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Home My WebLink AboutWI0400176_W/ CORRECTIVE ACTION UPDATE_20171031pENk USE oNLY: 'I (❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event #: NC DENR I I Environmental Monitoring Division of Waste Management - Solid Waste Reporting Form Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6). Instructions: Prepare one form for each individually monitored unit. Please type or print legibly. Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing condition, etc.). Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i). Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646. Solid Waste Monitorina'Data Submittal Information Name of entity submitting data (laboratory, consultant, facility owner): Municipal Engineering Services Co., PA Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: Jonathan Pfohl E-mail: jpfohl@mesco.com Phone: (919)772-5393 NC Landfill Rule: Actual sampling dates (e.g., Facility name: Facility Address: Facility Permit # (.0500 or. 1600) October 20-24, 2006) Surry County Closed C&D and 237 Landfill Road Closed MSW Landfill -Mt. Airy Mt. Airy, NC 27030 86 02 .1600 May 31 June 1, 2017 Environmental Status: (Check all that apply) ❑ Initial/Background Monitoring X❑ Detection Monitoring OX Assessment Monitoring ❑X Corrective Action of data submitted: (Check all that apply) Groundwater monitoring data from monitoring wells Groundwater monitoring data from private water supply wells ❑X Leachate monitoring data El water monitoring data Methane gas monitoring data Corrective action data (specify) MNA parameters on 7 wells Other(specify) Notification attached? No. No groundwater or surface water standards were exceeded. X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. Certification To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Steven R. Gandy, Ph.D., P.E. Senior Project Manager (919) 772-5393 Facility Representative Name (Print) ,� Title (Area Code) Telephone Number 7; P.O. BOX 97, Garner, NC 27529 Facility Representative Address C-0281 NC PE Firm License Number (if applicable effective May 1, 2009) Revised 6/2009 Affix NC Licensed/ I pfbI;kCr4dirpgI gist Seal f�0 ®®®� 7 / ® 91020 ® .a ® (j' �,A '�®i�alto4ee�� ,t ( Semi -Annual Water Quality Monitoring Report with Corrective Action Update Prepared for Surry County Closed C&D and Closed MSWLF, Mt. Airy Mt. Airy, North Carolina May 2017 Permit Number: 86-02 MESCO Project Number: G17024.0 Municipal Engineering Services f Compasry, PA. Garner; NC 1 Boone, NC P.O. Box 97 Municipal Engineering Services Company, P.A Gamer, NC 27529 Gamer and Boone, North Carolina License No. C-0281 TABLE OF CONTENTS SECTION Introduction ........................................ Background........................................... Sampling Procedures............ Field Parameter Data Laboratory Results .................... Quality Control Samples Groundwater Samples......... Surface Water Samples..... Corrective Action Undati 1 2 2 2 3 3 4 5 5 MNA Analysis (AOCs Northern, Southern and MW-11)...................................................................................................................................................................................Page 5 Enhanced Bioremediation via Substrate Injection (AOC Southern and Northern)....................................................................................................Page 5 MW-I I AOC Investigations................................................................................................................................................................................................................................................................................Page 6 Groundwaterand Surface Water Characterization..........................................................................................................................................................................................................Page 7 Findings..................................................................................................................................................................................................................................................................................................................................................Page 7 Closing....................................................................................................................................................................................................................................................................................................................................................Page 8 Topographic Map with Site Location................................................................. Single Event Potentiometric Map of Uppermost Aquifer FIGURES 1 2 Total Cumulative VOC Concentrations Pre/Post Injection Comparison........................................................................................................................._Figure 1 Total Cumulative VOC Concentrations Time Series Graphs/Table........................................................................................................................................_Figure 2 TABLES Groundwater Monitoring Well Construction Table....................................................................................................................................................................................................Table 1 FieldObservations of Monitoring Locations.........................................................................................................................................................................................................................Table 2 FieldParameter Data Summary ................................................................................................................................................................................................................................................................. Table 3 Samplingand Analysis Summary ............................................................................................................................................................................................................................................................Table 4 Groundwaterand QC Sample Detections..................................................................................................................................................................................................................................Table 5 SurfaceWater Sample Detections............................................................................................................................................................................................................................................................Table 6 MNAParameter Data Summary .................................................................................................................................................................................................................................................................Table 7 Hydrologic Properties at Monitoring Well Locations.............................................................................................................................................................................................Table 8 APPENDICIES Laboratory Analysis Report and Chains of Custody................................................................................................................................................................................_Appendix A FieldSampling Parameter Data Sheet(s).......................................................................................................................................................................................................................Appendix B License No. C-0281 CIVILISANITARYIENVIRONMENTAL ENGINEERS Municipal Services SITE PLANNING ISUBDIVISIONS SOLID WASTE MANAGEMENT Engineering Company, P.A. SUBSURFACE UTILITY ENGINEERING (SUE) October 31, 2017 Ms. Jaclynne Drummond Solid Waste Section (SWS) 2090 US 70 Highway Swannanoa, NC 28778 Re: Semi -Annual Water Quality Monitoring Report with Corrective Action Update Surry County Closed C&D and Closed MSWLF, Mount Airy Permit No. 86-02 MESCO Project No. G17025.0 Event Date(s): May 31-June 1, 2017 Dear Ms. Drummond: Introduction On behalf of Surry County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this Semi - Annual Water Quality Report with Corrective Action Update for the spring 2017 event performed at the Surry County closed construction and demolition (C&D) and closed municipal solid waste landfill (MSWLF)-Mount Airy. NCDENR Solid Waste Rules 15A NCAC 1313.1632 requires that Surry County provide this report to the NC Solid Waste Section (SWS) on a semi-annual basis. This report documents the quality of the ground and surface waters during this monitoring event performed on May 31-June 1, 2017. Laboratory analytical results, which included targeting Appendix II constituents, indicate volatile organic compounds (VOCs) in concentrations in excess of SWSL and 2L Standards continue to persist in samples collected from three wells that monitor the uppermost aquifer. The surface water samples collected from the local discharge feature remain unimpacted. Corrective action to remediate VOCs in groundwater is ongoing within all three areas of concern (AOC) as defined in the Corrective Action Plan (CAP) and improvement has been observed with updated information presented herein. PO Box 97, Garner, North Carolina 27529 (919) 772-5393 PO Box 349, Boone, NC 28607 (828) 262-1767 Background The Surry County closed C&D and MSWLF, permit #86-02, is located at 237 Landfill Road in Mt. Airy North Carolina. The site location topographic map is depicted in the attached Sheet 1. Prior to becoming a C&D landfill the site operated as a MSW unlined sanitary landfill that consisted of two units. The northern unit was closed prior to October 1991. The southern unit is comprised of two contiguous portions. The first part stopped receiving waste prior to October 1991 and the second part stopped receiving waste prior to January 1, 1999. Both portions of the southern unit were properly closed with a low permeability cohesive cap per the Transition Plan. The top portion of the southern unit served as an exclusive C&D landfill until prior to June 1, 2008 at which time it was properly closed with another cohesive cap in accordance with the Closure Plan. For continuity, both the northern and the southern units are monitored and reported together. Water quality at this facility has been monitored at least semi-annually since 1989 with historical data available since 1994. This event was performed in accordance with the NC SWS rules/regulations as promulgated in 15A NCAC 13B and as a condition of the post -closure portion of the permit to operate and memorandums this report contains sampling procedures, field and laboratory results, groundwater and surface water characterization, and findings. This report also contains a table of detections compared to Standards, field data results table, groundwater flow directions/rates table, field observations of the monitoring network table, a potentiometric map of the uppermost aquifer, histograms of historical detections, statistical trend analysis, laboratory analytical reports with chains -of - custody (C-O-C) and quality assurance/quality control data. Sampling Procedures The water quality monitoring program, current as of this event date, includes sampling locations and parameters as outlined in the Water Quality Sampling and Analysis Plan (SAP) (DIN:18936) dated April 30, 2013 and approved by the SWS (DIN: 18938) on May 10, 2013. Monitoring locations are shown on the enclosed potentiometric map (Sheet 2). MESCO personnel collected water samples from 20 downgradient groundwater monitoring wells (MW- 3R, MW-4, MW-6 through MW-11, MW-125, MW-12D, MW-13 through MW-23), one background well (MW-1), four surface water locations (SW-1, SW-2, SW-3 and SW-4), and the water supply well (SCALEHOUSE) that serves the facility. Data from two surface water points (SWN-1 and SWN-2) designated in the SAP for the adjacent Subtitle D Lined MSWLF are presented because this local discharge feature is shared by both permits. Quality control measures implemented during this event included the quantification of potential artifact contaminants via equipment (EB), field (FB) and travel (TB) blanks. Samples were not analyzed from the six injection wells (IW-1), (IW-2/MW- 2), (IW-3/MW-3RS), (IW-4/MW-4), (IW-5/MW-5) and (IW-6/MW-8) since they are exempt due to the presence of injectant residue which would yield unrepresentative water quality results. 2 A summary of the construction of the water monitoring wells is presented on Table 1. The function and integrity of all monitoring locations were visually evaluated as documented on Table 2. The depth to water in each well was electronically gaged prior to purging to quantify the static water level elevation. Low -flow pumping methodology or bailing was utilized to adequately purge the wells to a minimum of three times the volume of standing water in the well or until dry. Surface water samples were collected from Stoney Creek discharge feature at previously designated locations. During well purging and surface water sample collection the required field parameters were recorded. The samples were then placed into laboratory -prepared, pre -preserved containers via a new disposable polyethylene bailer. Samples were collected, kept on ice, and transported to a NC -certified laboratory under proper C-O-C protocols within the specified hold times for each analysis. Field Parameter Data Stabilized field parameters were recorded during purging which included depth to water, pH, dissolved oxygen (DO), temperature, oxidation reduction potential (ORP), specific conductance and turbidity. The field parameter data indicates the monitored groundwater is slightly acidic, reducing conditions, with relatively low specific conductance which is generally consistent relative to each other and congruent with data historically reported. Field parameter data recorded at the surface water locations were neutral in regard to pH and low specific conductance which is consistent with uncontaminated water. A summary of the field parameter data is presented in Table 3 and the field sampling data sheet is enclosed in Appendix B. Laboratory Results Pace Analytical Laboratory (PACE) of Huntersville and Asheville, NC performed the laboratory analysis of groundwater and surface water samples for the total recoverable constituents listed in 40 CFR Appendix I and II. Pace also analyzed samples collected from seven wells for monitored natural attenuation (MNA) parameters. A sampling and analysis table summarizing the locations, constituents, and methods is presented on Table 4. Laboratory results and C-O-Cs are contained in Appendix A. Water samples were analyzed to the laboratory -established Method Detection Limits (MDL), which are at or below the current Solid Waste Section Limit (SWSL). Table 5 summarizes constituents detected in groundwater and QC samples that attain or were above the current SWSL, SWS adopted Groundwater Protection Standards (GWP), North Carolina Groundwater Standards (2L) or the Maximum Contaminant Level (MCL) commonly referenced as the Federal "Drinking Water Standard". Table 6 lists the constituents detected in surface water and QC samples compared to the SWSL, the North Carolina Surface Water Standards (213) for a Class C water -body and the MCL. Quality Control Samples Acetone was detected in EB and FB and chloromethane was found in TB. Acetone was also detected in the majority of ground and surface water samples in comparable levels which is inconsistent with previous events. The detections of acetone are believed to be lab induced false positives. Since acetone levels were below regulatory Standards the acetone detections are largely inconsequential. However, acetone concentrations were not included when calculating the total cumulative VOCs which were used for statistical trend analysis. 3 Groundwater Samples Six metals were detected above the NC 2L/GWP Standard in samples collected from 13 wells including the background well (MW-1) as summarized in the following table. Metals Detected Above 2L/GWP Standards in Groundwater Cd Cr Co Pb Tl Va SWSL 1 10 10 10 5.5 25 2L/GWP STD. 2 10 1 15 0.28 0.3 MW-1 (BG Well) 21 MW-6 51.6 0.3 j MW-7 50.7 MW-9 166 0.33 j MW-11 11.7 MW-13 11 MW-14 12.4 13.1 18 j MW-15 2.7 j 3.1 j MW-16 242 MW-19 4.1 j 8.2 j MW-20 12.3 0.32 j MW-21 4.8 j MW-23 12.11 Concentrations in ug/L j = "j-qualified" since below the SWSL thus value is considered an estimate Seven VOCs were detected above the NC 2L Standard in samples collected from five wells as summarized in the following table. VOCs Detected Above 2L Standards in Groundwater 1,2-DCA 1,2-DCB 1,2-DCE 1,2-DCA Acetone Benzene VC SWSL 5 5 1 1 100 1 1 2L STD. 6 20 0.4 6 6000 1 0.03 MW-9 2.4 18.7 MW-13 0.96 j MW-15 9.7 0.58 j 1.6 MW-16 0.81 j 1.3 MW-21 0.49 j Loncentrations ill ug/L. j --i-quahIled" since below the 5 W JL thus value 1s considered an estimate 4 The majority of the monitoring locations that were found to contain VOCs included a mixture of dissolved phase aromatic hydrocarbons and chlorinated aliphatic hydrocarbons. The only constituent which originated from an anthropogenic source in levels above the EPA established maximum contaminant levels (MCLs) primary "Drinking Water Standards" was vinyl chloride in sample MW-9. A site map depicting the concentrations and estimated horizontal extent of VOCs that exceeded the 2L Standard during this event is presented on Sheet 2. The on -site water supply well (SCALEHOUSE) continues to lack detections in exceedance of current groundwater or drinking water Standards. Surface Water Samples Contaminants were not detected in any of the surface water samples above any established NC 2B Surface Water Standards. Corrective Action Update Groundwater remediation continues to be implemented per the approved Corrective Action Plan (CAP) at the three designated areas of concern (AOC) (Northern, Southern and MW-11). A Corrective Action Evaluation Report (CAER) (DIN: 19361) was submitted on May 1, 2013 which demonstrated that the plumes continue to decrease and was approved by the the SWS on July 24, 2013 (DIN:19366). A historical summary of corrective actions performed to date are briefly presented in the following sections. MNA Analysis (AOCs Northern, Southern and MW-11) Semi-annual MNA monitoring of a subset of 12 wells for the full suite of SWS recommended parameters was initiated on May 18, 2010 and performed for four consecutive semi-annual events to establish a baseline. A revised SAP prescribing 7 wells with various targeted MNA constituents was approved by the SWS and initiated during an event performed in May 2013. MNA monitoring was performed during this event for the parameters and frequency as listed in the current SAP. MNA parameters quantified during this event included alkalinity, sulfate, sulfide, chloride, TOC, COD, ferrous iron, CO2, turbidity, DO and ORP. MNA parameters are presented on Table 7. Enhanced Bioremediation via Substrate Injection (AOC Southern and Northern) Per the SWS approved Corrective Action Plan enhanced bioremediation via substrate and tracer injection was initiated in the Southern and Northern AOCs in accordance with requirements outlined in the Injection Well Permit Application and Well Permit No. WI0400176 (5/6/11) in an effort to reduce low level aliphatic and aromatic chlorinated hydrocarbons in groundwater to below the 2L Standards. An edible oil substate (EOS)-water emulsion with sodium bromide tracer was injected into four wells (IW-1, IW-2, IW-3 and IW-5) on November 2-3, 2011. Similar substrates were injected into monitoring wells MW-4/IW-4 and MW-8/IW-6 on October 24-25, 2012. Details of the injection events are provided in the Injection Event Record dated November 4, 2011 and January 10, 2013. 5 As directed in the UIC Injection Well Permit renewed on April 15, 2013 semi-annual post -injection water quality monitoring of wells located downgradient of viable injection points (MW-3R, MW-7, MW-9, MW-12S, MW-13, MW-14, MW-15, MW-16, MW-17, MW-18, MW-19, MW-20, MW-21, MW-22, MW-23) and upgradient background well MW-1 was also performed in conjunction with this semi-annual event. Total VOC concentrations reported during this event were lower at all locations when compared to the respective moving averages of the five events preceding injection in the selected wells downgradient of the injection points (Figure 1). Evaluation of injection wells (IW-1, IW-2, IW-3, IW-4, IW-5, IW-6) continues to indicate that a considerable amount of white highly turbid (>1,000 NTU) viscous residual organic substrate and its byproducts remain in each of these wells rendering them unsuitable for representative water quality analysis. The viscosity of the water in the injection wells during this May 2014 event precludes sample collection as either a bailer will not descend or the check valve fails. IW-1 was verified to not be a viable injection well as less than 3 gallons of substrate was able to be injected into the low permeable fractured bedrock and injectant levels have remained above static conditions for over a year. For all intents and purposes IW-1 injection did not occur nor will be possible in the future. MW-11 AOC Investigations The CAP designated MW-11 as an area of concern due to detections of VOCs detected in exceedance of 2L Standards. MW-I I is located within the compliance boundary near the northern property line which is hydraulically upgradient of the closed northern landfill. The northern landfill closed before October 1991 which was before adoption of NC Section .1600 rules that address assessment and corrective action. VOCs have historically been detected in excess of the 2L Standard at MW-11 which include a mixture of aromatics (fuel hydrocarbons) and chlorinated hydocarbons (solvents). Over the past 4 years (8 semi-annual events) the only constituent detected in excess of 2L Standard and SWSL was 1,2-dichloropropane. During this event levels of 1,2-dichloropropane fell remain above the 2L Standard but fell below the SWSL thus ` j-qualified". The CAP prescribed MNA and enhanced biodegredation to remediate MW-I I AOC. MNA has been performed continuously semiannually at MW-11 the past 6 years. Enhanced biodegredation has not been initiated at MW-11 AOC since hydrogeologic conditions relative to the source and property boundaries preclude it as an effective technique. MW-11 is positioned hydraulically upgradient of the source and is within the review boundary. A well was attempted to be installed at the property line 110 feet north of MW-I I on January 26, 2015 to delineate the extent of contamination. The potentiometric head at B-11R was expected to be at 25 feet (1132 ft amsl) but the boring encountered very competent rock at 9 ft and remained dry to 55 ft. (1102 ft amsl) for over 48 hours so was abandoned. 6 Groundwater and Surface Water Characterization A potentiometric map constructed from water elevations taken from the uppermost aquifer which consists of both saprolite and the hydraulically connected upper portion of the fractured bedrock system is enclosed as Sheet 2. Groundwater flow directions and velocity rates were calculated through modified Darcy's equation as shown on Table 8. Consistent with previous events the groundwater apparently flows in a general southeasterly direction towards the tributaries of the Ararat River. The calculated average linear velocity of groundwater indicates an approximate average of 873 ft/yr in the wells screened in regolith and 297 ft/yr in the wells screened in the bedrock. The consistent disparity in flow rates between wells is indicative of heterogeneous geologic conditions and/or a product of the limitations of the linear velocity equation when applied to anisotropic conditions which are characteristic of the geology of the Piedmont. Streams located within the facility boundaries were observed to be of high volume and flow with low turbidity in response to recent rainfall. Findings The inorganic detections are believed to be a product of erosion of natural deposits and not an anthropogenic source. An ASD which provides technical site specific facts and site specific analytical data including evaluations of interwell (background), intrawell (baseline), metals in leachate, dissolved compared to total metals and a discussion that substantiating evidence that the metals are not anthropogenic was not approved by the SWS. The SWS requested that the ASD be amended to include additional information. More time will be needed to collect additional field data prior to amending the ASD. The on -site supply well and the surface water points remain unimpacted as indicated by the lack of detections in excess of the applicable Standards. The on -site supply well is not considered potable thus bottled water is provided for consumption and "Non -Potable Water" warning signs were observed. One or more Appendix I VOC(s) continue to be detected in quantifiable levels above the 2L Standard in samples collected from the uppermost aquifer at three locations (MW-9, MW-17 and MW-20). All VOC concentrations remain within their own respective historically identified range with the exception of vinyl chloride in sample MW-9. Qualitative evaluation of VOC concentrations indicate a decreasing trend over time and distance from the landfill. Total cumulative VOC concentrations during this event decreased at all locations compared to their respective five event averages preceding corrective action except for MW-9, MW-19 and MW-20 (Figure 2). Results of statistical temporal trend analysis, using Sen's Slope Estimator at a 95% confidence level, compared to when corrective action began 6.5 years ago indicate that none of the individual well's cumulative VOC concentrations, except MW-9, have increased. The Southern AOC and cumulative site -wide VOC levels continue to exhibit a decreasing trend. The area of the uppermost aquifer beyond the compliance boundary containing quantifiable concentrations of VOCs in exceedance of the 2L Standard during this event is estimated at 0.0 acres in the Northern AOC, 0.0 acres in the MW-11 AOC and 5.3 acres in the Southern AOC for a total facility wide area of 5.3 acres (Sheet 2). This is an estimated 34% retraction of facility -wide plume area (from 8 acres to 5.3 acres) compared to when corrective action was initiated 6.5 years ago. 7 Evaluation of the most current water quality data continues to support assertions drawn in previous reports. Corrective action will continue except enhanced biodegradation will not occur at AOC MW-I I as was planned. A few VOCs persist in the upper portion of the aquifer but concentrations are decreasing over time and distance away from the landfill. The local discharge features which are all located within the property boundaries remain unimpacted. Data continues to indicate that the plumes within each AOC have stabilized and/or decreasing and there is adequate evidence that groundwater is naturally attenuating. Closing Water quality monitoring and corrective action is planned to continue in November 2017. If you have any questions regarding this report, please contact us at (919) 772-5393 or by email at ipfolilginesco.com. Sincerely, MUNICIPAL ENGINEERING SERVICES CO., P.A. VJo ha Pfohl En i onmental Specialist Enclosures cc: Mr. Dennis Bledsoe Surry County �� 1 - It .1 � � Steven R. Gandy, Ph.D, P.E. Senior Project Manger 8 Figures Figure 1 Total Cumulative VOC Concentrations Pre/Post Injection Comparison October 22, 2009 - June 1, 2017 OOWNGRAOIENT OF IW4 JTGTA CIIWUTM NOC CONCENTR TIONS� OONMGRADIENT OF rX4 (FOUL CIIM UTNE NOC CONCENMMONSI Yy11FN911 TNy� G.pll ({qfl Tlny�eOey Gnpll i i °wM YR.fp WY.f� iIlK11 UWAGRADrEN TOF t4 J=L CUN1ULf fC CONCENTRATIONS) I - - o: N Q , f %FM1M INY >IFtiM LYY •wr-+e +rnw WMIK39 WNT OF N4 (MML CWRLATM NVC CI tlKENTRATNNB} •wFu arN.>r 9wFNM Average of first Five Corrective Oct May Oct May Oct Action May Statistical Trend* 2009 2010 2010 2011 2011 Events 2017 Difference Difference Between Oct Well ID (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (%) 2009-May 2017 INJECTION WELL (IW-1) UNSUCCESSFUL INJECTION SO DOWNGRADIENT WELLS NOT SHOWN INJECTION WELL (IW-2) MONITORED DOWNGRADIENT BY MW-12S, MW-13 & MW-18 MW-12S 0.00 0.00 0.00 0.00 5.40 1.08 0.00 -1.08 -100 "No Trend" MW-13 61.00 50.60 74.20 87.30 72.50 69.12 39.24 -29.88 -43 �Downward� MW-18 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 "No Trend" INJECTION WELL (IW-3) MONITORED DOWNGRADIENT BY MW-3R & MW-16 MW-3R 0.00 0.00 1 0.00 0.00 0.00 0.00 0.00 0.00 0 "No Trend" MW-16 1137.90 113.60 135.70 121.20 116.30 124.94 21.21 -103.73 -83 IDownwardl INJECTION WELL (IW-4) MONITORED DOWNGRADIENT BY MW-14, MW-21 & MW-23 MW-14 15.20 15.60 15.60 8.20 17.00 14.32 7.46 -6.86 -48 �Downward� MW-21 52.10 50.70 51.38 39.10 32.41 45.14 24.14 -21.00 -47 . Downward MW-23 4.30 0.00 0.00 0.00 0.00 0.86 0.82 -0.04 -5 "No Trend" INJECTION WELL (IW-5) MONITORED DOWNGRADIENT BY MW-15 & MW-19 MW-15 96.13 63.89 55.00 78.10 64.06 71.44 53.93 -17.51 -25 �Downward� MW-19 0.00 0.00 0.00 0.00 0.00 0.00 1.01 1.01 0 "No Trend" INJECTION WELL (IW-6) NOT SHOWN AS NO WELLS DOWNGRADIENT WITHIN ZONE OF INFLUENCE * = Statistical Trend analysis via Sen's Slope Estimator at a 95% confidence level Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Figure 2 Total Cumulative VOC Concentrations Time Series Graphs/Table October 22, 2009 - May 31, 2017 Total Cumulative VOCS Multi -Well Time -Series Graph (NC) repree 112 f f f Sample Oate r m v -A-S FAO N -A-11 �AIIWeIIs 3WJIIERN AM(TOTAL CUMI1UA V CONC ENTUMNS) mU*well TIW4td""h S ( .y�v-t} yryC,S �YN-t6 •YY/t1 .uN-it NM11 .N,ys urr •ew.m u,Me •Nwa NORTN[RN AOC (TOTAL CUMI1L MT YX CONCENTUMNS� mwld Y ll MIr.Betks G-h U-V*� AOC Well ID Oct 2009 May 2010 Oct 2010 May 2011 Oct 2011 Average of first Five Corrective Action Events May 2017 A Difference Difference Statistical Trend (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) N Oct 2009 - May 2017 Background MW-1 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend IW-2 (MW-2) 105.25 207.00 207.93 159.90 79.10 151.84 79.10 NS NS NS No Trend IW-3 (MW-3RS) 202.90 127.50 127.50 144.00 127.60 145.90 127.60 NS NS NS No Trend MW-3R 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend IW-4 (MW-4) 27.00 24.20 24.20 27.60 23.50 25.30 18.10 NS NS NS No Trend IW-5 (MW-5) 35.00 46.50 46.50 47.40 34.80 42.04 34.80 NS NS NS No Trend MW-12S 0.00 0.00 0.00 0.00 5.40 1.08 0.00 -1.08 -100 No Trend MW-12D 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend MW-13 61.00 50.60 74.20 87.30 72.50 69.12 39.24 -29.88 -43 Downward MW-14 15.20 15.60 15.60 8.20 17.00 14.32 7.46 -6.86 -48 Downward Southern MW-15 96.13 55.00 55.00 78.10 64.06 69.66 53.93 -15.73 -23 Downward MW-16 137.90 113.60 135.70 121.20 116.30 124.94 21.21 -103.73 -83 Downward MW-17 20.34 8.40 8.85 0.00 5.77 8.67 0.00 -8.67 -100 No Trend MW-18 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend MW-19 0.00 0.00 0.00 0.00 0.00 0.00 1.01 1.01 0 No Trend MW-21 52.10 50.70 51.38 39.10 32.41 45.14 24.14 -21.00 -47 Downward MW-22 28.90 23.80 23.80 11.66 5.20 18.67 3.09 -15.58 -83 Downward MW-23 4.30 0.00 0.00 0.00 0.00 0.86 0.82 -0.04 -5 No Trend Combined Total 786.02 722.90 770.66 724.46 583.64 717.54 410.50 -307.04 -43 Downward MW-6 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend MW-7 7.40 9.40 11.20 9.70 8.80 9.30 0.00 -9.30 -100 Downward IW-6 (MW-8) 22.00 23.90 16.00 12.30 12.60 17.36 12.60 NS NS NS No Trend Northern MW-9 23.50 20.40 23.20 25.80 22.90 23.16 54.50 31.34 135 Upward MW-20 0.00 0.00 0.00 0.00 0.00 0.00 0.64 0.64 0 No Trend Combined Total 52.90 53.70 50.40 47.80 44.30 49.82 67.74 17.92 36 No Trend MW-11 MW-11 10.10 6.00 6.00 5.44 23.20 10.15 6.24 -3.91 -39 No Trend SITEWIDE Combined Total 849.02 782.60 827.06 777.70 651.14 777.50 484.48 -293.02 -38 Downward NS = Not sampled this event so most recent concentration shown and used in calculations * = Statistical trend analysis via Sen's Slope Estimator at a 95% Confidence Level A = Arsenic concentrations in May 2017 not included in calculations since likely false positives Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Sheets Topographic Map with Site Location Surry County Landfill, Mt. Airy fl 237 Landfill Road Mount Airy, NC 28621 Lat: 36-26-30.065 Long:-80-34-15.314 Northing:983356.18 Easting:1537885.48 0 Surry Co Property Line O Closed Unlined C&D Landfill O Closed Unlined Sanitary Landfill O Active Lined MSW Landfill SHEET 1 rvv_6 1046.15 106126 MW 20 1083A8 SW-2 IN2 2 errr.,e M W-11 1131.30 :RECYCLtARIA t SCALEHOUSE IFACILITY NON -POTABLE WATER SUPPLY WELL) L_J 1 � 1 • I M W-1 I 1113.giI i ' � 1 -� 23 1&0T yy 971.80� . - 1 •13 vw1.•.'e....' okra 99OA7 •�' r •� - MW-3R r 1 (19T UPSTREAM) AAA 9 sx rvifs ✓,,• SW-3 • �i _ r _ f � C I MLW-A ' 010.50 ''�. .89.2 1 MW23 48 f 9A6 MW-19 MIA LkVED .l 987.26 7 1 ^ 1211198 ; : $W-4 tiAGO NW-2 _ 923A9 - 77YELINEa MWdp Myyyyd3925.48 PHASE 2 } j •., 933.22 PTO 1ti �t • A,pwN-2 r... 44y� . MW-6R 937.35 Mwa 910.1a sr cf�o .�k en .� • rf+ � � 7,9} j �a + nwxSfO°"°a rarerrAwuw i.liN ' 1 ! r rcmteae + e.a • • 0e 1 1 , !0 :MW i ) 1 } fr GRAPHIC' SCALE �2_. 47� [ IN FEET } Z w w X : ig GAR 0, 0�1wn[ri Z' o - PO TEN WYE I•RIC MAP (Vcy - r " a m Aqrh Vo s O IG C TE0 480Vf �+. S TOs- t NO 94 959.9T CAR FORMFRI 'r OWNEC• N&a5 -SHA WN.-A _UMMEF S r' TENL) E i rS PM', rOPOGRAPtfrC CON IOLIIPS E.VS?Ti1N6 ROA05 - EVIMA FED WASTE Y-Adi r5 ONONED MSW &.'OP C'&D --- ---LINER LifrrlTS OP' SUOTLE D LINED MSWLE (iWOMIOREO SEPERArltlti'1 �£1 TENT OF COHESIVE CLA rM-0SURE UPON CLOSED MS AND f,&D nR:")PEIITS I1NF CxTRAPOLATED FPOM SURVEY- AND Cis .......... );.'0LJA1VCF 80I.+NOARY j250' ;�RLW £OWf. 11' FROM r ROPEPT',' LINE) -1090- ;:;007NTIaL uPPFRUOST CR011NDW.4OZ_R CON70VRS ��E aM/CkEEI� ,�Riv£17 �iP. SUPPLI #F1I, iFACrLITr CONSIDERS iT PION -POTAB(E) SW-3 :.: 4-ACC WA QFr MONO,'f7RING POIN T MW10 VL)NfTORiNG WELL IW2 1NJECP0?q WELT- (NOT SAMPLED DURING THIS EVENT) St-DfWEN T 9ASiN Y`- E%TFNT OF VOC(ei OFF-C70 At70VF SWS'I .. _T,yn;n11Pil cr 9ErONp COMPOANCE R7fiNDRT7Y Groundwater Leek S VOCa,].[acted Ab-2L Swdnde AREAOF C(xJCERN per CAP t NO 94 959.9T CAR FORMFRI 'r OWNEC• N&a5 -SHA WN.-A _UMMEF S r' TENL) E i rS PM', rOPOGRAPtfrC CON IOLIIPS E.VS?Ti1N6 ROA05 - EVIMA FED WASTE Y-Adi r5 ONONED MSW &.'OP C'&D --- ---LINER LifrrlTS OP' SUOTLE D LINED MSWLE (iWOMIOREO SEPERArltlti'1 �£1 TENT OF COHESIVE CLA rM-0SURE UPON CLOSED MS AND f,&D nR:")PEIITS I1NF CxTRAPOLATED FPOM SURVEY- AND Cis .......... );.'0LJA1VCF 80I.+NOARY j250' ;�RLW £OWf. 11' FROM r ROPEPT',' LINE) -1090- ;:;007NTIaL uPPFRUOST CR011NDW.4OZ_R CON70VRS ��E aM/CkEEI� ,�Riv£17 �iP. SUPPLI #F1I, iFACrLITr CONSIDERS iT PION -POTAB(E) SW-3 :.: 4-ACC WA QFr MONO,'f7RING POIN T MW10 VL)NfTORiNG WELL IW2 1NJECP0?q WELT- (NOT SAMPLED DURING THIS EVENT) St-DfWEN T 9ASiN Y`- E%TFNT OF VOC(ei OFF-C70 At70VF SWS'I .. _T,yn;n11Pil cr 9ErONp COMPOANCE R7fiNDRT7Y Groundwater Leek S VOCa,].[acted Ab-2L Swdnde AREAOF C(xJCERN per CAP IM1ELLI❑ iOPOF CA&NG ELEV9RON OFFM TO WATER ELEI T�PON BEN2ENE 12-LCA i 1-0CA VCA1 PREAOF 2L EXCEE ANCES BEYOND CCWLVNCE BUMn w Fr Mr STOC FrXASL (UAI MJLI iuAl cuatl VZAES) 15A NCFC 2L Gmundnaler Oual rtySurrd and T 0.30 6 G.03 BACKGROUND MN-1 1134 35 1 20.W 1113.41 IW2 1066.86 40.% 1027.91 N11 rani Bled" an9W1Nw 2011 NW-3R' 101750 3g 28 97822 1W3 162057 M 10 99047 WSarrpkd Q-ed.dt.h -MINor 2011 W4 102626 3532 990.94 Nn SarW Cara Mee 10 MIKhm Wal Od 2212 11A15 1080 t8 NR NR wSKMwambledlan to YW INN 2011 MN- 12S 102580 1Z79 101301 NW-120, 1027 05 0.00 1027.05 NW43 1N8.48 2510 983.38 096 SOUTHERN WV-$4 101880 34.86 983.95 5.31 NNF 15 1075 96 5242 1023.54 0 68 r 9 70 160 PNANJ 6 999 54 2422 975 32 0 8101 1 30 NW-17 96S43 75S 957.98 WY-18 M.00 840 974.50 N0149 94627 9.01 937 26 NW-21 965 36 5 45 25991 0 49 NN122 96340 4.71 948.69 WY-23 966.31 S85 94846 WY-6 1067.67 2136 1046.31 NORTHERN NW-7 1073 50 1139 106212 0 r 149 4230 10015 NofS Ob. eiW lVH tm Ylgl Od 4,2 NAN-g 109d08807 32.81 106126 2.40 18 70 g1Af-2 0 1082.19 19.11 1063.00 NNJ 11 WV-1 1 1151.80 20.50 113130 1 1 1 0 nng (IY='j Ol alf ed m>wemrstion 6HEi mnaidered an eaemaca CLOSED C&D LANDFILL and CLOSED MSWLF FACILITY SURRY COUNTY MT. AIRY, NORTH CAROLINA SHEET 2 Municipal 7� Services T _ P.O. BOX 97 GARNER, N.C. 271129 - - 19191 n23393 LICENSE NU NBER: C4281 Engineering Company, P.A. P.O. BOX !49 BOONE. H.C. 26001 (US) 282-1707 Table Table 1 Groundwater Monitoring Well Construction Table May 30-31, 2017 Monitoring Well Date Installed Well Diameter Total Well Depth Top of Screen Depth Screen Length Geology of Screened Interval Top of Casing Elevation Ground Elevation Groundwater Elevation Depth to Water Latitude Longitude (inches) (ft bgs) (ft bgs) (ft) (ft amsl) (ft amsl) (ft amsl) (ft btoc) MW-1 11/28/89 2 40 30 10 Clay 1134.35 1133.15 1113.41 20.94 36.439211 -80.568133 IW-2 (was MW-2) 11/28/89 2 70 60 10 Clay 1068.86 1068.36 1027.91 40.95 36.435833 -80.568894 MW-3R 9/27/94 2 101 86 15 Rock 1017.50 1015.00 978.22 39.28 36.434725 -80.571989 IW-3 (was MW-3RS) 5/17/01 2 52 37 15 Rock 1020.57 1018.24 990.47 30.10 36.434656 -80.571858 IW-4 (was MW-4) 8/30/94 2 55.4 40.4 15 Rock 1026.26 1025.06 990.94 35.32 36.434686 -80.569200 IW-5 (was MW-5) 8/27/94 2 63 48 15 Rock 1080.18 1077.78 <1039.50 >40.68 36.434614 -80.570436 MW-6 9/7/94 2 29.7 14.7 15 Rock 1067.67 1065.61 1046.31 21.36 36.437431 -80.571067 MW-7 8/23/94 2 23 8 15 Rock 1073.50 1071.50 1062.12 11.38 36.438439 -80.570722 IW-6 (was MW-8) 8/16/94 2 54 39 15 Rock 1088.45 1086.45 1046.15 42.30 36.439278 -80.570381 MW-9 8/22/94 2 43.8 28.8 15 Rock 1094.07 1092.07 1061.26 32.81 36.439289 -80.571508 MW-11 8/15/94 2 40 25 15 Rock 1151.80 1150.40 1131.30 20.50 36.441589 -80.569558 MW-12S 5/31/01 2 51 11 40 Rock 1025.80 1023.25 1013.01 12.79 36.435942 -80.567972 MW-12D 5/30/01 2 100 90 10 Rock 1027.05 1023.75 1027.05 0.00 36.435964 -80.567994 MW-13 5/30/06 2 35.78 20.78 15 Saprolite 1008.48 1005.75 983.38 25.10 36.435036 -80.568183 MW-14 5/30/06 2 48.03 33.03 15 Rock 1018.80 1016.11 983.95 34.85 36.434267 -80.569239 MW-15 6/22/06 2 57 42 15 Rock 1075.96 1073.23 1023.54 52.42 36.433797 -80.570467 MW-16 6/21/06 2 36.3 21.3 15 Rock 999.54 996.67 975.32 24.22 36.434536 -80.572117 MW-17 6/1/07 2 15.32 5.32 10 Rock 965.43 962.26 957.88 7.55 36.433558 -80.572517 MW-18 6/1/07 2 18.15 8.15 10 Saprolite 983.00 980.00 974.60 8.40 36.435453 -80.567050 MW-19 6/1/07 2 17.1 7.1 10 PWR 946.27 942.97 937.26 9.01 36.432231 -80.570556 MW-20 6/1/07 2 25.64 10.64 15 Rock 1082.19 1079.12 1063.08 19.11 36.439025 -80.571650 MW-21 6/1/07 2 15.41 5.41 10 Saprolite/PWR 965.36 962.22 959.91 5.45 36.434214 -80.568717 MW-22 6/1/07 2 16.04 6.04 10 Saprolite 953.40 950.23 948.69 4.71 36.432928 -80.571678 MW-23 6/1/07 2 17.1 7.1 1 10 Sandy Silt 955.31 952.09 1 948.46 1 6.85 1 36.432828 -80.569156 NOTE: bgs = below ground surface amsl= above mean sea level btoc = below top of casing (PVC well casing) Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1 Table 2 Field Observations of Monitoring Locations May 31 - June 1, 2017 Location Viable Lack of Any Monitoring Evidence of Location Tampering Locked on Arrival & Departure Hinge/Hasp Operational Tagged or Labeled Concrete Surface Pad Appears Effective Comments MW-1 Yes Yes Yes Yes Yes Yes Pad cracked IW-1 No Yes Yes Yes Yes Yes Fouled since injection 11/2/11. IW-2 (was MW-2) No Yes Yes Yes Yes Yes Fouled since injection 11/2/11. No pad visible MW-3R Yes Yes Yes Yes Yes Yes No pad IW-3 (was MW-3RS) No Yes Yes Yes Yes Yes Fouled since injection 11/2/11. IW-4 (was MW-4) No Yes Yes Yes Yes Yes Fouled since injection 10/24/12. IW-5 (was MW-5) No Yes Yes Yes Yes Yes Fouled since injection 11/2/11. Bailer would not descend MW-6 Yes Yes Yes Yes Yes Yes No pad, red purge water MW-7 Yes Yes Yes Yes Yes Yes No pad IW-6 (was MW-8) No Yes Yes Yes Yes Yes Fouled since injection 10/24/12. No pad. Lock replaced MW-9 Yes Yes Yes Yes Yes Yes MW-11 Yes Yes Yes Yes Yes Yes No pad MW-12S Yes Yes Yes Yes Yes Yes MW-12D Yes Yes Yes Yes Yes Yes Flowing artesian MW-13 Yes Yes Yes Yes Yes Yes Can hear water cascade in well MW-14 Yes Yes Yes Yes Yes Yes MW-15 Yes Yes Yes Yes Yes Yes MW-16 Yes Yes Yes Yes Yes Yes Red purge water MW-17 Yes Yes Yes Yes Yes Yes MW-18 Yes Yes Yes Yes Yes Yes MW-19 Yes Yes Yes Yes Yes Yes MW-20 Yes Yes Yes Yes Yes Yes MW-21 Yes Yes Yes Yes Yes Yes MW-22 Yes Yes Yes Yes Yes Yes MW-23 Yes Yes Yes Yes Yes Yes SW-1 Yes High gage height & flow SW-2 Yes High gage height & flow SW-3 Yes High gage height & flow SW-4 Yes High gage height & flow SWN-1 Yes High gage height & flow SWN-2 Yes High gage height & flow SCALEHOUSE I Yes I I I I I I Sample from spigot next to well which is typical Any unusual field conditions, observations, or events: Injection wells (IW-1, IW-2, IW-3, IW-4, IW-5 and IW-6) exempt from laboratory analysis as SWS approved on May 10, 2013 (DIN:18938) Stormwater control improvements performed since May 2012 event. Visual markers (10 ft PVC pipes) remain secured to each monitoring well case Rain several evenings during event. Therfore surface waters were higher than normal Slurry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1 Table 3 Field Parameter Data Summary May 31 - June 1, 2017 Parameter Depth to Water Water Elevation TOC Elevation Temp. ORP DO pH Specific Conductance TDS Turbidity Units ft (btoc) ft (amsl) ft (amsl) C mV mg/L SU umhos/cm mg/L Visual or NTU MW-1 20.94 1108.20 1134.35 15.3 191 2.6 6.3 210 NR 6.7 IW-2 40.95 1028.65 1068.86 NR NR NR NR NR NR >1000 MW-3R 39.28 975.39 1017.50 15.3 NR NR 7.0 317 NR Clear IW-3 30.10 975.39 1020.57 NR NR NR NR NR NR >1000 IW-4 35.32 990.94 1026.26 NR NR NR NR NR NR >1000 IW-5 NR <1039.50 1080.18 NR NR NR NR NR NR NR MW-6 21.36 1044.66 1067.67 14.6 NR NR 6.7 246 NR Slight MW-7 11.38 1060.24 1073.50 15.3 203 1.8 5.5 227 NR 19.8 IW-6 42.30 1045.26 1088.45 NR NR NR NR NR NR >1000 MW-9 32.81 1060.85 1094.07 15.4 -19 0.5 6.1 427 NR 6.3 MW-11 20.50 1127.51 1151.80 15.7 36 3.0 6.5 320 NR 3.3 MW-12S 12.79 1011.65 1025.80 15.5 NR NR 6.3 193 NR Clear MW-12D 0.00 1027.05 1027.05 15.3 NR NR 6.1 262 NR Slight MW-13 25.10 982.79 1008.48 14.2 NR NR 5.5 231 NR Clear MW-14 34.85 981.39 1018.80 14.0 37 0.9 6.0 73 NR 19.8 MW-15 52.42 1026.32 1075.96 15.3 34 0.6 5.7 129 NR 701 MW-16 24.22 972.39 999.54 14.5 NR NR 6.1 367 NR Clear MW-17 7.55 955.72 965.43 14.4 NR NR 6.3 226 NR Clear MW-18 8.40 973.95 983.00 13.9 NR NR 6.1 306 NR Clear MW-19 9.01 937.41 946.27 13.8 NR NR 5.8 31 NR Clear MW-20 19.11 1062.74 1082.19 14.4 NR NR 6.2 109 NR Slight MW-21 5.45 959.42 965.36 14.1 138 2.2 5.6 192 NR 101 MW-22 4.71 948.35 953.40 15.1 NR NR 5.7 319 NR Clear MW-23 6.85 947.85 955.31 13.5 NR NR 6.1 49 NR Slight Scalehouse na na na 17.5 NR NR 7.6 242 NR Clear Minimum 0.00 937.41 946.27 13.5 -19 0.5 5.5 31 NR Clear Average 21.97 1008.87 1034.58 14.9 89 1.7 6.2 224 NR Slight Maximum 52.42 1127.51 1151.80 17.5 203 3.0 7.6 427 NR >1000 SW-1 - - - 15.3 NR NR 7.9 74 NR Clear SW-2 - - - 16.9 NR NR 7.3 110 NR Clear SW-3 - - - 17.8 NR NR 7.1 281 NR Clear SW-4 - - - 17.3 NR NR 7.7 73 NR Clear SWN-1 - - - 17.0 NR NR 7.3 39 NR Clear SWN-2 - - - 16.9 NR NR 7.4 41 NR Clear Minimum - - - 17.8 NR NR 7.9 281 NR Clear Average - - - 16.9 NR NR 7.5 103 NR Clear Maximum - - - 17.8 NR NR 7.9 281 NR Clear btoc = Below top of casing amsl = Above mean sea level na = Not available NR = No reading attempted Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1 Table 4 Sampling and Analysis Summary May 31-June 1, 2017 App. I App. II MNA Field Parameter Tracer a Q a of O = N U m n O in a a > U o 0 H m () L _ O a C rn CL C1 C6 C `p CO O) = W C N U fn O N O ZT x 7 p y Q :2L_ N CU N >, « 6 Q Q CU CD = 76 N a)> C . C N W N 'O (U Y (U O` a N •> N w 0 U v ° N n p aE U m U m -2 o In o U O O O O N (U (U O 7 LL 5, N to Y_ 7 :3 L O o .- to 2 > H > H 2 fn d H fA > 2 0 a (n u) U Z 0 O H U H Q H CO 0 m m O a 0 m U? O (n O y � 0 CD O io O) O o 't CD... `s O O -Ito ONO CDccoo (D ONo Co M X X L N O O m 0 (00 N N N N N N N O a CDa a s a a a a 0 a 0 a 0= C _o CD o g CD o o 0 N a o a W a W W Cn a W W a W m M O O M M Cn M M LO N LO W a� W '� 2 '� 2 '� 2 2 '� 2 � '� CO 0 L L L N N N aa. a a a a a OJ CD JJJJ JJJ a a a LL W W J W m M J J LL LL LL LL LL LL LL W IW-1 Not sampled since injection wells are exempt MW-1 X X X X X X X X I X I X X I X X X I X X X X X X X IW-2 Not sampled since injection wells are exempt MW-3R X I X I I I I I I I I I I I I x1 X X X IW-3 Not sampled since injection wells are exempt IW-4 Not sampled since injection wells are exempt IW-5 Not sampled since injection wells are exempt MW-6 X X1 I I I I I I I I I I I X X X X MW-7 X X X I X I X X I X X X I X X X X X X X IW-6 Not sampled since injection wells are exempt MW-9 X X X X X X X X X X X X X X X X X X X X X MW-11 X X X X X X X X X X X X X MW-12S X X X X X X MW-12D X X X X X X MW-13 X X X X X X X X X X X MW-14 X X X X X X X X X X X X X X X X MW-15 X X X X X X X X X X X X X X X X X X X X X MW-16 X X X X X X X X X X X MW-17 X X X X X X X X X X X MW-18 X X X X X X MW-19 X X X X X X MW-20 X X X X X X MW-21 X X X X X X X X X X X X X X X X X X X X X MW-22 X X X X X X X X X X X MW-23 X X X X X X Scalehouse X X X X X X X X X X X SW-1 X X X X X X SW-2 X X X X X X SW-3 X X X X X X SW-4 X X X X X X SWN-1 X X X X X1 X SWN-2 X X X X X X EB X X X FB X X TB X App I & II Lists = From current 40 CFR 258 Injection wells exempt from monitoring except for turbidity and WLR per SWS approved SAP 118936] Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1 Table 5 Groundwater and QC Sample Detections May 31- June 1, 2017 Parameter Name MDL SWSL 2LIGWP MCL MW-1 MW-3R MW-6 MW-7 MW-9 MW-11 MW-12D MW-12S MW-13 MW-14 MW-15 MW-16 MW-17 MW-i6 MW-19 MW-20 MW-21 MW-22 MW-23 SCALEHOUSE EB FB TB Std B S S S S S S S S S S S S S S S S S S SuoDly Well QC QC QC Metals endix I Barium, total 2.5 100 700 2000 92.9 J 7.4 J 92.4 J 55.1 J 48.2 J 40.7 J 7.3 J 23.5 J 85.7 J 84 J 49.2 J 68 J 27.5 J 28.4 J 70.2 J 27.6 J 60.5 J 56.9 J 33.8 J 14.4 J Beryllium, total 0.5 1 4 4 0.61 J Cadmium, total 0.5 1 2 5 0.89 J 1.3 1.4 0.66 J 1.5 0.52 J 0.63 J 2.1 (N) Chromium, total 2.5 10 10 100 3.2 J 2.8 J 12.4 (N) 7 J 2.6 J 5.6 J Cobalt, total 2.5 10 1 NE 51.6 (N) 50.7 (N) 166 (N) 11.7 (N) 11 (N) 13.1 (N) 2.7 J (N) 242 (N) 4.1 J (N) 12.3 (N) 4.8 J (N) Copper, total 2.5 10 1000 1300 356 4.2 J 2.7 J 3.5 J 6.9 J 3.8 J 122 4.4 J 5 J Lead, total 2.5 10 15 15 21 (N) 2.8 J 2.6 J 3 J 2.7 J 9.2 J 3 J Nickel, total 2.5 50 100 NE 4.5 J 3.6 J 6.6 J 2.7 J 2.8 J 2.6 J 8.6 J 3.1 J 13.2 J 3.2 J 2.6 J Thallium, total 0.02 5.5 0.28 2 0.026 J 0.3 J (N) 0.11 J 0.33 J (N) 0.061 J 0.12 J 0.16 J 0.091 J 0.2 J 0.054 0.081 J 0.32 J 0.11 J 0.024 J Vanadium, total 1 2.5 25 0.3 NE 1B J (N) 3.1 J (N) B.2 J (N) Zinc, total 5 10 1000 NE 256 10.7 10.7 38.3 19.4 6.6 J 8.4 J 36.1 10.7 14.7 5.1 J 10.7 20.2 7.7 J 5.3 J 6.3 J 6.5 J 16 VOCs endix I 1,1-Dichloroethane 0.32 5 6 NE 2.4 J 0.37 J 4 J 2.6 J 9.7 (L) 0.58 J 0.36 J 4.1 J 0.63 J 0.43 J 1,2-Dichlorobenzene 0.3 5 20 NE 1.5 J 0.48 J 1,2-Dichloroethane 0.24 1 0.4 5 0.96 J (L) 0.58 J 0.81 J 0.49 J (L) 1,4-Dichlorobenzene 0.33 1 6 75 2.2 5.7 2.5 3.6 3.7 4.3 1.1 Acetone 10 100 6000 NE ki 29.5 J 21.4 J 13.5 J 20.7 J 16.1 J 14.4 J 111 15.2 J 12.9 J 14A J 10.2 Benzene 0.25 1 1 5 0.3 J 2.4 (L) 0.62 J 0.65 J 0.44 J Chlorobenzene 0.23 3 50 100 3.9 2.2 J 0.87 J 1.6 J 2.4 J 1.8 J 0.25 J 0.42 J J014J Chloroethane 0.54 10 3000 NE 1.9 J Chloromethane 0.11 1 3 11 NE I I 1 0.32 J 0.14 J cis-1,2-Dichloroethene 0.19 5 70 70 0.28 J 19.7 1 J 28.1 4 J 33.3 11.5 0.65 J 0.64 J 18.6 0.94 J 0.39 J 0.22 J Tetrachloroethene 0.46 1 0.7 5 0.54 J Toluene 0.26 1 600 1000 0.88 J Trichloroethene 0.47 1 3 5 0.98 J 2 0.7 J Vinyl chloride 0.62 1 0.03 2 18.7 U 1 1.6 (L) 1.3 (L) Assessement Monitorina Parameters endix II Acrolein 1.6 53 4 NE -- -- -- 2.1 J -- -- -- -- - -- - Allyl chloride 1.5 10 NE NE -- -- -- 8.2 J -- -- -- -- - -- - 4.1 J Cyanide 4 10 70 NE -- -- -- -- -- -- -- 4.6 J 12.7 5.2 J -- - -- 4.7 J - - -- Tin total 2.5 100 1 2000 1 NE 1 3.9 J 1-- -- -- -- -- -- 5.3 J I-- -- -- -- -- Units gIL, Blank cells means Not Detected, -- means not tested Red sold Above Established MCL12UGWP Std. VeIlcw Highlighted Above Established Federal MCL Drinking Water Std. No regulatory compliance significance. MDL = Method Detection Limit, SWSL = Sold Waste Section Limit, 2LIGWP StandaN = NC 2L sod IMAC Standards aclopted by SINS, MCL = Mmo um Contaminant Leval for Drinking Water J = "J-qualified". Concentration detected between MDL and SWSL. Considered estimated value (N) Preliminary source is baliavad to be Natural originating from erosion of natural dap.h. Source not anthropogenic. (L) Prelllminary source Is belleved to be anihropogeoic with leachate a landfill gas as transport mechanism A definitive source of the detections was not detaminetl as part of this report. BG = Background Well Sample, QC = Quality Control Sample, S = Sengnal Well Sample Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1 Table 6 Surface Water and QC Sample Detections June 1, 2017 Parameter Name MDL I SWSL 2B Std MCL SWN-1 SW-1 SW-2 SW-3 SW-4 SW -A SW-13 SWN-2 EB FB TB U D D D D D D D QC QC QC Metals endix I Barium, total 2.5 100 200000 2000 21.3 J 26.8 J 17 J 21.8 J 22 J -- 20.4 J -- Cobalt, total 2.5 10 270 NE 16.8 8 J -- -- Thallium, total 0.02 5.5 0.47 2 0.048 J 0.054 J -- -- Vanadium, total 2.5 25 NE NE -- 2.8 J -- Zinc, total 5 10 50 NE 9.1 J 7.4 J 7 J -- 5.4 J -- VOCs (Appendix 1) Acetone 10 100 2000 NE 13.3 J 19.3 J 12.2 J 11.6 J 14.4 J 10.2 J Chloromethane 0.11 1 550 NE 0.13 J 0.13 J 0.14 J cis-1,2-Dichloroethene 0.19 5 1 4900 1 70 2.4 J Units ug/L, Blank cells means Not Detected, — means not tested Red Bold Above Established 2B Std. Regulatory compliance Standard Yellow Highlighted Above Established Federal MCL Drinking Water Std. No regulatory compliance significance. MDL = Method Detection Limit, SWSL = Solid Waste Section Limit, 2B Standard = NC 2B Surface Water Standards adopted by SWS, MCL = Maximum Contaminant Level for Drinking Water J = "J-qualified". Concentration detected between MDL and SWSL. Considered estimated value U = Upstream of monitored unit, D= Downstream of monitored unit Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1 Table 7 MNA Parameter Data Summary May 31 - June 1, 2017 Parameters Method MDL* Units MW-1 MW-7 MW-9 MW-11 MW-14 MW-15 MW-21 6/1/17 6/1/17 6/1/17 6/1/17 6/1/17 5/31/17 5/31/17 VFA — Acetic Acid AM23G NS ug/L NS NS NS NS NS NS NS VFA — Butyric Acid AM23G NS ug/L NS NS NS NS NS NS NS VFA — Lactic Acid AM23G NS ug/L NS NS NS NS NS NS NS VFA — Propionic Acid AM23G NS ug/L NS NS NS NS NS NS NS VFA — Pyruvic Acid AM23G NS ug/L NS NS NS NS NS NS NS Hydrogen AM20GAX NS nM NS NS NS NS NS NS NS Methane AM20GAX NS ug/L NS NS NS NS NS NS NS Ethene AM20GAX NS ug/L NS NS NS NS NS NS NS Ethane AM20GAX NS ug/L NS NS NS NS NS NS NS CO2-Dissolved Field HACH Kit 10 mg/L 20 >100 >100 >100 >100 >100 >100 Alkalinity SM 2320B 1000 ug/L 42200 69200 44800 NS NS 43700 34900 Sulfate EPA 300.0 1000 ug/L 8830 5520 984 NS 2060 1180 1380 Sulfide SM 4500-S21D 100 ug/L <100 <100 <100 NS 115 NS NS Chloride SM 4500-CI-E 500 ug/L 3770 31200 28300 NS 2280 1450 28800 TOC SM 5310B 500 ug/L 605 2400 2250 NS 1420 675 1200 COD SM 5220D 12500 ug/L <12500 20000 23000 NS 13000 <12500 <12500 BOD SM5210B NS ug/L NS NS NS NS NS NS NS Ferrous Iron EPA 6010 500 ug/L <500 <500 1300 NS <500 1700 <500 Nitrate EPA 353.2 NS ug/L NS NS NS NS NS NS NS Temperature Field Instrument 0 C 15.3 15.3 15.4 15.7 14.0 15.3 14.1 ORP Field Instrument -900 mV 191 203 -19 36 37 34 138 DO Field Instrument 0 mg/L 2.6 1.8 0.5 3 0.9 0.6 2.2 pH Field Instrument 0 SU 6.3 5.5 6.1 6.5 6 5.7 5.6 Specific Conductance Field Instrument 0 us/cm 210 227 427 320 73 129 192 Turbidity Visual 1 0 Visual 1 6.7 1 19.8 6.3 3.3 19.8 701 101 Notes: VFA = Volatile Fatty Acids MDL* = Lab Method Detection Limit or lowest field measurement possible. Constituents detected below quantifiable limits are shown as < MDL value. >100 = CO2 Concentration exceeds maximum capability of method used. NS = Not Sampled Surry County Closed CDLF and CLosed MSWLF, Mt. Airy Page 1 of 1 Table 8 Hydrogeolofic Properties at Monitoring Well Locations May 31-June 1, 2017 Well Hydraulic Conductivity Effective Porosity Hydraulic Gradient Groundwater Average Linear Velocity Rate Flow Direction Immum Distance From Upgradient EOW (ft) Ground Water Depth Groundwater Potentiometric Elevation Screened Interval Lithology (cm/second) (ft/day) (°/u) (feet/feet) (feet/year) (feet btoc) (feet amsl) MWA 4.30E-05 0.12 15 0.054 16 S20W 0 20.94 1113.41 Clay IW-2 4.30E-05 0.12 15 0.238 71 S50E - 40.95 1027.91 Clay MW-7 8.10E-04 2.30 15 0.891 4,977 N69W 704 11.38 1062.12 PWR / Fractured Rock IW-6 4.40E-04 1.25 15 0.101 305 S51E - 42.30 1046.15 PWR/ Fractured Rock MW-9 1.90E-04 0.54 15 0.069 90 S54E 614 32.81 1061.26 Sandy Sift MW-13 2.06E-04 0.58 23 0.464 430 S29W 1850 25.10 983.38 Saprolite MW-18 2.04E-03 5.78 15 0.142 na S24E 0 8.40 974.60 Saprolite MW-19 1.10E-03 3.12 3 0.056 2,121 S12W 2663 9.01 937.26 PWR MW-21 1.28E-03 3.63 3 0.003 124 S66E 2041 5.45 959.91 Saprolite/PWR MW-22 9.88E-04 2.80 15 0.073 498 S28W 2506 4.71 948.69 Saprolite MW-23 3.04E-04 0.86 15 0.046 96 S32E 2610 6.85 948.46 Sandy Sift Minimum 4.30E-05 0.12 3 0.003 16 0 4.71 937.26 Average 6.77E-04 1.92 14 0.194 873 1443 18.90 1005.74 Maximum 2.04E-03 5.78 23 0.891 4,977 2663 42.30 1113.41 MW-3R 2.40E-04 0.68 5 na na na 1,994 39.28 978.22 Fractured Rock IW-3 2.40E-05 0.07 5 0.394 196 S37W - 30.10 990.47 Fractured Rock IW-4 1.10E-04 0.31 5 0.139 317 S45E 35.32 990.94 Fractured Rock IW-5 1.50E-05 0.04 5 - S61E - - - Fractured Rock MW-6 1.90E-05 0.05 5 0.174 68 S85W 963 21.36 1046.31 Fractured Rock MW-11 3.10E-04 0.88 5 0.040 256 S18W 0 20.50 1131.30 Fractured Rock MW-12S na na 3 0.179 na S07E 0 12.79 1013.01 Fractured Rock MW-12D 1.30E-06 0.00 5 na na na 0 0.00 1027.05 Fractured Rock MW-14 7.45E-03 21.12 3 0.163 41,990 S74E 2098 34.85 983.95 Fractured Rock MW-15 7.21E-05 0.20 3 0.212 528 S08E 52.42 1023.54 Fractured Rock MW-16 2.82E-05 0.08 3 0.094 91 S53W 2089 24.22 975.32 Fractured Rock MW-17 2.94E-04 0.83 3 0.027 272 S77W 2547 7.55 957.88 Rock MW-20 1.92E-04 0.54 3 0.097 644 S22E 692 19.11 1063.08 Rock Minimum 1.30E-06 0.00 3 0.027 68 0 0.00 957.88 Average 7.30E-04 2.07 4 0.152 297 1154 24.79 1015.09 Maximum 7.45E-03 21.12 5 0.394 644 2547 52.42 1131.30 NOTE: Values for hydraulic conductivity determined via slug test by GAI, MESCO, or Joyce. Hydrologic gradient from water levels recorded on May 31-June 1, 2017. Wells screened entirely in rock were not utilized for flow directions/gradients. Screens that traverse both rock and regolith assumed flow in regolith dominates. Hydraulic Conducitivity value and flow rate for MW-14 was considered an outlier; therefore not included in the average or maximum. na = Not available/applicable Average Linear Velocity (Q) is defined by modified Darcy's equation: K A K= hydraulic conductivity where Q ri dl ne= effective porosity e dh=head difference dl= horizontal distance Slurry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Appendix A Laboratory Analysis Reports Chains of Custody lacieAnalXical" www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 June 19, 2017 Mr. Jonathan Pfohl Municipal Engineering Services 68 Shipwash Dr. Garner, NC 27529 RE: Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory on June 02, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Trey Carter trey. carter@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 54 lacmnalytical' www.pacelabs.corn Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 Ormond Beach Certification IDs 8 East Tower Circle, Ormond Beach, FL 32174 Alabama Certification #: 41320 Connecticut Certification #: PH-0216 Delaware Certification: FL NELAC Reciprocity Florida Certification #: E83079 Georgia Certification #: 955 Guam Certification: FL NELAC Reciprocity Hawaii Certification: FL NELAC Reciprocity Illinois Certification #: 200068 Indiana Certification: FL NELAC Reciprocity Kansas Certification #: E-10383 Louisiana Certification #: FL NELAC Reciprocity Louisiana Environmental Certificate #: 05007 Maryland Certification: #346 Michigan Certification #: 9911 Mississippi Certification: FL NELAC Reciprocity Missouri Certification #: 236 Montana Certification #: Cart 0074 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Nebraska Certification: NE-OS-28-14 Nevada Certification: FL NELAC Reciprocity New York Certification #: 11608 North Carolina Environmental Certificate #: 667 North Carolina Certification #: 12710 Oklahoma Certification #: D9947 Pennsylvania Certification #: 68-00547 Puerto Rico Certification M FLO1264 South Carolina Certification: #96042001 Tennessee Certification #: TN02974 Texas Certification: FL NELAC Reciprocity US Virgin Islands Certification: FL NELAC Reciprocity Virginia Environmental Certification #: 460165 Wyoming Certification: FL NELAC Reciprocity West Virginia Certification #: 9962C Wisconsin Certification #: 399079670 Wyoming (EPA Region 8): FL NELAC Reciprocity South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 Lab ID Sample ID Matrix Date Collected Date Received 92342784001 MW-6 Water 06/01/17 15:00 06/02/17 08:00 92342784002 MW-12D Water 06/01/17 09:35 06/02/17 08:00 92342784003 MW-11 Water 06/01/17 12:02 06/02/17 08:00 92342784004 SCALE HOUSE Water 06/01/17 16:22 06/02/17 08:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: SURRY CLOSED -MT. AIRY (AM) 92342784 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92342784001 MW-6 EPA6010 SH1 14 PASI-A EPA 6020E CDF 1 PASI-A EPA 8260 GAW 50 PASI-C 92342784002 MW-12D EPA6010 SH1 14 PASI-A EPA 6020E CDF 1 PASI-A EPA 8260 GAW 50 PASI-C 92342784003 MW-11 EPA 8081 RES 21 PASI-C EPA 8082 HSK 8 PASI-C EPA 8151 LJM 6 PASI-O EPA6010 SH1 15 PASI-A EPA 6020E CDF 1 PASI-A EPA 7470 KAL 1 PASI-A EPA 8270 BPJ 111 PASI-C EPA 8260 GAW 67 PASI-C SM 4500-S2D MVC 1 PASI-A SM 4500-CN-E AES2 1 PASI-A 92342784004 SCALE HOUSE EPA 8081 RES 21 PASI-C EPA 8082 HSK 8 PASI-C EPA 8151 LJM 6 PASI-O EPA6010 SH1 15 PASI-A EPA 6020E CDF 1 PASI-A EPA 7470 KAL 1 PASI-A EPA 8270 BPJ 111 PASI-C EPA 8260 GAW 67 PASI-C SM 4500-S2D MVC 1 PASI-A SM 4500-CN-E AES2 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 Sample: MW-6 Lab ID: 92342784001 Collected: 06/01/17 15:00 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Antimony ND ug/L 6.0 3.9 1 06/04/17 16:40 06/14/17 22:31 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:31 7440-38-2 Barium 92.4J ug/L 100 2.5 1 06/04/17 16:40 06/14/17 22:31 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:31 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:31 7440-43-9 Chromium 3.2J ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:31 7440-47-3 Cobalt 51.6 ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:31 7440-48-4 Copper ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:31 7440-50-8 Lead 2.8J ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:31 7439-92-1 Nickel 3.6J ug/L 50.0 2.5 1 06/04/17 16:40 06/14/17 22:31 7440-02-0 Selenium ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:31 7782-49-2 Silver ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:31 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 06/04/17 16:40 06/14/17 22:31 7440-62-2 Zinc 10.7 ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:31 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Thallium 0.30J ug/L 5.5 0.020 1 06/06/17 02:45 06/09/17 20:20 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 06/04/17 15:00 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 06/04/17 15:00 107-13-1 Benzene ND ug/L 1.0 0.25 1 06/04/17 15:00 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 06/04/17 15:00 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 06/04/17 15:00 75-27-4 Bromoform ND ug/L 3.0 0.26 1 06/04/17 15:00 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 06/04/17 15:00 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 06/04/17 15:00 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 06/04/17 15:00 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 06/04/17 15:00 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 06/04/17 15:00 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 06/04/17 15:00 75-00-3 Chloroform ND ug/L 5.0 0.14 1 06/04/17 15:00 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 06/04/17 15:00 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 06/04/17 15:00 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 06/04/17 15:00 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 06/04/17 15:00 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 06/04/17 15:00 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 06/04/17 15:00 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 06/04/17 15:00 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/04/17 15:00 110-57-6 L1 1,1-Dichloroethane ND ug/L 5.0 0.32 1 06/04/17 15:00 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 06/04/17 15:00 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/04/17 15:00 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 06/04/17 15:00 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/04/17 15:00 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 06/04/17 15:00 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 Sample: MW-6 Lab ID: 92342784001 Collected: 06/01/17 15:00 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/04/17 15:00 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/17 15:00 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/17 15:00 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/04/17 15:00 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/17 15:00 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/17 15:00 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/17 15:00 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/04/17 15:00 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/17 15:00 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/17 15:00 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/17 15:00 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/17 15:00 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/17 15:00 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/17 15:00 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/17 15:00 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/17 15:00 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/17 15:00 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/17 15:00 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/17 15:00 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/17 15:00 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 103 % 70-130 1 06/04/17 15:00 460-00-4 1,2-Dichloroethane-d4 (S) 88 % 70-130 1 06/04/17 15:00 17060-07-0 Toluene-d8 (S) 110 % 70-130 1 06/04/17 15:00 2037-26-5 Date: 06/19/2017 12:26 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 Sample: MW-12D Lab ID: 92342784002 Collected: 06/01/17 09:35 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Antimony ND ug/L 6.0 3.9 1 06/04/17 16:40 06/14/17 22:34 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:34 7440-38-2 Barium 7.3J ug/L 100 2.5 1 06/04/17 16:40 06/14/17 22:34 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:34 7440-41-7 Cadmium 1.4 ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:34 7440-43-9 Chromium ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:34 7440-47-3 Cobalt ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:34 7440-48-4 Copper ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:34 7440-50-8 Lead ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:34 7439-92-1 Nickel ND ug/L 50.0 2.5 1 06/04/17 16:40 06/14/17 22:34 7440-02-0 Selenium ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:34 7782-49-2 Silver ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:34 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 06/04/17 16:40 06/14/17 22:34 7440-62-2 Zinc ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:34 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Thallium ND ug/L 5.5 0.020 1 06/06/17 02:45 06/09/17 20:28 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 06/04/17 15:18 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 06/04/17 15:18 107-13-1 Benzene ND ug/L 1.0 0.25 1 06/04/17 15:18 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 06/04/17 15:18 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 06/04/17 15:18 75-27-4 Bromoform ND ug/L 3.0 0.26 1 06/04/17 15:18 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 06/04/17 15:18 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 06/04/17 15:18 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 06/04/17 15:18 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 06/04/17 15:18 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 06/04/17 15:18 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 06/04/17 15:18 75-00-3 Chloroform ND ug/L 5.0 0.14 1 06/04/17 15:18 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 06/04/17 15:18 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 06/04/17 15:18 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 06/04/17 15:18 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 06/04/17 15:18 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 06/04/17 15:18 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 06/04/17 15:18 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 06/04/17 15:18 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/04/17 15:18 110-57-6 L1 1,1-Dichloroethane ND ug/L 5.0 0.32 1 06/04/17 15:18 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 06/04/17 15:18 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/04/17 15:18 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 06/04/17 15:18 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/04/17 15:18 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 06/04/17 15:18 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 Sample: MW-12D Lab ID: 92342784002 Collected: 06/01/17 09:35 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/04/17 15:18 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/17 15:18 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/17 15:18 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/04/17 15:18 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/17 15:18 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/17 15:18 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/17 15:18 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/04/17 15:18 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/17 15:18 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/17 15:18 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/17 15:18 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/17 15:18 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/17 15:18 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/17 15:18 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/17 15:18 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/17 15:18 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/17 15:18 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/17 15:18 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/17 15:18 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/17 15:18 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 06/04/17 15:18 460-00-4 1,2-Dichloroethane-d4 (S) 92 % 70-130 1 06/04/17 15:18 17060-07-0 Toluene-d8 (S) 109 % 70-130 1 06/04/17 15:18 2037-26-5 Date: 06/19/2017 12:26 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 Sample: MW-11 Lab ID: 92342784003 Collected: 06/01/17 12:02 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 Organochlorine Pesticides Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Surrogates Decachlorobiphenyl (S) 8151 Chlorinated Herbicides 2,4-D Dinoseb Pentachlorophenol 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 6010 MET ICP Antimony Arsenic Date: 06/19/2017 12:26 PM Analytical Method: EPA 8081 Preparation Method: EPA 3510 ND ug/L 0.050 0.050 1 06/05/1717:30 06/06/1712:16 309-00-2 ND ug/L 0.050 0.050 1 06/05/1717:30 06/06/1712:16 319-84-6 ND ug/L 0.050 0.050 1 06/05/1717:30 06/06/1712:16 319-85-7 ND ug/L 0.050 0.050 1 06/05/1717:30 06/06/1712:16 319-86-8 ND ug/L 0.050 0.050 1 06/05/1717:30 06/06/1712:16 58-89-9 ND ug/L 0.50 0.20 1 06/05/1717:30 06/06/1712:16 57-74-9 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1712:16 72-54-8 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1712:16 72-55-9 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1712:16 50-29-3 ND ug/L 0.075 0.050 1 06/05/1717:30 06/06/1712:16 60-57-1 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1712:16 959-98-8 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1712:16 33213-65-9 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1712:16 1031-07-8 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1712:16 72-20-8 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1712:16 7421-93-4 ND ug/L 0.050 0.050 1 06/05/1717:30 06/06/1712:16 76-44-8 ND ug/L 0.075 0.050 1 06/05/1717:30 06/06/1712:16 1024-57-3 ND ug/L 1.0 0.15 1 06/05/1717:30 06/06/1712:16 72-43-5 ND ug/L 1.5 0.20 1 06/05/1717:30 06/06/1712:16 8001-35-2 99 % 20-130 1 06/05/1717:30 06/06/1712:16 877-09-8 63 % 20-130 1 06/05/1717:30 06/06/1712:16 2051-24-3 Analytical Method: EPA 8082 Preparation Method: EPA 3510 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1718:47 12674-11-2 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1718:47 11104-28-2 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1718:47 11141-16-5 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1718:47 53469-21-9 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1718:47 12672-29-6 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1718:47 11097-69-1 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1718:47 11096-82-5 56 % 10-132 1 06/05/1717:30 06/06/1718:47 2051-24-3 Analytical Method: EPA 8151 Preparation Method: EPA 8151 ND ug/L 0.97 0.23 1 06/07/17 16:00 06/10/17 05:36 94-75-7 ND ug/L 0.20 0.059 1 06/07/17 16:00 06/10/17 05:36 88-85-7 ND ug/L 0.029 0.018 1 06/07/17 16:00 06/10/17 05:36 87-86-5 ND ug/L 0.20 0.044 1 06/07/17 16:00 06/10/17 05:36 93-76-5 ND ug/L 0.20 0.051 1 06/07/17 16:00 06/10/17 05:36 93-72-1 86 % 39-139 1 06/07/17 16:00 06/10/17 05:36 19719-28-9 Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 06/04/17 16:40 06/14/17 22:37 7440-36-0 ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:37 7440-38-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 9 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 Sample: MW-11 Lab ID: 92342784003 Collected: 06/01/17 12:02 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Tin Vanadium Zinc 6020 MET ICPMS Thallium 7470 Mercury Mercury 8270 MSSV Semivolatile Organic Acenaphthene Acenaphthylene Acetophenone 2-Acetylaminofluorene 4-Aminobiphenyl Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-ChIoro-3-methyl phenol 4-Chloroaniline Chlorobenzilate bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Diallate Dibenz(a,h)anthracene Date: 06/19/2017 12:26 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010A 40.7J ug/L 100 2.5 1 06/04/17 16:40 06/14/17 22:37 7440-39-3 ND ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:37 7440-41-7 1.3 ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:37 7440-43-9 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:37 7440-47-3 11.7 ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:37 7440-48-4 2.7J ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:37 7440-50-8 2.6J ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:37 7439-92-1 2.7J ug/L 50.0 2.5 1 06/04/17 16:40 06/14/17 22:37 7440-02-0 ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:37 7782-49-2 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:37 7440-22-4 ND ug/L 100 2.5 1 06/04/17 16:40 06/14/17 22:37 7440-31-5 ND ug/L 25.0 2.5 1 06/04/17 16:40 06/14/17 22:37 7440-62-2 19.4 ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:37 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3010A 0.061J ug/L 5.5 0.020 1 06/03/17 02:25 06/09/17 16:26 7440-28-0 Analytical Method: EPA 7470 Preparation Method: EPA 7470 ND ug/L 0.20 0.10 1 06/04/17 20:45 06/07/17 03:12 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1718:56 83-32-9 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1718:56 208-96-8 ND ug/L 10.0 1.9 1 06/07/1717:10 06/14/1718:56 98-86-2 ND ug/L 20.0 1.6 1 06/07/1717:10 06/14/1718:56 53-96-3 ND ug/L 20.0 1.7 1 06/07/1717:10 06/14/1718:56 92-67-1 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1718:56 120-12-7 ND ug/L 10.0 2.1 1 06/07/1717:10 06/14/1718:56 56-55-3 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1718:56 50-32-8 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1718:56 205-99-2 ND ug/L 10.0 2.1 1 06/07/1717:10 06/14/1718:56 191-24-2 ND ug/L 10.0 2.0 1 06/07/1717:10 06/14/1718:56 207-08-9 ND ug/L 20.0 3.1 1 06/07/1717:10 06/14/1718:56 100-51-6 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1718:56 101-55-3 ND ug/L 10.0 2.5 1 06/07/1717:10 06/14/1718:56 85-68-7 ND ug/L 20.0 2.8 1 06/07/1717:10 06/14/1718:56 59-50-7 ND ug/L 20.0 2.8 1 06/07/1717:10 06/14/1718:56 106-47-8 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1718:56 510-15-6 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1718:56 111-91-1 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1718:56 111-44-4 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1718:56 91-58-7 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1718:56 95-57-8 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1718:56 7005-72-3 ND ug/L 10.0 2.1 1 06/07/1717:10 06/14/1718:56 218-01-9 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1718:56 2303-16-4 ND ug/L 10.0 2.0 1 06/07/1717:10 06/14/1718:56 53-70-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. L2 Page 10 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 Sample: MW-11 Lab ID: 92342784003 Collected: 06/01/17 12:02 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Dibenzofuran ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 18:56 132-64-9 3,3'-Dichlorobenzidine ND ug/L 20.0 3.9 1 06/07/17 17:10 06/14/17 18:56 91-94-1 2,4-Dichlorophenol ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 18:56 120-83-2 2,6-Dichlorophenol ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 18:56 87-65-0 Diethylphthalate ND ug/L 6000 1.6 1 06/07/17 17:10 06/14/17 18:56 84-66-2 Dimethoate ND ug/L 20.0 1.8 1 06/07/17 17:10 06/14/17 18:56 60-51-5 P-Dimethylaminoazobenzene ND ug/L 10.0 1.0 1 06/07/17 17:10 06/14/17 18:56 60-11-7 7,12-Dimethylbenz(a)anthracene ND ug/L 10.0 2.4 1 06/07/17 17:10 06/14/17 18:56 57-97-6 3,3'-Dimethylbenzidine ND ug/L 10.0 3.9 1 06/07/17 17:10 06/14/17 18:56 119-93-7 2,4-Dimethylphenol ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 18:56 105-67-9 Dimethylphthalate ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 18:56 131-11-3 Di-n-butylphthalate ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 18:56 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 50.0 2.2 1 06/07/17 17:10 06/14/17 18:56 534-52-1 1,3-Dinitrobenzene ND ug/L 20.0 1.3 1 06/07/17 17:10 06/14/17 18:56 99-65-0 2,4-Dinitrophenol ND ug/L 50.0 5.1 1 06/07/17 17:10 06/14/17 18:56 51-28-5 2,4-Dinitrotoluene ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 18:56 121-14-2 2,6-Dinitrotoluene ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 18:56 606-20-2 Di-n-octylphthalate ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 18:56 117-84-0 Diphenylamine ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 18:56 122-39-4 Disulfoton ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 18:56 298-04-4 bis(2- Ethyl hexyl)phthalate ND ug/L 15.0 2.3 1 06/07/17 17:10 06/14/17 18:56 117-81-7 Ethyl methanesulfonate ND ug/L 20.0 1.6 1 06/07/17 17:10 06/14/17 18:56 62-50-0 Famphur ND ug/L 20.0 5.7 1 06/07/17 17:10 06/14/17 18:56 52-85-7 Fluoranthene ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 18:56 206-44-0 Fluorene ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 18:56 86-73-7 Hexachlorobenzene ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 18:56 118-74-1 Hexachlorocyclopentadiene ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 18:56 77-47-4 Hexachloroethane ND ug/L 10.0 1.8 1 06/07/17 17:10 06/14/17 18:56 67-72-1 Hexachloropropene ND ug/L 10.0 1.2 1 06/07/17 17:10 06/14/17 18:56 1888-71-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 18:56 193-39-5 Isodrin ND ug/L 20.0 2.5 1 06/07/17 17:10 06/14/17 18:56 465-73-6 Isophorone ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 18:56 78-59-1 Isosafrole ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 18:56 120-58-1 Kepone ND ug/L 20.0 4.5 1 06/07/17 17:10 06/14/17 18:56 143-50-0 Methapyrilene ND ug/L 100 3.0 1 06/07/17 17:10 06/14/17 18:56 91-80-5 3-Methylcholanthrene ND ug/L 10.0 2.7 1 06/07/17 17:10 06/14/17 18:56 56-49-5 Methyl methanesulfonate ND ug/L 10.0 1.1 1 06/07/17 17:10 06/14/17 18:56 66-27-3 2-Methylnaphthalene ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 18:56 91-57-6 Methyl parathion ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 18:56 298-00-0 2-Methylphenol(o-Cresol) ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 18:56 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 18:56 15831-10-4 1-Naphthalenamine ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 18:56 134-32-7 2-Naphthalenamine ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 18:56 91-59-8 1,4-Naphthoquinone ND ug/L 10.0 0.99 1 06/07/17 17:10 06/14/17 18:56 130-15-4 2-Nitroaniline ND ug/L 50.0 2.3 1 06/07/17 17:10 06/14/17 18:56 88-74-4 3-Nitroaniline ND ug/L 50.0 2.7 1 06/07/17 17:10 06/14/17 18:56 99-09-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 Sample: MW-11 Lab ID: 92342784003 Collected: 06/01/17 12:02 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 4-Nitroaniline ND ug/L 20.0 3.4 1 06/07/17 17:10 06/14/17 18:56 100-01-6 Nitrobenzene ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 18:56 98-95-3 2-Nitrophenol ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 18:56 88-75-5 4-Nitrophenol ND ug/L 50.0 4.3 1 06/07/17 17:10 06/14/17 18:56 100-02-7 5-Nitro-o-toluidine ND ug/L 10.0 1.9 1 06/07/17 17:10 06/14/17 18:56 99-55-8 N-Nitrosodiethylamine ND ug/L 20.0 1.4 1 06/07/17 17:10 06/14/17 18:56 55-18-5 N-Nitrosodimethylamine ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 18:56 62-75-9 N-Nitroso-di-n-butylamine ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 18:56 924-16-3 N-Nitroso-di-n-propylamine ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 18:56 621-64-7 N-Nitrosodiphenylamine ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 18:56 86-30-6 N-Nitrosomethylethylamine ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 18:56 10595-95-6 N-Nitrosopiperidine ND ug/L 20.0 1.7 1 06/07/17 17:10 06/14/17 18:56 100-75-4 N-Nitrosopyrrolidine ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 18:56 930-55-2 O,O,O-Triethylphosphorothioate ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 18:56 126-68-1 2,2'-Oxybis(1-chloropropane) ND ug/L 10.0 1.8 1 06/07/17 17:10 06/14/17 18:56 108-60-1 Parathion (Ethyl parathion) ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 18:56 56-38-2 Pentachlorobenzene ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 18:56 608-93-5 Pentachloronitrobenzene ND ug/L 20.0 1.7 1 06/07/17 17:10 06/14/17 18:56 82-68-8 Pentachlorophenol ND ug/L 25.0 3.5 1 06/07/17 17:10 06/14/17 18:56 87-86-5 Phenacetin ND ug/L 20.0 1.9 1 06/07/17 17:10 06/14/17 18:56 62-44-2 Phenanthrene ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 18:56 85-01-8 Phenol ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 18:56 108-95-2 p-Phenylenediamine ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 18:56 106-50-3 Phorate ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 18:56 298-02-2 Pronamide ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 18:56 23950-58-5 Pyrene ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 18:56 129-00-0 Safrole ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 18:56 94-59-7 1,2,4,5-Tetrachlorobenzene ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 18:56 95-94-3 2,3,4,6-Tetrachlorophenol ND ug/L 10.0 2.9 1 06/07/17 17:10 06/14/17 18:56 58-90-2 Thionazin ND ug/L 20.0 1.7 1 06/07/17 17:10 06/14/17 18:56 297-97-2 O-Toluidine ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 18:56 95-53-4 2,4,5-Trichlorophenol ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 18:56 95-95-4 2,4,6-Trichlorophenol ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 18:56 88-06-2 1,3,5-Trinitrobenzene ND ug/L 10.0 1.2 1 06/07/17 17:10 06/14/17 18:56 99-35-4 Surrogates Nitrobenzene-d5 (S) 67 % 21-110 1 06/07/17 17:10 06/14/17 18:56 4165-60-0 2-Fluorobiphenyl (S) 82 % 27-110 1 06/07/17 17:10 06/14/17 18:56 321-60-8 Terphenyl-d14 (S) 75 % 31-107 1 06/07/17 17:10 06/14/17 18:56 1718-51-0 Phenol-d6 (S) 22 % 10-110 1 06/07/17 17:10 06/14/17 18:56 13127-88-3 2-Fluorophenol (S) 36 % 12-110 1 06/07/17 17:10 06/14/17 18:56 367-12-4 2,4,6-Tribromophenol (S) 78 % 27-110 1 06/07/17 17:10 06/14/17 18:56 118-79-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 21.4J ug/L 100 10.0 1 06/04/1715:36 67-64-1 Acetonitrile ND ug/L 55.0 2.2 1 06/04/1715:36 75-05-8 Acrolein ND ug/L 53.0 1.6 1 06/04/1715:36 107-02-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 Sample: MW-11 Lab ID: 92342784003 Collected: 06/01/17 12:02 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Acrylonitrile Allyl chloride Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane Chloroprene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene 2-Hexanone lodomethane Isobutanol Methacrylonitrile Methylene Chloride Methyl methacrylate 4-Methyl-2-pentanone (MIBK) Naphthalene Date: 06/19/2017 12:26 PM Analytical Method: EPA 8260 ND ug/L 200 1.9 1 06/04/1715:36 107-13-1 8.2J ug/L 10.0 1.5 1 06/04/1715:36 107-05-1 0.62J ug/L 1.0 0.25 1 06/04/1715:36 71-43-2 ND ug/L 3.0 0.17 1 06/04/1715:36 74-97-5 ND ug/L 1.0 0.18 1 06/04/1715:36 75-27-4 ND ug/L 3.0 0.26 1 06/04/1715:36 75-25-2 ND ug/L 10.0 0.29 1 06/04/1715:36 74-83-9 ND ug/L 100 0.96 1 06/04/1715:36 78-93-3 ND ug/L 100 1.2 1 06/04/1715:36 75-15-0 ND ug/L 1.0 0.25 1 06/04/1715:36 56-23-5 0.87J ug/L 3.0 0.23 1 06/04/1715:36 108-90-7 ND ug/L 10.0 0.54 1 06/04/1715:36 75-00-3 ND ug/L 5.0 0.14 1 06/04/1715:36 67-66-3 ND ug/L 1.0 0.11 1 06/04/1715:36 74-87-3 ND ug/L 20.0 0.27 1 06/04/1715:36 126-99-8 ND ug/L 13.0 2.0 1 06/04/1715:36 96-12-8 ND ug/L 3.0 0.21 1 06/04/1715:36 124-48-1 ND ug/L 1.0 0.27 1 06/04/1715:36 106-93-4 ND ug/L 10.0 0.21 1 06/04/1715:36 74-95-3 ND ug/L 5.0 0.30 1 06/04/1715:36 95-50-1 ND ug/L 5.0 0.24 1 06/04/1715:36 541-73-1 2.5 ug/L 1.0 0.33 1 06/04/1715:36 106-46-7 ND ug/L 100 1.0 1 06/04/1715:36 110-57-6 ND ug/L 5.0 0.21 1 06/04/1715:36 75-71-8 0.37J ug/L 5.0 0.32 1 06/04/1715:36 75-34-3 ND ug/L 1.0 0.24 1 06/04/1715:36 107-06-2 ND ug/L 5.0 0.56 1 06/04/1715:36 75-35-4 1.0J ug/L 5.0 0.19 1 06/04/1715:36 156-59-2 ND ug/L 5.0 0.49 1 06/04/1715:36 156-60-5 ND ug/L 1.0 0.27 1 06/04/1715:36 78-87-5 ND ug/L 1.0 0.28 1 06/04/1715:36 142-28-9 ND ug/L 15.0 0.13 1 06/04/1715:36 594-20-7 ND ug/L 5.0 0.49 1 06/04/1715:36 563-58-6 ND ug/L 1.0 0.13 1 06/04/1715:36 10061-01-5 ND ug/L 1.0 0.26 1 06/04/1715:36 10061-02-6 ND ug/L 1.0 0.30 1 06/04/1715:36 100-41-4 ND ug/L 10.0 0.20 1 06/04/1715:36 97-63-2 ND ug/L 10.0 0.71 1 06/04/1715:36 87-68-3 ND ug/L 50.0 0.46 1 06/04/1715:36 591-78-6 ND ug/L 10.0 0.32 1 06/04/1715:36 74-88-4 ND ug/L 100 35.0 1 06/04/1715:36 78-83-1 ND ug/L 100 0.93 1 06/04/1715:36 126-98-7 ND ug/L 1.0 0.97 1 06/04/1715:36 75-09-2 ND ug/L 30.0 2.0 1 06/04/1715:36 80-62-6 ND ug/L 100 0.33 1 06/04/1715:36 108-10-1 ND ug/L 10.0 0.24 1 06/04/1715:36 91-20-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. L1 Page 13 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 Sample: MW-11 Lab ID: 92342784003 Collected: 06/01/17 12:02 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Propionitrile ND ug/L 150 3.6 1 06/04/17 15:36 107-12-0 Styrene ND ug/L 1.0 0.26 1 06/04/17 15:36 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/17 15:36 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/17 15:36 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/17 15:36 127-18-4 Toluene 0.881 ug/L 1.0 0.26 1 06/04/17 15:36 108-88-3 1,2,4-Trichlorobenzene ND ug/L 10.0 0.35 1 06/04/17 15:36 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/17 15:36 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/17 15:36 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/17 15:36 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/17 15:36 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/17 15:36 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/17 15:36 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/17 15:36 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/17 15:36 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 06/04/17 15:36 460-00-4 1,2-Dichloroethane-d4 (S) 90 % 70-130 1 06/04/17 15:36 17060-07-0 Toluene-d8 (S) 108 % 70-130 1 06/04/17 15:36 2037-26-5 4500S2D Sulfide Water Analytical Method: SM 4500-S2D Sulfide ND ug/L 1000 100 1 06/06/17 21:30 18496-25-8 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E Cyanide ND ug/L 10.0 4.0 1 06/14/1711:46 57-12-5 Date: 06/19/2017 12:26 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 14 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 Sample: SCALE HOUSE Lab ID: 92342784004 Collected: 06/01/17 16:22 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 Organochlorine Pesticides Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Surrogates Decachlorobiphenyl (S) 8151 Chlorinated Herbicides 2,4-D Dinoseb Pentachlorophenol 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 6010 MET ICP Antimony Arsenic Date: 06/19/2017 12:26 PM Analytical Method: EPA 8081 Preparation Method: EPA 3510 ND ug/L 0.050 0.050 1 06/05/1717:30 06/06/1712:34 309-00-2 ND ug/L 0.050 0.050 1 06/05/1717:30 06/06/1712:34 319-84-6 ND ug/L 0.050 0.050 1 06/05/1717:30 06/06/1712:34 319-85-7 ND ug/L 0.050 0.050 1 06/05/1717:30 06/06/1712:34 319-86-8 ND ug/L 0.050 0.050 1 06/05/1717:30 06/06/1712:34 58-89-9 ND ug/L 0.50 0.20 1 06/05/1717:30 06/06/1712:34 57-74-9 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1712:34 72-54-8 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1712:34 72-55-9 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1712:34 50-29-3 ND ug/L 0.075 0.050 1 06/05/1717:30 06/06/1712:34 60-57-1 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1712:34 959-98-8 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1712:34 33213-65-9 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1712:34 1031-07-8 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1712:34 72-20-8 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1712:34 7421-93-4 ND ug/L 0.050 0.050 1 06/05/1717:30 06/06/1712:34 76-44-8 ND ug/L 0.075 0.050 1 06/05/1717:30 06/06/1712:34 1024-57-3 ND ug/L 1.0 0.15 1 06/05/1717:30 06/06/1712:34 72-43-5 ND ug/L 1.5 0.20 1 06/05/1717:30 06/06/1712:34 8001-35-2 76 % 20-130 1 06/05/1717:30 06/06/1712:34 877-09-8 82 % 20-130 1 06/05/1717:30 06/06/1712:34 2051-24-3 Analytical Method: EPA 8082 Preparation Method: EPA 3510 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1719:08 12674-11-2 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1719:08 11104-28-2 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1719:08 11141-16-5 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1719:08 53469-21-9 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1719:08 12672-29-6 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1719:08 11097-69-1 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1719:08 11096-82-5 78 % 10-132 1 06/05/1717:30 06/06/1719:08 2051-24-3 Analytical Method: EPA 8151 Preparation Method: EPA 8151 ND ug/L 0.98 0.23 1 06/07/17 16:00 06/10/17 06:06 94-75-7 ND ug/L 0.20 0.059 1 06/07/17 16:00 06/10/17 06:06 88-85-7 ND ug/L 0.030 0.018 1 06/07/17 16:00 06/10/17 06:06 87-86-5 ND ug/L 0.20 0.044 1 06/07/17 16:00 06/10/17 06:06 93-76-5 ND ug/L 0.20 0.051 1 06/07/17 16:00 06/10/17 06:06 93-72-1 90 % 39-139 1 06/07/17 16:00 06/10/17 06:06 19719-28-9 Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 06/04/17 16:40 06/14/17 22:40 7440-36-0 ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:40 7440-38-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 15 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 Sample: SCALE HOUSE Lab ID: 92342784004 Collected: 06/01/17 16:22 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Tin Vanadium Zinc 6020 MET ICPMS Thallium 7470 Mercury Mercury 8270 MSSV Semivolatile Organic Acenaphthene Acenaphthylene Acetophenone 2-Acetylaminofluorene 4-Aminobiphenyl Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-ChIoro-3-methyl phenol 4-Chloroaniline Chlorobenzilate bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Diallate Dibenz(a,h)anthracene Date: 06/19/2017 12:26 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010A 14.4J ug/L 100 2.5 1 06/04/17 16:40 06/14/17 22:40 7440-39-3 ND ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:40 7440-41-7 ND ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:40 7440-43-9 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:40 7440-47-3 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:40 7440-48-4 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:40 7440-50-8 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:40 7439-92-1 ND ug/L 50.0 2.5 1 06/04/17 16:40 06/14/17 22:40 7440-02-0 ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:40 7782-49-2 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:40 7440-22-4 ND ug/L 100 2.5 1 06/04/17 16:40 06/14/17 22:40 7440-31-5 ND ug/L 25.0 2.5 1 06/04/17 16:40 06/14/17 22:40 7440-62-2 16.0 ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:40 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3010A ND ug/L 5.5 0.020 1 06/03/17 02:25 06/09/17 16:28 7440-28-0 Analytical Method: EPA 7470 Preparation Method: EPA 7470 ND ug/L 0.20 0.10 1 06/04/17 20:45 06/07/17 03:14 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1719:25 83-32-9 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1719:25 208-96-8 ND ug/L 10.0 1.9 1 06/07/1717:10 06/14/1719:25 98-86-2 ND ug/L 20.0 1.6 1 06/07/1717:10 06/14/1719:25 53-96-3 ND ug/L 20.0 1.7 1 06/07/1717:10 06/14/1719:25 92-67-1 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1719:25 120-12-7 ND ug/L 10.0 2.1 1 06/07/1717:10 06/14/1719:25 56-55-3 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1719:25 50-32-8 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1719:25 205-99-2 ND ug/L 10.0 2.1 1 06/07/1717:10 06/14/1719:25 191-24-2 ND ug/L 10.0 2.0 1 06/07/1717:10 06/14/1719:25 207-08-9 ND ug/L 20.0 3.1 1 06/07/1717:10 06/14/1719:25 100-51-6 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1719:25 101-55-3 ND ug/L 10.0 2.5 1 06/07/1717:10 06/14/1719:25 85-68-7 ND ug/L 20.0 2.8 1 06/07/1717:10 06/14/1719:25 59-50-7 ND ug/L 20.0 2.8 1 06/07/1717:10 06/14/1719:25 106-47-8 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1719:25 510-15-6 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1719:25 111-91-1 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1719:25 111-44-4 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1719:25 91-58-7 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1719:25 95-57-8 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1719:25 7005-72-3 ND ug/L 10.0 2.1 1 06/07/1717:10 06/14/1719:25 218-01-9 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1719:25 2303-16-4 ND ug/L 10.0 2.0 1 06/07/1717:10 06/14/1719:25 53-70-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. L2 Page 16 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 Sample: SCALE HOUSE Lab ID: 92342784004 Collected: 06/01/17 16:22 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Dibenzofuran ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 19:25 132-64-9 3,3'-Dichlorobenzidine ND ug/L 20.0 3.9 1 06/07/17 17:10 06/14/17 19:25 91-94-1 2,4-Dichlorophenol ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 19:25 120-83-2 2,6-Dichlorophenol ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 19:25 87-65-0 Diethylphthalate ND ug/L 6000 1.6 1 06/07/17 17:10 06/14/17 19:25 84-66-2 Dimethoate ND ug/L 20.0 1.8 1 06/07/17 17:10 06/14/17 19:25 60-51-5 P-Dimethylaminoazobenzene ND ug/L 10.0 1.0 1 06/07/17 17:10 06/14/17 19:25 60-11-7 7,12-Dimethylbenz(a)anthracene ND ug/L 10.0 2.4 1 06/07/17 17:10 06/14/17 19:25 57-97-6 3,3'-Dimethylbenzidine ND ug/L 10.0 3.9 1 06/07/17 17:10 06/14/17 19:25 119-93-7 2,4-Dimethylphenol ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 19:25 105-67-9 Dimethylphthalate ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 19:25 131-11-3 Di-n-butylphthalate ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 19:25 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 50.0 2.2 1 06/07/17 17:10 06/14/17 19:25 534-52-1 1,3-Dinitrobenzene ND ug/L 20.0 1.3 1 06/07/17 17:10 06/14/17 19:25 99-65-0 2,4-Dinitrophenol ND ug/L 50.0 5.1 1 06/07/17 17:10 06/14/17 19:25 51-28-5 2,4-Dinitrotoluene ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 19:25 121-14-2 2,6-Dinitrotoluene ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 19:25 606-20-2 Di-n-octylphthalate ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 19:25 117-84-0 Diphenylamine ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 19:25 122-39-4 Disulfoton ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 19:25 298-04-4 bis(2- Ethyl hexyl)phthalate ND ug/L 15.0 2.3 1 06/07/17 17:10 06/14/17 19:25 117-81-7 Ethyl methanesulfonate ND ug/L 20.0 1.6 1 06/07/17 17:10 06/14/17 19:25 62-50-0 Famphur ND ug/L 20.0 5.7 1 06/07/17 17:10 06/14/17 19:25 52-85-7 Fluoranthene ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 19:25 206-44-0 Fluorene ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 19:25 86-73-7 Hexachlorobenzene ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 19:25 118-74-1 Hexachlorocyclopentadiene ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 19:25 77-47-4 Hexachloroethane ND ug/L 10.0 1.8 1 06/07/17 17:10 06/14/17 19:25 67-72-1 Hexachloropropene ND ug/L 10.0 1.2 1 06/07/17 17:10 06/14/17 19:25 1888-71-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 19:25 193-39-5 Isodrin ND ug/L 20.0 2.5 1 06/07/17 17:10 06/14/17 19:25 465-73-6 Isophorone ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 19:25 78-59-1 Isosafrole ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 19:25 120-58-1 Kepone ND ug/L 20.0 4.5 1 06/07/17 17:10 06/14/17 19:25 143-50-0 Methapyrilene ND ug/L 100 3.0 1 06/07/17 17:10 06/14/17 19:25 91-80-5 3-Methylcholanthrene ND ug/L 10.0 2.7 1 06/07/17 17:10 06/14/17 19:25 56-49-5 Methyl methanesulfonate ND ug/L 10.0 1.1 1 06/07/17 17:10 06/14/17 19:25 66-27-3 2-Methylnaphthalene ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 19:25 91-57-6 Methyl parathion ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 19:25 298-00-0 2-Methylphenol(o-Cresol) ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 19:25 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 19:25 15831-10-4 1-Naphthalenamine ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 19:25 134-32-7 2-Naphthalenamine ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 19:25 91-59-8 1,4-Naphthoquinone ND ug/L 10.0 0.99 1 06/07/17 17:10 06/14/17 19:25 130-15-4 2-Nitroaniline ND ug/L 50.0 2.3 1 06/07/17 17:10 06/14/17 19:25 88-74-4 3-Nitroaniline ND ug/L 50.0 2.7 1 06/07/17 17:10 06/14/17 19:25 99-09-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 Sample: SCALE HOUSE Lab ID: 92342784004 Collected: 06/01/17 16:22 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol 5-Nitro-o-toluidine N-Nitrosodiethylamine N-Nitrosodimethylamine N-Nitroso-di-n-butylamine N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine N-Nitrosomethylethylamine N-Nitrosopiperidine N-Nitrosopyrrolidine O,O,O-Triethylphosphorothioate 2,2'-Oxybis(1-chloropropane) Parathion (Ethyl parathion) Pentachlorobenzene Pentachloronitrobenzene Pentachlorophenol Phenacetin Phenanthrene Phenol p-Phenylenediamine Phorate Pronamide Pyrene Safrole 1,2,4,5-Tetrachlorobenzene 2,3,4,6-Tetrachlorophenol Thionazin O-Toluidine 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 1,3,5-Trinitrobenzene Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) 8260 MSV Low Level Landfill Acetone Acetonitrile Acrolein Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ug/L 20.0 3.4 1 06/07/1717:10 06/14/1719:25 100-01-6 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1719:25 98-95-3 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1719:25 88-75-5 ND ug/L 50.0 4.3 1 06/07/1717:10 06/14/1719:25 100-02-7 ND ug/L 10.0 1.9 1 06/07/1717:10 06/14/1719:25 99-55-8 ND ug/L 20.0 1.4 1 06/07/1717:10 06/14/1719:25 55-18-5 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1719:25 62-75-9 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1719:25 924-16-3 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1719:25 621-64-7 ND ug/L 10.0 1.4 1 06/07/1717:10 06/14/1719:25 86-30-6 ND ug/L 10.0 1.4 1 06/07/1717:10 06/14/1719:25 10595-95-6 ND ug/L 20.0 1.7 1 06/07/1717:10 06/14/1719:25 100-75-4 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1719:25 930-55-2 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1719:25 126-68-1 ND ug/L 10.0 1.8 1 06/07/1717:10 06/14/1719:25 108-60-1 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1719:25 56-38-2 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1719:25 608-93-5 ND ug/L 20.0 1.7 1 06/07/1717:10 06/14/1719:25 82-68-8 ND ug/L 25.0 3.5 1 06/07/1717:10 06/14/1719:25 87-86-5 ND ug/L 20.0 1.9 1 06/07/1717:10 06/14/1719:25 62-44-2 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1719:25 85-01-8 ND ug/L 10.0 1.3 1 06/07/1717:10 06/14/1719:25 108-95-2 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1719:25 106-50-3 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1719:25 298-02-2 ND ug/L 10.0 2.0 1 06/07/1717:10 06/14/1719:25 23950-58-5 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1719:25 129-00-0 ND ug/L 10.0 1.3 1 06/07/1717:10 06/14/1719:25 94-59-7 ND ug/L 10.0 1.3 1 06/07/1717:10 06/14/1719:25 95-94-3 ND ug/L 10.0 2.9 1 06/07/1717:10 06/14/1719:25 58-90-2 ND ug/L 20.0 1.7 1 06/07/1717:10 06/14/1719:25 297-97-2 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1719:25 95-53-4 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1719:25 95-95-4 ND ug/L 10.0 1.4 1 06/07/1717:10 06/14/1719:25 88-06-2 ND ug/L 10.0 1.2 1 06/07/1717:10 06/14/1719:25 99-35-4 82 % 21-110 1 06/07/1717:10 06/14/1719:25 4165-60-0 97 % 27-110 1 06/07/1717:10 06/14/1719:25 321-60-8 89 % 31-107 1 06/07/1717:10 06/14/1719:25 1718-51-0 28 % 10-110 1 06/07/1717:10 06/14/1719:25 13127-88-3 43 % 12-110 1 06/07/1717:10 06/14/1719:25 367-12-4 90 % 27-110 1 06/07/1717:10 06/14/1719:25 118-79-6 Analytical Method: EPA 8260 12.9J ug/L 100 10.0 1 06/04/1715:53 67-64-1 ND ug/L 55.0 2.2 1 06/04/1715:53 75-05-8 ND ug/L 53.0 1.6 1 06/04/1715:53 107-02-8 REPORT OF LABORATORY ANALYSIS M1 This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 Sample: SCALE HOUSE Lab ID: 92342784004 Collected: 06/01/17 16:22 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Acrylonitrile Allyl chloride Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane Chloroprene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene 2-Hexanone lodomethane Isobutanol Methacrylonitrile Methylene Chloride Methyl methacrylate 4-Methyl-2-pentanone (MIBK) Naphthalene Date: 06/19/2017 12:26 PM Analytical Method: EPA 8260 ND ug/L 200 1.9 1 06/04/1715:53 107-13-1 4.1J ug/L 10.0 1.5 1 06/04/1715:53 107-05-1 ND ug/L 1.0 0.25 1 06/04/1715:53 71-43-2 ND ug/L 3.0 0.17 1 06/04/1715:53 74-97-5 ND ug/L 1.0 0.18 1 06/04/1715:53 75-27-4 ND ug/L 3.0 0.26 1 06/04/1715:53 75-25-2 ND ug/L 10.0 0.29 1 06/04/1715:53 74-83-9 ND ug/L 100 0.96 1 06/04/1715:53 78-93-3 ND ug/L 100 1.2 1 06/04/1715:53 75-15-0 ND ug/L 1.0 0.25 1 06/04/1715:53 56-23-5 ND ug/L 3.0 0.23 1 06/04/1715:53 108-90-7 ND ug/L 10.0 0.54 1 06/04/1715:53 75-00-3 ND ug/L 5.0 0.14 1 06/04/1715:53 67-66-3 0.14J ug/L 1.0 0.11 1 06/04/1715:53 74-87-3 ND ug/L 20.0 0.27 1 06/04/1715:53 126-99-8 ND ug/L 13.0 2.0 1 06/04/1715:53 96-12-8 ND ug/L 3.0 0.21 1 06/04/1715:53 124-48-1 ND ug/L 1.0 0.27 1 06/04/1715:53 106-93-4 ND ug/L 10.0 0.21 1 06/04/1715:53 74-95-3 ND ug/L 5.0 0.30 1 06/04/1715:53 95-50-1 ND ug/L 5.0 0.24 1 06/04/1715:53 541-73-1 ND ug/L 1.0 0.33 1 06/04/1715:53 106-46-7 ND ug/L 100 1.0 1 06/04/1715:53 110-57-6 ND ug/L 5.0 0.21 1 06/04/1715:53 75-71-8 ND ug/L 5.0 0.32 1 06/04/1715:53 75-34-3 ND ug/L 1.0 0.24 1 06/04/1715:53 107-06-2 ND ug/L 5.0 0.56 1 06/04/1715:53 75-35-4 0.22J ug/L 5.0 0.19 1 06/04/1715:53 156-59-2 ND ug/L 5.0 0.49 1 06/04/1715:53 156-60-5 ND ug/L 1.0 0.27 1 06/04/1715:53 78-87-5 ND ug/L 1.0 0.28 1 06/04/1715:53 142-28-9 ND ug/L 15.0 0.13 1 06/04/1715:53 594-20-7 ND ug/L 5.0 0.49 1 06/04/1715:53 563-58-6 ND ug/L 1.0 0.13 1 06/04/1715:53 10061-01-5 ND ug/L 1.0 0.26 1 06/04/1715:53 10061-02-6 ND ug/L 1.0 0.30 1 06/04/1715:53 100-41-4 ND ug/L 10.0 0.20 1 06/04/1715:53 97-63-2 ND ug/L 10.0 0.71 1 06/04/1715:53 87-68-3 ND ug/L 50.0 0.46 1 06/04/1715:53 591-78-6 ND ug/L 10.0 0.32 1 06/04/1715:53 74-88-4 ND ug/L 100 35.0 1 06/04/1715:53 78-83-1 ND ug/L 100 0.93 1 06/04/1715:53 126-98-7 ND ug/L 1.0 0.97 1 06/04/1715:53 75-09-2 ND ug/L 30.0 2.0 1 06/04/1715:53 80-62-6 ND ug/L 100 0.33 1 06/04/1715:53 108-10-1 ND ug/L 10.0 0.24 1 06/04/1715:53 91-20-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. L1 Page 19 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 Sample: SCALE HOUSE Lab ID: 92342784004 Collected: 06/01/17 16:22 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Propionitrile ND ug/L 150 3.6 1 06/04/17 15:53 107-12-0 Styrene ND ug/L 1.0 0.26 1 06/04/17 15:53 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/17 15:53 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/17 15:53 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/17 15:53 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/17 15:53 108-88-3 1,2,4-Trichlorobenzene ND ug/L 10.0 0.35 1 06/04/17 15:53 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/17 15:53 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/17 15:53 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/17 15:53 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/17 15:53 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/17 15:53 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/17 15:53 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/17 15:53 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/17 15:53 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 101 % 70-130 1 06/04/17 15:53 460-00-4 1,2-Dichloroethane-d4 (S) 88 % 70-130 1 06/04/17 15:53 17060-07-0 Toluene-d8 (S) 108 % 70-130 1 06/04/17 15:53 2037-26-5 4500S2D Sulfide Water Analytical Method: SM 4500-S2D Sulfide ND ug/L 1000 100 1 06/06/17 21:30 18496-25-8 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E Cyanide ND ug/L 10.0 4.0 1 06/14/1711:47 57-12-5 Date: 06/19/2017 12:26 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 20 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 QC Batch: 363333 Analysis Method: EPA 7470 QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury Associated Lab Samples: 92342784003, 92342784004 METHOD BLANK: 2014275 Matrix: Water Associated Lab Samples: 92342784003, 92342784004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Mercury ug/L ND 0.20 0.10 06/07/17 02:15 LABORATORY CONTROL SAMPLE: 2014276 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.3 93 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2014277 2014278 MS MSD 92342769001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Mercury ug/L ND 125 125 ND ND 0 0 75-125 25 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 QC Batch: 363321 Analysis Method: EPA 6010 QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92342784001, 92342784002, 92342784003, 92342784004 METHOD BLANK: 2014222 Matrix: Water Associated Lab Samples: 92342784001, 92342784002, 92342784003, 92342784004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Antimony ug/L ND 5.0 3.9 06/14/17 21:19 Arsenic ug/L ND 10.0 5.0 06/14/17 21:19 Barium ug/L ND 5.0 2.5 06/14/17 21:19 Beryllium ug/L ND 1.0 0.50 06/14/17 21:19 Cadmium ug/L ND 1.0 0.50 06/14/17 21:19 Chromium ug/L ND 5.0 2.5 06/14/17 21:19 Cobalt ug/L ND 5.0 2.5 06/14/17 21:19 Copper ug/L ND 5.0 2.5 06/14/17 21:19 Lead ug/L ND 5.0 2.5 06/14/17 21:19 Nickel ug/L ND 5.0 2.5 06/14/17 21:19 Selenium ug/L ND 10.0 5.0 06/14/17 21:19 Silver ug/L ND 5.0 2.5 06/14/17 21:19 Tin ug/L ND 5.0 2.5 06/14/17 21:19 Vanadium ug/L ND 5.0 2.5 06/14/17 21:19 Zinc ug/L ND 10.0 5.0 06/14/17 21:19 LABORATORY CONTROL SAMPLE: 2014223 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Antimony ug/L 500 496 99 80-120 Arsenic ug/L 500 475 95 80-120 Barium ug/L 500 511 102 80-120 Beryllium ug/L 500 457 91 80-120 Cadmium ug/L 500 512 102 80-120 Chromium ug/L 500 463 93 80-120 Cobalt ug/L 500 498 100 80-120 Copper ug/L 500 494 99 80-120 Lead ug/L 500 486 97 80-120 Nickel ug/L 500 463 93 80-120 Selenium ug/L 500 501 100 80-120 Silver ug/L 250 235 94 80-120 Tin ug/L 500 485 97 80-120 Vanadium ug/L 500 456 91 80-120 Zinc ug/L 500 472 94 80-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: SURRY CLOSED -MT. 92342784 AIRY (AM) MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2014224 2014225 MS MSD 92342605016 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 517 501 103 100 75-125 3 20 Arsenic ug/L 174 500 500 672 657 100 97 75-125 2 20 Barium ug/L 8.0 500 500 546 530 108 104 75-125 3 20 Beryllium ug/L 0.73J 500 500 481 471 96 94 75-125 2 20 Cadmium ug/L 1.7 500 500 540 524 108 105 75-125 3 20 Chromium ug/L ND 500 500 486 470 97 94 75-125 3 20 Cobalt ug/L 75.0 500 500 594 577 104 100 75-125 3 20 Copper ug/L ND 500 500 522 509 104 102 75-125 3 20 Lead ug/L 4AJ 500 500 506 491 100 97 75-125 3 20 Nickel ug/L 3.2J 500 500 481 466 96 93 75-125 3 20 Selenium ug/L ND 500 500 511 501 102 100 75-125 2 20 Silver ug/L ND 250 250 246 238 99 95 75-125 4 20 Tin ug/L ND 500 500 503 484 101 97 75-125 4 20 Vanadium ug/L ND 500 500 482 466 96 93 75-125 3 20 Zinc ug/L 5.8J 500 500 495 479 98 95 75-125 3 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 QC Batch: 363273 Analysis Method: EPA 6020B QC Batch Method: EPA 3010A Analysis Description: 6020 MET Associated Lab Samples: 92342784003, 92342784004 METHOD BLANK: 2014038 Matrix: Water Associated Lab Samples: 92342784003, 92342784004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Thallium ug/L ND 0.10 0.020 06/09/1716:01 LABORATORY CONTROL SAMPLE: 2014039 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Thallium ug/L 100 91.8 92 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2014040 2014041 MS MSD 92342600010 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Thallium ug/L ND 100 100 90.7 93.4 91 93 75-125 3 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 QC Batch: 363479 Analysis Method: EPA 6020B QC Batch Method: EPA 3010A Analysis Description: 6020 MET Associated Lab Samples: 92342784001, 92342784002 METHOD BLANK: 2015143 Matrix: Water Associated Lab Samples: 92342784001, 92342784002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Thallium ug/L ND 0.10 0.020 06/09/17 20:05 LABORATORY CONTROL SAMPLE: 2015144 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Thallium ug/L 100 93.7 94 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2015145 2015146 MS MSD 92342730002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Thallium ug/L 0.048J 100 100 94.4 94.8 94 95 75-125 0 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 QC Batch: 363311 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92342784001, 92342784002, 92342784003, 92342784004 METHOD BLANK: 2014186 Matrix: Water Associated Lab Samples: 92342784001, 92342784002, 92342784003, 92342784004 Blank Reporting Parameter Units Result Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 0.33 06/04/17 06:59 1,1,1-Trichloroethane ug/L ND 1.0 0.48 06/04/17 06:59 1,1,2,2-Tetrachloroethane ug/L ND 3.0 0.40 06/04/17 06:59 1,1,2-Trichloroethane ug/L ND 1.0 0.29 06/04/17 06:59 1,1-Dichloroethane ug/L ND 5.0 0.32 06/04/17 06:59 1,1-Dichloroethene ug/L ND 5.0 0.56 06/04/17 06:59 1,1-Dichloropropene ug/L ND 5.0 0.49 06/04/17 06:59 1,2,3-Trichloropropane ug/L ND 1.0 0.41 06/04/17 06:59 1,2,4-Trichlorobenzene ug/L ND 10.0 0.35 06/04/17 06:59 1,2-Dibromo-3-chloropropane ug/L ND 13.0 2.0 06/04/17 06:59 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 06/04/17 06:59 1,2-Dichlorobenzene ug/L ND 5.0 0.30 06/04/17 06:59 1,2-Dichloroethane ug/L ND 1.0 0.24 06/04/17 06:59 1,2-Dichloropropane ug/L ND 1.0 0.27 06/04/17 06:59 1,3-Dichlorobenzene ug/L ND 5.0 0.24 06/04/17 06:59 1,3-Dichloropropane ug/L ND 1.0 0.28 06/04/17 06:59 1,4-Dichlorobenzene ug/L ND 1.0 0.33 06/04/17 06:59 2,2-Dichloropropane ug/L ND 15.0 0.13 06/04/17 06:59 2-Butanone (MEK) ug/L ND 100 0.96 06/04/17 06:59 2-Hexanone ug/L ND 50.0 0.46 06/04/17 06:59 4-Methyl-2-pentanone (MIBK) ug/L ND 100 0.33 06/04/17 06:59 Acetone ug/L ND 100 10.0 06/04/17 06:59 Acetonitrile ug/L ND 55.0 2.2 06/04/17 06:59 Acrolein ug/L ND 53.0 1.6 06/04/17 06:59 Acrylonitrile ug/L ND 200 1.9 06/04/17 06:59 Allyl chloride ug/L ND 10.0 1.5 06/04/17 06:59 Benzene ug/L ND 1.0 0.25 06/04/17 06:59 Bromochloromethane ug/L ND 3.0 0.17 06/04/17 06:59 Bromodichloromethane ug/L ND 1.0 0.18 06/04/17 06:59 Bromoform ug/L ND 3.0 0.26 06/04/17 06:59 Bromomethane ug/L ND 10.0 0.29 06/04/17 06:59 Carbon disulfide ug/L ND 100 1.2 06/04/17 06:59 Carbon tetrachloride ug/L ND 1.0 0.25 06/04/17 06:59 Chlorobenzene ug/L ND 3.0 0.23 06/04/17 06:59 Chloroethane ug/L ND 10.0 0.54 06/04/17 06:59 Chloroform ug/L ND 5.0 0.14 06/04/17 06:59 Chloromethane ug/L ND 1.0 0.11 06/04/17 06:59 Chloroprene ug/L ND 20.0 0.27 06/04/17 06:59 cis-1,2-Dichloroethene ug/L ND 5.0 0.19 06/04/17 06:59 cis-1,3-Dichloropropene ug/L ND 1.0 0.13 06/04/17 06:59 Dibromochloromethane ug/L ND 3.0 0.21 06/04/17 06:59 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 METHOD BLANK: 2014186 Matrix: Water Associated Lab Samples: 92342784001, 92342784002, 92342784003, 92342784004 Blank Reporting Parameter Units Result Limit MDL Analyzed Dibromomethane ug/L ND 10.0 0.21 06/04/17 06:59 Dichlorodifluoromethane ug/L ND 5.0 0.21 06/04/17 06:59 Ethyl methacrylate ug/L ND 10.0 0.20 06/04/17 06:59 Ethylbenzene ug/L ND 1.0 0.30 06/04/17 06:59 Hexachloro-1,3-butadiene ug/L ND 10.0 0.71 06/04/17 06:59 lodomethane ug/L ND 10.0 0.32 06/04/17 06:59 Isobutanol ug/L ND 100 35.0 06/04/17 06:59 Methacrylonitrile ug/L ND 100 0.93 06/04/17 06:59 Methyl methacrylate ug/L ND 30.0 2.0 06/04/17 06:59 Methylene Chloride ug/L ND 1.0 0.97 06/04/17 06:59 Naphthalene ug/L ND 10.0 0.24 06/04/17 06:59 Propionitrile ug/L ND 150 3.6 06/04/17 06:59 Styrene ug/L ND 1.0 0.26 06/04/17 06:59 Tetrachloroethene ug/L ND 1.0 0.46 06/04/17 06:59 Toluene ug/L ND 1.0 0.26 06/04/17 06:59 trans-1,2-Dichloroethene ug/L ND 5.0 0.49 06/04/17 06:59 trans- 1,3-Dichloropropene ug/L ND 1.0 0.26 06/04/17 06:59 trans-1,4-Dichloro-2-butene ug/L ND 100 1.0 06/04/17 06:59 Trichloroethene ug/L ND 1.0 0.47 06/04/17 06:59 Trichlorofluoromethane ug/L ND 1.0 0.20 06/04/17 06:59 Vinyl acetate ug/L ND 50.0 0.35 06/04/17 06:59 Vinyl chloride ug/L ND 1.0 0.62 06/04/17 06:59 Xylene (Total) ug/L ND 5.0 0.66 06/04/17 06:59 1,2-Dichloroethane-d4 (S) % 89 70-130 06/04/17 06:59 4-Bromofluorobenzene (S) % 99 70-130 06/04/17 06:59 Toluene-d8 (S) % 106 70-130 06/04/17 06:59 LABORATORY CONTROL SAMPLE: Parameter 2014187 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 49.7 99 80-125 1,1,1-Trichloroethane ug/L 50 50.8 102 71-129 1,1,2,2-Tetrachloroethane ug/L 50 53.1 106 79-124 1,1,2-Trichloroethane ug/L 50 51.5 103 85-125 1,1-Dichloroethane ug/L 50 52.3 105 73-126 1,1-Dichloroethene ug/L 50 51.6 103 66-135 1,1-Dichloropropene ug/L 50 50.1 100 74-135 1,2,3-Trichloropropane ug/L 50 47.0 94 75-130 1,2,4-Trichlorobenzene ug/L 50 43.7 87 75-134 1,2-Dibromo-3-chloropropane ug/L 50 47.3 95 71-133 1,2-Dibromoethane (EDB) ug/L 50 54.1 108 83-124 1,2-Dichlorobenzene ug/L 50 48.2 96 80-133 1,2-Dichloroethane ug/L 50 48.4 97 67-128 1,2-Dichloropropane ug/L 50 52.7 105 75-132 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 LABORATORY CONTROL SAMPLE: Parameter 2014187 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,3-Dichlorobenzene ug/L 50 47.9 96 77-130 1,3-Dichloropropane ug/L 50 55.1 110 76-131 1,4-Dichlorobenzene ug/L 50 45.6 91 78-130 2,2-Dichloropropane ug/L 50 46.4 93 40-160 2-Butanone (MEK) ug/L 100 138 138 61-144 2-Hexanone ug/L 100 108 108 68-143 4-Methyl-2-pentanone (MIBK) ug/L 100 107 107 72-135 Acetone ug/L 100 123 123 48-146 Acetonitrile ug/L 500 524 105 62-150 Acrolein ug/L 250 339 136 24-160 Acrylonitrile ug/L 250 286 114 40-160 Allyl chloride ug/L 50 47.4 95 66-137 Benzene ug/L 50 52.5 105 80-125 Bromochloromethane ug/L 50 48.3 97 71-125 Bromodichloromethane ug/L 50 48.5 97 78-124 Bromoform ug/L 50 48.5 97 71-128 Bromomethane ug/L 50 44.8 90 40-160 Carbon disulfide ug/L 50 52.8J 106 50-160 Carbon tetrachloride ug/L 50 44.2 88 69-131 Chlorobenzene ug/L 50 49.9 100 81-122 Chloroethane ug/L 50 43.6 87 39-148 Chloroform ug/L 50 52.2 104 73-127 Chloromethane ug/L 50 58.1 116 44-146 Chloroprene ug/L 50 49.1 98 75-145 cis-1,2-Dichloroethene ug/L 50 54.0 108 74-124 cis-1,3-Dichloropropene ug/L 50 52.4 105 72-132 Dibromochloromethane ug/L 50 48.7 97 78-125 Dibromomethane ug/L 50 46.0 92 82-120 Dichlorodifluoromethane ug/L 50 45.4 91 34-157 Ethyl methacrylate ug/L 50 48.2 96 82-121 Ethylbenzene ug/L 50 48.0 96 79-121 Hexachloro-1,3-butadiene ug/L 50 46.0 92 72-131 lodomethane ug/L 100 95.1 95 39-154 Isobutanol ug/L 1000 1260 126 34-160 Methacrylonitrile ug/L 500 616 123 74-134 Methyl methacrylate ug/L 50 46.9 94 84-124 Methylene Chloride ug/L 50 53.3 107 64-133 Naphthalene ug/L 50 51.1 102 73-133 Propionitrile ug/L 500 640 128 73-140 Styrene ug/L 50 48.3 97 84-126 Tetrachloroethene ug/L 50 47.9 96 78-122 Toluene ug/L 50 48.3 97 80-121 trans-1,2-Dichloroethene ug/L 50 53.8 108 71-127 trans- 1,3-Dichloropropene ug/L 50 51.4 103 69-141 trans-1,4-Dichloro-2-butene ug/L 50 99.7J 199 40-160 L1 Trichloroethene ug/L 50 49.5 99 78-122 Trichlorofluoromethane ug/L 50 46.5 93 53-137 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 LABORATORY CONTROL SAMPLE: 2014187 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Vinyl acetate ug/L 100 103 103 40-160 Vinyl chloride ug/L 50 46.9 94 58-137 Xylene (Total) ug/L 150 141 94 81-126 1,2-Dichloroethane-d4 (S) % 95 70-130 4-Bromofluorobenzene (S) % 99 70-130 Toluene-d8 (S) % 95 70-130 MATRIX SPIKE SAMPLE: 2014189 92342784004 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 19.2 96 70-130 1,1,1-Trichloroethane ug/L ND 20 22.8 114 70-130 1,1,2,2-Tetrachloroethane ug/L ND 20 21.3 106 70-130 1,1,2-Trichloroethane ug/L ND 20 21.1 105 70-130 1,1-Dichloroethane ug/L ND 20 24.1 120 70-130 1,1-Dichloroethene ug/L ND 20 24.1 120 70-166 1,1-Dichloropropene ug/L ND 20 23.3 116 70-130 1,2,3-Trichloropropane ug/L ND 20 20.3 102 70-130 1,2,4-Trichlorobenzene ug/L ND 20 23.5 118 70-130 1,2-Dibromo-3-chloropropane ug/L ND 20 19.7 99 70-130 1,2-Dibromoethane (EDB) ug/L ND 20 20.6 103 70-130 1,2-Dichlorobenzene ug/L ND 20 22.0 110 70-130 1,2-Dichloroethane ug/L ND 20 20.7 104 70-130 1,2-Dichloropropane ug/L ND 20 22.8 114 70-130 1,3-Dichlorobenzene ug/L ND 20 23.3 117 70-130 1,3-Dichloropropane ug/L ND 20 21.5 107 70-130 1,4-Dichlorobenzene ug/L ND 20 21.8 109 70-130 2,2-Dichloropropane ug/L ND 20 22.8 114 70-130 2-Butanone (MEK) ug/L ND 40 46.8J 117 70-130 2-Hexanone ug/L ND 40 41.2J 103 70-130 4-Methyl-2-pentanone (MIBK) ug/L ND 40 42.3J 106 70-130 Acetone ug/L 12.9J 40 49.1 J 90 70-130 Acetonitrile ug/L ND 200 222 111 70-130 Acrolein ug/L ND 100 132 132 70-130 M1 Acrylonitrile ug/L ND 100 1111 111 70-130 Allyl chloride ug/L 4.1J 20 23.6 98 70-130 Benzene ug/L ND 20 23.7 119 70-148 Bromochloromethane ug/L ND 20 21.9 109 70-130 Bromodichloromethane ug/L ND 20 22.4 112 70-130 Bromoform ug/L ND 20 17.7 88 70-130 Bromomethane ug/L ND 20 23.2 116 70-130 Carbon disulfide ug/L ND 20 24.5J 123 70-130 Carbon tetrachloride ug/L ND 20 21.2 106 70-130 Chlorobenzene ug/L ND 20 22.5 112 70-146 Chloroethane ug/L ND 20 18.9 94 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 MATRIX SPIKE SAMPLE: Parameter 2014189 Units 92342784004 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers Chloroform ug/L ND 20 22.3 111 70-130 Chloromethane ug/L 0.14J 20 24.4 121 70-130 Chloroprene ug/L ND 20 21.9 109 70-130 cis-1,2-Dichloroethene ug/L 0.22J 20 24.8 123 70-130 cis-1,3-Dichloropropene ug/L ND 20 22.5 113 70-130 Dibromochloromethane ug/L ND 20 19.2 96 70-130 Dibromomethane ug/L ND 20 21.3 107 70-130 Dichlorodifluoromethane ug/L ND 20 20.2 101 70-130 Ethyl methacrylate ug/L ND 20 19.5 97 70-130 Ethylbenzene ug/L ND 20 22.2 111 70-130 Hexachloro-1,3-butadiene ug/L ND 20 23.5 118 70-130 lodomethane ug/L ND 40 44.2 110 70-130 Isobutanol ug/L ND 400 475 119 70-130 Methacrylonitrile ug/L ND 200 221 111 70-130 Methyl methacrylate ug/L ND 20 19.8J 99 70-130 Methylene Chloride ug/L ND 20 22.6 113 70-130 Naphthalene ug/L ND 20 24.5 123 70-130 Propionitrile ug/L ND 200 235 118 70-130 Styrene ug/L ND 20 21.3 107 70-130 Tetrachloroethene ug/L ND 20 20.7 103 70-130 Toluene ug/L ND 20 22.2 111 70-155 trans-1,2-Dichloroethene ug/L ND 20 23.7 118 70-130 trans- 1,3-Dichloropropene ug/L ND 20 22.0 110 70-130 trans-1,4-Dichloro-2-butene ug/L ND 20 24.7J 124 70-130 Trichloroethene ug/L ND 20 23.5 117 69-151 Trichlorofluoromethane ug/L ND 20 22.5 112 70-130 Vinyl acetate ug/L ND 40 38.6J 96 70-130 Vinyl chloride ug/L ND 20 21.5 107 70-130 1,2-Dichloroethane-d4 (S) % 95 70-130 4-Bromofluorobenzene (S) % 94 70-130 Toluene-d8 (S) % 99 70-130 SAMPLE DUPLICATE: 2014188 92342784003 Dup Max Parameter Units Result Result RPD RPD Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND ND 30 1,1,1-Trichloroethane ug/L ND ND 30 1,1,2,2-Tetrachloroethane ug/L ND ND 30 1,1,2-Trichloroethane ug/L ND ND 30 1,1-Dichloroethane ug/L 0.37J 0.35J 30 1,1-Dichloroethene ug/L ND ND 30 1,1-Dichloropropene ug/L ND ND 30 1,2,3-Trichloropropane ug/L ND ND 30 1,2,4-Trichlorobenzene ug/L ND ND 30 1,2-Dibromo-3-chloropropane ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 SAMPLE DUPLICATE: 2014188 92342784003 Dup Max Parameter Units Result Result RPD RPD Qualifiers 1,2-Dibromoethane (EDB) ug/L ND ND 30 1,2-Dichlorobenzene ug/L ND ND 30 1,2-Dichloroethane ug/L ND ND 30 1,2-Dichloropropane ug/L ND 0.86J 30 1,3-Dichlorobenzene ug/L ND ND 30 1,3-Dichloropropane ug/L ND ND 30 1,4-Dichlorobenzene ug/L 2.5 2.4 5 30 2,2-Dichloropropane ug/L ND ND 30 2-Butanone (MEK) ug/L ND ND 30 2-Hexanone ug/L ND ND 30 4-Methyl-2-pentanone (MIBK) ug/L ND ND 30 Acetone ug/L 21 AJ 13.9J 30 Acetonitrile ug/L ND ND 30 Acrolein ug/L ND ND 30 Acrylonitrile ug/L ND ND 30 Allyl chloride ug/L 8.2J ND 30 Benzene ug/L 0.62J 0.52J 30 Bromochloromethane ug/L ND ND 30 Bromodichloromethane ug/L ND ND 30 Bromoform ug/L ND ND 30 Bromomethane ug/L ND ND 30 Carbon disulfide ug/L ND ND 30 Carbon tetrachloride ug/L ND ND 30 Chlorobenzene ug/L 0.87J 0.97J 30 Chloroethane ug/L ND ND 30 Chloroform ug/L ND ND 30 Chloromethane ug/L ND 0.111 30 Chloroprene ug/L ND ND 30 cis-1,2-Dichloroethene ug/L 1.0J 1.01 3 30 cis-1,3-Dichloropropene ug/L ND ND 30 Dibromochloromethane ug/L ND ND 30 Dibromomethane ug/L ND ND 30 Dichlorodifluoromethane ug/L ND 0.31J 30 Ethyl methacrylate ug/L ND ND 30 Ethylbenzene ug/L ND ND 30 Hexachloro-1,3-butadiene ug/L ND ND 30 lodomethane ug/L ND ND 30 Isobutanol ug/L ND ND 30 Methacrylonitrile ug/L ND ND 30 Methyl methacrylate ug/L ND ND 30 Methylene Chloride ug/L ND ND 30 Naphthalene ug/L ND ND 30 Propionitrile ug/L ND ND 30 Styrene ug/L ND ND 30 Tetrachloroethene ug/L ND ND 30 Toluene ug/L 0.88J 0.911 30 trans-1,2-Dichloroethene ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 SAMPLE DUPLICATE: 2014188 Parameter trans- 1,3-Dichloropropene trans-1,4-Dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylene (Total) 1,2-Dichloroethane-d4 (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) QUALITY CONTROL DATA Units 92342784003 Result Dup Result ug/L ND ND ug/L ND ND ug/L ND ND ug/L ND ND ug/L ND ND ug/L ND ND ug/L ND ND 90 90 % 99 98 108 105 IVV 0 2 3 Max RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 QC Batch: 363426 Analysis Method: EPA 8081 QC Batch Method: EPA 3510 Analysis Description: 8081A GCS Pesticides Associated Lab Samples: 92342784003, 92342784004 METHOD BLANK: 2014786 Matrix: Water Associated Lab Samples: 92342784003, 92342784004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 4,4'-DDD ug/L ND 0.10 0.050 06/06/17 13:28 4,4'-DDE ug/L ND 0.10 0.050 06/06/17 13:28 4,4'-DDT ug/L ND 0.10 0.050 06/06/17 13:28 Aldrin ug/L ND 0.050 0.050 06/06/17 13:28 alpha-BHC ug/L ND 0.050 0.050 06/06/17 13:28 beta-BHC ug/L ND 0.050 0.050 06/06/17 13:28 Chlordane (Technical) ug/L ND 0.50 0.20 06/06/17 13:28 delta-BHC ug/L ND 0.050 0.050 06/06/17 13:28 Dieldrin ug/L ND 0.075 0.050 06/06/17 13:28 Endosulfan I ug/L ND 0.10 0.050 06/06/17 13:28 Endosulfan II ug/L ND 0.10 0.050 06/06/17 13:28 Endosulfan sulfate ug/L ND 0.10 0.050 06/06/17 13:28 Endrin ug/L ND 0.10 0.050 06/06/17 13:28 Endrin aldehyde ug/L ND 0.10 0.050 06/06/17 13:28 gamma-BHC (Lindane) ug/L ND 0.050 0.050 06/06/17 13:28 Heptachlor ug/L ND 0.050 0.050 06/06/17 13:28 Heptachlor epoxide ug/L ND 0.075 0.050 06/06/17 13:28 Methoxychlor ug/L ND 1.0 0.15 06/06/17 13:28 Toxaphene ug/L ND 1.5 0.20 06/06/17 13:28 Decachlorobiphenyl (S) % 78 20-130 06/06/17 13:28 Tetrachloro-m-xylene (S) % 51 20-130 06/06/17 13:28 LABORATORY CONTROL SAMPLE & LCSD: 2014787 2014788 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers 4,4'-DDD ug/L .25 0.22 0.23 90 92 20-150 2 30 4,4'-DDE ug/L .25 0.21 0.20 84 79 20-150 7 30 4,4'-DDT ug/L .25 0.23 0.24 94 95 20-150 1 30 Aldrin ug/L .25 0.16 0.15 64 60 20-150 8 30 alpha-BHC ug/L .25 0.19 0.19 79 78 20-150 1 30 beta-BHC ug/L .25 0.17 0.19 70 75 20-150 7 30 delta-BHC ug/L .25 0.21 0.20 84 79 20-150 7 30 Dieldrin ug/L .25 0.21 0.21 86 83 20-150 3 30 Endosulfan I ug/L .25 0.22 0.21 87 84 20-150 3 30 Endosulfan II ug/L .25 0.23 0.22 91 90 20-150 1 30 Endosulfan sulfate ug/L .25 0.24 0.24 97 97 20-150 0 30 Endrin ug/L .25 0.23 0.23 93 93 20-150 0 30 Endrin aldehyde ug/L .25 0.21 0.22 87 89 20-150 3 30 gamma-BHC (Lindane) ug/L .25 0.21 0.21 83 85 20-150 2 30 Heptachlor ug/L .25 0.17 0.15 68 62 20-150 9 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 LABORATORY CONTROL SAMPLE & LCSD: 2014787 2014788 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Heptachlor epoxide ug/L .25 0.20 0.17 82 70 20-150 16 30 Methoxychlor ug/L .74 0.72J 0.72J 97 97 20-150 1 30 Decachlorobiphenyl (S) % 78 64 20-130 Tetrachloro-m-xylene (S) % 81 69 20-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 QC Batch: 363427 Analysis Method: EPA 8082 QC Batch Method: EPA 3510 Analysis Description: 8082 GCS PCB Associated Lab Samples: 92342784003, 92342784004 METHOD BLANK: 2014798 Matrix: Water Associated Lab Samples: 92342784003, 92342784004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers PCB-1016 (Aroclor 1016) ug/L ND 0.50 0.50 06/06/17 20:10 PCB-1221 (Aroclor 1221) ug/L ND 0.50 0.50 06/06/17 20:10 PCB-1232 (Aroclor 1232) ug/L ND 0.50 0.50 06/06/17 20:10 PCB-1242 (Aroclor 1242) ug/L ND 0.50 0.50 06/06/17 20:10 PCB-1248 (Aroclor 1248) ug/L ND 0.50 0.50 06/06/17 20:10 PCB-1254 (Aroclor 1254) ug/L ND 0.50 0.50 06/06/17 20:10 PCB-1260 (Aroclor 1260) ug/L ND 0.50 0.50 06/06/17 20:10 Decachlorobiphenyl (S) % 75 10-132 06/06/17 20:10 LABORATORY CONTROL SAMPLE & LCSD: 2014799 2014800 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers PCB-1016 (Aroclor 1016) ug/L 5 3.3 3.5 66 69 50-150 5 30 PCB-1260 (Aroclor 1260) ug/L 5 3.2 3.0 63 60 50-150 5 30 Decachlorobiphenyl (S) % 34 37 10-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 QC Batch: 373221 Analysis Method: EPA 8151 QC Batch Method: EPA 8151 Analysis Description: 8151A GCS Herbicides Associated Lab Samples: 92342784003, 92342784004 METHOD BLANK: 2017562 Matrix: Water Associated Lab Samples: 92342784003, 92342784004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 2,4,5-T ug/L ND 0.19 0.042 06/09/17 20:42 2,4,5-TP (Silvex) ug/L ND 0.19 0.049 06/09/17 20:42 2,4-D ug/L ND 0.94 0.22 06/09/17 20:42 Dinoseb ug/L ND 0.19 0.057 06/09/17 20:42 Pentachlorophenol ug/L ND 0.028 0.017 06/09/17 20:42 2,4-DCAA (S) % 74 39-139 06/09/17 20:42 LABORATORY CONTROL SAMPLE: 2017563 Parameter Units 2,4,5-T ug/L 2,4,5-TP (Silvex) ug/L 2,4-D ug/L Dinoseb ug/L Pentachlorophenol ug/L 2,4-DCAA (S) % Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 1.2 1.3 109 37-133 1.2 1.3 110 53-134 6 5.5 91 35-124 1.2 1.2 99 13-116 .18 0.17 94 39-170 85 39-139 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2018719 2018720 MS MSD 35316294004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 2,4,5-T ug/L 0.043U 1.2 1.4 1.2 1.2 100 90 37-133 3 40 2,4,5-TP (Silvex) ug/L 0.050U 1.2 1.4 1.2 1.2 97 88 53-134 2 40 2,4-D ug/L 0.23U 6 6.8 5.1 5.2 84 76 35-124 3 40 Dinoseb ug/L 0.058U 1.2 1.4 1.1 0.98 91 72 13-116 11 40 Pentachlorophenol ug/L 0.017U .18 .2 0.15 0.057 82 28 39-170 89 40 M1,R1 2,4-DCAA (S) % 69 85 39-139 40 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 QC Batch: 364049 Analysis Method: EPA 8270 QC Batch Method: EPA 3510 Analysis Description: 8270 Water MSSV Associated Lab Samples: 92342784003, 92342784004 METHOD BLANK: 2018678 Associated Lab Samples: 92342784003, 92342784004 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed 1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 1.3 06/14/17 13:23 1,3,5-Trinitrobenzene ug/L ND 10.0 1.2 06/14/17 13:23 1,3-Dinitrobenzene ug/L ND 20.0 1.3 06/14/17 13:23 1,4-Naphthoquinone ug/L ND 10.0 0.99 06/14/17 13:23 1-Naphthalenamine ug/L ND 10.0 1.3 06/14/17 13:23 2,2'-Oxybis(1-chloropropane) ug/L ND 10.0 1.8 06/14/17 13:23 2,3,4,6-Tetrachlorophenol ug/L ND 10.0 2.9 06/14/17 13:23 2,4,5-Trichlorophenol ug/L ND 10.0 1.5 06/14/17 13:23 2,4,6-Trichlorophenol ug/L ND 10.0 1.4 06/14/17 13:23 2,4-Dichlorophenol ug/L ND 10.0 1.6 06/14/17 13:23 2,4-Dimethylphenol ug/L ND 10.0 1.6 06/14/17 13:23 2,4-Dinitrophenol ug/L ND 50.0 5.1 06/14/17 13:23 2,4-Dinitrotoluene ug/L ND 10.0 1.5 06/14/17 13:23 2,6-Dichlorophenol ug/L ND 10.0 1.5 06/14/17 13:23 2,6-Dinitrotoluene ug/L ND 10.0 1.4 06/14/17 13:23 2-Acetylaminofluorene ug/L ND 20.0 1.6 06/14/17 13:23 2-Chloronaphthalene ug/L ND 10.0 1.6 06/14/17 13:23 2-Chlorophenol ug/L ND 10.0 1.5 06/14/17 13:23 2-Methylnaphthalene ug/L ND 10.0 1.4 06/14/17 13:23 2-Methylphenol(o-Cresol) ug/L ND 10.0 1.6 06/14/17 13:23 2-Naphthalenamine ug/L ND 10.0 2.2 06/14/17 13:23 2-Nitroaniline ug/L ND 50.0 2.3 06/14/17 13:23 2-Nitrophenol ug/L ND 10.0 1.6 06/14/17 13:23 3&4-Methyl phenol (m&p Cresol) ug/L ND 10.0 1.4 06/14/17 13:23 3,3'-Dichlorobenzidine ug/L ND 20.0 3.9 06/14/17 13:23 3,3'-Dimethylbenzidine ug/L ND 10.0 3.9 06/14/17 13:23 3-Methylcholanthrene ug/L ND 10.0 2.7 06/14/17 13:23 3-Nitroaniline ug/L ND 50.0 2.7 06/14/17 13:23 4,6-Dinitro-2-methyl phenol ug/L ND 50.0 2.2 06/14/17 13:23 4-Aminobiphenyl ug/L ND 20.0 1.7 06/14/17 13:23 4-Bromophenylphenyl ether ug/L ND 10.0 1.5 06/14/17 13:23 4-ChIoro-3-methyl phenol ug/L ND 20.0 2.8 06/14/17 13:23 4-Chloroaniline ug/L ND 20.0 2.8 06/14/17 13:23 4-Chlorophenylphenyl ether ug/L ND 10.0 1.6 06/14/17 13:23 4-Nitroaniline ug/L ND 20.0 3.4 06/14/17 13:23 4-Nitrophenol ug/L ND 50.0 4.3 06/14/17 13:23 5-Nitro-o-toluidine ug/L ND 10.0 1.9 06/14/17 13:23 7,12-Dimethylbenz(a)anthracene ug/L ND 10.0 2.4 06/14/17 13:23 Acenaphthene ug/L ND 10.0 1.6 06/14/17 13:23 Acenaphthylene ug/L ND 10.0 1.5 06/14/17 13:23 Acetophenone ug/L ND 10.0 1.9 06/14/17 13:23 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 METHOD BLANK: 2018678 Associated Lab Samples: 92342784003, 92342784004 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Anthracene ug/L ND 10.0 1.7 06/14/17 13:23 Benzo(a)anthracene ug/L ND 10.0 2.1 06/14/17 13:23 Benzo(a)pyrene ug/L ND 10.0 2.2 06/14/17 13:23 Benzo(b)fluoranthene ug/L ND 10.0 2.2 06/14/17 13:23 Benzo(g,h,i)perylene ug/L ND 10.0 2.1 06/14/17 13:23 Benzo(k)fluoranthene ug/L ND 10.0 2.0 06/14/17 13:23 Benzyl alcohol ug/L ND 20.0 3.1 06/14/17 13:23 bis(2-Chloroethoxy)methane ug/L ND 10.0 1.6 06/14/17 13:23 bis(2-Chloroethyl) ether ug/L ND 10.0 1.7 06/14/17 13:23 bis(2-Ethylhexyl)phthalate ug/L ND 15.0 2.3 06/14/17 13:23 Butylbenzylphthalate ug/L ND 10.0 2.5 06/14/17 13:23 Chlorobenzilate ug/L ND 10.0 2.2 06/14/17 13:23 Chrysene ug/L ND 10.0 2.1 06/14/17 13:23 Di-n-butylphthalate ug/L ND 10.0 2.0 06/14/17 13:23 Di-n-octylphthalate ug/L ND 10.0 1.5 06/14/17 13:23 Diallate ug/L ND 10.0 1.6 06/14/17 13:23 Dibenz(a,h)anthracene ug/L ND 10.0 2.0 06/14/17 13:23 Dibenzofuran ug/L ND 10.0 1.7 06/14/17 13:23 Diethylphthalate ug/L ND 6000 1.6 06/14/17 13:23 Dimethoate ug/L ND 20.0 1.8 06/14/17 13:23 Dimethylphthalate ug/L ND 10.0 1.4 06/14/17 13:23 Diphenylamine ug/L ND 10.0 1.4 06/14/17 13:23 Disulfoton ug/L ND 10.0 1.5 06/14/17 13:23 Ethyl methanesulfonate ug/L ND 20.0 1.6 06/14/17 13:23 Famphur ug/L ND 20.0 5.7 06/14/17 13:23 Fluoranthene ug/L ND 10.0 2.2 06/14/17 13:23 Fluorene ug/L ND 10.0 1.6 06/14/17 13:23 Hexachlorobenzene ug/L ND 10.0 1.7 06/14/17 13:23 Hexachlorocyclopentadiene ug/L ND 10.0 1.3 06/14/17 13:23 Hexachloroethane ug/L ND 10.0 1.8 06/14/17 13:23 Hexachloropropene ug/L ND 10.0 1.2 06/14/17 13:23 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 2.0 06/14/17 13:23 Isodrin ug/L ND 20.0 2.5 06/14/17 13:23 Isophorone ug/L ND 10.0 1.5 06/14/17 13:23 Isosafrole ug/L ND 10.0 1.5 06/14/17 13:23 Kepone ug/L ND 20.0 4.5 06/14/17 13:23 Methapyrilene ug/L ND 100 3.0 06/14/17 13:23 Methyl methanesulfonate ug/L ND 10.0 1.1 06/14/17 13:23 Methyl parathion ug/L ND 10.0 1.6 06/14/17 13:23 N-Nitroso-di-n-butylamine ug/L ND 10.0 1.6 06/14/17 13:23 N-Nitroso-di-n-propylamine ug/L ND 10.0 1.7 06/14/17 13:23 N-Nitrosodiethylamine ug/L ND 20.0 1.4 06/14/17 13:23 N-Nitrosodimethylamine ug/L ND 10.0 1.6 06/14/17 13:23 N-Nitrosodiphenylamine ug/L ND 10.0 1.4 06/14/17 13:23 N-Nitrosomethylethylamine ug/L ND 10.0 1.4 06/14/17 13:23 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 METHOD BLANK: 2018678 Associated Lab Samples: 92342784003, 92342784004 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed N-Nitrosopiperidine ug/L ND 20.0 1.7 06/14/17 13:23 N-Nitrosopyrrolidine ug/L ND 10.0 1.7 06/14/17 13:23 Nitrobenzene ug/L ND 10.0 1.6 06/14/17 13:23 O,O,O-Triethylphosphorothioate ug/L ND 10.0 1.7 06/14/17 13:23 O-Toluidine ug/L ND 10.0 1.7 06/14/17 13:23 P-Dimethylaminoazobenzene ug/L ND 10.0 1.0 06/14/17 13:23 p-Phenylenediamine ug/L ND 10.0 2.2 06/14/17 13:23 Parathion (Ethyl parathion) ug/L ND 10.0 1.5 06/14/17 13:23 Pentachlorobenzene ug/L ND 10.0 1.5 06/14/17 13:23 Pentachloronitrobenzene ug/L ND 20.0 1.7 06/14/17 13:23 Pentachlorophenol ug/L ND 25.0 3.5 06/14/17 13:23 Phenacetin ug/L ND 20.0 1.9 06/14/17 13:23 Phenanthrene ug/L ND 10.0 1.6 06/14/17 13:23 Phenol ug/L ND 10.0 1.3 06/14/17 13:23 Phorate ug/L ND 10.0 1.7 06/14/17 13:23 Pronamide ug/L ND 10.0 2.0 06/14/17 13:23 Pyrene ug/L ND 10.0 2.2 06/14/17 13:23 Safrole ug/L ND 10.0 1.3 06/14/17 13:23 Thionazin ug/L ND 20.0 1.7 06/14/17 13:23 2,4,6-Tribromophenol (S) % 74 27-110 06/14/17 13:23 2-Fluorobiphenyl (S) % 77 27-110 06/14/17 13:23 2-Fluorophenol (S) % 37 12-110 06/14/17 13:23 Nitrobenzene-d5 (S) % 62 21-110 06/14/17 13:23 Phenol-d6 (S) % 25 10-110 06/14/17 13:23 Terphenyl-d14 (S) % 87 31-107 06/14/17 13:23 LABORATORY CONTROL SAMPLE: Parameter 2018679 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,2,4,5-Tetrachlorobenzene ug/L 50 34.4 69 16-129 1,3,5-Trinitrobenzene ug/L 50 32.6 65 55-125 1,3-Dinitrobenzene ug/L 50 42.5 85 30-122 1,4-Naphthoquinone ug/L 50 41.8 84 31-120 1-Naphthalenamine ug/L 50 27.0 54 37-126 2,2'-Oxybis(1-chloropropane) ug/L 50 52.9 106 18-120 2,3,4,6-Tetrachlorophenol ug/L 50 82.3 165 54-276 2,4,5-Trichlorophenol ug/L 50 43.1 86 43-113 2,4,6-Trichlorophenol ug/L 50 50.8 102 42-120 2,4-Dichlorophenol ug/L 50 42.7 85 30-120 2,4-Dimethylphenol ug/L 50 37.9 76 29-111 2,4-Dinitrophenol ug/L 250 246 98 19-132 2,4-Dinitrotoluene ug/L 50 45.1 90 58-128 2,6-Dichlorophenol ug/L 50 43.6 87 54-128 2,6-Dinitrotoluene ug/L 50 47.0 94 54-129 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 LABORATORY CONTROL SAMPLE: Parameter 2018679 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2-Acetylaminofluorene ug/L 50 38.7 77 81-160 L2 2-Chloronaphthalene ug/L 50 53.0 106 43-117 2-Chlorophenol ug/L 50 41.9 84 37-120 2-Methylnaphthalene ug/L 50 37.6 75 33-120 2-Methylphenol(o-Cresol) ug/L 50 34.3 69 31-120 2-Naphthalenamine ug/L 50 34.1 68 41-136 2-Nitroaniline ug/L 100 88.7 89 48-121 2-Nitrophenol ug/L 50 40.7 81 25-116 3&4-Methyl phenol (m&p Cresol) ug/L 50 29.8 60 23-120 3,3'-Dichlorobenzidine ug/L 250 88.8 36 10-154 3,3'-Dimethylbenzidine ug/L 100 41.5 42 10-157 3-Methylcholanthrene ug/L 50 46.8 94 65-130 3-Nitroaniline ug/L 100 107 107 43-115 4,6-Dinitro-2-methyl phenol ug/L 100 87.7 88 44-124 4-Aminobiphenyl ug/L 50 25.7 51 21-125 4-Bromophenylphenyl ether ug/L 50 34.8 70 34-113 4-ChIoro-3-methyl phenol ug/L 100 73.8 74 31-110 4-Chloroaniline ug/L 100 87.8 88 20-120 4-Chlorophenylphenyl ether ug/L 50 41.7 83 34-116 4-Nitroaniline ug/L 100 111 111 46-128 4-Nitrophenol ug/L 250 79.5 32 11-120 5-Nitro-o-toluidine ug/L 50 45.6 91 78-160 7,12-Dimethylbenz(a)anthracene ug/L 50 46.0 92 47-124 Acenaphthene ug/L 50 47.2 94 48-114 Acenaphthylene ug/L 50 48.6 97 48-112 Acetophenone ug/L 50 42.4 85 24-120 Anthracene ug/L 50 43.2 86 57-118 Benzo(a)anthracene ug/L 50 42.8 86 56-121 Benzo(a)pyrene ug/L 50 45.9 92 55-127 Benzo(b)fluoranthene ug/L 50 48.8 98 53-128 Benzo(g,h,i)perylene ug/L 50 39.6 79 54-125 Benzo(k)fluoranthene ug/L 50 46.1 92 51-123 Benzyl alcohol ug/L 100 77.8 78 27-120 bis(2-Chloroethoxy)methane ug/L 50 33.2 66 32-120 bis(2-Chloroethyl) ether ug/L 50 34.2 68 33-111 bis(2-Ethylhexyl)phthalate ug/L 50 43.0 86 50-145 Butylbenzylphthalate ug/L 50 45.0 90 54-138 Chlorobenzilate ug/L 50 42.8 86 65-132 Chrysene ug/L 50 42.6 85 58-127 Di-n-butylphthalate ug/L 50 46.0 92 56-125 Di-n-octylphthalate ug/L 50 41.1 82 50-134 Diallate ug/L 50 33.1 66 47-123 Dibenz(a,h)anthracene ug/L 50 43.7 87 53-129 Dibenzofuran ug/L 50 48.3 97 45-120 Diethylphthalate ug/L 50 46.7J 93 53-120 Dimethoate ug/L 50 39.7 79 57-139 Dimethylphthalate ug/L 50 48.6 97 55-116 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 40 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 LABORATORY CONTROL SAMPLE: Parameter 2018679 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Diphenylamine ug/L 50 44.9 90 42-120 Disulfoton ug/L 50 33.3 67 49-156 Ethyl methanesulfonate ug/L 50 31.0 62 43-120 Famphur ug/L 100 107 107 40-160 Fluoranthene ug/L 50 44.4 89 57-125 Fluorene ug/L 50 46.5 93 53-118 Hexachlorobenzene ug/L 50 39.8 80 49-116 Hexachlorocyclopentadiene ug/L 50 35.4 71 26-158 Hexachloroethane ug/L 50 25.8 52 30-114 Hexachloropropene ug/L 50 24.1 48 13-137 Indeno(1,2,3-cd)pyrene ug/L 50 42.1 84 55-128 Isodrin ug/L 50 40.0 80 68-129 Isophorone ug/L 50 36.5 73 31-118 Isosafrole ug/L 50 40.9 82 48-107 Kepone ug/L 100 65.8 66 10-124 Methapyrilene ug/L 50 21.OJ 42 40-160 Methyl methanesulfonate ug/L 50 46.3 93 25-114 Methyl parathion ug/L 50 42.9 86 58-137 N-Nitroso-di-n-butylamine ug/L 50 35.4 71 36-115 N-Nitroso-di-n-propylamine ug/L 50 43.8 88 32-119 N-Nitrosodiethylamine ug/L 50 34.6 69 47-115 N-Nitrosodimethylamine ug/L 50 23.1 46 13-120 N-Nitrosodiphenylamine ug/L 50 44.9 90 43-120 N-Nitrosomethylethylamine ug/L 50 28.0 56 39-120 N-Nitrosopiperidine ug/L 50 41.6 83 43-113 N-Nitrosopyrrolidine ug/L 50 41.7 83 32-110 Nitrobenzene ug/L 50 31.5 63 33-110 O,O,O-Triethylphosphorothioate ug/L 50 38.1 76 51-127 O-Toluidine ug/L 50 32.1 64 27-120 P-Dimethylaminoazobenzene ug/L 100 17.3 17 10-120 p-Phenylenediamine ug/L 50 37.6 75 72-143 Parathion (Ethyl parathion) ug/L 50 35.4 71 56-140 Pentachlorobenzene ug/L 50 42.9 86 30-137 Pentachloronitrobenzene ug/L 50 44.1 88 70-124 Pentachlorophenol ug/L 250 97.2 39 10-137 Phenacetin ug/L 50 37.0 74 60-130 Phenanthrene ug/L 50 43.1 86 57-117 Phenol ug/L 50 18.9 38 10-120 Phorate ug/L 50 32.6 65 55-126 Pronamide ug/L 50 40.4 81 75-124 Pyrene ug/L 50 45.3 91 55-122 Safrole ug/L 50 41.4 83 41-120 Thionazin ug/L 50 35.2 70 63-137 2,4,6-Tribromophenol (S) % 90 27-110 2-Fluorobiphenyl (S) % 90 27-110 2-Fluorophenol(S) % 46 12-110 Nitrobenzene-d5(S) % 67 21-110 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 LABORATORY CONTROL SAMPLE: 2018679 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phenol-d6 (S) % 34 10-110 Terphenyl-d14 (S) % 91 31-107 MATRIX SPIKE SAMPLE: 2022108 92342530002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,2,4,5-Tetrachlorobenzene ug/L ND 50 37.7 75 50-150 1,3,5-Trinitrobenzene ug/L ND 50 33.6 67 50-150 1,3-Dinitrobenzene ug/L ND 50 41.4 83 50-150 1,4-Naphthoquinone ug/L ND 50 44.8 90 50-150 1-Naphthalenamine ug/L ND 50 14.2 28 50-150 M1 2,2'-Oxybis(1-chloropropane) ug/L ND 50 52.0 104 50-150 2,3,4,6-Tetrachlorophenol ug/L ND 50 85.5 171 50-150 M1 2,4,5-Trichlorophenol ug/L ND 50 44.7 89 19-105 2,4,6-Trichlorophenol ug/L ND 50 52.4 105 13-108 2,4-Dichlorophenol ug/L ND 50 39.5 79 29-111 2,4-Dimethylphenol ug/L ND 50 36.2 72 21-103 2,4-Dinitrophenol ug/L ND 250 207 83 10-109 2,4-Dinitrotoluene ug/L ND 50 46.7 93 27-104 2,6-Dichlorophenol ug/L ND 50 40.5 81 50-150 2,6-Dinitrotoluene ug/L ND 50 48.5 97 28-101 2-Acetylaminofluorene ug/L ND 50 36.8 73 50-150 2-Chloronaphthalene ug/L ND 50 58.1 116 14-102 M1 2-Chlorophenol ug/L ND 50 36.3 73 16-110 2-Methylnaphthalene ug/L ND 50 36.8 74 13-110 2-Methylphenol(o-Cresol) ug/L ND 50 29.7 59 19-110 2-Naphthalenamine ug/L ND 50 11.5 23 50-150 M1 2-Nitroaniline ug/L ND 100 95.3 95 26-103 2-Nitrophenol ug/L ND 50 36.5 73 20-110 3&4-Methyl phenol (m&p Cresol) ug/L ND 50 25.5 51 20-110 3,3'-Dichlorobenzidine ug/L ND 250 78.3 31 25-112 3,3'-Dimethylbenzidine ug/L ND 100 20.1 20 50-150 M1 3-Methylcholanthrene ug/L ND 50 44.5 89 50-150 3-Nitroaniline ug/L ND 100 104 104 29-110 4,6-Dinitro-2-methyl phenol ug/L ND 100 73.6 74 10-117 4-Aminobiphenyl ug/L ND 50 21.2 42 50-150 M1 4-Bromophenylphenyl ether ug/L ND 50 35.3 71 20-105 4-ChIoro-3-methyl phenol ug/L ND 100 69.2 69 22-110 4-Chloroaniline ug/L ND 100 59.4 59 20-100 4-Chlorophenylphenyl ether ug/L ND 50 45.0 90 19-102 4-Nitroaniline ug/L ND 100 112 112 29-110 M1 4-Nitrophenol ug/L ND 250 78.0 31 10-110 5-Nitro-o-toluidine ug/L ND 50 46.3 93 50-150 7,12-Dimethylbenz(a)anthracene ug/L ND 50 46.5 93 50-150 Acenaphthene ug/L ND 50 50.2 100 17-100 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 MATRIX SPIKE SAMPLE: 2022108 92342530002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Acenaphthylene ug/L ND 50 51.2 102 21-100 M1 Acetophenone ug/L ND 50 36.5 73 50-150 Anthracene ug/L ND 50 44.4 89 24-109 Benzo(a)anthracene ug/L ND 50 41.6 83 22-117 Benzo(a)pyrene ug/L ND 50 44.7 89 23-104 Benzo(b)fluoranthene ug/L ND 50 48.9 98 23-103 Benzo(g,h,i)perylene ug/L ND 50 40.5 81 18-111 Benzo(k)fluoranthene ug/L ND 50 45.1 90 22-113 Benzyl alcohol ug/L ND 100 63.0 63 19-101 bis(2-Chloroethoxy)methane ug/L ND 50 31.8 64 22-110 bis(2-Chloroethyl) ether ug/L ND 50 33.1 66 16-110 bis(2-Ethylhexyl)phthalate ug/L ND 50 44.8 90 23-102 Butylbenzylphthalate ug/L ND 50 45.6 91 25-110 Chlorobenzilate ug/L ND 50 42.7 85 50-150 Chrysene ug/L ND 50 42.2 84 23-115 Di-n-butylphthalate ug/L ND 50 48.3 97 26-110 Di-n-octylphthalate ug/L ND 50 41.5 83 22-110 Diallate ug/L ND 50 35.2 70 50-150 Dibenz(a,h)anthracene ug/L ND 50 42.0 84 21-112 Dibenzofuran ug/L ND 50 51.2 102 19-102 Diethylphthalate ug/L ND 50 50.2J 100 29-110 Dimethoate ug/L ND 50 42.9 86 50-150 Dimethylphthalate ug/L ND 50 51.5 103 27-110 Diphenylamine ug/L ND 50 45.8 92 50-150 Disulfoton ug/L ND 50 35.4 71 50-150 Ethyl methanesulfonate ug/L ND 50 27.4 55 50-150 Famphur ug/L ND 100 130 130 50-150 Fluoranthene ug/L ND 50 45.8 92 23-112 Fluorene ug/L ND 50 49.1 98 22-104 Hexachlorobenzene ug/L ND 50 40.0 80 21-116 Hexachlorocyclopentadiene ug/L ND 50 35.9 72 10-110 Hexachloroethane ug/L ND 50 27.2 54 10-110 Hexachloropropene ug/L ND 50 25.5 51 50-150 Indeno(1,2,3-cd)pyrene ug/L ND 50 42.4 85 20-113 Isodrin ug/L ND 50 42.3 85 50-150 Isophorone ug/L ND 50 35.6 71 50-150 Isosafrole ug/L ND 50 43.6 87 50-150 Kepone ug/L ND 100 72.4 72 50-150 Methapyrilene ug/L ND 50 33.3J 67 50-150 Methyl methanesulfonate ug/L ND 50 42.5 85 50-150 Methyl parathion ug/L ND 50 42.9 86 50-150 N-Nitroso-di-n-butylamine ug/L ND 50 32.3 65 50-150 N-Nitroso-di-n-propylamine ug/L ND 50 37.2 74 21-105 N-Nitrosodiethylamine ug/L ND 50 28.7 57 50-150 N-Nitrosodimethylamine ug/L ND 50 20.7 41 10-110 N-Nitrosodiphenylamine ug/L ND 50 45.8 92 23-107 N-Nitrosomethylethylamine ug/L ND 50 23.7 47 50-150 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 MATRIX SPIKE SAMPLE: 2022108 92342530002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers N-Nitrosopiperidine ug/L ND 50 37.2 74 50-150 N-Nitrosopyrrolidine ug/L ND 50 28.6 57 50-150 Nitrobenzene ug/L ND 50 30.4 61 20-110 O,O,O-Triethylphosphorothioate ug/L ND 50 36.8 74 50-150 O-Toluidine ug/L ND 50 20.6 41 50-150 M1 P-Dimethylaminoazobenzene ug/L ND 100 16.8 17 50-150 M1 p-Phenylenediamine ug/L ND 50 35.2 70 50-150 Parathion (Ethyl parathion) ug/L ND 50 36.6 73 50-150 Pentachlorobenzene ug/L ND 50 44.7 89 50-150 Pentachloronitrobenzene ug/L ND 50 44.8 90 50-150 Pentachlorophenol ug/L ND 250 88.9 36 10-118 Phenacetin ug/L ND 50 37.1 74 50-150 Phenanthrene ug/L ND 50 44.8 90 24-106 Phenol ug/L ND 50 15.3 31 12-110 Phorate ug/L ND 50 33.6 67 50-150 Pronamide ug/L ND 50 41.6 83 50-150 Pyrene ug/L ND 50 45.0 90 24-114 Safrole ug/L ND 50 38.4 77 50-150 Thionazin ug/L ND 50 38.0 76 50-150 2,4,6-Tribromophenol (S) % 87 27-110 2-Fluorobiphenyl (S) % 95 27-110 2-Fluorophenol(S) % 39 12-110 Nitrobenzene-d5 (S) % 62 21-110 Phenol-d6 (S) % 27 10-110 Terphenyl-d14 (S) % 74 31-107 SAMPLE DUPLICATE: 2018681 92342530004 Dup Max Parameter Units Result Result RPD RPD Qualifiers 1,2,4,5-Tetrachlorobenzene ug/L ND ND 30 1,3,5-Trinitrobenzene ug/L ND ND 30 1,3-Dinitrobenzene ug/L ND ND 30 1,4-Naphthoquinone ug/L ND ND 30 1-Naphthalenamine ug/L ND ND 30 2,2'-Oxybis(1-chloropropane) ug/L ND ND 30 2,3,4,6-Tetrachlorophenol ug/L ND ND 30 2,4,5-Trichlorophenol ug/L ND ND 30 2,4,6-Trichlorophenol ug/L ND ND 30 2,4-Dichlorophenol ug/L ND ND 30 2,4-Dimethylphenol ug/L ND ND 30 2,4-Dinitrophenol ug/L ND ND 30 2,4-Dinitrotoluene ug/L ND ND 30 2,6-Dichlorophenol ug/L ND ND 30 2,6-Dinitrotoluene ug/L ND ND 30 2-Acetylaminofluorene ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 SAMPLE DUPLICATE: 2018681 Parameter Units 92342530004 Result Dup Result 2-Chloronaphthalene ug/L ND ND 2-Chlorophenol ug/L ND ND 2-Methylnaphthalene ug/L ND ND 2-Methylphenol(o-Cresol) ug/L ND ND 2-Naphthalenamine ug/L ND ND 2-Nitroaniline ug/L ND ND 2-Nitrophenol ug/L ND ND 3&4-Methyl phenol (m&p Cresol) ug/L ND ND 3,3'-Dichlorobenzidine ug/L ND ND 3,3'-Dimethylbenzidine ug/L ND ND 3-Methylcholanthrene ug/L ND ND 3-Nitroaniline ug/L ND ND 4,6-Dinitro-2-methyl phenol ug/L ND ND 4-Aminobiphenyl ug/L ND ND 4-Bromophenylphenyl ether ug/L ND ND 4-Chloro-3-methylphenol ug/L ND ND 4-Chloroaniline ug/L ND ND 4-Chlorophenylphenyl ether ug/L ND ND 4-Nitroaniline ug/L ND ND 4-Nitrophenol ug/L ND ND 5-Nitro-o-toluidine ug/L ND ND 7,12-Dimethylbenz(a)anthracene ug/L ND ND Acenaphthene ug/L ND ND Acenaphthylene ug/L ND ND Acetophenone ug/L ND ND Anthracene ug/L ND ND Benzo(a)anthracene ug/L ND ND Benzo(a)pyrene ug/L ND ND Benzo(b)fluoranthene ug/L ND ND Benzo(g,h,i)perylene ug/L ND ND Benzo(k)fluoranthene ug/L ND ND Benzyl alcohol ug/L ND ND bis(2-Chloroethoxy)methane ug/L ND ND bis(2-Chloroethyl) ether ug/L ND ND bis(2-Ethylhexyl)phthalate ug/L ND ND Butylbenzylphthalate ug/L ND ND Chlorobenzilate ug/L ND ND Chrysene ug/L ND ND Di-n-butylphthalate ug/L ND ND Di-n-octylphthalate ug/L ND ND Diallate ug/L ND ND Dibenz(a,h)anthracene ug/L ND ND Dibenzofuran ug/L ND ND Diethylphthalate ug/L ND ND Dimethoate ug/L ND ND Dimethylphthalate ug/L ND ND Diphenylamine ug/L ND ND Max RPD RPD Qualifiers 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 SAMPLE DUPLICATE: 2018681 Parameter Units 92342530004 Result Dup Result RPD Max RPD Disulfoton ug/L ND ND 30 Ethyl methanesulfonate ug/L ND ND 30 Famphur ug/L ND ND 30 Fluoranthene ug/L ND ND 30 Fluorene ug/L ND ND 30 Hexachlorobenzene ug/L ND ND 30 Hexachlorocyclopentadiene ug/L ND ND 30 Hexachloroethane ug/L ND ND 30 Hexachloropropene ug/L ND ND 30 Indeno(1,2,3-cd)pyrene ug/L ND ND 30 Isodrin ug/L ND ND 30 Isophorone ug/L ND ND 30 Isosafrole ug/L ND ND 30 Kepone ug/L ND ND 30 Methapyrilene ug/L ND ND 30 Methyl methanesulfonate ug/L ND ND 30 Methyl parathion ug/L ND ND 30 N-Nitroso-di-n-butylamine ug/L ND ND 30 N-Nitroso-di-n-propylamine ug/L ND ND 30 N-Nitrosodiethylamine ug/L ND ND 30 N-Nitrosodimethylamine ug/L ND ND 30 N-Nitrosodiphenylamine ug/L ND ND 30 N-Nitrosomethylethylamine ug/L ND ND 30 N-Nitrosopiperidine ug/L ND ND 30 N-Nitrosopyrrolidine ug/L ND ND 30 Nitrobenzene ug/L ND ND 30 O,O,O-Triethylphosphorothioate ug/L ND ND 30 O-Toluidine ug/L ND ND 30 P-Dimethylaminoazobenzene ug/L ND ND 30 p-Phenylenediamine ug/L ND ND 30 Parathion (Ethyl parathion) ug/L ND ND 30 Pentachlorobenzene ug/L ND ND 30 Pentachloronitrobenzene ug/L ND ND 30 Pentachlorophenol ug/L ND ND 30 Phenacetin ug/L ND ND 30 Phenanthrene ug/L ND ND 30 Phenol ug/L ND ND 30 Phorate ug/L ND ND 30 Pronamide ug/L ND ND 30 Pyrene ug/L ND ND 30 Safrole ug/L ND ND 30 Thionazin ug/L ND ND 30 2,4,6-Tribromophenol (S) % 71 88 23 2-Fluorobiphenyl (S) % 70 88 23 2-Fluorophenol(S) % 32 40 23 Nitrobenzene-d5 (S) % 57 69 20 Phenol-d6 (S) % 20 27 28 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 SAMPLE DUPLICATE: 2018681 92342530004 Dup Max Parameter Units Result Result RPD RPD Terphenyl-d14(S) % 76 60 24 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 QC Batch: 363647 Analysis Method: SM 4500-S2D QC Batch Method: SM 4500-S2D Analysis Description: 4500S2D Sulfide Water Associated Lab Samples: 92342784003, 92342784004 METHOD BLANK: 2016111 Matrix: Water Associated Lab Samples: 92342784003, 92342784004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfide ug/L ND 1000 100 06/06/17 21:30 LABORATORY CONTROL SAMPLE: 2016112 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 528J 106 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2016113 2016114 MS MSD 92342742003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 546J 573J 102 107 80-120 5 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2016115 2016116 MS MSD 92342742013 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 526J 553J 105 111 80-120 5 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 QC Batch: 364584 Analysis Method: SM 4500-CN-E QC Batch Method: SM 4500-CN-E Analysis Description: 450OCNE Cyanide, Total Associated Lab Samples: 92342784003, 92342784004 METHOD BLANK: 2021203 Matrix: Water Associated Lab Samples: 92342784003, 92342784004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Cyanide ug/L ND 10.0 4.0 06/14/1711:34 LABORATORY CONTROL SAMPLE: 2021204 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 99.1 99 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2021205 2021206 MS MSD 92343009001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 94.3 88.3 93 87 80-120 7 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2021207 2021208 MS MSD 92342553005 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L 5.5J 100 100 63.2 62.7 58 57 80-120 1 10 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 49 of 54 Pace Analytical Services, LLC aceAnalXical� 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALIFIERS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92342784 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte PASI-O Pace Analytical Services - Ormond Beach ANALYTE QUALIFIERS L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high. L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated samples may be biased low. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 50 of 54 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: SURRY CLOSED -MT. AIRY (AM) 92342784 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92342784003 MW-11 EPA 3510 363426 EPA 8081 363552 92342784004 SCALE HOUSE EPA 3510 363426 EPA 8081 363552 92342784003 MW-11 EPA 3510 363427 EPA 8082 363555 92342784004 SCALE HOUSE EPA 3510 363427 EPA 8082 363555 92342784003 MW-11 EPA 8151 373221 EPA 8151 373976 92342784004 SCALE HOUSE EPA 8151 373221 EPA 8151 373976 92342784001 MW-6 EPA 3010A 363321 EPA 6010 364621 92342784002 MW-12D EPA 3010A 363321 EPA 6010 364621 92342784003 MW-11 EPA 3010A 363321 EPA 6010 364621 92342784004 SCALE HOUSE EPA 3010A 363321 EPA 6010 364621 92342784001 MW-6 EPA 3010A 363479 EPA 6020B 363773 92342784002 MW-12D EPA 3010A 363479 EPA 6020B 363773 92342784003 MW-11 EPA 3010A 363273 EPA 6020B 363378 92342784004 SCALE HOUSE EPA 3010A 363273 EPA 6020B 363378 92342784003 MW-11 EPA 7470 363333 EPA 7470 363334 92342784004 SCALE HOUSE EPA 7470 363333 EPA 7470 363334 92342784003 MW-11 EPA 3510 364049 EPA 8270 364817 92342784004 SCALE HOUSE EPA 3510 364049 EPA 8270 364817 92342784001 MW-6 EPA 8260 363311 92342784002 MW-12D EPA 8260 363311 92342784003 MW-11 EPA 8260 363311 92342784004 SCALE HOUSE EPA 8260 363311 92342784003 MW-11 SM 4500-S2D 363647 92342784004 SCALE HOUSE SM 4500-S2D 363647 92342784003 MW-11 SM 4500-CN-E 364584 92342784004 SCALE HOUSE SM 4500-CN-E 364584 Date: 06/19/2017 12:26 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 51 of 54 Document Name: Document Revised: Sept. 21, 2016 Sample Condition Upon Receipt(SCUR) Page 1 of 2 �'IceAnalytical a Document No.: Issuing Authority: F-CAR-CS-033-Rev,01 Pace Quality Office Laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ Huntersvill6] Raleigh[] Mechanicsville[] Sample Condition Upon Client Name:Receipt Pr O 342784 Courier: ❑Fe Ex ❑UPS ❑USPS ❑Clien ❑ l �l��l�llti t�tl� Commercial ace ❑Other: 19234 92342784 Custody Seal Present? ❑Yes D<01 Seals Intact? ❑Yes ❑No fir Date/Initials Person Exam Packing Material: ❑Bubble Wrap ubble Bags ❑None ❑Other: Thermometer: ❑ I Gun ID: )Pe of Ice: et [_]Blue Blue ❑None ples on ice, coaling process has begun Correction Factor: Cooler Temp Corrected ('�. Biological Tissue Frozen? ❑Yes [:]No .ErN/A Temp should be above freezing to 6°C USDA Regulated Soil (❑ N/A, water sample) Did samples origina ❑Yes ❑No ein a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (inter tonally, including Hawaii and Puerto Rico)?nYes No Comments/Discrepancy: Chain of Custody Present? es ❑No ❑N/A 1. Samples Arrived within Hold Time? Zes [:]No ❑N/A 2. Short Hold Time Analysis (<72 hr.)? lQYes [:]No El N/A 3. Rush Turn Around Time Requested? ❑Yes ZNo ❑N/A 4. SufficientVolume? ❑Yes iZNo [I N/A S. Correct Containers Used? Zyes ❑No ❑N/A 6. -Pace Containers Used? 2res []No ❑N/A Containers Intact? Zres ❑No ❑N A 7. Samples Field Filtered? ❑Yes ❑No N/A Nate if sediment is visibli in the disspived container Sample Labels Match COC? ❑Yes No ❑N/A F -Includes Date/Time/ID/Analysis Matrix: C 10. Headspace in VOA Vials (>5-6mm)? ❑Yes []No ❑N/A Trip Blank Present? ❑Yes [:]NoN!A 11, Trip Blank Custody Seals Present? ❑Yes []No ❑N!/A LLMN I IYU 1 IHCATIUN/RE50LUTION Person Contacted: Comment_/5ample Discrepancy: Project Manager SCURF Review: — (C Project Manager SRF Review: TC Field Data Required? ❑Yes ❑No Date/Time: Date: & S / Date: S /� Note; Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le, Out of hold, incorrect preservative, out of temp, incorrect containers) Page 52 of 54 Document Name: Sample Condition Upon Receipt(SCUR) aceAnalytical" " Document No.: F-CAR-CS•033-Rev.01 *Check mark top half of box if pH and/or dechlorination Project is verified and within the acceptance range for preservation samples. **Bottom half of box is to list number of bottles Document Revised: Sept. 21, 2016 Page 2of2 Issuing Authority: W4# Office : 9�23142784 PM: RWC Due Date: 06/16/17 CLIENT: 92-Municipal xt E d z -0 a Da u ra a E Ln N a a m a z a a V ra a E d In a. a m a z a a V d I O O a N a m Z ci Z N ci ¢ a V m v — H a an V `r _ N a O N 2 .� a E p en M a m N Y a O z V a E Ln irl z M a m = z 0, v a " z N V .@ a E O a. M a m u v fV = a 2 Q z }, A a E Q u a. a m f6 L7 } 7 W a Z ° C _ E ¢ m _ r-I 0 U' Q a U _ .°1a E w _ r-I 2 N l7 a = ? v m c E ¢ E a ul fV a M l7 Q ry v a O = .n E `m �' ,..� J1 H C7 Q N v V a = ¢ E ON sn [7 Q Q < z U p = ? Q E o N M O ¢ M C7 Q 2 U 2 a O I a 2 U t7 O ? O N 4 Z ¢ O > E O H 0 l7 7 z O E 2 0 l7 7 ¢ V O E a a 0 l7 O z Y o ! a N a b V Y Q 0 7 a > ii N m M, SC U 7 N i Z V) J E N rq r � cn Q z -- U V1 J E O Vl N a in�z n m O W) N y a -J E o Y�i M m m G d u a Z G .� cn J E b l7 Z 47 1 2 V ,3 � 1 r % 3 \X\IN n' 4 1 5 6 7 N \\N 9 10 li 12 I pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot# Page 53 of 54 v L0 0 v CHAIN -OF -CUSTODY 1 Analytical Request Document ce 4nalytc f The Chain -of -Custody is a LEGAL DOCUMENT_ All relevant fields must be completed accurately_ 1L i Section A Section B Section C Required Client Infom7ation: Required Project Information: Invoice Information: FP-9Q - 1 Of 1 Company. Munici al Engineering Services Report To: Jonathan Pfchl Attention. Municipal Engineering Services Address P.O. Box 97 Copy To. Company Name. Garner, NC 27529 Address. Regulatory Agency Email To. jpfohipmesco cam Purchase Order No. Pace quote Reference' Phone. 919-772-5393 Fax Client Project ID SUrry CiCSed-Mt. Airy (AM} Pace Project Manager: Trey Carter Stake! Location Requested Due DaiefTAT. 10 Day (Default) Conlainer Order Number Pace Profile #-, North Carolina Requested Analysis Filtered (YIN) Z COLLECTED Preservatives N N N N N N N N N cv nnnTMX cooE D-W.g Walw a n n SAMPLE ID mar v✓w o START END P L/ One Character per box. smusoua SL a — > VVI a USample amc�a�- N Ids must be unique N, AR rCW ¢rO n cvy OmeOT Tu7a a W z Zm w[d o cmmm QN vf Qa l~it 4 O _ U CATE TIME DATE T�MF g 1 MW 6 Wi G (o( 1 3,00 x I x 2 MW-11 V+T G G 1 ) a d x x x x x x x x 3 3 MW-12D VVT G S 9.35 x x �UU4 Scalehouse Lias �� 4 VVT G fat ( x x x x x x x x 1 5 6 7 8 9 10 11 1 — 12 — ± +H—F. ADDITIONAL COMMENTS LINQUISHED BY / AFFILIATION DATE TIME ACCEPTED BY f AFFILIATION DATE TIME SAMPLE CONDITIONS 6 (a f a — : _. 611� 3� Q, SAMPLER NAME AND SIGNATURE v L) o azMI tn i — PRINT Name of SAMPLER: l v� to y z m 2 } o E z SIGNATURE of SAMPLER: DATE Signed: / �g 3 U rn } I lacieAnalXical" www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 June 19, 2017 Mr. Jonathan Pfohl Municipal Engineering Services 68 Shipwash Dr. Garner, NC 27529 RE: Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory between May 31, 2017 and June 02, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Trey Carter trey. carter@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 166 lacmnalytical' www.pacelabs.corn Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Ormond Beach Certification IDs 8 East Tower Circle, Ormond Beach, FL 32174 Alabama Certification #: 41320 Connecticut Certification #: PH-0216 Delaware Certification: FL NELAC Reciprocity Florida Certification #: E83079 Georgia Certification #: 955 Guam Certification: FL NELAC Reciprocity Hawaii Certification: FL NELAC Reciprocity Illinois Certification #: 200068 Indiana Certification: FL NELAC Reciprocity Kansas Certification #: E-10383 Louisiana Certification #: FL NELAC Reciprocity Louisiana Environmental Certificate #: 05007 Maryland Certification: #346 Michigan Certification #: 9911 Mississippi Certification: FL NELAC Reciprocity Missouri Certification #: 236 Montana Certification #: Cart 0074 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Nebraska Certification: NE-OS-28-14 Nevada Certification: FL NELAC Reciprocity New York Certification #: 11608 North Carolina Environmental Certificate #: 667 North Carolina Certification #: 12710 Oklahoma Certification #: D9947 Pennsylvania Certification #: 68-00547 Puerto Rico Certification M FLO1264 South Carolina Certification: #96042001 Tennessee Certification #: TN02974 Texas Certification: FL NELAC Reciprocity US Virgin Islands Certification: FL NELAC Reciprocity Virginia Environmental Certification #: 460165 Wyoming Certification: FL NELAC Reciprocity West Virginia Certification #: 9962C Wisconsin Certification #: 399079670 Wyoming (EPA Region 8): FL NELAC Reciprocity South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Lab ID Sample ID Matrix Date Collected Date Received 92342478001 MW-3R Water 05/31/17 08:05 05/31/17 15:00 92342478002 MW-23 Water 05/31/1710:10 05/31/17 15:00 92342478003 MW-15 Water 05/31/17 09:30 05/31/17 15:00 92342478004 MW-1 Water 06/01/17 12:35 06/02/17 08:00 92342478005 MW-9 Water 06/01/17 15:40 06/02/17 08:00 92342478006 MW-7 Water 06/01/17 14:45 06/02/17 08:00 92342478007 MW-12S Water 06/01/17 09:50 06/02/17 08:00 92342478008 MW-14 Water 06/01/17 09:00 06/02/17 08:00 92342478009 MW-18 Water 06/01/17 10:15 06/02/17 08:00 92342478010 MW-19 Water 05/31/17 09:00 06/02/17 08:00 92342478011 MW-20 Water 06/01/17 15:30 06/02/17 08:00 92342530001 MW-13 Water 05/31/17 17:35 06/01/17 07:55 92342530002 MW-16 Water 05/31/17 16:50 06/01/17 07:55 92342530003 MW-17 Water 05/31/17 16:30 06/01/17 07:55 92342530004 MW-21 Water 05/31/17 17:20 06/01/17 07:55 92342530005 MW-22 Water 05/31/17 16:10 06/01/17 07:55 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: SURRY CLOSED -MT. AIRY (UIC) 92342478 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92342478001 MW-3R EPA6010 SH1 14 PASI-A EPA 6020E CDF 1 PASI-A EPA 8260 ZDO 50 PASI-C 92342478002 MW-23 EPA6010 SH1 14 PASI-A EPA 6020E CDF 1 PASI-A EPA 8260 ZDO 50 PASI-C 92342478003 MW-15 EPA 8081 RES 21 PASI-C EPA 8082 HSK 8 PASI-C EPA 8151 LJM 6 PASI-O EPA6010 SH1 15 PASI-A EPA 6020E CDF 1 PASI-A EPA 7470 KAL 1 PASI-A EPA 8270 BPJ 111 PASI-C EPA 8260 ZDO 67 PASI-C SM 4500-S2D MVC 1 PASI-A SM 4500-CN-E AES2 1 PASI-A 92342478004 MW-1 EPA 8081 RES 21 PASI-C EPA 8082 HSK 8 PASI-C EPA 8151 LJM 6 PASI-O EPA6010 SH1 15 PASI-A EPA 6020E CDF 1 PASI-A EPA 7470 WAB 1 PASI-A EPA 8270 BPJ 111 PASI-C EPA 8260 GAW 67 PASI-C 92342478005 MW-9 EPA 8081 RES 21 PASI-C EPA 8082 HSK 8 PASI-C EPA 8151 LJM 6 PASI-O EPA6010 SH1 15 PASI-A EPA 6020E CDF 1 PASI-A EPA 7470 WAB 1 PASI-A EPA 8270 BPJ 111 PASI-C EPA 8260 GAW 67 PASI-C 92342478006 MW-7 EPA6010 SH1 14 PASI-A EPA 6020E CDF 1 PASI-A EPA 8260 GAW 50 PASI-C 92342478007 MW-12S EPA6010 SH1 14 PASI-A EPA 6020E CDF 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Lab ID Sample ID Method Analysts Analytes Reported Laboratory EPA 8260 GAW 50 PASI-C 92342478008 MW-14 EPA6010 SH1 14 PASI-A EPA 6020E CDF 1 PASI-A EPA 8260 GAW 50 PASI-C 92342478009 MW-18 EPA6010 SH1 14 PASI-A EPA 6020E CDF 1 PASI-A EPA 8260 GAW 50 PASI-C 92342478010 MW-19 EPA6010 SH1 14 PASI-A EPA 6020E CDF 1 PASI-A EPA 8260 GAW 50 PASI-C 92342478011 MW-20 EPA6010 SH1 14 PASI-A EPA 6020E CDF 1 PASI-A EPA 8260 GAW 50 PASI-C 92342530001 MW-13 EPA 8081 RES 21 PASI-C EPA 8082 HSK 8 PASI-C EPA 8151 LJM 6 PASI-O EPA6010 SH1 15 PASI-A EPA 6020E CDF 1 PASI-A EPA 7470 KAL 1 PASI-A EPA 8270 BPJ 111 PASI-C EPA 8260 ZDO 67 PASI-C SM 4500-S2D MVC 1 PASI-A SM 4500-CN-E AES2 1 PASI-A 92342530002 MW-16 EPA 8081 RES 21 PASI-C EPA 8082 HSK 8 PASI-C EPA 8151 LJM 6 PASI-O EPA6010 SH1 15 PASI-A EPA 6020E CDF 1 PASI-A EPA 7470 KAL 1 PASI-A EPA 8270 BPJ 111 PASI-C EPA 8260 ZDO 67 PASI-C SM 4500-S2D MVC 1 PASI-A SM 4500-CN-E AES2 1 PASI-A 92342530003 MW-17 EPA 8081 RES 21 PASI-C EPA 8082 HSK 8 PASI-C EPA 8151 LJM 6 PASI-O EPA6010 SH1 15 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 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AIRY (UIC) Pace Project No.: 92342478 Lab ID Sample ID Method Analysts Analytes Reported Laboratory EPA 6020E CDF 1 PASI-A EPA 7470 KAL 1 PASI-A EPA 8270 BPJ 111 PASI-C EPA 8260 ZDO 67 PASI-C SM 4500-S2D MVC 1 PASI-A SM 4500-CN-E AES2 1 PASI-A 92342530004 MW-21 EPA 8081 RES 21 PASI-C EPA 8082 HSK 8 PASI-C EPA 8151 LJM 6 PASI-O EPA6010 SH1 15 PASI-A EPA 6020E CDF 1 PASI-A EPA 7470 KAL 1 PASI-A EPA 8270 BPJ 111 PASI-C EPA 8260 GAW 67 PASI-C SM 4500-S2D MVC 1 PASI-A SM 4500-CN-E AES2 1 PASI-A 92342530005 MW-22 EPA 8081 RES 21 PASI-C EPA 8082 HSK 8 PASI-C EPA 8151 LJM 6 PASI-O EPA6010 SH1 15 PASI-A EPA 6020E CDF 1 PASI-A EPA 7470 KAL 1 PASI-A EPA 8270 BPJ 111 PASI-C EPA 8260 ZDO 67 PASI-C SM 4500-S2D MVC 1 PASI-A SM 4500-CN-E AES2 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-3R Lab ID: 92342478001 Collected: 05/31/17 08:05 Received: 05/31/17 15:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Vanadium Zinc 6020 MET ICPMS Thallium 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane Date: 06/19/2017 01:10 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 06/02/1715:20 06/09/1718:25 7440-36-0 ND ug/L 10.0 5.0 1 06/02/1715:20 06/09/1718:25 7440-38-2 7.4J ug/L 100 2.5 1 06/02/1715:20 06/09/1718:25 7440-39-3 ND ug/L 1.0 0.50 1 06/02/1715:20 06/09/1718:25 7440-41-7 ND ug/L 1.0 0.50 1 06/02/1715:20 06/09/1718:25 7440-43-9 ND ug/L 10.0 2.5 1 06/02/1715:20 06/09/1718:25 7440-47-3 ND ug/L 10.0 2.5 1 06/02/1715:20 06/09/1718:25 7440-48-4 4.2J ug/L 10.0 2.5 1 06/02/1715:20 06/09/1718:25 7440-50-8 ND ug/L 10.0 2.5 1 06/02/1715:20 06/09/1718:25 7439-92-1 ND ug/L 50.0 2.5 1 06/02/1715:20 06/09/1718:25 7440-02-0 ND ug/L 10.0 5.0 1 06/02/1715:20 06/09/1718:25 7782-49-2 ND ug/L 10.0 2.5 1 06/02/1715:20 06/09/1718:25 7440-22-4 ND ug/L 25.0 2.5 1 06/02/1715:20 06/09/1718:25 7440-62-2 ND ug/L 10.0 5.0 1 06/02/1715:20 06/09/1718:25 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3010A ND ug/L 5.5 0.020 1 06/03/17 02:25 06/07/17 15:40 7440-28-0 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 06/02/17 01:30 67-64-1 ND ug/L 200 1.9 1 06/02/17 01:30 107-13-1 ND ug/L 1.0 0.25 1 06/02/17 01:30 71-43-2 ND ug/L 3.0 0.17 1 06/02/17 01:30 74-97-5 ND ug/L 1.0 0.18 1 06/02/17 01:30 75-27-4 ND ug/L 3.0 0.26 1 06/02/17 01:30 75-25-2 ND ug/L 10.0 0.29 1 06/02/17 01:30 74-83-9 ND ug/L 100 0.96 1 06/02/17 01:30 78-93-3 ND ug/L 100 1.2 1 06/02/17 01:30 75-15-0 ND ug/L 1.0 0.25 1 06/02/17 01:30 56-23-5 ND ug/L 3.0 0.23 1 06/02/17 01:30 108-90-7 ND ug/L 10.0 0.54 1 06/02/17 01:30 75-00-3 ND ug/L 5.0 0.14 1 06/02/17 01:30 67-66-3 ND ug/L 1.0 0.11 1 06/02/17 01:30 74-87-3 ND ug/L 13.0 2.0 1 06/02/17 01:30 96-12-8 ND ug/L 3.0 0.21 1 06/02/17 01:30 124-48-1 ND ug/L 1.0 0.27 1 06/02/17 01:30 106-93-4 ND ug/L 10.0 0.21 1 06/02/17 01:30 74-95-3 ND ug/L 5.0 0.30 1 06/02/17 01:30 95-50-1 ND ug/L 1.0 0.33 1 06/02/17 01:30 106-46-7 ND ug/L 100 1.0 1 06/02/17 01:30 110-57-6 ND ug/L 5.0 0.32 1 06/02/17 01:30 75-34-3 ND ug/L 1.0 0.24 1 06/02/17 01:30 107-06-2 ND ug/L 5.0 0.56 1 06/02/17 01:30 75-35-4 ND ug/L 5.0 0.19 1 06/02/17 01:30 156-59-2 ND ug/L 5.0 0.49 1 06/02/17 01:30 156-60-5 ND ug/L 1.0 0.27 1 06/02/17 01:30 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. M1 Page 7 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-3R Lab ID: 92342478001 Collected: 05/31/17 08:05 Received: 05/31/17 15:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/02/17 01:30 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/02/17 01:30 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/02/17 01:30 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/02/17 01:30 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/02/17 01:30 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/02/17 01:30 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/02/17 01:30 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/02/17 01:30 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/02/17 01:30 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/02/17 01:30 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/02/17 01:30 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/02/17 01:30 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/02/17 01:30 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/02/17 01:30 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/02/17 01:30 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/02/17 01:30 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/02/17 01:30 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/02/17 01:30 108-05-4 M1 Vinyl chloride ND ug/L 1.0 0.62 1 06/02/17 01:30 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/02/17 01:30 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 115 % 70-130 1 06/02/17 01:30 460-00-4 1,2-Dichloroethane-d4 (S) 99 % 70-130 1 06/02/17 01:30 17060-07-0 Toluene-d8 (S) 112 % 70-130 1 06/02/17 01:30 2037-26-5 Date: 06/19/2017 01:10 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-23 Lab ID: 92342478002 Collected: 05/31/17 10:10 Received: 05/31/17 15:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 301 OA Antimony ND ug/L 6.0 3.9 1 06/02/1715:20 06/09/1718:28 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/02/1715:20 06/09/1718:28 7440-38-2 Barium 33.8J ug/L 100 2.5 1 06/02/1715:20 06/09/1718:28 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 06/02/1715:20 06/09/1718:28 7440-41-7 Cadmium 2.1 ug/L 1.0 0.50 1 06/02/1715:20 06/09/1718:28 7440-43-9 Chromium ND ug/L 10.0 2.5 1 06/02/1715:20 06/09/1718:28 7440-47-3 Cobalt ND ug/L 10.0 2.5 1 06/02/1715:20 06/09/1718:28 7440-48-4 Copper 5.OJ ug/L 10.0 2.5 1 06/02/1715:20 06/09/1718:28 7440-50-8 Lead ND ug/L 10.0 2.5 1 06/02/1715:20 06/09/1718:28 7439-92-1 Nickel ND ug/L 50.0 2.5 1 06/02/1715:20 06/09/1718:28 7440-02-0 Selenium ND ug/L 10.0 5.0 1 06/02/1715:20 06/09/1718:28 7782-49-2 Silver ND ug/L 10.0 2.5 1 06/02/1715:20 06/09/1718:28 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 06/02/1715:20 06/09/1718:28 7440-62-2 Zinc 6.5J ug/L 10.0 5.0 1 06/02/1715:20 06/09/1718:28 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Thallium 0.024J ug/L 5.5 0.020 1 06/03/17 02:25 06/06/17 18:59 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 06/02/17 01:47 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 06/02/17 01:47 107-13-1 Benzene ND ug/L 1.0 0.25 1 06/02/17 01:47 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 06/02/17 01:47 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 06/02/17 01:47 75-27-4 Bromoform ND ug/L 3.0 0.26 1 06/02/17 01:47 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 06/02/17 01:47 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 06/02/17 01:47 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 06/02/17 01:47 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 06/02/17 01:47 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 06/02/17 01:47 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 06/02/17 01:47 75-00-3 Chloroform ND ug/L 5.0 0.14 1 06/02/17 01:47 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 06/02/17 01:47 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 06/02/17 01:47 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 06/02/17 01:47 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 06/02/17 01:47 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 06/02/17 01:47 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 06/02/17 01:47 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 06/02/17 01:47 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/02/17 01:47 110-57-6 1,1-Dichloroethane 0.43J ug/L 5.0 0.32 1 06/02/17 01:47 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 06/02/17 01:47 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/02/17 01:47 75-35-4 cis-1,2-Dichloroethene 0.39J ug/L 5.0 0.19 1 06/02/17 01:47 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/02/17 01:47 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 06/02/17 01:47 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-23 Lab ID: 92342478002 Collected: 05/31/17 10:10 Received: 05/31/17 15:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/02/17 01:47 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/02/17 01:47 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/02/17 01:47 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/02/17 01:47 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/02/17 01:47 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/02/17 01:47 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/02/17 01:47 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/02/17 01:47 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/02/17 01:47 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/02/17 01:47 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/02/17 01:47 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/02/17 01:47 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/02/17 01:47 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/02/17 01:47 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/02/17 01:47 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/02/17 01:47 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/02/17 01:47 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/02/17 01:47 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/02/17 01:47 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/02/17 01:47 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 113 % 70-130 1 06/02/17 01:47 460-00-4 1,2-Dichloroethane-d4 (S) 100 % 70-130 1 06/02/17 01:47 17060-07-0 Toluene-d8 (S) 111 % 70-130 1 06/02/17 01:47 2037-26-5 Date: 06/19/2017 01:10 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-15 Lab ID: 92342478003 Collected: 05/31/17 09:30 Received: 05/31/17 15:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 Organochlorine Pesticides Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Surrogates Decachlorobiphenyl (S) 8151 Chlorinated Herbicides 2,4-D Dinoseb Pentachlorophenol 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 6010 MET ICP Antimony Arsenic Date: 06/19/2017 01:10 PM Analytical Method: EPA 8081 Preparation Method: EPA 3510 ND ug/L 0.050 0.050 1 06/02/1710:09 06/06/1719:11 309-00-2 ND ug/L 0.050 0.050 1 06/02/1710:09 06/06/1719:11 319-84-6 ND ug/L 0.050 0.050 1 06/02/1710:09 06/06/1719:11 319-85-7 ND ug/L 0.050 0.050 1 06/02/1710:09 06/06/1719:11 319-86-8 ND ug/L 0.050 0.050 1 06/02/1710:09 06/06/1719:11 58-89-9 ND ug/L 0.50 0.20 1 06/02/1710:09 06/06/1719:11 57-74-9 ND ug/L 0.10 0.050 1 06/02/1710:09 06/06/1719:11 72-54-8 ND ug/L 0.10 0.050 1 06/02/1710:09 06/06/1719:11 72-55-9 ND ug/L 0.10 0.050 1 06/02/1710:09 06/06/1719:11 50-29-3 ND ug/L 0.075 0.050 1 06/02/1710:09 06/06/1719:11 60-57-1 ND ug/L 0.10 0.050 1 06/02/1710:09 06/06/1719:11 959-98-8 ND ug/L 0.10 0.050 1 06/02/1710:09 06/06/1719:11 33213-65-9 ND ug/L 0.10 0.050 1 06/02/1710:09 06/06/1719:11 1031-07-8 ND ug/L 0.10 0.050 1 06/02/1710:09 06/06/1719:11 72-20-8 ND ug/L 0.10 0.050 1 06/02/1710:09 06/06/1719:11 7421-93-4 ND ug/L 0.050 0.050 1 06/02/1710:09 06/06/1719:11 76-44-8 ND ug/L 0.075 0.050 1 06/02/1710:09 06/06/1719:11 1024-57-3 ND ug/L 1.0 0.15 1 06/02/1710:09 06/06/1719:11 72-43-5 ND ug/L 1.5 0.20 1 06/02/1710:09 06/06/1719:11 8001-35-2 95 % 20-130 1 06/02/1710:09 06/06/1719:11 877-09-8 54 % 20-130 1 06/02/1710:09 06/06/1719:11 2051-24-3 Analytical Method: EPA 8082 Preparation Method: EPA 3510 ND ug/L 0.50 0.50 1 06/02/1710:09 06/02/1719:52 12674-11-2 ND ug/L 0.50 0.50 1 06/02/1710:09 06/02/1719:52 11104-28-2 ND ug/L 0.50 0.50 1 06/02/1710:09 06/02/1719:52 11141-16-5 ND ug/L 0.50 0.50 1 06/02/1710:09 06/02/1719:52 53469-21-9 ND ug/L 0.50 0.50 1 06/02/1710:09 06/02/1719:52 12672-29-6 ND ug/L 0.50 0.50 1 06/02/1710:09 06/02/1719:52 11097-69-1 ND ug/L 0.50 0.50 1 06/02/1710:09 06/02/1719:52 11096-82-5 47 % 10-132 1 06/02/1710:09 06/02/1719:52 2051-24-3 Analytical Method: EPA 8151 Preparation Method: EPA 8151 ND ug/L 0.91 0.22 1 06/02/17 16:30 06/06/17 06:46 94-75-7 ND ug/L 0.18 0.055 1 06/02/17 16:30 06/06/17 06:46 88-85-7 ND ug/L 0.028 0.017 1 06/02/17 16:30 06/06/17 06:46 87-86-5 ND ug/L 0.18 0.041 1 06/02/17 16:30 06/06/17 06:46 93-76-5 ND ug/L 0.18 0.048 1 06/02/17 16:30 06/06/17 06:46 93-72-1 75 % 39-139 1 06/02/17 16:30 06/06/17 06:46 19719-28-9 Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 06/02/1715:20 06/09/1716:27 7440-36-0 ND ug/L 10.0 5.0 1 06/02/1715:20 06/09/1716:27 7440-38-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-15 Lab ID: 92342478003 Collected: 05/31/17 09:30 Received: 05/31/17 15:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Tin Vanadium Zinc 6020 MET ICPMS Thallium 7470 Mercury Mercury 8270 MSSV Semivolatile Organic Acenaphthene Acenaphthylene Acetophenone 2-Acetylaminofluorene 4-Aminobiphenyl Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-ChIoro-3-methyl phenol 4-Chloroaniline Chlorobenzilate bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Diallate Dibenz(a,h)anthracene Date: 06/19/2017 01:10 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010A 49.2J ug/L 100 2.5 1 06/02/1715:20 06/09/1716:27 7440-39-3 ND ug/L 1.0 0.50 1 06/02/1715:20 06/09/1716:27 7440-41-7 ND ug/L 1.0 0.50 1 06/02/1715:20 06/09/1716:27 7440-43-9 ND ug/L 10.0 2.5 1 06/02/1715:20 06/09/1716:27 7440-47-3 2.7J ug/L 10.0 2.5 1 06/02/1715:20 06/09/1716:27 7440-48-4 ND ug/L 10.0 2.5 1 06/02/1715:20 06/09/1716:27 7440-50-8 ND ug/L 10.0 2.5 1 06/02/1715:20 06/09/1716:27 7439-92-1 3.1J ug/L 50.0 2.5 1 06/02/1715:20 06/09/1716:27 7440-02-0 ND ug/L 10.0 5.0 1 06/02/1715:20 06/09/1716:27 7782-49-2 ND ug/L 10.0 2.5 1 06/02/1715:20 06/09/1716:27 7440-22-4 ND ug/L 100 2.5 1 06/02/1715:20 06/09/1716:27 7440-31-5 3.1J ug/L 25.0 2.5 1 06/02/1715:20 06/09/1716:27 7440-62-2 10.7 ug/L 10.0 5.0 1 06/02/1715:20 06/09/1716:27 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3010A 0.0911 ug/L 5.5 0.020 1 06/03/17 02:25 06/06/17 19:01 7440-28-0 Analytical Method: EPA 7470 Preparation Method: EPA 7470 ND ug/L 0.20 0.10 1 06/04/17 20:45 06/07/17 02:29 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ug/L 10.0 1.6 1 06/07/1716:10 06/13/1718:57 83-32-9 ND ug/L 10.0 1.5 1 06/07/1716:10 06/13/1718:57 208-96-8 ND ug/L 10.0 1.9 1 06/07/1716:10 06/13/1718:57 98-86-2 ND ug/L 20.0 1.6 1 06/07/1716:10 06/13/1718:57 53-96-3 ND ug/L 20.0 1.7 1 06/07/1716:10 06/13/1718:57 92-67-1 ND ug/L 10.0 1.7 1 06/07/1716:10 06/13/1718:57 120-12-7 ND ug/L 10.0 2.1 1 06/07/1716:10 06/13/1718:57 56-55-3 ND ug/L 10.0 2.2 1 06/07/1716:10 06/13/1718:57 50-32-8 ND ug/L 10.0 2.2 1 06/07/1716:10 06/13/1718:57 205-99-2 ND ug/L 10.0 2.1 1 06/07/1716:10 06/13/1718:57 191-24-2 ND ug/L 10.0 2.0 1 06/07/1716:10 06/13/1718:57 207-08-9 ND ug/L 20.0 3.1 1 06/07/1716:10 06/13/1718:57 100-51-6 ND ug/L 10.0 1.5 1 06/07/1716:10 06/13/1718:57 101-55-3 ND ug/L 10.0 2.5 1 06/07/1716:10 06/13/1718:57 85-68-7 ND ug/L 20.0 2.8 1 06/07/1716:10 06/13/1718:57 59-50-7 ND ug/L 20.0 2.8 1 06/07/1716:10 06/13/1718:57 106-47-8 ND ug/L 10.0 2.2 1 06/07/1716:10 06/13/1718:57 510-15-6 ND ug/L 10.0 1.6 1 06/07/1716:10 06/13/1718:57 111-91-1 ND ug/L 10.0 1.7 1 06/07/1716:10 06/13/1718:57 111-44-4 ND ug/L 10.0 1.6 1 06/07/1716:10 06/13/1718:57 91-58-7 ND ug/L 10.0 1.5 1 06/07/1716:10 06/13/1718:57 95-57-8 ND ug/L 10.0 1.6 1 06/07/1716:10 06/13/1718:57 7005-72-3 ND ug/L 10.0 2.1 1 06/07/1716:10 06/13/1718:57 218-01-9 ND ug/L 10.0 1.6 1 06/07/1716:10 06/13/1718:57 2303-16-4 ND ug/L 10.0 2.0 1 06/07/1716:10 06/13/1718:57 53-70-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. L2 L2 L2 L2 L2 L2 Page 12 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-15 Lab ID: 92342478003 Collected: 05/31/17 09:30 Received: 05/31/17 15:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Dibenzofuran ND ug/L 10.0 1.7 1 06/07/17 16:10 06/13/17 18:57 132-64-9 3,3'-Dichlorobenzidine ND ug/L 20.0 3.9 1 06/07/17 16:10 06/13/17 18:57 91-94-1 2,4-Dichlorophenol ND ug/L 10.0 1.6 1 06/07/17 16:10 06/13/17 18:57 120-83-2 2,6-Dichlorophenol ND ug/L 10.0 1.5 1 06/07/17 16:10 06/13/17 18:57 87-65-0 Diethylphthalate ND ug/L 6000 1.6 1 06/07/17 16:10 06/13/17 18:57 84-66-2 Dimethoate ND ug/L 20.0 1.8 1 06/07/17 16:10 06/13/17 18:57 60-51-5 P-Dimethylaminoazobenzene ND ug/L 10.0 1.0 1 06/07/17 16:10 06/13/17 18:57 60-11-7 7,12-Dimethylbenz(a)anthracene ND ug/L 10.0 2.4 1 06/07/17 16:10 06/13/17 18:57 57-97-6 3,3'-Dimethylbenzidine ND ug/L 10.0 3.9 1 06/07/17 16:10 06/13/17 18:57 119-93-7 2,4-Dimethylphenol ND ug/L 10.0 1.6 1 06/07/17 16:10 06/13/17 18:57 105-67-9 Dimethylphthalate ND ug/L 10.0 1.4 1 06/07/17 16:10 06/13/17 18:57 131-11-3 Di-n-butylphthalate ND ug/L 10.0 2.0 1 06/07/17 16:10 06/13/17 18:57 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 50.0 2.2 1 06/07/17 16:10 06/13/17 18:57 534-52-1 1,3-Dinitrobenzene ND ug/L 20.0 1.3 1 06/07/17 16:10 06/13/17 18:57 99-65-0 2,4-Dinitrophenol ND ug/L 50.0 5.1 1 06/07/17 16:10 06/13/17 18:57 51-28-5 2,4-Dinitrotoluene ND ug/L 10.0 1.5 1 06/07/17 16:10 06/13/17 18:57 121-14-2 2,6-Dinitrotoluene ND ug/L 10.0 1.4 1 06/07/17 16:10 06/13/17 18:57 606-20-2 Di-n-octylphthalate ND ug/L 10.0 1.5 1 06/07/17 16:10 06/13/17 18:57 117-84-0 Diphenylamine ND ug/L 10.0 1.4 1 06/07/17 16:10 06/13/17 18:57 122-39-4 Disulfoton ND ug/L 10.0 1.5 1 06/07/17 16:10 06/13/17 18:57 298-04-4 bis(2- Ethyl hexyl)phthalate ND ug/L 15.0 2.3 1 06/07/17 16:10 06/13/17 18:57 117-81-7 Ethyl methanesulfonate ND ug/L 20.0 1.6 1 06/07/17 16:10 06/13/17 18:57 62-50-0 Famphur ND ug/L 20.0 5.7 1 06/07/17 16:10 06/13/17 18:57 52-85-7 Fluoranthene ND ug/L 10.0 2.2 1 06/07/17 16:10 06/13/17 18:57 206-44-0 Fluorene ND ug/L 10.0 1.6 1 06/07/17 16:10 06/13/17 18:57 86-73-7 Hexachlorobenzene ND ug/L 10.0 1.7 1 06/07/17 16:10 06/13/17 18:57 118-74-1 Hexachlorocyclopentadiene ND ug/L 10.0 1.3 1 06/07/17 16:10 06/13/17 18:57 77-47-4 Hexachloroethane ND ug/L 10.0 1.8 1 06/07/17 16:10 06/13/17 18:57 67-72-1 Hexachloropropene ND ug/L 10.0 1.2 1 06/07/17 16:10 06/13/17 18:57 1888-71-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 2.0 1 06/07/17 16:10 06/13/17 18:57 193-39-5 Isodrin ND ug/L 20.0 2.5 1 06/07/17 16:10 06/13/17 18:57 465-73-6 Isophorone ND ug/L 10.0 1.5 1 06/07/17 16:10 06/13/17 18:57 78-59-1 Isosafrole ND ug/L 10.0 1.5 1 06/07/17 16:10 06/13/17 18:57 120-58-1 Kepone ND ug/L 20.0 4.5 1 06/07/17 16:10 06/13/17 18:57 143-50-0 Methapyrilene ND ug/L 100 3.0 1 06/07/17 16:10 06/13/17 18:57 91-80-5 3-Methylcholanthrene ND ug/L 10.0 2.7 1 06/07/17 16:10 06/13/17 18:57 56-49-5 Methyl methanesulfonate ND ug/L 10.0 1.1 1 06/07/17 16:10 06/13/17 18:57 66-27-3 2-Methylnaphthalene ND ug/L 10.0 1.4 1 06/07/17 16:10 06/13/17 18:57 91-57-6 Methyl parathion ND ug/L 10.0 1.6 1 06/07/17 16:10 06/13/17 18:57 298-00-0 2-Methylphenol(o-Cresol) ND ug/L 10.0 1.6 1 06/07/17 16:10 06/13/17 18:57 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/L 10.0 1.4 1 06/07/17 16:10 06/13/17 18:57 15831-10-4 1-Naphthalenamine ND ug/L 10.0 1.3 1 06/07/17 16:10 06/13/17 18:57 134-32-7 2-Naphthalenamine ND ug/L 10.0 2.2 1 06/07/17 16:10 06/13/17 18:57 91-59-8 1,4-Naphthoquinone ND ug/L 10.0 0.99 1 06/07/17 16:10 06/13/17 18:57 130-15-4 2-Nitroaniline ND ug/L 50.0 2.3 1 06/07/17 16:10 06/13/17 18:57 88-74-4 3-Nitroaniline ND ug/L 50.0 2.7 1 06/07/17 16:10 06/13/17 18:57 99-09-2 REPORT OF LABORATORY ANALYSIS L2 L2 L2 L2 L2 L2 L2 L2 L2 L2 L2 This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-15 Lab ID: 92342478003 Collected: 05/31/17 09:30 Received: 05/31/17 15:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol 5-Nitro-o-toluidine N-Nitrosodiethylamine N-Nitrosodimethylamine N-Nitroso-di-n-butylamine N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine N-Nitrosomethylethylamine N-Nitrosopiperidine N-Nitrosopyrrolidine O,O,O-Triethylphosphorothioate 2,2'-Oxybis(1-chloropropane) Parathion (Ethyl parathion) Pentachlorobenzene Pentachloronitrobenzene Pentachlorophenol Phenacetin Phenanthrene Phenol p-Phenylenediamine Phorate Pronamide Pyrene Safrole 1,2,4,5-Tetrachlorobenzene 2,3,4,6-Tetrachlorophenol Thionazin O-Toluidine 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 1,3,5-Trinitrobenzene Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) 8260 MSV Low Level Landfill Acetone Acetonitrile Acrolein Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ug/L 20.0 3.4 1 06/07/1716:10 06/13/1718:57 100-01-6 ND ug/L 10.0 1.6 1 06/07/1716:10 06/13/1718:57 98-95-3 L2 ND ug/L 10.0 1.6 1 06/07/1716:10 06/13/1718:57 88-75-5 L2 ND ug/L 50.0 4.3 1 06/07/1716:10 06/13/1718:57 100-02-7 ND ug/L 10.0 1.9 1 06/07/1716:10 06/13/1718:57 99-55-8 L2 ND ug/L 20.0 1.4 1 06/07/1716:10 06/13/1718:57 55-18-5 L2 ND ug/L 10.0 1.6 1 06/07/1716:10 06/13/1718:57 62-75-9 ND ug/L 10.0 1.6 1 06/07/1716:10 06/13/1718:57 924-16-3 L2 ND ug/L 10.0 1.7 1 06/07/1716:10 06/13/1718:57 621-64-7 L2 ND ug/L 10.0 1.4 1 06/07/1716:10 06/13/1718:57 86-30-6 ND ug/L 10.0 1.4 1 06/07/1716:10 06/13/1718:57 10595-95-6 L2 ND ug/L 20.0 1.7 1 06/07/1716:10 06/13/1718:57 100-75-4 L2 ND ug/L 10.0 1.7 1 06/07/1716:10 06/13/1718:57 930-55-2 L2 ND ug/L 10.0 1.7 1 06/07/1716:10 06/13/1718:57 126-68-1 L2 ND ug/L 10.0 1.8 1 06/07/1716:10 06/13/1718:57 108-60-1 ND ug/L 10.0 1.5 1 06/07/1716:10 06/13/1718:57 56-38-2 L2 ND ug/L 10.0 1.5 1 06/07/1716:10 06/13/1718:57 608-93-5 ND ug/L 20.0 1.7 1 06/07/1716:10 06/13/1718:57 82-68-8 ND ug/L 25.0 3.5 1 06/07/1716:10 06/13/1718:57 87-86-5 ND ug/L 20.0 1.9 1 06/07/1716:10 06/13/1718:57 62-44-2 ND ug/L 10.0 1.6 1 06/07/1716:10 06/13/1718:57 85-01-8 ND ug/L 10.0 1.3 1 06/07/1716:10 06/13/1718:57 108-95-2 ND ug/L 10.0 2.2 1 06/07/1716:10 06/13/1718:57 106-50-3 L2 ND ug/L 10.0 1.7 1 06/07/1716:10 06/13/1718:57 298-02-2 L2 ND ug/L 10.0 2.0 1 06/07/1716:10 06/13/1718:57 23950-58-5 L2 ND ug/L 10.0 2.2 1 06/07/1716:10 06/13/1718:57 129-00-0 ND ug/L 10.0 1.3 1 06/07/1716:10 06/13/1718:57 94-59-7 L2 ND ug/L 10.0 1.3 1 06/07/1716:10 06/13/1718:57 95-94-3 ND ug/L 10.0 2.9 1 06/07/1716:10 06/13/1718:57 58-90-2 ND ug/L 20.0 1.7 1 06/07/1716:10 06/13/1718:57 297-97-2 L2 ND ug/L 10.0 1.7 1 06/07/1716:10 06/13/1718:57 95-53-4 L2 ND ug/L 10.0 1.5 1 06/07/1716:10 06/13/1718:57 95-95-4 ND ug/L 10.0 1.4 1 06/07/1716:10 06/13/1718:57 88-06-2 ND ug/L 10.0 1.2 1 06/07/1716:10 06/13/1718:57 99-35-4 L2 80 % 21-110 1 06/07/1716:10 06/13/1718:57 4165-60-0 1g 101 % 27-110 1 06/07/1716:10 06/13/1718:57 321-60-8 104 % 31-107 1 06/07/1716:10 06/13/1718:57 1718-51-0 33 % 10-110 1 06/07/1716:10 06/13/1718:57 13127-88-3 49 % 12-110 1 06/07/1716:10 06/13/1718:57 367-12-4 86 % 27-110 1 06/07/1716:10 06/13/1718:57 118-79-6 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 ND ug/L 55.0 2.2 1 ND ug/L 53.0 1.6 1 REPORT OF LABORATORY ANALYSIS 06/02/17 02:22 67-64-1 06/02/17 02:22 75-05-8 06/02/17 02:22 107-02-8 This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-15 Lab ID: 92342478003 Collected: 05/31/17 09:30 Received: 05/31/17 15:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acrylonitrile ND ug/L 200 1.9 1 06/02/17 02:22 107-13-1 Allyl chloride ND ug/L 10.0 1.5 1 06/02/17 02:22 107-05-1 Benzene 0.65J ug/L 1.0 0.25 1 06/02/17 02:22 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 06/02/17 02:22 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 06/02/17 02:22 75-27-4 Bromoform ND ug/L 3.0 0.26 1 06/02/17 02:22 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 06/02/17 02:22 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 06/02/17 02:22 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 06/02/17 02:22 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 06/02/17 02:22 56-23-5 Chlorobenzene 2.4J ug/L 3.0 0.23 1 06/02/17 02:22 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 06/02/17 02:22 75-00-3 Chloroform ND ug/L 5.0 0.14 1 06/02/17 02:22 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 06/02/17 02:22 74-87-3 Chloroprene ND ug/L 20.0 0.27 1 06/02/17 02:22 126-99-8 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 06/02/17 02:22 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 06/02/17 02:22 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 06/02/17 02:22 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 06/02/17 02:22 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 06/02/17 02:22 95-50-1 1,3-Dichlorobenzene ND ug/L 5.0 0.24 1 06/02/17 02:22 541-73-1 1,4-Dichlorobenzene 3.7 ug/L 1.0 0.33 1 06/02/17 02:22 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/02/17 02:22 110-57-6 Dichlorodifluoromethane ND ug/L 5.0 0.21 1 06/02/17 02:22 75-71-8 1,1-Dichloroethane 9.7 ug/L 5.0 0.32 1 06/02/17 02:22 75-34-3 1,2-Dichloroethane 0.58J ug/L 1.0 0.24 1 06/02/17 02:22 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/02/17 02:22 75-35-4 cis-1,2-Dichloroethene 33.3 ug/L 5.0 0.19 1 06/02/17 02:22 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/02/17 02:22 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 06/02/17 02:22 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 06/02/17 02:22 142-28-9 2,2-Dichloropropane ND ug/L 15.0 0.13 1 06/02/17 02:22 594-20-7 1,1-Dichloropropene ND ug/L 5.0 0.49 1 06/02/17 02:22 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/02/17 02:22 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/02/17 02:22 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/02/17 02:22 100-41-4 Ethyl methacrylate ND ug/L 10.0 0.20 1 06/02/17 02:22 97-63-2 Hexachloro-1,3-butadiene ND ug/L 10.0 0.71 1 06/02/17 02:22 87-68-3 2-Hexanone ND ug/L 50.0 0.46 1 06/02/17 02:22 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/02/17 02:22 74-88-4 Isobutanol ND ug/L 100 35.0 1 06/02/17 02:22 78-83-1 Methacrylonitrile ND ug/L 100 0.93 1 06/02/17 02:22 126-98-7 Methylene Chloride ND ug/L 1.0 0.97 1 06/02/17 02:22 75-09-2 Methyl methacrylate ND ug/L 30.0 2.0 1 06/02/17 02:22 80-62-6 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/02/17 02:22 108-10-1 Naphthalene ND ug/L 10.0 0.24 1 06/02/17 02:22 91-20-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-15 Lab ID: 92342478003 Collected: 05/31/17 09:30 Received: 05/31/17 15:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Propionitrile ND ug/L 150 3.6 1 06/02/17 02:22 107-12-0 Styrene ND ug/L 1.0 0.26 1 06/02/17 02:22 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/02/17 02:22 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/02/17 02:22 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/02/17 02:22 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/02/17 02:22 108-88-3 1,2,4-Trichlorobenzene ND ug/L 10.0 0.35 1 06/02/17 02:22 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/02/17 02:22 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/02/17 02:22 79-00-5 Trichloroethene 2.0 ug/L 1.0 0.47 1 06/02/17 02:22 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/02/17 02:22 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/02/17 02:22 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/02/17 02:22 108-05-4 Vinyl chloride 1.6 ug/L 1.0 0.62 1 06/02/17 02:22 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/02/17 02:22 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 114 % 70-130 1 06/02/17 02:22 460-00-4 1,2-Dichloroethane-d4 (S) 98 % 70-130 1 06/02/17 02:22 17060-07-0 Toluene-d8 (S) 111 % 70-130 1 06/02/17 02:22 2037-26-5 4500S2D Sulfide Water Analytical Method: SM 4500-S2D Sulfide ND ug/L 1000 100 1 06/06/17 22:15 18496-25-8 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E Cyanide 4.6J ug/L 10.0 4.0 1 06/01/1717:39 57-12-5 Date: 06/19/2017 01:10 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 16 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-1 Lab ID: 92342478004 Collected: 06/01/17 12:35 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 Organochlorine Pesticides Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Surrogates Decachlorobiphenyl (S) 8151 Chlorinated Herbicides 2,4-D Dinoseb Pentachlorophenol 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 6010 MET ICP Antimony Arsenic Date: 06/19/2017 01:10 PM Analytical Method: EPA 8081 Preparation Method: EPA 3510 ND ug/L 0.050 0.050 1 06/05/1717:30 06/06/1712:52 309-00-2 ND ug/L 0.050 0.050 1 06/05/1717:30 06/06/1712:52 319-84-6 ND ug/L 0.050 0.050 1 06/05/1717:30 06/06/1712:52 319-85-7 ND ug/L 0.050 0.050 1 06/05/1717:30 06/06/1712:52 319-86-8 ND ug/L 0.050 0.050 1 06/05/1717:30 06/06/1712:52 58-89-9 ND ug/L 0.50 0.20 1 06/05/1717:30 06/06/1712:52 57-74-9 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1712:52 72-54-8 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1712:52 72-55-9 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1712:52 50-29-3 ND ug/L 0.075 0.050 1 06/05/1717:30 06/06/1712:52 60-57-1 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1712:52 959-98-8 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1712:52 33213-65-9 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1712:52 1031-07-8 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1712:52 72-20-8 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1712:52 7421-93-4 ND ug/L 0.050 0.050 1 06/05/1717:30 06/06/1712:52 76-44-8 ND ug/L 0.075 0.050 1 06/05/1717:30 06/06/1712:52 1024-57-3 ND ug/L 1.0 0.15 1 06/05/1717:30 06/06/1712:52 72-43-5 ND ug/L 1.5 0.20 1 06/05/1717:30 06/06/1712:52 8001-35-2 73 % 20-130 1 06/05/1717:30 06/06/1712:52 877-09-8 72 % 20-130 1 06/05/1717:30 06/06/1712:52 2051-24-3 Analytical Method: EPA 8082 Preparation Method: EPA 3510 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1719:29 12674-11-2 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1719:29 11104-28-2 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1719:29 11141-16-5 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1719:29 53469-21-9 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1719:29 12672-29-6 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1719:29 11097-69-1 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1719:29 11096-82-5 70 % 10-132 1 06/05/1717:30 06/06/1719:29 2051-24-3 Analytical Method: EPA 8151 Preparation Method: EPA 8151 ND ug/L 0.98 0.23 1 06/07/17 16:00 06/10/17 04:37 94-75-7 ND ug/L 0.20 0.059 1 06/07/17 16:00 06/10/17 04:37 88-85-7 ND ug/L 0.030 0.018 1 06/07/17 16:00 06/10/17 04:37 87-86-5 ND ug/L 0.20 0.044 1 06/07/17 16:00 06/10/17 04:37 93-76-5 ND ug/L 0.20 0.051 1 06/07/17 16:00 06/10/17 04:37 93-72-1 81 % 39-139 1 06/07/17 16:00 06/10/17 04:37 19719-28-9 Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 06/04/17 16:40 06/14/17 22:43 7440-36-0 ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:43 7440-38-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 17 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-1 Lab ID: 92342478004 Collected: 06/01/17 12:35 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Tin Vanadium Zinc 6020 MET ICPMS Thallium 7470 Mercury Mercury 8270 MSSV Semivolatile Organic Acenaphthene Acenaphthylene Acetophenone 2-Acetylaminofluorene 4-Aminobiphenyl Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-ChIoro-3-methyl phenol 4-Chloroaniline Chlorobenzilate bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Diallate Dibenz(a,h)anthracene Date: 06/19/2017 01:10 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010A 92.9J ug/L 100 2.5 1 06/04/17 16:40 06/14/17 22:43 7440-39-3 ND ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:43 7440-41-7 0.89J ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:43 7440-43-9 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:43 7440-47-3 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:43 7440-48-4 356 ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:43 7440-50-8 21.0 ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:43 7439-92-1 4.5J ug/L 50.0 2.5 1 06/04/17 16:40 06/14/17 22:43 7440-02-0 ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:43 7782-49-2 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:43 7440-22-4 3.9J ug/L 100 2.5 1 06/04/17 16:40 06/14/17 22:43 7440-31-5 ND ug/L 25.0 2.5 1 06/04/17 16:40 06/14/17 22:43 7440-62-2 256 ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:43 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3010A 0.026J ug/L 5.5 0.020 1 06/03/17 02:25 06/09/17 16:30 7440-28-0 Analytical Method: EPA 7470 Preparation Method: EPA 7470 ND ug/L 0.20 0.10 1 06/05/17 20:00 06/06/17 10:06 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1719:54 83-32-9 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1719:54 208-96-8 ND ug/L 10.0 1.9 1 06/07/1717:10 06/14/1719:54 98-86-2 ND ug/L 20.0 1.6 1 06/07/1717:10 06/14/1719:54 53-96-3 ND ug/L 20.0 1.7 1 06/07/1717:10 06/14/1719:54 92-67-1 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1719:54 120-12-7 ND ug/L 10.0 2.1 1 06/07/1717:10 06/14/1719:54 56-55-3 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1719:54 50-32-8 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1719:54 205-99-2 ND ug/L 10.0 2.1 1 06/07/1717:10 06/14/1719:54 191-24-2 ND ug/L 10.0 2.0 1 06/07/1717:10 06/14/1719:54 207-08-9 ND ug/L 20.0 3.1 1 06/07/1717:10 06/14/1719:54 100-51-6 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1719:54 101-55-3 ND ug/L 10.0 2.5 1 06/07/1717:10 06/14/1719:54 85-68-7 ND ug/L 20.0 2.8 1 06/07/1717:10 06/14/1719:54 59-50-7 ND ug/L 20.0 2.8 1 06/07/1717:10 06/14/1719:54 106-47-8 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1719:54 510-15-6 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1719:54 111-91-1 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1719:54 111-44-4 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1719:54 91-58-7 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1719:54 95-57-8 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1719:54 7005-72-3 ND ug/L 10.0 2.1 1 06/07/1717:10 06/14/1719:54 218-01-9 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1719:54 2303-16-4 ND ug/L 10.0 2.0 1 06/07/1717:10 06/14/1719:54 53-70-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. L2 Page 18 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-1 Lab ID: 92342478004 Collected: 06/01/17 12:35 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Dibenzofuran ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 19:54 132-64-9 3,3'-Dichlorobenzidine ND ug/L 20.0 3.9 1 06/07/17 17:10 06/14/17 19:54 91-94-1 2,4-Dichlorophenol ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 19:54 120-83-2 2,6-Dichlorophenol ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 19:54 87-65-0 Diethylphthalate ND ug/L 6000 1.6 1 06/07/17 17:10 06/14/17 19:54 84-66-2 Dimethoate ND ug/L 20.0 1.8 1 06/07/17 17:10 06/14/17 19:54 60-51-5 P-Dimethylaminoazobenzene ND ug/L 10.0 1.0 1 06/07/17 17:10 06/14/17 19:54 60-11-7 7,12-Dimethylbenz(a)anthracene ND ug/L 10.0 2.4 1 06/07/17 17:10 06/14/17 19:54 57-97-6 3,3'-Dimethylbenzidine ND ug/L 10.0 3.9 1 06/07/17 17:10 06/14/17 19:54 119-93-7 2,4-Dimethylphenol ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 19:54 105-67-9 Dimethylphthalate ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 19:54 131-11-3 Di-n-butylphthalate ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 19:54 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 50.0 2.2 1 06/07/17 17:10 06/14/17 19:54 534-52-1 1,3-Dinitrobenzene ND ug/L 20.0 1.3 1 06/07/17 17:10 06/14/17 19:54 99-65-0 2,4-Dinitrophenol ND ug/L 50.0 5.1 1 06/07/17 17:10 06/14/17 19:54 51-28-5 2,4-Dinitrotoluene ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 19:54 121-14-2 2,6-Dinitrotoluene ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 19:54 606-20-2 Di-n-octylphthalate ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 19:54 117-84-0 Diphenylamine ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 19:54 122-39-4 Disulfoton ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 19:54 298-04-4 bis(2- Ethyl hexyl)phthalate ND ug/L 15.0 2.3 1 06/07/17 17:10 06/14/17 19:54 117-81-7 Ethyl methanesulfonate ND ug/L 20.0 1.6 1 06/07/17 17:10 06/14/17 19:54 62-50-0 Famphur ND ug/L 20.0 5.7 1 06/07/17 17:10 06/14/17 19:54 52-85-7 Fluoranthene ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 19:54 206-44-0 Fluorene ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 19:54 86-73-7 Hexachlorobenzene ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 19:54 118-74-1 Hexachlorocyclopentadiene ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 19:54 77-47-4 Hexachloroethane ND ug/L 10.0 1.8 1 06/07/17 17:10 06/14/17 19:54 67-72-1 Hexachloropropene ND ug/L 10.0 1.2 1 06/07/17 17:10 06/14/17 19:54 1888-71-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 19:54 193-39-5 Isodrin ND ug/L 20.0 2.5 1 06/07/17 17:10 06/14/17 19:54 465-73-6 Isophorone ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 19:54 78-59-1 Isosafrole ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 19:54 120-58-1 Kepone ND ug/L 20.0 4.5 1 06/07/17 17:10 06/14/17 19:54 143-50-0 Methapyrilene ND ug/L 100 3.0 1 06/07/17 17:10 06/14/17 19:54 91-80-5 3-Methylcholanthrene ND ug/L 10.0 2.7 1 06/07/17 17:10 06/14/17 19:54 56-49-5 Methyl methanesulfonate ND ug/L 10.0 1.1 1 06/07/17 17:10 06/14/17 19:54 66-27-3 2-Methylnaphthalene ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 19:54 91-57-6 Methyl parathion ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 19:54 298-00-0 2-Methylphenol(o-Cresol) ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 19:54 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 19:54 15831-10-4 1-Naphthalenamine ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 19:54 134-32-7 2-Naphthalenamine ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 19:54 91-59-8 1,4-Naphthoquinone ND ug/L 10.0 0.99 1 06/07/17 17:10 06/14/17 19:54 130-15-4 2-Nitroaniline ND ug/L 50.0 2.3 1 06/07/17 17:10 06/14/17 19:54 88-74-4 3-Nitroaniline ND ug/L 50.0 2.7 1 06/07/17 17:10 06/14/17 19:54 99-09-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-1 Lab ID: 92342478004 Collected: 06/01/17 12:35 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol 5-Nitro-o-toluidine N-Nitrosodiethylamine N-Nitrosodimethylamine N-Nitroso-di-n-butylamine N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine N-Nitrosomethylethylamine N-Nitrosopiperidine N-Nitrosopyrrolidine O,O,O-Triethylphosphorothioate 2,2'-Oxybis(1-chloropropane) Parathion (Ethyl parathion) Pentachlorobenzene Pentachloronitrobenzene Pentachlorophenol Phenacetin Phenanthrene Phenol p-Phenylenediamine Phorate Pronamide Pyrene Safrole 1,2,4,5-Tetrachlorobenzene 2,3,4,6-Tetrachlorophenol Thionazin O-Toluidine 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 1,3,5-Trinitrobenzene Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) 8260 MSV Low Level Landfill Acetone Acetonitrile Acrolein Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ug/L 20.0 3.4 1 06/07/1717:10 06/14/1719:54 100-01-6 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1719:54 98-95-3 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1719:54 88-75-5 ND ug/L 50.0 4.3 1 06/07/1717:10 06/14/1719:54 100-02-7 ND ug/L 10.0 1.9 1 06/07/1717:10 06/14/1719:54 99-55-8 ND ug/L 20.0 1.4 1 06/07/1717:10 06/14/1719:54 55-18-5 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1719:54 62-75-9 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1719:54 924-16-3 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1719:54 621-64-7 ND ug/L 10.0 1.4 1 06/07/1717:10 06/14/1719:54 86-30-6 ND ug/L 10.0 1.4 1 06/07/1717:10 06/14/1719:54 10595-95-6 ND ug/L 20.0 1.7 1 06/07/1717:10 06/14/1719:54 100-75-4 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1719:54 930-55-2 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1719:54 126-68-1 ND ug/L 10.0 1.8 1 06/07/1717:10 06/14/1719:54 108-60-1 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1719:54 56-38-2 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1719:54 608-93-5 ND ug/L 20.0 1.7 1 06/07/1717:10 06/14/1719:54 82-68-8 ND ug/L 25.0 3.5 1 06/07/1717:10 06/14/1719:54 87-86-5 ND ug/L 20.0 1.9 1 06/07/1717:10 06/14/1719:54 62-44-2 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1719:54 85-01-8 ND ug/L 10.0 1.3 1 06/07/1717:10 06/14/1719:54 108-95-2 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1719:54 106-50-3 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1719:54 298-02-2 ND ug/L 10.0 2.0 1 06/07/1717:10 06/14/1719:54 23950-58-5 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1719:54 129-00-0 ND ug/L 10.0 1.3 1 06/07/1717:10 06/14/1719:54 94-59-7 ND ug/L 10.0 1.3 1 06/07/1717:10 06/14/1719:54 95-94-3 ND ug/L 10.0 2.9 1 06/07/1717:10 06/14/1719:54 58-90-2 ND ug/L 20.0 1.7 1 06/07/1717:10 06/14/1719:54 297-97-2 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1719:54 95-53-4 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1719:54 95-95-4 ND ug/L 10.0 1.4 1 06/07/1717:10 06/14/1719:54 88-06-2 ND ug/L 10.0 1.2 1 06/07/1717:10 06/14/1719:54 99-35-4 63 % 21-110 1 06/07/1717:10 06/14/1719:54 4165-60-0 84 % 27-110 1 06/07/1717:10 06/14/1719:54 321-60-8 82 % 31-107 1 06/07/1717:10 06/14/1719:54 1718-51-0 25 % 10-110 1 06/07/1717:10 06/14/1719:54 13127-88-3 38 % 12-110 1 06/07/1717:10 06/14/1719:54 367-12-4 74 % 27-110 1 06/07/1717:10 06/14/1719:54 118-79-6 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 ND ug/L 55.0 2.2 1 ND ug/L 53.0 1.6 1 REPORT OF LABORATORY ANALYSIS 06/04/17 22:05 67-64-1 06/04/17 22:05 75-05-8 06/04/17 22:05 107-02-8 This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-1 Lab ID: 92342478004 Collected: 06/01/17 12:35 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acrylonitrile ND ug/L 200 1.9 1 06/04/17 22:05 107-13-1 Allyl chloride ND ug/L 10.0 1.5 1 06/04/17 22:05 107-05-1 Benzene ND ug/L 1.0 0.25 1 06/04/17 22:05 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 06/04/17 22:05 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 06/04/17 22:05 75-27-4 Bromoform ND ug/L 3.0 0.26 1 06/04/17 22:05 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 06/04/17 22:05 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 06/04/17 22:05 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 06/04/17 22:05 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 06/04/17 22:05 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 06/04/17 22:05 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 06/04/17 22:05 75-00-3 Chloroform ND ug/L 5.0 0.14 1 06/04/17 22:05 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 06/04/17 22:05 74-87-3 Chloroprene ND ug/L 20.0 0.27 1 06/04/17 22:05 126-99-8 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 06/04/17 22:05 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 06/04/17 22:05 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 06/04/17 22:05 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 06/04/17 22:05 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 06/04/17 22:05 95-50-1 1,3-Dichlorobenzene ND ug/L 5.0 0.24 1 06/04/17 22:05 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 06/04/17 22:05 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/04/17 22:05 110-57-6 Dichlorodifluoromethane ND ug/L 5.0 0.21 1 06/04/17 22:05 75-71-8 1,1-Dichloroethane ND ug/L 5.0 0.32 1 06/04/17 22:05 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 06/04/17 22:05 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/04/17 22:05 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 06/04/17 22:05 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/04/17 22:05 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 06/04/17 22:05 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 06/04/17 22:05 142-28-9 2,2-Dichloropropane ND ug/L 15.0 0.13 1 06/04/17 22:05 594-20-7 1,1-Dichloropropene ND ug/L 5.0 0.49 1 06/04/17 22:05 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/04/17 22:05 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/17 22:05 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/17 22:05 100-41-4 Ethyl methacrylate ND ug/L 10.0 0.20 1 06/04/17 22:05 97-63-2 Hexachloro-1,3-butadiene ND ug/L 10.0 0.71 1 06/04/17 22:05 87-68-3 2-Hexanone ND ug/L 50.0 0.46 1 06/04/17 22:05 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/17 22:05 74-88-4 Isobutanol ND ug/L 100 35.0 1 06/04/17 22:05 78-83-1 Methacrylonitrile ND ug/L 100 0.93 1 06/04/17 22:05 126-98-7 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/17 22:05 75-09-2 Methyl methacrylate ND ug/L 30.0 2.0 1 06/04/17 22:05 80-62-6 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/17 22:05 108-10-1 Naphthalene ND ug/L 10.0 0.24 1 06/04/17 22:05 91-20-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-1 Lab ID: 92342478004 Collected: 06/01/17 12:35 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Propionitrile ND ug/L 150 3.6 1 06/04/17 22:05 107-12-0 Styrene ND ug/L 1.0 0.26 1 06/04/17 22:05 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/17 22:05 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/17 22:05 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/17 22:05 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/17 22:05 108-88-3 1,2,4-Trichlorobenzene ND ug/L 10.0 0.35 1 06/04/17 22:05 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/17 22:05 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/17 22:05 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/17 22:05 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/17 22:05 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/17 22:05 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/17 22:05 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/17 22:05 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/17 22:05 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 116 % 70-130 1 06/04/17 22:05 460-00-4 1,2-Dichloroethane-d4 (S) 92 % 70-130 1 06/04/17 22:05 17060-07-0 Toluene-d8 (S) 110 % 70-130 1 06/04/17 22:05 2037-26-5 Date: 06/19/2017 01:10 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 22 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-9 Lab ID: 92342478005 Collected: 06/01/17 15:40 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 Organochlorine Pesticides Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Surrogates Decachlorobiphenyl (S) 8151 Chlorinated Herbicides 2,4-D Dinoseb Pentachlorophenol 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 6010 MET ICP Antimony Arsenic Date: 06/19/2017 01:10 PM Analytical Method: EPA 8081 Preparation Method: EPA 3510 ND ug/L 0.050 0.050 1 06/05/1717:30 06/06/1713:10 309-00-2 ND ug/L 0.050 0.050 1 06/05/1717:30 06/06/1713:10 319-84-6 ND ug/L 0.050 0.050 1 06/05/1717:30 06/06/1713:10 319-85-7 ND ug/L 0.050 0.050 1 06/05/1717:30 06/06/1713:10 319-86-8 ND ug/L 0.050 0.050 1 06/05/1717:30 06/06/1713:10 58-89-9 ND ug/L 0.50 0.20 1 06/05/1717:30 06/06/1713:10 57-74-9 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1713:10 72-54-8 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1713:10 72-55-9 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1713:10 50-29-3 ND ug/L 0.075 0.050 1 06/05/1717:30 06/06/1713:10 60-57-1 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1713:10 959-98-8 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1713:10 33213-65-9 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1713:10 1031-07-8 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1713:10 72-20-8 ND ug/L 0.10 0.050 1 06/05/1717:30 06/06/1713:10 7421-93-4 ND ug/L 0.050 0.050 1 06/05/1717:30 06/06/1713:10 76-44-8 ND ug/L 0.075 0.050 1 06/05/1717:30 06/06/1713:10 1024-57-3 ND ug/L 1.0 0.15 1 06/05/1717:30 06/06/1713:10 72-43-5 ND ug/L 1.5 0.20 1 06/05/1717:30 06/06/1713:10 8001-35-2 65 % 20-130 1 06/05/1717:30 06/06/1713:10 877-09-8 67 % 20-130 1 06/05/1717:30 06/06/1713:10 2051-24-3 Analytical Method: EPA 8082 Preparation Method: EPA 3510 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1719:50 12674-11-2 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1719:50 11104-28-2 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1719:50 11141-16-5 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1719:50 53469-21-9 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1719:50 12672-29-6 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1719:50 11097-69-1 ND ug/L 0.50 0.50 1 06/05/1717:30 06/06/1719:50 11096-82-5 69 % 10-132 1 06/05/1717:30 06/06/1719:50 2051-24-3 Analytical Method: EPA 8151 Preparation Method: EPA 8151 ND ug/L 0.98 0.23 1 06/07/17 16:00 06/10/17 05:06 94-75-7 ND ug/L 0.20 0.059 1 06/07/17 16:00 06/10/17 05:06 88-85-7 ND ug/L 0.030 0.018 1 06/07/17 16:00 06/10/17 05:06 87-86-5 ND ug/L 0.20 0.044 1 06/07/17 16:00 06/10/17 05:06 93-76-5 ND ug/L 0.20 0.051 1 06/07/17 16:00 06/10/17 05:06 93-72-1 88 % 39-139 1 06/07/17 16:00 06/10/17 05:06 19719-28-9 Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 06/04/17 16:40 06/14/17 22:47 7440-36-0 ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:47 7440-38-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 23 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-9 Lab ID: 92342478005 Collected: 06/01/17 15:40 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Tin Vanadium Zinc 6020 MET ICPMS Thallium 7470 Mercury Mercury 8270 MSSV Semivolatile Organic Acenaphthene Acenaphthylene Acetophenone 2-Acetylaminofluorene 4-Aminobiphenyl Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-ChIoro-3-methyl phenol 4-Chloroaniline Chlorobenzilate bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Diallate Dibenz(a,h)anthracene Date: 06/19/2017 01:10 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010A 48.2J ug/L 100 2.5 1 06/04/17 16:40 06/14/17 22:47 7440-39-3 ND ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:47 7440-41-7 ND ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:47 7440-43-9 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:47 7440-47-3 166 ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:47 7440-48-4 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:47 7440-50-8 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:47 7439-92-1 6.6J ug/L 50.0 2.5 1 06/04/17 16:40 06/14/17 22:47 7440-02-0 ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:47 7782-49-2 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:47 7440-22-4 ND ug/L 100 2.5 1 06/04/17 16:40 06/14/17 22:47 7440-31-5 ND ug/L 25.0 2.5 1 06/04/17 16:40 06/14/17 22:47 7440-62-2 38.3 ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:47 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3010A 0.33J ug/L 5.5 0.020 1 06/03/17 02:25 06/09/17 16:31 7440-28-0 Analytical Method: EPA 7470 Preparation Method: EPA 7470 ND ug/L 0.20 0.10 1 06/05/17 20:00 06/06/17 10:09 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 20:23 83-32-9 ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 20:23 208-96-8 ND ug/L 10.0 1.9 1 06/07/17 17:10 06/14/17 20:23 98-86-2 ND ug/L 20.0 1.6 1 06/07/17 17:10 06/14/17 20:23 53-96-3 ND ug/L 20.0 1.7 1 06/07/17 17:10 06/14/17 20:23 92-67-1 ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 20:23 120-12-7 ND ug/L 10.0 2.1 1 06/07/17 17:10 06/14/17 20:23 56-55-3 ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 20:23 50-32-8 ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 20:23 205-99-2 ND ug/L 10.0 2.1 1 06/07/17 17:10 06/14/17 20:23 191-24-2 ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 20:23 207-08-9 ND ug/L 20.0 3.1 1 06/07/17 17:10 06/14/17 20:23 100-51-6 ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 20:23 101-55-3 ND ug/L 10.0 2.5 1 06/07/17 17:10 06/14/17 20:23 85-68-7 ND ug/L 20.0 2.8 1 06/07/17 17:10 06/14/17 20:23 59-50-7 ND ug/L 20.0 2.8 1 06/07/17 17:10 06/14/17 20:23 106-47-8 ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 20:23 510-15-6 ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 20:23 111-91-1 ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 20:23 111-44-4 ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 20:23 91-58-7 ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 20:23 95-57-8 ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 20:23 7005-72-3 ND ug/L 10.0 2.1 1 06/07/17 17:10 06/14/17 20:23 218-01-9 ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 20:23 2303-16-4 ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 20:23 53-70-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. L2 Page 24 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-9 Lab ID: 92342478005 Collected: 06/01/17 15:40 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Dibenzofuran ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 20:23 132-64-9 3,3'-Dichlorobenzidine ND ug/L 20.0 3.9 1 06/07/17 17:10 06/14/17 20:23 91-94-1 2,4-Dichlorophenol ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 20:23 120-83-2 2,6-Dichlorophenol ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 20:23 87-65-0 Diethylphthalate ND ug/L 6000 1.6 1 06/07/17 17:10 06/14/17 20:23 84-66-2 Dimethoate ND ug/L 20.0 1.8 1 06/07/17 17:10 06/14/17 20:23 60-51-5 P-Dimethylaminoazobenzene ND ug/L 10.0 1.0 1 06/07/17 17:10 06/14/17 20:23 60-11-7 7,12-Dimethylbenz(a)anthracene ND ug/L 10.0 2.4 1 06/07/17 17:10 06/14/17 20:23 57-97-6 3,3'-Dimethylbenzidine ND ug/L 10.0 3.9 1 06/07/17 17:10 06/14/17 20:23 119-93-7 2,4-Dimethylphenol ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 20:23 105-67-9 Dimethylphthalate ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 20:23 131-11-3 Di-n-butylphthalate ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 20:23 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 50.0 2.2 1 06/07/17 17:10 06/14/17 20:23 534-52-1 1,3-Dinitrobenzene ND ug/L 20.0 1.3 1 06/07/17 17:10 06/14/17 20:23 99-65-0 2,4-Dinitrophenol ND ug/L 50.0 5.1 1 06/07/17 17:10 06/14/17 20:23 51-28-5 2,4-Dinitrotoluene ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 20:23 121-14-2 2,6-Dinitrotoluene ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 20:23 606-20-2 Di-n-octylphthalate ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 20:23 117-84-0 Diphenylamine ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 20:23 122-39-4 Disulfoton ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 20:23 298-04-4 bis(2- Ethyl hexyl)phthalate ND ug/L 15.0 2.3 1 06/07/17 17:10 06/14/17 20:23 117-81-7 Ethyl methanesulfonate ND ug/L 20.0 1.6 1 06/07/17 17:10 06/14/17 20:23 62-50-0 Famphur ND ug/L 20.0 5.7 1 06/07/17 17:10 06/14/17 20:23 52-85-7 Fluoranthene ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 20:23 206-44-0 Fluorene ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 20:23 86-73-7 Hexachlorobenzene ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 20:23 118-74-1 Hexachlorocyclopentadiene ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 20:23 77-47-4 Hexachloroethane ND ug/L 10.0 1.8 1 06/07/17 17:10 06/14/17 20:23 67-72-1 Hexachloropropene ND ug/L 10.0 1.2 1 06/07/17 17:10 06/14/17 20:23 1888-71-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 20:23 193-39-5 Isodrin ND ug/L 20.0 2.5 1 06/07/17 17:10 06/14/17 20:23 465-73-6 Isophorone ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 20:23 78-59-1 Isosafrole ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 20:23 120-58-1 Kepone ND ug/L 20.0 4.5 1 06/07/17 17:10 06/14/17 20:23 143-50-0 Methapyrilene ND ug/L 100 3.0 1 06/07/17 17:10 06/14/17 20:23 91-80-5 3-Methylcholanthrene ND ug/L 10.0 2.7 1 06/07/17 17:10 06/14/17 20:23 56-49-5 Methyl methanesulfonate ND ug/L 10.0 1.1 1 06/07/17 17:10 06/14/17 20:23 66-27-3 2-Methylnaphthalene ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 20:23 91-57-6 Methyl parathion ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 20:23 298-00-0 2-Methylphenol(o-Cresol) ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 20:23 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 20:23 15831-10-4 1-Naphthalenamine ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 20:23 134-32-7 2-Naphthalenamine ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 20:23 91-59-8 1,4-Naphthoquinone ND ug/L 10.0 0.99 1 06/07/17 17:10 06/14/17 20:23 130-15-4 2-Nitroaniline ND ug/L 50.0 2.3 1 06/07/17 17:10 06/14/17 20:23 88-74-4 3-Nitroaniline ND ug/L 50.0 2.7 1 06/07/17 17:10 06/14/17 20:23 99-09-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-9 Lab ID: 92342478005 Collected: 06/01/17 15:40 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 4-Nitroaniline ND ug/L 20.0 3.4 1 06/07/17 17:10 06/14/17 20:23 100-01-6 Nitrobenzene ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 20:23 98-95-3 2-Nitrophenol ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 20:23 88-75-5 4-Nitrophenol ND ug/L 50.0 4.3 1 06/07/17 17:10 06/14/17 20:23 100-02-7 5-Nitro-o-toluidine ND ug/L 10.0 1.9 1 06/07/17 17:10 06/14/17 20:23 99-55-8 N-Nitrosodiethylamine ND ug/L 20.0 1.4 1 06/07/17 17:10 06/14/17 20:23 55-18-5 N-Nitrosodimethylamine ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 20:23 62-75-9 N-Nitroso-di-n-butylamine ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 20:23 924-16-3 N-Nitroso-di-n-propylamine ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 20:23 621-64-7 N-Nitrosodiphenylamine ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 20:23 86-30-6 N-Nitrosomethylethylamine ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 20:23 10595-95-6 N-Nitrosopiperidine ND ug/L 20.0 1.7 1 06/07/17 17:10 06/14/17 20:23 100-75-4 N-Nitrosopyrrolidine ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 20:23 930-55-2 O,O,O-Triethylphosphorothioate ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 20:23 126-68-1 2,2'-Oxybis(1-chloropropane) ND ug/L 10.0 1.8 1 06/07/17 17:10 06/14/17 20:23 108-60-1 Parathion (Ethyl parathion) ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 20:23 56-38-2 Pentachlorobenzene ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 20:23 608-93-5 Pentachloronitrobenzene ND ug/L 20.0 1.7 1 06/07/17 17:10 06/14/17 20:23 82-68-8 Pentachlorophenol ND ug/L 25.0 3.5 1 06/07/17 17:10 06/14/17 20:23 87-86-5 Phenacetin ND ug/L 20.0 1.9 1 06/07/17 17:10 06/14/17 20:23 62-44-2 Phenanthrene ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 20:23 85-01-8 Phenol ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 20:23 108-95-2 p-Phenylenediamine ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 20:23 106-50-3 Phorate ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 20:23 298-02-2 Pronamide ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 20:23 23950-58-5 Pyrene ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 20:23 129-00-0 Safrole ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 20:23 94-59-7 1,2,4,5-Tetrachlorobenzene ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 20:23 95-94-3 2,3,4,6-Tetrachlorophenol ND ug/L 10.0 2.9 1 06/07/17 17:10 06/14/17 20:23 58-90-2 Thionazin ND ug/L 20.0 1.7 1 06/07/17 17:10 06/14/17 20:23 297-97-2 O-Toluidine ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 20:23 95-53-4 2,4,5-Trichlorophenol ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 20:23 95-95-4 2,4,6-Trichlorophenol ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 20:23 88-06-2 1,3,5-Trinitrobenzene ND ug/L 10.0 1.2 1 06/07/17 17:10 06/14/17 20:23 99-35-4 Surrogates Nitrobenzene-d5 (S) 70 % 21-110 1 06/07/17 17:10 06/14/17 20:23 4165-60-0 2-Fluorobiphenyl (S) 84 % 27-110 1 06/07/17 17:10 06/14/17 20:23 321-60-8 Terphenyl-d14 (S) 84 % 31-107 1 06/07/17 17:10 06/14/17 20:23 1718-51-0 Phenol-d6 (S) 24 % 10-110 1 06/07/17 17:10 06/14/17 20:23 13127-88-3 2-Fluorophenol (S) 38 % 12-110 1 06/07/17 17:10 06/14/17 20:23 367-12-4 2,4,6-Tribromophenol (S) 78 % 27-110 1 06/07/17 17:10 06/14/17 20:23 118-79-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 29.5J ug/L 100 10.0 1 06/04/17 22:23 67-64-1 Acetonitrile ND ug/L 55.0 2.2 1 06/04/17 22:23 75-05-8 Acrolein 2.1J ug/L 53.0 1.6 1 06/04/17 22:23 107-02-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-9 Lab ID: 92342478005 Collected: 06/01/17 15:40 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acrylonitrile ND ug/L 200 1.9 1 06/04/17 22:23 107-13-1 Allyl chloride ND ug/L 10.0 1.5 1 06/04/17 22:23 107-05-1 Benzene 2.4 ug/L 1.0 0.25 1 06/04/17 22:23 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 06/04/17 22:23 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 06/04/17 22:23 75-27-4 Bromoform ND ug/L 3.0 0.26 1 06/04/17 22:23 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 06/04/17 22:23 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 06/04/17 22:23 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 06/04/17 22:23 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 06/04/17 22:23 56-23-5 Chlorobenzene 2.2J ug/L 3.0 0.23 1 06/04/17 22:23 108-90-7 Chloroethane 1.91 ug/L 10.0 0.54 1 06/04/17 22:23 75-00-3 Chloroform ND ug/L 5.0 0.14 1 06/04/17 22:23 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 06/04/17 22:23 74-87-3 Chloroprene ND ug/L 20.0 0.27 1 06/04/17 22:23 126-99-8 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 06/04/17 22:23 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 06/04/17 22:23 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 06/04/17 22:23 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 06/04/17 22:23 74-95-3 1,2-Dichlorobenzene 1.5J ug/L 5.0 0.30 1 06/04/17 22:23 95-50-1 1,3-Dichlorobenzene ND ug/L 5.0 0.24 1 06/04/17 22:23 541-73-1 1,4-Dichlorobenzene 5.7 ug/L 1.0 0.33 1 06/04/17 22:23 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/04/17 22:23 110-57-6 Dichlorodifluoromethane ND ug/L 5.0 0.21 1 06/04/17 22:23 75-71-8 1,1-Dichloroethane 2.4J ug/L 5.0 0.32 1 06/04/17 22:23 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 06/04/17 22:23 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/04/17 22:23 75-35-4 cis-1,2-Dichloroethene 19.7 ug/L 5.0 0.19 1 06/04/17 22:23 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/04/17 22:23 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 06/04/17 22:23 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 06/04/17 22:23 142-28-9 2,2-Dichloropropane ND ug/L 15.0 0.13 1 06/04/17 22:23 594-20-7 1,1-Dichloropropene ND ug/L 5.0 0.49 1 06/04/17 22:23 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/04/17 22:23 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/17 22:23 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/17 22:23 100-41-4 Ethyl methacrylate ND ug/L 10.0 0.20 1 06/04/17 22:23 97-63-2 Hexachloro-1,3-butadiene ND ug/L 10.0 0.71 1 06/04/17 22:23 87-68-3 2-Hexanone ND ug/L 50.0 0.46 1 06/04/17 22:23 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/17 22:23 74-88-4 Isobutanol ND ug/L 100 35.0 1 06/04/17 22:23 78-83-1 Methacrylonitrile ND ug/L 100 0.93 1 06/04/17 22:23 126-98-7 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/17 22:23 75-09-2 Methyl methacrylate ND ug/L 30.0 2.0 1 06/04/17 22:23 80-62-6 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/17 22:23 108-10-1 Naphthalene ND ug/L 10.0 0.24 1 06/04/17 22:23 91-20-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-9 Lab ID: 92342478005 Collected: 06/01/17 15:40 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Propionitrile ND ug/L 150 3.6 1 06/04/17 22:23 107-12-0 Styrene ND ug/L 1.0 0.26 1 06/04/17 22:23 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/17 22:23 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/17 22:23 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/17 22:23 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/17 22:23 108-88-3 1,2,4-Trichlorobenzene ND ug/L 10.0 0.35 1 06/04/17 22:23 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/17 22:23 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/17 22:23 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/17 22:23 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/17 22:23 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/17 22:23 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/17 22:23 108-05-4 Vinyl chloride 18.7 ug/L 1.0 0.62 1 06/04/17 22:23 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/17 22:23 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 107 % 70-130 1 06/04/17 22:23 460-00-4 1,2-Dichloroethane-d4 (S) 93 % 70-130 1 06/04/17 22:23 17060-07-0 Toluene-d8 (S) 109 % 70-130 1 06/04/17 22:23 2037-26-5 Date: 06/19/2017 01:10 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 28 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-7 Lab ID: 92342478006 Collected: 06/01/17 14:45 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Antimony ND ug/L 6.0 3.9 1 06/04/17 16:40 06/14/17 22:50 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:50 7440-38-2 Barium 55.1J ug/L 100 2.5 1 06/04/17 16:40 06/14/17 22:50 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:50 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:50 7440-43-9 Chromium ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:50 7440-47-3 Cobalt 50.7 ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:50 7440-48-4 Copper ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:50 7440-50-8 Lead ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:50 7439-92-1 Nickel ND ug/L 50.0 2.5 1 06/04/17 16:40 06/14/17 22:50 7440-02-0 Selenium ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:50 7782-49-2 Silver ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:50 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 06/04/17 16:40 06/14/17 22:50 7440-62-2 Zinc 10.7 ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:50 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Thallium 0.11J ug/L 5.5 0.020 1 06/03/17 02:25 06/09/17 16:33 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 06/04/17 22:41 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 06/04/17 22:41 107-13-1 Benzene 0.30J ug/L 1.0 0.25 1 06/04/17 22:41 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 06/04/17 22:41 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 06/04/17 22:41 75-27-4 Bromoform ND ug/L 3.0 0.26 1 06/04/17 22:41 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 06/04/17 22:41 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 06/04/17 22:41 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 06/04/17 22:41 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 06/04/17 22:41 56-23-5 Chlorobenzene 3.9 ug/L 3.0 0.23 1 06/04/17 22:41 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 06/04/17 22:41 75-00-3 Chloroform ND ug/L 5.0 0.14 1 06/04/17 22:41 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 06/04/17 22:41 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 06/04/17 22:41 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 06/04/17 22:41 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 06/04/17 22:41 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 06/04/17 22:41 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 06/04/17 22:41 95-50-1 1,4-Dichlorobenzene 2.2 ug/L 1.0 0.33 1 06/04/17 22:41 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/04/17 22:41 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 06/04/17 22:41 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 06/04/17 22:41 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/04/17 22:41 75-35-4 cis-1,2-Dichloroethene 0.28J ug/L 5.0 0.19 1 06/04/17 22:41 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/04/17 22:41 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 06/04/17 22:41 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-7 Lab ID: 92342478006 Collected: 06/01/17 14:45 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/04/17 22:41 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/17 22:41 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/17 22:41 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/04/17 22:41 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/17 22:41 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/17 22:41 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/17 22:41 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/04/17 22:41 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/17 22:41 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/17 22:41 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/17 22:41 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/17 22:41 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/17 22:41 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/17 22:41 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/17 22:41 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/17 22:41 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/17 22:41 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/17 22:41 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/17 22:41 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/17 22:41 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 108 % 70-130 1 06/04/17 22:41 460-00-4 1,2-Dichloroethane-d4 (S) 89 % 70-130 1 06/04/17 22:41 17060-07-0 Toluene-d8 (S) 110 % 70-130 1 06/04/17 22:41 2037-26-5 Date: 06/19/2017 01:10 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 30 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-12S Lab ID: 92342478007 Collected: 06/01/17 09:50 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Antimony ND ug/L 6.0 3.9 1 06/04/1717:05 06/09/1718:50 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/04/1717:05 06/09/1718:50 7440-38-2 Barium 23.5J ug/L 100 2.5 1 06/04/1717:05 06/09/1718:50 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 06/04/1717:05 06/09/1718:50 7440-41-7 Cadmium 0.66J ug/L 1.0 0.50 1 06/04/1717:05 06/09/1718:50 7440-43-9 Chromium ND ug/L 10.0 2.5 1 06/04/1717:05 06/09/1718:50 7440-47-3 Cobalt ND ug/L 10.0 2.5 1 06/04/1717:05 06/09/1718:50 7440-48-4 Copper 3.5J ug/L 10.0 2.5 1 06/04/1717:05 06/09/1718:50 7440-50-8 Lead ND ug/L 10.0 2.5 1 06/04/1717:05 06/09/1718:50 7439-92-1 Nickel 2.8J ug/L 50.0 2.5 1 06/04/1717:05 06/09/1718:50 7440-02-0 Selenium ND ug/L 10.0 5.0 1 06/04/1717:05 06/09/1718:50 7782-49-2 Silver ND ug/L 10.0 2.5 1 06/04/1717:05 06/09/1718:50 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 06/04/1717:05 06/09/1718:50 7440-62-2 Zinc 6.6J ug/L 10.0 5.0 1 06/04/1717:05 06/09/1718:50 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Thallium ND ug/L 5.5 0.020 1 06/03/17 02:25 06/09/17 16:44 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 06/04/17 22:58 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 06/04/17 22:58 107-13-1 Benzene ND ug/L 1.0 0.25 1 06/04/17 22:58 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 06/04/17 22:58 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 06/04/17 22:58 75-27-4 Bromoform ND ug/L 3.0 0.26 1 06/04/17 22:58 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 06/04/17 22:58 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 06/04/17 22:58 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 06/04/17 22:58 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 06/04/17 22:58 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 06/04/17 22:58 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 06/04/17 22:58 75-00-3 Chloroform ND ug/L 5.0 0.14 1 06/04/17 22:58 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 06/04/17 22:58 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 06/04/17 22:58 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 06/04/17 22:58 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 06/04/17 22:58 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 06/04/17 22:58 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 06/04/17 22:58 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 06/04/17 22:58 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/04/17 22:58 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 06/04/17 22:58 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 06/04/17 22:58 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/04/17 22:58 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 06/04/17 22:58 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/04/17 22:58 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 06/04/17 22:58 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-12S Lab ID: 92342478007 Collected: 06/01/17 09:50 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/04/17 22:58 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/17 22:58 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/17 22:58 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/04/17 22:58 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/17 22:58 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/17 22:58 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/17 22:58 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/04/17 22:58 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/17 22:58 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/17 22:58 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/17 22:58 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/17 22:58 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/17 22:58 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/17 22:58 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/17 22:58 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/17 22:58 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/17 22:58 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/17 22:58 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/17 22:58 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/17 22:58 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 103 % 70-130 1 06/04/17 22:58 460-00-4 1,2-Dichloroethane-d4 (S) 87 % 70-130 1 06/04/17 22:58 17060-07-0 Toluene-d8 (S) 107 % 70-130 1 06/04/17 22:58 2037-26-5 Date: 06/19/2017 01:10 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 32 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-14 Lab ID: 92342478008 Collected: 06/01/17 09:00 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Antimony ND ug/L 6.0 3.9 1 06/04/1717:05 06/09/1719:08 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/04/1717:05 06/09/1719:08 7440-38-2 Barium 84.OJ ug/L 100 2.5 1 06/04/1717:05 06/09/1719:08 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 06/04/1717:05 06/09/1719:08 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 06/04/1717:05 06/09/1719:08 7440-43-9 Chromium 12.4 ug/L 10.0 2.5 1 06/04/1717:05 06/09/1719:08 7440-47-3 Cobalt 13.1 ug/L 10.0 2.5 1 06/04/1717:05 06/09/1719:08 7440-48-4 Copper 6.9J ug/L 10.0 2.5 1 06/04/1717:05 06/09/1719:08 7440-50-8 Lead 3.OJ ug/L 10.0 2.5 1 06/04/1717:05 06/09/1719:08 7439-92-1 Nickel 8.6J ug/L 50.0 2.5 1 06/04/1717:05 06/09/1719:08 7440-02-0 Selenium ND ug/L 10.0 5.0 1 06/04/1717:05 06/09/1719:08 7782-49-2 Silver ND ug/L 10.0 2.5 1 06/04/1717:05 06/09/1719:08 7440-22-4 Vanadium 18.01 ug/L 25.0 2.5 1 06/04/1717:05 06/09/1719:08 7440-62-2 Zinc 36.1 ug/L 10.0 5.0 1 06/04/1717:05 06/09/1719:08 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Thallium 0.16J ug/L 5.5 0.020 1 06/03/17 02:25 06/09/17 16:46 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 13.5J ug/L 100 10.0 1 06/04/17 23:16 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 06/04/17 23:16 107-13-1 Benzene ND ug/L 1.0 0.25 1 06/04/17 23:16 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 06/04/17 23:16 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 06/04/17 23:16 75-27-4 Bromoform ND ug/L 3.0 0.26 1 06/04/17 23:16 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 06/04/17 23:16 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 06/04/17 23:16 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 06/04/17 23:16 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 06/04/17 23:16 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 06/04/17 23:16 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 06/04/17 23:16 75-00-3 Chloroform ND ug/L 5.0 0.14 1 06/04/17 23:16 67-66-3 Chloromethane 0.32J ug/L 1.0 0.11 1 06/04/17 23:16 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 06/04/17 23:16 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 06/04/17 23:16 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 06/04/17 23:16 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 06/04/17 23:16 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 06/04/17 23:16 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 06/04/17 23:16 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/04/17 23:16 110-57-6 1,1-Dichloroethane 2.6J ug/L 5.0 0.32 1 06/04/17 23:16 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 06/04/17 23:16 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/04/17 23:16 75-35-4 cis-1,2-Dichloroethene 4.OJ ug/L 5.0 0.19 1 06/04/17 23:16 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/04/17 23:16 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 06/04/17 23:16 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-14 Lab ID: 92342478008 Collected: 06/01/17 09:00 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/04/17 23:16 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/17 23:16 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/17 23:16 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/04/17 23:16 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/17 23:16 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/17 23:16 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/17 23:16 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/04/17 23:16 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/17 23:16 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/17 23:16 79-34-5 Tetrachloroethene 0.54J ug/L 1.0 0.46 1 06/04/17 23:16 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/17 23:16 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/17 23:16 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/17 23:16 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/17 23:16 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/17 23:16 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/17 23:16 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/17 23:16 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/17 23:16 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/17 23:16 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 06/04/17 23:16 460-00-4 1,2-Dichloroethane-d4 (S) 90 % 70-130 1 06/04/17 23:16 17060-07-0 Toluene-d8 (S) 108 % 70-130 1 06/04/17 23:16 2037-26-5 Date: 06/19/2017 01:10 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 34 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-18 Lab ID: 92342478009 Collected: 06/01/17 10:15 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Antimony ND ug/L 6.0 3.9 1 06/04/1717:05 06/09/1719:11 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/04/1717:05 06/09/1719:11 7440-38-2 Barium 28.4J ug/L 100 2.5 1 06/04/1717:05 06/09/1719:11 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 06/04/1717:05 06/09/1719:11 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 06/04/1717:05 06/09/1719:11 7440-43-9 Chromium 2.6J ug/L 10.0 2.5 1 06/04/1717:05 06/09/1719:11 7440-47-3 Cobalt ND ug/L 10.0 2.5 1 06/04/1717:05 06/09/1719:11 7440-48-4 Copper 122 ug/L 10.0 2.5 1 06/04/1717:05 06/09/1719:11 7440-50-8 Lead 9.2J ug/L 10.0 2.5 1 06/04/1717:05 06/09/1719:11 7439-92-1 Nickel ND ug/L 50.0 2.5 1 06/04/1717:05 06/09/1719:11 7440-02-0 Selenium ND ug/L 10.0 5.0 1 06/04/1717:05 06/09/1719:11 7782-49-2 Silver ND ug/L 10.0 2.5 1 06/04/1717:05 06/09/1719:11 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 06/04/1717:05 06/09/1719:11 7440-62-2 Zinc 10.7 ug/L 10.0 5.0 1 06/04/1717:05 06/09/1719:11 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Thallium ND ug/L 5.5 0.020 1 06/03/17 02:25 06/09/17 16:47 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 06/04/17 23:34 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 06/04/17 23:34 107-13-1 Benzene ND ug/L 1.0 0.25 1 06/04/17 23:34 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 06/04/17 23:34 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 06/04/17 23:34 75-27-4 Bromoform ND ug/L 3.0 0.26 1 06/04/17 23:34 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 06/04/17 23:34 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 06/04/17 23:34 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 06/04/17 23:34 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 06/04/17 23:34 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 06/04/17 23:34 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 06/04/17 23:34 75-00-3 Chloroform ND ug/L 5.0 0.14 1 06/04/17 23:34 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 06/04/17 23:34 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 06/04/17 23:34 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 06/04/17 23:34 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 06/04/17 23:34 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 06/04/17 23:34 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 06/04/17 23:34 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 06/04/17 23:34 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/04/17 23:34 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 06/04/17 23:34 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 06/04/17 23:34 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/04/17 23:34 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 06/04/17 23:34 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/04/17 23:34 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 06/04/17 23:34 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-18 Lab ID: 92342478009 Collected: 06/01/17 10:15 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/04/17 23:34 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/17 23:34 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/17 23:34 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/04/17 23:34 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/17 23:34 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/17 23:34 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/17 23:34 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/04/17 23:34 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/17 23:34 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/17 23:34 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/17 23:34 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/17 23:34 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/17 23:34 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/17 23:34 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/17 23:34 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/17 23:34 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/17 23:34 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/17 23:34 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/17 23:34 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/17 23:34 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 103 % 70-130 1 06/04/17 23:34 460-00-4 1,2-Dichloroethane-d4 (S) 88 % 70-130 1 06/04/17 23:34 17060-07-0 Toluene-d8 (S) 115 % 70-130 1 06/04/17 23:34 2037-26-5 Date: 06/19/2017 01:10 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 36 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-19 Lab ID: 92342478010 Collected: 05/31/17 09:00 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Antimony ND ug/L 6.0 3.9 1 06/04/1717:05 06/09/1719:15 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/04/1717:05 06/09/1719:15 7440-38-2 Barium 70.2J ug/L 100 2.5 1 06/04/1717:05 06/09/1719:15 7440-39-3 Beryllium 0.61J ug/L 1.0 0.50 1 06/04/1717:05 06/09/1719:15 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 06/04/1717:05 06/09/1719:15 7440-43-9 Chromium 5.6J ug/L 10.0 2.5 1 06/04/1717:05 06/09/1719:15 7440-47-3 Cobalt 4.1J ug/L 10.0 2.5 1 06/04/1717:05 06/09/1719:15 7440-48-4 Copper 4.4J ug/L 10.0 2.5 1 06/04/1717:05 06/09/1719:15 7440-50-8 Lead 3.OJ ug/L 10.0 2.5 1 06/04/1717:05 06/09/1719:15 7439-92-1 Nickel ND ug/L 50.0 2.5 1 06/04/1717:05 06/09/1719:15 7440-02-0 Selenium ND ug/L 10.0 5.0 1 06/04/1717:05 06/09/1719:15 7782-49-2 Silver ND ug/L 10.0 2.5 1 06/04/1717:05 06/09/1719:15 7440-22-4 Vanadium 8.2J ug/L 25.0 2.5 1 06/04/1717:05 06/09/1719:15 7440-62-2 Zinc 20.2 ug/L 10.0 5.0 1 06/04/1717:05 06/09/1719:15 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Thallium 0.081J ug/L 5.5 0.020 1 06/03/17 02:25 06/09/17 16:49 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 06/04/17 23:52 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 06/04/17 23:52 107-13-1 Benzene ND ug/L 1.0 0.25 1 06/04/17 23:52 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 06/04/17 23:52 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 06/04/17 23:52 75-27-4 Bromoform ND ug/L 3.0 0.26 1 06/04/17 23:52 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 06/04/17 23:52 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 06/04/17 23:52 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 06/04/17 23:52 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 06/04/17 23:52 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 06/04/17 23:52 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 06/04/17 23:52 75-00-3 Chloroform ND ug/L 5.0 0.14 1 06/04/17 23:52 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 06/04/17 23:52 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 06/04/17 23:52 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 06/04/17 23:52 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 06/04/17 23:52 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 06/04/17 23:52 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 06/04/17 23:52 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 06/04/17 23:52 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/04/17 23:52 110-57-6 1,1-Dichloroethane 0.36J ug/L 5.0 0.32 1 06/04/17 23:52 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 06/04/17 23:52 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/04/17 23:52 75-35-4 cis-1,2-Dichloroethene 0.65J ug/L 5.0 0.19 1 06/04/17 23:52 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/04/17 23:52 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 06/04/17 23:52 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-19 Lab ID: 92342478010 Collected: 05/31/17 09:00 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/04/17 23:52 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/17 23:52 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/17 23:52 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/04/17 23:52 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/17 23:52 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/17 23:52 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/17 23:52 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/04/17 23:52 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/17 23:52 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/17 23:52 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/17 23:52 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/17 23:52 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/17 23:52 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/17 23:52 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/17 23:52 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/17 23:52 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/17 23:52 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/17 23:52 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/17 23:52 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/17 23:52 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 103 % 70-130 1 06/04/17 23:52 460-00-4 1,2-Dichloroethane-d4 (S) 92 % 70-130 1 06/04/17 23:52 17060-07-0 Toluene-d8 (S) 109 % 70-130 1 06/04/17 23:52 2037-26-5 Date: 06/19/2017 01:10 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 38 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-20 Lab ID: 92342478011 Collected: 06/01/17 15:30 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Vanadium Zinc 6020 MET ICPMS Thallium 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane Date: 06/19/2017 01:10 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 06/04/1717:05 06/09/1719:18 7440-36-0 ND ug/L 10.0 5.0 1 06/04/1717:05 06/09/1719:18 7440-38-2 27.6J ug/L 100 2.5 1 06/04/1717:05 06/09/1719:18 7440-39-3 ND ug/L 1.0 0.50 1 06/04/1717:05 06/09/1719:18 7440-41-7 ND ug/L 1.0 0.50 1 06/04/1717:05 06/09/1719:18 7440-43-9 ND ug/L 10.0 2.5 1 06/04/1717:05 06/09/1719:18 7440-47-3 12.3 ug/L 10.0 2.5 1 06/04/1717:05 06/09/1719:18 7440-48-4 ND ug/L 10.0 2.5 1 06/04/1717:05 06/09/1719:18 7440-50-8 ND ug/L 10.0 2.5 1 06/04/1717:05 06/09/1719:18 7439-92-1 ND ug/L 50.0 2.5 1 06/04/1717:05 06/09/1719:18 7440-02-0 ND ug/L 10.0 5.0 1 06/04/1717:05 06/09/1719:18 7782-49-2 ND ug/L 10.0 2.5 1 06/04/1717:05 06/09/1719:18 7440-22-4 ND ug/L 25.0 2.5 1 06/04/1717:05 06/09/1719:18 7440-62-2 7.7J ug/L 10.0 5.0 1 06/04/1717:05 06/09/1719:18 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3010A 0.32J ug/L 5.5 0.020 1 06/03/17 02:25 06/09/17 16:51 7440-28-0 Analytical Method: EPA 8260 14.4J ug/L 100 10.0 1 06/05/17 00:27 67-64-1 ND ug/L 200 1.9 1 06/05/17 00:27 107-13-1 ND ug/L 1.0 0.25 1 06/05/17 00:27 71-43-2 ND ug/L 3.0 0.17 1 06/05/17 00:27 74-97-5 ND ug/L 1.0 0.18 1 06/05/17 00:27 75-27-4 ND ug/L 3.0 0.26 1 06/05/17 00:27 75-25-2 ND ug/L 10.0 0.29 1 06/05/17 00:27 74-83-9 ND ug/L 100 0.96 1 06/05/17 00:27 78-93-3 ND ug/L 100 1.2 1 06/05/17 00:27 75-15-0 ND ug/L 1.0 0.25 1 06/05/17 00:27 56-23-5 ND ug/L 3.0 0.23 1 06/05/17 00:27 108-90-7 ND ug/L 10.0 0.54 1 06/05/17 00:27 75-00-3 ND ug/L 5.0 0.14 1 06/05/17 00:27 67-66-3 ND ug/L 1.0 0.11 1 06/05/17 00:27 74-87-3 ND ug/L 13.0 2.0 1 06/05/17 00:27 96-12-8 ND ug/L 3.0 0.21 1 06/05/17 00:27 124-48-1 ND ug/L 1.0 0.27 1 06/05/17 00:27 106-93-4 ND ug/L 10.0 0.21 1 06/05/17 00:27 74-95-3 ND ug/L 5.0 0.30 1 06/05/17 00:27 95-50-1 ND ug/L 1.0 0.33 1 06/05/17 00:27 106-46-7 ND ug/L 100 1.0 1 06/05/17 00:27 110-57-6 ND ug/L 5.0 0.32 1 06/05/17 00:27 75-34-3 ND ug/L 1.0 0.24 1 06/05/17 00:27 107-06-2 ND ug/L 5.0 0.56 1 06/05/17 00:27 75-35-4 0.64J ug/L 5.0 0.19 1 06/05/17 00:27 156-59-2 ND ug/L 5.0 0.49 1 06/05/17 00:27 156-60-5 ND ug/L 1.0 0.27 1 06/05/17 00:27 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 39 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-20 Lab ID: 92342478011 Collected: 06/01/17 15:30 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/05/17 00:27 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/05/17 00:27 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/05/17 00:27 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/05/17 00:27 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/05/17 00:27 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/05/17 00:27 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/05/17 00:27 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/05/17 00:27 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/05/17 00:27 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/05/17 00:27 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/05/17 00:27 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/05/17 00:27 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/05/17 00:27 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/05/17 00:27 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/05/17 00:27 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/05/17 00:27 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/05/17 00:27 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/05/17 00:27 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/05/17 00:27 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/05/17 00:27 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 103 % 70-130 1 06/05/17 00:27 460-00-4 1,2-Dichloroethane-d4 (S) 89 % 70-130 1 06/05/17 00:27 17060-07-0 Toluene-d8 (S) 110 % 70-130 1 06/05/17 00:27 2037-26-5 Date: 06/19/2017 01:10 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 40 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-13 Lab ID: 92342530001 Collected: 05/31/17 17:35 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 Organochlorine Pesticides Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Surrogates Decachlorobiphenyl (S) 8151 Chlorinated Herbicides 2,4-D Dinoseb Pentachlorophenol 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 6010 MET ICP Antimony Arsenic Date: 06/19/2017 01:10 PM Analytical Method: EPA 8081 Preparation Method: EPA 3510 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 22:13 309-00-2 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 22:13 319-84-6 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 22:13 319-85-7 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 22:13 319-86-8 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 22:13 58-89-9 ND ug/L 0.50 0.20 1 06/02/17 10:09 06/06/17 22:13 57-74-9 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 22:13 72-54-8 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 22:13 72-55-9 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 22:13 50-29-3 ND ug/L 0.075 0.050 1 06/02/17 10:09 06/06/17 22:13 60-57-1 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 22:13 959-98-8 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 22:13 33213-65-9 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 22:13 1031-07-8 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 22:13 72-20-8 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 22:13 7421-93-4 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 22:13 76-44-8 ND ug/L 0.075 0.050 1 06/02/17 10:09 06/06/17 22:13 1024-57-3 ND ug/L 1.0 0.15 1 06/02/17 10:09 06/06/17 22:13 72-43-5 ND ug/L 1.5 0.20 1 06/02/17 10:09 06/06/17 22:13 8001-35-2 53 % 20-130 1 06/02/17 10:09 06/06/17 22:13 877-09-8 50 % 20-130 1 06/02/17 10:09 06/06/17 22:13 2051-24-3 Analytical Method: EPA 8082 Preparation Method: EPA 3510 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/17 20:42 12674-11-2 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/17 20:42 11104-28-2 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/17 20:42 11141-16-5 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/17 20:42 53469-21-9 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/17 20:42 12672-29-6 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/17 20:42 11097-69-1 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/17 20:42 11096-82-5 44 % 10-132 1 06/02/17 10:09 06/03/17 20:42 2051-24-3 Analytical Method: EPA 8151 Preparation Method: EPA 8151 ND ug/L 1.0 0.24 1 06/07/17 16:00 06/10/17 00:39 94-75-7 ND ug/L 0.20 0.061 1 06/07/17 16:00 06/10/17 00:39 88-85-7 ND ug/L 0.030 0.018 1 06/07/17 16:00 06/10/17 00:39 87-86-5 ND ug/L 0.20 0.045 1 06/07/17 16:00 06/10/17 00:39 93-76-5 ND ug/L 0.20 0.052 1 06/07/17 16:00 06/10/17 00:39 93-72-1 66 % 39-139 1 06/07/17 16:00 06/10/17 00:39 19719-28-9 Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 06/02/17 11:25 06/09/17 21:26 7440-36-0 ND ug/L 10.0 5.0 1 06/02/17 11:25 06/09/17 21:26 7440-38-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 41 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-13 Lab ID: 92342530001 Collected: 05/31/17 17:35 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Tin Vanadium Zinc 6020 MET ICPMS Thallium 7470 Mercury Mercury 8270 MSSV Semivolatile Organic Acenaphthene Acenaphthylene Acetophenone 2-Acetylaminofluorene 4-Aminobiphenyl Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-ChIoro-3-methyl phenol 4-Chloroaniline Chlorobenzilate bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Diallate Dibenz(a,h)anthracene Date: 06/19/2017 01:10 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010A 85.7J ug/L 100 2.5 1 06/02/17 11:25 06/09/17 21:26 7440-39-3 ND ug/L 1.0 0.50 1 06/02/17 11:25 06/09/17 21:26 7440-41-7 1.5 ug/L 1.0 0.50 1 06/02/17 11:25 06/09/17 21:26 7440-43-9 2.8J ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:26 7440-47-3 11.0 ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:26 7440-48-4 ND ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:26 7440-50-8 ND ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:26 7439-92-1 2.6J ug/L 50.0 2.5 1 06/02/17 11:25 06/09/17 21:26 7440-02-0 ND ug/L 10.0 5.0 1 06/02/17 11:25 06/09/17 21:26 7782-49-2 ND ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:26 7440-22-4 ND ug/L 100 2.5 1 06/02/17 11:25 06/09/17 21:26 7440-31-5 ND ug/L 25.0 2.5 1 06/02/17 11:25 06/09/17 21:26 7440-62-2 8.4J ug/L 10.0 5.0 1 06/02/17 11:25 06/09/17 21:26 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3010A 0.12J ug/L 5.5 0.020 1 06/06/17 02:45 06/09/17 17:12 7440-28-0 Analytical Method: EPA 7470 Preparation Method: EPA 7470 ND ug/L 0.20 0.10 1 06/05/17 20:00 06/07/17 01:43 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1715:31 83-32-9 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1715:31 208-96-8 ND ug/L 10.0 1.9 1 06/07/1717:10 06/14/1715:31 98-86-2 ND ug/L 20.0 1.6 1 06/07/1717:10 06/14/1715:31 53-96-3 ND ug/L 20.0 1.7 1 06/07/1717:10 06/14/1715:31 92-67-1 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1715:31 120-12-7 ND ug/L 10.0 2.1 1 06/07/1717:10 06/14/1715:31 56-55-3 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1715:31 50-32-8 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1715:31 205-99-2 ND ug/L 10.0 2.1 1 06/07/1717:10 06/14/1715:31 191-24-2 ND ug/L 10.0 2.0 1 06/07/1717:10 06/14/1715:31 207-08-9 ND ug/L 20.0 3.1 1 06/07/1717:10 06/14/1715:31 100-51-6 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1715:31 101-55-3 ND ug/L 10.0 2.5 1 06/07/1717:10 06/14/1715:31 85-68-7 ND ug/L 20.0 2.8 1 06/07/1717:10 06/14/1715:31 59-50-7 ND ug/L 20.0 2.8 1 06/07/1717:10 06/14/1715:31 106-47-8 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1715:31 510-15-6 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1715:31 111-91-1 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1715:31 111-44-4 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1715:31 91-58-7 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1715:31 95-57-8 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1715:31 7005-72-3 ND ug/L 10.0 2.1 1 06/07/1717:10 06/14/1715:31 218-01-9 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1715:31 2303-16-4 ND ug/L 10.0 2.0 1 06/07/1717:10 06/14/1715:31 53-70-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. L2 Page 42 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-13 Lab ID: 92342530001 Collected: 05/31/17 17:35 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Dibenzofuran ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 15:31 132-64-9 3,3'-Dichlorobenzidine ND ug/L 20.0 3.9 1 06/07/17 17:10 06/14/17 15:31 91-94-1 2,4-Dichlorophenol ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 15:31 120-83-2 2,6-Dichlorophenol ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 15:31 87-65-0 Diethylphthalate ND ug/L 6000 1.6 1 06/07/17 17:10 06/14/17 15:31 84-66-2 Dimethoate ND ug/L 20.0 1.8 1 06/07/17 17:10 06/14/17 15:31 60-51-5 P-Dimethylaminoazobenzene ND ug/L 10.0 1.0 1 06/07/17 17:10 06/14/17 15:31 60-11-7 7,12-Dimethylbenz(a)anthracene ND ug/L 10.0 2.4 1 06/07/17 17:10 06/14/17 15:31 57-97-6 3,3'-Dimethylbenzidine ND ug/L 10.0 3.9 1 06/07/17 17:10 06/14/17 15:31 119-93-7 2,4-Dimethylphenol ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 15:31 105-67-9 Dimethylphthalate ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 15:31 131-11-3 Di-n-butylphthalate ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 15:31 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 50.0 2.2 1 06/07/17 17:10 06/14/17 15:31 534-52-1 1,3-Dinitrobenzene ND ug/L 20.0 1.3 1 06/07/17 17:10 06/14/17 15:31 99-65-0 2,4-Dinitrophenol ND ug/L 50.0 5.1 1 06/07/17 17:10 06/14/17 15:31 51-28-5 2,4-Dinitrotoluene ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 15:31 121-14-2 2,6-Dinitrotoluene ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 15:31 606-20-2 Di-n-octylphthalate ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 15:31 117-84-0 Diphenylamine ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 15:31 122-39-4 Disulfoton ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 15:31 298-04-4 bis(2- Ethyl hexyl)phthalate ND ug/L 15.0 2.3 1 06/07/17 17:10 06/14/17 15:31 117-81-7 Ethyl methanesulfonate ND ug/L 20.0 1.6 1 06/07/17 17:10 06/14/17 15:31 62-50-0 Famphur ND ug/L 20.0 5.7 1 06/07/17 17:10 06/14/17 15:31 52-85-7 Fluoranthene ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 15:31 206-44-0 Fluorene ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 15:31 86-73-7 Hexachlorobenzene ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 15:31 118-74-1 Hexachlorocyclopentadiene ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 15:31 77-47-4 Hexachloroethane ND ug/L 10.0 1.8 1 06/07/17 17:10 06/14/17 15:31 67-72-1 Hexachloropropene ND ug/L 10.0 1.2 1 06/07/17 17:10 06/14/17 15:31 1888-71-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 15:31 193-39-5 Isodrin ND ug/L 20.0 2.5 1 06/07/17 17:10 06/14/17 15:31 465-73-6 Isophorone ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 15:31 78-59-1 Isosafrole ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 15:31 120-58-1 Kepone ND ug/L 20.0 4.5 1 06/07/17 17:10 06/14/17 15:31 143-50-0 Methapyrilene ND ug/L 100 3.0 1 06/07/17 17:10 06/14/17 15:31 91-80-5 3-Methylcholanthrene ND ug/L 10.0 2.7 1 06/07/17 17:10 06/14/17 15:31 56-49-5 Methyl methanesulfonate ND ug/L 10.0 1.1 1 06/07/17 17:10 06/14/17 15:31 66-27-3 2-Methylnaphthalene ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 15:31 91-57-6 Methyl parathion ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 15:31 298-00-0 2-Methylphenol(o-Cresol) ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 15:31 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 15:31 15831-10-4 1-Naphthalenamine ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 15:31 134-32-7 2-Naphthalenamine ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 15:31 91-59-8 1,4-Naphthoquinone ND ug/L 10.0 0.99 1 06/07/17 17:10 06/14/17 15:31 130-15-4 2-Nitroaniline ND ug/L 50.0 2.3 1 06/07/17 17:10 06/14/17 15:31 88-74-4 3-Nitroaniline ND ug/L 50.0 2.7 1 06/07/17 17:10 06/14/17 15:31 99-09-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-13 Lab ID: 92342530001 Collected: 05/31/17 17:35 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol 5-Nitro-o-toluidine N-Nitrosodiethylamine N-Nitrosodimethylamine N-Nitroso-di-n-butylamine N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine N-Nitrosomethylethylamine N-Nitrosopiperidine N-Nitrosopyrrolidine O,O,O-Triethylphosphorothioate 2,2'-Oxybis(1-chloropropane) Parathion (Ethyl parathion) Pentachlorobenzene Pentachloronitrobenzene Pentachlorophenol Phenacetin Phenanthrene Phenol p-Phenylenediamine Phorate Pronamide Pyrene Safrole 1,2,4,5-Tetrachlorobenzene 2,3,4,6-Tetrachlorophenol Thionazin O-Toluidine 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 1,3,5-Trinitrobenzene Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) 8260 MSV Low Level Landfill Acetone Acetonitrile Acrolein Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ug/L 20.0 3.4 1 06/07/1717:10 06/14/1715:31 100-01-6 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1715:31 98-95-3 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1715:31 88-75-5 ND ug/L 50.0 4.3 1 06/07/1717:10 06/14/1715:31 100-02-7 ND ug/L 10.0 1.9 1 06/07/1717:10 06/14/1715:31 99-55-8 ND ug/L 20.0 1.4 1 06/07/1717:10 06/14/1715:31 55-18-5 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1715:31 62-75-9 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1715:31 924-16-3 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1715:31 621-64-7 ND ug/L 10.0 1.4 1 06/07/1717:10 06/14/1715:31 86-30-6 ND ug/L 10.0 1.4 1 06/07/1717:10 06/14/1715:31 10595-95-6 ND ug/L 20.0 1.7 1 06/07/1717:10 06/14/1715:31 100-75-4 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1715:31 930-55-2 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1715:31 126-68-1 ND ug/L 10.0 1.8 1 06/07/1717:10 06/14/1715:31 108-60-1 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1715:31 56-38-2 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1715:31 608-93-5 ND ug/L 20.0 1.7 1 06/07/1717:10 06/14/1715:31 82-68-8 ND ug/L 25.0 3.5 1 06/07/1717:10 06/14/1715:31 87-86-5 ND ug/L 20.0 1.9 1 06/07/1717:10 06/14/1715:31 62-44-2 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1715:31 85-01-8 ND ug/L 10.0 1.3 1 06/07/1717:10 06/14/1715:31 108-95-2 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1715:31 106-50-3 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1715:31 298-02-2 ND ug/L 10.0 2.0 1 06/07/1717:10 06/14/1715:31 23950-58-5 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1715:31 129-00-0 ND ug/L 10.0 1.3 1 06/07/1717:10 06/14/1715:31 94-59-7 ND ug/L 10.0 1.3 1 06/07/1717:10 06/14/1715:31 95-94-3 ND ug/L 10.0 2.9 1 06/07/1717:10 06/14/1715:31 58-90-2 ND ug/L 20.0 1.7 1 06/07/1717:10 06/14/1715:31 297-97-2 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1715:31 95-53-4 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1715:31 95-95-4 ND ug/L 10.0 1.4 1 06/07/1717:10 06/14/1715:31 88-06-2 ND ug/L 10.0 1.2 1 06/07/1717:10 06/14/1715:31 99-35-4 48 % 21-110 1 06/07/1717:10 06/14/1715:31 4165-60-0 52 % 27-110 1 06/07/1717:10 06/14/1715:31 321-60-8 31 % 31-107 1 06/07/1717:10 06/14/1715:31 1718-51-0 18 % 10-110 1 06/07/1717:10 06/14/1715:31 13127-88-3 27 % 12-110 1 06/07/1717:10 06/14/1715:31 367-12-4 53 % 27-110 1 06/07/1717:10 06/14/1715:31 118-79-6 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 ND ug/L 55.0 2.2 1 ND ug/L 53.0 1.6 1 REPORT OF LABORATORY ANALYSIS 06/02/17 09:19 67-64-1 06/02/17 09:19 75-05-8 06/02/17 09:19 107-02-8 This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-13 Lab ID: 92342530001 Collected: 05/31/17 17:35 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acrylonitrile ND ug/L 200 1.9 1 06/02/17 09:19 107-13-1 Allyl chloride ND ug/L 10.0 1.5 1 06/02/17 09:19 107-05-1 Benzene ND ug/L 1.0 0.25 1 06/02/17 09:19 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 06/02/17 09:19 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 06/02/17 09:19 75-27-4 Bromoform ND ug/L 3.0 0.26 1 06/02/17 09:19 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 06/02/17 09:19 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 06/02/17 09:19 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 06/02/17 09:19 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 06/02/17 09:19 56-23-5 Chlorobenzene 1.6J ug/L 3.0 0.23 1 06/02/17 09:19 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 06/02/17 09:19 75-00-3 Chloroform ND ug/L 5.0 0.14 1 06/02/17 09:19 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 06/02/17 09:19 74-87-3 Chloroprene ND ug/L 20.0 0.27 1 06/02/17 09:19 126-99-8 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 06/02/17 09:19 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 06/02/17 09:19 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 06/02/17 09:19 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 06/02/17 09:19 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 06/02/17 09:19 95-50-1 1,3-Dichlorobenzene ND ug/L 5.0 0.24 1 06/02/17 09:19 541-73-1 1,4-Dichlorobenzene 3.6 ug/L 1.0 0.33 1 06/02/17 09:19 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/02/17 09:19 110-57-6 Dichlorodifluoromethane ND ug/L 5.0 0.21 1 06/02/17 09:19 75-71-8 1,1-Dichloroethane 4.OJ ug/L 5.0 0.32 1 06/02/17 09:19 75-34-3 1,2-Dichloroethane 0.96J ug/L 1.0 0.24 1 06/02/17 09:19 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/02/17 09:19 75-35-4 cis-1,2-Dichloroethene 28.1 ug/L 5.0 0.19 1 06/02/17 09:19 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/02/17 09:19 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 06/02/17 09:19 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 06/02/17 09:19 142-28-9 2,2-Dichloropropane ND ug/L 15.0 0.13 1 06/02/17 09:19 594-20-7 1,1-Dichloropropene ND ug/L 5.0 0.49 1 06/02/17 09:19 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/02/17 09:19 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/02/17 09:19 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/02/17 09:19 100-41-4 Ethyl methacrylate ND ug/L 10.0 0.20 1 06/02/17 09:19 97-63-2 Hexachloro-1,3-butadiene ND ug/L 10.0 0.71 1 06/02/17 09:19 87-68-3 2-Hexanone ND ug/L 50.0 0.46 1 06/02/17 09:19 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/02/17 09:19 74-88-4 Isobutanol ND ug/L 100 35.0 1 06/02/17 09:19 78-83-1 Methacrylonitrile ND ug/L 100 0.93 1 06/02/17 09:19 126-98-7 Methylene Chloride ND ug/L 1.0 0.97 1 06/02/17 09:19 75-09-2 Methyl methacrylate ND ug/L 30.0 2.0 1 06/02/17 09:19 80-62-6 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/02/17 09:19 108-10-1 Naphthalene ND ug/L 10.0 0.24 1 06/02/17 09:19 91-20-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-13 Lab ID: 92342530001 Collected: 05/31/17 17:35 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Propionitrile ND ug/L 150 3.6 1 06/02/17 09:19 107-12-0 Styrene ND ug/L 1.0 0.26 1 06/02/17 09:19 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/02/17 09:19 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/02/17 09:19 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/02/17 09:19 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/02/17 09:19 108-88-3 1,2,4-Trichlorobenzene ND ug/L 10.0 0.35 1 06/02/17 09:19 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/02/17 09:19 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/02/17 09:19 79-00-5 Trichloroethene 0.98J ug/L 1.0 0.47 1 06/02/17 09:19 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/02/17 09:19 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/02/17 09:19 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/02/17 09:19 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/02/17 09:19 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/02/17 09:19 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 117 % 70-130 1 06/02/17 09:19 460-00-4 1,2-Dichloroethane-d4 (S) 103 % 70-130 1 06/02/17 09:19 17060-07-0 Toluene-d8 (S) 111 % 70-130 1 06/02/17 09:19 2037-26-5 4500S2D Sulfide Water Analytical Method: SM 4500-S2D Sulfide ND ug/L 1000 100 1 06/06/17 23:00 18496-25-8 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E Cyanide ND ug/L 10.0 4.0 1 06/07/1713:31 57-12-5 Date: 06/19/2017 01:10 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 46 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-16 Lab ID: 92342530002 Collected: 05/31/17 16:50 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 Organochlorine Pesticides Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Surrogates Decachlorobiphenyl (S) 8151 Chlorinated Herbicides 2,4-D Dinoseb Pentachlorophenol 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 6010 MET ICP Antimony Arsenic Date: 06/19/2017 01:10 PM Analytical Method: EPA 8081 Preparation Method: EPA 3510 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 22:31 309-00-2 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 22:31 319-84-6 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 22:31 319-85-7 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 22:31 319-86-8 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 22:31 58-89-9 ND ug/L 0.50 0.20 1 06/02/17 10:09 06/06/17 22:31 57-74-9 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 22:31 72-54-8 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 22:31 72-55-9 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 22:31 50-29-3 ND ug/L 0.075 0.050 1 06/02/17 10:09 06/06/17 22:31 60-57-1 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 22:31 959-98-8 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 22:31 33213-65-9 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 22:31 1031-07-8 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 22:31 72-20-8 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 22:31 7421-93-4 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 22:31 76-44-8 ND ug/L 0.075 0.050 1 06/02/17 10:09 06/06/17 22:31 1024-57-3 ND ug/L 1.0 0.15 1 06/02/17 10:09 06/06/17 22:31 72-43-5 ND ug/L 1.5 0.20 1 06/02/17 10:09 06/06/17 22:31 8001-35-2 94 % 20-130 1 06/02/17 10:09 06/06/17 22:31 877-09-8 70 % 20-130 1 06/02/17 10:09 06/06/17 22:31 2051-24-3 Analytical Method: EPA 8082 Preparation Method: EPA 3510 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1712:43 12674-11-2 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1712:43 11104-28-2 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1712:43 11141-16-5 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1712:43 53469-21-9 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1712:43 12672-29-6 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1712:43 11097-69-1 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1712:43 11096-82-5 84 % 10-132 1 06/02/17 10:09 06/03/1712:43 2051-24-3 Analytical Method: EPA 8151 Preparation Method: EPA 8151 ND ug/L 0.98 0.23 1 06/07/17 16:00 06/10/17 01:09 94-75-7 ND ug/L 0.20 0.059 1 06/07/17 16:00 06/10/17 01:09 88-85-7 ND ug/L 0.030 0.018 1 06/07/17 16:00 06/10/17 01:09 87-86-5 ND ug/L 0.20 0.044 1 06/07/17 16:00 06/10/17 01:09 93-76-5 ND ug/L 0.20 0.051 1 06/07/17 16:00 06/10/17 01:09 93-72-1 78 % 39-139 1 06/07/17 16:00 06/10/17 01:09 19719-28-9 Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 06/02/17 11:25 06/09/17 21:29 7440-36-0 ND ug/L 10.0 5.0 1 06/02/17 11:25 06/09/17 21:29 7440-38-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 47 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-16 Lab ID: 92342530002 Collected: 05/31/17 16:50 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Tin Vanadium Zinc 6020 MET ICPMS Thallium 7470 Mercury Mercury 8270 MSSV Semivolatile Organic Acenaphthene Acenaphthylene Acetophenone 2-Acetylaminofluorene 4-Aminobiphenyl Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-ChIoro-3-methyl phenol 4-Chloroaniline Chlorobenzilate bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Diallate Dibenz(a,h)anthracene Date: 06/19/2017 01:10 PM Analytical Method: EPA 6010 Preparation Method: EPA 301 OA 68.OJ ug/L 100 2.5 1 06/02/17 11:25 06/09/17 21:29 7440-39-3 ND ug/L 1.0 0.50 1 06/02/17 11:25 06/09/17 21:29 7440-41-7 0.52J ug/L 1.0 0.50 1 06/02/17 11:25 06/09/17 21:29 7440-43-9 7.OJ ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:29 7440-47-3 242 ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:29 7440-48-4 3.8J ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:29 7440-50-8 2.7J ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:29 7439-92-1 13.2J ug/L 50.0 2.5 1 06/02/17 11:25 06/09/17 21:29 7440-02-0 ND ug/L 10.0 5.0 1 06/02/17 11:25 06/09/17 21:29 7782-49-2 ND ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:29 7440-22-4 ND ug/L 100 2.5 1 06/02/17 11:25 06/09/17 21:29 7440-31-5 ND ug/L 25.0 2.5 1 06/02/17 11:25 06/09/17 21:29 7440-62-2 14.7 ug/L 10.0 5.0 1 06/02/17 11:25 06/09/17 21:29 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3010A 0.20J ug/L 5.5 0.020 1 06/06/17 02:45 06/09/17 17:14 7440-28-0 Analytical Method: EPA 7470 Preparation Method: EPA 7470 ND ug/L 0.20 0.10 1 06/05/17 20:00 06/07/17 01:46 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1716:00 83-32-9 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1716:00 208-96-8 ND ug/L 10.0 1.9 1 06/07/1717:10 06/14/1716:00 98-86-2 ND ug/L 20.0 1.6 1 06/07/1717:10 06/14/1716:00 53-96-3 ND ug/L 20.0 1.7 1 06/07/1717:10 06/14/1716:00 92-67-1 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1716:00 120-12-7 ND ug/L 10.0 2.1 1 06/07/1717:10 06/14/1716:00 56-55-3 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1716:00 50-32-8 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1716:00 205-99-2 ND ug/L 10.0 2.1 1 06/07/1717:10 06/14/1716:00 191-24-2 ND ug/L 10.0 2.0 1 06/07/1717:10 06/14/1716:00 207-08-9 ND ug/L 20.0 3.1 1 06/07/1717:10 06/14/1716:00 100-51-6 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1716:00 101-55-3 ND ug/L 10.0 2.5 1 06/07/1717:10 06/14/1716:00 85-68-7 ND ug/L 20.0 2.8 1 06/07/1717:10 06/14/1716:00 59-50-7 ND ug/L 20.0 2.8 1 06/07/1717:10 06/14/1716:00 106-47-8 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1716:00 510-15-6 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1716:00 111-91-1 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1716:00 111-44-4 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1716:00 91-58-7 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1716:00 95-57-8 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1716:00 7005-72-3 ND ug/L 10.0 2.1 1 06/07/1717:10 06/14/1716:00 218-01-9 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1716:00 2303-16-4 ND ug/L 10.0 2.0 1 06/07/1717:10 06/14/1716:00 53-70-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. M1 L2 M1 Page 48 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-16 Lab ID: 92342530002 Collected: 05/31/17 16:50 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Dibenzofuran ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 16:00 132-64-9 3,3'-Dichlorobenzidine ND ug/L 20.0 3.9 1 06/07/17 17:10 06/14/17 16:00 91-94-1 2,4-Dichlorophenol ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:00 120-83-2 2,6-Dichlorophenol ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:00 87-65-0 Diethylphthalate ND ug/L 6000 1.6 1 06/07/17 17:10 06/14/17 16:00 84-66-2 Dimethoate ND ug/L 20.0 1.8 1 06/07/17 17:10 06/14/17 16:00 60-51-5 P-Dimethylaminoazobenzene ND ug/L 10.0 1.0 1 06/07/17 17:10 06/14/17 16:00 60-11-7 7,12-Dimethylbenz(a)anthracene ND ug/L 10.0 2.4 1 06/07/17 17:10 06/14/17 16:00 57-97-6 3,3'-Dimethylbenzidine ND ug/L 10.0 3.9 1 06/07/17 17:10 06/14/17 16:00 119-93-7 2,4-Dimethylphenol ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:00 105-67-9 Dimethylphthalate ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 16:00 131-11-3 Di-n-butylphthalate ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 16:00 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 50.0 2.2 1 06/07/17 17:10 06/14/17 16:00 534-52-1 1,3-Dinitrobenzene ND ug/L 20.0 1.3 1 06/07/17 17:10 06/14/17 16:00 99-65-0 2,4-Dinitrophenol ND ug/L 50.0 5.1 1 06/07/17 17:10 06/14/17 16:00 51-28-5 2,4-Dinitrotoluene ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:00 121-14-2 2,6-Dinitrotoluene ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 16:00 606-20-2 Di-n-octylphthalate ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:00 117-84-0 Diphenylamine ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 16:00 122-39-4 Disulfoton ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:00 298-04-4 bis(2- Ethyl hexyl)phthalate ND ug/L 15.0 2.3 1 06/07/17 17:10 06/14/17 16:00 117-81-7 Ethyl methanesulfonate ND ug/L 20.0 1.6 1 06/07/17 17:10 06/14/17 16:00 62-50-0 Famphur ND ug/L 20.0 5.7 1 06/07/17 17:10 06/14/17 16:00 52-85-7 Fluoranthene ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 16:00 206-44-0 Fluorene ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:00 86-73-7 Hexachlorobenzene ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 16:00 118-74-1 Hexachlorocyclopentadiene ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 16:00 77-47-4 Hexachloroethane ND ug/L 10.0 1.8 1 06/07/17 17:10 06/14/17 16:00 67-72-1 Hexachloropropene ND ug/L 10.0 1.2 1 06/07/17 17:10 06/14/17 16:00 1888-71-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 16:00 193-39-5 Isodrin ND ug/L 20.0 2.5 1 06/07/17 17:10 06/14/17 16:00 465-73-6 Isophorone ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:00 78-59-1 Isosafrole ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:00 120-58-1 Kepone ND ug/L 20.0 4.5 1 06/07/17 17:10 06/14/17 16:00 143-50-0 Methapyrilene ND ug/L 100 3.0 1 06/07/17 17:10 06/14/17 16:00 91-80-5 3-Methylcholanthrene ND ug/L 10.0 2.7 1 06/07/17 17:10 06/14/17 16:00 56-49-5 Methyl methanesulfonate ND ug/L 10.0 1.1 1 06/07/17 17:10 06/14/17 16:00 66-27-3 2-Methylnaphthalene ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 16:00 91-57-6 Methyl parathion ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:00 298-00-0 2-Methylphenol(o-Cresol) ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:00 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 16:00 15831-10-4 1-Naphthalenamine ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 16:00 134-32-7 2-Naphthalenamine ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 16:00 91-59-8 1,4-Naphthoquinone ND ug/L 10.0 0.99 1 06/07/17 17:10 06/14/17 16:00 130-15-4 2-Nitroaniline ND ug/L 50.0 2.3 1 06/07/17 17:10 06/14/17 16:00 88-74-4 3-Nitroaniline ND ug/L 50.0 2.7 1 06/07/17 17:10 06/14/17 16:00 99-09-2 REPORT OF LABORATORY ANALYSIS M1 M1 M1 This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 49 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-16 Lab ID: 92342530002 Collected: 05/31/17 16:50 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 4-Nitroaniline ND ug/L 20.0 3.4 1 06/07/17 17:10 06/14/17 16:00 100-01-6 M1 Nitrobenzene ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:00 98-95-3 2-Nitrophenol ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:00 88-75-5 4-Nitrophenol ND ug/L 50.0 4.3 1 06/07/17 17:10 06/14/17 16:00 100-02-7 5-Nitro-o-toluidine ND ug/L 10.0 1.9 1 06/07/17 17:10 06/14/17 16:00 99-55-8 N-Nitrosodiethylamine ND ug/L 20.0 1.4 1 06/07/17 17:10 06/14/17 16:00 55-18-5 N-Nitrosodimethylamine ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:00 62-75-9 N-Nitroso-di-n-butylamine ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:00 924-16-3 N-Nitroso-di-n-propylamine ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 16:00 621-64-7 N-Nitrosodiphenylamine ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 16:00 86-30-6 N-Nitrosomethylethylamine ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 16:00 10595-95-6 M1 N-Nitrosopiperidine ND ug/L 20.0 1.7 1 06/07/17 17:10 06/14/17 16:00 100-75-4 N-Nitrosopyrrolidine ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 16:00 930-55-2 O,O,O-Triethylphosphorothioate ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 16:00 126-68-1 2,2'-Oxybis(1-chloropropane) ND ug/L 10.0 1.8 1 06/07/17 17:10 06/14/17 16:00 108-60-1 Parathion (Ethyl parathion) ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:00 56-38-2 Pentachlorobenzene ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:00 608-93-5 Pentachloronitrobenzene ND ug/L 20.0 1.7 1 06/07/17 17:10 06/14/17 16:00 82-68-8 Pentachlorophenol ND ug/L 25.0 3.5 1 06/07/17 17:10 06/14/17 16:00 87-86-5 Phenacetin ND ug/L 20.0 1.9 1 06/07/17 17:10 06/14/17 16:00 62-44-2 Phenanthrene ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:00 85-01-8 Phenol ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 16:00 108-95-2 p-Phenylenediamine ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 16:00 106-50-3 Phorate ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 16:00 298-02-2 Pronamide ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 16:00 23950-58-5 Pyrene ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 16:00 129-00-0 Safrole ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 16:00 94-59-7 1,2,4,5-Tetrachlorobenzene ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 16:00 95-94-3 2,3,4,6-Tetrachlorophenol ND ug/L 10.0 2.9 1 06/07/17 17:10 06/14/17 16:00 58-90-2 M1 Thionazin ND ug/L 20.0 1.7 1 06/07/17 17:10 06/14/17 16:00 297-97-2 O-Toluidine ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 16:00 95-53-4 M1 2,4,5-Trichlorophenol ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:00 95-95-4 2,4,6-Trichlorophenol ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 16:00 88-06-2 1,3,5-Trinitrobenzene ND ug/L 10.0 1.2 1 06/07/17 17:10 06/14/17 16:00 99-35-4 Surrogates Nitrobenzene-d5 (S) 54 % 21-110 1 06/07/17 17:10 06/14/17 16:00 4165-60-0 2-Fluorobiphenyl (S) 66 % 27-110 1 06/07/17 17:10 06/14/17 16:00 321-60-8 Terphenyl-d14 (S) 66 % 31-107 1 06/07/17 17:10 06/14/17 16:00 1718-51-0 Phenol-d6 (S) 21 % 10-110 1 06/07/17 17:10 06/14/17 16:00 13127-88-3 2-Fluorophenol (S) 32 % 12-110 1 06/07/17 17:10 06/14/17 16:00 367-12-4 2,4,6-Tribromophenol (S) 73 % 27-110 1 06/07/17 17:10 06/14/17 16:00 118-79-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 20.7J ug/L 100 10.0 1 06/02/17 09:36 67-64-1 Acetonitrile ND ug/L 55.0 2.2 1 06/02/17 09:36 75-05-8 Acrolein ND ug/L 53.0 1.6 1 06/02/17 09:36 107-02-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 50 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-16 Lab ID: 92342530002 Collected: 05/31/17 16:50 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acrylonitrile ND ug/L 200 1.9 1 06/02/17 09:36 107-13-1 Allyl chloride ND ug/L 10.0 1.5 1 06/02/17 09:36 107-05-1 Benzene 0.44J ug/L 1.0 0.25 1 06/02/17 09:36 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 06/02/17 09:36 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 06/02/17 09:36 75-27-4 Bromoform ND ug/L 3.0 0.26 1 06/02/17 09:36 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 06/02/17 09:36 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 06/02/17 09:36 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 06/02/17 09:36 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 06/02/17 09:36 56-23-5 Chlorobenzene 1.81 ug/L 3.0 0.23 1 06/02/17 09:36 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 06/02/17 09:36 75-00-3 Chloroform ND ug/L 5.0 0.14 1 06/02/17 09:36 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 06/02/17 09:36 74-87-3 Chloroprene ND ug/L 20.0 0.27 1 06/02/17 09:36 126-99-8 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 06/02/17 09:36 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 06/02/17 09:36 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 06/02/17 09:36 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 06/02/17 09:36 74-95-3 1,2-Dichlorobenzene 0.48J ug/L 5.0 0.30 1 06/02/17 09:36 95-50-1 1,3-Dichlorobenzene ND ug/L 5.0 0.24 1 06/02/17 09:36 541-73-1 1,4-Dichlorobenzene 4.3 ug/L 1.0 0.33 1 06/02/17 09:36 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/02/17 09:36 110-57-6 Dichlorodifluoromethane ND ug/L 5.0 0.21 1 06/02/17 09:36 75-71-8 1,1-Dichloroethane 0.58J ug/L 5.0 0.32 1 06/02/17 09:36 75-34-3 1,2-Dichloroethane 0.81J ug/L 1.0 0.24 1 06/02/17 09:36 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/02/17 09:36 75-35-4 cis-1,2-Dichloroethene 11.5 ug/L 5.0 0.19 1 06/02/17 09:36 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/02/17 09:36 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 06/02/17 09:36 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 06/02/17 09:36 142-28-9 2,2-Dichloropropane ND ug/L 15.0 0.13 1 06/02/17 09:36 594-20-7 1,1-Dichloropropene ND ug/L 5.0 0.49 1 06/02/17 09:36 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/02/17 09:36 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/02/17 09:36 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/02/17 09:36 100-41-4 Ethyl methacrylate ND ug/L 10.0 0.20 1 06/02/17 09:36 97-63-2 Hexachloro-1,3-butadiene ND ug/L 10.0 0.71 1 06/02/17 09:36 87-68-3 2-Hexanone ND ug/L 50.0 0.46 1 06/02/17 09:36 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/02/17 09:36 74-88-4 Isobutanol ND ug/L 100 35.0 1 06/02/17 09:36 78-83-1 Methacrylonitrile ND ug/L 100 0.93 1 06/02/17 09:36 126-98-7 Methylene Chloride ND ug/L 1.0 0.97 1 06/02/17 09:36 75-09-2 Methyl methacrylate ND ug/L 30.0 2.0 1 06/02/17 09:36 80-62-6 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/02/17 09:36 108-10-1 Naphthalene ND ug/L 10.0 0.24 1 06/02/17 09:36 91-20-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 51 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-16 Lab ID: 92342530002 Collected: 05/31/17 16:50 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Propionitrile ND ug/L 150 3.6 1 06/02/17 09:36 107-12-0 Styrene ND ug/L 1.0 0.26 1 06/02/17 09:36 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/02/17 09:36 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/02/17 09:36 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/02/17 09:36 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/02/17 09:36 108-88-3 1,2,4-Trichlorobenzene ND ug/L 10.0 0.35 1 06/02/17 09:36 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/02/17 09:36 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/02/17 09:36 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/02/17 09:36 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/02/17 09:36 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/02/17 09:36 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/02/17 09:36 108-05-4 Vinyl chloride 1.3 ug/L 1.0 0.62 1 06/02/17 09:36 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/02/17 09:36 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 117 % 70-130 1 06/02/17 09:36 460-00-4 1,2-Dichloroethane-d4 (S) 104 % 70-130 1 06/02/17 09:36 17060-07-0 Toluene-d8 (S) 112 % 70-130 1 06/02/17 09:36 2037-26-5 4500S2D Sulfide Water Analytical Method: SM 4500-S2D Sulfide ND ug/L 1000 100 1 06/06/17 23:00 18496-25-8 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E Cyanide 12.7 ug/L 10.0 4.0 1 06/07/1713:32 57-12-5 Date: 06/19/2017 01:10 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 52 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-17 Lab ID: 92342530003 Collected: 05/31/17 16:30 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 Organochlorine Pesticides Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Surrogates Decachlorobiphenyl (S) 8151 Chlorinated Herbicides 2,4-D Dinoseb Pentachlorophenol 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 6010 MET ICP Antimony Arsenic Date: 06/19/2017 01:10 PM Analytical Method: EPA 8081 Preparation Method: EPA 3510 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 22:49 309-00-2 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 22:49 319-84-6 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 22:49 319-85-7 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 22:49 319-86-8 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 22:49 58-89-9 ND ug/L 0.50 0.20 1 06/02/17 10:09 06/06/17 22:49 57-74-9 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 22:49 72-54-8 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 22:49 72-55-9 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 22:49 50-29-3 ND ug/L 0.075 0.050 1 06/02/17 10:09 06/06/17 22:49 60-57-1 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 22:49 959-98-8 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 22:49 33213-65-9 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 22:49 1031-07-8 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 22:49 72-20-8 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 22:49 7421-93-4 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 22:49 76-44-8 ND ug/L 0.075 0.050 1 06/02/17 10:09 06/06/17 22:49 1024-57-3 ND ug/L 1.0 0.15 1 06/02/17 10:09 06/06/17 22:49 72-43-5 ND ug/L 1.5 0.20 1 06/02/17 10:09 06/06/17 22:49 8001-35-2 91 % 20-130 1 06/02/17 10:09 06/06/17 22:49 877-09-8 71 % 20-130 1 06/02/17 10:09 06/06/17 22:49 2051-24-3 Analytical Method: EPA 8082 Preparation Method: EPA 3510 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1714:27 12674-11-2 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1714:27 11104-28-2 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1714:27 11141-16-5 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1714:27 53469-21-9 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1714:27 12672-29-6 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1714:27 11097-69-1 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1714:27 11096-82-5 77 % 10-132 1 06/02/17 10:09 06/03/1714:27 2051-24-3 Analytical Method: EPA 8151 Preparation Method: EPA 8151 ND ug/L 0.97 0.23 1 06/07/17 16:00 06/10/17 01:38 94-75-7 ND ug/L 0.20 0.059 1 06/07/17 16:00 06/10/17 01:38 88-85-7 ND ug/L 0.029 0.018 1 06/07/17 16:00 06/10/17 01:38 87-86-5 ND ug/L 0.20 0.043 1 06/07/17 16:00 06/10/17 01:38 93-76-5 ND ug/L 0.20 0.051 1 06/07/17 16:00 06/10/17 01:38 93-72-1 75 % 39-139 1 06/07/17 16:00 06/10/17 01:38 19719-28-9 Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 06/02/17 11:25 06/09/17 21:32 7440-36-0 ND ug/L 10.0 5.0 1 06/02/17 11:25 06/09/17 21:32 7440-38-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 53 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-17 Lab ID: 92342530003 Collected: 05/31/17 16:30 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Tin Vanadium Zinc 6020 MET ICPMS Thallium 7470 Mercury Mercury 8270 MSSV Semivolatile Organic Acenaphthene Acenaphthylene Acetophenone 2-Acetylaminofluorene 4-Aminobiphenyl Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-ChIoro-3-methyl phenol 4-Chloroaniline Chlorobenzilate bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Diallate Dibenz(a,h)anthracene Date: 06/19/2017 01:10 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010A 27.5J ug/L 100 2.5 1 06/02/17 11:25 06/09/17 21:32 7440-39-3 ND ug/L 1.0 0.50 1 06/02/17 11:25 06/09/17 21:32 7440-41-7 ND ug/L 1.0 0.50 1 06/02/17 11:25 06/09/17 21:32 7440-43-9 ND ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:32 7440-47-3 ND ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:32 7440-48-4 ND ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:32 7440-50-8 ND ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:32 7439-92-1 3.2J ug/L 50.0 2.5 1 06/02/17 11:25 06/09/17 21:32 7440-02-0 ND ug/L 10.0 5.0 1 06/02/17 11:25 06/09/17 21:32 7782-49-2 ND ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:32 7440-22-4 5.3J ug/L 100 2.5 1 06/02/17 11:25 06/09/17 21:32 7440-31-5 ND ug/L 25.0 2.5 1 06/02/17 11:25 06/09/17 21:32 7440-62-2 5.1J ug/L 10.0 5.0 1 06/02/17 11:25 06/09/17 21:32 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3010A 0.054J ug/L 5.5 0.020 1 06/06/17 02:45 06/09/17 17:16 7440-28-0 Analytical Method: EPA 7470 Preparation Method: EPA 7470 ND ug/L 0.20 0.10 1 06/05/17 20:00 06/07/17 01:48 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1716:29 83-32-9 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1716:29 208-96-8 ND ug/L 10.0 1.9 1 06/07/1717:10 06/14/1716:29 98-86-2 ND ug/L 20.0 1.6 1 06/07/1717:10 06/14/1716:29 53-96-3 ND ug/L 20.0 1.7 1 06/07/1717:10 06/14/1716:29 92-67-1 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1716:29 120-12-7 ND ug/L 10.0 2.1 1 06/07/1717:10 06/14/1716:29 56-55-3 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1716:29 50-32-8 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1716:29 205-99-2 ND ug/L 10.0 2.1 1 06/07/1717:10 06/14/1716:29 191-24-2 ND ug/L 10.0 2.0 1 06/07/1717:10 06/14/1716:29 207-08-9 ND ug/L 20.0 3.1 1 06/07/1717:10 06/14/1716:29 100-51-6 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1716:29 101-55-3 ND ug/L 10.0 2.5 1 06/07/1717:10 06/14/1716:29 85-68-7 ND ug/L 20.0 2.8 1 06/07/1717:10 06/14/1716:29 59-50-7 ND ug/L 20.0 2.8 1 06/07/1717:10 06/14/1716:29 106-47-8 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1716:29 510-15-6 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1716:29 111-91-1 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1716:29 111-44-4 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1716:29 91-58-7 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1716:29 95-57-8 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1716:29 7005-72-3 ND ug/L 10.0 2.1 1 06/07/1717:10 06/14/1716:29 218-01-9 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1716:29 2303-16-4 ND ug/L 10.0 2.0 1 06/07/1717:10 06/14/1716:29 53-70-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. L2 Page 54 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-17 Lab ID: 92342530003 Collected: 05/31/17 16:30 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Dibenzofuran ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 16:29 132-64-9 3,3'-Dichlorobenzidine ND ug/L 20.0 3.9 1 06/07/17 17:10 06/14/17 16:29 91-94-1 2,4-Dichlorophenol ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:29 120-83-2 2,6-Dichlorophenol ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:29 87-65-0 Diethylphthalate ND ug/L 6000 1.6 1 06/07/17 17:10 06/14/17 16:29 84-66-2 Dimethoate ND ug/L 20.0 1.8 1 06/07/17 17:10 06/14/17 16:29 60-51-5 P-Dimethylaminoazobenzene ND ug/L 10.0 1.0 1 06/07/17 17:10 06/14/17 16:29 60-11-7 7,12-Dimethylbenz(a)anthracene ND ug/L 10.0 2.4 1 06/07/17 17:10 06/14/17 16:29 57-97-6 3,3'-Dimethylbenzidine ND ug/L 10.0 3.9 1 06/07/17 17:10 06/14/17 16:29 119-93-7 2,4-Dimethylphenol ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:29 105-67-9 Dimethylphthalate ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 16:29 131-11-3 Di-n-butylphthalate ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 16:29 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 50.0 2.2 1 06/07/17 17:10 06/14/17 16:29 534-52-1 1,3-Dinitrobenzene ND ug/L 20.0 1.3 1 06/07/17 17:10 06/14/17 16:29 99-65-0 2,4-Dinitrophenol ND ug/L 50.0 5.1 1 06/07/17 17:10 06/14/17 16:29 51-28-5 2,4-Dinitrotoluene ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:29 121-14-2 2,6-Dinitrotoluene ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 16:29 606-20-2 Di-n-octylphthalate ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:29 117-84-0 Diphenylamine ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 16:29 122-39-4 Disulfoton ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:29 298-04-4 bis(2- Ethyl hexyl)phthalate ND ug/L 15.0 2.3 1 06/07/17 17:10 06/14/17 16:29 117-81-7 Ethyl methanesulfonate ND ug/L 20.0 1.6 1 06/07/17 17:10 06/14/17 16:29 62-50-0 Famphur ND ug/L 20.0 5.7 1 06/07/17 17:10 06/14/17 16:29 52-85-7 Fluoranthene ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 16:29 206-44-0 Fluorene ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:29 86-73-7 Hexachlorobenzene ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 16:29 118-74-1 Hexachlorocyclopentadiene ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 16:29 77-47-4 Hexachloroethane ND ug/L 10.0 1.8 1 06/07/17 17:10 06/14/17 16:29 67-72-1 Hexachloropropene ND ug/L 10.0 1.2 1 06/07/17 17:10 06/14/17 16:29 1888-71-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 16:29 193-39-5 Isodrin ND ug/L 20.0 2.5 1 06/07/17 17:10 06/14/17 16:29 465-73-6 Isophorone ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:29 78-59-1 Isosafrole ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:29 120-58-1 Kepone ND ug/L 20.0 4.5 1 06/07/17 17:10 06/14/17 16:29 143-50-0 Methapyrilene ND ug/L 100 3.0 1 06/07/17 17:10 06/14/17 16:29 91-80-5 3-Methylcholanthrene ND ug/L 10.0 2.7 1 06/07/17 17:10 06/14/17 16:29 56-49-5 Methyl methanesulfonate ND ug/L 10.0 1.1 1 06/07/17 17:10 06/14/17 16:29 66-27-3 2-Methylnaphthalene ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 16:29 91-57-6 Methyl parathion ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:29 298-00-0 2-Methylphenol(o-Cresol) ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:29 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 16:29 15831-10-4 1-Naphthalenamine ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 16:29 134-32-7 2-Naphthalenamine ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 16:29 91-59-8 1,4-Naphthoquinone ND ug/L 10.0 0.99 1 06/07/17 17:10 06/14/17 16:29 130-15-4 2-Nitroaniline ND ug/L 50.0 2.3 1 06/07/17 17:10 06/14/17 16:29 88-74-4 3-Nitroaniline ND ug/L 50.0 2.7 1 06/07/17 17:10 06/14/17 16:29 99-09-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 55 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-17 Lab ID: 92342530003 Collected: 05/31/17 16:30 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 4-Nitroaniline ND ug/L 20.0 3.4 1 06/07/17 17:10 06/14/17 16:29 100-01-6 Nitrobenzene ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:29 98-95-3 2-Nitrophenol ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:29 88-75-5 4-Nitrophenol ND ug/L 50.0 4.3 1 06/07/17 17:10 06/14/17 16:29 100-02-7 5-Nitro-o-toluidine ND ug/L 10.0 1.9 1 06/07/17 17:10 06/14/17 16:29 99-55-8 N-Nitrosodiethylamine ND ug/L 20.0 1.4 1 06/07/17 17:10 06/14/17 16:29 55-18-5 N-Nitrosodimethylamine ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:29 62-75-9 N-Nitroso-di-n-butylamine ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:29 924-16-3 N-Nitroso-di-n-propylamine ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 16:29 621-64-7 N-Nitrosodiphenylamine ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 16:29 86-30-6 N-Nitrosomethylethylamine ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 16:29 10595-95-6 N-Nitrosopiperidine ND ug/L 20.0 1.7 1 06/07/17 17:10 06/14/17 16:29 100-75-4 N-Nitrosopyrrolidine ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 16:29 930-55-2 O,O,O-Triethylphosphorothioate ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 16:29 126-68-1 2,2'-Oxybis(1-chloropropane) ND ug/L 10.0 1.8 1 06/07/17 17:10 06/14/17 16:29 108-60-1 Parathion (Ethyl parathion) ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:29 56-38-2 Pentachlorobenzene ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:29 608-93-5 Pentachloronitrobenzene ND ug/L 20.0 1.7 1 06/07/17 17:10 06/14/17 16:29 82-68-8 Pentachlorophenol ND ug/L 25.0 3.5 1 06/07/17 17:10 06/14/17 16:29 87-86-5 Phenacetin ND ug/L 20.0 1.9 1 06/07/17 17:10 06/14/17 16:29 62-44-2 Phenanthrene ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:29 85-01-8 Phenol ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 16:29 108-95-2 p-Phenylenediamine ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 16:29 106-50-3 Phorate ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 16:29 298-02-2 Pronamide ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 16:29 23950-58-5 Pyrene ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 16:29 129-00-0 Safrole ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 16:29 94-59-7 1,2,4,5-Tetrachlorobenzene ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 16:29 95-94-3 2,3,4,6-Tetrachlorophenol ND ug/L 10.0 2.9 1 06/07/17 17:10 06/14/17 16:29 58-90-2 Thionazin ND ug/L 20.0 1.7 1 06/07/17 17:10 06/14/17 16:29 297-97-2 O-Toluidine ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 16:29 95-53-4 2,4,5-Trichlorophenol ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:29 95-95-4 2,4,6-Trichlorophenol ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 16:29 88-06-2 1,3,5-Trinitrobenzene ND ug/L 10.0 1.2 1 06/07/17 17:10 06/14/17 16:29 99-35-4 Surrogates Nitrobenzene-d5 (S) 72 % 21-110 1 06/07/17 17:10 06/14/17 16:29 4165-60-0 2-Fluorobiphenyl (S) 95 % 27-110 1 06/07/17 17:10 06/14/17 16:29 321-60-8 Terphenyl-d14 (S) 86 % 31-107 1 06/07/17 17:10 06/14/17 16:29 1718-51-0 Phenol-d6 (S) 26 % 10-110 1 06/07/17 17:10 06/14/17 16:29 13127-88-3 2-Fluorophenol (S) 40 % 12-110 1 06/07/17 17:10 06/14/17 16:29 367-12-4 2,4,6-Tribromophenol (S) 92 % 27-110 1 06/07/17 17:10 06/14/17 16:29 118-79-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 16.1J ug/L 100 10.0 1 06/02/17 09:54 67-64-1 Acetonitrile ND ug/L 55.0 2.2 1 06/02/17 09:54 75-05-8 Acrolein ND ug/L 53.0 1.6 1 06/02/17 09:54 107-02-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 56 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-17 Lab ID: 92342530003 Collected: 05/31/17 16:30 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acrylonitrile ND ug/L 200 1.9 1 06/02/17 09:54 107-13-1 Allyl chloride ND ug/L 10.0 1.5 1 06/02/17 09:54 107-05-1 Benzene ND ug/L 1.0 0.25 1 06/02/17 09:54 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 06/02/17 09:54 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 06/02/17 09:54 75-27-4 Bromoform ND ug/L 3.0 0.26 1 06/02/17 09:54 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 06/02/17 09:54 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 06/02/17 09:54 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 06/02/17 09:54 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 06/02/17 09:54 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 06/02/17 09:54 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 06/02/17 09:54 75-00-3 Chloroform ND ug/L 5.0 0.14 1 06/02/17 09:54 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 06/02/17 09:54 74-87-3 Chloroprene ND ug/L 20.0 0.27 1 06/02/17 09:54 126-99-8 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 06/02/17 09:54 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 06/02/17 09:54 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 06/02/17 09:54 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 06/02/17 09:54 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 06/02/17 09:54 95-50-1 1,3-Dichlorobenzene ND ug/L 5.0 0.24 1 06/02/17 09:54 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 06/02/17 09:54 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/02/17 09:54 110-57-6 Dichlorodifluoromethane ND ug/L 5.0 0.21 1 06/02/17 09:54 75-71-8 1,1-Dichloroethane ND ug/L 5.0 0.32 1 06/02/17 09:54 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 06/02/17 09:54 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/02/17 09:54 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 06/02/17 09:54 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/02/17 09:54 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 06/02/17 09:54 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 06/02/17 09:54 142-28-9 2,2-Dichloropropane ND ug/L 15.0 0.13 1 06/02/17 09:54 594-20-7 1,1-Dichloropropene ND ug/L 5.0 0.49 1 06/02/17 09:54 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/02/17 09:54 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/02/17 09:54 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/02/17 09:54 100-41-4 Ethyl methacrylate ND ug/L 10.0 0.20 1 06/02/17 09:54 97-63-2 Hexachloro-1,3-butadiene ND ug/L 10.0 0.71 1 06/02/17 09:54 87-68-3 2-Hexanone ND ug/L 50.0 0.46 1 06/02/17 09:54 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/02/17 09:54 74-88-4 Isobutanol ND ug/L 100 35.0 1 06/02/17 09:54 78-83-1 Methacrylonitrile ND ug/L 100 0.93 1 06/02/17 09:54 126-98-7 Methylene Chloride ND ug/L 1.0 0.97 1 06/02/17 09:54 75-09-2 Methyl methacrylate ND ug/L 30.0 2.0 1 06/02/17 09:54 80-62-6 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/02/17 09:54 108-10-1 Naphthalene ND ug/L 10.0 0.24 1 06/02/17 09:54 91-20-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 57 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-17 Lab ID: 92342530003 Collected: 05/31/17 16:30 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Propionitrile ND ug/L 150 3.6 1 06/02/17 09:54 107-12-0 Styrene ND ug/L 1.0 0.26 1 06/02/17 09:54 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/02/17 09:54 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/02/17 09:54 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/02/17 09:54 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/02/17 09:54 108-88-3 1,2,4-Trichlorobenzene ND ug/L 10.0 0.35 1 06/02/17 09:54 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/02/17 09:54 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/02/17 09:54 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/02/17 09:54 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/02/17 09:54 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/02/17 09:54 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/02/17 09:54 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/02/17 09:54 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/02/17 09:54 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 113 % 70-130 1 06/02/17 09:54 460-00-4 1,2-Dichloroethane-d4 (S) 102 % 70-130 1 06/02/17 09:54 17060-07-0 Toluene-d8 (S) 112 % 70-130 1 06/02/17 09:54 2037-26-5 4500S2D Sulfide Water Analytical Method: SM 4500-S2D Sulfide ND ug/L 1000 100 1 06/06/17 23:00 18496-25-8 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E Cyanide 5.2J ug/L 10.0 4.0 1 06/07/1713:33 57-12-5 Date: 06/19/2017 01:10 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 58 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-21 Lab ID: 92342530004 Collected: 05/31/17 17:20 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 Organochlorine Pesticides Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Surrogates Decachlorobiphenyl (S) 8151 Chlorinated Herbicides 2,4-D Dinoseb Pentachlorophenol 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 6010 MET ICP Antimony Arsenic Date: 06/19/2017 01:10 PM Analytical Method: EPA 8081 Preparation Method: EPA 3510 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 23:07 309-00-2 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 23:07 319-84-6 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 23:07 319-85-7 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 23:07 319-86-8 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 23:07 58-89-9 ND ug/L 0.50 0.20 1 06/02/17 10:09 06/06/17 23:07 57-74-9 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 23:07 72-54-8 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 23:07 72-55-9 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 23:07 50-29-3 ND ug/L 0.075 0.050 1 06/02/17 10:09 06/06/17 23:07 60-57-1 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 23:07 959-98-8 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 23:07 33213-65-9 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 23:07 1031-07-8 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 23:07 72-20-8 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 23:07 7421-93-4 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 23:07 76-44-8 ND ug/L 0.075 0.050 1 06/02/17 10:09 06/06/17 23:07 1024-57-3 ND ug/L 1.0 0.15 1 06/02/17 10:09 06/06/17 23:07 72-43-5 ND ug/L 1.5 0.20 1 06/02/17 10:09 06/06/17 23:07 8001-35-2 71 % 20-130 1 06/02/17 10:09 06/06/17 23:07 877-09-8 78 % 20-130 1 06/02/17 10:09 06/06/17 23:07 2051-24-3 Analytical Method: EPA 8082 Preparation Method: EPA 3510 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1715:09 12674-11-2 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1715:09 11104-28-2 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1715:09 11141-16-5 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1715:09 53469-21-9 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1715:09 12672-29-6 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1715:09 11097-69-1 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1715:09 11096-82-5 79 % 10-132 1 06/02/17 10:09 06/03/1715:09 2051-24-3 Analytical Method: EPA 8151 Preparation Method: EPA 8151 ND ug/L 0.99 0.24 1 06/07/17 16:00 06/10/17 02:08 94-75-7 ND ug/L 0.20 0.060 1 06/07/17 16:00 06/10/17 02:08 88-85-7 ND ug/L 0.030 0.018 1 06/07/17 16:00 06/10/17 02:08 87-86-5 ND ug/L 0.20 0.044 1 06/07/17 16:00 06/10/17 02:08 93-76-5 ND ug/L 0.20 0.052 1 06/07/17 16:00 06/10/17 02:08 93-72-1 74 % 39-139 1 06/07/17 16:00 06/10/17 02:08 19719-28-9 Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 06/02/17 11:25 06/09/17 21:45 7440-36-0 ND ug/L 10.0 5.0 1 06/02/17 11:25 06/09/17 21:45 7440-38-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 59 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-21 Lab ID: 92342530004 Collected: 05/31/17 17:20 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Tin Vanadium Zinc 6020 MET ICPMS Thallium 7470 Mercury Mercury 8270 MSSV Semivolatile Organic Acenaphthene Acenaphthylene Acetophenone 2-Acetylaminofluorene 4-Aminobiphenyl Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-ChIoro-3-methyl phenol 4-Chloroaniline Chlorobenzilate bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Diallate Dibenz(a,h)anthracene Date: 06/19/2017 01:10 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010A 60.5J ug/L 100 2.5 1 06/02/17 11:25 06/09/17 21:45 7440-39-3 ND ug/L 1.0 0.50 1 06/02/17 11:25 06/09/17 21:45 7440-41-7 ND ug/L 1.0 0.50 1 06/02/17 11:25 06/09/17 21:45 7440-43-9 ND ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:45 7440-47-3 4.8J ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:45 7440-48-4 ND ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:45 7440-50-8 ND ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:45 7439-92-1 ND ug/L 50.0 2.5 1 06/02/17 11:25 06/09/17 21:45 7440-02-0 ND ug/L 10.0 5.0 1 06/02/17 11:25 06/09/17 21:45 7782-49-2 ND ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:45 7440-22-4 ND ug/L 100 2.5 1 06/02/17 11:25 06/09/17 21:45 7440-31-5 ND ug/L 25.0 2.5 1 06/02/17 11:25 06/09/17 21:45 7440-62-2 5.3J ug/L 10.0 5.0 1 06/02/17 11:25 06/09/17 21:45 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3010A ND ug/L 5.5 0.020 1 06/06/17 02:45 06/09/17 17:18 7440-28-0 Analytical Method: EPA 7470 Preparation Method: EPA 7470 ND ug/L 0.20 0.10 1 06/05/17 20:00 06/07/17 01:50 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1716:59 83-32-9 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1716:59 208-96-8 ND ug/L 10.0 1.9 1 06/07/1717:10 06/14/1716:59 98-86-2 ND ug/L 20.0 1.6 1 06/07/1717:10 06/14/1716:59 53-96-3 ND ug/L 20.0 1.7 1 06/07/1717:10 06/14/1716:59 92-67-1 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1716:59 120-12-7 ND ug/L 10.0 2.1 1 06/07/1717:10 06/14/1716:59 56-55-3 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1716:59 50-32-8 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1716:59 205-99-2 ND ug/L 10.0 2.1 1 06/07/1717:10 06/14/1716:59 191-24-2 ND ug/L 10.0 2.0 1 06/07/1717:10 06/14/1716:59 207-08-9 ND ug/L 20.0 3.1 1 06/07/1717:10 06/14/1716:59 100-51-6 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1716:59 101-55-3 ND ug/L 10.0 2.5 1 06/07/1717:10 06/14/1716:59 85-68-7 ND ug/L 20.0 2.8 1 06/07/1717:10 06/14/1716:59 59-50-7 ND ug/L 20.0 2.8 1 06/07/1717:10 06/14/1716:59 106-47-8 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1716:59 510-15-6 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1716:59 111-91-1 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1716:59 111-44-4 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1716:59 91-58-7 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1716:59 95-57-8 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1716:59 7005-72-3 ND ug/L 10.0 2.1 1 06/07/1717:10 06/14/1716:59 218-01-9 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1716:59 2303-16-4 ND ug/L 10.0 2.0 1 06/07/1717:10 06/14/1716:59 53-70-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. L2 Page 60 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-21 Lab ID: 92342530004 Collected: 05/31/17 17:20 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Dibenzofuran ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 16:59 132-64-9 3,3'-Dichlorobenzidine ND ug/L 20.0 3.9 1 06/07/17 17:10 06/14/17 16:59 91-94-1 2,4-Dichlorophenol ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:59 120-83-2 2,6-Dichlorophenol ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:59 87-65-0 Diethylphthalate ND ug/L 6000 1.6 1 06/07/17 17:10 06/14/17 16:59 84-66-2 Dimethoate ND ug/L 20.0 1.8 1 06/07/17 17:10 06/14/17 16:59 60-51-5 P-Dimethylaminoazobenzene ND ug/L 10.0 1.0 1 06/07/17 17:10 06/14/17 16:59 60-11-7 7,12-Dimethylbenz(a)anthracene ND ug/L 10.0 2.4 1 06/07/17 17:10 06/14/17 16:59 57-97-6 3,3'-Dimethylbenzidine ND ug/L 10.0 3.9 1 06/07/17 17:10 06/14/17 16:59 119-93-7 2,4-Dimethylphenol ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:59 105-67-9 Dimethylphthalate ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 16:59 131-11-3 Di-n-butylphthalate ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 16:59 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 50.0 2.2 1 06/07/17 17:10 06/14/17 16:59 534-52-1 1,3-Dinitrobenzene ND ug/L 20.0 1.3 1 06/07/17 17:10 06/14/17 16:59 99-65-0 2,4-Dinitrophenol ND ug/L 50.0 5.1 1 06/07/17 17:10 06/14/17 16:59 51-28-5 2,4-Dinitrotoluene ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:59 121-14-2 2,6-Dinitrotoluene ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 16:59 606-20-2 Di-n-octylphthalate ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:59 117-84-0 Diphenylamine ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 16:59 122-39-4 Disulfoton ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:59 298-04-4 bis(2- Ethyl hexyl)phthalate ND ug/L 15.0 2.3 1 06/07/17 17:10 06/14/17 16:59 117-81-7 Ethyl methanesulfonate ND ug/L 20.0 1.6 1 06/07/17 17:10 06/14/17 16:59 62-50-0 Famphur ND ug/L 20.0 5.7 1 06/07/17 17:10 06/14/17 16:59 52-85-7 Fluoranthene ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 16:59 206-44-0 Fluorene ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:59 86-73-7 Hexachlorobenzene ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 16:59 118-74-1 Hexachlorocyclopentadiene ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 16:59 77-47-4 Hexachloroethane ND ug/L 10.0 1.8 1 06/07/17 17:10 06/14/17 16:59 67-72-1 Hexachloropropene ND ug/L 10.0 1.2 1 06/07/17 17:10 06/14/17 16:59 1888-71-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 16:59 193-39-5 Isodrin ND ug/L 20.0 2.5 1 06/07/17 17:10 06/14/17 16:59 465-73-6 Isophorone ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:59 78-59-1 Isosafrole ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:59 120-58-1 Kepone ND ug/L 20.0 4.5 1 06/07/17 17:10 06/14/17 16:59 143-50-0 Methapyrilene ND ug/L 100 3.0 1 06/07/17 17:10 06/14/17 16:59 91-80-5 3-Methylcholanthrene ND ug/L 10.0 2.7 1 06/07/17 17:10 06/14/17 16:59 56-49-5 Methyl methanesulfonate ND ug/L 10.0 1.1 1 06/07/17 17:10 06/14/17 16:59 66-27-3 2-Methylnaphthalene ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 16:59 91-57-6 Methyl parathion ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:59 298-00-0 2-Methylphenol(o-Cresol) ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:59 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 16:59 15831-10-4 1-Naphthalenamine ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 16:59 134-32-7 2-Naphthalenamine ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 16:59 91-59-8 1,4-Naphthoquinone ND ug/L 10.0 0.99 1 06/07/17 17:10 06/14/17 16:59 130-15-4 2-Nitroaniline ND ug/L 50.0 2.3 1 06/07/17 17:10 06/14/17 16:59 88-74-4 3-Nitroaniline ND ug/L 50.0 2.7 1 06/07/17 17:10 06/14/17 16:59 99-09-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. 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AIRY (UIC) Pace Project No.: 92342478 Sample: MW-21 Lab ID: 92342530004 Collected: 05/31/17 17:20 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 4-Nitroaniline ND ug/L 20.0 3.4 1 06/07/17 17:10 06/14/17 16:59 100-01-6 Nitrobenzene ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:59 98-95-3 2-Nitrophenol ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:59 88-75-5 4-Nitrophenol ND ug/L 50.0 4.3 1 06/07/17 17:10 06/14/17 16:59 100-02-7 5-Nitro-o-toluidine ND ug/L 10.0 1.9 1 06/07/17 17:10 06/14/17 16:59 99-55-8 N-Nitrosodiethylamine ND ug/L 20.0 1.4 1 06/07/17 17:10 06/14/17 16:59 55-18-5 N-Nitrosodimethylamine ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:59 62-75-9 N-Nitroso-di-n-butylamine ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:59 924-16-3 N-Nitroso-di-n-propylamine ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 16:59 621-64-7 N-Nitrosodiphenylamine ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 16:59 86-30-6 N-Nitrosomethylethylamine ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 16:59 10595-95-6 N-Nitrosopiperidine ND ug/L 20.0 1.7 1 06/07/17 17:10 06/14/17 16:59 100-75-4 N-Nitrosopyrrolidine ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 16:59 930-55-2 O,O,O-Triethylphosphorothioate ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 16:59 126-68-1 2,2'-Oxybis(1-chloropropane) ND ug/L 10.0 1.8 1 06/07/17 17:10 06/14/17 16:59 108-60-1 Parathion (Ethyl parathion) ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:59 56-38-2 Pentachlorobenzene ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:59 608-93-5 Pentachloronitrobenzene ND ug/L 20.0 1.7 1 06/07/17 17:10 06/14/17 16:59 82-68-8 Pentachlorophenol ND ug/L 25.0 3.5 1 06/07/17 17:10 06/14/17 16:59 87-86-5 Phenacetin ND ug/L 20.0 1.9 1 06/07/17 17:10 06/14/17 16:59 62-44-2 Phenanthrene ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 16:59 85-01-8 Phenol ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 16:59 108-95-2 p-Phenylenediamine ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 16:59 106-50-3 Phorate ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 16:59 298-02-2 Pronamide ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 16:59 23950-58-5 Pyrene ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 16:59 129-00-0 Safrole ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 16:59 94-59-7 1,2,4,5-Tetrachlorobenzene ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 16:59 95-94-3 2,3,4,6-Tetrachlorophenol ND ug/L 10.0 2.9 1 06/07/17 17:10 06/14/17 16:59 58-90-2 Thionazin ND ug/L 20.0 1.7 1 06/07/17 17:10 06/14/17 16:59 297-97-2 O-Toluidine ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 16:59 95-53-4 2,4,5-Trichlorophenol ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 16:59 95-95-4 2,4,6-Trichlorophenol ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 16:59 88-06-2 1,3,5-Trinitrobenzene ND ug/L 10.0 1.2 1 06/07/17 17:10 06/14/17 16:59 99-35-4 Surrogates Nitrobenzene-d5 (S) 57 % 21-110 1 06/07/17 17:10 06/14/17 16:59 4165-60-0 2-Fluorobiphenyl (S) 70 % 27-110 1 06/07/17 17:10 06/14/17 16:59 321-60-8 Terphenyl-d14 (S) 76 % 31-107 1 06/07/17 17:10 06/14/17 16:59 1718-51-0 Phenol-d6 (S) 20 % 10-110 1 06/07/17 17:10 06/14/17 16:59 13127-88-3 2-Fluorophenol (S) 32 % 12-110 1 06/07/17 17:10 06/14/17 16:59 367-12-4 2,4,6-Tribromophenol (S) 71 % 27-110 1 06/07/17 17:10 06/14/17 16:59 118-79-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 11.0J ug/L 100 10.0 1 06/04/17 07:52 67-64-1 Acetonitrile ND ug/L 55.0 2.2 1 06/04/17 07:52 75-05-8 Acrolein ND ug/L 53.0 1.6 1 06/04/17 07:52 107-02-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 62 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-21 Lab ID: 92342530004 Collected: 05/31/17 17:20 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Acrylonitrile Allyl chloride Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane Chloroprene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene 2-Hexanone lodomethane Isobutanol Methacrylonitrile Methylene Chloride Methyl methacrylate 4-Methyl-2-pentanone (MIBK) Naphthalene Date: 06/19/2017 01:10 PM Analytical Method: EPA 8260 ND ug/L 200 1.9 1 06/04/17 07:52 107-13-1 ND ug/L 10.0 1.5 1 06/04/17 07:52 107-05-1 ND ug/L 1.0 0.25 1 06/04/17 07:52 71-43-2 ND ug/L 3.0 0.17 1 06/04/17 07:52 74-97-5 ND ug/L 1.0 0.18 1 06/04/17 07:52 75-27-4 ND ug/L 3.0 0.26 1 06/04/17 07:52 75-25-2 ND ug/L 10.0 0.29 1 06/04/17 07:52 74-83-9 ND ug/L 100 0.96 1 06/04/17 07:52 78-93-3 ND ug/L 100 1.2 1 06/04/17 07:52 75-15-0 ND ug/L 1.0 0.25 1 06/04/17 07:52 56-23-5 0.25J ug/L 3.0 0.23 1 06/04/17 07:52 108-90-7 ND ug/L 10.0 0.54 1 06/04/17 07:52 75-00-3 ND ug/L 5.0 0.14 1 06/04/17 07:52 67-66-3 ND ug/L 1.0 0.11 1 06/04/17 07:52 74-87-3 ND ug/L 20.0 0.27 1 06/04/17 07:52 126-99-8 ND ug/L 13.0 2.0 1 06/04/17 07:52 96-12-8 ND ug/L 3.0 0.21 1 06/04/17 07:52 124-48-1 ND ug/L 1.0 0.27 1 06/04/17 07:52 106-93-4 ND ug/L 10.0 0.21 1 06/04/17 07:52 74-95-3 ND ug/L 5.0 0.30 1 06/04/17 07:52 95-50-1 ND ug/L 5.0 0.24 1 06/04/17 07:52 541-73-1 ND ug/L 1.0 0.33 1 06/04/17 07:52 106-46-7 ND ug/L 100 1.0 1 06/04/17 07:52 110-57-6 ND ug/L 5.0 0.21 1 06/04/17 07:52 75-71-8 4.1J ug/L 5.0 0.32 1 06/04/17 07:52 75-34-3 0.49J ug/L 1.0 0.24 1 06/04/17 07:52 107-06-2 ND ug/L 5.0 0.56 1 06/04/17 07:52 75-35-4 18.6 ug/L 5.0 0.19 1 06/04/17 07:52 156-59-2 ND ug/L 5.0 0.49 1 06/04/17 07:52 156-60-5 ND ug/L 1.0 0.27 1 06/04/17 07:52 78-87-5 ND ug/L 1.0 0.28 1 06/04/17 07:52 142-28-9 ND ug/L 15.0 0.13 1 06/04/17 07:52 594-20-7 ND ug/L 5.0 0.49 1 06/04/17 07:52 563-58-6 ND ug/L 1.0 0.13 1 06/04/17 07:52 10061-01-5 ND ug/L 1.0 0.26 1 06/04/17 07:52 10061-02-6 ND ug/L 1.0 0.30 1 06/04/17 07:52 100-41-4 ND ug/L 10.0 0.20 1 06/04/17 07:52 97-63-2 ND ug/L 10.0 0.71 1 06/04/17 07:52 87-68-3 ND ug/L 50.0 0.46 1 06/04/17 07:52 591-78-6 ND ug/L 10.0 0.32 1 06/04/17 07:52 74-88-4 ND ug/L 100 35.0 1 06/04/17 07:52 78-83-1 ND ug/L 100 0.93 1 06/04/17 07:52 126-98-7 ND ug/L 1.0 0.97 1 06/04/17 07:52 75-09-2 ND ug/L 30.0 2.0 1 06/04/17 07:52 80-62-6 ND ug/L 100 0.33 1 06/04/17 07:52 108-10-1 ND ug/L 10.0 0.24 1 06/04/17 07:52 91-20-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. L1 Page 63 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-21 Lab ID: 92342530004 Collected: 05/31/17 17:20 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Propionitrile ND ug/L 150 3.6 1 06/04/17 07:52 107-12-0 Styrene ND ug/L 1.0 0.26 1 06/04/17 07:52 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/17 07:52 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/17 07:52 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/17 07:52 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/17 07:52 108-88-3 1,2,4-Trichlorobenzene ND ug/L 10.0 0.35 1 06/04/17 07:52 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/17 07:52 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/17 07:52 79-00-5 Trichloroethene 0.70J ug/L 1.0 0.47 1 06/04/17 07:52 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/17 07:52 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/17 07:52 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/17 07:52 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/17 07:52 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/17 07:52 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 105 % 70-130 1 06/04/17 07:52 460-00-4 1,2-Dichloroethane-d4 (S) 90 % 70-130 1 06/04/17 07:52 17060-07-0 Toluene-d8 (S) 109 % 70-130 1 06/04/17 07:52 2037-26-5 4500S2D Sulfide Water Analytical Method: SM 4500-S2D Sulfide ND ug/L 1000 100 1 06/06/17 23:00 18496-25-8 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E Cyanide ND ug/L 10.0 4.0 1 06/07/1713:34 57-12-5 Date: 06/19/2017 01:10 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 64 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-22 Lab ID: 92342530005 Collected: 05/31/17 16:10 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 Organochlorine Pesticides Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Surrogates Decachlorobiphenyl (S) 8151 Chlorinated Herbicides 2,4-D Dinoseb Pentachlorophenol 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 6010 MET ICP Antimony Arsenic Date: 06/19/2017 01:10 PM Analytical Method: EPA 8081 Preparation Method: EPA 3510 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 23:25 309-00-2 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 23:25 319-84-6 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 23:25 319-85-7 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 23:25 319-86-8 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 23:25 58-89-9 ND ug/L 0.50 0.20 1 06/02/17 10:09 06/06/17 23:25 57-74-9 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 23:25 72-54-8 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 23:25 72-55-9 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 23:25 50-29-3 ND ug/L 0.075 0.050 1 06/02/17 10:09 06/06/17 23:25 60-57-1 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 23:25 959-98-8 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 23:25 33213-65-9 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 23:25 1031-07-8 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 23:25 72-20-8 ND ug/L 0.10 0.050 1 06/02/17 10:09 06/06/17 23:25 7421-93-4 ND ug/L 0.050 0.050 1 06/02/17 10:09 06/06/17 23:25 76-44-8 ND ug/L 0.075 0.050 1 06/02/17 10:09 06/06/17 23:25 1024-57-3 ND ug/L 1.0 0.15 1 06/02/17 10:09 06/06/17 23:25 72-43-5 ND ug/L 1.5 0.20 1 06/02/17 10:09 06/06/17 23:25 8001-35-2 72 % 20-130 1 06/02/17 10:09 06/06/17 23:25 877-09-8 62 % 20-130 1 06/02/17 10:09 06/06/17 23:25 2051-24-3 Analytical Method: EPA 8082 Preparation Method: EPA 3510 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1715:30 12674-11-2 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1715:30 11104-28-2 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1715:30 11141-16-5 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1715:30 53469-21-9 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1715:30 12672-29-6 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1715:30 11097-69-1 ND ug/L 0.50 0.50 1 06/02/17 10:09 06/03/1715:30 11096-82-5 65 % 10-132 1 06/02/17 10:09 06/03/1715:30 2051-24-3 Analytical Method: EPA 8151 Preparation Method: EPA 8151 ND ug/L 0.98 0.23 1 06/07/17 16:00 06/10/17 03:08 94-75-7 ND ug/L 0.20 0.060 1 06/07/17 16:00 06/10/17 03:08 88-85-7 ND ug/L 0.030 0.018 1 06/07/17 16:00 06/10/17 03:08 87-86-5 ND ug/L 0.20 0.044 1 06/07/17 16:00 06/10/17 03:08 93-76-5 ND ug/L 0.20 0.051 1 06/07/17 16:00 06/10/17 03:08 93-72-1 64 % 39-139 1 06/07/17 16:00 06/10/17 03:08 19719-28-9 Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 06/02/17 11:25 06/09/17 21:48 7440-36-0 ND ug/L 10.0 5.0 1 06/02/17 11:25 06/09/17 21:48 7440-38-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 65 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-22 Lab ID: 92342530005 Collected: 05/31/17 16:10 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Tin Vanadium Zinc 6020 MET ICPMS Thallium 7470 Mercury Mercury 8270 MSSV Semivolatile Organic Acenaphthene Acenaphthylene Acetophenone 2-Acetylaminofluorene 4-Aminobiphenyl Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzyl alcohol 4-Bromophenylphenyl ether Butylbenzylphthalate 4-ChIoro-3-methyl phenol 4-Chloroaniline Chlorobenzilate bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Diallate Dibenz(a,h)anthracene Date: 06/19/2017 01:10 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010A 56.9J ug/L 100 2.5 1 06/02/17 11:25 06/09/17 21:48 7440-39-3 ND ug/L 1.0 0.50 1 06/02/17 11:25 06/09/17 21:48 7440-41-7 0.63J ug/L 1.0 0.50 1 06/02/17 11:25 06/09/17 21:48 7440-43-9 ND ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:48 7440-47-3 ND ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:48 7440-48-4 ND ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:48 7440-50-8 ND ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:48 7439-92-1 2.6J ug/L 50.0 2.5 1 06/02/17 11:25 06/09/17 21:48 7440-02-0 ND ug/L 10.0 5.0 1 06/02/17 11:25 06/09/17 21:48 7782-49-2 ND ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:48 7440-22-4 ND ug/L 100 2.5 1 06/02/17 11:25 06/09/17 21:48 7440-31-5 ND ug/L 25.0 2.5 1 06/02/17 11:25 06/09/17 21:48 7440-62-2 6.3J ug/L 10.0 5.0 1 06/02/17 11:25 06/09/17 21:48 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3010A 0.11J ug/L 5.5 0.020 1 06/06/17 02:45 06/09/17 17:20 7440-28-0 Analytical Method: EPA 7470 Preparation Method: EPA 7470 ND ug/L 0.20 0.10 1 06/05/17 20:00 06/07/17 01:53 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1717:57 83-32-9 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1717:57 208-96-8 ND ug/L 10.0 1.9 1 06/07/1717:10 06/14/1717:57 98-86-2 ND ug/L 20.0 1.6 1 06/07/1717:10 06/14/1717:57 53-96-3 ND ug/L 20.0 1.7 1 06/07/1717:10 06/14/1717:57 92-67-1 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1717:57 120-12-7 ND ug/L 10.0 2.1 1 06/07/1717:10 06/14/1717:57 56-55-3 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1717:57 50-32-8 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1717:57 205-99-2 ND ug/L 10.0 2.1 1 06/07/1717:10 06/14/1717:57 191-24-2 ND ug/L 10.0 2.0 1 06/07/1717:10 06/14/1717:57 207-08-9 ND ug/L 20.0 3.1 1 06/07/1717:10 06/14/1717:57 100-51-6 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1717:57 101-55-3 ND ug/L 10.0 2.5 1 06/07/1717:10 06/14/1717:57 85-68-7 ND ug/L 20.0 2.8 1 06/07/1717:10 06/14/1717:57 59-50-7 ND ug/L 20.0 2.8 1 06/07/1717:10 06/14/1717:57 106-47-8 ND ug/L 10.0 2.2 1 06/07/1717:10 06/14/1717:57 510-15-6 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1717:57 111-91-1 ND ug/L 10.0 1.7 1 06/07/1717:10 06/14/1717:57 111-44-4 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1717:57 91-58-7 ND ug/L 10.0 1.5 1 06/07/1717:10 06/14/1717:57 95-57-8 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1717:57 7005-72-3 ND ug/L 10.0 2.1 1 06/07/1717:10 06/14/1717:57 218-01-9 ND ug/L 10.0 1.6 1 06/07/1717:10 06/14/1717:57 2303-16-4 ND ug/L 10.0 2.0 1 06/07/1717:10 06/14/1717:57 53-70-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. L2 Page 66 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-22 Lab ID: 92342530005 Collected: 05/31/17 16:10 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Dibenzofuran ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 17:57 132-64-9 3,3'-Dichlorobenzidine ND ug/L 20.0 3.9 1 06/07/17 17:10 06/14/17 17:57 91-94-1 2,4-Dichlorophenol ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 17:57 120-83-2 2,6-Dichlorophenol ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 17:57 87-65-0 Diethylphthalate ND ug/L 6000 1.6 1 06/07/17 17:10 06/14/17 17:57 84-66-2 Dimethoate ND ug/L 20.0 1.8 1 06/07/17 17:10 06/14/17 17:57 60-51-5 P-Dimethylaminoazobenzene ND ug/L 10.0 1.0 1 06/07/17 17:10 06/14/17 17:57 60-11-7 7,12-Dimethylbenz(a)anthracene ND ug/L 10.0 2.4 1 06/07/17 17:10 06/14/17 17:57 57-97-6 3,3'-Dimethylbenzidine ND ug/L 10.0 3.9 1 06/07/17 17:10 06/14/17 17:57 119-93-7 2,4-Dimethylphenol ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 17:57 105-67-9 Dimethylphthalate ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 17:57 131-11-3 Di-n-butylphthalate ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 17:57 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 50.0 2.2 1 06/07/17 17:10 06/14/17 17:57 534-52-1 1,3-Dinitrobenzene ND ug/L 20.0 1.3 1 06/07/17 17:10 06/14/17 17:57 99-65-0 2,4-Dinitrophenol ND ug/L 50.0 5.1 1 06/07/17 17:10 06/14/17 17:57 51-28-5 2,4-Dinitrotoluene ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 17:57 121-14-2 2,6-Dinitrotoluene ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 17:57 606-20-2 Di-n-octylphthalate ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 17:57 117-84-0 Diphenylamine ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 17:57 122-39-4 Disulfoton ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 17:57 298-04-4 bis(2- Ethyl hexyl)phthalate ND ug/L 15.0 2.3 1 06/07/17 17:10 06/14/17 17:57 117-81-7 Ethyl methanesulfonate ND ug/L 20.0 1.6 1 06/07/17 17:10 06/14/17 17:57 62-50-0 Famphur ND ug/L 20.0 5.7 1 06/07/17 17:10 06/14/17 17:57 52-85-7 Fluoranthene ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 17:57 206-44-0 Fluorene ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 17:57 86-73-7 Hexachlorobenzene ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 17:57 118-74-1 Hexachlorocyclopentadiene ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 17:57 77-47-4 Hexachloroethane ND ug/L 10.0 1.8 1 06/07/17 17:10 06/14/17 17:57 67-72-1 Hexachloropropene ND ug/L 10.0 1.2 1 06/07/17 17:10 06/14/17 17:57 1888-71-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 17:57 193-39-5 Isodrin ND ug/L 20.0 2.5 1 06/07/17 17:10 06/14/17 17:57 465-73-6 Isophorone ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 17:57 78-59-1 Isosafrole ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 17:57 120-58-1 Kepone ND ug/L 20.0 4.5 1 06/07/17 17:10 06/14/17 17:57 143-50-0 Methapyrilene ND ug/L 100 3.0 1 06/07/17 17:10 06/14/17 17:57 91-80-5 3-Methylcholanthrene ND ug/L 10.0 2.7 1 06/07/17 17:10 06/14/17 17:57 56-49-5 Methyl methanesulfonate ND ug/L 10.0 1.1 1 06/07/17 17:10 06/14/17 17:57 66-27-3 2-Methylnaphthalene ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 17:57 91-57-6 Methyl parathion ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 17:57 298-00-0 2-Methylphenol(o-Cresol) ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 17:57 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 17:57 15831-10-4 1-Naphthalenamine ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 17:57 134-32-7 2-Naphthalenamine ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 17:57 91-59-8 1,4-Naphthoquinone ND ug/L 10.0 0.99 1 06/07/17 17:10 06/14/17 17:57 130-15-4 2-Nitroaniline ND ug/L 50.0 2.3 1 06/07/17 17:10 06/14/17 17:57 88-74-4 3-Nitroaniline ND ug/L 50.0 2.7 1 06/07/17 17:10 06/14/17 17:57 99-09-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 67 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-22 Lab ID: 92342530005 Collected: 05/31/17 16:10 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 4-Nitroaniline ND ug/L 20.0 3.4 1 06/07/17 17:10 06/14/17 17:57 100-01-6 Nitrobenzene ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 17:57 98-95-3 2-Nitrophenol ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 17:57 88-75-5 4-Nitrophenol ND ug/L 50.0 4.3 1 06/07/17 17:10 06/14/17 17:57 100-02-7 5-Nitro-o-toluidine ND ug/L 10.0 1.9 1 06/07/17 17:10 06/14/17 17:57 99-55-8 N-Nitrosodiethylamine ND ug/L 20.0 1.4 1 06/07/17 17:10 06/14/17 17:57 55-18-5 N-Nitrosodimethylamine ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 17:57 62-75-9 N-Nitroso-di-n-butylamine ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 17:57 924-16-3 N-Nitroso-di-n-propylamine ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 17:57 621-64-7 N-Nitrosodiphenylamine ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 17:57 86-30-6 N-Nitrosomethylethylamine ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 17:57 10595-95-6 N-Nitrosopiperidine ND ug/L 20.0 1.7 1 06/07/17 17:10 06/14/17 17:57 100-75-4 N-Nitrosopyrrolidine ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 17:57 930-55-2 O,O,O-Triethylphosphorothioate ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 17:57 126-68-1 2,2'-Oxybis(1-chloropropane) ND ug/L 10.0 1.8 1 06/07/17 17:10 06/14/17 17:57 108-60-1 Parathion (Ethyl parathion) ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 17:57 56-38-2 Pentachlorobenzene ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 17:57 608-93-5 Pentachloronitrobenzene ND ug/L 20.0 1.7 1 06/07/17 17:10 06/14/17 17:57 82-68-8 Pentachlorophenol ND ug/L 25.0 3.5 1 06/07/17 17:10 06/14/17 17:57 87-86-5 Phenacetin ND ug/L 20.0 1.9 1 06/07/17 17:10 06/14/17 17:57 62-44-2 Phenanthrene ND ug/L 10.0 1.6 1 06/07/17 17:10 06/14/17 17:57 85-01-8 Phenol ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 17:57 108-95-2 p-Phenylenediamine ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 17:57 106-50-3 Phorate ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 17:57 298-02-2 Pronamide ND ug/L 10.0 2.0 1 06/07/17 17:10 06/14/17 17:57 23950-58-5 Pyrene ND ug/L 10.0 2.2 1 06/07/17 17:10 06/14/17 17:57 129-00-0 Safrole ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 17:57 94-59-7 1,2,4,5-Tetrachlorobenzene ND ug/L 10.0 1.3 1 06/07/17 17:10 06/14/17 17:57 95-94-3 2,3,4,6-Tetrachlorophenol ND ug/L 10.0 2.9 1 06/07/17 17:10 06/14/17 17:57 58-90-2 Thionazin ND ug/L 20.0 1.7 1 06/07/17 17:10 06/14/17 17:57 297-97-2 O-Toluidine ND ug/L 10.0 1.7 1 06/07/17 17:10 06/14/17 17:57 95-53-4 2,4,5-Trichlorophenol ND ug/L 10.0 1.5 1 06/07/17 17:10 06/14/17 17:57 95-95-4 2,4,6-Trichlorophenol ND ug/L 10.0 1.4 1 06/07/17 17:10 06/14/17 17:57 88-06-2 1,3,5-Trinitrobenzene ND ug/L 10.0 1.2 1 06/07/17 17:10 06/14/17 17:57 99-35-4 Surrogates Nitrobenzene-d5 (S) 74 % 21-110 1 06/07/17 17:10 06/14/17 17:57 4165-60-0 2-Fluorobiphenyl (S) 89 % 27-110 1 06/07/17 17:10 06/14/17 17:57 321-60-8 Terphenyl-d14 (S) 89 % 31-107 1 06/07/17 17:10 06/14/17 17:57 1718-51-0 Phenol-d6 (S) 24 % 10-110 1 06/07/17 17:10 06/14/17 17:57 13127-88-3 2-Fluorophenol (S) 37 % 12-110 1 06/07/17 17:10 06/14/17 17:57 367-12-4 2,4,6-Tribromophenol (S) 86 % 27-110 1 06/07/17 17:10 06/14/17 17:57 118-79-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 15.2J ug/L 100 10.0 1 06/02/1710:29 67-64-1 Acetonitrile ND ug/L 55.0 2.2 1 06/02/1710:29 75-05-8 Acrolein ND ug/L 53.0 1.6 1 06/02/1710:29 107-02-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 68 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-22 Lab ID: 92342530005 Collected: 05/31/17 16:10 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acrylonitrile ND ug/L 200 1.9 1 06/02/17 10:29 107-13-1 Allyl chloride ND ug/L 10.0 1.5 1 06/02/17 10:29 107-05-1 Benzene ND ug/L 1.0 0.25 1 06/02/17 10:29 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 06/02/17 10:29 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 06/02/17 10:29 75-27-4 Bromoform ND ug/L 3.0 0.26 1 06/02/17 10:29 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 06/02/17 10:29 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 06/02/17 10:29 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 06/02/17 10:29 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 06/02/17 10:29 56-23-5 Chlorobenzene 0.42J ug/L 3.0 0.23 1 06/02/17 10:29 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 06/02/17 10:29 75-00-3 Chloroform ND ug/L 5.0 0.14 1 06/02/17 10:29 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 06/02/17 10:29 74-87-3 Chloroprene ND ug/L 20.0 0.27 1 06/02/17 10:29 126-99-8 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 06/02/17 10:29 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 06/02/17 10:29 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 06/02/17 10:29 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 06/02/17 10:29 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 06/02/17 10:29 95-50-1 1,3-Dichlorobenzene ND ug/L 5.0 0.24 1 06/02/17 10:29 541-73-1 1,4-Dichlorobenzene 1.1 ug/L 1.0 0.33 1 06/02/17 10:29 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/02/17 10:29 110-57-6 Dichlorodifluoromethane ND ug/L 5.0 0.21 1 06/02/17 10:29 75-71-8 1,1-Dichloroethane 0.63J ug/L 5.0 0.32 1 06/02/17 10:29 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 06/02/17 10:29 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/02/17 10:29 75-35-4 cis-1,2-Dichloroethene 0.94J ug/L 5.0 0.19 1 06/02/17 10:29 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/02/17 10:29 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 06/02/17 10:29 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 06/02/17 10:29 142-28-9 2,2-Dichloropropane ND ug/L 15.0 0.13 1 06/02/17 10:29 594-20-7 1,1-Dichloropropene ND ug/L 5.0 0.49 1 06/02/17 10:29 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/02/17 10:29 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/02/17 10:29 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/02/17 10:29 100-41-4 Ethyl methacrylate ND ug/L 10.0 0.20 1 06/02/17 10:29 97-63-2 Hexachloro-1,3-butadiene ND ug/L 10.0 0.71 1 06/02/17 10:29 87-68-3 2-Hexanone ND ug/L 50.0 0.46 1 06/02/17 10:29 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/02/17 10:29 74-88-4 Isobutanol ND ug/L 100 35.0 1 06/02/17 10:29 78-83-1 Methacrylonitrile ND ug/L 100 0.93 1 06/02/17 10:29 126-98-7 Methylene Chloride ND ug/L 1.0 0.97 1 06/02/17 10:29 75-09-2 Methyl methacrylate ND ug/L 30.0 2.0 1 06/02/17 10:29 80-62-6 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/02/17 10:29 108-10-1 Naphthalene ND ug/L 10.0 0.24 1 06/02/17 10:29 91-20-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 69 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Sample: MW-22 Lab ID: 92342530005 Collected: 05/31/17 16:10 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Propionitrile ND ug/L 150 3.6 1 06/02/17 10:29 107-12-0 Styrene ND ug/L 1.0 0.26 1 06/02/17 10:29 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/02/17 10:29 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/02/17 10:29 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/02/17 10:29 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/02/17 10:29 108-88-3 1,2,4-Trichlorobenzene ND ug/L 10.0 0.35 1 06/02/17 10:29 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/02/17 10:29 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/02/17 10:29 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/02/17 10:29 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/02/17 10:29 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/02/17 10:29 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/02/17 10:29 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/02/17 10:29 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/02/17 10:29 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 126 % 70-130 1 06/02/17 10:29 460-00-4 1,2-Dichloroethane-d4 (S) 101 % 70-130 1 06/02/17 10:29 17060-07-0 Toluene-d8 (S) 99 % 70-130 1 06/02/17 10:29 2037-26-5 4500S2D Sulfide Water Analytical Method: SM 4500-S2D Sulfide ND ug/L 1000 100 1 06/06/17 23:00 18496-25-8 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E Cyanide 4.7J ug/L 10.0 4.0 1 06/07/1713:35 57-12-5 Date: 06/19/2017 01:10 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 70 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 QC Batch: 363333 Analysis Method: EPA 7470 QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury Associated Lab Samples: 92342478003 METHOD BLANK: 2014275 Matrix: Water Associated Lab Samples: 92342478003 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Mercury ug/L ND 0.20 0.10 06/07/17 02:15 LABORATORY CONTROL SAMPLE: 2014276 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.3 93 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2014277 2014278 MS MSD 92342769001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Mercury ug/L ND 125 125 ND ND 0 0 75-125 25 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 71 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 QC Batch: 363457 Analysis Method: EPA 7470 QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury Associated Lab Samples: 92342530001, 92342530002, 92342530003, 92342530004, 92342530005 METHOD BLANK: 2015058 Matrix: Water Associated Lab Samples: 92342530001, 92342530002, 92342530003, 92342530004, 92342530005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Mercury ug/L ND 0.20 0.10 06/07/17 00:47 LABORATORY CONTROL SAMPLE: 2015059 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.4 96 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2015060 2015061 MS MSD 92342619002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Mercury ug/L ND 2.5 2.5 2.5 2.5 100 101 75-125 1 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 72 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 QC Batch: 363459 Analysis Method: EPA 7470 QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury Associated Lab Samples: 92342478004, 92342478005 METHOD BLANK: 2015066 Matrix: Water Associated Lab Samples: 92342478004, 92342478005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Mercury ug/L ND 0.20 0.10 06/06/17 09:31 LABORATORY CONTROL SAMPLE: 2015067 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.4 95 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2015068 2015069 MS MSD 92342658001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Mercury ug/L ND 2.5 2.5 2.4 1.6 93 62 75-125 40 25 M1,R1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 73 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 QC Batch: 363009 Analysis Method: EPA 6010 QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92342478001, 92342478002 METHOD BLANK: 2012414 Associated Lab Samples: 92342478001, 92342478002 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Antimony ug/L ND 5.0 3.9 06/09/1717:07 Arsenic ug/L ND 10.0 5.0 06/09/1717:07 Barium ug/L ND 5.0 2.5 06/09/1717:07 Beryllium ug/L ND 1.0 0.50 06/09/1717:07 Cadmium ug/L ND 1.0 0.50 06/09/1717:07 Chromium ug/L ND 5.0 2.5 06/09/1717:07 Cobalt ug/L ND 5.0 2.5 06/09/1717:07 Copper ug/L ND 5.0 2.5 06/09/1717:07 Lead ug/L ND 5.0 2.5 06/09/1717:07 Nickel ug/L ND 5.0 2.5 06/09/1717:07 Selenium ug/L ND 10.0 5.0 06/09/1717:07 Silver ug/L ND 5.0 2.5 06/09/1717:07 Vanadium ug/L ND 5.0 2.5 06/09/1717:07 Zinc ug/L ND 10.0 5.0 06/09/1717:07 LABORATORY CONTROL SAMPLE: Parameter 2012415 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 500 512 102 80-120 Arsenic ug/L 500 488 98 80-120 Barium ug/L 500 518 104 80-120 Beryllium ug/L 500 518 104 80-120 Cadmium ug/L 500 504 101 80-120 Chromium ug/L 500 513 103 80-120 Cobalt ug/L 500 520 104 80-120 Copper ug/L 500 532 106 80-120 Lead ug/L 500 504 101 80-120 Nickel ug/L 500 507 101 80-120 Selenium ug/L 500 490 98 80-120 Silver ug/L 250 254 102 80-120 Vanadium ug/L 500 511 102 80-120 Zinc ug/L 500 512 102 80-120 Qualifiers Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2012416 2012417 MS MSD 92342475013 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 490 502 98 100 75-125 2 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 74 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: SURRY CLOSED -MT. 92342478 AIRY (UIC) MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2012416 2012417 MS MSD 92342475013 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Arsenic ug/L ND 500 500 477 494 95 99 75-125 4 20 Barium ug/L 30.9 500 500 539 552 102 104 75-125 2 20 Beryllium ug/L 0.60J 500 500 510 524 102 105 75-125 3 20 Cadmium ug/L ND 500 500 493 505 99 101 75-125 3 20 Chromium ug/L 6.2 500 500 511 525 101 104 75-125 3 20 Cobalt ug/L ND 500 500 499 515 99 103 75-125 3 20 Copper ug/L 7.1 500 500 524 538 103 106 75-125 3 20 Lead ug/L 2.7J 500 500 486 498 97 99 75-125 2 20 Nickel ug/L 4.2J 500 500 492 507 98 101 75-125 3 20 Selenium ug/L ND 500 500 496 508 98 101 75-125 2 20 Silver ug/L ND 250 250 251 256 100 102 75-125 2 20 Vanadium ug/L 19.2 500 500 518 534 100 103 75-125 3 20 Zinc ug/L 9.5J 500 500 512 528 100 104 75-125 3 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 75 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 QC Batch: 363010 Analysis Method: EPA 6010 QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92342478003 METHOD BLANK: 2012421 Associated Lab Samples: 92342478003 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Qualifiers Antimony ug/L ND 5.0 3.9 06/09/1714:55 Arsenic ug/L ND 10.0 5.0 06/09/1714:55 Barium ug/L ND 5.0 2.5 06/11/17 04:04 Beryllium ug/L ND 1.0 0.50 06/11/17 04:04 Cadmium ug/L ND 1.0 0.50 06/09/1714:55 Chromium ug/L ND 5.0 2.5 06/09/1714:55 Cobalt ug/L ND 5.0 2.5 06/09/1714:55 Copper ug/L ND 5.0 2.5 06/11/17 04:04 Lead ug/L ND 5.0 2.5 06/09/1714:55 Nickel ug/L ND 5.0 2.5 06/09/1714:55 Selenium ug/L ND 10.0 5.0 06/09/1714:55 Silver ug/L ND 5.0 2.5 06/11/17 04:04 Tin ug/L ND 5.0 2.5 06/09/1714:55 Vanadium ug/L ND 5.0 2.5 06/09/1714:55 Zinc ug/L ND 10.0 5.0 06/09/1714:55 LABORATORY CONTROL SAMPLE: 2012422 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Antimony ug/L 500 506 101 80-120 Arsenic ug/L 500 486 97 80-120 Barium ug/L 500 507 101 80-120 Beryllium ug/L 500 475 95 80-120 Cadmium ug/L 500 500 100 80-120 Chromium ug/L 500 500 100 80-120 Cobalt ug/L 500 503 101 80-120 Copper ug/L 500 500 100 80-120 Lead ug/L 500 494 99 80-120 Nickel ug/L 500 491 98 80-120 Selenium ug/L 500 507 101 80-120 Silver ug/L 250 248 99 80-120 Tin ug/L 500 505 101 80-120 Vanadium ug/L 500 495 99 80-120 Zinc ug/L 500 503 101 80-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 76 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: SURRY CLOSED -MT. 92342478 AIRY (UIC) MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2012423 2012424 MS MSD 92342479004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 492 487 98 97 75-125 1 20 Arsenic ug/L ND 500 500 481 475 96 94 75-125 1 20 Barium ug/L 69.9J 500 500 572 555 100 97 75-125 3 20 Beryllium ug/L ND 500 500 469 498 94 99 75-125 6 20 Cadmium ug/L 4.6 500 500 498 488 99 97 75-125 2 20 Chromium ug/L 3.1J 500 500 498 488 99 97 75-125 2 20 Cobalt ug/L ND 500 500 497 488 99 97 75-125 2 20 Copper ug/L ND 500 500 496 504 99 100 75-125 2 20 Lead ug/L ND 500 500 485 476 96 95 75-125 2 20 Nickel ug/L 2.5J 500 500 488 476 97 95 75-125 2 20 Selenium ug/L ND 500 500 501 491 100 98 75-125 2 20 Silver ug/L ND 250 250 243 248 97 99 75-125 2 20 Tin ug/L ND 500 500 499 490 100 98 75-125 2 20 Vanadium ug/L 5.3J 500 500 495 488 98 97 75-125 1 20 Zinc ug/L 13.0 500 500 507 499 99 97 75-125 1 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 77 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 QC Batch: 363146 Analysis Method: EPA 6010 QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92342530001, 92342530002, 92342530003, 92342530004, 92342530005 METHOD BLANK: 2013277 Matrix: Water Associated Lab Samples: 92342530001, 92342530002, 92342530003, 92342530004, 92342530005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Antimony ug/L ND 5.0 3.9 06/09/17 20:33 Arsenic ug/L ND 10.0 5.0 06/09/17 20:33 Barium ug/L ND 5.0 2.5 06/09/17 20:33 Beryllium ug/L ND 1.0 0.50 06/09/17 20:33 Cadmium ug/L ND 1.0 0.50 06/09/17 20:33 Chromium ug/L ND 5.0 2.5 06/10/1716:23 Cobalt ug/L ND 5.0 2.5 06/09/17 20:33 Copper ug/L ND 5.0 2.5 06/09/17 20:33 Lead ug/L ND 5.0 2.5 06/09/17 20:33 Nickel ug/L ND 5.0 2.5 06/10/1716:23 Selenium ug/L ND 10.0 5.0 06/09/17 20:33 Silver ug/L ND 5.0 2.5 06/09/17 20:33 Tin ug/L ND 5.0 2.5 06/09/17 20:33 Vanadium ug/L ND 5.0 2.5 06/09/17 20:33 Zinc ug/L ND 10.0 5.0 06/09/17 20:33 LABORATORY CONTROL SAMPLE: 2013278 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Antimony ug/L 500 493 99 80-120 Arsenic ug/L 500 474 95 80-120 Barium ug/L 500 497 99 80-120 Beryllium ug/L 500 497 99 80-120 Cadmium ug/L 500 496 99 80-120 Chromium ug/L 500 494 99 80-120 Cobalt ug/L 500 494 99 80-120 Copper ug/L 500 496 99 80-120 Lead ug/L 500 489 98 80-120 Nickel ug/L 500 485 97 80-120 Selenium ug/L 500 495 99 80-120 Silver ug/L 250 247 99 80-120 Tin ug/L 500 492 98 80-120 Vanadium ug/L 500 484 97 80-120 Zinc ug/L 500 496 99 80-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 78 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: SURRY CLOSED -MT. 92342478 AIRY (UIC) MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2013279 2013280 MS MSD 92342472012 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 491 503 98 101 75-125 2 20 Arsenic ug/L ND 500 500 472 483 94 97 75-125 2 20 Barium ug/L 0.091 500 500 582 602 98 102 75-125 3 20 mg/L Beryllium ug/L ND 500 500 494 510 99 102 75-125 3 20 Cadmium ug/L ND 500 500 495 506 99 101 75-125 2 20 Chromium ug/L ND 500 500 493 508 99 102 75-125 3 20 Cobalt ug/L ND 500 500 492 503 98 101 75-125 2 20 Copper ug/L ND 500 500 494 508 99 101 75-125 3 20 Lead ug/L ND 500 500 485 496 97 99 75-125 2 20 Nickel ug/L 0.016 500 500 500 510 97 99 75-125 2 20 mg/L Selenium ug/L ND 500 500 490 507 98 101 75-125 3 20 Silver ug/L ND 250 250 247 252 99 101 75-125 2 20 Tin ug/L ND 500 500 494 503 99 100 75-125 2 20 Vanadium ug/L ND 500 500 482 495 96 99 75-125 3 20 Zinc ug/L 0.066 500 500 557 569 98 101 75-125 2 20 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 79 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 QC Batch: 363321 Analysis Method: EPA 6010 QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92342478004, 92342478005, 92342478006 METHOD BLANK: 2014222 Matrix: Water Associated Lab Samples: 92342478004, 92342478005, 92342478006 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Antimony ug/L ND 5.0 3.9 06/14/17 21:19 Arsenic ug/L ND 10.0 5.0 06/14/17 21:19 Barium ug/L ND 5.0 2.5 06/14/17 21:19 Beryllium ug/L ND 1.0 0.50 06/14/17 21:19 Cadmium ug/L ND 1.0 0.50 06/14/17 21:19 Chromium ug/L ND 5.0 2.5 06/14/17 21:19 Cobalt ug/L ND 5.0 2.5 06/14/17 21:19 Copper ug/L ND 5.0 2.5 06/14/17 21:19 Lead ug/L ND 5.0 2.5 06/14/17 21:19 Nickel ug/L ND 5.0 2.5 06/14/17 21:19 Selenium ug/L ND 10.0 5.0 06/14/17 21:19 Silver ug/L ND 5.0 2.5 06/14/17 21:19 Tin ug/L ND 5.0 2.5 06/14/17 21:19 Vanadium ug/L ND 5.0 2.5 06/14/17 21:19 Zinc ug/L ND 10.0 5.0 06/14/17 21:19 LABORATORY CONTROL SAMPLE: 2014223 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Antimony ug/L 500 496 99 80-120 Arsenic ug/L 500 475 95 80-120 Barium ug/L 500 511 102 80-120 Beryllium ug/L 500 457 91 80-120 Cadmium ug/L 500 512 102 80-120 Chromium ug/L 500 463 93 80-120 Cobalt ug/L 500 498 100 80-120 Copper ug/L 500 494 99 80-120 Lead ug/L 500 486 97 80-120 Nickel ug/L 500 463 93 80-120 Selenium ug/L 500 501 100 80-120 Silver ug/L 250 235 94 80-120 Tin ug/L 500 485 97 80-120 Vanadium ug/L 500 456 91 80-120 Zinc ug/L 500 472 94 80-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 80 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: SURRY CLOSED -MT. 92342478 AIRY (UIC) MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2014224 2014225 MS MSD 92342605016 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 517 501 103 100 75-125 3 20 Arsenic ug/L 174 500 500 672 657 100 97 75-125 2 20 Barium ug/L 8.0 500 500 546 530 108 104 75-125 3 20 Beryllium ug/L 0.73J 500 500 481 471 96 94 75-125 2 20 Cadmium ug/L 1.7 500 500 540 524 108 105 75-125 3 20 Chromium ug/L ND 500 500 486 470 97 94 75-125 3 20 Cobalt ug/L 75.0 500 500 594 577 104 100 75-125 3 20 Copper ug/L ND 500 500 522 509 104 102 75-125 3 20 Lead ug/L 4AJ 500 500 506 491 100 97 75-125 3 20 Nickel ug/L 3.2J 500 500 481 466 96 93 75-125 3 20 Selenium ug/L ND 500 500 511 501 102 100 75-125 2 20 Silver ug/L ND 250 250 246 238 99 95 75-125 4 20 Tin ug/L ND 500 500 503 484 101 97 75-125 4 20 Vanadium ug/L ND 500 500 482 466 96 93 75-125 3 20 Zinc ug/L 5.8J 500 500 495 479 98 95 75-125 3 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 81 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 QC Batch: 363322 Analysis Method: EPA 6010 QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92342478007, 92342478008, 92342478009, 92342478010, 92342478011 METHOD BLANK: 2014226 Matrix: Water Associated Lab Samples: 92342478007, 92342478008, 92342478009, 92342478010, 92342478011 Blank Reporting Parameter Units Result Limit MDL Antimony ug/L ND 5.0 Arsenic ug/L ND 10.0 Barium ug/L ND 5.0 Beryllium ug/L ND 1.0 Cadmium ug/L ND 1.0 Chromium ug/L ND 5.0 Cobalt ug/L ND 5.0 Copper ug/L ND 5.0 Lead ug/L ND 5.0 Nickel ug/L ND 5.0 Selenium ug/L ND 10.0 Silver ug/L ND 5.0 Vanadium ug/L ND 5.0 Zinc ug/L ND 10.0 Analyzed 3.9 06/09/1718:44 5.0 06/09/1718:44 2.5 06/09/1718:44 0.50 06/09/1718:44 0.50 06/09/1718:44 2.5 06/09/1718:44 2.5 06/09/1718:44 2.5 06/09/1718:44 2.5 06/09/1718:44 2.5 06/09/1718:44 5.0 06/09/1718:44 2.5 06/09/1718:44 2.5 06/09/1718:44 5.0 06/09/1718:44 LABORATORY CONTROL SAMPLE: Parameter 2014227 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 500 515 103 80-120 Arsenic ug/L 500 496 99 80-120 Barium ug/L 500 514 103 80-120 Beryllium ug/L 500 510 102 80-120 Cadmium ug/L 500 516 103 80-120 Chromium ug/L 500 507 101 80-120 Cobalt ug/L 500 514 103 80-120 Copper ug/L 500 520 104 80-120 Lead ug/L 500 508 102 80-120 Nickel ug/L 500 505 101 80-120 Selenium ug/L 500 521 104 80-120 Silver ug/L 250 258 103 80-120 Vanadium ug/L 500 499 100 80-120 Zinc ug/L 500 514 103 80-120 Qualifiers Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2014228 2014229 MS MSD 92342478007 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 518 489 103 98 75-125 6 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 82 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: SURRY CLOSED -MT. 92342478 AIRY (UIC) MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2014228 2014229 MS MSD 92342478007 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Arsenic ug/L ND 500 500 506 479 101 96 75-125 6 20 Barium ug/L 23.5J 500 500 544 519 104 99 75-125 5 20 Beryllium ug/L ND 500 500 518 492 104 98 75-125 5 20 Cadmium ug/L 0.66J 500 500 520 495 104 99 75-125 5 20 Chromium ug/L ND 500 500 516 497 103 99 75-125 4 20 Cobalt ug/L ND 500 500 513 490 102 97 75-125 5 20 Copper ug/L 3.5J 500 500 526 503 105 100 75-125 5 20 Lead ug/L ND 500 500 503 482 100 96 75-125 4 20 Nickel ug/L 2.8J 500 500 503 481 100 96 75-125 4 20 Selenium ug/L ND 500 500 522 497 104 99 75-125 5 20 Silver ug/L ND 250 250 260 249 104 99 75-125 5 20 Vanadium ug/L ND 500 500 513 491 102 98 75-125 4 20 Zinc ug/L 6.6J 500 500 522 500 103 99 75-125 4 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 83 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 QC Batch: 363272 Analysis Method: EPA 6020B QC Batch Method: EPA 3010A Analysis Description: 6020 MET Associated Lab Samples: 92342478001, 92342478002, 92342478003 METHOD BLANK: 2014034 Matrix: Water Associated Lab Samples: 92342478001, 92342478002, 92342478003 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Thallium ug/L ND 0.10 0.020 06/06/1718:13 LABORATORY CONTROL SAMPLE: 2014035 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Thallium ug/L 100 94.5 95 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2014036 2014037 MS MSD 92342297004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Thallium ug/L 0.30J 100 100 97.2 95.7 97 95 75-125 2 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 84 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 QC Batch: 363273 Analysis Method: EPA 6020B QC Batch Method: EPA 3010A Analysis Description: 6020 MET Associated Lab Samples: 92342478004, 92342478005, 92342478006, 92342478007, 92342478008, 92342478009, 92342478010, 92342478011 METHOD BLANK: 2014038 Matrix: Water Associated Lab Samples: 92342478004, 92342478005, 92342478006, 92342478007, 92342478008, 92342478009, 92342478010, 92342478011 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Thallium ug/L ND 0.10 0.020 06/09/1716:01 LABORATORY CONTROL SAMPLE: 2014039 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Thallium ug/L 100 91.8 92 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2014040 2014041 MS MSD 92342600010 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Thallium ug/L ND 100 100 90.7 93.4 91 93 75-125 3 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 85 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 QC Batch: 363478 Analysis Method: EPA 6020B QC Batch Method: EPA 3010A Analysis Description: 6020 MET Associated Lab Samples: 92342530001, 92342530002, 92342530003, 92342530004, 92342530005 METHOD BLANK: 2015139 Matrix: Water Associated Lab Samples: 92342530001, 92342530002, 92342530003, 92342530004, 92342530005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Thallium ug/L ND 0.10 0.020 06/09/1716:55 LABORATORY CONTROL SAMPLE: 2015140 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Thallium ug/L 100 90.8 91 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2015141 2015142 MS MSD 92342795001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Thallium ug/L 0.0901 100 100 91.9 96.1 92 96 75-125 4 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 86 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 QC Batch: 363024 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92342478001, 92342478002, 92342478003 METHOD BLANK: 2012502 Matrix: Associated Lab Samples: 92342478001, 92342478002, 92342478003 Blank Parameter Units Result Water Reporting Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 0.33 06/02/17 00:55 1,1,1-Trichloroethane ug/L ND 1.0 0.48 06/02/17 00:55 1,1,2,2-Tetrachloroethane ug/L ND 3.0 0.40 06/02/17 00:55 1,1,2-Trichloroethane ug/L ND 1.0 0.29 06/02/17 00:55 1,1-Dichloroethane ug/L ND 5.0 0.32 06/02/17 00:55 1,1-Dichloroethene ug/L ND 5.0 0.56 06/02/17 00:55 1,1-Dichloropropene ug/L ND 5.0 0.49 06/02/17 00:55 1,2,3-Trichloropropane ug/L ND 1.0 0.41 06/02/17 00:55 1,2,4-Trichlorobenzene ug/L ND 10.0 0.35 06/02/17 00:55 1,2-Dibromo-3-chloropropane ug/L ND 13.0 2.0 06/02/17 00:55 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 06/02/17 00:55 1,2-Dichlorobenzene ug/L ND 5.0 0.30 06/02/17 00:55 1,2-Dichloroethane ug/L ND 1.0 0.24 06/02/17 00:55 1,2-Dichloropropane ug/L ND 1.0 0.27 06/02/17 00:55 1,3-Dichlorobenzene ug/L ND 5.0 0.24 06/02/17 00:55 1,3-Dichloropropane ug/L ND 1.0 0.28 06/02/17 00:55 1,4-Dichlorobenzene ug/L ND 1.0 0.33 06/02/17 00:55 2,2-Dichloropropane ug/L ND 15.0 0.13 06/02/17 00:55 2-Butanone (MEK) ug/L ND 100 0.96 06/02/17 00:55 2-Hexanone ug/L ND 50.0 0.46 06/02/17 00:55 4-Methyl-2-pentanone (MIBK) ug/L ND 100 0.33 06/02/17 00:55 Acetone ug/L ND 100 10.0 06/02/17 00:55 Acetonitrile ug/L ND 55.0 2.2 06/02/17 00:55 Acrolein ug/L ND 53.0 1.6 06/02/17 00:55 Acrylonitrile ug/L ND 200 1.9 06/02/17 00:55 Allyl chloride ug/L ND 10.0 1.5 06/02/17 00:55 Benzene ug/L ND 1.0 0.25 06/02/17 00:55 Bromochloromethane ug/L ND 3.0 0.17 06/02/17 00:55 Bromodichloromethane ug/L ND 1.0 0.18 06/02/17 00:55 Bromoform ug/L ND 3.0 0.26 06/02/17 00:55 Bromomethane ug/L ND 10.0 0.29 06/02/17 00:55 Carbon disulfide ug/L ND 100 1.2 06/02/17 00:55 Carbon tetrachloride ug/L ND 1.0 0.25 06/02/17 00:55 Chlorobenzene ug/L ND 3.0 0.23 06/02/17 00:55 Chloroethane ug/L ND 10.0 0.54 06/02/17 00:55 Chloroform ug/L ND 5.0 0.14 06/02/17 00:55 Chloromethane ug/L ND 1.0 0.11 06/02/17 00:55 Chloroprene ug/L ND 20.0 0.27 06/02/17 00:55 cis-1,2-Dichloroethene ug/L ND 5.0 0.19 06/02/17 00:55 cis-1,3-Dichloropropene ug/L ND 1.0 0.13 06/02/17 00:55 Dibromochloromethane ug/L ND 3.0 0.21 06/02/17 00:55 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 87 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 METHOD BLANK: 2012502 Matrix: Associated Lab Samples: 92342478001, 92342478002, 92342478003 Blank Parameter Units Result Water Reporting Limit MDL Analyzed Dibromomethane ug/L ND 10.0 0.21 06/02/17 00:55 Dichlorodifluoromethane ug/L ND 5.0 0.21 06/02/17 00:55 Ethyl methacrylate ug/L ND 10.0 0.20 06/02/17 00:55 Ethylbenzene ug/L ND 1.0 0.30 06/02/17 00:55 Hexachloro-1,3-butadiene ug/L ND 10.0 0.71 06/02/17 00:55 lodomethane ug/L ND 10.0 0.32 06/02/17 00:55 Isobutanol ug/L ND 100 35.0 06/02/17 00:55 Methacrylonitrile ug/L ND 100 0.93 06/02/17 00:55 Methyl methacrylate ug/L ND 30.0 2.0 06/02/17 00:55 Methylene Chloride ug/L ND 1.0 0.97 06/02/17 00:55 Naphthalene ug/L ND 10.0 0.24 06/02/17 00:55 Propionitrile ug/L ND 150 3.6 06/02/17 00:55 Styrene ug/L ND 1.0 0.26 06/02/17 00:55 Tetrachloroethene ug/L ND 1.0 0.46 06/02/17 00:55 Toluene ug/L ND 1.0 0.26 06/02/17 00:55 trans-1,2-Dichloroethene ug/L ND 5.0 0.49 06/02/17 00:55 trans- 1,3-Dichloropropene ug/L ND 1.0 0.26 06/02/17 00:55 trans-1,4-Dichloro-2-butene ug/L ND 100 1.0 06/02/17 00:55 Trichloroethene ug/L ND 1.0 0.47 06/02/17 00:55 Trichlorofluoromethane ug/L ND 1.0 0.20 06/02/17 00:55 Vinyl acetate ug/L ND 50.0 0.35 06/02/17 00:55 Vinyl chloride ug/L ND 1.0 0.62 06/02/17 00:55 Xylene (Total) ug/L ND 5.0 0.66 06/02/17 00:55 1,2-Dichloroethane-d4 (S) % 99 70-130 06/02/17 00:55 4-Bromofluorobenzene (S) % 115 70-130 06/02/17 00:55 Toluene-d8 (S) % 110 70-130 06/02/17 00:55 LABORATORY CONTROL SAMPLE: Parameter 2012503 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 50.9 102 80-125 1,1,1-Trichloroethane ug/L 50 46.3 93 71-129 1,1,2,2-Tetrachloroethane ug/L 50 54.2 108 79-124 1,1,2-Trichloroethane ug/L 50 50.1 100 85-125 1,1-Dichloroethane ug/L 50 44.0 88 73-126 1,1-Dichloroethene ug/L 50 38.4 77 66-135 1,1-Dichloropropene ug/L 50 50.3 101 74-135 1,2,3-Trichloropropane ug/L 50 54.5 109 75-130 1,2,4-Trichlorobenzene ug/L 50 43.1 86 75-134 1,2-Dibromo-3-chloropropane ug/L 50 46.8 94 71-133 1,2-Dibromoethane (EDB) ug/L 50 51.8 104 83-124 1,2-Dichlorobenzene ug/L 50 45.7 91 80-133 1,2-Dichloroethane ug/L 50 44.1 88 67-128 1,2-Dichloropropane ug/L 50 47.5 95 75-132 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 88 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 LABORATORY CONTROL SAMPLE: Parameter 2012503 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,3-Dichlorobenzene ug/L 50 46.7 93 77-130 1,3-Dichloropropane ug/L 50 52.1 104 76-131 1,4-Dichlorobenzene ug/L 50 46.8 94 78-130 2,2-Dichloropropane ug/L 50 42.6 85 40-160 2-Butanone (MEK) ug/L 100 105 105 61-144 2-Hexanone ug/L 100 99.7 100 68-143 4-Methyl-2-pentanone (MIBK) ug/L 100 103 103 72-135 Acetone ug/L 100 107 107 48-146 Acetonitrile ug/L 500 527 105 62-150 Acrolein ug/L 250 280 112 24-160 Acrylonitrile ug/L 250 234 94 40-160 Allyl chloride ug/L 50 41.5 83 66-137 Benzene ug/L 50 47.5 95 80-125 Bromochloromethane ug/L 50 45.7 91 71-125 Bromodichloromethane ug/L 50 47.1 94 78-124 Bromoform ug/L 50 57.5 115 71-128 Bromomethane ug/L 50 50.3 101 40-160 Carbon disulfide ug/L 50 40.5J 81 50-160 Carbon tetrachloride ug/L 50 47.0 94 69-131 Chlorobenzene ug/L 50 46.6 93 81-122 Chloroethane ug/L 50 46.9 94 39-148 Chloroform ug/L 50 42.9 86 73-127 Chloromethane ug/L 50 52.8 106 44-146 Chloroprene ug/L 50 46.0 92 75-145 cis-1,2-Dichloroethene ug/L 50 45.4 91 74-124 cis-1,3-Dichloropropene ug/L 50 50.6 101 72-132 Dibromochloromethane ug/L 50 53.6 107 78-125 Dibromomethane ug/L 50 45.1 90 82-120 Dichlorodifluoromethane ug/L 50 39.3 79 34-157 Ethyl methacrylate ug/L 50 52.1 104 82-121 Ethylbenzene ug/L 50 48.1 96 79-121 Hexachloro-1,3-butadiene ug/L 50 44.2 88 72-131 lodomethane ug/L 100 71.3 71 39-154 Isobutanol ug/L 1000 1050 105 34-160 Methacrylonitrile ug/L 500 520 104 74-134 Methyl methacrylate ug/L 50 46.9 94 84-124 Methylene Chloride ug/L 50 48.2 96 64-133 Naphthalene ug/L 50 45.2 90 73-133 Propionitrile ug/L 500 503 101 73-140 Styrene ug/L 50 51.0 102 84-126 Tetrachloroethene ug/L 50 49.0 98 78-122 Toluene ug/L 50 48.2 96 80-121 trans-1,2-Dichloroethene ug/L 50 44.5 89 71-127 trans- 1,3-Dichloropropene ug/L 50 53.1 106 69-141 trans-1,4-Dichloro-2-butene ug/L 50 63.5J 127 40-160 Trichloroethene ug/L 50 48.8 98 78-122 Trichlorofluoromethane ug/L 50 45.9 92 53-137 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 89 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 LABORATORY CONTROL SAMPLE: 2012503 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Vinyl acetate ug/L 100 92.9 93 40-160 Vinyl chloride ug/L 50 41.9 84 58-137 Xylene (Total) ug/L 150 147 98 81-126 1,2-Dichloroethane-d4 (S) % 100 70-130 4-Bromofluorobenzene (S) % 113 70-130 Toluene-d8 (S) % 100 70-130 MATRIX SPIKE SAMPLE: Parameter 2012504 Units 92342478001 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 19.5 98 70-130 1,1,1-Trichloroethane ug/L ND 20 22.4 112 70-130 1,1,2,2-Tetrachloroethane ug/L ND 20 21.4 107 70-130 1,1,2-Trichloroethane ug/L ND 20 18.0 90 70-130 1,1-Dichloroethane ug/L ND 20 21.8 109 70-130 1,1-Dichloroethene ug/L ND 20 25.9 129 70-166 1,1-Dichloropropene ug/L ND 20 22.9 114 70-130 1,2,3-Trichloropropane ug/L ND 20 20.9 105 70-130 1,2,4-Trichlorobenzene ug/L ND 20 18.5 92 70-130 1,2-Dibromo-3-chloropropane ug/L ND 20 16.9 85 70-130 1,2-Dibromoethane (EDB) ug/L ND 20 16.9 85 70-130 1,2-Dichlorobenzene ug/L ND 20 19.7 98 70-130 1,2-Dichloroethane ug/L ND 20 19.8 99 70-130 1,2-Dichloropropane ug/L ND 20 21.1 105 70-130 1,3-Dichlorobenzene ug/L ND 20 19.9 99 70-130 1,3-Dichloropropane ug/L ND 20 16.9 85 70-130 1,4-Dichlorobenzene ug/L ND 20 19.9 99 70-130 2,2-Dichloropropane ug/L ND 20 17.2 86 70-130 2-Butanone (MEK) ug/L ND 40 32.6J 82 70-130 2-Hexanone ug/L ND 40 31AJ 78 70-130 4-Methyl-2-pentanone (MIBK) ug/L ND 40 30.1J 75 70-130 Acetone ug/L ND 40 39.6J 99 70-130 Acetonitrile ug/L ND 200 182 91 70-130 Acrolein ug/L ND 100 110 110 70-130 Acrylonitrile ug/L ND 100 94.7J 95 70-130 Allyl chloride ug/L ND 20 21.2 106 70-130 Benzene ug/L ND 20 21.0 105 70-148 Bromochloromethane ug/L ND 20 22.2 111 70-130 Bromodichloromethane ug/L ND 20 20.6 103 70-130 Bromoform ug/L ND 20 20.1 100 70-130 Bromomethane ug/L ND 20 22.6 113 70-130 Carbon disulfide ug/L ND 20 25.5J 127 70-130 Carbon tetrachloride ug/L ND 20 21.6 108 70-130 Chlorobenzene ug/L ND 20 20.5 102 70-146 Chloroethane ug/L ND 20 23.9 119 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 90 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 MATRIX SPIKE SAMPLE: 2012504 92342478001 Spike MS MS Parameter Units Result Conc. Result % Rec Chloroform ug/L ND 20 20.5 102 Chloromethane ug/L ND 20 26.6 133 Chloroprene ug/L ND 20 20.9 105 cis-1,2-Dichloroethene ug/L ND 20 22.1 110 cis-1,3-Dichloropropene ug/L ND 20 16.1 80 Dibromochloromethane ug/L ND 20 16.7 83 Dibromomethane ug/L ND 20 19.5 98 Dichlorodifluoromethane ug/L ND 20 17.4 87 Ethyl methacrylate ug/L ND 20 15.2 76 Ethylbenzene ug/L ND 20 21.7 109 Hexachloro-1,3-butadiene ug/L ND 20 18.9 94 lodomethane ug/L ND 40 42.4 106 Isobutanol ug/L ND 400 301 75 Methacrylonitrile ug/L ND 200 188 94 Methyl methacrylate ug/L ND 20 17AJ 87 Methylene Chloride ug/L ND 20 21.7 108 Naphthalene ug/L ND 20 17.8 89 Propionitrile ug/L ND 200 188 94 Styrene ug/L ND 20 22.4 112 Tetrachloroethene ug/L ND 20 17.2 86 Toluene ug/L ND 20 18.6 93 trans-1,2-Dichloroethene ug/L ND 20 21.8 109 trans- 1,3-Dichloropropene ug/L ND 20 17.1 85 trans-1,4-Dichloro-2-butene ug/L ND 20 18.9J 94 Trichloroethene ug/L ND 20 21.9 109 Trichlorofluoromethane ug/L ND 20 23.6 118 Vinyl acetate ug/L ND 40 25AJ 64 Vinyl chloride ug/L ND 20 21.3 106 1,2-Dichloroethane-d4 (S) % 102 4-Bromofluorobenzene (S) % 116 Toluene-d8 (S) % 85 SAMPLE DUPLICATE: 2012505 92342478002 Dup Max Parameter Units Result Result RPD RPD 1,1,1,2-Tetrachloroethane ug/L ND ND 30 1,1,1-Trichloroethane ug/L ND ND 30 1,1,2,2-Tetrachloroethane ug/L ND ND 30 1,1,2-Trichloroethane ug/L ND ND 30 1,1-Dichloroethane ug/L 0.43J 0.48J 30 1,1-Dichloroethene ug/L ND ND 30 1,1-Dichloropropene ug/L ND ND 30 1,2,3-Trichloropropane ug/L ND ND 30 1,2,4-Trichlorobenzene ug/L ND ND 30 1,2-Dibromo-3-chloropropane ug/L ND ND 30 % Rec Limits Qualifiers 70-130 70-130 M1 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-155 70-130 70-130 70-130 69-151 70-130 70-130 M1 70-130 70-130 70-130 70-130 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 91 of 166 Pace Analytical Services, LLC aceAnalXical� 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 SAMPLE DUPLICATE: 2012505 Parameter Units 92342478002 Result Dup Result RPD Max RPD Qualifiers 1,2-Dibromoethane (EDB) ug/L ND ND 30 1,2-Dichlorobenzene ug/L ND ND 30 1,2-Dichloroethane ug/L ND ND 30 1,2-Dichloropropane ug/L ND ND 30 1,3-Dichlorobenzene ug/L ND ND 30 1,3-Dichloropropane ug/L ND ND 30 1,4-Dichlorobenzene ug/L ND ND 30 2,2-Dichloropropane ug/L ND ND 30 2-Butanone (MEK) ug/L ND ND 30 2-Hexanone ug/L ND ND 30 4-Methyl-2-pentanone (MIBK) ug/L ND ND 30 Acetone ug/L ND ND 30 Acetonitrile ug/L ND ND 30 Acrolein ug/L ND ND 30 Acrylonitrile ug/L ND ND 30 Allyl chloride ug/L ND ND 30 Benzene ug/L ND ND 30 Bromochloromethane ug/L ND ND 30 Bromodichloromethane ug/L ND ND 30 Bromoform ug/L ND ND 30 Bromomethane ug/L ND ND 30 Carbon disulfide ug/L ND ND 30 Carbon tetrachloride ug/L ND ND 30 Chlorobenzene ug/L ND ND 30 Chloroethane ug/L ND ND 30 Chloroform ug/L ND ND 30 Chloromethane ug/L ND ND 30 Chloroprene ug/L ND ND 30 cis-1,2-Dichloroethene ug/L 0.39J 0.43J 30 cis-1,3-Dichloropropene ug/L ND ND 30 Dibromochloromethane ug/L ND ND 30 Dibromomethane ug/L ND ND 30 Dichlorodifluoromethane ug/L ND ND 30 Ethyl methacrylate ug/L ND ND 30 Ethylbenzene ug/L ND ND 30 Hexachloro-1,3-butadiene ug/L ND ND 30 lodomethane ug/L ND ND 30 Isobutanol ug/L ND ND 30 Methacrylonitrile ug/L ND ND 30 Methyl methacrylate ug/L ND ND 30 Methylene Chloride ug/L ND ND 30 Naphthalene ug/L ND ND 30 Propionitrile ug/L ND ND 30 Styrene ug/L ND ND 30 Tetrachloroethene ug/L ND ND 30 Toluene ug/L ND ND 30 trans-1,2-Dichloroethene ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 92 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 SAMPLE DUPLICATE: 2012505 Parameter trans- 1,3-Dichloropropene trans-1,4-Dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylene (Total) 1,2-Dichloroethane-d4 (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) QUALITY CONTROL DATA Units 92342478002 Result Dup Result ug/L ND ND ug/L ND ND ug/L ND ND ug/L ND ND ug/L ND ND ug/L ND ND ug/L ND ND 100 103 113 114 111 113 IVV 3 1 1 Max RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 93 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 QC Batch: 363026 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92342530001, 92342530002, 92342530003, 92342530005 METHOD BLANK: 2012510 Matrix: Water Associated Lab Samples: 92342530001, 92342530002, 92342530003, 92342530005 Blank Reporting Parameter Units Result Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 0.33 06/02/17 01:12 1,1,1-Trichloroethane ug/L ND 1.0 0.48 06/02/17 01:12 1,1,2,2-Tetrachloroethane ug/L ND 3.0 0.40 06/02/17 01:12 1,1,2-Trichloroethane ug/L ND 1.0 0.29 06/02/17 01:12 1,1-Dichloroethane ug/L ND 5.0 0.32 06/02/17 01:12 1,1-Dichloroethene ug/L ND 5.0 0.56 06/02/17 01:12 1,1-Dichloropropene ug/L ND 5.0 0.49 06/02/17 01:12 1,2,3-Trichloropropane ug/L ND 1.0 0.41 06/02/17 01:12 1,2,4-Trichlorobenzene ug/L ND 10.0 0.35 06/02/17 01:12 1,2-Dibromo-3-chloropropane ug/L ND 13.0 2.0 06/02/17 01:12 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 06/02/17 01:12 1,2-Dichlorobenzene ug/L ND 5.0 0.30 06/02/17 01:12 1,2-Dichloroethane ug/L ND 1.0 0.24 06/02/17 01:12 1,2-Dichloropropane ug/L ND 1.0 0.27 06/02/17 01:12 1,3-Dichlorobenzene ug/L ND 5.0 0.24 06/02/17 01:12 1,3-Dichloropropane ug/L ND 1.0 0.28 06/02/17 01:12 1,4-Dichlorobenzene ug/L ND 1.0 0.33 06/02/17 01:12 2,2-Dichloropropane ug/L ND 15.0 0.13 06/02/17 01:12 2-Butanone (MEK) ug/L ND 100 0.96 06/02/17 01:12 2-Hexanone ug/L ND 50.0 0.46 06/02/17 01:12 4-Methyl-2-pentanone (MIBK) ug/L ND 100 0.33 06/02/17 01:12 Acetone ug/L ND 100 10.0 06/02/17 01:12 Acetonitrile ug/L ND 55.0 2.2 06/02/17 01:12 Acrolein ug/L ND 53.0 1.6 06/02/17 01:12 Acrylonitrile ug/L ND 200 1.9 06/02/17 01:12 Allyl chloride ug/L ND 10.0 1.5 06/02/17 01:12 Benzene ug/L ND 1.0 0.25 06/02/17 01:12 Bromochloromethane ug/L ND 3.0 0.17 06/02/17 01:12 Bromodichloromethane ug/L ND 1.0 0.18 06/02/17 01:12 Bromoform ug/L ND 3.0 0.26 06/02/17 01:12 Bromomethane ug/L ND 10.0 0.29 06/02/17 01:12 Carbon disulfide ug/L ND 100 1.2 06/02/17 01:12 Carbon tetrachloride ug/L ND 1.0 0.25 06/02/17 01:12 Chlorobenzene ug/L ND 3.0 0.23 06/02/17 01:12 Chloroethane ug/L ND 10.0 0.54 06/02/17 01:12 Chloroform ug/L ND 5.0 0.14 06/02/17 01:12 Chloromethane ug/L ND 1.0 0.11 06/02/17 01:12 Chloroprene ug/L ND 20.0 0.27 06/02/17 01:12 cis-1,2-Dichloroethene ug/L ND 5.0 0.19 06/02/17 01:12 cis-1,3-Dichloropropene ug/L ND 1.0 0.13 06/02/17 01:12 Dibromochloromethane ug/L ND 3.0 0.21 06/02/17 01:12 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 94 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 METHOD BLANK: 2012510 Matrix: Water Associated Lab Samples: 92342530001, 92342530002, 92342530003, 92342530005 Blank Reporting Parameter Units Result Limit MDL Analyzed Dibromomethane ug/L ND 10.0 0.21 06/02/17 01:12 Dichlorodifluoromethane ug/L ND 5.0 0.21 06/02/17 01:12 Ethyl methacrylate ug/L ND 10.0 0.20 06/02/17 01:12 Ethylbenzene ug/L ND 1.0 0.30 06/02/17 01:12 Hexachloro-1,3-butadiene ug/L ND 10.0 0.71 06/02/17 01:12 lodomethane ug/L ND 10.0 0.32 06/02/17 01:12 Isobutanol ug/L ND 100 35.0 06/02/17 01:12 Methacrylonitrile ug/L ND 100 0.93 06/02/17 01:12 Methyl methacrylate ug/L ND 30.0 2.0 06/02/17 01:12 Methylene Chloride ug/L ND 1.0 0.97 06/02/17 01:12 Naphthalene ug/L ND 10.0 0.24 06/02/17 01:12 Propionitrile ug/L ND 150 3.6 06/02/17 01:12 Styrene ug/L ND 1.0 0.26 06/02/17 01:12 Tetrachloroethene ug/L ND 1.0 0.46 06/02/17 01:12 Toluene ug/L ND 1.0 0.26 06/02/17 01:12 trans-1,2-Dichloroethene ug/L ND 5.0 0.49 06/02/17 01:12 trans- 1,3-Dichloropropene ug/L ND 1.0 0.26 06/02/17 01:12 trans-1,4-Dichloro-2-butene ug/L ND 100 1.0 06/02/17 01:12 Trichloroethene ug/L ND 1.0 0.47 06/02/17 01:12 Trichlorofluoromethane ug/L ND 1.0 0.20 06/02/17 01:12 Vinyl acetate ug/L ND 50.0 0.35 06/02/17 01:12 Vinyl chloride ug/L ND 1.0 0.62 06/02/17 01:12 Xylene (Total) ug/L ND 5.0 0.66 06/02/17 01:12 1,2-Dichloroethane-d4 (S) % 102 70-130 06/02/17 01:12 4-Bromofluorobenzene (S) % 114 70-130 06/02/17 01:12 Toluene-d8 (S) % 111 70-130 06/02/17 01:12 LABORATORY CONTROL SAMPLE: Parameter 2012511 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 50.8 102 80-125 1,1,1-Trichloroethane ug/L 50 45.5 91 71-129 1,1,2,2-Tetrachloroethane ug/L 50 55.1 110 79-124 1,1,2-Trichloroethane ug/L 50 51.2 102 85-125 1,1-Dichloroethane ug/L 50 43.3 87 73-126 1,1-Dichloroethene ug/L 50 37.0 74 66-135 1,1-Dichloropropene ug/L 50 49.6 99 74-135 1,2,3-Trichloropropane ug/L 50 55.2 110 75-130 1,2,4-Trichlorobenzene ug/L 50 44.4 89 75-134 1,2-Dibromo-3-chloropropane ug/L 50 48.0 96 71-133 1,2-Dibromoethane (EDB) ug/L 50 51.9 104 83-124 1,2-Dichlorobenzene ug/L 50 46.2 92 80-133 1,2-Dichloroethane ug/L 50 42.2 84 67-128 1,2-Dichloropropane ug/L 50 47.8 96 75-132 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 95 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 LABORATORY CONTROL SAMPLE: Parameter 2012511 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,3-Dichlorobenzene ug/L 50 47.5 95 77-130 1,3-Dichloropropane ug/L 50 51.9 104 76-131 1,4-Dichlorobenzene ug/L 50 47.2 94 78-130 2,2-Dichloropropane ug/L 50 42.0 84 40-160 2-Butanone (MEK) ug/L 100 104 104 61-144 2-Hexanone ug/L 100 104 104 68-143 4-Methyl-2-pentanone (MIBK) ug/L 100 106 106 72-135 Acetone ug/L 100 103 103 48-146 Acetonitrile ug/L 500 501 100 62-150 Acrolein ug/L 250 342 137 24-160 Acrylonitrile ug/L 250 230 92 40-160 Allyl chloride ug/L 50 39.9 80 66-137 Benzene ug/L 50 47.9 96 80-125 Bromochloromethane ug/L 50 44.6 89 71-125 Bromodichloromethane ug/L 50 46.8 94 78-124 Bromoform ug/L 50 57.3 115 71-128 Bromomethane ug/L 50 51.4 103 40-160 Carbon disulfide ug/L 50 42.2J 84 50-160 Carbon tetrachloride ug/L 50 47.0 94 69-131 Chlorobenzene ug/L 50 46.8 94 81-122 Chloroethane ug/L 50 47.2 94 39-148 Chloroform ug/L 50 44.0 88 73-127 Chloromethane ug/L 50 51.0 102 44-146 Chloroprene ug/L 50 45.5 91 75-145 cis-1,2-Dichloroethene ug/L 50 44.5 89 74-124 cis-1,3-Dichloropropene ug/L 50 51.4 103 72-132 Dibromochloromethane ug/L 50 54.7 109 78-125 Dibromomethane ug/L 50 45.7 91 82-120 Dichlorodifluoromethane ug/L 50 38.3 77 34-157 Ethyl methacrylate ug/L 50 52.5 105 82-121 Ethylbenzene ug/L 50 48.2 96 79-121 Hexachloro-1,3-butadiene ug/L 50 40.4 81 72-131 lodomethane ug/L 100 90.6 91 39-154 Isobutanol ug/L 1000 1060 106 34-160 Methacrylonitrile ug/L 500 514 103 74-134 Methyl methacrylate ug/L 50 48.0 96 84-124 Methylene Chloride ug/L 50 46.6 93 64-133 Naphthalene ug/L 50 46.3 93 73-133 Propionitrile ug/L 500 489 98 73-140 Styrene ug/L 50 51.3 103 84-126 Tetrachloroethene ug/L 50 49.2 98 78-122 Toluene ug/L 50 48.6 97 80-121 trans-1,2-Dichloroethene ug/L 50 43.7 87 71-127 trans- 1,3-Dichloropropene ug/L 50 53.5 107 69-141 trans-1,4-Dichloro-2-butene ug/L 50 61.6J 123 40-160 Trichloroethene ug/L 50 49.4 99 78-122 Trichlorofluoromethane ug/L 50 41.0 82 53-137 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 96 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 LABORATORY CONTROL SAMPLE: 2012511 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Vinyl acetate ug/L 100 91.3 91 40-160 Vinyl chloride ug/L 50 40.8 82 58-137 Xylene (Total) ug/L 150 147 98 81-126 1,2-Dichloroethane-d4 (S) % 98 70-130 4-Bromofluorobenzene (S) % 112 70-130 Toluene-d8 (S) % 100 70-130 MATRIX SPIKE SAMPLE: 2013904 92342317013 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 21.4 107 70-130 1,1,1-Trichloroethane ug/L ND 20 22.2 111 70-130 1,1,2,2-Tetrachloroethane ug/L ND 20 20.3 101 70-130 1,1,2-Trichloroethane ug/L ND 20 21.5 108 70-130 1,1-Dichloroethane ug/L ND 20 22.0 110 70-130 1,1-Dichloroethene ug/L ND 20 24.0 120 70-166 1,1-Dichloropropene ug/L ND 20 22.5 113 70-130 1,2,3-Trichloropropane ug/L ND 20 19.8 99 70-130 1,2,4-Trichlorobenzene ug/L ND 20 22.4 112 70-130 1,2-Dibromo-3-chloropropane ug/L ND 20 20.6 103 70-130 1,2-Dibromoethane (EDB) ug/L ND 20 20.4 102 70-130 1,2-Dichlorobenzene ug/L ND 20 21.0 105 70-130 1,2-Dichloroethane ug/L ND 20 22.0 110 70-130 1,2-Dichloropropane ug/L ND 20 21.9 109 70-130 1,3-Dichlorobenzene ug/L ND 20 20.3 101 70-130 1,3-Dichloropropane ug/L ND 20 21.4 107 70-130 1,4-Dichlorobenzene ug/L ND 20 19.9 99 70-130 2,2-Dichloropropane ug/L ND 20 11.51 57 70-130 M1 2-Butanone (MEK) ug/L ND 40 40.8J 102 70-130 2-Hexanone ug/L ND 40 39.5J 99 70-130 4-Methyl-2-pentanone (MIBK) ug/L ND 40 41.2J 103 70-130 Acetone ug/L 11.2J 40 52.9J 104 70-130 Acetonitrile ug/L ND 200 196 98 70-130 Acrolein ug/L ND 100 120 120 70-130 Acrylonitrile ug/L ND 100 102J 102 70-130 Allyl chloride ug/L ND 20 17.9 89 70-130 Benzene ug/L ND 20 21.9 110 70-148 Bromochloromethane ug/L ND 20 23.3 116 70-130 Bromodichloromethane ug/L ND 20 22.2 111 70-130 Bromoform ug/L ND 20 15.9 80 70-130 Bromomethane ug/L ND 20 27.0 135 70-130 M1 Carbon disulfide ug/L ND 20 22.8J 114 70-130 Carbon tetrachloride ug/L ND 20 22.0 110 70-130 Chlorobenzene ug/L ND 20 21.0 105 70-146 Chloroethane ug/L ND 20 19.0 95 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 97 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 MATRIX SPIKE SAMPLE: 2013904 92342317013 Spike MS MS Parameter Units Result Conc. Result % Rec Chloroform ug/L ND 20 22.8 114 Chloromethane ug/L ND 20 18.7 93 Chloroprene ug/L ND 20 20.1 101 cis-1,2-Dichloroethene ug/L ND 20 23.1 115 cis-1,3-Dichloropropene ug/L ND 20 19.8 99 Dibromochloromethane ug/L ND 20 20.8 104 Dibromomethane ug/L ND 20 22.1 110 Dichlorodifluoromethane ug/L ND 20 18.7 93 Ethyl methacrylate ug/L ND 20 19.5 97 Ethylbenzene ug/L ND 20 21.3 107 Hexachloro-1,3-butadiene ug/L ND 20 22.3 112 lodomethane ug/L ND 40 42.3 106 Isobutanol ug/L ND 400 361 90 Methacrylonitrile ug/L ND 200 211 105 Methyl methacrylate ug/L ND 20 19.91 100 Methylene Chloride ug/L ND 20 18.5 92 Naphthalene ug/L ND 20 25.2 126 Propionitrile ug/L ND 200 201 100 Styrene ug/L ND 20 20.8 104 Tetrachloroethene ug/L ND 20 19.0 95 Toluene ug/L ND 20 22.5 112 trans-1,2-Dichloroethene ug/L ND 20 22.5 112 trans- 1,3-Dichloropropene ug/L ND 20 18.9 94 trans-1,4-Dichloro-2-butene ug/L ND 20 14.6J 73 Trichloroethene ug/L ND 20 21.6 108 Trichlorofluoromethane ug/L ND 20 23.0 115 Vinyl acetate ug/L ND 40 23.3J 58 Vinyl chloride ug/L ND 20 21.0 105 1,2-Dichloroethane-d4 (S) % 110 4-Bromofluorobenzene (S) % 96 Toluene-d8 (S) % 102 SAMPLE DUPLICATE: 2012513 92342317012 Dup Max Parameter Units Result Result RPD RPD 1,1,1,2-Tetrachloroethane ug/L ND ND 30 1,1,1-Trichloroethane ug/L ND ND 30 1,1,2,2-Tetrachloroethane ug/L ND ND 30 1,1,2-Trichloroethane ug/L ND ND 30 1,1-Dichloroethane ug/L ND ND 30 1,1-Dichloroethene ug/L ND ND 30 1,1-Dichloropropene ug/L ND ND 30 1,2,3-Trichloropropane ug/L ND ND 30 1,2,4-Trichlorobenzene ug/L ND ND 30 1,2-Dibromo-3-chloropropane ug/L ND ND 30 % Rec Limits Qualifiers 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-130 70-155 70-130 70-130 70-130 69-151 70-130 70-130 M1 70-130 70-130 70-130 70-130 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 98 of 166 Pace Analytical Services, LLC aceAnalXical� 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 SAMPLE DUPLICATE: 2012513 Parameter Units 92342317012 Result Dup Result RPD Max RPD Qualifiers 1,2-Dibromoethane (EDB) ug/L ND ND 30 1,2-Dichlorobenzene ug/L ND ND 30 1,2-Dichloroethane ug/L ND ND 30 1,2-Dichloropropane ug/L ND ND 30 1,3-Dichlorobenzene ug/L ND ND 30 1,3-Dichloropropane ug/L ND ND 30 1,4-Dichlorobenzene ug/L ND ND 30 2,2-Dichloropropane ug/L ND ND 30 2-Butanone (MEK) ug/L ND ND 30 2-Hexanone ug/L ND ND 30 4-Methyl-2-pentanone (MIBK) ug/L ND ND 30 Acetone ug/L 12.1J 10AJ 30 Acetonitrile ug/L ND ND 30 Acrolein ug/L ND ND 30 Acrylonitrile ug/L ND ND 30 Allyl chloride ug/L ND ND 30 Benzene ug/L ND ND 30 Bromochloromethane ug/L ND ND 30 Bromodichloromethane ug/L ND ND 30 Bromoform ug/L ND ND 30 Bromomethane ug/L ND ND 30 Carbon disulfide ug/L ND ND 30 Carbon tetrachloride ug/L ND ND 30 Chlorobenzene ug/L ND ND 30 Chloroethane ug/L ND ND 30 Chloroform ug/L ND ND 30 Chloromethane ug/L ND ND 30 Chloroprene ug/L ND ND 30 cis-1,2-Dichloroethene ug/L ND ND 30 cis-1,3-Dichloropropene ug/L ND ND 30 Dibromochloromethane ug/L ND ND 30 Dibromomethane ug/L ND ND 30 Dichlorodifluoromethane ug/L ND ND 30 Ethyl methacrylate ug/L ND ND 30 Ethylbenzene ug/L ND ND 30 Hexachloro-1,3-butadiene ug/L ND ND 30 lodomethane ug/L ND ND 30 Isobutanol ug/L ND ND 30 Methacrylonitrile ug/L ND ND 30 Methyl methacrylate ug/L ND ND 30 Methylene Chloride ug/L ND ND 30 Naphthalene ug/L ND ND 30 Propionitrile ug/L ND ND 30 Styrene ug/L ND ND 30 Tetrachloroethene ug/L ND ND 30 Toluene ug/L ND ND 30 trans-1,2-Dichloroethene ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 99 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 SAMPLE DUPLICATE: 2012513 Parameter Units 92342317012 Result Dup Result trans- 1,3-Dichloropropene ug/L ND ND trans-1,4-Dichloro-2-butene ug/L ND ND Trichloroethene ug/L ND ND Trichlorofluoromethane ug/L 1.0 1.2 Vinyl acetate ug/L ND ND Vinyl chloride ug/L ND ND Xylene (Total) ug/L ND ND 1,2-Dichloroethane-d4 (S) % 99 99 4-Bromofluorobenzene (S) % 119 112 Toluene-d8(S) % 112 83 IVV 17 0 7 30 Max RPD Qualifiers 30 30 30 30 30 30 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 100 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 QC Batch: 363307 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92342530004 METHOD BLANK: 2014180 Associated Lab Samples: 92342530004 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 0.33 06/04/17 06:41 1,1,1-Trichloroethane ug/L ND 1.0 0.48 06/04/17 06:41 1,1,2,2-Tetrachloroethane ug/L ND 3.0 0.40 06/04/17 06:41 1,1,2-Trichloroethane ug/L ND 1.0 0.29 06/04/17 06:41 1,1-Dichloroethane ug/L ND 5.0 0.32 06/04/17 06:41 1,1-Dichloroethene ug/L ND 5.0 0.56 06/04/17 06:41 1,1-Dichloropropene ug/L ND 5.0 0.49 06/04/17 06:41 1,2,3-Trichloropropane ug/L ND 1.0 0.41 06/04/17 06:41 1,2,4-Trichlorobenzene ug/L ND 10.0 0.35 06/04/17 06:41 1,2-Dibromo-3-chloropropane ug/L ND 13.0 2.0 06/04/17 06:41 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 06/04/17 06:41 1,2-Dichlorobenzene ug/L ND 5.0 0.30 06/04/17 06:41 1,2-Dichloroethane ug/L ND 1.0 0.24 06/04/17 06:41 1,2-Dichloropropane ug/L ND 1.0 0.27 06/04/17 06:41 1,3-Dichlorobenzene ug/L ND 5.0 0.24 06/04/17 06:41 1,3-Dichloropropane ug/L ND 1.0 0.28 06/04/17 06:41 1,4-Dichlorobenzene ug/L ND 1.0 0.33 06/04/17 06:41 2,2-Dichloropropane ug/L ND 15.0 0.13 06/04/17 06:41 2-Butanone (MEK) ug/L ND 100 0.96 06/04/17 06:41 2-Hexanone ug/L ND 50.0 0.46 06/04/17 06:41 4-Methyl-2-pentanone (MIBK) ug/L ND 100 0.33 06/04/17 06:41 Acetone ug/L ND 100 10.0 06/04/17 06:41 Acetonitrile ug/L ND 55.0 2.2 06/04/17 06:41 Acrolein ug/L ND 53.0 1.6 06/04/17 06:41 Acrylonitrile ug/L ND 200 1.9 06/04/17 06:41 Allyl chloride ug/L ND 10.0 1.5 06/04/17 06:41 Benzene ug/L ND 1.0 0.25 06/04/17 06:41 Bromochloromethane ug/L ND 3.0 0.17 06/04/17 06:41 Bromodichloromethane ug/L ND 1.0 0.18 06/04/17 06:41 Bromoform ug/L ND 3.0 0.26 06/04/17 06:41 Bromomethane ug/L ND 10.0 0.29 06/04/17 06:41 Carbon disulfide ug/L ND 100 1.2 06/04/17 06:41 Carbon tetrachloride ug/L ND 1.0 0.25 06/04/17 06:41 Chlorobenzene ug/L ND 3.0 0.23 06/04/17 06:41 Chloroethane ug/L ND 10.0 0.54 06/04/17 06:41 Chloroform ug/L ND 5.0 0.14 06/04/17 06:41 Chloromethane ug/L ND 1.0 0.11 06/04/17 06:41 Chloroprene ug/L ND 20.0 0.27 06/04/17 06:41 cis-1,2-Dichloroethene ug/L ND 5.0 0.19 06/04/17 06:41 cis-1,3-Dichloropropene ug/L ND 1.0 0.13 06/04/17 06:41 Dibromochloromethane ug/L ND 3.0 0.21 06/04/17 06:41 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 101 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 METHOD BLANK: 2014180 Associated Lab Samples: 92342530004 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Dibromomethane ug/L ND 10.0 0.21 06/04/17 06:41 Dichlorodifluoromethane ug/L ND 5.0 0.21 06/04/17 06:41 Ethyl methacrylate ug/L ND 10.0 0.20 06/04/17 06:41 Ethylbenzene ug/L ND 1.0 0.30 06/04/17 06:41 Hexachloro-1,3-butadiene ug/L 1.6J 10.0 0.71 06/04/17 06:41 lodomethane ug/L ND 10.0 0.32 06/04/17 06:41 Isobutanol ug/L ND 100 35.0 06/04/17 06:41 Methacrylonitrile ug/L ND 100 0.93 06/04/17 06:41 Methyl methacrylate ug/L ND 30.0 2.0 06/04/17 06:41 Methylene Chloride ug/L ND 1.0 0.97 06/04/17 06:41 Naphthalene ug/L ND 10.0 0.24 06/04/17 06:41 Propionitrile ug/L ND 150 3.6 06/04/17 06:41 Styrene ug/L ND 1.0 0.26 06/04/17 06:41 Tetrachloroethene ug/L ND 1.0 0.46 06/04/17 06:41 Toluene ug/L ND 1.0 0.26 06/04/17 06:41 trans-1,2-Dichloroethene ug/L ND 5.0 0.49 06/04/17 06:41 trans- 1,3-Dichloropropene ug/L ND 1.0 0.26 06/04/17 06:41 trans-1,4-Dichloro-2-butene ug/L ND 100 1.0 06/04/17 06:41 Trichloroethene ug/L ND 1.0 0.47 06/04/17 06:41 Trichlorofluoromethane ug/L ND 1.0 0.20 06/04/17 06:41 Vinyl acetate ug/L ND 50.0 0.35 06/04/17 06:41 Vinyl chloride ug/L ND 1.0 0.62 06/04/17 06:41 Xylene (Total) ug/L ND 5.0 0.66 06/04/17 06:41 1,2-Dichloroethane-d4 (S) % 89 70-130 06/04/17 06:41 4-Bromofluorobenzene (S) % 113 70-130 06/04/17 06:41 Toluene-d8 (S) % 106 70-130 06/04/17 06:41 LABORATORY CONTROL SAMPLE: Parameter 2014181 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 50.1 100 80-125 1,1,1-Trichloroethane ug/L 50 48.8 98 71-129 1,1,2,2-Tetrachloroethane ug/L 50 57.0 114 79-124 1,1,2-Trichloroethane ug/L 50 51.1 102 85-125 1,1-Dichloroethane ug/L 50 49.9 100 73-126 1,1-Dichloroethene ug/L 50 44.7 89 66-135 1,1-Dichloropropene ug/L 50 49.9 100 74-135 1,2,3-Trichloropropane ug/L 50 47.3 95 75-130 1,2,4-Trichlorobenzene ug/L 50 48.0 96 75-134 1,2-Dibromo-3-chloropropane ug/L 50 48.7 97 71-133 1,2-Dibromoethane (EDB) ug/L 50 56.3 113 83-124 1,2-Dichlorobenzene ug/L 50 50.9 102 80-133 1,2-Dichloroethane ug/L 50 45.7 91 67-128 1,2-Dichloropropane ug/L 50 54.4 109 75-132 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 102 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 LABORATORY CONTROL SAMPLE: Parameter 2014181 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,3-Dichlorobenzene ug/L 50 48.3 97 77-130 1,3-Dichloropropane ug/L 50 54.6 109 76-131 1,4-Dichlorobenzene ug/L 50 47.7 95 78-130 2,2-Dichloropropane ug/L 50 44.6 89 40-160 2-Butanone (MEK) ug/L 100 136 136 61-144 2-Hexanone ug/L 100 110 110 68-143 4-Methyl-2-pentanone (MIBK) ug/L 100 109 109 72-135 Acetone ug/L 100 116 116 48-146 Acetonitrile ug/L 500 541 108 62-150 Acrolein ug/L 250 336 134 24-160 Acrylonitrile ug/L 250 274 110 40-160 Allyl chloride ug/L 50 47.1 94 66-137 Benzene ug/L 50 52.5 105 80-125 Bromochloromethane ug/L 50 47.8 96 71-125 Bromodichloromethane ug/L 50 49.3 99 78-124 Bromoform ug/L 50 48.1 96 71-128 Bromomethane ug/L 50 41.9 84 40-160 Carbon disulfide ug/L 50 50.8J 102 50-160 Carbon tetrachloride ug/L 50 44.5 89 69-131 Chlorobenzene ug/L 50 51.4 103 81-122 Chloroethane ug/L 50 43.7 87 39-148 Chloroform ug/L 50 48.3 97 73-127 Chloromethane ug/L 50 53.8 108 44-146 Chloroprene ug/L 50 47.0 94 75-145 cis-1,2-Dichloroethene ug/L 50 51.0 102 74-124 cis-1,3-Dichloropropene ug/L 50 53.8 108 72-132 Dibromochloromethane ug/L 50 47.7 95 78-125 Dibromomethane ug/L 50 48.5 97 82-120 Dichlorodifluoromethane ug/L 50 41.3 83 34-157 Ethyl methacrylate ug/L 50 46.6 93 82-121 Ethylbenzene ug/L 50 50.3 101 79-121 Hexachloro-1,3-butadiene ug/L 50 41.6 83 72-131 lodomethane ug/L 100 95.3 95 39-154 Isobutanol ug/L 1000 1200 120 34-160 Methacrylonitrile ug/L 500 566 113 74-134 Methyl methacrylate ug/L 50 50.8 102 84-124 Methylene Chloride ug/L 50 49.9 100 64-133 Naphthalene ug/L 50 52.9 106 73-133 Propionitrile ug/L 500 623 125 73-140 Styrene ug/L 50 49.7 99 84-126 Tetrachloroethene ug/L 50 45.9 92 78-122 Toluene ug/L 50 49.6 99 80-121 trans-1,2-Dichloroethene ug/L 50 51.4 103 71-127 trans- 1,3-Dichloropropene ug/L 50 53.3 107 69-141 trans-1,4-Dichloro-2-butene ug/L 50 94.OJ 188 40-160 L1 Trichloroethene ug/L 50 50.6 101 78-122 Trichlorofluoromethane ug/L 50 45.0 90 53-137 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 103 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 LABORATORY CONTROL SAMPLE: 2014181 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Vinyl acetate ug/L 100 96.4 96 40-160 Vinyl chloride ug/L 50 45.1 90 58-137 Xylene (Total) ug/L 150 141 94 81-126 1,2-Dichloroethane-d4 (S) % 90 70-130 4-Bromofluorobenzene (S) % 98 70-130 Toluene-d8 (S) % 100 70-130 MATRIX SPIKE SAMPLE: Parameter 2014183 Units 92342730006 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 19.1 96 70-130 1,1,1-Trichloroethane ug/L ND 20 22.5 112 70-130 1,1,2,2-Tetrachloroethane ug/L ND 20 22.0 110 70-130 1,1,2-Trichloroethane ug/L ND 20 20.1 100 70-130 1,1-Dichloroethane ug/L ND 20 22.3 112 70-130 1,1-Dichloroethene ug/L ND 20 23.0 115 70-166 1,1-Dichloropropene ug/L ND 20 24.2 121 70-130 1,2,3-Trichloropropane ug/L ND 20 18.1 90 70-130 1,2,4-Trichlorobenzene ug/L ND 20 19.2 96 70-130 1,2-Dibromo-3-chloropropane ug/L ND 20 18.9 94 70-130 1,2-Dibromoethane (EDB) ug/L ND 20 21.1 106 70-130 1,2-Dichlorobenzene ug/L ND 20 21.2 106 70-130 1,2-Dichloroethane ug/L ND 20 20.3 101 70-130 1,2-Dichloropropane ug/L ND 20 22.9 115 70-130 1,3-Dichlorobenzene ug/L ND 20 20.0 100 70-130 1,3-Dichloropropane ug/L ND 20 20.6 103 70-130 1,4-Dichlorobenzene ug/L ND 20 20.2 101 70-130 2,2-Dichloropropane ug/L ND 20 22.2 111 70-130 2-Butanone (MEK) ug/L ND 40 46.6J 116 70-130 2-Hexanone ug/L ND 40 44.9J 112 70-130 4-Methyl-2-pentanone (MIBK) ug/L ND 40 42.OJ 105 70-130 Acetone ug/L 11.6J 40 49.1 J 94 70-130 Acetonitrile ug/L ND 200 232 116 70-130 Acrolein ug/L ND 100 128 128 70-130 Acrylonitrile ug/L ND 100 113J 113 70-130 Allyl chloride ug/L ND 20 23.2 116 70-130 Benzene ug/L ND 20 23.2 116 70-148 Bromochloromethane ug/L ND 20 20.9 105 70-130 Bromodichloromethane ug/L ND 20 21.3 106 70-130 Bromoform ug/L ND 20 17.3 86 70-130 Bromomethane ug/L ND 20 22.4 112 70-130 Carbon disulfide ug/L ND 20 23.6J 118 70-130 Carbon tetrachloride ug/L ND 20 21.0 105 70-130 Chlorobenzene ug/L ND 20 22.0 110 70-146 Chloroethane ug/L ND 20 20.9 104 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 104 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 MATRIX SPIKE SAMPLE: 2014183 92342730006 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Chloroform ug/L ND 20 22.8 114 70-130 Chloromethane ug/L ND 20 24.6 123 70-130 Chloroprene ug/L ND 20 21.8 109 70-130 cis-1,2-Dichloroethene ug/L ND 20 22.8 114 70-130 cis-1,3-Dichloropropene ug/L ND 20 22.4 112 70-130 Dibromochloromethane ug/L ND 20 19.5 98 70-130 Dibromomethane ug/L ND 20 21.8 109 70-130 Dichlorodifluoromethane ug/L ND 20 18.2 91 70-130 Ethyl methacrylate ug/L ND 20 20.4 102 70-130 Ethylbenzene ug/L ND 20 22.3 112 70-130 Hexachloro-1,3-butadiene ug/L ND 20 20.5 103 70-130 lodomethane ug/L ND 40 41.2 103 70-130 Isobutanol ug/L ND 400 463 116 70-130 Methacrylonitrile ug/L ND 200 217 108 70-130 Methyl methacrylate ug/L ND 20 19AJ 97 70-130 Methylene Chloride ug/L ND 20 21.8 109 70-130 Naphthalene ug/L ND 20 22.6 113 70-130 Propionitrile ug/L ND 200 228 114 70-130 Styrene ug/L ND 20 20.9 104 70-130 Tetrachloroethene ug/L ND 20 20.8 104 70-130 Toluene ug/L ND 20 22.5 113 70-155 trans-1,2-Dichloroethene ug/L ND 20 23.9 119 70-130 trans- 1,3-Dichloropropene ug/L ND 20 22.7 114 70-130 trans-1,4-Dichloro-2-butene ug/L ND 20 28.2J 141 70-130 MO Trichloroethene ug/L ND 20 22.5 112 69-151 Trichlorofluoromethane ug/L ND 20 21.7 109 70-130 Vinyl acetate ug/L ND 40 40.5J 101 70-130 Vinyl chloride ug/L ND 20 21.2 106 70-130 1,2-Dichloroethane-d4 (S) % 100 70-130 4-Bromofluorobenzene (S) % 102 70-130 Toluene-d8(S) % 104 70-130 SAMPLE DUPLICATE: 2014182 92342730005 Dup Max Parameter Units Result Result RPD RPD Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND ND 30 1,1,1-Trichloroethane ug/L ND ND 30 1,1,2,2-Tetrachloroethane ug/L ND ND 30 1,1,2-Trichloroethane ug/L ND ND 30 1,1-Dichloroethane ug/L ND ND 30 1,1-Dichloroethene ug/L ND ND 30 1,1-Dichloropropene ug/L ND ND 30 1,2,3-Trichloropropane ug/L ND ND 30 1,2,4-Trichlorobenzene ug/L ND ND 30 1,2-Dibromo-3-chloropropane ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 105 of 166 Pace Analytical Services, LLC aceAnalXical� 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 SAMPLE DUPLICATE: 2014182 Parameter Units 92342730005 Result Dup Result RPD Max RPD Qualifiers 1,2-Dibromoethane (EDB) ug/L ND ND 30 1,2-Dichlorobenzene ug/L ND ND 30 1,2-Dichloroethane ug/L ND ND 30 1,2-Dichloropropane ug/L ND ND 30 1,3-Dichlorobenzene ug/L ND ND 30 1,3-Dichloropropane ug/L ND ND 30 1,4-Dichlorobenzene ug/L ND ND 30 2,2-Dichloropropane ug/L ND ND 30 2-Butanone (MEK) ug/L ND ND 30 2-Hexanone ug/L ND ND 30 4-Methyl-2-pentanone (MIBK) ug/L ND ND 30 Acetone ug/L ND 13.6J 30 Acetonitrile ug/L ND ND 30 Acrolein ug/L ND ND 30 Acrylonitrile ug/L ND ND 30 Allyl chloride ug/L ND ND 30 Benzene ug/L ND ND 30 Bromochloromethane ug/L ND ND 30 Bromodichloromethane ug/L ND ND 30 Bromoform ug/L ND ND 30 Bromomethane ug/L ND ND 30 Carbon disulfide ug/L ND ND 30 Carbon tetrachloride ug/L ND ND 30 Chlorobenzene ug/L ND ND 30 Chloroethane ug/L ND ND 30 Chloroform ug/L ND ND 30 Chloromethane ug/L 0.13J 0.16J 30 Chloroprene ug/L ND ND 30 cis-1,2-Dichloroethene ug/L ND ND 30 cis-1,3-Dichloropropene ug/L ND ND 30 Dibromochloromethane ug/L ND ND 30 Dibromomethane ug/L ND ND 30 Dichlorodifluoromethane ug/L ND ND 30 Ethyl methacrylate ug/L ND ND 30 Ethylbenzene ug/L ND ND 30 Hexachloro-1,3-butadiene ug/L ND ND 30 lodomethane ug/L ND ND 30 Isobutanol ug/L ND ND 30 Methacrylonitrile ug/L ND ND 30 Methyl methacrylate ug/L ND ND 30 Methylene Chloride ug/L ND ND 30 Naphthalene ug/L ND ND 30 Propionitrile ug/L ND ND 30 Styrene ug/L ND ND 30 Tetrachloroethene ug/L ND ND 30 Toluene ug/L ND ND 30 trans-1,2-Dichloroethene ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 106 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 SAMPLE DUPLICATE: 2014182 Parameter trans- 1,3-Dichloropropene trans-1,4-Dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylene (Total) 1,2-Dichloroethane-d4 (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) QUALITY CONTROL DATA Units 92342730005 Result Dup Result ug/L ND ND ug/L ND ND ug/L ND ND ug/L ND ND ug/L ND ND ug/L ND ND ug/L ND ND % 92 87 102 100 109 108 IVV 6 2 1 Max RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 107 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 QC Batch: 363328 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92342478004, 92342478005, 92342478006, 92342478007, 92342478008, 92342478009, 92342478010, 92342478011 METHOD BLANK: 2014255 Matrix: Water Associated Lab Samples: 92342478004, 92342478005, 92342478006, 92342478007, 92342478008, 92342478009, 92342478010, 92342478011 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 5.0 0.33 06/04/17 20:01 1,1,1-Trichloroethane ug/L ND 1.0 0.48 06/04/17 20:01 1,1,2,2-Tetrachloroethane ug/L ND 3.0 0.40 06/04/17 20:01 1,1,2-Trichloroethane ug/L ND 1.0 0.29 06/04/17 20:01 1,1-Dichloroethane ug/L ND 5.0 0.32 06/04/17 20:01 1,1-Dichloroethene ug/L ND 5.0 0.56 06/04/17 20:01 1,1-Dichloropropene ug/L ND 5.0 0.49 06/04/17 20:01 1,2,3-Trichloropropane ug/L ND 1.0 0.41 06/04/17 20:01 1,2,4-Trichlorobenzene ug/L ND 10.0 0.35 06/04/17 20:01 1,2-Dibromo-3-chloropropane ug/L ND 13.0 2.0 06/04/17 20:01 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 06/04/17 20:01 1,2-Dichlorobenzene ug/L ND 5.0 0.30 06/04/17 20:01 1,2-Dichloroethane ug/L ND 1.0 0.24 06/04/17 20:01 1,2-Dichloropropane ug/L ND 1.0 0.27 06/04/17 20:01 1,3-Dichlorobenzene ug/L ND 5.0 0.24 06/04/17 20:01 1,3-Dichloropropane ug/L ND 1.0 0.28 06/04/17 20:01 1,4-Dichlorobenzene ug/L ND 1.0 0.33 06/04/17 20:01 2,2-Dichloropropane ug/L ND 15.0 0.13 06/04/17 20:01 2-Butanone (MEK) ug/L ND 100 0.96 06/04/17 20:01 2-Hexanone ug/L ND 50.0 0.46 06/04/17 20:01 4-Methyl-2-pentanone (MIBK) ug/L ND 100 0.33 06/04/17 20:01 Acetone ug/L ND 100 10.0 06/04/17 20:01 Acetonitrile ug/L ND 55.0 2.2 06/04/17 20:01 Acrolein ug/L ND 53.0 1.6 06/04/17 20:01 Acrylonitrile ug/L ND 200 1.9 06/04/17 20:01 Allyl chloride ug/L ND 10.0 1.5 06/04/17 20:01 Benzene ug/L ND 1.0 0.25 06/04/17 20:01 Bromochloromethane ug/L ND 3.0 0.17 06/04/17 20:01 Bromodichloromethane ug/L ND 1.0 0.18 06/04/17 20:01 Bromoform ug/L ND 3.0 0.26 06/04/17 20:01 Bromomethane ug/L ND 10.0 0.29 06/04/17 20:01 Carbon disulfide ug/L ND 100 1.2 06/04/17 20:01 Carbon tetrachloride ug/L ND 1.0 0.25 06/04/17 20:01 Chlorobenzene ug/L ND 3.0 0.23 06/04/17 20:01 Chloroethane ug/L ND 10.0 0.54 06/04/17 20:01 Chloroform ug/L ND 5.0 0.14 06/04/17 20:01 Chloromethane ug/L ND 1.0 0.11 06/04/17 20:01 Chloroprene ug/L ND 20.0 0.27 06/04/17 20:01 cis-1,2-Dichloroethene ug/L ND 5.0 0.19 06/04/17 20:01 cis-1,3-Dichloropropene ug/L ND 1.0 0.13 06/04/17 20:01 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 108 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 METHOD BLANK: 2014255 Matrix: Water Associated Lab Samples: 92342478004, 92342478005, 92342478006, 92342478007, 92342478008, 92342478009, 92342478010, 92342478011 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Dibromochloromethane ug/L ND 3.0 0.21 06/04/17 20:01 Dibromomethane ug/L ND 10.0 0.21 06/04/17 20:01 Dichlorodifluoromethane ug/L ND 5.0 0.21 06/04/17 20:01 Ethyl methacrylate ug/L ND 10.0 0.20 06/04/17 20:01 Ethylbenzene ug/L ND 1.0 0.30 06/04/17 20:01 Hexachloro-1,3-butadiene ug/L ND 10.0 0.71 06/04/17 20:01 lodomethane ug/L ND 10.0 0.32 06/04/17 20:01 Isobutanol ug/L ND 100 35.0 06/04/17 20:01 Methacrylonitrile ug/L ND 100 0.93 06/04/17 20:01 Methyl methacrylate ug/L ND 30.0 2.0 06/04/17 20:01 Methylene Chloride ug/L ND 1.0 0.97 06/04/17 20:01 Naphthalene ug/L ND 10.0 0.24 06/04/17 20:01 Propionitrile ug/L ND 150 3.6 06/04/17 20:01 Styrene ug/L ND 1.0 0.26 06/04/17 20:01 Tetrachloroethene ug/L ND 1.0 0.46 06/04/17 20:01 Toluene ug/L ND 1.0 0.26 06/04/17 20:01 trans-1,2-Dichloroethene ug/L ND 5.0 0.49 06/04/17 20:01 trans- 1,3-Dichloropropene ug/L ND 1.0 0.26 06/04/17 20:01 trans-1,4-Dichloro-2-butene ug/L ND 100 1.0 06/04/17 20:01 Trichloroethene ug/L ND 1.0 0.47 06/04/17 20:01 Trichlorofluoromethane ug/L ND 1.0 0.20 06/04/17 20:01 Vinyl acetate ug/L ND 50.0 0.35 06/04/17 20:01 Vinyl chloride ug/L ND 1.0 0.62 06/04/17 20:01 Xylene (Total) ug/L ND 5.0 0.66 06/04/17 20:01 1,2-Dichloroethane-d4 (S) % 85 70-130 06/04/17 20:01 4-Bromofluorobenzene (S) % 100 70-130 06/04/17 20:01 Toluene-d8 (S) % 115 70-130 06/04/17 20:01 LABORATORY CONTROL SAMPLE: 2014256 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 46.6 93 80-125 1,1,1-Trichloroethane ug/L 50 50.7 101 71-129 1,1,2,2-Tetrachloroethane ug/L 50 49.8 100 79-124 1,1,2-Trichloroethane ug/L 50 48.9 98 85-125 1,1-Dichloroethane ug/L 50 49.6 99 73-126 1,1-Dichloroethene ug/L 50 46.9 94 66-135 1,1-Dichloropropene ug/L 50 51.9 104 74-135 1,2,3-Trichloropropane ug/L 50 46.5 93 75-130 1,2,4-Trichlorobenzene ug/L 50 46.5 93 75-134 1,2-Dibromo-3-chloropropane ug/L 50 46.7 93 71-133 1,2-Dibromoethane (EDB) ug/L 50 54.5 109 83-124 1,2-Dichlorobenzene ug/L 50 47.5 95 80-133 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 109 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 LABORATORY CONTROL SAMPLE: Parameter 2014256 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,2-Dichloroethane ug/L 50 47.0 94 67-128 1,2-Dichloropropane ug/L 50 53.4 107 75-132 1,3-Dichlorobenzene ug/L 50 48.1 96 77-130 1,3-Dichloropropane ug/L 50 54.1 108 76-131 1,4-Dichlorobenzene ug/L 50 47.9 96 78-130 2,2-Dichloropropane ug/L 50 50.7 101 40-160 2-Butanone (MEK) ug/L 100 126 126 61-144 2-Hexanone ug/L 100 101 101 68-143 4-Methyl-2-pentanone (MIBK) ug/L 100 94.9J 95 72-135 Acetone ug/L 100 115 115 48-146 Acetonitrile ug/L 500 525 105 62-150 Acrolein ug/L 250 320 128 24-160 Acrylonitrile ug/L 250 268 107 40-160 Allyl chloride ug/L 50 47.6 95 66-137 Benzene ug/L 50 52.1 104 80-125 Bromochloromethane ug/L 50 48.9 98 71-125 Bromodichloromethane ug/L 50 48.5 97 78-124 Bromoform ug/L 50 43.1 86 71-128 Bromomethane ug/L 50 42.1 84 40-160 Carbon disulfide ug/L 50 49.3J 99 50-160 Carbon tetrachloride ug/L 50 45.1 90 69-131 Chlorobenzene ug/L 50 48.8 98 81-122 Chloroethane ug/L 50 40.8 82 39-148 Chloroform ug/L 50 50.9 102 73-127 Chloromethane ug/L 50 49.9 100 44-146 Chloroprene ug/L 50 49.3 99 75-145 cis-1,2-Dichloroethene ug/L 50 52.5 105 74-124 cis-1,3-Dichloropropene ug/L 50 54.1 108 72-132 Dibromochloromethane ug/L 50 47.5 95 78-125 Dibromomethane ug/L 50 44.2 88 82-120 Dichlorodifluoromethane ug/L 50 41.1 82 34-157 Ethyl methacrylate ug/L 50 45.7 91 82-121 Ethylbenzene ug/L 50 50.1 100 79-121 Hexachloro-1,3-butadiene ug/L 50 43.5 87 72-131 lodomethane ug/L 100 91.7 92 39-154 Isobutanol ug/L 1000 1130 113 34-160 Methacrylonitrile ug/L 500 563 113 74-134 Methyl methacrylate ug/L 50 43.5 87 84-124 Methylene Chloride ug/L 50 53.6 107 64-133 Naphthalene ug/L 50 48.6 97 73-133 Propionitrile ug/L 500 562 112 73-140 Styrene ug/L 50 51.0 102 84-126 Tetrachloroethene ug/L 50 44.8 90 78-122 Toluene ug/L 50 46.4 93 80-121 trans-1,2-Dichloroethene ug/L 50 52.3 105 71-127 trans- 1,3-Dichloropropene ug/L 50 52.4 105 69-141 trans-1,4-Dichloro-2-butene ug/L 50 68.3J 137 40-160 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 110 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 LABORATORY CONTROL SAMPLE: 2014256 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Trichloroethene ug/L 50 50.4 101 78-122 Trichlorofluoromethane ug/L 50 45.4 91 53-137 Vinyl acetate ug/L 100 99.2 99 40-160 Vinyl chloride ug/L 50 41.9 84 58-137 Xylene (Total) ug/L 150 149 99 81-126 1,2-Dichloroethane-d4 (S) % 103 70-130 4-Bromofluorobenzene (S) % 107 70-130 Toluene-d8 (S) % 96 70-130 MATRIX SPIKE SAMPLE: 2014258 92342478011 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 20.0 100 70-130 1,1,1-Trichloroethane ug/L ND 20 23.0 115 70-130 1,1,2,2-Tetrachloroethane ug/L ND 20 22.1 110 70-130 1,1,2-Trichloroethane ug/L ND 20 22.2 111 70-130 1,1-Dichloroethane ug/L ND 20 23.1 116 70-130 1,1-Dichloroethene ug/L ND 20 23.0 115 70-166 1,1-Dichloropropene ug/L ND 20 23.3 116 70-130 1,2,3-Trichloropropane ug/L ND 20 19.5 98 70-130 1,2,4-Trichlorobenzene ug/L ND 20 19.3 97 70-130 1,2-Dibromo-3-chloropropane ug/L ND 20 18.2 91 70-130 1,2-Dibromoethane (EDB) ug/L ND 20 19.7 99 70-130 1,2-Dichlorobenzene ug/L ND 20 20.9 105 70-130 1,2-Dichloroethane ug/L ND 20 21.3 106 70-130 1,2-Dichloropropane ug/L ND 20 24.1 120 70-130 1,3-Dichlorobenzene ug/L ND 20 21.7 108 70-130 1,3-Dichloropropane ug/L ND 20 20.4 102 70-130 1,4-Dichlorobenzene ug/L ND 20 21.1 105 70-130 2,2-Dichloropropane ug/L ND 20 21.2 106 70-130 2-Butanone (MEK) ug/L ND 40 47.7J 119 70-130 2-Hexanone ug/L ND 40 40.9J 102 70-130 4-Methyl-2-pentanone (MIBK) ug/L ND 40 43.2J 108 70-130 Acetone ug/L 14AJ 40 93.5J 198 70-130 M1 Acetonitrile ug/L ND 200 219 110 70-130 Acrolein ug/L ND 100 117 117 70-130 Acrylonitrile ug/L ND 100 114J 114 70-130 Allyl chloride ug/L ND 20 26.8 134 70-130 M1 Benzene ug/L ND 20 23.4 117 70-148 Bromochloromethane ug/L ND 20 21.4 107 70-130 Bromodichloromethane ug/L ND 20 22.4 112 70-130 Bromoform ug/L ND 20 16.5 83 70-130 Bromomethane ug/L ND 20 19.8 99 70-130 Carbon disulfide ug/L ND 20 23AJ 117 70-130 Carbon tetrachloride ug/L ND 20 22.4 112 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 111 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 MATRIX SPIKE SAMPLE: Parameter 2014258 Units 92342478011 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers Chlorobenzene ug/L ND 20 22.1 110 70-146 Chloroethane ug/L ND 20 21.7 108 70-130 Chloroform ug/L ND 20 23.2 116 70-130 Chloromethane ug/L ND 20 25.8 129 70-130 Chloroprene ug/L ND 20 22.8 114 70-130 cis-1,2-Dichloroethene ug/L 0.64J 20 24.5 119 70-130 cis-1,3-Dichloropropene ug/L ND 20 23.4 117 70-130 Dibromochloromethane ug/L ND 20 18.4 92 70-130 Dibromomethane ug/L ND 20 21.7 108 70-130 Dichlorodifluoromethane ug/L ND 20 19.2 96 70-130 Ethyl methacrylate ug/L ND 20 19.4 97 70-130 Ethylbenzene ug/L ND 20 23.0 115 70-130 Hexachloro-1,3-butadiene ug/L ND 20 19.3 96 70-130 lodomethane ug/L ND 40 41.6 104 70-130 Isobutanol ug/L ND 400 419 105 70-130 Methacrylonitrile ug/L ND 200 230 115 70-130 Methyl methacrylate ug/L ND 20 19.7J 98 70-130 Methylene Chloride ug/L ND 20 23.2 116 70-130 Naphthalene ug/L ND 20 21.6 108 70-130 Propionitrile ug/L ND 200 243 121 70-130 Styrene ug/L ND 20 22.3 112 70-130 Tetrachloroethene ug/L ND 20 19.4 97 70-130 Toluene ug/L ND 20 22.7 113 70-155 trans-1,2-Dichloroethene ug/L ND 20 25.0 125 70-130 trans- 1,3-Dichloropropene ug/L ND 20 21.8 109 70-130 trans-1,4-Dichloro-2-butene ug/L ND 20 21.3J 106 70-130 Trichloroethene ug/L ND 20 23.8 119 69-151 Trichlorofluoromethane ug/L ND 20 22.1 111 70-130 Vinyl acetate ug/L ND 40 37.6J 94 70-130 Vinyl chloride ug/L ND 20 21.8 109 70-130 1,2-Dichloroethane-d4 (S) % 97 70-130 4-Bromofluorobenzene (S) % 109 70-130 Toluene-d8 (S) % 99 70-130 SAMPLE DUPLICATE: 2014257 92342478010 Dup Max Parameter Units Result Result RPD RPD Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND ND 30 1,1,1-Trichloroethane ug/L ND ND 30 1,1,2,2-Tetrachloroethane ug/L ND ND 30 1,1,2-Trichloroethane ug/L ND ND 30 1,1-Dichloroethane ug/L 0.36J 0.50J 30 1,1-Dichloroethene ug/L ND ND 30 1,1-Dichloropropene ug/L ND ND 30 1,2,3-Trichloropropane ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 112 of 166 Pace Analytical Services, LLC aceAnalXical� 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 SAMPLE DUPLICATE: 2014257 Parameter Units 92342478010 Result Dup Result RPD Max RPD Qualifiers 1,2,4-Trichlorobenzene ug/L ND ND 30 1,2-Dibromo-3-chloropropane ug/L ND ND 30 1,2-Dibromoethane (EDB) ug/L ND ND 30 1,2-Dichlorobenzene ug/L ND ND 30 1,2-Dichloroethane ug/L ND ND 30 1,2-Dichloropropane ug/L ND ND 30 1,3-Dichlorobenzene ug/L ND ND 30 1,3-Dichloropropane ug/L ND ND 30 1,4-Dichlorobenzene ug/L ND ND 30 2,2-Dichloropropane ug/L ND ND 30 2-Butanone (MEK) ug/L ND ND 30 2-Hexanone ug/L ND ND 30 4-Methyl-2-pentanone (MIBK) ug/L ND ND 30 Acetone ug/L ND ND 30 Acetonitrile ug/L ND ND 30 Acrolein ug/L ND ND 30 Acrylonitrile ug/L ND ND 30 Allyl chloride ug/L ND ND 30 Benzene ug/L ND ND 30 Bromochloromethane ug/L ND ND 30 Bromodichloromethane ug/L ND ND 30 Bromoform ug/L ND ND 30 Bromomethane ug/L ND ND 30 Carbon disulfide ug/L ND ND 30 Carbon tetrachloride ug/L ND ND 30 Chlorobenzene ug/L ND ND 30 Chloroethane ug/L ND ND 30 Chloroform ug/L ND ND 30 Chloromethane ug/L ND 0.29J 30 Chloroprene ug/L ND ND 30 cis-1,2-Dichloroethene ug/L 0.65J 0.88J 30 cis-1,3-Dichloropropene ug/L ND ND 30 Dibromochloromethane ug/L ND ND 30 Dibromomethane ug/L ND ND 30 Dichlorodifluoromethane ug/L ND ND 30 Ethyl methacrylate ug/L ND ND 30 Ethylbenzene ug/L ND ND 30 Hexachloro-1,3-butadiene ug/L ND ND 30 lodomethane ug/L ND ND 30 Isobutanol ug/L ND ND 30 Methacrylonitrile ug/L ND ND 30 Methyl methacrylate ug/L ND ND 30 Methylene Chloride ug/L ND ND 30 Naphthalene ug/L ND ND 30 Propionitrile ug/L ND ND 30 Styrene ug/L ND ND 30 Tetrachloroethene ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 113 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 SAMPLE DUPLICATE: 2014257 Parameter Units 92342478010 Result Dup Result Toluene ug/L ND ND trans-1,2-Dichloroethene ug/L ND ND trans- 1,3-Dichloropropene ug/L ND ND trans-1,4-Dichloro-2-butene ug/L ND ND Trichloroethene ug/L ND ND Trichlorofluoromethane ug/L ND ND Vinyl acetate ug/L ND ND Vinyl chloride ug/L ND ND Xylene (Total) ug/L ND ND 1,2-Dichloroethane-d4 (S) % 92 92 4-Bromofluorobenzene (S) % 103 105 Toluene-d8 (S) % 109 108 IVV 0 2 2 Max RPD 30 30 30 30 30 30 30 30 30 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. 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AIRY (UIC) Pace Project No.: 92342478 QC Batch: 363163 Analysis Method: EPA 8081 QC Batch Method: EPA 3510 Analysis Description: 8081A GCS Pesticides Associated Lab Samples: 92342478003, 92342530001, 92342530002, 92342530003, 92342530004, 92342530005 METHOD BLANK: 2013349 Matrix: Water Associated Lab Samples: 92342478003, 92342530001, 92342530002, 92342530003, 92342530004, 92342530005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 4,4'-DDD ug/L ND 0.10 0.050 06/06/17 20:06 4,4'-DDE ug/L ND 0.10 0.050 06/06/17 20:06 4,4'-DDT ug/L ND 0.10 0.050 06/06/17 20:06 Aldrin ug/L ND 0.050 0.050 06/06/17 20:06 alpha-BHC ug/L ND 0.050 0.050 06/06/17 20:06 beta-BHC ug/L ND 0.050 0.050 06/06/17 20:06 Chlordane (Technical) ug/L ND 0.50 0.20 06/06/17 20:06 delta-BHC ug/L ND 0.050 0.050 06/06/17 20:06 Dieldrin ug/L ND 0.075 0.050 06/06/17 20:06 Endosulfan I ug/L ND 0.10 0.050 06/06/17 20:06 Endosulfan II ug/L ND 0.10 0.050 06/06/17 20:06 Endosulfan sulfate ug/L ND 0.10 0.050 06/06/17 20:06 Endrin ug/L ND 0.10 0.050 06/06/17 20:06 Endrin aldehyde ug/L ND 0.10 0.050 06/06/17 20:06 gamma-BHC (Lindane) ug/L ND 0.050 0.050 06/06/17 20:06 Heptachlor ug/L ND 0.050 0.050 06/06/17 20:06 Heptachlor epoxide ug/L ND 0.075 0.050 06/06/17 20:06 Methoxychlor ug/L ND 1.0 0.15 06/06/17 20:06 Toxaphene ug/L ND 1.5 0.20 06/06/17 20:06 Decachlorobiphenyl (S) % 95 20-130 06/06/17 20:06 Tetrachloro-m-xylene (S) % 80 20-130 06/06/17 20:06 LABORATORY CONTROL SAMPLE: Parameter 2013350 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 4,4'-DDD ug/L .25 0.24 98 20-150 4,4'-DDE ug/L .25 0.22 89 20-150 4,4'-DDT ug/L .25 0.26 105 20-150 Aldrin ug/L .25 0.18 73 20-150 alpha-BHC ug/L .25 0.20 79 20-150 beta-BHC ug/L .25 0.19 78 20-150 delta-BHC ug/L .25 0.23 92 20-150 Dieldrin ug/L .25 0.23 91 20-150 Endosulfan I ug/L .25 0.23 92 20-150 Endosulfan II ug/L .25 0.24 99 20-150 Endosulfan sulfate ug/L .25 0.26 105 20-150 Endrin ug/L .25 0.25 100 20-150 Endrin aldehyde ug/L .25 0.23 94 20-150 gamma-BHC (Lindane) ug/L .25 0.22 88 20-150 Heptachlor ug/L .25 0.18 75 20-150 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 115 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 LABORATORY CONTROL SAMPLE: 2013350 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Heptachlor epoxide ug/L .25 0.21 83 20-150 Methoxychlor ug/L .74 0.76J 102 20-150 Decachlorobiphenyl (S) % 86 20-130 Tetrachloro-m-xylene (S) % 54 20-130 MATRIX SPIKE SAMPLE: 2013351 92342479004 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 4,4'-DDD ug/L ND .25 0.22 89 20-150 4,4'-DDE ug/L ND .25 0.21 84 20-150 4,4'-DDT ug/L ND .25 0.24 98 20-150 Aldrin ug/L ND .25 0.18 71 20-150 alpha-BHC ug/L ND .25 0.19 77 20-150 beta-BHC ug/L ND .25 0.17 69 20-150 delta-BHC ug/L ND .25 0.21 84 20-150 Dieldrin ug/L ND .25 0.21 84 20-150 Endosulfan I ug/L ND .25 0.21 87 20-150 Endosulfan II ug/L ND .25 0.23 91 20-150 Endosulfan sulfate ug/L ND .25 0.25 99 20-150 Endrin ug/L ND .25 0.23 93 20-150 Endrin aldehyde ug/L ND .25 0.23 95 20-150 gamma-BHC (Lindane) ug/L ND .25 0.20 81 20-150 Heptachlor ug/L ND .25 0.18 74 20-150 Heptachlor epoxide ug/L ND .25 0.20 83 20-150 Methoxychlor ug/L ND .74 0.70J 94 20-150 Decachlorobiphenyl (S) % 47 20-130 Tetrachloro-m-xylene (S) % 76 20-130 SAMPLE DUPLICATE: 2013352 92342479005 Dup Max Parameter Units Result Result RPD RPD Qualifiers 4,4'-DDD ug/L ND ND 30 4,4'-DDE ug/L ND ND 30 4,4'-DDT ug/L ND ND 30 Aldrin ug/L ND ND 30 alpha-BHC ug/L ND ND 30 beta-BHC ug/L ND ND 30 Chlordane (Technical) ug/L ND ND 30 delta-BHC ug/L ND ND 30 Dieldrin ug/L ND ND 30 Endosulfan I ug/L ND ND 30 Endosulfan II ug/L ND ND 30 Endosulfan sulfate ug/L ND ND 30 Endrin ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 116 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 SAMPLE DUPLICATE: 2013352 Parameter Endrin aldehyde gamma-BHC (Lindane) Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) QUALITY CONTROL DATA Units 92342479005 Result Dup Result ug/L ND ND ug/L ND ND ug/L ND ND ug/L ND ND ug/L ND ND ug/L ND ND % 84 68 101 87 lVV 21 15 Max RPD 30 30 30 30 30 30 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 117 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 QC Batch: 363426 Analysis Method: EPA 8081 QC Batch Method: EPA 3510 Analysis Description: 8081A GCS Pesticides Associated Lab Samples: 92342478004, 92342478005 METHOD BLANK: 2014786 Associated Lab Samples: 92342478004, 92342478005 Parameter Units 4,4'-DDD ug/L 4,4'-DDE ug/L 4,4'-DDT ug/L Aldrin ug/L alpha-BHC ug/L beta-BHC ug/L Chlordane (Technical) ug/L delta-BHC ug/L Dieldrin ug/L Endosulfan I ug/L Endosulfan II ug/L Endosulfan sulfate ug/L Endrin ug/L Endrin aldehyde ug/L gamma-BHC (Lindane) ug/L Heptachlor ug/L Heptachlor epoxide ug/L Methoxychlor ug/L Toxaphene ug/L Decachlorobiphenyl (S) % Tetrachloro-m-xylene (S) % Matrix: Water Blank Result Reporting Limit MDL Analyzed ND 0.10 0.050 06/06/1713:28 ND 0.10 0.050 06/06/1713:28 ND 0.10 0.050 06/06/1713:28 ND 0.050 0.050 06/06/1713:28 ND 0.050 0.050 06/06/1713:28 ND 0.050 0.050 06/06/1713:28 ND 0.50 0.20 06/06/1713:28 ND 0.050 0.050 06/06/1713:28 ND 0.075 0.050 06/06/1713:28 ND 0.10 0.050 06/06/1713:28 ND 0.10 0.050 06/06/1713:28 ND 0.10 0.050 06/06/1713:28 ND 0.10 0.050 06/06/1713:28 ND 0.10 0.050 06/06/1713:28 ND 0.050 0.050 06/06/1713:28 ND 0.050 0.050 06/06/1713:28 ND 0.075 0.050 06/06/1713:28 ND 1.0 0.15 06/06/1713:28 ND 1.5 0.20 06/06/1713:28 78 20-130 06/06/1713:28 51 20-130 06/06/17 13:28 Qualifiers LABORATORY CONTROL SAMPLE & LCSD: 2014787 2014788 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers 4,4'-DDD ug/L .25 0.22 0.23 90 92 20-150 2 30 4,4'-DDE ug/L .25 0.21 0.20 84 79 20-150 7 30 4,4'-DDT ug/L .25 0.23 0.24 94 95 20-150 1 30 Aldrin ug/L .25 0.16 0.15 64 60 20-150 8 30 alpha-BHC ug/L .25 0.19 0.19 79 78 20-150 1 30 beta-BHC ug/L .25 0.17 0.19 70 75 20-150 7 30 delta-BHC ug/L .25 0.21 0.20 84 79 20-150 7 30 Dieldrin ug/L .25 0.21 0.21 86 83 20-150 3 30 Endosulfan I ug/L .25 0.22 0.21 87 84 20-150 3 30 Endosulfan II ug/L .25 0.23 0.22 91 90 20-150 1 30 Endosulfan sulfate ug/L .25 0.24 0.24 97 97 20-150 0 30 Endrin ug/L .25 0.23 0.23 93 93 20-150 0 30 Endrin aldehyde ug/L .25 0.21 0.22 87 89 20-150 3 30 gamma-BHC (Lindane) ug/L .25 0.21 0.21 83 85 20-150 2 30 Heptachlor ug/L .25 0.17 0.15 68 62 20-150 9 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 118 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 LABORATORY CONTROL SAMPLE & LCSD: 2014787 2014788 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Heptachlor epoxide ug/L .25 0.20 0.17 82 70 20-150 16 30 Methoxychlor ug/L .74 0.72J 0.72J 97 97 20-150 1 30 Decachlorobiphenyl (S) % 78 64 20-130 Tetrachloro-m-xylene (S) % 81 69 20-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. 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AIRY (UIC) Pace Project No.: 92342478 QC Batch: 363162 Analysis Method: EPA 8082 QC Batch Method: EPA 3510 Analysis Description: 8082 GCS PCB Associated Lab Samples: 92342478003, 92342530001, 92342530002, 92342530003, 92342530004, 92342530005 METHOD BLANK: 2013345 Matrix: Water Associated Lab Samples: 92342478003, 92342530001, 92342530002, 92342530003, 92342530004, 92342530005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers PCB-1016 (Aroclor 1016) ug/L ND 0.50 0.50 06/03/17 13:25 PCB-1221 (Aroclor 1221) ug/L ND 0.50 0.50 06/03/17 13:25 PCB-1232 (Aroclor 1232) ug/L ND 0.50 0.50 06/03/17 13:25 PCB-1242 (Aroclor 1242) ug/L ND 0.50 0.50 06/03/17 13:25 PCB-1248 (Aroclor 1248) ug/L ND 0.50 0.50 06/03/17 13:25 PCB-1254 (Aroclor 1254) ug/L ND 0.50 0.50 06/03/17 13:25 PCB-1260 (Aroclor 1260) ug/L ND 0.50 0.50 06/03/17 13:25 Decachlorobiphenyl (S) % 93 10-132 06/03/17 13:25 LABORATORY CONTROL SAMPLE: 2013346 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers PCB-1016 (Aroclor 1016) ug/L 2.5 1.9 76 50-150 PCB-1260 (Aroclor 1260) ug/L 2.5 2.3 91 50-150 Decachlorobiphenyl (S) % 64 10-132 MATRIX SPIKE SAMPLE: 2013347 92342530001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers PCB-1016 (Aroclor 1016) ug/L ND 2.5 1.5 61 50-150 PCB-1260 (Aroclor 1260) ug/L ND 2.5 1.4 55 50-150 Decachlorobiphenyl (S) % 32 10-132 SAMPLE DUPLICATE: 2013348 92342530003 Dup Max Parameter Units Result Result RPD RPD Qualifiers PCB-1016 (Aroclor 1016) ug/L ND ND 30 PCB-1221 (Aroclor 1221) ug/L ND ND 30 PCB-1232 (Aroclor 1232) ug/L ND ND 30 PCB-1242 (Aroclor 1242) ug/L ND ND 30 PCB-1248 (Aroclor 1248) ug/L ND ND 30 PCB-1254 (Aroclor 1254) ug/L ND ND 30 PCB-1260 (Aroclor 1260) ug/L ND ND 30 Decachlorobiphenyl (S) % 77 59 27 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 120 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 QC Batch: 363427 Analysis Method: EPA 8082 QC Batch Method: EPA 3510 Analysis Description: 8082 GCS PCB Associated Lab Samples: 92342478004, 92342478005 METHOD BLANK: 2014798 Matrix: Water Associated Lab Samples: 92342478004, 92342478005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers PCB-1016 (Aroclor 1016) ug/L ND 0.50 0.50 06/06/17 20:10 PCB-1221 (Aroclor 1221) ug/L ND 0.50 0.50 06/06/17 20:10 PCB-1232 (Aroclor 1232) ug/L ND 0.50 0.50 06/06/17 20:10 PCB-1242 (Aroclor 1242) ug/L ND 0.50 0.50 06/06/17 20:10 PCB-1248 (Aroclor 1248) ug/L ND 0.50 0.50 06/06/17 20:10 PCB-1254 (Aroclor 1254) ug/L ND 0.50 0.50 06/06/17 20:10 PCB-1260 (Aroclor 1260) ug/L ND 0.50 0.50 06/06/17 20:10 Decachlorobiphenyl (S) % 75 10-132 06/06/17 20:10 LABORATORY CONTROL SAMPLE & LCSD: 2014799 2014800 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers PCB-1016 (Aroclor 1016) ug/L 5 3.3 3.5 66 69 50-150 5 30 PCB-1260 (Aroclor 1260) ug/L 5 3.2 3.0 63 60 50-150 5 30 Decachlorobiphenyl (S) % 34 37 10-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 121 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 QC Batch: 372315 Analysis Method: EPA 8151 QC Batch Method: EPA 8151 Analysis Description: 8151A GCS Herbicides Associated Lab Samples: 92342478003 METHOD BLANK: 2012657 Matrix: Water Associated Lab Samples: 92342478003 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 2,4,5-T ug/L ND 0.19 0.042 06/06/17 01:19 2,4,5-TP (Silvex) ug/L ND 0.19 0.049 06/06/17 01:19 2,4-D ug/L ND 0.94 0.22 06/06/17 01:19 Dinoseb ug/L ND 0.19 0.057 06/06/17 01:19 Pentachlorophenol ug/L ND 0.028 0.017 06/06/17 01:19 2,4-DCAA (S) % 94 39-139 06/06/17 01:19 LABORATORY CONTROL SAMPLE & LCSD: 2012658 2013105 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers 2,4,5-T ug/L 1.2 1.2 1.2 100 97 37-133 3 40 2,4,5-TP (Silvex) ug/L 1.2 1.1 1.2 92 97 53-134 5 40 2,4-D ug/L 6 5.5 5.7 91 95 35-124 5 40 Dinoseb ug/L 1.2 0.89 1.0 74 83 13-116 12 40 Pentachlorophenol ug/L .18 0.22 0.22 122 124 39-170 2 40 2,4-DCAA (S) % 83 85 39-139 40 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 122 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 QC Batch: 373221 Analysis Method: EPA 8151 QC Batch Method: EPA 8151 Analysis Description: 8151A GCS Herbicides Associated Lab Samples: 92342478004,92342478005,92342530001,92342530002,92342530003,92342530004,92342530005 METHOD BLANK: 2017562 Matrix: Water Associated Lab Samples: 92342478004, 92342478005, 92342530001, 92342530002, 92342530003, 92342530004, 92342530005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 2,4,5-T ug/L ND 0.19 0.042 06/09/17 20:42 2,4,5-TP (Silvex) ug/L ND 0.19 0.049 06/09/17 20:42 2,4-D ug/L ND 0.94 0.22 06/09/17 20:42 Dinoseb ug/L ND 0.19 0.057 06/09/17 20:42 Pentachlorophenol ug/L ND 0.028 0.017 06/09/17 20:42 2,4-DCAA (S) % 74 39-139 06/09/17 20:42 LABORATORY CONTROL SAMPLE: 2017563 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 2,4,5-T ug/L 1.2 1.3 109 37-133 2,4,5-TP (Silvex) ug/L 1.2 1.3 110 53-134 2,4-D ug/L 6 5.5 91 35-124 Dinoseb ug/L 1.2 1.2 99 13-116 Pentachlorophenol ug/L .18 0.17 94 39-170 2,4-DCAA (S) % 85 39-139 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2018719 2018720 MS MSD 35316294004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 2,4,5-T ug/L 0.043U 1.2 1.4 1.2 1.2 100 90 37-133 3 40 2,4,5-TP (Silvex) ug/L 0.050U 1.2 1.4 1.2 1.2 97 88 53-134 2 40 2,4-D ug/L 0.23U 6 6.8 5.1 5.2 84 76 35-124 3 40 Dinoseb ug/L 0.058U 1.2 1.4 1.1 0.98 91 72 13-116 11 40 Pentachlorophenol ug/L 0.017U .18 .2 0.15 0.057 82 28 39-170 89 40 M1,R1 2,4-DCAA (S) % 69 85 39-139 40 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 123 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 QC Batch: 363842 Analysis Method: EPA 8270 QC Batch Method: EPA 3510 Analysis Description: 8270 Water MSSV Associated Lab Samples: 92342478003 METHOD BLANK: 2017031 Associated Lab Samples: 92342478003 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed 1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 1.3 06/13/17 11:37 1,3,5-Trinitrobenzene ug/L ND 10.0 1.2 06/13/17 11:37 1,3-Dinitrobenzene ug/L ND 20.0 1.3 06/13/17 11:37 1,4-Naphthoquinone ug/L ND 10.0 0.99 06/13/17 11:37 1-Naphthalenamine ug/L ND 10.0 1.3 06/13/17 11:37 2,2'-Oxybis(1-chloropropane) ug/L ND 10.0 1.8 06/13/17 11:37 2,3,4,6-Tetrachlorophenol ug/L ND 10.0 2.9 06/13/17 11:37 2,4,5-Trichlorophenol ug/L ND 10.0 1.5 06/13/17 11:37 2,4,6-Trichlorophenol ug/L ND 10.0 1.4 06/13/17 11:37 2,4-Dichlorophenol ug/L ND 10.0 1.6 06/13/17 11:37 2,4-Dimethylphenol ug/L ND 10.0 1.6 06/13/17 11:37 2,4-Dinitrophenol ug/L ND 50.0 5.1 06/13/17 11:37 2,4-Dinitrotoluene ug/L ND 10.0 1.5 06/13/17 11:37 2,6-Dichlorophenol ug/L ND 10.0 1.5 06/13/17 11:37 2,6-Dinitrotoluene ug/L ND 10.0 1.4 06/13/17 11:37 2-Acetylaminofluorene ug/L ND 20.0 1.6 06/13/17 11:37 2-Chloronaphthalene ug/L ND 10.0 1.6 06/13/17 11:37 2-Chlorophenol ug/L ND 10.0 1.5 06/13/17 11:37 2-Methylnaphthalene ug/L ND 10.0 1.4 06/13/17 11:37 2-Methylphenol(o-Cresol) ug/L ND 10.0 1.6 06/13/17 11:37 2-Naphthalenamine ug/L ND 10.0 2.2 06/13/17 11:37 2-Nitroaniline ug/L ND 50.0 2.3 06/13/17 11:37 2-Nitrophenol ug/L ND 10.0 1.6 06/13/17 11:37 3&4-Methyl phenol (m&p Cresol) ug/L ND 10.0 1.4 06/13/17 11:37 3,3'-Dichlorobenzidine ug/L ND 20.0 3.9 06/13/17 11:37 3,3'-Dimethylbenzidine ug/L ND 10.0 3.9 06/13/17 11:37 3-Methylcholanthrene ug/L ND 10.0 2.7 06/13/17 11:37 3-Nitroaniline ug/L ND 50.0 2.7 06/13/17 11:37 4,6-Dinitro-2-methyl phenol ug/L ND 50.0 2.2 06/13/17 11:37 4-Aminobiphenyl ug/L ND 20.0 1.7 06/13/17 11:37 4-Bromophenylphenyl ether ug/L ND 10.0 1.5 06/13/17 11:37 4-ChIoro-3-methyl phenol ug/L ND 20.0 2.8 06/13/17 11:37 4-Chloroaniline ug/L ND 20.0 2.8 06/13/17 11:37 4-Chlorophenylphenyl ether ug/L ND 10.0 1.6 06/13/17 11:37 4-Nitroaniline ug/L ND 20.0 3.4 06/13/17 11:37 4-Nitrophenol ug/L ND 50.0 4.3 06/13/17 11:37 5-Nitro-o-toluidine ug/L ND 10.0 1.9 06/13/17 11:37 7,12-Dimethylbenz(a)anthracene ug/L ND 10.0 2.4 06/13/17 11:37 Acenaphthene ug/L ND 10.0 1.6 06/13/17 11:37 Acenaphthylene ug/L ND 10.0 1.5 06/13/17 11:37 Acetophenone ug/L ND 10.0 1.9 06/13/17 11:37 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 124 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 METHOD BLANK: 2017031 Associated Lab Samples: 92342478003 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Anthracene ug/L ND 10.0 1.7 06/13/17 11:37 Benzo(a)anthracene ug/L ND 10.0 2.1 06/13/17 11:37 Benzo(a)pyrene ug/L ND 10.0 2.2 06/13/17 11:37 Benzo(b)fluoranthene ug/L ND 10.0 2.2 06/13/17 11:37 Benzo(g,h,i)perylene ug/L ND 10.0 2.1 06/13/17 11:37 Benzo(k)fluoranthene ug/L ND 10.0 2.0 06/13/17 11:37 Benzyl alcohol ug/L ND 20.0 3.1 06/13/17 11:37 bis(2-Chloroethoxy)methane ug/L ND 10.0 1.6 06/13/17 11:37 bis(2-Chloroethyl) ether ug/L ND 10.0 1.7 06/13/17 11:37 bis(2-Ethylhexyl)phthalate ug/L ND 15.0 2.3 06/13/17 11:37 Butylbenzylphthalate ug/L ND 10.0 2.5 06/13/17 11:37 Chlorobenzilate ug/L ND 10.0 2.2 06/13/17 11:37 Chrysene ug/L ND 10.0 2.1 06/13/17 11:37 Di-n-butylphthalate ug/L ND 10.0 2.0 06/13/17 11:37 Di-n-octylphthalate ug/L ND 10.0 1.5 06/13/17 11:37 Diallate ug/L ND 10.0 1.6 06/13/17 11:37 Dibenz(a,h)anthracene ug/L ND 10.0 2.0 06/13/17 11:37 Dibenzofuran ug/L ND 10.0 1.7 06/13/17 11:37 Diethylphthalate ug/L ND 6000 1.6 06/13/17 11:37 Dimethoate ug/L ND 20.0 1.8 06/13/17 11:37 Dimethylphthalate ug/L ND 10.0 1.4 06/13/17 11:37 Diphenylamine ug/L ND 10.0 1.4 06/13/17 11:37 Disulfoton ug/L ND 10.0 1.5 06/13/17 11:37 Ethyl methanesulfonate ug/L ND 20.0 1.6 06/13/17 11:37 Famphur ug/L ND 20.0 5.7 06/13/17 11:37 Fluoranthene ug/L ND 10.0 2.2 06/13/17 11:37 Fluorene ug/L ND 10.0 1.6 06/13/17 11:37 Hexachlorobenzene ug/L ND 10.0 1.7 06/13/17 11:37 Hexachlorocyclopentadiene ug/L ND 10.0 1.3 06/13/17 11:37 Hexachloroethane ug/L ND 10.0 1.8 06/13/17 11:37 Hexachloropropene ug/L ND 10.0 1.2 06/13/17 11:37 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 2.0 06/13/17 11:37 Isodrin ug/L ND 20.0 2.5 06/13/17 11:37 Isophorone ug/L ND 10.0 1.5 06/13/17 11:37 Isosafrole ug/L ND 10.0 1.5 06/13/17 11:37 Kepone ug/L ND 20.0 4.5 06/13/17 11:37 Methapyrilene ug/L ND 100 3.0 06/13/17 11:37 Methyl methanesulfonate ug/L ND 10.0 1.1 06/13/17 11:37 Methyl parathion ug/L ND 10.0 1.6 06/13/17 11:37 N-Nitroso-di-n-butylamine ug/L ND 10.0 1.6 06/13/17 11:37 N-Nitroso-di-n-propylamine ug/L ND 10.0 1.7 06/13/17 11:37 N-Nitrosodiethylamine ug/L ND 20.0 1.4 06/13/17 11:37 N-Nitrosodimethylamine ug/L ND 10.0 1.6 06/13/17 11:37 N-Nitrosodiphenylamine ug/L ND 10.0 1.4 06/13/17 11:37 N-Nitrosomethylethylamine ug/L ND 10.0 1.4 06/13/17 11:37 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 125 of 166 Pace Analytical Services, LLC aceAnalXical� 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 METHOD BLANK: 2017031 Associated Lab Samples: 92342478003 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Qualifiers N-Nitrosopiperidine ug/L ND 20.0 1.7 06/13/17 11:37 N-Nitrosopyrrolidine ug/L ND 10.0 1.7 06/13/17 11:37 Nitrobenzene ug/L ND 10.0 1.6 06/13/17 11:37 O,O,O-Triethylphosphorothioate ug/L ND 10.0 1.7 06/13/17 11:37 O-Toluidine ug/L ND 10.0 1.7 06/13/17 11:37 P-Dimethylaminoazobenzene ug/L ND 10.0 1.0 06/13/17 11:37 p-Phenylenediamine ug/L ND 10.0 2.2 06/13/17 11:37 Parathion (Ethyl parathion) ug/L ND 10.0 1.5 06/13/17 11:37 Pentachlorobenzene ug/L ND 10.0 1.5 06/13/17 11:37 Pentachloronitrobenzene ug/L ND 20.0 1.7 06/13/17 11:37 Pentachlorophenol ug/L ND 25.0 3.5 06/13/17 11:37 Phenacetin ug/L ND 20.0 1.9 06/13/17 11:37 Phenanthrene ug/L ND 10.0 1.6 06/13/17 11:37 Phenol ug/L ND 10.0 1.3 06/13/17 11:37 Phorate ug/L ND 10.0 1.7 06/13/17 11:37 Pronamide ug/L ND 10.0 2.0 06/13/17 11:37 Pyrene ug/L ND 10.0 2.2 06/13/17 11:37 Safrole ug/L ND 10.0 1.3 06/13/17 11:37 Thionazin ug/L ND 20.0 1.7 06/13/17 11:37 2,4,6-Tribromophenol (S) % 76 27-110 06/13/17 11:37 2-Fluorobiphenyl (S) % 85 27-110 06/13/17 11:37 2-Fluorophenol (S) % 41 12-110 06/13/17 11:37 Nitrobenzene-d5 (S) % 69 21-110 06/13/17 11:37 Phenol-d6 (S) % 27 10-110 06/13/17 11:37 Terphenyl-d14 (S) % 90 31-107 06/13/17 11:37 LABORATORY CONTROL SAMPLE: Parameter 2017032 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,2,4,5-Tetrachlorobenzene ug/L 50 11.9 24 16-129 1,3,5-Trinitrobenzene ug/L 50 26.1 52 55-125 L2 1,3-Dinitrobenzene ug/L 50 31.8 64 30-122 1,4-Naphthoquinone ug/L 50 29.2 58 31-120 1-Naphthalenamine ug/L 50 21.4 43 37-126 2,2'-Oxybis(1-chloropropane) ug/L 50 16.9 34 18-120 2,3,4,6-Tetrachlorophenol ug/L 50 62.9 126 54-276 2,4,5-Trichlorophenol ug/L 50 28.1 56 43-113 2,4,6-Trichlorophenol ug/L 50 28.0 56 42-120 2,4-Dichlorophenol ug/L 50 14.4 29 30-120 L2 2,4-Dimethylphenol ug/L 50 12.6 25 29-111 L2 2,4-Dinitrophenol ug/L 250 170 68 19-132 2,4-Dinitrotoluene ug/L 50 35.5 71 58-128 2,6-Dichlorophenol ug/L 50 13.0 26 54-128 L2 2,6-Dinitrotoluene ug/L 50 34.8 70 54-129 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 126 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 LABORATORY CONTROL SAMPLE: Parameter 2017032 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2-Acetylaminofluorene ug/L 50 27.9 56 81-160 L2 2-Chloronaphthalene ug/L 50 20.7 41 43-117 L2 2-Chlorophenol ug/L 50 12.6 25 37-120 L2 2-Methylnaphthalene ug/L 50 12.5 25 33-120 L2 2-Methylphenol(o-Cresol) ug/L 50 9.8J 20 31-120 L2 2-Naphthalenamine ug/L 50 26.8 54 41-136 2-Nitroaniline ug/L 100 68.2 68 48-121 2-Nitrophenol ug/L 50 11.3 23 25-116 L2 3&4-Methyl phenol (m&p Cresol) ug/L 50 7.8J 16 23-120 L2 3,3'-Dichlorobenzidine ug/L 250 66.9 27 10-154 3,3'-Dimethylbenzidine ug/L 100 37.3 37 10-157 3-Methylcholanthrene ug/L 50 37.2 74 65-130 3-Nitroaniline ug/L 100 82.7 83 43-115 4,6-Dinitro-2-methyl phenol ug/L 100 63.9 64 44-124 4-Aminobiphenyl ug/L 50 25.6 51 21-125 4-Bromophenylphenyl ether ug/L 50 26.9 54 34-113 4-ChIoro-3-methyl phenol ug/L 100 44.0 44 31-110 4-Chloroaniline ug/L 100 33.6 34 20-120 4-Chlorophenylphenyl ether ug/L 50 28.0 56 34-116 4-Nitroaniline ug/L 100 89.4 89 46-128 4-Nitrophenol ug/L 250 64.6 26 11-120 5-Nitro-o-toluidine ug/L 50 36.3 73 78-160 L2 7,12-Dimethylbenz(a)anthracene ug/L 50 37.6 75 47-124 Acenaphthene ug/L 50 26.4 53 48-114 Acenaphthylene ug/L 50 26.4 53 48-112 Acetophenone ug/L 50 12.6 25 24-120 Anthracene ug/L 50 35.0 70 57-118 Benzo(a)anthracene ug/L 50 33.0 66 56-121 Benzo(a)pyrene ug/L 50 37.1 74 55-127 Benzo(b)fluoranthene ug/L 50 39.8 80 53-128 Benzo(g,h,i)perylene ug/L 50 33.5 67 54-125 Benzo(k)fluoranthene ug/L 50 38.9 78 51-123 Benzyl alcohol ug/L 100 21.4 21 27-120 L2 bis(2-Chloroethoxy)methane ug/L 50 10.4 21 32-120 L2 bis(2-Chloroethyl) ether ug/L 50 11.0 22 33-111 L2 bis(2-Ethylhexyl)phthalate ug/L 50 34.7 69 50-145 Butylbenzylphthalate ug/L 50 35.8 72 54-138 Chlorobenzilate ug/L 50 33.9 68 65-132 Chrysene ug/L 50 33.0 66 58-127 Di-n-butylphthalate ug/L 50 38.4 77 56-125 Di-n-octylphthalate ug/L 50 31.1 62 50-134 Diallate ug/L 50 26.7 53 47-123 Dibenz(a,h)anthracene ug/L 50 36.2 72 53-129 Dibenzofuran ug/L 50 29.7 59 45-120 Diethylphthalate ug/L 50 38.5J 77 53-120 Dimethoate ug/L 50 34.3 69 57-139 Dimethylphthalate ug/L 50 38.4 77 55-116 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 127 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 LABORATORY CONTROL SAMPLE: Parameter 2017032 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Diphenylamine ug/L 50 35.3 71 42-120 Disulfoton ug/L 50 26.7 53 49-156 Ethyl methanesulfonate ug/L 50 9.5J 19 43-120 L2 Famphur ug/L 100 122 122 40-160 Fluoranthene ug/L 50 35.7 71 57-125 Fluorene ug/L 50 32.5 65 53-118 Hexachlorobenzene ug/L 50 31.5 63 49-116 Hexachlorocyclopentadiene ug/L 50 9.5J 19 26-158 L2 Hexachloroethane ug/L 50 8.3J 17 30-114 L2 Hexachloropropene ug/L 50 7.OJ 14 13-137 Indeno(1,2,3-cd)pyrene ug/L 50 35.2 70 55-128 Isodrin ug/L 50 34.4 69 68-129 Isophorone ug/L 50 13.3 27 31-118 L2 Isosafrole ug/L 50 19.0 38 48-107 L2 Kepone ug/L 100 69.7 70 10-124 Methapyrilene ug/L 50 22AJ 45 40-160 Methyl methanesulfonate ug/L 50 15.9 32 25-114 Methyl parathion ug/L 50 33.7 67 58-137 N-Nitroso-di-n-butylamine ug/L 50 15.0 30 36-115 L2 N-Nitroso-di-n-propylamine ug/L 50 12.8 26 32-119 L2 N-Nitrosodiethylamine ug/L 50 10.91 22 47-115 L2 N-Nitrosodimethylamine ug/L 50 8.7J 17 13-120 N-Nitrosodiphenylamine ug/L 50 35.3 71 43-120 N-Nitrosomethylethylamine ug/L 50 9.7J 19 39-120 L2 N-Nitrosopiperidine ug/L 50 12.1J 24 43-113 L2 N-Nitrosopyrrolidine ug/L 50 12.5 25 32-110 L2 Nitrobenzene ug/L 50 10.8 22 33-110 L2 O,O,O-Triethylphosphorothioate ug/L 50 10.6 21 51-127 L2 O-Toluidine ug/L 50 10.0 20 27-120 L2 P-Dimethylaminoazobenzene ug/L 100 13.5 13 10-120 p-Phenylenediamine ug/L 50 25.7 51 72-143 L2 Parathion (Ethyl parathion) ug/L 50 27.4 55 56-140 L2 Pentachlorobenzene ug/L 50 25.0 50 30-137 Pentachloronitrobenzene ug/L 50 37.1 74 70-124 Pentachlorophenol ug/L 250 70.3 28 10-137 Phenacetin ug/L 50 29.9 60 60-130 Phenanthrene ug/L 50 35.3 71 57-117 Phenol ug/L 50 5.6J 11 10-120 Phorate ug/L 50 26.1 52 55-126 L2 Pronamide ug/L 50 33.2 66 75-124 L2 Pyrene ug/L 50 37.0 74 55-122 Safrole ug/L 50 11.8 24 41-120 L2 Thionazin ug/L 50 29.4 59 63-137 L2 2,4,6-Tribromophenol (S) % 69 27-110 2-Fluorobiphenyl (S) % 37 27-110 2-Fluorophenol(S) % 15 12-110 Nitrobenzene-d5(S) % 23 21-110 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 128 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 LABORATORY CONTROL SAMPLE: 2017032 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phenol-d6 (S) % 10 10-110 Terphenyl-d14 (S) % 72 31-107 MATRIX SPIKE SAMPLE: 2017033 92342479002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,2,4,5-Tetrachlorobenzene ug/L ND 50 32.2 64 50-150 1,3,5-Trinitrobenzene ug/L ND 50 30.0 60 50-150 1,3-Dinitrobenzene ug/L ND 50 38.3 77 50-150 1,4-Naphthoquinone ug/L ND 50 49.0 98 50-150 1-Naphthalenamine ug/L ND 50 19.0 38 50-150 M1 2,2'-Oxybis(1-chloropropane) ug/L ND 50 53.8 108 50-150 2,3,4,6-Tetrachlorophenol ug/L ND 50 75.8 152 50-150 M1 2,4,5-Trichlorophenol ug/L ND 50 39.7 79 19-105 2,4,6-Trichlorophenol ug/L ND 50 46.5 93 13-108 2,4-Dichlorophenol ug/L ND 50 39.0 78 29-111 2,4-Dimethylphenol ug/L ND 50 36.9 74 21-103 2,4-Dinitrophenol ug/L ND 250 223 89 10-109 2,4-Dinitrotoluene ug/L ND 50 41.4 83 27-104 2,6-Dichlorophenol ug/L ND 50 40.3 81 50-150 2,6-Dinitrotoluene ug/L ND 50 43.6 87 28-101 2-Acetylaminofluorene ug/L ND 50 30.1 60 50-150 2-Chloronaphthalene ug/L ND 50 46.6 93 14-102 2-Chlorophenol ug/L ND 50 37.5 75 16-110 2-Methylnaphthalene ug/L ND 50 34.5 69 13-110 2-Methylphenol(o-Cresol) ug/L ND 50 32.6 65 19-110 2-Naphthalenamine ug/L ND 50 8.3J 17 50-150 M1 2-Nitroaniline ug/L ND 100 88.7 89 26-103 2-Nitrophenol ug/L ND 50 37.5 75 20-110 3&4-Methyl phenol (m&p Cresol) ug/L ND 50 28.3 57 20-110 3,3'-Dichlorobenzidine ug/L ND 250 61.8 25 25-112 3,3'-Dimethylbenzidine ug/L ND 100 7.8J 8 50-150 M1 3-Methylcholanthrene ug/L ND 50 38.4 76 50-150 3-Nitroaniline ug/L ND 100 97.2 97 29-110 4,6-Dinitro-2-methyl phenol ug/L ND 100 77.9 78 10-117 4-Aminobiphenyl ug/L ND 50 21.1 42 50-150 M1 4-Bromophenylphenyl ether ug/L ND 50 32.3 65 20-105 4-ChIoro-3-methyl phenol ug/L ND 100 67.6 68 22-110 4-Chloroaniline ug/L ND 100 74.3 74 20-100 4-Chlorophenylphenyl ether ug/L ND 50 39.1 78 19-102 4-Nitroaniline ug/L ND 100 105 105 29-110 4-Nitrophenol ug/L ND 250 77.4 31 10-110 5-Nitro-o-toluidine ug/L ND 50 41.8 84 50-150 7,12-Dimethylbenz(a)anthracene ug/L ND 50 41.0 81 50-150 Acenaphthene ug/L ND 50 44.6 89 17-100 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 129 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 MATRIX SPIKE SAMPLE: 2017033 92342479002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Acenaphthylene ug/L ND 50 45.8 92 21-100 Acetophenone ug/L ND 50 40.0 80 50-150 Anthracene ug/L ND 50 40.1 80 24-109 Benzo(a)anthracene ug/L ND 50 35.4 71 22-117 Benzo(a)pyrene ug/L ND 50 40.4 81 23-104 Benzo(b)fluoranthene ug/L ND 50 45.1 90 23-103 Benzo(g,h,i)perylene ug/L ND 50 37.7 75 18-111 Benzo(k)fluoranthene ug/L ND 50 41.3 83 22-113 Benzyl alcohol ug/L ND 100 66.1 66 19-101 bis(2-Chloroethoxy)methane ug/L ND 50 32.1 64 22-110 bis(2-Chloroethyl) ether ug/L ND 50 33.2 66 16-110 bis(2-Ethylhexyl)phthalate ug/L ND 50 35.4 71 23-102 Butylbenzylphthalate ug/L ND 50 36.7 73 25-110 Chlorobenzilate ug/L ND 50 34.4 68 50-150 Chrysene ug/L ND 50 35.4 71 23-115 Di-n-butylphthalate ug/L ND 50 42.4 85 26-110 Di-n-octylphthalate ug/L ND 50 33.7 67 22-110 Diallate ug/L ND 50 31.3 63 50-150 Dibenz(a,h)anthracene ug/L ND 50 40.0 80 21-112 Dibenzofuran ug/L ND 50 45.7 91 19-102 Diethylphthalate ug/L ND 50 44.8J 90 29-110 Dimethoate ug/L ND 50 40.8 82 50-150 Dimethylphthalate ug/L ND 50 46.7 93 27-110 Diphenylamine ug/L ND 50 38.5 77 50-150 Disulfoton ug/L ND 50 27.8 56 50-150 Ethyl methanesulfonate ug/L ND 50 29.7 59 50-150 Famphur ug/L ND 100 160 160 50-150 M1 Fluoranthene ug/L ND 50 41.8 84 23-112 Fluorene ug/L ND 50 43.8 88 22-104 Hexachlorobenzene ug/L ND 50 36.3 73 21-116 Hexachlorocyclopentadiene ug/L ND 50 33.7 67 10-110 Hexachloroethane ug/L ND 50 23.5 47 10-110 Hexachloropropene ug/L ND 50 21.5 43 50-150 M1 Indeno(1,2,3-cd)pyrene ug/L ND 50 39.3 79 20-113 Isodrin ug/L ND 50 37.9 76 50-150 Isophorone ug/L ND 50 35.8 72 50-150 Isosafrole ug/L ND 50 38.1 76 50-150 Kepone ug/L ND 100 96.4 96 50-150 Methapyrilene ug/L ND 50 6.9J 14 50-150 M1 Methyl methanesulfonate ug/L ND 50 48.5 97 50-150 Methyl parathion ug/L ND 50 40.0 80 50-150 N-Nitroso-di-n-butylamine ug/L ND 50 33.8 68 50-150 N-Nitroso-di-n-propylamine ug/L ND 50 43.0 86 21-105 N-Nitrosodiethylamine ug/L ND 50 33.4 67 50-150 N-Nitrosodimethylamine ug/L ND 50 23.3 47 10-110 N-Nitrosodiphenylamine ug/L ND 50 38.5 77 23-107 N-Nitrosomethylethylamine ug/L ND 50 26.6 53 50-150 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 130 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 MATRIX SPIKE SAMPLE: 2017033 92342479002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers N-Nitrosopiperidine ug/L ND 50 38.5 77 50-150 N-Nitrosopyrrolidine ug/L ND 50 37.8 76 50-150 Nitrobenzene ug/L ND 50 31.4 63 20-110 O,O,O-Triethylphosphorothioate ug/L ND 50 37.0 74 50-150 O-Toluidine ug/L ND 50 26.6 53 50-150 P-Dimethylaminoazobenzene ug/L ND 100 11.2 11 50-150 M1 p-Phenylenediamine ug/L ND 50 35.5 71 50-150 Parathion (Ethyl parathion) ug/L ND 50 32.0 64 50-150 Pentachlorobenzene ug/L ND 50 40.2 80 50-150 Pentachloronitrobenzene ug/L ND 50 41.7 83 50-150 Pentachlorophenol ug/L ND 250 83.9 34 10-118 Phenacetin ug/L ND 50 35.0 70 50-150 Phenanthrene ug/L ND 50 40.5 81 24-106 Phenol ug/L ND 50 16.5 33 12-110 Phorate ug/L ND 50 30.0 60 50-150 Pronamide ug/L ND 50 37.6 75 50-150 Pyrene ug/L ND 50 36.3 73 24-114 Safrole ug/L ND 50 38.0 76 50-150 Thionazin ug/L ND 50 34.4 69 50-150 2,4,6-Tribromophenol (S) % 78 27-110 2-Fluorobiphenyl (S) % 88 27-110 2-Fluorophenol(S) % 42 12-110 Nitrobenzene-d5 (S) % 66 21-110 Phenol-d6 (S) % 30 10-110 Terphenyl-d14 (S) % 61 31-107 SAMPLE DUPLICATE: 2018660 92342479007 Dup Max Parameter Units Result Result RPD RPD Qualifiers 1,2,4,5-Tetrachlorobenzene ug/L ND ND 30 1,3,5-Trinitrobenzene ug/L ND ND 30 1,3-Dinitrobenzene ug/L ND ND 30 1,4-Naphthoquinone ug/L ND ND 30 1-Naphthalenamine ug/L ND ND 30 2,2'-Oxybis(1-chloropropane) ug/L ND ND 30 2,3,4,6-Tetrachlorophenol ug/L ND ND 30 2,4,5-Trichlorophenol ug/L ND ND 30 2,4,6-Trichlorophenol ug/L ND ND 30 2,4-Dichlorophenol ug/L ND ND 30 2,4-Dimethylphenol ug/L ND ND 30 2,4-Dinitrophenol ug/L ND ND 30 2,4-Dinitrotoluene ug/L ND ND 30 2,6-Dichlorophenol ug/L ND ND 30 2,6-Dinitrotoluene ug/L ND ND 30 2-Acetylaminofluorene ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 131 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 SAMPLE DUPLICATE: 2018660 Parameter Units 92342479007 Result Dup Result 2-Chloronaphthalene ug/L ND ND 2-Chlorophenol ug/L ND ND 2-Methylnaphthalene ug/L ND ND 2-Methylphenol(o-Cresol) ug/L ND ND 2-Naphthalenamine ug/L ND ND 2-Nitroaniline ug/L ND ND 2-Nitrophenol ug/L ND ND 3&4-Methyl phenol (m&p Cresol) ug/L ND ND 3,3'-Dichlorobenzidine ug/L ND ND 3,3'-Dimethylbenzidine ug/L ND ND 3-Methylcholanthrene ug/L ND ND 3-Nitroaniline ug/L ND ND 4,6-Dinitro-2-methyl phenol ug/L ND ND 4-Aminobiphenyl ug/L ND ND 4-Bromophenylphenyl ether ug/L ND ND 4-Chloro-3-methylphenol ug/L ND ND 4-Chloroaniline ug/L ND ND 4-Chlorophenylphenyl ether ug/L ND ND 4-Nitroaniline ug/L ND ND 4-Nitrophenol ug/L ND ND 5-Nitro-o-toluidine ug/L ND ND 7,12-Dimethylbenz(a)anthracene ug/L ND ND Acenaphthene ug/L ND ND Acenaphthylene ug/L ND ND Acetophenone ug/L ND ND Anthracene ug/L ND ND Benzo(a)anthracene ug/L ND ND Benzo(a)pyrene ug/L ND ND Benzo(b)fluoranthene ug/L ND ND Benzo(g,h,i)perylene ug/L ND ND Benzo(k)fluoranthene ug/L ND ND Benzyl alcohol ug/L ND ND bis(2-Chloroethoxy)methane ug/L ND ND bis(2-Chloroethyl) ether ug/L ND ND bis(2-Ethylhexyl)phthalate ug/L ND ND Butylbenzylphthalate ug/L ND ND Chlorobenzilate ug/L ND ND Chrysene ug/L ND ND Di-n-butylphthalate ug/L ND ND Di-n-octylphthalate ug/L ND ND Diallate ug/L ND ND Dibenz(a,h)anthracene ug/L ND ND Dibenzofuran ug/L ND ND Diethylphthalate ug/L ND ND Dimethoate ug/L ND ND Dimethylphthalate ug/L ND ND Diphenylamine ug/L ND ND Max RPD RPD Qualifiers 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 132 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 SAMPLE DUPLICATE: 2018660 Parameter Units 92342479007 Result Dup Result RPD Max RPD Disulfoton ug/L ND ND 30 Ethyl methanesulfonate ug/L ND ND 30 Famphur ug/L ND ND 30 Fluoranthene ug/L ND ND 30 Fluorene ug/L ND ND 30 Hexachlorobenzene ug/L ND ND 30 Hexachlorocyclopentadiene ug/L ND ND 30 Hexachloroethane ug/L ND ND 30 Hexachloropropene ug/L ND ND 30 Indeno(1,2,3-cd)pyrene ug/L ND ND 30 Isodrin ug/L ND ND 30 Isophorone ug/L ND ND 30 Isosafrole ug/L ND ND 30 Kepone ug/L ND ND 30 Methapyrilene ug/L ND ND 30 Methyl methanesulfonate ug/L ND ND 30 Methyl parathion ug/L ND ND 30 N-Nitroso-di-n-butylamine ug/L ND ND 30 N-Nitroso-di-n-propylamine ug/L ND ND 30 N-Nitrosodiethylamine ug/L ND ND 30 N-Nitrosodimethylamine ug/L ND ND 30 N-Nitrosodiphenylamine ug/L ND ND 30 N-Nitrosomethylethylamine ug/L ND ND 30 N-Nitrosopiperidine ug/L ND ND 30 N-Nitrosopyrrolidine ug/L ND ND 30 Nitrobenzene ug/L ND ND 30 O,O,O-Triethylphosphorothioate ug/L ND ND 30 O-Toluidine ug/L ND ND 30 P-Dimethylaminoazobenzene ug/L ND ND 30 p-Phenylenediamine ug/L ND ND 30 Parathion (Ethyl parathion) ug/L ND ND 30 Pentachlorobenzene ug/L ND ND 30 Pentachloronitrobenzene ug/L ND ND 30 Pentachlorophenol ug/L ND ND 30 Phenacetin ug/L ND ND 30 Phenanthrene ug/L ND ND 30 Phenol ug/L ND ND 30 Phorate ug/L ND ND 30 Pronamide ug/L ND ND 30 Pyrene ug/L ND ND 30 Safrole ug/L ND ND 30 Thionazin ug/L ND ND 30 2,4,6-Tribromophenol (S) % 89 84 6 2-Fluorobiphenyl (S) % 90 100 10 2-Fluorophenol (S) % 44 41 7 Nitrobenzene-d5 (S) % 72 81 13 Phenol-d6 (S) % 28 26 7 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 133 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 SAMPLE DUPLICATE: 2018660 92342479007 Dup Max Parameter Units Result Result RPD RPD Terphenyl-d14 (S) % 98 81 19 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. 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AIRY (UIC) Pace Project No.: 92342478 QC Batch: 364049 Analysis Method: EPA 8270 QC Batch Method: EPA 3510 Analysis Description: 8270 Water MSSV Associated Lab Samples: 92342478004, 92342478005, 92342530001, 92342530002, 92342530003, 92342530004, 92342530005 METHOD BLANK: 2018678 Matrix: Water Associated Lab Samples: 92342478004, 92342478005, 92342530001, 92342530002, 92342530003, 92342530004, 92342530005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 1.3 06/14/17 13:23 1,3,5-Trinitrobenzene ug/L ND 10.0 1.2 06/14/17 13:23 1,3-Dinitrobenzene ug/L ND 20.0 1.3 06/14/17 13:23 1,4-Naphthoquinone ug/L ND 10.0 0.99 06/14/17 13:23 1-Naphthalenamine ug/L ND 10.0 1.3 06/14/17 13:23 2,2'-Oxybis(1-chloropropane) ug/L ND 10.0 1.8 06/14/17 13:23 2,3,4,6-Tetrachlorophenol ug/L ND 10.0 2.9 06/14/17 13:23 2,4,5-Trichlorophenol ug/L ND 10.0 1.5 06/14/17 13:23 2,4,6-Trichlorophenol ug/L ND 10.0 1.4 06/14/17 13:23 2,4-Dichlorophenol ug/L ND 10.0 1.6 06/14/17 13:23 2,4-Dimethylphenol ug/L ND 10.0 1.6 06/14/17 13:23 2,4-Dinitrophenol ug/L ND 50.0 5.1 06/14/17 13:23 2,4-Dinitrotoluene ug/L ND 10.0 1.5 06/14/17 13:23 2,6-Dichlorophenol ug/L ND 10.0 1.5 06/14/17 13:23 2,6-Dinitrotoluene ug/L ND 10.0 1.4 06/14/17 13:23 2-Acetylaminofluorene ug/L ND 20.0 1.6 06/14/17 13:23 2-Chloronaphthalene ug/L ND 10.0 1.6 06/14/17 13:23 2-Chlorophenol ug/L ND 10.0 1.5 06/14/17 13:23 2-Methylnaphthalene ug/L ND 10.0 1.4 06/14/17 13:23 2-Methylphenol(o-Cresol) ug/L ND 10.0 1.6 06/14/17 13:23 2-Naphthalenamine ug/L ND 10.0 2.2 06/14/17 13:23 2-Nitroaniline ug/L ND 50.0 2.3 06/14/17 13:23 2-Nitrophenol ug/L ND 10.0 1.6 06/14/17 13:23 3&4-Methyl phenol (m&p Cresol) ug/L ND 10.0 1.4 06/14/17 13:23 3,3'-Dichlorobenzidine ug/L ND 20.0 3.9 06/14/17 13:23 3,3'-Dimethylbenzidine ug/L ND 10.0 3.9 06/14/17 13:23 3-Methylcholanthrene ug/L ND 10.0 2.7 06/14/17 13:23 3-Nitroaniline ug/L ND 50.0 2.7 06/14/17 13:23 4,6-Dinitro-2-methyl phenol ug/L ND 50.0 2.2 06/14/17 13:23 4-Aminobiphenyl ug/L ND 20.0 1.7 06/14/17 13:23 4-Bromophenylphenyl ether ug/L ND 10.0 1.5 06/14/17 13:23 4-ChIoro-3-methyl phenol ug/L ND 20.0 2.8 06/14/17 13:23 4-Chloroaniline ug/L ND 20.0 2.8 06/14/17 13:23 4-Chlorophenylphenyl ether ug/L ND 10.0 1.6 06/14/17 13:23 4-Nitroaniline ug/L ND 20.0 3.4 06/14/17 13:23 4-Nitrophenol ug/L ND 50.0 4.3 06/14/17 13:23 5-Nitro-o-toluidine ug/L ND 10.0 1.9 06/14/17 13:23 7,12-Dimethylbenz(a)anthracene ug/L ND 10.0 2.4 06/14/17 13:23 Acenaphthene ug/L ND 10.0 1.6 06/14/17 13:23 Acenaphthylene ug/L ND 10.0 1.5 06/14/17 13:23 Acetophenone ug/L ND 10.0 1.9 06/14/17 13:23 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 135 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 METHOD BLANK: 2018678 Matrix: Water Associated Lab Samples: 92342478004, 92342478005, 92342530001, 92342530002, 92342530003, 92342530004, 92342530005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Anthracene ug/L ND 10.0 1.7 06/14/17 13:23 Benzo(a)anthracene ug/L ND 10.0 2.1 06/14/17 13:23 Benzo(a)pyrene ug/L ND 10.0 2.2 06/14/17 13:23 Benzo(b)fluoranthene ug/L ND 10.0 2.2 06/14/17 13:23 Benzo(g,h,i)perylene ug/L ND 10.0 2.1 06/14/17 13:23 Benzo(k)fluoranthene ug/L ND 10.0 2.0 06/14/17 13:23 Benzyl alcohol ug/L ND 20.0 3.1 06/14/17 13:23 bis(2-Chloroethoxy)methane ug/L ND 10.0 1.6 06/14/17 13:23 bis(2-Chloroethyl) ether ug/L ND 10.0 1.7 06/14/17 13:23 bis(2-Ethylhexyl)phthalate ug/L ND 15.0 2.3 06/14/17 13:23 Butylbenzylphthalate ug/L ND 10.0 2.5 06/14/17 13:23 Chlorobenzilate ug/L ND 10.0 2.2 06/14/17 13:23 Chrysene ug/L ND 10.0 2.1 06/14/17 13:23 Di-n-butylphthalate ug/L ND 10.0 2.0 06/14/17 13:23 Di-n-octylphthalate ug/L ND 10.0 1.5 06/14/17 13:23 Diallate ug/L ND 10.0 1.6 06/14/17 13:23 Dibenz(a,h)anthracene ug/L ND 10.0 2.0 06/14/17 13:23 Dibenzofuran ug/L ND 10.0 1.7 06/14/17 13:23 Diethylphthalate ug/L ND 6000 1.6 06/14/17 13:23 Dimethoate ug/L ND 20.0 1.8 06/14/17 13:23 Dimethylphthalate ug/L ND 10.0 1.4 06/14/17 13:23 Diphenylamine ug/L ND 10.0 1.4 06/14/17 13:23 Disulfoton ug/L ND 10.0 1.5 06/14/17 13:23 Ethyl methanesulfonate ug/L ND 20.0 1.6 06/14/17 13:23 Famphur ug/L ND 20.0 5.7 06/14/17 13:23 Fluoranthene ug/L ND 10.0 2.2 06/14/17 13:23 Fluorene ug/L ND 10.0 1.6 06/14/17 13:23 Hexachlorobenzene ug/L ND 10.0 1.7 06/14/17 13:23 Hexachlorocyclopentadiene ug/L ND 10.0 1.3 06/14/17 13:23 Hexachloroethane ug/L ND 10.0 1.8 06/14/17 13:23 Hexachloropropene ug/L ND 10.0 1.2 06/14/17 13:23 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 2.0 06/14/17 13:23 Isodrin ug/L ND 20.0 2.5 06/14/17 13:23 Isophorone ug/L ND 10.0 1.5 06/14/17 13:23 Isosafrole ug/L ND 10.0 1.5 06/14/17 13:23 Kepone ug/L ND 20.0 4.5 06/14/17 13:23 Methapyrilene ug/L ND 100 3.0 06/14/17 13:23 Methyl methanesulfonate ug/L ND 10.0 1.1 06/14/17 13:23 Methyl parathion ug/L ND 10.0 1.6 06/14/17 13:23 N-Nitroso-di-n-butylamine ug/L ND 10.0 1.6 06/14/17 13:23 N-Nitroso-di-n-propylamine ug/L ND 10.0 1.7 06/14/17 13:23 N-Nitrosodiethylamine ug/L ND 20.0 1.4 06/14/17 13:23 N-Nitrosodimethylamine ug/L ND 10.0 1.6 06/14/17 13:23 N-Nitrosodiphenylamine ug/L ND 10.0 1.4 06/14/17 13:23 N-Nitrosomethylethylamine ug/L ND 10.0 1.4 06/14/17 13:23 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 136 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 METHOD BLANK: 2018678 Matrix: Water Associated Lab Samples: 92342478004, 92342478005, 92342530001, 92342530002, 92342530003, 92342530004, 92342530005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers N-Nitrosopiperidine ug/L ND 20.0 1.7 06/14/17 13:23 N-Nitrosopyrrolidine ug/L ND 10.0 1.7 06/14/17 13:23 Nitrobenzene ug/L ND 10.0 1.6 06/14/17 13:23 O,O,O-Triethylphosphorothioate ug/L ND 10.0 1.7 06/14/17 13:23 O-Toluidine ug/L ND 10.0 1.7 06/14/17 13:23 P-Dimethylaminoazobenzene ug/L ND 10.0 1.0 06/14/17 13:23 p-Phenylenediamine ug/L ND 10.0 2.2 06/14/17 13:23 Parathion (Ethyl parathion) ug/L ND 10.0 1.5 06/14/17 13:23 Pentachlorobenzene ug/L ND 10.0 1.5 06/14/17 13:23 Pentachloronitrobenzene ug/L ND 20.0 1.7 06/14/17 13:23 Pentachlorophenol ug/L ND 25.0 3.5 06/14/17 13:23 Phenacetin ug/L ND 20.0 1.9 06/14/17 13:23 Phenanthrene ug/L ND 10.0 1.6 06/14/17 13:23 Phenol ug/L ND 10.0 1.3 06/14/17 13:23 Phorate ug/L ND 10.0 1.7 06/14/17 13:23 Pronamide ug/L ND 10.0 2.0 06/14/17 13:23 Pyrene ug/L ND 10.0 2.2 06/14/17 13:23 Safrole ug/L ND 10.0 1.3 06/14/17 13:23 Thionazin ug/L ND 20.0 1.7 06/14/17 13:23 2,4,6-Tribromophenol (S) % 74 27-110 06/14/17 13:23 2-Fluorobiphenyl (S) % 77 27-110 06/14/17 13:23 2-Fluorophenol (S) % 37 12-110 06/14/17 13:23 Nitrobenzene-d5 (S) % 62 21-110 06/14/17 13:23 Phenol-d6 (S) % 25 10-110 06/14/17 13:23 Terphenyl-d14 (S) % 87 31-107 06/14/17 13:23 LABORATORY CONTROL SAMPLE: Parameter 2018679 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,2,4,5-Tetrachlorobenzene ug/L 50 34.4 69 16-129 1,3,5-Trinitrobenzene ug/L 50 32.6 65 55-125 1,3-Dinitrobenzene ug/L 50 42.5 85 30-122 1,4-Naphthoquinone ug/L 50 41.8 84 31-120 1-Naphthalenamine ug/L 50 27.0 54 37-126 2,2'-Oxybis(1-chloropropane) ug/L 50 52.9 106 18-120 2,3,4,6-Tetrachlorophenol ug/L 50 82.3 165 54-276 2,4,5-Trichlorophenol ug/L 50 43.1 86 43-113 2,4,6-Trichlorophenol ug/L 50 50.8 102 42-120 2,4-Dichlorophenol ug/L 50 42.7 85 30-120 2,4-Dimethylphenol ug/L 50 37.9 76 29-111 2,4-Dinitrophenol ug/L 250 246 98 19-132 2,4-Dinitrotoluene ug/L 50 45.1 90 58-128 2,6-Dichlorophenol ug/L 50 43.6 87 54-128 2,6-Dinitrotoluene ug/L 50 47.0 94 54-129 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 137 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 LABORATORY CONTROL SAMPLE: Parameter 2018679 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2-Acetylaminofluorene ug/L 50 38.7 77 81-160 L2 2-Chloronaphthalene ug/L 50 53.0 106 43-117 2-Chlorophenol ug/L 50 41.9 84 37-120 2-Methylnaphthalene ug/L 50 37.6 75 33-120 2-Methylphenol(o-Cresol) ug/L 50 34.3 69 31-120 2-Naphthalenamine ug/L 50 34.1 68 41-136 2-Nitroaniline ug/L 100 88.7 89 48-121 2-Nitrophenol ug/L 50 40.7 81 25-116 3&4-Methyl phenol (m&p Cresol) ug/L 50 29.8 60 23-120 3,3'-Dichlorobenzidine ug/L 250 88.8 36 10-154 3,3'-Dimethylbenzidine ug/L 100 41.5 42 10-157 3-Methylcholanthrene ug/L 50 46.8 94 65-130 3-Nitroaniline ug/L 100 107 107 43-115 4,6-Dinitro-2-methyl phenol ug/L 100 87.7 88 44-124 4-Aminobiphenyl ug/L 50 25.7 51 21-125 4-Bromophenylphenyl ether ug/L 50 34.8 70 34-113 4-ChIoro-3-methyl phenol ug/L 100 73.8 74 31-110 4-Chloroaniline ug/L 100 87.8 88 20-120 4-Chlorophenylphenyl ether ug/L 50 41.7 83 34-116 4-Nitroaniline ug/L 100 111 111 46-128 4-Nitrophenol ug/L 250 79.5 32 11-120 5-Nitro-o-toluidine ug/L 50 45.6 91 78-160 7,12-Dimethylbenz(a)anthracene ug/L 50 46.0 92 47-124 Acenaphthene ug/L 50 47.2 94 48-114 Acenaphthylene ug/L 50 48.6 97 48-112 Acetophenone ug/L 50 42.4 85 24-120 Anthracene ug/L 50 43.2 86 57-118 Benzo(a)anthracene ug/L 50 42.8 86 56-121 Benzo(a)pyrene ug/L 50 45.9 92 55-127 Benzo(b)fluoranthene ug/L 50 48.8 98 53-128 Benzo(g,h,i)perylene ug/L 50 39.6 79 54-125 Benzo(k)fluoranthene ug/L 50 46.1 92 51-123 Benzyl alcohol ug/L 100 77.8 78 27-120 bis(2-Chloroethoxy)methane ug/L 50 33.2 66 32-120 bis(2-Chloroethyl) ether ug/L 50 34.2 68 33-111 bis(2-Ethylhexyl)phthalate ug/L 50 43.0 86 50-145 Butylbenzylphthalate ug/L 50 45.0 90 54-138 Chlorobenzilate ug/L 50 42.8 86 65-132 Chrysene ug/L 50 42.6 85 58-127 Di-n-butylphthalate ug/L 50 46.0 92 56-125 Di-n-octylphthalate ug/L 50 41.1 82 50-134 Diallate ug/L 50 33.1 66 47-123 Dibenz(a,h)anthracene ug/L 50 43.7 87 53-129 Dibenzofuran ug/L 50 48.3 97 45-120 Diethylphthalate ug/L 50 46.7J 93 53-120 Dimethoate ug/L 50 39.7 79 57-139 Dimethylphthalate ug/L 50 48.6 97 55-116 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 138 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 LABORATORY CONTROL SAMPLE: Parameter 2018679 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Diphenylamine ug/L 50 44.9 90 42-120 Disulfoton ug/L 50 33.3 67 49-156 Ethyl methanesulfonate ug/L 50 31.0 62 43-120 Famphur ug/L 100 107 107 40-160 Fluoranthene ug/L 50 44.4 89 57-125 Fluorene ug/L 50 46.5 93 53-118 Hexachlorobenzene ug/L 50 39.8 80 49-116 Hexachlorocyclopentadiene ug/L 50 35.4 71 26-158 Hexachloroethane ug/L 50 25.8 52 30-114 Hexachloropropene ug/L 50 24.1 48 13-137 Indeno(1,2,3-cd)pyrene ug/L 50 42.1 84 55-128 Isodrin ug/L 50 40.0 80 68-129 Isophorone ug/L 50 36.5 73 31-118 Isosafrole ug/L 50 40.9 82 48-107 Kepone ug/L 100 65.8 66 10-124 Methapyrilene ug/L 50 21.OJ 42 40-160 Methyl methanesulfonate ug/L 50 46.3 93 25-114 Methyl parathion ug/L 50 42.9 86 58-137 N-Nitroso-di-n-butylamine ug/L 50 35.4 71 36-115 N-Nitroso-di-n-propylamine ug/L 50 43.8 88 32-119 N-Nitrosodiethylamine ug/L 50 34.6 69 47-115 N-Nitrosodimethylamine ug/L 50 23.1 46 13-120 N-Nitrosodiphenylamine ug/L 50 44.9 90 43-120 N-Nitrosomethylethylamine ug/L 50 28.0 56 39-120 N-Nitrosopiperidine ug/L 50 41.6 83 43-113 N-Nitrosopyrrolidine ug/L 50 41.7 83 32-110 Nitrobenzene ug/L 50 31.5 63 33-110 O,O,O-Triethylphosphorothioate ug/L 50 38.1 76 51-127 O-Toluidine ug/L 50 32.1 64 27-120 P-Dimethylaminoazobenzene ug/L 100 17.3 17 10-120 p-Phenylenediamine ug/L 50 37.6 75 72-143 Parathion (Ethyl parathion) ug/L 50 35.4 71 56-140 Pentachlorobenzene ug/L 50 42.9 86 30-137 Pentachloronitrobenzene ug/L 50 44.1 88 70-124 Pentachlorophenol ug/L 250 97.2 39 10-137 Phenacetin ug/L 50 37.0 74 60-130 Phenanthrene ug/L 50 43.1 86 57-117 Phenol ug/L 50 18.9 38 10-120 Phorate ug/L 50 32.6 65 55-126 Pronamide ug/L 50 40.4 81 75-124 Pyrene ug/L 50 45.3 91 55-122 Safrole ug/L 50 41.4 83 41-120 Thionazin ug/L 50 35.2 70 63-137 2,4,6-Tribromophenol (S) % 90 27-110 2-Fluorobiphenyl (S) % 90 27-110 2-Fluorophenol(S) % 46 12-110 Nitrobenzene-d5(S) % 67 21-110 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 139 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 LABORATORY CONTROL SAMPLE: 2018679 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phenol-d6 (S) % 34 10-110 Terphenyl-d14 (S) % 91 31-107 MATRIX SPIKE SAMPLE: 2022108 92342530002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,2,4,5-Tetrachlorobenzene ug/L ND 50 37.7 75 50-150 1,3,5-Trinitrobenzene ug/L ND 50 33.6 67 50-150 1,3-Dinitrobenzene ug/L ND 50 41.4 83 50-150 1,4-Naphthoquinone ug/L ND 50 44.8 90 50-150 1-Naphthalenamine ug/L ND 50 14.2 28 50-150 M1 2,2'-Oxybis(1-chloropropane) ug/L ND 50 52.0 104 50-150 2,3,4,6-Tetrachlorophenol ug/L ND 50 85.5 171 50-150 M1 2,4,5-Trichlorophenol ug/L ND 50 44.7 89 19-105 2,4,6-Trichlorophenol ug/L ND 50 52.4 105 13-108 2,4-Dichlorophenol ug/L ND 50 39.5 79 29-111 2,4-Dimethylphenol ug/L ND 50 36.2 72 21-103 2,4-Dinitrophenol ug/L ND 250 207 83 10-109 2,4-Dinitrotoluene ug/L ND 50 46.7 93 27-104 2,6-Dichlorophenol ug/L ND 50 40.5 81 50-150 2,6-Dinitrotoluene ug/L ND 50 48.5 97 28-101 2-Acetylaminofluorene ug/L ND 50 36.8 73 50-150 2-Chloronaphthalene ug/L ND 50 58.1 116 14-102 M1 2-Chlorophenol ug/L ND 50 36.3 73 16-110 2-Methylnaphthalene ug/L ND 50 36.8 74 13-110 2-Methylphenol(o-Cresol) ug/L ND 50 29.7 59 19-110 2-Naphthalenamine ug/L ND 50 11.5 23 50-150 M1 2-Nitroaniline ug/L ND 100 95.3 95 26-103 2-Nitrophenol ug/L ND 50 36.5 73 20-110 3&4-Methyl phenol (m&p Cresol) ug/L ND 50 25.5 51 20-110 3,3'-Dichlorobenzidine ug/L ND 250 78.3 31 25-112 3,3'-Dimethylbenzidine ug/L ND 100 20.1 20 50-150 M1 3-Methylcholanthrene ug/L ND 50 44.5 89 50-150 3-Nitroaniline ug/L ND 100 104 104 29-110 4,6-Dinitro-2-methyl phenol ug/L ND 100 73.6 74 10-117 4-Aminobiphenyl ug/L ND 50 21.2 42 50-150 M1 4-Bromophenylphenyl ether ug/L ND 50 35.3 71 20-105 4-ChIoro-3-methyl phenol ug/L ND 100 69.2 69 22-110 4-Chloroaniline ug/L ND 100 59.4 59 20-100 4-Chlorophenylphenyl ether ug/L ND 50 45.0 90 19-102 4-Nitroaniline ug/L ND 100 112 112 29-110 M1 4-Nitrophenol ug/L ND 250 78.0 31 10-110 5-Nitro-o-toluidine ug/L ND 50 46.3 93 50-150 7,12-Dimethylbenz(a)anthracene ug/L ND 50 46.5 93 50-150 Acenaphthene ug/L ND 50 50.2 100 17-100 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 140 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 MATRIX SPIKE SAMPLE: 2022108 92342530002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Acenaphthylene ug/L ND 50 51.2 102 21-100 M1 Acetophenone ug/L ND 50 36.5 73 50-150 Anthracene ug/L ND 50 44.4 89 24-109 Benzo(a)anthracene ug/L ND 50 41.6 83 22-117 Benzo(a)pyrene ug/L ND 50 44.7 89 23-104 Benzo(b)fluoranthene ug/L ND 50 48.9 98 23-103 Benzo(g,h,i)perylene ug/L ND 50 40.5 81 18-111 Benzo(k)fluoranthene ug/L ND 50 45.1 90 22-113 Benzyl alcohol ug/L ND 100 63.0 63 19-101 bis(2-Chloroethoxy)methane ug/L ND 50 31.8 64 22-110 bis(2-Chloroethyl) ether ug/L ND 50 33.1 66 16-110 bis(2-Ethylhexyl)phthalate ug/L ND 50 44.8 90 23-102 Butylbenzylphthalate ug/L ND 50 45.6 91 25-110 Chlorobenzilate ug/L ND 50 42.7 85 50-150 Chrysene ug/L ND 50 42.2 84 23-115 Di-n-butylphthalate ug/L ND 50 48.3 97 26-110 Di-n-octylphthalate ug/L ND 50 41.5 83 22-110 Diallate ug/L ND 50 35.2 70 50-150 Dibenz(a,h)anthracene ug/L ND 50 42.0 84 21-112 Dibenzofuran ug/L ND 50 51.2 102 19-102 Diethylphthalate ug/L ND 50 50.2J 100 29-110 Dimethoate ug/L ND 50 42.9 86 50-150 Dimethylphthalate ug/L ND 50 51.5 103 27-110 Diphenylamine ug/L ND 50 45.8 92 50-150 Disulfoton ug/L ND 50 35.4 71 50-150 Ethyl methanesulfonate ug/L ND 50 27.4 55 50-150 Famphur ug/L ND 100 130 130 50-150 Fluoranthene ug/L ND 50 45.8 92 23-112 Fluorene ug/L ND 50 49.1 98 22-104 Hexachlorobenzene ug/L ND 50 40.0 80 21-116 Hexachlorocyclopentadiene ug/L ND 50 35.9 72 10-110 Hexachloroethane ug/L ND 50 27.2 54 10-110 Hexachloropropene ug/L ND 50 25.5 51 50-150 Indeno(1,2,3-cd)pyrene ug/L ND 50 42.4 85 20-113 Isodrin ug/L ND 50 42.3 85 50-150 Isophorone ug/L ND 50 35.6 71 50-150 Isosafrole ug/L ND 50 43.6 87 50-150 Kepone ug/L ND 100 72.4 72 50-150 Methapyrilene ug/L ND 50 33.3J 67 50-150 Methyl methanesulfonate ug/L ND 50 42.5 85 50-150 Methyl parathion ug/L ND 50 42.9 86 50-150 N-Nitroso-di-n-butylamine ug/L ND 50 32.3 65 50-150 N-Nitroso-di-n-propylamine ug/L ND 50 37.2 74 21-105 N-Nitrosodiethylamine ug/L ND 50 28.7 57 50-150 N-Nitrosodimethylamine ug/L ND 50 20.7 41 10-110 N-Nitrosodiphenylamine ug/L ND 50 45.8 92 23-107 N-Nitrosomethylethylamine ug/L ND 50 23.7 47 50-150 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 141 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 MATRIX SPIKE SAMPLE: 2022108 92342530002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers N-Nitrosopiperidine ug/L ND 50 37.2 74 50-150 N-Nitrosopyrrolidine ug/L ND 50 28.6 57 50-150 Nitrobenzene ug/L ND 50 30.4 61 20-110 O,O,O-Triethylphosphorothioate ug/L ND 50 36.8 74 50-150 O-Toluidine ug/L ND 50 20.6 41 50-150 M1 P-Dimethylaminoazobenzene ug/L ND 100 16.8 17 50-150 M1 p-Phenylenediamine ug/L ND 50 35.2 70 50-150 Parathion (Ethyl parathion) ug/L ND 50 36.6 73 50-150 Pentachlorobenzene ug/L ND 50 44.7 89 50-150 Pentachloronitrobenzene ug/L ND 50 44.8 90 50-150 Pentachlorophenol ug/L ND 250 88.9 36 10-118 Phenacetin ug/L ND 50 37.1 74 50-150 Phenanthrene ug/L ND 50 44.8 90 24-106 Phenol ug/L ND 50 15.3 31 12-110 Phorate ug/L ND 50 33.6 67 50-150 Pronamide ug/L ND 50 41.6 83 50-150 Pyrene ug/L ND 50 45.0 90 24-114 Safrole ug/L ND 50 38.4 77 50-150 Thionazin ug/L ND 50 38.0 76 50-150 2,4,6-Tribromophenol (S) % 87 27-110 2-Fluorobiphenyl (S) % 95 27-110 2-Fluorophenol(S) % 39 12-110 Nitrobenzene-d5 (S) % 62 21-110 Phenol-d6 (S) % 27 10-110 Terphenyl-d14 (S) % 74 31-107 SAMPLE DUPLICATE: 2018681 92342530004 Dup Max Parameter Units Result Result RPD RPD Qualifiers 1,2,4,5-Tetrachlorobenzene ug/L ND ND 30 1,3,5-Trinitrobenzene ug/L ND ND 30 1,3-Dinitrobenzene ug/L ND ND 30 1,4-Naphthoquinone ug/L ND ND 30 1-Naphthalenamine ug/L ND ND 30 2,2'-Oxybis(1-chloropropane) ug/L ND ND 30 2,3,4,6-Tetrachlorophenol ug/L ND ND 30 2,4,5-Trichlorophenol ug/L ND ND 30 2,4,6-Trichlorophenol ug/L ND ND 30 2,4-Dichlorophenol ug/L ND ND 30 2,4-Dimethylphenol ug/L ND ND 30 2,4-Dinitrophenol ug/L ND ND 30 2,4-Dinitrotoluene ug/L ND ND 30 2,6-Dichlorophenol ug/L ND ND 30 2,6-Dinitrotoluene ug/L ND ND 30 2-Acetylaminofluorene ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 142 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 SAMPLE DUPLICATE: 2018681 Parameter Units 92342530004 Result Dup Result 2-Chloronaphthalene ug/L ND ND 2-Chlorophenol ug/L ND ND 2-Methylnaphthalene ug/L ND ND 2-Methylphenol(o-Cresol) ug/L ND ND 2-Naphthalenamine ug/L ND ND 2-Nitroaniline ug/L ND ND 2-Nitrophenol ug/L ND ND 3&4-Methyl phenol (m&p Cresol) ug/L ND ND 3,3'-Dichlorobenzidine ug/L ND ND 3,3'-Dimethylbenzidine ug/L ND ND 3-Methylcholanthrene ug/L ND ND 3-Nitroaniline ug/L ND ND 4,6-Dinitro-2-methyl phenol ug/L ND ND 4-Aminobiphenyl ug/L ND ND 4-Bromophenylphenyl ether ug/L ND ND 4-Chloro-3-methylphenol ug/L ND ND 4-Chloroaniline ug/L ND ND 4-Chlorophenylphenyl ether ug/L ND ND 4-Nitroaniline ug/L ND ND 4-Nitrophenol ug/L ND ND 5-Nitro-o-toluidine ug/L ND ND 7,12-Dimethylbenz(a)anthracene ug/L ND ND Acenaphthene ug/L ND ND Acenaphthylene ug/L ND ND Acetophenone ug/L ND ND Anthracene ug/L ND ND Benzo(a)anthracene ug/L ND ND Benzo(a)pyrene ug/L ND ND Benzo(b)fluoranthene ug/L ND ND Benzo(g,h,i)perylene ug/L ND ND Benzo(k)fluoranthene ug/L ND ND Benzyl alcohol ug/L ND ND bis(2-Chloroethoxy)methane ug/L ND ND bis(2-Chloroethyl) ether ug/L ND ND bis(2-Ethylhexyl)phthalate ug/L ND ND Butylbenzylphthalate ug/L ND ND Chlorobenzilate ug/L ND ND Chrysene ug/L ND ND Di-n-butylphthalate ug/L ND ND Di-n-octylphthalate ug/L ND ND Diallate ug/L ND ND Dibenz(a,h)anthracene ug/L ND ND Dibenzofuran ug/L ND ND Diethylphthalate ug/L ND ND Dimethoate ug/L ND ND Dimethylphthalate ug/L ND ND Diphenylamine ug/L ND ND Max RPD RPD Qualifiers 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 143 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 SAMPLE DUPLICATE: 2018681 Parameter Units 92342530004 Result Dup Result RPD Max RPD Disulfoton ug/L ND ND 30 Ethyl methanesulfonate ug/L ND ND 30 Famphur ug/L ND ND 30 Fluoranthene ug/L ND ND 30 Fluorene ug/L ND ND 30 Hexachlorobenzene ug/L ND ND 30 Hexachlorocyclopentadiene ug/L ND ND 30 Hexachloroethane ug/L ND ND 30 Hexachloropropene ug/L ND ND 30 Indeno(1,2,3-cd)pyrene ug/L ND ND 30 Isodrin ug/L ND ND 30 Isophorone ug/L ND ND 30 Isosafrole ug/L ND ND 30 Kepone ug/L ND ND 30 Methapyrilene ug/L ND ND 30 Methyl methanesulfonate ug/L ND ND 30 Methyl parathion ug/L ND ND 30 N-Nitroso-di-n-butylamine ug/L ND ND 30 N-Nitroso-di-n-propylamine ug/L ND ND 30 N-Nitrosodiethylamine ug/L ND ND 30 N-Nitrosodimethylamine ug/L ND ND 30 N-Nitrosodiphenylamine ug/L ND ND 30 N-Nitrosomethylethylamine ug/L ND ND 30 N-Nitrosopiperidine ug/L ND ND 30 N-Nitrosopyrrolidine ug/L ND ND 30 Nitrobenzene ug/L ND ND 30 O,O,O-Triethylphosphorothioate ug/L ND ND 30 O-Toluidine ug/L ND ND 30 P-Dimethylaminoazobenzene ug/L ND ND 30 p-Phenylenediamine ug/L ND ND 30 Parathion (Ethyl parathion) ug/L ND ND 30 Pentachlorobenzene ug/L ND ND 30 Pentachloronitrobenzene ug/L ND ND 30 Pentachlorophenol ug/L ND ND 30 Phenacetin ug/L ND ND 30 Phenanthrene ug/L ND ND 30 Phenol ug/L ND ND 30 Phorate ug/L ND ND 30 Pronamide ug/L ND ND 30 Pyrene ug/L ND ND 30 Safrole ug/L ND ND 30 Thionazin ug/L ND ND 30 2,4,6-Tribromophenol (S) % 71 88 23 2-Fluorobiphenyl (S) % 70 88 23 2-Fluorophenol(S) % 32 40 23 Nitrobenzene-d5 (S) % 57 69 20 Phenol-d6 (S) % 20 27 28 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 144 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 SAMPLE DUPLICATE: 2018681 92342530004 Dup Max Parameter Units Result Result RPD RPD Terphenyl-d14(S) % 76 60 24 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 145 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 QC Batch: 363621 Analysis Method: SM 4500-S2D QC Batch Method: SM 4500-S2D Analysis Description: 4500S2D Sulfide Water Associated Lab Samples: 92342478003 METHOD BLANK: 2015987 Matrix: Water Associated Lab Samples: 92342478003 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfide ug/L ND 1000 100 06/06/17 22:15 LABORATORY CONTROL SAMPLE: 2015988 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 464J 93 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2015989 2015990 MS MSD 92342281006 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 433J 524J 87 105 80-120 19 10 R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2015991 2015992 MS MSD 92342472017 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 470J 468J 85 85 80-120 0 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 146 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 QC Batch: 363623 Analysis Method: SM 4500-S2D QC Batch Method: SM 4500-S2D Analysis Description: 4500S2D Sulfide Water Associated Lab Samples: 92342530001, 92342530002, 92342530003, 92342530004, 92342530005 METHOD BLANK: 2016031 Matrix: Water Associated Lab Samples: 92342530001, 92342530002, 92342530003, 92342530004, 92342530005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfide ug/L ND 1000 100 06/06/17 23:00 LABORATORY CONTROL SAMPLE: 2016032 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 470J 94 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2016033 2016034 MS MSD 92342317011 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 454J 463J 91 93 80-120 2 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2016035 2016036 MS MSD 92342530004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 408J 423J 82 85 80-120 4 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 147 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 QC Batch: 362992 Analysis Method: SM 4500-CN-E QC Batch Method: SM 4500-CN-E Analysis Description: 450OCNE Cyanide, Total Associated Lab Samples: 92342478003 METHOD BLANK: 2012287 Matrix: Water Associated Lab Samples: 92342478003 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Cyanide ug/L ND 10.0 4.0 06/01/1717:52 LABORATORY CONTROL SAMPLE: 2012288 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 109 109 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2012289 2012290 MS MSD 92342479002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L 4AJ 100 100 109 100 104 96 80-120 8 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2012291 2012292 MS MSD 92342478003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L 4.6J 100 100 97.4 103 93 99 80-120 6 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 148 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 QC Batch: 363513 Analysis Method: SM 4500-CN-E QC Batch Method: SM 4500-CN-E Analysis Description: 450OCNE Cyanide, Total Associated Lab Samples: 92342530001, 92342530002, 92342530003, 92342530004, 92342530005 METHOD BLANK: 2015224 Matrix: Water Associated Lab Samples: 92342530001, 92342530002, 92342530003, 92342530004, 92342530005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Cyanide ug/L ND 10.0 4.0 06/07/1713:52 LABORATORY CONTROL SAMPLE: 2015225 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 101 101 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2015226 2015227 MS MSD 92342317015 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 97.6 95.4 94 91 80-120 2 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2015228 2015229 MS MSD 92342712006 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L 0.013 100 100 41.2 31.4 29 19 80-120 27 10 M1,R1 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 149 of 166 Pace Analytical Services, LLC aceAnalXical� 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALIFIERS Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte PASI-O Pace Analytical Services - Ormond Beach BATCH QUALIFIERS Batch: 372970 [M5] A matrix spike/matrix spike duplicate was not performed for this batch due to insufficient sample volume. ANALYTE QUALIFIERS 1g Sample re -extracted outside method hold time. Results of re -analysis confirmed original analysis performed within hold time. L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high. L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated samples may be biased low. MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 150 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: SURRY CLOSED -MT. 92342478 AIRY (UIC) Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92342478003 MW-15 EPA 3510 363163 EPA 8081 363590 92342530001 MW-13 EPA 3510 363163 EPA 8081 363590 92342530002 MW-16 EPA 3510 363163 EPA 8081 363590 92342530003 MW-17 EPA 3510 363163 EPA 8081 363590 92342530004 MW-21 EPA 3510 363163 EPA 8081 363590 92342530005 MW-22 EPA 3510 363163 EPA 8081 363590 92342478004 MW-1 EPA 3510 363426 EPA 8081 363552 92342478005 MW-9 EPA 3510 363426 EPA 8081 363552 92342478003 MW-15 EPA 3510 363162 EPA 8082 363349 92342530001 MW-13 EPA 3510 363162 EPA 8082 363349 92342530002 MW-16 EPA 3510 363162 EPA 8082 363349 92342530003 MW-17 EPA 3510 363162 EPA 8082 363349 92342530004 MW-21 EPA 3510 363162 EPA 8082 363349 92342530005 MW-22 EPA 3510 363162 EPA 8082 363349 92342478004 MW-1 EPA 3510 363427 EPA 8082 363555 92342478005 MW-9 EPA 3510 363427 EPA 8082 363555 92342478003 MW-15 EPA 8151 372315 EPA 8151 372970 92342530001 MW-13 EPA 8151 373221 EPA 8151 373976 92342530002 MW-16 EPA 8151 373221 EPA 8151 373976 92342530003 MW-17 EPA 8151 373221 EPA 8151 373976 92342530004 MW-21 EPA 8151 373221 EPA 8151 373976 92342530005 MW-22 EPA 8151 373221 EPA 8151 373976 92342478004 MW-1 EPA 8151 373221 EPA 8151 373976 92342478005 MW-9 EPA 8151 373221 EPA 8151 373976 92342478001 MW-311 EPA 3010A 363009 EPA 6010 363688 92342478002 MW-23 EPA 3010A 363009 EPA 6010 363688 92342478003 MW-15 EPA 3010A 363010 EPA 6010 363689 92342530001 MW-13 EPA 3010A 363146 EPA 6010 364135 92342530002 MW-16 EPA 3010A 363146 EPA 6010 364135 92342530003 MW-17 EPA 3010A 363146 EPA 6010 364135 92342530004 MW-21 EPA 3010A 363146 EPA 6010 364135 92342530005 MW-22 EPA 3010A 363146 EPA 6010 364135 92342478004 MW-1 EPA 3010A 363321 EPA 6010 364621 92342478005 MW-9 EPA 3010A 363321 EPA 6010 364621 92342478006 MW-7 EPA 3010A 363321 EPA 6010 364621 92342478007 MW-12S EPA 3010A 363322 EPA 6010 363795 92342478008 MW-14 EPA 3010A 363322 EPA 6010 363795 92342478009 MW-18 EPA 3010A 363322 EPA 6010 363795 92342478010 MW-19 EPA 3010A 363322 EPA 6010 363795 92342478011 MW-20 EPA 3010A 363322 EPA 6010 363795 92342478001 MW-3R EPA 3010A 363272 EPA 6020B 363377 92342478002 MW-23 EPA 3010A 363272 EPA 6020B 363377 92342478003 MW-15 EPA 3010A 363272 EPA 6020B 363377 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 151 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: SURRY CLOSED -MT. 92342478 AIRY (UIC) Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92342530001 MW-13 EPA 3010A 363478 EPA 6020B 363771 92342530002 MW-16 EPA 3010A 363478 EPA 6020B 363771 92342530003 MW-17 EPA 3010A 363478 EPA 6020B 363771 92342530004 MW-21 EPA 3010A 363478 EPA 6020B 363771 92342530005 MW-22 EPA 3010A 363478 EPA 6020B 363771 92342478004 MW-1 EPA 3010A 363273 EPA 6020B 363378 92342478005 MW-9 EPA 3010A 363273 EPA 6020B 363378 92342478006 MW-7 EPA 3010A 363273 EPA 6020B 363378 92342478007 MW-12S EPA 3010A 363273 EPA 6020B 363378 92342478008 MW-14 EPA 3010A 363273 EPA 6020B 363378 92342478009 MW-18 EPA 3010A 363273 EPA 6020B 363378 92342478010 MW-19 EPA 3010A 363273 EPA 6020B 363378 92342478011 MW-20 EPA 3010A 363273 EPA 6020B 363378 92342478003 MW-15 EPA 7470 363333 EPA 7470 363334 92342530001 MW-13 EPA 7470 363457 EPA 7470 363483 92342530002 MW-16 EPA 7470 363457 EPA 7470 363483 92342530003 MW-17 EPA 7470 363457 EPA 7470 363483 92342530004 MW-21 EPA 7470 363457 EPA 7470 363483 92342530005 MW-22 EPA 7470 363457 EPA 7470 363483 92342478004 MW-1 EPA 7470 363459 EPA 7470 363485 92342478005 MW-9 EPA 7470 363459 EPA 7470 363485 92342478003 MW-15 EPA 3510 363842 EPA 8270 364328 92342530001 MW-13 EPA 3510 364049 EPA 8270 364817 92342530002 MW-16 EPA 3510 364049 EPA 8270 364817 92342530003 MW-17 EPA 3510 364049 EPA 8270 364817 92342530004 MW-21 EPA 3510 364049 EPA 8270 364817 92342530005 MW-22 EPA 3510 364049 EPA 8270 364817 92342478004 MW-1 EPA 3510 364049 EPA 8270 364817 92342478005 MW-9 EPA 3510 364049 EPA 8270 364817 92342478001 MW-3R EPA 8260 363024 92342478002 MW-23 EPA 8260 363024 92342478003 MW-15 EPA 8260 363024 92342530001 MW-13 EPA 8260 363026 92342530002 MW-16 EPA 8260 363026 92342530003 MW-17 EPA 8260 363026 92342530004 MW-21 EPA 8260 363307 92342530005 MW-22 EPA 8260 363026 92342478004 MW-1 EPA 8260 363328 92342478005 MW-9 EPA 8260 363328 92342478006 MW-7 EPA 8260 363328 92342478007 MW-12S EPA 8260 363328 92342478008 MW-14 EPA 8260 363328 92342478009 MW-18 EPA 8260 363328 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/19/2017 01:10 PM without the written consent of Pace Analytical Services, LLC. Page 152 of 166 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: SURRY CLOSED -MT. AIRY (UIC) Pace Project No.: 92342478 Lab ID Sample ID QC Batch Method QC Batch 92342478010 MW-19 EPA 8260 363328 92342478011 MW-20 EPA 8260 363328 92342478003 MW-15 SM 4500-S2D 363621 92342530001 MW-13 SM 4500-S2D 363623 92342530002 MW-16 SM 4500-S2D 363623 92342530003 MW-17 SM 4500-S2D 363623 92342530004 MW-21 SM 4500-S2D 363623 92342530005 MW-22 SM 4500-S2D 363623 92342478003 MW-15 SM 4500-CN-E 362992 92342530001 MW-13 SM 4500-CN-E 363513 92342530002 MW-16 SM 4500-CN-E 363513 92342530003 MW-17 SM 4500-CN-E 363513 92342530004 MW-21 SM 4500-CN-E 363513 92342530005 MW-22 SM 4500-CN-E 363513 Date: 06/19/2017 01:10 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Method Analytical Batch Page 153 of 166 �7aoAnalytical Laboratory receiving samples: Asheville ❑ Eden❑ Sample Condition Upon Receipt{SCUR) Page 1 of 2 Document No.: I ssu Ing Authority: F-CAR-CS-033-Rev.01 Pace Quality Office Greenwood ❑ Huntersvllle(]� Raleigh❑ Mechanicsville❑ Sample Condition Upon Client Name: WO# : 92342475 Receipt N( 0 Project Courier: ❑Fed Ex ❑U ❑LISPS []Client ❑ Commercial 11--�ce ❑other: 92342478 Custody Seal Present? ❑Yes Seals Intact? Dyes Date/Initials Person Examining Contents: Packing Material: []Bubble Wrap bble Bags ❑None ❑Other: Thermometer: �— tet ❑Blue ❑None I,Gun ID: Iype,of Ice: Correction Fa or: Cooler Temp Corrected (°C): Temp should be above freezing to 6°C USDA Regulated Soil ( r)/A, water sample) Did sampl riginate i arantine zone within the United States: CA, NY, or SC (check maps)? I—lyP.R rldn ' 5 mples on ice, cooling process has begun Biological Tissue Frozen? Des N�Jft ❑N/A Did samples originate from a foreign source (ii teTTionaliy, Comments/Discrepancy: Chain of Custody Present? es LINO ❑N/A 1. Samples Arrived within Hold Time? es ❑No ❑N/A 2. Short Hold Time Analysis (<72 hr.)? ❑Yes o ❑N/A 3. Rush Turn Around Time Requested? ❑Yes o ❑N/A 4. Sufficient Volume? Na ❑N/A S. Correct Containers Used? -Pace Containers Used? -0— es s ❑No []No ❑N/A ❑N/A 6. Containers Intact? s ❑No ❑N/A 7. Samples Field Filtered? ❑Yes ❑No A 8. Note if sediment is visible in the dissolved container Sample Labels Match COC? -Includes Date/Time/ID/Analysis Matrix: Headspace in VOA Vials (>5-6mm)? Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes El Yes ❑Yes [:]Yes❑No )lo // a 4. ❑N/A ❑N/A ❑LN/A /A 9. CW 1 �(� rgxi � slut"k �, "I +" t. nU 10. 11. CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Sample Discrepancy: Date/Time: Field Data Required? []Yes ❑No Project Manager SCURF Review: [ Date: (c/Z/f ? Project Manager SRF Review: { e Date: G/Z� Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers) Page 154 of 166 Document Name: Document Revised: Sept. 21, 2016 aeeAnalytical Sample Condition Upon Receipt(SCUR) Page 2 of 2 Document No.: issuing Authority: F-CAR-CS-033-Rev.01 Pace Quality dffice *Check mark top half of box if pH and/or dechlorination Project' WO# ; 92342478 is verified and within the acceptance range for 1 PM: RWC Due Date: 06/14/17 preservation samples. **Bottom half of box is to list number of bottles 1 CLIENT: 92-Municipal m V ¢ = Q _ 0 U m C Q ¢ n ¢ a � z m v Ys ? ? N v + j m v v Z ¢ v v v a a Y n Z v aNi a+ u ro v a Q � 0 m = m c c c :i O z Q 0 2 c q N E z z v o a42 > > a N Z z e U N z Q +n a CL ^ ? a a u u S N Z y 7 2 J C] m C m r N u u u t a v E m Z x s Y a = m 2 M � o a n n E O Q ¢ ¢ Q y d iu a a a a a a g a E E Q E ¢ ry O q q O a p_ N 0 E Q Q J 7 N E E E E E E E E ro n w E a` E ran a E Ln o o ._ p o 0 0 +gam = - o, 0 s.7 0 0 0 } in o N N In ri N N N N rl r-1 N .-I N a Y ``"'-' ri N E 7 7 M Z N m t�s 7 2 en to M a = (n M d X U' 6nn N E a m eV CL m M M M 0 0 m 0 m M m m a 0 ¢ ° m m m m m m m m 3 a a a d Q Q a 7 � 0 O 4M � 3 a s 6 7 S 9 10 11 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot # Page 155 of 166 Document Name: Document Revised: Sept. 21, 2016 Sample Condition Upon Receipt(SCUR) Page 2 of 2 __ aeeAnalytical Document No.: issuing Authority: F-CAR-CS-033-Rev.01 Pace Quality Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. **Bottom half of box is to list number of bottles Projec*`" hU : 92342478 P9 2— PM: RWC Due Date: 06/14/17 CLIENT: 92—Municipal Q Y 2 Z Z Z. Z N C Z N Z N N '-f a w m v v v ^ v 2 2 ¢ a N N a c o v a Z z GJ N d `a a `o a O " 2 b a a a a O 4 0 LA C C C Q N z Z O U' C U O N E ? ✓1 2 2 O c T = N Z y 2 = = S J U m u U u u u U u s w iu E 2 faM ro I fa fa m Na a a �o a a a a ° E E d E ¢ N O � a a J � 7 > E E E y E E E E -o v a` E `m E m E E E N-S 0 r+ O Ln c-i N o ,1 a O V 7 6 j 6 Z N V u 2 2 fA VA d 2 F= y4 a a a 0M. a a a l7 l7 ID 0 LO (7 Q 0 m m m m CO m m CO 3 a a a d d d o> s Y 2 3 4 S 6 7 S 9 10 11 12 n z },- I I Oi z ¢ 4 O E O Q j a Z a O E O IT O - Ln M N a " W >7 � 7 Q �a V 7 z a N E N H � CL Ln z C °- n E Ln r NLq Zn o Z a E In N a m C U G U E � > [7 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot# Page 156 of 166 ..PaceAnaiytrca1 Section A Required Client Information: Company Municipal En ineerin� Address: P.O. Box 97 Garner, NC 27529 Email To: j pfohl(Wiresro.Com Phone: 919-772-5393 Fax Requested Due DatefrATl 10 Day (E SAMPLE ID One Character per box. (A-Z, 0-9 1, -1 Sample Ids must be unique = L L, ; Lrt F 1 MVtf-1 L MW-3R 2 3 MW-7 L 4 MW-g (J 5 MW-11 L 6 MW-12S 4 7 MW-13 8 MW-14 L MW-15 9 MW-16 10 11 MW-17 12 1 MvV-18 ADDITIONAL COMMENTS Section B Required Project Information Report To: Jonathan Pfohl Copy To: Purchase Order No. Client Project ID. Slurry Closed -Mt. Container Order Number, CHAIN -OF -CUSTODY 1 Analytical Request Document t� 1 The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. 5 �� cK-1 w Section C m !Z Invoice Information: Pa e : 1 Of 2 Attention. Municipal Engineering Services Company Name: Address: 1 Regulatory Agency Pace Quote Reference: ,Iry (UIC) Pace Project Manager: Trey Carter State! Location Pace Profile #: 2103-316 North Carolina Requested Analysis Filtered (Y/N) Z I COLLECTED Preservatives N N N N N N N N N N w MATRIX ranE Drmkog W.I. DW Wabr or U ZD h V U oie vPJvu o Li START END a a O Poe m ¢ T S., .1-d SL 9 4 1 y C Oil OL We WP m V N ~ _ AIr AA V ¢ ¢ atria OT w a z .n m r N ry a L U d O m t] T— Ts Q a ¢ m to w c m w J•+�� w ZO O 10 Q Q v t 6 U n >J n O U O t ` L a m r w DATE TIME DATE TIME # _ _ = Z Z O � `cm VVT G 4 1 3 x x x x x x x x . G "i�i �7'-L7 4 1 3 x x BYYI,AFFILIATION DATE TIME PLER NAME AND SIGNATURE SIGNATURE of SAMPLER: ACCEPTED BY! AFFILIATION Pfohl DATE Signed: DATE I TIME 777-7 iSCD SAMPLE CONDITIONS m _ U c o m 10 5 Z a} m �9 UU ,� . 11/tnalyAlca! Section A Required Client Information Company: Municipal Engineerinc Address: P.O. Box 97 Garner, NC 27529 Email To: 0pfohl@mesco.com Phone', 919-772-5393 Fax Requested Due DateFAT: 10 DaV (C Section B Information: athan Pfohl Purchase Order No. Client Project ID Slurry Closed -Mt. Container Order Number: w 0 00 CHAIN -OF -CUSTODY / Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. o_ Section C Invoice Information: Page: 2 4f 2 AttenticnMunicipal Engineering Services Company Name: Address: Regulatory Agency Pace Quote Reference'. ,iry (UIC) Pace Project Manager Trey Carter State I Location Pace Profile #: 7 V I North Carolina Requested Analysis Futered (YIN) Z COLLECTED Preservatives >- N N N N NJ N N N N N N M MATRtx CO3)E Q 4 OI�king Wale' I1W Wale' WT SAMPLE ID waaewaler wW a o START END a m a PraaIe a One Character per box. sanrselm sr (A-Z. 0-9 1, -} w flc OLwp [p.> y m c n a rn Sample Ids must be unique mr AR Q N Other o7 Z p n L m p m 1� Ti;we 75 w 00 Y v N N V� o m Q O W 1?' 5 a ' 7 nu I U I m C) 0 o 2 a N N m -di � y 'U [.+ t E 'E F i .'✓� (/ 4 4 m DATE TIME DATE TIME 4 rn O a C O N = Z 2 Vcl z z 2 O O 0. T d rn h 5 1 MW-19 yIII- G 1 1 ;�gl 11 -C 4 1 3 1 1 1 1 x x 2 MW-20 3 MW-21 L 4 MW-22 G 5 MW-23 6 7 8 9 11l ti 12 ,A.—% ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION DATE TIME ACCEPTED BY 1 AFFILIATION DATE TIME SAMPLE CONDITIONS 1 SAMPLER NAME AND SIGNATURE a m PRINT Name of SAMPLER: Jo athan Pfohl0. C a n -- Z �_ mZ a `9 Y o SIGNATURE of SAMPLER:+ DATE Signed: ) \\fir f '� M H u o U a E _Z vs } �aceAnalXical0 UOcument Name: Sample Condition Upon Receipt(SCUR) Document No.: F-CAR-CS-033-Rev.0 Document Revised: Sept. 21, 201b Page 1 of 2 Issuing Authority: Pace Quality Office Laboratory receiving samples: Asheville ❑ Eden[] Courier: ❑ Commercial Custody Seal Present? Greenwood [] Huntersvillex Raleigh❑ Mechanicsville❑ r._ ClientName:�WO# 92342478 roject #: PM: RWC Due Date: 06/14/27 ❑Fed Ex ❑UPS ❑USPS ❑Client CLIENT: 92—Municipal Place ❑Other. []Yes PNo seals Intact? ❑Yes ®No Date/initials Person Examining Co Packing Material: ❑Bubble Wrap ®Bubble Bags ❑None 70ther: Thermometer 1 ❑ IR Gun ID: _ Type of ice: Wet ❑Blue ❑None ❑Samples on ice, cooling process has begun Correction Factor: Cooler Temp Corrected (°C): n Biological Tissue Frozen? []Yes [ No [—]N/A Temp should be above freezing to 6°C USDA Regulated Soil (❑ N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, IlYes M. A m_ oi'..573 rw..' Mhi- y Comments/Discrepancy: Chain of Custody Present? Yes ❑No []N/A 1. Samples Arrived within Hold Time? INYes ❑No ❑N/A 2. Short Hold Time Analysis (02 hr.)? ❑Yes NNo ❑N/A 3. Rush Turn Around Time Requested? ❑Yes No ❑N/A 4. Sufficient Volume? Yes ❑No ❑N/A 5. Correct Containers Used? -Pace Containers Used? ®Yes Yes ❑No ❑No ❑N/A ❑N/A 6. Containers Intact? Yes ❑No ❑N/A 7. Samples Field Filtered? []Yes No []N/A 8, Note if sediment is visible in the dissolved container Sample Labels MatchCOC? Includes Date/Time/ID/Analysis Matrix: ❑Yes JQNo ❑N/A 9.l�id6i ""Pte,3'`AL0 3ii�1) — t lj!)?tL % 1 Headspace in VOA Vials (>5-6mm)? ❑Yes No ❑N/A 10. ! % / Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes ❑Yes [ fNo I _No ❑N/A ❑N/A 11. j it -� U Lt sZ� 1 C." - �[i�- Z__. (*[ CLIENT NOTIFICATION/RESOLUTION Person Contacted: Commen' ,/Sample Discrepancy: Date/Time: Field Data Required? ❑Yes ❑No Project Manager SCURF Review: (L date: ; Project Manager 5RF Review: CC Date: !°NI Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers) Page 159 of 166 Document Name: Document Revised: Sept. 21, 2016 Sample Condition Upon Receipt(SCUR) Page 2 of 2 1� ,jC aceAnalytieal Document No.: Issuing Authority: 1 F-CAR-CS•033-Rev.01 Pace Quality Office *Check mark top half of box if pH and/or dechlorination Project # Wa# : 92342478 is verified and within the acceptance range for PM: RWC Due Date: 06/14/17 preservation samples. CLIENT: 92-Municipal **Bottom half of box is to list number of bottles U 0 u Q Z a v a c Z) u d E n cN-I m Z a m ` c a u 0. E O N j a. z v Z c � V d E o N 3 a. ? d v a 16 w !l ei m U v x a O 2 V 0,Q a N 0 m M a O =z N E b N z m =O z 06 ,01, ro N u d E q N N m u �- N A _ a O m Z u 0. E O N u m a 7 @ d E o 3 v Q � v i W o E Q = rl e.i U a ry v E Q = ri x ea C9 a a v m a]a E ¢ J ` v�i tV co 0 a � M L E a `m J, .4 C7 a w a N 07 Q J 0,� v� m C7 a < z z E d r`nv m lJ 8 ¢ m C7 a 2 ¢ O E o x M Q a Oz ti M Z Q O E a d Cn rn C7 7 a Q O E o C m W > ¢ O h ¢ O E a V In m 14 a o y a N '4 a O n ¢ Y a Z a N '° } .M.� ac C7 a � d y V) J E N ri N .n d N f0 ¢ ? a 61 a `v, J E N r e� a v, of cv v O ve z U m a J E N m a m c s 2 U z o M c J rev 7 (7 H Z 11 1 IN N N N I `.. 2 3 \ I \ ') — 4 \\,NN 3 5 6 i N\j\\ 9 10 11 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot # Page 160 of 166 N ro O -c v v m m a K ro v x c a n � o _ D Q 4 = w H iii .r � v rD m rt d r o O 7 M a a O C � N ro T n fa y i9 C m w a N N N ro N � o rp b 0 0 C M m D n D_ v ro m n m m K m Ja h+ Y Y N Y o lD D> __J m N A Lo N N Item# z—zzzzzzz—zzzz.. BP4U-125 mL Plastic Unpreserved (N/A) (Cl-) BP3U-250 mL Plastic Unpreserved (N/A) EP2U-500 mL Plastic Unpreserved (N/A) BP1U-1 liter Plastic Unpreserved (N/A) BP3S-250 mL Plastic H2SO4 (pH < 2) (CI-) BP3N-250 mL plastic HNO3 (pH < 2) BP3Z-250 mL Plastic ZN Acetate & NaOH (>9) zz BP3C-250 mL Plastic MOH (pH > 12) (CI-) WGFU-Wide-mouthed Glass jar Unpreserved AG1U-1 liter Amber Unpreserved (N/A) (Cl-) :;�Z:72zz Zzzz AG11i-1liter Amber HCI (pH <2) AGN-250 mL Amber Unpreserved (N/A) (Cl-) AG1S-1 liter Amber H2SO4 (pH < 2) AG35-250 mL Amber H2SO4 {pH < 2} AG3A(DG3A)-250 mL Amber NH4CI (N/A)(CI-) uj DG9H-40 mL VOA HCI (N/A) VG9T-40 mL VOA Na2S203 (N/A) VG9U-40 mLVOA Unp (N/A) DG9P-40 mL VOA H3PO4 (N/A) VOAK (S vials per kit)-5035 kit (N/A) V/GK (3 vials per kit)-VPH/Gas kit (N/A) SPST-125 mL Sterile Plastic (N/A — lab) SP2T-250 mL Sterile Plastic (N/A— lab) zzz:7111 MA-250 mL Plastic (NH2)2504 (9.3-9.7) Cubitainer VSGU-20 mL Scintillation vials (N/A) GN * -O O S O� ON '+ ns a � w CL O v * O 3 z3 X �^ S d, O CD Cr v O cn n x 3 3 Cr nffl 3 f9 7 v h O O Cr 0. O o n t S v, O 3 0 O .Q O r CHAIN -OF -CUSTODY ! Analytical Request Document �eanar i The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Required Client Information: Required Project Informatlon: Invoice Information: Pa E : 1 Of Campany Municipal Engineering Services Report To Jonathan Pfohl Attention, Municipal Engineering Services Address_ P.O. Box 97 Copy To Company Name' Garner, NC 27529 Address Regulatory Agency Email To (pfahl Cg)mescA.Com Purchase Order No. Pace Quote Reference'. Phone: 919-772-5393 Fax Client Project ID: Surry Closed -Mt. Airy (UIC) Pace Project Manager Trey Carter State I Location Requested Due DalefrAT. 10 Day (Default) Container Order Number. Pace Profile #: North Carolina Requested Analvsls Filtered tYlNl Z I COLLECTED Preservatives N N N N N N N N N N a nna.TRix coot Drrniung W w Dw Z m a Walur VJT SAMPLE ID v✓vV wuecwaeer START END U ry n a U s rj O Prod P Q One Character per box. a Wv Iia sL Sample Ids must be unique A„ AR Dino: oT w W Z d Na rya Qa N mc O m a O 17 I J O O W mQ m QT.s a v W u 7 S= U z i J= E D a 6 TO N �. - N DATE TIME DATE TIME m 2 > E u- S a w I— cn 1 Nil WT G �a(I la'3S 1 3 x x x x x x x x 2 MW-3R P NlT G 1 3 x x 3 M W-7 W G a• SF T z x 4 MW-9vvf G 5MVV-11 Wr G 6I 1 3 x x x x x x x x B MW-125 VVT G 1� $4 4 1 3 x x 7 MW-13 WT G 4 1 3 x x x x x x x x 8 MW-14 WT G 1 TOO 4 1 3 x x 9 MW-15 l WT G 4 1 g x x x x xRTIME 10 MW 16 1 WT G 4 1 3 xxx11 MW-17 Mr G q 1 3 tX x x x 12 MW-18 VVT G fa I ja�Is 4 1 3 x x ADDITIONAL COMMENTS INQUISHED BY I AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION DATE Ton •Z � NAME AND SIGNATURE Pfohl W SAMPLER: DATE Signed: I -„ �"eAnalyhtal Section A Reouired Client Information: 919- 10 SAMPLE ID One Character per box. tA-T, 0-91, -] Sample Ids must be unique ill F- 1 M4N-19 2 MW-20 3 MW-21 4 Mw-22 5 MW-23 6 9 10 11 12 p ADDITIONAL COMMENTS CHAIN -OF -CUSTODY If Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section B Section C Required Project Information: Invoice Informatlon: Page : 2 Of 2 Purchase Order No. "`- Client Project lD: Surry Closed -Mt. Airy (UIC) Pace Project Manager Trey Carter State I Location Container Order Number: Pace Profile 9 North Carolina Requested Analysis Filtered (Y/N] z COLLECTED Preservatives r N N N N N N N IN N N �' hl a _ MATRIX CODE a or�aag w— trvv Water wr w11'I , ww �y END F -- U Cj 1 ouct P Pid Sa USOIId SL - START 4 W �+ m ¢ W w Oil Oi Wipe WP AR `-< v o Ln m ar Omn oT a a z ino N w ry r i n -c U 91 J C Tlasuo TS a u I f;l fI' 1 t r F o Z m O _ a a a a o c b g n U1 U C Q U u� DATE TIME DATE TIME v¢} a C = = S z z ,;u O 0 g li = a N in VVT G C :1 �t`N� 4 1 1 3 3 x x WT G b(t 3. 0 A x x L7 BY f AFFILIATION DATE I TIME ACCEPTED BY 1 AFFILIATION DATE TIME SAMPLER NAME AND SIGNATURE PRINT Name of SAMPLER: Orl an NOW SIGNATURE of SAMPLER: DATE Signed: SAMPLE CONDITIONS a o - y z o `m - Cry U 0 In �ZeAnalytical® Laboratory receiving samples: Asheville ❑ Eden❑ Document Name: Document Revised: Sept. 21, 2016 Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.01 Pace Quality Office Greenwood ❑ Huntersviile,E Raleigh❑ Mechanicsville❑ ConditionSample p+ ClientNarne: F" 92342478 ReceiDt Projectile WO# . mg/14/1'? Courier: Due Date: ❑ Commercial ❑F d Ex UPS ❑USPS Client PM� RWCtynicip ❑ al Pace ❑Other; CL104T : 92— Custody Seal Present? ❑Yes No Seals intact? ❑Yes ❑No Packing Material: ❑Bubble Wrap EYubble Bags []None ❑Other: Thermometer: �pe ❑IRGunID: ° of Ice: wet ❑Blue ❑None ❑�ples on ice, cooling process has begun Correction Factor: Cooler Temp Corrected { � Biological Tissue Frozen? ❑Yes ❑No �A Temp should be above free 'ng to 6°C USDA Regulated Soil ( [?N/A, water sample) Did samples origina%rfn�a quarantine zone within the United States: CA, NY, or SC (check maps)? Chain of Custody Present? Samples Arrived within Hold Time? Short Hold Time Analysis (<72 hr.)? Rush Turn Around Time Requested? Sufficient Volume? Correct Containers Used? -Pace Containers Used? Containers Intact? Samples Field Filtered? Sample Labels Match COC? -includes Date/Time/ID/Analysis Matrix:�� Headspace in VOA Vials (15-6mm)? Trip Blank Present? Trip Blank Custody Seals Present? CLIENT NOTIFICATION/RESOLUTION Person Contacted: Commence /Sample Discrepancy: Project Manager SCURF Review: Project Manager SRF Review: IJNo uN/A 1 1, []No ❑N/A 2. 60 ❑N/A 3. dNo ❑N/A 4. []No ❑N/A 5. ❑No ❑N/A 6. lJYes LUNo LAN/A 7. Des []No 2 N/A 8. Noi El Yes EKO ❑N/A 9. W 1JYes UNo UN/A 10. El Yes ❑No d/A 11. []Yes ❑Na N!A Date/Initials Person Examining ContdnWll Did samples originate from a foreign source (inttionally, including Hawaii and Puerto Rico)? []Yes Na Comments/Discrepancy: e if sedi eq is visible in the - solved container c� J Field data Required? ❑Yes ❑No Date/Time: Pate:, A- I7 Date: Co/5 17 Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers) Page 164 of 166 3 m Q �C 0 m m a m 2 v 0 n rb _ D CL O r► m v mrb w r- o 3 UQ _ O o -0 a fD Ln rD � C n CL C a � N � In' � a � � 0 rp n 0 0 m o IL Q v m a m 2 a t 0 Item# zzzzzzzzzzzz BP4U-125 mL Plastic Unpreserved (N/A) (CI-) BP3U-250 mL Plastic Unpreserved (N/A) BP2U-500 mL Plastic Unpreserved (N/A) BP1U-1 liter Plastic Unpreserved (N/A) BP3S-250 mL Plastic H2SO4 (pH < 2) (Cl-) BP3N-250 ml plastic HNO3 (pH < 2) BP3Z-250 mL Plastic ZN Acetate & NaOH (>9) f BP3C-2S0 mL Plastic NaOH (pH > 12) (CI-) GFU-Wide-mouthed Glass jar Unpreserved �-IA V I CJ( V ` I AG1U-1 liter Amber Unpreserved (N/A) (CI-) ,xXxxZZZ—zz,zzz,xz AG111-1 liter Amber HC1(pH <2) AG3U-250 mLAmber Unpreserved (N/A) (CI-) AGIS-1 liter Amber H2SO4 (pH < 2) AG3S-250 mL Amber H2SO4 (pH < 2) AG3A(DG3A)-250 mLAmber NH4CI (N/A)(CI-) AG91-11-40 mL VOA HCl (N/A) VG9T-40 mL VOA Na2S203 (N/A) VG9U-40 mLVOA U n p (N/A) DG9P-40 mL VOA H,PO4 (N/A) VOAK (b vials per kit)-5035 kit (N/A) V/GK (3 vials per kit)-VPH/Gas kit (N/A) SPST-125 mL Sterile Plastic (N/A- lab) SP2T-250 mL Sterile Plastic (N/A -lab) Axx BP3A-250 mL Plastic (NH2)2SO4 (9.3-9.7) Cubitainer VSGU-20 ml.Scintillation vials (N/A) i T1 GN o M rp c 5 �k m a S G Cu v � � y Q. C x H 3 rr rn X r+ m O Cu vi n �* m 3 � O QY Cr n m m � z 0 Di h O tS OQ m R O m v, C9 m A r+ -4 O r+ U N N 4k 4 Co CHAIN -OF -CUSTODY 1 Analytical Request Document 6 IZAnalAicat The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. a m Section A Section B Section C Required Client Information: Required Project Information: Invoice Information: Page : Of Company. Municipal Engineering Services Report To Jonathan Pfohl Attention: Municipal Engineering Services Address: P.O. Box 97 Copy TO: Company Name: Garner, NC 27529 Address: Regulatory Agency Email To: jpfohl &mesco.com Purchase Order No. r IV }3 �' ' ry �nr �,'�„ Pace Quote Reference: Phone: 919-772-5393 JFax (919) 772-1176 Client Project ID: Pace Project Manager Trey Carter State! Location Requested flue DalerTAT: 10 Day (Default) Container Order Number: Pace Profile #: 2103-6 North Carolina Requested Analysis Filtered (YIN) 2 COLLECTED Preservatives N N N N N N N N Y M%TRIx CODE c D-king wale[ Dw o `.-'4 `"s Wr V = SAMPLE ID Poeewat° ww v START END One Character per box. 5om5oib s4 (A-Z,D-91,-} ail oL w,Pe wP p m ¢ p " m l Sample Ids must 4e unique A., AR ¢ Ulf- Olhe, OT�— T,-.. TS < 9 ry N x o ti v O L 111 r W a y O X = O N= r Q U O m ~ 0 DATE TIME DATE TIME N u : = z z 2 D 7 D [1 1 h Ctrfi9GiJ � w � :J 4141iV G S 1 �] �- 1 3 X X X X X X X X X X ay , 2 MW-IL,=sc CC 3 4 MVJ •�� i 6 7 8 9 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY r AFFILIATION DATE TIME ACCEPTED BY 1 AFFILIATION DATE TIME SAMPLE CONDITIONS SJ410:7 SAMPLER NAME AND SIGNATURE ten' u 0 o m Z m Z co y c PRINT Name of SAMPLER: Joltipan Pfohl SIGNATURE of SAMPLER: DATE Signed: 5 ` �+ 2 w m} m m -6 7 0 E z r \; @, lacieAnalXical" www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 June 26, 2017 Mr. Jonathan Pfohl Municipal Engineering Services 68 Shipwash Dr. Garner, NC 27529 RE: Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory between June 01, 2017 and June 02, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Trey Carter trey. carter@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 Lab ID Sample ID Matrix Date Collected Date Received 92342553001 MW-15 Water 05/31/17 17:00 06/01/17 07:55 92342553002 MW-21 Water 05/31/17 17:20 06/01/17 07:55 92342553003 MW-1 Water 06/01/17 12:35 06/02/17 08:00 92342553004 MW-7 Water 06/01/17 14:45 06/02/17 08:00 92342553005 MW-9 Water 06/01/17 15:40 06/02/17 08:00 92342553006 MW-14 Water 06/01/17 09:00 06/02/17 08:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: SURRY CLOSED -MT. AIRY (MNA) 92342553 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92342553001 MW-15 SM 2320B KDF1 1 PASI-A SM 3500-Fe B CJH1 1 PASI-A EPA 300.0 CDC 1 PASI-A SM 4500-CI-E DMN 1 PASI-A SM 5220D CJH1 1 PASI-A SM 5310B KDF1 1 PASI-A 92342553002 MW-21 SM 2320B KDF1 1 PASI-A SM 3500-Fe B CJH1 1 PASI-A EPA 300.0 CDC 1 PASI-A SM 4500-CI-E DMN 1 PASI-A SM 5220D CJH1 1 PASI-A SM 5310B KDF1 1 PASI-A 92342553003 MW-1 SM 2320B KDF1 1 PASI-A SM 3500-Fe B CJH1 1 PASI-A SM 4500-S2D MVC 1 PASI-A EPA 300.0 CDC 1 PASI-A SM 4500-CI-E CJH1 1 PASI-A SM 4500-CN-E AES2 1 PASI-A SM 5220D CJH1 1 PASI-A SM 5310B KDF1 1 PASI-A 92342553004 MW-7 SM 2320B KDF1 1 PASI-A SM 3500-Fe B CJH1 1 PASI-A SM 4500-S2D MVC 1 PASI-A EPA 300.0 CDC 1 PASI-A SM 4500-CI-E CJH1 1 PASI-A SM 5220D CJH1 1 PASI-A SM 5310B KDF1 1 PASI-A 92342553005 MW-9 SM 2320B KDF1 1 PASI-A SM 3500-Fe B CJH1 1 PASI-A SM 4500-S2D MVC 1 PASI-A EPA 300.0 CDC 1 PASI-A SM 4500-CI-E CJH1 1 PASI-A SM 4500-CN-E AES2 1 PASI-A SM 5220D CJH1 1 PASI-A SM 5310B KDF1 1 PASI-A 92342553006 MW-14 SM 2320B KDF1 1 PASI-A SM 3500-Fe B CJH1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 Analytes Lab ID Sample ID Method Analysts Reported Laboratory SM 4500-S2D MVC 1 PASI-A EPA 300.0 CDC 1 PASI-A SM 4500-CI-E CJH1 1 PASI-A SM 5220D CJH1 1 PASI-A SM 5310B KDF1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 Sample: MW-15 Lab ID: 92342553001 Collected: 05/31/17 17:00 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 43700 ug/L 5000 1000 1 06/03/17 09:30 Iron, Ferrous Analytical Method: SM 3500-Fe B Iron, Ferrous 1.7 mg/L 0.50 0.50 1 06/06/17 01:32 H1,N2 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate 11801 ug/L 250000 500 1 06/05/1718:27 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E Chloride 1450 ug/L 1000 500 1 06/05/1711:22 16887-00-6 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand ND ug/L 25000 12500 1 06/09/17 04:30 531013 TOC Analytical Method: SM 5310B Total Organic Carbon 675J ug/L 1000 500 1 06/03/17 00:35 7440-44-0 Date: 06/26/2017 04:24 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 Sample: MW-21 Lab ID: 92342553002 Collected: 05/31/17 17:20 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 34900 ug/L 5000 1000 1 06/03/17 09:42 Iron, Ferrous Analytical Method: SM 3500-Fe B Iron, Ferrous ND mg/L 0.50 0.50 1 06/06/17 01:32 H1,N2 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate 1380J ug/L 250000 500 1 06/05/1719:36 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E Chloride 28800 ug/L 1000 500 1 06/05/1711:26 16887-00-6 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand ND ug/L 25000 12500 1 06/09/17 04:30 531013 TOC Analytical Method: SM 5310B Total Organic Carbon 1200 ug/L 1000 500 1 06/03/17 00:46 7440-44-0 Date: 06/26/2017 04:24 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 Sample: MW-1 Lab ID: 92342553003 Collected: 06/01/17 12:35 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 42200 ug/L 5000 1000 1 06/06/17 01:12 Iron, Ferrous Analytical Method: SM 3500-Fe B Iron, Ferrous ND mg/L 0.50 0.50 1 06/06/17 01:32 H1,N2 4500S2D Sulfide Water Analytical Method: SM 4500-S2D Sulfide ND ug/L 1000 100 1 06/06/17 21:30 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate 8830J ug/L 250000 500 1 06/10/1719:44 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E Chloride 3770 ug/L 1000 500 1 06/14/17 02:48 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E Cyanide ND ug/L 10.0 4.0 1 06/24/1718:46 57-12-5 H1 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand ND ug/L 25000 12500 1 06/09/17 04:30 531013 TOC Analytical Method: SM 5310B Total Organic Carbon 605J ug/L 1000 500 1 06/07/17 03:09 7440-44-0 Date: 06/26/2017 04:24 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 Sample: MW-7 Lab ID: 92342553004 Collected: 06/01/17 14:45 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 69200 ug/L 5000 1000 1 06/06/17 01:24 Iron, Ferrous Analytical Method: SM 3500-Fe B Iron, Ferrous ND mg/L 0.50 0.50 1 06/06/17 01:32 H1,N2 4500S2D Sulfide Water Analytical Method: SM 4500-S2D Sulfide ND ug/L 1000 100 1 06/06/17 21:30 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate 5520J ug/L 250000 500 1 06/10/17 20:01 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E Chloride 31200 ug/L 1000 500 1 06/14/17 02:49 16887-00-6 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 20000J ug/L 25000 12500 1 06/09/17 04:30 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 2400 ug/L 1000 500 1 06/07/17 03:20 7440-44-0 Date: 06/26/2017 04:24 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 9 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 Sample: MW-9 Lab ID: 92342553005 Collected: 06/01/17 15:40 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 44800 ug/L 5000 1000 1 06/06/17 01:55 Iron, Ferrous Analytical Method: SM 3500-Fe B Iron, Ferrous 1.3 mg/L 0.50 0.50 1 06/06/17 01:32 H1,N2 4500S2D Sulfide Water Analytical Method: SM 4500-S2D Sulfide ND ug/L 1000 100 1 06/06/17 21:30 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate 984J ug/L 250000 500 1 06/10/17 20:17 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E Chloride 28300 ug/L 1000 500 1 06/14/17 02:50 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E Cyanide 5.51 ug/L 10.0 4.0 1 06/14/1711:48 57-12-5 M1 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 23000J ug/L 25000 12500 1 06/09/17 04:30 531013 TOC Analytical Method: SM 5310B Total Organic Carbon 2250 ug/L 1000 500 1 06/07/17 03:34 7440-44-0 Date: 06/26/2017 04:24 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 Sample: MW-14 Lab ID: 92342553006 Collected: 06/01/17 09:00 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 31600 ug/L 5000 1000 1 06/06/17 02:06 Iron, Ferrous Analytical Method: SM 3500-Fe B Iron, Ferrous ND mg/L 0.50 0.50 1 06/06/17 01:32 H1,N2 4500S2D Sulfide Water Analytical Method: SM 4500-S2D Sulfide 115J ug/L 1000 100 1 06/06/17 21:30 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate 2060J ug/L 250000 500 1 06/11/17 01:18 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E Chloride 2280 ug/L 1000 500 1 06/14/17 02:51 16887-00-6 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 13000J ug/L 25000 12500 1 06/09/17 04:30 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1420 ug/L 1000 500 1 06/07/17 03:49 7440-44-0 Date: 06/26/2017 04:24 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 QC Batch: 363125 Analysis Method: SM 2320B QC Batch Method: SM 2320B Analysis Description: 2320E Alkalinity Associated Lab Samples: 92342553001, 92342553002 METHOD BLANK: 2013190 Matrix: Water Associated Lab Samples: 92342553001, 92342553002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Alkalinity, Total as CaCO3 ug/L ND 5000 1000 06/05/17 12:06 LABORATORY CONTROL SAMPLE: 2013191 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 51100 102 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2013192 2013193 MS MSD 92342496001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 19.6 mg/L 50000 50000 70800 67200 103 95 80-120 5 25 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2013194 2013195 MS MSD 92342317011 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 32300 50000 50000 83100 82500 102 100 80-120 1 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/26/2017 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 QC Batch: 363343 Analysis Method: SM 2320B QC Batch Method: SM 2320B Analysis Description: 2320E Alkalinity Associated Lab Samples: 92342553003, 92342553004, 92342553005, 92342553006 METHOD BLANK: 2014291 Matrix: Water Associated Lab Samples: 92342553003, 92342553004, 92342553005, 92342553006 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Alkalinity, Total as CaCO3 ug/L ND 5000 1000 06/05/17 20:55 LABORATORY CONTROL SAMPLE: 2014292 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 50800 102 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2014293 2014294 MS MSD 92342317017 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 587000 50000 50000 642000 636000 110 97 80-120 1 25 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2014295 2014296 MS MSD 92342317020 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 135000 50000 50000 167000 169000 65 68 80-120 1 25 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/26/2017 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 QC Batch: 363473 Analysis Method: SM 3500-Fe B QC Batch Method: SM 3500-Fe B Analysis Description: Iron, Ferrous Associated Lab Samples: 92342553001, 92342553002, 92342553003, 92342553004, 92342553005, 92342553006 METHOD BLANK: 2015125 Matrix: Water Associated Lab Samples: 92342553001, 92342553002, 92342553003, 92342553004, 92342553005, 92342553006 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Iron, Ferrous mg/L ND 0.50 0.50 06/06/17 01:32 N2 LABORATORY CONTROL SAMPLE: 2015126 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Iron, Ferrous mg/L 1.5 1.5 102 90-110 N2 SAMPLE DUPLICATE: 2015127 92342553001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Iron, Ferrous mg/L 1.7 1.7 2 10 H1,N2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/26/2017 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 QC Batch: 363647 Analysis Method: SM 4500-S2D QC Batch Method: SM 4500-S2D Analysis Description: 4500S2D Sulfide Water Associated Lab Samples: 92342553003, 92342553004, 92342553005, 92342553006 METHOD BLANK: 2016111 Matrix: Water Associated Lab Samples: 92342553003, 92342553004, 92342553005, 92342553006 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfide ug/L ND 1000 100 06/06/17 21:30 LABORATORY CONTROL SAMPLE: 2016112 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 528J 106 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2016113 2016114 MS MSD 92342742003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 546J 573J 102 107 80-120 5 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2016115 2016116 MS MSD 92342742013 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 526J 553J 105 111 80-120 5 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/26/2017 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 QC Batch: 363396 Analysis Method: EPA 300.0 QC Batch Method: EPA 300.0 Analysis Description: 300.0 IC Anions Associated Lab Samples: 92342553001, 92342553002 METHOD BLANK: 2014592 Matrix: Water Associated Lab Samples: 92342553001, 92342553002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfate ug/L ND 250000 500 06/05/1716:44 LABORATORY CONTROL SAMPLE: 2014593 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate ug/L 50000 50400J 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2014594 2014595 MS MSD 92342317015 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 18200 50000 50000 68600J 69700J 101 103 90-110 2 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2014596 2014597 MS MSD 92342600004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 58400 50000 50000 60100J 97400J 3 78 90-110 47 10 M1,R1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/26/2017 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 QC Batch: 364291 Analysis Method: EPA 300.0 QC Batch Method: EPA 300.0 Analysis Description: 300.0 IC Anions Associated Lab Samples: 92342553003, 92342553004, 92342553005 METHOD BLANK: 2020011 Matrix: Water Associated Lab Samples: 92342553003, 92342553004, 92342553005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfate ug/L ND 250000 500 06/10/1711:47 LABORATORY CONTROL SAMPLE: 2020012 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate ug/L 50000 50200J 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2020015 2020016 MS MSD 92343524006 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 14.8 mg/L 50000 50000 63800J 65100J 98 101 90-110 2 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2020039 2020040 MS MSD 92343485001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 1830 mg/L 50000 50000 1860000 1860000 59 57 90-110 0 10 M6 J J Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/26/2017 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 QC Batch: 364314 Analysis Method: EPA 300.0 QC Batch Method: EPA 300.0 Analysis Description: 300.0 IC Anions Associated Lab Samples: 92342553006 METHOD BLANK: 2020086 Matrix: Water Associated Lab Samples: 92342553006 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfate ug/L ND 250000 500 06/11/17 00:44 LABORATORY CONTROL SAMPLE: 2020087 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate ug/L 50000 49000J 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2020088 2020089 MS MSD 92342553006 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 2060J 50000 50000 53600J 54700J 103 105 90-110 2 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2020090 2020091 MS MSD 92343524013 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 13.6 mg/L 50000 50000 67100J 65800J 107 104 90-110 2 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/26/2017 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 QC Batch: 363371 Analysis Method: SM 4500-CI-E QC Batch Method: SM 4500-CI-E Analysis Description: 4500 Chloride Associated Lab Samples: 92342553001, 92342553002 METHOD BLANK: 2014368 Matrix: Water Associated Lab Samples: 92342553001, 92342553002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Chloride ug/L ND 1000 500 06/05/1710:58 LABORATORY CONTROL SAMPLE: 2014369 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride ug/L 20000 19600 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2014370 2014371 MS MSD 92342674001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 80.8 mg/L 10000 10000 130000 130000 489 492 90-110 0 10 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2014372 2014373 MS MSD 92342496003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 2.3 mg/L 10000 10000 12300 12200 100 100 90-110 0 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/26/2017 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 QC Batch: 364538 Analysis Method: SM 4500-CI-E QC Batch Method: SM 4500-CI-E Analysis Description: 4500 Chloride Associated Lab Samples: 92342553003, 92342553004, 92342553005, 92342553006 METHOD BLANK: 2021020 Matrix: Water Associated Lab Samples: 92342553003, 92342553004, 92342553005, 92342553006 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Chloride ug/L ND 1000 500 06/14/17 03:57 LABORATORY CONTROL SAMPLE: 2021021 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride ug/L 20000 20400 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2021022 2021023 MS MSD 92342317019 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 318000 10000 10000 315000 173000 -22 -1450 90-110 58 10 M6,R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2021024 2021025 MS MSD 92343251002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 23.3 mg/L 10000 10000 32900 32900 96 96 90-110 0 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/26/2017 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 QC Batch: 364584 Analysis Method: SM 4500-CN-E QC Batch Method: SM 4500-CN-E Analysis Description: 450OCNE Cyanide, Total Associated Lab Samples: 92342553005 METHOD BLANK: 2021203 Matrix: Water Associated Lab Samples: 92342553005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Cyanide ug/L ND 10.0 4.0 06/14/1711:34 LABORATORY CONTROL SAMPLE: 2021204 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 99.1 99 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2021205 2021206 MS MSD 92343009001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 94.3 88.3 93 87 80-120 7 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2021207 2021208 MS MSD 92342553005 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L 5.5J 100 100 63.2 62.7 58 57 80-120 1 10 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/26/2017 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 QC Batch: 366221 Analysis Method: SM 4500-CN-E QC Batch Method: SM 4500-CN-E Analysis Description: 450OCNE Cyanide, Total Associated Lab Samples: 92342553003 METHOD BLANK: 2030002 Matrix: Water Associated Lab Samples: 92342553003 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Cyanide ug/L ND 10.0 4.0 06/24/17 20:31 LABORATORY CONTROL SAMPLE: 2030003 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 103 103 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2030004 2030005 MS MSD 92345320006 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 103 101 99 98 80-120 2 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2030006 2030007 MS MSD 92345112002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L 0.012 100 100 5.8J 15.1 -6 3 80-120 10 M1 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/26/2017 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 QC Batch: 364072 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92342553001, 92342553002, 92342553003, 92342553004, 92342553005, 92342553006 METHOD BLANK: 2018787 Matrix: Water Associated Lab Samples: 92342553001, 92342553002, 92342553003, 92342553004, 92342553005, 92342553006 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Chemical Oxygen Demand ug/L ND 25000 12500 06/09/17 04:30 LABORATORY CONTROL SAMPLE: 2018788 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand ug/L 750000 755000 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2018789 2018790 MS MSD 92343255002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chemical Oxygen Demand ug/L 469 mg/L 750000 750000 1140000 1080000 90 82 90-110 6 3 M1,R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2018791 2018792 MS MSD 92342740001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chemical Oxygen Demand ug/L 81.0 mg/L 750000 750000 877000 855000 106 103 90-110 3 3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/26/2017 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 QC Batch: 363127 Analysis Method: SM 5310B QC Batch Method: SM 5310B Analysis Description: 5310E TOC Associated Lab Samples: 92342553001, 92342553002 METHOD BLANK: 2013202 Matrix: Water Associated Lab Samples: 92342553001, 92342553002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Organic Carbon ug/L ND 1000 500 06/02/17 22:46 LABORATORY CONTROL SAMPLE: 2013203 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carbon ug/L 25000 23700 95 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2013204 2013205 MS MSD 92342496002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Total Organic Carbon ug/L 1.7 mg/L 25000 25000 24100 24900 90 93 90-110 3 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/26/2017 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 QC Batch: 363536 Analysis Method: SM 5310B QC Batch Method: SM 5310B Analysis Description: 5310E TOC Associated Lab Samples: 92342553003, 92342553004, 92342553005, 92342553006 METHOD BLANK: 2015350 Matrix: Water Associated Lab Samples: 92342553003, 92342553004, 92342553005, 92342553006 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Organic Carbon ug/L ND 1000 500 06/07/17 08:18 LABORATORY CONTROL SAMPLE: 2015351 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carbon ug/L 25000 25200 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2015352 2015353 MS MSD 92342745003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Total Organic Carbon ug/L 6.6 mg/L 25000 25000 28100 28000 86 86 90-110 0 10 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/26/2017 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville ANALYTE QUALIFIERS H1 Analysis conducted outside the EPA method holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. N2 The lab does not hold NELAC/TNI accreditation for this parameter. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/26/2017 04:24 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 33 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: SURRY CLOSED -MT. AIRY (MNA) Pace Project No.: 92342553 Lab ID Sample ID QC Batch Method QC Batch 92342553001 MW-15 SM 2320B 363125 92342553002 MW-21 SM 2320B 363125 92342553003 MW-1 SM 2320B 363343 92342553004 MW-7 SM 2320B 363343 92342553005 MW-9 SM 2320B 363343 92342553006 MW-14 SM 2320B 363343 92342553001 MW-15 SM 3500-Fe B 363473 92342553002 MW-21 SM 3500-Fe B 363473 92342553003 MW-1 SM 3500-Fe B 363473 92342553004 MW-7 SM 3500-Fe B 363473 92342553005 MW-9 SM 3500-Fe B 363473 92342553006 MW-14 SM 3500-Fe B 363473 92342553003 MW-1 SM 4500-S2D 363647 92342553004 MW-7 SM 4500-S2D 363647 92342553005 MW-9 SM 4500-S2D 363647 92342553006 MW-14 SM 4500-S2D 363647 92342553001 MW-15 EPA 300.0 363396 92342553002 MW-21 EPA 300.0 363396 92342553003 MW-1 EPA 300.0 364291 92342553004 MW-7 EPA 300.0 364291 92342553005 MW-9 EPA 300.0 364291 92342553006 MW-14 EPA 300.0 364314 92342553001 MW-15 SM 4500-CI-E 363371 92342553002 MW-21 SM 4500-CI-E 363371 92342553003 MW-1 SM 4500-CI-E 364538 92342553004 MW-7 SM 4500-CI-E 364538 92342553005 MW-9 SM 4500-CI-E 364538 92342553006 MW-14 SM 4500-CI-E 364538 92342553003 MW-1 SM 4500-CN-E 366221 92342553005 MW-9 SM 4500-CN-E 364584 92342553001 MW-15 SM 5220D 364072 92342553002 MW-21 SM 5220D 364072 92342553003 MW-1 SM 5220D 364072 92342553004 MW-7 SM 5220D 364072 92342553005 MW-9 SM 5220D 364072 92342553006 MW-14 SM 5220D 364072 92342553001 MW-15 SM 5310B 363127 92342553002 MW-21 SM 5310B 363127 92342553003 MW-1 SM 5310B 363536 92342553004 MW-7 SM 5310B 363536 92342553005 MW-9 SM 5310B 363536 92342553006 MW-14 SM 5310B 363536 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/26/2017 04:24 PM without the written consent of Pace Analytical Services, LLC. Analytical Analytical Method Batch Page 27 of 33 Document Name: Document Revised: Sept. 21, 2016 aC8.4RaIj/tlCat'e Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: i F-CAR-CS-033-Rev.01 Pace Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville /� Raleigh❑ Mechanicsville[] Sample Conditidn Upon Client Name: Wa# :92342553 Receipt` Project #: Courier: ❑F d Ex ❑UPS ❑USPS [--]Client ❑ Commercial Z Pate ❑Other: 92342553 1 Custody Seal Present? []Yes No Seals Intact? ❑Yes No PackingMaterial: Date/Initials Person Examining Contents: ❑Bubble Wrap Efoubble Bags ❑None ❑Other: Thermometer: �, // ❑ IR Gun ID: Type of Ice: L /Wet ❑Blue ❑None Samples on ice, cooling focess has begun Correction Factor: .Cooler Temp Corrected (°C): Biological Tissue Frozen? ❑Yes No ❑N/A Temp should be above fre zingto 6°C USDA Regulated Soil N/A, water sample) Did samples hginate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (intJN.oionaily, ❑Yes QNincluding Hawaii and Puerto Rico)? ❑Yes Chain of Custody Present? Samples Arrived within Hold Time? Short Hold Time Analysis (<72 hr.)? Rush Turn Around Time Requested? Sufficient Volume? Correct Containers Used? -Pace Containers Used? Containers Intact? Samples Field Filtered? Sample Labels Match COC? -Includes Date/Time/ID/Analysis Matrix: W -f Headspace in VOA Vials (>5-6mm)? Trip Blank Present? Trip Blank Custody Seals Present? CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Sample Discrepancy: IJNo ❑N/A 1 1. ❑ N/ 2. ❑N/A 3. (ONO ❑N/A 4. [-]No ❑N/A S. ❑Nn ❑N/A 6. ❑No ❑N/A UYes LJNQ, ❑N/A 7. ❑Yes EKo ❑N/A 8. Note if sediment is visible 1n the dissolved container � 4Ir�esEld. ❑N/A 9.- �•�l ntrl r2�irL 5L'1jt[ i�'lW -I`f ❑Yes o ❑N/A 10-- �1 t� nv [ cp S ti f ti h ❑Yes No ❑ /A El 11, [--]Yes❑No Field Data Required? ❑Yes ❑No Date/Time: Project Manager SCURF Review: �C Date: Project Manager SRF Review: is Date: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i,e. Out of hold, incorrect preservative, out of temp, incorrect containers) Page 28 of 33 61 a m O m 0 m rD °t `m x D ID -a ro_ a � _Q o m � ro rF 3v m rD m e�-r 0 to C O � C � rL _! C m w C, _a C � m • CL C a � o ( a 3 v 4 CL n v ro � m 0 o_ N M lO o 00 -4 Item# xzzzzBP4U-125 mL Plastic Unpreserved (N/A) (Cl-) y BP31.1-250 mL Plastic Unpreserved (N/A) BP2U-500 mL Plastic Unpreserved (N/A) BP11.1-1 liter Plastic Unpreserved (N/A) BP3S-250 mL Plastic H2504 (pH < 2) (CI-) BM-250 mt plastic HNO3 (pH < 2) Bp3Z-250 mL Plastic ZN Acetate & NaOH (>9) zzz Z BP3C-250 mL Plastic NaOH (pH > 12) (Cl-) WGFU-Wide-mouthed Glass jar Unpreserved AG1U-1 liter Amber Unpreserved (N/A) (CI-) AG1H-1liter Amber HCl (pH <2) AG3U-250 mL Amber Unpreserved (N/A) (Cl-) AG1S-1 liter Amber H2SO4 (pH < 2) AG3S-250 mLAmber H2504 (pH < 2) AG3A(DG3A)-250 mL Amber NH4Cl (N/A)(CI-) DG9H-40 mL VOA HCI (N/A) VG9T-40 mL VOA Na25203 (N/A) VG9U-40 mLVOA Unp (N/A) W DG9P-40 mL VOA H3PO4 (N/A) JVOAK (6 vials per kit)-5035 kit (N/A) V/GK (3 vials per kit)-VPH/Gas kit (N/A) 5PST-125 mLSte rile Plastic (N/A— lab) SP2T-250 mL Sterile Plastic (N/A —lab) BP3A-250 mL Plastic (NH2)2SO4 (93-9.7) Cubitainer VSGU-20 mL Scintillation vials (N/A) GN * -0 * m ro O M ro ro 0a C. 3 7- O m CL W O 1 Cr '6 S T O ro . 3 w YC ;� r* o M s w C n x fu z ro ru M CL ai, n� O 3 Cr a- O ro ( O = 3 m cn O a @ rl T r+ n 3 O a 0 n Q 0 {^n 3 CD a ro C w 0 w o Z Z m n ro o @ w N PaceArralyl;cal Section A n...,r.i—h M.- t..f.,....ari— Section B Required Praiect Information_ CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section C Invoice Information: Paae : 1 Of 1 Company: Municipal Engineering Services Report To. Jonathan Pfohl Attentions Municipal Engineering Services Address: P.O. Box 97 Copy TD: Company Name. Garner, NC 27529 Address- Regulatory Agency Emi jpfohl@mesco.com_ Purchase Order No. Pace Quote Reference: Phone: 919-772-5393 Fax Client Project ID: Slurry Closed -Mt. Airy (MNA) Pace Project Manager. Trey Carter State 1 Location Requested Due DateFrAT: 10 Day (Default) Container Order Number: Pace Profile #. 2103-6 North Carolina Requested Analysis Filtered (YIN) Z COLLECTED Preservatives N N N N N N N N N N N N MATRIX GODE Dnnhing W6ter DW SAMPLE ID Mt" W1 ware wsler ww s R O u START END z One Character per box. Pr si°— d sL s O W �� [A-Z, 0-91, -) oil OL I4 Sample Ids must he unique wipe wP ij U H A., AR Other or Q W N T-- TS w } S = m O C w a a ni W Z O n m M C c m m UJ ~ niV- s N DATE TIME DATE TIME u a = O 2 z O z 2 r L O Q t0 Q is D C=.7 C] O 1 Mw-1 VJT G X x x x x x X 2 MN!-7 L f wT G x x x x x X x 3 MW-9 ! u5 wr G x x x x x x x 4 MW-11 r�,1_{,.� UUT G x X x x x X X 5 Mw-14 VTr G Y ran f;` s- x x x x x x x 6 Mw-15 WT G ^f�l�t !'�� x x x x x x x 7 Mw-21 VVT G S13;ir� S'-l� x x x x x x x i ilfL s 9 i t] 11 12 ADDITIONAL COMMENTS RELINQUISHEDBY 1 AFFILIATION DATE TIME ACCEPTED BY! AFFILIATION DATE TIME SAMPLE CONDITIONS - -- - SAMPLER NAME AND SIGNATURE I m 2� a � 5- 5- o d E PRINT Name of SAMPLER: onaljlai NOW SIGNATURE of SAMPLER: \ DATE Signed: I f w m m . o m} �.J ail H rY - 00 rn-- aceAnalyfical vucurnenL ivarDe: Condition Upon Recei Document No.: F-CAR-CS-033-Rev.01 uocument Revised: Sept, 21, 2016 Page 1 of 2 Issuing Authority: Pace Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville IX Raleigh[] Mechanicsville❑ -Sample Condition Upon Name:�c r g2342553 Unit: Receipt Project I PM: RWC Due Date: 06/15/17 Courier: ❑Fed Ex ❑UPS ❑LISPS ❑ Commercial Pace ❑Client CLIENT: 92-Municipal ❑0ther: Custody Seal Present? ❑Yes [�No Seals intact? ❑Yes ®No Packing Material: ❑bubble Wrap 17 Bubble Bags ❑None ❑Other: Date/Initials Person Examining Contents: Thermometer: ❑ IR Gun ID: Type of Ice: r}Wet ❑Blue ❑None 05amples on ice, cooling process has begun Correction Factor: Cooler Temp Corrected (°C): (J Biological Tissue Frozen? ❑Yes �No [-]N/A Temp should be above freezing to VC USDA Regulated Soil (❑ N/A, water sample) Did samples originate in a quarantine zone within the ❑Yes No United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, including Hawaii and Puerto Rico)? Dyes 4No Comments/Discrepancy: Chain of Custody Present? ®Yes ❑Nv ❑N/A 1. Samples Arrived within Hold Time? Yes []No 2. Short Hold Time Analysis (<72 hr.)? --[]N/A ❑Yes No ❑N/A 3. Rush Turn Around Time Requested? ❑Yes MNo ❑N/A 4. Sufficient Volume? Yes ❑No ❑N/A 5, Correct Containers Used? [PYes [-]No ❑N/A 6. -Pace Containers Used? Yes ❑No []N/A Containers Intact? Yes ❑No ❑N/A 7. Samples Field Filtered? []Yes NNo ❑N/A S. Note if sediment is visible in the dissolved container Sample Labels Match C 0C? I Yes INN. ❑N/A -Includes Date/Time/ID/Analysis Matrix: �1.r 1 /Vil 'Z- cxh P �k� �/. I Headspace in VOA Vials (>5-6mm)? ❑Yes JNc ❑N/A 10.1 Q` �— GWt 1 c Trip Blank Present? Trip Blank Custody ]Yes (�No ❑N/A li. %r fit; 4 Seals Present? ❑Yes Na ❑N/A CLIENT N07fFICATi4N/RESOLUTION. ()'rr IY�r`_ Fuld Data Required? ❑Yes ❑No Person Contacted: � pi (L -P Comment: -/Sample Date/Time��,JD Discrepancy: Project Manager SCURF Review: -cc Date:. G/5 Project Manager SRF Review: tC Date: Note: Whenever there is a discrepancy affecting North Carolina compffance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers) Page 31 of 33 Sample Condition Upon Recei aceAnalyfrcal Document No,: F-CAR-CS-033-Rev.01 *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. **Bottom half of box is to list number of bottles )t(SCUR) Page 2 of 2 Issuing Authority: Pace Quality Office Project ;92342553 1� �O Due Date: 06/15/ pm : R4lC ,i iFINT : 92-Mt ""Pal « -p N a C u a E ry4a 0. 'G N w C 7 y a E M 0. Cam 4 1C7 N m C Y a E O N d \ 2 S' N W c D 14 a COCOm v N a:Z v O N M u E O V] VI M a N V M O = U y Z M M 0 O Z 06 f0 d ¢ z N u mCL J LA N M a COCOdo� v N 1-1a CL z O Z u E Vl U M a a ^ H R a a 4. U 3 d ti a ¢ c ? E .- ri Q a V z a U _ E r`i (J a \ V� a a C O LA CV M 0 a w N Q a O t�v = = A N C7 4 ry V a v O N 2 d E aM V7 M l7 a C a n Q J E 1 O 0 M C7 a Q \ Z '_� LI x ¢ 01 l} a Z m a cn IN6 Z q T [7 7 ¢ Z, a Ja QV m l7 Q \ ? V a 05 l9 a Q Z Y n O Vl ao W a O � C d > CL NLn v f;J 7 Z H d �Jry E r4 F- V1 a V! Q _ a J E O F- N a W1 V7 N S z JmE O L1 N M a m ;O 7 Q a Z N n O _ NcuE 'JO C7 V)m � � 1 I � 3 � J 4 5 5 7 8 9 10 11 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot # Page 32 of 33 M tin 0 Cl) M eanalytrra! CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT, All relevant fields must be completed accurately_ d Section A Section B Section C Required Client Information: Required Project Information: Invoice Information: Page : 1 Of 1 Company Murici al Engineering Services Report To Jonathan Pfohl Atlenlion Munici al Engineering Services Address. P.O. Box 97 Copy To Compary Name. Garner, NC 27529 Address: Regulatory Agency Email To j pfohl(Wmesco.COm Purchase Order No. Pace quote Reference: Phone 919-772-5393 1 Fax Clienl Project ID: Slurry Closed -Mt. Airy (MNA) Pace Project Manager Trey Carter State I Location Requested Due Dale7TAT: 10 Day (Default) Container Order Number, Pace Profile #: North Carolina Requested Analysis Filtered (YIN) z COLLECTED Preservatives } N N N N N N N N N N N N MATRIX CODE was wmo� Dw i q W, SAMPLE ID w°'" - START END Wosic water V'I'N t� z O Proeuct One Character per box.SL o (A-Z, 0-9 1, -) 0 vsoea oL s c J Sample Ids must be unique wa vw ii Ar AR U - dthw 07 T.— TS WO W aV 1 Q q 0 `--s G o r21r it O J W O Q m _ w F a U o N a 0Z 4 U Q C Q _ Y— m o [� P P DATE TIME DATE TIME v`S a _ _ = z z r� 0 [n U 1 MW-1 WT G (S I .3� x x W1 x x x x 2 MW-7 WT G 611 1•`fS x x x x x x x 3 MW-9 WT G 611 3--lb x x x x x x 0 4 MW-11 WT G G t( li '"i 1a ( �4 x x x x x x 5 MW-14 wT G :op x x x x x x x a V UF 6 MW-15 WT G l� :34 x x$ x x x x 7 Muv-21 VV7 G x x x x x x 8 9 16 11 12 L ADDITIONAL COMMENTS EINQUISHED BYI AFFILIATION DATE TIME ACCEPTED BY i'AFFILIATION DATE TIME SAMPLE CONDITIONS i �I�� •UT) s � /� +� gad SAMPLER NAME AND SIGNATURE °1 m p z c PRINT Name of SAMPLER: Jonat an Pohlai zi g E SIGNATURE of SAMPLER: DATE Signed: a, r UU tn} lacieAnalXical" www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 June 16, 2017 Mr. Jonathan Pfohl Municipal Engineering Services 68 Shipwash Dr. Garner, NC 27529 RE: Project: SURRY MSWLF SWS Pace Project No.: 92342549 Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory between June 01, 2017 and June 02, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Trey Carter trey. carter@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SURRY MSWLF SWS Pace Project No.: 92342549 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: SURRY MSWLF SWS Pace Project No.: 92342549 Lab ID Sample ID Matrix Date Collected Date Received 92342549001 SW-3 Water 05/31/17 00:00 06/01/17 07:55 92342730001 SW-1 Water 06/01/17 10:25 06/02/17 08:00 92342730002 SW-2 Water 06/01/17 16:00 06/02/17 08:00 92342730004 SW-4 Water 06/01/17 10:35 06/02/17 08:00 92342730005 SWN-1 Water 06/01/17 11:00 06/02/17 08:00 92342730006 SWN-2 Water 06/01/17 14:00 06/02/17 08:00 92342730007 SW -A Water 06/01/17 12:10 06/02/17 08:00 92342730008 SW-13 Water 06/01/17 12:30 06/02/17 08:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: SURRY MSWLF SWS 92342549 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92342549001 SW-3 EPA6010 SH1 14 PASI-A EPA 6020E CDF 1 PASI-A EPA 8260 GAW 50 PASI-C 92342730001 SW-1 EPA6010 SH1 14 PASI-A EPA 6020E CDF 1 PASI-A EPA 8260 GAW 50 PASI-C 92342730002 SW-2 EPA6010 SH1 14 PASI-A EPA 6020E CDF 1 PASI-A EPA 8260 GAW 50 PASI-C 92342730004 SW-4 EPA6010 SH1 14 PASI-A EPA 6020E CDF 1 PASI-A EPA 8260 GAW 50 PASI-C 92342730005 SWN-1 EPA6010 SH1 14 PASI-A EPA 6020E CDF 1 PASI-A EPA 8260 GAW 50 PASI-C 92342730006 SWN-2 EPA6010 SH1 14 PASI-A EPA 6020E CDF 1 PASI-A EPA 8260 GAW 50 PASI-C 92342730007 SW -A EPA 8260 GAW 50 PASI-C 92342730008 SW-B EPA 8260 GAW 50 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92342549 Sample: SW-3 Lab ID: 92342549001 Collected: 05/31/17 00:00 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Antimony ND ug/L 6.0 3.9 1 06/02/17 11:25 06/09/17 21:51 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/02/17 11:25 06/09/17 21:51 7440-38-2 Barium 21.8J ug/L 100 2.5 1 06/02/17 11:25 06/09/17 21:51 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 06/02/17 11:25 06/09/17 21:51 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 06/02/17 11:25 06/09/17 21:51 7440-43-9 Chromium ND ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:51 7440-47-3 Cobalt 8.01 ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:51 7440-48-4 Copper ND ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:51 7440-50-8 Lead ND ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:51 7439-92-1 Nickel ND ug/L 50.0 2.5 1 06/02/17 11:25 06/09/17 21:51 7440-02-0 Selenium ND ug/L 10.0 5.0 1 06/02/17 11:25 06/09/17 21:51 7782-49-2 Silver ND ug/L 10.0 2.5 1 06/02/17 11:25 06/09/17 21:51 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 06/02/17 11:25 06/09/17 21:51 7440-62-2 Zinc 7.4J ug/L 10.0 5.0 1 06/02/17 11:25 06/09/17 21:51 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Thallium ND ug/L 5.5 0.020 1 06/06/17 02:45 06/09/17 17:22 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 06/04/17 08:10 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 06/04/17 08:10 107-13-1 Benzene ND ug/L 1.0 0.25 1 06/04/17 08:10 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 06/04/17 08:10 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 06/04/17 08:10 75-27-4 Bromoform ND ug/L 3.0 0.26 1 06/04/17 08:10 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 06/04/17 08:10 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 06/04/17 08:10 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 06/04/17 08:10 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 06/04/17 08:10 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 06/04/17 08:10 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 06/04/17 08:10 75-00-3 Chloroform ND ug/L 5.0 0.14 1 06/04/17 08:10 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 06/04/17 08:10 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 06/04/17 08:10 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 06/04/17 08:10 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 06/04/17 08:10 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 06/04/17 08:10 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 06/04/17 08:10 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 06/04/17 08:10 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/04/17 08:10 110-57-6 L1 1,1-Dichloroethane ND ug/L 5.0 0.32 1 06/04/17 08:10 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 06/04/17 08:10 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/04/17 08:10 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 06/04/17 08:10 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/04/17 08:10 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 06/04/17 08:10 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2017 01:32 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92342549 Sample: SW-3 Lab ID: 92342549001 Collected: 05/31/17 00:00 Received: 06/01/17 07:55 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/04/17 08:10 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/17 08:10 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/17 08:10 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/04/17 08:10 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/17 08:10 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/17 08:10 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/17 08:10 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/04/17 08:10 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/17 08:10 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/17 08:10 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/17 08:10 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/17 08:10 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/17 08:10 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/17 08:10 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/17 08:10 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/17 08:10 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/17 08:10 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/17 08:10 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/17 08:10 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/17 08:10 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 102 % 70-130 1 06/04/17 08:10 460-00-4 1,2-Dichloroethane-d4 (S) 90 % 70-130 1 06/04/17 08:10 17060-07-0 Toluene-d8 (S) 107 % 70-130 1 06/04/17 08:10 2037-26-5 Date: 06/16/2017 01:32 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92342549 Sample: SW-1 Lab ID: 92342730001 Collected: 06/01/17 10:25 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Antimony ND ug/L 6.0 3.9 1 06/04/17 16:40 06/14/17 22:06 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:06 7440-38-2 Barium 26.8J ug/L 100 2.5 1 06/04/17 16:40 06/14/17 22:06 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:06 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:06 7440-43-9 Chromium ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:06 7440-47-3 Cobalt ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:06 7440-48-4 Copper ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:06 7440-50-8 Lead ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:06 7439-92-1 Nickel ND ug/L 50.0 2.5 1 06/04/17 16:40 06/14/17 22:06 7440-02-0 Selenium ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:06 7782-49-2 Silver ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:06 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 06/04/17 16:40 06/14/17 22:06 7440-62-2 Zinc ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:06 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Thallium ND ug/L 5.5 0.020 1 06/06/17 02:45 06/09/17 17:51 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 06/04/17 11:43 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 06/04/17 11:43 107-13-1 Benzene ND ug/L 1.0 0.25 1 06/04/17 11:43 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 06/04/17 11:43 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 06/04/17 11:43 75-27-4 Bromoform ND ug/L 3.0 0.26 1 06/04/17 11:43 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 06/04/17 11:43 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 06/04/17 11:43 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 06/04/17 11:43 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 06/04/17 11:43 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 06/04/17 11:43 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 06/04/17 11:43 75-00-3 Chloroform ND ug/L 5.0 0.14 1 06/04/17 11:43 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 06/04/17 11:43 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 06/04/17 11:43 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 06/04/17 11:43 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 06/04/17 11:43 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 06/04/17 11:43 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 06/04/17 11:43 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 06/04/17 11:43 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/04/17 11:43 110-57-6 L1 1,1-Dichloroethane ND ug/L 5.0 0.32 1 06/04/17 11:43 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 06/04/17 11:43 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/04/17 11:43 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 06/04/17 11:43 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/04/17 11:43 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 06/04/17 11:43 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2017 01:32 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92342549 Sample: SW-1 Lab ID: 92342730001 Collected: 06/01/17 10:25 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/04/17 11:43 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/17 11:43 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/17 11:43 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/04/17 11:43 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/17 11:43 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/17 11:43 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/17 11:43 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/04/17 11:43 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/17 11:43 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/17 11:43 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/17 11:43 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/17 11:43 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/17 11:43 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/17 11:43 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/17 11:43 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/17 11:43 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/17 11:43 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/17 11:43 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/17 11:43 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/17 11:43 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 103 % 70-130 1 06/04/17 11:43 460-00-4 1,2-Dichloroethane-d4 (S) 92 % 70-130 1 06/04/17 11:43 17060-07-0 Toluene-d8 (S) 108 % 70-130 1 06/04/17 11:43 2037-26-5 Date: 06/16/2017 01:32 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92342549 Sample: SW-2 Lab ID: 92342730002 Collected: 06/01/17 16:00 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 301 OA Antimony ND ug/L 6.0 3.9 1 06/04/17 16:40 06/14/17 22:09 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:09 7440-38-2 Barium 17.OJ ug/L 100 2.5 1 06/04/17 16:40 06/14/17 22:09 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:09 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:09 7440-43-9 Chromium ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:09 7440-47-3 Cobalt 16.8 ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:09 7440-48-4 Copper ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:09 7440-50-8 Lead ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:09 7439-92-1 Nickel ND ug/L 50.0 2.5 1 06/04/17 16:40 06/14/17 22:09 7440-02-0 Selenium ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:09 7782-49-2 Silver ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:09 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 06/04/17 16:40 06/14/17 22:09 7440-62-2 Zinc ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:09 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Thallium 0.048J ug/L 5.5 0.020 1 06/06/17 02:45 06/09/17 20:09 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone 13.3J ug/L 100 10.0 1 06/04/17 12:01 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 06/04/17 12:01 107-13-1 Benzene ND ug/L 1.0 0.25 1 06/04/17 12:01 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 06/04/17 12:01 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 06/04/17 12:01 75-27-4 Bromoform ND ug/L 3.0 0.26 1 06/04/17 12:01 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 06/04/17 12:01 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 06/04/17 12:01 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 06/04/17 12:01 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 06/04/17 12:01 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 06/04/17 12:01 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 06/04/17 12:01 75-00-3 Chloroform ND ug/L 5.0 0.14 1 06/04/17 12:01 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 06/04/17 12:01 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 06/04/17 12:01 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 06/04/17 12:01 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 06/04/17 12:01 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 06/04/17 12:01 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 06/04/17 12:01 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 06/04/17 12:01 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/04/17 12:01 110-57-6 L1 1,1-Dichloroethane ND ug/L 5.0 0.32 1 06/04/17 12:01 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 06/04/17 12:01 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/04/17 12:01 75-35-4 cis-1,2-Dichloroethene 2.4J ug/L 5.0 0.19 1 06/04/17 12:01 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/04/17 12:01 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 06/04/17 12:01 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2017 01:32 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92342549 Sample: SW-2 Lab ID: 92342730002 Collected: 06/01/17 16:00 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/04/17 12:01 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/17 12:01 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/17 12:01 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/04/17 12:01 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/17 12:01 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/17 12:01 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/17 12:01 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/04/17 12:01 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/17 12:01 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/17 12:01 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/17 12:01 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/17 12:01 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/17 12:01 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/17 12:01 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/17 12:01 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/17 12:01 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/17 12:01 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/17 12:01 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/17 12:01 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/17 12:01 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 108 % 70-130 1 06/04/17 12:01 460-00-4 1,2-Dichloroethane-d4 (S) 90 % 70-130 1 06/04/17 12:01 17060-07-0 Toluene-d8 (S) 108 % 70-130 1 06/04/17 12:01 2037-26-5 Date: 06/16/2017 01:32 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92342549 Sample: SW-4 Lab ID: 92342730004 Collected: 06/01/17 10:35 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Vanadium Zinc 6020 MET ICPMS Thallium 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane Date: 06/16/2017 01:32 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 06/04/17 16:40 06/14/17 22:12 7440-36-0 ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:12 7440-38-2 22.OJ ug/L 100 2.5 1 06/04/17 16:40 06/14/17 22:12 7440-39-3 ND ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:12 7440-41-7 ND ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:12 7440-43-9 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:12 7440-47-3 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:12 7440-48-4 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:12 7440-50-8 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:12 7439-92-1 ND ug/L 50.0 2.5 1 06/04/17 16:40 06/14/17 22:12 7440-02-0 ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:12 7782-49-2 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:12 7440-22-4 ND ug/L 25.0 2.5 1 06/04/17 16:40 06/14/17 22:12 7440-62-2 7.OJ ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:12 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3010A 0.054J ug/L 5.5 0.020 1 06/06/17 02:45 06/09/17 20:14 7440-28-0 Analytical Method: EPA 8260 19.3J ug/L 100 10.0 1 06/04/1712:19 67-64-1 ND ug/L 200 1.9 1 06/04/1712:19 107-13-1 ND ug/L 1.0 0.25 1 06/04/1712:19 71-43-2 ND ug/L 3.0 0.17 1 06/04/1712:19 74-97-5 ND ug/L 1.0 0.18 1 06/04/1712:19 75-27-4 ND ug/L 3.0 0.26 1 06/04/1712:19 75-25-2 ND ug/L 10.0 0.29 1 06/04/1712:19 74-83-9 ND ug/L 100 0.96 1 06/04/1712:19 78-93-3 ND ug/L 100 1.2 1 06/04/1712:19 75-15-0 ND ug/L 1.0 0.25 1 06/04/1712:19 56-23-5 ND ug/L 3.0 0.23 1 06/04/1712:19 108-90-7 ND ug/L 10.0 0.54 1 06/04/1712:19 75-00-3 ND ug/L 5.0 0.14 1 06/04/1712:19 67-66-3 0.13J ug/L 1.0 0.11 1 06/04/1712:19 74-87-3 ND ug/L 13.0 2.0 1 06/04/1712:19 96-12-8 ND ug/L 3.0 0.21 1 06/04/1712:19 124-48-1 ND ug/L 1.0 0.27 1 06/04/1712:19 106-93-4 ND ug/L 10.0 0.21 1 06/04/1712:19 74-95-3 ND ug/L 5.0 0.30 1 06/04/1712:19 95-50-1 ND ug/L 1.0 0.33 1 06/04/1712:19 106-46-7 ND ug/L 100 1.0 1 06/04/1712:19 110-57-6 ND ug/L 5.0 0.32 1 06/04/1712:19 75-34-3 ND ug/L 1.0 0.24 1 06/04/1712:19 107-06-2 ND ug/L 5.0 0.56 1 06/04/1712:19 75-35-4 ND ug/L 5.0 0.19 1 06/04/1712:19 156-59-2 ND ug/L 5.0 0.49 1 06/04/1712:19 156-60-5 ND ug/L 1.0 0.27 1 06/04/1712:19 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. L1 Page 11 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92342549 Sample: SW-4 Lab ID: 92342730004 Collected: 06/01/17 10:35 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/04/17 12:19 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/17 12:19 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/17 12:19 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/04/17 12:19 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/17 12:19 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/17 12:19 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/17 12:19 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/04/17 12:19 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/17 12:19 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/17 12:19 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/17 12:19 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/17 12:19 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/17 12:19 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/17 12:19 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/17 12:19 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/17 12:19 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/17 12:19 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/17 12:19 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/17 12:19 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/17 12:19 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 104 % 70-130 1 06/04/17 12:19 460-00-4 1,2-Dichloroethane-d4 (S) 95 % 70-130 1 06/04/17 12:19 17060-07-0 Toluene-d8 (S) 108 % 70-130 1 06/04/17 12:19 2037-26-5 Date: 06/16/2017 01:32 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 12 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92342549 Sample: SWN-1 Lab ID: 92342730005 Collected: 06/01/17 11:00 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Vanadium Zinc 6020 MET ICPMS Thallium 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane Date: 06/16/2017 01:32 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 06/04/17 16:40 06/14/17 22:24 7440-36-0 ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:24 7440-38-2 21.3J ug/L 100 2.5 1 06/04/17 16:40 06/14/17 22:24 7440-39-3 ND ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:24 7440-41-7 ND ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:24 7440-43-9 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:24 7440-47-3 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:24 7440-48-4 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:24 7440-50-8 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:24 7439-92-1 ND ug/L 50.0 2.5 1 06/04/17 16:40 06/14/17 22:24 7440-02-0 ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:24 7782-49-2 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:24 7440-22-4 ND ug/L 25.0 2.5 1 06/04/17 16:40 06/14/17 22:24 7440-62-2 9.1J ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:24 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3010A ND ug/L 5.5 0.020 1 06/06/17 02:45 06/09/17 20:16 7440-28-0 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 06/04/1712:37 67-64-1 ND ug/L 200 1.9 1 06/04/1712:37 107-13-1 ND ug/L 1.0 0.25 1 06/04/1712:37 71-43-2 ND ug/L 3.0 0.17 1 06/04/1712:37 74-97-5 ND ug/L 1.0 0.18 1 06/04/1712:37 75-27-4 ND ug/L 3.0 0.26 1 06/04/1712:37 75-25-2 ND ug/L 10.0 0.29 1 06/04/1712:37 74-83-9 ND ug/L 100 0.96 1 06/04/1712:37 78-93-3 ND ug/L 100 1.2 1 06/04/1712:37 75-15-0 ND ug/L 1.0 0.25 1 06/04/1712:37 56-23-5 ND ug/L 3.0 0.23 1 06/04/1712:37 108-90-7 ND ug/L 10.0 0.54 1 06/04/1712:37 75-00-3 ND ug/L 5.0 0.14 1 06/04/1712:37 67-66-3 0.13J ug/L 1.0 0.11 1 06/04/1712:37 74-87-3 ND ug/L 13.0 2.0 1 06/04/1712:37 96-12-8 ND ug/L 3.0 0.21 1 06/04/1712:37 124-48-1 ND ug/L 1.0 0.27 1 06/04/1712:37 106-93-4 ND ug/L 10.0 0.21 1 06/04/1712:37 74-95-3 ND ug/L 5.0 0.30 1 06/04/1712:37 95-50-1 ND ug/L 1.0 0.33 1 06/04/1712:37 106-46-7 ND ug/L 100 1.0 1 06/04/1712:37 110-57-6 ND ug/L 5.0 0.32 1 06/04/1712:37 75-34-3 ND ug/L 1.0 0.24 1 06/04/1712:37 107-06-2 ND ug/L 5.0 0.56 1 06/04/1712:37 75-35-4 ND ug/L 5.0 0.19 1 06/04/1712:37 156-59-2 ND ug/L 5.0 0.49 1 06/04/1712:37 156-60-5 ND ug/L 1.0 0.27 1 06/04/1712:37 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. L1 Page 13 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92342549 Sample: SWN-1 Lab ID: 92342730005 Collected: 06/01/17 11:00 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/04/17 12:37 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/17 12:37 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/17 12:37 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/04/17 12:37 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/17 12:37 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/17 12:37 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/17 12:37 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/04/17 12:37 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/17 12:37 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/17 12:37 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/17 12:37 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/17 12:37 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/17 12:37 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/17 12:37 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/17 12:37 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/17 12:37 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/17 12:37 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/17 12:37 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/17 12:37 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/17 12:37 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 102 % 70-130 1 06/04/17 12:37 460-00-4 1,2-Dichloroethane-d4 (S) 92 % 70-130 1 06/04/17 12:37 17060-07-0 Toluene-d8 (S) 109 % 70-130 1 06/04/17 12:37 2037-26-5 Date: 06/16/2017 01:32 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 14 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92342549 Sample: SWN-2 Lab ID: 92342730006 Collected: 06/01/17 14:00 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Vanadium Zinc 6020 MET ICPMS Thallium 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane Date: 06/16/2017 01:32 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 06/04/17 16:40 06/14/17 22:28 7440-36-0 ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:28 7440-38-2 20.4J ug/L 100 2.5 1 06/04/17 16:40 06/14/17 22:28 7440-39-3 ND ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:28 7440-41-7 ND ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:28 7440-43-9 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:28 7440-47-3 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:28 7440-48-4 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:28 7440-50-8 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:28 7439-92-1 ND ug/L 50.0 2.5 1 06/04/17 16:40 06/14/17 22:28 7440-02-0 ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:28 7782-49-2 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:28 7440-22-4 2.8J ug/L 25.0 2.5 1 06/04/17 16:40 06/14/17 22:28 7440-62-2 5.4J ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:28 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3010A ND ug/L 5.5 0.020 1 06/06/17 02:45 06/09/17 20:18 7440-28-0 Analytical Method: EPA 8260 11.6J ug/L 100 10.0 1 06/04/1712:55 67-64-1 ND ug/L 200 1.9 1 06/04/1712:55 107-13-1 ND ug/L 1.0 0.25 1 06/04/1712:55 71-43-2 ND ug/L 3.0 0.17 1 06/04/1712:55 74-97-5 ND ug/L 1.0 0.18 1 06/04/1712:55 75-27-4 ND ug/L 3.0 0.26 1 06/04/1712:55 75-25-2 ND ug/L 10.0 0.29 1 06/04/1712:55 74-83-9 ND ug/L 100 0.96 1 06/04/1712:55 78-93-3 ND ug/L 100 1.2 1 06/04/1712:55 75-15-0 ND ug/L 1.0 0.25 1 06/04/1712:55 56-23-5 ND ug/L 3.0 0.23 1 06/04/1712:55 108-90-7 ND ug/L 10.0 0.54 1 06/04/1712:55 75-00-3 ND ug/L 5.0 0.14 1 06/04/1712:55 67-66-3 ND ug/L 1.0 0.11 1 06/04/1712:55 74-87-3 ND ug/L 13.0 2.0 1 06/04/1712:55 96-12-8 ND ug/L 3.0 0.21 1 06/04/1712:55 124-48-1 ND ug/L 1.0 0.27 1 06/04/1712:55 106-93-4 ND ug/L 10.0 0.21 1 06/04/1712:55 74-95-3 ND ug/L 5.0 0.30 1 06/04/1712:55 95-50-1 ND ug/L 1.0 0.33 1 06/04/1712:55 106-46-7 ND ug/L 100 1.0 1 06/04/1712:55 110-57-6 ND ug/L 5.0 0.32 1 06/04/1712:55 75-34-3 ND ug/L 1.0 0.24 1 06/04/1712:55 107-06-2 ND ug/L 5.0 0.56 1 06/04/1712:55 75-35-4 ND ug/L 5.0 0.19 1 06/04/1712:55 156-59-2 ND ug/L 5.0 0.49 1 06/04/1712:55 156-60-5 ND ug/L 1.0 0.27 1 06/04/1712:55 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. I0i1IT, G: Page 15 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92342549 Sample: SWN-2 Lab ID: 92342730006 Collected: 06/01/17 14:00 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/04/17 12:55 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/17 12:55 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/17 12:55 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 06/04/17 12:55 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/17 12:55 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/17 12:55 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/17 12:55 108-10-1 Styrene ND ug/L 1.0 0.26 1 06/04/17 12:55 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/17 12:55 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/17 12:55 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/17 12:55 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/17 12:55 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/17 12:55 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/17 12:55 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/17 12:55 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/17 12:55 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/17 12:55 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/17 12:55 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/17 12:55 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/17 12:55 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 106 % 70-130 1 06/04/17 12:55 460-00-4 1,2-Dichloroethane-d4 (S) 88 % 70-130 1 06/04/17 12:55 17060-07-0 Toluene-d8 (S) 123 % 70-130 1 06/04/17 12:55 2037-26-5 Date: 06/16/2017 01:32 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 16 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92342549 Sample: SW -A Lab ID: 92342730007 Collected: 06/01/17 12:10 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Date: 06/16/2017 01:32 PM Analytical Method: EPA 8260 12.2J ug/L 100 10.0 1 06/04/1714:24 67-64-1 ND ug/L 200 1.9 1 06/04/1714:24 107-13-1 ND ug/L 1.0 0.25 1 06/04/1714:24 71-43-2 ND ug/L 3.0 0.17 1 06/04/1714:24 74-97-5 ND ug/L 1.0 0.18 1 06/04/1714:24 75-27-4 ND ug/L 3.0 0.26 1 06/04/1714:24 75-25-2 ND ug/L 10.0 0.29 1 06/04/1714:24 74-83-9 ND ug/L 100 0.96 1 06/04/1714:24 78-93-3 ND ug/L 100 1.2 1 06/04/1714:24 75-15-0 ND ug/L 1.0 0.25 1 06/04/1714:24 56-23-5 ND ug/L 3.0 0.23 1 06/04/1714:24 108-90-7 ND ug/L 10.0 0.54 1 06/04/1714:24 75-00-3 ND ug/L 5.0 0.14 1 06/04/1714:24 67-66-3 ND ug/L 1.0 0.11 1 06/04/1714:24 74-87-3 ND ug/L 13.0 2.0 1 06/04/1714:24 96-12-8 ND ug/L 3.0 0.21 1 06/04/1714:24 124-48-1 ND ug/L 1.0 0.27 1 06/04/1714:24 106-93-4 ND ug/L 10.0 0.21 1 06/04/1714:24 74-95-3 ND ug/L 5.0 0.30 1 06/04/1714:24 95-50-1 ND ug/L 1.0 0.33 1 06/04/1714:24 106-46-7 ND ug/L 100 1.0 1 06/04/1714:24 110-57-6 ND ug/L 5.0 0.32 1 06/04/1714:24 75-34-3 ND ug/L 1.0 0.24 1 06/04/1714:24 107-06-2 ND ug/L 5.0 0.56 1 06/04/1714:24 75-35-4 ND ug/L 5.0 0.19 1 06/04/1714:24 156-59-2 ND ug/L 5.0 0.49 1 06/04/1714:24 156-60-5 ND ug/L 1.0 0.27 1 06/04/1714:24 78-87-5 ND ug/L 1.0 0.13 1 06/04/1714:24 10061-01-5 ND ug/L 1.0 0.26 1 06/04/1714:24 10061-02-6 ND ug/L 1.0 0.30 1 06/04/1714:24 100-41-4 ND ug/L 50.0 0.46 1 06/04/1714:24 591-78-6 ND ug/L 10.0 0.32 1 06/04/1714:24 74-88-4 ND ug/L 1.0 0.97 1 06/04/1714:24 75-09-2 ND ug/L 100 0.33 1 06/04/1714:24 108-10-1 ND ug/L 1.0 0.26 1 06/04/1714:24 100-42-5 ND ug/L 5.0 0.33 1 06/04/1714:24 630-20-6 ND ug/L 3.0 0.40 1 06/04/1714:24 79-34-5 ND ug/L 1.0 0.46 1 06/04/1714:24 127-18-4 ND ug/L 1.0 0.26 1 06/04/1714:24 108-88-3 ND ug/L 1.0 0.48 1 06/04/1714:24 71-55-6 ND ug/L 1.0 0.29 1 06/04/1714:24 79-00-5 ND ug/L 1.0 0.47 1 06/04/1714:24 79-01-6 ND ug/L 1.0 0.20 1 06/04/1714:24 75-69-4 ND ug/L 1.0 0.41 1 06/04/1714:24 96-18-4 ND ug/L 50.0 0.35 1 06/04/1714:24 108-05-4 ND ug/L 1.0 0.62 1 06/04/1714:24 75-01-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. L1 Page 17 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92342549 Sample: SW -A Lab ID: 92342730007 Collected: 06/01/17 12:10 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/17 14:24 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 105 % 70-130 1 06/04/17 14:24 460-00-4 1,2-Dichloroethane-d4 (S) 92 % 70-130 1 06/04/17 14:24 17060-07-0 Toluene-d8 (S) 104 % 70-130 1 06/04/17 14:24 2037-26-5 Date: 06/16/2017 01:32 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 18 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92342549 Sample: SW-B Lab ID: 92342730008 Collected: 06/01/17 12:30 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Date: 06/16/2017 01:32 PM Analytical Method: EPA 8260 ND ug/L 100 10.0 1 06/04/1714:42 67-64-1 ND ug/L 200 1.9 1 06/04/1714:42 107-13-1 ND ug/L 1.0 0.25 1 06/04/1714:42 71-43-2 ND ug/L 3.0 0.17 1 06/04/1714:42 74-97-5 ND ug/L 1.0 0.18 1 06/04/1714:42 75-27-4 ND ug/L 3.0 0.26 1 06/04/1714:42 75-25-2 ND ug/L 10.0 0.29 1 06/04/1714:42 74-83-9 ND ug/L 100 0.96 1 06/04/1714:42 78-93-3 ND ug/L 100 1.2 1 06/04/1714:42 75-15-0 ND ug/L 1.0 0.25 1 06/04/1714:42 56-23-5 ND ug/L 3.0 0.23 1 06/04/1714:42 108-90-7 ND ug/L 10.0 0.54 1 06/04/1714:42 75-00-3 ND ug/L 5.0 0.14 1 06/04/1714:42 67-66-3 ND ug/L 1.0 0.11 1 06/04/1714:42 74-87-3 ND ug/L 13.0 2.0 1 06/04/1714:42 96-12-8 ND ug/L 3.0 0.21 1 06/04/1714:42 124-48-1 ND ug/L 1.0 0.27 1 06/04/1714:42 106-93-4 ND ug/L 10.0 0.21 1 06/04/1714:42 74-95-3 ND ug/L 5.0 0.30 1 06/04/1714:42 95-50-1 ND ug/L 1.0 0.33 1 06/04/1714:42 106-46-7 ND ug/L 100 1.0 1 06/04/1714:42 110-57-6 ND ug/L 5.0 0.32 1 06/04/1714:42 75-34-3 ND ug/L 1.0 0.24 1 06/04/1714:42 107-06-2 ND ug/L 5.0 0.56 1 06/04/1714:42 75-35-4 ND ug/L 5.0 0.19 1 06/04/1714:42 156-59-2 ND ug/L 5.0 0.49 1 06/04/1714:42 156-60-5 ND ug/L 1.0 0.27 1 06/04/1714:42 78-87-5 ND ug/L 1.0 0.13 1 06/04/1714:42 10061-01-5 ND ug/L 1.0 0.26 1 06/04/1714:42 10061-02-6 ND ug/L 1.0 0.30 1 06/04/1714:42 100-41-4 ND ug/L 50.0 0.46 1 06/04/1714:42 591-78-6 ND ug/L 10.0 0.32 1 06/04/1714:42 74-88-4 ND ug/L 1.0 0.97 1 06/04/1714:42 75-09-2 ND ug/L 100 0.33 1 06/04/1714:42 108-10-1 ND ug/L 1.0 0.26 1 06/04/1714:42 100-42-5 ND ug/L 5.0 0.33 1 06/04/1714:42 630-20-6 ND ug/L 3.0 0.40 1 06/04/1714:42 79-34-5 ND ug/L 1.0 0.46 1 06/04/1714:42 127-18-4 ND ug/L 1.0 0.26 1 06/04/1714:42 108-88-3 ND ug/L 1.0 0.48 1 06/04/1714:42 71-55-6 ND ug/L 1.0 0.29 1 06/04/1714:42 79-00-5 ND ug/L 1.0 0.47 1 06/04/1714:42 79-01-6 ND ug/L 1.0 0.20 1 06/04/1714:42 75-69-4 ND ug/L 1.0 0.41 1 06/04/1714:42 96-18-4 ND ug/L 50.0 0.35 1 06/04/1714:42 108-05-4 ND ug/L 1.0 0.62 1 06/04/1714:42 75-01-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. L1 Page 19 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY MSWLF SWS Pace Project No.: 92342549 Sample: SW-B Lab ID: 92342730008 Collected: 06/01/17 12:30 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/17 14:42 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 06/04/17 14:42 460-00-4 1,2-Dichloroethane-d4 (S) 87 % 70-130 1 06/04/17 14:42 17060-07-0 Toluene-d8 (S) 108 % 70-130 1 06/04/17 14:42 2037-26-5 Date: 06/16/2017 01:32 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 20 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY MSWLF SWS Pace Project No.: 92342549 QC Batch: 363146 Analysis Method: EPA 6010 QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92342549001 METHOD BLANK: 2013277 Associated Lab Samples: 92342549001 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Antimony ug/L ND 5.0 3.9 06/09/17 20:33 Arsenic ug/L ND 10.0 5.0 06/09/17 20:33 Barium ug/L ND 5.0 2.5 06/09/17 20:33 Beryllium ug/L ND 1.0 0.50 06/09/17 20:33 Cadmium ug/L ND 1.0 0.50 06/09/17 20:33 Chromium ug/L ND 5.0 2.5 06/10/1716:23 Cobalt ug/L ND 5.0 2.5 06/09/17 20:33 Copper ug/L ND 5.0 2.5 06/09/17 20:33 Lead ug/L ND 5.0 2.5 06/09/17 20:33 Nickel ug/L ND 5.0 2.5 06/10/1716:23 Selenium ug/L ND 10.0 5.0 06/09/17 20:33 Silver ug/L ND 5.0 2.5 06/09/17 20:33 Vanadium ug/L ND 5.0 2.5 06/09/17 20:33 Zinc ug/L ND 10.0 5.0 06/09/17 20:33 LABORATORY CONTROL SAMPLE: Parameter 2013278 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 500 493 99 80-120 Arsenic ug/L 500 474 95 80-120 Barium ug/L 500 497 99 80-120 Beryllium ug/L 500 497 99 80-120 Cadmium ug/L 500 496 99 80-120 Chromium ug/L 500 494 99 80-120 Cobalt ug/L 500 494 99 80-120 Copper ug/L 500 496 99 80-120 Lead ug/L 500 489 98 80-120 Nickel ug/L 500 485 97 80-120 Selenium ug/L 500 495 99 80-120 Silver ug/L 250 247 99 80-120 Vanadium ug/L 500 484 97 80-120 Zinc ug/L 500 496 99 80-120 Qualifiers Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2013279 2013280 MS MSD 92342472012 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 491 503 98 101 75-125 2 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2017 01:32 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: SURRY MSWLF SWS 92342549 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2013279 2013280 MS MSD 92342472012 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Arsenic ug/L ND 500 500 472 483 94 97 75-125 2 20 Barium ug/L 0.091 500 500 582 602 98 102 75-125 3 20 mg/L Beryllium ug/L ND 500 500 494 510 99 102 75-125 3 20 Cadmium ug/L ND 500 500 495 506 99 101 75-125 2 20 Chromium ug/L ND 500 500 493 508 99 102 75-125 3 20 Cobalt ug/L ND 500 500 492 503 98 101 75-125 2 20 Copper ug/L ND 500 500 494 508 99 101 75-125 3 20 Lead ug/L ND 500 500 485 496 97 99 75-125 2 20 Nickel ug/L 0.016 500 500 500 510 97 99 75-125 2 20 mg/L Selenium ug/L ND 500 500 490 507 98 101 75-125 3 20 Silver ug/L ND 250 250 247 252 99 101 75-125 2 20 Vanadium ug/L ND 500 500 482 495 96 99 75-125 3 20 Zinc ug/L 0.066 500 500 557 569 98 101 75-125 2 20 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2017 01:32 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY MSWLF SWS Pace Project No.: 92342549 QC Batch: 363321 Analysis Method: EPA 6010 QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92342730001, 92342730002, 92342730004, 92342730005, 92342730006 METHOD BLANK: 2014222 Matrix: Water Associated Lab Samples: 92342730001, 92342730002, 92342730004, 92342730005, 92342730006 Blank Reporting Parameter Units Result Limit MDL Analyzed Antimony ug/L ND 5.0 3.9 06/14/17 21:19 Arsenic ug/L ND 10.0 5.0 06/14/17 21:19 Barium ug/L ND 5.0 2.5 06/14/17 21:19 Beryllium ug/L ND 1.0 0.50 06/14/17 21:19 Cadmium ug/L ND 1.0 0.50 06/14/17 21:19 Chromium ug/L ND 5.0 2.5 06/14/17 21:19 Cobalt ug/L ND 5.0 2.5 06/14/17 21:19 Copper ug/L ND 5.0 2.5 06/14/17 21:19 Lead ug/L ND 5.0 2.5 06/14/17 21:19 Nickel ug/L ND 5.0 2.5 06/14/17 21:19 Selenium ug/L ND 10.0 5.0 06/14/17 21:19 Silver ug/L ND 5.0 2.5 06/14/17 21:19 Vanadium ug/L ND 5.0 2.5 06/14/17 21:19 Zinc ug/L ND 10.0 5.0 06/14/17 21:19 LABORATORY CONTROL SAMPLE: Parameter 2014223 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 500 496 99 80-120 Arsenic ug/L 500 475 95 80-120 Barium ug/L 500 511 102 80-120 Beryllium ug/L 500 457 91 80-120 Cadmium ug/L 500 512 102 80-120 Chromium ug/L 500 463 93 80-120 Cobalt ug/L 500 498 100 80-120 Copper ug/L 500 494 99 80-120 Lead ug/L 500 486 97 80-120 Nickel ug/L 500 463 93 80-120 Selenium ug/L 500 501 100 80-120 Silver ug/L 250 235 94 80-120 Vanadium ug/L 500 456 91 80-120 Zinc ug/L 500 472 94 80-120 Qualifiers Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2014224 2014225 MS MSD 92342605016 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 517 501 103 100 75-125 3 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2017 01:32 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: SURRY MSWLF SWS 92342549 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2014224 2014225 MS MSD 92342605016 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Arsenic ug/L 174 500 500 672 657 100 97 75-125 2 20 Barium ug/L 8.0 500 500 546 530 108 104 75-125 3 20 Beryllium ug/L 0.73J 500 500 481 471 96 94 75-125 2 20 Cadmium ug/L 1.7 500 500 540 524 108 105 75-125 3 20 Chromium ug/L ND 500 500 486 470 97 94 75-125 3 20 Cobalt ug/L 75.0 500 500 594 577 104 100 75-125 3 20 Copper ug/L ND 500 500 522 509 104 102 75-125 3 20 Lead ug/L 4AJ 500 500 506 491 100 97 75-125 3 20 Nickel ug/L 3.2J 500 500 481 466 96 93 75-125 3 20 Selenium ug/L ND 500 500 511 501 102 100 75-125 2 20 Silver ug/L ND 250 250 246 238 99 95 75-125 4 20 Vanadium ug/L ND 500 500 482 466 96 93 75-125 3 20 Zinc ug/L 5.8J 500 500 495 479 98 95 75-125 3 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2017 01:32 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY MSWLF SWS Pace Project No.: 92342549 QC Batch: 363478 Analysis Method: EPA 6020B QC Batch Method: EPA 3010A Analysis Description: 6020 MET Associated Lab Samples: 92342549001, 92342730001 METHOD BLANK: 2015139 Matrix: Water Associated Lab Samples: 92342549001, 92342730001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Thallium ug/L ND 0.10 0.020 06/09/1716:55 LABORATORY CONTROL SAMPLE: 2015140 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Thallium ug/L 100 90.8 91 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2015141 2015142 MS MSD 92342795001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Thallium ug/L 0.0901 100 100 91.9 96.1 92 96 75-125 4 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2017 01:32 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY MSWLF SWS Pace Project No.: 92342549 QC Batch: 363479 Analysis Method: EPA 6020B QC Batch Method: EPA 3010A Analysis Description: 6020 MET Associated Lab Samples: 92342730002, 92342730004, 92342730005, 92342730006 METHOD BLANK: 2015143 Matrix: Water Associated Lab Samples: 92342730002, 92342730004, 92342730005, 92342730006 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Thallium ug/L ND 0.10 0.020 06/09/17 20:05 LABORATORY CONTROL SAMPLE: 2015144 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Thallium ug/L 100 93.7 94 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2015145 2015146 MS MSD 92342730002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Thallium ug/L 0.048J 100 100 94.4 94.8 94 95 75-125 0 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2017 01:32 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY MSWLF SWS Pace Project No.: 92342549 QC Batch: 363307 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92342549001, 92342730001, 92342730002, 92342730004, 92342730005, 92342730006 METHOD BLANK: 2014180 Matrix: Water Associated Lab Samples: 92342549001, 92342730001, 92342730002, 92342730004, 92342730005, 92342730006 Blank Reporting Parameter Units Result Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 0.33 06/04/17 06:41 1,1,1-Trichloroethane ug/L ND 1.0 0.48 06/04/17 06:41 1,1,2,2-Tetrachloroethane ug/L ND 3.0 0.40 06/04/17 06:41 1,1,2-Trichloroethane ug/L ND 1.0 0.29 06/04/17 06:41 1,1-Dichloroethane ug/L ND 5.0 0.32 06/04/17 06:41 1,1-Dichloroethene ug/L ND 5.0 0.56 06/04/17 06:41 1,2,3-Trichloropropane ug/L ND 1.0 0.41 06/04/17 06:41 1,2-Dibromo-3-chloropropane ug/L ND 13.0 2.0 06/04/17 06:41 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 06/04/17 06:41 1,2-Dichlorobenzene ug/L ND 5.0 0.30 06/04/17 06:41 1,2-Dichloroethane ug/L ND 1.0 0.24 06/04/17 06:41 1,2-Dichloropropane ug/L ND 1.0 0.27 06/04/17 06:41 1,4-Dichlorobenzene ug/L ND 1.0 0.33 06/04/17 06:41 2-Butanone (MEK) ug/L ND 100 0.96 06/04/17 06:41 2-Hexanone ug/L ND 50.0 0.46 06/04/17 06:41 4-Methyl-2-pentanone (MIBK) ug/L ND 100 0.33 06/04/17 06:41 Acetone ug/L ND 100 10.0 06/04/17 06:41 Acrylonitrile ug/L ND 200 1.9 06/04/17 06:41 Benzene ug/L ND 1.0 0.25 06/04/17 06:41 Bromochloromethane ug/L ND 3.0 0.17 06/04/17 06:41 Bromodichloromethane ug/L ND 1.0 0.18 06/04/17 06:41 Bromoform ug/L ND 3.0 0.26 06/04/17 06:41 Bromomethane ug/L ND 10.0 0.29 06/04/17 06:41 Carbon disulfide ug/L ND 100 1.2 06/04/17 06:41 Carbon tetrachloride ug/L ND 1.0 0.25 06/04/17 06:41 Chlorobenzene ug/L ND 3.0 0.23 06/04/17 06:41 Chloroethane ug/L ND 10.0 0.54 06/04/17 06:41 Chloroform ug/L ND 5.0 0.14 06/04/17 06:41 Chloromethane ug/L ND 1.0 0.11 06/04/17 06:41 cis-1,2-Dichloroethene ug/L ND 5.0 0.19 06/04/17 06:41 cis-1,3-Dichloropropene ug/L ND 1.0 0.13 06/04/17 06:41 Dibromochloromethane ug/L ND 3.0 0.21 06/04/17 06:41 Dibromomethane ug/L ND 10.0 0.21 06/04/17 06:41 Ethylbenzene ug/L ND 1.0 0.30 06/04/17 06:41 lodomethane ug/L ND 10.0 0.32 06/04/17 06:41 Methylene Chloride ug/L ND 1.0 0.97 06/04/17 06:41 Styrene ug/L ND 1.0 0.26 06/04/17 06:41 Tetrachloroethene ug/L ND 1.0 0.46 06/04/17 06:41 Toluene ug/L ND 1.0 0.26 06/04/17 06:41 trans-1,2-Dichloroethene ug/L ND 5.0 0.49 06/04/17 06:41 trans- 1,3-Dichloropropene ug/L ND 1.0 0.26 06/04/17 06:41 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2017 01:32 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY MSWLF SWS Pace Project No.: 92342549 METHOD BLANK: 2014180 Matrix: Water Associated Lab Samples: 92342549001, 92342730001, 92342730002, 92342730004, 92342730005, 92342730006 Blank Reporting Parameter Units Result Limit MDL Analyzed trans-1,4-Dichloro-2-butene ug/L ND 100 1.0 06/04/17 06:41 Trichloroethene ug/L ND 1.0 0.47 06/04/17 06:41 Trichlorofluoromethane ug/L ND 1.0 0.20 06/04/17 06:41 Vinyl acetate ug/L ND 50.0 0.35 06/04/17 06:41 Vinyl chloride ug/L ND 1.0 0.62 06/04/17 06:41 Xylene (Total) ug/L ND 5.0 0.66 06/04/17 06:41 1,2-Dichloroethane-d4 (S) % 89 70-130 06/04/17 06:41 4-Bromofluorobenzene (S) % 113 70-130 06/04/17 06:41 Toluene-d8 (S) % 106 70-130 06/04/17 06:41 LABORATORY CONTROL SAMPLE: Parameter 2014181 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 50.1 100 80-125 1,1,1-Trichloroethane ug/L 50 48.8 98 71-129 1,1,2,2-Tetrachloroethane ug/L 50 57.0 114 79-124 1,1,2-Trichloroethane ug/L 50 51.1 102 85-125 1,1-Dichloroethane ug/L 50 49.9 100 73-126 1,1-Dichloroethene ug/L 50 44.7 89 66-135 1,2,3-Trichloropropane ug/L 50 47.3 95 75-130 1,2-Dibromo-3-chloropropane ug/L 50 48.7 97 71-133 1,2-Dibromoethane (EDB) ug/L 50 56.3 113 83-124 1,2-Dichlorobenzene ug/L 50 50.9 102 80-133 1,2-Dichloroethane ug/L 50 45.7 91 67-128 1,2-Dichloropropane ug/L 50 54.4 109 75-132 1,4-Dichlorobenzene ug/L 50 47.7 95 78-130 2-Butanone (MEK) ug/L 100 136 136 61-144 2-Hexanone ug/L 100 110 110 68-143 4-Methyl-2-pentanone (MIBK) ug/L 100 109 109 72-135 Acetone ug/L 100 116 116 48-146 Acrylonitrile ug/L 250 274 110 40-160 Benzene ug/L 50 52.5 105 80-125 Bromochloromethane ug/L 50 47.8 96 71-125 Bromodichloromethane ug/L 50 49.3 99 78-124 Bromoform ug/L 50 48.1 96 71-128 Bromomethane ug/L 50 41.9 84 40-160 Carbon disulfide ug/L 50 50.8J 102 50-160 Carbon tetrachloride ug/L 50 44.5 89 69-131 Chlorobenzene ug/L 50 51.4 103 81-122 Chloroethane ug/L 50 43.7 87 39-148 Chloroform ug/L 50 48.3 97 73-127 Chloromethane ug/L 50 53.8 108 44-146 cis-1,2-Dichloroethene ug/L 50 51.0 102 74-124 cis-1,3-Dichloropropene ug/L 50 53.8 108 72-132 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2017 01:32 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY MSWLF SWS Pace Project No.: 92342549 LABORATORY CONTROL SAMPLE: 2014181 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Dibromochloromethane ug/L 50 47.7 95 78-125 Dibromomethane ug/L 50 48.5 97 82-120 Ethylbenzene ug/L 50 50.3 101 79-121 lodomethane ug/L 100 95.3 95 39-154 Methylene Chloride ug/L 50 49.9 100 64-133 Styrene ug/L 50 49.7 99 84-126 Tetrachloroethene ug/L 50 45.9 92 78-122 Toluene ug/L 50 49.6 99 80-121 trans-1,2-Dichloroethene ug/L 50 51.4 103 71-127 trans- 1,3-Dichloropropene ug/L 50 53.3 107 69-141 trans-1,4-Dichloro-2-butene ug/L 50 94.OJ 188 40-160 L1 Trichloroethene ug/L 50 50.6 101 78-122 Trichlorofluoromethane ug/L 50 45.0 90 53-137 Vinyl acetate ug/L 100 96.4 96 40-160 Vinyl chloride ug/L 50 45.1 90 58-137 Xylene (Total) ug/L 150 141 94 81-126 1,2-Dichloroethane-d4 (S) % 90 70-130 4-Bromofluorobenzene (S) % 98 70-130 Toluene-d8 (S) % 100 70-130 MATRIX SPIKE SAMPLE: 2014183 92342730006 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 19.1 96 70-130 1,1,1-Trichloroethane ug/L ND 20 22.5 112 70-130 1,1,2,2-Tetrachloroethane ug/L ND 20 22.0 110 70-130 1,1,2-Trichloroethane ug/L ND 20 20.1 100 70-130 1,1-Dichloroethane ug/L ND 20 22.3 112 70-130 1,1-Dichloroethene ug/L ND 20 23.0 115 70-166 1,2,3-Trichloropropane ug/L ND 20 18.1 90 70-130 1,2-Dibromo-3-chloropropane ug/L ND 20 18.9 94 70-130 1,2-Dibromoethane (EDB) ug/L ND 20 21.1 106 70-130 1,2-Dichlorobenzene ug/L ND 20 21.2 106 70-130 1,2-Dichloroethane ug/L ND 20 20.3 101 70-130 1,2-Dichloropropane ug/L ND 20 22.9 115 70-130 1,4-Dichlorobenzene ug/L ND 20 20.2 101 70-130 2-Butanone (MEK) ug/L ND 40 46.6J 116 70-130 2-Hexanone ug/L ND 40 44.9J 112 70-130 4-Methyl-2-pentanone (MIBK) ug/L ND 40 42.OJ 105 70-130 Acetone ug/L 11.6J 40 49.1 J 94 70-130 Acrylonitrile ug/L ND 100 113J 113 70-130 Benzene ug/L ND 20 23.2 116 70-148 Bromochloromethane ug/L ND 20 20.9 105 70-130 Bromodichloromethane ug/L ND 20 21.3 106 70-130 Bromoform ug/L ND 20 17.3 86 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2017 01:32 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SURRY MSWLF SWS Pace Project No.: 92342549 MATRIX SPIKE SAMPLE: 2014183 Parameter Units Bromomethane ug/L Carbon disulfide ug/L Carbon tetrachloride ug/L Chlorobenzene ug/L Chloroethane ug/L Chloroform ug/L Chloromethane ug/L cis-1,2-Dichloroethene ug/L cis-1,3-Dichloropropene ug/L Dibromochloromethane ug/L Dibromomethane ug/L Ethylbenzene ug/L lodomethane ug/L Methylene Chloride ug/L Styrene ug/L Tetrachloroethene ug/L Toluene ug/L trans-1,2-Dichloroethene ug/L trans- 1,3-Dichloropropene ug/L trans-1,4-Dichloro-2-butene ug/L Trichloroethene ug/L Trichlorofluoromethane ug/L Vinyl acetate ug/L Vinyl chloride ug/L 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Toluene-d8 (S) % lyULTil»: a bill 9I N_,II: 11i�1kilSEII. a Parameter Units 1,1,1,2Jet rachIoroethane ug/L 1,1,1-Trichloroethane ug/L 1,1,2,2Jet rachIoroethane ug/L 1,1,2-Trichloroethane ug/L 1,1-Dichloroethane ug/L 1,1-Dichloroethene ug/L 1,2,3-Trichloropropane ug/L 1,2-Dibromo-3-chloropropane ug/L 1,2-Dibromoethane (EDB) ug/L 1,2-Dichlorobenzene ug/L 1,2-Dichloroethane ug/L 1,2-Dichloropropane ug/L 1,4-Dichlorobenzene ug/L 2-Butanone (MEK) ug/L QUALITY CONTROL DATA 92342730006 Result Spike Conc. MS Result ND 20 22.4 ND 20 23.6J ND 20 21.0 ND 20 22.0 ND 20 20.9 ND 20 22.8 ND 20 24.6 ND 20 22.8 ND 20 22.4 ND 20 19.5 ND 20 21.8 ND 20 22.3 ND 40 41.2 ND 20 21.8 ND 20 20.9 ND 20 20.8 ND 20 22.5 ND 20 23.9 ND 20 22.7 ND 20 28.2J ND 20 22.5 ND 20 21.7 ND 40 40.5J ND 20 21.2 92342730005 Dup Result Result RPD MS % Rec % Rec Limits Qualifiers 112 70-130 118 70-130 105 70-130 110 70-146 104 70-130 114 70-130 123 70-130 114 70-130 112 70-130 98 70-130 109 70-130 112 70-130 103 70-130 109 70-130 104 70-130 104 70-130 113 70-155 119 70-130 114 70-130 141 70-130 MO 112 69-151 109 70-130 101 70-130 106 70-130 100 70-130 102 70-130 104 70-130 Max RPD Qualifiers ND ND 30 ND ND 30 ND ND 30 ND ND 30 ND ND 30 ND ND 30 ND ND 30 ND ND 30 ND ND 30 ND ND 30 ND ND 30 ND ND 30 ND ND 30 ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2017 01:32 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY MSWLF SWS Pace Project No.: 92342549 SAMPLE DUPLICATE: 2014182 Parameter Units 92342730005 Result Dup Result 2-Hexanone ug/L ND ND 4-Methyl-2-pentanone (MIBK) ug/L ND ND Acetone ug/L ND 13.6J Acrylonitrile ug/L ND ND Benzene ug/L ND ND Bromochloromethane ug/L ND ND Bromodichloromethane ug/L ND ND Bromoform ug/L ND ND Bromomethane ug/L ND ND Carbon disulfide ug/L ND ND Carbon tetrachloride ug/L ND ND Chlorobenzene ug/L ND ND Chloroethane ug/L ND ND Chloroform ug/L ND ND Chloromethane ug/L 0.13J 0.16J cis-1,2-Dichloroethene ug/L ND ND cis-1,3-Dichloropropene ug/L ND ND Dibromochloromethane ug/L ND ND Dibromomethane ug/L ND ND Ethylbenzene ug/L ND ND lodomethane ug/L ND ND Methylene Chloride ug/L ND ND Styrene ug/L ND ND Tetrachloroethene ug/L ND ND Toluene ug/L ND ND trans-1,2-Dichloroethene ug/L ND ND trans- 1,3-Dichloropropene ug/L ND ND trans-1,4-Dichloro-2-butene ug/L ND ND Trichloroethene ug/L ND ND Trichlorofluoromethane ug/L ND ND Vinyl acetate ug/L ND ND Vinyl chloride ug/L ND ND Xylene (Total) ug/L ND ND 1,2-Dichloroethane-d4 (S) % 92 87 4-Bromofluorobenzene (S) % 102 100 Toluene-d8 (S) % 109 108 Max RPD RPD Qualifiers 6 2 1 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2017 01:32 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY MSWLF SWS Pace Project No.: 92342549 QC Batch: 363311 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92342730007, 92342730008 METHOD BLANK: 2014186 Associated Lab Samples: 92342730007, 92342730008 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 0.33 06/04/17 06:59 1,1,1-Trichloroethane ug/L ND 1.0 0.48 06/04/17 06:59 1,1,2,2-Tetrachloroethane ug/L ND 3.0 0.40 06/04/17 06:59 1,1,2-Trichloroethane ug/L ND 1.0 0.29 06/04/17 06:59 1,1-Dichloroethane ug/L ND 5.0 0.32 06/04/17 06:59 1,1-Dichloroethene ug/L ND 5.0 0.56 06/04/17 06:59 1,2,3-Trichloropropane ug/L ND 1.0 0.41 06/04/17 06:59 1,2-Dibromo-3-chloropropane ug/L ND 13.0 2.0 06/04/17 06:59 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 06/04/17 06:59 1,2-Dichlorobenzene ug/L ND 5.0 0.30 06/04/17 06:59 1,2-Dichloroethane ug/L ND 1.0 0.24 06/04/17 06:59 1,2-Dichloropropane ug/L ND 1.0 0.27 06/04/17 06:59 1,4-Dichlorobenzene ug/L ND 1.0 0.33 06/04/17 06:59 2-Butanone (MEK) ug/L ND 100 0.96 06/04/17 06:59 2-Hexanone ug/L ND 50.0 0.46 06/04/17 06:59 4-Methyl-2-pentanone (MIBK) ug/L ND 100 0.33 06/04/17 06:59 Acetone ug/L ND 100 10.0 06/04/17 06:59 Acrylonitrile ug/L ND 200 1.9 06/04/17 06:59 Benzene ug/L ND 1.0 0.25 06/04/17 06:59 Bromochloromethane ug/L ND 3.0 0.17 06/04/17 06:59 Bromodichloromethane ug/L ND 1.0 0.18 06/04/17 06:59 Bromoform ug/L ND 3.0 0.26 06/04/17 06:59 Bromomethane ug/L ND 10.0 0.29 06/04/17 06:59 Carbon disulfide ug/L ND 100 1.2 06/04/17 06:59 Carbon tetrachloride ug/L ND 1.0 0.25 06/04/17 06:59 Chlorobenzene ug/L ND 3.0 0.23 06/04/17 06:59 Chloroethane ug/L ND 10.0 0.54 06/04/17 06:59 Chloroform ug/L ND 5.0 0.14 06/04/17 06:59 Chloromethane ug/L ND 1.0 0.11 06/04/17 06:59 cis-1,2-Dichloroethene ug/L ND 5.0 0.19 06/04/17 06:59 cis-1,3-Dichloropropene ug/L ND 1.0 0.13 06/04/17 06:59 Dibromochloromethane ug/L ND 3.0 0.21 06/04/17 06:59 Dibromomethane ug/L ND 10.0 0.21 06/04/17 06:59 Ethylbenzene ug/L ND 1.0 0.30 06/04/17 06:59 lodomethane ug/L ND 10.0 0.32 06/04/17 06:59 Methylene Chloride ug/L ND 1.0 0.97 06/04/17 06:59 Styrene ug/L ND 1.0 0.26 06/04/17 06:59 Tetrachloroethene ug/L ND 1.0 0.46 06/04/17 06:59 Toluene ug/L ND 1.0 0.26 06/04/17 06:59 trans-1,2-Dichloroethene ug/L ND 5.0 0.49 06/04/17 06:59 trans- 1,3-Dichloropropene ug/L ND 1.0 0.26 06/04/17 06:59 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2017 01:32 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY MSWLF SWS Pace Project No.: 92342549 METHOD BLANK: 2014186 Matrix: Water Associated Lab Samples: 92342730007, 92342730008 Blank Reporting Parameter Units Result Limit MDL trans-1,4-Dichloro-2-butene ug/L ND 100 Trichloroethene ug/L ND 1.0 Trichlorofluoromethane ug/L ND 1.0 Vinyl acetate ug/L ND 50.0 Vinyl chloride ug/L ND 1.0 Xylene (Total) ug/L ND 5.0 1,2-Dichloroethane-d4 (S) % 89 70-130 4-Bromofluorobenzene (S) % 99 70-130 Toluene-d8 (S) % 106 70-130 Analyzed 1.0 06/04/17 06:59 0.47 06/04/17 06:59 0.20 06/04/17 06:59 0.35 06/04/17 06:59 0.62 06/04/17 06:59 0.66 06/04/17 06:59 06/04/17 06:59 06/04/17 06:59 06/04/17 06:59 LABORATORY CONTROL SAMPLE: Parameter 2014187 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 49.7 99 80-125 1,1,1-Trichloroethane ug/L 50 50.8 102 71-129 1,1,2,2-Tetrachloroethane ug/L 50 53.1 106 79-124 1,1,2-Trichloroethane ug/L 50 51.5 103 85-125 1,1-Dichloroethane ug/L 50 52.3 105 73-126 1,1-Dichloroethene ug/L 50 51.6 103 66-135 1,2,3-Trichloropropane ug/L 50 47.0 94 75-130 1,2-Dibromo-3-chloropropane ug/L 50 47.3 95 71-133 1,2-Dibromoethane (EDB) ug/L 50 54.1 108 83-124 1,2-Dichlorobenzene ug/L 50 48.2 96 80-133 1,2-Dichloroethane ug/L 50 48.4 97 67-128 1,2-Dichloropropane ug/L 50 52.7 105 75-132 1,4-Dichlorobenzene ug/L 50 45.6 91 78-130 2-Butanone (MEK) ug/L 100 138 138 61-144 2-Hexanone ug/L 100 108 108 68-143 4-Methyl-2-pentanone (MIBK) ug/L 100 107 107 72-135 Acetone ug/L 100 123 123 48-146 Acrylonitrile ug/L 250 286 114 40-160 Benzene ug/L 50 52.5 105 80-125 Bromochloromethane ug/L 50 48.3 97 71-125 Bromodichloromethane ug/L 50 48.5 97 78-124 Bromoform ug/L 50 48.5 97 71-128 Bromomethane ug/L 50 44.8 90 40-160 Carbon disulfide ug/L 50 52.8J 106 50-160 Carbon tetrachloride ug/L 50 44.2 88 69-131 Chlorobenzene ug/L 50 49.9 100 81-122 Chloroethane ug/L 50 43.6 87 39-148 Chloroform ug/L 50 52.2 104 73-127 Chloromethane ug/L 50 58.1 116 44-146 cis-1,2-Dichloroethene ug/L 50 54.0 108 74-124 cis-1,3-Dichloropropene ug/L 50 52.4 105 72-132 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2017 01:32 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY MSWLF SWS Pace Project No.: 92342549 LABORATORY CONTROL SAMPLE: 2014187 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Dibromochloromethane ug/L 50 48.7 97 78-125 Dibromomethane ug/L 50 46.0 92 82-120 Ethylbenzene ug/L 50 48.0 96 79-121 lodomethane ug/L 100 95.1 95 39-154 Methylene Chloride ug/L 50 53.3 107 64-133 Styrene ug/L 50 48.3 97 84-126 Tetrachloroethene ug/L 50 47.9 96 78-122 Toluene ug/L 50 48.3 97 80-121 trans-1,2-Dichloroethene ug/L 50 53.8 108 71-127 trans- 1,3-Dichloropropene ug/L 50 51.4 103 69-141 trans-1,4-Dichloro-2-butene ug/L 50 99.7J 199 40-160 L1 Trichloroethene ug/L 50 49.5 99 78-122 Trichlorofluoromethane ug/L 50 46.5 93 53-137 Vinyl acetate ug/L 100 103 103 40-160 Vinyl chloride ug/L 50 46.9 94 58-137 Xylene (Total) ug/L 150 141 94 81-126 1,2-Dichloroethane-d4 (S) % 95 70-130 4-Bromofluorobenzene (S) % 99 70-130 Toluene-d8 (S) % 95 70-130 MATRIX SPIKE SAMPLE: 2014189 92342784004 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 19.2 96 70-130 1,1,1-Trichloroethane ug/L ND 20 22.8 114 70-130 1,1,2,2-Tetrachloroethane ug/L ND 20 21.3 106 70-130 1,1,2-Trichloroethane ug/L ND 20 21.1 105 70-130 1,1-Dichloroethane ug/L ND 20 24.1 120 70-130 1,1-Dichloroethene ug/L ND 20 24.1 120 70-166 1,2,3-Trichloropropane ug/L ND 20 20.3 102 70-130 1,2-Dibromo-3-chloropropane ug/L ND 20 19.7 99 70-130 1,2-Dibromoethane (EDB) ug/L ND 20 20.6 103 70-130 1,2-Dichlorobenzene ug/L ND 20 22.0 110 70-130 1,2-Dichloroethane ug/L ND 20 20.7 104 70-130 1,2-Dichloropropane ug/L ND 20 22.8 114 70-130 1,4-Dichlorobenzene ug/L ND 20 21.8 109 70-130 2-Butanone (MEK) ug/L ND 40 46.8J 117 70-130 2-Hexanone ug/L ND 40 41.2J 103 70-130 4-Methyl-2-pentanone (MIBK) ug/L ND 40 42.3J 106 70-130 Acetone ug/L 12.9J 40 49.1 J 90 70-130 Acrylonitrile ug/L ND 100 1111 111 70-130 Benzene ug/L ND 20 23.7 119 70-148 Bromochloromethane ug/L ND 20 21.9 109 70-130 Bromodichloromethane ug/L ND 20 22.4 112 70-130 Bromoform ug/L ND 20 17.7 88 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2017 01:32 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY MSWLF SWS Pace Project No.: 92342549 MATRIX SPIKE SAMPLE: 2014189 92342784004 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Bromomethane ug/L ND 20 23.2 116 70-130 Carbon disulfide ug/L ND 20 24.5J 123 70-130 Carbon tetrachloride ug/L ND 20 21.2 106 70-130 Chlorobenzene ug/L ND 20 22.5 112 70-146 Chloroethane ug/L ND 20 18.9 94 70-130 Chloroform ug/L ND 20 22.3 111 70-130 Chloromethane ug/L 0.14J 20 24.4 121 70-130 cis-1,2-Dichloroethene ug/L 0.22J 20 24.8 123 70-130 cis-1,3-Dichloropropene ug/L ND 20 22.5 113 70-130 Dibromochloromethane ug/L ND 20 19.2 96 70-130 Dibromomethane ug/L ND 20 21.3 107 70-130 Ethylbenzene ug/L ND 20 22.2 111 70-130 lodomethane ug/L ND 40 44.2 110 70-130 Methylene Chloride ug/L ND 20 22.6 113 70-130 Styrene ug/L ND 20 21.3 107 70-130 Tetrachloroethene ug/L ND 20 20.7 103 70-130 Toluene ug/L ND 20 22.2 111 70-155 trans-1,2-Dichloroethene ug/L ND 20 23.7 118 70-130 trans- 1,3-Dichloropropene ug/L ND 20 22.0 110 70-130 trans-1,4-Dichloro-2-butene ug/L ND 20 24.7J 124 70-130 Trichloroethene ug/L ND 20 23.5 117 69-151 Trichlorofluoromethane ug/L ND 20 22.5 112 70-130 Vinyl acetate ug/L ND 40 38.6J 96 70-130 Vinyl chloride ug/L ND 20 21.5 107 70-130 1,2-Dichloroethane-d4 (S) % 95 70-130 4-Bromofluorobenzene (S) % 94 70-130 Toluene-d8 (S) % 99 70-130 SAMPLE DUPLICATE: 2014188 92342784003 Dup Max Parameter Units Result Result RPD RPD Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND ND 30 1,1,1-Trichloroethane ug/L ND ND 30 1,1,2,2-Tetrachloroethane ug/L ND ND 30 1,1,2-Trichloroethane ug/L ND ND 30 1,1-Dichloroethane ug/L 0.37J 0.35J 30 1,1-Dichloroethene ug/L ND ND 30 1,2,3-Trichloropropane ug/L ND ND 30 1,2-Dibromo-3-chloropropane ug/L ND ND 30 1,2-Dibromoethane (EDB) ug/L ND ND 30 1,2-Dichlorobenzene ug/L ND ND 30 1,2-Dichloroethane ug/L ND ND 30 1,2-Dichloropropane ug/L ND 0.86J 30 1,4-Dichlorobenzene ug/L 2.5 2.4 5 30 2-Butanone (MEK) ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2017 01:32 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY MSWLF SWS Pace Project No.: 92342549 SAMPLE DUPLICATE: 2014188 Parameter Units 92342784003 Result Dup Result 2-Hexanone ug/L ND ND 4-Methyl-2-pentanone (MIBK) ug/L ND ND Acetone ug/L 21 AJ 13.9J Acrylonitrile ug/L ND ND Benzene ug/L 0.62J 0.52J Bromochloromethane ug/L ND ND Bromodichloromethane ug/L ND ND Bromoform ug/L ND ND Bromomethane ug/L ND ND Carbon disulfide ug/L ND ND Carbon tetrachloride ug/L ND ND Chlorobenzene ug/L 0.87J 0.97J Chloroethane ug/L ND ND Chloroform ug/L ND ND Chloromethane ug/L ND 0.11J cis-1,2-Dichloroethene ug/L 1.0J 1.0J cis-1,3-Dichloropropene ug/L ND ND Dibromochloromethane ug/L ND ND Dibromomethane ug/L ND ND Ethylbenzene ug/L ND ND lodomethane ug/L ND ND Methylene Chloride ug/L ND ND Styrene ug/L ND ND Tetrachloroethene ug/L ND ND Toluene ug/L 0.88J 0.911 trans-1,2-Dichloroethene ug/L ND ND trans- 1,3-Dichloropropene ug/L ND ND trans-1,4-Dichloro-2-butene ug/L ND ND Trichloroethene ug/L ND ND Trichlorofluoromethane ug/L ND ND Vinyl acetate ug/L ND ND Vinyl chloride ug/L ND ND Xylene (Total) ug/L ND ND 1,2-Dichloroethane-d4 (S) % 90 90 4-Bromofluorobenzene (S) % 99 98 Toluene-d8 (S) % 108 105 Max RPD RPD 3 0 2 3 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2017 01:32 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 44 Pace Analytical Services, LLC aceAnalXical� 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALIFIERS Project: SURRY MSWLF SWS Pace Project No.: 92342549 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high. MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2017 01:32 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 44 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: SURRY MSWLF SWS 92342549 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92342549001 SW-3 EPA 3010A 363146 EPA 6010 364135 92342730001 SW-1 EPA 3010A 363321 EPA 6010 364621 92342730002 SW-2 EPA 3010A 363321 EPA 6010 364621 92342730004 SW-4 EPA 3010A 363321 EPA 6010 364621 92342730005 SWN-1 EPA 3010A 363321 EPA 6010 364621 92342730006 SWN-2 EPA 3010A 363321 EPA 6010 364621 92342549001 SW-3 EPA 3010A 363478 EPA 6020B 363771 92342730001 SW-1 EPA 3010A 363478 EPA 6020B 363771 92342730002 SW-2 EPA 3010A 363479 EPA 6020B 363773 92342730004 SW-4 EPA 3010A 363479 EPA 6020B 363773 92342730005 SWN-1 EPA 3010A 363479 EPA 6020B 363773 92342730006 SWN-2 EPA 3010A 363479 EPA 6020B 363773 92342549001 SW-3 EPA 8260 363307 92342730001 SW-1 EPA 8260 363307 92342730002 SW-2 EPA 8260 363307 92342730004 SW-4 EPA 8260 363307 92342730005 SWN-1 EPA 8260 363307 92342730006 SWN-2 EPA 8260 363307 92342730007 SW -A EPA 8260 363311 92342730008 SW-B EPA 8260 363311 Date: 06/16/2017 01:32 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 38 of 44 �aceAnalXical Laboratory receiving samples: Asheville ❑ Eden[] Document Name: Sample Condition Upon Receipt(SCUR) Document No.: F-CAR-CS-033-Rev.01 Greenwood ❑ Huntersville Document Revised: Sept. 21, 2016 Page 1 of 2 Issuing Authority: Pace Quality Office Raleigh❑ Mechanicsville❑ Sample Condition Upon Client dame: WO# : 92342549 Receipt Project l EUx LISPSCourier: d ❑❑nt❑ C#: 92342549 2I3�41�25I 4I�9 ommercial Pace ❑Other: Custody Seal Present? ❑Yes rANo Seals Intact? ❑Yeso Date/Initials Person Examining Contents:�� Packing Material: ❑Bubble Wrap ',LBubble Bags ❑None ❑Other: Thermometer/ 1 IR Gun ID: T pe of Ice; Wet ❑glue ❑None �Samples on ice, cooling process has begun Correction Factor: Cooler Temp Corrected {°C): , Ll Biological Tissue Frozen? ❑Yes VNo []N/A Temp should be above f ezing to 6°C USDA Regulated Soil N/A, water sample) Did sample riginate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (inter ationally, ❑Yes No including Hawaii and Puerto Rico)? ❑Yes ZNo Chain of Custody Present? Yes ❑No ❑N/A 1. Samples Arrived within Hold Time? E�EEE]Yes Yes ❑No ❑N/A 2. Short Hold Time Analysis (<72 hr.)? o ❑N/A 3. Rush Turn Around Time Requested? ❑Yes No ❑N/A 4. Sufficient Volume? Yes ❑No ❑N/A S. Correct Containers Used? Yes [-]No ❑N/A 6. -Pace Containers Used? Yes [O]N. ❑N/A Containers Intact? Yes ❑No ❑N/A 7. Samples Field Filtered? ❑Yes No ❑N/A S. Note if sediment is visible in the dissolved container Sample Labels match COC? yfYes ❑No ❑N/A 9. -Includes Date/Time/ID/Analysis Matrix: Headspace in VOA Vials (>5-6mm)? ❑Yes No ❑N/A 10. Trip Blank Present? ❑Yes o ❑N/A 11. Trip Blank Custody Seals Present? ❑Yes No ❑N/A CLIENT NOTIFICATION/RESOLUTION Field Data Required? ❑Yes ❑No Person Contacted: Date/Time: Comment:,/Sample Discrepancy: Project Manager SCURF Review: " Date:. C9 ] /A Project Manager SRF Review: T C Date: 6 .5J I Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i,e. Out of Fold, incorrect preservative, out of temp, incorrect containers) Page 39 of 44 n aceAnaVicai Document Name: Sample Condition Upon Receipt(SCUR) Document Revised: Sept. 21, 2016 Page 2 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.01 Pace Quality Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. **Bottom half of box is to list number of bottles Project# 7WO# : %2342549 PM: RWC Due Date: 06/15/17 CLIENT: 92-Municip81 St z m aNl u N a Ln E N W Tr Tr CO z m ` u 1N0 a E �O/1 N M a 00 z 11 (Udl V fN0 d E O u1 7 a CO �` a+ ro }a '= 14 M a m `� a O i+ a J E O N U1 a m _ N n M z U a E O N 2 C6 rM CO z pty v a1 z N a E 4 N N M U ni n Z N a E O N U a m L 4- D ; l7 s 7 v p � li �. ¢ z Z 'a" = E Q ° _ rl 7 N i7 4 v lJ _ J.] E Q v _ rl 2 H C7 a z �4J ` j E Q J E N 3 M C9 4 N z a a = E Q ° - �..5 v� •+ W Q rw V ¢ 0 s w E Q J E O N v1 M (9 Q z C z V E O N M {ry 0 6 M Q Q _ Q z 2 Q O E O �' = 61 C7 O z M Z Q p 7 J E O C H Q7 0 7 4 ? a a Q O E O � 7 QI 0 7 = ? vp a, 2 Q O E O a d C1 0 O ¢ y Y m iOr1 Y v a N " a v X Q O 7 z Y o j Y� a N % } .M-. Y (� � 10 Ql n J E ul ri N a 0 Q z ° a y w J E O N N a U) p n z f6 d J E Q N Q M a m 3 U Z N m o ,C y E p N '� 7 Z l7 \�N 3 N 3 N\N N\ 4 \\N N\ 5 1 11q \\�\ NN N N\ 1 7 N\ 9 �s\N - 10 \\N 11 \\\N \LL--+ 12 F \NLN pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot # Page 40 of 44 ;' ,PacesUiafytical CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Required Client Information: Required Project Information: Invoice Information: Page: i Of 1 company Municipal Engineering Services Report To: Jonathan Pfohl Attention Municipal Engineering Services Address P.O. Box 97 Copy To. Company Name. Garner, NC 27529 Address Regulatory Agency -- Email To. jpfohl(a)meSCO.com Purchase Order No. Pace Quote Reference. Phone 919-772-5393 IF@x. Client Project IDSurry MSWLF SWs Pace Project Manager: Trey Carter Statef Location Requested Due Date/TAT 10 Day (Default) Container Order Number: Pace Profile #. 2103-3 North Carolina Requested Analysts Fittered (YIN) z v a COLLECTED Preservatives Y N N MAMIx CODE nnnking Walor ow _ Z O waver WT Wuslc Walor R 8 m U w J 1 SAMPLE ID SCOSulid SL One Character per box. N START END ¢ wipo we tA-Z, 0-9 1, -j Air AR w¢ a z (gyp N Sample Ids must be unique Otn.r oT o } M m v a Q # Tissue Ts ° z 0 0 ¢ m z DATE TIME DATE TIME uqi o 1 3W-1 WT G 11 1 4 1 3 x x 2 SW-2 WT G 4 1 3 x x SW 3 `' 3 WT G 4 1 3 x x v SW-4 4 Vv f G 4 3 x x SWN-1 5 WT G 4 1 3 x x 6 1 SWN-2 vwT I G 1 1 4 1 3 1 x x 7 SWN-3 Vdr G 4 1 3 x x 8 SW -A WT G 4 1 3 x x 9 SW B WT G 4 1 1 1 1 3 x x 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY r AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS Ir Q hary SAMPLER NAME AND SIGNATURE m m o w z 5 PRINT Name of SAMPLER: Jonathan Pfohl a Z a v } m w o o E z SIGNATURE of SAMPLER: DATE Signed: w m m �ZeAnalytical Laboratory receiving samples: Asheville ❑ Eden[] Document Name: Document Revised: Sept. 21, 2016 Sample Condition Upon Receipt(SCUR) Pagel of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.01 Pace Quality Office Greenwood ❑ Huntersville 0/ Raleigh[] Mechanicsville❑ Sample Condition Upon Client Name:Receipt Project I: WO# : 92342730 Courier: ❑Fed Ex DupS ❑USPS ❑Client ❑ Commercial 5pace ❑Other: / 92342730 Custody Seal Present? ❑Yes 2No Seals Intact? ❑Yes ❑No Date/initials Person Examining Contents: Z r ! $'l Packing Material: ❑Bubble Wrap ❑Bubble Bags ❑None ❑Other: Thermometer: ❑ IR Gun ID: Type of Ice: et ❑alue ❑None Samples on ice, cooling process has begun Correction Factor: Cooler Temp Corrected (°C): f �j , `� Biological Tissue Frozen? ❑Yes QNo ❑N/A Temp should be above fre. zing to VC USDA Regul d Soil (® N/A, water sample} � Did sample , riginate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (interdationally, F-1YeS VINn :--k.— - n.. n1-- -, r-1 - I a- u Comments/Discrepancy: Chain of Custody Present? Efyps [--]No ❑N/A 1. Samples Arrived within Hold Time? i [Yes ❑N// ❑N/A 2. Short Hold Time Analysis (<72 hr.)? ❑Yes Wo ❑N/A 3. Rush Turn Around Time Requested? ❑Y s 6No ❑N/A 4. Sufficient Volume? f ©YVs []NO ❑N/A S. Correct Containers Used? -Pace Containers Used? vv� [IN.❑N/A ❑Na ❑N/A 6. Containers Intact? EYe5 ❑ o ❑N/A 7. Samples Field Filtered? ❑Y s Nn ❑N/A 8. Note if sediment is visible in the dissolved container Sample Labels Match CC1C? -Includes Date/Time/ID/Analysis Matrix: 1 s EN. -L-11 kt ❑ N/A 9. ��y.,,� jt++�+ Headspace in VOA Vials (>5-6mm)? []Yes o ❑N/A 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes ❑Yes [ENo ❑No ❑ i/A N/A 11. CLIENT NOTIFICATIONIRESOLUTION Person Contacted: Comment. -/Sample Discrepa ncy: Project Manager SCURF Review: Project Manager SRF Review: {L field Data Required? ❑Yes ❑No Date/Time: Date: Date: Al -7 Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le, Out of hold, incorrect preservative, out of temp, incorrect containers) Page 42 of 44 9y1 3 ro v m v m 2 w m n x a 0 n a D Q v C. m LA r•F a u 3 CD w m a .-r r o 00 n 0 C � f a t fD w 3 � w n Q _Q Lei f° N W C C- D M � N n 3 0 a 0 rz C v 1° m Q n C m O N i-s o l0 W J Ql Lis F W N F-s '1F fA -1F Item# W fD C i/i fD r+ 0 ZZZ7 BP4U-125 mL Plastic Unpreserved (N/A) (CI-) = M XIAZZZr+ O C -.;r C- y BP3U-250 mL Plastic Unpreserved (N/A) =t s 0 ci m :3 n � 8P2U-500 mL Plastic Unpreserved (N/A) W O 0 * ft BP1U-1 liter Plastic Unpreserved (N/A) Cr a �INNII X 7 _h BP3S-250 mL Plastic H2SO4 (pH < 2) (Cl-) � O Cr BP3N-250 mL plastic HNO3 (pH < 2) n X �- 1+ ry ; BP3Z-250 mL Plastic ZN Acetate & NaOH (>9) 13 It _ 3 s zzzzzBP3C-250 mL Plastic NaOH (pH > 12) (CI-) = rho M WGFU-Wide-mouthed Glass jar Unpreserved 0� O Cr aq AG1U-1 liter Amber Unpreserved (N/A) (CI-) 0 En zz ZF z 77Z zzAG1H-1literAmber HCl (pH <2) �' ,�—D O AG3U-250 mL Amber Unpreserved (N/A) (Cl-) r+ =- o G15-1 liter Amber H2SO4 (pH < 2) 3 y a o 3 C ID gAG3S-250mL Amber H2SO4 (pH < 2) w ' o z Z IDG3A(DG3A)-250 mLAmber NH4Cl (N/A)(CI-) c f° i ^ o r+ m �3 �A " v �/J DG9H-40mLVOAHCI (N/A) O n VG9T-40 mL VQA Na25203 (N/A) n M VG9U-40 mL VOA Unp (N/A) 3 H -- DG9P-40 mL VOA HBP04 (N/A) D " A VOAK (6 vials per kit)-5035 kit (N/A) N i V/GK (3 vials per kit)-VPN/Gas kit (N/A) =C w �^ SPST-125 mL Sterile Plastic (N/A— lab) C3 II lC0 rr c' N SP2T-250 mL Sterile Plastic (N/A —lab) m ha-< 0 0 0 o 0 N a rr 1. M (DD77 7 zz zz .. Z XZZZZ BP3A-250 mL Plastic (NH2)2504 (9.3-9.7) Q171 Q Cubitainer VSGU-20 mLScintillation vials (N/A) v GN v 0 CHAIN -OF -CUSTODY 1 Analytical Request Document ace 4nalyiical (D The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. d Section A Section 9 Section C Required Client Information: Required Project Information: Invoice Information: Page : 1 Of 1 Company: Municipal Engineering Services Re;orl To: Jonathan Pfohl Attention Municipal Engineering Services Address. P.O. BOX 97 Copy To Company Name' Garner, NC 27529 Address: Regulatory Agency Email To ipfohl@mesco.cpm Purchase Order No. Pace Quote Reference. Phone, 919-772-5393 Fax Client Project ID: Slurry MSWLF SWS Pace Project Manager: Trey Carter State! Location Requested Due DatefTAT: 10 Day (Default) Container Order Number. Pace Profile #: 2103-3 North Carolina Requested Analysis Filtered (Y/N) Z I m a COLLECTED Preservatives NJ N MATRIX CODE $ O Dunking We,DW V ZO Watci WT o U r U Wosla Wote, WW SAMPLE ID Z"US-ld 9L m � START END d One Character per box. oil OL N G)¢ IA-Z. n-9 , -j A,, AR W w y .� m sample Ids must be unique Other CT p a w m a. TI354[ TS U I J m Q L Q Lu a a n O �O n� m Q s L) ~ s DATE TIME DATE TIME= i i z z i7 j 1 SW-1 WT G (oil 0--x 4 i 1 3 x x 2 SW-2 yM G 4d9) 4 1 3 x x 3 SW-3 WT G (D g i 4 1 3 x x 4 SW-4 WT G 4 1 3 x x 6 SWN-1 wT G Inf 1 =o� 4 1 3 x x 6 SWN-2 V4T G (y j o� Ob 4 1 3 x x cai 7 BVV" WT G 4 1 3 x x $ SW -A NIT G L!b 1 3 1 1 x A 9 SW B VYT G //� t04AL3v -3 3 3 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS r�DATE SAMPLER NAME AND SIGNATURE m — o S PRINT Name of SAMPLER: .) y Jonathan MOW m - w } m m g o a E Z m} SIGNATURE of SAMPLER: DATE Signed:'m a [D r � � c� ca rn lacieAnalXical" www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 June 15, 2017 Mr. Jonathan Pfohl Municipal Engineering Services 68 Shipwash Dr. Garner, NC 27529 RE: Project: SURRY BANKS Pace Project No.: 92342727 Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory on June 02, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Trey Carter trey. carter@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 28 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SURRY BANKS Pace Project No.: 92342727 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 28 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: SURRY BANKS Pace Project No.: 92342727 Lab ID Sample ID Matrix Date Collected Date Received 92342727001 EB Water 06/01/17 18:00 06/02/17 08:00 92342727002 FB Water 06/01/17 17:55 06/02/17 08:00 92342727003 TB Water 06/01/17 00:00 06/02/17 08:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 28 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: SURRY BANKS 92342727 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92342727001 EB EPA6010 SH1 15 PASI-A EPA 6020E CDF 1 PASI-A EPA 7470 WAB 1 PASI-A EPA 8260 GAW 67 PASI-C SM 4500-CN-E AES2 1 PASI-A 92342727002 FB EPA 6010 SH1 15 PASI-A EPA 6020E CDF 1 PASI-A EPA 7470 WAB 1 PASI-A EPA 8260 GAW 67 PASI-C 92342727003 TB EPA 8260 GAW 67 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 28 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY BANKS Pace Project No.: 92342727 Sample: EB Lab ID: 92342727001 Collected: 06/01/17 18:00 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Tin Vanadium Zinc 6020 MET ICPMS Thallium 7470 Mercury Mercury 8260 MSV Low Level Landfill Acetone Acetonitrile Acrolein Acrylonitrile Allyl chloride Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane Chloroprene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene Date: 06/15/2017 04:16 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 06/04/17 16:40 06/14/17 21:59 7440-36-0 ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 21:59 7440-38-2 ND ug/L 100 2.5 1 06/04/17 16:40 06/14/17 21:59 7440-39-3 ND ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 21:59 7440-41-7 ND ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 21:59 7440-43-9 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 21:59 7440-47-3 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 21:59 7440-48-4 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 21:59 7440-50-8 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 21:59 7439-92-1 ND ug/L 50.0 2.5 1 06/04/17 16:40 06/14/17 21:59 7440-02-0 ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 21:59 7782-49-2 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 21:59 7440-22-4 ND ug/L 100 2.5 1 06/04/17 16:40 06/14/17 21:59 7440-31-5 ND ug/L 25.0 2.5 1 06/04/17 16:40 06/14/17 21:59 7440-62-2 ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 21:59 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3010A ND ug/L 5.5 0.020 1 06/06/17 02:45 06/09/17 17:47 7440-28-0 Analytical Method: EPA 7470 Preparation Method: EPA 7470 ND ug/L 0.20 0.10 1 06/05/17 20:00 06/06/17 09:42 7439-97-6 Analytical Method: EPA 8260 14.4J ug/L 100 10.0 1 06/04/17 21:12 67-64-1 ND ug/L 55.0 2.2 1 06/04/17 21:12 75-05-8 ND ug/L 53.0 1.6 1 06/04/17 21:12 107-02-8 ND ug/L 200 1.9 1 06/04/17 21:12 107-13-1 ND ug/L 10.0 1.5 1 06/04/17 21:12 107-05-1 ND ug/L 1.0 0.25 1 06/04/17 21:12 71-43-2 ND ug/L 3.0 0.17 1 06/04/17 21:12 74-97-5 ND ug/L 1.0 0.18 1 06/04/17 21:12 75-27-4 ND ug/L 3.0 0.26 1 06/04/17 21:12 75-25-2 ND ug/L 10.0 0.29 1 06/04/17 21:12 74-83-9 ND ug/L 100 0.96 1 06/04/17 21:12 78-93-3 ND ug/L 100 1.2 1 06/04/17 21:12 75-15-0 ND ug/L 1.0 0.25 1 06/04/17 21:12 56-23-5 ND ug/L 3.0 0.23 1 06/04/17 21:12 108-90-7 ND ug/L 10.0 0.54 1 06/04/17 21:12 75-00-3 ND ug/L 5.0 0.14 1 06/04/17 21:12 67-66-3 ND ug/L 1.0 0.11 1 06/04/17 21:12 74-87-3 ND ug/L 20.0 0.27 1 06/04/17 21:12 126-99-8 ND ug/L 13.0 2.0 1 06/04/17 21:12 96-12-8 ND ug/L 3.0 0.21 1 06/04/17 21:12 124-48-1 ND ug/L 1.0 0.27 1 06/04/17 21:12 106-93-4 ND ug/L 10.0 0.21 1 06/04/17 21:12 74-95-3 ND ug/L 5.0 0.30 1 06/04/17 21:12 95-50-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 28 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY BANKS Pace Project No.: 92342727 Sample: EB Lab ID: 92342727001 Collected: 06/01/17 18:00 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 1,3-Dichlorobenzene ND ug/L 5.0 0.24 1 06/04/17 21:12 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 06/04/17 21:12 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/04/17 21:12 110-57-6 Dichlorodifluoromethane ND ug/L 5.0 0.21 1 06/04/17 21:12 75-71-8 1,1-Dichloroethane ND ug/L 5.0 0.32 1 06/04/17 21:12 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 06/04/17 21:12 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/04/17 21:12 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 06/04/17 21:12 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/04/17 21:12 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 06/04/17 21:12 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 06/04/17 21:12 142-28-9 2,2-Dichloropropane ND ug/L 15.0 0.13 1 06/04/17 21:12 594-20-7 1,1-Dichloropropene ND ug/L 5.0 0.49 1 06/04/17 21:12 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/04/17 21:12 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/17 21:12 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/17 21:12 100-41-4 Ethyl methacrylate ND ug/L 10.0 0.20 1 06/04/17 21:12 97-63-2 Hexachloro-1,3-butadiene ND ug/L 10.0 0.71 1 06/04/17 21:12 87-68-3 2-Hexanone ND ug/L 50.0 0.46 1 06/04/17 21:12 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/17 21:12 74-88-4 Isobutanol ND ug/L 100 35.0 1 06/04/17 21:12 78-83-1 Methacrylonitrile ND ug/L 100 0.93 1 06/04/17 21:12 126-98-7 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/17 21:12 75-09-2 Methyl methacrylate ND ug/L 30.0 2.0 1 06/04/17 21:12 80-62-6 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/17 21:12 108-10-1 Naphthalene ND ug/L 10.0 0.24 1 06/04/17 21:12 91-20-3 Propionitrile ND ug/L 150 3.6 1 06/04/17 21:12 107-12-0 Styrene ND ug/L 1.0 0.26 1 06/04/17 21:12 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/17 21:12 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/17 21:12 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/17 21:12 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/17 21:12 108-88-3 1,2,4-Trichlorobenzene ND ug/L 10.0 0.35 1 06/04/17 21:12 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/17 21:12 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/17 21:12 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/17 21:12 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/17 21:12 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/17 21:12 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/17 21:12 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/17 21:12 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/17 21:12 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 109 % 70-130 1 06/04/17 21:12 460-00-4 1,2-Dichloroethane-d4 (S) 87 % 70-130 1 06/04/17 21:12 17060-07-0 Toluene-d8 (S) 106 % 70-130 1 06/04/17 21:12 2037-26-5 Date: 06/15/2017 04:16 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 28 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY BANKS Pace Project No.: 92342727 Sample: EB Lab ID: 92342727001 Collected: 06/01/17 18:00 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E Cyanide ND ug/L 10.0 4.0 1 06/07/1713:50 57-12-5 Date: 06/15/2017 04:16 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 28 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY BANKS Pace Project No.: 92342727 Sample: FB Lab ID: 92342727002 Collected: 06/01/17 17:55 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Tin Vanadium Zinc 6020 MET ICPMS Thallium 7470 Mercury Mercury 8260 MSV Low Level Landfill Acetone Acetonitrile Acrolein Acrylonitrile Allyl chloride Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane Chloroprene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene Date: 06/15/2017 04:16 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 06/04/17 16:40 06/14/17 22:03 7440-36-0 ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:03 7440-38-2 ND ug/L 100 2.5 1 06/04/17 16:40 06/14/17 22:03 7440-39-3 ND ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:03 7440-41-7 ND ug/L 1.0 0.50 1 06/04/17 16:40 06/14/17 22:03 7440-43-9 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:03 7440-47-3 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:03 7440-48-4 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:03 7440-50-8 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:03 7439-92-1 ND ug/L 50.0 2.5 1 06/04/17 16:40 06/14/17 22:03 7440-02-0 ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:03 7782-49-2 ND ug/L 10.0 2.5 1 06/04/17 16:40 06/14/17 22:03 7440-22-4 ND ug/L 100 2.5 1 06/04/17 16:40 06/14/17 22:03 7440-31-5 ND ug/L 25.0 2.5 1 06/04/17 16:40 06/14/17 22:03 7440-62-2 ND ug/L 10.0 5.0 1 06/04/17 16:40 06/14/17 22:03 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3010A ND ug/L 5.5 0.020 1 06/06/17 02:45 06/09/17 17:49 7440-28-0 Analytical Method: EPA 7470 Preparation Method: EPA 7470 ND ug/L 0.20 0.10 1 06/05/17 20:00 06/06/17 09:45 7439-97-6 Analytical Method: EPA 8260 10.2J ug/L 100 10.0 1 06/04/17 21:30 67-64-1 ND ug/L 55.0 2.2 1 06/04/17 21:30 75-05-8 ND ug/L 53.0 1.6 1 06/04/17 21:30 107-02-8 ND ug/L 200 1.9 1 06/04/17 21:30 107-13-1 ND ug/L 10.0 1.5 1 06/04/17 21:30 107-05-1 ND ug/L 1.0 0.25 1 06/04/17 21:30 71-43-2 ND ug/L 3.0 0.17 1 06/04/17 21:30 74-97-5 ND ug/L 1.0 0.18 1 06/04/17 21:30 75-27-4 ND ug/L 3.0 0.26 1 06/04/17 21:30 75-25-2 ND ug/L 10.0 0.29 1 06/04/17 21:30 74-83-9 ND ug/L 100 0.96 1 06/04/17 21:30 78-93-3 ND ug/L 100 1.2 1 06/04/17 21:30 75-15-0 ND ug/L 1.0 0.25 1 06/04/17 21:30 56-23-5 ND ug/L 3.0 0.23 1 06/04/17 21:30 108-90-7 ND ug/L 10.0 0.54 1 06/04/17 21:30 75-00-3 ND ug/L 5.0 0.14 1 06/04/17 21:30 67-66-3 ND ug/L 1.0 0.11 1 06/04/17 21:30 74-87-3 ND ug/L 20.0 0.27 1 06/04/17 21:30 126-99-8 ND ug/L 13.0 2.0 1 06/04/17 21:30 96-12-8 ND ug/L 3.0 0.21 1 06/04/17 21:30 124-48-1 ND ug/L 1.0 0.27 1 06/04/17 21:30 106-93-4 ND ug/L 10.0 0.21 1 06/04/17 21:30 74-95-3 ND ug/L 5.0 0.30 1 06/04/17 21:30 95-50-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 28 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY BANKS Pace Project No.: 92342727 Sample: FB Lab ID: 92342727002 Collected: 06/01/17 17:55 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 1,3-Dichlorobenzene ND ug/L 5.0 0.24 1 06/04/17 21:30 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 06/04/17 21:30 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/04/17 21:30 110-57-6 Dichlorodifluoromethane ND ug/L 5.0 0.21 1 06/04/17 21:30 75-71-8 1,1-Dichloroethane ND ug/L 5.0 0.32 1 06/04/17 21:30 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 06/04/17 21:30 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/04/17 21:30 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 06/04/17 21:30 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/04/17 21:30 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 06/04/17 21:30 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 06/04/17 21:30 142-28-9 2,2-Dichloropropane ND ug/L 15.0 0.13 1 06/04/17 21:30 594-20-7 1,1-Dichloropropene ND ug/L 5.0 0.49 1 06/04/17 21:30 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/04/17 21:30 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/17 21:30 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/17 21:30 100-41-4 Ethyl methacrylate ND ug/L 10.0 0.20 1 06/04/17 21:30 97-63-2 Hexachloro-1,3-butadiene ND ug/L 10.0 0.71 1 06/04/17 21:30 87-68-3 2-Hexanone ND ug/L 50.0 0.46 1 06/04/17 21:30 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/17 21:30 74-88-4 Isobutanol ND ug/L 100 35.0 1 06/04/17 21:30 78-83-1 Methacrylonitrile ND ug/L 100 0.93 1 06/04/17 21:30 126-98-7 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/17 21:30 75-09-2 Methyl methacrylate ND ug/L 30.0 2.0 1 06/04/17 21:30 80-62-6 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/17 21:30 108-10-1 Naphthalene ND ug/L 10.0 0.24 1 06/04/17 21:30 91-20-3 Propionitrile ND ug/L 150 3.6 1 06/04/17 21:30 107-12-0 Styrene ND ug/L 1.0 0.26 1 06/04/17 21:30 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/17 21:30 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/17 21:30 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/17 21:30 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/17 21:30 108-88-3 1,2,4-Trichlorobenzene ND ug/L 10.0 0.35 1 06/04/17 21:30 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/17 21:30 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/17 21:30 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/17 21:30 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/17 21:30 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/17 21:30 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/17 21:30 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/17 21:30 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/17 21:30 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 103 % 70-130 1 06/04/17 21:30 460-00-4 1,2-Dichloroethane-d4 (S) 89 % 70-130 1 06/04/17 21:30 17060-07-0 Toluene-d8 (S) 106 % 70-130 1 06/04/17 21:30 2037-26-5 Date: 06/15/2017 04:16 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 9 of 28 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY BANKS Pace Project No.: 92342727 Sample: TB Lab ID: 92342727003 Collected: 06/01/17 00:00 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 06/04/17 21:48 67-64-1 Acetonitrile ND ug/L 55.0 2.2 1 06/04/17 21:48 75-05-8 Acrolein ND ug/L 53.0 1.6 1 06/04/17 21:48 107-02-8 Acrylonitrile ND ug/L 200 1.9 1 06/04/17 21:48 107-13-1 Allyl chloride ND ug/L 10.0 1.5 1 06/04/17 21:48 107-05-1 Benzene ND ug/L 1.0 0.25 1 06/04/17 21:48 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 06/04/17 21:48 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 06/04/17 21:48 75-27-4 Bromoform ND ug/L 3.0 0.26 1 06/04/17 21:48 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 06/04/17 21:48 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 06/04/17 21:48 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 06/04/17 21:48 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 06/04/17 21:48 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 06/04/17 21:48 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 06/04/17 21:48 75-00-3 Chloroform ND ug/L 5.0 0.14 1 06/04/17 21:48 67-66-3 Chloromethane 0.14J ug/L 1.0 0.11 1 06/04/17 21:48 74-87-3 Chloroprene ND ug/L 20.0 0.27 1 06/04/17 21:48 126-99-8 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 06/04/17 21:48 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 06/04/17 21:48 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 06/04/17 21:48 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 06/04/17 21:48 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 06/04/17 21:48 95-50-1 1,3-Dichlorobenzene ND ug/L 5.0 0.24 1 06/04/17 21:48 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 06/04/17 21:48 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 06/04/17 21:48 110-57-6 Dichlorodifluoromethane ND ug/L 5.0 0.21 1 06/04/17 21:48 75-71-8 1,1-Dichloroethane ND ug/L 5.0 0.32 1 06/04/17 21:48 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 06/04/17 21:48 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 06/04/17 21:48 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 06/04/17 21:48 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 06/04/17 21:48 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 06/04/17 21:48 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 06/04/17 21:48 142-28-9 2,2-Dichloropropane ND ug/L 15.0 0.13 1 06/04/17 21:48 594-20-7 1,1-Dichloropropene ND ug/L 5.0 0.49 1 06/04/17 21:48 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 06/04/17 21:48 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 06/04/17 21:48 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 06/04/17 21:48 100-41-4 Ethyl methacrylate ND ug/L 10.0 0.20 1 06/04/17 21:48 97-63-2 Hexachloro-1,3-butadiene ND ug/L 10.0 0.71 1 06/04/17 21:48 87-68-3 2-Hexanone ND ug/L 50.0 0.46 1 06/04/17 21:48 591-78-6 lodomethane ND ug/L 10.0 0.32 1 06/04/17 21:48 74-88-4 Isobutanol ND ug/L 100 35.0 1 06/04/17 21:48 78-83-1 Methacrylonitrile ND ug/L 100 0.93 1 06/04/17 21:48 126-98-7 Methylene Chloride ND ug/L 1.0 0.97 1 06/04/17 21:48 75-09-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/15/2017 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 28 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY BANKS Pace Project No.: 92342727 Sample: TB Lab ID: 92342727003 Collected: 06/01/17 00:00 Received: 06/02/17 08:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Methyl methacrylate ND ug/L 30.0 2.0 1 06/04/17 21:48 80-62-6 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 06/04/17 21:48 108-10-1 Naphthalene ND ug/L 10.0 0.24 1 06/04/17 21:48 91-20-3 Propionitrile ND ug/L 150 3.6 1 06/04/17 21:48 107-12-0 Styrene ND ug/L 1.0 0.26 1 06/04/17 21:48 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 06/04/17 21:48 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 06/04/17 21:48 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 06/04/17 21:48 127-18-4 Toluene ND ug/L 1.0 0.26 1 06/04/17 21:48 108-88-3 1,2,4-Trichlorobenzene ND ug/L 10.0 0.35 1 06/04/17 21:48 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 06/04/17 21:48 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 06/04/17 21:48 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 06/04/17 21:48 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 06/04/17 21:48 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 06/04/17 21:48 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 06/04/17 21:48 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 06/04/17 21:48 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 06/04/17 21:48 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 06/04/17 21:48 460-00-4 1,2-Dichloroethane-d4 (S) 89 % 70-130 1 06/04/17 21:48 17060-07-0 Toluene-d8 (S) 107 % 70-130 1 06/04/17 21:48 2037-26-5 Date: 06/15/2017 04:16 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 28 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BANKS Pace Project No.: 92342727 QC Batch: 363459 Analysis Method: EPA 7470 QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury Associated Lab Samples: 92342727001, 92342727002 METHOD BLANK: 2015066 Matrix: Water Associated Lab Samples: 92342727001, 92342727002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Mercury ug/L ND 0.20 0.10 06/06/17 09:31 LABORATORY CONTROL SAMPLE: 2015067 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.4 95 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2015068 2015069 MS MSD 92342658001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Mercury ug/L ND 2.5 2.5 2.4 1.6 93 62 75-125 40 25 M1,R1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/15/2017 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 28 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BANKS Pace Project No.: 92342727 QC Batch: 363321 Analysis Method: EPA 6010 QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92342727001, 92342727002 METHOD BLANK: 2014222 Associated Lab Samples: 92342727001, 92342727002 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Qualifiers Antimony ug/L ND 5.0 3.9 06/14/17 21:19 Arsenic ug/L ND 10.0 5.0 06/14/17 21:19 Barium ug/L ND 5.0 2.5 06/14/17 21:19 Beryllium ug/L ND 1.0 0.50 06/14/17 21:19 Cadmium ug/L ND 1.0 0.50 06/14/17 21:19 Chromium ug/L ND 5.0 2.5 06/14/17 21:19 Cobalt ug/L ND 5.0 2.5 06/14/17 21:19 Copper ug/L ND 5.0 2.5 06/14/17 21:19 Lead ug/L ND 5.0 2.5 06/14/17 21:19 Nickel ug/L ND 5.0 2.5 06/14/17 21:19 Selenium ug/L ND 10.0 5.0 06/14/17 21:19 Silver ug/L ND 5.0 2.5 06/14/17 21:19 Tin ug/L ND 5.0 2.5 06/14/17 21:19 Vanadium ug/L ND 5.0 2.5 06/14/17 21:19 Zinc ug/L ND 10.0 5.0 06/14/17 21:19 LABORATORY CONTROL SAMPLE: 2014223 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Antimony ug/L 500 496 99 80-120 Arsenic ug/L 500 475 95 80-120 Barium ug/L 500 511 102 80-120 Beryllium ug/L 500 457 91 80-120 Cadmium ug/L 500 512 102 80-120 Chromium ug/L 500 463 93 80-120 Cobalt ug/L 500 498 100 80-120 Copper ug/L 500 494 99 80-120 Lead ug/L 500 486 97 80-120 Nickel ug/L 500 463 93 80-120 Selenium ug/L 500 501 100 80-120 Silver ug/L 250 235 94 80-120 Tin ug/L 500 485 97 80-120 Vanadium ug/L 500 456 91 80-120 Zinc ug/L 500 472 94 80-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/15/2017 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 28 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: SURRY BANKS 92342727 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2014224 2014225 MS MSD 92342605016 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 517 501 103 100 75-125 3 20 Arsenic ug/L 174 500 500 672 657 100 97 75-125 2 20 Barium ug/L 8.0 500 500 546 530 108 104 75-125 3 20 Beryllium ug/L 0.73J 500 500 481 471 96 94 75-125 2 20 Cadmium ug/L 1.7 500 500 540 524 108 105 75-125 3 20 Chromium ug/L ND 500 500 486 470 97 94 75-125 3 20 Cobalt ug/L 75.0 500 500 594 577 104 100 75-125 3 20 Copper ug/L ND 500 500 522 509 104 102 75-125 3 20 Lead ug/L 4AJ 500 500 506 491 100 97 75-125 3 20 Nickel ug/L 3.2J 500 500 481 466 96 93 75-125 3 20 Selenium ug/L ND 500 500 511 501 102 100 75-125 2 20 Silver ug/L ND 250 250 246 238 99 95 75-125 4 20 Tin ug/L ND 500 500 503 484 101 97 75-125 4 20 Vanadium ug/L ND 500 500 482 466 96 93 75-125 3 20 Zinc ug/L 5.8J 500 500 495 479 98 95 75-125 3 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/15/2017 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 28 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BANKS Pace Project No.: 92342727 QC Batch: 363478 Analysis Method: EPA 6020B QC Batch Method: EPA 3010A Analysis Description: 6020 MET Associated Lab Samples: 92342727001, 92342727002 METHOD BLANK: 2015139 Matrix: Water Associated Lab Samples: 92342727001, 92342727002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Thallium ug/L ND 0.10 0.020 06/09/1716:55 LABORATORY CONTROL SAMPLE: 2015140 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Thallium ug/L 100 90.8 91 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2015141 2015142 MS MSD 92342795001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Thallium ug/L 0.0901 100 100 91.9 96.1 92 96 75-125 4 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/15/2017 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 28 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BANKS Pace Project No.: 92342727 QC Batch: 363328 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92342727001, 92342727002, 92342727003 METHOD BLANK: 2014255 Matrix: Associated Lab Samples: 92342727001, 92342727002, 92342727003 Blank Parameter Units Result Water Reporting Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 0.33 06/04/17 20:01 1,1,1-Trichloroethane ug/L ND 1.0 0.48 06/04/17 20:01 1,1,2,2-Tetrachloroethane ug/L ND 3.0 0.40 06/04/17 20:01 1,1,2-Trichloroethane ug/L ND 1.0 0.29 06/04/17 20:01 1,1-Dichloroethane ug/L ND 5.0 0.32 06/04/17 20:01 1,1-Dichloroethene ug/L ND 5.0 0.56 06/04/17 20:01 1,1-Dichloropropene ug/L ND 5.0 0.49 06/04/17 20:01 1,2,3-Trichloropropane ug/L ND 1.0 0.41 06/04/17 20:01 1,2,4-Trichlorobenzene ug/L ND 10.0 0.35 06/04/17 20:01 1,2-Dibromo-3-chloropropane ug/L ND 13.0 2.0 06/04/17 20:01 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 06/04/17 20:01 1,2-Dichlorobenzene ug/L ND 5.0 0.30 06/04/17 20:01 1,2-Dichloroethane ug/L ND 1.0 0.24 06/04/17 20:01 1,2-Dichloropropane ug/L ND 1.0 0.27 06/04/17 20:01 1,3-Dichlorobenzene ug/L ND 5.0 0.24 06/04/17 20:01 1,3-Dichloropropane ug/L ND 1.0 0.28 06/04/17 20:01 1,4-Dichlorobenzene ug/L ND 1.0 0.33 06/04/17 20:01 2,2-Dichloropropane ug/L ND 15.0 0.13 06/04/17 20:01 2-Butanone (MEK) ug/L ND 100 0.96 06/04/17 20:01 2-Hexanone ug/L ND 50.0 0.46 06/04/17 20:01 4-Methyl-2-pentanone (MIBK) ug/L ND 100 0.33 06/04/17 20:01 Acetone ug/L ND 100 10.0 06/04/17 20:01 Acetonitrile ug/L ND 55.0 2.2 06/04/17 20:01 Acrolein ug/L ND 53.0 1.6 06/04/17 20:01 Acrylonitrile ug/L ND 200 1.9 06/04/17 20:01 Allyl chloride ug/L ND 10.0 1.5 06/04/17 20:01 Benzene ug/L ND 1.0 0.25 06/04/17 20:01 Bromochloromethane ug/L ND 3.0 0.17 06/04/17 20:01 Bromodichloromethane ug/L ND 1.0 0.18 06/04/17 20:01 Bromoform ug/L ND 3.0 0.26 06/04/17 20:01 Bromomethane ug/L ND 10.0 0.29 06/04/17 20:01 Carbon disulfide ug/L ND 100 1.2 06/04/17 20:01 Carbon tetrachloride ug/L ND 1.0 0.25 06/04/17 20:01 Chlorobenzene ug/L ND 3.0 0.23 06/04/17 20:01 Chloroethane ug/L ND 10.0 0.54 06/04/17 20:01 Chloroform ug/L ND 5.0 0.14 06/04/17 20:01 Chloromethane ug/L ND 1.0 0.11 06/04/17 20:01 Chloroprene ug/L ND 20.0 0.27 06/04/17 20:01 cis-1,2-Dichloroethene ug/L ND 5.0 0.19 06/04/17 20:01 cis-1,3-Dichloropropene ug/L ND 1.0 0.13 06/04/17 20:01 Dibromochloromethane ug/L ND 3.0 0.21 06/04/17 20:01 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/15/2017 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 28 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BANKS Pace Project No.: 92342727 METHOD BLANK: 2014255 Matrix: Associated Lab Samples: 92342727001, 92342727002, 92342727003 Blank Parameter Units Result Water Reporting Limit MDL Analyzed Dibromomethane ug/L ND 10.0 0.21 06/04/17 20:01 Dichlorodifluoromethane ug/L ND 5.0 0.21 06/04/17 20:01 Ethyl methacrylate ug/L ND 10.0 0.20 06/04/17 20:01 Ethylbenzene ug/L ND 1.0 0.30 06/04/17 20:01 Hexachloro-1,3-butadiene ug/L ND 10.0 0.71 06/04/17 20:01 lodomethane ug/L ND 10.0 0.32 06/04/17 20:01 Isobutanol ug/L ND 100 35.0 06/04/17 20:01 Methacrylonitrile ug/L ND 100 0.93 06/04/17 20:01 Methyl methacrylate ug/L ND 30.0 2.0 06/04/17 20:01 Methylene Chloride ug/L ND 1.0 0.97 06/04/17 20:01 Naphthalene ug/L ND 10.0 0.24 06/04/17 20:01 Propionitrile ug/L ND 150 3.6 06/04/17 20:01 Styrene ug/L ND 1.0 0.26 06/04/17 20:01 Tetrachloroethene ug/L ND 1.0 0.46 06/04/17 20:01 Toluene ug/L ND 1.0 0.26 06/04/17 20:01 trans-1,2-Dichloroethene ug/L ND 5.0 0.49 06/04/17 20:01 trans- 1,3-Dichloropropene ug/L ND 1.0 0.26 06/04/17 20:01 trans-1,4-Dichloro-2-butene ug/L ND 100 1.0 06/04/17 20:01 Trichloroethene ug/L ND 1.0 0.47 06/04/17 20:01 Trichlorofluoromethane ug/L ND 1.0 0.20 06/04/17 20:01 Vinyl acetate ug/L ND 50.0 0.35 06/04/17 20:01 Vinyl chloride ug/L ND 1.0 0.62 06/04/17 20:01 Xylene (Total) ug/L ND 5.0 0.66 06/04/17 20:01 1,2-Dichloroethane-d4 (S) % 85 70-130 06/04/17 20:01 4-Bromofluorobenzene (S) % 100 70-130 06/04/17 20:01 Toluene-d8 (S) % 115 70-130 06/04/17 20:01 LABORATORY CONTROL SAMPLE: Parameter 2014256 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 46.6 93 80-125 1,1,1-Trichloroethane ug/L 50 50.7 101 71-129 1,1,2,2-Tetrachloroethane ug/L 50 49.8 100 79-124 1,1,2-Trichloroethane ug/L 50 48.9 98 85-125 1,1-Dichloroethane ug/L 50 49.6 99 73-126 1,1-Dichloroethene ug/L 50 46.9 94 66-135 1,1-Dichloropropene ug/L 50 51.9 104 74-135 1,2,3-Trichloropropane ug/L 50 46.5 93 75-130 1,2,4-Trichlorobenzene ug/L 50 46.5 93 75-134 1,2-Dibromo-3-chloropropane ug/L 50 46.7 93 71-133 1,2-Dibromoethane (EDB) ug/L 50 54.5 109 83-124 1,2-Dichlorobenzene ug/L 50 47.5 95 80-133 1,2-Dichloroethane ug/L 50 47.0 94 67-128 1,2-Dichloropropane ug/L 50 53.4 107 75-132 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/15/2017 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 28 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BANKS Pace Project No.: 92342727 LABORATORY CONTROL SAMPLE: Parameter 2014256 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,3-Dichlorobenzene ug/L 50 48.1 96 77-130 1,3-Dichloropropane ug/L 50 54.1 108 76-131 1,4-Dichlorobenzene ug/L 50 47.9 96 78-130 2,2-Dichloropropane ug/L 50 50.7 101 40-160 2-Butanone (MEK) ug/L 100 126 126 61-144 2-Hexanone ug/L 100 101 101 68-143 4-Methyl-2-pentanone (MIBK) ug/L 100 94.9J 95 72-135 Acetone ug/L 100 115 115 48-146 Acetonitrile ug/L 500 525 105 62-150 Acrolein ug/L 250 320 128 24-160 Acrylonitrile ug/L 250 268 107 40-160 Allyl chloride ug/L 50 47.6 95 66-137 Benzene ug/L 50 52.1 104 80-125 Bromochloromethane ug/L 50 48.9 98 71-125 Bromodichloromethane ug/L 50 48.5 97 78-124 Bromoform ug/L 50 43.1 86 71-128 Bromomethane ug/L 50 42.1 84 40-160 Carbon disulfide ug/L 50 49.3J 99 50-160 Carbon tetrachloride ug/L 50 45.1 90 69-131 Chlorobenzene ug/L 50 48.8 98 81-122 Chloroethane ug/L 50 40.8 82 39-148 Chloroform ug/L 50 50.9 102 73-127 Chloromethane ug/L 50 49.9 100 44-146 Chloroprene ug/L 50 49.3 99 75-145 cis-1,2-Dichloroethene ug/L 50 52.5 105 74-124 cis-1,3-Dichloropropene ug/L 50 54.1 108 72-132 Dibromochloromethane ug/L 50 47.5 95 78-125 Dibromomethane ug/L 50 44.2 88 82-120 Dichlorodifluoromethane ug/L 50 41.1 82 34-157 Ethyl methacrylate ug/L 50 45.7 91 82-121 Ethylbenzene ug/L 50 50.1 100 79-121 Hexachloro-1,3-butadiene ug/L 50 43.5 87 72-131 lodomethane ug/L 100 91.7 92 39-154 Isobutanol ug/L 1000 1130 113 34-160 Methacrylonitrile ug/L 500 563 113 74-134 Methyl methacrylate ug/L 50 43.5 87 84-124 Methylene Chloride ug/L 50 53.6 107 64-133 Naphthalene ug/L 50 48.6 97 73-133 Propionitrile ug/L 500 562 112 73-140 Styrene ug/L 50 51.0 102 84-126 Tetrachloroethene ug/L 50 44.8 90 78-122 Toluene ug/L 50 46.4 93 80-121 trans-1,2-Dichloroethene ug/L 50 52.3 105 71-127 trans- 1,3-Dichloropropene ug/L 50 52.4 105 69-141 trans-1,4-Dichloro-2-butene ug/L 50 68.3J 137 40-160 Trichloroethene ug/L 50 50.4 101 78-122 Trichlorofluoromethane ug/L 50 45.4 91 53-137 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/15/2017 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 28 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BANKS Pace Project No.: 92342727 LABORATORY CONTROL SAMPLE: 2014256 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Vinyl acetate ug/L 100 99.2 99 40-160 Vinyl chloride ug/L 50 41.9 84 58-137 Xylene (Total) ug/L 150 149 99 81-126 1,2-Dichloroethane-d4 (S) % 103 70-130 4-Bromofluorobenzene (S) % 107 70-130 Toluene-d8 (S) % 96 70-130 MATRIX SPIKE SAMPLE: 2014258 92342478011 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 20.0 100 70-130 1,1,1-Trichloroethane ug/L ND 20 23.0 115 70-130 1,1,2,2-Tetrachloroethane ug/L ND 20 22.1 110 70-130 1,1,2-Trichloroethane ug/L ND 20 22.2 111 70-130 1,1-Dichloroethane ug/L ND 20 23.1 116 70-130 1,1-Dichloroethene ug/L ND 20 23.0 115 70-166 1,1-Dichloropropene ug/L ND 20 23.3 116 70-130 1,2,3-Trichloropropane ug/L ND 20 19.5 98 70-130 1,2,4-Trichlorobenzene ug/L ND 20 19.3 97 70-130 1,2-Dibromo-3-chloropropane ug/L ND 20 18.2 91 70-130 1,2-Dibromoethane (EDB) ug/L ND 20 19.7 99 70-130 1,2-Dichlorobenzene ug/L ND 20 20.9 105 70-130 1,2-Dichloroethane ug/L ND 20 21.3 106 70-130 1,2-Dichloropropane ug/L ND 20 24.1 120 70-130 1,3-Dichlorobenzene ug/L ND 20 21.7 108 70-130 1,3-Dichloropropane ug/L ND 20 20.4 102 70-130 1,4-Dichlorobenzene ug/L ND 20 21.1 105 70-130 2,2-Dichloropropane ug/L ND 20 21.2 106 70-130 2-Butanone (MEK) ug/L ND 40 47.7J 119 70-130 2-Hexanone ug/L ND 40 40.9J 102 70-130 4-Methyl-2-pentanone (MIBK) ug/L ND 40 43.2J 108 70-130 Acetone ug/L 14AJ 40 93.5J 198 70-130 M1 Acetonitrile ug/L ND 200 219 110 70-130 Acrolein ug/L ND 100 117 117 70-130 Acrylonitrile ug/L ND 100 114J 114 70-130 Allyl chloride ug/L ND 20 26.8 134 70-130 M1 Benzene ug/L ND 20 23.4 117 70-148 Bromochloromethane ug/L ND 20 21.4 107 70-130 Bromodichloromethane ug/L ND 20 22.4 112 70-130 Bromoform ug/L ND 20 16.5 83 70-130 Bromomethane ug/L ND 20 19.8 99 70-130 Carbon disulfide ug/L ND 20 23AJ 117 70-130 Carbon tetrachloride ug/L ND 20 22.4 112 70-130 Chlorobenzene ug/L ND 20 22.1 110 70-146 Chloroethane ug/L ND 20 21.7 108 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/15/2017 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 28 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BANKS Pace Project No.: 92342727 MATRIX SPIKE SAMPLE: Parameter 2014258 Units 92342478011 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers Chloroform ug/L ND 20 23.2 116 70-130 Chloromethane ug/L ND 20 25.8 129 70-130 Chloroprene ug/L ND 20 22.8 114 70-130 cis-1,2-Dichloroethene ug/L 0.64J 20 24.5 119 70-130 cis-1,3-Dichloropropene ug/L ND 20 23.4 117 70-130 Dibromochloromethane ug/L ND 20 18.4 92 70-130 Dibromomethane ug/L ND 20 21.7 108 70-130 Dichlorodifluoromethane ug/L ND 20 19.2 96 70-130 Ethyl methacrylate ug/L ND 20 19.4 97 70-130 Ethylbenzene ug/L ND 20 23.0 115 70-130 Hexachloro-1,3-butadiene ug/L ND 20 19.3 96 70-130 lodomethane ug/L ND 40 41.6 104 70-130 Isobutanol ug/L ND 400 419 105 70-130 Methacrylonitrile ug/L ND 200 230 115 70-130 Methyl methacrylate ug/L ND 20 19.7J 98 70-130 Methylene Chloride ug/L ND 20 23.2 116 70-130 Naphthalene ug/L ND 20 21.6 108 70-130 Propionitrile ug/L ND 200 243 121 70-130 Styrene ug/L ND 20 22.3 112 70-130 Tetrachloroethene ug/L ND 20 19.4 97 70-130 Toluene ug/L ND 20 22.7 113 70-155 trans-1,2-Dichloroethene ug/L ND 20 25.0 125 70-130 trans- 1,3-Dichloropropene ug/L ND 20 21.8 109 70-130 trans-1,4-Dichloro-2-butene ug/L ND 20 21.3J 106 70-130 Trichloroethene ug/L ND 20 23.8 119 69-151 Trichlorofluoromethane ug/L ND 20 22.1 111 70-130 Vinyl acetate ug/L ND 40 37.6J 94 70-130 Vinyl chloride ug/L ND 20 21.8 109 70-130 1,2-Dichloroethane-d4 (S) % 97 70-130 4-Bromofluorobenzene (S) % 109 70-130 Toluene-d8 (S) % 99 70-130 SAMPLE DUPLICATE: 2014257 92342478010 Dup Max Parameter Units Result Result RPD RPD Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND ND 30 1,1,1-Trichloroethane ug/L ND ND 30 1,1,2,2-Tetrachloroethane ug/L ND ND 30 1,1,2-Trichloroethane ug/L ND ND 30 1,1-Dichloroethane ug/L 0.36J 0.50J 30 1,1-Dichloroethene ug/L ND ND 30 1,1-Dichloropropene ug/L ND ND 30 1,2,3-Trichloropropane ug/L ND ND 30 1,2,4-Trichlorobenzene ug/L ND ND 30 1,2-Dibromo-3-chloropropane ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/15/2017 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 28 Pace Analytical Services, LLC aceAnalXical� 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: SURRY BANKS Pace Project No.: 92342727 SAMPLE DUPLICATE: 2014257 Parameter Units 92342478010 Result Dup Result RPD Max RPD Qualifiers 1,2-Dibromoethane (EDB) ug/L ND ND 30 1,2-Dichlorobenzene ug/L ND ND 30 1,2-Dichloroethane ug/L ND ND 30 1,2-Dichloropropane ug/L ND ND 30 1,3-Dichlorobenzene ug/L ND ND 30 1,3-Dichloropropane ug/L ND ND 30 1,4-Dichlorobenzene ug/L ND ND 30 2,2-Dichloropropane ug/L ND ND 30 2-Butanone (MEK) ug/L ND ND 30 2-Hexanone ug/L ND ND 30 4-Methyl-2-pentanone (MIBK) ug/L ND ND 30 Acetone ug/L ND ND 30 Acetonitrile ug/L ND ND 30 Acrolein ug/L ND ND 30 Acrylonitrile ug/L ND ND 30 Allyl chloride ug/L ND ND 30 Benzene ug/L ND ND 30 Bromochloromethane ug/L ND ND 30 Bromodichloromethane ug/L ND ND 30 Bromoform ug/L ND ND 30 Bromomethane ug/L ND ND 30 Carbon disulfide ug/L ND ND 30 Carbon tetrachloride ug/L ND ND 30 Chlorobenzene ug/L ND ND 30 Chloroethane ug/L ND ND 30 Chloroform ug/L ND ND 30 Chloromethane ug/L ND 0.29J 30 Chloroprene ug/L ND ND 30 cis-1,2-Dichloroethene ug/L 0.65J 0.88J 30 cis-1,3-Dichloropropene ug/L ND ND 30 Dibromochloromethane ug/L ND ND 30 Dibromomethane ug/L ND ND 30 Dichlorodifluoromethane ug/L ND ND 30 Ethyl methacrylate ug/L ND ND 30 Ethylbenzene ug/L ND ND 30 Hexachloro-1,3-butadiene ug/L ND ND 30 lodomethane ug/L ND ND 30 Isobutanol ug/L ND ND 30 Methacrylonitrile ug/L ND ND 30 Methyl methacrylate ug/L ND ND 30 Methylene Chloride ug/L ND ND 30 Naphthalene ug/L ND ND 30 Propionitrile ug/L ND ND 30 Styrene ug/L ND ND 30 Tetrachloroethene ug/L ND ND 30 Toluene ug/L ND ND 30 trans-1,2-Dichloroethene ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/15/2017 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 28 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SURRY BANKS Pace Project No.: 92342727 SAMPLE DUPLICATE: 2014257 Parameter trans- 1,3-Dichloropropene trans-1,4-Dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylene (Total) 1,2-Dichloroethane-d4 (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) QUALITY CONTROL DATA Units 92342478010 Result Dup Result ug/L ND ND ug/L ND ND ug/L ND ND ug/L ND ND ug/L ND ND ug/L ND ND ug/L ND ND % 92 92 103 105 109 108 IVV 0 2 2 Max RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/15/2017 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 28 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BANKS Pace Project No.: 92342727 QC Batch: 363513 Analysis Method: SM 4500-CN-E QC Batch Method: SM 4500-CN-E Analysis Description: 450OCNE Cyanide, Total Associated Lab Samples: 92342727001 METHOD BLANK: 2015224 Matrix: Water Associated Lab Samples: 92342727001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Cyanide ug/L ND 10.0 4.0 06/07/1713:52 LABORATORY CONTROL SAMPLE: 2015225 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 101 101 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2015226 2015227 MS MSD 92342317015 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 97.6 95.4 94 91 80-120 2 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2015228 2015229 MS MSD 92342712006 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L 0.013 100 100 41.2 31.4 29 19 80-120 27 10 M1,R1 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/15/2017 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 28 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: SURRY BANKS Pace Project No.: 92342727 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/15/2017 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 28 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: SURRY BANKS 92342727 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92342727001 EB EPA 3010A 363321 EPA 6010 364621 92342727002 FB EPA 3010A 363321 EPA 6010 364621 92342727001 EB EPA 3010A 363478 EPA 6020B 363771 92342727002 FB EPA 3010A 363478 EPA 6020B 363771 92342727001 EB EPA 7470 363459 EPA 7470 363485 92342727002 FB EPA 7470 363459 EPA 7470 363485 92342727001 EB EPA 8260 363328 92342727002 FB EPA 8260 363328 92342727003 TB EPA 8260 363328 92342727001 EB SM 4500-CN-E 363513 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/15/2017 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 28 Document Name: Document Revised: Sept. 21, 2016 a Sample Condition Upon Receipt(5CUR) Page 1 of 2 �acr3Analytical Document No.: Issuing Authority: F-CAR-CS•033-Rev.01 Pace Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville 12, Raleigh❑ Mechanicsville❑ Sample , •� Client Name: Project a WO7T g2342727 ❑ ed Ex UPS USPS ❑Client ❑Courier; Commercial Vace ❑other: 1111111111111111111111 1 92342727 CustodySeal Present? ? Dyes QNo Seals Intact. ❑Yes DNo Date/Initials Person Examining Contents; Packing Material: ❑Bubble Wrap ❑Bubble Bags ❑None` [—]Other: Thermometer: ❑ IR Gun ID: 71 k� Type of Ice: 0wet ❑Blue []None. Samples on ice, cooling rocess has begun Correction Factor: Cooler Temp Corrected (°C): 3, Biological Tissue Frozen? ❑Yes �r N/A Temp should be above fre zing to VC USDA Regulated Soil ( N/A, water sample) Did samples pfiginate in a quarantine Yes ❑✓ No zone within the United States; CA, NY, or SC (check maps)? Did samples originate from a foreign source (inter ationalfy, indudin¢ Hawaii and Puerto Rico)? nYes No Comments/Discrepancy: Chain of Custody Present? L` es ❑No ❑N/A 1. Samples Arrived within Hold Time? Yes LJ No ❑N/A 2, Short Hold Time Analysis (02 hr.)? ❑Yes N ❑N/A 3, Rush Turn Around Time Requested? ❑ye No El NIA 4. Sufficient Volume? Ye / [:]No [—]N/A 5. Correct Containers Used? -Pace Containers Used? �1--5 ❑No ❑No ❑N/A ❑N/A fi. Containers Intact? E34s ❑ qo ❑N/A 7. Samples Field Filtered? EN , f7i/No ❑N/A 8. Note if sediment is visible in the dissolved container Sample Labels Match COC? -Includes Date/Time/ID/Analysis Matrix: E24s ❑No [--]N/A 9. Headspace in VOAVials (>5.6mm)? ❑Y s lD o ❑N/A 10. Trip Blank Present? Trip Blank Custody Seals Present? E0 0 DYes []No ❑No ❑N/A ❑N/A 11. CLIENT NOTIFICATION/RESOLUTION Field Data Required? ❑Yes ❑No Person Contacted: Date/Time: Commen,:/Sample Discrepancy: Project Manager SCURF Review: Date; Project Manager SRF Review: {� Date: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office {i.e. Out of hold, incorrect preservative, out of temp, incorrect containers) Page 26 of 28 Document Name: Document Revised: Sept. 21, 2016 Sample Condition Upon Receipt(SCUR) Page 2 of 2 Document No.: Issuing Authority: aCBAI]aMical F-CAR-CS-033-Rev.01 _ Pace Q�ity Office +O� W 9 342 # *Check mark top half of box if pH and/or dech[orination Project PM: RWC Due Date: 06/16/17 is verified and within the acceptance range for preservation samples. CLIENT: 92-Municipal "Bottom half of box is to list number of bottles u _ z Z] " U z z z z ry Z v Q ? m m a a v Z . N Z 0 ,:I d a a v Q a a N v a O sfY p v u `" x ro m 2 n C O N Q 2 z M O ¢ z z a Y U) a 2 z u �n i c a C N = Z z N O z y C 7 U 2 N = 2 Q Jcc �_ U v7 tNa a c A m = o 4. al z u O N u a V nR u a m a n `6 ro o E E E ¢ E Q o n ¢ O ¢ O ¢ O Q O ; a a n a u J E Ln J E J E a a J J E d O a E O Q Q ` J ¢ J E O J J E J J N J Ln J OLM J oN C J E rq O On N m n u m u •i w m .r m rn m m ai a, a rn N m :C NOEo t7 a a m a t0 ry a c0 P a m en a m a m a m a m ty [7 Q l7 Q C7 d l7 d l7 Q l7 d 0 O U 9 0 ? C7 O O 7 N cn CO u l7 1 t 3 2\NN}/ 3 4 5 6 7 S 9 \\N\ N to 11 12 I J pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot# Page 27 of 28 ,/ �aceAllaryrra� Section A Required Client Information: Due DateiTAT: 10 Section B Required Project Information: Report To: Jonathan Pfol Copy To: Purchase Order No. Ghent Project ID: Surry Blar Container Order Number: 00 N O CHAIN -OF -CUSTODY 1 Analytical Request Document N The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. m Section C I D_ Invoice Information: Page : Of 1 Pace Quote Reference: Pace Project Manages Trey Carter Pace Profile 2 COLLECTED Preservatives } MATRIX CODE 06,kin9Watar 6W w M WateSAMPLE ID vv-i wT waaa watel ww O START END Z o Product P One Character per box. samsaed SL Ia' (A-Z, 0-9 1. -1 on a4 — a4 L7 0 H WP Sample Ids must be unique Air m �j F m F AR Olhar OT G liaj N Timm TS a a 4 N w z m O ° m tY a U a O Z a con DATE TIME TIME N _ z z z 01 EB UVT G /DATE ipl uoo t 3 2 FB WT G 3 TB WT G 4 5 6 7 8 4 10 11 12 N I N State ! Location North Carolina Filtered (YlNi N c U ADDITIONAL COMMENTS R INQUISHED BY ! AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS nc s�s:dA,P i�..,TA kv7m Tsr-p (OIafl e6 �11� PLEB NAME AND SIGNATURE PRINT Name of SAMPLER: SIGNATURE of SAMPLER: n Pfohl DATE Signed: m 0. W a U U In Appendix B Field Sampling Parameter Data Sheet(s) La M M Field Sampling Data Sheet Project: Surry Co Closed C&D and Closed MSWLF-Mt. Airy MYnidVW �I� L'ngincc�ioe Samplers: J. Pfohl Page_1_of 1 Sampling Parameters Water Quality Parameters (Stabilized) Monitoring Point Sample Date Sample Time Depth to Water (BTOP) Static Lab Parameters to be analyzed for Volume Purged (Gal) Sample , Type Goes Dry During Purge Total Depth Measured as expected Total Depth Expected CO2 (mg/1) DO (mg/L) ORP pH Temp. © Specific Cond. (us/cm T-O3 (m9/L) iE ~ CH4 Gas Vapors MW-1 f(+li c> - `` i, r UIC ( r, ;Fr 40- IW-2 t15 �t1.,� s WLR & T - - - ^�'� 1�; ;�,�.1 68.08 - - - - - - - - i tI it MW-3R UIC . r P 100 - 5 ? i f-1t'_ WLR & T - - - 52 - - - - IW-4 j,'] WLR & T - - - 57 IW-5 WLR & T - - - •1C _:r, 64 - - - - - - - MW-6 (j t ( 3',b)) AM_ MW-7 UIC ,^ 25 IW-6a; WLR & T - - - �,� r�= �,_, 56 - - - - - - - ?1 ' t MW-9 1. �° , 1 UIC 46 MW-11 r c=+i Afvl 40,;7 MW-12D 6o AM- r' sT _ MW-12S UIC 51 F�•I i�3 �-�sP�. MW-13 UIC 35.78 - MW-14r+llt; UIC 48.03 I`f,a MW-15 �30UIC. Li Ij� 1: �;1 MW-16 ;,flf :cC 7,�r'� UIC �� .f k: �� i `'36.28 MW-17 17 UIC 15.32 - _ 1 c% MW-18 �ftii Lf_,a UIC. r' 18.15 MW-19b', + ;r UtC d 17.1 MW-20 G I1I k. UIC. 25.64 MW-21 5 31( S;aD tl; UIC 15.41 K,! MW-22 5(31 UIC 'c 6.04 - MW-23 alai. C' la f�� UIC b st`_' _17.1 SCALEHOU E6f j l h _ 222 - 7,6 t 7.- SS B=Stainless Steel Baler. D B=Disoosable Baler. P=Low flow Pump. PD=Puroed Dry VT=Very Turbid, MT=Moderately Turbid, ST=Slightly Turbid, C=Clear NR=No Reading Attempted, NS=No Sample Obtained � - '�" ✓ �ya+71*�l - ,'.i I.+i P, ;u;5.� �j (i % � r ? J� 1' i �' i Field Sampling Data Sheet m `� Project: Surry Co Closed C&D over Closed MSWLF & Active Subtitle D Lined- Mt. Airy (Shared Surface Waters) Samplers: J. Pfohl Page_1_of 1 Sampling Parameters Water Quality Parameters (Stabilized) Monitoring Point Sample Date Sample Time Visual Flow Rate Lab Parameters to be analyzed forPurge Visual Guage Ht.Type Sample Goes Dry During Total Depth Measured as expected Comments O �� (m /L) ORP pH Temp. © Specific Cond. (us/cm TDS (mg/L) � `� � CH4 Gas Vapors (ppm) .I SW—f i ^;� eta-e;F�e ,. :, I i�-o, il)' — `� R r:.'�. `{ € — SW-2 — SW-3 SW-4 it s5 SWN-1a— SWN-2 SWN-3 0i,a— SWN-4 SW —A Downstream MW-2 ! _ SW-B l , _ I Downstream MW-6R # SS B=Stainless Steel Baler, D B=Disposable Baler, P=Low flow Pump, PD=Purged Dry VT=Very Turbid, MT=Moderately Turbid, ST=Slightly Turbid, C=Clear NR=No Reading Attempted, NS=No Sample Obtained