cane.
COnc
Raawll
RaaWt
% R.v %Rac
Wrri4
RPO RP[) Owl
1,f-DlgJwv.6ren.
Nryl
2.6]
50
5o
50-6
36.3
96
66
7LL1a6
31 30 R!
9►neana
u9R.
3-8
SO
50
53.0
53.1
as
99
7o-tfa
0 30
Chkrobancane
upiL
M
50
5o
60a
59.9
97
97
70-141
0 30
Tahrana
uprL
No
60
50
49.a
492
100
96
7W 165
1 10
TMchlwnalhwe
uyL
3A
M
50
54 a
552
101
!04
so-n51
1 ]0
1,2•olulwroe9l.n.�4 (3)
%
95
94
70.130
i•Bromca-Feben.en.(S}
%
92
96
70-130
D13-11U.. elh-M)
%
104
97
10-130
Toluspe-aa Is
%
100
99
10-1]0
REPORT OF LABORATORY ANALYSIS
Tfw f.1- NW •.� du d .... rl
Do k- ON2ar2013 10:49 AM r,.wl1M. wlwe awe I or P.:. Ar. -,- S.mu. vr_
P496 51 W 77
OC Smith : MSVI21191 Anerpk M.1MudEPA 9294
OC Belch Maalad: EPA 6260 Au "ft oeett &M. 6290 MSV Low Lwml Landaa
ABoacisted Lob Sanplms: 92169663007, 92l59653006, 92159851009, 1r215053015
MCWD BLANK: 96a4TO
Mebt:: "let
AnodMad Lab Smmplea: 02159"5007, 9x! 59a53006, w159a53009, 92I59653015
slant
Rapwtk g
Parminsler
UMMa R-All
Wrrat AnWytad
2-T h.M.-M.-
u901,
NO
5.0 o"NIa 04 M
n,1,A•TAldu9rv. than{
u9R
NO
1.0 06m&1304.08
11 �.TabatNalOma+Ne
UVL
NO
1.0 O6A511304.0a
l,l,x•TrlWvr..9lane
uyL
NO
1.0 OW0511304.08
}.I�cNorwar.ne
u91L
N0
5,0 OWN 1304-08
1.1A1rh1awmrn.
VL
NO
11.0 O6l05l1304-0a
1�,}Tnd>torpprvp.ne
WYL
NO
1.0 O6r0204.06
1,2{llbrama-3•d4mopl uparl.
u9R
ND
13.0 06" 304.6a
1,2.04romaatlune(EOB)
u*L
NO
1.0 06m611304.Oa
12-MMvrvbennne
uWL
NO
5.0 06MV]304.00
1,x�IcNvrve9l.ne
uiJA
No
1.0 OWN 1304'.Pa
1A4�1,Mvrea-p.n.
uyL
NO
1 ❑ 0g 10: ] 04 Da
1,3-0Idgarapropmne
vWL
NO
!.0 06f0V 04-as
1,i-DlWupbanrana
VL
NO
1.0 O61OS11]04,08
&Bulanans (MEK)
uyL
No
100 O61p5111 04:01
24ivtt l
uWL
ND
50.0 o6f05f 1304:00
4-M.py4x�enl.nene IMIBKj
uA
No
100 OIIM505 w Oa
Acetun.
uyL
No
10O DOM503 b4 08
AerypmlerWo
uWL
NO
200 06N511] 0400
a-,.-
coil-
NO
1.0 OW5113 04:04
&vmvwwam.thena
uyL
NO
3.0 06Aa11304:0a
8r9madchloromeman.
uprL
NO
1.0 0MNI304.06
&vrnvform
upfL
No
3.0 0aA5113 04.01
ftramammmme
yyl
No
A0.0 00R1511] 01,06
Cuban dla�ilee
uyL
NO
$00 06R1511] W:06
Cuban 4"Mcl xlaa
6WL
NO
1.0 O WI304oa
Ghlvrvb.n4en.
uyL
No
3A OW5413 04:0a
Chl-Mlh n.
uyL
No
10-0 aamN1104:06
Chk,Mf&m
n a
No
5.0 66mw$304:Oil
Chlprvmadlme
uyL
No
1-0 96r0611364.06
or-1,2-iXdnarv.ar.ne
uyL
No
5-0 Od0511a 04.06
da• 1, 3.Omh1ofn propene
uyL
NO
lA 06f0311304.08
plhremodrWremeN.n.
uyL
No
3A 0a1 N 304'06
olbrmm�melhana
uyL
No
10-0 0116AW 304-06
Elhribm..nq
uyL
Na
10 061091304 oa
Iveome7r.ue
uyL
NO
10-0 OWN 130406
Mealyle.. CAlrrlde
vok
NO
lA 0WOU 1504'04
Sly-
uyL
NO
1,0 06 UNIT 046 0a
Teb..Mvrv.9r.ne
u911-
NO
1.0 OW913 04:00
Taluan.
uyL
NO
1.0 o"Vi104'0
bane-1,2-0 r.Mlwv m-
uyL
NO
5-0 05M W 1304:011
Dd,lW.prrrpene
uyL
NO
1.0 OWN 04:Oa
tr.rn-1,4-prhlorv-Z but-
uyL
NO
100 M1061n304:08
REPORT OF LABORATORY
ANALYSIS
Trw ,.pert ehw nel a i.vfeei<w, ...W. k*
Dale: 06 u2w 3 0'49 AM
Mltwi are •.Alen oa -t
el pear Arr.lyaeel S.mw.. K
OulAa.v
P.w M."car Mof ., Ina.
am Kk1ae1 Aes $ . sw
rk.wrw9., Na 2MIS
I7WJ67Sad0
P.9e 52 of 77

Peq AI1m yINm aenl.n, Im. P... AnYVOW a.nt[.e, In I.
■ a�eAnalytft al • ] a 7..t M .d.. Rew . 6,41. A 42 5 Rnn.d. m
tin. Pa.`a, mm Ed . NC 272M AN.W . HC 25ka4
t 3354n,lP71 1476I734.117a
QUALITY CONTROL DATA
prvJrr! S1111Y ClaredFM, MY (WCI
Pace Pre}eMx Nv. 02158053
METHOD BLANK 968410
Matrix: Ye.ter
AeePClel ed LOP Sr apes:
92150053007, 92151663006. 921596530D9, 97159153015
BIan4
Reponlnp
Pe1.Mne4w
I1n96
Revell
Lrrmt AImdo d Q1-4114r.
7rrrntRl.elh&,.
uyL
NO
1.0 o670511304:01
TrIchlwgflua Mm Ilene
uyL
NO
1.0 06rosm 3 04.04
VlnTt 1-1.1.
uyL
NO
50.0 06N013 w:01
VnA dmild.
uyL
NO
1.0 WOW 1304:05
Xyt.ne lsoleq
uyL
ND
5.0 06105y1304:01
1?Pic+m.roan.n.�a (8y
%
a1
70-130 D&Cjn 30401
4 arom ilimo6enul M
H
06
70-330 060051170404
DbfemRallllr4nlral.ne 15}
%
410
70-no 06r05113 04 01
T.k-.-A 181
%
1 DO
7D 130 OMW 13 04-01
eru An.rytlul Pa.e Anr Meal •.m.er, Inc. P.r. Anerypsy ae"Y s, In..
DeeaT 14nc.r A.. 6M4e. IM 205 E.N rJ..O Row &r "A 7225 ihvrele. 0M
lu.d.M. a NL 1607e / aceMaly[ical
i i;d.n, rrt 77]1E RweMr. N[ J4401
[7M111675,0w7 1 IMP1 -ml 429125471 Ia
QUALITY CONTROL DATA
Protrcl S,rrry pvE.tl-MI NrY �111CI
Pmce Proled No.: 02/59651
LABORATORY CONTROL SMIPLE.
Pmnmeael
916411
U."
Spite
Co..
LCS
R.mAt
LCS
%R6c
% Rec
LW*M O"ok"
Malradner9mlhmna
uyL
SD
44.3
69
70430
1,1,1-TrxJ,lmvethene
uyL
50
45.7
11
70-130
2,2• Ta0ochic a ..
uyL
%
46.0
92
10.130
e,1,2 Trkww--*wa
uyL
SO
41.2
61
70-130
IA-Vi emerwelen4
PyL
50
40.8
100
70.130
1.1.OIchlao4Prepa
uyL
50
4t-6
02
70-132
},2,Vr lWwom p.n.
uyL
50
41.1
Be
10-13u
1,2•Dlhf=3-I4wwoprvvw*
uyL
$0
40.2
1Do
70.130
t,2 Dlkr9mve0mna (EDO)
WL
Flo
46.0
97
70.130
1,2-DldAervhMrniene
uyL
5o
40.3
H
70-170
t,2.omomm0e01eop
uyL
30
42.0
84
70.130
1,2-DId"Opll7we
uyL
SO
470
94
70.130
1,3-DkN ropreWlle
vyL
50
40.0
90
70-130
1,4-0IdAwoh-ii
uyL
59
47.1
95
70-00
2-BWenw. IMEKI
uyL
100
101
101
70.145
2-Ha mwo
uyL
+00
101
103
70444
"-"-2-penlmw9 IMIMR
wWL
100
07.34
97
70.1 40
Acatwe
uyL
100
WAd
91
WITS
An Wina
uyL
:50
241
97
70.141
Bon4em
uyL
50
47.0
95
70.130
ervmorJooromewen.
uyL
50
49-4
99
7&130
BrwnodchWrememene
uyL
so
44.1
16
70.150
BremolPrm
uyL
50
61-6
103
T0.430
&vmon+eth.n.
UOIL
50
54.9
110
54-130
Cwtm4 rAelAlde
uwlL
50
45.71
61
70.131
Cwnvn IelnchkMNe
uwrt,
50
43.7
67
70.132
Cluoroheneene
uyL
50
46.6
94
70.130
CMwoemme
uyL
50
61-0
102
61.134
CMorolorm
uyL
50
46.0
02
7o•T30
CHM."mans
uyL
W
54-5
101
94.130
ma-+,7-0K4,l-kh.n.
p7'L
w
493
99
Y0.431
on•1,3. OILiIIPropl opene
uyL
5A
44.9
90
70-130
REPORT OF LABORATORY ANALYSIS
Ne. rep.n na rwla r.emdlKee. -Ft 4. hm.
Data 06f21R 0111 10 49 AM .m me rnuneen..m el Peu Arelrew 1.m . Inc
Pre. A.MyN.1 Mmeel, Ine.
mmov .r A.e SWe,DD
IM.NIIIN/.. NC 23070
rhfl,gM"2
IAROFATORY CONTROL SAMPLE- 961A1}
Spite
LCS
LCS
% Rac
pea4me4er
41ndm
Lane
Resale
% ROC
LIMP
Ckllllma
Onrvmvd,twvme6uuie
uwL
54
466
97
70-130
ptlomvn+elh.na
vyl
60
472
94
70.131
Elhy4h4n2ene
uyL
$0
45.5
93
70-130
laft"thons
Npri
log
as
13
411-110
Methylene Cwll6r
uw+L
5D
"A
101
63-130
Sly-
uyL
50
450
92
mom
Tek4thh19a9+an.
uWL
50
46.3
93
M130
Tmarne
I19JL
50
45.0
93
70.110
aln.-}3-Ltiwo ver ene
uyL
50
46.2
16
70.130
Vona. l,3.
IMyt
$0
44.2
11
M-132
Vane- 1,4.01CN"*-2.vutene
uWL
50
51.4J
103
70.141
TI1cn1ar6eW4na
uyL
50
41.9
11
M-130
TIk1,bl.kraomeulene
vWL
$0
427
15
82.03
lMyl aceule
uwL
108
M
103
66.161
vow ctllmlda
uyL
50
52.9
lug
64130
XYWA (Totm)
uyL
ISO
117
91
70.1M
1.2-Dkhlerwtmm�e-W �s}
%
61
70.130
4Br61rw6uaeben7enr(S)
%
07
70.130
Oib. a wwathwe(SI
►L
91
70-130
Tai.ene-d6 (S)
%
too
M130
MATRIX SPIKE 4 MATRIX SPIKE DUPLICATE
980412
961413
M9
WC
#7159153015
Spike
Spike
MS
MSD
MS MSO
% Rec
Mm
Pal am. 141
Oulu
Aluldt
Ceee.
Cvnc.
A.eldl
RewX
%Rec %Ree
LMs
RPO RPD Cum
1,1-pldmerve61ene
vyL
NO
5o
So
40.91
36.8
62
70
M.I"
3 10
Ben2ana
uyL
NO
50
5o
49.11
52.T
105
104
M 149
4 30
C,7ilp/ehenfalle
Yyi
NO
56
50
41.9
41 }
am
96
7✓1-145
1 36
T9lvrne
uyL
NO
50
50
i8.]
502
97
100
70-155
4 30
Trld,lvroelllene
uyL
0.851
50
SO
SO 6
5] 1
100
106
60-151
6 30
1.2.OIM:14m" Mone e4M
%
93
92
70430
4�rvlrw6uwaWn7en. IS)
%
96
94
10-13D
Od--lmlvromelh-.IS)
x
101
193
10.130
Toluene.ve ls}
%
07
100
10-110
REPORT OF LABORATORY ANALYSIS
TM repwt titr net b npmdkc" -pt In Its.
P.04 S3 of 77 Dole : 06+2&2011 e0.49 AM wo-I II. y.Aern Rs,wr I.f Fen A-i"" 6nmee. ft.
P4pm SA W 7I

P... A nr 1Ue6I Mr.lc... l,... F... An.lyticel.w4e... 4.. pelt A.WV9Eal lrrrlrr.. ln..
F..., M..ae. A- . u�i . im Fr.r - 0. 66017111.ngM 6�1. 1[O
Ed- NE 27Me r.r-m. "2� r1C 211b78
rj3mJ5238971 8MlM. 71M j7W)ere-m
QUALITY CONTROL DATA
P,.J6 : 3yrry Clear}MeNry (urM
Paca Pr.*d Ra.; 92t59653
AC Batcfi. MBV123261 An.lyzi. Melhod EPA 1260
OC 9.kh M.ewd: EPA 1260 Anely6le Demo 1pow 460 MW 1.- Lewl Lan d64
AWecimed Lap 34"s 9215053031, 92152653012.92159661O13. 92159853014,921 S9653015.92156853017. 92159663018.
92159e530 1.
METHOD BLANK. 990166
Meek. VVil4r
+Wvgeled Lab Sample.: 9215B653011, 92159633012,
92169663013, P2159a6101{, 9213P657g 16, 9�21596S141 T, 92159657af e,
92T59653019
Blank
Reporting
Paramotan
LM44
Reeull
Lima A~ Ow66ere
l,l,t,i-T�trelNWeari4M
uyL
HD
6.0 061fi1131&5I
I,f.1•Tdddomsllmo
uyL
HD
1-0 0611111314:51
1,1,2,2-Tetravllorveel.r,e
uyL
MD
34 owl,
6r1 A314,61
4,1,2-Td�lvrer6,anr
uyL
NO
to Will" 14:61
i,1-DndAarve6,anr
LprL
ND
1.0 9u117i3 f4:51
f,1471cr11vrv6 rime
uyL
HD
5.6 08111r1314:51
1,1•GWa+grpp6ne
uyL
NO
5.0 Ml I r1514:61
5 R.3-Trrwvnprap.r,e
UyL
NO
1.a 05)111111411
5,2.4•Tdchwrvbrnr.ne
uyL
RD
$0.1 0611i1131431
1,2-0Ihrvmv-7-d+lwvprvp.nr
uyL
NO
$a. 0611111314os1
1,2-OlbrvmvaO,ene IEDEI}
'A
No
1.0 0971111314;61
1,2-0IdaOrvbmlxena
uyL
ND
5.0 061101314, 5,
1,;-pworveVaene
uyL
ND
1.0 owl V131461
1,2-Dcwwopropene
uyL
ND
1.0 Owl In 14:51
13-0kglm0hen2en.
uyL
NO
14-0 06r1111314:61
I, I4Nd%loroprvpane
uyL
ND
1.0 W110314:51
1,4dchhrohen2ene
uyL
NO
1.0 06/11113 f1;51
2,2.Okhiafuprvp6nr
uyL
NO
16.0 O611 I fi311'51
I-Butanvn. {MEN}
uyL
No
100 au1111314:51
2-Hrxanvne
uyL
NO
50.0 9O11$113141$
4-Methyl-2-pa'.... (MIBK)
1vt
ND
10 gN I'll 314:61
AveWe
uyL
ND
toil 0&1111114-51
AcHvnrrsr
ug&
NO
55.0 9u1N1314:01
Auolrly
uyL
NO
$3.0 04111AI14AI
M mIt'ee
uyL
NO
200 06111/15 Will
ADA dlkHld4
.OrL
NO
100 Owl R314AJ
Bmrrne
uyL
ND
f A 06,11113 "I'll,&omeWwvmelhene
uyL
No
1.0 OG1111314:Si
&omodmPvme6enr
uprL
NO
1.0 mull 14;s1
Bry 01-
OWL
NO
].0 W1111514�51
&0me74100ne
uyL
RE)10.0
011AIII314:51
Cerbm---I a
uyL
ND
ISO gut N1314-61
C.rbm IeprMlvrlde
uyL
ME)
1.0 0311111314:51
Cravr96.ne6nr
uyL
0 291
3.0 Out V13 44:51
Crd9fer616ne
uyL
NO
10 0 06r1131314:51
CMwoklm
uprL
NO
50 OMI'll 1c51
C.Muvmelh.ne
uyL
NO
1.0 4wr11113 KAI
CMvrvprvn.
uyL
NO
2a,g gw11111114:51
cY-1,2-DlchlavaNme
uyL
ND
5.0 06111N711:61
do 1, 3.Okhl.raprepen.
uyL
ND
1.0 06.,31.111
Dpremvd,l.rumelh.ne
uyL
NO
30 0011711314:61
',a P.r6 ANNrtkal n.rvlee e, lnc. v.... an6lrll eat e.rric.f, l7'
a C'e1rMl?�y[ICd� - E..L...- R •Samna IBMr.w [>.
ew r<�am. Ed.n. NC 3riB8 •W..h rrC 79N)t
l3%•i• n am [ raze I2�+.1 i re
QUALITY CONTROL DATA
PF*gt: 3ulry Cb"ed-Mt A";Ulr)
Pece Pr.1ad NO.: 02169653
11xp vrc.r I... SuN �o]
Hw+Ywe. Nc 2eare
ITti+ 117S 90P7
METHOD BLANK' WMI19 M.bd: VYklcr
Aeevtlel.d Lb Sknoo: 92159653011, 42f596330 n2. 42159673013.921 S4e53014. 92159653016, 921S9e53017. SP2159653016.
92159653019
Blink
Reporrjn
Peremele,
UMN
R-Al
IJmN Arr47sed QUARA.nr
OAromomeUr4nr
UyL
ND
10.0 Ou1111314:61,
04chlorodl6uwnmed+one
-A
ND
6.0 0611111314:51
E00 mrri.veyl.lr
"OIL
ND
16,0 Owl. 14;e1
EOtylbanAanr
uWL
NO
1.0 06111R314:51
Hal eohlwu-T-3•tmade"
uyL
NO
10.0 mlIn314:61
Iodorrlalh-
uyL
NO
100 Ou1111s 14AI
na061R.r,o+
u91L
ND
f00 owl II:114-61
met.-M.
uyL
NO
foil au11N3f4:61
Me8,y1 meth.crylm.
uyL
ND
no M111S 14:61
M.9rylmr CMnda6
UyL
NO
1 A Willi
N6phQ,dme
uyL
NO
10-0 Don V131415,
PrppwNMa
uyL
00
$50 WIIA314:51
6trr4ne
uyL
ND
1,0 067111:114:s1
TetraWoroeln.n4
uyL
ND
IA 067111] f431
T.W.-.
uyL
ND
1 O 06111l's 14.61
tr.n.-1,2-p Wwvelheru
uyL
NO
SO owl I1214;51
trans-1,3-plcMwvprupena
uyL
NO
14 0611111I f4:51
tr.n.-1,4-prhlvrv-2-butane
uyL
ND
100 09111h314:61
Trld+tkro6elene
%VL
NO
1.0 OWII1131611
Tricnwn06uorometl,en4
OWL
NO
1,0 0 IWI314:51
VPO aulale
uyL
NO
50,0 Out In314:J1
1An0 chioldd
uyL
NO
1.g 9er1H1314",
Arlene (rvl.0
uyL
NO
6A Will ] 14:61
!,2•D:U+Iwoe4lan..d4 I%
%
96
70.130 MIIM 314151
4•Broma 6uvroben2en61S)
%
t0O
79-130 WIV1314:5f
D1-11-emed,.ne 115)
%
99
70.130 Wrl1"1 4i4
Tclurr,a-dd(3)
%
97
n-130 =I H1314:51
LABORATORY CONTROL SAMPLE:
Paramour
SM31M
Ltea.
6411ke
Carrc.
LC6
Result
LC3
%Roc
%Mv
LWAS Olra46m
2•Texedrl0reer,ene
uyL
50
45-4
91
70.130
1,t,1•increarpalMnr
uyL
e0
4]-7
e7
70.136
1,1�,2•Te9acngrve4iane
uyL
50
46.6
94
70.130
1,1,2-Trkhlnrdnhune
uyL
50
46.6
44
70.130
11,,11-0lvhhtN
pl
SO
47A
9S
1-0cMau9unn
70.130
ve
uyL
91
70.52
1,l.dchluvp,vpene
uyL
50
M-7
91
704m
1,2,3-TrkAwreprvpane
UyL
50
44.0
8a
70.11S
I.2,4•TdWprpbeneene
uyL
50
47-7
95
70.114
1,2-Dlbrvmo-3 d11v,vprvp.n.
uyL
5o
46.6
91
70.110
1 ,24A Dino a6lana JEOB)
uyL
50
46.9
94
70.130
1,2.O:Wor o+oen2ene
uyL
SO
47.6
95
70.1 sO
},2-pchlervrol we
uyL
50
41.4
e4
70-130
REPORT OF LABORATORY ANALYSIS REPORT OF LABORATORY ANALYSIS
TNr M6"net er ner�..-P. n Ka. TNa-W en.a ml br mpmduoed. reupr m M.
0.1a: ower201110 49 AM �r "oe .-.eol.4 P.c..e.tre g �.. Inc. Pop 55 vT 77 Dale: W29a 013 10:49 AM -01a A"wHern ay M or Phu An."Se-.. I- Pipe 56 or 17

r 2aceAna)ytical'
MS EaM A4e+row Nwd � SwEr A mn Ilr4rekla a
. wrA.xlfm me Syr.. NC 272aa Aahr+N NG 74ew
p]nh:3aY2+ (r]ajYh711a
QUALITY CONTROL DATA
PrapcP 8ulry Closed-11MA" IUIC)
Poco Propd No.- 42ti96S]
P... A.Myce aervluf-Vn[.
Belot Kirrex Arr Suh V00
+lu.rrfrr.. NC 2007e
LABORATORY CONTROL SAMPLE:
Puom4ler
990310
V1114
$plie
C.-.
LG5
Ream
LCS
%Roc
%Wc
Urnile 011alRom
I2-UWpropl*Pnne
uyL
50
45-7
9L
70.130
1.1 QomwebaN.ne
"W1-
so
47,0
96
70.130
I.3.11lcmm9pl peno
U90L
50
"A
69
70-130
1,44Sdea.b. .n4
U94-
Sd
47-1
25
70-130
?-2-0IbNoroprop.ne
upl
50
44.2
92
36.145
I-bwwcoo (MEK)
UA
100
lie
1la
10-145
2-R.xanme
OWL
100
91.6
14
70-144
4 main Z-pbmw ne(MIBK)
UVL
ltl0
94.71
65
10•e40
AOoz.
uyL
100
167
107
54l75
ACal9nIY4a
UyL
500
6w
112
70-130
Aawom
NWL
250
209
64
70-139
AaN.t*m
uVL
750
251
100
M143
/WI d4w Ida
uyL
50
44-3
19
70.130
Baruenr
ilyL
50
47.0
94
10.130
Srpmachlawmrlhule
uyL
50
39.9
a0
70•I30
&om.dchlpr9m.lhane
UyL
50
42.5
15
M130
Blwn.bum
ug7L
50
40.1
52
70.130
N mome9lan.
4p+L
50
61.4
123
54.130 F3
cut)p 4xlut4da
u0L
50
49.21
H
IO•I31
Croon lea.chlrlde
u01L
5o
44-$
59
10•I32
cNa benceno
uyL
50
46-15
94
70-130
CIA -thon4
uWL
56
45.4
91
64.IN
CI+Ial.?wm
uyL
w
44.1
all
70.130
C4,M-olu..
OL
is
36A
73
64-130
Cli,olepr.0.
uyL
50
45.9
92
70.136
c14-1,2-DIdU9t.alhom
uyL
SO
45.4
92
70-I3I
da- 1.YL11dUIXOplopr n4
uyL
w
43.4
a7
70-Im
DErpnn-fni methane
uyL
SO
44.0
ae
70-130
061emoma0tu+e
ilplL
50
47.0
94
M131
bkhlwodlAuxApmr lh.n.
u%fL
w
39,0
74
66-136
fipnyp M.M."O.J.
uOtL
50
49.6
96
70.130
Erhylh.nr.ne
,WL
w
47.7
94
70-130
ke><4cNup-t.3 Wodlen.
ugtL
50
49.4
100
70.110
Iodnrhelh."
uyL
100
e6.1
66
49-166
I.ow"ll,
JWL
low
1130
113
70110
Malnauy w*rIte
uyL
500
504
101
70.110
Me9ryt melhocrYlere
u11L
50
45 2
96
70.130
M.9,0_4 CNOrlde
uyL
5o
410
82
63-130
Nep1t91e1.n0
uyL
50
47 5
95
70.123
Pt9Plonlbee
uyL
500
501
100
M130
SMru+e
uWL
50
46 4
93
10-130
T.1rlluhl.... dn.
uyL
50
41.6
95
70-130
Toluene
uyL
50
46.2
92
70• 130
1r4na-1,7-LNd4xr.. ih.ne
uyL
%
46.7
93
7OL130
it v..]•i7ldXoroprrytena
uyL
50
43.6
57
70-132
9arrc 1 4pchlarR-2-bUlena
U91L
50
42-41
at
70-141
irld,prae9l ane
+111L
50
11-P
66
10-130
Tri hWro Suoromelhane
uytL
50
44.7
69
er-137
/917
•
Pen AnNy9e.lMrvWff, In[.
Pan Analyllcal 1-1... , Ine.
Pew Anlylle.l6ervlew,ane.
.PaceAi i
N6E.W M..Mw Rpla-SWrA
222%A..r Or
9lAw 91IYiql
WrMwr
� ,+
Lbn, NL 7726a
AY.rree, w xew
#k-" wAr.. NC 10070
I3m,mm4911
1e 261754 1,re
1701I6759062
QUALITY CONTROL DATA
PraNct: 41rry C9ne6Ml "y (UIC)
peen PtraJan4 Np,: 97159653
LABORATORY COWROL SAMPLE:
990390
Sphe
LCS Lcs
% Rec
Paramemo
Lk"
Colic.
Revel %Rec
Llmld 00410...
14ny1 ackwo
LWL
100
102 I N
66-157
WO chlxlda
4L
50
49.6 99
69.130
%y1en4 (Tout]
41.1
I SO
139 91
70.110
1,2-GGdoraalRone•da IS)
%
100
70-114
4•&om9 M1uwnb.nrem (S)
%
on
70.130
VivomnlluuM"lh" VS)
%
93
70-130
Teklane•de (5)
%
99
7OL130
MATRIX SPIKE & MATRi%SPIKE OUPLICAT E: 996391
990392
Ms
hiso
92160307012
Spike
spike
MS
MSO
MS
MSD
%Rac
Max
Pararr+rar
LMW
Rnwl
Cana.
Cwc
RmAl
Result
% Roo
% Rw
UmIN
RP0
Rot, Dual
1,1-Ndkiro.I11ene
uglL
NO
50
54
441
50.6
66
102
78(66
14
30
Benzene
ugtL
RD
50
S0
54A
55.0
109
110
70-141
1
30
Chlwpbenrene
uWL
NO
60
a0
51.1
572
162
106
70-144
4
30
Touene
UpA,
RA
50
50
61-6
52.5
103
1(15
1SS
MI
2
36
irlphlpwetl+ene
uGA-
NO
50
50
54A
57.0
112
114
a9-I51
2
9a
1.2-Olch1a aelhane-d4(8}
%
93
95
70-130
4-gramaluolahenxene(3)
%
0
102
70-130
g4rrpinp Punpma9lanr [5)
'A
97
99
70.130
T.luene-da IS)
%
95
99
70-130
REPORT OF LABORATORY ANALYSIS RE PORT OF LABORATORY ANALYSIS
Tar. ulrarl xhM ae+a r4Pma,ced exrael n.I, f iex npoh Max rqt W npeisuPW axuM n M
EMI.: 06725f7613 10.49 AM ,w.wn n. wnn.n u.n..m of Pw AruiTeai F.r.Ao.[ x.e page 51.177 3.Ie. W.W2013 10:49 AM +r fijya w heNt.e, he Page 51,0 77

Paen ABM ye.N b.n1..., Im. Pee. AMeyecN 1NTvk.f, 1, P P... A.W
d:.l a.rrl..., mk.
.� y,y
Ayl+ca,•
7os E.0 M...aw R..d - Suy A 2225 R","Jo R o600
If.K.y An Sul. IM
Jl f•
EMn. RG a1 ]Ee AY "., Rc ?m l4nrr.n-..
Nc 2W la
[lJapZJd971 I6xi125e-7e76
I7Oe 075- W7
QUALITY CONTROL DATA
WoJacL 91ttry CwsadMl say lulCy
Pen PIN"I No.; 92159653
OC Batch: VWTY25626 An.ryals Method SM 2320B
OC Batch Memo : SM 23208 Ana"ki Oaea4p9oo: 2320BNkµNry
Assataled Lab Samplao.
a2159153001, 9215965]002. 9I150651003, 92159653005, 92159653W6,92158653007,P215965700E-
92159113009, 9215"53010, 92159653012
Mf�THOD%ANK: 96595S
Mekk- 9LYMr
Aaaodaltd Lek Samples
92159653001. 9215"53002, 92159653003, w159153005, 92159653006. 921 we 53007, 92159e53006,
92159653001, 92159153Of O, 9215053012
Blank RegMlnp
P00.01W
12nh Revell Umlt AnoWad Oua66us
Attorm, Told a C1003
uprL TIP • 00 OEMA113 1050
LABORATORY CONTROL SAMPLEr 955VA
Spin. LCS LCS %Roc
Paa"&w
LIAM C-0 c Revell %Rem LINAt. au.@aars
AA.1N1y, Tu1al M CoCa3
UWL 60000 49700 99 00.110
MATRIX SPIKE A. MATRIX SP1Kp dyPLKATF_ 165Y57 965166
MS MSO
22159853001 Spike SPW MS MSC MS MSO %R.c
Max
Pu mal.r
LA%M Re A C.M. Caine- RaaMl Result %Roc %R.c Llmlls
RPD RPO Clue,
AkokAy. Tar el CaCO3
UA M119 WOW 50000 120DOO 120D00 95 95 M 125
0 20
MATRIX SPIKE A MATRIX SPIKE DUPLIGLTE= 115959 DOW
MS M5D
92159929M 7plke SpkA MS MSO Ma MSD %Rac
Mak
Psnmot"
Urdh Revell Cone. Co". Resell Raoult % Rec % Rac UmIM
RPD RPO Ouol
Alkali", Tate) as CoCO3
U9IL 29.1 60600 SM00 79000 78700 96 9a 75.125
0 20
ih,#L
REPORT OF LA90RATORY ANALYSIS
TNf r.pprt .h.e not he r.proMa.d, except h AM,
D•ieDy26f2013 10 49 AM .rvw i".ml.e epnfae1.4 Paa K-h*Y 3wv"k Pape 59 .171
• pp" A—Iyry..l
6""., rn.. P.- 4-ty0w 6w.lf.f, Ise.
Pa.. A.Wytle.i a.Ma.., Inc.
a�eAr�aiytical W$ E..e le..,,
Real • yp.A 7=21 Rw.rrh Or
9e00
K ­ ,Ah 5W 100
Eden. NC 27Ma Asi. 40o, NC 2004
I wr a.. W 260701
[�Oap2:1-ae21 feMJ25.-717a
17Oelm r5i137
QUALITY CONTROL DATA
PF*Cl: Sur y CWeedaAtA" iUMl
P1ee PF*CI No.; 9215S153
OC Balch WETt25736
ArMlyek Method- SM 23206
OC Batch Method; SM 23206
Am"Is Ooealplm: 21290 Akx"
Aeaodated La43ampMe- 121S96S3013, p2sS11S3014, 9215PoS30I5, 92159653059, 92159153017, 92151653656, 92t59653019
METH005LANK: 990141
Matti: ftw
Aisodeted Loh Samples- 92159653013, 12159153014, p25S1153015, 92159653016, 92159657017, 921591.730i1, 92159as3619
Blank R.poMq
Paramelar Units
Raaull ufm An*nd 13w16en
Alka6nlly. Tolol as CaCC3 upR
NO 5000 O6f11713 f 0' IA
LABORATORY CONTROL SAMPLE: 990142
seek@ LCS LIDS % Rae
Pvw&mr 1lnsa
Cone- ROVA %Rao LI-ft 0-s6en
AlkaWAV, TOW a@ CACO3 UWL
50000 45400 91 00.110
MATRIX $P" 6 MATRIX SPIKE. OLWLICATE: 220,13
990144
MS MSO
92160591003
Spike $pik. MS MSO M$ M5❑
%Rec
Max
Parameter VnIM AowM
Coec. Lau. Revell ReauLt %Rec %Rec
LI-4
RPD RPD Qum,
AlkokJly, TwW as CaCO3 uplL 22.9
50000 Small 73200 72M 101 99
75-125
1 20�
mprL
MATRIX SPICE S MATRIX SPIKE DUPLICATE' 990145
99010
MS NASD
921596936i6
Spike Spike us MSD MS MS0
%Rec
Mar
Pvommler LAd4 Revell.
Cw Cvnc. IT"Ot Ream % Rec % Rao
Limit
RPD RPO Opal
ANaw ty, Tolal n CaCO3 halt 42100
50M 50000 WOO 91300 99 96
75.125
0 20
REPORT OF LABORATORY ANALYSIS
TN. mW NY n.l he mplvdhe.d. wwo At k#..
Vol.: 06f26✓2013 10: A9 AM .*-Ad* —ft. pev..n10 P.c. stashed 1.ni Mc Pea. t10 v1 77

Pace Anal yas.l d.rrkee. M.. rase Anaytlwe d.rvleee, Inv. P... An.erewl
- ace 4rra�yti�a�• ?ar F..r M.wow Row wie. A '2l Rn.,.ee p, smn erc.r Ar. Su . Im
xr. w.ree o.. Ewn. B Il266 loners. rk 78e0A HwY1w+e
I [336�Bi341971 feealzl4-i17a [791�67S9D92
QUA LITY CONTROL DATA
P10Mcl- Sorry Closed Aft A" IVIC}
Pace P,.J.n N. 92 i 59153
OC Belch1NETr25561 An.4.1. M.14-1 SM 521 DB
OC Belch Melhsd SM 52108 AnFFO. Pnalpllm. 52108 HOD, 5 day
Aasodeled Led So rrpidd. 92SS963]001, 92169653002, 92159653003, 9215053005. 92159853000, 9215985D007. 9215053000,
97159653009, 92159653010
METHOD BLANK: 914276 Mali. ySYta!
Aeeodeled Lob Sampled. 921596$1001. 92159851002, 6115965'1003, 9215946U*5, 92159853006, 02159853D07, 92 I59013006,
92159663D09, 921 S965313 10
Bonk Repww'a
Par.m.l.r U.N. Redo! Lkrl! Anelyz.d Ou.a9er.
BOO,5 day uyL NO 20DD DUW131140
LABORA70MY CON i ROL SAMPLE. 964219
Spke LCS LCS % Roc
PAramalrr unaa Cone RnuR %Raa Linsta W619.m
am, 5 day LVL 195DDO 202000 109 84.5-115,4
SAMPLE DUPLICATE: 914210
92159703001 DVp malt
P.,.m.Iw Lln]ts R.wl R—M RPD RPD Ouaa
BOP, 5 'ley ug1L NO NO 20
P.ee
Any ye.N +.m.n, lnd- .... An.i
yee.i e.rvl.. r, lnv-
A... A—IlA..1 e...1..., k.e.
L`e �"dr• 206 En!
Mood— RPM -5W.A
2M RvereNaM
aedu— VA.: Sw.1W
Ed .HL VW
..We- NC Za6Ol
11yr�r..er.e-RC MOM
13"012}i071
IM)254.7170
17a la7s9D92
1
OLIALITY CONTROL DATA
Pr9{ecL Sorry Clcaeo-MIAky IVIC1
Pace ProNc! No.' 12i 59853
OC B.leh: NVET1256131 me"[e. Method' SM 52106
OC Bakh M-Owd: SM 3Z108 Ana"s Dedalpson. 52108 BOO, 5 day
Ad odwed Lad Sampled 02159851012, 92159855013. 92159853014, 9Zf59653015, 92t 59853010, 92159653017, 9215965301e,
92159851011
METHOD BLANK: UUNW M t i.: ~.r
Aadadated Lab Sampled. 12159853012. 92159653013, 92159853014, 02159053015, 92119853D 15, 92152883D 17. 971 S2653016,
IV s1653a 19
Blank Reperllnp
Pvamel., 4Jnk. Re.1yq UAW Analyzed OVda6er4
BOR, 5 d.y PprL NO ZOOS 08108f13 10: 15
LABORATORY CONTROL SAMPLE: 98%91
"0 LCS LCS % Rat:
Par.m.ln Vne. Cone. R..tm %Red tbAIA Q-55er.
ROD, 5 day uP'L 19N000 I ND" 99 6d 5.115 4
SAMPLE DUPLICATE. 98506Z
92150853014 Oup ley.
Parameter UN1. RaM1 R.aW1 RPD RPD 0u6e6ar.
800, $ day NO NO 20 62
REPORT OF LABORATORY ANALYSIS REPORT OF LABORATORY ANALYSIS
1 N.1.een NY net ee 1em.d.e+d. ..up1 n Iw, Tyre.14n w1 wl W rapvarad. e..ep! Y nA.
D.le:6r2 06f1013 10'49 PJ,f yr.wW ar r,ne.n mnynl .t P.c. Anrlrec4 5. . Irc Pala 81 of 77 DoW OWW2015 1049 AM .. l—H!,., ntka,. C n — el Pere Anairycei 154—%. ine P.1. 62 .177

Pee. Anelya.ol i.M.e., I—P.- A-1yol-I 6crvk 1, Inc.
Poet, .rcl AeAywol aeee, Inc,
. aceAnaai 2P6 E.v Wed— Reed - 8u222 1. A 5 R-vd. P
MOD" —VA.. SM tp0
Cdn- NC 279ee A.IyA.. t4C 7vea
Ih.r`rma.. HE MN
r
ii67623d92, t620454-7tle
M41675-9002
QUALITY CONTROL DATA
P,pj.ec SwreChu.d-MtAkyluIC)
Pace Nopcl No.: 122159953
OC SNICN: WET+41548]
Ana1yW Mdhud: EPA]D0.0
OC Belch Mo0wel EPA SOO 0
Anofysls OncrpOon; 300 0 1C ANono
Aaaodcled Lab Senipka: 921598530DI
METHOD SUNK: M5724
M.kh: Wehr
A. -.pal NO LW 5amplea 92159653D01
elrnk Repwlklp
Par.m.l.r U.N.
Revel I-Inve Aeraly9ad Ouaalsfs
WOO- uplL
ND 2609% 06f01r13 14:55
LABORATORY CONTROL SMPLE 015725
Splks LCS LCS %Ree
Poramolor I1nMa
Can@. RonAl %Rec Llm9a
Ou41114.
Sulhl. uWL
20NO ISOM 95 90•TSO
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 916126
965727
MS MSO
9Y t600010,7S
BPI%. Splk. MS MSD MS
M6D
%Rse
Mao
Par.melef c7n1d Rvnil
Conc. Cane. R..WI Recall To It*.
%Roe
LM.Ro
RPp APO Dual
Sullala NAIL so
20000 20000 29606J 29500.1 1D0
all
90.110
1 20
ffplL
MATRIX SPIKE L MATRIX SPIKE DUPLICATE 965729
9e5729
MS MSD
921597000001
Spike Spike MS MSD MS
MSD
%Rec
Mao
Pwomalsf Lk4L RuWt
C.— Conc. R4.WI Rosati %Roc
%Roc
Li-ty
RPD RPD Qyel
SWlala UWL 7-6
20000 20000 219014 26611W 1OS
Ica
90-110
1 20
mot
REPORT OF LABORATORY ANALYSIS
iN. n�rl i1M ror W nprrrdlcM-..c.p[ n aN,
Dale: 0WWO13 TO'49 AM w►rad w. .mlt.n --I W Poe. An.1,1eM 5.nwa. me Pep. 63 0177
Paw AnWyp..i a.rMen, Inc. Pee. AnNyScal tleMsea, lne- Pew A.M)M" 6.Meae. ax-
Ia�eAr�aJytical a 705 f.N Me rtivw Re - $wH A x2x6 Rn. ee. d 6eo01an A.. stM. lau
1 ...r•ya. wa E W . NL 27296 A.h.yN., fK 26004 144ra.r.M.. NC 2.62e
1334nx]-097i 16201x54 7176 t7941a7s-aOn
QUA LITT CONTROL DATA
Prrrl.cl Scary ClpaeJI-MI Airy JUIC)
Pace Project No.: 92159951
OC S.T01 k9ETAf15469 Aa.lyal. M.IMd EPA 3000
OC Vmh moth all EPA 3000 Anetyala Dasv4p0en! SOO.OICASkms
A. ... Wed Leh Sempl— 92159653002, 92159653D03. 92159657003. 92t5%53006, 92f59653007, 9215963]006, 92t 59853009,
92159853010, 92159857012,92159657917, 9Y15965701i, 92f 5965]Ol S, 9Y159651016, 921596Sj017,
92159A330f e, WI5965SO19
METHOD BLANK: 966112 Meal.. ktkter
49060led Leh SampLes 921596530a2, 921i965300], 97159653005, 9215965]DOB, 92159e57007, 92159973906, 92159951m9,
B2159kSOptp, g2159657012. 92559653013,92159657Dt+, 92159657015, 92159653016, 92t5963]017,
92159653016, 9215965301a
Blank R.pwMg
Panmder UI K. Recall LJ 1 MsNoed 0ad6er9
5Wlele up1L ND 250000 DVON1317:01
LABORATORY CONTROL SAMPLE: 9e6tt3
Spike LCS LCS % Rea
Par".l6f Line. Conc. R.a» It %Rec Limp. Oualraerc
SWI.t. upn, 26000 190mi 95 90-110
MATRIX SPOKE d MATRIX SPIKE DUPLICATE 986114 IBOI15
MS MSD
92151IWO 2 Spike Spike MS MSD MS MSo %Rae Mar
Peram.ler lMuh Reau11 Cone. Co". RnWI Raeuk %R.e -A Rea Unoft RPp RPp Oa.l
Swlale OWL 371W 200W 20006 226wi 225OW 94 W p0.1f0 0 n
MATRIX SPIKE $ MATRIX SPIKE DUPLICATE 966t16 966117
M6 MSD
92159653012 Spike Splk. MS MSD MS MSD % Ree Moo
Poramelar units Ruuft Conc. Conc. R&WAI Ronal % Rae % Rea LiPIM RPD APO QUal
sdwa uWL 799W 20000 20000 30M NOSOOJ 114 113 9KF110 1 20 M1
REPORT OF LABORATORY ANALYSIS
TN. repan eW ml tr. r.prakad-..ape In kA.
Del. 06+26RO13 10:49 AM P004 64 al 77

V... FrYyllu,l a.rWeu, IM. P... A.WY11 y1 aarvle.., M.'. FAr. AnW,0::i S.Mca., I"
aCBAnalyfcal' PSF..1u..rwRP.tl-9..A 2275R W. 9WOK.r.7A,. 9r.1.,00
r„ar,y nlr. EGn RC 277e8 .i1A6.116. NC ]8004 Nunwr.re.- NC 7e076
f3]679 -m-0 482e l254-717e R01075IKW
QUALITY CONTROL DATA
prowl $wry Closed. MI AD y(LHCI
PA" Pr9pd No 92159651
QC Balch: YYEYAl155% AM1ayan Method' SM 4500-CI E
OC Balch Md%.d SM 46MC1-E Anayah O.Wipaon. 4500 Cmeirt"
Aaaocialed Lab Samplaa 9215995,3WI,92159953002,992159S0
9I S995109, 021596S7B10,a2t59651012,91013,91596yy01 a, 9215965]007, 92139657006,
92 t 50653PIO
METHOOSLANK: 990661 Ma M. YAler
Aaaockrl6d le6 $arryNe. 92559651001.92179853002,97159651001, 92159L5]005, 9215965]008, 9215965300T, 92159e5]OOa.
9}159653009, 92t59a53010.2215 953012,921 S9a53017.92159653014,9216965301S
B16Rk R.Pofma
Patemelor Lk,as Result umil Analyzed orla6Am
CAlondo 14L NO IBM 06A7l1320-22
I AWOATORY CONTROL aAMPLE: 990562
Spike LCS LCS % R6c
an Paramafu L4*5 Ct- Rewll %Roe LNnll6 G..kh6n
Chlarde UWL 20000 20400 t02 90-110
MATRIK SPACE 6 MATFtLK SPIKE DUPLICA]E: 990661
9906641
MS
MSc
92150S3001
Spike
Spike
MS
USO
MS
MSO
%Rec
USA
parameter chats Raault
Cenc.
Cone.
R6wllt
Reauk
%Rec
%Rat
LNIad
RP0 RPO Qual
Chlollde uyL 070
20M
20M
23300
21300
96
96
75 175
0 20 T
MATRIX SPIKE 6 MATRIX SPIKE CUPLICATE: 990965
390e88
MS
MSQ
IP2150853002
Spike
Spike
MS
m5b
MS
MBO
%Rec
U"
Paramator Lunn R410
Coec.
Corte.
Reoult
Reaull
%Rec
%Rep
Unvoa
RP0 RPO Ouai
ChielldE r.glL ]460
20000
20000
VOW
22M
96
97
75-125
0 20
REPORT OF LABORATORY ANALYSIS
1N. r.pwt a "-4 E6 r.proGewe-.alai n hN.
13m: 06f1Bl2013 10 49 AM +nn�0 M wr61.n —..r1 or P.c. A,ylAcy Suv.ral rrc
Page 55 0f 77
p... An""A"' Inez r.[. An61.Us61 IwP.., I'
P... A.Wyaal I-vL-., In..
aCEiVMlyf�LLl1' ]mEa.IY..CewRCW-A 2mA�w.trd.d,
YIOOMwarAin &. rm
J,
1 ,�yyypr Ee.n NC 77M A.h.�wr NC 7Mo1
1*~.M, NC 2m70
�f 0361673Ao:1 ra2ao?176
m4lalfiam
QUALITY CONTROL DATA
Pt*CL Swri 01w.d-MI Airy ILIICI
Para "es No.: 92159651
Of Batoh; V&TNI5576 Anayua Method. 61h aSaa CI-E
CC Be" Maa,od: SM 4500•[ -F Anry.l6 Do.cr"-: 4500 CMorldo
Aauciated Lab Sampla%: 92IS965WIS. 92169653017, 02150951011, 9215915]010
METHOO BLANK- 902127 Motrd. Water
A,evparad L.b SarRplaa; 92159e53618, 92159653017, 9215965]Ot6, 92159a53019
elanx Papering
Palalnelet Un6a RIVA LI M Am"d Oula6an
CIIICFKSa uyL No low 06711r1122:27
LABORATORY CONTROL SAMPLE. 992826
Spike LCS LCS %Rae
Pa.amalat Units Cvnc. Paull %Reo urrits OuMAen
[xaalma uyl 200o0 19600 90 60.110
MATRIX SPIKE i MATRIX SPIKE DUPLICATE- 992629 992!10
MS MSO
921 "1153016 601,0 Spike MS MSD MS MSO
% Rep Lip
Param.16r C]nlle Reelal Con.. Cone. Rn1dl R... N %Rae %Re.
0",41 RPD RPO OuM
COolldo uA 1Tu0 2001M 20000 65000 $5190 1>0 i v,
75.125 0 74 Mt
REPORT OF LABORATORY ANALYSIS
1 M. rAPon riN nor b. r.producW. 6ro.p n AM
VA I.. ONW201 ] 10.9 AM waw.."x W�, ran.r.1 of Pry. anrreyry 56mr.6 Nc
Page 89 0177

P.0 A -I yd[.Ia W'.r-1n[. Pau Anaryu..16arH[rr, Ina
P.uAn.lytl[eraervlur,ln[-
,""
An' !+kcal" 2G5 F.,1 W •Arw Ra,O 5�,,. A 7225 Rr.,.ida Or
9eW Kv,crTAr. 1 W
- ,µAll EJr. HC 2'"7115 �W[ . HC ]1665
IMW=ffi[ Ht 7ddT6
131d w 23-aw, [exel25[-71 m
[7qm wH-Pm
QUALITY CONTROL DATA
Protect: S,JRy Good -MI AaY (UIC)
Pace Pr9jed N9.= 92159653
OC Batch: WETAM546A An.1nu Mmm d. SM 531OB
OC BeNh Melrwd SM 53109 Ana7ale Opadpaon: 53108 IOC
Aawc4lad Led Somp14.: 92159653001, 92159653002, 92159653O0S, 92159651006, 921S96S3006,12159653007,Y215053006-
92169653106, W159953010, 92569653112, 92159653017, 92159653111/
METHODSLAMK: Y65731 Mold.: VAI.,
Aa.vael ad Leh S.rnpl.e 92159651001, Y210153004 92159651000. 921596S1005. 92159E 530K 021596510a7- 92139651006,
91159653009,$2159653010, 92159653o 12- 92 T 5 9953013,117 1590 S3014
Blank R.Whrig
P.famaw Lk1Aa Reauh LImN Analyzed L'IuaAM1en
Total OrgWc C.rhm vwL ND I= 0670Sf13 15:16
LABORATORY CONTROL&AM": 965j12
Spilka LCS LCS % Ric
Aaremrrwr Link. Corte RanAt % Ric LMN Qu.a6ar.
Tow O Wow Carhop uOfL 25000 2woo 102 90.110
MATRIX SPIKE & MATRIX SPME DUPUCATE 965733 9ltmol
MS AISD
R1597524116 Soke Spwe MS MSG MS MSD
%Re. Mac
p.romaler LMdN Raw" Cent. Cana. RMIAI Re" %Ria %Rae
UtrMs RPD RPD anal
Total Orgwac Carhon ayl 1T.A 2S000 26000 SS600 36500 73 72
75-125 1 20 Mt
MGR
MATRIX SPIKE. & MATRIX SPIKE DUPLICATE 965735 1195735
MS MST)
92159651905 3prke Spilka MS MSD MS MSD
%Rea Max
paremein tMWe Re wit Cone. Cvec. Rmll Re.ult %Rey %Re.
LIMIa RPO RPD 06pal
Tow Deperaa CorlaR uWL 1440 250M 25000 25600 25700 91t 97
75-125 T 20
REPORT OF LABORATORY ANALYSIS
i,w spun N,1 not a ,.ptod,xW, qugln M
Dale QW WO 1) 10 49 AM sle.eut"wn— p tof Paee AnOrhal Sams. k,c Pall. p7 al 77
Pea: An�y6.N O.Mua, lrw. P... Ar+aIydchl 6a.11ar I. Me- Pau Anevffir Item..' Me.
a�� l • i05 Erb M[.dow Ro.d 5,n1. A 2M H—We Or IiWO KI—,v . Si Im IW
l ww. '� i1 mn Ewn NC 2nw An.M.. NC 2690 r.,nanvlre HC 2M75
r i3]e1e23Ev2+ 162e I2Sr-r11e I7O1!eiS9We
QUALITY CONTROL DATA
Pe WA: SWrY Goad-ktl AJry IVK:j
Pew PMI@d Na.: 92159131
OC Binh: I19ErAMN06 Anelyrh M.6+od: SM 531o6
OC 6I tch M.U.J. SM 33W0B Anatyal. Da..4pibn: 5310E TOC
Aaaodat.d Lai Saslptee- 92159353015, 92159653016, 92159651017, 92i59653(116, 921596S3B19
METH009LANK: M121 MAIR. YAate,
A.ao6.1.d L.l S.nplee: 42150653015, 9215965m16, 92150553017, 92159e51016, 9215765101Y
Blank Repotting
pv.mela, Lbn . Re.uk Umlt A..lyr.d Ou.a9ar.
Total Q'VWIc CarovR trgL ND 10p0 0616571 ] 2120
LABORATORY CONT ROL SAMPLE: 1IM172
Spike LCS LCS %Ric
pmenalar UnMe Corm. RmIII %Re,
LIPo4 OuaE6m
ToNI Or96Na Caton uGfL, 25000 26190 Wo 90-110
MATRIX SPIKE & MATRIX SPIKE DIJPUCATE: 966721 966124
M9 MSD
9215W63015 Spike Spike MS MSD MS M50 %Ric Max
Paramelar U'n W Rndl Cane. Corm. Result RsuA %Roo %Mac Lim1A RPO RPD Dual
Tpral Orgeme Cwbw vok 6940 25000 2ww 27100 266100 51 79 75-125 1 20 W
REPORT OF LABORATORY ANALYSIS
THS,o wl 04,4[6e W.u-W-kA.
Date 067 WOI0 10.49 AM w1dw,.e ate.nlr weem VIP" md"y sm . . I —
Peg. 68 of 72

Pace Ana1vWW aomeea, Ine Pen Amlyu Ul tonlen, rn,.
areAn lytica1 • )M £..h M..d.w I d - S,w1. A 7225 Rw.•eda a
A PR �,on Edam, NC 27269 W,..w. r,C 266W
33ap471a97r ta7a175L7I7a
QUALIFIERS
Proj4cl. Surry Cmaed•Mt Amy IUIC)
Pau Ptetaa No. 02139/53
Pace Analy11aal Ionic,., Ine.
9600 lunar Are S... 400
rt---We, ryC 16075
rM416MKO2
DEFINITION$
DF - DaRI9n F.otor, 0 repated• repre.enta the lac -Log appWnd to Ihw repmled ua1. due 1e Ch4npe4 o. 7ea4d. p.ap Pel.nn. N6,hpl of
pt the ..me allw.l, or mw.rur. toot..!
NO • Nut Deeded ec P1 ahoy. aq}r.IM rep. tn0 A"
3 - Elnmated conrentr It— .boys the adiu, led me Shod del schon bme and below She ad}R Me! ieportk.0 Nmq
MD- - Ad2ualed Momod ❑.hoc non Lars,.
PRL - P.C. R►p.Msllt L1fM.
RL • Aaporam9 L1r".
S - Bun o0ns
1,2.plphenylhyeraxNle(1270 Nged smaFrfs2 J.e mpo,-t. Aaehenren..
Cw.wsok.AW EPA prnd41o1ea- u..awdad dale ere di"A.y.d.nd her. h44m urad le e.FwF.re %r.[o y sod f1Pd rW­l
LC-%D)-L*Wpalory Cmbrw SamfAe IOuplleale)
MSIU) - Ma91, Spore (pupuc.le)
pup S.mpl. ISupkmb
RPD - Rr11IN4 Pffl e"I pilferenca
NC - NW Calwlahle
SG - Smu Cd • Clew -tip
U - 1nd;h lee We comp9und ". sn.lytad foe, but not det.sled.
k Nlraaodpnarh41 m1M4 Baca nlpOfe4 end c4r.r.pP he eepsNled k.m pipnanylamna uHrp Mellad 127p The reaWl r.poned 1n.
each 010NIC h a c.m A.W1.d earleenlraUm.
Rqd prsaan.Vpn may net be spleop.{ele In 2-Chlorowlhylwryl etller- Sryren., and VAr.y1 t7dmida
Pecs A alyual I. TM .cuadred. Conla.l yow Pace PIA 1. the ovnenl Nor 61 aocndlmd analyla.
ITN -The NELAC ina9Nda
LABORATORIES
PASI-A P.C. Analy s d Salvku - Aah.rlll.
PASI•C P.- Andyllsd S. 1caa - Chs.1e114
ANALTTE OUALUNERS
92 OayOen u.e1a Fs 1e.y thm l 2 C for .a dlu0ons art. The reported Value la r eallmatsel Ian therm valw and IC uwp Wod
IV the dPUV9n ulnq the most amorod PI sample
Th. recovery o1 dr $e %d source at.ndsrd ..ad t. vdmfy rho Ilnfal tamiNdw l wive IV two fnrlyta M wulde Nu
Ial>mdolt a tonaol lnsla. The rows M a4tlrnalad
M} Ma1Fe yplfr H[wary e3C4ed4d flC 11nJq. Bflth eCoapled paned on Lbrcdary e.mtr.l ..rrpls (LCS) rem9.ry
R} RPD v W w.a outs Ida .-I,.P Nmhe.
89 SWOON a r.r uv wry outsld. Isboratmy Conte or Pilafs
REPORT OF LABORATORY ANALYSIS
tr," "ehN aW-.a,—ad...Gptn kA.
V.I.: 01M2&2013 10 49 AM .. we wdrn..sr.s.n a- P.c. A-Ink.I 5.—. sae Pelt. 19.f 71
Tice A00,4N.1
a.M[er, roc- Pea. Aeel V09al 1lwrrc. ln.. P.e. A.Wyv,w aontc.a, toe.
jjjj�lVf�,aj • 205 fuel MIe kaa9.5.eu h 2225 R_w b "Cu.4.ra1 Aye 5r. lw
1 aww^^JJ l6, Edon. NC 7775a A .M. ryC 28eG4 v..w.- Mc x 16
1336p]3-092. r6261254. 71 76 1704 N754VA,
QUALITY CONTROL DATA CROSS REFERENCE TABLE
P"hecl
Sw.y Claeed Mt AA [U ICI
P.- Pru!ecl No
9215955"
Ane"Cep
Lsh N]
Semple ID
QC Batch Mathed
OE Balch Alulytical Math4d
Batch
121He63001
MW1
SM 303X
MPPI340 EPA601f0
cP11264
rrp112264
527l1002
MW-
SM W30C
MPRP134415 EPA 600
l271630
W7i5
SM X0C
MPRA346 EA 5010
CP1122540
iFPl1225li
0
W
M MW
MP11
PRP13445 EPAd60
9214l163006
MYy-16
SAI 3030C
MPRP113445 EPA60TO
ICP112254
lit Ha63067
a,W-19
SM 3050C
MPAP11344B EPA 1010
ICP112254
l21df/6700/
MW-t1
SM 3030C
MPRPI13447 EPA 6010
MP1122M
921816f3007
MW-12O
SM 307OC
WWI M47 EPA 6010
ICP1127S5
0181e53010
MVY-19
SM S030C
OAPRP113447 EPA 601E
ICPM2256
l211l61012
M7
SM 030C
MPR1141M EPAW10
ICP112I14
11
44 Im3
9
SM 3070C
M1
PRP+3465 EPA 60
CPl22A
92135I51014
MW-13
SM 1030C
MPRPM3465 EPA 6010
N:P1122a4
921 "a 6"1 a
AI3Y-14
SM 3030C
1APRP113465 EPA 6010
ICPl12244
/216I!l301!
MW-11
SM S0301C
MPRPI1346S EPA SOi0
1CP1122a4
i211!lf 3017
MLV-20
SM 3030C
1APRP111465 EPA1010
rCp112284
9276916301E
MW21
SM 3030C
MPRP1134A5 EPA 5010
ICP1122a4
9216l163019
MW22
SM1070C
MPRPlf 3465 EPAS010
ICP1122l4
!l167a$300;
MW-1
EPA6260
MSV123197
17161611002
MW-SR
EPA a260
MSVf2S197
.1.1115Au
MW.128
EPAa260
MSV1211
921f9a67006
MW-23
EPAa260
MSV=197
92161863011E
MLV-13
EPAaM
MSWf23197
92tlfa6]907
MW-19
EPA1260
MSV12161:9
l2715a 67908
MW-18
EPA a2a0
.12310
1216013001
MWI2O
EPA 9260
MS11f23199
92169653011
MW-16
EPAS210
MSV723261
92t f9k63G12
MW-7
EPA
MSW23261
91111f l63053
MW9
EPA 1260
MSV/n261
22$59163014
MW-12
EPA "so
MSW23261
9219986301E
MW1r
EPA 1260
6ASV12ST99
9256916301f
MW-12
EPA 1260
MSVF23261
l215a85]Ot7
MW2^
EPA 626E
MSVft]261
12139113014
MW21
EPA 1260
MSW22211
02160051019
MW-22
EPA 126p
.WR3261
l2t39If3
IMAI",l2
SM 2120E
WETl25e26d0
92I902
Mvv-2azon
WETr2626
9216a 510
W
SM 232M
VVEW25625
92983011E
]
W1921
SM 2120B
VJETQ5626881d300fi
SM232GB
WeT125126
921191O07
MvW4I
SM2340E
WET12564
21 IiWl7 2
MW.
SM 2120E
WET1252695
W-
M12
M
WET7262600
92169a83010
MW-16
SM23206
WETf25626
92161663012
MW7
SM 2320E
WET125M
REPORT OF LABORATORY
ANALYSIS
T" rap" ti P net a rep -hi ,. yrhA
.l, re W2912013 1
0.49 AM
_Ww i e. worn w.,snl of P.[e M,lv" 6e= sr
F.D. 70 or 77

d R.- Anal OV V 6aeWr.., Inc- Para Anel y9a1l a-1ee., I.. P.c. AnMV-1 6.rrlcrl, I-C, 4 Paea AnaPytleal $.rvls.., Ina. P1 e. Ana1y11 eat 6ervleea, Pne. Paea An=-- 5-1w1, 1n e.
2% Ea 11 M..W. Ro.d - SW W A 7775 R�..rv;. 0r 360d h .r A.. Sub. 10p Y �L'e f II�'�"�� 7a5 k.N Veamw Ropy • $uM 1, 7)Y+Rr.i�d. Or 9600 nirc�v M. 6�r� 1 W
Edm- IfC Z]7A8 4M,..^.. HC IH66. PI�nW rn�.. HC Z9976 - ,r,^�.' ` Pw E4-. HC Zl Z66 A0, .. ; 786Ua �r.na.. HC 79a iP
PMA2 M1 (Za)754-7176 (7O41B7541092 IlOe)679�921 [97B)754.7179 jTu )B759097
QUALITY CONTROL DATA CROSS REFERENCE TABLE QUALITY CONTROL DATA CROSS REFERENCE TABLE
PF*917 awy Clwe-�Ml AAY (VIC} PP.lad; Saly cTw.d-m uIC)
PAie Pf019d NO.: 92159850 PIo9 PP004 NO. 92159451
Anlllyfkal Analytical
Lab ID Sample 1D W 5a1eh M-Mod QC Balch Analyee.l M.Ihod Beerh Lab 10 9a p1910 QC S§Ub Mnhod W BRICb AMIV41u1 M.IhOd Bahl,
92169163D13 MW9 SM 2320B VVET725T38 9p161663OOT MW.19 SM 4500-CI•E WETAAM5
1216986101A MW-13 SM 2320E WE765738 12191153001 MW-11 SM 4500-C1-E VOEiN15355
12199163016 Mw-14 sM 23206 WETn5738 92161161009 Mw-M SM 45oO-ME YYETN15555
92169663014 MW.iy SM 7320E VVET725736 12169863010 MW.16 9M 4500•CI•E YVETN16655
92161863017 MW30 am 23208 WET125736 12169861012 MWi SM 4500-CI-E M7AF15556
132159863016 MW-2t SM 23206 WET125736 92169163013 MW9 am 4500•C1•E MTN15555
921698530f9 MW-22 SM 2320E WEYIW36 19119161014 MW-13 9M 4500•C-E WETN15555
92569863001 MW-1 SM 5209 WET125511 SM 52108 WET725582 12169163015 MW-14 BM 4500LFE WEYN15555
9 11/53002 MW.3R SM 52108 YVETf25S61 SM 52108 WET125542 12169043016 MW17 SM 4500•0•E WETN13578
921:90631301 MW.128 5M S210B YVETf25i81 SM SZIDo WET12S562 1p169163017 MW-20 SM 4500-CI•E WETN13575
92169663006 MW-23 SM 52108 WET125581 SM 52108 WET1Y5462 121896S3016 MW21 BM45DO-C-E WETN1S576
92159093005 KW-16 SM 52106 YVEW25501 SM S210B VVET125582 9p151883019 MW-22 SM A500•Cl•E WETNI5675
1215911310OT PAW11 SM52106 VVETQ5591 SM 5210E VWTR26417 921696630al MYY11 SM 5310E WETNISA 94
12159163001 MW-19 SM 5210B WEV255al SM5210S WETMM2 92159BB3002 MWAR SM 53f0B VVETN1646A
92169663009 MW-12P SM S7105 WETM541 am $2100 YVCTIM12 12169853003 MW-173 SM 53we WL:MIu BA
12169163010 Mw-16 SM 52105 9VEM5581 SM 52100 VVETfZ5562
9p169867006 MW23 58153108 WETN16484
92169a67012 MW.T SM $2106 V1N-7n o$ SPA B2100 N B2100 WETf25502 12159953006 MVV-16 SM 531DIETN1S4a4
92149667a111 MWY W 5210B WEMM01 SM 52108 VVET07M02 12169667p07 MW-19 SM 5310E WETN15464
921AND014 MW-13 am 52108 WETIM01 SM 52108 WETRSa02 121191"Dol MW-11 SI4 5310B YVETN15464
921698SWs MW-14 SM 52108 iNET125601 SM 62WOB 6VEM25602 621699S3a09 MW-12D SM 53108 WETN1SMM
,WD300010 MW1T SM 525DS VVEMM01 am 52106 VAW25602 1210115301D MW1B SM5310B YVETN15404
9216981301T MW20 am Sp1DB YVETR56D1 SM $2106 VYET25602 12169163012 MW-7 SM5MOB WETN15484
92159863016 M W-21 SM 52108 WET125601 SM 52100 WETQW7 92169163011 MW9 SM 53106 AETN1 W84
92169853019 MW-22 SM WIOA WET125601 SM 521081 WETl26602 12169a83014 MW-1 S SM 53100 VYETAP16484
W 59663OD1 IAW1 EPA 300.0 YVETN15463 9615988301S MW14 SM 5310E WETN15460
92166663002 Mw•3R EPA 300.0 YY£TN154a1 01189693019 MW-17 SM 531011 WETNIN90
12119853003 MW-12S EPA300,0 YV-TN154a0 92161463917 Mw•20 SM S31OWETN15490
l2169153OD6 MW21 EPA 3000 WETN15469 92119a53a16 MW2SM $3i0S ETNt5490
92169963DO1 MW15 EPANO-0 WETN15481 9Y1i6867D19 MW-22 SM 53S0B YyWETNf549D
12159863007 Mw•19 EPA300-0 VYETNIS489
12159163005 MWAS EPA300-0 WETN15469
621691630D9 MVV-12D EPA30O-0 WETN15419
S211961301D Mw-18 EPA 300.0 WETN15409
92169951012 MW7 EPA300.0 VVE AF15409
S21M03013 MW4 EPA 3D0.0 WETAIISA19
92199853016 MWA3 EPA 300.0 WETN15469
92,159853019 KW-14 EPA 300.0 VVE7N154a9
92159653016 MW-I? EPA 300.0 WETN15489
92199853017 MW20 EPA 300.0 WETNI5489
121698638t1 MW.21 EPA 300.0 WETN15489
52159153012 MW-32 EPA NO.0 VVETA115459
SM0113001 MW1 SM 4500-C1•E WETN15555
92169163D02 Mwin 91h 4500•CA•E WETNOM
0210161003 MW129 W4500-C>C WETN"556
92169903006 MW23 SM 4500•CI-E WETNIIW55
12160963009 MW16 SM 4500-C1-E WE7N5565
REPORT OF LABORATORY ANALYSIS REPORT OF LABORATORY ANALYSIS
7N r.Pen &n.1 netW nomere.n,.—PI n ha. TPd. opal wr nm b nPw�,..-P1 n ".
Dal.: Wr26l2013 50:49 AM .�I" w t.n c.e M 01 P.c. MA10o1 B. %. Irk PAge Ti el 77 Date: 060MOt3 10:49 AM n.Mui IV w1P9en rm.enl VP Plc. AtiIy" Sprvk Irc Page 7p of 77

�'7 fwwu,arn Irnnfn.
a Sam In Condlllan U On Racal i SCUR ywV '� PaI e 1 of 2 W y y
UvwmeM Number: Issuing Authority.
F.CHlt.C8.a7ve._ 111 1 P_ Hunlersvllle ouallty Offlae
Client Name-
Where Received: Hunlersville ❑ Asheville [] Cdnfi [] Raleigh
Courier: 0 Fod IX ❑ UPS❑ USPU Client D Commorda0 Pace Other jai . rCyAG
Custody goal on CoolerrBa: Presenl: ❑ yae E ino Sonia Intact ❑ yea ❑ no
Packing Material: ❑ Buhble Wrap Bubble Begs ❑ mono 11 ❑ kor
Thermometer Used; At dun T4101 Q216 Type of Ice; cl Blue None a.Mims 0n ice, c "pfap ha.!a-wum
T.,.... r`...,rwlr..w G. Y7 7 n7 • Mn r.,rrsnrL­ T71 n7, Mn r—ki—
au end ul s o[ r aminlrrp
Corrected Cooler Temp.l r. � C BIOIOpIc#! 7{aQUQ Is Fra#s+r: YM
Tamp thould ae shove IraMMs is e•C ComrrlQr":
Clwin of Cuslony present Y.. Ohio OHrA
1.
Chain of Custody Filled Out: Y.. ON. Own
2.
Chain of Cuslody Reh ulahed: Ye. ON. 17wA
9.
Sampler Nome d SI nolm on Cool Yu Ora DWA
4-
Sam lea Arrived vldhln Hard Tlme: l..r ON, UWA
5,
Short Hold Time Anal Is 472hr : Y.s Own
8-
Rush Tum Around Time Requested: OY.. IJAW ONA
7.
Sufficient Volume: a+ ON. OwA
B.
Correct Conlolnars Usod: ON. OruA
-Pace Contalnora Used: . Y.. ONa ONA
Q.
Containers lnlact: Y.s l7WA
w 5
Fikeratl Volume recelyed for Olasoheed !oats Ova. ON. wA
11.
Sample Labatt match COC, pYet ON. ONA
-I netudas d.7leAirneADlAnal sia Mefnx: —I--
/2,1, f4e aJ.r,j AJ 0
7] Far
Aa conlsinba n6awV pi .awed n heye ben chenrea Ty,YM Olw 13WA
Alf contalnms natft presomaGon are bled io be YI fhY.r Uri Own
umplunu nAri EPA remmm er:dallon. r
n Owr VOA 000M TOC• GAG. Y1 ORO fw Elyp N.
13. u r � 4�- o
Som Ida cherked for dechlorloallon: a ON. OwA
14-
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CHAIHAF-CUSTODY 1 Analytical Request Document
' Q Th. CN—vf4Cuema� is a LEGAL oacuWErrr m www odes mutt be mrww. .q a".

EnvIronmentaI Conservation Laboratoriss, Inc.
101-A W W4~f k,&AkM Cprrl
CMc7 MC, 17Stt
7i.p...: 90AS M FM 11arc17isis
Wednesday, June 19, 2013
Munropal Fnglneering Services [MUOUI]
A[tn: Jonathan Pfohl
P.O.8o1 97
Gamer, NC 27529
RE: Laboratory Results for
P roje Ct Nam In a,i G11024 Z'OSC d, Project Name/Desc: Sul rry Co. Closed MSWLF - Bromide
t NCO Workorder(s1: C306645
Dear jona[han WOW,
Enclosed Is a copy of your laboratory report ror test samples received by our tabvratory on
Wednesday, June 5, 2013.
Unless otherwise noted in an attached pr*ot narrative, all samples were received In
aaeptabie Condition and prrrcessed IM aomrdante with the referenced methW procedures.
RmIts for these procedures apply only to the samples as submitted -
The anaybcal rewRs contained In tots report are In compliance with NELAC standards, except
as noted In the prdyect narrative. This report shall not be reproduced exmpt In full, without
the winner, approve[ of the Labural bry.
This report contains only fFwse anaryses performed try Environmental conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary, Data rrom
crud side org a nizatlons will be reported under separate cover.
I you have arry questions or require further information, please do not hesitate to meact me
Sincerely,
OLLC-:;�UA
Qiuck Snuth
Fralec[ Marwger
Enclosure(5)
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ANALYTICAL RESULTS
Lap Sample ID: 006645 01
Sampled: 05jXf I3 lf1:40
Sampred ey: k.mtw Pr9ht
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Mahler GrMM WNer Sampled: 0WniI) 11 05
Project: Surry Co. Clpred MSWCF - f&pn We S.mpkd hp Jar e— prohl
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Pwo act: Surrr CA. CwAd MSWIi - Bryn Wv Sampled fy: knM W PfeN
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Ilecen'ed: OW651Sj 0:25
Wor%Orde: 006A4S
Ckss}cai Chemistry Parameters
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Matrix., Ground Water Sampled: f7WIW%] 14; 15
Prnyecl: S." Co Cbwd MSWLF - Ero-We 5an.p led By-. )a-lww PkN
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o"CrIption: MW-21 "h Semple 101 C]06h45-05
M.1rie: G,-.d Weer Sampled: OSjWB 14'30
Project: Sn rry Ca. Cased M-1,WV - womwc Sw pW ey: i-Khan Pfohl
Classical Chemistry Parameters
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FLAG 5I NO TES AN➢ DEFINITIONS
d The aSaslta was detected 1n"ass xioted method blank.
0 The sample was "Fried at dlklbon-
] The IM*Ud value Is between the laboratory method detection Imit SMOL) and the taboratdry "wood
reporting Lmlt (MRL), adjusted fa actual sample prepratw data and moisture content, whve appimbk.
U The &wAfte was "Wed Mr but not detected to the kvet shvlvn, adptsted for actual sample preparatlon
data and molsnre c Fte% where applcable.
E The CorKeneatlgn t"cated for thL5 an "IS an estimated vacua above the Calibration r" Of the
Insnimmnt. This Yaile Is u r1 x,E an a Iimate.
MILL Met lydd ReWMQ Limit- The Mill. IS roul;J* e"Olerrt to did prackleal Cuanptadon Im1t (PW AN IS
twsed on the law pOlnt & the calC1at10n curve, wtsen 8MCidb40, Sample prepantMn factor, *knldn
factor, and, to the case of sari samples, molsture content-
QM-05 the spke reahvey was ixdLu a ecceptar Ionics. fer the M5 arldla MSD due tp malrlx
Interference. The LCS andlw LCSD were wl thin acceptmxe IrmLS shuvnng that the labmtary Is
In control and the dot? IS acceptable -
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