WQ0014543_Regional Office Historical File Pre 2018

♦Y QLVL LxLovLu LiGJ
Environmental Quality
May 9, 2017
Mr. L.F. Hudson, Jr. Director of Water Resources
City of Statesville
P.O. Box 1111
Statesville, North Carolina 28687
Dear Mr. Hudson:
P
ROY COOPER
Governor
MICHAEL S. R(EGAN
S. JAY ZIMMERMAN
Director
Subject: Non -Discharge Permit Inspection
Land Application of Residual - Permit WQ0014543
Iredell County
The Mooresville Regional Office (MRO) conducted a review of Land Application of Residuals
Emergency Permit for the City of Statesville. This permit is due to expire on February 281, 2019. Please
be sure to submit'the application for permit renewal 180 days prior to the expiration of the current permit.
This report should be considered as a compliance inspection for this permit.
I may be reached by phone at [phone] or email [e-mail]., should you have
questions.
Sincerely,
Edward Watson, Hydrogeologist
Mooresville Regional Office
Water Quality Regional Operations Section
Division_ of Water Resources, NCDEQ
Attachment: Inspection Report
CC: Land Application Compliance,. Central Office, Raleigh (via email)
Andy Smith, City of Statesville (via email)
Eric Bruce, Synagro (via email)
State of North Carolina I Environmental Quality I Water Resources I Water Quality Regional Operations
Mooresville Regional Office 1610 East Center Avenue, Suite 3011 Mooresville, North Carolina 29115
704-663-1699

Compliance Inspection Report
Effective: 09/17/13 Expiration:., 02% !8!19. Owner.:.City of Statesville
Effective: Expiration: Facility: City of Statesville Residuals Land Application P
County: Iredell PO Box 1111
Region: Mooresville..
Statesville NC 286871111
Contact Person: Joe Hudson Title: Phone: [phone]
Directions to Facility:
System Classifications: LA,
Primary ORC: Certification:. Phone:
Secondary ORC(s):
On -Site Representative(s):
Related Permits:
NCO031836 City of Statesville - Fourth Creek WWTP
NCO020591 City of Statesville - Third Creek WWTP
Inspection Date: 05/03/2017 Entry Time 10:OOAM Exit Time: 10:15AM
Primary Inspector: Edward Watson Phone:
Secondary Inspector(s):
Reason for Inspection: Routine Inspection Type: Compliance Evaluation
Permit Inspection Type: Land Application of Residual Solids (503)
Facility Status: Compliant . Not Compliant
Question Areas:
Miscellaneous Questions Record Keeping Treatment
Land Application Site Pathogen and Vector Attraction
(See attachment summary)
Page: 1

IsPermit: WQ0014543 Owner - Facility: City of Statesville
pection Date: 05/03/2017 Inspection Type: Compliance Evaluation Reason for Visit: Routine
Inspection Summary:
This permit is .in force -as a back-up, emergency land application permit. No material has ever been applied under this
permit.
Page: 2

a p p-
CO
0 -0
_ _
0 0 0
CD -1 O
CD
a a
v 3
n CD o 0
N w
D O w N
co O CD O
— c N
(D
0 = _
3 a N' N'
w w
w ? O
a
A n n
n
U) cn
cn cn
D
Z
N
3
a
ID
C
m
0
0
0
U)
K
co
N
N
N
0
(i
N
cn
cn
0
v
n m
CD
fn
f v
D 0
� o
CD 3
c
c co
0-
CD m
A
n
O cn
D
Z O
Z
a p�
(a
N
3
❑
❑
❑
❑
❑ O
cn
■
■
■
■ D
CO
❑
El
El
❑
❑ m
0
O
3
(D
D D
0 CD
N v
cn cn
CD CD
0co cn
0
a a
3 w
N p�
II7 0•
CD 7 (D
Cl J
Cl-
Q.
v
7
a
C
0
a
w
(D
•J
D D D 2 D D
D 0
C: CD CD D D
�' m m a Z Z n�
'0 m cn
0 m CD -art r-
0 0 v CCDn CD D -0y a o o cn
0 CD CD w
w cn
'O - 3 Q •J
CD ; 3 m w
v 5• 3 Co
7 CD cnw—.
O 0 7
m 3 a
N J
O N � `<
o'
J O 0 v O
to J (D <
0 a
•J
FA
•J
D cn u, D
cD w m
c>
5
0 CD
CD'< co c01 D
w o D v
c CD `<
0 m
cn Z) ani
n m M w
(D. 0 3 O'
0. (A O _w
w 0 3 O
7 J -0 0
J
n
cn _
w
w
0'
J J
O
O
3 Q.
O
CD
0 CD
in
0'
m
cn
O
O
7
a
C
CD
m
a
(D
c
(D
a
•J
❑
■
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
■
❑
❑
❑
❑
e y
y
■
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
O
O
❑❑❑❑❑❑❑❑❑❑❑❑❑❑❑❑❑�❑❑m
m
� O
N
0
O
7 -n
-I w
� O•
a =
CD
n n
3
a o
w cn
m
< -
w
c
w
o'
X
CD
w
cn
O
7
O
C
N
M
O
C
N

14543 Owner - Facility: City of Statesville
2017 Inspection Type : Compliance Evaluation Reason for Visit: Routine
®. ❑❑4❑
Digester (MCRT) ❑
Compost ❑ .
Class A lime stabilization ❑
f. Volatile Solids CeLlculations ❑ ❑ N ❑
g. Bench -top Aerobic/Anaerobic digestion results ❑ ❑ N ❑
Comment: Material would be land Apllied under Synagro Piedmont Region Permit WQ0016247. The
materials would meet the requirements of a Class "B" Residual material.
Treatment
Check all that apply
Aerobic Digestion
Anaerobic Digestion
Alkaline Pasteurization.(Class A)
Alkaline Stabilization (Class B)
Yes No NA NE
Compost ❑
Drying Beds ❑
Other
Comment: Dewatering and beltpresses are operated at both 3rd and 4th Creek facilities. Processed
material is stored at the 4th Creek facility.
Land Application Site
Is a copy of the permit on -site during application events?
Is the application site in overall good condition?
Is the site free of runoff/ponding?
If present, is the application equipment in good operating condition?
Are buffers being maintained?
Are limiting slopes buffered?
10% for surface application
18% for subsurface application
Are there access restrictions and/or signs?
Is the application site free of odors or vectors? ; .
Have performance requirements for application method been met?.
For injection?
For incorporation?
Does permit require monitoring wells?
Have required MWs been installed?
Are MWs properly located w/ respect to RB and CB?
Yes No NA NE
❑❑■❑
❑❑■❑
❑ ❑ N ❑
❑❑■❑
❑ ❑l ❑ ❑
Page: 4

WQ0014543 Owner - Facility: City of Statesville
spection Date: 05/03/2017 Inspection Type : Compliance Evaluation Reason for Visit: Routine
Are MWs properly constructed (ihcluding screened inteivC`1i)% ❑ 0 MEY
Is the surrounding area served by public water? ❑ ❑ 0 ❑
If Annual Report indicates overapplication of PAN, are wells nearby that may be impacted? ❑ ❑ 0 ❑
Are soil types consistent w/ Soil Scientist report/evaluation? ❑ ❑ ❑ ❑
Is the water table greater than 173' bls. ❑ ❑ 0 ❑
Is application occurring at the time of the inspection? ❑ ❑ M ❑
Comment: No material as ever been applied under this permit. The City of Statesville keeps this permit
active for emergency use only.
Page: 5

Compliance Inspection Report
rerma: vv�w 1- u: o Effective: 09/17/13 Expiration: 02/28/19 Owner : City of Statesville
SOC: Effective: Expiration: Facility: City of Statesville Residuals Land Application Progra
County: Iredell PO Box 1111
Region: Mooresville
Statesville NC 286871111
Contact Person: Joe Hudson Title: Phone: [phone]
Directions to Facility:
System Classifications: LA.
Primary ORC:
Secondary ORC(s):
On -Site Representative(s):
Certification: Phone:
Related Permits:
NC0031836 City of Statesville - Fourth Creek WWTP
NC0020591 City of Statesville - Third Creek WWTP
Inspection Date: 03/07/2017 Entry Time: 04:OOPM
Primary Inspector: Edward Watson
Secondary Inspector(s):
Reason for Inspection: Routine
Permit Inspection Type: Land Application of Residual Solids (503)
Facility Status: Compliant ❑ Not Compliant
Question Areas:
Miscellaneous Questions Record Keeping
(See attachment summary)
Exit Time: 05:OOPM
Phone:
Inspection Type: Annual Report Review
Page: 1

Permit: WQ0014543 Owner - Facility: City of Statesville
Inspection Date: 03/07/2017 Inspection Type: Annual Report Review Reason for Visit: Routine
Inspection Summary:
No land application occurred under this permit for 2016. This permit is in place as an "emergency" land application permit
for class B residuals only. The City of Statesville does not utilize this permit. The permit is kept active in the event it may
be needed for some future time.
Page: 2

9
■
❑ IUD)
2
N
O
Z
D
Z
W
m
n =
O N
3 w
3
C
� w
0'
o
0
� Ci
O.
M n
C
(D O.
G (p
m
m
O vw
O
zy
CDn�
X
CD
O O
1. M.
C3) O
D o
7
C j
w o_
O
J
D D
m m
= :T
w w
C C
7 7
(n (n
n n
0 0
a o.
(n N
3 w
w w
w
7
N Q
CD
CD (p
OJ
.
w
a
0
a
w
CD
�J
D D D 2 D D
m m m N m m
D 5 s
m m D D D
m. a m o_ Z Z Q w
7 w O- O'
chi = = a ww m Co n
-oo 0 0D
0 0 0. Cn w w
Na D Q _�
O (D w N
C O O >
w C 7 0_ cn
p� �' w N
(D3 N W a J
w CD COCc,)
CD
w N O cD N
3 0- �
0 0'
J 7 > w y
(n •J (D G
� ' O_ (n
•D J
•J
D y D
c 0
� m
m l< co (o
D o D w
3 c m <
m q --L G)
°i ' m =-� 5
w 2 w
d CDO w
_� 7
fD 7 0 O'
.O+ C6 O d
w m 3 o
N J (=n
N J
N (D
w o
w m
Q �
(D
•J •J
� 0
3 M
O
o �
Q
CD
co
0
O.
O
0
o.
M
c
co
D_
•J
❑ DEEDED ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑CD
N
❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ Z
1
v
O O
� m
0
7 T
i m
O.
D C)
D <
� o
w
m m
v
O CD
N
(D (p
(D
io
d
w
O
7
O
N
0
O
N

Governor
NCDENR
North Carolina Department of Environment and Natural o Y` S.
f it
day n der Vaart
retary
June 12, 2015
Mr. L.F. Hudson, Jr.; Director of Water Resources
City of Statesville
P.O. Box 1111
Statesville, North Carolina 28687
Mr. Marshall Puryear, Manager (Electronic mail)
Synagro Central, LLC
284 Boger Road
Mocksville, NC 27028
Subject: Non -Discharge Permit Inspections
City of'Slatesville�
Distribution of Residuals — Permit No.: WQ0006245
Land Application of Residuals—rPermit-No::'1NQ0014543;,
Iredell County
and Synagro Western Regional
Land Application of Residuals — Permit No.:WQ0016247
Alexander County
Dear Mr. Hudson and Mr. Puryear:
The Mooresville Regional Office (MRO) conducted a compliance inspection on May 27U', 2015,
which included a land application event of Third Creek residuals under the SYNAGRO Permit; and,
a records review and the residuals processing and storage at the Fourth Creek WWTP.. The MRO
would like to thank Eric Thompson (Synagro) and Andy Smith (Statesville) for their time during the
inspections.
Permit expiration dates are listed below for your convenience.
W00004040 Third Creek Monofill, expires 12/30/2018
The monofill units were not inspected at this time.
W00006245 Statesville Class A — Lime Stabilized, expires 09/30/2020
Log entries for the lime stabilization analyses and cross referenced records for the pH
meter calibration appeared well organized and improved since the previous inspection.
WQ0014543 Statesville Class B - Emergency Land Application, expires 02/28/2019
There is currently no activity under this permit.
WQ0016247 SYNAGRO Class B - Land Application, expires 02/28/2018
This permit is held by SYNAGRO, but they rely on Statesville to collect and analyze for all
required parameters including Pathogen and Vector Attraction Reduction (PVAR), which
Mooresville Regional Office
610 East Center Avenue, Suite 301, Mooresville, North Carolina 28155
Phone: [phone] I Fax: [phone] / Customer Service 1-877-623-6748
Internet: www.ncdenr.gov
An Fnual nnnnrhmily 1 Affirmnfiva Anfinn Fmnlnvar— MadR in mart by rarrnlwl nanar

also apply to Statesville's Class B permit #WQ0014543, were it being utilized for land
ition.
��nversation with Andy Smith, the City of Statesville has increased the. residuals
"SOUR" testing to once/month to help address odor and vector concerns noted in a
previous inspection and to ensure VAR is met, particularly with the Third Creek residuals,
which typically have more odors than the Fourth Creek residuals. The once/month
sampling.exceeds the permit requirement; therefore, the City of Statesville may reduce
sampling frequency back to once/quarter at their discretion.
The attached report should be self-explanatory; however, should you have questions please
contact me by phone [phone]) or email (maria.schutte(D-ncdenr.gov).
Sincerely,
—+ Vfr
Maria Schutte, Environmental Specialist
Mooresville Regional Office
Water Quality Regional Operations Section
Division of Water Resources, NCDENR
Attachment: Inspection Report June 2015
CC: . Mr. Andy Smith, Town of Statesville (email)
Mr. Eric Thompson, SYNAGRO (email)

PVState of North Carolina
""'.Department -of Environment
and Natural Resources
Division of Water Resources
Pat McCrory, Governor
Donald van der Vaart, Secretary
NCDENR
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
City/Town/Owner: Statesville County: Iredell
Permit No.: WQ0006245 Class A Lime Issued: 04/02/2015 Expiration: 09/30/2020
Permit No.: WQ0014543 Class B emer eM Issued: 09/17/2013 Expiration: 02/28/2019
Permit No.: W00016247 SYNAGRO Land Application Issued: 03/27/2009 Expiration: 02/28/2018
Permittee Contact: Andy Smith (4d' Creek WWTP ORC) Telephone No.: 704-878-3438
LA ORC: Marshall R. Piggear SYNAGRO LA #994465 Telephone No.: 434-738-8002
LA BUORC: Froncy M. Dail (SYNAGRO) LA #13197 Telephone No.: 910-443-7696
Reason for Inspection
X ROUTINE COMPLAINT FOLLOW-UP OTHER
Type of inspection
Collection System Spray Irrigation X Sludge Other
Inspection Date(s): May 27, 2015
Inspection ,Summary: (additional comments may be included on attached pages)
This inspection included an active land application (LA), of Third Creek residuals at field NC-IR-20-03,
under the Synagro — WQ0016247 permit; and, a review of records and residuals storage at Statesville's
Fourth Creek WWTP, for both of their permits referenced above. The 4th creek plant was undergoing
construction for repairs at the lime processing and storage areas, at the time of this visit. Statesville
maintains separate bay areas for the "class A" residuals storage and distribution, and the 3rd creek and 4t`
creek "class B" residuals handled by SYNAGRO.
® Strong odors were noticed in the Class B residuals at the field LA site; however, vectors
(flies) were minimal. Statesville has increased sampling frequency for SOUR testing to
ensure VAR is met. The once/month testing is at the discretion of the City of Statesville and
may be reduced to the permit requirement of once/quarter at anytime.
® Please contact maria.schutte(a,ncdenr.gov with any corrections to the contact information
noted above.
Is a follow up inspection necessary _yes X no
Inspector(s): Maria Schulte - Environmental Specialist
Telephone No.: 704-663-1699 Fax No.: 704-663-6040
Date of Inspection: May 27�', 2015

pg. 2
WQ0014543 Statesville & WQ0016247 Synagro
idual
7 and WQ0014543
Tlication- (class B)
Y -yes iN-no NE -not evaluated
Record Keeping (class B)
WQ0006245
X Distribution and Marketing (class A)
NA -not applicable
Y Copy of current permit
Y 'Current metals and nutrient analysis
Y TCLP analysis
*Y SSFA (Standard Soil Fertility Analysis)
*Y Nutrient and metals loading calculations
*Y - Hauling records
*Y Field loading records
*Y Field site maps and information
NE Records of lime purchased
Y Pathogen & Vector Attraction Reduction
Record Keeping (class A)
Y Copy of current permit
Y Current metals and nutrient analysis
Y TCLP analysis
NA SSFA (Standard Soil Fertility Analysis)
NA Nutrient and metals loading calculations
Y Hauling records
NA Field loading records
NA Field site maps and information
Y Records of lime purchased
• Pathogen & Vector Attraction Reduction
* Comments: Most data was reviewed as part of 2014 Annual Report. The only fleld maps reviewed were
for the land application sites visited.
Pathogen & Vector Attraction Reduction Records
Fecal coliform
X SM 9221 E (Class A or B)
SM 9222 D (Class B only)
Salmonella (Class A, all tests must be < 3MPN / 4 grams dry)
Class A lime stabilization X
SOUR X
pH records for lime stabilization (Class A or B) x
Comments: The records were well organized. It was noted that the pH time and temp logs for the Class A
product and cross referencing to the pH calibration logbook appeared complete and improved over last
year.
Treatment
X Aerobic digestion anaerobic digestion
X Alkaline Stabilization Lime other -describe:
Transport
Spill control plan in transport vehicle? Y
Does transport vehicle appear to be maintained? Y
Stogie The 4th Creek residuals storage was only viewed from a plant vehicle due to construction activity.
Number of days/weeks/months of storage: Approxi�
Describe storage: Cake residuals are stored at the 4`
A, 3rd Creek Class B and 4`h Creek Class B residuah
Odors present NE Vectors present NE
the Cl

pg. 3
14543 Statesville & WQ0016247 Synagro
Sampling and analyses are handled by the City of Statesville.
;? NE Is sampling representative? Y, if the O&M plan is followed
Field Sites (end use for class B biosolids): NC-IR-20-03. This portion of the inspection is the
responsibility ofSYNAGRO under their permit #WQ0016247
Y Permit on site during application Y Spill plan on site
Y Buffers adequate. Y Cover crop specified in permit
N Documented exceedances of PAN limits Y Site condition adequate
N Signs of runoff / ponding (if no, improvements recommended)
Y Rain Gauge on site during application
Are there any limiting slopes on fields?
Y 10 % for surface application N 18% for subsurface application
Comments: There were odors but minimal vectors detected at the land application site. The odors are
hLg,h1jghted in this report just to remind all permittees of the potential for complaints & nuisance conditions
Adjacent fields had been flagged for application. Per conversation with Eric Thompson the existing maps
were obsolete due to setback changes. The buffers he flagged appeared adequate at the time of this
inspection.
Monitoring wells) Y/N: N
If yes, location of well(s): These permits currently do not require groundwater monitoring.
Odors/vectors
Describe any nuisance conditions. and any corrective actions needed. There were odors and minimal
vectors present at the LA site. The Fourth Creek residuals storage area was only viewed via drive -by in a
plant truck due to construction activity.
Odors present Y
Vectors present minimal
Other noted conditions:

tl
mwf SMAb= EaiE& i rr,&bi :k €LIfWg=GIOWl a �i-i � fi�� � 427Statesvi'l
g-"i C'L5 � ? C Lcr-SS
o �� l
., Directions to 232 Pum� Statt)on R, NC 2862�
30.2 mi — about 46 mins
Park
-13
��j".�r , �`�x xb�� �•
IR
StatesviRe
T
aw -x
70
:j
t
W
5 mf,
m
a
fr1 t��i o13 Google
5 -eelC>igQi ga la -eel AYQC ,l AL61 QD§-W&SMHH EiA[�H i I FU ggEtei g8R' C4}-QWQM-PE NP

U
NLArP rr,@Li 97*' -66
610 E Center Ave, Mooresville, NC 28115
.....................................................................................................................................................................................................__.........._..
1. Head west on E Center Ave toward E Statesville Ave
_........_... ............... _.... ........
go 0.6 mi
About 1 min
total 0.6 mi
2. Turn left onto S Main St
go 397 ft
total 0.7 mi
3. Take the 1st right onto W McLelland Ave
go 1.0 mi
About 2 mins
total 1.6 mi
4. Turn left onto E Plaza Dr
go 0.4 m
1
About 2 mins
total 2.1 mi
5. Keep left at the fork
go 1.3 mi
About 2 mins
total 3.4 mi
6. Turn right to merge onto 1-77 N
go 12.4 m
About 11 mins
total 15.8 mi
7. Take exit 49A for Garner Bagnal Boulevard/US-70
go 0.3 mi
total 16.1 mi
70
8. Turn right onto US-70 E/Garner Bagnal Blvd
go 1.5 mi
Continue to follow US-70 E
total 17.6 mi
About 2 mins
9. Turn right onto 3rd Creek Rd
go 1.3 mi
=i b., or the right"
total 18.8 mi
About 3 mins
Total: 18.8 mi - about 25 mins
444 3rd Creek Rd, Statesville, NC 28677
total 0.0 mi
10. Head north on 3rd Creek Rd toward Magnolia Hill Ln
go 1.3 mi
About 3 mins
total 1.3 mi
70
11. Turn right onto US-70 E/Salisbury Hwy
go 1.4 mi
About 2 mins
total 2.7 mi
12. Turret left onto Salisbury Hwy
go 0.2 mi
About 1 min
total 2.9 mi
13. Take the 1st left onto Bell Farm Rd
go 1.9 mi
A nat=c, r .§ ,i be the r:gn'i.
total 4.7 mi
About 4 mins
Total: 4.7 mi - about 10 mins
629 Bell Farm Rd, Statesville, NC 28625
total 0.0 mi
14. Head north on Bell Farm Rd toward Farmwood Dr go 2.1 mi
About 4 mins total 2.1 mi
64 15. Turn left onto US-64 W/Mocksville Hwy go 1.9 mi
About 3 mins total 4.0 mi
a 16. Take the ramp onto 1-40 W go 2.0 mi
About 2 mins total 6.1 mi
17. Take exit 151 for US-21 N toward Harmony goo. 1 mi
total 6.2 mi
a -eerC � b2�a la -ee\ f�EQ e�i e4EZe� QCe-QQa�SNA bH Ea(F� I i �hJ gr,6�e1�10FF CC,-QWQM-P!E ap

"
`
muu� sm4b�- E�gnL&^/01 vqd�bmO*' *Uwe; *U'oWIu&P+kA=E) 9:p+nE�O98:k' *oaCF4dnnnEtl -66
. ^ 18. Turn right onto0��21 0/Sm0U�/en Rd ' ' '' � � ' ' ' go 0.4 nni
c�/ Continue tofollow UG-21N total 6.6mi
- About min
' .
419� 19. Turn left onto Pump Station Rd gn4Sft
W OemUnWionvviU beon thehQht tota|S.6 mi
About 47secs
1 232 Pump Station Rd, Statesville, NC 28625
These directions are for planning purposes only. You may find that construction projects, traffic, weather, or other events may cause
conditions to differfromthe map results, and you should plan your route accordingly. You must obey all signs or notices regarding your route.
Nlapdata @2U13Guog|o
Directions weren't right? Rease find your route on maps.google.com and click "Report a problem" at the bottom left.
5-e6OvCmbvm[A-66\FZVD�9/oL61QG�-VWamm`*F�Ax�Tf/$M »qff�smOm'nV'QX000+PE pip

Administration
Page 1 of 1
Official Website of the City of Statesville, North Carolina
Y
Airport
City Manager & City Clerk
Civic Center
Economic Development
Electric Utilities
Finance
Fire Department
Human Resources
Planning & Zoning
Police Department
Public Works
Recreation & Parks
SIGI - Gang Initiative
Water Resources
Administration
Drought Update
Permitting Process
Public Notices & Reports
Rainfall Reports
Rate Schedule
Sta-Lime
Treatment Capacities
Water Source
Frequently Asked Questions
All Forms and Documents
Photo Gallery
Departments < Water Resources < Administration
Administration
Administrative Offices
Fourth Creek Wastewater Treatment Plant
693 Bell Farm Road
Statesville, NC 28625
Phone: [phone]
Fax:[phone]
Third Creels Wastewater Treatment Plant
444 Third Creek Road
Statesville, NC 28677
Phone:[phone]
Fax:[phone]
Water Treatment Plant
232 Pump Station Road
Statesville, NC 28677
Phone:[phone]
Fax:[phone]
Site Map I Forms & Documents I Contact Us
Government I Departments I Calendar
Statesville provides continuous, 24-hour per day, water and sewer service. There is
always a certified operator on duty at each plant as required by the state. This
ensures that the city's water supply and the water returned to nearby streams are
of the best quality possible. Operators are certified through the N.C. Division of
Environmental Management.
Statesville actively promotes beneficial reuse of water and wastewater treatment
byproducts. Water and wastewater processes produce sludge as a byproduct of
treatment. Statesville dewaters the sludge and blends it with lime and a drying
agent to produce an alkaline stabilized product, called Sta-Lime. Sta-Lime is
distributed locally to farmers as a liming agent.
GO
Joe Hudson,
Director
704-878-3438
email Joe
Jerry Byerly,
Assistant Director
704-878-3438
email Jerry
Brandy Johnson,
Pretreatment
704-878-3438
emaii Brandy
Scott Austin, Third
Creek Wastewater
Treatment
704-872-9621
email Scott
Andy Smith, Fourth
Creek Wastewater
. Treatment
704-878-3438
email Andy
Weston Johnson,
Water Treatment
704-878-3441
e-mail Weston.
Resident I visitor I Business j Government I Departments i Contact Us I Calendar ( Forms & Documents I Site Map
Home
MAILING ADDRESS: PO BOX 1111, Statesville, NC 28687-1111 1 PHYSICAL ADDRESS: 301 S. Center Street
704.878.3683 PHONE [phone] FAX
SITE DESIGNED BY: Granite Sky Design i SITE PROGRAMMED BY: Customer Connect
http://www.ci.statesville.nc.us/DepartmentslWaterResourceslAdministration/tabid1243IDefault.aspx 1/8/2013

To see all the details that are visible on the
screen, use the "Print" link next to the map.
a -&eOq. O�bka la -ee\ N CbWAMA i]a 94Bpa M;eZSVPH E�*t-& Fbq-Qti-iEei ibFk' K1sm 5 ZtC&2r gcJXO§ZC(hE-WMLE ND

5,� k
tt j
- E
v ! t ;
r 1^�
azi'

`� Pik < " � m - f°°. �.V � P•,c
,a r
e
TRWtf'
e
.x
;w 5s it
4y,S7
_ r
cs,
�3s l a J
- �. Via' • ,. • - k... ,�,. ° � ,
�a`

�. C-
�-P '

Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By,
Analysis Date/Time:
Analyzed By,
Sample Volume;
Beginning Temperature;
End Temperature;
Time Dissolved Oxygen Level
(minutes) m /I)
0
6.55
1
6.53
2
6.86
3
6.97
4
6.91
5
6.7
6
6.77
7
6.73
8
6.65
9
6.55
10
%
6.47
11
6.46
12
6.33
13
6.31
14
6.25
15
6.27
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
4/11/2012
16.6
4/11/12 9:34 AM
RG
4/11/12 9:44 AM
BJ
300
n15.715.9
milliliters
legrees Celsius
legrees Celsius
2.18 mg Oxygen/hr
0.50 mg Oxygen/g/hr
16 degrees Celsius
1.31079601
Temperature Corrected Specific Oxygen Uptake Rate:1 0.65 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Fourth Creek
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time-
Sampled By:
Analysis Date/Time:
Analyzed By:
Samole Volume:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
illiliters
Celsius
Celsius
mg Oxygen/hr
mg Oxygen/g/hr
degrees Celsius
Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically..

• ��� NI AT �9Q Michael F. Easley
�O G Governor
r William G. Ross, Jr.,Secretary
>_ North Carolina Department of Environment and Natural Resources
Kerr T. Stevens, Director
Division of Water Quality
July 10, 2001
Mr. L.F. Hudson, Jr. Director
Water Resources
City of Statesville
PO Box 1111
Statesville, NC 28687
Subject: Non -Discharge Permit Inspection
City of Statesville
Permit Nos. WQ0006245 & kW4=ODt1-4543)
Iredell County
Dear Mr. Hudson:
Enclosed are two non -discharge facility inspection reports for the inspections of the class A
lime facility and the residuals land application (emergency) facility conducted on June 28, 2001 by
Ms. Ellen Huffman with this Office.
Both reports indicate compliance, including proper lab data and record keeping. There has
been no land application activity reported since the permit was issued in 1998. The inspection for
permit #WQ0006245 revealed that the City plans to replace the overhead conveyor from the de -
watering facility to the lime mixer/reactor with an auger type conveyor to correct the clogging and
spillage problem.
The City of Statesville is also listed as a source of sludge for a land application permit issued
to SYNAGRO (permit #WQ0016247). This arrangement could cause the City problems with its land
application program should the City's current land application contract be discontinued with
SYNAGRO. Permit WQ 0016247 reflects only 29.4 acres of land available for land application.
There is also the issue with compliance, as SYNAGRO has no treatment control over the sludge that
the City produces. The Mooresville Regional Office plans to recommend that this permit be issued to
the generator (the City) or combined with the City's existing (emergency) land application permit
(WQ0014543) when it is up for renewal.
The inspection report should be self-explanatory; however, if you have any questions, please
contact Mrs. Huffinan-or me at [phone].
Sincerely,
D. Rex GZeason, P.E.
Water Quality Regional Supervisor
Attachment
ANA cc: Non -Discharge Compliance/Enforcement Unit
Customer Service Mooresville Regional Office PHONE [phone]
1 800 623-7748 919 North Main Street, Mooresville, NC 28115 FAX [phone]

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Wayne McDevitt, Secretary
Kerr T. Stevens, Director
NCDENR
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
City/Town/Owner City of Statesville
Permit No. W00014543
Issuance Date February 16, 1998
If applicable SOC Issuance Date n/a
Permittee Contact Mr. L.F. Hudson
ORC Name Judy Wilcox
24hr Contact Name
Reason for Inspection
County Iredell
Class B emergency land application
Expiration Date January 31, 2003
Expiration Date n/a
Telephone No. 704/878-3438
Telephone No. 704/878-3438
Telephone No. 704/878-3438
X ROUTINE COMPLAINT FOLLOW-UP OTHER
_Type of inspection
Collection System Spray Irrigation X Sludge Other
Inspection Summary: (additional comments may be included on attached pates)
The City of Statesville uses the subject facility as an emergency alternative. This facility has not
been used since the permit was issued in 1998. The City has a Marketing and Distribution Permit
(class A lime stabilization WQ0006245) that is the City's main end use option for the sludge
produced at the Third Creek and Fourth Creek WWTPs. The City also has a contract with
SYNAGRO, formerly Wheelabrator/ Bio Gro (Permit WQ.0016247) for class `B" land
application from the Third and Fourth Creek WWTPs. Records reflect compliance with the City's
Permit. There is no sludge storage at the Third Creek plant. Sludge is de -watered at the plant and
stored at the Fourth Creek WWTP.
Is a follow-up inspection necessary _yes X no
Inspector(s) Name(s)/Title(s) Ellen B. Huffman /Environmental Technician V
Telephone No. 704/663-1699 Fax No. 704/663-6040
Date of Inspection 06-28-01

Residuals Inspection
City of Statesville WQ0014543 (emergency land application)
Type of Residual
X Land Application (class B) Distribution and Marketing (class A)
Record Keeping
Y/N
Y Copy of current permit available at residual generating site
pg 1
Y Current metals and nutrient analysis (see permit for frequency)
Y TCLP analysis N/A SSFA (Standard Soil Fertility Analysis)
Y Nutrient and metals loading calculations (to determine most limiting parameter) YTD!
N/A Hauling records- # gal/tons hauled during calendar year to date
N/A Field loading records X Field site maps and information
N/A Records of lime purchased
Y Pathogen & Vector Attraction Reduction
Comments: No land application activity
Pathogen & Vector Attraction Reduction records (check which methods apply)
Fecal coliform
X SM 9221 E (Class A or B)
(Class A, all test must be <1000 MPN / dry gram)
(Class B, Geo. mean of 7 samples/monitoring period - <2.0* 106 CFU / dry gram)
SM 9222 D (Class B only)
(Geo. mean of 7 samples/monitoring period for Class B <2.0* 106 CFU / dry gram)
Salmonella (Class A, all tests must be < 3MPN / 4 grams dry )
Time / Temp records n/a
Digester (MCRT) Compost Class A lime stabilization
Volatile Solids Calculations SOUR X
Bench -top aerobic/anaerobic digestion results
pH records for lime stabilization ( Class A or B )
Treatment (check treatment type(s) used)
X Aerobic digestion Autothermal Thermophilic Aerobic Digestion (ATAD)
Anaerobic digestion Drying beds (may not meet 503's)
Alkaline Stabilization Lime other

Residuals Inspection
City of Statesville WQ0014543 (emergency land application)
Compost (check treatment type used) N/A '
Windrow Aerated Static Pile In vessel Other
Transport No land application activity
Permit in transport vehicle? Spill control plan in transport vehicle?
Does transport vehicle appear to be maintained?
Operation & Maintenance records No land application activity
Condition of land application equipment on site
Res. pg 2
Storage
Number of months storage- 3
Describe storage: The covered cement pad at the 4`h Creek WWTP has four bays with push walls on
three sides. De -watered sludsze from the 3`d Creek WWTP is stored at the 0 Creek plant in a
designated covered bay. There is gporoximately 2 acres of paved uncovered storage next to the
storage bay area. The entire storage area has stormwater collection. Stormwater is returned to the
head of the plant.
Lagoon N/A Concrete storage pads
Above ground tank N/A In ground tank N/A
Aerated Mixed Aerated Mixed
X* Drying beds *Drying beds are not used
Sampling No land application activity
Describe Sampling — The contractor samples prior to land application.
Is sampling adequate Is sampling representative
Field Sites (end use for class B biosolids)
No land application activity
Permit on site during application Spill plan on site
Buffers adequate Cover crop specified in permit
Documented exceedances of PAN limits Site condition adequate
Signs of runoff / ponding (if no, improvements recommended)
Rain Gauge on site during application
Are there any limiting slopes on fields? Y/N N
10 % for surface application 18% for subsurface application)

Residuals Inspection Res. pg 3
City of Statesville WQ0014543 (emergency land application)
Monitoring well(s) in permit: N/A
If yes, Location of well(s)
Odors/vectors
Odors present Vectors present
Describe any nuisance Conditions and any corrective actions needed

7:."W2
A
.
NCEDEN
JAMES B. HUNT JR.
GOVERNOR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
MOORESVILLE REGIONAL OFFICE
Division of Water Quality
December 28, 1999
BILL HOLMAN
SECRETARY P.4r. L.F. Hudscn, Jr. Dlrectcr
Water Resources
City of Statesville
PO Box 1111
Statesville, NC 28687
Subject: Class B Land Application Inspection
City of Statesville
Permit No. WQ0014543
Iredell County
Dear Mr. Hudson:
Enclosed is the Class B permit inspection report that was conducted on
December 16, 1999 by Mrs. Ellen Huffman with this Office. This inspection is part of
our initiative to inspect all non -discharge programs during each calendar year. _
The report indicates full compliance including lab data, record keeping, and field
conditions. You and your staff should be commended for their dedication in keeping this
program in compliance with all permit requirements.
The report of inspection should be self-explanatory; however, if you have any
questions, please contact Mrs. Huffman or me at [phone].
Sincerely,
D. Rex Gleason, P.E.
Water Quality Regional Supervisor
Attachment
cc: Non -Discharge Compliance/Enforcement Unit
Ms. Judy Wilcox, Residuals Manager "
h:statesvilleI299.doc 3
919 NORTH MAIN STREET, MOORESVILLE, NORTH CAROLINA 281 15
PHONE [phone] FAX [phone]
AN EQUAL OPPORTUNITY / AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/10io POST -CONSUMER PAPER

r
State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Wayne McDevitt, Secretary
Kerr T. Stevens, Director
01?OW'A
NCDENR
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
City/Town/Owner Cily of Statesville
Permit No. W00014543
Issuance Date February 16, 1998
If applicable SOC Issuance Date n/a
Permittee Contact Mr. L.F. Hudson
ORC Name Judy Wilcox
24hr Contact Name
Reason for Inspection
County Iredell
Class B biosolids for land application
Expiration Date JanuM 31, 2003
Expiration Date n/a
Telephone No. 704/878-3438
Telephone No. 704/878-3438
Telephone No. 704/878-3438
X ROUTINE COMPLAINT FOLLOW-UP OTHER
Tvpe of inspection
Collection System Spray Irrigation X Sludge Other
Inspection Summary: (additional comments may be included on attached pages)
The City of Statesville holds this land application permit as an alternative (emergency) option for
sludge end use. This permit has not been used during the 1999 annual reporting period. The City
has a class "A" (lime stabilization) permit (WQ0006245) which is their main end use option for
the sludges produced at Third and Fourth Creek WWTPs. Statesville has also used Wheelabrator
BioGro (permit WQ0016247) for class `B" product from the Third and Fourth Creek WWTPs
during 1999. Both Third and Fourth Creek sludges reflect compliance with current permit.
Is a follow-up inspection necessary _des X no
Inspector(s) Name(s)/Title(s) Ellen B. Huf1mgjj `
Telephone No. 704/663-1699 Fax No. 704/663-6
Date of Inspection 12-16-99

P
Residuals Inspection Check List
City of Statesville WQ0014543
Type of Residual
X Land Application (class B)
Record Keeping
Y/N
Distribution and Marketing (class A)
pg 1
Y Copy of current permit available at residual generating site
Y Current metals and nutrient analysis (see permit for frequency)
* TCLP analysis SSFA (Standard Soil Fertility Analysis)
Y Nutrient and metals loading calculations (to determine most limiting parameter) YTD!
n/a Hauling records- # gal/tons hauled during calendar year to date
n/a Field loading records X Field site maps and information
n/a Records of lime purchased
Y Pathogen & Vector Attraction Reduction
Comments *TCLP samples have been taken Results have not been received from the lab. No
land application performed during 1999 annual reporting_ period Sour testing shows compliance.
Pathogen & Vector Attraction Reduction records (check which methods apply)
Fecal coliform
X SM 9221 E (Class A or B)
(Class A, all test must be <1000 MPN / dry gram)
(Class B, Geo. mean of 7 samples/monitoring period - <2.0* 106 CFU / dry gram)
SM 9222 D (Class B only)
(Geo. mean of 7 samples/monitoring period for Class B <2.0* 106 CFU / dry gram)
Salmonella (Class A, all tests must be < 3MPN / 4 grams dry )
Time / Temp records n/a
Digester (MCRT) Compost Class A lime stabilization
Volatile Solids Calculations X SOUR .
Bench -top aerobic/anaerobic digestion results
pH records for lime stabilization ( Class A or B )
Treatment (check treatment type(s) used)
X Aerobic digestion Autothermal Thermophilic Aerobic Digestion (ATAD)
Anaerobic digestion Drying beds (may not meet 503's)
Alkaline Stabilization Lime other
Compost (check treatment type used) n/a
Windrow Aerated Static Pile In vessel Other

r
Residuals Inspection Res. pg 2
City of Statesville WQ0014543
Transport n/a
Permit in transport vehicle? Spill control plan in transport vehicle?
Does transport vehicle appear to be maintained?
Operation & Maintenance records n/a
Calibration records of land application equipment
Condition of land application equipment on site —
Storage
Number of months storage- 3
describe storage -3 acre paved with runoff collection partially covered area with pushwalls.
(if more than 2 yrs, does facility have Surface Disposal Permit?)
Spill control plan on storage site?
N/a Lagoon - Is lagoon lined_
Above ground tank n/a
Aerated Mixed
X* Drying beds
*Drying beds are not used
Concrete storage pads
In ground tank n/a
Aerated Mixed
Sampling
Describe Sampling — Sampling is performed by the contractor prior to land application. Sampling
is performed according to EPA 40 CFR part 503 guidelines.
Is sampling adequate Y Is sampling representative Y
Field Sites (end use for class B biosolids) n/a
Permit on site during application
Buffers adequate
Documented exceedances of PAN limits
Signs of runoff / ponding
Rain Gauge on site during application
Comments
Spill plan on site
Cover crop specified in permit
Site condition adequate
(if no, improvements recommended)

Residuals Inspection Res. pg 3
City of Statesville WQ0014543
Are there any limiting slopes on fields? Y/N X
10 % for surface application 18% for subsurface application)
Monitoring well(s) in permit: n/a
If yes, Location of well(s)
Odors/vectors
Odors present no Vectors present no
Describe any nuisance Conditions and any corrective actions needed

JAMES B. HUNT JR.
GOVERNOR
d
FORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATuRAL RESOURCES
MOORESVILLE REGIONAL OFFICE
Division of Water Quality
December 28, 1999
BILL HOLMAN
SECRETARY Mr. L.F. Hudson, Jr. Director
Water Resources
City of Statesville
PO Box 1111
Statesville, NC 28687
Subject: Class B Land Application Inspection
City of Statesville
Permit No. WQ0014543
Iredell County
Dear Mr. Hudson:
Enclosed is the Class B permit inspection report that was conducted on
December 16, 1999 by Mrs. Ellen Huffinan with this Office. This inspection is part of
our initiative to inspect all non -discharge programs during each calendar year.
The report indicates full compliance including lab data, record keeping, and field
conditions. You and your staff should be commended for their dedication in keeping this
program in compliance with all permit requirements.
The report of inspection should be self-explanatory; however, if you have any
questions, please contact Mrs. Huffman or me at [phone].
Sincerely,
D. Rex Gleason, P.E.
Water Quality Regional Supervisor
Attachment
cc: Non -Discharge Compliance/Enforcement Unit
Ms. Judy Wilcox, Residuals Manager
AIR,-�r
h:statesville1299.doc
919 NORTH MAIN STREET, MOORESVILLE, NORTH CAROLINA 281 15
PHONE [phone] FAX [phone]
AN EQUAL OPPORTUNITY / AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/10% POST -CONSUMER PAPER

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Wayne McDevitt, Secretary
Kerr T., Stevens, Director
NCDENR
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
City/Town/Owner City of Statesville
Permit No. W00014543
Issuance Date February 16, 1998
If applicable SOC Issuance Date n/a
Permittee Contact Mr. L.F. Hudson
ORC Name Judy Wilcox
24hr Contact Name
Reason for Inspection
County Iredell
Class B biosolids for land application
Expiration Date January 31, 2003
Expiration Date n/a
Telephone No. 704/878-3438
Telephone No. 704/878-3438
Telephone No. 704/878-3438
X ROUTINE COMPLAINT FOLLOW-UP OTHER,
Type of inspection
Collection System Spray Irrigation X Sludge Other
Inspection Summary: (additional comments may be included on attached pages)
The City of Statesville holds this land application permit as an alternative (emergency) option for
sludge end use. This permit has not been used during the 1999 annual reporting period. The City
has a class "A" (lime stabilization) permit (WQ0006245) which is their main end use option for
the sludges produced at Third and Fourth Creek WWTPs. Statesville has also used Wheelabrator
BioGro (permit WQ0016247) for class `B" product from the Third and Fourth Creek WWTPs
during 1999. Both Third and Fourth Creek sludges reflect compliance with current permit.
Is a follow-up inspection necessary _yes X no
Inspector(s) Name(s)/Title(s) Ellen B. Huffma GEnvironmental T
Telephone No. 704/663-1699 Fax No. 704/ 63-6040
Date of Inspection 12-16-99

Residuals Inspection Check List
City of Statesville WQ0014543
Type of Residual
X Land Application (class B)
Record Keeping
Y/N
Distribution and Marketing (class A)
pg 1
Y Copy of current permit available at residual generating site
Y Current metals and nutrient analysis (see permit for frequency)
* TCLP analysis SSFA (Standard Soil Fertility Analysis)
Y Nutrient and metals loading calculations (to determine most limiting parameter) YTD!
n/a Hauling records- # gal/tons hauled during calendar year to date
n/a Field loading records X Field site maps and information
n/a Records of lime purchased
Y Pathogen & Vector Attraction Reduction
Comments *TCLP samples have been taken. Results have not been received from the lab. No
land application performed during 1999 annual reporting period. Sour testing shows compliance.
Pathogen & Vector Attraction Reduction records (check which methods apply)
Fecal coliform
X SM 9221 E (Class A or B)
(Class A, all test must be <1000 MPN / dry gram)
(Class B, Geo. mean of 7 samples/monitoring period - <2.0* 106 CFU / dry gram)
SM 9222 D (Class B only)
(Geo. mean of 7 samples/monitoring period for Class B <2.0* 106 CFU / dry gram)
Salmonella (Class A, all tests must be < 3MPN / 4 grams dry )
Time / Temp records n/a
Digester (MCRT) Compost Class A lime stabilization
Volatile Solids Calculations X SOUR
Bench -top aerobic/anaerobic digestion results
pH records for lime stabilization ( Class A or B )
Treatment (check treatment type(s) used)
X Aerobic digestion Autothermal Thermophilic Aerobic Digestion (ATAD)
Anaerobic digestion Drying beds (may not meet 503's)
Alkaline Stabilization Lime other
Compost (check treatment type used) n/a
Windrow Aerated Static Pile In vessel Other

Residuals Inspection Res. pg 2
City of Statesville WQ0014543
Transport n/a
Permit in transport vehicle? Spill control plan in transport vehicle?
Does transport vehicle appear to be maintained?
Operation & Maintenance records n/a
Calibration records of land application equipment
Condition of land application equipment on site _
Storage
Number of months storage- 3
describe storage -3 acre paved with runoff collection partially covered area with pushwalls.
(if more than 2 yrs, does facility have Surface Disposal Permit?)
Spill control plan on storage site?
N/a Lagoon - Is lagoon lined
Above ground tank n/a
Aerated Mixed
X* Drying beds
*Drying beds are not used
Concrete storage pads
In ground tank n/a
Aerated Mixed
Sampling
Describe Sampling — Sampling is performed by the contractor prior to land application. Sampling
is performed according to EPA 40 CFR part 503 guidelines.
Is sampling adequate Y Is sampling representative Y
Field Sites (end use for class B biosolids) n/a
Permit on site during application
Buffers adequate
Documented exceedances of PAN limits
Signs of runoff / ponding
Rain Gauge on site during application
Comments
Spill plan on site
Cover crop specified in permit
Site condition adequate
(if no, improvements recommended)

Residuals Inspection
City of Statesville WQ0014543
Are there any limiting slopes on fields? Y/N X
10 % for surface application 18% for subsurface application)
Monitoring well(s) in permit: n/a
If yes, Location of well(s)
Odors/vectors
Odors present no Vectors present no
Describe any nuisance Conditions and any corrective actions needed
Res. pg 3

10E, i t
•
�.. Wax 1111 *tntesuffle, Nort4 &roftna 28687
February 18, 2016
r,
Attention: Ed Hardee
NCDWR
Water Quality Non -Discharge Permitting Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1636
RE: Annual Report for 2015
City of Statesville Land Application (WQ0014543)
Dear Mr. Hardee:
Enclosed, you will find 1 original and 2 copies of the required forms and lab data for the City of
Statesville Land Application, permit #WQ0014543. This land application program has never been utilized.
However, the City of Statesville wishes to keep this permit activeincase of an emergency.
This permit was compliant for the year.
Should you require more information, or if further action is required, please contact me at 704- 878-343-8.
Pit
h
WWTP Supervisor, Fourth Creek WWTP

FACILITY NAME:
LOCATION:
MAILING ADDRESS:
RESPONSIBLE OFFICIAL:
FACILITY OPERATOR:
RESIDUALS ORC:
APPLICATION:
GENERAL INFORMATION
LAND APPLICATION
CALENDAR YEAR 2015
Permit No. WQ0014543
Fourth Creek WWTP-NPDES NCO031836
Third Creek WWTP- NPDES NCO020591
693 Bell Farm Rd.
444 Third Creek Rd.
P. O. Box 1111
Statesville, NC 28687-1111
[phone]
[phone]
L. F. "Joe" Hudson, Jr., Director
Dept. of Water Resources
P. O. Box 1111
Statesville, NC 28687-1111
[phone]
Andy Smith
P. O. Box 1111
Statesville, NC 28687-1 l 11
[phone]
Andy Smith
P. O. Box 1111
Statesville, NC 28687-1111
[phone]
Land Application
No Residuals land applied in 2015

ANNUAL LAND APPLICATION CERTIFICATION FORM
. Il=1.
`WQ Permit#: WQ0014543 County:
Facility. Name (as shown on permit):
Land Application Operator:
Iredell Year: 2015
Fourth Creek WWTP
Land application of residuals as allowed by the permit occurred during the past calendar year?
❑ Yes 0 No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summa
Total number of application fields in the ermit:
Total number of fields utilized for land application during the year:
Total amount of dry tons applied during the year for all application sites:
Total number of acres utilizes for land application during the year:
878-343 8
Part B - Annual Compiance Statement:
Facility was compliant during calendar year with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. ❑ Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated.facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true; accurate;
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
A d4 4Z�"
Pe itt Name and Title (type or print) Signature of Permittee Date
of Preparer*
Date " Signature of Land Applier
Date
(if different from Permittee) . (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

Pat McCrory
Governor
NCDENR
North Carolina Department'of Environment and Natural Resources
March 4, 2015
Mr. L.F. Hudson, Jr., Director of Water Resources
City of Statesville
P.O. Box 1111
Statesville, North Carolina 28687
Dear Mr. Hudson:
Donald van der Vaart
Secretary
Subject: Acknowledgement of Receipt of the 2014 Annual Report
City of Statesville — Permit No.: WQ0014543
Land Application of Residuals
Iredell County
The Mooresville Regional Office (MRO) received and reviewed the 2014 Annual Report for the
above permit. The form submitted indicates there was no land application activity conducted
under this permit during 2014. The MRO plans to conduct a facility inspection within the year;
however, please contact me at [phone], should you have any immediate questions or
concerns.
Sincerely,
i
Maria Schutte, Environmental Specialist
Mooresville Regional Office
Water Quality Regional Operations Section
Division of Water Resources, NCDENR
CC: Andy Smith, Town of Statesville, WWTP Supervisor and Residuals ORC (Email)
Ed Hardee, LAU Compliance, CO -Raleigh (Email)
Mooresville Regional Office
610 East Center Avenue, Suite 301, Mooresville, North Carolina 28115
Phone: [phone]_L_Eax:-704-663-60.40/CustomerService_1-87.7-623=67.48
Internet: www.ncdenr.gov
An Equal opportunity \ Affirmative Action Employer— Made in part by recycled paper

�t o R' 1t'rs I�IPIl�IaNFt1�VtlfS
*t j Utll
V. 0. fox 1111 • �tntesuille, North &rolina 28587 MQQOP `?1L� 91oNALoFFICE
February 16, 2017
Attention: Ed Hardee
NCDWR
Water Quality Non -Discharge Permitting Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1636
RE: Annual Report for 2016
City of Statesville Land Application (WQ0014543)
Dear Mr. Hardee:
R_ Ce
FEB 22N
'oggiig Unit
Erfocma®°W-'�r �Q ctio»
Enclosed, you will find 1 original and 2 copies of the required forms and lab data for the City of
Statesville Land Application, permit #WQ0014543. This land application program has never been utilized.
However, the City of Statesville wishes to keep this permit active in case of an emergency.
This pen -nit was compliant for the year.
Should you require more inf6nnation, or if further action is required, please contact me at 704- 878-3438.
4n r y
And Smith
WW P Supervisor, Fourth Creek WWTP

GENERAL INFORMATION
LAND APPLICATION
CALENDAR YEAR 2016
Permit No. WQ0014543
FACILITY NAME: Fourth Creek WWTP-NPDES NCO031836
Third Creek WWTP- NPDES NCO020591
LOCATION: 693 Bell Farm Rd.
444 Third Creek Rd.
MAILING ADDRESS: P. O. Box I I I I
Statesville, NC 28687-1111
[phone]
[phone]
RESPONSIBLE OFFICIAL: L. F. "Joe" Hudson, Jr., Director
Dept. of Water Resources
P.O.Box IIII
Statesville, NC 28687-1111
[phone]
FACILITY OPERATOR: Andy Smith
P.O.Box IIII
Statesville, NC 28687-1111
[phone]
RESIDUALS ORC: Andy Smith
P.O.Box IIII
Statesville, NC 28687-1111
[phone]
APPLICATION: Land Application
No Residuals land applied in 2016.

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0014543 County: Iredell Year: 2016
Facility Name (as shown on permit):
Land Application Operator:
Andy Smith
Fourth Creek WWTP
Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
® Yes 0 No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals AV EIVEDINCDENR/DWI
generated but not land applied, please attach an explanation on how the residuals were handled. F LB .9, 7 201 /
Part A - Residuals Application Summary:
Total number of application fields in thepermit: AorW r
Total number of fields utilized for land application during the year:
Total amount of dry tons applied during the year for all application sites:
Total number of acres utilizes for land application during the year:
Part B - Annual Comniance Statement:
Facility was compliant during calendar year with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. ® Yes ® No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T. I I I l were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Permittr Name and Ti� (type or print)
-47
Signa ure of Permittee Date
ICE
arer*
Signature of Land Applier
Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
n[:Nfp r:nRnn nrr: 11010nnaN

A *'i
01.13-tv of 0I
#tatesuffile
I7M. Isax 1111 i§tatjesuffle,Nvrt4 Qraft
4th CREEK& 3rd CREEK WWTP SLUDGE NARRATIVE
Andy Smith
Both WWTP's generate biosolids that are currently stabilized using an aerobic digester, and dewatered
using a belt press. After dewatering, the residuals are transferred to the N-Viro lime stabilization process
area where the biosolids are set aside for contract land application off of the plant site. The contractor is
Synagro and they hold permit # WQ0016247 for this. The primary method of biosolids disposal is the N-
Viro process and that permit # is WQ0006245.

D t V SI,ON t"aF !'kVVT'F_R QUALITY
ivlA° 2015
_ ;?J
V. (0. Nux 1111 ° :§tatesuille, Nort4 ar>alina 28687
February 12, 2015
Attention: Ed Hardee
NCDWR
Water Quality Non -Discharge Permitting Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1636
RE: Annual Reports for 2014
City of Statesville Land Application (WQ0014543)
Dear Mr. Hardee:
Enclosed, you will find 1 original and 2 copies of the required forms and lab data for the City of
Statesville Land Application, permit #WQ0014543. This land application program has never been utilized.
However, the City of Statesville wishes to keep this permit active in case of an emergency.
This pennit was compliant for the year.
Should you require more information, or if further action is required, please contact me at 704- 878-3438.
A
4a
h
W WTP Supervisor, Fourth Creel: W WTP

GENERAL, INFORMATION
LAND APPLICATION
CALENDAR YEAR 2014
Permit No. WQ0014543
FACILITY NAME: Fourth Creek W WTP-NPDES NC0031836
Third Creek WWTP-NPDES N00020591
LOCATION: 693 Bell Farm Rd.
444 Third Creel: Rd.
MAILING ADDRESS: P. O. Box 11 l 1
Statesville, NC 28687-1 l 1 1
[phone]
[phone]
RESPONSIBLE OFFICIAL: L. F. "Joe" Hudson, Jr., Director
Dept. of Water Resources
P. O. Box 11 1 1
Statesville, NC 28687-1111
[phone]
FACILITY OPERATOR: Andy Smith
P.O. Box 1111
Statesville, NC 28687-1111
[phone]
RESIDUALS ORC: Andy Smith
P. O. Box 1111
Statesville, NC 28687-1 11 1
[phone]
APPLICATION: Land Application
No residuals laud applied in 2014

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0014543 County: Iredell Year:
2014
Facility Name (as shown on permit):
Land Application Operator:
Fourth Creek WWTP
Andy Smith Phone:
Land application of residuals as allowed by the permit occurred during the past calendar year?
Yes 21 No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
704-878-343 8
Total number of application fields in the ermit:
Total number of fields utilized for land application during the year:
Total amount of dry tons applied during the year for all application sites:
Total number of acres utilizes for land application during the year:
Part B - Annual Compiance Statement:
Facility was compliant during calendar year with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. E-11 YesI No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T. I 1 I i were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
1 1) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
N
Perm
or print)
Signature of Permittee Date
SkAature Preparer`` Date Signature of Land Applier Date
(if differeiftfi-oin Permittee) (if different from Permittee and Preparer)
:� Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
DENR FORM ACF (12/2006)

r,
.9
a�i Iof N
i
4th CREEK & .fir d CREEK WWTP SLUDGE NARRATIVE
Andy Smith
Both WWTP's generate biosolids that are currently stabilized using an aerobic digester, and dewatered
using a belt press. After dewatering, the residuals are transferred to the N-Viro lime stabilization process
area where the biosolids are set aside for contract land application off of the plant site. The contractor is
Synagro and they hold permit # WQ0016247 for this. The primary method of biosolids disposal is the N-
Viro process and that permit # is WQ0006245.

r
"ALE
`r
NCDENR
North Carolina Department of Environment and Natural Resources
Pat McCrory
Governor
August 13, 2014
Mr. L.F. Hudson, Jr., Director of Water Resources
City of Statesville
P.O. Box 1111
Statesville, North Carolina 28687
Dear Mr. Hudson:
John E. Skvarla, III
. Secretary
Subject: Non -Discharge Permit Inspection and Acknowledgement
of Receipt of the 2013 Annual Report
Permit Nos. WQ0004040, WQ006254, WQ0014543 and
WQ0016247 (SYNAGRO)
City of Statesville, Iredell County
The Mooresville Regional Office (MRO) conducted a compliance inspection on June 23rd, 2014,
which included a land application event, records review and residuals processing and storage at
the Third Creek and Fourth Creek WWTPs. The MRO would like to thank Andy Smith for his time
during the inspection.
Please note the expiration dates and potential compliance issues are listed under each permit
below. Time sensitive matters and issues of most concern are highlighted.
W00004040 Third Creek Monofill, expires 12/30/2018
The monofill units were not inspected at this time. This permit is mentioned to acknowledge
the receipt of the 2013 Annual Report, which reflected there was no disposal of residuals in
the monofill.
WQ0006254 Class A — Lime Stabilized, expires 09/30/2015
• The permit renewal application is due 180 days prior to expiration, which is
03131 /2015.
• Records for the pH meter calibration are incomplete. Calibration dates should
match dates for the lime stabilization analyses. This was discussed with Andy
Smith for correction on future log entries.
WQ0014543 Class B - Emergency Land Application, expires 02/28/2019
There is currently no activity under this permit.
WQ0016247 Class B - SYNAGRO Land Application, expires 02/28/2018
This permit is held by SYNAGRO, but they rely on Statesville to collect and analyze for all
required parameters including Pathogen and Vector Attraction Reduction (PVAR). In
addition, the comments below would also apply to Statesville's Class B permit
#W00014543, were it being utilized for land application.
• Odors and flies were detected at both the residuals storage area and the land
application sites. This is an indication that VAR is not being properly met.
Mooresville Regional Office, 610 East Center Avenue, Mooresville, North Carolina 28155
Phone: [phone] Internet: www.ncdenr.gov
An Equal Opportunity 1 Affirmative Action Employer— Made in part by recycled paper

e
• The city of Statesville meets both their PVAR requirements once per quarter. To
maintain compliance with permit conditions, it is recommended that SYNAGRO,
schedule land application events to coincide as close as possible to the PVAR
results time frame, and that ONLY currently, stored and analyzed residuals be
land applied.
The attached report should be self-explanatory; however, should you have questions please
contact me by phone [phone]) or email (maria.schutteca-)ncdenr.gov).
Sincerely,
Maria Schutte, Environmental Specialist
Mooresville Regional Office
Water Quality Regional Operations Section
Division of Water Resources, NCDENR
Attachment: Inspection Report June 2014
CC: Mr. Andy Smith, Town of Statesville (email)
Mr. Marshall Puryear, SYNAGRO (email)

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Resources
Pat McCrory, Governor.
John E. Skvarla, III, Secretary
kT.:?W,A
A-&4
_7610
=000M
NCDENR
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
City/Town/Owner: Statesville County: Iredell
Permit No.: WQ0006245 Class A Lime Issued: 10/20/2006 Expiration: 09/30/2015
Permit No.: W00014543 Class B emergency Issued: 09/17/2013 Expiration: 02/28/2019
Permit No.: W00016247 SYNAGRO Land Application Issued: 03/27/2009 Expiration: 02/28/2018
Permittee Contact: Andy Smith (4th Creek WWTP ORC) Telephone No.: 704-878-3438
LA ORC: Marshall R. Puryear (SYNAGRO) LA #994465 Telephone No.: 434-738-8002
LA BUORC: Froncy M. Dail (SYNAGRO) LA #13197 Telephone No.: 910-443-7696
Reason for Inspection
X ROUTINE COMPLAINT FOLLOW-UP OTHER
Type of inspection
Collection System Spray Irrigation X Sludge Other
Inspection Date(s): . June 23, 2014
Inspection Summary: (additional comments may be included on attached mazes)
This inspection included the Third Creek WWTP, Fourth Creek WWTP, and covers all three City of
Statesville residuals permits: #WQ0006245 (Class A), WQ0014543 (Emergency LA - not used) and
WQ0016247 (Class B - Synagro LA). The third Creek Monofill, permit #WQ0004040, was not inspected
for this report. It is only mentioned here to note the receipt and review of the 2013 Annual Report.
The 4th creek plant was the only plant actively processing sludge (dewatering), at the time of inspection,
and 4th creek is where all residuals are stored. There are separate bay areas for the "class A" residuals
storage and distribution, and the 3rd creek and 4th creek "class B" residuals handled by SYNAGRO. Issues
to address to maintain compliance are noted here and in the cover letter.
• Strong odors and vectors were noticed in the Class B residuals storage areas and at the field
Land Application sites. More timely land application is recommended upon passing PVAR
parameters.
• The pH calibration log for the Alkaline Stabilization meter should have matching dates to
the pH time and temperature records.
Is a follow-up inspection necessary _yes X no
Inspector(s): Maria Schulte - Environmental Specialist
Telephone No.: 704-663-1699 Fax No.: 704-663-6040
Date of Inspection: June 23rd, 2014

Residuals Inspection pg. 2
WQ0006245, WQ0014543, WQ0016247 Statesville, Iredell County
Type of Residual
WQ0006247 and WQ0014543 WQ0006245 .
X Land Application (class B) X Distribution and Marketing (class A)
Y-yes N-no NE -not evaluated NA -not applicable
Record Keeping (class B)
Record Keeping (class A)
Y
Copy of current permit
Y
Copy of current permit
Y
Current metals and nutrient analysis
Y
Current metals and nutrient analysis
Y
TCLP analysis
Y
TCLP analysis
*Y
SSFA (Standard Soil Fertility Analysis)
NA
SSFA (Standard Soil Fertility Analysis)
*Y
Nutrient and metals loading calculations
NA
Nutrient and metals loading calculations
*Y
Hauling records
Y
Hauling records
*Y
Field loading records
NA
Field loading records
*Y
Field site maps and information
NA
Field site maps and information
NE
Records of lime purchased
Y
Records of lime purchased
Y
Pathogen & Vector Attraction Reduction
Y
Pathogen & Vector Attraction Reduction
* Comments: Most data was reviewed as part of 2013 Annual Report The only field maps reviewed were
for the land application sites visited.
Pathogen & Vector Attraction Reduction Records
Fecal coliform
X SM 9221 E (Class A or B)
ISM 9222 D (Class. B only)
Salmonella (Class A, all tests must be < 3MPN / 4 grams dry)
Class A lime stabilization X
SOUR X
pH records for lime stabilization (Class A or B) X
Comments: It was noted that the pH time and temp logs for the Class A product appeared complete which
was an improvement over last year; however, the logbook for the pH meter calibration was missing dates
that should have coincided with the Class A analytical dates. This was discussed with And Smith during the
inspection.
Treatment
X Aerobic digestion anaerobic digestion
X Alkaline Stabilization Lime other -describe:
Transport
Spill control plan in transport vehicle? Y
Does transport vehicle appear to be maintained? Y
Comments: A transport vehicle was followed from the 4th creek WWTP to a land application site.

icesiuuais inspection pg. 3
WQ0006245, WQ0014543, WQ0016247 Statesville, Iredell County
d
Storaue
Number of days/weeks/months of storage: Approximately 3 montl
Describe storage: Cake residuals are stored at the 4rh creek WWTP
A, 3rd Creek Class B and 4th Creek Class B residuals
Odors present Y Vectors present Y
Comments: The odors and vectors detected were associated with the Class B materials not the Class A
and appeared to be more prevalent with the 3rd creek material
Samnlin�
Describe Sampling: Sampling and analyses are handled b the he City of Statesville
Is sampling adequate? NE Is sampling representative? NE
Field Sites (end use for class B biosolids)
Y Permit on site during application Y Spill plan on site
Y Buffers adequate Y Cover crop specified in permit
N Documented exceedances of PAN limits Y Site condition adequate
N Signs of runoff / ponding (if no, improvements recommended)
NE Rain Gauge on site during application
Are there any limiting slopes on fields?
Y 10 % for surface application N 18% for subsurface application
Comments: There were odors and vectors detected at both land application sites visited Vectors were
mostly concentrated at the staging areas as this is where the odors were most siynificant Odors and vectors
were not detected on portions of the fields where spreading had taken place as residuals were significantly
less concentrated.
Monitoring well(s) Y/N: N
If yes, location of well(s): This permit currently does not require ,groundwater monitories
Odors/vectors
Describe any nuisance conditions and any corrective actions needed. There were odors and vectors
present at the residuals storage and the LA sites Improved communication and coordination of land
application events with PVAR sampling results is suggested as a possible solution to alleviate nuisance
conditions. Per conversation with And Smith there have been delays with recent LA due to scheduling
difficulties.
Odors present Y
Vectors present Y
Other noted conditions: Per request from the Central Of ice in Raleigh, future annual reports can still
be mailed in the same package but should be com iled separately so as not to cause confusion for those
unfamiliar with facility operations. This will also reduce the risk of any of your reports being overlooked
and not properly received at the data processing acility_

GENERAL INFORMATION
LAND APPLICATION
CALENDAR YEAR 2013
Permit No. WQ0014543
C11;s, At'
GJ�.2a7/
FEB 2 � 2014
VLA I th"UrILII Y Stcrlary
��{ nf?�A4TIn�t ��(1(`F^^fAIr I IN1'
FACILITY NAME: Fourth Creek WWTP-NPDES NC0031836
Third Creek WWTP- NPDES NCO020591
LOCATION: 693 Bell Farm Rd.
444 Third Creek Rd.
MAILING ADDRESS:
RESPONSIBLE OFFICIAL:
FACILITY OPERATOR:
RESIDUALS ORC:
P. O. Box 1111
Statesville, NC 28687-1111
[phone]
[phone]
L. F. "Joe" Hudson, Jr., Director
Dept. of Water Resources
P.O.Box I I I I
Statesville, NC 28687-1111
[phone]
Andy Smith
P.O.Box IIII
Statesville, NC 28687-1111
[phone]
Andy Smith
P. O. Box 1111
Statesville, NC 28687-1111
[phone]
IJI
2014 �yI
APPLICATION: Land Application
No Residuals land applied in 2013

jo. (@. Nux 1111 • �Natesuille, NvO4 &rulina 28687
4th CREEK & 3rd CREEK WWTP SLUDGE NARRATIVE
Both WWTP's generate biosolids that are currently stabilized using an aerobic digester, and dewatered
using a belt press. After dewatering, the residuals are transferred to the N-Viro lime stabilization process
area where the biosolids are set aside for contract land application off of the plant site. The contractor is
Synagro and they hold permit # WQ0016247 for this. The primary method of biosolids disposal is the N-
Viro process and that permit # is WQ0006245.

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0014543 County:
Facility Name (as shown on permit):
Land Application Operator:
Iredell
Andy Smith
Year: 2013
Fourth Creek. WWTP
Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
® Yes R1 No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
- Residuals
F Total number of application fields in the permit:
Total number of fields utilized for land application during the year:
Total amount of dry tons applied during the year for all application sites:
Total number of acres utilizes for land application during the year:
Part B - Annual Compiance Statement:
Facility was compliant during calendar year with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. ® Yes Cl No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
oe-a'k ff A GL a1L)6!.A Weou rct S
Per 'tte ame and 'Ole (type o rint) % ignature of Permittee Date
�`/ l
Sig ature o Preparer* Date Signature of Land Applier Date
(if differen from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

s
r�
V. (9. Nox 1111 • 3tatouille, Nart4 &rulina 20687
January 30, 2013
Attention: Ed.Hardee
NCDENR
1617 Mail Service Center
Raleigh, North Carolina 27699-1601
RE: Annual Reports for 2012
Third Creek Monofil (WQ0004040)
Land Application (WQ0014543)
Alkaline Stabilization (WQ0006245)
Dear Mr. Hardee:
Enclosed, you will find 3 copies each of the annual reports as referenced above.
All of the above referenced permits were in compliance for the calendar year 2012.
The 4`h Creek WWTP Monofil (WQ0001759) permit has been rescinded and the monitoring wells
have been properly abandoned. Enclosed are the well abandonment records and the letter of Rescission of
Surface Disposal of Residuals Permit.
Should you require more information, or if further action is required, please contact me at 704- 878-3438.
AI
ith
WWTP Supervisor, Fourth Creek WWTP
l
RECEIVEDIDENRIDWQ ¢.t
FEB 06 CUiJ
Aquifer Protection Section

GENERAL INFORMATION
LAND APPLICATION
CALENDAR YEAR 2012
Permit No. WQ0014543
FACILITY NAME: Fourth Creek WWTP NPDES NCO031836
Third Creek WWTP- NPDES NCO020591
LOCATION: 693 Bell Farm Rd.
444 Third Creek Rd.
MAILING ADDRESS: P. O. Box 1111
Statesville, NC 28687-1111
[phone]
[phone]
RESPONSIBLE OFFICIAL: L. F. "Joe" Hudson, Jr., Director
Dept. of Water Resources
P. O. Box 1111
Statesville, NC 28687-1111
[phone]
FACILITY OPERATOR: Andy Smith
P. O. Box 1111
Statesville, NC 28687-1111
[phone]
RESIDUALS ORC: Andy Smith
P:O.Box IIII
Statesville, NC 28687-1111
[phone]
APPLICATION: Land Application
No Residuals land applied in 2012
FEB 0 5 2013
Aquifer Protection Section

r
,Y � � f '
nr ,
!�
'�'..

ANNUAL LAND APPLICATION CERTIFICATION FORM
1 L
WQ Permit#: WQ0014543 County: Iredell Year:
Facility Name (as shown on permit):
Fourth Creek WWTP
2012
Land Application Operator: Andy Smith Phone:
Land application of residuals as allowed by the permit occurred during the past calendar year?
❑ Yes 0 No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
704-878-3438
Total number of application fields in thepermit:
Total number of fields utilized for land application during the year:
Total amount of dry tons applied during the year for all application sites:
Total number of acres utilizes for land application during the year:
Part B - Annual Compiance Statement:
Facility was compliant during calendar year with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. ❑ Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results ark attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
.%i/k• I-d. C, d4�c✓
Pery 4tteeAName and Title (type or print)
r
� / -674) ��
Signature of Permittee Date
Signature f Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
FSC Certification No. 99012
Full -Service Analytical &
NC Drinking Water Cert No. 37735
Environmental Solutions VA Certification No. 1287
Project: Sludge (Hazardous Testing)
Project No.: 4th Creek Sludge
Lab Submittal Date: 07/23/2012
Prism Work Order. 2070499
Case Narrative
08/06/2012
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
TCLP Herbicide analysis was subcontracted to AES. Reactivity analysis was subcontracted to GCAL.
Laboratory reports are attached.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By
SR Surrogate recovery outside the QC limits.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone]-Toll Free Number: 1-8001529-6364- Fax: [phone] Page 1 of23

6y � ,� I S I Full -Service Analytical
_JI Environmental Solutions
Q.i LAHORPTORIE$ ING
Sample Receipt Summary
08/06/2012
Prism Work Order: 2070499
Client Sample 10 Lab Sample ID Matrix Date Sampled Date Received
Fourth Creek Sludge 2070499-01 Solid 07/23/12 07/23/12
Samples received in good condition at 5.8 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of 23

/I
ifE, n R
a�ueorulonieS we
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Full -Service Analytical &
Environmental Solutions
Project: Sludge (Hazardous Testing)
Project No.: 4th Creek Sludge
Sample Matrix: Solid
Laboratory Report
08106/2012
Client Sample ID: Fourth Creek Sludge
Prism Sample ID: 2070499-01
Prism Work Order: 2070499
Time Collected: 07/23/12 13:20
Time Submitted: 07/23/12 15:15
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Tme ID
General Chemistry Parameters
% Solids
15.6
% by 0.100
0.100 1
'SM2540 G
712,4112 14:30
LTB
P2130435
Weight
Corrosivity-pH
4.8
pH Units
1
'9045D
7126112 11:00
JAB
P2130499
Ignitability
Pass
mm/sec 0.10
1
*1030
8/1/12 8:30
JAB
P21-10005
TCLP Extraction by EPA 1311
TCLP Extraction
Complete
N/A
1
`1311
7/27/12 9:30
MEH
P2G053D
TCLP Extraction
Complete
N/A
1
•1311 ZHE
7/31/12 9:00
ANG
P2130552
TCLP Metals
Mercury
BRL
mg/L
0.010
0.0000070
1
`7470A
7/30/12 18:01
MEH
P2130550
Arsenic
BRL
mg/L
0.050
0.010
1
'6010C
7/30/12 18:10
BGM
P2G0532
Barium
BRL
mg/L
5.0
0.013
1
'6010C
7/30/12 18:10
BGM
P2G0532
Cadmium
BRL
mg/L
0.025
0.00043
1
'6010C
7/30/12 18:10
BGM
P2130532
Chromium
BRL
mg/L
0.25
0.00085
1
'6010C
7/30/12 18:10
BGM
P2130532
Lead
BRL
mg/L
0.050
0.0038
1
`6010C
7/30/12 18:10
BGM
P2130532
Selenium
BRL
mg/L
0.10
0.012
1
'6010C
7/30/12 18:10
BGM
132130532
Silver
BRL
mg/L
0.25
0.0017
1
'6010C
7/30/12 18:10
BGM
P2130532
TCLP Organochlorme Pesticides by GC/ECD
Chlordane
BRL
ug/L
2.5
0.16
1
'808113
7/31/12 19:42
JMV
P2130560
Dieldrin
BRL
ug/L
0.50
0.0084
1
`808113
7/31/12 19:42
JMV
P2G0560
Endrin
BRL
ug/L
0.50
0.013
1
`808113
7/31/12 19.42
JMV
P2G0560
gamma-BHC
BRL
ug/L
0.50
0.0097
1
`80818
7131/12 19:42
JMV
P2130560
Heptachlor
BRL
ug/L
0.50
0.017
1
'80818
7/31/12 19:42
JMV
P2130560
Heptachlor Epoxide
BRL
ug/L
0.50
0.014
1
'80816
7131/12 19:42
JMV
P2130560
Methoxychlor
BRL
ug/L
0.50
0.024
1
'80818
7/31/12 19:42
JMV
P2G0560
Toxaphene
BRL
ug/L
25
0.14
1
•808113
7/31/12 19.42
JMV
P2G0560
Surrogate
Recovery
Control Limits
Decachlorobiphenyl 118 % 13-186
Tetrachloro-rrFxylene 105 % 40-134
TCLP Semivolatile Organic Compounds by GC/MS
2,4,5-Tdchlorophenol
BRL
mg/L
0.25
0.010
1
'8270D
7/31/12 15:10
KC
P2G0538
2,4,6-Trichlorophenol
BRL
mg/L
0.10
0.011
1
'8270D
7/31/12 15:10
KC
P2G0538
2,4-Dinitrotoluene
BRL
mg/L
0.050
0.0059
1
'8270D
7/31/12 15:10
KC
P2130538
2-Methylphenol
BRL
mg/L
0.050
0.012
1
`8270D
7/31/12 15:10
KC
P2G0538
3/4-Methylphenol
BRL
mg/L
0.050
0.0098
1
'8270D
7/31/12 15:10
KC
P2G0538
Hexachlorobenzene
BRL
mg/L
0.050
0.0039
1
'8270D
7/31/12 15:10
KC
P2130538
Hexachlorobutadiene
BRL
mg/L
0.050
0.016
1
'8270D
7/31/12 15:10
KC
P2130538
Hexachloroethane
BRL
mg/L
0.050
0.018
1
'8270D
7/31/12 15:10
KC
P2130538
Nitrobenzene
BRL
mg/L
0.050
0.014
1
'8270D
7/31112 15:10
KC
P2130538
Pentachlorophenol
BRL
mg/L
0.25
0.0092
1
'8270D
7/31/12 15:10
KC
P2130538
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 Of 23

RR
�"�. ?ueoanlowES �r+c.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Full -Service Analytical &
Environmental Solutions
Project: Sludge (Hazardous Testing)
Project No.: 4th Creek Sludge
Sample Matrix: Solid
Laboratory Report
08/06/2012
Client Sample ID: Fourth Creek Sludge
Prism Sample ID: 2070499-01
Prism Work Order: 2070499
Time Collected: 07/23/12 13:20
Time Submitted: 07/23/12 15:15
Parameter Result Units Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Pyridine BRL mg/L 0.25
0.011 1
*8270D 7/31/12 15:10 KC
132130538
Surrogate Recovery Control Limits
2,4,6-Tribromophenol
90 %
49-109
2-Fluorobiphenyl
76 %
55-96
2-Fluorophenol
52 %
27-74
Nitrobenzene•d5
75 %
53-99
Phenol-d5
34 %
11-52
Terphenyl-d14
82 %
42-133
TCLP Volatile Organic Compounds by GC/MS
1,1-Dichloroethylene
BRL
ug/L
35
0.078
1
*8260B
8/3112 15:09
VHL
P21-10094
1,2-Dichloroethane
BRL
ug/L
25
0.14
1
*8260B
8/3112 15:09
VHL
P21-10094
1,4-Dichlorobenzene
BRL
ug/L
380
0.068
1
*8260B
8/3/12 15:09
VHL
1321-10094
Benzene
BRL
ug/L
25
0.072
1
*8260B
8/3/12 15:09
VHL
P21-10094
Carbon Tetrachloride
BRL
ug/L
25
0.12
1
*8260B
8/3/12 15:09
VHL
P21-10094
Chlorobenzene
BRL
ug/L
5000
0.061
1
*826013
8/3/12 15:09
VHL
P21-10094
Chloroform
BRL
ug/L
300
0.089
1
*8260B
8/3/12 15:09
VHL
P21-10094
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/L
10000
0.90
1
*8260B
8/3/12 15:09
VHL
P2H0094
Tetrachloroethylene
BRL
ug/L
35
0.069
1
*8260B
8/3/12 15:09
VHL
P21-10094
Trichloroethylene
BRL
ug/L
25
0.054
1
*8260B
8/3/12 15:09
VHL
P21-10094
Vinyl chloride
BRL
ug/L
10
0.16
1
*8260B
8/3/12 15:09
VHL
P21-10094
Surrogate Recovery Control Limits
4-Bromofluorobenzene 112 % 80-124
Dibromofluoromethane 105 % 75-129
Toluene-d8 108 % 77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone]-W9 Page 4 of 23

' 1 l
Sample Extraction Data
Prep Method: 1311
Lab Number
Batch Initial
Final
Dateliime
2070499-01
P2G0552 25 g
500 mL
07/30/12 14:30
2070499-01
P2G0530 100 g
2000 mL
07/26/12 15:30
Prep Method: 3010A
Lab Number
Batch Initial
Final
DateFrime
2070499-01
P2G0532 10 mL
50 mL
07/30/12 8:30
Prep Method: 7470A
Lab Number
Batch Initial
Final
Date/7 me
2070499-01
P2G0550 20 mL
30 mL
07/30/12 12:00
Prep Method: 3510C GC
Lab Number
Batch Initial
Final
Daternme
2070499-01
P2G0560 200 mL
10 mL
07/30/12 13:00
Prep Method: 3510C MS
Lab Number
Batch Initial
Final
DateMme
2070499-91
P2G0538 200 mL
1 mL
07/30/12 8:45
Prep Method: 50308
Lab Number
Batch Initial
Final
DateMme
2070499-01
P21-10094 10 mL
10 mL
08/03/12 9:31
Subcontracted Analyses
The following analyses were subcontracted to Analytical Environmental Services,
Inc.
Lab Number
Analysis
2070499-01
Herbicides TCLP (Sub)
The following analyses were subcontracted to Gulf Coast Analytical Labs, Inc.
Lab Number
Analysis
2070499-01
Reactivity, Cyanide (Sub)
2070499-01
Reactivity, Sulfide (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number.1-8001529-8364 - Fax: [phone]-M9 Page 5 of 23

Full-ServIce AnalyticalEnvironmental SoludionserAVI
449 Springbrook Road • P.O. Box 240543 • Charlotte, NC 28224-0543
Phone:[phone] • Fax.[phone]
Client Company Name: CIAO
Report To/Contact Name: A. . 31+1144
Reporting Address: P, a &)e Orr
_ • S taiess" lie NC
CHAIN OF CUSTODY RECORD
PAGE _ OF _ QUOTE P TO ENSURE PROPER BILLING6
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
*Please ATTACH any project specific reporting (QC LEVEL 111111 IV)
provisions and/or QC Requirements
Invoice To:
Address:
rnunu; •...- - •- ��... raxqLep troop -• • Purchase Order NoAlIling Reference
Email (Yes) (No) Email Address
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days Cl5 Days
EDD Type: PDF_ Excel_Other
Certification: NELAC ' USACE FL NC
"Working Days" ❑ 6-9 Days ❑ Standard 10 days Cl Rush Work Must Be
Site Location Name: A"a % Creak 14W TP Pre -Approved
SC_ OTHER N/A
Samples received after 15:00 will be processed next business day.
493 Bell Far,,, R, Turnaround
Site Location Physical Address: time Is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO_
S& asYr Ile NC RE BY PRISSE FOR MLABORATORES, INC. TCLIENT) DING SERVICES
Semple Iced Upon Collection: YES _NO _
CLIENT
DATE
TIME
COLLECTED
MATRIX
(SOIL,
SAMPLE CONTAINER
ANALYSES REQUESTED
PRISM
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
PRESERVA-
TIVES
REMARKS
LAB
'TYPE
HOURS
SLUDGE)SEE
BELOW
NO.
SIZE
ID N0.
FOL414A ere7-.A-34A
13 A0
S
(�'
C
r s:
7'CrtP /�/
S/
An
Mr
St.,-
Val
V
FCA.
P
ru
P
66i
' o
Sampler's Signature Sampled By•(Print Name) Affiliation
Upon rolin wishing, this Chain of Custody la your authorization for'Prism to proceed with the analyses as requested above. Any changes must be
submitted In writing to the Prism Project Manager, There will be charges for any changes after analyses have been initialized.PRISM USE ONLY
Relinquished By: (Signature) v a tart' oure Additional Comments: 0� "" n ;fir I T( `' tt I ..'
Relin ule : (SI Received By: (Sign ale
I,e1 r .fef.:
WWI Refinqulshed Igneture) Beat ,•r< J 5
P Lebo
eceWed r Date
ode J�
0 o Sh prnent: E A SAMPLE C SHOULD BE TAPED SHUT PORT I N THE LABORATORY. Group o.
SAMPLES ARE NOT A EPTED AND VERIFED AGAINST COO UNTIL RECEIVED AT LABORATORY.
<a
N :ad tat ❑UPS ❑ Hand ❑ zo
Field Servk� ❑ Other :�
-delivered
C DES: UST: QRO NDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER: � � 'O NS
C ❑ SC ❑ NC ❑ SC I ❑ NC ❑ SC lo- ❑NC ❑SC • I❑ NC ❑ SC I ❑NC ❑SC ❑NC ❑SCI ❑NC ❑SCI ❑NC ❑SCTERMS
❑ ❑ ❑ ❑ ❑ ❑ ❑' ORIGINAL
NTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
r•

C£ls-
ANAMCAL,1K.
ANALYTICAL REPORT
CLIENT
Prism Laboratories
PO Box 240543
Charlotte NC 282240543
ATTENTION
Robbie A. Jones
PROJECT ID
2070499
LABORATORY REPORT NUMBER
1207128
Primary Data Review By
7 r 06,
Kathryn Waters
Project Manager, AES
DATE
August 04, 2012
Secondary Data Review By
Ashley Amick
Project Manager, Access Analytical
[e-mail]
PLEASE NOTE:
- Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc),
3785 Presidential Parkway, Atlanta, GA 30340.
- AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582,
NELAP certified laboratory # E87582
- Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a
representative of AES serving client in the SC/NOGA areas. All questions regarding this report should be directed
to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243
Pagel 0 1
Page 7 of 23 I

AMISI r 1 lEwAronmentalSokitions
Full -Service Analytical ' V'
�u�ernum�a�a�
SUBCONTRACT ORDER
Certification: NELAC USACE_
Prism Laboratories, Inc.
SC Other c ,
2070499
NIA
SENDING LABORATORY:
RECEB G LABORATORY:
Prism Laboratories, Inc.
Analytical Environmental Services, Inc.
P. O. Box 240543
3785 Presidential Parkway
Charlotte, NC 28224-0543
Atlanta, GA 30340
Phone: [phone]
Phone :[phone]
Fax: [phone]
Fax: NA
Project Manager: Robbi A. Jones
Analysis Due Expires Laboratory ID Comments
d
Sample ED: 2070499-01 Solid Sampled:07/2311213:20 C
Herbicides TCLP (Sub) 07/30/1213:20
Containers Supplied
I LM-R CLEAR C,1ASs 01MRE5609D
ACS
i
.Il L
2 s 112 ion ze9
F ,
Released By Date Rcceived By Date
Released By Daft Received By Date
Page l of 2
Page 2 of 6
Page 8 of 23

Analytical Environmental Services, Inc. Date: 04Aug-12
CLIENT:
Prism Laboratories
Client Sample ID: 2070499-01
Lab Order:
1207128
Tag Number: Fourth Creek Sludge
Project:
2070499
Collection Date: 7/23/20121:20:00 PM
Lab ID:
1207128-OOIA
Matrix: SLUDGE
Analyses
Result Qua]
MDL
Limit Units BatchID DF Date Analyzed
HERBICIDES, TCLP SW131118151A
(SW3510C) Analyst: AK
2,4,5-TP (Silvex)
BRL
0.024
0.20 mg/L 164439 1 8/1/2012 921:00 PM
2,4-D
BRL
0.048
020 mg/L 164439 1 8/1/2012 9:21.00 PM
Surr.DCAA
93.6
0
47.1-151 %REC 164439 1 8/l/2012921:00PM i
i
Qualifiers: ;
Value exceeds Mammtmm Contaminant Level
<
Less than Result value
>
Greater than Result value
B
Analyte detected in the associated Method Blank
BRL
Below Reporting Limit
E
Estimated value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Estimated value detected below Reporting Limit
N
Analyte not NELAC certified
Rpt Lim
Reporting Limit Page 1 of 1
S
Spike Recovery outside limits due to matrix
Page 3 of 6
Page 9 of 23

a 1 ,
Analytical Environmental Services, Inc.
Sample/Cooler Receipt Checklist
Client _ �,ce55 Al Sht Work Order Number � 1�
Checklist completed by
Signature Date
Carrier name: FedEX Z S Y Courier Client— US Mail _ Other
Shipping container/cooler in good condition? Yes 1 No _
Custody seals intact on shipping container/cooler? Yes _ No _
Custody seals intact on sample bottles? Yes _ No
Container/Temp Blank temperature in compliance? (4°Ctk2)* Yes Z No _
Cooler #1 3,,5' Cooler #2 Cooler #3 Cooler #4
Not Present _
Not Present 1
Not Present
Cooler#S Cooler #6
Chain of custody present?
Yes
z
No r
Chain of custody signed when relinquished and received?
Yes
No _
/
Chain of custody agrees with sample labels?
Yes
No ,
/
Samples in proper container/bottle?
Yes
No —
Sample containers intact?
Yes
I/
No _
/
Sufficient sample volume for indicated test?
Yes
No —
All samples received within holding time?
Yes
No _
Was TAT marked on the COC?
Yes
_
No
Proceed with Standard TAT as per project history?
Yes
No _
Water- VOA vials have zero headspace? No VOA vials submitted
Yes _
Ndt Applicable_
No
Water - pH acceptable upon receipt? Yes _ No _ Not Applicable /
Adjusted? Checked by
Sample Condition: Good / Other(Explain)
(For diffusive samples or AIHA lead) Is a known blank included? Yes _ No
See Case Narrative for resolution of the Non -Conformance.
• Samples do not have to comply with the given range for certain parameters
1UQuality AssurrnceThecklists Procedures Sign-0tiTemplates%ChecklistslSample Receipt ChecklistslSample Cooler Receipt Checklist
Page 4 of 6
Page 10 of 23

Analytical Environmental Services, Inc
Date: 4-Aug-12
Client: Prism Laboratories
Project: 2070499 Dates Report
Lab Order: 1207128
Lab Sample ID Client Sample ID Collection Date Matrix Test Name
1207128-001A 2070499-01 7/23/2012 1:20:OO13M Sludge HERBICIDES, TCLP Leached
TCLP Date Prep Date Analysis Date
07/27/2012 07/30/2012 08/01/2012
Page 5 of 6

Analytical Environmental Services, Inc Date: 2-Aug-12
Client: Prism Laboratories ANALYTICAL QC SUMMARY REPORT
Project Name: 2070499
Workorder: 1207I28 BatchID: 164439
Sample ID: MB-164439
Client ID;
Units: mg/L
Prep Date: 07/30/2012
Run No: 226215
SampleType: MBLK
TestCode: HERBICIDES, TCLP SW1311/8151A
BatchID: 164439
Analysis Date: 08/01/2012
Seq No: 4735101
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2,4,5-TP (Silvex)
0.02398
0.20
0
0
0
0
0
0
0
0 U
2,4-1)
0.04768
0.20
0
0
0
0
0
0
0
0 U
Surr: DCAA
0.3895
0
0.5
0
77.9
47.1
151
0
0
0
Sample ID: LCS-164439
Client ID:
Units: mg/L
Prep Date: 07/30/2012
Run No: 226215
SampleType: LCS
TestCode: HERBICIDES, TCLP SW131V8151A
BatchID: 164439
Analysis Date: 09/01/2012
Seq No: 4735103
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2,4,5-TP (Silvex)
0.4209
0.20
0.5
0
84.2
61.8
129
0
0
0
2,4-D
0.4017
0.20
0.5
0
80.3
62.3
132
0
0
0
Sun: DCAA
0.2845
0
0.5
0
56.9
47.1
151
0
0
0
Sample 1D: 1207I26-001AMS
Client ID:
Units: mg/L
Prep Date: 07/30/2012
Run No: 226215
SampleType: MS
TestCode: HERBICIDES, TCLP SW1311/8151A
BatchID: 164439
Analysis Date: 08/01/2012
Seq No: 4735107
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val 0/.RPD
RPD Limit Qual
2,4,5-TP (Silvex) 0.4266 0.20 0.5 0 85.3 66.3 130 0 0 0
2,4-D 0.3403 0.20 0.5 0 68.1 66.4 135 0 0 0
Surr. DCAA 0.4824 0 0.5 0 96.5 47.1 151 0 0 0
FLDEllQuAllerst
W
cc V Indicates that the anslyte was detected In both the sample and the method blank J Estimated value
CD
U Indicates that the compound was analyzed for but not detected Q Sample held beyond the accepted holding time
N I The reported value isbetwaatthelabomtorymethoddeteadonlimitandthelaborotorypracticalquantitadonlimit
O_
N
W
AE5 LaboratoryQuailnersr
< Less that result value S Spike recovery outside limits due to matrix
> Greater than result value R RPD outside limits due to matrix
Page 6 of 6

Acass
A YncAL, INC.
ANALYTICAL REPORT
CLIENT
Prism Laboratories Inc.
PO BOX 240543
Charlotte, NC 28224
ATTENTION
Robbi Jones
PROJECTID
2070499
LABORATORY REPORT NUMBER
212072531
DATE
07/27/2012
Primary Data Review By Secondary Data Review By
Ashley B. Amick
Curtis Ekker Project Manager, Access Analytical, Inc.
Data Validation Manager, GCAL [e-mail]
PLEASE NOTE:
- Unless otherwise noted, all analysis on this report performed at Gulf Coast Analytical Labs (GCAL), 7979 GSRI
Avenue, Baton Rouge, LA 70820.
- GCAL is SCDHEC certified laboratory # 73006, NCDENR certified lab # 618, GA certified lab # LA-01955, NELAP
certified laboratory # 01955
- Local support services for this project are provided by Access Analytical, Inc.. Access Analytical is a representative of
GCAL serving clients in the SC/NC/GA areas. All questions regarding this report should be directed to your local Access
Analytical representative at 803.781.4243 or toll free at 888.315.4243.
Page 13 of 23

NELAP CERTIFICATE NUMBER 09955
DOD FLAP CERTIFICATE NUMBER ADE - 9482
ANALYTICAL RESULTS
PERFORMED BY
GULF COAST ANALYTICAL LABORATORIES, INC.
7979 GSRI Avenue
Baton Rouge, LA 70820
Report Date 07/27/2012
iridrtnil�iii7siia
Deliver To Prism Laboratories Inc.
PO BOX 240543
Charlotte, NC 28224
706-529-6364
Aftn Robbi Jones
Project 2070499
Page 14 of 23

CASE NARRATIVE
Client: Access Analytical Report: 212072531
Gulf Coast Analytical Laboratories received and analyzed the sample(s) listed
on the sample cross-reference page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
No anomalies were found for the analyzed sample(s).
Page 15 of 23

t { J
Laboratory Endorsement
Sample analysis was performed in accordance with approved methodologies provided by the
Environmental Protection Agency or other recognized agencies. The samples and their corresponding
extracts will be maintained for a period of 30 days unless otherwise arranged. Following this retention
period the samples will be disposed in accordance with GCAL's Standard Operating Procedures.
Common Abbreviations Utilized In this Report
ND Indicates the result was Not Detected at the specified RDL
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FLD Indicates the analysis was performed in the Field
PQL Practical Quantitation Limit
MDL Method. Detection Limit
RDL Reporting Detection Limit
00:00 Reported as a time equivalent to 12:00 AM
Reporting Flags Utilized in this Report
J Indicates the result is between the MDL and RDL
U Indicates the compound was analyzed for but not detected
B Indicates the analyte was detected in the associated Method Blank
Sample receipt at GCAL is documented through the attached chain of custody. In accordance with
NELAC, this report shall be reproduced only in full and with the written permission of GCAL. The results
contained within this report relate only to the samples reported. The documented results are presented
within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as
a permanent record thereof. The results contained within this report are intended for the use of the client
Any unauthorized use of the information contained in this report is prohibited.
I certify that this data package is in compliance with the NELAC standard and terms and conditions of the
contract and Statement of Work both technically and for completeness, for other than the conditions in the
case narrative. Release of the data contained in this hardcopy data package and in the
computer -readable data submitted has been authorized by the Quality Assurance Manager or his/her
designee, as verified by the following signature.
Estimated uncertainty of measurement is available upon request This report is in compliance with the
DOD QSM as specified in the contract if applicable.
Robyn Migues
Technical Director
GCAL REPORT 212072531 j
THIS REPORT CONTAINS + PAGES.
Page 16 of 23

r f J
Report Sample Summary
GCAL ID Client ID Matrix Collect Datefrime Receive DateMme
21207253101 FOURTH CREEK SLUDGE Solid 07/231201213:20 07/25/2012 09:55
GOAL Report 212072531
Page 17 of 23

r ♦ �
Summary of Compounds Detected
There were no detects
GCAL Report 212072531
Page 18 of 23

SV
SV
i 9012A Reactivity CN
)ate Prep Batch Prep Method . Dilution Analyzed By Analytical Batch
201217:30 486218 7.3.3.2 1 07/261201212:02 AEL 486374
CAS# Parameter
57-12-511 Reactivity Cyanide
Result
RDL
MDL
Units
25OU
250
250
mg/kg
V-846 9034 Reactivity Sulfide
Prep Date Prep Batch Prep Method Dilution Analyzed By Analytical Batch
07/25/201217:30 486219 Sec 7.3A2 1 .07/26/20121326 MDT 486403
CAS# Parameter Result RDL MDL Units
18496-25-BR Reactivity Sulfide 80U 80 80 mg/kg
RESULTS REPORTED ON A DRY WEIGHT BASIS
GCAL Report 212072531
Page 19 of 23

General Chemistry Quality Control Summary
Analytical Batch 488374
Client ID
MB486218
•LCS486218
Prep Batch 486218
GCAL ID
1089601
1089602
Prep Method 7.3.3.2
Sample Type
Method Blank
LCS
Prep Date
07/25/201217:30
07/25/201217:30
Analytical Date
07/26/201211:50
07/26/201211:51
Matrix
Solid
Solid
SW-846 9012A Reactivity CN
Unite mg/kg
Spike
Result
Control
Result
Rli Uded
1
% R
Limits % R
57-12-5R Reactivity Cyanide
250U 260
250
20.4
8.1
1 1 - 25
Analytical Batch 486374
Client ID
SS281-WL-01 0712
1089517DUP
Prep Batch 486218
GCAL ID
21207241802
1089603
Prep Method 7.3.3.2
Sample Type
SAMPLE
DUP
Prep Date
07/25/201217:30
07/25/201217:30
Analytical Date
07126/201211:55
07/26/201211:56
Matrix
I Solid
Solid
SW-846 9012A Reactivity CN
Units mg/kg
Result RDL
Result
RPD
RPD
Limit
57-12-511 Reactivity Cyanide
0.0 250
0.0
0.0
25
ca GCAL Report 212072531
CD
N
O
O
N
W

General Chemistry Quality Control Summary
Analytical Batch 486409
Client ID
MB486219
LCS486219
Prep Batch 486219
GCAL ID
1089604
1089605
Prep Method Sec 7.3.4.2
Sample Type
Method Blank
LCS
Prep Date
07/251201217:30
07/25/201217:30
Analytical Date
07/26/201213:26
071261201213:26
Matrix
Solid
Solid
SW-846 9034 Reactivity Sulfide
Units mg/kg
Spike
Result
Control
Result
ROUded
% R
Limits % R
18496-25-8R Reactivity Sulfide
801.1 80
689
625
90.7
1 20 - 114
Analytical Batch 486403
Client ID
SS281-WL-01 0712
1089517DUP
Prep Batch 486219
GCAL ID
21207241802
1089606
Prep Method Sec 7.3.4.2
Sample Type
SAMPLE
DUP
Prep Date
07/251201217:30
07/25/201217:30
Analytical Date
071261201213:26
07/26/201213:26
Matrix
I Solid
Solid
SW-846 9034 Reactivity Sulfide
Units mg/kg Result RDL
Result
RPD
RPD
Limit
18496.25-811 , Reactivity Sulfide
0 80
0
0
25
GCAL Report 212072531

£Z Jo ZZ a6ed
13o i a ova dg POA� wa SE%Z Lbd)9 °}$bL
wa LSPMUMH alga -- Aspamia2I
---)42 J
'F-R 25WJCM 51W) ?1V-n9 ?/Zt 7 1 .pjjddnS.VaWL,)UOj
We MONO (qns) OPPZ`O Amipwd
OVET WO£/LO
I-- ;Sp OrC[ ZIICVLO:paidmsg PHOS 10'661p000Z=UA+1--bi
SWWMOD al6japiopl sandxa ana 99499V
saaop •-r lggog =ftU2N PafWd
LIL9`L9L (SU) Mil 6O60-SZS-VOL -'Md
000-69L (SZ - =O'Id "£9-6ZS^008 :auogd
OZ80L V l `anog ao;eg £i�50-t�LZ8Z Ori ` I�
==AV THSO 6L6L £bSm XO$ •O 'd
'jW `sga'I ice. 4mV :pwo 3InD •o>d `sauoP�oge'I ms!Id
�axosvxoav i of =auozvxoavz OMMM
Vex 66tOLOZ
---jP JMBO as •au l =uajr-xoq ][ ms.ua
SDvsnl Dvmm :uou ► uaO
WQm0 J.7VXUNOOgnIS
-jib
I WtOSpopAp le wWe,,.!AUR
Hn:L I HSI
81liLlguYea!NaS-iln3
Z l 1 Z L OZ 1Z/9 Wqnovv
p.,w

NOTES 212 0 7 2 5 3
Revislon 1.1
ca
m
N
W
O
N
Page 1 of i