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HomeMy WebLinkAboutWI0400176_W/ CORRECTIVE ACTION UPDATE_20140910Semi Annual Water uality Monitoring Report with Corrective Action Update Prepared for Surry County Closed C&D and Closed MSWLF, Mt. Airy Mt. Airy, North Carolina May 2014 Permit Number: 86-02 MESCO Project Number: G14024.0 Submitted: September 10, 2014 Municipal Engineering Services f Compasry, PA. Garner, NC 1 Boone, NC P.O. BOX 97 Municipal Engineering Services Company, P.A. Garner, NC 27529 Gamer and Boone, North Carolina License No. C-0281 Data - Email CD (data loaded: Yes / No) Doc/Event #: LNG DENR I I Environmental Monitoring Division of Waste Management - Solid Waste Reporting Form Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6). Instructions: • Prepare one form for each individually monitored unit. Please type or print legibly. Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing condition, etc.). • Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. • Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(1). Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646. Solid Waste Monitoring -,Data Submittal Information " Name of entity submitting data (laboratory, consultant, facility owner): Municipal Engineering Services Co., PA Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: Jonathan Pfohl E-mail: jpfohl@mesco.com Phone: (919)772-5393 NC Landfill Rule: Actual sampling dates (e.g., Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006) Suny County Closed C&D and 237 Landfill Road 86-02 .1600 May 27-29, 2014 Closed MSW Landfill -Mt. Airy Mt. Airy, NC 27030 Environmental Status: (Check all that apply) ❑ Initial/Background Monitoring �X Detection Monitoring ❑X Assessment Monitoring Corrective Action of data submitted: (Check all that apply) Groundwater monitoring data from monitoring wells Groundwater monitoring data from private water supply wells ❑X Leachate monitoring data 1-1Surface water monitoring data Methane gas monitoring data Corrective action data (specify) MNA parameters on 7 wells Other(specify) Notification attached? No. No groundwater or surface water standards were exceeded. X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. Certification To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Steven R. Gandy, Ph.D., P.E. Facility Representative Name W Signature P.O. BOX 97, Garner, NC 27529 Facility Representative Address C-0281 Senior Project Manager Title Date NC PE Firm License Number (if applicable effective May 1, 2009) Revised 6/2009 (919) 772-5393 (Area Code) Telephone Number Affix NC Licensed/ Professional Geologist Seal �� H 1 CA 0 i Q SEAL 7• _ _ 031020 _ IIII11 TABLE OF CONTENTS SECTION Introduction................................................................................................................................................................................................................................................................................Page 1 Background.................................................................................................................................................................................................................................................................................. Page 1 SamplingProcedures......................................................................................................................................................................................................................................................Page 2 FieldParameter Data......................................................................................................................................................................................................................................................Page 2 LaboratoryResults.............................................................................................................................................................................................................................................................Page 2 QualityControl Samples.........................................................................................................................................................................................................................................Page 3 GroundwaterSamples...................................................................................................................................................................................................................................................Page 3 SurfaceWater Samples...............................................................................................................................................................................................................................................Page 3 CorrectiveAction Update........................................................................................................................................................................................................................................Page 3 MNA Analysis (AOCs Northern, Southern and MW-11).......................................................................................................................................Page 3 Enhanced Bioremediation via Substrate Injection (AOC Southern and Northern).............................................................Page 3 Groundwater and Surface Water Characterization.............................................................................................................................................................Page 4 Findings............................................................................................................................................................................................................................................................................................. Page 4 Closing............................................................................................................................................................................................................................................................................................... Page 5 FIGURES TopographicMap with Site Location..............................................................................................................................................................................................Figure 1 Potentiometric Map of Uppermost Aquifer w/ VOCs Detected Above 2L Standards...........................................Figure 2 Total VOC Concentrations Pre/Post Injection Comparison.........................................................................................................................Figure 3 Bromide Tracer Concentrations Time Series Graph and Table..............................................................................................................Figure 4 Total Cumulative VOC Concentrations Time Series Graphs/Table................................................................................................Figure 5 TABLES Samplingand Analysis Summary............................................................................................................................................................................................................Table 1 Detections that Attain or are Above SWSL, GWP, 2L, or 2B (Appendix I)...........................................................................Table 2 Detections in Water Samples above MDL (Appendix II Exclusive).................................................................................................. Table 3 Hydrologic Properties at Monitoring Well Locations.................................................................................................................................................Table 4 Field Observations of Monitoring Locations........................................................................................................................................................................... Table 5 FieldParameter Data Summary.................................................................................................................................................................................................................Table 6 MNAParameter Data Summary...............................................................................................................................................................................................................Table 7 APPENDICIES Laboratory Analysis Report and Chains of Custody.....................................................................................................................................Appendix A Field Sampling Parameter Data Sheet(s)......................................................................................................................................................................... Appendix B License No. C-0281 CIVILISANITARYIENVIRONMENTAL ENGINEERS Municipal Services SITE PLANNING ISUBDIVISIONS SOLID WASTE MANAGEMENT Engineering Company, P.A. SUBSURFACE UTILITY ENGINEERING (SUE) September 10, 2014 Ms. Jaclynne Drummond Solid Waste Section Division of Waste Management North Carolina Department of Environment and Natural Resources 401 Oberlin Road, Suite 150 Raleigh, NC 27605 Re: Semi Annual Water Quality Monitoring Report with Corrective Action Update Surry County Closed C&D and Closed MSWLF, Mount Airy Permit No. 86-02 MESCO Project No. G13025.0 Event Date(s): May 27-29, 2014 Dear Ms. Drummond: Introduction On behalf of Surry County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this Semi -Annual Water Quality Report with Corrective Action Update for the spring 2014 event performed at the Surry County closed construction and demolition (C&D) and closed municipal solid waste landfill (MSWLF)-Mount Airy. NCDENR Solid Waste Rules 15A NCAC 13B.1632 requires that Surry County provide this report to the NC Solid Waste Section (SWS) on a semi-annual basis. This report documents the quality of the ground and surface waters during this monitoring event performed on May 27-29, 2014. Laboratory analytical results indicate volatile organic compounds (VOCs) in concentrations in excess of SWSL and 2L Standards continue to persist in samples collected from four wells that monitor the uppermost aquifer. The surface water samples collected from the local discharge feature remain unimpacted. Corrective action to remediate VOCs in groundwater is ongoing within the Northern and Southern areas of concern (AOC) with updated information presented herein. Background The Surry County closed C&D and MSWLF, permit #86-02, is located at 237 Landfill Road in Mt. Airy North Carolina. The site location topographic map is depicted in the attached Figure 1. Prior to becoming a C&D landfill the site operated as a MSW unlined sanitary landfill that consisted of two units. The northern unit was closed prior to October 1991. The southern unit is comprised of two contiguous portions. The first part stopped receiving waste prior to October 1991 and the second part stopped receiving waste prior to January 1, 1999. Both portions of the southern unit were properly closed with a low permeability cohesive cap per the Transition Plan. The top portion of the southern unit served as an exclusive C&D landfill until prior to June 1, 2008 at which time it was properly closed with another cohesive cap in accordance with the Closure Plan. For continuity, both the northern and the southern units are monitored and reported together. Water quality at this facility has been monitored at least semi-annually since 1989 with historical data available since 1994. This event was performed in accordance with the NC SWS rules/regulations as promulgated in 15A NCAC 13B and as a condition of the post -closure portion of the permit to operate. As specified within 15A NCAC 13B.16320) and the SWS Environmental Monitoring Report Form this report contains sampling procedures, field and laboratory results, statistical analysis, groundwater and surface water characterization, and findings. A table of detections compared to Standards, field data results table, groundwater flow directions/rates table, field observations of the monitoring network table, a potentiometric map of the uppermost aquifer, histograms of historical detections, laboratory analytical reports with chains -of -custody (C-O- C), quality assurance/quality control data. PO Box 97, Garner, North Carolina 27529 (919) 772-5393 PO Box 349. Boone. NC 28607 (828) 202-1767 Sampling Procedures The water quality monitoring program, current as of this event date, includes sampling locations and parameters as outlined in the Water Quality Sampling and Analysis Plan (SAP) (DIN:18936) dated April 30, 2013 and approved by the SWS (DIN: 18938) on May 10, 2013. Monitoring locations are shown on the enclosed potentiometric map (Figure 2). MESCO personnel collected water samples from 20 downgradient groundwater monitoring wells (MW- 3R, MW-4, MW-6 through MW-11, MW-12S, MW-12D, MW-13 through MW-23), one background well (MW-1), four surface water locations (SW-1, SW-2, SW-3 and SW-4), and the water supply well (SCALEHOUSE) that serves the facility. Data from two surface water points (SWN-1 and SWN-2) designated in the SAP for the adjacent Subtitle D Lined MSWLF are presented because this local discharge feature is shared by both permits. Quality control measures implemented during this event included the submittal and subsequent quantification of blanks equipment (EB), field (FB) and travel (TB). Samples were not analyzed from the six injection wells (IW-1), (IW- 2/MW-2), (IW-3/MW-3RS), (IW-4/MW-4), (IW-5/MW-5) and (IW-6/MW-8) since they are exempt due to the presence of injectant residue which would yield unrepresentative water quality results. Monitoring location integrity was visually evaluated with no deficiencies noticed as documented in Table 5. The depth to water in each well was electronically gaged prior to purging to quantify the static water level elevation. Low -flow pumping methodology or bailing was utilized to adequately purge the wells to a minimum of three times the volume of standing water in the well or until dry. Surface water samples were collected from Stoney Creek discharge feature at previously designated locations. During well purging and surface water sample collection the required field parameters were recorded. The samples were then placed into laboratory -prepared, pre -preserved containers via a new disposable polyethylene bailer. Samples were collected, kept on ice, and transported to a NC - certified laboratory under proper C-O-C protocols within the specified hold times for each analysis. Field Parameter Data Stabilized field parameters were recorded during purging which included depth to water, pH, dissolved oxygen (DO), temperature, oxidation reduction potential (ORP), specific conductance, total dissolved solids (TDS) and turbidity. The field parameter data indicates the monitored groundwater is slightly acidic, low DO, with relatively low specific conductance which is generally consistent relative to each other and congruent with data historically reported. Field parameter data recorded at the surface water locations were neutral in regard to pH and low specific conductance which is consistent with uncontaminated water. A summary of the field parameter data is presented in Table 6 and the field sampling data sheet is enclosed in Appendix B. Laboratory Results Pace Analytical Laboratory (PACE) of Huntersville and Asheville, NC performed the laboratory analysis of groundwater samples for the total recoverable constituents listed in 40 CFR Appendix I and the few Appendix II exclusive constituents detected during the previous fall event. Pace analyzed samples collected from six wells for monitored natural attenuation (MNA) parameters. Environmental Conservation Laboratories (ENCO) of Cary NC tested the six samples for dissolved methane. Additionally, ENCO reported results from seven samples for bromide tracer to assess migration of previous remediation injectants. The surface water samples were analyzed for the parameters listed in 40 CFR Appendix I. A sampling and analysis table summarizing the locations, constituents, and methods is presented on Table 1. Laboratory results and C-O-Cs are contained in Appendix A. Water samples were reported to the laboratory specific Method Detection Limits (MDL), which are quantifiable at or below the current Solid Waste Section detection limits (SWSL). Table 2 summarizes Appendix I constituents detected in the water samples in concentrations above the current SWSL, Groundwater Protection Standards (GWP), North Carolina Groundwater Standards (2L) or the North Carolina Surface Water Standards (2B) for the applicable Class C water body. Table 3 summarizes Appendix II exclusive (defined in this report as constituents not also listed in Appendix 1) constituents detected above the MDL. 2 Quality Control Samples The quality control samples EB contained methylene chloride. Since methylene chloride was not detected in any other sample the data set appears to not be affected by false positives or high bias attributed to the identified laboratory induced artifact contamination. Groundwater Samples Total metals were not detected at levels above their respective 2L Standards. One or more VOC(s) were detected in quantifiable concentrations (> SWSL) above their respective 2L Standard in samples collected from four monitoring wells (MW-9, MW-15, MW-16 and MW-21). The majority of the monitoring locations that were found to contain VOCs included a mixture of dissolved phase aromatic hydrocarbons and chlorinated aliphatic hydrocarbons. The only constituents detected above the EPA established maximum contaminant levels (MCLs) primary "Drinking Water Standards" were vinyl chloride (MW-9, MW-16) and 1,1- dichloroethene (MW-15). A site map depicting the concentrations and estimated horizontal extent of VOCs that exceeded the 2L Standard during this event is presented on Figure 2. None of the targeted Appendix II exclusive constituents were detected above allowable 2L Standards. The on -site water supply well (SCALEHOUSE) continues to lack target detections in exceedance of current groundwater or drinking water Standards. Surface Water Samples Constituent(s) were not detected in any surface water sample in concentrations in exceedance of applicable 2B Standards. Corrective Action Update Groundwater remediation continues to be implemented per the approved CAP at the three designated areas of concern (AOC) (Northern, Southern and MW-11). A Corrective Action Evaluation Report (CAER) (DIN: 19361) was submitted on May 1, 2013 which demonstrated that the plumes continue to decrease and was approved by the the SWS on July 24, 2013 (DIN:19366). A historical summary of corrective actions performed to date are briefly presented in the following sections. MNA Analysis (AOCs Northern, Southern and MW-11) Semi-annual MNA monitoring of a subset of 12 wells for the full suite of SWS recommended parameters was initiated on May 18, 2010 and performed for four consecutive semi-annual events to establish a baseline. A revised SAP prescribing 7 wells with varying targeted MNA constituents was approved by the SWS and initiated during an event performed in May 2013. MNA monitoring was performed during this event for the parameters and frequency as listed in the current SAP. MNA data presented in Table 7 continues to indicate that favorable geochemical conditions exist for continued natural attenuation. Enhanced Bioremediation via Substrate Injection (AOC Southern and Northern) Per the SWS approved Corrective Action Plan enhanced bioremediation via substrate and tracer injection was initiated in the Southern and Northern AOCs in accordance with requirements outlined in the Injection Well Permit Application and Well Permit No. WI0400176 (5/6/11) in an effort to reduce low level aliphatic and aromatic chlorinated hydrocarbons in groundwater to below the 2L Standards. An edible oil substate (EOS)-water emulsion with sodium bromide tracer was injected into four wells (IW-1, IW-2, IW-3 and IW-5) on November 2-3, 2011. Similar substrates were injected into monitoring wells MW-4/IW-4 and MW-8/IW-6 on October 24-25, 2012. Details of the injection events are provided in the Injection Event Record dated November 4, 2011 and January 10, 2013. As directed in the UIC Injection Well Permit renewed on April 15, 2013 semi-annual post -injection water quality monitoring of wells located downgradient of viable injection points (MW-3R, MW-7, MW-9, MW-12S, MW-13, MW-14, MW-15, MW-16, MW-17, MW-18, MW-19, MW-20, MW-21, MW-22, MW-23) and upgradient background well MW-1 was also performed in conjunction with this semi-annual event. Total VOC concentrations reported during this event were lower at all locations when compared to the respective moving averages of the five events preceding injection in the selected wells downgradient of the injection points (Figure 3). Evaluation of injection wells (IW-1, IW-2, IW-3, IW-4, IW-5, IW-6) continues to indicate that a considerable amount of white highly turbid (>1,000 NTU) viscous residual organic substrate and its byproducts remain in each of these wells rendering them unsuitable for representative water quality analysis. The viscosity of the water in the injection wells during this May 2014 event precludes sample collection as either a bailer will not descend or the check valve fails. IW-1 was verified to not be a viable injection well as less than 3 gallons of substrate was able to be injected into the low permeable fractured bedrock and injectant levels have remained above static conditions for over a year. For all intents and purposes IW-1 injection did not occur nor will be possible in the future. In an attempt to track migration of injectants bromide was targeted at MW-3R, MW-13, MW-14, MW-15, MW-16, MW-21 and background well MW-1. MW-16, located 86 feet downgradient of IW-3, is the only location exhibiting tracer levels which may potentially indicate injectant communication. Based on the average linear velocity rates of IW-3 and MW-16 reported since injection the injectant was expected to reach MW-16 in May 2012. Bromide concentrations exhibited a consistent increasing trend in MW-16 the first year following injection then has decreased the last year (Figure 4). Calculations performed following injection indicates that reported levels of bromide injected was insufficient to provide clear evidence of migration within the uppermost aquifer. Groundwater and Surface Water Characterization A potentiometric map constructed from water elevations taken from the uppermost aquifer which consists of both saprolite and the hydraulically connected upper portion of the fractured bedrock system is enclosed as Figure 2. Groundwater flow directions and velocity rates were calculated through modified Darcy's equation as shown on Table 4. Consistent with previous events the groundwater apparently flows in a general southeasterly direction towards the tributaries of the Ararat River. The calculated average linear velocity of groundwater indicates an approximate average of 838 ft/yr in the wells screened in regolith and 392 ft/yr in the wells screened in the bedrock. The consistent disparity in flow rates between wells is indicative of heterogeneous geologic conditions and/or a product of the limitations of the linear velocity equation when applied to anisotropic conditions which are characteristic of the geology of the Piedmont. Streams located within the facility boundaries were observed to be of moderate volume and flow with low turbidity. Findings Total metals were not detected in any sample above 2L Standards. The on -site supply well and the surface water points remain unimpacted as indicated by the lack of detections in excess of the applicable Standards. One or more Appendix I VOC(s) continue to be detected in quantifiable levels above the 2L Standard in samples collected from the uppermost aquifer at four locations (MW-9, MW-15, MW-16 and MW-21). All VOCs detected in concentrations exceeding the 2L Standard remain within their own respective historically identified range. Qualitative evaluation of VOC concentrations indicate a decreasing trend over time and distance from the landfill. Total cumulative VOC concentrations decreased at all locations, except for MW-9, during this event compared to their respective five event averages preceding corrective action (Figure 5). Results of statistical temporal trend analysis, using Sen's Slope Estimator at a 95% confidence level, indicate that none of the individual well's cumulative VOC concentrations have exhibited a statistically significant increase and the Southern AOC and cumulative site - wide levels continue to show a decreasing trend since corrective action was initiated 4.5 years ago. The area of the uppermost aquifer beyond the compliance boundary containing quantifiable concentrations of VOCs in exceedance of the 2L Standard during this event is estimated at 0.0 acres in the Northern AOC, 0.0 acres in the MW-I I AOC and 5.8 acres in the Southern AOC for a total facility wide area of 5.8 acres (Figure 2). This is an estimated 28% retraction of facility -wide plume area (from 8 acres to 5.8 acres) compared to when corrective action was initiated in May 2010. Evaluation of the most current water quality data continues to support assertions drawn in previous reports. A few VOCs persist in the upper portion of the aquifer but concentrations are decreasing over time and distance away from the landfill and the local discharge features which are all located within the property boundaries remain unimpacted. Data continues to indicate that the plumes within each AOC have stabilized and/or decreasing and there is adequate evidence that natural attenuation is actively occurring beneath the facility. 4 Closing Water quality monitoring and corrective action will continue with the next event tentatively scheduled for October 2014. If you have any questions regarding this report, please contact us at (919) 772-5393 or by email at ipfohl@mesco.com or sgandy@mesco.com. Sincerely, MUNICIPAL ENGINEERING SERVICES CO., P.A. �ti t s Jonah n Pfohl Env nmental Specialist Enclosures cc: Mr. Dennis Bledsoe Surry County ,k ywit05 Steven R. Gandy, Ph.D, P.E. Senior Project Manger Figures Topographic Map with Site Location Surry County Closed Unlined C&D and Closed Unlined MSWLF, Mt. Airy fl 237 Landfill Road Mount Airy, NC 28621 Lat:36-26-30.065 Long:-80-34-15.314 Northing:983356.18 Easting:1537885.48 ROAD CLASSIFICATION Primary highway, Light -duty road, hard or hard surface................. improved surface......._W_ Secondary highway, hard surface. . ... . ... -- Unimproved road._ OInterstate Route 0 U. S. Route O State Route Closed Unlined C&D Landfill Closed Unlined Sanitary Landfill 1 0 1 MILE FIGURE I 0iMW-11 SCALEHOUSE 1,2-Dichloropropane - 1.0 (j)ug/I / J (FACILITY NON -POTABLE WATER SUPPLY WELL) 2,37 LANDFILL ROAD 11 0.41 CC E:0 RECYCLE ARE\-( �l N 0 W OR FORMERLY ^\ I'! I 1� ,� J I I ❑�j\ \\ �� TWE \\ 0 WN ED B Y ,IIII, L �o I I I I\ MSWLF CLO FORE J JOHNN Y COX // I llllll., BER9, 1991 Qc9 \ -� 110 , Q IW-6 / I 1 llll I Q 1047.47 , 1061.08 1,4-Dichlorobenzene - 6.6 ug/I \ \\ \\\\ - _ _ ��� �i \ / / / / Benzene - 3.3 ug/I \ \ \ \ \\ / _- ==,� �G - Qy�' ; / / 1 NEWLAi'/ 'J /// MW-20 --,OPD =' '/MW-1 1062.78 10751109.55 COVERED TIRES / i/ 1rII 8t,NG��-7 SURR Y COUNTY / I ' I 1 / / I I r - - ti&I'S _ / IN, MAINTENANCE 1061.69 h / / -,� I I -BUILDING N / / / l I l l l l l l l �t I /( l l If 11 \ _ , - / - III 1 r / / /'/ \\ 11I// �� ; IIII\'\_J_ Is. IMIST � / 1 I I BASING SIN \ \ - BAGJ I I \ \ \ (// I \\� -- ��Olt I \ \ X} I\\ l y1\I IlIIIII Ili i _'�/J / �n MW-6 ^l )j)J y I / I � / 1045.29%ice/''�llllllll��\\� 11 \ \ I I _IIIII �\�JI I Ilillll^ It/ 11 ll II llllI STOPPCLOSED C&D OVER ED REC IV NG&U BOEFORE JUNE 1, 2008 STOPPED RECEIVING MSW BY JANUARY 1, 1999 ACTIVE GCCS I \\ / MW-3R 976.55* /� 1 \ /j/ // // I/II IIII /� / //// // / I I III I l 1 i1/ 1,,/j/// ✓ IlII/ lIIIIIl ///l//\/ /1/ I /// ///////�lll/// / �r//j///��// i/ // �//�/////S/"/ �// // / / / / \0�0 / if/lI1/ 11I1I1I IIIIII I1►6tIW-3 I I I \\\ MW-16 989.62 \� 973.85 /5 I* '\\#W-12D>1027.0 MW 16 * 12-Dichloroe-3.2ug/I 2 4W-12S1012.42 4Dichlorobenzene /i \ - - \ - 15.0 ug/I 1,2-Dichloroethane-2.4ug/I Benzene - 1.8 ug/I Vinyl chloride - 6.7 ug/I l � / Ill I/l j �// IIII/ l / I / � l IIIII III Ifl -18J 1 I� IIII llllll ,1111 �� 957.04 \ I/ / III Ill I� III/ \ \ / � II MW-17 MW-13 J r / �/ / //// 983.25 ,// /r� - )�)1 // MW-13 \\ \ / 1,2-Dichloroethane \\\\\\ \ \ \\ " " _ / // Aso\ \\\\��\ SV-3 \ ////i/ i I / ,��•; t // , / / / / IW-4 / / / / / / / / 992.32 MW-21 \_�\\�� /l//lljll//IIII // ��,k �l \59.92 OO \1I II ( \\\ 1,1-D-i2 %MDcWchh1l loorrooeetthhaannee -- 0642uQg)ug/I= /I3 V W-14 983.41 DENSE 'BEES M W 14 \ 1 Tetrachloroethene - 0.89 ' u /1 NOW OR FORMERLY OWNED BY 1024.84 MW-15 2-Dichloroethane - 0.58�) ug/I -2 SHA WNA SUMMERS i I 1111\I \11\ \\\ \ ✓ `\ �; \\ \\ \\` ® \\\� �\ \\ \ II ehn-94() ug/I94 \ chlooethene3�1 2 Vinyl Chloride - 1.9 ug/I hloroet0.510) ug/I1Dicoff 1-Dichloroethane - 14.2 ug/I Nx MW-19936.43----- \�\\/ EXISTING TOPOGRAPHIC CONTOURS li 9\\/ry`j l!l Jl8) l EXISITING ROADS ACTIVE GCC- 1 /, = ' ��////i/ // ////// /// li I I ♦ //l//// �/ i/ 4 ESTIMATED WASTE LIMITS UNLINED MSW &/OR C&D , l / ll/llllll LINER LIMITS OF SUBI TLE D LINED MSWLF (MONITORED SEPERATELY) II(/� EXTENT OF COHESIVE CLAY CLOSURE UPON CLOSED MSW AND C&D i/ii///� f \1�\ /I111111111111 II" r-_\ PROPERTY LINE EXTRAPOLATED FROM SURVEY AND GIS // //ll17/i/jllllllllll A COMPLIANCE BOUNDARY (250 FROM EOW or 50 FROM PROPERTY LINE) \�\ V'y - ^ / J __ 5 %//%��"'� / EXTENT OF VOC(s) DETECTED ABOVE SWSL & 2L STANDARD BEYOND COMPLIANCE BOUNDAR CTIVE LINEzD 1090 EQUI PO TEN TI AL UPPERMOST GROUNDWATER CONTOURS ,�- PHASE 2����! i / // i/ S TREAMICREEKIRI VER T011/20/09 I.(� / /// / // / WATER SUPPLY WELL (FACILITY CONSIDERS IT NON-POTABLE) <�\ \� � SW-3 44 SURFACE WATER MONITORING POINT \ \0 1 \ \ \\\ 6 \ \`1� 11Ln\ \ `/ --� �w MONITORING WELL \ \ \1 III Il,� I ol\ \ \\ \//�-� //� - / IIII \\\\\\I L� IW-2 I INJECTION WELL NOT SAMPLED DURING THIS EVENT 936.43 GROUNDWATER PO TEN TIOMETRI C ELEVATION (AMSL) *NOTE. ELEVATION NOT USED FOR CONTOURS \\\IN��`\,� -\l i SEDIMENT BASIN SWN-4 _\ _ =Y = l / l J I \\\\\\� \\\\ , , \\ \ DRY Ro� /1,T0 ��/ I \ \ �\\ \x \� \N Groundwater Levels & VOCs Detected Above 2L Standards May 27 & 28, 2014 _ / =_=__ __ 0 WN ED B Y 200 GRAPHIC SCALE 100 200 4W ( IN FEET ) 1 inch = 200 ft. 800 SURR Y COUN TY AREA OF CONCERN per CAP WELL # TOP OF CASING ELEVATIO (FT AMSL DEPTH TO WATER (FT BTOC GROUNDWATER OTENTIOMETRIC ELEVATION (FT AMSL) BENZENE (UG/L) 1,4-DCB (UG/L) PCE (UG/L) TCE (UG/L) 1,2-DCA (UG/L) 1,1-DCA (UG/L) VCM (UG/L) 1,2-DCP (UG/L) AREA OF SWSL & 2L EXCEEDANCES BEYOND COMPLIANCE BOUNDARY ACRES 15A NCAC 2L Groundwater Quality Standard 1 6 0.7 3 0.38 6 0.03 0.6 BACKGROUND MW-1 1134.35 1 24.80 1109.55 1 1 0 IW-2 1068.86 39.61 1029.25 Not Sampled Converted to Injection Well Nov. 2011 MW-3R 1017.50 40.77 975.16' IW-3 1020.57 30.95 989.62 Not Sampled Converted to Injection Well Nov. 2011 IW-4 1026.26 33.94 992.32 Not Sampled Converted to Injection Well Oct. 2012 IW-5 1080.18 39.94 1040.24 Not Sampled Converted to Injection Well Nov. 2011 MW-12S 1025.80 13.38 1012.42 SOUTHERN MW-12D 1027.05 0.00 >1027.05* 5.8 MW-13 1008.48 25.23 983.25 0.47 MW-14 1018.80 35.39 983.41 0.89 MW-15 1075.96 51.12 1024.84 2.3 0.74 (j) 3.6 0.58 (j) 14.2 1.9 MW-16 999.54 25.69 973.85 1.8 15 2.4 6.7 3.2 MW-17 965.43 8.39 957.04 MW-18 983.00 9.17 973.83 MW-19 946.27 9.84 936.43 MW-21 965.36 5.44 959.92 0.42 6.3 MW-22 953.40 5.22 948.18 0.51 MW-23 955.31 7.39 947.92 NORTHERN MW-6 1067.67 22.38 1045.29 0 M W-7 1073.50 1 11.81 1061.69 IW-6 1088.45 1 40.98 1046.64* Not Sam led Converted to Injection Well Oct. 2012 MW-9 1094.07 1 32.99 1061.08 3.3 6.6 10.8 M W-20 1082.19 1 19.41 1062.58* MW-11 MW_11 1 1151.80 1 21.39 1130.41 1 1 1 1 1 1 1 1.0 0 - = urounawater eievauon not usea tar contouring 0) ='j" Qualified concentration <SWSL considered an estimate FIGURE 2 Figure 3 Total Cumulative VOC Concentrations Pre/Post Injection Comparison October 22, 2009 - May 28, 2014 P Ncn ENT of a 7 (711.1 cvmvlatl�e vcc cwic,n�rvrWn. •• P4. arswa,l w ii fer�rsn.. c..yn w � w H w ro P NOfNP of WAvpc cw�c,n�Mwn. �•�1.ar8W9L1 6 H N �o N O DO-1-7 of rvea g-�.I, We cu•untr gqn a.ML ar sway w� # U� 1F M • - I DO-1-7 of IW-5 �rW,�cwnul.n.. WC cpnuimaeom a• rq� o� sway w o w Lu C a Z : T � M Average of first Five Corrective Oct May Oct May Oct Action May Statistical Trend" 2009 2010 2010 2011 2011 Events 2014 Difference Difference Between Oct Well ID (ug/L) (ug/L) (ug/L) I (ug/L) (ug/L) (ug/L) I (ug/L) (ug/L) (%) 2009-May 2014 INJECTION WELL (IW-1) UNSUCCESSFUL INJECTION SO DOWNGRADIENT WELLS NOT SHOWN INJECTION WELL (IW-2) MONITORED DOWNGRADIENT BY MW-12S, MW-13 & MW-18 MW-12S 0.00 0.00 0.00 0.00 5.40 1.08 0.00 -1.08 -100 No Trend MW-13 61.00 50.60 74.20 87.30 72.50 69.12 20.50 -48.62 -70 Downward MW-18 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend INJECTION WELL (IW-3) MONITORED DOWNGRADIENT BY MW-3R & MW-16 MW-3R 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend MW-16 137.90 113.60 135.70 121.20 116.30 124.94 81.50 -43.44 -35 Downward INJECTION WELL (IW-4) MONITORED DOWNGRADIENT BY MW-14, MW-21 & MW-23 MW-14 15.20 15.60 15.60 8.20 17.00 14.32 0.00 -14.32 -100 No Trend MW-21 52.10 50.70 51.38 39.10 32.41 45.14 27.90 -17.24 -38 Downward MW-23 4.30 0.00 0.00 0.00 0.00 0.86 0.00 -0.86 -100 No Trend INJECTION WELL (IW-5) MONITORED DOWNGRADIENT BY MW-15 & MW-19 MW-15 96.13 63.89 55.00 78.10 64.06 71.44 58.99 -12.45 -17 No Trend MW-19 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend INJECTION WELL (IW-6) NOT SHOWN AS NO WELLS DOWNGRADIENT WITHIN ZONE OF INFLUENCE = Statistical Trend analysis via Sen's Slope Estimator at a 95% confidence level Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Figure 4 Bromide Tracer Concentrations Time Series Graph and Table February 9, 2012 — May 28, 2014 Bromide Tracer Levels in MW-16 Located 87 feet Downgradient of IW-3 which was Injected on November 2, 2011 0.3000 0.2500 3 0.2000 s J 0.1500 0.1000 0.0500 c 0.0000 ono,8\�ti o�\�o�^ti o�\�o��� ^o\^ti�o\175 Date ♦ MW-16 Date MW-16 2/9/2012 0.03800) 5/30/2012 0.13000) 8/20/2012 0.26000) 10/23/2012 0.28000) 5/30/2013 0.14000) 10/31 /2013 0.11000) 5/28/2014 0.2200 (I) Q) = The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), = May 25, 2012 Calculated date injectant expected to reach MW-16 using average flow rates of IW-3 and MW-16 (155 fdyr) since injection occurred. Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Figure 5 Total Cumulative VOC Concentrations Time Series Graphs/Table October 22, 2009 - May 28, 2014 Total Cumulative VOC Concentrations a= PQL or SWSL U-PW D. -AOC SourMrn •AOC NoMwn •AOC MW-11 -NI Weirs SOM MAOC{roW Camuh Ne VAC Concerranons-POLa SMI SOUTH M=(ToW Oiemkdn WC Cmanti m -PODa SMI IULLYR➢Tmn5n'es �xn ., kAw"T 81-4" wo� -YMIC JIMII•MY]E .M4Il � MiI�WNA3 rH+•MFfr W ,N •M ,N r 15i 17 W1.11 MMH YRt•wa AOC Well ID Oct 2009 (ug/L) May 2010 (ug/L) Oct 2010 (ug/L) May 2011 (ug/L) Oct 2011 (ug/L) Average of Preceding Five Events (ug/L) May 2014 (ug/L) Difference (ug/L) 0.00 Difference (%) Statistical Trend Between Oct 2009 - May 2014 Background MW-1 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend IW-2 (MW-2) 105.25 207.00 207.93 159.90 79.10 151.84 79.10 Ns NS NS No Trend IW-3 (MW-3RS) 202.90 127.50 127.50 144.00 127.60 145.90 127.60 Ns NS NS No Trend MW-3R 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend IW-4 (MW-4) 27.00 24.20 24.20 27.60 23.50 25.30 18.10 NS NS NS No Trend IW-5 (MW-5) 35.00 46.50 46.50 47.40 34.80 42.04 34.80 NS NS NS No Trend MW-12S 0.00 0.00 0.00 0.00 5.40 1.08 0.00 -1.08 -100 No Trend MW-12D 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend MW-13 61.00 50.60 74.20 87.30 72.50 69.12 20.50 -48.62 -70 Downward MW-14 15.20 15.60 15.60 8.20 17.00 14.32 0.00 -14.32 -100 No Trend Southern MW-15 96.13 55.00 55.00 78.10 64.06 69.66 60.80 -8.86 -13 No Trend MW-16 137.90 113.60 135.70 121.20 116.30 124.94 81.50 -43.44 -35 Downward MW-17 20.34 8.40 8.85 0.00 5.77 8.67 0.00 -8.67 -100 No Trend MW-18 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend MW-19 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend MW-21 52.10 50.70 51.38 39.10 32.41 45.14 27.90 -17.24 -38 Downward MW-22 28.90 23.80 23.80 11.66 5.20 18.67 2.40 -16.27 -87 Downward MW-23 4.30 0.00 0.00 0.00 0.00 0.86 0.00 -0.86 -100 No Trend Combined Total 786.02 722.90 770.66 724.46 583.64 717.54 452.70 -264.84 -37 Downward MW-6 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend MW-7 7.40 9.40 11.20 9.70 8.80 9.30 8.40 -0.90 -10 No Trend IW-6 (MW-8) 22.00 23.90 16.00 12.30 12.60 17.36 12.60 NS NS NS No Trend Northern MW-9 23.50 20.40 23.20 25.80 22.90 23.16 26.40 3.24 14 No Trend MW-20 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend Combined Total 52.90 53.70 50.40 47.80 44.30 49.82 47.40 -2.42 -5 No Trend MW-11 MW-11 10.10 6.00 6.00 5.44 23.20 10.15 0.00 -10.15 -100 No Trend SITEWIDE Combined Total 1849.02 782.60 827.06 777.70 651.14 777.50 500.10 -277.40 -36 Downward N5 = Not sampled this event so most recent concentration shown and used in calculations * = Statistical trend analysis via Sen's Slope Estimator at a 95% Confidence Level Surry County Closed C&D and Closed MSW LF, Mt. Airy Page 1 of 1 Tables Table 1 Sampling and Analysis Summary May 27-29, 2014 Field Parameter • • • • • • .. ©©mm©m©©©©©©©©©©©©©©©© ®W ©©mmmnn n©©©©©©©©©©©©©© App 1 & II = Appendix 1 & II List from current 40 CFR 258 E = Exempt from sampling per SWS approved SAP [18936] Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Table 2 Detections in Water Samples above SWSL, GWP, 2L or 2B (Appendix 1) May 27-29, 2014 Sample ID Parameter Name, Sample Date Result Unit z MDL 3 SWSL 5 2L, 2B 6 GWP 7 MCL 2L or GWP Exceedance Amount Preliminary Cause' MW-6 Cobalt, total 5/29/14 81 ug/L 5 10 70 NE 11 MW-7 1,4-Dichlorobenzene 5/28/14 2.7 ug/L 0.33 1 6 75 MW-7 Antimony, total 5/28/14 9.8 ug/L 5 6 1.4 NE 8.4 MW-7 Chlorobenzene 5/28/14 5.7 ug/L 0.23 3 50 100 MW-7 Cobalt, total 5/28/14 77.3 ug/L 5 10 70 NE 7.3 MW-9 1,4-Dichlorobenzene 5/28114 6.6 ug/L 0.33 1 6 75 0.6 L &/or LFG MW-9 Benzene 5/28/14 3.3 ug/L 0.25 1 1 5 2.3 L &/or LFG MW-9 cis- 1,2-Dichloroethene 5/28/14 5.7 ug/L 0.19 5 70 70 MW-9 Cobalt, total 5/28/14 140 ug/L 5 10 70 NE 70 MW-9 Vinyl chloride 5/28/14 10.8 ug/L 0.62 1 0.03 5 10.77 L &/or LFG MW-11 1,2-Dichloropropane 5/28/14 1 j ug/L 0.27 1 0.6 5 0.4 LFG MW-13 1,2-Dichloroethane 5/28114 0.47 j ug/L 0.12 1 0.4 5 0.07 L &/or LFG MW-13 cis- 1,2-Dichloroethene 5/28/14 19.3 ug/L 0.19 5 70 70 MW-13 Trichloroethene 5/28/14 1.2 ug/L 0.47 1 3 5 MW-14 Tetrachloroethene 5/28/14 0.89 j ug/L 0.46 1 0.7 5 0.19 L &/or LFG MW-15 1,1-Dichloroethane 5/28/14 14.2 ug/L 0.32 5 6 7 8.2 L &/or LFG MW-15 1,2-Dichloroethane 5/28/14 0.58 j ug/L 0.12 1 0.4 5 0.18 L &/or LFG MW-15 1,4-Dichlorobenzene 5/28/14 3.6 ug/L 0.33 1 6 75 MW-15 Benzene 5/28/14 2.3 ug/L 0.25 1 1 5 1.3 L &/or LFG MW-15 cis- 1,2-Dichloroethene 5/28/14 35.2 ug/L 0.19 5 70 70 MW-15 Tetrachloroethene 5/28/14 0.74 j ug/L 0.46 1 0.7 5 0.04 L &/or LFG MW-15 Trichloroethene 5/28/14 3.6 ug/L 0.47 1 3 5 0.6 L &/or LFG MW-15 Vinyl chloride 5/28/14 1.9 ug/L 0.62 1 0.03 5 1.87 L Wor LFG MW-16 1,2-Dichloroethane 5/28/14 2.4 ug/L 0.12 1 0.4 5 2 L &/or LFG MW-16 1,2-Dichloropropane 5/28/14 3.2 ug/L 0.27 1 0.6 5 2.6 L &/or LFG MW-16 1,4-Dichlorobenzene 5/28/14 15 ug/L 0.33 1 6 75 9 L &/or LFG MW-16 Antimony, total 5/28/14 15.9 ug/L 5 6 1.4 NE 14.5 MW-16 Barium, total 5/28/14 117 ug/L 5 100 2000 2000 MW-16 Benzene 5/28/14 1.8 ug/L 0.25 1 1 5 0.8 L &/or LFG MW-16 Chlorobenzene 5/28/14 5.8 ug/L 0.23 3 50 100 MW-16 cis- 1,2-Dichloroethene 5/28/14 46.6 ug/L 0.19 5 70 70 MW-16 Cobalt, total 5/28/14 325 ug/L 5 10 70 NE 255 MW-16 Thallium, total 5/28/14 9.5 ug/L 5.4 5.5 0.28 2 9.22 MW-16 Vinyl chloride 5/28/14 6.7 ug/L 0.62 1 0.03 5 6.67 L &/or LFG MW-16 Zinc, total 5/28/14 13.5 ug/L 10 10 1000 5000 MW-17 Cobalt, total 5/28/14 44.3 ug/L 5 10 70 NE Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 2 Sample Sample 2 3 5 6 ID Parameter Name, Date Result Unit MDL SWSL 2L^ 2B GWP MCL 2L or GWP preliminary Exceedance Cause 8 Amount MW-19 Vanadium, total 5/27/14 6.4 j ug/L 5 25 3.5 NE 2.9 MW-19 Zinc, total 5/27/14 10.1 ug/L 10 10 1000 5000 MW-20 Cobalt, total 5/27/14 14.2 ug/L 5 10 70 NE MW-21 1,1-Dichloroethane 5/28/14 6.3 ug/L 0.32 5 6 7 0.3 L &/or LFG MW-21 1,2-Dichloroethane 5/28/14 0.42 j ug/L 0.12 1 0.4 5 0.02 L &/or LFG MW-21 cis- 1,2-Dichloroethene 5/28/14 20.1 ug/L 0.19 5 70 70 MW-21 Trichloroethene 5/28/14 1.5 ug/L 0.47 1 3 5 MW-22 1,2-Dichloroethane 5/28114 0.51 j ug/L 0.12 1 0.4 5 0.11 L &/or LFG MW-22 1,4-Dichlorobenzene 5/28/14 2.4 ug/L 0.33 1 6 75 MW-22 Cobalt, total 5/28/14 37.3 ug/L 5 10 70 NE SW-2 Cobalt, total 5/28/14 20.8 ug/L 5 10 270 NE EB Methylene Chloride 5/29/14 1 j ug/L 0.97 1 4.6 5 1 Table contains Appendix I constituents detected at or above SWSL, GWP, 2L, or 213 Z MDL = Method Detection Limit ISWSL = Solid Waste Section Reporting Limit 4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard 5 213 = North Carolina 15 NCAC 26 Surface Water Quality Standard for this Specific Stream Classification 6 GWP = Groundwater Protection Standard ' MCL = Maximum Contaminant Level (Drinking Water Standard) not applicable regulatory Standard but shown for comparison purposes 8 Preliminary Cause = Refers to a preliminary analysis of the cause and/or source of a detection over the respective 2L/2B Standard. A definitive source of the detection was not determined as part of this report. j =The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable L = Leachate LFG = Landfill Gas BOLD = Concentration > 2L, or 26 Standard Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 2 of 2 Table 3 Detections in Water Samples above MDL (Appendix II Exclusive) May 27-29, 2014 Sample ID Parameter Name + Sample Result Unit MDL' SWSL' 2L4 GWP' Exceedance Preliminary Date Cause MW-6 Cyanide, total 5/29/14 8.9 j ug/L 5 10 70 MW-7 Cyanide, total 5/28/14 5.6 j ug/L 5 10 70 MW-14 Mercury 5/28/14 0.14 j ug/L 0.1 0.2 1.1 MW-16 Cyanide, total 5/28/14 11 ug/L 5 10 70 1 Table contains App II exclusive constituents detected over MDL 2 MDL = Method Detection Limit 3 SWSL = Solid Waste Section Reporting Limit 4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard e GWP = Groundwater Protection Standard Preliminary Cause = Refers to a preliminary analysis of the cause and/or source of a detection over the respective 2L/2B Standard. A definitive source of the detection was not determined as part of this report. j = The reported value is estimated & between the laboratory MDL & the SWSL, adjusted for actual sample preparation data and moisture content BOLD = Concentration >applicable 2L Standard Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Table 4 Hydrologic Properties at Monitoring Well Locations May 27-28, 2014 Monitoring Well Hydraulic Conductivity (cm/second) Effective Porosity (°�0) Hydraulic Gradient (feet/feet) Groundwater Average Linear Velocity Rate (feet/year) Flow Direction Groundwater Depth (feet btoc) Groundwater Potentiometric Elevation (feet amsl) Screened Interval Lithology MW-1 4.30E-05 15 0.083 25 S18W 24.80 1109.55 Clay IW-2 4.30E-05 15 0.024 7 S76E 39.61 1029.25 Clay MW-7 8.10E-04 15 0.319 1,785 N84W 11.81 1061.69 PWR/Fractured Rock IW-6 4.40E-04 15 0.113 342 S14E 40.98 1047.47 PWR/Fractured Rock MW-9 1.90E-04 15 0.038 50 S53E 32.99 1061.08 Sandy Silt MW-13 2.06E-04 23 0.063 59 S36E 25.23 983.25 Saprolite MW-18 2.04E-03 15 0.117 na S39E 9.17 973.83 Saprolite MW-19 1.10E-03 3 0.093 3,519 S14W 9.84 936.43 PWR MW-21 1.28E-03 3 0.033 1,453 S55E 5.44 959.92 Saprolite/PWR MW-22 9.88E-04 15 0.120 821 S29W 5.22 948.18 Saprolite MW-23 3.04E-04 15 0.154 324 S40E 7.39 947.92 Sandy Silt Minimum 4.30E-05 3 0.024 7 - 5.22 936.43 - Average 6.77E-04 14 0.105 838 - 19.32 1005.32 - Maximum 2.04E-03 23 0.319 3,519 - 40.98 1109.55 - MW-3R 2.40E-04 5 na na na 40.77 976.73 Fractured Rock IW-3 2.40E-05 5 0.028 14 S40W 30.95 989.62 Fractured Rock IW-4 1.10E-04 5 0.205 466 S41 E 33.94 992.32 Fractured Rock IW-5 1.50E-05 5 0.161 50 S63W 39.94 1040.24 Fractured Rock MW-6 1.90E-05 5 0.191 75 S80W 22.38 1045.29 Fractured Rock MW-11 3.10E-04 5 0.088 563 S20W 21.39 1130.41 Fractured Rock MW-12S na 3 0.104 na SO4W 13.38 1012.42 Fractured Rock MW-12D 1.30E-06 5 na na na 0.00 1027.05 Fractured Rock MW-14 7.45E-03 3 0.305 78,438 S72E 35.39 983.41 Fractured Rock MW-15 7.21 E-05 3 0.190 473 S06W 51.12 1024.84 Fractured Rock MW-16 2.82E-05 3 0.157 152 S40W 25.69 973.85 Fractured Rock MW-17 2.94E-04 3 0.102 1,031 S64W 8.39 957.04 Rock MW-20 1.92E-04 3 0.107 707 S03E 19.41 1062.78 Rock Minimum 1.30E-06 3 0.028 14 - 0.00 957.04 - Average 7.30E-04 4 0.149 392 - 26.37 1016.62 - Maximum 7.45E-03 5 0.305 1,031 - 51.12 1130.41 - NOTE: Values for hydraulic conductivity determined via slug test by GAI, MESCO, or Joyce. Hydrologic gradient from water levels recorded on May 27-28, 2014. Wells screened entirely in rock were not utilized for flow directions/gradients. Screens that traverse both rock and regolith assumed flow in regolith dominates. Flow rate for MW-14 was considered an outlier; therefore not included in the average or maximum. na = Not available/applicable Average Linear Velocity (Q) is defined by modified Darcy's equation: K A K= hydraulic conductivity where Q - - n - dl ne= effective porosity dh= head difference dl= horizontal distance Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Table 5 Field Observations of Monitoring Locations May 27-29, 2014 Viable Lack of Any Locked on Hinge/Hasp Tagged Concrete Surface Pad Location Monitoring Evidence of Arrival & Operational or Appears Comments Location Tampering Departure Labeled Effective MW-1 Yes Yes Yes Yes Yes Yes IW-1 No Yes Yes Yes Yes Yes Fouled since injection 11/2/11. IW-2 (was MW-2) No Yes Yes Yes Yes Yes Fouled since injection 11/2/11. MW-3R Yes Yes Yes Yes Yes Yes IW-3 (was MW-3RS) No Yes Yes Yes Yes Yes Fouled since injection 11/2/11. IW-4 (was MW-4) No Yes Yes Yes Yes Yes Fouled since injection 10/24/12. IW-5 (was MW-5) No Yes Yes Yes Yes Yes Fouled since injection 11/2/11. Bailer would not descend MW-6 Yes Yes Yes Yes Yes Yes MW-7 Yes Yes Yes Yes Yes Yes IW-6 (was MW-8) No Yes Yes Yes Yes Yes Fouled since injection 10/24/12. MW-9 Yes Yes Yes Yes Yes Yes MW-11 Yes Yes Yes Yes Yes Yes MW-12S Yes Yes Yes Yes Yes Yes Slow recharge MW-12D Yes Yes Yes Yes Yes Yes Artesian & very slow recharge MW-13 Yes Yes Yes Yes Yes Yes MW-14 Yes Yes Yes Yes Yes Yes MW-15 Yes Yes Yes Yes Yes Yes MW-16 Yes Yes Yes Yes Yes Yes Red algae in purge water MW-17 Yes Yes Yes Yes Yes Yes MW-18 Yes Yes Yes Yes Yes Yes MW-19 Yes Yes Yes Yes Yes Yes MW-20 Yes Yes Yes Yes Yes Yes Purged dry for 2nd consecutive event which is atypical for this well MW-21 Yes Yes Yes Yes Yes Yes MW-22 Yes Yes Yes Yes Yes Yes MW-23 Yes Yes Yes Yes Yes Yes SW-1 Yes Moderate gage height & flow SW-2 Yes Moderate gage height & flow SW-3 Yes Moderate gage height & flow SW-4 Yes Moderate gage height & flow SWN-1 Yes Moderate gage height & flow SWN-2 Yes Moderate gage height & flow SCALEHOUSE Yes Sample from spigot next to well which is Any unusual field conditions, observations, or events: Injection wells (IW-1, IW-2, IW-3, IW-4, IW-5 and IW-6) exempt from laboratory analysis as SWS approved on May 10, 2013 (DIN:18938) Stormwater control improvements performed since May 2012 event. Visual markers (10 ft PVC pipes) secured to each monitoring well case. Locks lubricated with vegetable oil spray after work at each well completed. Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Table 6 Field Parameter Data Summary May 27-28, 2014 Depth to Water TOC Specific Parameter Water" Elevation Elevation Temp. ORP DO pH Conductance TDS Turbidity Units ft (btoc) ft (amsl) ft (amsl) C mV mg/L SU umhos/cm mg/L Visual or NTU MW-1 24.80 1109.55 1134.35 14.8 201 2.3 6.03 300 140 16.2 IW-2 39.61 1029.25 1068.86 NR NR NR NR NR NR >1000 MW-3R 30.95 986.55 1017.50 15.2 119 0.5 7.82 200 90 Clear IW-3 40.77 979.80 1020.57 NR NR NR NR NR NR >1000 IW-4 33.94 992.32 1026.26 NR NR NR NR NR NR >1000 IW-5 39.94 1040.24 1080.18 NR NR NR NR NR NR >1000 MW-6 22.38 1045.29 1067.67 13.9 -23 1.1 6.35 500 240 Slight MW-7 11.81 1061.69 1073.50 14.6 201 2.6 5.43 330 160 18.1 IW-6 40.98 1047.47 1088.45 NR NR NR NR NR NR >1000 MW-9 32.99 1061.08 1094.07 15.9 30 0.1 6.27 480 240 13.1 MW-11 21.39 1130.41 1151.80 16.5 152 0.8 4.85 120 60 12.9 MW-12S 13.38 1012.42 1025.80 14.0 60 3.3 7.26 410 200 Clear MW-12D 0.00 1027.05 1027.05 14.1 -91 1.4 7.35 160 120 Clear MW-13 25.23 983.25 1008.48 14.6 206 2.3 5.30 250 120 Clear MW-14 35.39 983.41 1018.80 14.3 21 2.2 5.26 100 50 20.1 MW-15 51.12 1024.84 1075.96 14.8 27 0.4 5.32 140 70 >1000 MW-16 25.69 973.85 999.54 16.0 82 0.6 5.74 520 250 Clear MW-17 8.39 957.04 965.43 13.1 78 1.4 6.05 310 150 Clear MW-18 9.17 973.83 983.00 13.0 191 6.3 5.81 30 10 Slight MW-19 9.84 936.43 946.27 13.1 273 3.0 5.52 50 30 Slight MW-20 19.41 1062.78 1082.19 13.4 201 1.2 5.38 80 40 Clear MW-21 5.44 959.92 965.36 13.7 203 1.9 5.01 210 100 163 MW-22 5.22 948.18 953.40 16.4 233 4.1 5.83 280 140 Clear MW-23 7.39 947.92 955.31 14.7 211 4.3 6.98 100 40 Clear Scalehouse na na na 14.9 179 4.7 7.03 910 440 Clear Minimum Average Maximum 0.00 936.43 946.27 13.0 23.13 1011.44 1034.58 14.6 51.12 1130.41 1151.80 16.5 -91 128 273 0.1 2.2 6.3 4.85 6.03 7.82 30 274 910 10 135 440 12.90 Slight >1000 SW-1 - - - 16.4 NR NR 6.81 70 30 Clear SW-2 - - - 16.3 NR NR 7.03 220 100 Clear SW-3 - - - 17.1 NR NR 6.89 280 130 Clear SW-4 - - - 18.5 NR NR 6.95 80 40 Clear SWN-1 - - - 18.1 NR NR 7.11 100 50 Clear SWN-2 - - - 17.3 NR NR 7.47 70 30 Clear Minimum - - - 16.3 NR NR 6.81 70 30 Clear Average - - - 17.3 NR NR 7.04 137 63 Clear Maximum - - - 18.5 NR NR 7.47 280 130 Clear btoc = Below top of casing amsl = Above mean sea level na = Not available NR = No reading attempted Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Table 7 MNA Parameter Data Summary May 28, 2014 Parameters Method MDL* Units MW-1 MW-7 MW-9 MW-11 MW-14 MW-15 MW-21 5/28/14 5/28/14 5/28/14 5/28/14 5/28/14 5/28/14 5/28/14 VFA — Acetic Acid AM23G NS ug/L NS NS NS NS NS NS NS VFA — Butyric Acid AM23G NS ug/L NS NS NS NS NS NS NS VFA — Lactic Acid AM23G NS ug/L NS NS NS NS NS NS NS VFA — Propionic Acid AM23G NS ug/L NS NS NS NS NS NS NS VFA — Pyruvic Acid AM23G NS ug/L NS NS NS NS NS NS NS Hydrogen AM20GAX NS nM NS NS NS NS NS NS NS Methane RSK175 400 ug/L <400 93500 1530000 21 164000 5.25 1570 95700021 <400 Ethene AM20GAX NS ug/L NS NS NS NS NS NS NS Ethane AM20GAX NS ug/L NS NS NS NS NS NS NS CO2-Dissolved Field HACH Kit NS mg/L NS NS NS NS NS NS NS Alkalinity SM 2320B 1000 ug/L 81500 79100 112000 NS 32400 44000 34500 Sulfate EPA 300.0 2000 ug/L 7940 6570 <2000 NS 2210 <2000 <2000 Sulfide SM 4500-S21D 100 ug/L <100 <100 <100 NS <100 <100 <100 Chloride SM 4500-CI-E 1000 ug/L 3270 288002 45100 5 NS 2710 1890 27600 TOC SM 5310B 1000 ug/L 2960 13900 8070 NS 5660 86705 10700 COD SM 5220D 25000 ug/L <25000 35000 33000 NS <25000 <25000 <25000 BOD SM5210B NS ug/L NS NS NS NS NS NS NS Iron EPA 6010 50 ug/L 167 <50 44900 NS 245 2640 <50 Nitrate EPA 353.2 <20 ug/L NS NS NS NS NS NS NS Temperature Field Instrument 0 C 14.8 2.6 15.9 16.5 14.3 14.8 13.7 ORP Field Instrument -900 mV 201 201 30 152 21 27 203 DO Field Instrument 0 mg/L 2.3 2.6 0.8 0.8 2.2 0.4 1.9 pH Field Instrument 0 SU 6.03 5.43 6.27 4.85 5.26 5.32 5.01 Specific Conductance Field Instrument 0 us/cm 300 330 480 120 100 140 210 Turbidity Field Instrument 0 NTU 16.2 18.1 13.1 12.9 20.1 >1000 163 Notes: MDL' = Lab Method Detection Limit or lowest field measurement possible. Constituents detected below quantifiable limits are shown as < MDL value. >100 = CO2 Concentration exceeds maximum capability of method used. 5 Indicates dilution factor used NS = Not Sampled Surry County Closed C&D and CLosed MSWLF, Mt. Airy Page 1 of 1 Appendix A Laboratory Analysis Reports Chains of Custody aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 June 09, 2014 Mr. Jonathan Pfohl Municipal Engineering Services PO Box 97 Garner, NC 27529 RE: Project: SURRY CLOSED - MT AIRY (AM) Pace Project No.: 92203116 Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory between May 28, 2014 and May 29, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Godwin kevin.godwin@pacelabs.com Project Manager Enclosures Q _Kok r REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 Project: SURRY CLOSED - MT AIRY (AM) Pace Project No.: 92203116 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 SAMPLE SUMMARY Project: SURRY CLOSED - MT AIRY (AM) Pace Project No.: 92203116 Lab ID Sample ID Matrix Date Collected Date Received 92203116001 MW-12D Water 05/27/1414:05 05/28/1417:00 92203116002 SCALEHOUSE Water 05/27/1417:35 05/28/1417:00 92203116003 MW-6 Water 05/29/1412:25 05/29/1415:20 92203116004 MW-11 Water 05/28/1416:45 05/29/1415:20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: SURRY CLOSED - MT AIRY (AM) 92203116 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92203116001 MW-12D EPA 6010 JMW 15 PASI-A EPA 8260 MCK 51 PASI-C 92203116002 SCALEHOUSE EPA 6010 JMW 15 PASI-A EPA 8260 MCK 51 PASI-C 92203116003 MW-6 EPA 6010 JMW 16 PASI-A EPA 7470 MTS 1 PASI-A EPA 8260 NU1 51 PASI-C SM 4500-CN-E JDA 1 PASI-A 92203116004 MW-11 EPA 6010 JMW 15 PASI-A EPA 7470 MTS 1 PASI-A EPA 8260 NU1 51 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED - MT AIRY (AM) Pace Project No.: 92203116 Sample: MW-12D Lab ID: 92203116001 Collected: 05/27/14 14:05 Received: 05/28/14 17:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 5.0 1 05/29/14 15:55 05/30/14 19:47 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 19:47 7440-38-2 Barium 6.1J ug/L 100 5.0 1 05/29/14 15:55 05/30/14 19:47 7440-39-3 Beryllium ND ug/L 1.0 1.0 1 05/29/14 15:55 05/30/14 19:47 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 05/29/14 15:55 05/30/14 19:47 7440-43-9 Chromium ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 19:47 7440-47-3 Cobalt ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 19:47 7440-48-4 Copper ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 19:47 7440-50-8 Lead ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 19:47 7439-92-1 Nickel ND ug/L 50.0 5.0 1 05/29/14 15:55 05/30/14 19:47 7440-02-0 Selenium ND ug/L 10.0 10.0 1 05/29/14 15:55 05/30/14 19:47 7782-49-2 Silver ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 19:47 7440-22-4 Thallium ND ug/L 5.5 5.4 1 05/29/14 15:55 05/30/14 19:47 7440-28-0 Vanadium ND ug/L 25.0 5.0 1 05/29/14 15:55 05/30/14 19:47 7440-62-2 Zinc ND ug/L 10.0 10.0 1 05/29/14 15:55 05/30/14 19:47 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 05/29/14 23:19 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 05/29/14 23:19 107-13-1 Benzene ND ug/L 1.0 0.25 1 05/29/14 23:19 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 05/29/14 23:19 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 05/29/14 23:19 75-27-4 Bromoform ND ug/L 3.0 0.26 1 05/29/14 23:19 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 05/29/14 23:19 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 05/29/14 23:19 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 05/29/14 23:19 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 05/29/14 23:19 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 05/29/14 23:19 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 05/29/14 23:19 75-00-3 Chloroform ND ug/L 5.0 0.14 1 05/29/14 23:19 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 05/29/14 23:19 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 05/29/14 23:19 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 05/29/14 23:19 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 05/29/14 23:19 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 05/29/14 23:19 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 05/29/14 23:19 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 05/29/14 23:19 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 05/29/14 23:19 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 05/29/14 23:19 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 05/29/14 23:19 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 05/29/14 23:19 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 05/29/14 23:19 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 05/29/14 23:19 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 05/29/14 23:19 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 05/29/14 23:19 142-28-9 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 05/29/14 23:19 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2014 02:31 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED - MT AIRY (AM) Pace Project No.: 92203116 Sample: MW-12D Lab ID: 92203116001 Collected: 05/27/14 14:05 Received: 05/28/14 17:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 05/29/14 23:19 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 05/29/14 23:19 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 05/29/14 23:19 591-78-6 lodomethane ND ug/L 10.0 0.32 1 05/29/14 23:19 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 05/29/14 23:19 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 05/29/14 23:19 108-10-1 Styrene ND ug/L 1.0 0.26 1 05/29/14 23:19 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 05/29/14 23:19 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 05/29/14 23:19 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 05/29/14 23:19 127-18-4 Toluene ND ug/L 1.0 0.26 1 05/29/14 23:19 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 05/29/14 23:19 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 05/29/14 23:19 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 05/29/14 23:19 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 05/29/14 23:19 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 05/29/14 23:19 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 05/29/14 23:19 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 05/29/14 23:19 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 05/29/14 23:19 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 05/29/14 23:19 460-00-4 1,2-Dichloroethane-d4 (S) 100 % 70-130 1 05/29/14 23:19 17060-07-0 Toluene-d8 (S) 98 % 70-130 1 05/29/14 23:19 2037-26-5 Date: 06/09/2014 02:31 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED - MT AIRY (AM) Pace Project No.: 92203116 Sample: SCALEHOUSE Lab ID: 92203116002 Collected: 05/27/14 17:35 Received: 05/28/14 17:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 5.0 1 05/29/14 15:55 05/30/14 19:56 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 19:56 7440-38-2 Barium 11.6J ug/L 100 5.0 1 05/29/14 15:55 05/30/14 19:56 7440-39-3 Beryllium ND ug/L 1.0 1.0 1 05/29/14 15:55 05/30/14 19:56 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 05/29/14 15:55 05/30/14 19:56 7440-43-9 Chromium ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 19:56 7440-47-3 Cobalt ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 19:56 7440-48-4 Copper ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 19:56 7440-50-8 Lead ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 19:56 7439-92-1 Nickel ND ug/L 50.0 5.0 1 05/29/14 15:55 05/30/14 19:56 7440-02-0 Selenium ND ug/L 10.0 10.0 1 05/29/14 15:55 05/30/14 19:56 7782-49-2 Silver ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 19:56 7440-22-4 Thallium ND ug/L 5.5 5.4 1 05/29/14 15:55 05/30/14 19:56 7440-28-0 Vanadium ND ug/L 25.0 5.0 1 05/29/14 15:55 05/30/14 19:56 7440-62-2 Zinc ND ug/L 10.0 10.0 1 05/29/14 15:55 05/30/14 19:56 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 05/29/14 23:35 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 05/29/14 23:35 107-13-1 Benzene ND ug/L 1.0 0.25 1 05/29/14 23:35 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 05/29/14 23:35 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 05/29/14 23:35 75-27-4 Bromoform ND ug/L 3.0 0.26 1 05/29/14 23:35 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 05/29/14 23:35 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 05/29/14 23:35 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 05/29/14 23:35 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 05/29/14 23:35 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 05/29/14 23:35 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 05/29/14 23:35 75-00-3 Chloroform ND ug/L 5.0 0.14 1 05/29/14 23:35 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 05/29/14 23:35 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 05/29/14 23:35 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 05/29/14 23:35 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 05/29/14 23:35 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 05/29/14 23:35 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 05/29/14 23:35 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 05/29/14 23:35 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 05/29/14 23:35 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 05/29/14 23:35 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 05/29/14 23:35 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 05/29/14 23:35 75-35-4 cis-1,2-Dichloroethene 0.26J ug/L 5.0 0.19 1 05/29/14 23:35 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 05/29/14 23:35 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 05/29/14 23:35 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 05/29/14 23:35 142-28-9 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 05/29/14 23:35 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2014 02:31 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED - MT AIRY (AM) Pace Project No.: 92203116 Sample: SCALEHOUSE Lab ID: 92203116002 Collected: 05/27/14 17:35 Received: 05/28/14 17:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 05/29/14 23:35 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 05/29/14 23:35 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 05/29/14 23:35 591-78-6 lodomethane ND ug/L 10.0 0.32 1 05/29/14 23:35 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 05/29/14 23:35 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 05/29/14 23:35 108-10-1 Styrene ND ug/L 1.0 0.26 1 05/29/14 23:35 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 05/29/14 23:35 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 05/29/14 23:35 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 05/29/14 23:35 127-18-4 Toluene ND ug/L 1.0 0.26 1 05/29/14 23:35 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 05/29/14 23:35 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 05/29/14 23:35 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 05/29/14 23:35 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 05/29/14 23:35 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 05/29/14 23:35 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 05/29/14 23:35 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 05/29/14 23:35 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 05/29/14 23:35 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 95 % 70-130 1 05/29/14 23:35 460-00-4 1,2-Dichloroethane-d4 (S) 100 % 70-130 1 05/29/14 23:35 17060-07-0 Toluene-d8 (S) 97 % 70-130 1 05/29/14 23:35 2037-26-5 Date: 06/09/2014 02:31 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 8 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED - MT AIRY (AM) Pace Project No.: 92203116 Sample: MW-6 Lab ID: 92203116003 Collected: 05/29/14 12:25 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Tin Vanadium Zinc 7470 Mercury Mercury 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene Date: 06/09/2014 02:31 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010 ND ug/L 6.0 5.0 1 06/03/14 12:30 06/05/14 23:51 7440-36-0 ND ug/L 10.0 5.0 1 06/03/14 12:30 06/05/14 23:51 7440-38-2 91.6J ug/L 100 5.0 1 06/03/14 12:30 06/05/14 23:51 7440-39-3 ND ug/L 1.0 1.0 1 06/03/14 12:30 06/05/14 23:51 7440-41-7 ND ug/L 1.0 1.0 1 06/03/14 12:30 06/05/14 23:51 7440-43-9 ND ug/L 10.0 5.0 1 06/03/14 12:30 06/05/14 23:51 7440-47-3 81.0 ug/L 10.0 5.0 1 06/03/14 12:30 06/05/14 23:51 7440-48-4 ND ug/L 10.0 5.0 1 06/03/14 12:30 06/05/14 23:51 7440-50-8 ND ug/L 10.0 5.0 1 06/03/14 12:30 06/05/14 23:51 7439-92-1 ND ug/L 50.0 5.0 1 06/03/14 12:30 06/05/14 23:51 7440-02-0 ND ug/L 10.0 10.0 1 06/03/14 12:30 06/05/14 23:51 7782-49-2 ND ug/L 10.0 5.0 1 06/03/14 12:30 06/05/14 23:51 7440-22-4 ND ug/L 5.5 5.4 1 06/03/14 12:30 06/05/14 23:51 7440-28-0 ND ug/L 100 5.0 1 06/03/14 12:30 06/05/14 23:51 7440-31-5 ND ug/L 25.0 5.0 1 06/03/14 12:30 06/05/14 23:51 7440-62-2 ND ug/L 10.0 10.0 1 06/03/14 12:30 06/05/14 23:51 7440-66-6 Analytical Method: EPA 7470 Preparation Method: EPA 7470 ND ug/L 0.20 0.10 1 06/02/14 19:30 06/04/14 13:40 7439-97-6 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 05/31/14 01:54 67-64-1 ND ug/L 200 1.9 1 05/31/14 01:54 107-13-1 0.42J ug/L 1.0 0.25 1 05/31/14 01:54 71-43-2 ND ug/L 3.0 0.17 1 05/31/14 01:54 74-97-5 ND ug/L 1.0 0.18 1 05/31/14 01:54 75-27-4 ND ug/L 3.0 0.26 1 05/31/14 01:54 75-25-2 ND ug/L 10.0 0.29 1 05/31/14 01:54 74-83-9 ND ug/L 100 0.96 1 05/31/14 01:54 78-93-3 ND ug/L 100 1.2 1 05/31/14 01:54 75-15-0 ND ug/L 1.0 0.25 1 05/31/14 01:54 56-23-5 0.38J ug/L 3.0 0.23 1 05/31/14 01:54 108-90-7 ND ug/L 10.0 0.54 1 05/31/14 01:54 75-00-3 ND ug/L 5.0 0.14 1 05/31/14 01:54 67-66-3 ND ug/L 1.0 0.11 1 05/31/14 01:54 74-87-3 ND ug/L 13.0 2.5 1 05/31/14 01:54 96-12-8 ND ug/L 3.0 0.21 1 05/31/14 01:54 124-48-1 ND ug/L 1.0 0.27 1 05/31/14 01:54 106-93-4 ND ug/L 10.0 0.21 1 05/31/14 01:54 74-95-3 ND ug/L 5.0 0.30 1 05/31/14 01:54 95-50-1 0.42J ug/L 1.0 0.33 1 05/31/14 01:54 106-46-7 ND ug/L 100 1.0 1 05/31/14 01:54 110-57-6 ND ug/L 5.0 0.32 1 05/31/14 01:54 75-34-3 ND ug/L 1.0 0.12 1 05/31/14 01:54 107-06-2 ND ug/L 5.0 0.56 1 05/31/14 01:54 75-35-4 ND ug/L 5.0 0.19 1 05/31/14 01:54 156-59-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 9 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED - MT AIRY (AM) Pace Project No.: 92203116 Sample: MW-6 Lab ID: 92203116003 Collected: 05/29/14 12:25 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 450OCNE Cyanide, Total Cyanide Date: 06/09/2014 02:31 PM Analytical Method: EPA 8260 ND ug/L 5.0 0.49 1 05/31/14 01:54 156-60-5 ND ug/L 1.0 0.27 1 05/31/14 01:54 78-87-5 ND ug/L 1.0 0.28 1 05/31/14 01:54 142-28-9 ND ug/L 1.0 0.13 1 05/31/14 01:54 10061-01-5 ND ug/L 1.0 0.26 1 05/31/14 01:54 10061-02-6 ND ug/L 1.0 0.30 1 05/31/14 01:54 100-41-4 ND ug/L 50.0 0.46 1 05/31/14 01:54 591-78-6 ND ug/L 10.0 0.32 1 05/31/14 01:54 74-88-4 ND ug/L 1.0 0.97 1 05/31/14 01:54 75-09-2 ND ug/L 100 0.33 1 05/31/14 01:54 108-10-1 ND ug/L 1.0 0.26 1 05/31/14 01:54 100-42-5 ND ug/L 5.0 0.33 1 05/31/14 01:54 630-20-6 ND ug/L 3.0 0.40 1 05/31/14 01:54 79-34-5 ND ug/L 1.0 0.46 1 05/31/14 01:54 127-18-4 ND ug/L 1.0 0.26 1 05/31/14 01:54 108-88-3 ND ug/L 1.0 0.48 1 05/31/14 01:54 71-55-6 ND ug/L 1.0 0.29 1 05/31/14 01:54 79-00-5 ND ug/L 1.0 0.47 1 05/31/14 01:54 79-01-6 ND ug/L 1.0 0.20 1 05/31/14 01:54 75-69-4 ND ug/L 1.0 0.41 1 05/31/14 01:54 96-18-4 ND ug/L 50.0 0.35 1 05/31/14 01:54 108-05-4 ND ug/L 1.0 0.62 1 05/31/14 01:54 75-01-4 ND ug/L 5.0 0.66 1 05/31/14 01:54 1330-20-7 99 % 70-130 1 05/31/14 01:54 460-00-4 99 % 70-130 1 05/31/14 01:54 17060-07-0 99 % 70-130 1 05/31/14 01:54 2037-26-5 Analytical Method: SM 4500-CN-E 8.9J ug/L 10.0 5.0 1 06/09/14 11:10 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED - MT AIRY (AM) Pace Project No.: 92203116 Sample: MW-11 Lab ID: 92203116004 Collected: 05/28/14 16:45 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 5.0 1 06/03/14 12:30 06/05/14 23:54 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/03/14 12:30 06/05/14 23:54 7440-38-2 Barium 31.3J ug/L 100 5.0 1 06/03/14 12:30 06/05/14 23:54 7440-39-3 Beryllium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/05/14 23:54 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/05/14 23:54 7440-43-9 Chromium ND ug/L 10.0 5.0 1 06/03/14 12:30 06/05/14 23:54 7440-47-3 Cobalt 9.5J ug/L 10.0 5.0 1 06/03/14 12:30 06/05/14 23:54 7440-48-4 Copper ND ug/L 10.0 5.0 1 06/03/14 12:30 06/05/14 23:54 7440-50-8 Lead ND ug/L 10.0 5.0 1 06/03/14 12:30 06/05/14 23:54 7439-92-1 Nickel ND ug/L 50.0 5.0 1 06/03/14 12:30 06/05/14 23:54 7440-02-0 Selenium ND ug/L 10.0 10.0 1 06/03/14 12:30 06/05/14 23:54 7782-49-2 Silver ND ug/L 10.0 5.0 1 06/03/14 12:30 06/05/14 23:54 7440-22-4 Thallium ND ug/L 5.5 5.4 1 06/03/14 12:30 06/05/14 23:54 7440-28-0 Vanadium ND ug/L 25.0 5.0 1 06/03/14 12:30 06/05/14 23:54 7440-62-2 Zinc ND ug/L 10.0 10.0 1 06/03/14 12:30 06/05/14 23:54 7440-66-6 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury ND ug/L 0.20 0.10 1 06/02/14 19:30 06/04/14 13:42 7439-97-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 05/31/14 02:10 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 05/31/14 02:10 107-13-1 Benzene ND ug/L 1.0 0.25 1 05/31/14 02:10 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 05/31/14 02:10 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 05/31/14 02:10 75-27-4 Bromoform ND ug/L 3.0 0.26 1 05/31/14 02:10 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 05/31/14 02:10 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 05/31/14 02:10 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 05/31/14 02:10 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 05/31/14 02:10 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 05/31/14 02:10 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 05/31/14 02:10 75-00-3 Chloroform ND ug/L 5.0 0.14 1 05/31/14 02:10 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 05/31/14 02:10 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 05/31/14 02:10 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 05/31/14 02:10 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 05/31/14 02:10 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 05/31/14 02:10 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 05/31/14 02:10 95-50-1 1,4-Dichlorobenzene 0.55J ug/L 1.0 0.33 1 05/31/14 02:10 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 05/31/14 02:10 110-57-6 1,1-Dichloroethane 0.53J ug/L 5.0 0.32 1 05/31/14 02:10 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 05/31/14 02:10 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 05/31/14 02:10 75-35-4 cis-1,2-Dichloroethene 1.3J ug/L 5.0 0.19 1 05/31/14 02:10 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 05/31/14 02:10 156-60-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2014 02:31 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED - MT AIRY (AM) Pace Project No.: 92203116 Sample: MW-11 Lab ID: 92203116004 Collected: 05/28/14 16:45 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 1,2-Dichloropropane 1.OJ ug/L 1.0 0.27 1 05/31/14 02:10 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 05/31/14 02:10 142-28-9 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 05/31/14 02:10 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 05/31/14 02:10 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 05/31/14 02:10 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 05/31/14 02:10 591-78-6 lodomethane ND ug/L 10.0 0.32 1 05/31/14 02:10 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 05/31/14 02:10 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 05/31/14 02:10 108-10-1 Styrene ND ug/L 1.0 0.26 1 05/31/14 02:10 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 05/31/14 02:10 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 05/31/14 02:10 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 05/31/14 02:10 127-18-4 Toluene ND ug/L 1.0 0.26 1 05/31/14 02:10 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 05/31/14 02:10 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 05/31/14 02:10 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 05/31/14 02:10 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 05/31/14 02:10 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 05/31/14 02:10 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 05/31/14 02:10 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 05/31/14 02:10 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 05/31/14 02:10 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 05/31/14 02:10 460-00-4 1,2-Dichloroethane-d4 (S) 95 % 70-130 1 05/31/14 02:10 17060-07-0 Toluene-d8 (S) 99 % 70-130 1 05/31/14 02:10 2037-26-5 Date: 06/09/2014 02:31 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 12 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED - MT AIRY (AM) Pace Project No.: 92203116 QC Batch: MERP/6688 Analysis Method: EPA 7470 QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury Associated Lab Samples: 92203116003, 92203116004 METHOD BLANK: 1212160 Matrix: Water Associated Lab Samples: 92203116003, 92203116004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury ug/L ND 0.20 06/04/1412:31 LABORATORY CONTROL SAMPLE: 1212161 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.4 94 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1212162 1212163 MS MSD 92203313004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Mercury ug/L ND 2.5 2.5 1.3 1.2 53 48 75-125 9 25 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2014 02:31 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED - MT AIRY (AM) Pace Project No.: 92203116 QC Batch: MPRP/16067 Analysis Method: EPA6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET NC Groundwater Associated Lab Samples: 92203116001, 92203116002 METHOD BLANK: 1208932 Associated Lab Samples: 92203116001, 92203116002 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed Antimony ug/L ND 6.0 05/30/1419:41 Arsenic ug/L ND 10.0 05/30/1419:41 Barium ug/L ND 100 05/30/1419:41 Beryllium ug/L ND 1.0 05/30/1419:41 Cadmium ug/L ND 1.0 05/30/1419:41 Chromium ug/L ND 10.0 05/30/1419:41 Cobalt ug/L ND 10.0 05/30/1419:41 Copper ug/L ND 10.0 05/30/1419:41 Lead ug/L ND 10.0 05/30/1419:41 Nickel ug/L ND 50.0 05/30/1419:41 Selenium ug/L ND 10.0 05/30/1419:41 Silver ug/L ND 10.0 05/30/1419:41 Thallium ug/L ND 5.5 05/30/1419:41 Vanadium ug/L ND 25.0 05/30/1419:41 Zinc ug/L ND 10.0 05/30/1419:41 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 1208933 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 500 492 98 80-120 Arsenic ug/L 500 467 93 80-120 Barium ug/L 500 483 97 80-120 Beryllium ug/L 500 451 90 80-120 Cadmium ug/L 500 466 93 80-120 Chromium ug/L 500 465 93 80-120 Cobalt ug/L 500 480 96 80-120 Copper ug/L 500 466 93 80-120 Lead ug/L 500 475 95 80-120 Nickel ug/L 500 463 93 80-120 Selenium ug/L 500 480 96 80-120 Silver ug/L 250 234 93 80-120 Thallium ug/L 500 458 92 80-120 Vanadium ug/L 500 457 91 80-120 Zinc ug/L 500 457 91 80-120 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2014 02:31 PM without the written consent of Pace Analytical Services, Inc.. Page 14 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: SURRY CLOSED - MT AIRY (AM) 92203116 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1208934 1208935 MS MSD 92203116001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 507 509 101 102 75-125 0 25 Arsenic ug/L ND 500 500 480 485 96 97 75-125 1 25 Barium ug/L 6.1J 500 500 494 501 98 99 75-125 2 25 Beryllium ug/L ND 500 500 461 469 92 94 75-125 2 25 Cadmium ug/L ND 500 500 477 481 95 96 75-125 1 25 Chromium ug/L ND 500 500 472 484 94 97 75-125 2 25 Cobalt ug/L ND 500 500 482 490 96 98 75-125 2 25 Copper ug/L ND 500 500 478 485 96 97 75-125 1 25 Lead ug/L ND 500 500 476 485 95 97 75-125 2 25 Nickel ug/L ND 500 500 467 475 93 95 75-125 2 25 Selenium ug/L ND 500 500 487 493 97 99 75-125 1 25 Silver ug/L ND 250 250 238 241 95 96 75-125 1 25 Thallium ug/L ND 500 500 465 472 93 94 75-125 2 25 Vanadium ug/L ND 500 500 467 478 93 96 75-125 2 25 Zinc ug/L ND 500 500 460 471 92 94 75-125 2 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2014 02:31 PM without the written consent of Pace Analytical Services, Inc.. Page 15 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED - MT AIRY (AM) Pace Project No.: 92203116 QC Batch: MPRP/16106 Analysis Method: EPA6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET NC Groundwater Associated Lab Samples: 92203116003, 92203116004 METHOD BLANK: 1212509 Associated Lab Samples: 92203116003, 92203116004 Parameter Units Antimony ug/L Arsenic ug/L Barium ug/L Beryllium ug/L Cadmium ug/L Chromium ug/L Cobalt ug/L Copper ug/L Lead ug/L Nickel ug/L Selenium ug/L Silver ug/L Thallium ug/L Tin ug/L Vanadium ug/L Zinc ug/L Matrix: Water Blank Result Reporting Limit Analyzed ND 6.0 06/05/14 22:14 ND 10.0 06/05/14 22:14 ND 100 06/05/14 22:14 ND 1.0 06/05/14 22:14 ND 1.0 06/05/14 22:14 ND 10.0 06/05/14 22:14 ND 10.0 06/05/14 22:14 ND 10.0 06/05/14 22:14 ND 10.0 06/05/14 22:14 ND 50.0 06/05/14 22:14 ND 10.0 06/05/14 22:14 ND 10.0 06/05/14 22:14 ND 5.5 06/05/14 22:14 ND 100 06/05/14 22:14 ND 25.0 06/05/14 22:14 ND 10.0 06/05/14 22:14 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 1212510 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 500 522 104 80-120 Arsenic ug/L 500 504 101 80-120 Barium ug/L 500 525 105 80-120 Beryllium ug/L 500 511 102 80-120 Cadmium ug/L 500 496 99 80-120 Chromium ug/L 500 505 101 80-120 Cobalt ug/L 500 512 102 80-120 Copper ug/L 500 531 106 80-120 Lead ug/L 500 513 103 80-120 Nickel ug/L 500 508 102 80-120 Selenium ug/L 500 513 103 80-120 Silver ug/L 250 256 102 80-120 Thallium ug/L 500 506 101 80-120 Tin ug/L 500 509 102 80-120 Vanadium ug/L 500 525 105 80-120 Zinc ug/L 500 494 99 80-120 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2014 02:31 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: SURRY CLOSED - 92203116 MT AIRY (AM) MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1212511 1212512 MS MSD 92203313005 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 467 452 93 90 75-125 3 25 Arsenic ug/L ND 500 500 457 435 91 87 75-125 5 25 Barium ug/L 93.5 500 500 553 531 92 88 75-125 4 25 Beryllium ug/L ND 500 500 455 433 91 87 75-125 5 25 Cadmium ug/L ND 500 500 439 422 88 84 75-125 4 25 Chromium ug/L ND 500 500 447 428 89 85 75-125 4 25 Cobalt ug/L ND 500 500 450 432 90 86 75-125 4 25 Copper ug/L ND 500 500 474 459 94 91 75-125 3 25 Lead ug/L ND 500 500 450 434 90 87 75-125 4 25 Nickel ug/L ND 500 500 445 427 89 85 75-125 4 25 Selenium ug/L ND 500 500 456 448 91 89 75-125 2 25 Silver ug/L ND 250 250 235 228 94 91 75-125 3 25 Thallium ug/L ND 500 500 451 437 90 87 75-125 3 25 Tin ug/L ND 500 500 461 438 92 88 75-125 5 25 Vanadium ug/L ND 500 500 469 449 94 90 75-125 4 25 Zinc ug/L ND 500 500 438 421 88 84 75-125 4 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2014 02:31 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED - MT AIRY (AM) Pace Project No.: 92203116 QC Batch: MSV/26995 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92203116001, 92203116002 METHOD BLANK: 1209031 Associated Lab Samples: 92203116001, 92203116002 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 05/29/14 15:03 1,1,1-Trichloroethane ug/L ND 1.0 05/29/14 15:03 1,1,2,2-Tetrachloroethane ug/L ND 3.0 05/29/14 15:03 1,1,2-Trichloroethane ug/L ND 1.0 05/29/14 15:03 1,1-Dichloroethane ug/L ND 5.0 05/29/14 15:03 1,1-Dichloroethene ug/L ND 5.0 05/29/14 15:03 1,2,3-Trichloropropane ug/L ND 1.0 05/29/14 15:03 1,2-Dibromo-3-chloropropane ug/L ND 13.0 05/29/14 15:03 1,2-Dibromoethane (EDB) ug/L ND 1.0 05/29/14 15:03 1,2-Dichlorobenzene ug/L ND 5.0 05/29/14 15:03 1,2-Dichloroethane ug/L ND 1.0 05/29/14 15:03 1,2-Dichloropropane ug/L ND 1.0 05/29/14 15:03 1,3-Dichloropropane ug/L ND 1.0 05/29/14 15:03 1,4-Dichlorobenzene ug/L ND 1.0 05/29/14 15:03 2-Butanone (MEK) ug/L ND 100 05/29/14 15:03 2-Hexanone ug/L ND 50.0 05/29/14 15:03 4-Methyl-2-pentanone (MIBK) ug/L ND 100 05/29/14 15:03 Acetone ug/L ND 100 05/29/14 15:03 Acrylonitrile ug/L ND 200 05/29/14 15:03 Benzene ug/L ND 1.0 05/29/14 15:03 Bromochloromethane ug/L ND 3.0 05/29/14 15:03 Bromodichloromethane ug/L ND 1.0 05/29/14 15:03 Bromoform ug/L ND 3.0 05/29/14 15:03 Bromomethane ug/L ND 10.0 05/29/14 15:03 Carbon disulfide ug/L ND 100 05/29/14 15:03 Carbon tetrachloride ug/L ND 1.0 05/29/14 15:03 Chlorobenzene ug/L ND 3.0 05/29/14 15:03 Chloroethane ug/L ND 10.0 05/29/14 15:03 Chloroform ug/L ND 5.0 05/29/14 15:03 Chloromethane ug/L ND 1.0 05/29/14 15:03 cis-1,2-Dichloroethene ug/L ND 5.0 05/29/14 15:03 cis-1,3-Dichloropropene ug/L ND 1.0 05/29/14 15:03 Dibromochloromethane ug/L ND 3.0 05/29/14 15:03 Dibromomethane ug/L ND 10.0 05/29/14 15:03 Ethylbenzene ug/L ND 1.0 05/29/14 15:03 lodomethane ug/L ND 10.0 05/29/14 15:03 Methylene Chloride ug/L ND 1.0 05/29/14 15:03 Styrene ug/L ND 1.0 05/29/14 15:03 Tetrachloroethene ug/L ND 1.0 05/29/14 15:03 Toluene ug/L ND 1.0 05/29/14 15:03 trans-1,2-Dichloroethene ug/L ND 5.0 05/29/14 15:03 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2014 02:31 PM without the written consent of Pace Analytical Services, Inc.. Page 18 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED - MT AIRY (AM) Pace Project No.: 92203116 METHOD BLANK: 1209031 Associated Lab Samples: 92203116001, 92203116002 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed trans- 1,3-Dichloropropene ug/L ND 1.0 05/29/14 15:03 trans-1,4-Dichloro-2-butene ug/L ND 100 05/29/14 15:03 Trichloroethene ug/L ND 1.0 05/29/14 15:03 Trichlorofluoromethane ug/L ND 1.0 05/29/14 15:03 Vinyl acetate ug/L ND 50.0 05/29/14 15:03 Vinyl chloride ug/L ND 1.0 05/29/14 15:03 Xylene (Total) ug/L ND 5.0 05/29/14 15:03 1,2-Dichloroethane-d4 (S) % 92 70-130 05/29/14 15:03 4-Bromofluorobenzene (S) % 95 70-130 05/29/14 15:03 Toluene-d8 (S) % 97 70-130 05/29/14 15:03 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 1209032 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 50.6 101 70-130 1,1,1-Trichloroethane ug/L 50 48.1 96 70-130 1,1,2,2-Tetrachloroethane ug/L 50 51.3 103 70-130 1,1,2-Trichloroethane ug/L 50 50.6 101 70-130 1,1-Dichloroethane ug/L 50 47.0 94 70-130 1,1-Dichloroethene ug/L 50 47.0 94 70-132 1,2,3-Trichloropropane ug/L 50 48.1 96 70-130 1,2-Dibromo-3-chloropropane ug/L 50 48.2 96 70-130 1,2-Dibromoethane (EDB) ug/L 50 49.1 98 70-130 1,2-Dichlorobenzene ug/L 50 50.0 100 70-130 1,2-Dichloroethane ug/L 50 48.8 98 70-130 1,2-Dichloropropane ug/L 50 49.6 99 70-130 1,3-Dichloropropane ug/L 50 49.8 100 70-130 1,4-Dichlorobenzene ug/L 50 49.1 98 70-130 2-Butanone (MEK) ug/L 100 87.7J 88 70-145 2-Hexanone ug/L 100 97.1 97 70-144 4-Methyl-2-pentanone (MIBK) ug/L 100 91.7J 92 70-140 Acetone ug/L 100 94.OJ 94 50-175 Acrylonitrile ug/L 250 237 95 70-143 Benzene ug/L 50 54.1 108 70-130 Bromochloromethane ug/L 50 49.0 98 70-130 Bromodichloromethane ug/L 50 48.6 97 70-130 Bromoform ug/L 50 49.2 98 70-130 Bromomethane ug/L 50 32.2 64 54-130 Carbon disulfide ug/L 50 49.9J 100 70-131 Carbon tetrachloride ug/L 50 46.0 92 70-132 Chlorobenzene ug/L 50 47.4 95 70-130 Chloroethane ug/L 50 42.4 85 64-134 Chloroform ug/L 50 48.7 97 70-130 Chloromethane ug/L 50 34.3 69 64-130 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2014 02:31 PM without the written consent of Pace Analytical Services, Inc.. Page 19 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED - MT AIRY (AM) Pace Project No.: 92203116 LABORATORY CONTROL SAMPLE: Parameter 1209032 Units Spike Conc. LCS LCS Result % Rec cis-1,2-Dichloroethene ug/L 50 48.0 cis-1,3-Dichloropropene ug/L 50 51.2 Dibromochloromethane ug/L 50 47.8 Dibromomethane ug/L 50 47.1 Ethylbenzene ug/L 50 48.1 lodomethane ug/L 100 27.5 Methylene Chloride ug/L 50 48.1 Styrene ug/L 50 52.2 Tetrachloroethene ug/L 50 48.7 Toluene ug/L 50 49.7 trans-1,2-Dichloroethene ug/L 50 47.4 trans- 1,3-Dichloropropene ug/L 50 49.0 trans-1,4-Dichloro-2-butene ug/L 50 46.6J Trichloroethene ug/L 50 52.2 Trichlorofluoromethane ug/L 50 40.2 Vinyl acetate ug/L 100 100 Vinyl chloride ug/L 50 54.9 Xylene (Total) ug/L 150 147 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Toluene-d8 (S) % % Rec Limits Qualifiers 96 70-131 102 70-130 96 70-130 94 70-131 96 70-130 27 49-180 LO 96 63-130 104 70-130 97 70-130 99 70-130 95 70-130 98 70-132 93 70-141 104 70-130 80 62-133 100 66-157 110 69-130 98 70-130 91 70-130 97 70-130 100 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2014 02:31 PM without the written consent of Pace Analytical Services, Inc.. Page 20 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED - MT AIRY (AM) Pace Project No.: 92203116 QC Batch: MSV/27034 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92203116003, 92203116004 METHOD BLANK: 1210761 Associated Lab Samples: 92203116003, 92203116004 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 05/31/14 01:23 1,1,1-Trichloroethane ug/L ND 1.0 05/31/14 01:23 1,1,2,2-Tetrachloroethane ug/L ND 3.0 05/31/14 01:23 1,1,2-Trichloroethane ug/L ND 1.0 05/31/14 01:23 1,1-Dichloroethane ug/L ND 5.0 05/31/14 01:23 1,1-Dichloroethene ug/L ND 5.0 05/31/14 01:23 1,2,3-Trichloropropane ug/L ND 1.0 05/31/14 01:23 1,2-Dibromo-3-chloropropane ug/L ND 13.0 05/31/14 01:23 1,2-Dibromoethane (EDB) ug/L ND 1.0 05/31/14 01:23 1,2-Dichlorobenzene ug/L ND 5.0 05/31/14 01:23 1,2-Dichloroethane ug/L ND 1.0 05/31/14 01:23 1,2-Dichloropropane ug/L ND 1.0 05/31/14 01:23 1,3-Dichloropropane ug/L ND 1.0 05/31/14 01:23 1,4-Dichlorobenzene ug/L ND 1.0 05/31/14 01:23 2-Butanone (MEK) ug/L ND 100 05/31/14 01:23 2-Hexanone ug/L ND 50.0 05/31/14 01:23 4-Methyl-2-pentanone (MIBK) ug/L ND 100 05/31/14 01:23 Acetone ug/L ND 100 05/31/14 01:23 Acrylonitrile ug/L ND 200 05/31/14 01:23 Benzene ug/L ND 1.0 05/31/14 01:23 Bromochloromethane ug/L ND 3.0 05/31/14 01:23 Bromodichloromethane ug/L ND 1.0 05/31/14 01:23 Bromoform ug/L ND 3.0 05/31/14 01:23 Bromomethane ug/L ND 10.0 05/31/14 01:23 Carbon disulfide ug/L ND 100 05/31/14 01:23 Carbon tetrachloride ug/L ND 1.0 05/31/14 01:23 Chlorobenzene ug/L ND 3.0 05/31/14 01:23 Chloroethane ug/L ND 10.0 05/31/14 01:23 Chloroform ug/L ND 5.0 05/31/14 01:23 Chloromethane ug/L ND 1.0 05/31/14 01:23 cis-1,2-Dichloroethene ug/L ND 5.0 05/31/14 01:23 cis-1,3-Dichloropropene ug/L ND 1.0 05/31/14 01:23 Dibromochloromethane ug/L ND 3.0 05/31/14 01:23 Dibromomethane ug/L ND 10.0 05/31/14 01:23 Ethylbenzene ug/L ND 1.0 05/31/14 01:23 lodomethane ug/L ND 10.0 05/31/14 01:23 Methylene Chloride ug/L ND 1.0 05/31/14 01:23 Styrene ug/L ND 1.0 05/31/14 01:23 Tetrachloroethene ug/L ND 1.0 05/31/14 01:23 Toluene ug/L ND 1.0 05/31/14 01:23 trans-1,2-Dichloroethene ug/L ND 5.0 05/31/14 01:23 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2014 02:31 PM without the written consent of Pace Analytical Services, Inc.. Page 21 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED - MT AIRY (AM) Pace Project No.: 92203116 METHOD BLANK: 1210761 Associated Lab Samples: 92203116003, 92203116004 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed trans- 1,3-Dichloropropene ug/L ND 1.0 05/31/14 01:23 trans-1,4-Dichloro-2-butene ug/L ND 100 05/31/14 01:23 Trichloroethene ug/L ND 1.0 05/31/14 01:23 Trichlorofluoromethane ug/L ND 1.0 05/31/14 01:23 Vinyl acetate ug/L ND 50.0 05/31/14 01:23 Vinyl chloride ug/L ND 1.0 05/31/14 01:23 Xylene (Total) ug/L ND 5.0 05/31/14 01:23 1,2-Dichloroethane-d4 (S) % 97 70-130 05/31/14 01:23 4-Bromofluorobenzene (S) % 99 70-130 05/31/14 01:23 Toluene-d8 (S) % 100 70-130 05/31/14 01:23 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 1210762 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 46.3 93 70-130 1,1,1-Trichloroethane ug/L 50 47.2 94 70-130 1,1,2,2-Tetrachloroethane ug/L 50 48.1 96 70-130 1,1,2-Trichloroethane ug/L 50 49.6 99 70-130 1,1-Dichloroethane ug/L 50 44.5 89 70-130 1,1-Dichloroethene ug/L 50 50.3 101 70-132 1,2,3-Trichloropropane ug/L 50 50.0 100 70-130 1,2-Dibromo-3-chloropropane ug/L 50 49.9 100 70-130 1,2-Dibromoethane (EDB) ug/L 50 48.1 96 70-130 1,2-Dichlorobenzene ug/L 50 48.4 97 70-130 1,2-Dichloroethane ug/L 50 47.1 94 70-130 1,2-Dichloropropane ug/L 50 47.3 95 70-130 1,3-Dichloropropane ug/L 50 47.3 95 70-130 1,4-Dichlorobenzene ug/L 50 46.9 94 70-130 2-Butanone (MEK) ug/L 100 99.91 100 70-145 2-Hexanone ug/L 100 98.5 99 70-144 4-Methyl-2-pentanone (MIBK) ug/L 100 107 107 70-140 Acetone ug/L 100 96.9J 97 50-175 Acrylonitrile ug/L 250 247 99 70-143 Benzene ug/L 50 48.8 98 70-130 Bromochloromethane ug/L 50 49.0 98 70-130 Bromodichloromethane ug/L 50 46.3 93 70-130 Bromoform ug/L 50 48.6 97 70-130 Bromomethane ug/L 50 46.2 92 54-130 Carbon disulfide ug/L 50 48.OJ 96 70-131 Carbon tetrachloride ug/L 50 52.4 105 70-132 Chlorobenzene ug/L 50 45.4 91 70-130 Chloroethane ug/L 50 51.7 103 64-134 Chloroform ug/L 50 47.1 94 70-130 Chloromethane ug/L 50 47.7 95 64-130 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2014 02:31 PM without the written consent of Pace Analytical Services, Inc.. Page 22 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED - MT AIRY (AM) Pace Project No.: 92203116 LABORATORY CONTROL SAMPLE: Parameter 1210762 Units Spike Conc. LCS Result LCS % Rec % Rec Limits cis-1,2-Dichloroethene ug/L 50 47.4 95 70-131 cis-1,3-Dichloropropene ug/L 50 47.2 94 70-130 Dibromochloromethane ug/L 50 45.6 91 70-130 Dibromomethane ug/L 50 48.2 96 70-131 Ethylbenzene ug/L 50 45.4 91 70-130 lodomethane ug/L 100 95.0 95 49-180 Methylene Chloride ug/L 50 50.8 102 63-130 Styrene ug/L 50 48.7 97 70-130 Tetrachloroethene ug/L 50 49.5 99 70-130 Toluene ug/L 50 47.8 96 70-130 trans-1,2-Dichloroethene ug/L 50 48.3 97 70-130 trans- 1,3-Dichloropropene ug/L 50 47.5 95 70-132 trans-1,4-Dichloro-2-butene ug/L 50 49.6J 99 70-141 Trichloroethene ug/L 50 48.0 96 70-130 Trichlorofluoromethane ug/L 50 55.6 111 62-133 Vinyl acetate ug/L 100 99.1 99 66-157 Vinyl chloride ug/L 50 60.4 121 69-130 Xylene (Total) ug/L 150 139 93 70-130 1,2-Dichloroethane-d4 (S) % 97 70-130 4-Bromofluorobenzene (S) % 99 70-130 Toluene-d8 (S) % 102 70-130 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1211546 1211547 MS MSD 92203116003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,1-Dichloroethene ug/L ND 50 50 56.2 60.5 112 121 70-166 7 30 Benzene ug/L 0.42J 50 50 52.0 56.3 103 112 70-148 8 30 Chlorobenzene ug/L 0.38J 50 50 48.3 51.7 96 103 70-146 7 30 Toluene ug/L ND 50 50 48.5 52.1 97 104 70-155 7 30 Trichloroethene ug/L ND 50 50 54.1 57.7 108 115 69-151 7 30 1,2-Dichloroethane-d4 (S) % 99 100 70-130 4-Bromofluorobenzene (S) % 100 101 70-130 Toluene-d8(S) % 101 102 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2014 02:31 PM without the written consent of Pace Analytical Services, Inc.. Page 23 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED - MT AIRY (AM) Pace Project No.: 92203116 QC Batch: WETA/19244 Analysis Method: SM 4500-CN-E QC Batch Method: SM 4500-CN-E Analysis Description: 450OCNE Cyanide, Total Associated Lab Samples: 92203116003 METHOD BLANK: 1216413 Matrix: Water Associated Lab Samples: 92203116003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cyanide ug/L ND 10.0 06/09/1410:59 LABORATORY CONTROL SAMPLE: 1216414 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 110 110 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1216415 1216416 MS MSD 92203313004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 108 87.2 106 86 75-125 21 20 R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1216417 1216418 MS MSD 92203121007 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 89.6 90.3 87 88 75-125 1 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2014 02:31 PM without the written consent of Pace Analytical Services, Inc.. Page 24 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALIFIERS Project: SURRY CLOSED - MT AIRY (AM) Pace Project No.: 92203116 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2014 02:31 PM without the written consent of Pace Analytical Services, Inc.. Page 25 of 30 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: SURRY CLOSED - MT AIRY (AM) Pace Project No.: 92203116 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92203116001 MW-12D EPA3010 MPRP/16067 EPA6010 ICP/14532 92203116002 SCALEHOUSE EPA 3010 MPRP/16067 EPA6010 ICP/14532 92203116003 MW-6 EPA3010 MPRP/16106 EPA6010 ICP/14566 92203116004 MW-11 EPA3010 MPRP/16106 EPA6010 ICP/14566 92203116003 MW-6 EPA 7470 MERP/6688 EPA 7470 MERC/6448 92203116004 MW-11 EPA 7470 MERP/6688 EPA 7470 MERC/6448 92203116001 MW-12D EPA 8260 MSV/26995 92203116002 SCALEHOUSE EPA 8260 MSV/26995 92203116003 MW-6 EPA 8260 MSV/27034 92203116004 MW-11 EPA 8260 MSV/27034 92203116003 MW-6 SM 4500-CN-E WETA/19244 Date: 06/09/2014 02:31 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 26 of 30 Document Name: Document Revised: April 07. 2014 aceAri�7lyticat- Sample Condition Upon Receipt SCLIR Page 1 of 2 Document Number: Issuing Authority: F-CHR-CS-003-rev.14 Pace Huntersville Quali Office Client Name: Q n i L- j d Courier: ❑ Fed Ex ❑ UPS[] USPS❑ Client[] Commercialwlll�pace Other Optional Custody Seal on Cooler/Box Present: Elyes ❑ no Seals intact: ❑ yes ❑ no Prol• Due.: ate; Proj. Name:a: Packing Material: ❑ Bubble Wrap [1,136bble Bags ❑ None ❑ Other Thermometer Used: IR Gun T1102 T14 Type of Ice' LVll Blue None Samples on ice, cooling process has begun Tpmn r'.nrrprtinn Fartn► T1102: No Correction T1301: No Correction Corrected Cooler Temp.: -C Temp should be above freezing to 6°C Biological Tissue is Frozen: Yes N NI 9 Comments: Date and Initials of Derson examining contents: •- 7� Chain of Custody Present: ❑Yes ❑N❑ ©NIA [. Chain of Custody Filled Out: Ye ONo ❑NIA 2. Chain of Custody Relinquished: a ❑No ❑NIA 3, Sampler Name & Signature on COC: Ye DNo ❑N!A 4, Samples Arrived within Hold Time: Yes ONO ❑NIA 5, Short Hold Time Analysis r72hr}: ❑Yes to ❑N!A 6, Rush Turn Around Time Requested: ❑Yes ❑ ❑NIA 7, Sufficient Volume: Ery_ ON, ❑NIA 8. Correct Containers Used: -Pace Containers Used: ❑No ZONo ❑NIA ❑NIA 9. Containers Intact: Yes ONO 13N!X 10, Filtered volume received for Dissolved tests Dyes ©No ZNIA 11. Sample Labels match COC: -Includes date/time/ID/Analysis Matrix: IYes ❑No ❑NIA 12, All containers needing preservation have been checked. All containers needing preservation are found to be in compliance with EPA recommendation. exceptions: VOA, coliform, TOC, O&G, W-DRO (water) CTYes ONO ❑ es ONO 2❑No ❑N!A ❑NIA 13. f Samples checked for dechlorination: Ores ❑No 141A 14, Headspace in VOA Vials (>6mm): ❑Yes gNo ❑N! 15. Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # (if purchased): ❑Yes ❑Yes ❑No ❑Na ZIA 16. Client Notification/ Resolution: Field Data Required? Y I N Person Contacted: Datefrime: Comments/ Resolution: SCURF Review: Date: 14 _�y S RF Review: Date: AS 1 z Note: Whenever th41discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers) WO#:92203116 111111111111111111111 Page 27 of 30 r s ( �,1 s.�y,�.�� 0 14Wr21 CHAIN -OF -CUSTODY ! Analytical Request Document 0 t4lo-c5 w' ��00 The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Fo r10 ` r � o, W a Section A Section B Section C Required Client information: Required Project Information: Invoice Information: Pa @ : 1 Of .. 1 Company: Municipal Engineering Services Report To Jonathan Pfohl Attention: Municipal Engineering Services Address: P.O. Box 97 Copy To: Company Name: Garner, NC 27529 Address: 'Regulatory Agency I Email To: jpfohl(('�13lesco.COm Purchas rder No. Pace Quote Reference: Phone: 919-772-5393 Fax Client Project ID: Pace Project Manager: Kevin Godwin State f Location Requested Due DatelTAT: 10 Day (Default) Container Order Number: Pace Profile #: North Carolina Requested AnaW;s Filtered IN COLLECTED Preservatives } N N N N N N N N N N N N i MATRIX CODE on," wales ow c a _ SAMPLE ID �w � $ START END w One Character per box. 3a1usa1e sL (A-2, 0.9 1. -) chi OL wive VVP a o m Sample Ids must he unique Aj,of AR rL/ omn oT 145.a TS u 4n w a 2 3 e1 m Lr/J/ S tit H �' ¢ r�Ii DATE TIME DATE TIME ¢ cn ❑ u L rn _ Z = U x d z z N r O Q V O> TO F 1 Inf wT G ;;a LAB%131 1 Xx x } a wr & S-As 1 I. X. 3 4 5 6 7 8 9 ifl ti 12 ADA;TETIME 11 ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION ACCEPTED BY f AFFIU00N . DATE TIME SAMP ~ 60ROMONS ` 1 / lao � yj�/',- ,J� r } All SAMPLER NAME AND SIGNATURE m V O y Z C PRINT Name of SAMPLE •, JQD ha fOhl SIGNATURE of SAMPLER: DATE Signed: 5 Lu 0} o E z � �Q �} Document Name: Document Revised: April 07. 2014 - r�oeAr&7/ytiral ` Sample Condition Upon Receipt (SCUR) Page 1 of 2 Document Number: Issuing Authority: F-CHR-CS-003-rev.14 Pace Huntersville Quality Office Client Name: m'�',(';D� nc Courier: ❑ Fed Ex ❑ UPS[:] USPS❑ Client❑ Commercial Pace Other Custody Seal on Cooler/Box Present: ❑ yes e no Seals intact: ❑ yes ❑ no Packing Material: ❑ Bubble Wrap Bubble Bags ❑ None ❑ Other Thermometer Used: I Gun T1102 140 Type of Ice: e Blue None Samples on ice, cooling process has begun Temn Cnrrecfinn Far -Mr T1102• No CorrPrtion T1301 • Nn CnrrPction Corrected Cooler Temp.:,�] °C Biological Tissue is Frozen: Yes No /A Date and Initials of ersonexamining contents: Temp should be above freezing to 6°C Comments: Chain of Custody Present: Pes ❑No ❑N/A 1. Chain of Custody Filled Out: Y s ❑No ❑N/A 2• Chain of Custody Relinquished: EiYes ❑No ❑N/A 3. Sampler Name & Signature on COC: es ❑No ❑N/A 4. Samples Arrived within Hold Time: Yes ❑No ❑N/A 5. Short Hold Time Analysis (<72hr): ❑Yes 9 'N9 ❑N/A 6. Rush Turn Around Time Requested: ❑Yes No ❑N/A 7. Sufficient Volume: Ye s ❑No ❑N/A 8. Correct Containers Used: es ❑No ❑N/A 9. -Pace Containers Used: Wyes ❑No ❑N/A Containers Intact: Yes ❑No El N/A 10. Filtered volume received for Dissolved tests ❑Yes ❑No N/A 11. Sample Labels match COC: es El No ❑N/A 12. �t`.l Rs- -Includes date/time/ID/Analysis Matrix: All containers needing preservation have been checked. Yes ❑No ❑N/A 13. All containers needing preservation are found to be in Yes El No ❑N/A compliance with EPA recommendation. exceptions: VOA, coliform, TOC, 0&G, WI-DRO (water) Yes ❑No Samples checked for dechlorination: ❑Yes ❑No N/A 14. Headspace in VOA Vials (>6mm): ❑Yes JVNo ❑N/A 15. Trip Blank Present: ❑Yes ❑No 16N/A 16. Trip Blank Custody Seals Present ❑Yes ❑No VNIA Pace Trip Blank Lot # (if purchased): Client Notification/ Resolution: Person Contacted: Comments/ Resolution: Date/Time: ;CURF Review: I J Date: 7 zS tY SRF Review: Date: 3 Note: Whenever there i discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers) Field Data Required? Y / N Place label here `� 2--7-C)'' ' OR Handwrite project number (if no label available) Page 29 of 30 PaceAna4fical CHAIN -OF -CUSTODY / Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Required Client Information: Required Project Information: Invoice Information: Page ' 1 Of 1 Company: Municipal Engineering Services Report To: Jonathan Pfohl Attention: Municipal Engineering Services Address: P.O. BOX 97 Copy To: Company Name: Garner, NC 27529 Address: Regulatory Agency' Email To: jpfohl(o)mesco.Com Purchase Order No. Pace Quote Reference: Phone: 919-772-5393 jFax Client Project ID: Surry Closed -Mt. Airy (AM) Pace Project Manager: Kevin Godwin State ILocation Requested Due Date/TAT: 10 Day (Default) Container Order Number Pace Profile #: North Carolina Requested Analysis Filtered (YIN)'. Z r _ a COLLECTED Preservatives i N N N N N - MATRIX CODE Drinking Water DW Water WT a 2 2 O U O H Waste Water WW uct P SAMPLE ID sovsand s m START END J O '. N One Character per box. O'i OE 0 m ) (A-Z, 0-9 1, -) ArPe AR w w d w N _ o Ids must be unique aner FSample d oc 0 2 Tssue TS Z O u Q wN l 0 c Q W On - Q Ozz to to° E_ DATE TIME DATE TIME u O O g tj 1 M W-6 WTI G I ; /u d%jr x x x ex, 3 '2 .;.N1W-11 WT G t'jS x x x Q✓� 3 MW-12D WT G x x 4 Scalehouse W.I. G x x 5. 1 6 7 g,,., 9 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY AFFILIATION DATE : 'TIME j ACCEPTED BY / AFFILIAT DATE TIME SAMPLE CONDITIONS SAMPLER NAME AND SIGNATURE - d u U c 0 U) y PRINT Name of SAMPLER: o han Pfohl EL �E o } 0 o E z SIGNATURE of SAMPLE DATE Signed: S F W o UU (n } 0 cn 0 0 M at rn m 0_ aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 June 12, 2014 Mr. Jonathan Pfohl Municipal Engineering Services PO Box 97 Garner, NC 27529 RE: Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory between May 28, 2014 and May 29, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Godwin kevin.godwin@pacelabs.com Project Manager Enclosures Q _Kok r REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Dr., Asheville, INC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 SAMPLE SUMMARY Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Lab ID Sample ID Matrix Date Collected Date Received 92203121001 MW-12S Water 05/27/1414:35 05/28/1417:00 92203121002 MWA8 Water 05/27/1413:30 05/28/1417:00 92203121003 MW-19 Water 05/27/1415:10 05/28/1417:00 92203121004 MW-23 Water 05/27/1416:00 05/28/1417:00 92203121005 MWA Water 05/28/14 08:05 05/29/14 15:20 92203121006 MW-7 Water 05/28/1412:00 05/29/14 15:20 92203121007 MW-15 Water 05/28/14 09:45 05/29/14 15:20 92203121008 MW-21 Water 05/28/1413:40 05/29/14 15:20 92203121009 MW-9 Water 05/28/1411:35 05/29/14 15:20 92203121010 MW-14 Water 05/28/1410:15 05/29/14 15:20 92203121011 MW-3R Water 05/28/14 08:40 05/29/14 15:20 92203121012 MW-13 Water 05/28/1411:00 05/29/14 15:20 92203121013 MW-17 Water 05/28/1415:10 05/29/14 15:20 92203121014 MW-20 Water 05/27/14 06:05 05/29/14 15:20 92203121015 MW-16 Water 05/28/14 09:10 05/29/14 15:20 92203121016 MW-22 Water 05/28/1414:35 05/29/14 15:20 92203121017 MW-19 Water 05/27/1415:10 05/29/14 15:20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: Surry Closed -Mt. Airy (UIC) 92203121 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92203121001 MW-12S EPA 6010 JMW 15 PASI-A EPA 8260 MCK 51 PASI-C 92203121002 MW-18 EPA 6010 JMW 15 PASI-A EPA 8260 MCK 51 PASI-C 92203121003 MW-19 EPA 6010 JMW 15 PASI-A EPA 8260 MCK 51 PASI-C 92203121004 MW-23 EPA 6010 JMW 15 PASI-A EPA 8260 MCK 51 PASI-C 92203121005 MW-1 EPA 6010 JMW 16 PASI-A EPA 8260 NU1 51 PASI-C SM 2320B MDW 1 PASI-A SM 4500-S21D SAE 1 PASI-A EPA 300.0 SAE 1 PASI-A SM 4500-CI-E SMW 1 PASI-A SM 4500-CN-E JDA 1 PASI-A SM 5220D EWS 1 PASI-A SM 5310B SAE 1 PASI-A 92203121006 MW-7 EPA 6010 JMW 16 PASI-A EPA 8260 NU1 51 PASI-C SM 2320B MDW 1 PASI-A SM 4500-S21D SAE 1 PASI-A EPA 300.0 SAE 1 PASI-A SM 4500-CI-E SMW 1 PASI-A SM 4500-CN-E JDA 1 PASI-A SM 5220D EWS 1 PASI-A SM 5310B SAE 1 PASI-A 92203121007 MW-15 EPA 6010 JMW 16 PASI-A EPA 8260 NU1 51 PASI-C SM 2320B MDW 1 PASI-A SM 4500-S21D SAE 1 PASI-A EPA 300.0 SAE 1 PASI-A SM 4500-CI-E SMW 1 PASI-A SM 4500-CN-E JDA 1 PASI-A SM 5220D EWS 1 PASI-A SM 5310B SAE 1 PASI-A 92203121008 MW-21 EPA 6010 JMW 16 PASI-A EPA 8260 NU1 51 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Lab ID Sample ID Method Analysts Analytes Reported Laboratory SM 2320B MDW 1 PASI-A SM 4500-S21D SAE 1 PASI-A EPA 300.0 SAE 1 PASI-A SM 4500-CI-E SMW 1 PASI-A SM 4500-CN-E JDA 1 PASI-A SM 5220D EWS 1 PASI-A SM 5310B SAE 1 PASI-A 92203121009 MW-9 EPA 6010 JMW 16 PASI-A EPA8260 NU1 51 PASI-C SM 2320B MDW 1 PASI-A SM 4500-S21D SAE 1 PASI-A EPA 300.0 SAE 1 PASI-A SM 4500-CI-E SMW 1 PASI-A SM 5220D EWS 1 PASI-A SM 5310B SAE 1 PASI-A 92203121010 MW-14 EPA 6010 JMW 16 PASI-A EPA 7470 MTS 1 PASI-A EPA8260 NU1 51 PASI-C SM 2320B MDW 1 PASI-A SM 4500-S21D SAE 1 PASI-A EPA 300.0 SAE 1 PASI-A SM 4500-CI-E SMW 1 PASI-A SM 5220D EWS 1 PASI-A SM 5310B SAE 1 PASI-A 92203121011 MW-3R EPA 6010 JMW 15 PASI-A EPA8260 NU1 51 PASI-C 92203121012 MW-13 EPA 6010 JMW 15 PASI-A EPA8260 NU1 51 PASI-C 92203121013 MW-17 EPA 6010 JMW 15 PASI-A EPA8260 NU1 51 PASI-C 92203121014 MW-20 EPA 6010 JMW 15 PASI-A EPA8260 NU1 51 PASI-C 92203121015 MW-16 EPA 6010 JMW 15 PASI-A EPA8260 NU1 52 PASI-C SM 4500-CN-E JDA 1 PASI-A 92203121016 MW-22 EPA 6010 JMW 15 PASI-A EPA8260 NU1 51 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Analytes Lab ID Sample ID Method Analysts Reported Laboratory SM 4500-CN-E JDA 1 PASI-A 92203121017 MW-19 SM 4500-CN-E JDA 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-12S Lab ID: 92203121001 Collected: 05/27/14 14:35 Received: 05/28/14 17:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 5.0 1 05/29/14 15:55 05/30/14 19:59 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 19:59 7440-38-2 Barium 22.4J ug/L 100 5.0 1 05/29/14 15:55 05/30/14 19:59 7440-39-3 Beryllium ND ug/L 1.0 1.0 1 05/29/14 15:55 05/30/14 19:59 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 05/29/14 15:55 05/30/14 19:59 7440-43-9 Chromium ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 19:59 7440-47-3 Cobalt ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 19:59 7440-48-4 Copper ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 19:59 7440-50-8 Lead ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 19:59 7439-92-1 Nickel ND ug/L 50.0 5.0 1 05/29/14 15:55 05/30/14 19:59 7440-02-0 Selenium ND ug/L 10.0 10.0 1 05/29/14 15:55 05/30/14 19:59 7782-49-2 Silver ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 19:59 7440-22-4 Thallium ND ug/L 5.5 5.4 1 05/29/14 15:55 05/30/14 19:59 7440-28-0 Vanadium ND ug/L 25.0 5.0 1 05/29/14 15:55 05/30/14 19:59 7440-62-2 Zinc ND ug/L 10.0 10.0 1 05/29/14 15:55 05/30/14 19:59 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 05/29/14 23:52 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 05/29/14 23:52 107-13-1 Benzene ND ug/L 1.0 0.25 1 05/29/14 23:52 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 05/29/14 23:52 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 05/29/14 23:52 75-27-4 Bromoform ND ug/L 3.0 0.26 1 05/29/14 23:52 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 05/29/14 23:52 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 05/29/14 23:52 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 05/29/14 23:52 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 05/29/14 23:52 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 05/29/14 23:52 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 05/29/14 23:52 75-00-3 Chloroform ND ug/L 5.0 0.14 1 05/29/14 23:52 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 05/29/14 23:52 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 05/29/14 23:52 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 05/29/14 23:52 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 05/29/14 23:52 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 05/29/14 23:52 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 05/29/14 23:52 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 05/29/14 23:52 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 05/29/14 23:52 110-57-6 1,1-Dichloroethane 0.64J ug/L 5.0 0.32 1 05/29/14 23:52 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 05/29/14 23:52 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 05/29/14 23:52 75-35-4 cis-1,2-Dichloroethene 0.59J ug/L 5.0 0.19 1 05/29/14 23:52 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 05/29/14 23:52 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 05/29/14 23:52 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 05/29/14 23:52 142-28-9 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 05/29/14 23:52 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-12S Lab ID: 92203121001 Collected: 05/27/14 14:35 Received: 05/28/14 17:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 05/29/14 23:52 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 05/29/14 23:52 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 05/29/14 23:52 591-78-6 lodomethane ND ug/L 10.0 0.32 1 05/29/14 23:52 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 05/29/14 23:52 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 05/29/14 23:52 108-10-1 Styrene ND ug/L 1.0 0.26 1 05/29/14 23:52 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 05/29/14 23:52 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 05/29/14 23:52 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 05/29/14 23:52 127-18-4 Toluene ND ug/L 1.0 0.26 1 05/29/14 23:52 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 05/29/14 23:52 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 05/29/14 23:52 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 05/29/14 23:52 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 05/29/14 23:52 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 05/29/14 23:52 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 05/29/14 23:52 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 05/29/14 23:52 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 05/29/14 23:52 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 05/29/14 23:52 460-00-4 1,2-Dichloroethane-d4 (S) 99 % 70-130 1 05/29/14 23:52 17060-07-0 Toluene-d8 (S) 97 % 70-130 1 05/29/14 23:52 2037-26-5 Date: 06/12/2014 08:20 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 8 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-18 Lab ID: 92203121002 Collected: 05/27/14 13:30 Received: 05/28/14 17:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 5.0 1 05/29/14 15:55 05/30/14 20:02 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 20:02 7440-38-2 Barium 11.7J ug/L 100 5.0 1 05/29/14 15:55 05/30/14 20:02 7440-39-3 Beryllium ND ug/L 1.0 1.0 1 05/29/14 15:55 05/30/14 20:02 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 05/29/14 15:55 05/30/14 20:02 7440-43-9 Chromium ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 20:02 7440-47-3 Cobalt ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 20:02 7440-48-4 Copper ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 20:02 7440-50-8 Lead ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 20:02 7439-92-1 Nickel ND ug/L 50.0 5.0 1 05/29/14 15:55 05/30/14 20:02 7440-02-0 Selenium ND ug/L 10.0 10.0 1 05/29/14 15:55 05/30/14 20:02 7782-49-2 Silver ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 20:02 7440-22-4 Thallium ND ug/L 5.5 5.4 1 05/29/14 15:55 05/30/14 20:02 7440-28-0 Vanadium ND ug/L 25.0 5.0 1 05/29/14 15:55 05/30/14 20:02 7440-62-2 Zinc ND ug/L 10.0 10.0 1 05/29/14 15:55 05/30/14 20:02 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 05/30/14 00:08 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 05/30/14 00:08 107-13-1 Benzene ND ug/L 1.0 0.25 1 05/30/14 00:08 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 05/30/14 00:08 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 05/30/14 00:08 75-27-4 Bromoform ND ug/L 3.0 0.26 1 05/30/14 00:08 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 05/30/14 00:08 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 05/30/14 00:08 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 05/30/14 00:08 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 05/30/14 00:08 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 05/30/14 00:08 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 05/30/14 00:08 75-00-3 Chloroform ND ug/L 5.0 0.14 1 05/30/14 00:08 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 05/30/14 00:08 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 05/30/14 00:08 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 05/30/14 00:08 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 05/30/14 00:08 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 05/30/14 00:08 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 05/30/14 00:08 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 05/30/14 00:08 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 05/30/14 00:08 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 05/30/14 00:08 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 05/30/14 00:08 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 05/30/14 00:08 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 05/30/14 00:08 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 05/30/14 00:08 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 05/30/14 00:08 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 05/30/14 00:08 142-28-9 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 05/30/14 00:08 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 9 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-18 Lab ID: 92203121002 Collected: 05/27/14 13:30 Received: 05/28/14 17:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 05/30/14 00:08 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 05/30/14 00:08 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 05/30/14 00:08 591-78-6 lodomethane ND ug/L 10.0 0.32 1 05/30/14 00:08 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 05/30/14 00:08 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 05/30/14 00:08 108-10-1 Styrene ND ug/L 1.0 0.26 1 05/30/14 00:08 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 05/30/14 00:08 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 05/30/14 00:08 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 05/30/14 00:08 127-18-4 Toluene ND ug/L 1.0 0.26 1 05/30/14 00:08 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 05/30/14 00:08 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 05/30/14 00:08 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 05/30/14 00:08 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 05/30/14 00:08 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 05/30/14 00:08 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 05/30/14 00:08 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 05/30/14 00:08 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 05/30/14 00:08 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 94 % 70-130 1 05/30/14 00:08 460-00-4 1,2-Dichloroethane-d4 (S) 101 % 70-130 1 05/30/14 00:08 17060-07-0 Toluene-d8 (S) 97 % 70-130 1 05/30/14 00:08 2037-26-5 Date: 06/12/2014 08:20 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-19 Lab ID: 92203121003 Collected: 05/27/14 15:10 Received: 05/28/14 17:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 5.0 1 05/29/14 15:55 05/30/14 20:14 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 20:14 7440-38-2 Barium 54.8J ug/L 100 5.0 1 05/29/14 15:55 05/30/14 20:14 7440-39-3 Beryllium ND ug/L 1.0 1.0 1 05/29/14 15:55 05/30/14 20:14 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 05/29/14 15:55 05/30/14 20:14 7440-43-9 Chromium ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 20:14 7440-47-3 Cobalt ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 20:14 7440-48-4 Copper ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 20:14 7440-50-8 Lead ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 20:14 7439-92-1 Nickel ND ug/L 50.0 5.0 1 05/29/14 15:55 05/30/14 20:14 7440-02-0 Selenium ND ug/L 10.0 10.0 1 05/29/14 15:55 05/30/14 20:14 7782-49-2 Silver ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 20:14 7440-22-4 Thallium ND ug/L 5.5 5.4 1 05/29/14 15:55 05/30/14 20:14 7440-28-0 Vanadium 6.4J ug/L 25.0 5.0 1 05/29/14 15:55 05/30/14 20:14 7440-62-2 Zinc 10.1 ug/L 10.0 10.0 1 05/29/14 15:55 05/30/14 20:14 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 05/30/14 00:25 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 05/30/14 00:25 107-13-1 Benzene ND ug/L 1.0 0.25 1 05/30/14 00:25 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 05/30/14 00:25 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 05/30/14 00:25 75-27-4 Bromoform ND ug/L 3.0 0.26 1 05/30/14 00:25 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 05/30/14 00:25 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 05/30/14 00:25 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 05/30/14 00:25 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 05/30/14 00:25 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 05/30/14 00:25 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 05/30/14 00:25 75-00-3 Chloroform ND ug/L 5.0 0.14 1 05/30/14 00:25 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 05/30/14 00:25 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 05/30/14 00:25 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 05/30/14 00:25 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 05/30/14 00:25 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 05/30/14 00:25 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 05/30/14 00:25 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 05/30/14 00:25 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 05/30/14 00:25 110-57-6 1,1-Dichloroethane 2.3J ug/L 5.0 0.32 1 05/30/14 00:25 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 05/30/14 00:25 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 05/30/14 00:25 75-35-4 cis-1,2-Dichloroethene 3.1J ug/L 5.0 0.19 1 05/30/14 00:25 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 05/30/14 00:25 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 05/30/14 00:25 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 05/30/14 00:25 142-28-9 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 05/30/14 00:25 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 11 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-19 Lab ID: 92203121003 Collected: 05/27/14 15:10 Received: 05/28/14 17:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 05/30/14 00:25 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 05/30/14 00:25 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 05/30/14 00:25 591-78-6 lodomethane ND ug/L 10.0 0.32 1 05/30/14 00:25 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 05/30/14 00:25 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 05/30/14 00:25 108-10-1 Styrene ND ug/L 1.0 0.26 1 05/30/14 00:25 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 05/30/14 00:25 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 05/30/14 00:25 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 05/30/14 00:25 127-18-4 Toluene ND ug/L 1.0 0.26 1 05/30/14 00:25 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 05/30/14 00:25 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 05/30/14 00:25 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 05/30/14 00:25 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 05/30/14 00:25 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 05/30/14 00:25 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 05/30/14 00:25 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 05/30/14 00:25 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 05/30/14 00:25 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 05/30/14 00:25 460-00-4 1,2-Dichloroethane-d4 (S) 100 % 70-130 1 05/30/14 00:25 17060-07-0 Toluene-d8 (S) 98 % 70-130 1 05/30/14 00:25 2037-26-5 Date: 06/12/2014 08:20 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 12 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-23 Lab ID: 92203121004 Collected: 05/27/14 16:00 Received: 05/28/14 17:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 5.0 1 05/29/14 15:55 05/30/14 20:17 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 20:17 7440-38-2 Barium 39.8J ug/L 100 5.0 1 05/29/14 15:55 05/30/14 20:17 7440-39-3 Beryllium ND ug/L 1.0 1.0 1 05/29/14 15:55 05/30/14 20:17 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 05/29/14 15:55 05/30/14 20:17 7440-43-9 Chromium ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 20:17 7440-47-3 Cobalt ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 20:17 7440-48-4 Copper ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 20:17 7440-50-8 Lead ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 20:17 7439-92-1 Nickel ND ug/L 50.0 5.0 1 05/29/14 15:55 05/30/14 20:17 7440-02-0 Selenium ND ug/L 10.0 10.0 1 05/29/14 15:55 05/30/14 20:17 7782-49-2 Silver ND ug/L 10.0 5.0 1 05/29/14 15:55 05/30/14 20:17 7440-22-4 Thallium ND ug/L 5.5 5.4 1 05/29/14 15:55 05/30/14 20:17 7440-28-0 Vanadium ND ug/L 25.0 5.0 1 05/29/14 15:55 05/30/14 20:17 7440-62-2 Zinc ND ug/L 10.0 10.0 1 05/29/14 15:55 05/30/14 20:17 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 05/30/14 00:41 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 05/30/14 00:41 107-13-1 Benzene ND ug/L 1.0 0.25 1 05/30/14 00:41 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 05/30/14 00:41 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 05/30/14 00:41 75-27-4 Bromoform ND ug/L 3.0 0.26 1 05/30/14 00:41 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 05/30/14 00:41 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 05/30/14 00:41 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 05/30/14 00:41 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 05/30/14 00:41 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 05/30/14 00:41 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 05/30/14 00:41 75-00-3 Chloroform ND ug/L 5.0 0.14 1 05/30/14 00:41 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 05/30/14 00:41 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 05/30/14 00:41 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 05/30/14 00:41 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 05/30/14 00:41 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 05/30/14 00:41 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 05/30/14 00:41 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 05/30/14 00:41 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 05/30/14 00:41 110-57-6 1,1-Dichloroethane 1.1J ug/L 5.0 0.32 1 05/30/14 00:41 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 05/30/14 00:41 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 05/30/14 00:41 75-35-4 cis-1,2-Dichloroethene 1.OJ ug/L 5.0 0.19 1 05/30/14 00:41 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 05/30/14 00:41 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 05/30/14 00:41 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 05/30/14 00:41 142-28-9 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 05/30/14 00:41 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 13 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-23 Lab ID: 92203121004 Collected: 05/27/14 16:00 Received: 05/28/14 17:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 05/30/14 00:41 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 05/30/14 00:41 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 05/30/14 00:41 591-78-6 lodomethane ND ug/L 10.0 0.32 1 05/30/14 00:41 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 05/30/14 00:41 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 05/30/14 00:41 108-10-1 Styrene ND ug/L 1.0 0.26 1 05/30/14 00:41 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 05/30/14 00:41 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 05/30/14 00:41 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 05/30/14 00:41 127-18-4 Toluene ND ug/L 1.0 0.26 1 05/30/14 00:41 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 05/30/14 00:41 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 05/30/14 00:41 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 05/30/14 00:41 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 05/30/14 00:41 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 05/30/14 00:41 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 05/30/14 00:41 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 05/30/14 00:41 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 05/30/14 00:41 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 05/30/14 00:41 460-00-4 1,2-Dichloroethane-d4 (S) 101 % 70-130 1 05/30/14 00:41 17060-07-0 Toluene-d8 (S) 98 % 70-130 1 05/30/14 00:41 2037-26-5 Date: 06/12/2014 08:20 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 14 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MWA Lab ID: 92203121005 Collected: 05/28/14 08:05 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 5.0 1 06/03/14 12:30 06/04/14 20:08 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:08 7440-38-2 Barium 19.2J ug/L 100 5.0 1 06/03/14 12:30 06/04/14 20:08 7440-39-3 Beryllium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:08 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:08 7440-43-9 Chromium ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:08 7440-47-3 Cobalt ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:08 7440-48-4 Copper ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:08 7440-50-8 Iron 167J ug/L 300 50.0 1 06/03/14 12:30 06/04/14 20:08 7439-89-6 Lead ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:08 7439-92-1 Nickel ND ug/L 50.0 5.0 1 06/03/14 12:30 06/04/14 20:08 7440-02-0 Selenium ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:08 7782-49-2 Silver ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:08 7440-22-4 Thallium ND ug/L 5.5 5.4 1 06/03/14 12:30 06/04/14 20:08 7440-28-0 Vanadium ND ug/L 25.0 5.0 1 06/03/14 12:30 06/04/14 20:08 7440-62-2 Zinc ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:08 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 05/31/14 03:44 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 05/31/14 03:44 107-13-1 Benzene ND ug/L 1.0 0.25 1 05/31/14 03:44 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 05/31/14 03:44 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 05/31/14 03:44 75-27-4 Bromoform ND ug/L 3.0 0.26 1 05/31/14 03:44 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 05/31/14 03:44 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 05/31/14 03:44 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 05/31/14 03:44 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 05/31/14 03:44 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 05/31/14 03:44 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 05/31/14 03:44 75-00-3 Chloroform ND ug/L 5.0 0.14 1 05/31/14 03:44 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 05/31/14 03:44 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 05/31/14 03:44 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 05/31/14 03:44 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 05/31/14 03:44 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 05/31/14 03:44 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 05/31/14 03:44 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 05/31/14 03:44 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 05/31/14 03:44 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 05/31/14 03:44 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 05/31/14 03:44 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 05/31/14 03:44 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 05/31/14 03:44 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 05/31/14 03:44 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 05/31/14 03:44 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 05/31/14 03:44 142-28-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 15 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MWA Lab ID: 92203121005 Collected: 05/28/14 08:05 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 05/31/14 03:44 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 05/31/14 03:44 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 05/31/14 03:44 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 05/31/14 03:44 591-78-6 lodomethane ND ug/L 10.0 0.32 1 05/31/14 03:44 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 05/31/14 03:44 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 05/31/14 03:44 108-10-1 Styrene ND ug/L 1.0 0.26 1 05/31/14 03:44 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 05/31/14 03:44 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 05/31/14 03:44 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 05/31/14 03:44 127-18-4 Toluene ND ug/L 1.0 0.26 1 05/31/14 03:44 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 05/31/14 03:44 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 05/31/14 03:44 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 05/31/14 03:44 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 05/31/14 03:44 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 05/31/14 03:44 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 05/31/14 03:44 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 05/31/14 03:44 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 05/31/14 03:44 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 05/31/14 03:44 460-00-4 1,2-Dichloroethane-d4 (S) 98 % 70-130 1 05/31/14 03:44 17060-07-0 Toluene-d8 (S) 99 % 70-130 1 05/31/14 03:44 2037-26-5 2320E Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 81500 ug/L 5000 1000 1 06/03/14 14:00 4500S2D Sulfide Water Analytical Method: SM 4500-S2D Sulfide ND ug/L 1000 100 1 06/03/14 15:47 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate 7940J ug/L 250000 2000 1 06/03/14 07:53 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E Chloride 3270 ug/L 1000 1000 1 06/11/1418:00 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E Cyanide ND ug/L 10.0 5.0 1 06/09/14 11:11 57-12-5 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand ND ug/L 25000 25000 1 06/10/14 13:40 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 2960 ug/L 1000 1000 1 06/05/14 20:23 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 16 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-7 Lab ID: 92203121006 Collected: 05/28/14 12:00 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony 9.8 ug/L 6.0 5.0 1 06/03/14 12:30 06/04/14 20:11 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:11 7440-38-2 Barium 71.9J ug/L 100 5.0 1 06/03/14 12:30 06/04/14 20:11 7440-39-3 Beryllium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:11 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:11 7440-43-9 Chromium ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:11 7440-47-3 Cobalt 77.3 ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:11 7440-48-4 Copper ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:11 7440-50-8 Iron ND ug/L 300 50.0 1 06/03/14 12:30 06/04/14 20:11 7439-89-6 Lead ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:11 7439-92-1 Nickel ND ug/L 50.0 5.0 1 06/03/14 12:30 06/04/14 20:11 7440-02-0 Selenium ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:11 7782-49-2 Silver ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:11 7440-22-4 Thallium ND ug/L 5.5 5.4 1 06/03/14 12:30 06/04/14 20:11 7440-28-0 Vanadium ND ug/L 25.0 5.0 1 06/03/14 12:30 06/04/14 20:11 7440-62-2 Zinc ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:11 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 05/31/14 03:59 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 05/31/14 03:59 107-13-1 Benzene 0.72J ug/L 1.0 0.25 1 05/31/14 03:59 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 05/31/14 03:59 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 05/31/14 03:59 75-27-4 Bromoform ND ug/L 3.0 0.26 1 05/31/14 03:59 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 05/31/14 03:59 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 05/31/14 03:59 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 05/31/14 03:59 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 05/31/14 03:59 56-23-5 Chlorobenzene 5.7 ug/L 3.0 0.23 1 05/31/14 03:59 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 05/31/14 03:59 75-00-3 Chloroform ND ug/L 5.0 0.14 1 05/31/14 03:59 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 05/31/14 03:59 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 05/31/14 03:59 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 05/31/14 03:59 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 05/31/14 03:59 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 05/31/14 03:59 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 05/31/14 03:59 95-50-1 1,4-Dichlorobenzene 2.7 ug/L 1.0 0.33 1 05/31/14 03:59 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 05/31/14 03:59 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 05/31/14 03:59 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 05/31/14 03:59 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 05/31/14 03:59 75-35-4 cis-1,2-Dichloroethene 0.38J ug/L 5.0 0.19 1 05/31/14 03:59 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 05/31/14 03:59 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 05/31/14 03:59 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 05/31/14 03:59 142-28-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 17 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-7 Lab ID: 92203121006 Collected: 05/28/14 12:00 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 05/31/14 03:59 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 05/31/14 03:59 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 05/31/14 03:59 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 05/31/14 03:59 591-78-6 lodomethane ND ug/L 10.0 0.32 1 05/31/14 03:59 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 05/31/14 03:59 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 05/31/14 03:59 108-10-1 Styrene ND ug/L 1.0 0.26 1 05/31/14 03:59 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 05/31/14 03:59 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 05/31/14 03:59 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 05/31/14 03:59 127-18-4 Toluene ND ug/L 1.0 0.26 1 05/31/14 03:59 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 05/31/14 03:59 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 05/31/14 03:59 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 05/31/14 03:59 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 05/31/14 03:59 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 05/31/14 03:59 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 05/31/14 03:59 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 05/31/14 03:59 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 05/31/14 03:59 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 05/31/14 03:59 460-00-4 1,2-Dichloroethane-d4 (S) 99 % 70-130 1 05/31/14 03:59 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 05/31/14 03:59 2037-26-5 2320E Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 79100 ug/L 5000 1000 1 06/03/14 14:11 4500S2D Sulfide Water Analytical Method: SM 4500-S2D Sulfide ND ug/L 1000 100 1 06/03/14 15:47 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate 6570J ug/L 250000 2000 1 06/03/14 08:06 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E Chloride 28800 ug/L 2000 2000 2 06/11/1418:00 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E Cyanide 5.6J ug/L 10.0 5.0 1 06/09/14 11:12 57-12-5 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 35000 ug/L 25000 25000 1 06/10/14 13:40 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 13900 ug/L 1000 1000 1 06/06/14 00:16 7440-44-0 M1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 18 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-15 Lab ID: 92203121007 Collected: 05/28/14 09:45 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 5.0 1 06/03/14 12:30 06/04/14 20:15 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:15 7440-38-2 Barium 37.5J ug/L 100 5.0 1 06/03/14 12:30 06/04/14 20:15 7440-39-3 Beryllium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:15 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:15 7440-43-9 Chromium ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:15 7440-47-3 Cobalt ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:15 7440-48-4 Copper ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:15 7440-50-8 Iron 2640 ug/L 300 50.0 1 06/03/14 12:30 06/04/14 20:15 7439-89-6 Lead ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:15 7439-92-1 Nickel ND ug/L 50.0 5.0 1 06/03/14 12:30 06/04/14 20:15 7440-02-0 Selenium ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:15 7782-49-2 Silver ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:15 7440-22-4 Thallium ND ug/L 5.5 5.4 1 06/03/14 12:30 06/04/14 20:15 7440-28-0 Vanadium ND ug/L 25.0 5.0 1 06/03/14 12:30 06/04/14 20:15 7440-62-2 Zinc ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:15 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 05/31/14 04:15 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 05/31/14 04:15 107-13-1 Benzene 2.3 ug/L 1.0 0.25 1 05/31/14 04:15 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 05/31/14 04:15 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 05/31/14 04:15 75-27-4 Bromoform ND ug/L 3.0 0.26 1 05/31/14 04:15 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 05/31/14 04:15 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 05/31/14 04:15 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 05/31/14 04:15 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 05/31/14 04:15 56-23-5 Chlorobenzene 2.3J ug/L 3.0 0.23 1 05/31/14 04:15 108-90-7 Chloroethane 0.65J ug/L 10.0 0.54 1 05/31/14 04:15 75-00-3 Chloroform ND ug/L 5.0 0.14 1 05/31/14 04:15 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 05/31/14 04:15 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 05/31/14 04:15 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 05/31/14 04:15 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 05/31/14 04:15 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 05/31/14 04:15 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 05/31/14 04:15 95-50-1 1,4-Dichlorobenzene 3.6 ug/L 1.0 0.33 1 05/31/14 04:15 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 05/31/14 04:15 110-57-6 1,1-Dichloroethane 14.2 ug/L 5.0 0.32 1 05/31/14 04:15 75-34-3 1,2-Dichloroethane 0.58J ug/L 1.0 0.12 1 05/31/14 04:15 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 05/31/14 04:15 75-35-4 cis-1,2-Dichloroethene 35.2 ug/L 5.0 0.19 1 05/31/14 04:15 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 05/31/14 04:15 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 05/31/14 04:15 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 05/31/14 04:15 142-28-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 19 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-15 Lab ID: 92203121007 Collected: 05/28/14 09:45 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 05/31/14 04:15 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 05/31/14 04:15 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 05/31/14 04:15 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 05/31/14 04:15 591-78-6 lodomethane ND ug/L 10.0 0.32 1 05/31/14 04:15 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 05/31/14 04:15 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 05/31/14 04:15 108-10-1 Styrene ND ug/L 1.0 0.26 1 05/31/14 04:15 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 05/31/14 04:15 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 05/31/14 04:15 79-34-5 Tetrachloroethene 0.74J ug/L 1.0 0.46 1 05/31/14 04:15 127-18-4 Toluene ND ug/L 1.0 0.26 1 05/31/14 04:15 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 05/31/14 04:15 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 05/31/14 04:15 79-00-5 Trichloroethene 3.6 ug/L 1.0 0.47 1 05/31/14 04:15 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 05/31/14 04:15 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 05/31/14 04:15 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 05/31/14 04:15 108-05-4 Vinyl chloride 1.9 ug/L 1.0 0.62 1 05/31/14 04:15 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 05/31/14 04:15 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 05/31/14 04:15 460-00-4 1,2-Dichloroethane-d4 (S) 97 % 70-130 1 05/31/14 04:15 17060-07-0 Toluene-d8 (S) 99 % 70-130 1 05/31/14 04:15 2037-26-5 2320E Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 44000 ug/L 5000 1000 1 06/03/14 14:23 4500S2D Sulfide Water Analytical Method: SM 4500-S2D Sulfide ND ug/L 1000 100 1 06/03/14 15:47 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate ND ug/L 250000 2000 1 06/05/14 20:33 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E Chloride 1890 ug/L 1000 1000 1 06/11/1418:01 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E Cyanide ND ug/L 10.0 5.0 1 06/09/14 11:14 57-12-5 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand ND ug/L 25000 25000 1 06/10/14 13:40 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 8670 ug/L 5000 5000 5 06/06/14 10:13 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 20 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-21 Lab ID: 92203121008 Collected: 05/28/14 13:40 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 5.0 1 06/03/14 12:30 06/04/14 20:18 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:18 7440-38-2 Barium 53.4J ug/L 100 5.0 1 06/03/14 12:30 06/04/14 20:18 7440-39-3 Beryllium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:18 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:18 7440-43-9 Chromium ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:18 7440-47-3 Cobalt 5.1J ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:18 7440-48-4 Copper ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:18 7440-50-8 Iron ND ug/L 300 50.0 1 06/03/14 12:30 06/04/14 20:18 7439-89-6 Lead ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:18 7439-92-1 Nickel ND ug/L 50.0 5.0 1 06/03/14 12:30 06/04/14 20:18 7440-02-0 Selenium ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:18 7782-49-2 Silver ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:18 7440-22-4 Thallium ND ug/L 5.5 5.4 1 06/03/14 12:30 06/04/14 20:18 7440-28-0 Vanadium ND ug/L 25.0 5.0 1 06/03/14 12:30 06/04/14 20:18 7440-62-2 Zinc ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:18 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 05/31/14 04:31 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 05/31/14 04:31 107-13-1 Benzene ND ug/L 1.0 0.25 1 05/31/14 04:31 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 05/31/14 04:31 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 05/31/14 04:31 75-27-4 Bromoform ND ug/L 3.0 0.26 1 05/31/14 04:31 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 05/31/14 04:31 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 05/31/14 04:31 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 05/31/14 04:31 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 05/31/14 04:31 56-23-5 Chlorobenzene 0.36J ug/L 3.0 0.23 1 05/31/14 04:31 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 05/31/14 04:31 75-00-3 Chloroform ND ug/L 5.0 0.14 1 05/31/14 04:31 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 05/31/14 04:31 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 05/31/14 04:31 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 05/31/14 04:31 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 05/31/14 04:31 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 05/31/14 04:31 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 05/31/14 04:31 95-50-1 1,4-Dichlorobenzene 0.75J ug/L 1.0 0.33 1 05/31/14 04:31 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 05/31/14 04:31 110-57-6 1,1-Dichloroethane 6.3 ug/L 5.0 0.32 1 05/31/14 04:31 75-34-3 1,2-Dichloroethane 0.42J ug/L 1.0 0.12 1 05/31/14 04:31 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 05/31/14 04:31 75-35-4 cis-1,2-Dichloroethene 20.1 ug/L 5.0 0.19 1 05/31/14 04:31 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 05/31/14 04:31 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 05/31/14 04:31 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 05/31/14 04:31 142-28-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 21 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-21 Lab ID: 92203121008 Collected: 05/28/14 13:40 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 05/31/14 04:31 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 05/31/14 04:31 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 05/31/14 04:31 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 05/31/14 04:31 591-78-6 lodomethane ND ug/L 10.0 0.32 1 05/31/14 04:31 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 05/31/14 04:31 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 05/31/14 04:31 108-10-1 Styrene ND ug/L 1.0 0.26 1 05/31/14 04:31 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 05/31/14 04:31 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 05/31/14 04:31 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 05/31/14 04:31 127-18-4 Toluene ND ug/L 1.0 0.26 1 05/31/14 04:31 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 05/31/14 04:31 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 05/31/14 04:31 79-00-5 Trichloroethene 1.5 ug/L 1.0 0.47 1 05/31/14 04:31 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 05/31/14 04:31 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 05/31/14 04:31 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 05/31/14 04:31 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 05/31/14 04:31 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 05/31/14 04:31 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 05/31/14 04:31 460-00-4 1,2-Dichloroethane-d4 (S) 97 % 70-130 1 05/31/14 04:31 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 05/31/14 04:31 2037-26-5 2320E Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 34500 ug/L 5000 1000 1 06/03/14 14:54 4500S2D Sulfide Water Analytical Method: SM 4500-S2D Sulfide ND ug/L 1000 100 1 06/03/14 15:47 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate ND ug/L 250000 2000 1 06/05/14 20:47 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E Chloride 27600 ug/L 1000 1000 1 06/11/1418:02 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E Cyanide ND ug/L 10.0 5.0 1 06/09/14 11:17 57-12-5 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand ND ug/L 25000 25000 1 06/10/14 13:40 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 10700 ug/L 1000 1000 1 06/06/14 00:53 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 22 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-9 Lab ID: 92203121009 Collected: 05/28/14 11:35 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 5.0 1 06/03/14 12:30 06/04/14 20:21 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:21 7440-38-2 Barium 59.2J ug/L 100 5.0 1 06/03/14 12:30 06/04/14 20:21 7440-39-3 Beryllium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:21 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:21 7440-43-9 Chromium ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:21 7440-47-3 Cobalt 140 ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:21 7440-48-4 Copper ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:21 7440-50-8 Iron 44900 ug/L 300 50.0 1 06/03/14 12:30 06/04/14 20:21 7439-89-6 Lead ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:21 7439-92-1 Nickel ND ug/L 50.0 5.0 1 06/03/14 12:30 06/04/14 20:21 7440-02-0 Selenium ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:21 7782-49-2 Silver ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:21 7440-22-4 Thallium ND ug/L 5.5 5.4 1 06/03/14 12:30 06/04/14 20:21 7440-28-0 Vanadium ND ug/L 25.0 5.0 1 06/03/14 12:30 06/04/14 20:21 7440-62-2 Zinc ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:21 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 05/31/14 04:46 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 05/31/14 04:46 107-13-1 Benzene 3.3 ug/L 1.0 0.25 1 05/31/14 04:46 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 05/31/14 04:46 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 05/31/14 04:46 75-27-4 Bromoform ND ug/L 3.0 0.26 1 05/31/14 04:46 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 05/31/14 04:46 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 05/31/14 04:46 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 05/31/14 04:46 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 05/31/14 04:46 56-23-5 Chlorobenzene 2.4J ug/L 3.0 0.23 1 05/31/14 04:46 108-90-7 Chloroethane 1.9J ug/L 10.0 0.54 1 05/31/14 04:46 75-00-3 Chloroform ND ug/L 5.0 0.14 1 05/31/14 04:46 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 05/31/14 04:46 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 05/31/14 04:46 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 05/31/14 04:46 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 05/31/14 04:46 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 05/31/14 04:46 74-95-3 1,2-Dichlorobenzene 2.1J ug/L 5.0 0.30 1 05/31/14 04:46 95-50-1 1,4-Dichlorobenzene 6.6 ug/L 1.0 0.33 1 05/31/14 04:46 106-46-7 trans-1,4-DichIoro-2-butene ND ug/L 100 1.0 1 05/31/14 04:46 110-57-6 1,1-Dichloroethane 2.7J ug/L 5.0 0.32 1 05/31/14 04:46 75-34-3 1,2-Dichloroethane 0.23J ug/L 1.0 0.12 1 05/31/14 04:46 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 05/31/14 04:46 75-35-4 cis-1,2-Dichloroethene 5.7 ug/L 5.0 0.19 1 05/31/14 04:46 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 05/31/14 04:46 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 05/31/14 04:46 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 05/31/14 04:46 142-28-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 23 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-9 Lab ID: 92203121009 Collected: 05/28/14 11:35 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 05/31/14 04:46 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 05/31/14 04:46 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 05/31/14 04:46 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 05/31/14 04:46 591-78-6 lodomethane ND ug/L 10.0 0.32 1 05/31/14 04:46 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 05/31/14 04:46 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 05/31/14 04:46 108-10-1 Styrene ND ug/L 1.0 0.26 1 05/31/14 04:46 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 05/31/14 04:46 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 05/31/14 04:46 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 05/31/14 04:46 127-18-4 Toluene ND ug/L 1.0 0.26 1 05/31/14 04:46 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 05/31/14 04:46 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 05/31/14 04:46 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 05/31/14 04:46 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 05/31/14 04:46 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 05/31/14 04:46 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 05/31/14 04:46 108-05-4 Vinyl chloride 10.8 ug/L 1.0 0.62 1 05/31/14 04:46 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 05/31/14 04:46 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 05/31/14 04:46 460-00-4 1,2-Dichloroethane-d4 (S) 99 % 70-130 1 05/31/14 04:46 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 05/31/14 04:46 2037-26-5 2320E Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 112000 ug/L 5000 1000 1 06/03/14 15:28 4500S2D Sulfide Water Analytical Method: SM 4500-S2D Sulfide ND ug/L 1000 100 1 06/03/14 15:53 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate ND ug/L 250000 2000 1 06/05/14 21:00 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E Chloride 45100 ug/L 5000 5000 5 06/11/1418:02 16887-00-6 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 33000 ug/L 25000 25000 1 06/10/14 13:40 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 8070 ug/L 1000 1000 1 06/06/14 01:04 7440-44-0 Date: 06/12/2014 08:20 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 24 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-14 Lab ID: 92203121010 Collected: 05/28/14 10:15 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 5.0 1 06/03/14 12:30 06/04/14 20:24 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:24 7440-38-2 Barium 22.4J ug/L 100 5.0 1 06/03/14 12:30 06/04/14 20:24 7440-39-3 Beryllium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:24 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:24 7440-43-9 Chromium ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:24 7440-47-3 Cobalt ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:24 7440-48-4 Copper ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:24 7440-50-8 Iron 245J ug/L 300 50.0 1 06/03/14 12:30 06/04/14 20:24 7439-89-6 Lead ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:24 7439-92-1 Nickel ND ug/L 50.0 5.0 1 06/03/14 12:30 06/04/14 20:24 7440-02-0 Selenium ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:24 7782-49-2 Silver ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:24 7440-22-4 Thallium ND ug/L 5.5 5.4 1 06/03/14 12:30 06/04/14 20:24 7440-28-0 Vanadium ND ug/L 25.0 5.0 1 06/03/14 12:30 06/04/14 20:24 7440-62-2 Zinc ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:24 7440-66-6 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury 0.14J ug/L 0.20 0.10 1 06/02/14 19:45 06/03/14 18:41 7439-97-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 05/31/14 05:02 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 05/31/14 05:02 107-13-1 Benzene ND ug/L 1.0 0.25 1 05/31/14 05:02 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 05/31/14 05:02 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 05/31/14 05:02 75-27-4 Bromoform ND ug/L 3.0 0.26 1 05/31/14 05:02 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 05/31/14 05:02 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 05/31/14 05:02 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 05/31/14 05:02 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 05/31/14 05:02 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 05/31/14 05:02 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 05/31/14 05:02 75-00-3 Chloroform ND ug/L 5.0 0.14 1 05/31/14 05:02 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 05/31/14 05:02 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 05/31/14 05:02 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 05/31/14 05:02 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 05/31/14 05:02 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 05/31/14 05:02 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 05/31/14 05:02 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 05/31/14 05:02 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 05/31/14 05:02 110-57-6 1,1-Dichloroethane 3.6J ug/L 5.0 0.32 1 05/31/14 05:02 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 05/31/14 05:02 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 05/31/14 05:02 75-35-4 cis-1,2-Dichloroethene 4.8J ug/L 5.0 0.19 1 05/31/14 05:02 156-59-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 25 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-14 Lab ID: 92203121010 Collected: 05/28/14 10:15 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320E Alkalinity Alkalinity, Total as CaCO3 4500S2D Sulfide Water Sulfide 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 5220D COD Chemical Oxygen Demand 5310B TOC Total Organic Carbon Date: 06/12/2014 08:20 AM Analytical Method: EPA 8260 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 100 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 3.0 0.89J ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 0.77J ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 1.0 ND ug/L 5.0 99 % 70-130 97 % 70-130 100 % 70-130 Analytical Method: SM 2320B 32400 ug/L 5000 Analytical Method: SM 4500-S2D ND ug/L 1000 Analytical Method: EPA 300.0 2210J ug/L 250000 Analytical Method: SM 4500-CI-E 2710 ug/L 1000 Analytical Method: SM 5220D ND ug/L 25000 Analytical Method: SM 5310B 5660 ug/L 1000 0.49 1 05/31/14 05:02 156-60-5 0.27 1 05/31/14 05:02 78-87-5 0.28 1 05/31/14 05:02 142-28-9 0.13 1 05/31/14 05:02 10061-01-5 0.26 1 05/31/14 05:02 10061-02-6 0.30 1 05/31/14 05:02 100-41-4 0.46 1 05/31/14 05:02 591-78-6 0.32 1 05/31/14 05:02 74-88-4 0.97 1 05/31/14 05:02 75-09-2 0.33 1 05/31/14 05:02 108-10-1 0.26 1 05/31/14 05:02 100-42-5 0.33 1 05/31/14 05:02 630-20-6 0.40 1 05/31/14 05:02 79-34-5 0.46 1 05/31/14 05:02 127-18-4 0.26 1 05/31/14 05:02 108-88-3 0.48 1 05/31/14 05:02 71-55-6 0.29 1 05/31/14 05:02 79-00-5 0.47 1 05/31/14 05:02 79-01-6 0.20 1 05/31/14 05:02 75-69-4 0.41 1 05/31/14 05:02 96-18-4 0.35 1 05/31/14 05:02 108-05-4 0.62 1 05/31/14 05:02 75-01-4 0.66 1 05/31/14 05:02 1330-20-7 1 05/31/14 05:02 460-00-4 1 05/31/14 05:02 17060-07-0 1 05/31/14 05:02 2037-26-5 1000 1 06/03/14 15:41 100 1 06/03/14 15:53 18496-25-8 2000 1 06/05/14 21:41 14808-79-8 1000 1 06/11 /14 18:04 16887-00-6 25000 1 i[�AAiI REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 06/10/14 13:40 Page 26 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-3R Lab ID: 92203121011 Collected: 05/28/14 08:40 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 5.0 1 06/03/14 12:30 06/04/14 20:27 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:27 7440-38-2 Barium 6.1J ug/L 100 5.0 1 06/03/14 12:30 06/04/14 20:27 7440-39-3 Beryllium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:27 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:27 7440-43-9 Chromium ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:27 7440-47-3 Cobalt ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:27 7440-48-4 Copper ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:27 7440-50-8 Lead ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:27 7439-92-1 Nickel ND ug/L 50.0 5.0 1 06/03/14 12:30 06/04/14 20:27 7440-02-0 Selenium ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:27 7782-49-2 Silver ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:27 7440-22-4 Thallium ND ug/L 5.5 5.4 1 06/03/14 12:30 06/04/14 20:27 7440-28-0 Vanadium ND ug/L 25.0 5.0 1 06/03/14 12:30 06/04/14 20:27 7440-62-2 Zinc ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:27 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 05/31/14 05:17 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 05/31/14 05:17 107-13-1 Benzene ND ug/L 1.0 0.25 1 05/31/14 05:17 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 05/31/14 05:17 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 05/31/14 05:17 75-27-4 Bromoform ND ug/L 3.0 0.26 1 05/31/14 05:17 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 05/31/14 05:17 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 05/31/14 05:17 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 05/31/14 05:17 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 05/31/14 05:17 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 05/31/14 05:17 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 05/31/14 05:17 75-00-3 Chloroform ND ug/L 5.0 0.14 1 05/31/14 05:17 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 05/31/14 05:17 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 05/31/14 05:17 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 05/31/14 05:17 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 05/31/14 05:17 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 05/31/14 05:17 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 05/31/14 05:17 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 05/31/14 05:17 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 05/31/14 05:17 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 05/31/14 05:17 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 05/31/14 05:17 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 05/31/14 05:17 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 05/31/14 05:17 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 05/31/14 05:17 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 05/31/14 05:17 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 05/31/14 05:17 142-28-9 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 05/31/14 05:17 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 27 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-3R Lab ID: 92203121011 Collected: 05/28/14 08:40 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 05/31/14 05:17 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 05/31/14 05:17 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 05/31/14 05:17 591-78-6 lodomethane ND ug/L 10.0 0.32 1 05/31/14 05:17 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 05/31/14 05:17 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 05/31/14 05:17 108-10-1 Styrene ND ug/L 1.0 0.26 1 05/31/14 05:17 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 05/31/14 05:17 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 05/31/14 05:17 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 05/31/14 05:17 127-18-4 Toluene ND ug/L 1.0 0.26 1 05/31/14 05:17 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 05/31/14 05:17 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 05/31/14 05:17 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 05/31/14 05:17 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 05/31/14 05:17 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 05/31/14 05:17 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 05/31/14 05:17 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 05/31/14 05:17 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 05/31/14 05:17 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 05/31/14 05:17 460-00-4 1,2-Dichloroethane-d4 (S) 98 % 70-130 1 05/31/14 05:17 17060-07-0 Toluene-d8 (S) 99 % 70-130 1 05/31/14 05:17 2037-26-5 Date: 06/12/2014 08:20 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 28 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-13 Lab ID: 92203121012 Collected: 05/28/14 11:00 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 5.0 1 06/03/14 12:30 06/04/14 20:31 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:31 7440-38-2 Barium 55.7J ug/L 100 5.0 1 06/03/14 12:30 06/04/14 20:31 7440-39-3 Beryllium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:31 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:31 7440-43-9 Chromium ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:31 7440-47-3 Cobalt 7.4J ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:31 7440-48-4 Copper ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:31 7440-50-8 Lead ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:31 7439-92-1 Nickel ND ug/L 50.0 5.0 1 06/03/14 12:30 06/04/14 20:31 7440-02-0 Selenium ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:31 7782-49-2 Silver ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:31 7440-22-4 Thallium ND ug/L 5.5 5.4 1 06/03/14 12:30 06/04/14 20:31 7440-28-0 Vanadium ND ug/L 25.0 5.0 1 06/03/14 12:30 06/04/14 20:31 7440-62-2 Zinc ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:31 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 05/31/14 05:33 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 05/31/14 05:33 107-13-1 Benzene ND ug/L 1.0 0.25 1 05/31/14 05:33 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 05/31/14 05:33 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 05/31/14 05:33 75-27-4 Bromoform ND ug/L 3.0 0.26 1 05/31/14 05:33 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 05/31/14 05:33 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 05/31/14 05:33 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 05/31/14 05:33 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 05/31/14 05:33 56-23-5 Chlorobenzene 0.24J ug/L 3.0 0.23 1 05/31/14 05:33 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 05/31/14 05:33 75-00-3 Chloroform ND ug/L 5.0 0.14 1 05/31/14 05:33 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 05/31/14 05:33 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 05/31/14 05:33 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 05/31/14 05:33 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 05/31/14 05:33 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 05/31/14 05:33 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 05/31/14 05:33 95-50-1 1,4-Dichlorobenzene 0.51J ug/L 1.0 0.33 1 05/31/14 05:33 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 05/31/14 05:33 110-57-6 1,1-Dichloroethane 4.4J ug/L 5.0 0.32 1 05/31/14 05:33 75-34-3 1,2-Dichloroethane 0.47J ug/L 1.0 0.12 1 05/31/14 05:33 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 05/31/14 05:33 75-35-4 cis-1,2-Dichloroethene 19.3 ug/L 5.0 0.19 1 05/31/14 05:33 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 05/31/14 05:33 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 05/31/14 05:33 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 05/31/14 05:33 142-28-9 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 05/31/14 05:33 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 29 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-13 Lab ID: 92203121012 Collected: 05/28/14 11:00 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 05/31/14 05:33 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 05/31/14 05:33 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 05/31/14 05:33 591-78-6 lodomethane ND ug/L 10.0 0.32 1 05/31/14 05:33 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 05/31/14 05:33 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 05/31/14 05:33 108-10-1 Styrene ND ug/L 1.0 0.26 1 05/31/14 05:33 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 05/31/14 05:33 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 05/31/14 05:33 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 05/31/14 05:33 127-18-4 Toluene ND ug/L 1.0 0.26 1 05/31/14 05:33 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 05/31/14 05:33 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 05/31/14 05:33 79-00-5 Trichloroethene 1.2 ug/L 1.0 0.47 1 05/31/14 05:33 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 05/31/14 05:33 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 05/31/14 05:33 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 05/31/14 05:33 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 05/31/14 05:33 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 05/31/14 05:33 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 05/31/14 05:33 460-00-4 1,2-Dichloroethane-d4 (S) 99 % 70-130 1 05/31/14 05:33 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 05/31/14 05:33 2037-26-5 Date: 06/12/2014 08:20 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 30 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-17 Lab ID: 92203121013 Collected: 05/28/14 15:10 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony 5.5J ug/L 6.0 5.0 1 06/03/14 12:30 06/04/14 20:34 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:34 7440-38-2 Barium 57.8J ug/L 100 5.0 1 06/03/14 12:30 06/04/14 20:34 7440-39-3 Beryllium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:34 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:34 7440-43-9 Chromium ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:34 7440-47-3 Cobalt 44.3 ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:34 7440-48-4 Copper ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:34 7440-50-8 Lead ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:34 7439-92-1 Nickel 8.9J ug/L 50.0 5.0 1 06/03/14 12:30 06/04/14 20:34 7440-02-0 Selenium ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:34 7782-49-2 Silver ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:34 7440-22-4 Thallium ND ug/L 5.5 5.4 1 06/03/14 12:30 06/04/14 20:34 7440-28-0 Vanadium ND ug/L 25.0 5.0 1 06/03/14 12:30 06/04/14 20:34 7440-62-2 Zinc ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:34 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 05/31/14 05:49 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 05/31/14 05:49 107-13-1 Benzene ND ug/L 1.0 0.25 1 05/31/14 05:49 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 05/31/14 05:49 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 05/31/14 05:49 75-27-4 Bromoform ND ug/L 3.0 0.26 1 05/31/14 05:49 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 05/31/14 05:49 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 05/31/14 05:49 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 05/31/14 05:49 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 05/31/14 05:49 56-23-5 Chlorobenzene 0.29J ug/L 3.0 0.23 1 05/31/14 05:49 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 05/31/14 05:49 75-00-3 Chloroform ND ug/L 5.0 0.14 1 05/31/14 05:49 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 05/31/14 05:49 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 05/31/14 05:49 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 05/31/14 05:49 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 05/31/14 05:49 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 05/31/14 05:49 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 05/31/14 05:49 95-50-1 1,4-Dichlorobenzene 0.44J ug/L 1.0 0.33 1 05/31/14 05:49 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 05/31/14 05:49 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 05/31/14 05:49 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 05/31/14 05:49 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 05/31/14 05:49 75-35-4 cis-1,2-Dichloroethene 0.55J ug/L 5.0 0.19 1 05/31/14 05:49 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 05/31/14 05:49 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 05/31/14 05:49 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 05/31/14 05:49 142-28-9 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 05/31/14 05:49 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 31 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-17 Lab ID: 92203121013 Collected: 05/28/14 15:10 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 05/31/14 05:49 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 05/31/14 05:49 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 05/31/14 05:49 591-78-6 lodomethane ND ug/L 10.0 0.32 1 05/31/14 05:49 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 05/31/14 05:49 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 05/31/14 05:49 108-10-1 Styrene ND ug/L 1.0 0.26 1 05/31/14 05:49 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 05/31/14 05:49 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 05/31/14 05:49 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 05/31/14 05:49 127-18-4 Toluene ND ug/L 1.0 0.26 1 05/31/14 05:49 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 05/31/14 05:49 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 05/31/14 05:49 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 05/31/14 05:49 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 05/31/14 05:49 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 05/31/14 05:49 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 05/31/14 05:49 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 05/31/14 05:49 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 05/31/14 05:49 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 05/31/14 05:49 460-00-4 1,2-Dichloroethane-d4 (S) 97 % 70-130 1 05/31/14 05:49 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 05/31/14 05:49 2037-26-5 Date: 06/12/2014 08:20 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 32 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-20 Lab ID: 92203121014 Collected: 05/27/14 06:05 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 5.0 1 06/03/14 12:30 06/04/14 20:37 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:37 7440-38-2 Barium 23.4J ug/L 100 5.0 1 06/03/14 12:30 06/04/14 20:37 7440-39-3 Beryllium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:37 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:37 7440-43-9 Chromium ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:37 7440-47-3 Cobalt 14.2 ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:37 7440-48-4 Copper 7.8J ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:37 7440-50-8 Lead ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:37 7439-92-1 Nickel ND ug/L 50.0 5.0 1 06/03/14 12:30 06/04/14 20:37 7440-02-0 Selenium ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:37 7782-49-2 Silver ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:37 7440-22-4 Thallium ND ug/L 5.5 5.4 1 06/03/14 12:30 06/04/14 20:37 7440-28-0 Vanadium ND ug/L 25.0 5.0 1 06/03/14 12:30 06/04/14 20:37 7440-62-2 Zinc ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:37 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 05/31/14 06:35 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 05/31/14 06:35 107-13-1 Benzene ND ug/L 1.0 0.25 1 05/31/14 06:35 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 05/31/14 06:35 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 05/31/14 06:35 75-27-4 Bromoform ND ug/L 3.0 0.26 1 05/31/14 06:35 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 05/31/14 06:35 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 05/31/14 06:35 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 05/31/14 06:35 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 05/31/14 06:35 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 05/31/14 06:35 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 05/31/14 06:35 75-00-3 Chloroform ND ug/L 5.0 0.14 1 05/31/14 06:35 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 05/31/14 06:35 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 05/31/14 06:35 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 05/31/14 06:35 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 05/31/14 06:35 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 05/31/14 06:35 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 05/31/14 06:35 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 05/31/14 06:35 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 05/31/14 06:35 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 05/31/14 06:35 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 05/31/14 06:35 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 05/31/14 06:35 75-35-4 cis-1,2-Dichloroethene 0.78J ug/L 5.0 0.19 1 05/31/14 06:35 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 05/31/14 06:35 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 05/31/14 06:35 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 05/31/14 06:35 142-28-9 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 05/31/14 06:35 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 33 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-20 Lab ID: 92203121014 Collected: 05/27/14 06:05 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 05/31/14 06:35 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 05/31/14 06:35 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 05/31/14 06:35 591-78-6 lodomethane ND ug/L 10.0 0.32 1 05/31/14 06:35 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 05/31/14 06:35 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 05/31/14 06:35 108-10-1 Styrene ND ug/L 1.0 0.26 1 05/31/14 06:35 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 05/31/14 06:35 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 05/31/14 06:35 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 05/31/14 06:35 127-18-4 Toluene ND ug/L 1.0 0.26 1 05/31/14 06:35 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 05/31/14 06:35 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 05/31/14 06:35 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 05/31/14 06:35 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 05/31/14 06:35 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 05/31/14 06:35 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 05/31/14 06:35 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 05/31/14 06:35 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 05/31/14 06:35 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 05/31/14 06:35 460-00-4 1,2-Dichloroethane-d4 (S) 99 % 70-130 1 05/31/14 06:35 17060-07-0 Toluene-d8 (S) 99 % 70-130 1 05/31/14 06:35 2037-26-5 Date: 06/12/2014 08:20 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 34 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-16 Lab ID: 92203121015 Collected: 05/28/14 09:10 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony 15.9 ug/L 6.0 5.0 1 06/03/14 12:30 06/04/14 20:49 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:49 7440-38-2 Barium 117 ug/L 100 5.0 1 06/03/14 12:30 06/04/14 20:49 7440-39-3 Beryllium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:49 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:49 7440-43-9 Chromium 8.9J ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:49 7440-47-3 Cobalt 325 ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:49 7440-48-4 Copper ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:49 7440-50-8 Lead ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:49 7439-92-1 Nickel 18.8J ug/L 50.0 5.0 1 06/03/14 12:30 06/04/14 20:49 7440-02-0 Selenium ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:49 7782-49-2 Silver ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:49 7440-22-4 Thallium 9.5 ug/L 5.5 5.4 1 06/03/14 12:30 06/04/14 20:49 7440-28-0 Vanadium ND ug/L 25.0 5.0 1 06/03/14 12:30 06/04/14 20:49 7440-62-2 Zinc 13.5 ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:49 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 05/31/14 06:04 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 05/31/14 06:04 107-13-1 Benzene 1.8 ug/L 1.0 0.25 1 05/31/14 06:04 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 05/31/14 06:04 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 05/31/14 06:04 75-27-4 Bromoform ND ug/L 3.0 0.26 1 05/31/14 06:04 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 05/31/14 06:04 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 05/31/14 06:04 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 05/31/14 06:04 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 05/31/14 06:04 56-23-5 Chlorobenzene 5.8 ug/L 3.0 0.23 1 05/31/14 06:04 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 05/31/14 06:04 75-00-3 Chloroform ND ug/L 5.0 0.14 1 05/31/14 06:04 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 05/31/14 06:04 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 05/31/14 06:04 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 05/31/14 06:04 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 05/31/14 06:04 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 05/31/14 06:04 74-95-3 1,2-Dichlorobenzene 1.8J ug/L 5.0 0.30 1 05/31/14 06:04 95-50-1 1,3-Dichlorobenzene 0.29J ug/L 5.0 0.24 1 05/31/14 06:04 541-73-1 1,4-Dichlorobenzene 15.0 ug/L 1.0 0.33 1 05/31/14 06:04 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 05/31/14 06:04 110-57-6 1,1-Dichloroethane 2.8J ug/L 5.0 0.32 1 05/31/14 06:04 75-34-3 1,2-Dichloroethane 2.4 ug/L 1.0 0.12 1 05/31/14 06:04 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 05/31/14 06:04 75-35-4 cis-1,2-Dichloroethene 46.6 ug/L 5.0 0.19 1 05/31/14 06:04 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 05/31/14 06:04 156-60-5 1,2-Dichloropropane 3.2 ug/L 1.0 0.27 1 05/31/14 06:04 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 05/31/14 06:04 142-28-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 35 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-16 Lab ID: 92203121015 Collected: 05/28/14 09:10 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 4500CNE Cyanide, Total Cyanide Date: 06/12/2014 08:20 AM Analytical Method: EPA 8260 N D ug/L 1.0 0.13 1 05/31/14 06:04 10061-01-5 ND ug/L 1.0 0.26 1 05/31/14 06:04 10061-02-6 ND ug/L 1.0 0.30 1 05/31/14 06:04 100-41-4 ND ug/L 50.0 0.46 1 05/31/14 06:04 591-78-6 ND ug/L 10.0 0.32 1 05/31/14 06:04 74-88-4 ND ug/L 1.0 0.97 1 05/31/14 06:04 75-09-2 ND ug/L 100 0.33 1 05/31/14 06:04 108-10-1 ND ug/L 1.0 0.26 1 05/31/14 06:04 100-42-5 ND ug/L 5.0 0.33 1 05/31/14 06:04 630-20-6 ND ug/L 3.0 0.40 1 05/31/14 06:04 79-34-5 ND ug/L 1.0 0.46 1 05/31/14 06:04 127-18-4 ND ug/L 1.0 0.26 1 05/31/14 06:04 108-88-3 ND ug/L 1.0 0.48 1 05/31/14 06:04 71-55-6 ND ug/L 1.0 0.29 1 05/31/14 06:04 79-00-5 0.89J ug/L 1.0 0.47 1 05/31/14 06:04 79-01-6 ND ug/L 1.0 0.20 1 05/31/14 06:04 75-69-4 ND ug/L 1.0 0.41 1 05/31/14 06:04 96-18-4 ND ug/L 50.0 0.35 1 05/31/14 06:04 108-05-4 6.7 ug/L 1.0 0.62 1 05/31/14 06:04 75-01-4 ND ug/L 5.0 0.66 1 05/31/14 06:04 1330-20-7 100 % 70-130 1 05/31/14 06:04 460-00-4 97 % 70-130 1 05/31/14 06:04 17060-07-0 100 % 70-130 1 05/31/14 06:04 2037-26-5 Analytical Method: SM 4500-CN-E 11.0 ug/L 10.0 5.0 1 06/09/14 11:18 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 36 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-22 Lab ID: 92203121016 Collected: 05/28/14 14:35 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 5.0 1 06/03/14 12:30 06/04/14 20:53 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:53 7440-38-2 Barium 65.2J ug/L 100 5.0 1 06/03/14 12:30 06/04/14 20:53 7440-39-3 Beryllium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:53 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:53 7440-43-9 Chromium ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:53 7440-47-3 Cobalt 37.3 ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:53 7440-48-4 Copper ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:53 7440-50-8 Lead ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:53 7439-92-1 Nickel ND ug/L 50.0 5.0 1 06/03/14 12:30 06/04/14 20:53 7440-02-0 Selenium ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:53 7782-49-2 Silver ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:53 7440-22-4 Thallium ND ug/L 5.5 5.4 1 06/03/14 12:30 06/04/14 20:53 7440-28-0 Vanadium ND ug/L 25.0 5.0 1 06/03/14 12:30 06/04/14 20:53 7440-62-2 Zinc ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:53 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 05/31/14 06:51 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 05/31/14 06:51 107-13-1 Benzene 0.42J ug/L 1.0 0.25 1 05/31/14 06:51 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 05/31/14 06:51 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 05/31/14 06:51 75-27-4 Bromoform ND ug/L 3.0 0.26 1 05/31/14 06:51 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 05/31/14 06:51 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 05/31/14 06:51 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 05/31/14 06:51 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 05/31/14 06:51 56-23-5 Chlorobenzene 0.97J ug/L 3.0 0.23 1 05/31/14 06:51 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 05/31/14 06:51 75-00-3 Chloroform ND ug/L 5.0 0.14 1 05/31/14 06:51 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 05/31/14 06:51 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 05/31/14 06:51 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 05/31/14 06:51 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 05/31/14 06:51 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 05/31/14 06:51 74-95-3 1,2-Dichlorobenzene 0.35J ug/L 5.0 0.30 1 05/31/14 06:51 95-50-1 1,4-Dichlorobenzene 2.4 ug/L 1.0 0.33 1 05/31/14 06:51 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 05/31/14 06:51 110-57-6 1,1-Dichloroethane 1.4J ug/L 5.0 0.32 1 05/31/14 06:51 75-34-3 1,2-Dichloroethane 0.51J ug/L 1.0 0.12 1 05/31/14 06:51 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 05/31/14 06:51 75-35-4 cis-1,2-Dichloroethene 3.2J ug/L 5.0 0.19 1 05/31/14 06:51 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 05/31/14 06:51 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 05/31/14 06:51 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 05/31/14 06:51 142-28-9 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 05/31/14 06:51 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 37 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-22 Lab ID: 92203121016 Collected: 05/28/14 14:35 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 05/31/14 06:51 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 05/31/14 06:51 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 05/31/14 06:51 591-78-6 lodomethane ND ug/L 10.0 0.32 1 05/31/14 06:51 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 05/31/14 06:51 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 05/31/14 06:51 108-10-1 Styrene ND ug/L 1.0 0.26 1 05/31/14 06:51 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 05/31/14 06:51 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 05/31/14 06:51 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 05/31/14 06:51 127-18-4 Toluene ND ug/L 1.0 0.26 1 05/31/14 06:51 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 05/31/14 06:51 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 05/31/14 06:51 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 05/31/14 06:51 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 05/31/14 06:51 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 05/31/14 06:51 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 05/31/14 06:51 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 05/31/14 06:51 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 05/31/14 06:51 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 05/31/14 06:51 460-00-4 1,2-Dichloroethane-d4 (S) 97 % 70-130 1 05/31/14 06:51 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 05/31/14 06:51 2037-26-5 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E Cyanide ND ug/L 10.0 5.0 1 06/09/14 11:19 57-12-5 Date: 06/12/2014 08:20 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 38 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Sample: MW-19 Lab ID: 92203121017 Collected: 05/27/14 15:10 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E Cyanide ND ug/L 10.0 5.0 1 06/09/14 10:40 57-12-5 Date: 06/12/2014 08:20 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 39 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 QC Batch: MERP/6689 Analysis Method: EPA 7470 QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury Associated Lab Samples: 92203121010 METHOD BLANK: 1212169 Matrix: Water Associated Lab Samples: 92203121010 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury ug/L ND 0.20 06/03/1418:36 LABORATORY CONTROL SAMPLE: 1212170 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.7 109 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1212171 1212172 MS MSD 92203121010 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Mercury ug/L 0.14J 2.5 2.5 2.7 2.6 101 100 75-125 0 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 40 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 QC Batch: MPRP/16067 Analysis Method: EPA6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET NC Groundwater Associated Lab Samples: 92203121001, 92203121002, 92203121003, 92203121004 METHOD BLANK: 1208932 Matrix: Water Associated Lab Samples: 92203121001, 92203121002, 92203121003, 92203121004 Blank Reporting Parameter Units Result Limit Analyzed Antimony ug/L ND 6.0 05/30/1419:41 Arsenic ug/L ND 10.0 05/30/1419:41 Barium ug/L ND 100 05/30/1419:41 Beryllium ug/L ND 1.0 05/30/1419:41 Cadmium ug/L ND 1.0 05/30/1419:41 Chromium ug/L ND 10.0 05/30/1419:41 Cobalt ug/L ND 10.0 05/30/1419:41 Copper ug/L ND 10.0 05/30/1419:41 Lead ug/L ND 10.0 05/30/1419:41 Nickel ug/L ND 50.0 05/30/1419:41 Selenium ug/L ND 10.0 05/30/1419:41 Silver ug/L ND 10.0 05/30/1419:41 Thallium ug/L ND 5.5 05/30/1419:41 Vanadium ug/L ND 25.0 05/30/1419:41 Zinc ug/L ND 10.0 05/30/1419:41 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 1208933 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 500 492 98 80-120 Arsenic ug/L 500 467 93 80-120 Barium ug/L 500 483 97 80-120 Beryllium ug/L 500 451 90 80-120 Cadmium ug/L 500 466 93 80-120 Chromium ug/L 500 465 93 80-120 Cobalt ug/L 500 480 96 80-120 Copper ug/L 500 466 93 80-120 Lead ug/L 500 475 95 80-120 Nickel ug/L 500 463 93 80-120 Selenium ug/L 500 480 96 80-120 Silver ug/L 250 234 93 80-120 Thallium ug/L 500 458 92 80-120 Vanadium ug/L 500 457 91 80-120 Zinc ug/L 500 457 91 80-120 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 41 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: Surry Closed -Mt. Airy (UIC) 92203121 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1208934 1208935 MS MSD 92203116001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 507 509 101 102 75-125 0 25 Arsenic ug/L ND 500 500 480 485 96 97 75-125 1 25 Barium ug/L 6.1J 500 500 494 501 98 99 75-125 2 25 Beryllium ug/L ND 500 500 461 469 92 94 75-125 2 25 Cadmium ug/L ND 500 500 477 481 95 96 75-125 1 25 Chromium ug/L ND 500 500 472 484 94 97 75-125 2 25 Cobalt ug/L ND 500 500 482 490 96 98 75-125 2 25 Copper ug/L ND 500 500 478 485 96 97 75-125 1 25 Lead ug/L ND 500 500 476 485 95 97 75-125 2 25 Nickel ug/L ND 500 500 467 475 93 95 75-125 2 25 Selenium ug/L ND 500 500 487 493 97 99 75-125 1 25 Silver ug/L ND 250 250 238 241 95 96 75-125 1 25 Thallium ug/L ND 500 500 465 472 93 94 75-125 2 25 Vanadium ug/L ND 500 500 467 478 93 96 75-125 2 25 Zinc ug/L ND 500 500 460 471 92 94 75-125 2 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 42 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 QC Batch: MPRP/16107 Analysis Method: EPA6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET NC Groundwater Associated Lab Samples: 92203121005, 92203121006, 92203121007, 92203121008, 92203121009, 92203121010, 92203121011, 92203121012,92203121013,92203121014,92203121015,92203121016 METHOD BLANK: 1212519 Matrix: Water Associated Lab Samples: 92203121005, 92203121006, 92203121007, 92203121008, 92203121009, 92203121010, 92203121011, 92203121012,92203121013,92203121014,92203121015,92203121016 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Antimony ug/L ND 6.0 06/04/1419:28 Arsenic ug/L ND 10.0 06/04/1419:28 Barium ug/L ND 100 06/04/1419:28 Beryllium ug/L ND 1.0 06/04/1419:28 Cadmium ug/L ND 1.0 06/04/1419:28 Chromium ug/L ND 10.0 06/04/1419:28 Cobalt ug/L ND 10.0 06/04/1419:28 Copper ug/L ND 10.0 06/04/1419:28 Iron ug/L ND 300 06/04/1419:28 Lead ug/L ND 10.0 06/04/1419:28 Nickel ug/L ND 50.0 06/04/1419:28 Selenium ug/L ND 10.0 06/04/1419:28 Silver ug/L ND 10.0 06/04/1419:28 Thallium ug/L ND 5.5 06/04/1419:28 Vanadium ug/L ND 25.0 06/04/1419:28 Zinc ug/L ND 10.0 06/04/1419:28 LABORATORY CONTROL SAMPLE: Parameter 1212520 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Antimony ug/L 500 497 99 80-120 Arsenic ug/L 500 477 95 80-120 Barium ug/L 500 502 100 80-120 Beryllium ug/L 500 479 96 80-120 Cadmium ug/L 500 480 96 80-120 Chromium ug/L 500 486 97 80-120 Cobalt ug/L 500 495 99 80-120 Copper ug/L 500 494 99 80-120 Iron ug/L 5000 4700 94 80-120 Lead ug/L 500 497 99 80-120 Nickel ug/L 500 478 96 80-120 Selenium ug/L 500 495 99 80-120 Silver ug/L 250 242 97 80-120 Thallium ug/L 500 469 94 80-120 Vanadium ug/L 500 480 96 80-120 Zinc ug/L 500 478 96 80-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 43 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: Surry Closed -Mt. Airy (UIC) 92203121 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1212521 1212522 MS MSD 92203332001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 474 483 95 97 75-125 2 25 Arsenic ug/L ND 500 500 456 468 91 94 75-125 3 25 Barium ug/L 22.5J 500 500 490 511 94 98 75-125 4 25 Beryllium ug/L ND 500 500 454 471 91 94 75-125 4 25 Cadmium ug/L ND 500 500 456 467 91 93 75-125 2 25 Chromium ug/L ND 500 500 462 476 92 95 75-125 3 25 Cobalt ug/L ND 500 500 464 480 93 96 75-125 3 25 Copper ug/L ND 500 500 475 480 95 96 75-125 1 25 Iron ug/L 178J 5000 5000 4630 4800 89 93 75-125 4 25 Lead ug/L ND 500 500 465 478 93 96 75-125 3 25 Nickel ug/L ND 500 500 453 467 91 93 75-125 3 25 Selenium ug/L ND 500 500 467 479 93 96 75-125 2 25 Silver ug/L ND 250 250 229 235 91 94 75-125 3 25 Thallium ug/L ND 500 500 446 459 89 92 75-125 3 25 Vanadium ug/L ND 500 500 457 472 91 94 75-125 3 25 Zinc ug/L ND 500 500 457 467 91 93 75-125 2 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 44 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 QC Batch: MSV/26995 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92203121001, 92203121002, 92203121003, 92203121004 METHOD BLANK: 1209031 Matrix: Water Associated Lab Samples: 92203121001, 92203121002, 92203121003, 92203121004 Blank Reporting Parameter Units Result Limit Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 05/29/14 15:03 1,1,1-Trichloroethane ug/L ND 1.0 05/29/14 15:03 1,1,2,2-Tetrachloroethane ug/L ND 3.0 05/29/14 15:03 1,1,2-Trichloroethane ug/L ND 1.0 05/29/14 15:03 1,1-Dichloroethane ug/L ND 5.0 05/29/14 15:03 1,1-Dichloroethene ug/L ND 5.0 05/29/14 15:03 1,2,3-Trichloropropane ug/L ND 1.0 05/29/14 15:03 1,2-Dibromo-3-chloropropane ug/L ND 13.0 05/29/14 15:03 1,2-Dibromoethane (EDB) ug/L ND 1.0 05/29/14 15:03 1,2-Dichlorobenzene ug/L ND 5.0 05/29/14 15:03 1,2-Dichloroethane ug/L ND 1.0 05/29/14 15:03 1,2-Dichloropropane ug/L ND 1.0 05/29/14 15:03 1,3-Dichloropropane ug/L ND 1.0 05/29/14 15:03 1,4-Dichlorobenzene ug/L ND 1.0 05/29/14 15:03 2-Butanone (MEK) ug/L ND 100 05/29/14 15:03 2-Hexanone ug/L ND 50.0 05/29/14 15:03 4-Methyl-2-pentanone (MIBK) ug/L ND 100 05/29/14 15:03 Acetone ug/L ND 100 05/29/14 15:03 Acrylonitrile ug/L ND 200 05/29/14 15:03 Benzene ug/L ND 1.0 05/29/14 15:03 Bromochloromethane ug/L ND 3.0 05/29/14 15:03 Bromodichloromethane ug/L ND 1.0 05/29/14 15:03 Bromoform ug/L ND 3.0 05/29/14 15:03 Bromomethane ug/L ND 10.0 05/29/14 15:03 Carbon disulfide ug/L ND 100 05/29/14 15:03 Carbon tetrachloride ug/L ND 1.0 05/29/14 15:03 Chlorobenzene ug/L ND 3.0 05/29/14 15:03 Chloroethane ug/L ND 10.0 05/29/14 15:03 Chloroform ug/L ND 5.0 05/29/14 15:03 Chloromethane ug/L ND 1.0 05/29/14 15:03 cis-1,2-Dichloroethene ug/L ND 5.0 05/29/14 15:03 cis-1,3-Dichloropropene ug/L ND 1.0 05/29/14 15:03 Dibromochloromethane ug/L ND 3.0 05/29/14 15:03 Dibromomethane ug/L ND 10.0 05/29/14 15:03 Ethylbenzene ug/L ND 1.0 05/29/14 15:03 lodomethane ug/L ND 10.0 05/29/14 15:03 Methylene Chloride ug/L ND 1.0 05/29/14 15:03 Styrene ug/L ND 1.0 05/29/14 15:03 Tetrachloroethene ug/L ND 1.0 05/29/14 15:03 Toluene ug/L ND 1.0 05/29/14 15:03 trans-1,2-Dichloroethene ug/L ND 5.0 05/29/14 15:03 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 45 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 METHOD BLANK: 1209031 Matrix: Water Associated Lab Samples: 92203121001, 92203121002, 92203121003, 92203121004 Blank Reporting Parameter Units Result Limit Analyzed trans- 1,3-Dichloropropene ug/L ND 1.0 05/29/14 15:03 trans-1,4-Dichloro-2-butene ug/L ND 100 05/29/14 15:03 Trichloroethene ug/L ND 1.0 05/29/14 15:03 Trichlorofluoromethane ug/L ND 1.0 05/29/14 15:03 Vinyl acetate ug/L ND 50.0 05/29/14 15:03 Vinyl chloride ug/L ND 1.0 05/29/14 15:03 Xylene (Total) ug/L ND 5.0 05/29/14 15:03 1,2-Dichloroethane-d4 (S) % 92 70-130 05/29/14 15:03 4-Bromofluorobenzene (S) % 95 70-130 05/29/14 15:03 Toluene-d8 (S) % 97 70-130 05/29/14 15:03 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 1209032 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 50.6 101 70-130 1,1,1-Trichloroethane ug/L 50 48.1 96 70-130 1,1,2,2-Tetrachloroethane ug/L 50 51.3 103 70-130 1,1,2-Trichloroethane ug/L 50 50.6 101 70-130 1,1-Dichloroethane ug/L 50 47.0 94 70-130 1,1-Dichloroethene ug/L 50 47.0 94 70-132 1,2,3-Trichloropropane ug/L 50 48.1 96 70-130 1,2-Dibromo-3-chloropropane ug/L 50 48.2 96 70-130 1,2-Dibromoethane (EDB) ug/L 50 49.1 98 70-130 1,2-Dichlorobenzene ug/L 50 50.0 100 70-130 1,2-Dichloroethane ug/L 50 48.8 98 70-130 1,2-Dichloropropane ug/L 50 49.6 99 70-130 1,3-Dichloropropane ug/L 50 49.8 100 70-130 1,4-Dichlorobenzene ug/L 50 49.1 98 70-130 2-Butanone (MEK) ug/L 100 87.7J 88 70-145 2-Hexanone ug/L 100 97.1 97 70-144 4-Methyl-2-pentanone (MIBK) ug/L 100 91.7J 92 70-140 Acetone ug/L 100 94.OJ 94 50-175 Acrylonitrile ug/L 250 237 95 70-143 Benzene ug/L 50 54.1 108 70-130 Bromochloromethane ug/L 50 49.0 98 70-130 Bromodichloromethane ug/L 50 48.6 97 70-130 Bromoform ug/L 50 49.2 98 70-130 Bromomethane ug/L 50 32.2 64 54-130 Carbon disulfide ug/L 50 49.9J 100 70-131 Carbon tetrachloride ug/L 50 46.0 92 70-132 Chlorobenzene ug/L 50 47.4 95 70-130 Chloroethane ug/L 50 42.4 85 64-134 Chloroform ug/L 50 48.7 97 70-130 Chloromethane ug/L 50 34.3 69 64-130 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 46 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 LABORATORY CONTROL SAMPLE: Parameter 1209032 Units Spike Conc. LCS LCS Result % Rec cis-1,2-Dichloroethene ug/L 50 48.0 cis-1,3-Dichloropropene ug/L 50 51.2 Dibromochloromethane ug/L 50 47.8 Dibromomethane ug/L 50 47.1 Ethylbenzene ug/L 50 48.1 lodomethane ug/L 100 27.5 Methylene Chloride ug/L 50 48.1 Styrene ug/L 50 52.2 Tetrachloroethene ug/L 50 48.7 Toluene ug/L 50 49.7 trans-1,2-Dichloroethene ug/L 50 47.4 trans- 1,3-Dichloropropene ug/L 50 49.0 trans-1,4-Dichloro-2-butene ug/L 50 46.6J Trichloroethene ug/L 50 52.2 Trichlorofluoromethane ug/L 50 40.2 Vinyl acetate ug/L 100 100 Vinyl chloride ug/L 50 54.9 Xylene (Total) ug/L 150 147 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Toluene-d8 (S) % % Rec Limits Qualifiers 96 70-131 102 70-130 96 70-130 94 70-131 96 70-130 27 49-180 LO 96 63-130 104 70-130 97 70-130 99 70-130 95 70-130 98 70-132 93 70-141 104 70-130 80 62-133 100 66-157 110 69-130 98 70-130 91 70-130 97 70-130 100 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 47 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 QC Batch: MSV/27034 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92203121005, 92203121006, 92203121007, 92203121008, 92203121009, 92203121010, 92203121011, 92203121012,92203121013,92203121014,92203121015 METHOD BLANK: 1210761 Matrix: Water Associated Lab Samples: 92203121005, 92203121006, 92203121007, 92203121008, 92203121009, 92203121010, 92203121011, 92203121012,92203121013,92203121014,92203121015 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 5.0 05/31/14 01:23 1,1,1-Trichloroethane ug/L ND 1.0 05/31/14 01:23 1,1,2,2-Tetrachloroethane ug/L ND 3.0 05/31/14 01:23 1,1,2-Trichloroethane ug/L ND 1.0 05/31/14 01:23 1,1-Dichloroethane ug/L ND 5.0 05/31/14 01:23 1,1-Dichloroethene ug/L ND 5.0 05/31/14 01:23 1,2,3-Trichloropropane ug/L ND 1.0 05/31/14 01:23 1,2-Dibromo-3-chloropropane ug/L ND 13.0 05/31/14 01:23 1,2-Dibromoethane (EDB) ug/L ND 1.0 05/31/14 01:23 1,2-Dichlorobenzene ug/L ND 5.0 05/31/14 01:23 1,2-Dichloroethane ug/L ND 1.0 05/31/14 01:23 1,2-Dichloropropane ug/L ND 1.0 05/31/14 01:23 1,3-Dichlorobenzene ug/L ND 5.0 05/31/14 01:23 1,3-Dichloropropane ug/L ND 1.0 05/31/14 01:23 1,4-Dichlorobenzene ug/L ND 1.0 05/31/14 01:23 2-Butanone (MEK) ug/L ND 100 05/31/14 01:23 2-Hexanone ug/L ND 50.0 05/31/14 01:23 4-Methyl-2-pentanone (MIBK) ug/L ND 100 05/31/14 01:23 Acetone ug/L ND 100 05/31/14 01:23 Acrylonitrile ug/L ND 200 05/31/14 01:23 Benzene ug/L ND 1.0 05/31/14 01:23 Bromochloromethane ug/L ND 3.0 05/31/14 01:23 Bromodichloromethane ug/L ND 1.0 05/31/14 01:23 Bromoform ug/L ND 3.0 05/31/14 01:23 Bromomethane ug/L ND 10.0 05/31/14 01:23 Carbon disulfide ug/L ND 100 05/31/14 01:23 Carbon tetrachloride ug/L ND 1.0 05/31/14 01:23 Chlorobenzene ug/L ND 3.0 05/31/14 01:23 Chloroethane ug/L ND 10.0 05/31/14 01:23 Chloroform ug/L ND 5.0 05/31/14 01:23 Chloromethane ug/L ND 1.0 05/31/14 01:23 cis-1,2-Dichloroethene ug/L ND 5.0 05/31/14 01:23 cis-1,3-Dichloropropene ug/L ND 1.0 05/31/14 01:23 Dibromochloromethane ug/L ND 3.0 05/31/14 01:23 Dibromomethane ug/L ND 10.0 05/31/14 01:23 Ethylbenzene ug/L ND 1.0 05/31/14 01:23 lodomethane ug/L ND 10.0 05/31/14 01:23 Methylene Chloride ug/L ND 1.0 05/31/14 01:23 Styrene ug/L ND 1.0 05/31/14 01:23 Tetrachloroethene ug/L ND 1.0 05/31/14 01:23 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 48 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 METHOD BLANK: 1210761 Matrix: Water Associated Lab Samples: 92203121005, 92203121006, 92203121007, 92203121008, 92203121009, 92203121010, 92203121011, 92203121012,92203121013,92203121014,92203121015 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Toluene ug/L ND 1.0 05/31/14 01:23 trans-1,2-Dichloroethene ug/L ND 5.0 05/31/14 01:23 trans- 1,3-Dichloropropene ug/L ND 1.0 05/31/14 01:23 trans-1,4-Dichloro-2-butene ug/L ND 100 05/31/14 01:23 Trichloroethene ug/L ND 1.0 05/31/14 01:23 Trichlorofluoromethane ug/L ND 1.0 05/31/14 01:23 Vinyl acetate ug/L ND 50.0 05/31/14 01:23 Vinyl chloride ug/L ND 1.0 05/31/14 01:23 Xylene (Total) ug/L ND 5.0 05/31/14 01:23 1,2-Dichloroethane-d4 (S) % 97 70-130 05/31/14 01:23 4-Bromofluorobenzene (S) % 99 70-130 05/31/14 01:23 Toluene-d8 (S) % 100 70-130 05/31/14 01:23 LABORATORY CONTROL SAMPLE: Parameter 1210762 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 46.3 93 70-130 1,1,1-Trichloroethane ug/L 50 47.2 94 70-130 1,1,2,2-Tetrachloroethane ug/L 50 48.1 96 70-130 1,1,2-Trichloroethane ug/L 50 49.6 99 70-130 1,1-Dichloroethane ug/L 50 44.5 89 70-130 1,1-Dichloroethene ug/L 50 50.3 101 70-132 1,2,3-Trichloropropane ug/L 50 50.0 100 70-130 1,2-Dibromo-3-chloropropane ug/L 50 49.9 100 70-130 1,2-Dibromoethane (EDB) ug/L 50 48.1 96 70-130 1,2-Dichlorobenzene ug/L 50 48.4 97 70-130 1,2-Dichloroethane ug/L 50 47.1 94 70-130 1,2-Dichloropropane ug/L 50 47.3 95 70-130 1,3-Dichlorobenzene ug/L 50 47.4 95 70-130 1,3-Dichloropropane ug/L 50 47.3 95 70-130 1,4-Dichlorobenzene ug/L 50 46.9 94 70-130 2-Butanone (MEK) ug/L 100 99.91 100 70-145 2-Hexanone ug/L 100 98.5 99 70-144 4-Methyl-2-pentanone (MIBK) ug/L 100 107 107 70-140 Acetone ug/L 100 96.9J 97 50-175 Acrylonitrile ug/L 250 247 99 70-143 Benzene ug/L 50 48.8 98 70-130 Bromochloromethane ug/L 50 49.0 98 70-130 Bromodichloromethane ug/L 50 46.3 93 70-130 Bromoform ug/L 50 48.6 97 70-130 Bromomethane ug/L 50 46.2 92 54-130 Carbon disulfide ug/L 50 48.OJ 96 70-131 Carbon tetrachloride ug/L 50 52.4 105 70-132 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 49 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 LABORATORY CONTROL SAMPLE: Parameter 1210762 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Chlorobenzene ug/L 50 45.4 91 70-130 Chloroethane ug/L 50 51.7 103 64-134 Chloroform ug/L 50 47.1 94 70-130 Chloromethane ug/L 50 47.7 95 64-130 cis-1,2-Dichloroethene ug/L 50 47.4 95 70-131 cis-1,3-Dichloropropene ug/L 50 47.2 94 70-130 Dibromochloromethane ug/L 50 45.6 91 70-130 Dibromomethane ug/L 50 48.2 96 70-131 Ethylbenzene ug/L 50 45.4 91 70-130 lodomethane ug/L 100 95.0 95 49-180 Methylene Chloride ug/L 50 50.8 102 63-130 Styrene ug/L 50 48.7 97 70-130 Tetrachloroethene ug/L 50 49.5 99 70-130 Toluene ug/L 50 47.8 96 70-130 trans-1,2-Dichloroethene ug/L 50 48.3 97 70-130 trans- 1,3-Dichloropropene ug/L 50 47.5 95 70-132 trans-1,4-Dichloro-2-butene ug/L 50 49.6J 99 70-141 Trichloroethene ug/L 50 48.0 96 70-130 Trichlorofluoromethane ug/L 50 55.6 111 62-133 Vinyl acetate ug/L 100 99.1 99 66-157 Vinyl chloride ug/L 50 60.4 121 69-130 Xylene (Total) ug/L 150 139 93 70-130 1,2-Dichloroethane-d4 (S) % 97 70-130 4-Bromofluorobenzene (S) % 99 70-130 Toluene-d8 (S) % 102 70-130 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1211546 1211547 MS MSD 92203116003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,1-Dichloroethene ug/L ND 50 50 56.2 60.5 112 121 70-166 7 30 Benzene ug/L 0.42J 50 50 52.0 56.3 103 112 70-148 8 30 Chlorobenzene ug/L 0.38J 50 50 48.3 51.7 96 103 70-146 7 30 Toluene ug/L ND 50 50 48.5 52.1 97 104 70-155 7 30 Trichloroethene ug/L ND 50 50 54.1 57.7 108 115 69-151 7 30 1,2-Dichloroethane-d4 (S) % 99 100 70-130 4-Bromofluorobenzene (S) % 100 101 70-130 Toluene-d8(S) % 101 102 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 50 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 QC Batch: MSV/27035 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92203121016 METHOD BLANK: 1210768 Associated Lab Samples: 92203121016 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 05/31/14 01:07 1,1,1-Trichloroethane ug/L ND 1.0 05/31/14 01:07 1,1,2,2-Tetrachloroethane ug/L ND 3.0 05/31/14 01:07 1,1,2-Trichloroethane ug/L ND 1.0 05/31/14 01:07 1,1-Dichloroethane ug/L ND 5.0 05/31/14 01:07 1,1-Dichloroethene ug/L ND 5.0 05/31/14 01:07 1,2,3-Trichloropropane ug/L ND 1.0 05/31/14 01:07 1,2-Dibromo-3-chloropropane ug/L ND 13.0 05/31/14 01:07 1,2-Dibromoethane (EDB) ug/L ND 1.0 05/31/14 01:07 1,2-Dichlorobenzene ug/L ND 5.0 05/31/14 01:07 1,2-Dichloroethane ug/L ND 1.0 05/31/14 01:07 1,2-Dichloropropane ug/L ND 1.0 05/31/14 01:07 1,3-Dichloropropane ug/L ND 1.0 05/31/14 01:07 1,4-Dichlorobenzene ug/L ND 1.0 05/31/14 01:07 2-Butanone (MEK) ug/L ND 100 05/31/14 01:07 2-Hexanone ug/L ND 50.0 05/31/14 01:07 4-Methyl-2-pentanone (MIBK) ug/L ND 100 05/31/14 01:07 Acetone ug/L ND 100 05/31/14 01:07 Acrylonitrile ug/L ND 200 05/31/14 01:07 Benzene ug/L ND 1.0 05/31/14 01:07 Bromochloromethane ug/L ND 3.0 05/31/14 01:07 Bromodichloromethane ug/L ND 1.0 05/31/14 01:07 Bromoform ug/L ND 3.0 05/31/14 01:07 Bromomethane ug/L ND 10.0 05/31/14 01:07 Carbon disulfide ug/L ND 100 05/31/14 01:07 Carbon tetrachloride ug/L ND 1.0 05/31/14 01:07 Chlorobenzene ug/L ND 3.0 05/31/14 01:07 Chloroethane ug/L ND 10.0 05/31/14 01:07 Chloroform ug/L ND 5.0 05/31/14 01:07 Chloromethane ug/L ND 1.0 05/31/14 01:07 cis-1,2-Dichloroethene ug/L ND 5.0 05/31/14 01:07 cis-1,3-Dichloropropene ug/L ND 1.0 05/31/14 01:07 Dibromochloromethane ug/L ND 3.0 05/31/14 01:07 Dibromomethane ug/L ND 10.0 05/31/14 01:07 Ethylbenzene ug/L ND 1.0 05/31/14 01:07 lodomethane ug/L ND 10.0 05/31/14 01:07 Methylene Chloride ug/L ND 1.0 05/31/14 01:07 Styrene ug/L ND 1.0 05/31/14 01:07 Tetrachloroethene ug/L ND 1.0 05/31/14 01:07 Toluene ug/L ND 1.0 05/31/14 01:07 trans-1,2-Dichloroethene ug/L ND 5.0 05/31/14 01:07 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 51 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 METHOD BLANK: 1210768 Associated Lab Samples: 92203121016 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed trans- 1,3-Dichloropropene ug/L ND 1.0 05/31/14 01:07 trans-1,4-Dichloro-2-butene ug/L ND 100 05/31/14 01:07 Trichloroethene ug/L ND 1.0 05/31/14 01:07 Trichlorofluoromethane ug/L ND 1.0 05/31/14 01:07 Vinyl acetate ug/L ND 50.0 05/31/14 01:07 Vinyl chloride ug/L ND 1.0 05/31/14 01:07 Xylene (Total) ug/L ND 5.0 05/31/14 01:07 1,2-Dichloroethane-d4 (S) % 98 70-130 05/31/14 01:07 4-Bromofluorobenzene (S) % 99 70-130 05/31/14 01:07 Toluene-d8 (S) % 99 70-130 05/31/14 01:07 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 1210769 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 47.2 94 70-130 1,1,1-Trichloroethane ug/L 50 48.6 97 70-130 1,1,2,2-Tetrachloroethane ug/L 50 46.2 92 70-130 1,1,2-Trichloroethane ug/L 50 48.1 96 70-130 1,1-Dichloroethane ug/L 50 46.0 92 70-130 1,1-Dichloroethene ug/L 50 52.6 105 70-132 1,2,3-Trichloropropane ug/L 50 48.1 96 70-130 1,2-Dibromo-3-chloropropane ug/L 50 48.7 97 70-130 1,2-Dibromoethane (EDB) ug/L 50 47.6 95 70-130 1,2-Dichlorobenzene ug/L 50 49.0 98 70-130 1,2-Dichloroethane ug/L 50 48.0 96 70-130 1,2-Dichloropropane ug/L 50 47.9 96 70-130 1,3-Dichloropropane ug/L 50 47.2 94 70-130 1,4-Dichlorobenzene ug/L 50 47.7 95 70-130 2-Butanone (MEK) ug/L 100 93.1J 93 70-145 2-Hexanone ug/L 100 90.0 90 70-144 4-Methyl-2-pentanone (MIBK) ug/L 100 96.8J 97 70-140 Acetone ug/L 100 92.8J 93 50-175 Acrylonitrile ug/L 250 238 95 70-143 Benzene ug/L 50 50.0 100 70-130 Bromochloromethane ug/L 50 49.5 99 70-130 Bromodichloromethane ug/L 50 47.2 94 70-130 Bromoform ug/L 50 47.6 95 70-130 Bromomethane ug/L 50 45.8 92 54-130 Carbon disulfide ug/L 50 49.6J 99 70-131 Carbon tetrachloride ug/L 50 54.6 109 70-132 Chlorobenzene ug/L 50 46.1 92 70-130 Chloroethane ug/L 50 53.3 107 64-134 Chloroform ug/L 50 46.6 93 70-130 Chloromethane ug/L 50 49.3 99 64-130 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 52 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 LABORATORY CONTROL SAMPLE: Parameter 1210769 Units Spike Conc. LCS Result LCS % Rec % Rec Limits cis-1,2-Dichloroethene ug/L 50 48.2 96 70-131 cis-1,3-Dichloropropene ug/L 50 47.5 95 70-130 Dibromochloromethane ug/L 50 45.9 92 70-130 Dibromomethane ug/L 50 47.9 96 70-131 Ethylbenzene ug/L 50 46.5 93 70-130 lodomethane ug/L 100 92.1 92 49-180 Methylene Chloride ug/L 50 50.3 101 63-130 Styrene ug/L 50 49.0 98 70-130 Tetrachloroethene ug/L 50 50.6 101 70-130 Toluene ug/L 50 48.4 97 70-130 trans-1,2-Dichloroethene ug/L 50 50.3 101 70-130 trans- 1,3-Dichloropropene ug/L 50 46.6 93 70-132 trans-1,4-Dichloro-2-butene ug/L 50 45.9J 92 70-141 Trichloroethene ug/L 50 49.7 99 70-130 Trichlorofluoromethane ug/L 50 59.1 118 62-133 Vinyl acetate ug/L 100 96.7 97 66-157 Vinyl chloride ug/L 50 62.6 125 69-130 Xylene (Total) ug/L 150 141 94 70-130 1,2-Dichloroethane-d4 (S) % 97 70-130 4-Bromofluorobenzene (S) % 98 70-130 Toluene-d8 (S) % 100 70-130 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1211548 1211549 MS MSD 92203121016 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,1-Dichloroethene ug/L ND 50 50 59.4 71.6 119 143 70-166 19 30 Benzene ug/L 0.42J 50 50 54.7 67.4 109 134 70-148 21 30 Chlorobenzene ug/L 0.97J 50 50 51.1 62.7 100 124 70-146 20 30 Toluene ug/L ND 50 50 50.8 62.4 102 125 70-155 20 30 Trichloroethene ug/L ND 50 50 56.4 69.1 113 138 69-151 20 30 1,2-Dichloroethane-d4 (S) % 100 100 70-130 4-Bromofluorobenzene (S) % 100 100 70-130 Toluene-d8(S) % 100 100 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 53 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 QC Batch: WET/31334 Analysis Method: SM 2320B QC Batch Method: SM 2320B Analysis Description: 2320E Alkalinity Associated Lab Samples: 92203121005, 92203121006, 92203121007, 92203121008, 92203121009, 92203121010 METHOD BLANK: 1212368 Matrix: Water Associated Lab Samples: 92203121005, 92203121006, 92203121007, 92203121008, 92203121009, 92203121010 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Alkalinity, Total as CaCO3 ug/L ND 5000 06/03/14 11:38 LABORATORY CONTROL SAMPLE: 1212369 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 47600 95 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1212370 1212371 MS MSD 92203313010 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 163 50000 50000 198000 198000 70 70 75-125 0 20 M1 mg/L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1212372 1212373 MS MSD 92203121008 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 34500 50000 50000 81400 80400 94 92 75-125 1 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 54 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 QC Batch: WET/31323 Analysis Method: SM 4500-S2D QC Batch Method: SM 4500-S2D Analysis Description: 4500S2D Sulfide Water Associated Lab Samples: 92203121005, 92203121006, 92203121007, 92203121008 METHOD BLANK: 1211984 Matrix: Water Associated Lab Samples: 92203121005, 92203121006, 92203121007, 92203121008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfide ug/L ND 1000 06/03/1415:47 LABORATORY CONTROL SAMPLE: 1211985 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 508J 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1211988 1211989 MS MSD 92203023007 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 309J 309J 62 62 75-125 0 20 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1212570 1212571 MS MSD 92203023002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 484J 484J 97 97 75-125 0 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 55 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 QC Batch: WET/31324 Analysis Method: SM 4500-S2D QC Batch Method: SM 4500-S2D Analysis Description: 4500S2D Sulfide Water Associated Lab Samples: 92203121009, 92203121010 METHOD BLANK: 1211998 Matrix: Water Associated Lab Samples: 92203121009, 92203121010 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfide ug/L ND 1000 06/03/1415:53 LABORATORY CONTROL SAMPLE: 1211999 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 512J 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1212002 1212003 MS MSD 92203346002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 493J 493J 99 99 75-125 0 20 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1212481 1212482 MS MSD 92203313004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 385J 385J 77 77 75-125 0 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 56 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 QC Batch: WETA/19162 Analysis Method: EPA 300.0 QC Batch Method: EPA 300.0 Analysis Description: 300.0 IC Anions Associated Lab Samples: 92203121005, 92203121006 METHOD BLANK: 1210885 Matrix: Water Associated Lab Samples: 92203121005, 92203121006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfate ug/L ND 250000 06/03/14 01:32 LABORATORY CONTROL SAMPLE: 1210886 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate ug/L 20000 191001 95 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1210887 1210888 MS MSD 92203023012 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 85200 20000 20000 99900J 93900J 73 44 90-110 6 20 M6 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1210889 1210890 MS MSD 92203263009 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 13.2 20000 20000 38200J 37800J 125 123 90-110 1 20 M1 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 57 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 QC Batch: WETA/19211 Analysis Method: EPA 300.0 QC Batch Method: EPA 300.0 Analysis Description: 300.0 IC Anions Associated Lab Samples: 92203121007, 92203121008, 92203121009, 92203121010 METHOD BLANK: 1214099 Matrix: Water Associated Lab Samples: 92203121007, 92203121008, 92203121009, 92203121010 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfate ug/L ND 250000 06/05/1418:58 LABORATORY CONTROL SAMPLE: 1214100 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate ug/L 20000 19200J 96 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1214101 1214102 MS MSD 92203770001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 2030 20000 20000 2150000 2160000 623 646 90-110 0 20 M6 mg/L J J MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1214103 1214104 MS MSD 92203346005 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 7.8 20000 20000 28300J 28400J 103 103 90-110 0 20 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 58 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 QC Batch: WETA/19280 Analysis Method: SM 4500-CI-E QC Batch Method: SM 4500-CI-E Analysis Description: 4500 Chloride Associated Lab Samples: 92203121005, 92203121006, 92203121007, 92203121008, 92203121009 METHOD BLANK: 1219158 Matrix: Water Associated Lab Samples: 92203121005, 92203121006, 92203121007, 92203121008, 92203121009 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride ug/L ND 1000 06/11/1417:42 LABORATORY CONTROL SAMPLE: 1219159 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride ug/L 20000 20500 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1219160 1219161 MS MSD 92203236001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 2.2 20000 20000 20800 20700 93 92 75-125 0 20 mg/L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1219162 1219163 MS MSD 92203313012 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 36.7 20000 20000 46700 46900 50 51 75-125 0 20 M1 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 59 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 QC Batch: WETA/19281 Analysis Method: SM 4500-CI-E QC Batch Method: SM 4500-CI-E Analysis Description: 4500 Chloride Associated Lab Samples: 92203121010 METHOD BLANK: 1219164 Matrix: Water Associated Lab Samples: 92203121010 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride ug/L ND 1000 06/11/1418:03 LABORATORY CONTROL SAMPLE: 1219165 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride ug/L 20000 20400 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1219166 1219167 MS MSD 92203121010 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 2710 20000 20000 21800 21900 95 96 75-125 0 20 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1219168 1219169 MS MSD 92203397002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 17.7 20000 20000 37600 37100 99 97 75-125 1 20 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 60 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 QC Batch: WETA/19243 Analysis Method: SM 4500-CN-E QC Batch Method: SM 4500-CN-E Analysis Description: 450OCNE Cyanide, Total Associated Lab Samples: 92203121017 METHOD BLANK: 1216407 Matrix: Water Associated Lab Samples: 92203121017 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cyanide ug/L ND 10.0 06/09/1410:32 LABORATORY CONTROL SAMPLE: 1216408 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 107 107 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1216409 1216410 MS MSD 92203836001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 110 112 108 110 75-125 1 20 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1216411 1216412 MS MSD 92203023009 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 111 109 110 108 75-125 1 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 61 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 QC Batch: WETA/19244 Analysis Method: SM 4500-CN-E QC Batch Method: SM 4500-CN-E Analysis Description: 450OCNE Cyanide, Total Associated Lab Samples: 92203121005, 92203121006, 92203121007, 92203121008, 92203121015, 92203121016 METHOD BLANK: 1216413 Matrix: Water Associated Lab Samples: 92203121005, 92203121006, 92203121007, 92203121008, 92203121015, 92203121016 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cyanide ug/L ND 10.0 06/09/1410:59 LABORATORY CONTROL SAMPLE: 1216414 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 110 110 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1216415 1216416 MS MSD 92203313004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 108 87.2 106 86 75-125 21 20 R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1216417 1216418 MS MSD 92203121007 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 89.6 90.3 87 88 75-125 1 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 62 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 QC Batch: WETA/19250 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92203121005, 92203121006, 92203121007, 92203121008, 92203121009, 92203121010 METHOD BLANK: 1216637 Matrix: Water Associated Lab Samples: 92203121005, 92203121006, 92203121007, 92203121008, 92203121009, 92203121010 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand ug/L ND 25000 06/10/14 13:40 LABORATORY CONTROL SAMPLE: 1216638 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand ug/L 750000 745000 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1216639 1216640 MS MSD 92204031002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chemical Oxygen Demand ug/L 76.0 750000 750000 841000 843000 102 102 75-125 0 20 mg/L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1216641 1216642 MS MSD 92203121008 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chemical Oxygen Demand ug/L ND 750000 750000 728000 731000 97 97 75-125 0 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 63 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 QC Batch: WETA/19200 Analysis Method: SM 5310B QC Batch Method: SM 5310B Analysis Description: 5310E TOC Associated Lab Samples: 92203121005 METHOD BLANK: 1213002 Matrix: Water Associated Lab Samples: 92203121005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon ug/L ND 1000 06/05/14 14:41 LABORATORY CONTROL SAMPLE: 1213003 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carbon ug/L 25000 24600 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1213004 1213005 MS MSD 92203708001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Total Organic Carbon ug/L 2.0 25000 25000 28700 28700 107 107 75-125 0 20 mg/L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1213006 1213007 MS MSD 92203155012 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Total Organic Carbon ug/L 2.4 25000 25000 26800 26800 97 97 75-125 0 20 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 64 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 QC Batch: WETA/19212 Analysis Method: SM 5310B QC Batch Method: SM 5310B Analysis Description: 5310E TOC Associated Lab Samples: 92203121006, 92203121007, 92203121008, 92203121009, 92203121010 METHOD BLANK: 1214105 Matrix: Water Associated Lab Samples: 92203121006, 92203121007, 92203121008, 92203121009, 92203121010 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon ug/L ND 1000 06/05/14 20:52 LABORATORY CONTROL SAMPLE: 1214106 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carbon ug/L 25000 24800 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1214107 1214108 MS MSD 92203814001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Total Organic Carbon ug/L ND 25000 25000 24800 24800 99 99 75-125 0 20 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1214109 1214110 MS MSD 92203121006 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Total Organic Carbon ug/L 13900 25000 25000 32100 32000 73 73 75-125 0 20 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 65 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALIFIERS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference INC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 66 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: Surry Closed -Mt. Airy (UIC) 92203121 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92203121001 MW-12S EPA 3010 MPRP/16067 EPA6010 ICP/14532 92203121002 MW-18 EPA 3010 MPRP/16067 EPA6010 ICP/14532 92203121003 MW-19 EPA 3010 MPRP/16067 EPA6010 ICP/14532 92203121004 MW-23 EPA 3010 MPRP/16067 EPA6010 ICP/14532 92203121005 MW-1 EPA 3010 MPRP/16107 EPA6010 ICP/14568 92203121006 MW-7 EPA 3010 MPRP/16107 EPA6010 ICP/14568 92203121007 MW-15 EPA 3010 MPRP/16107 EPA6010 ICP/14568 92203121008 MW-21 EPA 3010 MPRP/16107 EPA6010 ICP/14568 92203121009 MW-9 EPA 3010 MPRP/16107 EPA6010 ICP/14568 92203121010 MW-14 EPA 3010 MPRP/16107 EPA6010 ICP/14568 92203121011 MW-3R EPA 3010 MPRP/16107 EPA6010 ICP/14568 92203121012 MW-13 EPA 3010 MPRP/16107 EPA6010 ICP/14568 92203121013 MW-17 EPA 3010 MPRP/16107 EPA6010 ICP/14568 92203121014 MW-20 EPA 3010 MPRP/16107 EPA6010 ICP/14568 92203121015 MW-16 EPA 3010 MPRP/16107 EPA6010 ICP/14568 92203121016 MW-22 EPA 3010 MPRP/16107 EPA6010 ICP/14568 92203121010 MW-14 EPA 7470 MERP/6689 EPA 7470 MERC/6449 92203121001 MW-12S EPA 8260 MSV/26995 92203121002 MW-18 EPA 8260 MSV/26995 92203121003 MW-19 EPA 8260 MSV/26995 92203121004 MW-23 EPA 8260 MSV/26995 92203121005 MW-1 EPA 8260 MSV/27034 92203121006 MW-7 EPA 8260 MSV/27034 92203121007 MW-15 EPA 8260 MSV/27034 92203121008 MW-21 EPA 8260 MSV/27034 92203121009 MW-9 EPA 8260 MSV/27034 92203121010 MW-14 EPA 8260 MSV/27034 92203121011 MW-3R EPA 8260 MSV/27034 92203121012 MW-13 EPA 8260 MSV/27034 92203121013 MW-17 EPA 8260 MSV/27034 92203121014 MW-20 EPA 8260 MSV/27034 92203121015 MW-16 EPA 8260 MSV/27034 92203121016 MW-22 EPA 8260 MSV/27035 92203121005 MW-1 SM 2320B WET/31334 92203121006 MW-7 SM 2320B WET/31334 92203121007 MW-15 SM 2320B WET/31334 92203121008 MW-21 SM 2320B WET/31334 92203121009 MW-9 SM 2320B WET/31334 92203121010 MW-14 SM 2320B WET/31334 92203121005 MW-1 SM 4500-S2D WET/31323 92203121006 MW-7 SM 4500-S2D WET/31323 92203121007 MW-15 SM 4500-S2D WET/31323 92203121008 MW-21 SM 4500-S2D WET/31323 92203121009 MW-9 SM 4500-S2D WET/31324 92203121010 MW-14 SM 4500-S2D WET/31324 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 67 of 73 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92203121 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92203121005 MW-1 EPA 300.0 WETA/19162 92203121006 MW-7 EPA 300.0 WETA/19162 92203121007 MW-15 EPA 300.0 WETA/19211 92203121008 MW-21 EPA 300.0 WETA/19211 92203121009 MW-9 EPA 300.0 WETA/19211 92203121010 MW-14 EPA 300.0 WETA/19211 92203121005 MW-1 SM 4500-CI-E WETA/19280 92203121006 MW-7 SM 4500-CI-E WETA/19280 92203121007 MW-15 SM 4500-CI-E WETA/19280 92203121008 MW-21 SM 4500-CI-E WETA/19280 92203121009 MW-9 SM 4500-CI-E WETA/19280 92203121010 MW-14 SM 4500-CI-E WETA/19281 92203121005 MW-1 SM 4500-CN-E WETA/19244 92203121006 MW-7 SM 4500-CN-E WETA/19244 92203121007 MW-15 SM 4500-CN-E WETA/19244 92203121008 MW-21 SM 4500-CN-E WETA/19244 92203121015 MW-16 SM 4500-CN-E WETA/19244 92203121016 MW-22 SM 4500-CN-E WETA/19244 92203121017 MW-19 SM 4500-CN-E WETA/19243 92203121005 MW-1 SM 5220D WETA/19250 92203121006 MW-7 SM 5220D WETA/19250 92203121007 MW-15 SM 5220D WETA/19250 92203121008 MW-21 SM 5220D WETA/19250 92203121009 MW-9 SM 5220D WETA/19250 92203121010 MW-14 SM 5220D WETA/19250 92203121005 MW-1 SM 5310B WETA/19200 92203121006 MW-7 SM 5310B WETA/19212 92203121007 MW-15 SM 5310B WETA/19212 92203121008 MW-21 SM 5310B WETA/19212 92203121009 MW-9 SM 5310B WETA/19212 92203121010 MW-14 SM 5310B WETA/19212 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/12/2014 08:20 AM without the written consent of Pace Analytical Services, Inc.. Page 68 of 73 qC0 Sample Condition U on ReSei Document Number: F-CH R-CS-003-rev.14 Page 1 of 2 Issuing Authority: Pace Huntersville Quality Office Client Name:_ r4 Un1 C Imo. _ Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Client❑ Commercial Pace Other Custody Seal on Cooler/Box Present: ❑ yes ';�rno Seals intact: ❑ yes Packing Material: ❑ Bubble Wrap ff Bubble Bags ❑ None [� , Other Thermometer Used: IR Gun T1102 14 Type of Ice: et Blue None T_�.� n�-....ter:..... r....a.-. T44A'1• K I r f-'.. n+inn To14r1o!• A!n i'nrrmnfinn ❑ no Samples on ice, cooling process has begun Corrected Cooler Temp.: . _ C Biological Tissue is Frozen: Yes No r Date and Initials of erson exams Jng contents: Temp should be above freezing to 6°C Comments: Chain of Custody Present: Yes ❑No ❑NIA 1. Chain of Custody Filled Out: es . ❑No ❑NIA 2. Chain of Custody Relinquished: es ONO El N/A 3_ Sampler Name & Signature on COG: Yes ❑No ❑NIA 4. Samples Arrived within Hold Time: Yes ❑N❑ ❑NIA 5. Short Hold Time Analysis {a72hr : ❑Yes 214-0 ❑NIA 6. Rush Turn Around Time Requested: Oyes a ❑NIA 7. Sufficient Volume: Eles ONO ❑NIA 8. Correct Containers Used: Ye ❑No ❑NIA g. -Pace Containers Used: Yes No ❑NIA Containers Intact: es ❑N❑ ❑NI 0. Filtered volume received for Dissolved tests Oyes ONO NIA 11. Sample Labels match COC: ❑Yes ONO ❑NIA 12. -Includes dateltimellD/Analysis Matrix: All containers needing preservation have been checked. P*es ❑No ❑NIA 13, All containers needing preservation are found to be in yes ❑N❑ ❑NIA compliance with EPA recommendation. exceptions: VOA, colirorm, TOC, 0&G, WI-DRO (water) Yes ❑N❑ Samples checked for dechlorination: ❑Yes ❑N❑ ❑N'tA 14. Headspace in VOA Vials ( >6mm): Oyes I io ❑NIA 15. Trip Blank Present: ❑Yes ❑No NIA A 6. Trip Blank Custody Seals Present ❑Yes ❑N❑ IA Pace Trip Blank Lot # (if purchased): Client Notification! Resolution: Field Data Required? Y I N Person Contacted: Comments/ Resolution: SCURF Review: Date: 1 5/-2 9 Date/Time: 5K1KOVIeW: I Y <7/ uale- ]�/ Note: Whenever ther a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers) WV# • J22V3121 IIPR111111111111 Page 69 of 73 CHAIN -OF -CUSTODY 1 Analytical Request Document CA S The Chain of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section 8 Section C Required Client Information: Required Project Information: Invoice Information: Page: 1 Of 1 Company: Municipal Engineering Services Report To: Jonathan Pfohl Attentian. Municipal EngineeringEnglneering Services Address: P.O. Box 97 Copy To- Company Name: Gamer, NC 27529 Address: Reg ulatoryr Agency Email To; jpfohi mesco.com Purchase Order No. SV [ I autl — Mt. Wel Pace Quote Reference: Phone: 919-772-5393 Fax Client Project IID: ftworwWwwwwr Pace Project Manager Kevin Godwin Stater Location Requested due DatefTAT: 10 Day (Default) lContainer Order Number: Pace Profile #: North Carolina Requested An tysis Filtered YIN z COLLECTED Preservatives N N N N N N N N N N N N MATRIX caDE Dri.Wq W.W DVY W.I. wr a E SAMPLE ID wa:zew.I. ww Prudw P $ ii START END a W One Character per box. Scerscea _ (AZ. 0.9 1 , -1 w" we } � o0 y m Sample Ids must he unique Air nrt a ¢ �] p•� } rf other os Tns TS a a- T F m to21 — w ik K W ry p w O C `m l6 ¢ m F C E r�li DATE TIME DATE TIME ¢ N D ac C n x== 2 U aN a `m z m r Q p a 1 wT c kAA 0_4k r to a i 2 w-las s a� 1 3 x 3m w-RtS U�' a MO-14 V Il s $ i 9 I 10 11 12 ADDITIONAL COMMENTS " LINQUISHED BY I AFFILIATION DATE TIME 1 :' ACCEPTED BY I AFFIL( ION DATE TIME SAM . NS C o - —Z �( 1 `kJ SAMPLER NAME AND SIGNATURE m m 0 ., z a. S " PRINT Name of SAMPLER: Jonat ri.:M11 a uJ a U N } SIGNATURE of SAMPLER: i DATE Signed: 0 Document Name: Document Revised: April 07. 2014 . aeeAmfjrtrcal" Sample Condition Upon Receipt (SCU!!L Page 1 of 2 Document Number: Issuing Authority: F-CHR-CS-003-rev.14 Pace Huntersville Ouality Dffice Client Name: un` ' Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Client❑ Commercia Pace Other gpflonal Custody Seal on CoolerlBox Present: ❑ yes �no Seals intact: ❑ yes ❑ no Proj; DueifJate: Proj. ivarre Packing Material: ❑ Bubble Wrap 0 Bubble Bags ❑ None ❑ Other Thermometer Used: IR Gun T1102 J 14t] Type of Ice: et Blue None Samples on ice, cooling process has begun Temn Correction Factor T1102 n C:nrrac:tinn T13 Nn C nrrPr.tinn Corrected Cooler Temp.: 'C $iolo ical Tissue Is Frozen: Yes No NIA g Date and In i s of erson examining contents:5��11�� Temp should be above freezing to 6°C Comments: Chain of Custody Present: Yes ONO ❑NIA 1. Chain of Custody Filled Out: Yes ONO ❑NIA 2, Chain of Custody Relinquished: Yes ONO ❑NIA 3. Sampler Name & Signature on COG: e ❑No ❑NIA 4. Samples Arrived within Hold Time: Yes ONO ❑NIA 5, Short Hold Time Analysis (<72hr): Oyes PN ❑NIA 6, Rush Turn Around Time Requested: Oyes dNo ❑NIA 7, Sufficient Volume: 6s ONO ©NIA 8, Correct Containers Used: El No ❑NIA g, -Pace Containers Used: 7yy� ❑No ❑NIA Containers Intact: Yes ONO 11NI4 10. Filtered volume received for Dissolved tests Oyes ❑No NIA 11. Sample Labels match COC: Oyes dNo ❑NIA -Includes dateltime/1D/Anal sis Matrix: All containers needing preservation have been checked. Yes El No ❑NIA 13. All containers needing preservatlon are found to be in Yes ONO ❑NIA compliance with EPA recommendation. exceptions: VOA, colif❑rm, TOC, O&G, V&DRo (water) Yes ❑No Samples checked for dechlorination: Xfyes ❑No El NIA 14. Headspace in VOA Vials (>6mm): ❑Yes PlNo El NIA 15. Trip Blank Present: ❑Yes ONO IA 16. Trip Blank Custody Seals Present []Yes ©No 7NIA Pace Trip Blank Lot # (if purchased): Client Notification/ Resolution: Field Data Required? Y I N Person Contacted: Comments/ Resolution: ❑atefrime: SCURF Review: Date: 5 � I yl SRF Review: bate: j❑ 1� Note; Whenever then a discrepancy affecting North Carolina compliance samples, a copy of this farm will be sent to the North Carolina ❑EHNR Certification Office (1.e out of hold, incorrect preservative, out of temp, incorrect containers) Place label here 17OR Handwrite project number (if no label available) Page 71 of 73 >ce analytrca► Section A Required Client Information: Company: llf}lirlid al Engineering Services Address: P.d. Box 97 Section B Required Project Information: Report To Jonathan Pfohl Copy 7o: CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUiNEPIT. All relevant fields must 6e completed accurately. Section C Invoice Information: pa e • 1 Attention: MUnICI al Engineering Services Company Name ^� Of 2 Garner, NC 27529 Address: Regulatory Agency Email To: Ipfohlomesco-corn Purchase Order No. Pace Quote Reference: Phone: 919-772-5393 1Fax Client Project ID: Surry Closed -Mt. Airy (UIC) Pace Project Manager: Kevin Godwin State 1 Location Requested Due DatBITAT: 10 Day (Default} Container Order Number: Pace Profile #: North Carolina Rersrrestnd A—W.is Filtere-d fY1N1 z w a COLLECTED Preservatives N N N N N N N N N N N N w.TRfx CODEQ M 0 0rineag waver Ov+ Water WT n V 2 ❑ — W-W Water VVw SAMPLE ID START END U ,-iusaie s>_ c One Character per box- [7 N W'" WP (A-Z, 0-9 1 , -7 n.r RR w ¢ z w — Sample Ids must be unique oulw 01 T.— Ta 0 0 F w F 2 0 0 � V1 r ¢ o 0 # x w a w OV m T O m i11 g O a c rfi V 2 V O m Nc W °i Q V a s �° U ❑ ❑ DATE TIME OA7E 71ME N u_= T 2 Z 0 d w U ¢ y U g 1 MW1 WTI G iS x x x x x x x x x x 2 MW-3R WT G 3 '8 C x 3 VW-7 wT G zs }�:az x x x x x x x x x 4 MW-9 WT G 9y I -3S x x x x x x x x 5 M W-12S WT G x I 6 MW-13 WT G S :4c x 7 MW-14 w7 G S �; x x I x x x x x x 8 MW-15 yM G 9, +cis x x x x x x x x 9 MW-16 yM G clar 11cV x x x x 10 MW-17 WT G 3,10 x x 11 MW-18 VJT G x x 12 MW-19 WT G ADDITIONAL COMMENTS RELINQUISHED BY IAFFILIATION DATE TIME ACCEPTED By IAFFILI !O DATE TIME mac. iP'/ Is�o � 5�'er�r •} — � ISZG SAMPLER NAME AND SIGNATURE r 1j� PRINT Name of SAMPLER; t �I�y Qtif�] ' I VA i ��+1 SIGNATURE of SAMPLER: � 1 No_ iAI t SIB 4f �� �� arfr t� i !J 5 3 T(003 4 ;AMPLE ONDITIONS � U _ m NOW N e N Z }• T 9 DATE Signed: r ❑ E 2 � 1r7.����4 ti fz � tic❑; r�mi? M 0 N aD rn ' ..�ae2AltaljRiCar Section A Required Client Information: Company. Municipal En Address: P.O. Box 97 Garner, NC 27529 Email To: jp{phl[[�me5G0 Phone: 919-772-5393 Requested Due DateiTAT. 1 ❑ SAMPLE ID One Character per box. (A,Z, ❑-s 1, -) Sample Ids must be unique tit F- 1 MVV-20 2 M W-21 3 MW-22 4 MW-23 5 s 7 a 9 1❑ 11 ?2 CHAIN -OF -CUSTODY 1 Analytical Request Document `Z2, 30 The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section B Section C Required Project Information: invoice Information: Page . 2 Of 2 lrvioes Report To: Jonathan Pfohl Attention: Municipal Engineering Services Copy To: Company Name; Address: Regulatory Agency Purchase Order No. Pace quote Reference: Client Project ID: SUETY Closed -Mt. Airy (UIC) Pace Project Manager: KeVln Godwin State 1 Location ult] Container Order Number Pace Profile #: North Carolina Requested Analysis Filtered (YIN) w a COLLECTED Preservatives N k N N N N N k N N N Y MATRIX D—Im ng Water Warr CODE Ow vV'r v oz Watf4 vftlr VAV Y U U s6v$welry o'i SL [7 START END o w w'Pa of WP j U a V ¢ N Air Ouxr T-" AR OT TS wW V m c-pa F x W O m DATE TEME DATE TIME v¢i S a= i 2 O g �j Q N v a o VVT G 5 _,7 s x x /�` 01 WT G x x x x x x x x x x VVT G 4 a•3S x x x No - ADDITIONAL COMMENTS RELINQUISHED BY I AF FI LIATION DATE TIME ACCEPTED BYI AFFILIATION SAMPLER NAME AND SIGNATURE PRINT Name of SAMPLER: Jonatha fohl SIGNATURE of SAMPLER: DATE TIME SAMPLE 9ONDITIONS Z�lIIIJ 1576 f r� l 1 A-1 E� O a m d z w Li c I- W .2 U U r 3 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 June 10, 2014 Mr. Jonathan Pfohl Municipal Engineering Services PO Box 97 Garner, NC 27529 RE: Project: SURRY MSWLF SWS Pace Project No.: 92203332 Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory on May 29, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Godwin kevin.godwin@pacelabs.com Project Manager Enclosures Q _Kok r REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 25 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 Project: SURRY MSWLF SWS Pace Project No.: 92203332 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Dr., Asheville, INC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 25 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 SAMPLE SUMMARY Project: SURRY MSWLF SWS Pace Project No.: 92203332 Lab ID Sample ID Matrix Date Collected Date Received 92203332001 SW-1 Water 05/27/1413:25 05/29/1415:20 92203332002 SW-2 Water 05/28/1418:20 05/29/1415:20 92203332003 SW-3 Water 05/28/1418:00 05/29/1415:20 92203332004 SWN-1 Water 05/28/1417:35 05/29/1415:20 92203332005 SWN-2 Water 05/28/1417:10 05/29/1415:20 92203332006 SW-4 Water 05/28/1417:00 05/29/1415:20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 25 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: SURRY MSWLF SWS 92203332 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92203332001 SW-1 EPA 6010 JMW 15 PASI-A EPA8260 NU1 51 PASI-C 92203332002 SW-2 EPA 6010 JMW 15 PASI-A EPA8260 NU1 51 PASI-C 92203332003 SW-3 EPA 6010 JMW 15 PASI-A EPA8260 NU1 51 PASI-C 92203332004 SWN-1 EPA 6010 JMW 15 PASI-A EPA8260 NU1 51 PASI-C 92203332005 SWN-2 EPA 6010 JMW 15 PASI-A EPA8260 NU1 51 PASI-C 92203332006 SW-4 EPA 6010 JMW 15 PASI-A EPA8260 NU1 51 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 25 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92203332 Sample: SW-1 Lab ID: 92203332001 Collected: 05/27/14 13:25 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 5.0 1 06/03/14 12:30 06/04/14 19:34 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:34 7440-38-2 Barium 22.5J ug/L 100 5.0 1 06/03/14 12:30 06/04/14 19:34 7440-39-3 Beryllium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 19:34 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 19:34 7440-43-9 Chromium ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:34 7440-47-3 Cobalt ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:34 7440-48-4 Copper ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:34 7440-50-8 Lead ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:34 7439-92-1 Nickel ND ug/L 50.0 5.0 1 06/03/14 12:30 06/04/14 19:34 7440-02-0 Selenium ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 19:34 7782-49-2 Silver ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:34 7440-22-4 Thallium ND ug/L 5.5 5.4 1 06/03/14 12:30 06/04/14 19:34 7440-28-0 Vanadium ND ug/L 25.0 5.0 1 06/03/14 12:30 06/04/14 19:34 7440-62-2 Zinc ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 19:34 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 05/31/14 06:20 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 05/31/14 06:20 107-13-1 Benzene ND ug/L 1.0 0.25 1 05/31/14 06:20 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 05/31/14 06:20 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 05/31/14 06:20 75-27-4 Bromoform ND ug/L 3.0 0.26 1 05/31/14 06:20 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 05/31/14 06:20 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 05/31/14 06:20 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 05/31/14 06:20 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 05/31/14 06:20 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 05/31/14 06:20 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 05/31/14 06:20 75-00-3 Chloroform ND ug/L 5.0 0.14 1 05/31/14 06:20 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 05/31/14 06:20 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 05/31/14 06:20 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 05/31/14 06:20 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 05/31/14 06:20 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 05/31/14 06:20 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 05/31/14 06:20 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 05/31/14 06:20 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 05/31/14 06:20 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 05/31/14 06:20 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 05/31/14 06:20 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 05/31/14 06:20 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 05/31/14 06:20 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 05/31/14 06:20 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 05/31/14 06:20 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 05/31/14 06:20 142-28-9 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 05/31/14 06:20 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/10/2014 12:19 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 25 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92203332 Sample: SW-1 Lab ID: 92203332001 Collected: 05/27/14 13:25 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 05/31/14 06:20 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 05/31/14 06:20 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 05/31/14 06:20 591-78-6 lodomethane ND ug/L 10.0 0.32 1 05/31/14 06:20 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 05/31/14 06:20 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 05/31/14 06:20 108-10-1 Styrene ND ug/L 1.0 0.26 1 05/31/14 06:20 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 05/31/14 06:20 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 05/31/14 06:20 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 05/31/14 06:20 127-18-4 Toluene ND ug/L 1.0 0.26 1 05/31/14 06:20 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 05/31/14 06:20 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 05/31/14 06:20 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 05/31/14 06:20 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 05/31/14 06:20 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 05/31/14 06:20 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 05/31/14 06:20 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 05/31/14 06:20 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 05/31/14 06:20 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 05/31/14 06:20 460-00-4 1,2-Dichloroethane-d4 (S) 98 % 70-130 1 05/31/14 06:20 17060-07-0 Toluene-d8 (S) 99 % 70-130 1 05/31/14 06:20 2037-26-5 Date: 06/10/2014 12:19 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 25 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92203332 Sample: SW-2 Lab ID: 92203332002 Collected: 05/28/14 18:20 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 5.0 1 06/03/14 12:30 06/04/14 19:43 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:43 7440-38-2 Barium 18.6J ug/L 100 5.0 1 06/03/14 12:30 06/04/14 19:43 7440-39-3 Beryllium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 19:43 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 19:43 7440-43-9 Chromium ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:43 7440-47-3 Cobalt 20.8 ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:43 7440-48-4 Copper ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:43 7440-50-8 Lead ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:43 7439-92-1 Nickel ND ug/L 50.0 5.0 1 06/03/14 12:30 06/04/14 19:43 7440-02-0 Selenium ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 19:43 7782-49-2 Silver ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:43 7440-22-4 Thallium ND ug/L 5.5 5.4 1 06/03/14 12:30 06/04/14 19:43 7440-28-0 Vanadium ND ug/L 25.0 5.0 1 06/03/14 12:30 06/04/14 19:43 7440-62-2 Zinc ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 19:43 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 05/31/14 02:26 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 05/31/14 02:26 107-13-1 Benzene ND ug/L 1.0 0.25 1 05/31/14 02:26 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 05/31/14 02:26 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 05/31/14 02:26 75-27-4 Bromoform ND ug/L 3.0 0.26 1 05/31/14 02:26 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 05/31/14 02:26 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 05/31/14 02:26 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 05/31/14 02:26 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 05/31/14 02:26 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 05/31/14 02:26 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 05/31/14 02:26 75-00-3 Chloroform ND ug/L 5.0 0.14 1 05/31/14 02:26 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 05/31/14 02:26 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 05/31/14 02:26 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 05/31/14 02:26 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 05/31/14 02:26 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 05/31/14 02:26 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 05/31/14 02:26 95-50-1 1,4-Dichlorobenzene 0.38J ug/L 1.0 0.33 1 05/31/14 02:26 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 05/31/14 02:26 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 05/31/14 02:26 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 05/31/14 02:26 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 05/31/14 02:26 75-35-4 cis-1,2-Dichloroethene 3.9J ug/L 5.0 0.19 1 05/31/14 02:26 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 05/31/14 02:26 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 05/31/14 02:26 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 05/31/14 02:26 142-28-9 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 05/31/14 02:26 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/10/2014 12:19 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 25 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92203332 Sample: SW-2 Lab ID: 92203332002 Collected: 05/28/14 18:20 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 05/31/14 02:26 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 05/31/14 02:26 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 05/31/14 02:26 591-78-6 lodomethane ND ug/L 10.0 0.32 1 05/31/14 02:26 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 05/31/14 02:26 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 05/31/14 02:26 108-10-1 Styrene ND ug/L 1.0 0.26 1 05/31/14 02:26 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 05/31/14 02:26 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 05/31/14 02:26 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 05/31/14 02:26 127-18-4 Toluene ND ug/L 1.0 0.26 1 05/31/14 02:26 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 05/31/14 02:26 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 05/31/14 02:26 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 05/31/14 02:26 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 05/31/14 02:26 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 05/31/14 02:26 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 05/31/14 02:26 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 05/31/14 02:26 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 05/31/14 02:26 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 05/31/14 02:26 460-00-4 1,2-Dichloroethane-d4 (S) 98 % 70-130 1 05/31/14 02:26 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 05/31/14 02:26 2037-26-5 Date: 06/10/2014 12:19 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 8 of 25 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92203332 Sample: SW-3 Lab ID: 92203332003 Collected: 05/28/14 18:00 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 5.0 1 06/03/14 12:30 06/04/14 19:46 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:46 7440-38-2 Barium 17.2J ug/L 100 5.0 1 06/03/14 12:30 06/04/14 19:46 7440-39-3 Beryllium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 19:46 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 19:46 7440-43-9 Chromium ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:46 7440-47-3 Cobalt ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:46 7440-48-4 Copper ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:46 7440-50-8 Lead ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:46 7439-92-1 Nickel ND ug/L 50.0 5.0 1 06/03/14 12:30 06/04/14 19:46 7440-02-0 Selenium ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 19:46 7782-49-2 Silver ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:46 7440-22-4 Thallium ND ug/L 5.5 5.4 1 06/03/14 12:30 06/04/14 19:46 7440-28-0 Vanadium ND ug/L 25.0 5.0 1 06/03/14 12:30 06/04/14 19:46 7440-62-2 Zinc ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 19:46 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 05/31/14 02:41 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 05/31/14 02:41 107-13-1 Benzene ND ug/L 1.0 0.25 1 05/31/14 02:41 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 05/31/14 02:41 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 05/31/14 02:41 75-27-4 Bromoform ND ug/L 3.0 0.26 1 05/31/14 02:41 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 05/31/14 02:41 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 05/31/14 02:41 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 05/31/14 02:41 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 05/31/14 02:41 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 05/31/14 02:41 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 05/31/14 02:41 75-00-3 Chloroform ND ug/L 5.0 0.14 1 05/31/14 02:41 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 05/31/14 02:41 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 05/31/14 02:41 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 05/31/14 02:41 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 05/31/14 02:41 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 05/31/14 02:41 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 05/31/14 02:41 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 05/31/14 02:41 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 05/31/14 02:41 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 05/31/14 02:41 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 05/31/14 02:41 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 05/31/14 02:41 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 05/31/14 02:41 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 05/31/14 02:41 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 05/31/14 02:41 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 05/31/14 02:41 142-28-9 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 05/31/14 02:41 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/10/2014 12:19 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 25 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92203332 Sample: SW-3 Lab ID: 92203332003 Collected: 05/28/14 18:00 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 05/31/14 02:41 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 05/31/14 02:41 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 05/31/14 02:41 591-78-6 lodomethane ND ug/L 10.0 0.32 1 05/31/14 02:41 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 05/31/14 02:41 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 05/31/14 02:41 108-10-1 Styrene ND ug/L 1.0 0.26 1 05/31/14 02:41 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 05/31/14 02:41 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 05/31/14 02:41 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 05/31/14 02:41 127-18-4 Toluene ND ug/L 1.0 0.26 1 05/31/14 02:41 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 05/31/14 02:41 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 05/31/14 02:41 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 05/31/14 02:41 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 05/31/14 02:41 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 05/31/14 02:41 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 05/31/14 02:41 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 05/31/14 02:41 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 05/31/14 02:41 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 05/31/14 02:41 460-00-4 1,2-Dichloroethane-d4 (S) 98 % 70-130 1 05/31/14 02:41 17060-07-0 Toluene-d8 (S) 101 % 70-130 1 05/31/14 02:41 2037-26-5 Date: 06/10/2014 12:19 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 25 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92203332 Sample: SWN-1 Lab ID: 92203332004 Collected: 05/28/14 17:35 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 5.0 1 06/03/14 12:30 06/04/14 19:50 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:50 7440-38-2 Barium 6.7J ug/L 100 5.0 1 06/03/14 12:30 06/04/14 19:50 7440-39-3 Beryllium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 19:50 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 19:50 7440-43-9 Chromium ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:50 7440-47-3 Cobalt ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:50 7440-48-4 Copper ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:50 7440-50-8 Lead ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:50 7439-92-1 Nickel ND ug/L 50.0 5.0 1 06/03/14 12:30 06/04/14 19:50 7440-02-0 Selenium ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 19:50 7782-49-2 Silver ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:50 7440-22-4 Thallium ND ug/L 5.5 5.4 1 06/03/14 12:30 06/04/14 19:50 7440-28-0 Vanadium ND ug/L 25.0 5.0 1 06/03/14 12:30 06/04/14 19:50 7440-62-2 Zinc ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 19:50 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 05/31/14 02:57 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 05/31/14 02:57 107-13-1 Benzene ND ug/L 1.0 0.25 1 05/31/14 02:57 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 05/31/14 02:57 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 05/31/14 02:57 75-27-4 Bromoform ND ug/L 3.0 0.26 1 05/31/14 02:57 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 05/31/14 02:57 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 05/31/14 02:57 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 05/31/14 02:57 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 05/31/14 02:57 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 05/31/14 02:57 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 05/31/14 02:57 75-00-3 Chloroform ND ug/L 5.0 0.14 1 05/31/14 02:57 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 05/31/14 02:57 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 05/31/14 02:57 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 05/31/14 02:57 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 05/31/14 02:57 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 05/31/14 02:57 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 05/31/14 02:57 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 05/31/14 02:57 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 05/31/14 02:57 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 05/31/14 02:57 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 05/31/14 02:57 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 05/31/14 02:57 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 05/31/14 02:57 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 05/31/14 02:57 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 05/31/14 02:57 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 05/31/14 02:57 142-28-9 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 05/31/14 02:57 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/10/2014 12:19 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 25 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92203332 Sample: SWN-1 Lab ID: 92203332004 Collected: 05/28/14 17:35 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 05/31/14 02:57 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 05/31/14 02:57 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 05/31/14 02:57 591-78-6 lodomethane ND ug/L 10.0 0.32 1 05/31/14 02:57 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 05/31/14 02:57 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 05/31/14 02:57 108-10-1 Styrene ND ug/L 1.0 0.26 1 05/31/14 02:57 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 05/31/14 02:57 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 05/31/14 02:57 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 05/31/14 02:57 127-18-4 Toluene ND ug/L 1.0 0.26 1 05/31/14 02:57 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 05/31/14 02:57 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 05/31/14 02:57 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 05/31/14 02:57 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 05/31/14 02:57 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 05/31/14 02:57 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 05/31/14 02:57 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 05/31/14 02:57 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 05/31/14 02:57 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 05/31/14 02:57 460-00-4 1,2-Dichloroethane-d4 (S) 98 % 70-130 1 05/31/14 02:57 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 05/31/14 02:57 2037-26-5 Date: 06/10/2014 12:19 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 12 of 25 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92203332 Sample: SWN-2 Lab ID: 92203332005 Collected: 05/28/14 17:10 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 5.0 1 06/03/14 12:30 06/04/14 19:53 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:53 7440-38-2 Barium 15.7J ug/L 100 5.0 1 06/03/14 12:30 06/04/14 19:53 7440-39-3 Beryllium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 19:53 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 19:53 7440-43-9 Chromium ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:53 7440-47-3 Cobalt ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:53 7440-48-4 Copper ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:53 7440-50-8 Lead ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:53 7439-92-1 Nickel ND ug/L 50.0 5.0 1 06/03/14 12:30 06/04/14 19:53 7440-02-0 Selenium ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 19:53 7782-49-2 Silver ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:53 7440-22-4 Thallium ND ug/L 5.5 5.4 1 06/03/14 12:30 06/04/14 19:53 7440-28-0 Vanadium ND ug/L 25.0 5.0 1 06/03/14 12:30 06/04/14 19:53 7440-62-2 Zinc ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 19:53 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 05/31/14 03:13 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 05/31/14 03:13 107-13-1 Benzene ND ug/L 1.0 0.25 1 05/31/14 03:13 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 05/31/14 03:13 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 05/31/14 03:13 75-27-4 Bromoform ND ug/L 3.0 0.26 1 05/31/14 03:13 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 05/31/14 03:13 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 05/31/14 03:13 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 05/31/14 03:13 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 05/31/14 03:13 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 05/31/14 03:13 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 05/31/14 03:13 75-00-3 Chloroform ND ug/L 5.0 0.14 1 05/31/14 03:13 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 05/31/14 03:13 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 05/31/14 03:13 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 05/31/14 03:13 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 05/31/14 03:13 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 05/31/14 03:13 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 05/31/14 03:13 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 05/31/14 03:13 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 05/31/14 03:13 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 05/31/14 03:13 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 05/31/14 03:13 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 05/31/14 03:13 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 05/31/14 03:13 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 05/31/14 03:13 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 05/31/14 03:13 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 05/31/14 03:13 142-28-9 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 05/31/14 03:13 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/10/2014 12:19 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 25 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92203332 Sample: SWN-2 Lab ID: 92203332005 Collected: 05/28/14 17:10 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 05/31/14 03:13 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 05/31/14 03:13 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 05/31/14 03:13 591-78-6 lodomethane ND ug/L 10.0 0.32 1 05/31/14 03:13 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 05/31/14 03:13 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 05/31/14 03:13 108-10-1 Styrene ND ug/L 1.0 0.26 1 05/31/14 03:13 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 05/31/14 03:13 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 05/31/14 03:13 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 05/31/14 03:13 127-18-4 Toluene ND ug/L 1.0 0.26 1 05/31/14 03:13 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 05/31/14 03:13 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 05/31/14 03:13 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 05/31/14 03:13 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 05/31/14 03:13 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 05/31/14 03:13 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 05/31/14 03:13 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 05/31/14 03:13 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 05/31/14 03:13 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 101 % 70-130 1 05/31/14 03:13 460-00-4 1,2-Dichloroethane-d4 (S) 99 % 70-130 1 05/31/14 03:13 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 05/31/14 03:13 2037-26-5 Date: 06/10/2014 12:19 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 14 of 25 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92203332 Sample: SW-4 Lab ID: 92203332006 Collected: 05/28/14 17:00 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010 Antimony ND ug/L 6.0 5.0 1 06/03/14 12:30 06/04/14 19:56 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:56 7440-38-2 Barium 16.6J ug/L 100 5.0 1 06/03/14 12:30 06/04/14 19:56 7440-39-3 Beryllium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 19:56 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 19:56 7440-43-9 Chromium ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:56 7440-47-3 Cobalt ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:56 7440-48-4 Copper ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:56 7440-50-8 Lead ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:56 7439-92-1 Nickel ND ug/L 50.0 5.0 1 06/03/14 12:30 06/04/14 19:56 7440-02-0 Selenium ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 19:56 7782-49-2 Silver ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 19:56 7440-22-4 Thallium ND ug/L 5.5 5.4 1 06/03/14 12:30 06/04/14 19:56 7440-28-0 Vanadium ND ug/L 25.0 5.0 1 06/03/14 12:30 06/04/14 19:56 7440-62-2 Zinc ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 19:56 7440-66-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 05/31/14 03:28 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 05/31/14 03:28 107-13-1 Benzene ND ug/L 1.0 0.25 1 05/31/14 03:28 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 05/31/14 03:28 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 05/31/14 03:28 75-27-4 Bromoform ND ug/L 3.0 0.26 1 05/31/14 03:28 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 05/31/14 03:28 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 05/31/14 03:28 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 05/31/14 03:28 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 05/31/14 03:28 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 05/31/14 03:28 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 05/31/14 03:28 75-00-3 Chloroform ND ug/L 5.0 0.14 1 05/31/14 03:28 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 05/31/14 03:28 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 05/31/14 03:28 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 05/31/14 03:28 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 05/31/14 03:28 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 05/31/14 03:28 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 05/31/14 03:28 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 05/31/14 03:28 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 05/31/14 03:28 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 05/31/14 03:28 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 05/31/14 03:28 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 05/31/14 03:28 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 05/31/14 03:28 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 05/31/14 03:28 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 05/31/14 03:28 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 05/31/14 03:28 142-28-9 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 05/31/14 03:28 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/10/2014 12:19 PM without the written consent of Pace Analytical Services, Inc.. Page 15 of 25 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92203332 Sample: SW-4 Lab ID: 92203332006 Collected: 05/28/14 17:00 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 05/31/14 03:28 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 05/31/14 03:28 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 05/31/14 03:28 591-78-6 lodomethane ND ug/L 10.0 0.32 1 05/31/14 03:28 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 05/31/14 03:28 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 05/31/14 03:28 108-10-1 Styrene ND ug/L 1.0 0.26 1 05/31/14 03:28 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 05/31/14 03:28 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 05/31/14 03:28 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 05/31/14 03:28 127-18-4 Toluene ND ug/L 1.0 0.26 1 05/31/14 03:28 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 05/31/14 03:28 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 05/31/14 03:28 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 05/31/14 03:28 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 05/31/14 03:28 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 05/31/14 03:28 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 05/31/14 03:28 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 05/31/14 03:28 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 05/31/14 03:28 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 05/31/14 03:28 460-00-4 1,2-Dichloroethane-d4 (S) 96 % 70-130 1 05/31/14 03:28 17060-07-0 Toluene-d8 (S) 99 % 70-130 1 05/31/14 03:28 2037-26-5 Date: 06/10/2014 12:19 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 16 of 25 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY MSWLF SWS Pace Project No.: 92203332 QC Batch: MPRP/16107 Analysis Method: EPA6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET NC Groundwater Associated Lab Samples: 92203332001, 92203332002, 92203332003, 92203332004, 92203332005, 92203332006 METHOD BLANK: 1212519 Matrix: Water Associated Lab Samples: 92203332001, 92203332002, 92203332003, 92203332004, 92203332005, 92203332006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Antimony ug/L ND 6.0 06/04/1419:28 Arsenic ug/L ND 10.0 06/04/1419:28 Barium ug/L ND 100 06/04/1419:28 Beryllium ug/L ND 1.0 06/04/1419:28 Cadmium ug/L ND 1.0 06/04/1419:28 Chromium ug/L ND 10.0 06/04/1419:28 Cobalt ug/L ND 10.0 06/04/1419:28 Copper ug/L ND 10.0 06/04/1419:28 Lead ug/L ND 10.0 06/04/1419:28 Nickel ug/L ND 50.0 06/04/1419:28 Selenium ug/L ND 10.0 06/04/1419:28 Silver ug/L ND 10.0 06/04/1419:28 Thallium ug/L ND 5.5 06/04/1419:28 Vanadium ug/L ND 25.0 06/04/1419:28 Zinc ug/L ND 10.0 06/04/1419:28 LABORATORY CONTROL SAMPLE: Parameter 1212520 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Antimony ug/L 500 497 99 80-120 Arsenic ug/L 500 477 95 80-120 Barium ug/L 500 502 100 80-120 Beryllium ug/L 500 479 96 80-120 Cadmium ug/L 500 480 96 80-120 Chromium ug/L 500 486 97 80-120 Cobalt ug/L 500 495 99 80-120 Copper ug/L 500 494 99 80-120 Lead ug/L 500 497 99 80-120 Nickel ug/L 500 478 96 80-120 Selenium ug/L 500 495 99 80-120 Silver ug/L 250 242 97 80-120 Thallium ug/L 500 469 94 80-120 Vanadium ug/L 500 480 96 80-120 Zinc ug/L 500 478 96 80-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/10/2014 12:19 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 25 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: SURRY MSWLF SWS 92203332 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1212521 1212522 MS MSD 92203332001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 474 483 95 97 75-125 2 25 Arsenic ug/L ND 500 500 456 468 91 94 75-125 3 25 Barium ug/L 22.5J 500 500 490 511 94 98 75-125 4 25 Beryllium ug/L ND 500 500 454 471 91 94 75-125 4 25 Cadmium ug/L ND 500 500 456 467 91 93 75-125 2 25 Chromium ug/L ND 500 500 462 476 92 95 75-125 3 25 Cobalt ug/L ND 500 500 464 480 93 96 75-125 3 25 Copper ug/L ND 500 500 475 480 95 96 75-125 1 25 Lead ug/L ND 500 500 465 478 93 96 75-125 3 25 Nickel ug/L ND 500 500 453 467 91 93 75-125 3 25 Selenium ug/L ND 500 500 467 479 93 96 75-125 2 25 Silver ug/L ND 250 250 229 235 91 94 75-125 3 25 Thallium ug/L ND 500 500 446 459 89 92 75-125 3 25 Vanadium ug/L ND 500 500 457 472 91 94 75-125 3 25 Zinc ug/L ND 500 500 457 467 91 93 75-125 2 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/10/2014 12:19 PM without the written consent of Pace Analytical Services, Inc.. Page 18 of 25 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY MSWLF SWS Pace Project No.: 92203332 QC Batch: MSV/27034 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92203332001, 92203332002, 92203332003, 92203332004, 92203332005, 92203332006 METHOD BLANK: 1210761 Matrix: Water Associated Lab Samples: 92203332001, 92203332002, 92203332003, 92203332004, 92203332005, 92203332006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 5.0 05/31/14 01:23 1,1,1-Trichloroethane ug/L ND 1.0 05/31/14 01:23 1,1,2,2-Tetrachloroethane ug/L ND 3.0 05/31/14 01:23 1,1,2-Trichloroethane ug/L ND 1.0 05/31/14 01:23 1,1-Dichloroethane ug/L ND 5.0 05/31/14 01:23 1,1-Dichloroethene ug/L ND 5.0 05/31/14 01:23 1,2,3-Trichloropropane ug/L ND 1.0 05/31/14 01:23 1,2-Dibromo-3-chloropropane ug/L ND 13.0 05/31/14 01:23 1,2-Dibromoethane (EDB) ug/L ND 1.0 05/31/14 01:23 1,2-Dichlorobenzene ug/L ND 5.0 05/31/14 01:23 1,2-Dichloroethane ug/L ND 1.0 05/31/14 01:23 1,2-Dichloropropane ug/L ND 1.0 05/31/14 01:23 1,3-Dichloropropane ug/L ND 1.0 05/31/14 01:23 1,4-Dichlorobenzene ug/L ND 1.0 05/31/14 01:23 2-Butanone (MEK) ug/L ND 100 05/31/14 01:23 2-Hexanone ug/L ND 50.0 05/31/14 01:23 4-Methyl-2-pentanone (MIBK) ug/L ND 100 05/31/14 01:23 Acetone ug/L ND 100 05/31/14 01:23 Acrylonitrile ug/L ND 200 05/31/14 01:23 Benzene ug/L ND 1.0 05/31/14 01:23 Bromochloromethane ug/L ND 3.0 05/31/14 01:23 Bromodichloromethane ug/L ND 1.0 05/31/14 01:23 Bromoform ug/L ND 3.0 05/31/14 01:23 Bromomethane ug/L ND 10.0 05/31/14 01:23 Carbon disulfide ug/L ND 100 05/31/14 01:23 Carbon tetrachloride ug/L ND 1.0 05/31/14 01:23 Chlorobenzene ug/L ND 3.0 05/31/14 01:23 Chloroethane ug/L ND 10.0 05/31/14 01:23 Chloroform ug/L ND 5.0 05/31/14 01:23 Chloromethane ug/L ND 1.0 05/31/14 01:23 cis-1,2-Dichloroethene ug/L ND 5.0 05/31/14 01:23 cis-1,3-Dichloropropene ug/L ND 1.0 05/31/14 01:23 Dibromochloromethane ug/L ND 3.0 05/31/14 01:23 Dibromomethane ug/L ND 10.0 05/31/14 01:23 Ethylbenzene ug/L ND 1.0 05/31/14 01:23 lodomethane ug/L ND 10.0 05/31/14 01:23 Methylene Chloride ug/L ND 1.0 05/31/14 01:23 Styrene ug/L ND 1.0 05/31/14 01:23 Tetrachloroethene ug/L ND 1.0 05/31/14 01:23 Toluene ug/L ND 1.0 05/31/14 01:23 trans-1,2-Dichloroethene ug/L ND 5.0 05/31/14 01:23 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/10/2014 12:19 PM without the written consent of Pace Analytical Services, Inc.. Page 19 of 25 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY MSWLF SWS Pace Project No.: 92203332 METHOD BLANK: 1210761 Matrix: Water Associated Lab Samples: 92203332001, 92203332002, 92203332003, 92203332004, 92203332005, 92203332006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers trans- 1,3-Dichloropropene ug/L ND 1.0 05/31/14 01:23 trans-1,4-Dichloro-2-butene ug/L ND 100 05/31/14 01:23 Trichloroethene ug/L ND 1.0 05/31/14 01:23 Trichlorofluoromethane ug/L ND 1.0 05/31/14 01:23 Vinyl acetate ug/L ND 50.0 05/31/14 01:23 Vinyl chloride ug/L ND 1.0 05/31/14 01:23 Xylene (Total) ug/L ND 5.0 05/31/14 01:23 1,2-Dichloroethane-d4 (S) % 97 70-130 05/31/14 01:23 4-Bromofluorobenzene (S) % 99 70-130 05/31/14 01:23 Toluene-d8 (S) % 100 70-130 05/31/14 01:23 LABORATORY CONTROL SAMPLE: Parameter 1210762 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 46.3 93 70-130 1,1,1-Trichloroethane ug/L 50 47.2 94 70-130 1,1,2,2-Tetrachloroethane ug/L 50 48.1 96 70-130 1,1,2-Trichloroethane ug/L 50 49.6 99 70-130 1,1-Dichloroethane ug/L 50 44.5 89 70-130 1,1-Dichloroethene ug/L 50 50.3 101 70-132 1,2,3-Trichloropropane ug/L 50 50.0 100 70-130 1,2-Dibromo-3-chloropropane ug/L 50 49.9 100 70-130 1,2-Dibromoethane (EDB) ug/L 50 48.1 96 70-130 1,2-Dichlorobenzene ug/L 50 48.4 97 70-130 1,2-Dichloroethane ug/L 50 47.1 94 70-130 1,2-Dichloropropane ug/L 50 47.3 95 70-130 1,3-Dichloropropane ug/L 50 47.3 95 70-130 1,4-Dichlorobenzene ug/L 50 46.9 94 70-130 2-Butanone (MEK) ug/L 100 99.91 100 70-145 2-Hexanone ug/L 100 98.5 99 70-144 4-Methyl-2-pentanone (MIBK) ug/L 100 107 107 70-140 Acetone ug/L 100 96.9J 97 50-175 Acrylonitrile ug/L 250 247 99 70-143 Benzene ug/L 50 48.8 98 70-130 Bromochloromethane ug/L 50 49.0 98 70-130 Bromodichloromethane ug/L 50 46.3 93 70-130 Bromoform ug/L 50 48.6 97 70-130 Bromomethane ug/L 50 46.2 92 54-130 Carbon disulfide ug/L 50 48.OJ 96 70-131 Carbon tetrachloride ug/L 50 52.4 105 70-132 Chlorobenzene ug/L 50 45.4 91 70-130 Chloroethane ug/L 50 51.7 103 64-134 Chloroform ug/L 50 47.1 94 70-130 Chloromethane ug/L 50 47.7 95 64-130 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/10/2014 12:19 PM without the written consent of Pace Analytical Services, Inc.. Page 20 of 25 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY MSWLF SWS Pace Project No.: 92203332 LABORATORY CONTROL SAMPLE: Parameter 1210762 Units Spike Conc. LCS Result LCS % Rec % Rec Limits cis-1,2-Dichloroethene ug/L 50 47.4 95 70-131 cis-1,3-Dichloropropene ug/L 50 47.2 94 70-130 Dibromochloromethane ug/L 50 45.6 91 70-130 Dibromomethane ug/L 50 48.2 96 70-131 Ethylbenzene ug/L 50 45.4 91 70-130 lodomethane ug/L 100 95.0 95 49-180 Methylene Chloride ug/L 50 50.8 102 63-130 Styrene ug/L 50 48.7 97 70-130 Tetrachloroethene ug/L 50 49.5 99 70-130 Toluene ug/L 50 47.8 96 70-130 trans-1,2-Dichloroethene ug/L 50 48.3 97 70-130 trans- 1,3-Dichloropropene ug/L 50 47.5 95 70-132 trans-1,4-Dichloro-2-butene ug/L 50 49.6J 99 70-141 Trichloroethene ug/L 50 48.0 96 70-130 Trichlorofluoromethane ug/L 50 55.6 111 62-133 Vinyl acetate ug/L 100 99.1 99 66-157 Vinyl chloride ug/L 50 60.4 121 69-130 Xylene (Total) ug/L 150 139 93 70-130 1,2-Dichloroethane-d4 (S) % 97 70-130 4-Bromofluorobenzene (S) % 99 70-130 Toluene-d8 (S) % 102 70-130 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1211546 1211547 MS MSD 92203116003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,1-Dichloroethene ug/L ND 50 50 56.2 60.5 112 121 70-166 7 30 Benzene ug/L 0.42J 50 50 52.0 56.3 103 112 70-148 8 30 Chlorobenzene ug/L 0.38J 50 50 48.3 51.7 96 103 70-146 7 30 Toluene ug/L ND 50 50 48.5 52.1 97 104 70-155 7 30 Trichloroethene ug/L ND 50 50 54.1 57.7 108 115 69-151 7 30 1,2-Dichloroethane-d4 (S) % 99 100 70-130 4-Bromofluorobenzene (S) % 100 101 70-130 Toluene-d8(S) % 101 102 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/10/2014 12:19 PM without the written consent of Pace Analytical Services, Inc.. Page 21 of 25 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALIFIERS Project: SURRY MSWLF SWS Pace Project No.: 92203332 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference INC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/10/2014 12:19 PM without the written consent of Pace Analytical Services, Inc.. Page 22 of 25 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: SURRY MSWLF SWS Pace Project No.: 92203332 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92203332001 SW-1 EPA 3010 MPRP/16107 EPA 6010 92203332002 SW-2 EPA 3010 MPRP/16107 EPA 6010 92203332003 SW-3 EPA 3010 MPRP/16107 EPA 6010 92203332004 SWN-1 EPA 3010 MPRP/16107 EPA 6010 92203332005 SWN-2 EPA 3010 MPRP/16107 EPA 6010 92203332006 SW-4 EPA 3010 MPRP/16107 EPA 6010 92203332001 SW-1 EPA 8260 MSV/27034 92203332002 SW-2 EPA 8260 MSV/27034 92203332003 SW-3 EPA 8260 MSV/27034 92203332004 SWN-1 EPA 8260 MSV/27034 92203332005 SWN-2 EPA 8260 MSV/27034 92203332006 SW-4 EPA 8260 MSV/27034 Date: 06/10/2014 12:19 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Analytical Batch ICP/14568 ICP/14568 ICP/14568 ICP/14568 ICP/14568 ICP/14568 Page 23 of 25 Document Name: Document Revised: April 07. 2014 aCeAnafytiCr� Sample Condition Upon Receipt (SCUR) Page 1 of 2 Document Number: Issuing Authority: F-CHR-CS-003-rev.14 Pace Huntersville Quali Office Client Name:,�;;x,� Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Client[] Commercla Pace Other Custody Seal on Cooler/Box Present: Elyes Kf no Seals intact: ❑ yes Packing Material: ❑ Bubble Wrap Bubble Sags ❑ None ❑ Other Thermometer Used: I Gun T1102 140 Type of Ice: et slue None Temp Correction Factor T1102: o Correction T1301: No Correction D tlonai ❑ no Pro}. Due Data: Proj. Name: Samples on ice, cooling process has begun ��,C 9 Date and Ini ' Is of ess"L examining Corrected Cooler Temp.: Biological Tissue is Frozen: Yes No IA contents: 'J a Temo should be above freexino to 6°C Comments: _ Chain of Custody Present: r s ❑No ❑N1A 1. Chain of Custody Filled Out: Y s ❑No ❑NIA 2. Chain of Custody Relinquished: 6es []No ❑NIA 3. Sampler Name & Signature on COG: es ❑No ❑NIA 4, Samples Arrived within Hold Time: Yes [:]No ❑NIA 5, Short Hold Time Analysis (<72hr): ❑Yes PK. ❑N1A 6. Rush Turn Around Time Requested: ❑Yes a ❑NIA 7. Sufficient Volume: Ye ❑No ❑NIA 8, Correct Containers Used: a ❑No ❑N1A g, -Pace Containers Used: es ❑N❑ ❑NIA Containers Intact: Yes ❑No ❑NI 10. Filtered volume received for Dissolved tests ❑Yes ©N❑ NIA 11. Sample Labels COC: ❑res ?(No ❑N1A 12. match -Includes date/time/ID/Analysis Matrix: All containers needing preservation have been checked. ra,,,,Ie/s LINO❑N!A 13. All containers needing preservation are found to be in G' El No ❑NIA compliance with EPA recommendation. �' exceptions: VOA, coliform, TOO, O&G, WI-DRO (water) es ❑No Samples checked for dechlorination: es LINO ❑NIA 14. Headspace in VOA Vials >6mm): ❑Yes VNo ❑NIA 15. Trip Blank Present: ❑Yes []No N/1A 16. Trip Blank Custody Seals Present ❑Yes ❑No E IA Pace Trip Blank Lot # (if purchased): Client Notification! Resolution: Field Data Required? Y I N Person Contacted: j U �f-2r Date/Time: 5 1-3 � Comments/ Resolution: r_(, r-4 ":/" ""�'� - V Lur - < 0IS' 2 7 SCURF Review:j Date: 1. 44 ' . SRF Review: �� iDate.5: 34' It Note: Whenever ther ' a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e out of hold, incorrect preservative, out of temp, incorrect containers] w0#:92203332 �iu�iiMon 92203332 Page 24 of 25 . PdceAnaPyfical CHAIN -OF -CUSTODY / Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Required Client Information: Required Project Information: Invoice Information: Page: 1 Of 1 Company: Municipal Engineering Services Report To: Jonathan Pfohl Attention: Municipal Engineering Services Address: P.O. BOX 97 Copy To: Company Name: Garner, NC 27529 Address: Regulatory Agency] Email To: I pfohl(CDmesCO.Com Purchase Order No. Pace Quote Reference: Phone: 919-772-5393 1 Fax Client Project ID: Slurry MSWLF SWs Pace Project Manager: Kevin Godwin State / Location Requested Due Date/TAT: 10 Day (Default) Container Order Number: Pace Profile #: North Carolina Requested Analysis Filtered (Y/N). Z_S _ COLLECTED Preservatives N N MATRIX CODE 2 Drinking Water DW Water WT v 0 U Z O Waste Water WW SAMPLE ID - START END W o w sen�som su d One Character per box. Oil O� Wipe WP i7 U F Q �. (A-Z, 0-9 1 Air AR W W z .� a) Sample Ids must be unique Other OT 0 y w < rn a n # Tissue 7S X J J °' O v°Ji n v OLILI ON N. o C " `N ~ w DATE TIME DATE TIME Z) N _ O _ = O z z 2 O Q O ;1 SW-1 - WT G 1 4 1 3 x x 2" SW-2 WT G J ao 4 1 3 x x '3 5W-3 WT G AWN (1-1-14; 4 1 3 x x 4 SW-4 ;' WT G 4 1 3 x x .$.. SWN-1 WT G S' 4 1 x x QO SWN-2 4 Z3 6 I'll x x 7__' SI 8 9_ 10 11 12' ADDITIONAL COMMENTS : RELINQUISHED BY/ AFFILIATION DATE : TIME ACCEPTED BY / AFFILIATION DATE TIME SAMPLE CONDITIONS PF/Y SAMPLER NAME AND SIGNATURE C N _ U � a ti Y PRINT Name of SAMPLER: Jon t n PfOhl ;Z 0 E z SIGNATURE of SAMPLER: .DATE Signed: N O LO N m rn m D_ Environmental Conservation Laboratories, Inc. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Friday, June 13, 2014 Municipal Engineering Services (M0001) Attn: Jonathan Pfohl P.O. Box 97 Garner, NC 27529 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Surry Co. Closed MSWLF - Mt. Airy ENCO Workorder(s): C406877 Dear Jonathan Pfohl, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Monday, June 2, 2014. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, 00, (/ L- - C�- A Chuck Smith Project Manager Enclosure(s) (� �C—o www.encolabs.com The total number of pages in this report, including this page is 13. (� �C-O www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: MW-1 A Lab ID: C406877-01 Sampled: 05/28/14 08:05 Received: 06/02/14 09:40 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - EPA 300.0 06/25/14 06/05/14 11:21 6/5/2014 21:08 Client ID: MW-3R Lab ID: C406877-02 Sampled: 05/28/14 08:40 Received: 06/02/14 09:40 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - EPA 300.0 06/25/14 06/05/14 11:21 6/5/2014 21:59 Client ID: MW-13 w Lab ID: C406877-03 Sampled: 05/28/14 11:00 Received: 06/02/14 09:40 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 06/25/14 06/05/14 11:21 6/5/2014 22:50 Client ID: MW-14 Lab ID: C406877-04 Sampled: 05/28/14 10:15 Received: 06/02/14 09:40 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - EPA 300.0 06/25/14 06/05/14 11:21 6/5/2014 23:07 Client ID: MW-15 Lab ID: C406877-05 Sampled: 05/28/14 09:45 Received: 06/02/14 09:40 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - EPA 300.0 06/25/14 06/05/14 11:21 6/5/2014 23:24 Client ID: MW-16 M Lab ID: C406877-06 Sampled: 05/28/14 09:10 Received: 06/02/14 09:40 Parameter Hold Date/Time(.) Prep Date/Time(s) Analysis Date/Time(s) - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - EPA 300.0 06/25/14 06/05/14 11:21 6/5/2014 23:41 Client ID: MW-21 Lab ID: C406877-07 Sampled: 05/28/14 13:40 Received: 06/02/14 09:40 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - EPA 300.0 06/25/14 06/05/14 11:21 6/5/2014 23:58 Page 2 of 13 (� 0a www.encolabs.com NORTH CAROLINA SWS SAMPLE DETECTION SUMMARY lient ID: MW-3R Lab ID: C406877-02 Analyte Bromide Results 0.040 Flag 3 DF 1 MDL 0.030 MRL 0.50 NC SWSL NE Units mg/L Method EPA 300.0 Notes lient ID: MW-13 Lab ID: C406877-03 Analyte Bromide Results 0.22 Flag 1 DF 1 MDL 0.030 MRL 0.50 NC SWSL NE Units mg/L Method EPA 300.0 Notes lient ID: MW-14 Lab ID: C406877-04 Analyte Bromide Results 0.044 Flag 1 DF 1 MDL 0.030 MRL 0.50 NC SWSL - - - - - NE Units - - - - mg/L Method - - - - - - - EPA 300.0 Notes - - - - - lient ID: MW-15 Lab ID: C406877-05 Analyte Bromide Results 0.033 Flag 1 DF 1 MDL 0.030 MRL 0.50 NC SWSL NE Units mg/L Method EPA 300.0 Notes lient ID: MW-16 Lab ID: C406877-06 Analyte Bromide Results 0.22 Flag 1 DF 1 MDL 0.030 MRL 0.50 NC SWSL - - NE Units - - - - mg/L Method - - - - - - - EPA 300.0 Notes - - - - - lient ID: MW-21 Lab ID: C406877-07 Analyte Bromide Results 0.23 Flag 1 DF 1 MDL 0.030 MRL - - 0.50 NC SWSL - - - - - NE Units - - - - mg/L Method - - - - - - - EPA 300.0 Notes - - - - - Page 3 of 13 (� 0a www.encolabs.com ANALYTICAL RESULTS Description: MW-1 Lab Sample ID: C406877-01 Received: 06/02/14 09:40 Matrix: Ground Water Sampled: 05/28/14 08:05 Work Order: C406877 Project: Surry Co. Closed MSWLF - Mt. Airy Sampled By: Tom Lager Classical Chemistry Parameters - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - ^ - ENCO Cary certlfied analyte [NC 591] Analyte rCAS Numberl Results Fla" Units DF MDL MRL NC SWSL Method Analyzed Notes Bromide [24959-67-9] ^ 0.030 U mg/L 1 0.030 0.50 NE EPA 300.0 06/05/14 21:08 CV This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 13 (� 0a www.encolabs.com Description: MW-3R Lab Sample ID: C406877-02 Received: 06/02/14 09:40 Matrix: Ground Water Sampled: 05/28/14 08:40 Work Order: C406877 Project: Surry Co. Closed MSWLF - Mt. Airy Sampled By: Tom Lager Classical Chemistry Parameters - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL MRL NC SWSL Method Analyzed Ay Notes Bromide [24959-67-9] ^ 0.040 J mg/L 1 0.030 0.50 NE EPA 300.0 06/05/14 21:59 CV This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 13 (� 0a www.encolabs.com Description: MW-13 Lab Sample ID: C406877-03 Received: 06/02/14 09:40 Matrix: Ground Water Sampled: 05/28/14 11:00 Work Order: C406877 Project: Surry Co. Closed MSWLF - Mt. Airy Sampled By: Tom Lager Classical Chemistry Parameters - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL MRL NC SWSL Method Analyzed Ay Notes Bromide [24959-67-9] ^ 0.22 J mg/L 1 0.030 0.50 NE EPA 300.0 06/05/14 22:50 CV This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 13 (� 0a www.encolabs.com Description: MW-14 Lab Sample ID: C406877-04 Received: 06/02/14 09:40 Matrix: Ground Water Sampled: 05/28/14 10:15 Work Order: C406877 Project: Surry Co. Closed MSWLF - Mt. Airy Sampled By: Tom Lager Classical Chemistry Parameters - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL MRL NC SWSL Method Analyzed Ay Notes Bromide [24959-67-9] ^ 0.044 J mg/L 1 0.030 0.50 NE EPA 300.0 06/05/14 23:07 CV This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 13 (� 0a www.encolabs.com Description: MW-15 Lab Sample ID: C406877-05 Received: 06/02/14 09:40 Matrix: Ground Water Sampled: 05/28/14 09:45 Work Order: C406877 Project: Surry Co. Closed MSWLF - Mt. Airy Sampled By: Tom Lager Classical Chemistry Parameters - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL MRL NC SWSL Method Analyzed Ay Notes Bromide [24959-67-9] ^ 0.033 J mg/L 1 0.030 0.50 NE EPA 300.0 06/05/14 23:24 CV This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 13 (� 0a www.encolabs.com Description: MW-16 Lab Sample ID: C406877-06 Received: 06/02/14 09:40 Matrix: Ground Water Sampled: 05/28/14 09:10 Work Order: C406877 Project: Surry Co. Closed MSWLF - Mt. Airy Sampled By: Tom Lager Classical Chemistry Parameters - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL MRL NC SWSL Method Analyzed Ay Notes Bromide [24959-67-9] ^ 0.22 J mg/L 1 0.030 0.50 NE EPA 300.0 06/05/14 23:41 CV This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 13 (� 0a www.encolabs.com Description: MW-21 Lab Sample ID: C406877-07 Received: 06/02/14 09:40 Matrix: Ground Water Sampled: 05/28/14 13:40 Work Order: C406877 Project: Surry Co. Closed MSWLF - Mt. Airy Sampled By: Tom Lager Classical Chemistry Parameters - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL MRL NC SWSL Method Analyzed Ay Notes Bromide [24959-67-9] ^ 0.23 J mg/L 1 0.030 0.50 NE EPA 300.0 06/05/14 23:58 CV This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 13 QUALITY CONTROL Classical Chemistry Parameters - Quality Control Batch 4FO5029 - NO PREP (� �C-O www.encolabs.com Blank (4F05029-BLK3) Prepared: 06/05/2014 11:21 Analyzed: 06/05/2014 19:09 �Analyte %REC RPD Result Flag MRL %REC Limits Limit Notes Bromide 0.030 U 0.50 mg/L - - - - - - - - - - - - - - LCS (4F05029-BS1) - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - Prepared: 06/05/2014 11:21 Analyzed: 06/05/2014 12:55 - - - - - - - - Spike Source %REC RPD Analyte Level Result %REC Limits RPD Limit Notes Bromide 2.5 0.50 mg/L 2.50 100 90-110 - - - - - - - - - - - - - - Matrix Spike (4F05029-MS1) - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - Prepared: 06/05/2014 11:21 Analyzed: 06/05/2014 21:25 - - - - - - - - Source:C406877-01 Spike Source %REC RPD Analyte Result Flag Units Level Result %REC Limits RPD Limit Notes Bromide 1.0 0.50 mg/L 1.00 0.030 U 102 90-110 Matrix Spike Dup (4F05029-MSD1) - - - - - - - - - - - - - - - - - - - - - - - - - - - Prepared: 06/05/2014 11:21 Analyzed: 06/05/2014 21:42 - - - - - - - - Source:C406877-01 �Analyte Spike Source %REC Result Flag MRL Units Level Result %REC Limits RPD Bromide 1.0 0.50 mg/L 1.00 0.030 U 103 90-110 1 10 Page 11 of 13 (� 0a www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. I The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. Page 12 of 13 { � ._ �. uy§ rr ° F1�f1. N AL CONSERVATION €_!�€�ONAT��€•�,�ES � N�IRONt��� c:���i�.EFV-C�1°_�L�ayTC.�I"�� RECORD 1 7�/y5 Central Part D.. 4ti10 Park Gourt 5:n➢ef1i IWA WoonV.grts Il r[tu rndCakirts } w - = rNi ndo FL32S2A ,lackscnV:Ih FL32-1G-rig59 C..ary NC2f511 a {4U7) 93.6-;314 Fax {407) 85G-6945 (904) 29a-3007 Fa+:(GP4) 29.(, BF4p (419) 167-3090 Fax (91W) 46'/,3S4b "lien) ha.ma Prn)ect NumPrtr„�.�.....�.u...,...�w,�.r.,�.zz..�.,u�... �� FtcquesSrd pnalyses� MtaM iP21 EntJineering Services (FOU001) ,...-- e _ +,.d9res,s ---� Arojec[ Namell)est - �— PC? Box 97 Surry Co Closed MSVVLF, Mi. Airy :;ityiS7i2iF Pnjv I Blllmg info Garner NC; 27529 Fax ReportingContact (913) 772-5393 (919) 'i 72-1176 Jonathan Pfohl SampleY(s) Name. Affriatlon (Print) — 3Illort2 Cnnlaei Toni lager', MESCO ACCOunts Payable co '.sJ �ionalwe �- �'—� ,�•������� ^arrrpie ID (Field lc eMt,ficaiion) Collection Date Facility tf {if regwrad) - CalEectiun � anx`� sce �.esa c Time,,COMP 1 GraG E 0 i � Preservation -�.���_� {Seee �odesj "� {Comnine as MW-1 _ 5/28114 &05 GRAB � GW_. 1� x M1�1f-3R ..�._--_.��___•._. 5128114 8:40 GRAB. . GW.`��. 1 X ___._ � ..__, fVIU1d-13 _ _......_._....,�._...,.,___.. 5I28114 11:00 CRaB.. _ _..__ .._._•_ MIIU-14•„_., ......_..._...-...._..__ 5128114 10:15 GRAB GW 1 X .,_.._ MW--15 5128/14 9:45 GRAB � G�1 1 - -- X — SJ€W•-16 a — 5/28/14 9:10 (-',RAB GW �u 1 Y 28/14 1:40 GPAB G\N 1 X Page of Requeste) Turnaround Times h!,-itr� rivan requests 5u4jeci to iiv iiie racilliy Standard Expedited Due I 1 ab VVorkorder Sample Comments G 8 I of@l # Ot uontainers -.r a 7.7:w �. - &ern�io Ili! Preparad By wire) rn�: Jonathan Pfoh Dalr:ll irne 2e -�i"C! �j �/ hate im� r z� �w❑Grl.�v�� L ! S Cuc,-rrrr•rs Uatefime Rece�v. Fi -- - Da el finis 17 '�•-� ❑[ilefTlme Reneivad By Dateffnne oo—OF "'st . 1 LIrnp in Rc:.011 ondition Upon Nriucipt r✓ d�cceptahle U R f•1a[tix GiVY Cruondvlaier s[}-5otl SF�Sedirrlant 5W-Surfn^OWaimr �1J�r-lrinstrx�ater /lfvt {3 Jther (de�;l In commr�nisY Presen�etiur�t Ic- H-NCI N Fil�3 h+�g04fdC1 NACH O�ihe+r d�c+iail in cornmenis) Nnie H(� s-�mplas s]urro-€led to Er1'16 tabs ire in aGcnrd;,; I; r, mhlh Ihrt inrrns an.{ � nnddinns Us;etl urr th=r�-:erse or IStiis folio 4nlFss pnA�NS�llen agr�cmehi_c e�Hst XG)�l Environmental Conservation Laboratories, Inc. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Thursday, June 12, 2014 Municipal Engineering Services (M0001) Attn: Jonathan Pfohl P.O. Box 97 Garner, NC 27529 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Surry Closed Mt. Airy (UIC) ENCO Workorder(s): C406310 Dear Jonathan Pfohl, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, May 30, 2014. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, 00, (/ L- - C�- A Chuck Smith Project Manager Enclosure(s) (� �C—o www.encolabs.com The total number of pages in this report, including this page is 13. (� �C_O www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: MW-1 Lab ID: C406310-01 Sampled: 05/28/14 08:05 Received: 05/30/14 11:05 Parameter - - - - - - Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) - - - - - - - - - - - - - - - - - - - - - - - - - - - RSK-175 06/11/14 06/04/14 11:07 6/4/2014 14:16 Client ID: MW-7 Lab ID: C406310-02 Sampled: 05/28/14 12:00 Received: 05/30/14 11:05 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - RSK-175 06/11/14 06/04/14 11:07 6/4/2014 14:33 Client ID: MW-9 w Lab ID: C406310-03RE1 Sampled: 05/28/14 11:35 Received: 05/30/14 11:05 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) RSK-175 06/11/14 06/04/14 11:07 6/4/2014 16:41 Client ID: MW-11 Lab ID: C406330-04RE1 Sampled: 05/28/14 16:45 Received: 05/30/14 11:05 Parameter - - - - - Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) - - - - - - - - - - - - - - - - - - - - - - - - - RSK-175 06/11/14 06/04/14 11:07 6/4/2014 17:13 Client ID: MW-14 Lab ID: C406310-05 Sampled: 05/28/14 10:15 Received: 05/30/14 11:05 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - RSK-175 06/11/14 06/04/14 11:07 6/4/2014 15:21 Client ID: MW-15 Lab ID: C406330-06RE1 Sampled: 05/28/14 09:45M Received: 05/30/14 11:05 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - RSK-175 06/11/14 06/04/14 11:07 6/4/2014 17:29 Client ID: MW-21 Lab ID: C406310-07 Sampled: 05/28/14 13:40 Received: 05/30/14 11:05 Parameter - - - Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) - - - - - - - - - - - - - - - - - - - - - - - - - - RSK-175 06/11/14 06/04/14 11:07 6/4/2014 15:53 Page 2 of 13 (� 0a www.encolabs.com NORTH CAROLINA SWS SAMPLE DETECTION SUMMARY lient ID: MW-7 Lab ID: C406310-02 Analyte Results Flag DF MDL- MRL NC SWSL Units Method Notes - - - - - - Methane - - - - - - - - - - - - - - - - - 0.0935 1 0.000400 - - - - - - - - - - 0.00100 NE - - - - - - - - - - - - - - - mg/L RSK-175 lient ID: MW-9 Lab ID: C406310-03RE1 Analyte Results Flag DF MDL MRL NC SWSL Units Method Notes Methane 1.53 D 21 0.008,10 - - 0.0210 NE - - - - - - - - - - - - - - - - mg/L RSK-175 lient ID: MW-11 Lab ID: C406310-04RE1 Analyte Results Flag DF MDL MRL NC SWSL Units Method Notes Methane 0.164 D 5.25 0.00210 0.00525 NE mg/L RSK-175 lient ID: MW-14 Lab ID: C406310-05 Analyte Results Flag DF MDL MRL NC SWSL Units Method Notes Methane 0.00157 1 0.000400 0.00100 NE mg/L RSK-175 lient ID: MW-15 Lab ID: C406310-06RE1 Analyte Results Flag DF MDL MRL NC SWSL Units Method Notes Methane 0.957 D 21 0.008,10 0.0210 NE mg/L RSK-175 Page 3 of 13 Description: MW-1 Matrix: Ground Water Project: Surry Closed Mt. Airy (UIC) ANALYTICAL RESULTS Lab Sample ID: C406310-01 Sampled: 05/28/14 08:05 Sampled By: Jonathan Pfohl (� 0a www.encolabs.com Received: 05/30/ 14 11:05 Work Order: C406310 Dissolved Gases by GC - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - Analyte [CAS Numberl Results Flaa Units DF MDL MRL NC SWSL Method Analyzed ft Notes Methane [74-82-8] 0.000400 u mg/L 1 0.000400 0.00100 NE RSK-175 06/04/14 14:16 LTS This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 13 Description: MW-7 Matrix: Ground Water Project: Surry Closed Mt. Airy (UIC) Lab Sample ID: C406310-02 Sampled: 05/28/ 14 12:00 Sampled By: Jonathan Pfohl (� 0a www.encolabs.com Received: 05/30/ 14 11:05 Work Order: C406310 Dissolved Gases by GC - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - Analyte rCAS Numberl Results Flaa Units DF MDL MRL NC SWSL Method Analyzed Ay Notes Methane [74-82-8] 0.0935 mg/L 1 0.000400 0.00100 NE RSK-175 06/04/14 14:33 LTS This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 13 Description: MW-9 Matrix: Ground Water Project: Surry Closed Mt. Airy (UIC) Lab Sample ID: C406310-03 Sampled: 05/28/ 14 11:35 Sampled By: Jonathan Pfohl (� 0a www.encolabs.com Received: 05/30/ 14 11:05 Work Order: C406310 Dissolved Gases by GC - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - Analyte rCAS Numberl Results Flaa Units DF MDL MRL NC SWSL Method Analyzed Ay Notes Methane [74-82-8] 1.53 D mg/L 21 0.00840 0.0210 NE RSK-175 06/04/14 16:41 LTS This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 13 (� 0a www.encolabs.com Description: MW-11 Lab Sample ID: C406310-04 Received: 05/30/14 11:05 Matrix: Ground Water Sampled: 05/28/14 16:45 Work Order: C406310 Project: Surry Closed Mt. Airy (UIC) Sampled By: Jonathan Pfohl Dissolved Gases by GC - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - Analvte rCAS Numberl Results Flaa Units DF MDL MRL NC SWSL Method Analyzed By Notes Methane [74-82-8] 0.164 D mg/L 5.25 0.00210 0.00525 NE RSK-175 06/04/14 17:13 LTS This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 13 Description: MW-14 Matrix: Ground Water Project: Surry Closed Mt. Airy (UIC) Lab Sample ID: C406310-05 Sampled: 05/28/ 14 10:15 Sampled By: Jonathan Pfohl (� 0a www.encolabs.com Received: 05/30/ 14 11:05 Work Order: C406310 Dissolved Gases by GC - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - Analyte rCAS Numberl Results Flaa Units DF MDL MRL NC SWSL Method Analyzed Ay Notes Methane [74-82-8] 0.00157 mg/L 1 0.000400 0.00100 NE RSK-175 06/04/14 15:21 LTS This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 13 Description: MW-15 Matrix: Ground Water Project: Surry Closed Mt. Airy (UIC) Lab Sample ID: C406310-06 Sampled: 05/28/14 09:45 Sampled By: Jonathan Pfohl (� 0a www.encolabs.com Received: 05/30/ 14 11:05 Work Order: C406310 Dissolved Gases by GC - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - Analyte rCAS Numberl Results Flaa Units DF MDL MRL NC SWSL Method Analyzed Ay Notes Methane [74-82-8] 0.957 D mg/L 21 0.00840 0.0210 NE RSK-175 06/04/14 17:29 LTS This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 13 Description: MW-21 Matrix: Ground Water Project: Surry Closed Mt. Airy (UIC) Lab Sample ID: C406310-07 Sampled: 05/28/ 14 13:40 Sampled By: Jonathan Pfohl (� 0a www.encolabs.com Received: 05/30/ 14 11:05 Work Order: C406310 Dissolved Gases by GC - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - Analyte rCAS Numberl Results Flaa Units DF MDL MRL NC SWSL Method Analyzed Ay Notes Methane [74-82-81 0.000400 u mg/L 1 0.000400 0.00100 NE RSK-175 06/04/14 15:53 LTS This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 13 QUALITY CONTROL Dissolved Gases by GC - Quality Control Batch 4FO4006 - Same (� �C-O www.encolabs.com Blank (4F04006-BLK3) Prepared: 06/04/2014 11:07 Analyzed: 06/04/2014 12:07 �Analyte %REC RPD Result Flag MRL %REC Limits Limit Notes Methane 0.000400 U 0.00100 mg/L - - - - - - - - - - - - - LCS (4F04006-BS1) - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - Prepared: 06/04/2014 11:07 Analyzed: 06/04/2014 12:23 - - - - - - - - �Analyte Spike Source %RECWL RPD Result Flag MRL Units Level Result %REC Limits imit Notes Methane 509 0.00100 mg/L 500 102 80-120 - - - - - - - - - - - - - LCS Dup (4F04006-BSD1) - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - Prepared: 06/04/2014 11:07 Analyzed: 06/04/2014 12:39 - - - - - - - - �Analyte Spike Source %REC Result Flag MRL Units Level Result %REC Limits RP Methane 536 0.00100 mg/L 500 107 80-120 5 25 Duplicate (4F04006-DUP1) Prepared: 06/04/2014 11:07 Analyzed: 06/04/2014 16:57 Source:C406310-01 �Analyte Spike Source %REC RPD Result Flag MRL Units Level Result %REC Limits RPD Limit Notes Methane 0.000400 U 0.00100 mg/L 0.000400 U 25 Page 11 of 13 (� 0a www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. I The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. Page 12 of 13 1$'q � C Sfr)o -)N LABORIJOROH" (,HA )F- U Y r4 U) w-ormonculabs.-com -NTJ j 1,NVIRONNIF -.CON'FRVATI( I , ", I. !"6i P,,,t -i,3 1I rl- PAI-C oI I ° 4L' I is 0--J�,jo Fl, J.,d, FLM216-61;,49 Page of s. Tow 0 al Containius, I r)%V I Ww-waulo%Qater A All 0 Othui Odt�-: ii r ;6 -40 Naf)H 0 Qlh- (,J-flm, i iflrNl L.91)S 810 11, .11 ll'. lW!''i . ,.S l.n[P.(j !t1' '11.9 ""1 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 June 10, 2014 Mr. Jonathan Pfohl Municipal Engineering Services PO Box 97 Garner, NC 27529 RE: Project: SURRY BLANKS Pace Project No.: 92203466 Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory on May 29, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Godwin kevin.godwin@pacelabs.com Project Manager Enclosures Q _Kok r REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 Project: SURRY BLANKS Pace Project No.: 92203466 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Dr., Asheville, INC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 SAMPLE SUMMARY Project: SURRY BLANKS Pace Project No.: 92203466 Lab ID Sample ID Matrix Date Collected Date Received 92203466001 EB Water 05/29/1414:20 05/29/1415:20 92203466002 FB Water 05/29/1414:30 05/29/1415:20 92203466003 TB Water 05/29/14 00:00 05/29/14 15:20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: SURRY BLANKS 92203466 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92203466001 EB EPA 6010 JMW 16 PASI-A EPA 7470 MTS 1 PASI-A EPA 8260 GAW 51 PASI-C SM 4500-S21D SAE 1 PASI-A SM 4500-CN-E JDA 1 PASI-A 92203466002 FB EPA 6010 JMW 16 PASI-A EPA 7470 MTS 1 PASI-A EPA 8260 GAW 51 PASI-C 92203466003 TB EPA 8260 GAW 51 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY BLANKS Pace Project No.: 92203466 Sample: EB Lab ID: 92203466001 Collected: 05/29/14 14:20 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Tin Vanadium Zinc 7470 Mercury Mercury 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene Date: 06/10/2014 07:52 AM Analytical Method: EPA 6010 Preparation Method: EPA 3010 ND ug/L 6.0 5.0 1 06/03/14 12:30 06/04/14 20:56 7440-36-0 ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:56 7440-38-2 ND ug/L 100 5.0 1 06/03/14 12:30 06/04/14 20:56 7440-39-3 ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:56 7440-41-7 ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:56 7440-43-9 ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:56 7440-47-3 ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:56 7440-48-4 ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:56 7440-50-8 ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:56 7439-92-1 ND ug/L 50.0 5.0 1 06/03/14 12:30 06/04/14 20:56 7440-02-0 ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:56 7782-49-2 ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:56 7440-22-4 ND ug/L 5.5 5.4 1 06/03/14 12:30 06/04/14 20:56 7440-28-0 ND ug/L 100 5.0 1 06/03/14 12:30 06/04/14 20:56 7440-31-5 ND ug/L 25.0 5.0 1 06/03/14 12:30 06/04/14 20:56 7440-62-2 ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:56 7440-66-6 Analytical Method: EPA 7470 Preparation Method: EPA 7470 ND ug/L 0.20 0.10 1 06/02/14 19:45 06/03/14 19:05 7439-97-6 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 06/01/1418:14 67-64-1 ND ug/L 200 1.9 1 06/01/1418:14 107-13-1 ND ug/L 1.0 0.25 1 06/01/1418:14 71-43-2 ND ug/L 3.0 0.17 1 06/01/1418:14 74-97-5 ND ug/L 1.0 0.18 1 06/01/1418:14 75-27-4 ND ug/L 3.0 0.26 1 06/01/1418:14 75-25-2 ND ug/L 10.0 0.29 1 06/01/1418:14 74-83-9 ND ug/L 100 0.96 1 06/01/1418:14 78-93-3 ND ug/L 100 1.2 1 06/01/1418:14 75-15-0 ND ug/L 1.0 0.25 1 06/01/1418:14 56-23-5 ND ug/L 3.0 0.23 1 06/01/1418:14 108-90-7 ND ug/L 10.0 0.54 1 06/01/1418:14 75-00-3 ND ug/L 5.0 0.14 1 06/01/1418:14 67-66-3 ND ug/L 1.0 0.11 1 06/01/1418:14 74-87-3 ND ug/L 13.0 2.5 1 06/01/1418:14 96-12-8 ND ug/L 3.0 0.21 1 06/01/1418:14 124-48-1 ND ug/L 1.0 0.27 1 06/01/1418:14 106-93-4 ND ug/L 10.0 0.21 1 06/01/1418:14 74-95-3 ND ug/L 5.0 0.30 1 06/01/1418:14 95-50-1 ND ug/L 1.0 0.33 1 06/01/1418:14 106-46-7 ND ug/L 100 1.0 1 06/01/1418:14 110-57-6 ND ug/L 5.0 0.32 1 06/01/1418:14 75-34-3 ND ug/L 1.0 0.12 1 06/01/1418:14 107-06-2 ND ug/L 5.0 0.56 1 06/01/1418:14 75-35-4 ND ug/L 5.0 0.19 1 06/01/1418:14 156-59-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY BLANKS Pace Project No.: 92203466 Sample: EB Lab ID: 92203466001 Collected: 05/29/14 14:20 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 4500S2D Sulfide Water Sulfide 450OCNE Cyanide, Total Cyanide Date: 06/10/2014 07:52 AM Analytical Method: EPA 8260 ND ug/L 5.0 0.49 1 06/01/1418:14 156-60-5 ND ug/L 1.0 0.27 1 06/01/1418:14 78-87-5 ND ug/L 1.0 0.28 1 06/01/1418:14 142-28-9 ND ug/L 1.0 0.13 1 06/01/1418:14 10061-01-5 ND ug/L 1.0 0.26 1 06/01/1418:14 10061-02-6 ND ug/L 1.0 0.30 1 06/01/1418:14 100-41-4 ND ug/L 50.0 0.46 1 06/01/1418:14 591-78-6 ND ug/L 10.0 0.32 1 06/01/1418:14 74-88-4 1.0 ug/L 1.0 0.97 1 06/01/14 18:14 75-09-2 ND ug/L 100 0.33 1 06/01/1418:14 108-10-1 ND ug/L 1.0 0.26 1 06/01/1418:14 100-42-5 ND ug/L 5.0 0.33 1 06/01/1418:14 630-20-6 ND ug/L 3.0 0.40 1 06/01/1418:14 79-34-5 ND ug/L 1.0 0.46 1 06/01/1418:14 127-18-4 ND ug/L 1.0 0.26 1 06/01/1418:14 108-88-3 ND ug/L 1.0 0.48 1 06/01/1418:14 71-55-6 ND ug/L 1.0 0.29 1 06/01/1418:14 79-00-5 ND ug/L 1.0 0.47 1 06/01/1418:14 79-01-6 ND ug/L 1.0 0.20 1 06/01/1418:14 75-69-4 ND ug/L 1.0 0.41 1 06/01/1418:14 96-18-4 ND ug/L 50.0 0.35 1 06/01/1418:14 108-05-4 ND ug/L 1.0 0.62 1 06/01/1418:14 75-01-4 ND ug/L 5.0 0.66 1 06/01/1418:14 1330-20-7 100 % 70-130 1 06/01 /14 18:14 460-00-4 102 % 70-130 1 06/01 /14 18:14 17060-07-0 97 % 70-130 1 06/01 /14 18:14 2037-26-5 Analytical Method: SM 4500-S21D ND ug/L 1000 100 1 06/04/14 13:25 18496-25-8 Analytical Method: SM 4500-CN-E ND ug/L 10.0 5.0 1 06/09/14 11:31 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY BLANKS Pace Project No.: 92203466 Sample: FB Lab ID: 92203466002 Collected: 05/29/14 14:30 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 ICP Groundwater Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Tin Vanadium Zinc 7470 Mercury Mercury 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene Date: 06/10/2014 07:52 AM Analytical Method: EPA 6010 Preparation Method: EPA 3010 ND ug/L 6.0 5.0 1 06/03/14 12:30 06/04/14 20:59 7440-36-0 ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:59 7440-38-2 ND ug/L 100 5.0 1 06/03/14 12:30 06/04/14 20:59 7440-39-3 ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:59 7440-41-7 ND ug/L 1.0 1.0 1 06/03/14 12:30 06/04/14 20:59 7440-43-9 ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:59 7440-47-3 ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:59 7440-48-4 ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:59 7440-50-8 ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:59 7439-92-1 ND ug/L 50.0 5.0 1 06/03/14 12:30 06/04/14 20:59 7440-02-0 ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:59 7782-49-2 ND ug/L 10.0 5.0 1 06/03/14 12:30 06/04/14 20:59 7440-22-4 ND ug/L 5.5 5.4 1 06/03/14 12:30 06/04/14 20:59 7440-28-0 ND ug/L 100 5.0 1 06/03/14 12:30 06/04/14 20:59 7440-31-5 ND ug/L 25.0 5.0 1 06/03/14 12:30 06/04/14 20:59 7440-62-2 ND ug/L 10.0 10.0 1 06/03/14 12:30 06/04/14 20:59 7440-66-6 Analytical Method: EPA 7470 Preparation Method: EPA 7470 ND ug/L 0.20 0.10 1 06/02/14 19:45 06/03/14 19:08 7439-97-6 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 06/01/1418:30 67-64-1 ND ug/L 200 1.9 1 06/01/1418:30 107-13-1 ND ug/L 1.0 0.25 1 06/01/1418:30 71-43-2 ND ug/L 3.0 0.17 1 06/01/1418:30 74-97-5 ND ug/L 1.0 0.18 1 06/01/1418:30 75-27-4 ND ug/L 3.0 0.26 1 06/01/1418:30 75-25-2 ND ug/L 10.0 0.29 1 06/01/1418:30 74-83-9 ND ug/L 100 0.96 1 06/01/1418:30 78-93-3 ND ug/L 100 1.2 1 06/01/1418:30 75-15-0 ND ug/L 1.0 0.25 1 06/01/1418:30 56-23-5 ND ug/L 3.0 0.23 1 06/01/1418:30 108-90-7 ND ug/L 10.0 0.54 1 06/01/1418:30 75-00-3 ND ug/L 5.0 0.14 1 06/01/1418:30 67-66-3 ND ug/L 1.0 0.11 1 06/01/1418:30 74-87-3 ND ug/L 13.0 2.5 1 06/01/1418:30 96-12-8 ND ug/L 3.0 0.21 1 06/01/1418:30 124-48-1 ND ug/L 1.0 0.27 1 06/01/1418:30 106-93-4 ND ug/L 10.0 0.21 1 06/01/1418:30 74-95-3 ND ug/L 5.0 0.30 1 06/01/1418:30 95-50-1 ND ug/L 1.0 0.33 1 06/01/1418:30 106-46-7 ND ug/L 100 1.0 1 06/01/1418:30 110-57-6 ND ug/L 5.0 0.32 1 06/01/1418:30 75-34-3 ND ug/L 1.0 0.12 1 06/01/1418:30 107-06-2 ND ug/L 5.0 0.56 1 06/01/1418:30 75-35-4 ND ug/L 5.0 0.19 1 06/01/1418:30 156-59-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 7 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY BLANKS Pace Project No.: 92203466 Sample: FB Lab ID: 92203466002 Collected: 05/29/14 14:30 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 06/10/2014 07:52 AM Analytical Method: EPA 8260 ND ug/L 5.0 0.49 1 06/01/1418:30 156-60-5 ND ug/L 1.0 0.27 1 06/01/1418:30 78-87-5 ND ug/L 1.0 0.28 1 06/01/1418:30 142-28-9 ND ug/L 1.0 0.13 1 06/01/1418:30 10061-01-5 ND ug/L 1.0 0.26 1 06/01/1418:30 10061-02-6 ND ug/L 1.0 0.30 1 06/01/1418:30 100-41-4 ND ug/L 50.0 0.46 1 06/01/1418:30 591-78-6 ND ug/L 10.0 0.32 1 06/01/1418:30 74-88-4 ND ug/L 1.0 0.97 1 06/01/1418:30 75-09-2 ND ug/L 100 0.33 1 06/01/1418:30 108-10-1 ND ug/L 1.0 0.26 1 06/01/1418:30 100-42-5 ND ug/L 5.0 0.33 1 06/01/1418:30 630-20-6 ND ug/L 3.0 0.40 1 06/01/1418:30 79-34-5 ND ug/L 1.0 0.46 1 06/01/1418:30 127-18-4 ND ug/L 1.0 0.26 1 06/01/1418:30 108-88-3 ND ug/L 1.0 0.48 1 06/01/1418:30 71-55-6 ND ug/L 1.0 0.29 1 06/01/1418:30 79-00-5 ND ug/L 1.0 0.47 1 06/01/1418:30 79-01-6 ND ug/L 1.0 0.20 1 06/01/1418:30 75-69-4 ND ug/L 1.0 0.41 1 06/01/1418:30 96-18-4 ND ug/L 50.0 0.35 1 06/01/1418:30 108-05-4 ND ug/L 1.0 0.62 1 06/01/1418:30 75-01-4 ND ug/L 5.0 0.66 1 06/01/1418:30 1330-20-7 100 % 70-130 1 06/01 /14 18:30 460-00-4 100 % 70-130 1 06/01 /14 18:30 17060-07-0 97 % 70-130 1 06/01 /14 18:30 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 8 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY BLANKS Pace Project No.: 92203466 Sample: TB Lab ID: 92203466003 Collected: 05/29/14 00:00 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 06/01/14 18:46 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 06/01/14 18:46 107-13-1 Benzene ND ug/L 1.0 0.25 1 06/01/14 18:46 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 06/01/14 18:46 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 06/01/14 18:46 75-27-4 Bromoform ND ug/L 3.0 0.26 1 06/01/14 18:46 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 06/01/14 18:46 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 06/01/14 18:46 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 06/01/14 18:46 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 06/01/14 18:46 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 06/01/14 18:46 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 06/01/14 18:46 75-00-3 Chloroform ND ug/L 5.0 0.14 1 06/01/14 18:46 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 06/01/14 18:46 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 06/01/14 18:46 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 06/01/14 18:46 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 06/01/14 18:46 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 06/01/14 18:46 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 06/01/14 18:46 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 06/01/14 18:46 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/01/14 18:46 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 06/01/14 18:46 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 06/01/14 18:46 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/01/14 18:46 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 06/01/14 18:46 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/01/14 18:46 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 06/01/14 18:46 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 06/01/14 18:46 142-28-9 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/01/14 18:46 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/01/14 18:46 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/01/14 18:46 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/01/14 18:46 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/01/14 18:46 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/01/14 18:46 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/01/14 18:46 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/01/14 18:46 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/01/14 18:46 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/01/14 18:46 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/01/14 18:46 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/01/14 18:46 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/01/14 18:46 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/01/14 18:46 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/01/14 18:46 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/01/14 18:46 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/01/14 18:46 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/01/14 18:46 108-05-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/10/2014 07:52 AM without the written consent of Pace Analytical Services, Inc.. Page 9 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY BLANKS Pace Project No.: 92203466 Sample: TB Lab ID: 92203466003 Collected: 05/29/14 00:00 Received: 05/29/14 15:20 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Vinyl chloride ND ug/L 1.0 0.62 1 06/01/14 18:46 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/01/14 18:46 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 06/01/14 18:46 460-00-4 1,2-Dichloroethane-d4 (S) 104 % 70-130 1 06/01/14 18:46 17060-07-0 Toluene-d8 (S) 97 % 70-130 1 06/01/14 18:46 2037-26-5 Date: 06/10/2014 07:52 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BLANKS Pace Project No.: 92203466 QC Batch: MERP/6689 Analysis Method: EPA 7470 QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury Associated Lab Samples: 92203466001, 92203466002 METHOD BLANK: 1212169 Matrix: Water Associated Lab Samples: 92203466001, 92203466002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury ug/L ND 0.20 06/03/1418:36 LABORATORY CONTROL SAMPLE: 1212170 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.7 109 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1212171 1212172 MS MSD 92203121010 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Mercury ug/L 0.14J 2.5 2.5 2.7 2.6 101 100 75-125 0 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/10/2014 07:52 AM without the written consent of Pace Analytical Services, Inc.. Page 11 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BLANKS Pace Project No.: 92203466 QC Batch: MPRP/16107 Analysis Method: EPA6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET NC Groundwater Associated Lab Samples: 92203466001, 92203466002 METHOD BLANK: 1212519 Associated Lab Samples: 92203466001, 92203466002 Parameter Units Antimony ug/L Arsenic ug/L Barium ug/L Beryllium ug/L Cadmium ug/L Chromium ug/L Cobalt ug/L Copper ug/L Lead ug/L Nickel ug/L Selenium ug/L Silver ug/L Thallium ug/L Tin ug/L Vanadium ug/L Zinc ug/L Matrix: Water Blank Result Reporting Limit Analyzed ND 6.0 06/04/1419:28 ND 10.0 06/04/1419:28 ND 100 06/04/1419:28 ND 1.0 06/04/1419:28 ND 1.0 06/04/1419:28 ND 10.0 06/04/1419:28 ND 10.0 06/04/1419:28 ND 10.0 06/04/1419:28 ND 10.0 06/04/1419:28 ND 50.0 06/04/1419:28 ND 10.0 06/04/1419:28 ND 10.0 06/04/1419:28 ND 5.5 06/04/1419:28 ND 100 06/04/1419:28 ND 25.0 06/04/1419:28 ND 10.0 06/04/1419:28 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 1212520 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 500 497 99 80-120 Arsenic ug/L 500 477 95 80-120 Barium ug/L 500 502 100 80-120 Beryllium ug/L 500 479 96 80-120 Cadmium ug/L 500 480 96 80-120 Chromium ug/L 500 486 97 80-120 Cobalt ug/L 500 495 99 80-120 Copper ug/L 500 494 99 80-120 Lead ug/L 500 497 99 80-120 Nickel ug/L 500 478 96 80-120 Selenium ug/L 500 495 99 80-120 Silver ug/L 250 242 97 80-120 Thallium ug/L 500 469 94 80-120 Tin ug/L 500 496 99 80-120 Vanadium ug/L 500 480 96 80-120 Zinc ug/L 500 478 96 80-120 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/10/2014 07:52 AM without the written consent of Pace Analytical Services, Inc.. Page 12 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: SURRY BLANKS 92203466 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1212521 1212522 MS MSD 92203332001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 474 483 95 97 75-125 2 25 Arsenic ug/L ND 500 500 456 468 91 94 75-125 3 25 Barium ug/L 22.5J 500 500 490 511 94 98 75-125 4 25 Beryllium ug/L ND 500 500 454 471 91 94 75-125 4 25 Cadmium ug/L ND 500 500 456 467 91 93 75-125 2 25 Chromium ug/L ND 500 500 462 476 92 95 75-125 3 25 Cobalt ug/L ND 500 500 464 480 93 96 75-125 3 25 Copper ug/L ND 500 500 475 480 95 96 75-125 1 25 Lead ug/L ND 500 500 465 478 93 96 75-125 3 25 Nickel ug/L ND 500 500 453 467 91 93 75-125 3 25 Selenium ug/L ND 500 500 467 479 93 96 75-125 2 25 Silver ug/L ND 250 250 229 235 91 94 75-125 3 25 Thallium ug/L ND 500 500 446 459 89 92 75-125 3 25 Tin ug/L ND 500 500 468 481 93 96 75-125 3 25 Vanadium ug/L ND 500 500 457 472 91 94 75-125 3 25 Zinc ug/L ND 500 500 457 467 91 93 75-125 2 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/10/2014 07:52 AM without the written consent of Pace Analytical Services, Inc.. Page 13 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BLANKS Pace Project No.: 92203466 QC Batch: MSV/27045 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92203466001, 92203466002, 92203466003 METHOD BLANK: 1211358 Matrix: Associated Lab Samples: 92203466001, 92203466002, 92203466003 Blank Parameter Units Result Water Reporting Limit Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/01/14 13:23 1,1,1-Trichloroethane ug/L ND 1.0 06/01/14 13:23 1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/01/14 13:23 1,1,2-Trichloroethane ug/L ND 1.0 06/01/14 13:23 1,1-Dichloroethane ug/L ND 5.0 06/01/14 13:23 1,1-Dichloroethene ug/L ND 5.0 06/01/14 13:23 1,2,3-Trichloropropane ug/L ND 1.0 06/01/14 13:23 1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/01/14 13:23 1,2-Dibromoethane (EDB) ug/L ND 1.0 06/01/14 13:23 1,2-Dichlorobenzene ug/L ND 5.0 06/01/14 13:23 1,2-Dichloroethane ug/L ND 1.0 06/01/14 13:23 1,2-Dichloropropane ug/L ND 1.0 06/01/14 13:23 1,3-Dichloropropane ug/L ND 1.0 06/01/14 13:23 1,4-Dichlorobenzene ug/L ND 1.0 06/01/14 13:23 2-Butanone (MEK) ug/L ND 100 06/01/14 13:23 2-Hexanone ug/L ND 50.0 06/01/14 13:23 4-Methyl-2-pentanone (MIBK) ug/L ND 100 06/01/14 13:23 Acetone ug/L ND 100 06/01/14 13:23 Acrylonitrile ug/L ND 200 06/01/14 13:23 Benzene ug/L ND 1.0 06/01/14 13:23 Bromochloromethane ug/L ND 3.0 06/01/14 13:23 Bromodichloromethane ug/L ND 1.0 06/01/14 13:23 Bromoform ug/L ND 3.0 06/01/14 13:23 Bromomethane ug/L ND 10.0 06/01/14 13:23 Carbon disulfide ug/L ND 100 06/01/14 13:23 Carbon tetrachloride ug/L ND 1.0 06/01/14 13:23 Chlorobenzene ug/L ND 3.0 06/01/14 13:23 Chloroethane ug/L ND 10.0 06/01/14 13:23 Chloroform ug/L ND 5.0 06/01/14 13:23 Chloromethane ug/L ND 1.0 06/01/14 13:23 cis-1,2-Dichloroethene ug/L ND 5.0 06/01/14 13:23 cis-1,3-Dichloropropene ug/L ND 1.0 06/01/14 13:23 Dibromochloromethane ug/L ND 3.0 06/01/14 13:23 Dibromomethane ug/L ND 10.0 06/01/14 13:23 Ethylbenzene ug/L ND 1.0 06/01/14 13:23 lodomethane ug/L ND 10.0 06/01/14 13:23 Methylene Chloride ug/L ND 1.0 06/01/14 13:23 Styrene ug/L ND 1.0 06/01/14 13:23 Tetrachloroethene ug/L ND 1.0 06/01/14 13:23 Toluene ug/L ND 1.0 06/01/14 13:23 trans-1,2-Dichloroethene ug/L ND 5.0 06/01/14 13:23 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/10/2014 07:52 AM without the written consent of Pace Analytical Services, Inc.. Page 14 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BLANKS Pace Project No.: 92203466 METHOD BLANK: 1211358 Matrix: Associated Lab Samples: 92203466001, 92203466002, 92203466003 Blank Parameter Units Result Water Reporting Limit Analyzed trans- 1,3-Dichloropropene ug/L ND 1.0 06/01/14 13:23 trans-1,4-Dichloro-2-butene ug/L ND 100 06/01/14 13:23 Trichloroethene ug/L ND 1.0 06/01/14 13:23 Trichlorofluoromethane ug/L ND 1.0 06/01/14 13:23 Vinyl acetate ug/L ND 50.0 06/01/14 13:23 Vinyl chloride ug/L ND 1.0 06/01/14 13:23 Xylene (Total) ug/L ND 5.0 06/01/14 13:23 1,2-Dichloroethane-d4 (S) % 99 70-130 06/01/14 13:23 4-Bromofluorobenzene (S) % 101 70-130 06/01/14 13:23 Toluene-d8 (S) % 96 70-130 06/01/14 13:23 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 1211359 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 59.3 119 70-130 1,1,1-Trichloroethane ug/L 50 53.5 107 70-130 1,1,2,2-Tetrachloroethane ug/L 50 53.7 107 70-130 1,1,2-Trichloroethane ug/L 50 54.3 109 70-130 1,1-Dichloroethane ug/L 50 49.4 99 70-130 1,1-Dichloroethene ug/L 50 49.4 99 70-132 1,2,3-Trichloropropane ug/L 50 53.2 106 70-130 1,2-Dibromo-3-chloropropane ug/L 50 48.4 97 70-130 1,2-Dibromoethane (EDB) ug/L 50 54.6 109 70-130 1,2-Dichlorobenzene ug/L 50 53.6 107 70-130 1,2-Dichloroethane ug/L 50 54.8 110 70-130 1,2-Dichloropropane ug/L 50 51.7 103 70-130 1,3-Dichloropropane ug/L 50 53.0 106 70-130 1,4-Dichlorobenzene ug/L 50 52.6 105 70-130 2-Butanone (MEK) ug/L 100 89.3J 89 70-145 2-Hexanone ug/L 100 99.7 100 70-144 4-Methyl-2-pentanone (MIBK) ug/L 100 99.1J 99 70-140 Acetone ug/L 100 95.5J 96 50-175 Acrylonitrile ug/L 250 250 100 70-143 Benzene ug/L 50 55.1 110 70-130 Bromochloromethane ug/L 50 54.4 109 70-130 Bromodichloromethane ug/L 50 56.4 113 70-130 Bromoform ug/L 50 53.1 106 70-130 Bromomethane ug/L 50 54.2 108 54-130 Carbon disulfide ug/L 50 50.9J 102 70-131 Carbon tetrachloride ug/L 50 56.9 114 70-132 Chlorobenzene ug/L 50 51.4 103 70-130 Chloroethane ug/L 50 40.9 82 64-134 Chloroform ug/L 50 52.3 105 70-130 Chloromethane ug/L 50 48.6 97 64-130 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/10/2014 07:52 AM without the written consent of Pace Analytical Services, Inc.. Page 15 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BLANKS Pace Project No.: 92203466 LABORATORY CONTROL SAMPLE: Parameter 1211359 Units Spike Conc. LCS Result LCS % Rec % Rec Limits cis-1,2-Dichloroethene ug/L 50 49.9 100 70-131 cis-1,3-Dichloropropene ug/L 50 55.6 111 70-130 Dibromochloromethane ug/L 50 51.3 103 70-130 Dibromomethane ug/L 50 54.4 109 70-131 Ethylbenzene ug/L 50 50.0 100 70-130 lodomethane ug/L 100 120 120 49-180 Methylene Chloride ug/L 50 52.4 105 63-130 Styrene ug/L 50 54.1 108 70-130 Tetrachloroethene ug/L 50 54.7 109 70-130 Toluene ug/L 50 51.6 103 70-130 trans-1,2-Dichloroethene ug/L 50 50.5 101 70-130 trans- 1,3-Dichloropropene ug/L 50 55.4 111 70-132 trans-1,4-Dichloro-2-butene ug/L 50 56.7J 113 70-141 Trichloroethene ug/L 50 56.8 114 70-130 Trichlorofluoromethane ug/L 50 48.2 96 62-133 Vinyl acetate ug/L 100 108 108 66-157 Vinyl chloride ug/L 50 57.1 114 69-130 Xylene (Total) ug/L 150 152 102 70-130 1,2-Dichloroethane-d4 (S) % 99 70-130 4-Bromofluorobenzene (S) % 102 70-130 Toluene-d8 (S) % 100 70-130 MATRIX SPIKE SAMPLE: 1211566 Qualifiers 92203468011 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 50 66.7 133 70-130 MO 1,1,1-Trichloroethane ug/L ND 50 64.7 129 70-130 1,1,2,2-Tetrachloroethane ug/L ND 50 59.2 118 70-130 1,1,2-Trichloroethane ug/L ND 50 61.2 122 70-130 1,1-Dichloroethane ug/L ND 50 58.7 117 70-130 1,1-Dichloroethene ug/L ND 50 61.3 123 70-166 1,2,3-Trichloropropane ug/L ND 50 58.9 118 70-130 1,2-Dibromo-3-chloropropane ug/L ND 50 49.3 99 70-130 1,2-Dibromoethane (EDB) ug/L ND 50 59.9 120 70-130 1,2-Dichlorobenzene ug/L ND 50 59.6 119 70-130 1,2-Dichloroethane ug/L ND 50 64.0 128 70-130 1,2-Dichloropropane ug/L ND 50 59.5 119 70-130 1,3-Dichloropropane ug/L ND 50 57.8 116 70-130 1,4-Dichlorobenzene ug/L ND 50 59.5 119 70-130 2-Butanone (MEK) ug/L ND 100 98.5J 99 70-130 2-Hexanone ug/L ND 100 110 110 70-130 4-Methyl-2-pentanone (MIBK) ug/L ND 100 109 109 70-130 Acetone ug/L ND 100 105 103 70-130 Acrylonitrile ug/L ND 250 284 114 70-130 Benzene ug/L ND 50 64.8 130 70-148 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/10/2014 07:52 AM without the written consent of Pace Analytical Services, Inc.. Page 16 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BLANKS Pace Project No.: 92203466 MATRIX SPIKE SAMPLE: Parameter 1211566 Units 92203468011 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers Bromochloromethane ug/L ND 50 62.5 125 70-130 Bromodichloromethane ug/L ND 50 64.4 129 70-130 Bromoform ug/L ND 50 55.8 112 70-130 Bromomethane ug/L ND 50 65.5 131 70-130 MO Carbon disulfide ug/L ND 50 60.5J 121 70-130 Carbon tetrachloride ug/L ND 50 69.6 139 70-130 MO Chlorobenzene ug/L ND 50 58.2 116 70-146 Chloroethane ug/L ND 50 44.4 89 70-130 Chloroform ug/L ND 50 61.3 123 70-130 Chloromethane ug/L ND 50 58.1 116 70-130 cis-1,2-Dichloroethene ug/L ND 50 59.7 119 70-130 cis-1,3-Dichloropropene ug/L ND 50 61.9 124 70-130 Dibromochloromethane ug/L ND 50 56.0 112 70-130 Dibromomethane ug/L ND 50 61.5 123 70-130 Ethylbenzene ug/L ND 50 57.0 114 70-130 lodomethane ug/L ND 100 149 149 70-130 MO Methylene Chloride ug/L ND 50 61.4 123 70-130 Styrene ug/L ND 50 61.3 123 70-130 Tetrachloroethene ug/L ND 50 63.5 127 70-130 Toluene ug/L ND 50 60.3 121 70-155 trans-1,2-Dichloroethene ug/L ND 50 61.4 123 70-130 trans- 1,3-Dichloropropene ug/L ND 50 61.9 124 70-130 trans-1,4-Dichloro-2-butene ug/L ND 50 61.8J 124 70-130 Trichloroethene ug/L ND 50 66.5 133 69-151 Trichlorofluoromethane ug/L ND 50 63.1 126 70-130 Vinyl acetate ug/L ND 100 121 121 70-130 Vinyl chloride ug/L ND 50 71.7 143 70-130 MO 1,2-Dichloroethane-d4 (S) % 100 70-130 4-Bromofluorobenzene (S) % 102 70-130 Toluene-d8 (S) % 100 70-130 SAMPLE DUPLICATE: 1211567 Parameter Units 92203468012 Result Dup Result RPD 1,1,1,2-Tetrachloroethane ug/L ND ND 1,1,1-Trichloroethane ug/L ND ND 1,1,2,2-Tetrachloroethane ug/L ND ND 1,1,2-Trichloroethane ug/L ND ND 1,1-Dichloroethane ug/L ND ND 1,1-Dichloroethene ug/L ND ND 1,2,3-Trichloropropane ug/L ND ND 1,2-Dibromo-3-chloropropane ug/L ND ND 1,2-Dibromoethane (EDB) ug/L ND ND 1,2-Dichlorobenzene ug/L ND ND 1,2-Dichloroethane ug/L ND ND Max RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/10/2014 07:52 AM without the written consent of Pace Analytical Services, Inc.. Page 17 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BLANKS Pace Project No.: 92203466 SAMPLE DUPLICATE: 1211567 Parameter Units 92203468012 Result 1,2-Dichloropropane ug/L ND 1,3-Dichloropropane ug/L ND 1,4-Dichlorobenzene ug/L ND 2-Butanone (MEK) ug/L ND 2-Hexanone ug/L ND 4-Methyl-2-pentanone (MIBK) ug/L ND Acetone ug/L ND Acrylonitrile ug/L ND Benzene ug/L ND Bromochloromethane ug/L ND Bromodichloromethane ug/L ND Bromoform ug/L ND Bromomethane ug/L ND Carbon disulfide ug/L ND Carbon tetrachloride ug/L ND Chlorobenzene ug/L ND Chloroethane ug/L ND Chloroform ug/L ND Chloromethane ug/L ND cis-1,2-Dichloroethene ug/L ND cis-1,3-Dichloropropene ug/L ND Dibromochloromethane ug/L ND Dibromomethane ug/L ND Ethylbenzene ug/L ND lodomethane ug/L ND Methylene Chloride ug/L ND Styrene ug/L ND Tetrachloroethene ug/L ND Toluene ug/L ND trans-1,2-Dichloroethene ug/L ND trans- 1,3-Dichloropropene ug/L ND trans-1,4-Dichloro-2-butene ug/L ND Trichloroethene ug/L ND Trichlorofluoromethane ug/L ND Vinyl acetate ug/L ND Vinyl chloride ug/L ND Xylene (Total) ug/L ND 1,2-Dichloroethane-d4 (S) % 103 4-Bromofluorobenzene (S) % 99 Toluene-d8 (S) % 96 Dup Result RPD ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 102 100 96 I Max RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/10/2014 07:52 AM without the written consent of Pace Analytical Services, Inc.. Page 18 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BLANKS Pace Project No.: 92203466 QC Batch: WET/31341 Analysis Method: SM 4500-S2D QC Batch Method: SM 4500-S2D Analysis Description: 4500S2D Sulfide Water Associated Lab Samples: 92203466001 METHOD BLANK: 1213017 Matrix: Water Associated Lab Samples: 92203466001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfide ug/L ND 1000 06/04/1413:25 LABORATORY CONTROL SAMPLE: 1213018 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 516J 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1213019 1213020 MS MSD 92203023014 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 499J 499J 100 100 75-125 0 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/10/2014 07:52 AM without the written consent of Pace Analytical Services, Inc.. Page 19 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BLANKS Pace Project No.: 92203466 QC Batch: WETA/19245 Analysis Method: SM 4500-CN-E QC Batch Method: SM 4500-CN-E Analysis Description: 450OCNE Cyanide, Total Associated Lab Samples: 92203466001 METHOD BLANK: 1216419 Matrix: Water Associated Lab Samples: 92203466001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cyanide ug/L ND 10.0 06/09/1411:27 LABORATORY CONTROL SAMPLE: 1216420 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 93.4 93 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1216421 1216422 MS MSD 92203385006 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 94.1 92.6 92 90 75-125 2 20 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1216423 1216424 MS MSD 92204279003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 90.7 89.8 89 88 75-125 1 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/10/2014 07:52 AM without the written consent of Pace Analytical Services, Inc.. Page 20 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALIFIERS Project: SURRY BLANKS Pace Project No.: 92203466 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference INC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/10/2014 07:52 AM without the written consent of Pace Analytical Services, Inc.. Page 21 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: SURRY BLANKS Pace Project No.: 92203466 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92203466001 EB EPA3010 MPRP/16107 EPA6010 ICP/14568 92203466002 FB EPA 3010 MPRP/16107 EPA 6010 ICP/14568 92203466001 EB EPA 7470 MERP/6689 EPA 7470 MERC/6449 92203466002 FB EPA 7470 MERP/6689 EPA 7470 MERC/6449 92203466001 EB EPA 8260 MSV/27045 92203466002 FB EPA 8260 MSV/27045 92203466003 TB EPA 8260 MSV/27045 92203466001 EB SM 4500-S2D WET/31341 92203466001 EB SM 4500-CN-E WETA/19245 Date: 06/10/2014 07:52 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 22 of 24 Document Name: Document Revised: April 0 (. 2014 yr26M,71�11hil' Sample Condition Upon Receipt (SCUR) Page 1 of 2 Document Number: Issuing Authority: F-CHR-CS-003-rev.14 Pace Huntersville Quality Office Client Name: 1 Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Client❑ mmerciaX Pace Other a tfonal CustodySeal on Cooler/Sox Present: ❑ yes no Seals intact: ❑ yes ❑ no Pro). Due Date: I-r I' Packing Material: ❑ Bubble WrapBubble Bags ❑ None ❑ Other Thermometer Used: IR Gun T1102 & Type of Ice: (,Q— Blue None ASamples on ice, cooling process has begun Temn Correction Factor T1102: No Correction T1301: No C:nrrertion Corrected Cooler Temp.:_ ���] °C Biological Tissue is Frozen: Yes No Date and Initi s of person examining NIA g contents: Temp should be above freezing to 6'C Comments: Chain of Custody Present: '41 LINO ❑NIA 1. Chain of Custody Filled Out: Y s LINO ❑NIA 2. Chain of Custody Relinquished: Xs LINO ❑NIA 3. Sampler Name & Signature on COC: Y s ONO ❑NIA 4. Samples Arrived within Hold Time: 16es ❑No ❑NIA 5, Short Hold Time Analysis ([72hr): ❑Yes No ❑NIA 6, Rush Turn Around Time Requested: ❑Yes N❑ ❑NIA 7, Sufficient Volume: Yes ❑N❑ ❑NIA g. Correct Containers Used: 1--]No ONrA 9. -Pace Containers Used: WY s ONO ❑NIA Containers Intact: Yes ONO ON/A 10. Filtered volume received for Dissolved tests ❑Yes LINO IA 11. Sample Labels match COC: PYls LINO ❑NIA 12, -Includes date/time/ID/Analysis Matrix: All containers needing preservation have been checked. Yes ❑ No ❑NIA 13. All containers needing preservation are found to be in compliance with EPA recommendation. es SI7�tr�+A exceptions: VOA, coliform, TOC, O&G, WI-aRO (water) Yes ❑No Samples checked for dechlorination: C7Yes ❑No /IA 14, Headspace in VOA Vials (>6mm): ❑Yes N❑ ❑NIA 15. Trip Blank Present: ❑Yes ❑N❑ XiA 16. Trip Blank Custody Seals Present 0Yes EINo NIA Pace Trip Blank Lot # if p urchased): Client Notifications Resolution: Person Contacted - Comments/ Resolution: Date/Time: SCURF Review:l Data: SRF Review: Date: 3d Note: Whenever there i discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers) Field Data Required? Y 1 N WO#:92203466 92203466 Page 23 of 24 c-� r . ceAIt246cai CHAIN -OF -CUSTODY I Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section 8 Section C Required Client Information: Required Project Information: Invoice Information: Page : 7 Of S Company: Municipal Engineering Services Report To: Jonathan Pfohl Attention: Municipal Engineering Services Address: P.D. Sox 97 Copy To. Company Name: Gamer, NC 27529 Address: Regulatory Agency Ernail To: jpfohlgmesco.com Purchase Order No Pace Quote Reference: Phone: 919-772-5393 IF= Client Project ID: Slurry Blanks Pace Project Manager- Kevin Godwin State I Location Requested Due Da[e1TAT: 10 Day [Default] Container Order Number: Pace Profile p: North Carolina Requested Analysis Filtered [YIN] _ COLLECTED Preservatives N N N N MATRIX CODE Drinking Water Dw _ [,] Water W r 3 SAMPLE I❑ wane w.Ier ww 'a m w 1 5 �,;Q 5 Ix START EN❑ 0- On a Character per box. Oil1. w,Pr, w �? Sample ids must be unique Qmw OT 7+ Rq p Ti... T$ W F Z M C @ C 4 F X ¢ J V dbi a V co O p Q ,y,! t L Q n N n PROVIIDE 2 LITERS OF Di DATE TIME DATE TIME a= r i 2 a O y WATER 1 ES WT C+ i4 3 3 f 3 2 f 7 x x x x x x x FS WT G v a'30 QLA 3 3 TS VIlr G �iri f ^' P 4 5 7 8 9 10 11 12 ADDITIONAL COMMENTS LINO UISHED BY I AFFILIATION DATE TIME ACCEPTED BYIAFFILIATION DATE TIME SAMPLE CONDITIONS SAMPLER NAME AND SIGNATURE m PRI NIT Nartle C] � Z C Of SAMPLER: J nath P hl SIGNATURE or SAMPLER: DATE Signed: � u } m E z LU w Appendix B Field Sampling Parameter Data Sheet(s) Sampling Data Sheet Project: Surry Co Closed C&D over Closed MSWLF-Mt. Airy Samplers: J. Pfohl PageL._l____pf 1 Sampling Parameters Water Quality Parameters Depth to Water (BTOP) Static Lab Parameters to be analyzed for Volume Purged (Gal) Sample Type Goes Dry Durirfg Purge Total Depth Measured as expected Total Depth Expected CO2 (mg/1) DO (mg/L) ORP pH Temp. @ Specific Cond. (US/cm TD,13 (mg/L:) CH4 Gas Vapor s (ppm) Monitoring Point Sample Date Sample Time MW-1 39M 40 IL �01 Cq,o3 IW-3 NS 36,15 52 100 MW-3R NS IW-4 33,9 57 71iDo0V NS IW-5 MW-6 5 10, ------ ---64 31 L, L JLLD <,F MW-7 IW-6 NS 56 M46 W MW-1 1 ;9�' 3 A) 40 MW-12S�14N_11 —Ju 31137 MW-12D Y 100 L 2 U-, MW-13 J a 31 N 48.03 ir V 56.98 A,q7 . MW-1 6 to -__Y36.28 s -LL. —A-11-L.- --C— L MW-17 E 15-32 ] - - __ i I � J_._ 18.15 MW-18 RP 1-3 1-9 5T- 6 11 30 MW-19 15 3 q "Et 17.1 Nq ID L A MW-20 25.64 4)' 15.41 IL u-T 10 5T] 16.04 �-22 J -4 /V-23 17.1 �11 09 E4 -7 �J qHOUSE 222 ,tainless Steel Baler, D B=Disposable Baler, P=Lo'W flow Pump, PD=Purged Dry' 1? -4- -y Turbid, MT=Modera*tely Turbid, ST=Slightly Turbid, C=Clear Reading Attempted, NS=No Sample Obtained I Sampling Data Sheet Project: Wq _1__of 1 Lf --M4. Ai / 7 SLMd �Ujfoce 44�5) Samplers: J. Pfohl Page. Monitoring Point Sample Date Sample 'Time Sampling Parameters Water Quality Parameters wt 0 Lab Parameters to be analyzed for V. I Sample Type t I M p d C el 'T t I a A& QRP pH Temp. @ Specific Cond. (us/cm TDS (mg/L) -z2, CH4 Gas Vapor (ppsm) SW--1 ll *as T, 4A ox� d-69 C- 7 7 71 z-z —1 1 - f) 4U, ex-2 "o LJ C ---L- 5—W --Li vat U�A I L"ul) 5-VA - ---------- SS B=Stainless Steel Baler, D B=Disposable Baler, P=Low flow Pump, PD=Purged Dry VT=Very Turbid, MT=Moderately Turbid, ST=Slightly Turbid, C=Clear NR=No Reading Attempted, NS=No Sample Obtained