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WQ0014543_Regional Office Historical File Pre 2018 (2)
ATA NCDENR North Carolina Department of Environment and Division of Water Resources Water Quality Programs Pat McCrory Thomas A. Reeder Governor Director September 17, 2013 Mr. Joe Hudson — Water Resources Director City of Statesville PO Box 1111 Statesville, NC 28687-1111 Dear Mr. Hudson: Natural Resources 7 III __._._.__... Secretary LIL SEP 2 3 2013 i , L NGDENR MRO LD'h/f . - AgUifOr nrotC'rtio Subject: Permit No. WQ0014543 Land Application of Class B Residuals (Non -dedicated) Iredell County In accordance with your permit renewal request received July 12, 2013, we are forwarding herewith Permit No. WQ0014543 dated September 17, 2013, to the City of Statesville for the operation of the subject residuals management program as an emergency backup alternative to Permit No. WQ0016247 (issued to Synagro Inc.) and Permit No. WQ0006245 (Sta-Lime distribution permit issued to the City of Statesville). Please be advised that the approved land application sites listed on Attachment B is not sufficient for land application of the residuals amount listed on Attachment A. Hence, additional land application sites may be required and must be approved prior to utilization. Please note that this renewed permit shall become effective on March 1, 2014 (i.e. the day after the expiration date of the existing permit), which may differ from the issuance date of this letter. This permit shall be effective from March 1, 2014 until February 28, 2019, and shall be subject to the conditions and limitations as specified. therein. Please pay particular attention to the monitoring requirements listed in Attachments A for they may differ from the previous permit issuance. Failure to establish an adequate system for collecting and maintaining the required operational information shall result in future compliance problems. Please note that on September 1, 2006, North Carolina Administrative Code Title 15A Subchapter 02T — Waste not Discharged to Surface Waters was adopted. Accordingly, this permit incorporates the requirements of these rules, therefore, please take the time to review this permit thoroughly. If any parts, requirements or limitations contained in this permit are unacceptable, the Pennittee has the right to request an adjudicatory hearing upon written request within 30 days following receipt of this permit. This request shall be in the form of a written petition, conforming to Chapter 150B of the North Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail AQUIFER PROTECTION SECTION 1636 Mail Service Center, Raleigh, North Carolina 27699-1636 Location: 512 N. Salisbury St., Raleigh, North Carolina 27604 Phone: 919-807-64641 FAX: 919-807-6496 Internet: http://portal.ncdenr.orq/web/wq/aps An Equal Opportunity \ Affirmative Action Employer Mr. Hudson September 17, 2013 Page 2 of 2 Service Center, Raleigh, NC 27699-6714. Unless such demands are made, this permit shall be final and binding. If you need additional information concerning this matter, please contact Chonticha McDaniel at (919) 807-6337 or chonticha.mcdaniel@ncdenr.gov. Sincerely, Thomas A. Reeder cc: Iredell County Health Department Booresvi.11e Regional-O ce;,4quifer Protection Section Beth Buffington, Aquifer Protection Section Permit File WQ0014543 Notebook File WQ0014543 NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES RALEIGH LAND APPLICATION OF CLASS B RESIDUAL SOLIDS PERMIT (NON -DEDICATED) In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, and other applicable Laws, Rules, and Regulations PERMISSION IS HEREBY GRANTED TO City of Statesville Iredell County FOR THE operation of a residuals management program as an emergency backup alternative for the City of Statesville and consisting of the land application of Class B residuals generated by the approved facilities listed in Attachment A to the approved sites listed in Attachment B with no discharge of wastes to surface waters, pursuant to the application received July 12, 2013, and in conformity with other supporting data subsequently filed and approved by the Department of Environment and Natural Resources and considered a part of this permit. The use and disposal of residuals are regulated under Title 40 Code of Federal Regulations Part 503. This permit does not exempt the Permittee from complying with the federal regulations. This permit shall be effective from March 1, 2014 until February 28, 2019, and shall be subject to the following specified conditions and limitations: I. SCHEDULES 1. No later than six months prior to the expiration of this permit, the Permittee shall request renewal of this permit on official Division forms. Upon receipt of the request, the Division will review the adequacy of the facilities described therein, and if warranted, will renew the permit for such period of time and under such conditions and limitations as it may deem appropriate. Please note Rule 15A NCAC 02T .0105(d) requires an updated site map to be submitted with the permit renewal application. 2. Prior to land applying residuals to the approved land application sites listed on Attachment B, the Permittee shall submit updated setback maps and O&M plan (in accordance with Condition III.4) to the Mooresville Regional Office. WQ0014543 Version 3.0 Shell Version 130801 Page 1 of 12 II. PERFORMANCE STANDARDS 1. The subject residuals management program shall be effectively maintained and operated at all times so there is no discharge to surface waters, nor any contravention of groundwater or surface water standards. In the event the facilities fail to perform satisfactorily, including the creation of nuisance conditions due to improper operation and maintenance, the Permittee shall immediately cease land applying residuals to the site, contact the Mooresville regional office's supervisor, and take any immediate corrective actions. 2. This permit shall not relieve the Permittee of their responsibility for damages to groundwater or surface water resulting from the operation of this residuals management program. 3. Only residuals generated by the facilities listed in Attachment A are approved for land application in accordance with this permit. 4. Only the sites listed in Attachment B are approved for residuals land application. 5. Pollutant concentrations in residuals applied to land application sites listed in Attachment B shall not exceed the following Ceiling Concentrations (i.e., dry weight basis) or Cumulative Pollutant Loading Rates (CPLRs): Parameter Ceiling Concentration (milligrams per kilogram) CPLR (pounds per acre) Arsenic 75 36 Cadmium 85 34 Copper 4,300 1,338 Lead 840 267 Mercury 57 15 Molybdenum 75 n/a Nickel 420 374 Selenium 100 89 Zinc 7,500 2,498 The Permittee shall determine compliance with the CPLRs using one of the following methods: a. By calculating the existing cumulative level of pollutants using actual analytical data from all historical land application events of residuals, or b. For land where residuals application have not occurred or for which the required data is incomplete, by determining background concentrations through representative soil sampling. 6. Residuals that are land applied shall meet Class B pathogen reduction requirements in 15A NCAC 02T .1106 (a) and (c). Exceptions to this requirement shall be specified in Attachment A. 7. Biological residuals (i.e. residuals generated during the treatment of domestic or animal processing wastewater, or the biological treatment of industrial wastewater, and as identified in Attachment A) that are land applied shall meet one of the vector attraction reduction alternatives in 15A NCAC 02T .1107(a). Exceptions to this requirement shall be specified in Attachment A. WQ0014543 Version 3.0 Shell Version 130801 Page 2 of 12 8. Setbacks for land application sites shall be as follows: Setback Description Setback by application type (feet) Vehicular Surface Application Irrigation Surface Application Injection / In corporation Habitable residence or place of public assembly under separate ownership or not to be maintained as part of the project site 400 400 200 Habitable residence or places of public assembly owned by the Permittee, the owner of the land, or the lessee/operator of the land to be maintained as part of the project site 0 200 0 Property lines 50 150 50 Public right of way 50 50 50 Private or public water supply 100 100 100 Surface waters (streams — intermittent and perennial, perennial waterbodies, and wetlands) 100 100 50 Surface water diversions (ephemeral streams, waterways, ditches) 25 100 25 Groundwater lowering ditches (where the bottom of the ditch intersects the SHWT) 25 100 25 Subsurface groundwater lowering system 0 100 0 Wells with exception to monitoring wells 100 100 100 Bedrock outcrops 25 25 25 Top of slope of embankments or cuts of two feet or more in vertical height 15 15 15 Building foundations or basements 0 15 0 Water lines 0 10 0 Swimming pools 100 100 100 Nitrification fields 0 20 0 9. Land application areas shall be clearly marked on each site prior to and during any residuals application event. 10. Bulk residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in exceedance of agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen requirements based on the determined Realistic Yield Expectations (RYE) using any of the following methods: a. Division's pre -approved site specific historical data for specific crop or soil types by calculating the mean of the best three yields of the last five consecutive crop harvests for each field. b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State University Department of Soil Science (http://nutrients.soil.ncsu.edu/yields/index.php). A copy shall be kept on file and reprinted every five years in accordance with Condition IV.7(j). WQ0014543 Version 3.0 Shell Version 130801 Page 3 of 12 c. If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the RYE and appropriate nutrient application rates reported in any of the following documents: i. Crop management plan as outlined by the local Cooperative Extension Office, the North Carolina Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, or other agronomist. ii. Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance Document: Chapter 1 (http://www.ncagr.gov/SWC/tech/documents/9th Guidance Doc100109.pdf). iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation Services (NRCS). These plans must meet the USDA-NRCS 590 Nutrient Management Standards (ftp://ftp-fc.sc.egov.usda.gov/NHQ/practice-standards/standards/590.pdf). d. If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall contact the Division to determine necessary action. 11. When residuals are land applied to grazed pasture, hay crop realistic nitrogen rate shall be reduced by 25% in accordance with the USDA-NRCS 590 Nutrient Management Standards. 12. If land application sites are to be over -seeded or double -cropped (e.g., bermuda grass in the summer and rye grass in the winter with both crops to receive residuals), then the second crop can receive an application of PAN at a rate not to exceed 50 pounds per acre per year (lbs/ac/yr). This practice may be allowed as long as the second crop is to be harvested or grazed. If the second crop is to be planted for erosion control only and is to be tilled into the soil, then no additional PAN shall be applied. 13. Prior to land application of residuals containing a sodium adsorption ratio (SAR) of 10 or higher, the Permittee shall obtain and implement recommendations from at least one of the following: the local Cooperative Extension Office; the Department of Agriculture and Consumer Services; the Natural Resource Conservation Service; a North Carolina Licensed Soil Scientist; or an agronomist. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth. The Permittee shall maintain written records of these recommendations and details of their implementation. 14. The compliance boundary for residual land application sites shall be specified in accordance with 15A NCAC 02L .0107(b). These sites were individually permitted on or after December 30, 1983; therefore, the compliance boundary is established at either 250 feet from the residual land application area, or 50 feet within the property boundary, whichever is closest to the residual land application area. An exceedance of groundwater standards at or beyond the compliance boundary is subject to remediation action according to 15A NCAC 02L .0106(d)(2) as well as enforcement actions in accordance with North Carolina General Statute 143-215.6A through 143-215.6C. Any approved relocation of the COMPLIANCE BOUNDARY will be noted in Attachment B. 15. In accordance with 15A NCAC 02L .0108, the review boundary shall be established midway between the compliance boundary and the residual land application area. Any exceedance of groundwater standards at the review boundary shall require action in accordance with 15A NCAC 02L .0106. III. OPERATION AND MAINTENANCE REQUIREMENTS 1, The residuals management program shall be properly maintained and operated at all times. The program shall be effectively maintained and operated as a non -discharge system to prevent any contravention of surface water or groundwater standards. WQ0014543 Version 3.0 Shell Version 130801 Page 4 of 12 2. The Mooresville Regional Office, telephone number (704) 663-1699, and the appropriate local government official (i.e., county manager, city manager, or health director) shall be notified at least 48 hours prior to the initial residuals land application to any new land application site. Notification to the Aquifer Protection Section's regional supervisor shall be made from 8:00 a.m. until 5:00 p.m. on Monday through Friday, excluding State Holidays. 3. The Mooresville Regional Office shall be notified via email or telephone, (704) 663-1699, at least 24 hours prior to conducting any land application activity. Such notification shall indicate, at a minimum, the anticipated application times, field IDs, and location of land application activities. If it becomes necessary to apply to additional fields due to unforeseen events, the Regional Office shall be notified prior to commencing the application to those fields. 4. The Permittee shall maintain an approved Operation and Maintenance Plan (O&M Plan) pursuant to 15A NCAC 02T .1110. Modifications to the O&M Plan shall be approved by the Division prior to utilization of the new plan. The O&M Plan, at the minimum, shall include: a) Operational functions; b) Maintenance schedules; c) Safety measures; d) Spill response plan; e) Inspection plan including the following information: i. Names and/or titles of personnel responsible for conducting the inspections; ii. Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program; iii. Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed pursuant to the noncompliance notification requirements under the monitoring and reporting section of the permit; f) Sampling and monitoring plan including the following information: i. Names and/or titles of personnel responsible for conducting the sampling and monitoring; ii. Detailed description of monitoring procedures including parameters to be monitored; iii. Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures). 5. Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC) classification of the facility, the Permittee shall designate and employ a certified operator in responsible charge (ORC) and one or more certified operators as back-up ORCs in accordance with 15A NCAC 08G .0201. The ORC or their back-up shall visit the facilities in accordance with 15A NCAC 08G. 0204; or as specified in the most recently approved O&M plan (i.e., see Condition I11.4), and shall comply with all other conditions of 15A NCAC 08G. 0204. For more information regarding classification and designation requirements, please contact the Division of Water Resources's Technical. Assistance & Certification Unit at (919) 733-0026. 6. When the Permittee land applies bulk residuals, a copy of this permit and a copy of O&M Plan shall be maintained at the land application sites during land application activities. WQ0014543 Version 3.0 Shell Version 130801 Page 5 of 12 7. When the Permittee transports or land applies bulk residuals, the spill control provisions shall be maintained in all residuals transport and application vehicles. 8. Residuals shall not be stored at any land application site, unless written approval has been requested and received from the Division. 9. When the Permittee land applies bulk residuals, adequate measures shall be taken to prevent wind erosion and surface runoff from conveying residuals from the land application sites onto adjacent properties or into surface waters. 10. When the Permittee land applies bulk residuals, a suitable vegetative cover shall be maintained on land application sites onto which residuals are applied in accordance with the crop management plan outlined by the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, or an agronomist and as approved by the Division. 11. Bulk residuals shall not be land applied under the following conditions: a. If the residuals are likely to adversely affect a threatened or endangered species listed under section 4 of the Endangered Species Act or its designated critical habitat; b. If the application causes prolonged nuisance conditions; c. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface water or groundwater standards; d. If the land is flooded, frozen or snow-covered, or is otherwise in a condition such that runoff of the residuals would occur; e. Within the 100-year flood elevation, unless the bulk residuals are injected or incorporated within a 24-hour period following a residuals land application event; f. During a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period; If the slope is greater than 10% for surface applied liquid residuals, or if the slope is greater than 18% for injected or incorporated bulk liquid residuals; h. If the soil pH is not maintained at 6.0 or greater, unless sufficient amounts of lime are applied to achieve a final soil pH of at least 6.0, or if an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the specified crop. Any approved variations to the acceptable soil pH (6.0) will be noted in this permit; i. If the land does not have an established vegetative cover unless the residuals are incorporated or injected within a 24-hour period following a residuals land application event. Any field that is in a USDA no -till program shall be exempted from meeting this vegetative cover requirement; j. If the vertical separation between the seasonal high water table and the depth of residuals application is less than one foot; k. If the vertical separation of bedrock and the depth of residuals application is less than one foot; 1. Application exceeds agronomic rates. g- 12. The following public access restrictions apply to residual land application sites: a. Public access to public contact sites (e.g., golf courses, parks, ball fields, etc.) shall be restricted for 365 days after a residuals land application event; b. Public access to non-public contact sites shall be restricted for 30 days after a residuals land application event. WQ0014543 Version 3.0 Shell Version 130801 Page 6 of 12 13. Public access controls shall include the posting of signs with a minimum area of 3 square feet (e.g., 1.5' x 2'). Each sign shall indicate the activities conducted at each site, permit number, and name and contact information, including the Permittee or applicator's telephone number. Signs shall be posted in a clearly visible and conspicuous manner at the entrance to each land application site during a land application event, and for as long as the public access restrictions required under D1.12 apply. 14. The following harvesting and grazing restrictions apply to residual land application sites after each land application event: Harvesting and Grazing Description Restricted Duration Animals shall not be allowed to graze during land application activities and restricted period. Sites that are to be used for grazing shall have fencing to prevent access after each land application event. 30 days Food crops, feed crops and fiber crops shall not be harvested for: 30 days Turf grown on land where residuals have been applied shall not be harvested for: 12 months Food crops with harvested parts that touch the residual/soil mixture and are totally above the land surface (e.g., tobacco, melons, cucumbers, squash, etc.) shall not be harvested for: 14 months When the residuals remain on the land surface for four months or longer prior to incorporation into the soil, food crops with harvested parts below the land surface (e.g., root crops such as potatoes, carrots, radishes, etc.) shall not be harvested for: 20 months When the residuals remain on the land surface for less than four months prior to incorporation into the soil, food crops with harvested parts below the land surface shall not be harvested for: 38 months 15. The Permittee shall acquire from each landowner or lessee/operator a statement detailing the volume of other nutrient sources (i.e., manufactured fertilizers, manures, or other animal waste products) that have been applied to the site, and a copy of the most recent Nutrient Management Plan (NMP) for those operations where a NMP is required by the US Department of Agriculture — National Resources Conservation Service (NRCS) or other State Agencies. The Permittee shall calculate allowable nutrient loading rates based on the provided information and use appropriate reductions. For the purpose of this permit condition, a Crop Management Plan (CMP), Waste Utilization Plan (WUP) or Certified Nutrient Management Plan (CNMP) shall also be considered a Nutrient Management Plan. 16. No residuals shall be land applied unless the submitted Land Owner Agreement Attachment (LOAA) between the Permittee and landowners or lessees/operators of the land application site is in full force and effect. These agreements shall be considered expired concurrent with the permit expiration date, and shall be renewed during the permit renewal process. IV. MONITORING AND REPORTING REQUIREMENTS 1. Any Division required monitoring (including groundwater, plant tissue, soil and surface water analyses) necessary to ensure groundwater and surface water protection shall be established, and an acceptable sample reporting schedule shall be followed. WQ0014543 Version 3.0 Shell Version 130801 Page 7 of 12 2. Residuals shall be analyzed to demonstrate they are non -hazardous under the Resource Conservation and Recovery Act (RCRA). The analyses [corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)] shall be performed at the frequency specified in Attachment A, and the Permittee shall maintain these results for a minimum of five years. If residuals generated by a particular residuals source -generating facility are land applied at a frequency less than that which is specified in the most recently -certified Attachment A of this permit, the analyses shall be required for each residuals land application event. Any exceptions from the requirements in this condition shall be specified in Attachment A. The TCLP analysis shall include the following parameters (the regulatory level in milligrams per liter is in parentheses): Arsenic (5.0) 1,4-Dichlorobenzene (7.5) Nitrobenzene (2.0) Barium (100.0) 1,2-Dichloroethane (0.5) Pentachlorophenol (100.0) Benzene (0.5) 1,1-Dichloroethylene (0.7) Pyridine (5.0) Cadmium (1.0) 2,4-Dinitrotoluene (0.13) Selenium (1.0) Carbon tetrachloride (0.5) Endrin (0.02) Silver (5.0) Chlordane (0.03) Hexachlorobenzene (0.13) Tetrachloroethylene (0.7) Chlorobenzene (100.0) Heptachlor (and its hydroxide) (0.008) Toxaphene (0.5) Chloroform (6.0) Hexachloro-1,3-butadiene (0.5) Trichloroethylene (0.5) Chromium (5.0) Hexachloroethane (3.0) 2,4,5-Trichlorophenol (400.0) m-Cresol (200.0) Lead (5.0) 2,4,6-Trichlorophenol (2.0) o-Cresol (200.0) Lindane (0.4) 2,4,5-TP (Silvex) (1.0) p-Cresol (200.0) Mercury (0.2) Vinyl chloride (0.2) Cresol (200.0) Methoxychlor (10.0) 2,4-D (10.0) Methyl ethyl ketone (200.0) Once the residuals have been monitored for two years at the frequency specified in Attachment A, the Permittee may submit a permit modification request to reduce the frequency of this monitoring requirement. In no case shall the monitoring frequency be less than once per permit cycle. 3. An analysis shall be conducted on residuals from each source generating facility at the frequency specified in Attachment A, and the Permittee shall maintain the results for a minimum of five years. The analysis shall include the following parameters: Aluminum Mercury Potassium Ammonia -Nitrogen Molybdenum Selenium Arsenic Nickel Sodium Cadmium Nitrate -Nitrite Nitrogen Sodium Adsorption Ratio (SAR) Calcium Percent Total Solids TKN Copper pH Zinc Lead Phosphorus Magnesium Plant Available Nitrogen (by calculation) WQ0014543 Version 3.0 Shell Version 130801 Page 8of12 4. Residuals shall be monitored for compliance with pathogen and vector attraction reduction requirements at the frequency specified in Attachment A, and at the time indicated in the sampling and monitoring sections of the approved O&M plan. The required data shall be specific to the stabilization process utilized, and sufficient to demonstrate compliance with the Class B pathogen reduction requirements in 15A NCAC 02T .1106 (a) and (c), and one vector attraction reduction requirement in 15A NCAC 02T .1107 (a) shall be met. Any exceptions from the requirements in this condition shall be specified in Attachment A. 5. An annual representative soils analysis (i.e., Standard Soil Fertility Analysis) shall be conducted on each land application site listed in Attachment B on which a residuals land application event will occur in the respective calendar year. This analysis shall be in accordance with the "Guidance on Soil Sampling" located in the Sampling Instructions section of the NC Department of Agriculture & Consumer Services' website (http://www.ncagr.gov/agronomi/pubs.htm). The Permittee shall maintain these results and a description of the sampling methodologies used to determine soil fertility for a period of no less than five years, and shall be made available to the Division upon request. At a minimum, the Standard Soil Fertility Analysis shall include the following parameters: Acidity Exchangeable Sodium Percentage Phosphorus Base Saturation (by calculation) Magnesium Potassium Calcium Manganese Sodium Cation Exchange Capacity Percent Humic Matter Zinc • Copper pH 6. Laboratory parameter analyses shall be performed on the residuals as they are land applied, and shall be in accordance with the monitoring requirements in 15A NCAC 02B .0505. 7. The Permittee shall maintain records tracking all residual land application events. At a minimum, these records shall include the following: a. Source of residuals; b. Date of land application; c. Location of land application (i.e., site, field, or zone number as listed in Attachment B); d. Approximate areas applied to (acres); e. Method of land application; f. Weather conditions (e.g., sunny, cloudy, raining, etc.); g. Predominant Soil Mapping Unit (e.g., CbB2); h. Soil conditions (e.g., dry, wet, frozen, etc.); i. Type of crop or crops to be grown on field; j. Nitrogen Application Rate based on RYEs (if using data obtained from the North Carolina State University Department of Soil Science Website, the printout page shall be kept on file and reprinted every five years); k. Volume of residuals land applied in gallons per acre, cubic yard per acre, dry tons per acre, or wet ton per acre; 1. Volume of animal waste or other nutrient source applied in gallons per acre, dry ton per acre, or wet tons per acre; m. Volume of soil amendments (e.g., lime, gypsum, etc.) applied in gallons per acre, dry ton per acre, or wet tons per acre; and W00014543 Version 3.0 Shell Version 130801 Page 9 of 12 n. Annual and cumulative totals in dry tons per acre of residuals as well as animal waste and other sources of nutrients (e.g., if applicable), annual and cumulative pounds per acre of each heavy metal (e.g., shall include, but shall not be limited to, arsenic, cadmium, copper, lead, mercury, molybdenum, nickel, selenium, and zinc), annual pounds per acre of PAN, and annual pounds per acre of phosphorus applied to each field. 8. Three copies of an annual report shall be submitted on or before March r`. The annual report shall meet the requirements described in the Instructions for Residuals Application Annual Reporting Forms. Instructions for reporting and annual report forms are available at http://portal.ncdenr.org/web/wq/aps/lau/reporting, or can be obtained by contacting the Land Application Unit directly. The annual report shall be submitted to the following address: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 9. Noncompliance Notification The Permittee shall report by telephone to the Mooresville Regional Office, telephone number (704) 663-1699, as soon as possible, but in no case more than 24 hours or on the next working day following the occurrence or first knowledge of the occurrence of any of the following: a. Any occurrence with the land application program resulting in the land application of significant amounts of wastes that are abnormal in quantity or characteristic. b. Any failure of the land application program resulting in a release of material to surface waters. c. Any time self -monitoring indicates the facility has gone out of compliance with its permit limitations. d. Any process unit failure, due to known or unknown reasons, rendering the facility incapable of adequate residual treatment. e. Any spill or discharge from a vehicle or piping system during residuals transportation. Any emergency requiring immediate reporting (e.g., discharges to surface waters, imminent failure of a storage structure, etc.) outside normal business hours shall be reported to the Division's Emergency Response personnel at telephone number (800) 662-7956, (800) 858-0368, or (919) 733-3300.Persons reporting such occurrences by telephone shall also file a written report in letter form within five days following first knowledge of the occurrence. This report shall outline the actions taken or proposed to be taken to ensure that the problem does not recur. V. INSPECTIONS 1. The Permittee shall provide adequate inspection and maintenance to ensure proper operation of the subject facilities and shall be in accordance with the approved O&M Plan. 2. Prior to each bulk residuals land application event, the Permittee or his designee shall inspect the residuals storage, transport and application facilities to prevent malfunctions, facility deterioration and operator errors resulting in discharges, which may cause the release of wastes to the environment, a threat to human health or a public nuisance. The Permittee shall maintain an inspection log that includes, at a minimum, the date and time of inspection, observations made, and any maintenance, repairs, or corrective actions taken. The Permittee shall maintain this inspection log for a period of five years from the date of inspection, and this log shall be made available to the Division upon request. WQ0014543 Version 3.0 Shell Version 130801 Page 10 of 12 3. Any duly authorized Division representative may, upon presentation of credentials, enter and inspect any property, premises or place on or related to the land application sites or facilities permitted herein at any reasonable time for the purpose of determining compliance with this permit; may inspect or copy any records required to be maintained under the terms and conditions of this permit; and may collect groundwater, surface water or leachate samples. VI. GENERAL CONDITIONS 1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to an enforcement action by the Division in accordance with North Carolina General Statutes 143- 215.6A to 143-215.6C. 2. This permit shall become voidable if the residuals land application events are not carried out in accordance with the conditions of this permit. 3. This permit is effective only with respect to the nature and volume of residuals described in the permit application and other supporting documentation. 4. The issuance of this permit does not exempt the Permittee from complying with any and all statutes, rules, regulations, or ordinances, which may be imposed by other jurisdictional government agencies (e.g., local, state, and federal). Of particular concern to the Division are applicable river buffer rules in 15A NCAC 02B .0200; erosion and sedimentation control requirements in 15A NCAC Chapter 4 and under the Division's General Permit NCG010000; any requirements pertaining to wetlands under 15A NCAC 02B .0200 and 02H .0500; and documentation of compliance with Article 21 Part 6 of Chapter 143 of the General Statutes. 5. In the event the residuals program changes ownership or the Permittee changes their name, a formal permit modification request shall be submitted to the Division. This request shall be made on official Division forms, and shall include appropriate documentation from the parties involved and other supporting documentation as necessary. The Permittee of record shall remain fully responsible for maintaining and operating the residuals program permitted herein until a permit is issued to the new owner. 6 This permit is subject to revocation or unilateral modification upon 60 days notice from the Division Director, in whole or part for the requirements listed in 15A NCAC 02T .0110. 7. Unless the Division Director grants a variance, . expansion of the permitted residuals program contained herein shall not be granted if the Permittee exemplifies any of the criteria in 15A NCAC 02T .0120(b). 8. The Penmittee shall pay the annual fee within 30 days after being billed by the Division. Failure to pay the annual fee accordingly shall be cause for the Division to revoke this permit pursuant to 15A NCAC 02T .0105(e)(3). W00014543 Version 3.0 Shell Version 130801 Page 11 of 12 Permit issued this the 17th day of September 2013 NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION A. Reeder, Director Division of Water Resources By Authority of the Environmental Management Commission Permit Number WQ0014543 WQ0014543 Version 3.0 Shell Version 130801 Page 12 of 12 ATTACHMENT A - Approved Residual Sources City of Statesville Certification Date: September 17, Z013 . Permit Number: WQ0014543 Version: 3.0 • Owner Facility Name County Permit Number Biological Residuals Maximum Dry Tons Per Year 1 Monitoring Frequency for Non-hazardous 2 CharacteristicsNutrients Monitoring Frequency for Metals and Monitoring Frequency for Pathogen & Vector Attraction Reductions "'s Approved Mineralization Rate City of Statesville Fourth Creek WWTP Iredell NC0031836 Yes 1,057 Annually See Table Below See Table Below 0.30 City of Statesville Third Creek WWTP Iredell NC0020591 Yes 975 Annually See Table Below See Table Below 0.30 Total 2,032 I . The dry tons per year of residuals listed here represents the total maximum volume of residuals generated by th's facility and may not be equivalent to the volume of residuals that may be land applied to the land application sites approved in the Attachment B. Note that residuals shall be land applied at or below agronomic rates (see Condition II.10) and, therefore, only certain volume of residuals shall be applied at the approved sites. 2. Analyses to demonstrate that residuals are non -hazardous (i.e., TCLP, ignitability, reactivity, and corrosivity) as stipulated under permit Condition IV.2. 3. Testing of metals and nutrients as stipulated under permit Condition IV.3. 4. Analyses of pathogen and vector attraction reductions as stipulated under permit Condition IV.4. 5. Monitoring frequencies are based on the actual dry tons applied per year using the table below, unless specified above. Dry Tons Generated (short tons per year) Monitoring Frequency (Established in 40 CFR 503 and 15A NCAC 02T .1111) <319 1/Year =>319 - <1,650 1/ Quarter (4 times per year) =>1,650 - <16,500 1/60 Days (6 times per year) _> 16,500 1/month (12 times per year) If no land application events occur during a required sampling period (e.g. no land application occur during an entire year when annual monitoring is required), then no sampling data is required during the period of inactivity. The annual report shall include an explanation for missing sampling data. Those required to submit the annual report to EPA may be required to make up the missed sampling, contact the EPA for additional information and clarification. Page 1 of 2 ATTACHMENT A - Approved Residual Sources Certification Date: September 17, 2013 City of Statesville Permit Number: WQ0014543 Version: 3.0 THIS PAGE BLANK Page 2 of 2 ATTACHMENT B - Approved Land Application Sites City of Statesville Field/ Site 01 02 Total Certification Date: September 17, 2013 . Permit Number: WQ0014543 Version: 3.0 • Owner Lessee County Latitude Longitude Net Acreage Dominant Soil Series Footnotes City of Statesville Iredell 35°46'12" 80°47'24" 15.30 Lloyd 1 City of Statesville Iredell 35°44'24" 80°50'24" 14.10 Cecil 1 29.40 1. The total net acreage associated with these land application sites is not sufficient to land apply the total maximum volume of residuals approved in the Attachment A at agronomic rates. Shoul the Permittee require additional back-up sites, a permit modification application package shall be submitted no later than 180 calendar days prior to land application of residuals on the new sites. Page 1 of 1 • V T Y MAP• Third Creek g Fourth Craek Si tesvil 15.1 I n g .4, 831 - FIELD 14.1 L OO 14 543 FOURTH CREE.K .SITE Tract Acreage: 15.3 Buffer Acreage: 7. 7' . Total Acreage: 23.0 Drawing Scale: 1"=200' Property One City Limits Line. OIMMI • 1 !J3 -f r' •f tLo #2 WQco 14543 THIRD CREEK SITE Tract Acreage: 14.1 =Buffer Acreage: 7.2 Total Acreage: 21.3 •A I Drawing Scale: 1 "=200' AQUIFER PROTECTION SECTION '- ; �P� APPLICATION REVIEW REQUEST FORM ,_ i ,., J. _ti ,, , ;� ;; 0' ,J, Date: July 17, 2013 �ja31 J 2 2t a20 (-', `` (�+/,' oUn -U - uAU_,c- i,i.p1 C- To: ❑ Landon Davidson, ARO-APS ❑ David May, WaRO-APS, -�`t F' ` r"r`t ` ' `', ❑ ❑ Morella King, WiRO-APS Art Barnhardt, FRO-APS Zf;' :tckft J r _' fir,' `' ., ® l\ndrewyittrewm Ro--7A-Psri ❑ Sherri Knight, WSRO-APS ❑ Rick Bolich, RRO-APS From: Chonticha McDaniel ❑AFO❑GW Protection❑GW Planning ®LAU E-Mail: chonticha.mcdaniel(a ncdenr.gov Telephone: (919) 807-6337 Fax:(919) 807-6496 A. Permit Number: WQ0014543 B. Owner: City of Statesville C. Facility/Operation: City of Statesville Residuals Land Application ❑ Proposed ® Existing ❑ Facility ® Operation D. Application: 1. Permit Type: ❑ Animal ❑ Surface Irrigation ❑ Reclaimed ❑ H-R Infiltration ❑ Recycle ❑ I/E Lagoon ❑ GW Remediation (ND) ❑ UIC - (5A7) open loop geothermal ❑ Single Family Residence Residuals 2. Project Type: ❑ New ❑ Major Mod. ❑ Minor Mod. ® Renewal ❑ Renewal w/ Mod. E. Comments/Other Information: ❑ I would like to accompany you on a site visit. Attached, you will fmd all information submitted in support of the above -referenced application for your review, comment, and/or action. Within 30 calendar days, please take the following actions: ❑ Return a Completed APSARR Form. ❑ BIMS indicates monitoring wells locations are not complete. Please% update monitoring well locations not currently in BIMS. ❑ BIMS indicates ongoing ❑ NDMR ❑NDAR ❑ GW monitoring violations. Please investigate reoccurring compliance issues and summarize results in staff report. ❑ Attach Well Construction Data Sheet. ❑ Process Attachment B for Certification by the Land Application Unit (LAU). ❑ Issue an Attachment B Certification from the RO.* *coordinating site visits and reviews, as well as additional information requests with other RO-APS representatives in order to prepare a complete Attachment B for certification. Refer to the RPP SOP for additional detail. Please indicate the name and date assigned in the spaces below, make a copy of this sheet, and return it to the appropriate Central Office -Aquifer Protection Section contact person listed above. RO-APS Reviewer: Date: FORM: APSARR 03/10 Page 1 of 1 ATA: NCDENR North Carolina Department of Environment and Natural Resources Division of Water Quality Pat McCrory Thomas A. Reeder John E. Skvarla, III Governor Acting Director Secretary July 17, 2013 Joe Hudson — Water Resources Director City of Statesville P.O. Box 1111 Statesville, NC 28687-1111 Dear Mr. Hudson: Subject: Acknowledgement of Application No. WQ0014543 City of Statesville Residuals Land Application Program Land Application of Residual Solids (503) System Iredell County The Aquifer Protection Section acknowledges receipt of your permit application and supporting documentation received on 07/12/2013. Your application package has been assigned the number listed above, and the primary reviewer is Chonticha McDaniel. Central and Mooresville Regional Office staff will perform a detailed review of the provided application, and may contact you with a request for additional information. To ensure maximum efficiency in processing permit applications, the Aquifer Protection Section requests your assistance in providing a timely and complete response to any additional information requests. Please note that processing standard review permit applications may take as long as 60 to 90 days after receipt of a complete application. If you have any questions, please contact Chonticha McDaniel at (919) 807-6337 or chonticha.mcdaniel@ncdenr.gov. cerely, for Jon Isgliard Land Application Unit Supervisor cc: {'Nlooreille Regi�onaL0ffice Aquifer Protectxon'Sectio Permit File WQ0014543 AQUIFER PROTECTION SECTION 1636 Mail Service Center, Raleigh, North Carolina 27699-1636 Location: 512 N. Salisbury St., Raleigh, North Carolina 27604 Phone: 919.807-64641 FAX: 919-807-6496 Internet: www.ncwaterouality.orq An Equal Opportunity! Affirmative Action Employer NorthCarolina ?attrrallji ;iIitg of 3ttttesnille V. (I. dux 1111 • 'tatesuille, North TarnUna 211687 July 10, 2013 Mr. Ed Hardee NCDENR — Division of Water Quality Raleigh Central Office 1636 Mail Service Center Raleigh, NC 27699-1617 CC: Files w h IVEDAR , Jv Aqilleattmnon Section EIVED/DENR/DWQ JUL I AQJiferP,rofection Section Re: Form RLAP 01-12 Fourth Creek Wastewater Treatment Plant City Land Application Permit Renewal Permit No. WQ0014543 Dear Mr. Hardee: Enclosed you will find the RLAP 01-12 form and supporting information per the instruction sheet for this form. As noted in previous permit applications, this permit has never been used since its inception. The N-Viro process is the primary biosolids program for the 4th Creek WWTP. We have a contract with Synagro to land apply dry cake biosolids from the 3`i Creek and 4th Creek WWTP's with the understanding that this would be the secondary biosolids program. The permit that is associated with the Synagro contract is in their name and they take care of all of the monitoring and general conditions for that specific permit. Should you require more information, or if further action is required, please contact me at 704- 878- 3438. Sin ely AidySm h Plant Su -rvisor, Fourth Creek WWTP FWATFn QG RECEIVEDIDENRIDWQ State of North Carolina JUL 12 2013 Department of Environment and Natural Resources Division of Water Quality Aquifer Protection Section RESIDUALS LAND APPLICATION PROGRAM INSTRUCTIONS FOR FORM: RLAP 01-12 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information or for an electronic version of this form, visit the Land Application Unit (LAU) web site at: http://portal. ncdenr. org/web/wq/aps/lazy General — This application is for treatment, storage, transport, and/or land application of Class B residuals (may include residuals that are generated from a water treatment plant or other type facilities) on the proposed or currently approved land application site(s) under 15A NCAC 02T .1100. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Land Application Program (FORM: RLAP 01-12) Application: (All Application Packages): ❑ Submit the completed and appropriately executed Residuals: Land Application Program (FORM: RLAP 01-12) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ❑ The Applicant's Certification on Page 5 of this form shall be signed in accordance with 15A NCAC 02T .0106(b). An alternate person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A NCAC 02T .0106(b). ❑ If this project is for a modification of an existing permit, submit one copy of the existing permit. ❑ Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units. B. _ Application Fee (New and Major Modification Application Packages) ❑ Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environment and Natural Resources (NCDENR). ❑ STANDARD REVIEW — Submit the appropriate fee for all new and major modification applications as listed in the table below. ❑ EXPRESS REVIEW — Visit the Express Review webpage for the Express Fee Schedule: STANDARD APPLICATION REVIEW FEES: Facility Classification Major (land are permitted for >— 300 acres) New Permit $1,310 Major Modification 1 $395 Minor (land are permitted for < 300 acres) $810 $245 ' - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage; adds additional land application areas not previously approved; adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted. There is no fee for minor permit modifications. C. Cover Letter (All Application Packages) ❑ List all items included in the application package, as well as a brief description of the requested permitting action. D. Environmental Assessments (May be Required — See 15A NCAC 1 C .0300) ❑ Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include information on any mitigating 'factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for the construction of the subject facilities. INSTRUCTIONS FOR FORM: RLAP 01-12 Page 1 of 3 E. Operation and Maintenance Plan (New and Renewal Application Packages) El For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan. ❑ Submit the O&M Plan in accordance with 15A NCAC 02T .1110 and include at a minimum: ❑ Operational functions; describe the operation of the program to show what operations are necessary for the program to function and by whom the functions are to be conducted. ❑ Maintenance schedules; may include equipments calibration, maintenance of signs, etc. ❑ Safety measures; may include safety training program, manuals, signs, etc. ❑ Spill response plan; including control, containment, remediation, emergency contact information, etc. ❑ Inspection plan including the following information; ❑ Names and titles of personnel responsible for conducting the inspections. • Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program. ❑ Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed. ❑ Sampling and monitoring plan including the following information; D Names and titles of personnel responsible for conducting the sampling and monitoring. ❑ Detailed description of monitoring procedures including parameters to be monitored. ❑ Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures. THE FOLLOWING ADDITIONAL ITEMS (G to M) ARE REQUIRED FOR DEDICATED PROGRAM ONLY. F. Program Determination ❑ Dedicated residuals land application programs are ones in which land application sites meet the criteria in 15A NCAC 02T .1102(12). Specifically, a residuals land application program is designated as dedicated if any of the following are applicable: ❑ Any land application site certified for the residuals land application program that receives residuals at rates or frequencies greater than agronomic rates. ❑ Any land application site certified for the residuals land application program that is used primarily for residuals disposal, and agricultural crop production is of secondary importance. ❑ Any land application site certified for the residuals land application program that receives residuals through fixed irrigation facilities or irrigation facilities fed through a fixed supply system. ❑ Please contact the Aquifer Protection Section if you need any assistance in determining whether your residuals program falls under the dedicated program definitions. G. Program Information O Provide an explanation of why a dedicated system is required instead of a conventional non -dedicated system. ❑ Provide an explanation of the dedicated system and its operation. H. Detailed Site Maps (All New or Modification Application Packages) ❑ Submit three (3) sets of standard size plans and two (2) sets of 11" by 17" plans (electronic format is acceptable - Adobe PDF only). For Modifications, submit plans specific to the modification(s) only. ❑ Plans must include the following minimum items: ❑ A general location map, a vicinity map and a topographic map with contours not exceeding 10 feet or 25% of the total site relief and showing all facility related structures and fences within the land application area. ❑ The location of all wells (including usage and construction details if available), streams (ephemeral, intermittent, and perennial), springs, lakes, ponds, and other surface drainage features within 500 feet of the land application site(s). 0 Delineation of the review and compliance boundaries ❑ Setbacks as required by 15A NCAC 02T .1108 ❑ Site property boundaries within 500 feet of all waste treatment, storage, and disposal site(s). ❑ A map showing the entire irrigation area with an overlay of the suitable irrigation area depicted by the soil scientist's evaluation. The irrigation plans shall show each nozzle/emitter and wetted area (when applicable). Clearly label spray irrigation zones as they will be operated. INSTRUCTIONS FOR FORM: RLAP 01-12 Page 2 of 3 ❑ Plans must depict a completed design and not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR CONSTRUCTION, etc.) that indicate that they are anything other than final plans. However, the plans may be labeled with the phrase: FINAL DESIGN - NOT RELEASED FOR CONSTRUCTION Project Evaluation and Receiver Site Management Plan (All New Application Packages or Modifications that include new sites) ❑ Submit a project evaluation and a receiver site management plan (if applicable) with recommendations concerning cover crops and their ability to accept the proposed application rates. J. Hydrogeologic Report (All New Application Packages or Modifications involving increasing the total design capacity) ❑ Submit a detailed hydrogeologic evaluation in accordance with 15A NCAC 02T .1104(d)(4) and current Division Policy available at: http://portal_ncdenr.orc/web/wq/aps/lau/policies. The document shall be signed, sealed and dated by a qualified professional. K. Engineering Design Documents (All New or Modification Application Packages with fixed irrigation facilities or irrigation facilities fed through fixed supply system) ❑ Submit engineering design documents that have been signed, sealed, and dated by a NC licensed Professional Engineer and/or Professional Land Surveyor in accordance with 15A NCAC 02T .1104(d)(2). For Modifications, submit an updated site map specific to the modification(s) only. ❑ The design documents must include the following minimum items: ❑ Engineering plans for the facility and equipment except those previouslypermitted unless they are directly tied into the new units or are critical to the understanding of the complete process; Specifications describing materials to be used, method of construction, and means for ensuring quality and integrity of the finished product including leaking testing; and ❑ Engineering calculations including hydraulic and pollutant loading, sizing criteria, hydraulic profile, total dynamic head curve analysis for each pump, and irrigation design. ❑ Soil mapping units shown on all disposal sites. L. Water Balance (All New Application Packages or Modifications that include new sites utilizing fixed irrigation facilities( or irrigation facilities fed through fixed supply systems) ❑ Submit a completed and accurate water balance in accordance with 15A NCAC 02T .1104(d)(5) and current Division Policy available at: http://portal.ncdenr.org/web/wq/aps/lau/policies. M. Property Ownership Documentation (All New or Modification Application Packages involving new and/or relocated treatment or irrigation components) Property ownership documentation shall consist of one of the following: 0 Legal documentation of ownership (i.e., GIS, deed or article of incorporation), or 0 Written notarized intent to purchase agreement signed by both parties with a plat or survey map, or 0 An easement running with the land specifically indicating the intended use of the property and meeting the requirements of 15A NCAC 02L .0107(f), or 0 A written notarized lease agreement signed by both parties, indicating the intended use of the property, as well as a plat or survey map. ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS: NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER QUALITY AQUIFER PROTECTION SECTION LAND APPLICATION UNIT By U.S. Postal Service: 1636 MAIL SERVICE CENTER RALEIGH, NORTH CAROLINA 27699-1636 TELEPHONE NUMBER: (919) 807-6300 By Courier/Special Delivery: 512 N. SALISBURY STREET RALEIGH, NORTH CAROLINA 27604 FAX NUMBER: (919) 807-6496 INSTRUCTIONS FOR FORM: RLAP 01-12 Page 3 of 3 RECEIVEDIDENR/DWO J;UL 12 State of North Carolina Department of Environment and Natural Resources Division of Water Quality AquiferP fry! art Salm I. APPLICANT INFORMATION: RESIDUALS LAND APPLICATION PROGRAM FORM: RLAP 01-12 RECEVEDIDENRIDWO JUL 12 ? ,A itiare'i ion Sectin' Applicant type: ❑ Individual ❑ Corporation ❑ General Partnership 0 Privately -Owned Public Utility Federal ❑ State X Municipal ❑ County Signature authority's name per 15A NCAC 02T .0106: Joe Hudson Title: Water Resources Director Applicant's mailing address: PO Box 1111 City: Statesville State: NC Zip: 28687-1111 Telephone number: (704) 878-3438 Email Address: ihudson@statesvillenc.net 2. Consultant's name: N/A License Number (for P.E.): Affiliation: El On Staff ❑ Retained (Firm: ) Consultant's mailing address: City: State: Telephone number: ( ) - 3. Agronomist's name: N/A Affiliation: ❑ N/A 0 On Staff Agronomist's mailing address: City: State: Telephone number: ( ) 4. Soil Scientist's name:N/A Affiliation: ❑ N/A ❑ On Staff Soil Scientist's mailing address: City: State: Telephone number: (_) - 5. Fee submitted: $810.00(See Instruction B) 1. Applicant's name: City of Statesville II. PERMIT INFORMATION: 1. Application is for (check all that apply): ❑ Zip: - Email Address: License Number: L Retained (Firm: Zip: Email Address: License Number: ❑ Retained (Firm: Zip: Email Address: new, ❑ modified, X renewed permit 2. If this application is being submitted to renew or modify an existing permit, provide the following: Permit number: W00014543 Date of most -recently issued permit: March 11, 2005 Date of most -recently certified Attachment A (if different than the permit): Date of most -recently certified Attachment B (if different than the permit): FORM: RLAP 01-12 Page 1,of5 III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION: 1. Residuals Processing Facility's physical address: 693 Bell Farm Road City: Statesville State: NC Zip: 28677- Coordinates: Latitude: 35° 46' 29"N Longitude: 80° 48' 50"W Datum: Level of accuracy: Method of measurement: GPS 2. County where residuals land application program is headquartered: Iredell 3. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application program, their certification numbers, and their affiliations in the following table: Designation Name Affiliation Certification Number ORC Andy Smith City of Statesville LA 985516 Back -Up ORC Scott Austin City of Statesville LA 991939 Additional Back -Up ORCs (if applicable) If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application program, provide the candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training school and certification test: 4. Complete the following tables regarding management of the residuals land application program: a. Plant Available Nitrogen Summary: Determine the maximum plant available nitrogen (PAN) generated by all residuals source -generating facilities as currently certified and proposed for certification with this application and list the results in the following table: Maximum amount of residuals to be certified: 4th Creek —1056/ 3`a Creek — 973 dry tons per year. PAN Pounds of PAN per Dry Ton (Weighted Average) Pounds of PAN per Year Surface Incorporation or Injection Surface Incorporation or Injection First -Year 4th _ rd 4 / 3 _ 4.0 4.117/3 a3.88 Five -Year Maximum Adjusted 19.5/19.95 20586/19409 b. Land Application Site Use Summary: Summarize information regarding the land application sites as currently certified and proposed for certification with this application: Category Use Acres Comments Crops Forest or Plantation Row Crops 15.3 Corn & small grain. (4th Creek ) Hay 14.1 Fescue hay. (3`d Creek ) Pasture Total: Methods Surface FORM: RLAP 01-12 Page 2 of 5 Incorporation or Injection Total: c. Residuals Land Application Summary: Determine the minimum acreage required to land apply the residuals as currently certified and proposed for certification assuming the scenarios listed in the following table: Assumed Application Rate (lbs PAN/ac-yr) Acres Required Using First -Year PAN Concentrations Acres Required Using Five -Year Maximum Adjusted PAN Concentrations Surface Incorporation or Injection Surface Incorporation or Injection 50 4th 82.3/3`d 77.64 4d' 411.7/3rd 388.2 100 4"' 41.17/3`d 38.82 4th 205.85/3`d 194 150 4t 27.4/3`d 25.88 4t 137/3`d 129.4 200 w th 4 19.4i 3 4th 102.9/3`d 97 6. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application of the proposed residuals due to the violation of North Carolina Administrative Code (e.g. not enough storage, not enough land, vector reduction practices not in place, etc.): 7. Specify type of residuals program (See Instruction F): X Non -dedicated ❑ Dedicated If Dedicated, specify the following (check all that apply): ❑ Residuals program contains any land application site(s) that receives residuals at rates or frequencies greater than agronomic rates, explain; ❑ Residuals program contains any land application site(s) that is used primarily for residuals disposal, and agricultural crop production is of secondary importance, explain; ❑ Residuals program contains any land application site(s) that receives residuals through fixed irrigation facilities or irrigation facilities fed through a fixed supply system, explain; IV. RESIDUALS SOURCE INFORMATION: (Not required if no new, renewed, or modified residuals source) Complete and submit the following Residuals Source Certification and all associated documentation. Residuals Source Certification V. LAND APPLICATION SITE INFORMATION: (Not required if no new, renewed, or modified land application site) Complete and submit the following Land Applications Site Certification and all associated documentation. Land Application Siite Certification.doc FORM: RLAP 01-12 Page 3 of 5 Note: Item VI. Applicable to Dedicated Program with fixed irrigation system only. VI. DESIGN INFORMATION FOR FIXED IRRIGATION SYSTEM 1. The irrigation system is: ❑ Spray ❑ Drip 2. Disposal system is: ❑ existing ❑ proposed. 3. Minimum depth to mean seasonal high water table (SHWT) within irrigation sites(s) per Soil Scientist's Evaluation: feet below ground surface. Rules 15A NCAC 02T .0505(p) requires at least one -foot vertical separation between SHWT and ground surface. 4. Are there any artificial drainage or water movement structures within 200 feet of any irrigation area? ❑ Yes or ❑ No If Yes, please explain if the soil scientist report addresses artificial structures and please indicate if structures are to be maintained or modified: 5. Loading rates recommended by the Soil Scientist Evaluation: Soil Series Fields within Soil Area Recommended Loading Rate (in/hr) Recommended Loading Rate (in/yr) 6. Design loading rates are equal or less than the loading rates recommended by Soil Scientist? ❑ Yes or D No If No, explain why 15A NCAC 02T .0505(n) is not met: 7. Non -dedicated System Design (fill in the appropriate information for either a spray or drip irrigation system): Field /Zone Design Area (ft2) Number of Nozzles Maximum Application Rate (gallons/hr) Design Annual Loading Rate (gallons/yr) Total (4 ,ft.)_.' ..>, .�.. a Spray Irrigation Design Element Plan Sheet Number Specification Page Number Wetted diameter of nozzles ft Wetted area of nozzles ft2 Nozzle capacity gpm Nozzle manufacturer / model / Elevation of highest nozzle ft FORM: RLAP 01-12 Page 4 of 5 Applicant's Certification (signing authority must be in compliance with 15A NCAC 02T.0106): The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with anyve compliance schedule, and do not have any overdue annual fees under Rule I5A NCAC 02T .0105. Yes 111 No, Explain; 1,� � � t� cA. c> j (Signature Authority's Name — PLEASE PRINT) r (Title) attest that this application for kit diC,-- A --da..tr/a,_-1-ed- �.`S \o.. c c (inIi�\^^ (Facility Name) has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Quality may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Quality should a condition of this permit be violated. I also understand that if all required parts of this application are not completed and that if all required supporting information and attachments are not included, this application package will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.6B, any person who knowingly makes any false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to exceed $10,000 as well as civil penalties up to $25,000 per violation. Signature: Date: 777 RECEIVEDIDENR/DWO JUL 122013 Aquifer Protection Section FORM: RLAP 01-12 Page 5 of 5 SPILL CONT ' OL PLAIN FOR RESIDUALS TRANSFER BETWEEN PLANTS, BY WATER RESOURCES DEPARTMENT PERSONNEL IN TIIE UNLIKELY EVENT OF A SPILL, THE FOLLOWING ACTIONS SHALL BE IMMEDIATELY TAKEN: 1. MANAGEMENT OF CLEAN UP ACTIVITIES: The first Water Resources Department representative at the scene will begin procedures to halt the spill and initiate clean up activities. Upon arrival, the Director or Assistant Director will take immediate action to coordinate all activity. City of Statesville labor and equipment are to be utilized. In the event additional labor and equipment are required, assistance shall be requested from private contractors (see attached list). The Public Information Director shall also communicate with the public on the scene, answering questions and advising of the clean up activities. 2. HALT SOURCE OF SPILL: Such as a ruptured container or damaged transport unit. 3. CONTAIN SPILL: Form a barrier. Sufficient quantities of straw shall be used for such purpose. Earthen barriers may be constructed to augment the straw bale containment area. The person in charge on the spill site will advise the clean up personnel where to get the straw, lime, and other items necessary to complete the clean up operation, i.e. local farmers, farm supply center, nursery, etc. 4. CLEAN UP: Employ front end loaders, vacuum equipment, sludge application vehicle, and/or local septic tank service to remove as much of the spilled material as possible. Straw and/or sand should be scattered in the spill area to soak up the remaining material. The straw and sand soaked material will be collected and removed to a disposal area approved by representatives of the State regulatory agency. 5. FINAL CLEAN UP: Employ rotary brush sweeper if needed, and apply lime to the spill area upon the approval of the clean up efforts by the State regulatory representative. If the event occurs on private property, the clean up will be completed to the satisfaction of the property owner and State regulatory representatives. The ultimate goal will be to restore the spill area to its original condition, if possible. 6. NOTIFICATION*: As soon as possible after the spill occurs, the Water Resource Department or assistant will notify the Mooresville Regional Office, and they will also be responsible for notifying other key City personnel. 7. REPORTING: Regional personnel and/or city/project personnel will notify the Regional Office of the D.E. M. by telephone as soon as possible, but not more than 24 hours, or on the next working day following the occurrence. The Director or Assistant Director shall provide a written report to the appropriate regional office of the D.E. M. within 5 days of the occurrence. The report shall list all relative information and actions taken. 11Page Spill Emergency Call List Water Resource Director Name: Joe Hudson Telephone: 704-878-3438 Mobile: 704-437-6289 Water Resource, Assistant Director Name: Jerry Byerly Telephone: 704-878-3438 Mobile: 704-437-6288 City Residuals Coordinator Name: Andy Smith Telephone: 704-878-3438 Mobile: 704-437-2792 Plant Operator Fourth Creek Office Name: Andy Smith Phone: 704-878-3438 Plant Mobile: 704-437-2414 Third Creek Office Name: Scott Austin Mobile: 704-437-2668 Phone: 704-872-9621 Plant Mobile: 704-437-2413 Water Treatment Plant Name: Weston Johnson Mobile: 704-437-2915 Phone: 704-878-3441 Plant Mobile: 704-437-2916 PUBLIC UTILITIES DIRECTOR Name: Scott Harrell Telephone: 704-878-3551 Mobile: 704-902-1914 City Public Information Director Name: Nancy Davis Telephone: 704-878-3586 Mobile: 704-437-6669 LOCAL POLICE — FIRE EMERGENCY: 911 DENR-WQ Regional Office: Mooresville: 704-663-1699 State of N.C. Warning Point: 1-800-662-7956 (Emergency # for nights, weekends and holidays) 2IPage SPILL/EMERGENCY INFORMATION TO BE USED FOR SLUDGE TRANSPOR1ED WITHIN WA'l'ER RESOURES. List below the names of companies, addresses, telephone numbers, and any other pertinent data. If you apply in or travel through more than one county, please include information for each of them. SEPTIC COMPANY Lentz Septic Service Office: 704-876-1834 BACKHOE Gilbert Engineering Inc. 704-872-0986 STRAW Tractor Supply 704-838-0220 LIME Tractor Supply 704-838-0220 SAND Church Sand and Stone 704-872-4862 LOCAL POLICE 911 LOCAL FIRE DEPT. 911 Wage Beverly Eaves Perdue Governor NCDENIZ North Carolina Department of Environment and Natural Resources Division of Water Quality Coleen H. Sullins Dee Freeman Director I� ,aECH E retary Mr. Joe Hudson - Water Resources Director City of Statesville Post Office Box 1111 Statesville, North Carolina 28687-1111 Dear Mr. Hudson: October 7, 2009 OCT - 9 2009 NC DfENR2 Ri�ii j DVVQ Ac uifer Protection Subject: Permit Extension and Return of Renewal Application Permit No. WQ0014543 Iredell County On August 5, 2009, Session Law 2009-406, entitled "An Act to Extend Certain Government Approvals Affecting the Development of Real Property Within the State," was enacted by the General Assembly and signed into law. The Act, known as the Permit Extension Act of 2009, extends the expiration date of certain government approvals and permits until February 28, 2013. Non -discharge permit WQ0014543, issued by the Division of Water Quality, falls within the scope of this Act and is therefore being extended until February 28, 2013. ' With this letter, the permit renewal application received August 5, 2009 is being returned. Please note per your permit, a renewal application must still be submitted six months in advance of the extended expiration date. If you have any questions regarding this request, please contact Division staff at (919) 733-3221. Thank you in advance for your cooperation. Sincerely, pao,;„ David Goodrich Aquifer Protection Section Enc: Permit Renewal Application cc: Mooresville Regional -Office, Aquifer Protection_5ection, Permit File WQ0014543 AQUIFER PROTECTION SECTION 1636 Mail Service Center, Raleigh, North Carolina 27699-1636 Location: 2728 Capital Boulevard, Raleigh, North Carolina 27604 Phone: 919-733-3221 \ FAX 1: 919-715-0588; FAX 2: 919-715-6048 \ Customer Service: 1-877-623-6748 Internet: www.ncwaterquality.orq An Equal Opportunity \ Afrirmative,Action Employer One N©rthCaro :ina I aura// or AQUIFER PROTECTION SECTION APPLICATION REVIEW REQUEST FORM Date: August 31, 2009 To: ❑ Landon Davidson, ARO-APS ❑ Art Barnhardt, FRO-APS X Andrew Pitner, MRO-APS ❑ Jay Zimmerman, RRO-APS FILE ❑ David May, WaRO-APS ❑ Charlie Stehman, WiRO-APS ❑ Sherri Knight, WSRO-APS From: David Goodrich , Land Application Unit t , Telephone: (919) 715-6162 Fax: 919 file•048 E-Mail: david.goodrich@ncmail.net l � err3 - 9 2009 A. Permit Number: WQ0014543 ....� B. Owner: City of Statesville M gal F' r}Alpt't __ �,r;,.Elft?; !�SC��`'GcIo9'! C. Facility/Operation: City of Statesville Residual Land Application Program (503) ❑ Proposed ® Existing ® Facility X Operation D. Application: 1. Permit Type: ❑ Animal n Surface Irrigation ❑ Reuse ❑ H-R Infiltration ❑ Recycle ❑ I/E Lagoon ❑ GW Remediation (ND) ❑ UIC - (5A7) open loop geothermal For Residuals: ❑ Land App. ❑ D&M n Surface Disposal X 503 ❑ 503 Exempt ] Animal 2. Project Type: ❑ New Il Major Mod.. 7 Minor Mod. X Renewal n Renewal w/ Mod. E. Comments/Other Information: n I would like to accompany you on a site visit. Statutory Date: 11/03/2009 Attached, you will find all information submitted in support of the above -referenced application for your review, comment, and/or action. Within 30 calendar days, please take the following actions: ® Return a Completed APSARR Form. ❑ Attach Well Construction Data Sheet. ❑ Attach Attachment B for Certification by the LAPCU. ❑ Issue an Attachment B Certification from the RO.* * Remember that you will be responsible for coordinating site visits and reviews, as well as additional information requests with other RO-APS representatives in order to prepare a complete Attachment B for certification. Refer to the RPP SOP for additional detail. When you receive this request form, please write yourname and dates in the spaces below, make a copy of this sheet, and return it to the appropriate Central Office -Aquifer Protection Section contact person listed above. , Date: .: '1 ! � LC . FORM: APSARR 07/06 Page 1 of 1 NON -DISCHARGE REGIONAL WATER QUALITY STAFF REPORT AND RECOMMENDATIONS Date: April 16, 2009 To: Non -Discharge Permitting Unit NDPU Reviewer: David Goodrich County: Iredell Permitee: City of Statesville Application No.: W00014543 GENERAL INFORMATION 1. This application is (check all that apply): ❑ New Renewal ❑ Minor Modification ❑ Major Modification n Surface Irrigation ❑ Reuse ❑ Recycle ❑ High Rate Infiltration ❑ Evaporation/Infiltration Lagoon ® Land Application of Residuals ❑ Attachment 3B included as appropriate ® 503 regulated ❑ 503 exempt ❑ Distribution of Residuals ❑ Surface Disposal 2. Was a site visit conducted in order to prepare this report? ❑ Yes or ® No. a. Date(s) of site visit(s): N/A b. Person contacted and contact information: Scott Berg. 336/998-7150 ext. 13 c. Site visit conducted by: N/A d. Inspection report attached: ❑ Yes or ® No. e. A review of all the new and modified sites was conducted. 3. Is the following information entered into the BIMS record for this application correct? ® Yes or❑No. For Treatment Facilities: a. Location: 4th Creek WWTP and 3rd Creek WWTP info in BIMS is correct. b. Driving Directions: c. USGS Quadrangle Map name and number: d. Latitude: Longitude: e. Regulated Activities / Type of Wastes (e.g., subdivision, food processing, municipal wastewater): Municipal wastewater For Disposal Sites: This field is located at the 4th Creek WWTP a. Location(s): 693 Bell Farm Road,Statesville, NC b. Driving Directions: c. USGS Quadrangle Map name and number: d. Latitude: Longitude: FORM: NDSRR 03/02 1 Permit renewal City of Statesville September 9, 2009 DESCRIPTION OF WASTE(S) AND FACILITIES 1. Are there appropriately certified ORCs for the facilities? ® Yes or ❑ No. Operator in Charge: Andy Smith Certificate #: LA 985516 Back- Operator in Charge: Scott Austin Certificate #: LA-991939 2. Is the design, maintenance and operation (e.g. adequate aeration, sludge wasting, sludge storage, effluent storage, etc) of the treatment facilities adequate for the type of waste and disposal system? Yes or ❑ No. If no, please explain: 3. Are the site conditions (soils, topography, etc) maintained appropriately and adequately assimilating the waste? ® Yes or ❑ No. If no, please explain: 4. Is the residuals management plan for the facility adequate and/or acceptable to the Division? Yes or ❑ No. If no, please explain: 6. 7. Is the type and/or volume of waste(s) as written in the existing permit correct? /1 Yes or ❑ No. If no, please explain: 8. Is the description of the facilities as written in the existing permit correct? ® Yes or ❑ No. If no, please explain: 9. Has a review of all self monitoring data been conducted? ® Yes or ❑ No. Please summarize any findings resulting from this review: The annual report reflects compliance. 10. Check all that apply: ►1 No compliance issues; n Notice(s) of violation within the last permit cycle; 5. Are the existing application rates (hydraulic or nutrient) still acceptable? /1 Yes or ❑ No. If no, please explain: Are there any buffer conflicts (treatment facilities or disposal sites)? ❑ Yes or ® No f Current enforcement action(s) ❑ Currently under SOC; n Currently under JOC; ❑ Currently under moratorium. If any items checked, please explain and attach any documents that may help clarify answer/comments (such as NOV, NOD etc): 11. Have all compliance dates/conditions in the existing permit, SOC, JOC, etc. been complied with? ❑ Yes or ❑ No. N/A 12. Are there any issues related to compliance/enforcement that should be resolved before issuing this permit? ❑ Yes or ❑ No. N/A FORM: NDSRR 03/02 2 EVALUATION AND RECOMMENDATIONS I. Provide any additional narrative regarding your review of the application.: This permit is for emergency use only. This permit is basically and insurance policy for the City in the event of a need to change contractors. the City has a permit in place to add or transfer fields to.. The land already permitted for this sludge source is in SYNAGRO's name. 2. List any items that you would like NDPU to obtain through an additional information request. Make sure that you provide a reason for each item: NIA 3. List specific Permit conditions that you recommend to be removed from the permit when issued. Make sure that you provide a reason for each condition: N/A 4. List specific special conditions or compliance schedules that you recommend to be included in the permit when issued. Make sure that you provide a reason for each special condition: N/A 5. Recommendation: ❑ Hold, pending receipt and review of additional information by regional office; n Hold, pending review of draft permit by regional office; ® Issue; n Deny. If deny, please state reasons: 6. Signature of report preparer: Signature of WQS regional supervisor: Date: r+r -O ADDITIONAL REGIONAL STAFF REVIEW ITEMS No additional items. FORM: NDSRR 03/02 3 Permit Number WQ0014543 Central Files: APS SWP 08/31/09 Permit Tracking Slip Program Category Non -discharge Permit Type Land Application of Residual Solids (503) Primary Reviewer david.goodrich Coastal SW Rule Permitted Flow Facility Status Project Type In review Renewal Version A Permit Classification Individual Permit Contact Affiliation Lenwood F. Hudson Jr. PO Box 1111 Statesville NC 286871111 Facility Name Major/Minor Region City of Statesville Residuals Land Application Minor Mooresville Program Location Address County PO Box 1111 Iredell Statesville Owner NC 286871111 Facility Contact Affiliation Owner Name Owner Type City of Statesville Government - Municipal Owner Affiliation Robert W. Hites Jr. PO Box 1111 Statesville Dates/Events NC 286871111 Orig Issue App Received Draft Initiated 02/17/98 08/05/09 Scheduled Issuance Public Notice Issue Regulated Activities Requested/Received Events Wastewater treatment and disposal Outfall NULL RO staff report requested RO staff report received Effective Expiration Waterbody Name Stream Index Number Current Class Subbasin 4 North Carolina Department of Environment and Natural Resources Beverly Eaves Perdue Governor Division of Water Quality Coleen H. Sullins Director August 31, 2009 Joe Hudson, Water Resources Director City of Statesville P.O. Box 1111 Statesville. NC 28687-1111 Subject: Acknowledgement of Application No. WQ0014543 City of Statesville Residuals Land Application Program Land Application of Residual Solids (503) Iredell Dear Mr. Hudson: SEP Dee Freeman Secretary an 2 2009 C DFNR MR0 DWQ _ A uifer Protection The Aquifer Protection Section of the Division of Water Quality (Division) acknowledges receipt of your permit application and supporting materials on August 5, 2009. This application package has been assigned the number listed above and will be reviewed by David Goodrich. The reviewer will perform a detailed review and contact you with a request for additional information if necessary. To ensure the maximum efficiency in processing permit applications, the Division requests your assistance in providing a timely and complete response to any additional information requests. Please be aware that the Division's Regional Office, copied below, must provide recommendations prior to final action by the Division. Please also note at this time, processing permit applications can take as long as 60 - 90 days after receipt of a complete application. If you have any questions, please contact David Goodrich at 919-715-6162, or via e-mail at david.goodrich@ncdenr.gov. If the reviewer is unavailable, you may leave a message, and they will respond promptly. Also note that the Division has reorganized. To review our new organizational chart, go to http://h2o.enr.state.nc.us/documents/dwq orgchart.pdf. PLEASE REFER TO THE ABOVE APPLICATION NUMBER WHEN MAKING INQUIRIES ON THIS PROJECT. for Jon Risgaard LAU Supervisor cc:Mooresyille Regtonalquifer 2rotect>on Secion Andy Smith, Creek WWTP Supervisor (City of Statesville) Permit Application File WQ0014543 AQUIFER PROTECTION SECTION 1636 Mail Service Center, Raleigh, North Carolina 27699-1636 Location: 2728 Capital Boulevard, Raleigh, North Carolina 27604 Phone: 919-733-3221 ! FAX 1: 919-715-0588 FAX 2: 919-715-6048 \ Customer Service: 1-877-623-6748 Internet: www.ncwaterquality.org An Equal Opportunity \ Affirmative Action Employer NNlonAhCarolina Tat rai/ ias '� #'tatr� uillz 13. ®. +.Jux 1111 s 'tatesuille. Nurtll Tarulina 28687 RECEIVED I DEoN section Aquifer . AIJ Cz 5 2009 July 22, 2009 Mr. Ed Hardee Central Office 1636 Mail Service Center Raleigh, NC 27699-1636 Re: Permit # WQ0014543 City Land Application Permit Renewal Application and Attachments Forms NDRLAP, RSCA, & LASCA Dear Mr. Hardee: NC DFNR MRO D - A. •uifer Protection Enclosed, you will find the forms, information and the required attachments per the instructions for the application. As noted in previous permit applications, this permit has never been used since its inception. The N Vro process is the primary biosolids program for the 4th Creek WIMP. We have a contract with Synagro to land apply dry cake biosolids from the 3"' Creek and 4th Creek WWTP's with the understanding that this would be the secondary biosolids program. The permit that is associated with the Synagro contract is in their name and they take care of all of the monitoring and general conditions for that specific permit. Should you require more information, or if further action is required, please contact me at 704- 878- 3438. Sinrel l Fourth WWTP Supervisor State of North Carolina Department of Environment and Natural Re ivision of Water Quality ih NON-IEDICATED RESI UAL S LAND APPLICAT (FORM: NDRLAP 070807) The Division of Water Quality will not accept this application unless all the instructions are followed. Failure to submit all of the required items will lead to additional processing and review time. For more information, visit our web site at: Info: 172o. e nr.star•_ . nc. us luu main. hnml eesSEP - 2 2009 NC DENT- iVIRO ft r. otection A. Application Form: (All Application Packages): ✓ Submit one original and two copies of the completed application package. Any changes made to this form will result in the application being returned. The Division of Water Quality will only accept application packages that have been fully completed and all applicable items are addressed. ✓ Non -dedicated residuals land application programs are ones in which all land application sites do not meet the criteria in 15A NCAC 2T .1102(12). Specifically, a residuals land application program cannot be designated as non -dedicated if any of the following is applicable: • Any land application site certified for the residuals land application program that receives residuals at rates or frequencies greater than agronomic rates. • Any land application site certified for the residuals land application program that is used primarily for residuals disposal, and agricultural crop production is of secondary importance. a Any land application site certified for the residuals land application program that receives residuals through fixed irrigation facilities or irrigation facilities fed through a fixed supply system. ✓ The signing official must meet the criteria stipulated in 15A NCAC 2T .0106(b). An alternate person may be designated as the signing official, provided that a delegation letter from a person who meets the referenced criteria is submitted. The delegation letter does not have to be resubmit(ed if the signing official has not changed since the last permitting action associated with this residuals land application program. • If this project involves a modification of an existing permit, submit one copy of the existing permit. ✓ Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to operation of proposed facility (ies) for application packages involving new or changes to treatment and storage units. 13. Application Fee (New and Major Modification Application Packages): ✓ For new permits submit a check in the amount of $I,310 if over or equal to 300 acres of land are being permitted for application (Major Permit), or $810 if less than 300 acres of land are being permitted for application (Minor Permit), made payable to: North Carolina Depai tment of Environment and Natural Resources (NCDENR). Major modification fee are $395 and $245, respectively. C. Cover Letter (Ail Application Packages) ✓ Submit a cover letter, which lists all items and attachments included in the application package as well as a brief project description. ✓ If necessary for clarity, include attachments to the application form. Such attachments will be considered part of the application package and should be numbered to correspond to the section to which they refer. D. Environmental Assessments (May be Required — See 15A NCAC IC .0300): ✓ Submit one copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for the construction of the subject facilities. Submission of Application Packages: ✓ To determine which attachment forms and supplemental attachments are required to make a complete application package, read the instructions of each attachment form carefully. Application packages should be organized and bound (i.e., stapled, placed in three-ring binder, etc.) in the following order prior to submission: • Cover letter and application fee. • Attachment Order 1: Non -Dedicated Residuals Land Application Programs (FORM: NDRLAP). > Attachment Order 1-a: Signing official delegation letter. • Attachment Order 2: Residuals Source Certification Attachment (FORM: RSCA). • Attachment Order 3: Land Application Site Certification Attachment (FORM: LASCA). ✓ The application package should be sent to the address at the end of this application form. Do not submit this application package to any Division regional office. r. FORM: NDRLAP 070807 Page 1 of 6 Attachment Order 1 RECENED I DENRI D oC1 Mau.- Protect,on S State of North Carolina F,111 /) 5 2009 Department of Environment and Natural Resources Divisions of Water Quality NON -DEDICATED RESIDUALS LAND APPLICATION PROGRAMS (FORM: NDRLAP 070807) (THIS FORM MAYBE PHOTOCOPIED FOR USE AS AN ORIGINAL) Application Number: (tq,_b V �r� Lle''Ite�d-byWQ I. OWNERSHIP INFORMATION: Tyc 1. Specify whether the process facility is owned by: ❑ County; ❑ Federal; X Municipal; ❑ State; ❑ Non -Government. 2. Owner's name (please specify the name of the municipality, corporation, individual, e City of Statesville Mailing address: PO Box 1111 City: Statesville Physical address: 693 Bell Farm Road City: Statesville S EP - 2 2009 NC DENR MRO DVVQ - A Iiifer Protection State: NC Zip: 28687-1111 State: NC Zip: 28677 Telephone number: ( 704) 878-3438 Facsimile number: ( 704) 878-8655 E-mail address: asnrith0,:statesvillenc.net 3. Signing official's name and title: (See Instruction A) Joe Hudson, Water Resources Director Mailing address: P.O. Box 1111 City: Statesville Physical address: 693 Bell Farm Road City: Statesville State: NC Zip: 28687-1111 State: NC Zip: 28677 Telephone number: ( 704) 704-878-3438 Facsimile number: ( 704) 878-8655 E-mail address: jhuclsoii rstatesvillenc.net H. PERMIT INFORMATION: 1. Application is for: ❑ new, ❑ modified, XEI renewed permit (check all that apply). 2. Fee Submitted: $ 810.00 (See Instruction B) 3. If this application is being submitted to renew or modify an existing permit, provide the following: Permit number WQ001453 Most recent issuance date March 11, 2005, and the expiration date February 28, 2010. Date of most -recently certified Attachment A: Date of most -recently certified Attachment B: FORM: NDRLAP 070807 Page 2 of 6 Attachment Order 1 4. Check all that apply to the requested permit modification: ❑ INCREASE 0 DECREASE the maximum permitted annual dry tonnage for existing residuals source -generating facility (ies) certified. ❑ ADD ❑ DELETE residuals source -generating facility (ies) to/from those certified. O INCREASE ❑ DECREASE the acreage associated with land applications site(s). ❑ ADD 0 DELETE land application site(s) to/from those certified. O OTHER. Explain: III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION: 1. County where residuals land application program is headquartered: Iredell County 2. County(ies) where residuals source -generating facilities are located: Iredell County 3. County(ies) where land application sites are located: Iredell County 4. Program contact person and/or consulting firm who prepared application: Andv Smith, 4th Creek WWTP Supervisor Mailing address: PO Box 1111 City: Statesville State: NC Zip: 28687-1111 Physical address: 693 Bell Farm Road City: Statesville State: NC Zip: 28677 Telephone number: (704) 878-3438 Facsimile number: ( 704 ) 878-8655 E-mail address: asmit/Tr�i stnlesrNlenc. net 5. Who will be responsible for the day-to-day management of the residuals land application program: X Permittee or ❑ residuals management firm. If a residuals management firm, complete the following: Firm contact person and title: Firm name: Mailing address: City: State: Zip: Telephone number: ( ) Facsimile number: ( ) E-mail address: FORM: NDRLAP 070807 Page 3 of 6 Attachment Order 1 6. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application program, their certification numbers, and their affiliations in the following table: Designation Name Affiliation Certification Number ORC Andy Smith City of Statesville LA 985516 Back -Up ORC - Soul Austin City of Statesville LA 991939 Additional Back -Up ORCs (if applicable) If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application program, provide the candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training school and certification test: 7. Complete the following tables regarding management of the residuals land application program: a. Plant Available Nitrogen Summary: Determine the maximum plant available nitrogen (PAN) generated by all residuals source -generating facilities as currently certified and proposed for certification with this application and list the results in the following table: Maximum amount of residuals to be certified: 4th Creek-1,056/ 3`d Creek- 973 dry tons per year. PAN Pounds of PAN per Dry Ton (Weighted Average) Pounds of PAN per Year Surface Incorporation or Injection Surface Incorporation or Injection First -Year 4rh-3.9/3'd-4.0 m /3( d 4 3,882 Five-Year Maximum Adjusted 19.5/19.95 20586/19409 b. Land Application Site Use Summary: Summarize information regarding the land application sites as currently certified and proposed for certification with this application: Category Use Acres Comments Crops Forest or Plantation Row Crops 15.3 Corn and small grain. (4`h Creek) Hay 14.1 Fescue Hay (3' 1 Creek ) Pasture Total: 29.4 Methods Surface 29.4 Incorporation or Injection Total: 29.4 Restrictions Year -Round Double cropped (spring &fall ) Seasonal 29.4 land crop not to exceed 50 lbs/ac/yr FORM: NDRLAP 070807 Page 4 of 6 Attachment Order 1 Total: c. Residuals Land Application Summary: Determine the minimum acreage required to land apply the residuals as currently certified and proposed for certification assuming the scenarios listed in the following table: Assumed App.icatio i Rate (lbs PAN/ac-yr) Acres Required Using First -Year PAN Concentrations Acres Required Using Five -Year Maximum Adjusted :'AN ' Concentrations Surface Incorporation or Injection Surface Incorporation or Injection 50 4th 82.34/3rd 77.64 41h 411.7/3rd 388.2 100 4th 41.17/3'd 38.82 4th 205.85/3` 1194 150 41h 274/3'125.88 41h 137/3r1129.4 200 4th 20.58/3`a 19.41 4th 102.9/ 3rd 97 8. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application of the proposed residuals due to the violation of North Carolina Administrative Code (e.g. not enough storage, not enough land, vector reduction practices not in place, etc.) ***FORM: NDRLAP CONTINUES ON NEXT PAGE*** FORM: NDRLAP 070807 Page 5 of 6 Attachment Order 1 RECEIVED / DENR / DWQ Aquifer Protection Section AUG 0 5 2009 Applicant's Certification: The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under Rule 2T .0105. s ❑ No, Explain; I, attest that this application for /g%Ojj . leoc/ 74e0f ji&-5# i44et if .4ope,G Q � �l�'dpy /' ,-0d has been reviewed by me and is accurate and complete to the beat' f myknowledg e. and tand that the Division of Water Quality may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Quality should a condition of this permit be violated. I also understand that if all required parts of this application are not completed and that if all required supporting information and attachments are not included, this application package will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes §143-215.6A and §143-215.6B, any person who knowingly makes any false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to exceed $10,000 as well as civil penalties up to $25,000 per violation. Signature: Date: THE COMPLETED APPLICATI s N PACKAGE, INCLUDING ALL SUPPORTING INFORMATION AND MATERIALS, SHOULD BE SENT TO THE FOLLOWING ADDRESS: NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER QUALITY AQUIFER PROTECTION SECTION LAND APPLICATION UNIT By U.S. Postal Service: 1636 MAIL SERVICE CENTER RALEIGH, NORTH CAROLINA 27699-1636 By Courier/Special Delivery: 2728 CAPITAL BOULEVARD RALEIGH, NORTH CAROLINA 27604 TELEPHONE NUMBER: (919) 733-3221 FORM: NDRLAP 070807 Page 6 of 6 Attachment Order 1 State of North Carolina epartment of Environment and Natural Resour MIECIEHE SEP - 2 2009 SEP 2 2009 Division of Water Quality L---- NC DENR MFR0 RESIDUALS SOURCE CERTIFICATION ATTACIAV� Aauiinr protection (FORM: RSCA 070807) (THIS FORM MAYBE PHOTOCOPIED FOR USE AS AN ORIGINAL) The Division of Water Quality (Division) will not accept this attachment unless all the instructions are followed. Failure to submit all required items will lead to additional processing and review time. For more information, visit our web site at: htlp://h2o.enr•.state.nc.rrs/Inrumain.htnrl INSTRUCTIONS TO THE APPLICANT: 4" Creek WillTP A. Attachment Form: ✓ Do not submit this attachment form for review without a corresponding residuals program application form (FORM: NDRLAP, FORM: DRS, or FORM: SDRS). ✓ Any changes to this attachment form will result in the application package being returned. ✓ For new residuals programs or renewed residuals programs, submit a separate attachment form for each residuals source -generating facility to be certified for this residuals program. ✓ For modified residuals programs in which any modification to the certified residuals -source generating facilities is proposed, submit a separate attachment form for only those residuals source -generating facilities that are affected by the proposed modification. ✓ The attachment should be organized prior to submission in the following order (i.e., by facility): o Attachment Order 2: Residuals Source Certification Attachment (FORM: RSCA). > Attachment Order 2-a: Vicinity map. > Attachment Order 2-b: Process flow diagram and/or narrative. > Attachment Order 2-c: Quantitative justification for residuals production rate. > Attachment Order 2-d: Sampling plan. > Attachment Order 2-e: Laboratory analytical reports and operational data. B. Residuals Source -Generating Facility Information: ✓ Attach a vicinity map that shows the location of the facility and meets all of the criteria in the latest version of the document entitled "Guidance for the Preparation of Vicinity/Buffer Maps for North Carolina Residuals Permitting Programs." ✓ Attach a detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. ✓ Attach a quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. C. Residuals Quality Information: ✓ Attach a detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. ✓ Attach reports for all laboratory analyses used to complete this attachment form. Attach documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ✓ Item II. 3. Does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only. FORM: RSCA 070807 Page 1 of 8 Attachment Order 2 State of North Carolina Department of E.rvironment and Natural Resources Division of Water Quality RECEIVED / DENR / DWQ Aquifer Protection Section AUG 0 5 2009 RESIDUALS SOURCE CERTIFICATION ATTAC! I F (FORM: RSCA 070807) (THIS FORM MAY BE PHOTOCOPIED FOR USE AS AN ORIGINAL; —1 SEP — 2 2009 Applicant's name: City of Statesville/ -!th Creel, 11 II "TP Check all that apply: ❑ INCREASE lJ V p} NCC DENR MRO ID NEW RESIDUALS PROGRAM X RENEWED RESIDLj -I'1 ! Asuifer Protection ❑ DECREASE the maximum permitted annual dry tonnage for this residuals generating facility certified for this residuals program. Current: 1,057 Dry Tons/yr. and proposed: 1,057 Dry Tons/yr. source- ❑ ADD ❑ DELETE this residuals source -generating facility to/from those certified for this residuals program. ❑ OTHER Explain: I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Name of facility: 4`h Creek WWTP 2. Facility permit holder: City of Statesville Facility permit holder is (check one): ❑ federal, ❑ state, X local government, or ❑ private. Facility permit number: NC0031836 Facility permit issued by (check one): X Div. of Water Quality, ❑ Div. of Environmental Health, or ❑ other (explain: ). 3. If the facility permit is not issued by the Div. of Water Quality, complete the following: a. Facility contact person and title: Facility complete mailing address: City: State: Zip: Telephone number: ( ) Facsimile number: ( ) E-mail address: b. Facility complete location address: City: State: Zip: Latitude: and longitude: 4. County where facility is located: Iredell 5. Purpose of the facility (check one): ❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater, ❑ treatment of potable water, ❑ treatment of 100% industrial wastewater, X treatment of industrial wastewater mixed with domestic wastewater, or (approximate percentages: 40 % industrial and 60 % domestic) ❑ other (explain: FORM: RSCA 070807 Page 2 of 8 Attachment Order 2 6. Does the facility have an approved pretreatment program: X yes ❑ no 7. Facility permitted/design flow: 6 MGD and facility average daily flow: 3 MGD. 8. Average amount of residuals being generated at this facility dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: 1.5 Million Gallon aerobic digester. 3 meter, 3 belt press. Dewatering polymer. Type and volume of residuals storage (i.e., outside of residuals treatment units): 1/3 acre concrete pad. II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under (check one): ❑ 40 CFR Part 503 or ❑ 40 CFR Part 257. 2. Specify if residuals are intended for (check one): ❑ Land Application/Distribution (Class A or Equivalent). Complete all items EXCEPT Items II. 4b. 7b. and 7c. X Land Application (Class B or Equivalent). Complete all items EXCEPT Items II. 4b. 7a. and 7c. ❑ Surface Disposal. Complete all items EXCEPT Items II. 4a. 5. 7a., 7b., and 8. ***FORM: RSCA CONTINUES ON NEXT PAGE*** FORM: RSCA 070807 Page 3 of 8 Attachment Order 2 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non- hazardous under RCRA: a. Are the residuals are listed in 40 CFR §261.31-§261.33: ❑ yes X no. If yes, List the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- §261.24: ❑ yes X no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: laboratory: Prism Laboratory and date of analysis: 7/28/08 Passed corrosivity test: X yes ❑ no. pH: s.u. (2 < pH < 12.5). Passed ignitability test: X yes ❑ no. Flashpoint: °F (> 140°F). Passed reactivity test: X yes ❑ no. HCN: mg/kg (<250) & H2S: mg/kg (<500). TCLP Parameter Limit (mg/L) Result (mg/L) TCLP Parameter Limit (mg/L) Result (mg/L) Arsenic 5.0 <0.050 Hexachlorobenzene 0.13 <0.010 Barium 100.0 <5.0 Hexachloro-1,3- Rntadiene 0.5 <0.050 Benzene 0.5 <0.050 Hexachloroethane 3.0 <0.050 Cadmium 1.0 <0.025 Lead 5.0 <0.050 Carbon Tetrachloride 0.5 <0.050 Lindane 0.4 <0.0005 Chlordane 0.03 <0.025 Mercury 0.2 <0.010 Chlorobenzene 100.0 <0.050 Methoxychlor 10.0 <0.0005 Chloroform 6.0 <0.050 Methyl Ethyl Ketone 200.0 <0.50 Chromium 5.0 <0.25 Nitrobenzene 2.0 <0.050 m-Cresol 200.0 Pentachlorophenol 100.0 <0.25 o-Cresol 200.0 Pyridine 5.0 <0.25 p-Cresol 200.0 Selenium 1.0 <0.050 Cresol 200.0 Silver 5.0 <0.25 2,4-D 10.0 ND Tetrachloroethylene 0.7 <0.050 1,4-Dichlorobenzene 7.5 <0.050 Toxaphene 0.5 <0.025 1,2-Dichloroethane 0.5 <0.050 Trichloroethylene 0.5 <0.050 1,1-Dichloroethylene 0.7 <0.050 2,4,5-Trichlorophenol 400.0 <0.25 2,4-Dinitrotoluene 0.13 <0.012 2,4,6-Trichlorophenol 2.0 <0.10 Endrin 0.02 <0.0005 2,4,5-TP (Silvex) 1.0 0.00500 Heptachlor and its Hydroxide 0.008 <0.0005 Vinyl Chloride 0.2 <0.020 FORM: RSCA 070807 Page 4 of 8 Attachment Order 2 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Class A or Class B: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: and date of analysis: Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (ForClass A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 Cadmium 85 39 Copper 4,300 1,500 No Residuals Lead 840 300 have been applied. Mercury 57 17 Molybdenum 75 n/a Nickel 420 420 Selenium 100 100 Zinc 7,500 2,800 b. For Surface Disposal: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: and date of analysis: Closest Distance to Property Lines (meters) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) > 0 but < 25 30 200 210 >_ 25 but < 50 34 220 240 >_ 50 but < 75 39 260 270 > 75 but < 100 46 300 320 > 100 but < 125 53 360 390 > 125 but < 150 62 450 420 >_ 150 73 600 420 FORM: RSCA 070807 Page 5 of 8 Attachment Order 2 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 19 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: laboratory: 4`" Creek WWTP Laboratory and date of analysis: Ongoing weekly. Parameter Result (mg/kg, dry weight) Aluminum Ammonia -Nitrogen Calcium No residuals have been applied Magnesium Nitrate -Nitrite Nitrogen pH (Standard Unit) Phosphorus Potassium Sodium Total Kjeldahl Nitrogen c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This rate is a ❑ default value or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: Calculate the PAN for the residuals (i.e., on a dry weight basis) and list the results in the following table: Application Method First Year PAN (mg/kg) Five -Year Maximum Adjusted PAN (mg/kg) Surface 3.9 19.5 Injection/Incorporation e. Are the residuals a registered fertilizer with the NC Department of Agriculture and Consumer Services: ❑ yes X no. If yes, provide date of registration approval: the current registration number: and the fertilizer equivalent: FORM: RSCA 070807 %, %, and Page 6 of 8 %. Attachment Order 2 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and list the results of the latest analyses: 7. Pathogen Reduction Determi ratio a: Specify which alternative(s) will be used to meet the pathogen reduction requirements: a. For Class A or Equivalent: ❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids. OR ❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the following (except for residuals regulated under 40 CFR Part 257 that are to be distributed): ❑ Alternative 1 [40 CFR §503.32 (a)(3)] - Time/Temperature Compliance. ❑ Alternative 2 [40 CFR §503.32 (a)(4)] - Alkaline Treatment. ❑ Alternative 3 [40 CFR §503.32 (a)(5)] - Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 4 [40 CFR §503.32 (a)(6)] - No Prior Testing for Enteric VirusNiable Helminth Ova. ❑ Alternative 5 [40 CFR §503.32 (a)(7)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment, ❑ pasteurization, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, or ❑ gamma ray irradiation. ❑ Alternative 6 [40 CFR §503.32 (a)(8)] - PFRP-Equivalent Process. Explain: b. For Class B or Equivalent: X Alternative 1 [40 CFR §503.32 (b)(2)] - Fecal Coliform Density Demonstration. ❑ Alternative 2 [40 CFR §503.32 (b)(3)] - Process to Significantly Reduce Pathogens (PFRP). Specify one: X aerobic digestion, ❑ air drying, ❑ anaerobic digestion, ❑ composting, or ❑ lime stabilization. ❑ Alternative 3 [40 CFR §503.32 (b)(4)] - PSRP-Equivalent Process. Explain: ❑ Not Applicable - Regulated under 40 CFR Part 257 with NO Domestic Wastewater Contribution. c. For Surface Disposal: ❑ Alternative for Surface Disposal Units Only [40 CFR §503.33 (b)(11)] - Soil/Other Material Cover. ❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. ❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. ❑ Not Applicable - Regulated under 40 CFR Part 257 with NO Domestic Wastewater Contribution. FORM: RSCA 070807 Page 7 of 8 Attachment Order 2 8. Vector Attraction Reduction Determination: Specify which alternative(s) will be used to meet the vector attraction reduction requirements: ❑ Alternative 1 [40 CFR §503.33 (b)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [40 CFR §503.33 (b)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). ❑ Alternative 3 [40 CFR §503.33 (b)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 [40 CFR §503.33 (b)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). X Alternative 5 [40 CFR §503.33 (b)(5)] - 14-Day Aerobic Processes. ❑ Alternative 6 [40 CFR §503.33 (b)(6)] - Alkaline Stabilization. ❑ Alternative 7 [40 CFR §503.33 (b)(7)] - Drying of Stabilized Residuals. ❑ Alternative 8 [40 CFR §503.33 (b)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [40 CFR §503.33 (b)(9)] - Injection. ❑ Alternative 10 [40 CFR §503.33 (b)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only [40 CFR §503.33 (b)(11)] - Soil/Other Material Cover. ❑ Alternatives for Animal Processing Residuals Only: Specify one: ❑ injection, ❑ incorporation, or ❑ lime addition to raise pH to 10. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. FORM: RSCA 070807 Page 8 of 8 Attachment Order 2 scNoi 0( `Illy cred WurP � ATTACHMENT 2b 4th CREEK & 3rd CREEK WIN R NARRATIVE Both of the WWTP's utilize a conventional activated sludge process that primarily treats domestic and industrial waste water generated from areas within and outside of the city. The raw sewage enters the WWTP via gravity main and from there it flows into a wet well or pump station. The flow enters one of two perforated panel type bar screens. At this point the raw sewage is mixed with return activated sludge and distributed into two aeration basins. The mixed liquor flows into secondary clarifiers . and then the RAS is pumped back into the influent of the WWTP. The effluent gravity flows from the secondary clarifiers to the chlorine contact basins where the final effluent is treated with Sodium Bisulfite for de -chlorination as it flows to the receiving stream. Both WWTP's generate biosolids that are currently stabilized using an aerobic digester, and dewatered using a belt press. After dewatering, the residuals are transferred to the N-Viro lime stabilization process area where the biosolids are set aside for contract land application off of the plant site. The primary method of biosolids disposal is the N-Viro process. 9 PLANT INFLUENT o MH BAR SCREENS INFLUENT PUMP STATION DECHLORINATION BUILDING CLARIFIERS ❑ 0-- AERATION BASIN NO. 'I AERATORS * FLOW DISTRIBUTION BOX METERING FLUME EFFLUENT M.- FLOW SPLITTER BOX WAS —❑ ❑ AERATION BASIN ❑ ❑ NO. 2 AERATORS L — STALIME SLUDGE TREATMENT FACILITIES CONVEYOR SLUDGE PUMPS COVERED SLUDGE STORAGE SLUDGE STORAGE PAD FLOW SCHEMATIC & WATER BALANCE FOURTH CREEK WASTEWATER TREATMENT PLANT CITY OF STATESVILLE tLit of ftt#eSltiilE . (4). lax 1111 tateout11e, Wurt11 Carolina 28687 July 21, 2009 Mr. Ed Hardee Central Office 1636 Mail Service Center Raleigh, NC 27699-1636 Re: Permit # WO0014543 , `u&a a Quantitative Justification for Residuals Production Rate f�1} Fourth Creek WWTP Dear Mr. Hardee: The 4th Creek WWTP would generate approximately 2,000 dry tons per year of biosolids. This would all go to the N-Viro process and /or the contracted Land Application contractor unless extenuating circumstances prevailed. Should you require more information, or if further action is required, please contact me at 878-3438. Sincerel r Forth C k WWTP Supervisor Eit of 'tatzo utile . ().'Snx 1111 ° 'tat£Suille, Nardi (Carolina 28687 July 21, 2009 Mr. Ed Hardee Central Office 1636 Mail Service Center Raleigh, NC 27699-1636 Re: Permit # WQ0014543 J-KAN .t,02 d- Biosolids Sampling Plan Fourth Creek WWTP Dear Mr. Hardee: The 46' Creek WWTP is currently using a 3 belt sludge press that pumps sludge out to the N-Viro process. As the press is operating, the operator would collect the required amount of sample per the permit to send to the designated lab. Should you require more information, or if further action is required, please contact me at 878-3438. Sincer y, /1(2114 Fourth reek WWTP Supervisor Full Service Awe & Environmental Solutions City of Statesville Attn: Mr. Andy Smith P.O. Box 1111 Statesville, NC 28687 NC Certification No. 402 SC Certification No. 99012 NC Drinking Water Cert. No. 37735 Project ID: Sta-Lime, 3rd Creek and 4th Creek Sludge with TCLP Sample Matrix: Solid Parameter Laboratory Report 08/14/08 Client Sample ID: Prism Sample ID: COG Group: Time Collected: Time Submitted: 4TH Creek Sludge 220582 G0708776 07/28/08 11:30 07/28/08 15:35 Result Units Report MDL Dilution Limit Factor pH, Corrosivity pH Ignitability of Solids Ignitability Reactive Cyanide Subcontract Report Method Analysis DateiTime Analyst Batch ID 6.9 pH units 0.10 0.10 1 Negative N/A See Attached * Analysis Note for Subcontract Report: 9045C 08/01/08 11:46 kpowers Q34366 1030 07/30/08 14:40 rloftin Q34306 See Attached Subcontracted to NC Certified Lab 618. Reactive Sulfide Subcontract Report See 1 See Attached Attached * Analysis Note for Subcontract Report: Subcontracted to NC Certified Lab 618. TCLP Extraction for Metals and/or Non -Volatile Organics TCLP Extraction (Metals/Organics) Complete Zero Headspace Extraction for Volatiles TCLP Extraction (ZHE-Volatiles) Complete Acid Herbicicides in TCLP Leacheate by GC-ECD Subcontract Report See Attached * Analysis Note for Subcontract Report: TCLP Leachable Mercury by CVAA Mercury Sample Preparation: TCLP Leachable Metals by ICP Arsenic Barium Cadmium BRL 1 1311 08/05/08 11:30 mbarber 1 1311 08/11/08 17:00 wconder Subcontracted to NC mg/L 0.010 0.000014 1 BRL mg/L BRL mg/L BRL mg/L 0.050 5.0 0.025 20 mL / 30 mL 0.0029 0.0019 0.00034 8151A Certified Lab 618. 7470A 08/08/08 18:07 mcampbell Q34590 7470A 08/08/08 9:30 mbarber P27775 6010B 08/07/08 1:47 mcampbell Q34496 6010E 08/07/08 1:47 mcampbell Q34496 601013 08/07/08 1:47 mcampbell Q34496 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page of12 Full Service Anatytiul & Environmental Solutions City of Statesville Attn: Mr. Andy Smith P.O. Box 1111 Statesville, NC 28687 NC Certification No. 402 SC Certification No. 99012 NC Drinking Water Cert. No. 37735 Project ID: Sta-Lime, 3rd Creek and 4th Creek Sludge with TCLP Sample Matrix: Solid Laboratory Report 08/14/08 Client Sample ID: Prism Sample ID: COC Group: Time Collected: Time Submitted: 4TH Creek Sludge 220582 G0708776 07/28/08 11:30 07/28/08 15:35 Parameter Chromium Lead Selenium Silver Result Units Report MDL Dilution Method Limit Factor Analysis Date/Time Analyst Batch ID Sample Preparation: BRL mg/L 0.25 0.0006 1 BRL mg/L 0.050 0.0021 1 BRL mg/L 0.050 0.0035 1 BRL mg/L 0.25 0.00025 1 TCLP Leachable Organochlorine Pesticides by GCIECD Chlordane Endrin Heptachlor Heptachlor Epoxide Lindane Methoxychlor Toxaphene Sample Preparation: 6010E 6010E 60108 6010B 50 mL / 50 mL 3010A BRL mg/L 0.0025 0.00072 1 BRL mglL 0.0005 0.000041 1 BRL mglL 0.0005 0.000079 1 BRL mg/L 0.0005 0.000044 1 BRL mg/L 0.0005 0.000041 1 BRL mg/L 0.0005 0.000087 1 BRL mg/L 0.025 0.00074 1 TCLP Leachable Semi -volatile Organics by GCI@AS 1,4-Dichlorobenzene 2,4,5-Trichlorophenol 2,4, 6-Trichlorophenol 2,4-Dinitrotoluene 2-Methylphenol 3&4-Methylphenol Hexachlorobenzene Hexachlorobutadiene 8081A 8081A 8081A 8081A 8081A 8081A 8081A 200 mL / 10 mL 3510C Surrogate 08/07/08 1:47 mcampbell 08/07/08 1:47 mcampbell 08/07/08 1:47 mcampbell 08/07/08 1:47 mcampbell 08/06/08 9:40 mbarber 08/07/08 23:25 jvogel 08/07/08 23:25 jvogel 08/07/08 23:25 jvogel 08/07/08 23:25 jvogel 08/07/08 23:25 jvogel 08/07/08 23:25 jvogel 08/07/08 23:25 jvogel 08/07/08 6:00 % Recovery Tetrachloro-m-xylene (TCMX) 98 Decachlorobiphenyl (DCB) 88 Q34496 Q34496 Q34496 034496 P22258 Q34533 Q34533 Q34533 Q34533 Q34533 Q34533 Q34533 smanivanh P22264 Control Limits 40 - 134 13-186 BRL mg/L 0.050 0.0028 1 8270C 08/12/08 8:08 kcampigotto BRL mg/L 0.25 0.0044 1 8270C 08/12/08 8:08 kcampigotto BRL mg/L 0.10 0.0046 1 8270C 08/12/08 8:08 kcampigotto BRL mg/L 0.012 0.0030 1 8270C 08/12/08 8:08 kcampigotto BRL mg/L 0.050 0.0052 1 8270C 08/12/08 8:08 kcampigotto BRL mg/L 0.050 0.0056 1 8270C 08/12/08 8:08 kcampigotto BRL mg/L 0.010 0.0014 1 8270C 08/12/08 8:08 kcampigotto BRL mg/L 0.050 0.0022 1 8270C 08/12/08 8:08 kcampigotto Q34621 Q34621 Q34621 Q34621 Q34621 Q34621 Q34621 Q34621 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 12 Full Service Analytical & EnulronnmNal Solutions City of Statesville Attn: Mr. Andy Smith P.O. Box 1111 Statesville, NC 28687 NC Certification No. 402 SC Certification No. 99012 NC Drinking Water Cert. No. 37735 Project ID: Sample Matrix: Parameter Sta-Lime, 3rd Creek and 4th Creek Sludge with TCLP Solid Laboratory Report 08/14/08 Client Sample ID: Prism Sample ID: COC Group: Time Collected: Time Submitted: 4TH Creek Sludge 220582 G0708776 07/28/08 11:30 07/28/08 15:35 Result Units Report MDL Dilution Method Analysis Analyst Hexachloroethane Nitrobenzene Pentachlorophenol Pyridine BRL mg/L BRL mg/L BRL mg/L BRL mg/L Limit 0.050 0.050 0.25 0.25 Factor 0.0046 1 0.0030 0.0042 0.0036 One surrogate recovery was outside of the control Sample Preparation: TCLP Leachable Volatile Organics by GCIMS 1,1-Dichloroethene 1,2-Dichloroethane 1,4-Dichlorobenzene Benzene Carbon tetrachloride Chlorobenzene Chloroform Methyl ethyl ketone (MEK) Tetrachloroethene Trichloroethene Vinyl chloride BRL mglL 0.050 BRL mg/L 0.050 BRL mg/L 0.050 mg/L 0.050 mglL 0.050 mg/L 0.050 mg/L 0.050 mg/L 0.50 mg/L 0.050 mg/L 0.050 mg/L 0.020 BRL BRL BRL BRL BRL BRL BRL BRL Daterme Batch ID 8270C 08/12/08 8:08 kcampigotto 8270C 08/12/08 8:08 kcampigotto 8270C 08/12/08 8:08 kcampigotto 8270C 08/12/08 8:08 kcampigotto limits. Matrix interference is suspected. Q34621 Q34621 Q34621 Q34621 200 mL / 1 mL 3510C 08/11/08 13:00 smanivanh P22306 Surrogate % Recovery Control Limits Terphenyl-d14 91 41 - 136 Phenol-d5 9 # 10 - 78 Nitrobenzene-d5 52 13 -107 2-Fluorophenol 14 10 - 75 2-Fluorobiphenyl 56 27 -107 2,4,6-Tribromophenol 49 38 -117 0.013 10 0.0021 10 0.0033 10 0.0028 10 0.0012 10 0.00094 10 0.017 10 0.017 10 0.0036 10 0.0033 10 0.011 10 8260B 08/12/08 13:44 erussell 8260B 08/12/08 13:44 erussell 8260E 08/12/08 13:44 erussell 8260E 08/12/08 13:44 erussell 8260E 08/12/08 13:44 erussell 8260E 08/12/08 13:44 erussell 8260E 08/12/08 13:44 erussell 8260B 08/12/08 13:44 erussell 8260E 08/12/08 13:44 erussell 8260B 08/12/08 13:44 erussell 8260E 08/12/08 13:44 erussell Thls report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Q34644 Q34644 Q34644 Q34644 Q34644 Q34644 Q34644 Q34644 Q34644 Q34644 Q34644 Page 3 of 12 Full Service Analytical & Environmental Solutions City of Statesville Attn: Mr. Andy Smith P.O. Box 1111 Statesville, NC 28687 Parameter Sample Comment(s): NC Certification No. 402 SC Certification No. 99012 NC Drinking Water Cert. No. 37735 Project ID: Sta-Lime, 3rd Creek and 4th Creek Sludge with TCLP Sample Matrix: Solid Laboratory Report 08/14/08 Client Sample ID: Prism Sample ID: COC Group: Time Collected: Time Submitted: 4TH Creek Sludge 220582 G0708776 07/28/08 11:30 07/28/08 15:35 Result Units Report MDL Dilution Method Analysis Limit Factor Date/Time Analyst Batch ID Surrogate % Recovery Control Limits Toluene-d8 99 75 -121 Dibromofluoromethane 102 74 -133 Bromofluorobenzene 102 69 - 139 BRL = Below Reporting Limit Values are reported down to the reporting limits only. No J-Nags applied. The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than NELAC certification except for those instances indicated in the case narrative and/or test comments. All results are reported on a wet -weight basis Angela D. Overcash, V.P. Laboratory Services This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number:1-800/529-6364 - Fax: 704/525-0409 Page 4 of 12 GCAL ID a_ Client.ID 2080731.1901 •220582.• 7 ricIL u Matrix. • Collect Datell ime Receive Date/Time ' .Solid 07/28/2008 11:30 07/31/2008 0931 SW-846 8151 A TCLP Prep Date Prep Batch 08/08/2008 17:30 394786 Prep Method 3510C Dilution Analyzed By Analytical Batch 1 08/11 /2008 04:44 TLS 395060 CAS# 94-75-7 93-72-1 Parameter 2.4'-D 2,4,5-TP (Silvex) CAS# Surrogate 19719-28-9 DCAA RESULTS REPORTED ON A WET WEIGHT BASIS Result 0.00000U 0.00001 U RDL 0.00500 0.00500 MDL 0.00000 0.00001 Units mg/L mg/L Conc. Spiked Conc. Rec Units % Recovery Rec Limits 20 13.9 ug/L 70 41 - 128 GCAL Report 208073119 GCAL ID Client lD :u: 208073.11901. 220582 7�'(-re Matrix. CollectpateNme. Receive-Datemme Solid . 07/28,2008 11:30 07/31/2008 09:31 : SW-846 9012A Reactivity CN Prep Date Prep Batch 08/02/2008 09:00 394040 Prep Method 7.3.3.2 Dilution Analyzed By Analytical Batch 1 08/07/2008 15:04 AEL 394657 CAS# Parameter 57-12-5R Reactivity Cyanide RESULTS REPORTED ON A WET WEIGHT BASIS Result 250U RDL 250 MDL 250 Units mg/kg GCAL Report 208073119 GCAL ID -,:,;Client ID , C-C.ek iVlatrhc Collect Datefriroe Receive Date/Time • • . • . SI Solid 20807311901 220582 - je 07/2812008 11:30 07/31/2008 0931 SW-846 9034 Reactivity Sulfide I Prep Date Prep Batch Prep Method 08/02/2008 09:00 394041 Sec 7.3.4.2 Dilution Analyzed By Analytical Batch 1 08/04/2008 04:30 JEM 394347 CAS# Parameter 18496-25-8R Reactivity Sulfide RESULTS REPORTED ON A WET WEIGHT BASIS Result RDL MDL 80U 80 80 Units mg/kg GCAL Report 208073119 State of North Carolina Department of Environment and Natural Res Division of Water Quality RESIDUALS SOURCE CERTIFICATION ATT .CRAW (FORM: RSCA 070807) (THIS FORM MAY BE PHOTOCOPIED FOR USE AS AN ORIGINAL) The Division of Water Quality (Division) will not accept this attachment unless all the instructions are followed. Failure to submit all required items will lead to additional processing and review time. For more information. visit our web site at: httpr%h2o.cnr.state.nc.urs,!lurr'main.html INSTRUCTIONS TO THE APPLICANT: 3" r Creel, ► Jt'TP pir,fla16) ILO __ S EP - 2 2009 uifer Protection A. Attachment Form: ✓ Do not submit this attachment form for review without a corresponding residuals program application form (FORM: NDRLAP, FORM: DRS, or FORM: SDRS). ✓ Any changes to this attachment form will result in the application package being returned. ✓ For new residuals programs or renewed residuals programs, submit a separate attachment form for each residuals source -generating facility to be certified for this residuals. program. ✓ For modified residuals programs in which any modification to the certified residuals -source generating facilities is proposed, submit a separate attachment form for only those residuals source -generating facilities that are affected by the proposed modification. ✓ The attachment should be organized prior to submission in the following order (i.e., by facility): ® Attachment Order 2: Residuals Source Certification Attachment (FORM: RSCA). > Attachment Order 2-a: Vicinity map. > Attachment Order 2-b: Process flow diagram and/or narrative. > Attachment Order 2-c: Quantitative justification for residuals production rate. > Attachment Order 2-d: Sampling plan. > Attachment Order 2-e: Laboratory analytical reports and operational data. B. Residuals Source -Generating Facility Information: ✓ Attach a vicinity map that shows the Location of the facility and meets all of the criteria in the latest version of the document entitled "Guidance for the Preparation of Vicinity/Buffer Maps for North Carolina Residuals Permitting Programs." ✓ Attach a detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. ✓ Attach a quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. C. Residuals Quality Information: ✓ Attach a detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. ✓ Attach reports for all laboratory analyses used to complete this attachment form. Attach documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ✓ Item It 3. Does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only. FORM: RSCA 070807 Page 1 of 8 Attachment Order 2 State of North Carolina Department of Environment and Natural Resotyl ee --- Division of Water Quality l SEP - 2 2009 RESIDUALS SOURCE CERTIFICATION ATTACH ENT (FORM: RSCA 070807)" iri ff `���•�-�,.... PIC D?�i�l�t ��fii�;0 (THIS FORM MAY BE PHOTOCOPIED FOR USE AS AN ORIGI A L) DWC) - Acuifer Protection Applicant's name: City ofStatesville/ 3" r Creek Ih`II'"TP Check all that apply: ❑ NEW RESIDUALS PROGRAM X RENEWED RESIDUALS PROGRAM ❑ INCREASE ❑ DECREASE the maximum permitted annual dry tonnage for this residuals source - generating facility certified for this residuals program. Current: 1,000 Dry Tons/yr. and proposed: 1,000 Dry Tons/yr. ❑ ADD ❑ DELETE this residuals source -generating facility to/from those certified for this residuals program. ❑ OTHER Explain: I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Name of facility: 3'1 Creek WWTP 2. Facility permit holder: City of Statesville Facility permit holder is (check one): ❑ federal, ❑ state, X local government, or ❑ private. Facility permit number: NC0020591 Facility permit issued by (check one): X Div. of Water Quality, ❑ Div. of Environmental Health, or ❑ other (explain: ). 3. If the facility permit is not issued by the Div. of Water Quality, complete the following: a. Facility contact person and title: Facility complete mailing address: City: State: Zip: Telephone number: ( ) Facsimile number: ( ) E-mail address: b. Facility complete location address: City: State: Zip: Latitude: and longitude: 4. County where facility is located: Iredell 5. Purpose of the facility (check one): ❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater, ❑ treatment of potable water, ❑ treatment of 100% industrial wastewater, X treatment of industrial wastewater mixed with domestic wastewater, or (approximate percentages: 60 % industrial and 40 % domestic) ❑ other (explain: FORM: RSCA 070807 Page 2 of 8 Attachment Order 2 6. Does the facility have an approved pretreatment program: X yes ❑ no 7. Facility permitted/design flow: 4 MGD and facility average daily flow: 2 MGD. 8. Average amount of residuals being generated at this facility dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: 0.9 Million Gallon aerobic digester, belt filter press. Dewatering polymer. Type and volume of residuals storage (i.e., outside of residuals treatment units): 1/3 acre concrete pad. II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under (check one): ❑ 40 CFR Part 503 or ❑ 40 CFR Part 257. 2. Specify if residuals are intended for (check one): ❑ Land Application/Distribution (Class A or Equivalent). Complete all items EXCEPT Items II. 4b. 7b. and 7c. X Land Application (Class B or Equivalent). Complete all items EXCEPT Items II. 4b. 7a. and 7c. ❑ Surface Disposal. Complete all items EXCEPT Items 11. 4a. 5. 7a., 7b., and 8. ***FORM: RSCA CONTINUES ON NEXT PAGE*** FORM: RSCA 070807 Page 3 of 8 Attachment Order 2 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non- hazardous under RCRA: a. Are the residuals are listed in 40 CFR §261.31-§261.33: ❑ yes X no. If yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- §261.24: ❑ yes X no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: laboratory: Prism Laboratory and date of analysis: 7/28/08 Passed corrosivity test: X yes ❑ no. pH: s.u. (2 < pH < 12.5). Passed ignitability test: X yes ❑ no. Flashpoint: °F (> 140°F). Passed reactivity test: X yes ❑ no. HCN: mg/kg (<250) & H2S: mg/kg (<500). TCLP Parameter Limit (mg/L) Result (mg/L) TCLP Parameter Limit (mg/L) Result (mg/L) Arsenic 5.0 <0.050 Hexachlorobenzene 0.13 <0.010 Barium 100.0 <5.0 Hexachloro-1,3- R11t4diene 0.5 <0.050 Benzene 0.5 <0.050 Hexachloroethane 3.0 <0.050 Cadmium 1.0 <0.025 Lead 5.0 <0.050 Carbon Tetrachloride 0.5 <0.050 Lindane 0.4 <0.0005 Chlordane • 0.03 <0.0025 Mercury 0.2 <0.010 Chlorobenzene 100.0 <0.050 Methoxychlor 10.0 <0.0005 Chloroform 6.0 <0.050 Methyl Ethyl Ketone 200.0 <0.50 Chromium 5.0 <0.25 Nitrobenzene 2.0 <0.050 m-Cresol 200.0 Pentachlorophenol 100.0 <0.25 o-Cresol 200.0 Pyridine 5.0 <0.25 p-Cresol 200.0 Selenium 1.0 <0.050 Cresol 200.0 Silver 5.0 <0.25 2,4-D 10.0 ND Tetrachloroethylene 0.7 <0.050 1,4-Dichlorobenzene 7.5 <0.050 Toxaphene 0.5 <0.025 1,2-Dichloroethane 0.5 <0.050 Trichloroethylene 0.5 <0.050 1,1-Dichloroethylene 0.7 <0.050 2,4,5-Trichlorophenol 400.0 <0.25 2,4-Dinitrotoluene 0.13 <0.012 2,4,6-Trichlorophenol 2.0 <0.10 Endrin 0.02 <0.0005 2,4,5-TP (Silvex) 1.0 0.00500 Heptachlor and its Hydroxide 0.008 <0.0005 Vinyl Chloride 0.2 <0.020 FORM: RSCA 070807 Page 4 of 8 Attachment Order 2 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Class A or Class B: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: and date of analysis: Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (For Class A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 Cadmium 85 39 Copper 4,300 1,500 No Residuals Lead 840 300 have been applied Mercury 57 17 Molybdenum 75 n/a Nickel 420 420 Selenium 100 100 Zinc 7,500 2,800 b. For Surface Disposal: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: and date of analysis: Closest Distance to Property Lines (meters) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) > O but < 25 30 200 210 > 25 but < 50 34 220 240 >_ 50 but < 75 39 260 270 >_ 75 but < 100 46 300 320 > 100 but < 125 53 360 390 > 125 but < 150 62 450 420 > 150 73 600 420 FORM: RSCA 070807 Page 5 of 8 Attachment Order 2 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 19 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: laboratory: 4th Creek WWTP Laboratory and date of analysis: Ongoing weekly. Parameter Result (mg/kg, dry weight) Aluminum Ammonia -Nitrogen Calcium No residuals have been applied. Magnesium Nitrate -Nitrite Nitrogen pH (Standard Unit) Phosphorus Potassium Sodium Total Kjeldahl Nitrogen c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This rate is a ❑ default value or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: Calculate the PAN for the residuals (i.e., on a dry weight basis) and list the results in the following table: Application Method First Year PAN (mg/kg) Five -Year Maximum Adjusted PAN (mg/kg) Surface 4 19.95 Injection/Incorporation e. Are the residuals a registered fertilizer with the NC Department of Agriculture and Consumer Services: ❑ yes X no. If yes, provide date of registration approval: the current registration number: and the fertilizer equivalent: %, %, and %. FORM: RSCA 070807 Page 6 of 8 Attachment Order 2 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and list the results of the latest analyses: 7. Pathogen Reduction Determination: Specify which alternative(s) will be used to meet the pathogen reduction requirements: a. For Class A or Equivalent: ❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids. OR ❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the following (except for residuals regulated under 40 CFR Part 257 that are to be distributed): ❑ Alternative 1 [40 CFR §503.32 (a)(3)] - Time/Temperature Compliance. ❑ Alternative 2 [40 CFR §503.32 (a)(4)] - Alkaline Treatment. ❑ Alternative 3 [40 CFR §503.32 (a)(5)] - Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 4 [40 CFR §503.32 (a)(6)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 5 [40 CFR §503.32 (a)(7)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment, ❑ pasteurization, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, or ❑ gamma ray irradiation. ❑ Alternative 6 [40 CFR §503.32 (a)(8)] - PFRP-Equivalent Process. Explain: b. For Class B or Equivalent: X Alternative 1 [40 CFR §503.32 (b)(2)] - Fecal Coliform Density Demonstration. ❑ Alternative 2 [40 CFR §503.32 (b)(3)] - Process to Significantly Reduce Pathogens (PFRP). Specify one: X aerobic digestion, ❑ air drying, ❑ anaerobic digestion, ❑ composting, or ❑ lime stabilization. ❑ Alternative 3 [40 CFR §503.32 (b)(4)] - PSRP-Equivalent Process. Explain: ❑ Not Applicable - Regulated under 40 CFR Part 257 with NO Domestic Wastewater Contribution. c. For Surface Disposal: ❑ Alternative for Surface Disposal Units Only [40 CFR §503.33 (b)(11)] - SoiVOther Material Cover. ❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. ❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. ❑ Not Applicable - Regulated under 40 CFR Part 257 with NO Domestic Wastewater Contribution. FORM: RSCA 070807 Page 7 of 8 Attachment Order 2 8. Vector Attraction Reduction Determination: Specify which alternative(s) will be used to meet the vector attraction reduction requirements: ❑ Alternative 1 [40 CFR §503.33 (b)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [40 CFR §503.33 (b)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). ❑ Alternative 3 [40 CFR §503.33 (b)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 [40 CFR §503.33 (b)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). X Alternative 5 [40 CFR §503.33 (b)(5)] - 14-Day Aerobic Processes. ❑ Alternative 6 [40 CFR §503.33 (b)(6)] - Alkaline Stabilization. ❑ Alternative 7 [40 CFR §503.33 (b)(7)] - Drying of Stabilized Residuals. ❑ Alternative 8 [40 CFR §503.33 (b)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [40 CFR §503.33 (b)(9)] - Injection. ❑ Alternative 10 [40 CFR §503.33 (b)(10)] - Incorporation. El Alternative for Surface Disposal Units Only [40 CFR §503.33 (b)(11)] - Soil/Other Material Cover. El Alternatives for Animal Processing Residuals Only: Specify one: ❑ injection, ❑ incorporation, or ❑ lime addition to raise pH to 10. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. FORM: RSCA 070807 Page 8 of 8 Attachment Order 2 ji 3 n? C1 0s- wao2A ATTACHMENT 2b 4th CREEK & 3rn' CREEK WWTP NARRATIVE Both of the WWTP's utilize a conventional activated sludge process that primarily treats domestic and industrial waste water generated from areas within and outside of the city. The raw sewage enters the WWTP via gravity main and from there it flows into a wet well or pump station. The flow enters one of two perforated panel type bar screens. At this point the raw sewage is mixed with return activated sludge and distributed into two aeration basins. The mixed liquor flows into secondary clarifiers . and then the RAS is pumped back into the influent of the WWTP. The effluent gravity flows from the secondary clarifiers to the chlorine contact basins where the final effluent is treated with Sodium Bisulfite for de -chlorination as it flows to the receiving stream. Both WWTP's generate biosolids that are currently stabilized using an aerobic digester, and dewatered using a belt press. After dewatering, the residuals are transferred to the N-Viro lime stabilization process area where the biosolids are set aside for contract land application off of the plant site. The primary method of biosolids disposal is the N-Viro process. *IA it of -ftttesniUc II. CO. Jnx 1111 • 3tatesuille, Nnrtll attrolina 28G87 July21, 2009 Mr. Ed Hardee Central Office 1636 Mail Service Center Raleigh, NC 27699-1636 Re: Permit # WO0014543 Quantitative Justification for Residuals Production Rate Third Creek WWTP Dear Mr. Hardee: )40,07.1-A The 3`d Creek WWTP would generate approximately 973 dry tons per year of biosolids. This would all go to the N-Viro process and /or the contracted Land Application contractor unless extenuating circumstances prevailed. Should you require more information, or if further action is required, please contact me at 878-3438. Sin Fourth Creek WWTP Supervisor OEit of 3tttte�nille 1,. (!. Nnx 1111 • 'ttttesuille, Nurtli Cnttrulina 28687 July 21, 2009 Mr. Ed Hardee Central Office 1636 Mail Service Center Raleigh, NC 27699-1636 Re: Permit # WQ0014543 2, Biosolids Sampling Plan/XS Third Creek WWTP Dear Mr. Hardee: The 3`d Creek WWTP is currently using a 2 belt sludge press for the process of its sludge. As the press is operating, the operator would collect the required amount of sample per the permit to send to the designated lab. Should you require more information, or if further action is required, please contact me at 878-3438. Sincerely, Fourth reek VWVTP Supervisor Full Service Analytical & Environmental Solutions City of Statesville Attn: Mr. Andy Smith P.O. Box 1111 Statesville, NC 28687 NC Certification No. 402 SC Certification No. 99012 NC Drinking Water Cert. No. 37735 Project ID: Sta-Lime, 3rd Creek and 4th Creek Sludge with TCLP Sample Matrix: Solid Laboratory Report 08/14/08 Client Sample ID: Prism Sample ID: COC Group: Time Collected: Time Submitted: 3RD Creek Sludge 220583 G0708776 07/28/08 11:30 07/28/08 15:35 Parameter pH, Corrosivity pH Ignitability of Solids Ignitability Result Units Report MDL Dilution Method Analysis Limit Factor Date/Time Analyst Batch ID 6.0 pH units 0.10 0.10 Negative N/A 1 9045C 08/01/08 11:44 kpowers 1030 07/30/08 14:44 rloftin Reactive Cyanide Subcontract Report See 1 See Attached Attached * Analysis Note for Subcontract Report: Subcontracted to NC Certified Lab 618. Reactive Sulfide Subcontract Report See 1 See Attached Attached * Analysis Note for Subcontract Report: Subcontracted to NC Certified Lab 618. TCLP Extraction for Metals and/or Non -Volatile Organics TCLP Extraction (Metals/Organics) Complete Zero Headspace Extraction for Volatiles TCLP Extraction (ZHE-Volatiles) Complete 1 1 1311 08/05/08 11:30 mbarber 1311 08/11/08 17:00 winder Acid Herbicicides in TCLP Leacheate by GC-ECD Subcontract Report See 1 8151A Attached * Analysis Note for Subcontract Report: Subcontracted to NC Certified Lab 618. TCLP Leachable Mercury by CVAA Mercury BRL mg/L 0.010 0.000014 1 7470A Sample Preparation: 20 mL / 30 mL 7470A 08/08/08 9:30 TCLP Leachable Metals by ICP Arsenic Barium Cadmium BRL mg/L 0.050 0.0029 1 6010B 08/07/08 2:07 BRL mg/L 5.0 0.0019 1 6010B 08/07/08 2:07 BRL mg/L 0.025 0.00034 1 6010B 08/07/08 2:07 034366 Q34306 08/08/08 18:19 mcampbeli Q34590 mbarber P22275 mcampbell mcampbell mcampbell Q34496 Q34496 Q34496 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page5of12 Full Service Analytical & Environmental Solutions City of Statesville Attn: Mr. Andy Smith P.O. Box 1111 Statesville, NC 28687 NC Certification No. 402 SC Certification No. 99012 NC Drinking Water Cert. No. 37735 Project ID: Sta-Lime, 3rd Creek and 4th Creek Sludge with TCLP Sample Matrix: Solid Laboratory Report 08/14/08 Client Sample ID: Prism Sample ID: COC Group: Time Collected: Time Submitted: 3RD Creek Sludge 220583 G0708776 07/28/08 11:30 07/28/08 15:35 Parameter Chromium Lead Selenium Silver Result Units Report MDL Dilution Limit Factor Method Analysis Date/Time Analyst Batch ID Sample Preparation: BRL mg/L 0.25 0.0006 1 BRL mg/L 0.050 0.0021 1 BRL mg/L 0.050 0.0035 1 BRL mg/L 0.25 0.00025 1 TCLP Leachable Organochlorine Pesticides by GC/ECD Chlordane BRL mg/L Endrin Heptachlor Heptachlor Epoxide Lindane Methoxychlor Toxaphene Sample Preparation: 50 mL / 50 mL 0.0025 0.00072 BRL mg/L 0.0005 0.000041 BRL mg/L 0.0005 0.000079 BRL mg/L 0.0005 0.000044 BRL mg/L 0.0005 0.000041 BRL mg/L 0.0005 0.000087 BRL mg/L 0.025 0.00074 TCLP Leachable Semi -volatile Organics by GC/MS 1,4-Dichlorobenzene BRL 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dinitrotoluene 2-Methylphenol 3&4-Methylphenol Hexachlorobenzene Hexachlorobutadiene BRL BRL BRL BRL BRL BRL BRL 1 1 1 1 1 1 200 mL / 10 mL 6010E 08/07/08 2:07 6010E 08/07/08 2:07 6010E 08/07/08 2:07 6010B 08/07/08 2:07 3010A 08/06/08 9:40 8081A 8081A 8081A 8081A 8081A 8081A 8081A mcampbell Q34496 mcampbell Q34496 mcampbell Q34496 mcampbell Q34496 mbarber P22258 08/08/08 0:06 jvogel 08/08/08 0:06 jvogel 08/08/08 0:06 jvogel 08/08/08 0:06 jvogel 08/08/08 0:06 jvogel 08/08/08 0:06 jvogel 08/08/08 0:06 jvogel 3510C 08/07/08 6:00 Surrogate % Recovery Tetrachloro-m-xylene (TCMX) 84 Decachlorobiphenyl (DCB) Q34533 Q34533 Q34533 Q34533 Q34533 Q34533 Q34533 smanivanh P22264 Control Limits 40-134 77 13-186 mg/L 0.050 0.0028 1 8270C 08/12/08 9:43 kcampigotto 034621 mg/L 0.25 0.0044 1 8270C 08/12/08 9:43 kcampigotto 434621 mg/L 0.10 0.0046 1 8270C 08/12/08 9:43 kcampigotto Q34621 mg/L 0.012 0.0030 1 8270C 08/12/08 9:43 kcampigotto Q34621 mg/L 0.050 0.0052 1 8270C 08/12/08 9:43 kcampigotto Q34621 mg/L 0.050 0.0056 1 8270C 08/12/08 9:43 kcampigotto Q34621 mg/L 0.010 0.0014 1 8270C 08/12/08 9:43 kcampigotto Q34621 mg/L 0.050 0.0022 1 6270C 08/12/08 9:43 kcampigotto Q34621 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 12 Full Service Analytical & Environmental &Miens City of Statesville Attn: Mr. Andy Smith P.O. Box 1111 Statesville, NC 28687 NC Certification No. 402 SC Certification No. 99012 NC Drinking Water Cert. No. 37735 Project ID: Sta-Lime, 3rd Creek and 4th Creek Sludge with TCLP Sample Matrix: Solid Laboratory Report 08/14/08 Client Sample ID: Prism Sample ID: COC Group: Time Collected: Time Submitted: 3RD Creek Sludge 220583 G0708776 07/28/08 11:30 07/28/08 15:35 Parameter Result Units Report MDL Dilution Method Limit Factor Hexachloroethane Nitrobenzene Pentachlorophenol Pyridine Sample Preparation: BRL mg/L 0.050 0.0046 1 Analysis Date/Time Analyst Batch ID 8270C 08/12/08 9:43 BRL mg/L 0.050 0.0030 1 8270C BRL mg/L 0.25 0.0042 1 8270C BRL mg/L 0.25 0.0036 1 8270C TCLP Leachable Volatile Organics by GC/MS 1,1-Dichloroethene BRL mg/L 1,2-Dichloroethane BRL mg/L 1,4-Dichlorober¢ene BRL mg/L Benzene BRL mg/L Carbon tetrachloride BRL mg/L Chlorobenzene BRL mg/L Chloroform BRL mg/L Methyl ethyl ketone (MEK) BRL mg/L Tetrachloroethene BRL mg/L Trichloroethene BRL mg/L Vinyl chloride BRL mg/L 08/12/08 9:43 08/12/08 9:43 08/12/08 9:43 kcampigotto Q34621 kcampigotto Q34621 kcampigotto Q34621 kcampigotto Q34621 200 mL / 1 mL 3510C 08/11/08 13:00 smanivanh P22306 0.050 0.050 0.050 0.050 0.050 0.050 0.050 0.50 0.050 0.050 0.020 Surrogate Terphenyl-d14 Phenol-d5 Nitrobenzene-d5 2-Fluorophenol 2-Fluorobiphenyl 2,4,6-Tribromophenol % Recovery Control Limits 88 11 64 14 65 38 41 -136 10-78 13-107 10-75 27-107 38 -117 0.013 10 0.0021 10 . 0.0033 10 0.0028 10 0.0012 10 0.00094 10 0.017 10 0.017 10 0.0036 10 0.0033 10 0.011 10 8260B 8260B 8260E 8260E 8260B 8260E 826013 8260B 8260E 8260B 8260B 08/12/08 14:15 erussell 08/12/08 14:15 erussell 08/12/08 14:15 erussell 08/12/08 14:15 erussell 08/12/08 14:15 erussell 08/12/08 14:15 erussell 08/12/08 14:15 erussell 08/12/08 14:15 erussell 08/12/08 14:15 erussell 08/12/08 14:15 erussell 08/12/08 14:15 enm-J.li Q34644 034644 Q34644 Q34644 Q34644 Q34644 Q34644 Q34644 Q34644 Q34644 Q34644 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 7 of 12 Full Srwleo Analytical & Environmental Solutions City of Statesville Attn: Mr. Andy Smith P.O. Box 1111 Statesville, NC 28687 Parameter Sample Comment(s): NC Certification No. 402 SC Certification No. 99012 NC Drinking Water Cert. No. 37735 Project ID: Sample Matrix: Sta-Lime, 3rd Creek and 4th Creek Sludge with TCLP Solid Laboratory Report Client Sample ID: Prism Sample ID: COC Group: Time Collected: Time Submitted: 08/14/08 3RD Creek Sludge 220583 G0708776 07/28/08 11:30 07/28/08 15:35 Result Units Report MDL Dilution Limit Factor Method Analysis Date/Time Surrogate Toluene-d8 Dibromofluoromethane Bromofluorobenzene Analyst Batch ID % Recovery Control Limits 99 75 - 121 101 74 -133 102 69-139 BRL = Below Reporting Limit Values are reported down to the reporting limits only. No J-flags applied. The results in this report relate only to the samples submitted for analysis and meet state certification requirements other than NELAC certification except for those instances indicated in the case narrative and/or test comments. All results are reported on a wet -weight basis Angela D. Overcash, V.P. Laboratory Services This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 8 of 12 GCAL„ip :. Clieiiii&. 2080731<1902 220583.' Matrix : Collect DateiTime: Receive Datemme Solid 07/28/200811:30 07/31/2008 09:31 SW-846 9034 Reactivity Sulfide Prep Date Prep Batch 08/02/2008 09:00 394041 Prep Method Sec 7.3.4.2 Dilution Analyzed By Analytical Batch 1 08/04/2008 04:30 JEM 394347 CAS# Parameter 18496-25-8R Reactivity Sulfide RESULTS REPORTED ON A WET WEIGHT BASIS Result 80U RDL 80 MDL B0 Units mg/kg GCAL Report 208073119 GCALID: Client ID • =20807311902.;..; :.220583 3 .. Matrix Solid Collect patelTime. 07/28/200cs ,1130--: Receive DatefTime 7/31f2008 09:31 . • SW-846 9012A Reactivity CN Prep Date Prep Batch 08/02/2008 09:00 394040 Prep Method 7.3.3.2 Dilution Analyzed By Analytical Batch 1 08/07/2008 15:05 AEL 394657 CAS# 57-12-5R Parameter Reactivity Cyanide RESULTS REPORTED ON A WET WEIGHT BASIS Result 250U RDL 250 MDL 250 Units mg/kg GCAL Report 208073119 , SCAL.ID ' Client ID 2080731.1902... 220583 Matrix CollectDate/Time. toJ �e. Solid . 07/28/2008 11:30 Receive DatelTime. • 07/31/2008 09:31 SW-846 8151A TCLP Prep Date Prep Batch 08/08/2008 17:30 394786 Prep Method 3510C Dilution Analyzed By Analytical Batch 1 08/11/2008 05:13 TLS 395060 CAS# 94-75-7 93-72 1 CAS# Surrogate Parameter 2,4'-D 2,4,5-TP (Silvex) 19719-28-9 DCAA RESULTS REPORTED ON A WET WEIGHT BASIS Result RDL MDL Units 0.00000U 0.00500 0.00000 mg/L 0.00001U 0.00500 0.00001 mg/L Conc. Spiked Conc. Rec Units % Recovery Rec Limits 20 15.8 ug/L 79 41 - 128 GCAL Report 208073119 State of North Carolina Department of Environment and Natural Reso Division of Water Quality LAND APPLICATION SITE CERTIFICATION ATT (FORM: LASCA 070807) (THIS FORM MAY BE PHOTOCOPIED FOR USE AS AN ORIGINAL) The Division of Water Quality (Division) will not accept this attachment unless all the instructions are followed. Failure to submit all required items will lead to additional processing and review time. For more information, visit our web site at:lutp:t/h7p.erer.state.nc.us/iauhnain.html INSTRUCTIONS TO THE APPLICANT: A. Attachment Form: ✓ Do not submit this attachment form for review without a corresponding residuals program application form (FORM: NDRLAP). ✓ Any changes to this attachment form will result in the application package being returned. ✓ For new residuals land application programs or renewed residuals land application programs, submit the requested information for all land application sites to be certified for this residuals land application program. ✓ For modified residuals land application programs in which any new/transferred land application sites or modification to the certified land application sites are proposed, submit the requested information for only those land application sites that are new/transferred or affected by the proposed modification. B. Land Application Site Information: ✓ Additional copies of Page 4 of 4 of this attachment form may be used if necessary. ✓ The status of the land application site with respect to this residuals land application program must be provided in the table in Item I. 1. The status categories and their corresponding codes are as follows: • New (N) • Renewed (R) ♦ Modified (M) rip E.OTW E SEP - 2 2009 D�"bNO Acuif=;r Protection + Transferred (T) ✓ If this is the first time that an application package is being submitted using Form NDRLAP, then a Watershed Classification Attachment (FORM: WSCA) must be completed for all existing land application sites. ✓ For each land application site with a status code of N, attach the following in the order specified: ♦ Attachment Order 3: Land Application Site Certification Attachment (FORM: LASCA). ➢ Attachment Order 3-a: Watershed Classification Attachment (FORM: WSCA). ➢ Attachment Order 3-b: County Manager Notification Attachment (FORM: CMNA). > By Land Application Site: ■ Attachment Order 3-c: Landowner Agreement Attachment (FORM: LOAA). • Attachment Order 3-d: Setback Waiver Agreement Attachment (FORM: SWAA). • Attachment Order 3-e: An updated vicinity/buffer map that meets all of the criteria in the latest version of the document entitled "Guidance for the Preparation of Vicinity/Buffer Maps for North Carolina Residuals Permitting Programs.", including review and compliance boundaries. ■ Attachment Order 3-f: A soils and agronomic evaluation that meets all of the criteria in the latest version of the document entitled "Soil Scientist Evaluation Guidance Document." ✓ For each land application site with a status code of R, attach the following in the order specified: • Attachment Order 3: Land Application Site Certification Attachment (FORM: LASCA). > By Land Application Site: ■ Attachment Order 3-c: Landowner Agreement Attachment (FORM: LOAA). • Attachment Order 3-d: Setback Waiver Agreement Attachment (FORM: SWAA). ■ Attachment Order 3-e: An updated vicinity/buffer map (i.e., see above for criteria guidance). ■ Attachment Order 3-g: An updated accounting of the land application site's cumulative pollutant loading rates (CPLRs) that are required by the permit of the residuals land application program from which the site is being transferred. ***INSTRUCTIONS CONTINUE ON NEXT PAGE*** FORM: LASCA 070807 Page 1 of 3 Attachment Order 3 • Attachment Order 3-h: (For sites without a previously permitted soil series name indicated in Attachment "B") County Soil Survey Map (or equivalent) clearly indicating the location and name of the all land application sites without a previously permitted soil type. The map must be legible and to a scale where the sites can be easily identified and differentiated from adjacent sites. The predominant soil -mapping units must be shown for each site. The map must include the mapping unit legend, the County name, the Applicants name, and the permit number. The Permittee must note in the narrative and provide documentation supported by a licensed soil scientist for approval of any soil -mapping unit submitted in this form that has not been previously approved and differs from that shown in the County Soil Survey. ✓ For each land application site with a status code of M. contact the appropriate Division's regional office to determine attachment requirements. ✓ For each land application site with a status code of T attach the following in the order specified: • Attachment Order 3: Land Application Site Certification Attachment (FORM: LASCA). ➢ Attachment Order 3-a: Watershed Classification Attachment (FORM: WSCA). ➢ Attachment Order 3-b: County Manager Notification Attachment (FORM: CMNA). > By Land Application Site: • Attachment Order 3-c: Landowner Agreement Attachment (FORM: LOAA). ■ Attachment Order 3-d: Setback Waiver Agreement Attachment (FORM: SWAA). • Attachment Order 3-e: An updated vicinity/buffer map that meets all of the criteria in the latest version of the document entitled "Guidance for the Preparation of Vicinity/Buffer Maps for North Carolina Residuals Permitting Programs." • Attachment Order 3-g: An updated accounting of the CPLRs (i.e., see above for criteria guidance). ■ Attachment Order 3-i: Acknowledgement of field transfer from Permittee relinquishing field. • Attachment Order 3-i: Acknowledgement of field transfer from Land Owner. Fields may not be permitted to multiple Permitees over the same time period. ✓ Crop Type should include the most likely crop types for the life of the permit (5 years). ✓ Predominant Soils Series Name must be either the name of the soil indicated in Attachment `B" of the existing permit, or name of the soil series as provided by the licensed soil scientist. ✓ Predominant Soil Mapping Unit or Representative Slope: Either the Soil Mapping Unit or the representative slope of each site must be provided. The predominant soil -mapping unit must be consistent with the predominant soil series name. Please note that the soil mapping units are variable between Counties, so care should be taken in properly identifying the correct mapping unit. If a representative slope is provided, it must be determined accordingly: • Sites previously permitted for use, but do not have an established soil mapping unit (the mapping unit provides information on both the soil series name and the slope of the soil), may determine the representative slope by using the average slope provided in the County Soil Survey (or equivalent). A soil type with a slope range of 4 - 8% would have a representative slope of 6%. ♦ New Sites to be permitted must have slopes determined as part of the soils report prepared by a licensed soil scientist. FORM: LASCA 070807 Page 2 of 4 Attachment Order 3 Applicant's name: City of Statesville Check all that apply: ❑ NEW RESIDUALS LAND APPLICATION PROGRAM X RENEWED RESIDUALS LAND APPLICATION PROGRAM ❑ ADD ❑ DELETE this/these land application site(s) to/from those certified for this residuals land application program. ❑ INCREASE ❑ DECREASE the net acreage associated with this/these land application site(s) currently certified. ❑ OTHER Explain: Land application sites currently certified: 4`J' —15. 3/ 3'd —14,1 net acres and Total to be certified: 29,4 I. LAND APPLICATION SITE INFORMATION (See Instruction B.): 1. Complete the following table with the requested information: net acres. Status Code a Site/Field ID Landowner(s) Lessee(s) or Operator(s) Net Acres County Crop(s) Predominant Soil Series Name* Mapping Unit or Rep. Slope ** R 01 City of Statesville City of Statesville 15.3 Iredell Corn/small grain Lloyd LcD3 R 02 City of Statesville City of Statesville 14.10 Iredell Fescue hay Cecil Cfc2 s Status Code for land application sites are: • N (New) • R (Renew) * Soil Series Name (i.e Cecil) FORM: LASCA 070807 o M (Modified) e T (Transferred) Page 3 of4 Attachment Order 3 Cumulative Pollutant Loading Rate 2009 Parameters Kilograms/Hectare LBS/Acre Arsenic 41 36 Cadmium 39 34 Copper 1,500 1,338 Lead 300 267 Mercury 17 15 Molybdenum NA NA Nickel 420 374 Selenium 100 89 Zinc 2,800 2,498 Michael F. Easley, Governor William G. Ross Jr., Secretary North Carolina Department of Environment and Natural Resources March 11, 2005 MR. L. F. "JoE" HUDSON, JR., DIRECTOR OF WATER RESOURCES CITY OF STATESVILLE POST OFFICE BOX 1111 STATESVILLE, NC 28677 Dear Mr. Hudson: Alan W. Klimek, P.E. Director Division of Water Quality ari�CC9i;]i��I SEP - 2 2009 NC DF,NR MRO DWQ - Ac uifor Protection Subject: Permit No. WQ0014543 . City of Statesville City of Statesville Residuals Land Application Program Land Application of Residual Solids (503) Iredell County In accordance with your permit renewal application package received on May 20, 2002 as well as the additional information received on August 9, 2002 and June 27, 2003; we are forwarding herewith a modified and renewed Permit No. WQ0014543, dated March 11, 2005, to the City of Statesville for the subject residuals land application program. This permit shall be effective from the date of issuance until February 28, 2010; shall void Permit No. WQ0014543, issued on February 16, 1998 and shall be subject to the conditions and limitations as specified therein. Make note of this permit's expiration date and the fact that a permit renewal application is due to the Division of Water Quality (Division) no later than six months prior to that date (i.e., see Condition VI. 7.), as the Division does not send reminders to apply for permit renewal. This permit is being issued to approve the continued operation of the residuals land application program for another five-year cycle as an emergency backup alternative to Permit No. WQ0016247. (a residuals land application permit issued to Synagro-WWT, Inc.) and Permit No. WQ0006245 (Sta-Lime distribution permit issued to the City of Statesville). Please be advised that the land application area being approved in the enclosed Attachment B is not sufficient to land apply all of the residuals being approved in the enclosed Attachment A. Hence, additional land application sites must be approved prior to land application of all of the residuals being approved in Attachment A. As always, remember to take the time to review this permit thoroughly, as some of the conditions contained therein may have been added, changed, or deleted since the last issuance. Pay particular attention to the monitoring requirements in this permit. Failure to establish an adequate system for collecting and maintaining the required operational information will result in future compliance problems. If any parts, requirements, and/or limitations contained in this permit are unacceptable, you have the right to request an adjudicatory hearing upon written request within 30 days following receipt of this permit. This request shall be in the from of a written petition, conforming to Chapter 150B of the North Carolina General Statutes and filed with the' Office of Administrative Hearings at 6714 Mail Service Center, Raleigh, North Carolina 27699-6714. Unless such demands are made, this permit shall be final and binding. Aquifer Protection Section 1636 Mail Service Center Raleigh, NC 27699-1636 Phone (919) 733-3221 Customer Service Internet: http://h2o.enr.state.nc.us 2728 Capital Boulevard Raleigh, NC 27604 Fax (919) 715-0588 1-877-623-6748 An Equal opportunity/Affirmative Action Employer — 50% Recycled/10% Post Consumer Paper Fax (919) 715-6048 Onc Carolina Naturally L: F. "Joe" Hudson, Jr. March 11, 2005 Page 2 If you need any additional information concerning this matter, please contact Mr. J. R. Joshi by telephone at (919) 715-6698, or via e-mail at jaya joshi @ncmail.net. Sincerely, or Alan W. Klimek, P.E. cc: .Iredell County Health Departinent Mooresville Regional Office -Aquifer Protection Section Technical Assistance and Certification Unit. APS Central Files APSuFiles? LAU Residuals Program Coordinator NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES RALEIGH LAND APPLICATION OF RESIDUAL SOLIDS (503) PERMIT. In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, and other applicable Laws, Rules, and Regulations PERMISSION IS HEREBY GRANTED TO City of Statesville Iredell County FOR THE continued operation of a residuals land application program for the City of Statesville and consisting of the land application of residuals generated by the residuals source -generating facilities listed in the most recently -certified Attachment A to the land application sites listed in the most recently -certified Attachment •B with no discharge of wastes to surface waters, pursuant to the permit modification and renewal application package received on May 20, 2002 as well as the additional information received on August 9, 2002 and June 27, 2003; and in conformity with the project plan, specifications, and other supporting data subsequently filed and approved by the Department of Environment and Natural Resources and considered a part of this permit. This permit shall be effective from the date of issuance until February 28, 2010; shall void Permit No. WQ0014543, issued on February 16, 1998; and shall be subject to the following specified conditions and limitations: . PERFORMANCE STANDARDS 1. The residuals land application program shall be effectively maintained and operated as a non - discharge system to prevent the discharge of any wastes resulting from the operation of this program. 2. This permit shall become voidable if the soils of the land application sites fail to assimilate the residuals adequately and may be rescinded unless the land application sites are maintained and operated in a manner that will protect the assigned water quality standards of the surface waters and groundwater. 3. The issuance of this permit shall not relieve the Permittee of the responsibility for damages to surface waters or groundwater resulting from the operation of this residuals land application program. 1 4. In the event that the residuals land application program is not operated satisfactorily, including the creation of nuisance conditions, the Permittee shall cease land applying residuals to the site, contact the Aquifer Protection Section of the appropriate Division of Water Quality's, (Division) regional office, and take any immediate corrective actions as may be required by the Division. 5. No residuals other than those generated by the residuals source -generating facilities listed in the most recently -certified Attachment A of this permit shall be approved for land application in accordance with this permit. . The pollutant concentrations in any residuals that are land applied to any land application site shall not exceed the following Ceiling Concentrations (i.e., dry weight basis): Parameter Ceiling Concentration (milligrams per kilogram) Arsenic 75 Cadmium 85 Copper 4,300 Lead 840 Mercury 57 Molybdenum . - 75 Nickel 420 - Selenium 100 Zinc 7,500 . 7. When residuals are land applied under the conditions of this permit, the Class A pathogen requirements and site restrictions . in 40 CFR Part 503.32(a) or the Class B pathogen requirements and site restrictions in 40 CFR Part 503.32(b), and one of vector attraction reduction requirements in 40 CFR Part 503.33 shall be met. Additionally, an evaluation shall be performed that demonstrates the residuals' ability to comply with this requirement. Upon request, a copy of this evaluation, including all test results and calculations, shall be submitted. Only residuals that are generated by the residuals source -generating facilities that are identified as being exempt from this condition in the most recently -certified Attachment A shall not be required to comply with, the specified pathogen reduction and vector attraction reduction requirements. 8 Only the land application sites listed in the most recently -certified Attachment B of this permit are approved for residuals land application. 9. This permit shall become . voidable unless the agreements between the Permittee and the landowners and lessees or operators of any land application sites listed in the most recently - certified Attachment B of this permit not owned by the Permittee are in full force and effect. These agreements shall be considered expired concurrent with the expiration date ' of the permit and shall be renewed at the same time the permit is renewed. 10 The appropriate local governmental official (i.e., county manager,. city manager, etc.) shall be notified at. least 24 hours prior to the initial residuals land application event to any new land application site. In addition, the appropriate county manager's office shall be notified prior to the initial residuals land application event on any new site so that they will be aware that residuals land application activities have commenced on the site. 11. The Aquifer Protection Section of the appropriate Division's regional office shall be notified at. least 24 hours prior to the initial residuals land application event on any new land application site. Such notification to the Regional Water Quality Supervisor shall be made during normal office hours (i.e., from 8:00 a.m. until 5:00 p.m.) between Monday and Friday, but excluding State Holidays. A list of the Division's regional offices, their county coverage, and their contact information may be downloaded from the web site at http://h2o.enr.state.nc.us/ndpu/. II. OPERATION AND MAINTENANCE REQUIREMENTS 1. The facilities and land application sites shall be properly maintained and operated at all times. 2. Upon classification of the residuals land application program by the Water Pollution Control System Operators Certification Commission (WPCSOCC), the Permittee shall designate a certified land application/residuals operator to be in responsible charge (ORC) of the program. The operator shall hold a certificate of the type classification assigned to the program by the WPCSOCC. The Permittee shall also designate a certified back-up operator of the appropriate type to comply with the conditions of 15A NCAC 8G .0202. 3. No residuals shall be. stored at any land application site at any time, unless written approval has first been requested and obtained from the Division. 4. A copy of this permit shall be maintained in all manned equipment at the land application sites when residuals are being land applied during the life of this permit. A spill prevention and control plan shall be maintained in all residuals transport and application vehicles. 5. When land applying residuals to any land application site, the following buffer zones shall be maintained at all times: a. 400 feet from residences or places of public assembly under separate ownership for surface application methods; however, the buffer zone requirement may be reduced to a minimum of 100 feet upon written consent of the owner and approval from the Aquifer Protection Section of the appropriate Division's regional office in Attachment B of this permit; b. 200 feet from residences or places of public assembly under separate ownership for subsurface application methods; however, the buffer zone requirement may be reduced to a minimum of 100 feet upon written consent of the owner and approval from the Aquifer Protection Section of the appropriate Division's regional office in Attachment B of this permit; c. 100 feet from any public or private water supply source, waters classified as SA or SB, and any Class I or Class II impounded reservoir used as a source of drinking water for both methods; d. 100 feet from any streams classified as WS or B, any other stream, canal, marsh or coastal waters and any other lake or impoundment for surface application; e. 50 feet from any streams classified as WS or B, any other stream, canal, marsh or coastal waters and any other lake or impoundment for subsurface application; f. 50 feet from property lines for both surface and subsurface application methods; g. 50 feet from public right of ways for both surface and subsurface application methods; h. . 10 feet from upslope interceptor drains and surface water diversions for both surface and subsurface application methods; and i. 25 feet from downslope interceptor drains, surface water diversions, groundwater drainage systems, and surface drainage ditches for both surface and subsurface application methods. 6. Maximum slope for land application of residuals shall be 10 percent for surface application methods and 18 percent for subsurface application methods. 7. Specific residuals land application area boundaries shall be clearly marked on each land application site prior to and during a residuals land application event. 8. The metal loading rates on any land application site shall not exceed the following Cumulative Pollutant Loading Rates (CPLRsI: Parameter CPLR (kilograms per hectare) CPLR (pounds per acre) Arsenic 41 36 Cadmium 39 34 Copper 1,500 1,338 Lead 300 267 Mercury 17 15 Molybdenum n/a n/a Nickel 420 374 Selenium 100 89 Zinc 2,800 2,498 An acceptable pH shall be maintained in the soil, residuals and lime mixture, greater than .6.0, on all land application sites onto which residuals are land applied to ensure optimum yield for the crops specified in Condition II. 13. The agronomist shall provide information on the pH best suited for the specified crop and the soil type. 10. Should any of the residuals generated by the residuals source -generating facilities listed in the most recently -certified Attachment A of this permit contain a high salt content (i.e., high sodium adsorption ratio (SAR) of five or higher), the exchangeable sodium percentage (ESP) or other method as approved by the Division, using the results from the annual soils analysis as required by this permit, shall be monitored on all of the land application sites. The local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina -licensed Soil Scientist, or other agronomist shall review the results and make recommendations regarding soil amendments (e.g., gypsum, etc.) or other ameliorative mechanism for maintaining the integrity of the site in terms of suitability for land application of residuals and maintaining conditions conducive to crop growth. The Permittee shall implement such recommendations accordingly and shall maintain written records of each monitoring event that includes details of the sites covered and rate of soil amendment application. 11. Prior to land applying residuals to any land application site that has previously received or is intended to receive animal waste (e.g., poultry litter, etc.) or other source of nutrients (e.g., fertilizer, etc.) in the future, the Permittee shall obtain information pertaining to the volume and analysis of the applied waste/nutrients from the landowner and/or lessee/operator of the site. The Permittee shall be responsible for verifying the volume of residuals that may be land applied to the site such that the plant available nitrogen (PAN) loading rate for the specified crop (i.e., see Condition II. 13.) shall not be exceeded by all of the sources of PAN applied. Should the maximum PAN loading rate be met or exceeded, then no additional residuals shall be land applied to the site. 12. A suitable vegetative cover, as listed in Condition II. 13., shall be maintained on land application sites onto which residuals are land applied in accordance with the crop management plan outlined by the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, or other agronomist and as approved by the Division. 13. Residuals and other sources of PAN shall be land applied to all land application sites at agronomic rates in accordance with the crop management plan outlined by the local Cooperative Extension Office, the North Carolina Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, or other agronomist. Under no circumstances shall the following PAN loading rates land applied to any site exceed the following for the specified crops: Crop PAN (pounds per Crop PAN (pounds per acre per year) Alfalfa 200 Forest (Hardwood or'Softwood) 75 Bermuda Grass (Hay or Pasture) 220 Milo 100 Blue Grass 120 Small Grain (Wheat, Barley, or Oats) 100 Corn (Grain) 160 Sorghum or Sudex (Pasture) 180 Corn (Silage) 200 Sorghum or Sudex (Silage) 220 Cotton 70 Soybeans 200 Fescue • 250 Timothy, Orchard, or Rye Grasses 200 The Permittee shall apply for and receive a modification of this permit before land applying residuals on any land application site that is to be established in a crop other than those listed above. A maximum PAN loading rate for the desired crop shall be approved with the permit modification. . If the land application sites are to be overseeded (e.g., bermuda grass in the summer and rye grass in the winter with BOTH crops to receive residuals), then the second crop shall receive an application of PAN at a rate of no greater than 50 pounds per acre per year. This practice shall be allowed as long as the second crop is to be harvested. If the second crop is to be planted for erosion control only and is to be tilled into the soil, then no residuals shall be land applied to these sites because the PAN will essentially be retumed to the soil. 5 Residuals shall not be land applied at rates greater than agronomic rates, unless authorized by the Division. 14. Animals shall not be grazed on any land application site for 30 days after any residuals land application event. Sites that are to be used for grazing shall have fencing that will be used to prevent access after each event. 15. Food crops, feed crops, and fiber crops that do not come in contact with the residuals shall not be harvested for 30 days after any residuals land application event. 16. Food crops with harvested parts that touch the residual/soil mixture and .are totally above the land surface (e.g., tobacco, melons, cucumbers, squash, etc.) shall not be harvested for 14 months after any residuals land application event. 17. Food crops with harvested parts below the surface of the land (i.e., root crops such as potatoes, carrots, radishes, etc.) shall not be harvested for 20 months after any residuals land application event when the residuals remain on the land surface for four months or longer prior to incorporation into the soil. 18. Food crops with harvested parts below the surface of the land shall not be harvested for 38 months after any residuals land application event when the residuals remain on the land surface for less than four months prior to incorporation into the soil. 19. Turf shall not be harvested for one year after any residuals land application' event. 20. Adequate provisions shall be taken to prevent wind erosion and surface runoff from conveying residuals from the land application sites onto adjacent properties or into any surface waters. 21. Adequate procedures shall be provided to prevent surface runoff from carrying any land applied or stored residuals into any surface waters. 22. Surface -applied residuals shall be plowed or disced within 24 hours after land application on land application sites with no cover crop established. 23. For land application sites that are prone to flooding or within the 100-year flood elevation, residuals shall be land applied only during periods of dry weather. The residuals shall be incorporated into the soil within 24 hours after land application. 24. Residuals shall not be land applied during inclement weather or until 24 hours following a rainfall event of 0.5-inch or greater in 24 hours. Any emergency residuals land application measures shall first be approved in writing by the Division. 25. Residuals shall not be land applied to any land application site that is flooded, frozen, or snow-covered. 26 Appropriate measures shall be taken to control public access to the land application sites during active site use and for the 12-month period following the last residuals land application event. Such controls may include the posting of signs indicating the activities being conducted at each site. I1T. MONITORING AND REPORTING REQUIREMENTS 1. Any monitoring (Le., including groundwater, surface water, residuals, soil, or plant tissue analyses) deemed necessary by the Division to ensure protection of the environment shall be established, and an acceptable sampling and reporting schedule shall be followed. 2. Residuals generated by each residuals source -generating facility listed in the most -recently - certified Attachment A of this permit shall be analyzed to demonstrate that they are non- hazardous under the Resource Conservation and Recovery Act (RCRA). A corrosivity, ignitability, and reactivity analysis as well as a•Toxicity Characteristics Leaching Procedure (TCLP) analysis shall be conducted on residuals generated by .each .residuals source - generating facility listed in the most recently -certified Attachment A of this permit. The analyses shall be performed at the frequency specified in the most recently -certified Attachment A of this permit, and the results shall be maintained on file by the Permittee for a minimum of five years. If residuals generated by a particular residuals source -generating facility are land applied at a frequency less than that which is specified in the most recently - certified Attachment A of this permit, the analyses shall be required for each residuals land application event. Only residuals that are generated by the residuals source -generating facilities that are identified as being exempt from this condition in the most recently -certified Attachment A of this permit shall not be. required to comply with this monitoring requirement. The TCLP analysis shall include the following parameters (i.e., note the regulatory level in milligrams per liter in parentheses): Arsenic (5.0) Barium (100.0) Benzene (0.5) Cadmium (1.0) Carbon tetrachloride (0.5) Chlordane (0.03) Chlorobenzene (100.0) Chloroform (6.0) Chromium (5.0) m-Cresol (200.0) o-Cresol (200.0) p-Cresol (200.0) Cresol (200.0) 2,4-D (10.0) 1,4-Dichlorobenzene (7.5) 1,2-Dichloroethane (0.5) 1,1-Dichloroethylene (0.7) 2,4-Dinitrotoluene (0.13) Endrin (0.02) Hexachlorobenzene (0.13) Heptachlor (and its hydroxide) (0.008) Hexachloro-1,3-butadiene (0.5) Hexachloroethane (3.0) Lead (5.0) Lindane (0.4) Mercury (0.2) Methoxychlor (10.0) Methyl ethyl ketone (200.0) Nitrobenzene (2.0) Pentachlorophenol (100.0) Pyridine (5.0) Selenium (1.0) Silver (5.0) Tetrachloroethylene (0.7) Toxaphene (0.5) Trichloroethylene (0.5) 2,4,5-Trichlorophenol (400.0) 2,4,6-Trichlorophenol (2.0) 2,4,5-TP (Silvex) (1.0) Vinyl chloride (0.2) After the residuals have been monitored as specified above for two years at the frequency specified in the most recently -certified Attachment A of this permit, the Permittee may submit a request to the Division for a permit modification to request a reduction of this monitoring requirement. In no case, however, shall the frequency of monitoring be less than once per permit cycle. 3. An analysis shall be conducted on residuals generated by each residuals source -generating facility listed in the most recently -certified Attachment A of this permit. The analysis shall be performed at the frequency specified in the most recently -certified Attachment A of this permit, and the results shall be maintained on file by the Permittee for a minimum of five years. If residuals generated by a particular residuals source -generating .facility are land applied at a frequency less than that which is specified in the most recently -certified Attachment A of this permit, an analysis shall be required for each residuals land application event. The analysis shall include, but shall not necessarilybe limited to, the following parameters: Aluminum Ammonia -Nitrogen Arsenic Cadmium Calcium Copper Lead Magnesium Mercury Molybdenum Nickel Nitrate -Nitrite Nitrogen Percent Total Solids pH Phosphorus Potassium Selenium. Sodium Total Kjeldahl Nitrogen Zinc Plant Available Nitrogen. (by calculation) After the residuals generated by a particular residuals source -generating facility have been monitored for two years at the frequency specified in the most recently -certified Attachment A of this permit, the Permittee may submit a request to the Division for a permit modification to reduce the frequency of this monitoring requirement. In no case, however, shall the frequency of this monitoring be less than once per year when a residuals land application event of residuals generated by the residuals source -generating facility occurs during that year. 4. Residuals generated by each residuals source -generating facility listed in the most recently - certified Attachment A of this permit shall be monitored for compliance with Condition I. 7. The monitoring shall be performed at the frequency specified in the most recently -certified Attachment A of this permit, and data to verify pathogen and vector attraction reduction of the residuals shall bemaintained on file by the Permittee for a minimum of five years. The required data shall be specific to the stabilization process utilized, but also shall be sufficient to demonstrate clear compliance with the Class A pathogen reduction requirements in 40 CFR Part 503.32(a) or the Class B pathogen reduction requirements and site restrictions in 40 CFR Part 503.32(b) as well as one of vector attraction reduction requirements in 40 CFR Part 503.33. In addition, the Environmental Protection Agency (EPA) certification statements concerning compliance with pathogen reduction requirements, vector attraction reduction requirements, and management practices shall be completed at the frequency specified in the most recently -certified Attachment A of this permit by the proper authority or authorities, if more than one is involved (i.e., either the person who prepares the residuals, the person who derives the material, or the person who applies the residuals). Only residuals that are generated by the residuals source -generating facilities that are identified as being exempt from Condition I. 7. in the most recently -certified Attachment A of this permit shall not be required to comply with this monitoring requirement. 5. Laboratory analyses as required by Condition III. 2., Condition III. 3., and Condition III. 4. shall be performed/gathered on the residuals - as they are to be land applied. Furthermore, analytical determinations made pursuant to the monitoring and reporting requirements of this permit shall be made by a laboratory certified by the Division for the required parameter(s) under 15A NCAC 2H .0800 or 15A NCAC 2H .1100. 8 6. Proper records shall be maintained by the Permittee tracking all residuals land application events. These records shall include, but are not necessarily limited to, the following information: a. Source of residuals; b. Date of land application; c. Location of land application (i.e., site, field, or zone number); d. Method of land application; e. Weather conditions (i.e., sunny, cloudy, raining, etc.); f. Soil conditions (i.e., dry, wet, frozen, etc.); g. Type of crop or crops to be grown on field; h. Volume of residuals land applied in gallons per acre, dry tons 'per acre, or kilograms per hectare; i. Volume of animal waste or other nutrient source applied in gallons per acre, dry ton per =acre, or kilograms per hectare (if applicable); Volume of soil amendments (i.e., lime, gypsum, etc:) applied in gallons per acre, dry ton per acre, or kilograms per hectare (if applicable); and k. Annual and cumulative totals of dry tons per acre of residuals as well as animal waste and other sources of nutrients (i.e., if applicable), annual and cumulative pounds per acre of each heavy metal (i.e., shall include, but shall not be limited to, arsenic, cadmium, copper, lead, mercury, molybdenum, nickel, selenium, and zinc), annual pounds per acre of PAN, and annual pounds per acre of phosphorus applied to each field. 7. A representative annual soils analysis (i.e., Standard Soil Fertility Analysis) shall be conducted on each land application site on which a residuals land application event in the respective calendar year has occurred or is to occur, and the results shall be maintained on file by the Permittee for a minimum of five years. The Standard Soil Fertility Analysis shall include, but is not necessarily limited to, the following parameters: Acidity Calcium Cation Exchange Capacity Copper Base Saturation (by calculation) Exchangeable Sodium Percentage (by calculation) Magnesium Phosphorus Manganese Percent Humic Matter pH Potassium Sodium Zinc. 8. Three copies of all required monitoring and reporting requirements as specified in Condition III. 1., Condition III. 2., Condition III. 3., Condition M. 4., Condition III, 5., Condition III, 6., and Condition III. 7. shall be submitted annually on or before March 1st of the year following the residuals land application event to the following address: NCDENR-DWQ Information Processing. Unit. 1617 Mail Service Center Raleigh, North Carolina 27699-1617 9. Noncompliance Notification: The Permittee shall report by telephone to the Aquifer Protection Section of the Division's Mooresville Regional Office at telephone number 704-663-1699, as soon as possible, but in no case more than 24 hours or on the next working day following the occurrence or first knowledge of the occurrence of any of the following: a. Any occurrence with the residuals land application program that results in the land application of significant amounts of residuals that are abnormal in quantity or characteristic. b. Any failure of the residuals land application program resulting in a release ofmaterial to receiving waters. c. Any time that self -monitoring information indicates that the residuals land application program has gone out of compliance with the conditions and limitations of this permit or the parameters on which the program system was designed. d. Any process unit failure, due to known or unknown reasons, that render the residuals land application program incapable of adequate residuals treatment. _ e. Any spillage or discharge from a vehicle or piping system transporting residuals to the application site. Persons reporting such occurrences by telephone shall also file a written report in letter form within five days following first knowledge of the occurrence. This report shall outline the actions taken or proposed to be taken to ensure that the problem does not recur. IV. GROUNDWATER REQUIREMENTS 1. Land Application Site Requirements: a. Each land application site identified with a GW-A in the most recently -certified Attachment B of this permit is dominated by soils with a mean seasonal high water table greater than three feet below the land surface. Residuals land application events may occur on these sites throughout the year. b. Each land application site identified with a GW-B in the most recently -certified Attachment B of this permit is dominated by soils with a mean seasonal high water table between one and three feet below the land surface. Residual land application events on these sites shall be prohibited from December through March, inclusive. No residuals shall be land applied to these sites when the vertical separation between the depth of residuals land application and the water table is less than three feet. The actual water table depth for seasonally -restricted soils shall be verified by soil borings within 24 hours prior to any residuals land application event that occurs from April through November, inclusive. The number of borings advanced shall be sufficient to characterize water table conditions across the land application site adequately. Any open borings shall be properly filled with native soil, prior to the residuals land application event, to decrease the chance of any residuals contaminating the groundwater. 10 2. Applicable Boundary Requirements: a. The COMPLIANCE BOUNDARY for residuals land application programs is specified by regulations in 15A NCAC 2L (i.e., "Groundwater Classifications and Standards"). The Compliance Boundary for each land application site is established at either 250 feet from the residuals land application area or 50 feet within the property boundary, whichever is closest to the residuals land application area. An exceedance of Groundwater Quality Standards at or beyond the Compliance Boundary is subject to immediate remediation action according to 15A NCAC 2L .0106 (d)(2). b. The REVIEW BOUNDARY shall be established around each land application site midway between the Compliance Boundary and the perimeter of the residuals land application area. Any exceedance of Groundwater Quality Standards at the Review Boundary shall require action in accordance with 15A NCAC 2L .0106 (d)(2). 3. Additional Requirements: a. Any groundwater quality monitoring, as deemed necessary by the Division, shall be provided. V. INSPECTIONS 1. Prior to each residuals land application event, the Permittee or his designee shall inspect the residuals storage, transport, and application facilities to prevent malfunctions and deterioration, operator errors, and discharges that may cause or lead to the release of wastes to the environment, a threat to human health, or a nuisance. The Permittee shall maintain an inspection Iog or summary including at least the.. date and time of inspection, observations made, and any maintenance, repairs, or corrective actions taken by the Permittee. This log of inspections shall be maintained by the Permittee for a period of five years from the date of the inspection and shall be made available to the Division or other permitting authority, upon request. 2. Any duly authorized officer, employee, or representative of the Division may, upon presentationof credentials, enter and inspect any property, premises, or place on or related to the land application sites or facilities at any reasonable time for the purpose of determining compliance with this permit; may inspect or copy any records that must be kept under the terms and conditions of this permit; and may obtain samples of groundwater, surface water, or leachate. VI. GENERAL CONDITIONS 1. This permit shall become voidable unless the residuals land application events are carried out in accordance with the conditions of this permit, the supporting materials, and in the manner approved by the Division. 2.. This permit shall be effective only with respect to the nature and volume of residuals described in the application and other supporting data. 3. Failure to abide by the conditions and limitations contained in this permit may subject the Permittee to an enforcement action by the Division in accordance with North Carolina General Statutes § 143-215.6A through § 143-2.15.6C. 11 4. The annual administering and compliance fee shall be paid by the Permittee within 30 days after being billed by the Division. Failure to pay the fee accordingly may cause the Division to initiate action to revoke this permit, as specified by 15 NCAC 2H .0205 (c)(4). 5 The issuance of this permit does not preclude the Permittee from complying with any and all statutes, rules, regulations, or ordinances that may be imposed by other government agencies (i.e., local, state, and federal) which have jurisdiction, including, but not limited to, applicable river buffer rules in 15A NCAC 2B .0200, soil erosion and sedimentation control requirements in 15A NCAC Chapter 4 and under the Division's General Permit NCG010000, and any requirements pertaining to wetlands under 15A NCAC 2B .0200 and 15A NCAC .0500. 6. This permit may be modified, revoked, and/or reissued to incorporate any conditions, Iirnitations and monitoring requirements the Division deems necessary in order to protect the environment and public health adequately. 7. The Permittee, at least six months prior to the expiration of this permit, shall request its extension. Upon receipt of the request, the Division shall review the adequacy of the facilities and residuals land application program described therein, and if warranted, shall extend the permit for such period of time and under such conditions and limitations as it may deem appropriate. 8. This permit shall not be automatically transferable. In the event that there is a desire for the residuals land application program to change ownership or to change the name of the Permittee, a formal permit request shall be submitted to the Division documentation from the parties involved and other supporting materials as may be appropriate. The approval of this request shall be considered on its merits and may or may not be approved. Permit issued this the eleventh day of March, 2005. NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION for Alan W. Klimek, P.E., Director Division of Water Quality By Authority of the Environmental Management Commission Permit Number WQ0014543 12 ATTACHMENT A - Approved Residual Source -Generating Facilities Permit No. WQ00014543 City of Statesville City of Statesville Residuals Laud Application Program Owner Facility Name County Permit Number Issued By Is 503? Maximum Dry Tons Per Year Monitoring Frequency for Condition III. 2. Monitoring Frequency for Condition III. 3. and Condition III. 4. Approved Mineralization Rate City of Statesville Fourth Creek WWTPa Iredell NC0031836 DWQ 503 1057.00 Annually Quarterly .30 City of Statesville Third Creek WWTPa Iredell NC0020591 DWQ 503 975.73 Annually Quarterly .30 Total 2,032.73 he dry tons per year of residuals listed for this residuals source -generating facility represents the total maximum volume of residuals generated by this facility and may not be equivalent to the volume of residuals that may be land applied to the land application sites approved in the most recently -certified Attachment B per year. In accordance with Condition II. 13., residuals shall be land applied at not greater than agronomic rates and, therefore, only that volume of residuals that may be assimilated by the approved sites shall be land applied. Permit No. WQ0014543 Page 1 of 1 Certification Date: March 11, 2005 ' li ,4%- 11 itY71! • 7 N T V Third. Creek g Fourzn ID ;\,1 A • III 1--k Creek Sizes - Property Line City Limits Line- 100. 00' \j6Li#1, I- Do 14543 FOURTH CREEK SITE Tract Acreage: 15.3 Buffer Acreage: 7.7 Total : Acreage: 23. 0 Drawing Scale: 1 =200' Watson, Edward M From: Sent: To: Subject: Andy Smith <asmith@statesvillenc.net> Wednesday, November 21, 2018 10:16 AM Watson, Edward M [External] 4th Creek Contact Information Ed, Ken Galloway is now the 4th Creek WWTP Supervisor and will be your contact for all of the residuals. You can reach him at the office # 704-878-3438 and his email is Ken Galloway <kgalloway@statesvillerc.net> Andy Smith, Assistant Director Water Resources Pursuant to NCGS Chapter 132, Public Records, this electronic mail message and any attachments hereto, as well as any electronic mail messages that may be sent in response to it may be considered public record and as such are subject to request and review by anyone at any time. If you are not the intended recipient of this message, please delete this message and inform the sender. i D_ R _ _ Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources WATER QUALITY REGIONAL OPERATIONS SECTION NON -DISCHARGE APPLICATION REVIEW REQUEST FORM To: I O-WQ:RTOS-: An drew Pitney July 26, 2018 RECEIVED/NCDENR/DWR /1@orey asing+ From: Troy Doby, Water Quality Permitting Section - Non -Discharge Branch JUL 31 2018 WQROS MOORESVILLE REGIONAL OFFICE Permit Number: WQ0014543 Permit Type: Land Application of Residual Solids (503) Applicant: City of Statesville Project Type: Renewal Owner Type: Municipal Owner in BIMS? Yes Facility Name: City of Statesville RLAP Facility in BIMS? Yes Signature Authority: Andy Smith Title: Assistant Director of Water Resources Address: PO Box 1111, Statesville, NC 28687-1111 County: Iredell Fee Category: Non -Discharge Minor Fee Amount: $0 - Renewal Comments/Other Information: Attached, you will find all information submitted in support of the above -referenced application for your review, comment, and/or action. Within 45 calendar days, please take the following actions: ® Return this form completed. I Return a completed staff report. n Attach an Attachment B for Certification. ❑ Issue an Attachment B Certification. When you receive this request form, please write your name and dates in the spaces below, make a copy of this sheet, and return it to the appropriate Central Office Water Quality Permitting Section contact person listed above. RO-WQROS Reviewer: Date: FORM: WQROSNDARR 09-15 Page 1 of 1 ROY COOPER cAlwonor MICHAEL S. R EGAN Secr ears. LINDA CULPEIPPER in(theta D&ertdry q Il-J]• 4tau NORTH CAROLINA Environmental Quality July 27, 2018 ANDY SMITH —ASSISTANT DIRECTOR OF WATER RESOURCES CITY OF STATESVILLE PO BOx 1111 STATESVILLE, NORTH CAROLINA 28687-1111 Subject: Acknowledgement of Application No. WQ0014543 City of Statesville RLAP Residuals Management System Iredell County Dear Mr. Smith: The Water Quality Permitting Section acknowledges receipt of your permit application and supporting documentation received on July 25, 2018. Your application package has been assigned the number listed above, and the primary reviewer is Troy Doby. Central and Regional Office staff will perform a detailed review of the provided application, and may contact you with a request for additional information. To ensure maximum efficiency in processing permit applications, the Division of Water Resources requests your assistance in providing a timely and complete response to any additional information requests. Please note that processing standard review permit applications may take as long as 60 to 90 days after receipt of a complete application. If you have any questions, please contact Troy Doby at (919) 707-3655 or troy.doby@ncdenr.gov. Sincerely, Nathaniel D. Thornburg, Supervisor Division of Water Resources cc: MporesSille"1Ze ionalzOfice;-7ater,,Quah yt R�eg_ibnal7,Op anions-e ctionr Permit File WQ0014543 ivaeerr.idlir 7e,niarti�,� \.dore‘ North Carolina Department of Environmental Quality I Division of Water Resources I Non -Discharge Branch 512 North Salisbury Street 11617 Mail Service Center I Raleigh, North Carolina 27699-1617 919.707.3654 CITYt of \'/ tae ejNORTH CAROLINA May 11,2018 Mr. Troy Doby, PhD, PE Non -Discharge Permitting Unit Water Quality Permitting Section Raleigh Central Office 1617 Mail Service Center Raleigh, NC 27699-1636 Re: City of Statesville Land Application Program Permit Renewal Permit No. WQ0014543 Dear Mr. Doby: The City of Statesville is requesting a permit renewal for permit # WQ0014543. RECEIVED/NCDEQ/DWR JUL 2 5 2018 Non-pischarge Permitting Unit Enclosed you will find Forms RLAP 06-16, RSC 06-16 and LASC 06-16 with additional supporting documents per the instruction sheet for the aforementioned forms. The following is a list of these documents. • A brief narrative explaining how the City of Statesville handles its bio solids. How the residuals are processed and treated, where the residuals will be stored and how the residuals will be distributed. • Lab data. • Vicinity maps. • Flow Schematic. • Spill Control Plan. • Sampling schedule for the bio-solids. • Sample and Monitoring Plan Narrative. CC: City of Statesville PO Box 1111 • Statesville, NC 28687 • ci.statesville.nc.us CITY of tatee NORTH CAROLINA The following is a brief narrative regarding the sludge management plan for the City of Statesville: • Bio solids generated at both of the WWTP's. The bio-solids at both of these facilities are currently stabilized using an aerobic digester and dewatered using a 2 meter belt filter press. After dewatering, the residuals are transferred by a dump truck to the sludge storage pad or pumped to the existing Sta-Lime processing area. After the Sta- Lime process has been completed, the final product is made available to the local farmers at no cost or set aside for land application by a private contractor through an existing agreement held with the City. The permit WQ0014543 has never been utilized and is considered a back-up to the existing permit's in the City of Statesville sludge management program. Should you require more information, or if further action is required, you can contact me at 704-878-3438 or email me at asmith@statesvillenc.net ndy S . ith Plant Supervisor, Fourth Creek WWTP PO Box 1111 • Statesville, NC 28687 • ci.statesville.nc.us Dvision of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources 15A NCAC 02T .1100 — RESIDUALS LAND APPLICATION PROGRAM INSTRUCTIONS FOR FORM: RLAP 06-16 & SUPPORTING DOCUMENTATION Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This application is for treatment, storage, transport, and/or land application of Class B residuals (may include residuals that are generated from a water treatment plant or other type facilities) on the proposed or currently approved land application site(s) under 15A NCAC 02T .1100. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Land Application Program (FORM: RLAP 06-16) Application: (All Application Packages): Submit the completed and appropriately executed Residuals Land Application Program (FORM: RLAP 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® The Applicant's Certification on Page 5 of this form shall be signed in accordance with _OA NOAC 0 .0106N. An alternate person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in i A NCAC On .O i 06(b). ❑ If this project is for a modification of an existing permit, submit one copy of the existing permit. ® Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units. B. Application Fee (New and Major Modification Application Packages) ® Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental Quality (NCDEQ). Facility Classification New Permit Major Modification 1 Major (land are permitted for > 300 acres) $1,310 i $395 Minor (land are permitted for < 300 acres) $810 j $245 1- A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage; adds additional land application areas not previously approved for that particular program [including transferring of field(s) from one program to another]; adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted. There is no fee for minor modifications to a permit. C. Cover Letter (All Application Packages) ® List all items included in the application package, as well as a brief description of the requested permitting action. D. Environmental Assessments (Maybe Required — See 15A NCAC 1C .0300) ❑ Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for the construction of the subject facilities. RECEIVEDINC®EU®WR INSTRUCTIONS FOR FORM: RLAP 06-16 JUL 2 5 2018 Non -Discharge Permitting Unit Page 1 of 3 E. Operation and Maintenance Plan (New and Renewal Application Packages) ❑ For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan. ® Submit the O&M Plan in accordance with 15A NCAC 02T .1110 and include at a minimum: ® Operational functions; describe the operation of the program to show what operations are necessary for the program to function and by whom the functions are to be conducted. ® Maintenance schedules; may include equipment calibration, maintenance of signs, etc. ® Safety measures; may include safety training program, manuals, signs, etc. ® Spill response plan; including control, containment, remediation, emergency contact information, etc. E Inspection plan including the following information; Names and titles of personnel responsible for conducting the inspections. E Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program. ® Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed. E Sampling and monitoring plan including the following information; ® Names and titles of personnel responsible for conducting the sampling and monitoring. ►1 Detailed description of monitoring procedures including parameters to be monitored. Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures. THE FOLLOWING ADDITIONAL ITEMS (G to M) ARE REQUIRED FOR DEDICATED PROGRAM ONLY. F. Program Determination ❑ Dedicated residuals land application programs are ones in which land application sites meet the criteria in i $A NCAO ill 11 OM). Vi). Specifically, a residuals land application program is designated as dedicated if any of the following are applicable: ❑ Any land application site certified for the residuals land application program that receives residuals at rates or frequencies greater than agronomic rates. ❑ Any land application site certified for the residuals land application program that is used primarily for residuals disposal, and agricultural crop production is of secondary importance. ❑ Any land application site certified for the residuals land application program that receives residuals through fixed irrigation facilities or irrigation facilities fed through a fixed supply system. ❑ Please contact the Non -Discharge Permitting Unit if you need any assistance in determining whether your residuals program falls under the dedicated program definitions. G. Program Information ❑ Provide an explanation of why a dedicated system is required instead of a conventional non -dedicated system. ❑ Provide an explanation of the dedicated system and its operation. H. Detailed Site Maps (All New or Modification Application Packages) ❑ Submit three (3) sets of standard size plans and two (2) sets of 11" by 17" plans (electronic format is acceptable - Adobe PDF only). For Modifications, submit plans specific to the modification(s) only. ❑ Plans must include the following minimum items: ❑ A general location map, a vicinity map and a topographic map with contours not exceeding 10 feet or 25% of the total site relief and showing all facility related structures and fences within the land application area. ❑ The location of all wells (including usage and construction details if available), streams (ephemeral, intermittent, and perennial), springs, lakes, ponds, and other surface drainage features within 500 feet of the land application site(s). ❑ Delineation of the review and compliance boundaries ❑ Setbacks as required by 15A NCAC 02T .1108 ❑ Site property boundaries within 500 feet of all waste treatment, storage, and disposal site(s). ❑ A map showing the entire irrigation area with an overlay of the suitable irrigation area depicted by the soil scientist's evaluation. The irrigation plans shall show each nozzle/emitter and wetted area (when applicable). Clearly label spray irrigation zones as they will be operated. ❑ Plans must depict a completed design and not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR CONSTRUCTION, etc.) that indicate that they are anything other than final plans. However, the plans may be labeled with the phrase: FINAL DESIGN - NOT RELEASED FOR CONSTRUCTION INSTRUCTIONS FOR FORM: RLAP 06-16 Page 2 of 3 7 Project Evaluation and Receiver Site Management Plan (All New Application Packages or Modifications that include new sites) ❑ Submit a project evaluation and a receiver site management plan (if applicable) with recommendations concerning cover crops and their ability to accept the proposed application rates. J. Hydrogeologic Report (All New Application Packages or Modifications involving increasing the total design capacity) ❑ Submit a detailed hydrogeologic evaluation in accordance with 15A NCAC 02T .1104(d)(4) and current Division Policy available at: http://www.ncwater.org/Rules Policies and Regulations/. The document shall be signed, sealed and dated by a qualified professional. K. Engineering Design Documents (All New or Modification Application Packages with fixed irrigation facilities or irrigation facilities fed through fixed supply system) ❑ Submit engineering design documents that have been signed, sealed, and dated by a NC licensed Professional Engineer and/or Professional Land Surveyor in accordance with 15A NCAC 02T .1 104(d)(2). For Modifications, submit an updated site map specific to the modification(s) only. ❑ The design documents must include the following minimum items: ❑ Engineering plans for the facility and equipment except those previously permitted unless they are directly tied into the new units or are critical to the understanding of the complete process; ❑ Specifications describing materials to be used, method of construction, and means for ensuring quality and integrity of the finished product including leaking testing; and ❑ Engineering calculations including hydraulic and pollutant loading, sizing criteria, hydraulic profile, total dynamic head curve analysis for each pump, and irrigation design. ❑ Soil mapping units shown on all disposal sites. L. Water Balance (All New Application Packages or Modifications that include new sites utilizing fixed irrigation facilities or irrigation facilities fed through fixed supply systems) ❑ Submit a completed and accurate water balance in accordance with 1 A N AC 02T .11941(1)(5) and current Division Policy available at: http;[Lwwoutcwater,or$/Rules_ Pelir,it jnd, ettlat(on L. M. Property Ownership Documentation (All New or Modification Application Packages involving new and/or relocated treatment or irrigation components) ❑ Property ownership documentation shall consist of one of the following: ❑ Legal documentation of ownership (i.e., MR, deed or article of incorporation), or ❑ Written notarized intent to purchase agreement signed by both parties with a plat or survey map, or ❑ An easement running with the land specifically indicating the intended use of the property and meeting the requirements of I sA CAC f1 1i .0101(1j, or ❑ A written notarized lease agreement signed by both parties, indicating the intended use of the property, as well as a plat or survey map. ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS: NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES WATER QUALITY PERMITTING SECTION NON -DISCHARGE PERMITTING UNIT By U.S. Postal Service: 1617 MAIL SERVICE CENTER RALEIGH, NORTH CAROLINA 27699-1617 TELEPHONE NUMBER: (919) 807-6464 By Courier/Special Delivery: 512 N. SALISBURY STREET RALEIGH, NORTH CAROLINA 27604 FAX NUMBER: (919) 807-6496 INSTRUCTIONS FOR FORM: RLAP 06-16 Page 3 of 3 State of North Carolina Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 — RESIDUALS LAND APPLICATION PROGRAM FORM: RLAP 06-16 I. APPLICANT INFORMATION: 1. Applicant's name: Applicant type: ❑ Individual ❑ Corporation ❑ General Partnership ❑ Privately -Owned Public Utility ❑ Federal ❑ State X❑ Municipal ❑ County Signature authority's name per 15A NCAC 02T .0106: Andy Smith Title: Assistant Director of Water Resources Applicant's mailing address: PO Box 1111 City: Statesville State: NC Zip: 28687-1111 Telephone number: (704) 878-3438 Email Address: asmith@statesvillenc.net 2. Consultant's name: License Number (for P.E.): Affiliation: ❑ On Staff ❑ Retained (Film: ) Consultant's mailing address: City: State: Telephone number: ( 3. Agronomist's name: Affiliation: ❑ N/A ❑ On Staff Agronomist's mailing address: City: State: Telephone number: (_) 4. Soil Scientist's name: Affiliation: ❑ N/A ❑ On Staff Soil Scientist's mailing address: City: State: Telephone number: ( ) 5. Fee submitted: $810 (See Instruction B) ') H. PERMIT INFORMATION: Zip: Email Address: License Number: 111 Retained (Firm: Zip: - Email Address: License Number: ❑ Retained (Firm:. ) Zip: Email Address: RECEIVED/NCDEQ/DWR JUL 2 5 2018 Non -Discharge Permitting Unit 1. Application is for (check all that apply): ❑ new, ❑ modified, X❑ renewed permit 2. If this application is being submitted to renew or modify an existing permit, provide the following: Permit number: W00014543 Date of most -recently issued permit: September, 2013 Date of most -recently certified Attachment A (if different than the permit): Date of most -recently certified Attachment B (if different than the permit): FORM: RLAP 06-16 Page 1 of 5 6 III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION: 1. Residuals Processing Facility's physical address: 693 Bell Farm Road City: Statesville State: NC Zip: 28677- Coordinates: Latitude: 25° 46' 29 N" Longitude: 80° 48' 50 W" Level of accuracy: Datum: Method of measurement: GPS 2. County where residuals land application program is headquartered: Iredell 3. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application program, their certification numbers, and their affiliations in the following table: Designation Name Affiliation Certification Number ORC Andy Smith City of Statesville LA 985516 Back -Up ORC Scott Austin City,of Statesville LA 991939 Additional Back -Up ORCs (if applicable) If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application program, provide the candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training school and certification test: 4. Complete the following tables regarding management of the residuals land application program: a. Plant Available Nitrogen Summary: Determine the maximum plant available nitrogen (PAN) generated by all residuals source -generating facilities as currently certified and proposed for certification with this application and list the results in the following table: Maximum amount of residuals to be certified: 4th Creek @ 1,056 dry tons per year. PAN Pounds of PAN per Dry Ton (Weighted Average) Pounds of PAN per Year Surface Incorporation or Injection Surface Incorporation or Injection First -Year 36.6 mg/kg 38,6501bs Five -Year Maximum Adjusted 183 mg/kg 193,2481bs b. Land Application Site Use Summary: Summarize information regarding the land application sites as currently certified and proposed for certification with this application: Category Use Acres Comments Crops Forest or Plantation Row Crops 15.3 Corn & Small Grain Hay Pasture Total: Methods Surface Incorporation or Injection Total: FORM: RLAP 06-16 Page 2 of 5 c. Residuals Land Application Summary: Determine the minimum acreage required to land apply the residuals as currently certified and proposed for certification assuming the scenarios listed in the following table: Assumed Application Rate (lbs PAN/ac yr) Acres Required Using First -Year PAN Concentrations Acres Required Using Five -Year Maximum Adjusted PAN Concentrations Surface Incorporation or Injection Surface Incorporation or Injection 50 773 3,865 100 387 1,935 150 258 1,290 200 193 965 6. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application of the proposed residuals due to the violation of North Carolina Administrative Code (e.g. not enough storage, not enough land, vector reduction practices not in place, etc.): 7. Specify type of residuals program (See Instruction F): X❑ Non -dedicated❑ Dedicated If Dedicated, specify the following (check all that apply): ❑ Residuals program contains any land application site(s) that receives residuals at rates or frequencies greater than agronomic rates, explain; ❑ Residuals program contains any land application site(s) that is used primarily for residuals disposal, and agricultural crop production is of secondary importance, explain; ❑ Residuals program contains any land application site(s) that receives residuals through fixed irrigation facilities or irrigation facilities fed through a fixed supply system, explain; IV. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source) Complete and submit the following Residuals Source Certification and all associated documentation. Residuals Source Certification V. LAND APPLICATION SITE INFORMATION: (Required for all new, renewed, or modified land application site) Complete and submit the following Land Applications Site Certification and all associated documentation. Land Application Site Certification. doc FORM: RLAP 06-16 Page 3 of 5 Note: Item VI. Applicable to Dedicated Program with fixed irrigation system only. VI. DESIGN INFORMATION FOR FIXED IRRIGATION SYSTEM 1. The irrigation system is: ❑ Spray ❑ Drip 2. Disposal system is: ❑ existing ❑ proposed. 3. Minimum depth to mean seasonal high water table (SHWT) within irrigation sites(s) per Soil Scientist's Evaluation: feet below ground surface. Rules 15A NCAC 02T .0505(p) requires at least one -foot vertical separation between SHWT and ground surface. 4. Are there any artificial drainage or water movement structures within 200 feet of any irrigation area? EI Yes or ❑ No If Yes, please explain if the soil scientist report addresses artificial structures and please indicate if structures are to be maintained or modified: 5. Loading rates recommended by the Soil Scientist Evaluation: Soil Series Fields within Soil Area Recommended Loading Rate (in/hr) Recommended Loading Rate (in/yr) 6. Design loading rates are equal or less than the loading rates recommended by Soil Scientist? ❑ Yes or ❑ No If No, explain why .g) is not met: 7. Non -dedicated System Design (fill in the appropriate information for either a spray or drip irrigation system): Field / Zone Design Area (ft2) Number of Nozzles Maximum Application Rate (gallons/hr) Design Annual Loading Rate (gallons/yr) Total >, Spray Irrigation Design Element Plan Sheet Number Specification Page Number Wetted diameter of nozzles ' ft Wetted area of nozzles ft2 Nozzle capacity : gpm Nozzle manufacturer / model / Elevation of highest nozzle ft FORM: RLAP 06-16 Page 4 of 5 attest that this application for Applicant's Certification (signing authority must be in compliance with 15A NCAC 02T .0106): The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105. ,rYes ❑ No, Explain; 1, s4\-c\� Lr Qe5ocS (Signature Authority's Name — PLEASE PRINT) (Title) rt _ . C, GcC rw do G�l, �c- Cal i� (Facility Name) has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed and that if all required supporting information and attachments are not included, this application package will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes §143-215.6A and §143-215.6B, any person who knowingly makes any false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to exceed $10,000 as well as civil penalties up to $25,000 per violation. Signature: Date: FORM: RLAP 06-16 Page 5 of 5 Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 11-15): ® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® For new or renewed permits, submit a separate certification for each source facility. ® For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. ® Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source -Generating Facility Information: ❑ For each source facility, attach the following: Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Out tiatiN rot' i.@gliatiAN LAM ApplitAtiun P m to". ® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. ® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: ® For each source facility, attach the following: ® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. ® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1 RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: Andy Smith Status Code a Facility Permit Holder Facility Name County Permit Number Maximum Dry Tons Per Year Current b Proposed R City of Statesville 4th Creek WWTP Iredell NC0031836 1,057 N/A a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted) b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility). SUMMARY FOR FORM: RSC 06-16 Page 1 Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: 4th Creek WWTP 2. Facility permit holder is: ❑ Federal, ❑ State, El Local Government, or ❑ Private. Facility permit issued by: El;' Div. of Water Resources, ❑ Div. of Environmental Health, or ❑ Other (explain: ' O. 3. Facility contact person and title: Andy Smith Complete mailing address: PO Box 1111 City: Statesville State: NC Zip: -28687 Telephone number: (704) 878-3438 E-mail address: asmith@statesvillenc.net 4. Facility physical address: 693 Bell Farm Road City: Statesville State: NC Zip: -28687 Coordinates: Latitude: 35° 46' 29 N" Longitude: 80° 48' 50 W" Datum: i 1 Level of accuracy: _ I Method of measurement: GPS 5. Purpose of the facility: E treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater, treatment of potable water, ❑ treatment of 100% industrial wastewater, E treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: 40 % industrial and 60 % domestic) El other (explain: " ). 6. Does the facility have an approved pretreatment program: ® Yes ❑ No 7. Facility permitted/design flow: 6.0 MGD and facility average daily flow: 2.5 MGD 8. Average amount of residuals being generated at this facility 1,235 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: 3 meter belt press Type and volume of residuals storage (i.e., outside of residuals treatment units): 1.5 MG aerobic digester H. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: E 40 CFR Part 503 or El 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: E Biological ❑ Non -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 06-16 Page 1 of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes El no. If yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: ❑ yes ®', no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Prism Labs and Date of analysis: 8/22/17 Passed corrosivity test: yes ❑', no. pH: s.u. (2 <pH < 12.5) Passed ignitability test: El yes ❑' no. Flashpoint: I °F (> 140°F) Passed reactivity test: ® yes Eno. HCN: i mg/kg (<250) & H2S: mg/kg (<500) TCLP Parameter Limit (mg/1) Result (mg/1) TCLP Parameter Limit (mg/1) Result (mg/1) Arsenic 5.0 <0.050 Hexachlorobenzene 0.13 <0.050 Barium 100.0 <5.0 Hexachloro-1,3-Butadiene 0.5 <0.050 Benzene 0.5 <0.025 Hexachloroethane 3.0 <0.050 Cadmium 1.0 <0.025 Lead 5.0 <0.050 Carbon Tetrachloride 0.5 <0.025 Lindane 0.4 Chlordane 0.03 <0.0025 Mercury 0.2 <0.010 Chlorobenzene 100.0 <5.0 Methoxychlor 10.0 <0.00050 Chloroform 6.0 <0.30 Methyl Ethyl Ketone 200.0 <10 Chromium 5.0 <0.25 Nitrobenzene 2.0 <0.050 m-Cresol 200.0 Pentachlorophenol 100.0 <0.25 o-Cresol 200.0 Pyridine 5.0 <0.25 p-Cresol 200.0 Selenium 1.0 <0.10) Cresol 200.0 Silver 5.0 <0.25 2,4-D 10.0 Tetrachloroethylene 0.7 , <0.035 1,4-Dichlorobenzene 7.5 <0.38 Toxaphene 0.5 <0.025 1,2-Dichloroethane 0.5 <0.025 Trichloroethylene 0.5 <0.025 1,1-Dichloroethylene 0.7 <0.035 2,4,5-Trichlorophenol 400.0 <0.25 2,4-Dinitrotoluene 0.13 <0.050 2,4,6-Trichlorophenol 2.0 <0.10 Endrin 0.02 <0.00050 2,4,5-TP (Silvex) 1.0 Heptachlor and its Hydroxide . 0.008 <0.00050 Vinyl Chloride 0.2 <0.020 FORM: RSC 06-16 Page 2 of 5 Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., basis) for the following metal parameters: Laboratory: Waypoint Analytical and Date of analysis: 10/4/17 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 3.13 Cadmium 85 39 2 Copper 4,300 1,500 242 Lead 840 300 18.9 Mercury 57 17 0.601 Molybdenum 75 n/a 9.9 Nickel 420 420 19.5 Selenium 100 100 <5 Zinc 7,500 2,800 307 residuals do not on a dry weight b. For Surface Disposal Unit (land/ill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: and Date of analysis:. Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) [� > 0 but < 25 30 200 210 0' > 25 but < 50 34 220 240 [t > 50 but < 75 39 260 270 Q > 75 but < 100 46 300 320 0 > 100 but < 125 53 360 390 0! > 125 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 14.08 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Waypoint Analytical and Date of analysis: 10/4/17 Parameter Result (mg/kg) Aluminum 22,700 Ammonia -Nitrogen 9,510 Calcium 3,440 Magnesium 1,160 Nitrate -Nitrite Nitrogen <2.39 pH (Standard Unit) 5.11 Phosphorus 23,600 . Potassium 1,770 Sodium 311 Total Kjeldahl Nitrogen 48,800 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 0.4378 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Depaitiuent of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to,be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This rate is a (check one): ❑ default value, or ® actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (1st) Year PAN (mg/kg) Five -Year Maximum Adjusted PAN (mg/kg) Surface 36.6 183 Injection/Incorporation 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: ;___ FORM: RSC 06-16 Page 4 of 5 Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: ❑j A fecal colifoini density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or ❑''. A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): El Alternative 1 [15A NCAC 02T.1106(b)(3)(A)] - Time/Temperature Compliance. ❑. Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment. Q Alternative 3 [15A NCAC 02T.1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 4 [15A NCAC 02T.1106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. ❑' Alternative 5 [15A NCAC 02T.1106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: Q composting, ❑ heat drying, El heat treatment, ❑j thermophilic aerobic digestion, ❑'' beta ray irradiation, ❑i! gamma ray irradiation, or ❑' pasteurization. b. For Land Application of Class B: Alternative 1 [15A NCAC 02T.1106(c)(1)] - Fecal Coliform Density Demonstration. Q Alternative 2 [15A NCAC 02T.1106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: IZ aerobic digestion, ❑ air drying, ❑ anaerobic digestion, El composting, or ❑' lime stabilization. c. For Surface Disposal: ID Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. El Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. ❑' Exempt - If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)]. • Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 1 NCAC t3 T.1 101, specify how residuals will meet the VAR requirements: Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑( Alternative 2 [15A NCAC 02T.1107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). [I] 3 [15A NCAC 02T.1107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). Alternative 4 [15A NCAC 02T.1107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). ❑' Alternative 5 [15A NCAC 02T.1107(a)(5)] - 14-Day Aerobic Processes. 0: Alternative 6 [15A NCAC 02T.1107(a)(6)] - Alkaline Stabilization. El Alternative 7 [15A NCAC 02T.1107(a)(7)] - Drying of Stabilized Residuals. • Alternative 8 [15A NCAC 02T.1107(a)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [15A NCAC 02T.1107(a)(9)] - Injection. El Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation. El Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.1107(b)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources LAND APPLICATION SITE CERTIFICATION INSTRUCTIONS FOR FORM: LASC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This certification provides detailed information of receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 06-16 or FORM: SDR 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Land Application Site Certification (FORM: LASC 06-16): ❑ Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® For new or renewed permits, submit the requested information for all land application sites. ❑ For modified permits, submit the requested information for only those sites that are new, transferred or affected by the proposed modification. B. Land Application Site Information: R The status of the land application site with respect to this residuals land application program must be provided in table I. The status categories and their corresponding codes are as follows: ♦ New (N) + Renewed (R) ♦ Modified (M) ♦ Transferred (T) ♦ Deleted (D) ❑ Attach the following in accordance with each status code: Required Item Status Code N R T M doc / County Notification. Board `r `/ `/ Land Owner Agreement (If applicable) Setback Waiver Agreement ✓ ✓ ✓ ✓ An updated for Residuals vicinity/setback map in accordance with the "Map Guidance V `./ ✓* Land Application Permits" A soils and Evaluation Policy"* agronomic evaluation in accordance with the "Soil Scientist ✓ INSTRUCTIONS FOR FORM: LASC 06-16 Page 1 of 3 An updated accounting of the land application site's cumulative pollutant loading rates (CPLRs) • ✓ V Required Item Status Code N R T M For previously permitted sites without a soil series name indicated in the Attachment B, submit County Soil Survey Map (or equivalent) clearly indicate the location of the land application site and in accordance with the soil map requirements in the "Soil Scientist Evaluation Policy" Acknowledgement of field transfer from Land Owner (Fields may not be permitted to multiple Permittees over the same time period) ✓ * This item may be required for land application site with a status code "M", p ease contact the Division if you need assistant in determining attachment requirements. • Crop Type should include the most likely crop types for the life of the permit (five years). ® Predominant Soils Series Name must be either the name of the soil indicated in Attachment `B" of the existing permit, or name of the soil series as provided by the licensed soil scientist. ® Predominant Soil Mapping Unit or Representative Slope: Either the Soil Mapping Unit or the representative slope of each site must be provided. The predominant soil -mapping unit must be consistent with the predominant soil series name. Please note that the soil mapping units are variable between Counties, so care should be taken in properly identifying the correct mapping unit. If a representative slope is provided, it must be determined accordingly: ❑ For sites previously permitted for use, but do not have an established soil mapping unit (the mapping unit provides information on both the soil series name and the slope of the soil), the Applicant may determine the representative slope by using the average slope provided in the County Soil Survey (or equivalent). A soil type with a slope range of 4 - 8% would have a representative slope of 6%. ❑ New Sites to be permitted must have slopes determined as part of the soils report prepared by a licensed soil scientist. Acceptable methods for determining location coordinates (i.e., latitude and longitude) and their corresponding codes are as follows: • Address Matching (ADD) • Aerial Photography with Ground Control (AER) • Cadastral Survey (SUR) • Conversion from Coordinate Plane (CP) • Conversion from Township -Section -Range (TSR) • Conversion from Universal Trans Merc (UTM) • Map Interpretation by Digital or Manual Extraction (MAP) C. Waterbody and Classifications Information: (new sites only) • Digital or Raw Photo Extraction (EXT) • Geodetic Quality GPS Survey (GEO) • LORAN-C Navigation Device (LOR) • Navigation Quality GPS (GPS) • Remote Sensing (RS) • Zip Code Centroid (ZIP) ❑ Use an 8.5 by 11-inch copy of the portion of a 7.5-minute USGS Topographic Map to identify the location where the residuals program activities are planned to occur as well as the closest downslope surface waters as clearly as possible. Each map portion must be labeled with the map name and number, the identified location, and be of clear and reproducible quality. ❑ Surface water body classifications information may be found at: hitillLdeq,ite ; out/dlvlsi.s nsiwater- resoure s/p1ann tnR/classificatlo_n-statxdards/r iassificatidns ❑ Any questions concerning the waterbody and its classification, please contact the Division's regional offices. ❑ A list of the Division's regional offices, their county coverage, and their contact information may be downloaded at: http :fide q.nc,gov/contact/regional-offices ❑ General Instructions: There are 17 river basins in North Carolina. Each basin has associated waterbodies with assigned subbasins, location descriptions, stream index numbers and established classifications. 1. Identify the project area on a 7.5 minute USGS topographical map (an 8.5 x 11-inch sheet showing the project area should be submitted with the permit application regardless of whether a Stream classification was completed). 2. Determine the names of all the closest down slope surface waters from the project site. For unnamed tributaries, see Table 1: Unnamed Tributaries Entering Other States or for Specific Basin Areas. Label any unnamed tributaries as "UT to- stream name" as the waterbody name. 3. Open the link http://deq.nc.gov/about/divisions/water-resources/planning/classification-standards/classifications. ❑ Stream Classification Process: One of the options below may be used depending on the known initial project information. ❑ KNOWN BASIN WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Select proper basin from the List all Waterbodies in Basin sorted report. Sort hydrologically as this will provide the proper location descriptions if multiple runs. INSTRUCTIONS FOR FORM: LASC 06-16 Page 2 of 3 Fr 2. Locate the name of the identified waterbody (from General Directions) on the list. 3. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 4. Record all Basins, Stream Index Numbers and Classifications applicable to the project. IIIKNOWN COUNTY WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Select the proper county from the List all Waterbodies in county, hydrologically report. 2. Locate the name of the identified waterbody (from General Directions) on the list. 3. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 4. Record all Basins, Stream Index Numbers and Classifications applicable to the project. ❑ UNKNOWN BASIN WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Use the Clickable basin map to hydrologically sorted list report. 2. Click on the approximate project location to bring up the hydrologically sorted list. 3. Locate the name of the identified waterbody (from General Directions) on the list. 4. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 5. Record all Basins, Stream Index Numbers and Classifications applicable to the project. ❑ Notes on index number and unnamed streams: Unnamed Streams 15A NCAC 02B .0301(1). ❑ Any stream which is not named in the schedule of stream classifications carries the same classification as that assigned to the stream segment to which it is tributary (at the point of entry) except: (A) unnamed streams specifically described in the schedule of classifications; (B) unnamed freshwaters tributary to tidal saltwaters will be classified "C"; or (C) after November 1, 1986, any newly created areas of tidal saltwater which are connected to Class SA waters by approved dredging projects will be classified "SC" unless case -by -case reclassification proceedings are conducted. ❑ The following river basins have different policies for unnamed streams entering other states or for specific areas of the basin: Unnamed Tributaries Entering Other States or for Specific Basin Areas Hiwassee River Basin Streams entering Georgia or Tennessee shall be classified "C Tr." Little Tennesse River Basin And Savannah River Drainage Area Streams entering Georgia or Tennessee shall be classified "C Tr." Such streams in the Savannah River drainage area entering South Carolina shall be classified "B Tr." French Broad River Basin Streams entering Tennessee will be classified "B." Watauga River Basin Streams entering the State of Tennessee are classified "C." Broad River Basin Streams entering South Carolina are classified "C." New River Basin Streams entering the State of Tennessee are classified "C." Catawba River Basin Streams entering South Carolina are classified "C." Yadkin -Pee Dee River Basin Streams entering Virginia are classified "C," and such streams entering South Carolina are classified "C." Lumber River Basin Streams entering South Carolina are classified "C Sw." Roanoke River Basin Streams entering Virginia are classified "C." Except that all backwaters of John H. Kerr Reservoir and the North Carolina portion of streams tributary thereto not otherwise named or described shall carry the classification "B," and all backwaters of Lake Gaston and the North Carolina portion of streams tributary thereto not otherwise named or described shall carry the classification "C and B." Chowan River Basin Streams entering Virginia are classified "C." Tar -Pamlico River Basin All drainage canals not noted in the schedule are classified "C Sw." except the main drainage canals to Pamlico Sound and its bays which shall be classified "SC." Pasquotank River Basin All drainage canals not noted in the schedule are classified "C." INSTRUCTIONS FOR FORM: LASC 06-16 Page 3 of 3 LAND APPLICATION SITE CERTIFICATION Applicant's name: City of Statesville Land application sites currently certified: 29.4 net acres and Total to be certified: 29.4 net acres. I. LAND APPLICATION SITE INFORMATION (See Instruction B): Status Code Site/Field Landowner(s) Lessee(s) or Operator(s) Net Acres County Crop(s) Predominant Soil SeriesMapping Nameb Unit or Rep. Slope' R 01 City of Statesville 4th Creek WWTP 15.30 Iredell Corn & Small Grain Lloyd LcC2 6-10% N , ___ ] ± N _— 1 �_ !- .. -.. j l - N — --- .--� ( t f '_-1 — Status Code for land application sites are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ T (Transferred) ♦ D (Deleted) b Soil Series Name (i.e. Appling, Cecil, etc.) `Mapping Unit must be consistent with those used in the County Soil Survey (i.e. for a 2-8% slope Cecil in Anson County the mapping unit is CeB2) II. WATERBODY AND CLASSIFICATIONS INFORMATION (See Instruction C): Site/Field ID Latitude Longitude g Location Datum Location Method Code Location Accuracy Waterbody Subbasin and Stream Index No. Current and Proposed Class p 01 35° 46' 12" 80° 47' 24" NAD 83 ADD Nearest Second 03-07-06/03040102 C _ C _.0 I NAD 83 ADD Nearest Second ( _'° " ° '' "' NAD 83 ADD Nearest Second - 1 - 5° ` I __III 0'' _" NAD 83 ADD Nearest Second i__ 1 1_ __.1 ° r... "' '° ' " " NAD 83 ADD Nearest Second i 1— T' - 1 ° , _, , NAD 83 ADD Nearest Second 1 L _--I :_. _: ° �" ,, F E '° -''_" NAD 83 ADD Nearest Second I 1 ° , ,, ' " '' '° ' , ' NAD 83 ADD Nearest Second I �i : Please keep the site information (I.) and waterbody information (IL) of the same field on the same page. FORM: LASC 06-16 Full -Service Analytical & Environmental Solutions LABORATORIES, INC. City of Statesville, NC Andy Smith P.O. Box 1111 Statesville, NC 28687 NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Project: Sludge (Hazardous Testing) Project No.: 4th Creek Sludge Lab Submittal Date: 08/22/2017 Prism Work Order: 7080390 Case Narrative 09/11 /2017 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Narrative Notes: Reactivity analysis was subcontracted to GCAL. TCLP Herbicide analysis was subcontracted to AES. Laboratory reports are attached. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. -ge-'.; Robbi A. Jones Reviewed By Robbi A. Jones President/Project Manager President/Project Manager Data Qualifiers Key Reference: CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken. D RPD value outside of the control limits. ICV ICV result is above the control limits. Analyte not detected in the sample. No further action taken. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 24 Client Sample ID Fourth Creek Sludge Full -Service Analytical & Environmental Solutions Sample Receipt Summary 09/11/2017 Prism Work Order: 7080390 Lab Sample ID Matrix Date Sampled Date Received 7080390-01 Solid 08/22/17 08/22/17 Samples were received in good condition at 3.9 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 24 7 1 JP ISM LABORATORIES, INC. City of Statesville, NC Attn: Andy Smith P.O. Box 1111 Statesville, NC 28687 Full-Servioe Analytical & Environmental Solutions Project: Sludge (Hazardous Testing) Project No.: 4th Creek Sludge Sample Matrix: Solid Laboratory Report 09/11/2017 Client Sample ID: Fourth Creek Sludge Prism Sample ID: 7080390-01 Prism Work Order: 7080390 Time Collected: 08/22/17 11:50 Time Submitted: 08/22/17 15:30 Parameter Result Units Report MDL Limit Dilution Method Analysis Analyst Factor DateMme Batch ID General Chemistry Parameters % Solids Corrosivity-pH Ignitability TCLP Extraction by EPA 1311 15.1 % by 0.100 Weight 5.9 pH Units Pass mm/sec 0.10 0.100 1 *SM2540 G 8/31/17 16:00 JLB P7I0012 1 *9045D 8/24/17 10:47 BMS P7H0445 1 *1030 8/24/17 9:00 BMS P7H0440 TCLP Extraction TCLP Extraction TCLP Metals Complete Complete N/A N/A 1 *1311 8/26/17 10:05 JAB P7H0487 1 *1311 ZHE 9/6/17 12:34 KDM P710063 Mercury Arsenic Barium Cadmium Chromium Lead Selenium Silver BRL BRL BRL BRL BRL BRL BRL BRL TCLP Organochlorine Pesticides by GC/ECD mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0.010 0.050 5.0 0.025 0.25 0.050 0.10 0.25 0.000030 1 0.012 1 0.0065 1 0.00065 1 0.0038 1 0.0080 1 0.022 1 0.00050 1 *7470A *6010D *6010D *6010D *6010D *6010D *6010D *6010D 9/1/17 12:34 8/28/17 15:18 8/28/17 15:18 8/28/17 15:18 8/28/17 15:18 8/28/17 15:18 8/28/17 15:18 8/28/17 15:18 JAB JAB JAB JAB JAB JAB JAB JAB P7H0572 P7H0505 P7H0505 P7H0505 P7H0505 P7H0505 P7H0505 P7H0505 Chlordane Dieldrin Endrin gamma-BHC Heptachlor Heptachlor Epoxide Methoxychlor Toxaphene BRL BRL BRL BRL BRL BRL BRL BRLCCV mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0.0025 0.00050 0.00050 0.00050 0.00050 0.00050 0.00050 0.025 0.00047 1 0.000070 1 0.000075 1 0.000065 1 0.000085 1 0.000065 1 0.00020 1 0.00037 1 *8081B *8081B *8081B *8081B *8081B *8081B *8081B *8081B 8/28/17 17:23 JMC 8/28/17 17:23 JMC 8/28/17 17:23 JMC 8/28/17 17:23 JMC 8/28/17 17:23 JMC 8/28/17 17:23 JMC 8/28/17 17:23 JMC 8/28/17 17:23 JMC P7H0495 P7H0495 P7H0495 P7H0495 P7H0495 P7H0495 P7H0495 P7H0495 Surrogate Recovery Control Limits Decachlorobiphenyl Tetrach to ro-m-xyl a ne TCLP Semivolatile Organic Compounds by GC/MS 73 % 13-186 81 % 40-134 2,4, 5-Trichlo rophe nol 2,4,6-Trichlo roph enol 2,4-Dinitrotoluene 2-Methylphenol 3/4-Methylphenol Hexachlorobenzene Hexachlorobutadiene Hexachloroethane Nitrobenzene Pentachlorophenol BRL BRL BRL BRL BRL BRL BRL BRLicv BRL BRL mg/L 0.25 0.0016 1 *8270D 8/29/17 18:32 JMV P7H0520 mg/L 0.10 0.0018 1 *8270D 8/29/17 18:32 JMV P7H0520 mg/L 0.050 0.0014 1 *8270D 8/29/17 18:32 JMV P7H0520 mg/L 0.050 0.0018 1 *8270D 8/29/17 18:32 JMV P7H0520 mg/L 0.050 0.0015 1 *8270D 8/29/17 18:32 JMV P7H0520 mg/L 0.050 0.0013 1 *8270D 8/29/17 18:32 JMV P7H0520 mg/L 0.050 0.0021 1 *8270D 8/29/17 18:32 JMV P7H0520 mg/L 0.050 0.0017 1 *8270D 8/29/17 18:32 JMV P7H0520 mg/L 0.050 0.0026 1 *8270D 8/29/17 18:32 JMV P7H0520 mg/L 0.25 0.0012 1 *8270D 8/29/17 18:32 JMV P7H0520 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525.0409 Page 3 of 24 Full -Service Analytical & Environmental Solutions City of Statesville, NC Attn: Andy Smith P.O. Box 1111 Statesville, NC 28687 Project: Sludge (Hazardous Testing) Project No.: 4th Creek Sludge Sample Matrix: Solid Laboratory Report 09/11/2017 Client Sample ID: Fourth Creek Sludge Prism Sample ID: 7080390-01 Prism Work Order: 7080390 Time Collected: 08/22/17 11:50 Time Submitted: 08/22/17 15:30 Parameter Result Units Report Limit MDL Dilution Method Analysis Analyst Factor Date/Time Batch ID Pyridine BRLICV mg/L 0.25 0.0010 1 *8270D 8/29/17 18:32 JMV P7H0520 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 2-Fluorobiphenyl 2-Fluorophenol Nitrobenzene-d5 Phenol-d5 Terp henyl-d 14 TCLP Volatile Organic Compounds by GC/MS 71 63 40 61 23 84 43-140 44-119 19-119 44-120 11-52 50-134 1,1-Dichloroethylene 1,2-Dichloroethane 1,4-D ichloro benzene Benzene Carbon Tetrachloride Chlorobenzene Chloroform Methyl Ethyl Ketone (2-Butanone) Tetrachloroethylene Trichloroethylene Vinyl chloride BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL mg/L 0.035 0.00083 1 *8260B mg/L 0.025 0.00066 1 *8260B mg/L 0.38 0.00050 1 *8260B mg/L 0.025 0.00048 1 *8260B mg/L 0.025 0.0011 1 *82603 mg/L 5.0 0.00062 1 *8260B mg/L 0.30 0.00076 1 *8260B mg/L 10 0.0024 1 *8260B mg/L 0.035 0.00098 1 *8260B mg/L 0.025 0.00078 1 *8260B mg/L 0.020 0.00097 1 *8260B 9/6/17 9/6/17 9/6/17 9/6/17 9/6/17 9/6/17 9/6/17 9/6/17 9/6/17 9/6/17 9/6/17 14:02 KDM P710064 14:02 KDM P710064 14:02 KDM P710064 14:02 KDM P710064 14:02 KDM P710064 14:02 KDM P710064 14:02 KDM P710064 14:02 KDM P710064 14:02 KDM P710064 14:02 KDM P710064 14:02 KDM P710064 Surrogate Recovery Control Limits 4-Bromofluorobenzene Dibromofluoromethane Toluene-d8 101 99 98 80-124 75-129 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Spring brook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 24 Sample Extraction Data ep Method: Solids, Dry Weight Lab Number Batch Initial Final Date/Time 7080390-01 Prep Method: 1311 P710012 30 g 30 g 08/31/17 16:00 Lab Number Batch Initial Final Date/Time 7080390-01 7080390-01 Prep Method: 3010A Lab Number P710063 P7H0487 Batch 12.5 g 250 mL 100 g 2000 mL 09/05/17 15:33 08/25/17 15:30 Initial Final Date/Time 7080390-01 Prep Method: 7470A Lab Number P7H0505 10 mL 50 mL 08/28/17 10:25 Batch Initial Final Date/Time 7080390-01 Prep Method: 3510C GC Lab Number P7H0572 20 mL 30 mL 09/01/17 7:25 Batch Initial Final Date/Time 7080390-01 Prep Method: 3510C MS Lab Number P7H0495 200 mL 10 mL 08/28/17 9:49 Batch Initial Final Date/Time 7080390-01 Prep Method: 5030E Lab Number P7H0520 200 mL 1 mL 08/29/17 9:41 Batch Initial Final Date/Time 7080390-01 P710064 1 mL 10 mL 09/06/17 9:52 Subcontracted Analyses The following analyses were subcontracted to Analytical Environmental Services , Inc. Lab Number Analysis 7080390-01 Herbicides TCLP (Sub) The following analyses were subcontracted to Gulf Coast Analytical Labs, Inc. Lab Number Analysis 7080390-01 Reactivity, Cyanide (Sub) 7080390-01 Reactivity, Sulfide (Sub) This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 24 LABORATORIES, INC. 44'1 Sprinjbrootc Road Phone 704/520-(-364 11 Ciiient Company Name: a �/ Full -Service Analytical R: Environmental Solutions Charlotte, r iG .25217 Fax: 704/525-040a ab S , s'r fro IDS Report To/Contact Mame: _{i cog s, co NA Reporting Address: • CMAII OF CUSTODY L CO{ D >` CAGE ©F QUOTE. 0 T© ENSURE PROPER SOLLOMO: Project Name: Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO) "Please ATTACH any project specific reporting (QC LEVEL 0 OI DI0 IV) provisions and/or QC Requirements Invoice To: Address: '.yam if ,„: '..YES .•NO Sentples`INTACT upon al'rivdt? Rc,colvcd:ON WLT ICI ? PRO;PD PRESERVATIVE'S indlcatecl? RoceivOc11NIT1-11N HOLDING TIMES? .CUSTODY, SL-.ALS'IN7ACT?..:'` • 'VOLAr iI E$ reo'd IN/QU7•1=1EADS ACE? PROPER CONTAINERS : used? :: ' TEMP: 'felrD 812-T7`Odq, �OCC;51 Cl• u"Mone: Ill"-a6 - c9'11 4 cax((Vej-9 (b9o): jUrli' i I'' " rJ 6 "J TO BE FILLED IN BY CLOENT/SAMPLD G PERSONNEL Certification: ilEOaAC D®D FL MC Purchase Order No./Filling Reference Email Address: Requested Due Date O 1 Day U 2 Days ❑ 3 Days U 4 Days 0 5 Days EDD Type: PDF_Excei Other "Working Days" ID 6-9 Days ❑ Standard 10 days U Be SC OTHER N/A pre A porovedust Site: Location Mame: Samples received after 14:00 will be processed next business day. Water Chlorinated: YES MO Sarripie iced Upon Coilection: YES— NO Site Location Physical Address: Turnaround time is based on business days, excluding weekends and holidays. (SEE REVERSE FOR TERMS U: CONDITIONS REGARDING SERVICES RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) CLIENT SAMPLE DESCRIPTION DATE COLLECTED TIME COLLECTED MATRIX (SOUL, SAMPLE CONTAINER R PRESERVA- TIVES ANALYSIS REQUESTED REMARKS /// / PRISM LAB ID NO. "TYPE SEE BELOW NO. SIZE MILITARY HOURS WATER OR SLUDGE) FO4os-�'Vfl Cc ! � i:.% i a D 6'J ",21 0 � � t e� O �Q dr g Z�0 J�N, /ry/ LL fI L' 0y ID 1 �L>79 /� ��a� ( f l% pp Sup u d r I, Sem v 4 ° gyp/F 2N II i� aY VO IA V, rs " Ci e 6 ci Q°.('�i? rc , p !fU ia(f6 ilia I�lf'h i5'' (a° OQ .- p�i ,y Sampler's Signature d �✓je-14-.- /:Y Sampled By � 11 - T 'u'til D e 4404' �• ....A. (Print Name) �,liy a� 1 ,f1C6( Affiliation Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be submitted in writingto the PrismProject Manager. There will be charges for any changes after analyses have been initialized. *-+ �� �°+ter i. � Ihn`'p Relinguhed By: (Signalur) ."p'� �j 17 ;� / c ,./` R56S> ed y: (Signs ur a �I Date Military/Hoursi s Additional Comments: Stel�nivalTlme Religci'f bed By: (Signat&re) jr rr� —2 %' k'adeived By: (Signaturc;'� " date ; Site' -De /alture•Tlliie... ,�j0 --r, ` ).-- 1t) /p h -ig0Iohed By: (Signals re) Received .+6r.hris ',yLaboratorie� Syr ! Date ' Field.Tsch•Fein {J� (Q`r�� l � �/ktts 4s--Z P —17/j' I Sad Mileage; !v ,od of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CU ODY SEALS FORT JSPORTArION ID THE LABORATORY. COC Grou No. (Q O) SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UN(IIL RECEIVED AT TI-lt LABORATORY.CD ad Ex ❑ UPS 0 Hand -delivered q,-47 m Field Service 0 Other ! 't. U tly v } q/ O DES: UST: GR .X1 HATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFOLL OTI-IER: "leis R .rT „1 ,IC IDSC UNC ®SC �0(I�C ®SC ©NC USC UNC USC UNCUSC UNC USC UNC USC UNC USC �sRiV("sa; or"o_ii �" sr' iv U ® ® U ® ® ® U 2.P.'G1 ,,1 J. )NTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Orcaanics Analysis (Zero Head Space) ACCESS ANAL ` flCAL, A ALYT CAL REPORT CLIENT Prism Laboratories PO Box 240543 Charlotte, NC 28224 ATTENTION Robbi Jones PROJECT ID 7080390 LABORATORY REPORT NUMBER 217082415 DATE 08/29/2017 Primary Data Review By f, Authorized Signature PLEASE NOTE: Secondary Data Review By Ashley B. Amick Project Manager, Access Analytical, Inc. aamick@accessanalyticalinc.com - Unless otherwise noted, ail analysis on this report performed at Gulf Coast Analytical Labs (GCAL), 7979 innovation Park Dr., Baton Rouge, LA 70820. - GCAL is SCDHEC certified laboratory # 73006, NCDENR certified lab # 618, GA certified lab # LA-01955, NELAP certified laboratory 01955 - Local support services for this project are provided by Access Analytical, Inc.. Access Analytical is a representative of GCAL serving clients in the SC/NC/GA areas. All questions regarding this report should be directed to your local Access Analytical representative at 803.781.4243 or toll free at 888.315.424.3. Lab Report#: 217082415 Page 1 of 11 Page 7 of 24 4.hhILYTdC,L-1 LAlifigATEUIEE, LLC A LYT NELAP CERTIFICATE NUMBER: 01955 DOD ELAP CERTIFICATE NUMBER: L14-243 CAL RESULTS PERFORMED BY GCAL, LLC 7979 kmovation Park Dr. Baton R uge, LA 71:i20 * Report Date 08/29/2017 GCAL Rep * 't 217082415 Project 7080390 ever To Robbi Jones Prism Laboratories PO Box 240543 Charlotte, NC 28224 800-529-6364 Addigional Recipients NONE TeMral,g, DbD ELAF Lab Report4: 217082415 Pale 2 of 11 Page 8 of 24 LIANALYTICAL LAC'OPATOFIES. Report#.: 217082415 Project ID: 7080390 Lab.rat®ry Endorsement Report Date: 08/29/2017 Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this retention period the samples will be disposed in accordance with GCAL's Standard Operating Procedures. Common Abbreviations that may be Utilized in this Report ND Indicates the result was Not Detected at the specified reporting limit NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030 DO Indicates the result was Diluted Out MI Indicates the result was subject to Matrix Interference TNTC Indicates the result was Too Numerous To Count SUBC Indicates the analysis was Sub -Contracted FLD Indicates the analysis was performed in the Field DL Detection Limit DL Diluted analysis — when appended to Client Sample ID LOD Limit of Detection LOQ Limit of Quantitation RE Re -analysis CF HPLC or GC Confirmation 00:01 Reported as a time equivalent to 12:00 AM Reporting Flags that may be Utilized in this Report J or I Indicates the result is between the MDL and LOQ J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria U Indicates the compound was analyzed for but not detected B or v Indicates the analyte was detected in the associated Method Blank Q Indicates a non -compliant QC Result (See Q Flag Application Report) Indicates a non -compliant or not applicable QC recovery or RPD — see narrative B The result is estimated because it exceeded the instrument calibration range E Metals - % diference for the serial dilution is > 10% P RPD between primary and confirmation result is greater than 40 Sample receipt at GCAL is documented through the attached chain of custody. In accordance with NELAC, this report shall be reproduced only in full and with the written permission of GCAL. The results contained within this report relate only to the samples reported. The documented results are presented within this report. This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited. I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee, as verified by the following signature. Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if applicable. 7 Authorized Signature GCAL Report 217082415 Lab Report#: 217082415 Pace 3 of 11 Page 9 of 24 Report#: 217082415 Project ID: 7080390 Certifications Report Date: 08/29/2017 Certification Certification Number DOD ELAP L14-243 Alabama 01955 Arkansas 12-060-0 Colorado 0'1955 Delaware 01955 Florida E87854 Georgia 01955 Hawaii 01955 Idaho 01955 Illinois 200048 Indiana 01955 Kansas E-10354 Kentucky 95 Louisiana 01955 Maryland 01955 Massachusetts 01955 Michigan 01955 Mississippi 01955 Missouri 01955 Montana N/A Nebraska 01955 New Mexico 01955 North Carolina 618 North Dakota R-195 Oklahoma 9403 South Carolina 73006001 South Dakota 01955 Tennessee 01955 Texas T104704178 Vermont 01955 Virginia 460215 USDA Soil Permit P330-10-00117 Lab Report#: 217082415 Panes 1 of 11 I Page 10 of 24 Report#: 217082415 Project ID: 7080390 Case Narrative CDient: Access Analytical Report: 217082415 Report Date: 08/29/2017 Gulf Coast Analytical Laboratories received and analyzed the sample(s) listed on the Report Sample Summary page of this report. Receipt of the sample(s) is documented by the attached chain of custody. This applies only to the sample(s) listed in this report. No sample integrity or quality control exceptions were identified unless noted below. No anomalies were found for the analyzed sample(s). Lab Report`: 217082415 o....= A of 44 I Page 11 of 24 I aNALVTICAL tIC GCAL ID 21708241501 Client ID Fourth Creek Sludge Report#: 217082415 Project ID: 7080390 Sample Summary Matrix Collect. Daterfirne Solid 08/22/2017 11:50 Report Date: 08/29/2017 Receive Date/Tirne 08/24/2017 11:20 Lab Report#: 217082415 Panp of 11 I Page 12 of 24 L' ?fit/, I.Yili:kL LAGOP.OMPI_S. LLG Report#: 217082415 ProjectIJ: 7080390 Summary of Compounds Detected No analytes were detected for analyses performed by GCAL. Report Date: 08/29/2017 Lab Report : 217082415 Pang 7 of 11 I Page 13 of 24 .S L.trICAL L s29RAt G5Ii5. LLC Fourth Creek % Age EPA 9012E Prep Date 08/24/2017 12:00 CAS# 57-12-5R EPA 9034 Prep Date 08/24/2017 12:00 CASE` 18496-25-8R Prep Batch 616831 Parameter Reactivity Cyanide Prep Batch 616832 Parameter Reactivity Sulfide Report#+': 217082415 Project ID: 7080390 SampleResults Collect Date 08/22/2017 11:50 Receive Date 08/24/2017 11:20 Prep Method EPA 7.3.3.2 Prep Method EPA 7.3.4.2 Dilution Analysis Date 1 08/25/2017 15:43 Report Date: 08/29/2017 GCAL ID 21708241501 Matrix • Solid By Analytical Batch DMT 616946 Result DL 250U 250. Dilution Analysis Date 1 08/25/2017 14:00 LOQ 250 By Analytical Batch MOS 616937 Result DL 250U 250 LOQ 250 Units mg/kg Units mg/kg Lab Report#: 217082415 Paae8of11 Page 14 of 24 ULY rlctL LCL'°P:.T°PIES. LLC L' Report#: 217082415 Project ID: 7080390 eneral Chemistry QC Summary Report Date: 08/29/2017 Analytical Batch Client ID 616937 GCAL ID Prep Batch Sample Type 616832 Prep Date Prep Method Analysis Date EPA 7.3.4.2 Matrix MB616832 1714951 MB 08/24/2017 10:00 08/25/2017 14:00 Solid LCS616832 1714952 LCS 08/24/2017 10:00 08/25/2017 14:00 Solid EPA ��� Units Result mg/kg DL Spikel Added Result %RI Control Limits%R Reactivity Sulfide 118496-25-8R 250U 250 1000 1074 107 47 -135 Analytical Batch Client ID 616937 GCAL ID Prep Batch Sample Type 616832 Prep Date Prep Method Analysis Date EPA 7.3.4.2 Matrix ATF 17-003; ATF Leaded .. 21708222001 SAMPLE 08/24/2017 10:00 08/25/2017 14:00 Solid 1714285DUP 1714953 DUP 08/24/2017 10:00 08/25/2017 14:00 Solid EPA 9034 Units Result I mg/kg DL Result RPD RPD Limit Reactivity Sulfide f 18496-25-8R 0 250 0 0 25 Analytical Batch Client ID 616946 GCAL ID Prep Batch Sample Type 616831 Prep Date Prep Method Analysis Date EPA 7.3.3.2 Matrix MI3616831 1714948 MB 08/24/2017 10:00 08/25/2017 15:11 Solid LCS616831 1714949 LCS 08/24/2017 10:00 08/25/2017 17:36 Solid EPA 90 12E Units Result mg/kg _ DL Spikel Added Result %R Control Limits%R Reactivity Cyanide I 57-12-5R 250U 250 250 3.2 1 1 - 25 Analytical Batch Client ID 616946 GCALID Prep Batch Sample Type 616831 Prep Date Prep Method Analysis Date EPA 7.3.3.2 Matrix ATF 17-003; ATF Leaded .. 21708222001 SAMPLE 08/24/2017 10:00 08/25/2017 15:16 Solid 1714285DUP • 1714950 DUP 08/24/2017 10:00 08/25/2017 15:18 Solid EPA 90 2 Units Result mg/kg DL Result) RPD I RPD Limit Reactivity Cyanide I 57-12-5R 0.0 250 0.0 0 20 Lab Report#: 217082415 pane Qof11 Page 15 of 24 I Client ID, • Recess Analytical, t-_-',- tom' LABORATORIES, @ INC LL.t SIDG 1 062415 Full -Service Analytical `4' •'T ' ill P. AEC Environmental Solutions SUBCONTRACT ORDER - 1 . 1 t Prism Laboratories, Inc_ Certification: NEji AC_ USACE NC, -r SC__ Other 7080390 NJA SENDING --.-- If ABORATORV: RECEIVING LA:DORATORY: Prism Lab, P. O. Box Charlotte; Phone: 80C-529-6364 Fax: 704-525-0409 Project Maraeer: ratories, Inc. Gulf Coast Analytical Labs, Inc. tff40543 1078) Coursey Blvd ,4C 28224-0543 Baton Rouge, LA 70816 Phone :(225) 769-4900 Fax: (225) 767-5717 Robbi A. Jones Analysis Due Expires Laboratory ID Comments Sample ID: 7080390-01 Solid Samulcd:0Si' 22/17 II:50 i''.,.3 ..: ` is " `) 3 0: 1 9e_-> Reactivity, Reactivity, containers S pZ ullide (Sub) 08/29/17 11:50 L..) yanide (Sub) 09/05/17 11:50 ipplied `E e P).. C?lv\ - t r -. l bO-lb1 -Zcl —_.....-------?.-A-11 ,— o()dn-0 Wased I3v L? Date Received By Date L ,-rtr-1-7 T i6C> s-V6q.L (T- - - Released B , Data Receiv- Ni L=i C- (� I Dais Released B i Date ReccivedBy Dale Date Received By Date Page1of1 Page 16 of 24. 173 Jo L e6e d AFIALVIIICAL 1.,111..ATOMES. SAMPLE RECEIVING CHECKLIST 2 1 0 8 2 4 5 SAMPLE DELIVERY GROUP 217082415 CHECKLaST YES NO Client PM AM 4565 - Access Analytical Transport Method fedex Samples received with proper thermal preservation? Radioactivity is <1600 cpm? If no, record cpm value COC relinquished and complete (including samplelDs, All containers received in good condition and within All sample labels and containers received match the • _ - 131 in notes section. V LI Profile Humber 80251 Received IS'iy Savage, Tiffany R collect times, and sampler)? ISI hold time? v. Line Item(s) 4 - Solid Receive Date(s) 08/24/17 chain of custody? .. Preservative added to any containers? If received, was headspace for VOC water containers Samples collected in containers provided by GCAL? IS < 6mm? s v COOLERS DISCRE-PANCOES LAB PRESERVATaONS Airbiii Thermometer ID: E29 Temp °C Nbne None 7700 9612 2948 4.5 NOTES ' Revision 1.6 Page 1 of 1 Lab Report*: 217082415 Page 11 of 11 Act.- ESS ,NA L IC L NC,. ANALYTICAL REPORT CLIENT Prism Laboratories PO Box 240543 Charlotte NC 282240543 ATTENTION Robbi A. Jones PROJECT ID 7080390 LABORATORY REPORT MJMBER 1708N85 DATE September 08, 2017 Primary Data Review Bv Secondary Data Review Bv (Z 7.7 / Chris Pafford Project Manager, AES PLEASE NOTE: Ashley Amick Project Manager, Access Analytical aamick@axs-inc.com Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc), 3080 Presidential Drive, Atlanta, GA30340. AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582, NELAP certified laboratory # E87582 AfflA-LAP,LLC Laboratory ID:100671 for Industrial Hygiene samples (Organics, Metals, PCM Asbestos, Gravimetric), Environmental Lead (Paint, Soil, Dust wipes, Air), and Environmental Microbiology (Fungal) Direct Examination. Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243 Page I Page 18 of 24 -,L'LABORATOR ES, INC I Full -Service Analytical & Environmental Solutions SUBCONTRACT ORDER Prism Laboratories, Inc. 7080390 Certification: NACUSACE NC L Sc Other N/A SENDING LABORATORY: Prism Laboratories, Inc. P. O. Box 240543 Charlotte, NC 28224-0543 Phone: 800-529-6364 Fax: 704-525-0409 Project Manager: Robbi A. Jones RECEIVING LABORATORY: Analytical Environmental Services, Inc. 3080 Presidential Parkway Atlanta, GA 30340 Phone :(770) 457-8177 Fax: NA Analysis Due Expires Sample ID: 7080390-01 Solid Herbicides TCLP (Sub) Containers Supplied: Sampled;08/22/17 11:50 08/29/17 11:50 Reused B}% - kL( Released By Date g-at/-r-7 Date Laboratory En Comments rt - Received Byy Date Received By ate s" d Released By Date Received By Date Released By Date Received By Date Page 1 of 1 Page Page 19 of 24 Full -Service Analytical & Environmental Solutions SENDING LABORATORY: Prism Laboratories, Inc_ P. 0. Box 240543 Charlotte, NC 28224-0543 Phone: 800-529-6364 Fax: 704-525-0409 Project Manager: Robbi A. Jones Analysis Due Sample ID: 7080390-01 Solid Herbicides TCLP (Sub) Containers Supplied: Vo 7- Reused B Released By JEJ SUBCONTRACT ORDER Prism Laboratories, Inc. 7080390 Expires S a m alg d:08/22/1711:50 Date Date 08/29/1711:50 7 Certification: NC N/A l ACUSACE SC Other RECEIVING LABORATORY: Analytical Environmental Services, Inc. 3080 Presidential Parkway Atlanta, GA30340 Phone :(770) 457-8177 77 Fax: NA Laboratory ID Comments Received Received By u GS Date 1•3 0 Released By Date Received By /013: Released By Date Received By I; Date • Page I of 1 Page Page 20 of 24 r Aualytiecafl Environmental Services, Inc La Client: Prism Laboratories Project: 7080390 b ID: 1708N85 Sample Receiving Nonconformance: Date: 8-Sep-17 Case Narrative Insufficient sample was received 08-24-17 for TCLP SW 1311/8151A. Additional sample was received 08-31-17 c@r 10.30. Page Page 21 of 24 Analytiical Enviitroia esital Services, inc Client: Prism Laboratories Lab Order 1708N85 Project Name: 7080390 Lab ID: 1708N85-001A Date: 8-Sep-17 Client Sample ID: Tag Number: Collection Date: Matrix: Fourth Creek Sludge 7080390-01 8/22/2017 11:50:00 AM Solid Analyses Result Qual MDL Reporting Units BatchlD DF Date Analyzed Analyst Limit HERBICIDES, TCLP SW131.1/8151A 2,4,5-TP (Silvex) 2,4-D Surr: DCAA BRL BRL 82.8 0.030 0.051 0 0.20 0.20 50.1-132 (SW351OC) mg/L 247636 mg/L 247636 %REC 247636 09/07/2017 13:23 09/07/2017 13:23 09/07/2017 13:23 El EI EI Qualifiers: ' Value exceeds maximum contaminant level BRL Not Detected at MDL H Holding times for preparation or analysis exceeded N Analyte not NELAC certified B Analyte detectedin the associated method blank E Estimated value above quantiation ranee S Spike Recovery outside limits due to matrix > Greater than Result value J Estimated value detected below Reporting Limit < Less than Result value Page Page 22 of 24 bZ Jo £Z e6ed AES ANALYTICAL ENVIRONMENTAL SjRVICLS, INC. 1. Client Name: Access Anaiyticafi, inc. SAMPLE/COOLER RECEIPT CHECKLIST 2. Carrier: FedEx Q UPS ❑ Usps❑ Client El Courier Other 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. Yes No N/A AES Work Order Number: 17081'485 Details Comments Shipping container/cooler received in good condition? I 0 C lJ damaged • leaking I. other. Custody seals present on shipping container? r ' o'� Custody seals intact on shipping container? Temperature blanks present? Cooler temperature(s) within limits of 0-6°C? [See item 13 and 14 for temperature recordings.] y �i . r) Cooling initiated for recently collected samples / ice present 1 Chain of Custody (COC) present? n Chain of Custody signed, dated, and timed when relinquished and received? Sampler name and/or signature on COC? o' r Were all samples received within holding time? (o (1 TAT marked on the COC? to 0 If no TAT indicated, proceeded with standard TAT per Te ms & Conditions. El 13. Cooler 1 Temperature 1.3 14, Cooler 5 Temperature 15. Comments: 16. 17. 18. 19. 20. 21. 22. 23, 24. 25. 26. °C Cooler 2 Temperature °C Cooler 6 Temperature °C Cooler 3 Temperature °C Cooler 7 Temperature °C Cooler 4 Temperature °C °C Cooler 8 Temperature °c Yes No N/A I certify that I have completed sections 1-15 (dated initials). Details Comments TD 8/24/17 Were sample containers intact upon receipt? ©.) () O Custody seals present on sample containers? ) io Custody seals intact on sample containers? 00 F/ Do sample container labels match the COC? 0 0 Q incomplete info illegible • no label 1 other • Are analyses requested indicated on the COC? t^' Were all of the samples listed on the COC received? 0 samples received but not listed on COC • samples listed on COC not received ■ Was the sample collection date/time noted? ;o Did we receive sufficient sample volume for indicated analyses? o 0 Were samples received in appropriate containers? o C Were VOA samples received without headspace (< 1/4" bubble)? (4`.) ;®' Were trip blanks submitted? 0 ro listed on COC • not listed on COC • 27. Comments: 28. 29. 30. This section only applies to samples where pH can be checked at Sample Receipt. Yes No N/A Details I certify that I have completed sections 16-27 (dated initials). Comments MJ 8/24/17 Have containers needing chemical preservation been checked?"' v I I Containers meet preservation, guidelines? —0 �'' J I (30_ Was pH adjusted at Sample Receipt? f� �LJ ( I) Note: Certain analyses require chemical preservation but must be checked in the laboratory and not upon Sample Receipt such as Coliforms, VOCs and Oil & Grease/TPH. I certify that I have completed sections 28-30 (dated initials). Checklist 6.9.17 Rev 2 MJ 8/24/17 Page 6 of 7 17Z 10 tZ abed Analytical Environmental Services, Inc Date: 8-Sep-17 Client: Project Name: Worlcorder: Prism Laboratories 7080390 1708N85 ANALYTICAL QC SUMMARY REPORT 1BatchlD: 247636 Sample ID: MB-247636 Client ID: SampleType: MBLK Analyte TestCode: HERBICIDES, TCLP SWI311/8151A Units: ug/L BatchID: 247636 Prep Date: 09/05/2017 Rim No: 351385 Analysis Date: 09/06/2017 Seq No: 7728375 Result RPT Limit SPI( value SPIC Ref Val %REC Low Limit Iligh Limit RPD Ref Val %RPD RPD Limit Qual 2,4,5-TP (Silvex) 2,4-D Suer: DCAA BRL BRL 0.3448 0.20 0.20 0 0.5000 69.0 50.1 132 Sample ID: LCS-247636 Client ID: SampleType: LCS TestCode: HERBICIDES, SW1311/13151A Units: ng/L BatchlD: 247636 Prep Date: 09/05/2017 Run No: 351385 Analysis Date: 09/06/2017 Seq No: 7728376 Analyte Result RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit Qual 2,4,5-TP (Silvex) 2,4-D Surr: DCAA 0.2936 0.2616 0.3058 0.20 0.20 0 0.5000 0.5000 0.5000 58.7 52.3 61.2 50.7 50.1 50.1 117 119 132 Sample ID: 1708544-001BMS Client ID: SampleType: MS Analyte TestCode: HERBICIDES, TCLP SW1311/8151A Units: mng/L BatchTD: 247636 Prep Date: 09/05/2017 Run No: 351385 Analysis Date: 09/06/2017 Seq No: 7728379 Result RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit Qual 2,4,5-TP (Silvex) 2,4-D Surr: DCAA 0.03509 0.2194 0.3162 0.20 0.20 0 0.5000 0.5000 0.5000 7.02 43.9 63.2 46.3 43.3 50.1 126 132 132 JS Qualifiers: > Greater than Result value BRL Below reporting limit J Estimated value detected below Reporting Limit Rpt Lim Reporting Limit < Less than Result value E Estimated (value above quentitation range) N Analyte not NELAC certified S Spike Recovery outside limits due to matrix 13 Analyte detected in the associated method blank I -I Holding times for preparation or analysis exceeded R RPD outside limits due to matrix Pagei7 of 7 Fourth MA Fourth Creek WWTP Vicinity Map 600 Feet Date: January 21, 2015 Dwg: 2015SWR004 PLANT INFLUENT MH BAR SCREENS INFLUENT PUMP STATION Raw Influent ► DECHLORINATION BUILDING CHLORINE BASIN METERING FLUME CLARIFIERS RAS RAS WET WELL SLUDGE PSTMP A. AERATION BASIN 1J NQ. Ell AERATORS * FLOW DISTRIBUTION BOX EFFLUENT FLOW SPLITTER BOX E AERATION BASIN NO. 2 B WAS AERATORS L - STALIME SLUDGE TREATMENT FACILITIES CONVEYOR SLUDGE PUMPS COVERED SLUDGE STORAGE SLUDGE STORAGE PAD FLOW SCHEMATIC & WATER BALANCE FOURTH CREEK WASTEWATER TREATMENT PLANT CITY OF STATESVILLE SPILL RESPONSE PLAN OJECT: City of Statesville Land Application Permit WQ0014543 IN THE UNLIKELY EVENT OF A SPILL, THE FOLLOWING ACTIONS SHALL BE TAKEN IMMEDIATELY: 1. MANAGEMENT OF SPILL CLEAN-UP ACTIVITIES: The Fourth Creek WWTP Supervisor shall take immediate charge and initiate clean-up activities. The City of Statesville labor and equipment is to be utilized. In the event additional labor and equipment is required, assistance may be requested from the NC Department of Transportation and other private contractors as necessary. 2. HALT THE SOURCE OF THE SPILL: Such as a ruptured container or damaged transport unit. 3. CONTAIN THE SPILL: Form a barrier. Sufficient quantities of straw shall be used for such purposes. Earthen barriers may be constructed to augment the straw bale containment area of the spill. The Operations Manager or the person in charge on the spill site will advise the clean-up personnel where to get the straw, lime, and other items necessary to complete the clean-up operation, i.e., local farmers, farm supply centers, nurseries, etc. 4. CLEAN-UP: Employ front-end loaders, vacuum equipment, sludge application vehicles, and/or local septic tank service to remove as much of the spilled material as possible. Straw and/or sand should be scattered in the spill area to soak up the remaining material. The straw- and sand -soaked material will be collected and removed to a disposal area approved by representatives of the state regulatory agency. 5. FINAL CLEAN-UP: Employ rotary brush sweeper if needed, and apply lime to the spill area upon the approval of the clean-up efforts by the state regulatory representative. If the event occurs on private property, the clean-up will be completed to the satisfaction of the property owner and state regulatory representatives. The ultimate goal will be to restore the spill area to its original condition if possible. 6. NOTIFICATION: As soon as possible after the spill occurs, the City of Statesville Operations staff will notify the Fourth Creek WWTP Supervisor, and they will then be responsible for notifying other key City of Statesville personnel. 7. REPORTING: The City of Statesville personnel will notify the Mooresville Regional office (704) 235-2198 as soon as possible, but not more than 24 hours after, or on the next working day following the occurrence. The Fourth Creek WWTP Supervisor shall provide a written report within 48 hours of the spill to the Technical Services Director. The report shall list all relative information and actions taken. The City of Statesville personnel will file a written report to the Mooresville Regional office of the NCDENR within 5 days of the occurrence. For after-hours reporting the Division's emergency number shall be called to report all incidences (800-662-7956 or 800-858-0368 or 919-733-3300) 11Page 5/2/2018 OPERATIONS AND MAINTENANCE PLAN The City of Statesville Land Application Permit WQ0014543 Inspection Plan ections for the Land Application site will be conducted on an as needed basis. The inspection frequency is based on the time frame t it is going to take to complete the project and the amount of dry tons to be processed from this facility. The inspections will onsist of inspecting the Bio-Solids loading area. These inspections will consist of: 1. Verifying that all of the equipment is working properly. 2. Verify that all containment walls and curbing are working properly. 3. Insure that all manned equipment has a copy of the spill control plan, the permit, and the operations and maintenance plan 4. Verifying that the correct number samples of the Class B product have been taken and that it meets the criteria for the Land Application Permit. 5. The records will be kept in the project files in the respective office for the project. 6. The Permittee or Inspector shall report by telephone to the Mooresville Regional Office at 704-235-2198 as soon as possible but no later than 24 hours after or the next working day following the occurrence or the first knowledge of the occurrence of the following. • Any occurrence with the distribution program resulting in the land application of significant amounts of material that is abnormal in quantity or characteristics. • Any time that self -monitoring indicates that the facility has gone out of compliance with the permit. • Any process failure that results in the system not adequately treating the residuals. • Any spill or discharge from a vehicle or piping system during residuals transportation. • Any release that requires immediate reporting outside of normal business hours shall be called in to DENR at 1800- 662-7956, 1-800-858-0368, or 1-919-733-3300. These numbers are to be called in the event of a release to surface waters, imminent failure of a storage system when the event occurs outside of normal business hours. • Within 5 days of the first notice of on occurrence a written response in the form of a letter shall be sent to DENR outlining the actions taken or purposed actions taken to ensure that the problem does not recur. Persons responsible for inspections on this project are as follows: Andy Smith, 4th Creek WWTP ORC or his designee Andy Smith is the designated WWTP ORC for this project and his designees are the backup ORC's for this project. 2IPage 5/2/2018 OPERATIONS AND MAINTENANCE PLAN The City of Statesville Land Application Permit WQ0014543 Sampling Plan Sampling for this project consists of sampling the residuals during the time that land application is occurring. This will result in one round of sampling to occur before land application commences in order to insure that the residuals are suitable for land application. Based on the dry tonnage of this plant this will be six samples for all parameters per year. The residuals shall be sampled annually for the following: (Regulatory level Arsenic (5.0) 1, 4-Dichlorobenzene (7.5) Barium (100.0) 1, 2-Dichloroethane (0.5) Benzene (0.5) 1, 1-Dichloroethylene (0.7) Cadmium (1.0) 2, 4-Dinitrotoluene (0.13) Carbon tetrachloride Endrin (0.02) (0.5) Chlordane (0.03) Chlorobenzene (100.0) Chloroform (6.0) Chromium (5.0) M-Cresol (200.0) o- Cresol (200.0) p- Cresol (200.0) Cresol (200.0) 2,4-D (10.0) in milligrams per liter in parentheses.) Nitrobenzene (2.0) Pentachlorophenol (100.0) Pyridine (5.0) Selenium (1.0) Silver (5.0) Hexachlorobenzene (0.13 Tetrachloroethylene (0.7) Heptachlor (and its hydroxide) (0.008)Toxaphene (0.5) Hexachloro-1,3-butadiene (0.5) Trichloroethylene (0.5) Hexachlorethane (3.0) Lead (5.0) Lindane (0.4) Mercury (0.2) Methoxychlor (10.0) Methyl ethyl ketone (200.0) 2,4,5-Trichlorophenol (400.0) 2,4,6-Trichlorophenol (2.0) 2,4,5 TP (Silvex) (1.0) Vinyl Chloride (0.2) The residuals will also be sampled based on the chart below for the following constituents Dry Tons Generated (short tons per year) Monitoring Frequency (Established in 40 CFR 503 and 15A NCAC 02T.1111) <319 1 time per year =>319-<1,650 1 per Quarter (4 times per year) =>1,650-<16,500 1 every 60 days (6 times per year) =>16,500 1 every month (12 times per year) Aluminum Ammonia -Nitrogen Arsenic Cadmium Calcium Copper Lead Sodium Adsorption Ratio (SAR) Magnesium Mercury Molybdenum Nickel Nitrate -Nitrite Nitrogen Phosphorous Potassium pH Plant Available Nitrogen (calculation) Selenium Sodium % Total Solids Total Kjeldahl Nitrogen Zinc In order to meet pathogen and vector requirements the material will go through an aerobically digested treatment process. The residuals will meet pathogen and vector requirements through pH, time and temperature requirements. The samples will be pulled from the storage pads that are currently holding the Sta-Lime product. The samples that will be pulled are a TCLP and nutrient and metals sample to prove that the material is suitable for distribution. The nutrient and metal and TCLP sample will be collected randomly and consist of individual samples mixed together in order to get the composite sample for these parameters. This material is very consistent based on the fact that these residuals are thoroughly digested and mixed before processing and should not experience any seasonal fluctuations in the residuals. The following people are responsible for sampling: Andy Smith, Plant Manager or his designee. 31Pae 5/2/2018 OPERATIONS AND MAINTENANCE PLAN The City of Statesville Land Application Permit WQ0014543 Operational Functions The operation function of this project is going to involve loading dewatered belt press sludge. The dewatered belt press sludge will be loaded into the trucks that are suitable to transport and spread this product without spillage or leakage during transport. The dewatered belt press sludge will be spread at agronomic rates that are determined by the soil samples from the fields that the City of Statesville staff has collected. SAFETY MEASURES The City of Statesville believes in operating in a safety conscious manner and is has all employees participate in monthly safety courses that are designed to help its employees recognize safety issues and take steps to prevent accidents from occurring. In addition all City of Statesville, Water Resources employees have the authority to stop operations if they think any aspect of the operation is going to cause environmental or personal harm. Maintenance Schedule The City of Statesville will follow the maintenance schedule as recommended by the processing equipment manufacturer. Wage 5/2/2018 of Water Resources V1sion State of North Carolina Department of Environmental Quality Division of Water Resources 15A NCAC 02T .1100 — RESIDUALS LAND APPLICATION PROGRAM INSTRUCTIONS FOR FORM: RLAP 06-16 & SUPPORTING DOCUMENTATION lease use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these structions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This application is for -treatment, storage, transport, and/or land application of Class B residuals (may include residuals that are generated from a water treatment plant or other type facilities) on the proposed or currently approved land application site(s) under 15A NCAC 02T .1100. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Land Application Program (FORM: RLAP 06-16) Application: (All Application Packages): ® Submit the completed and appropriately executed Residuals Land Application Program (FORM: RLAP 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® The Applicant's Certification on Page 5 of this form shall be signed in accordance with I3A NCAC 0 T .0106(b). An alternate person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 1SA N0.Ar, .0106). ❑ If this project is for a modification of an existing permit, submit one copy of the existing permit. ® Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units. B. Application Fee (New and Major Modification Application Packages) ® Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental Quality (NCDEQ). Facility Classification New Permit Major Modification Major (land are permitted for > 300 acres) $1,310 $395 Minor (land are permitted for <300 acres) $810 $245 1- A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage; adds additional land application areas not previously approved for that particular program [including transferring of field(s) from one program to another]; adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted. There is no fee for minor modifications to a permit. C. Cover Letter (All Application Packages) List all items included in the application package, as well as a brief description of the requested permitting action. D. Environmental Assessments (Maybe Required — See 15A NCAC IC .0300) ❑ Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for the construction of the subject facilities. INSTRUCTIONS FOR FORM: RLAP 06-16 Page 1 of 3 E. Operation and Maintenance Plan (New and Renewal Application Packages) ❑ For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan. ❑ Submit the O&M Plan in accordance with 15A NCAC 02T .1110 and include at a minimum: ® Operational functions; describe the operation of the program to show what operations are necessary for the program to function and by whom the functions are to be conducted. ® Maintenance schedules; may include equipment calibration, maintenance of signs, etc. Ei Safety measures; may include safety training program, manuals, signs, etc. ®I Spill response plan; including control, containment, remediation, emergency contact information, etc. -.-Inspection-plan-including_the following information; ®' Names and titles of personnel responsible for conducting the inspections. ® Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program. ® Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed. El Sampling and monitoring plan including the following information; ® Names and titles of personnel responsible for conducting the sampling and monitoring. ® Detailed description of monitoring procedures including parameters to be monitored. ▪ Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures. ' THE FOLLOWING ADDITIONAL ITEMS (G to M) ARE REQUIRED FOR DEDICATED PROGRAM ONLY. F. Program Determination ❑ Dedicated residuals land application programs are ones in which land application sites meet the criteria in 15 NF' ( On :1161(1 ). Specifically, a residuals land application program is designated as dedicated if any of the following are applicable: ❑ Any land application site certified for the residuals land application program that receives residuals at rates or frequencies greater than agronomic rates. ❑ Any land application site certified for the residuals land application program that is used primarily for residuals disposal, and agricultural crop production is of secondary importance. ❑ Any land application site certified for the residuals land application program that receives residuals through fixed irrigation facilities or irrigation facilities fed through a fixed supply system. ❑ Please contact the Non -Discharge Permitting Unit if you need any assistance in determining whether your residuals program falls under the dedicated program definitions. G. Program Information ❑ Provide an explanation of why a dedicated system is required instead of a conventional non -dedicated system. ❑ Provide an explanation of the dedicated system and its operation. H. Detailed Site Maps (All New or Modification Application Packages) ❑ Submit three (3) sets of standard size plans and two (2) sets of 11" by 17" plans (electronic format is acceptable - Adobe PDF only). For Modifications, submit plans specific to the modification(s) only. ❑ Plans must include the following minimum items: ❑ A general location map, a vicinity map and a topographic map with contours not exceeding 10 feet or 25% of the total site relief and showing all facility related structures and fences within the land application area. ❑ The location of all wells (including usage and construction details if available), streams (ephemeral, intermittent, and perennial), springs, lakes, ponds, and other surface drainage features within 500 feet of the land application site(s). ❑ Delineation of the review and compliance boundaries ❑ Setbacks as required by 15A NCAC 02T .1108 ❑ Site property boundaries within, 500 feet of all waste treatment, storage, and disposal site(s). ❑ A map showing the entire irrigation area with an overlay of the suitable irrigation area depicted by the soil scientist's evaluation. The irrigation plans shall show each nozzle/emitter and wetted area (when applicable). Clearly label spray irrigation zones as they will be operated. ❑ Plans must depict a completed design and not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR CONSTRUCTION, etc.) that indicate that they are anything other than final plans. However, the plans may be labeled with the phrase: FINAL DESIGN - NOT RELEASED FOR CONSTRUCTION INSTRUCTIONS FOR FORM: RLAP 06-16 Page 2 of 3 ect Evaluation and Receiver Site Management Plan (A11 New Application Packages or Modifications that include new s) Submit a project evaluation and a receiver site management plan (if applicable) with recommendations concerning cover crops and their ability to accept the proposed application rates. Hydrogeologic Report (All New Application Packages or Modifications involving increasing the total design capacity) ❑, Submit a detailed hydrogeologic evaluation in accordance with 15A NCAC 02T .1104(d)(4) and current Division Policy available at: http://www.ncwater.orc/Rules Policies and Regulations/. The document shall be signed, sealed and dated by a qualified professional. K. Engineering Design Documents (All New or Modification Application Packages with fixed irrigation facilities or irrigation facilities fed through fixed supply system) ❑ Submit engineering design documents that have been signed, sealed, and dated by a NC licensed Professional Engineer and/or Professional Land Surveyor in accordance with 15A NCAC 02T .1104(d)(2). For Modifications, submit an updated site map specific to the modification(s) only. ❑ The design documents must include the following minimum items: Engineering plans for the facility and equipment except those previously permitted unless they are directly tied into the new units or are critical to the understanding of the complete process; El Specifications describing materials to be used, method of construction, and means for ensuring quality and integrity of the finished product including leaking testing; and ❑ Engineering calculations including hydraulic and pollutant loading, sizing criteria, hydraulic profile, total dynamic head curve analysis for each pump, and irrigation design. ❑ Soil mapping units shown on all disposal sites. L. Water Balance (All New Application Packages or Modifications that include new sites utilizing fixed irrigation facilities or irrigation facilities fed through fixed supply systems) ❑ Submit a completed and accurate water balance in accordance with 15A NCAC 021 1104(c1).(5) and current Division Policy available at: Itti-p://mmAymovitcr.orgautes_ Policies ..and _Reg tions/. M. Property Ownership Documentation (All New or Modification Application Packages involving new and/or relocated treatment or irrigation components) El Property ownership documentation shall consist of one of the following: ❑ Legal documentation of ownership (i.e., Ci1g, deed or article of incorporation),'or ❑ Written notarized intent to purchase agreement signed by both parties with a plat or survey map, or An easement running with the land specifically indicating the intended use of the property and meeting the requirements of i. A NCAC OIL .0 i on, or El A written notarized lease agreement signed by both parties, indicating the intended use of the property, as well as a plat or survey map. ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS: NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES WATER QUALITY PERMITTING SECTION NON -DISCHARGE PERMITTING UNIT By U.S. Postal Service: 1617 MAIL SERVICE CENTER RALEIGH, NORTH CAROLINA 27699-1617 TELEPHONE NUMBER: (919) 807-6464 INSTRUCTIONS FOR FORM: RLAP 06-16 By Courier/Special Delivery: 512 N. SALISBURY STREET RALEIGH, NORTH CAROLINA 27604 FAX NUMBER: (919) 807-6496 Page 3 of 3 `DIvision of Water Resources State of North Carolin� Department of Environmental Q uality Division of Water Resources 15A NCAC 02T .1100 — RESIDUALS LAND APPLICATION PROGRAM FORM: RLAP 06-16 I. APPLICANT INFORMATION: 1. Applicant's name: Applicant type: ❑ Individual ❑ Corporation ❑ General Partnership ❑ Privately -Owned Public Utility Federal ❑ State NO Municipal ❑ County Signature authority's name per 15A NCAC 02T .0106: Andy Smith Title: Assistant Director of Water Resources Applicant's mailing address: PO Box 1111 City: Statesville State: NC Zip: 28687-1111 Telephone number: (704) 878-3438 Email Address: asmith@statesvillenc.net 2. Consultant's name: License Number (for P.E.): Affiliation: ❑ On Staff ❑ Retained (Firm: ) Consultant's mailing address: City: State: Zip: ' Telephone number: (_) . Email Address: 3. Agronomist's name: License Number: Affiliation: ❑ N/A ❑ On Staff ❑ Retained (Firm: ) Agronomist's mailing address: City: State: Zip: Telephone number: ( ) — Email Address: 4. Soil Scientist's name: License Number: Affiliation: ❑ N/A ❑ On Staff ❑ Retained (Fuui:. Soil Scientist's mailing address: City: State: ; Zip: 1 Telephone number: ( ) - Email Address: 5. Fee submitted: $810 (See Instruction B) II. PERMIT INFORMATION: 1. Application is for (check all that apply): ❑ new, ❑ modified, X❑ renewed permit 2. If this application is being submitted to renew or modify an existing permit, provide the following: Permit number: W00014543 Date of most -recently issued permit: September, 2013 Date of most -recently certified Attachment A (if different than the permit): Date of most -recently certified Attachment B (if different than the permit): FORM: RLAP 06-16 Page 1 of 5 r1. SIDUALS LAND APPLICATION PROGRAM INFORMATION: Residuals Processing Facility's physical address: 693 Bell Farm Road City: Statesville State: NC Zip: 28677- Coordinates: Latitude: 25° 46' 29 N" Longitude: 80° 48' 50 W" Datum: Method of measurement: GPS 2. County where residuals land application program is headquartered: Iredell 3. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application program, their certification numbers, and their affiliations in the following table: Level of accuracy: Designation Name Affiliation Certification Number ORC Andy Smith City of Statesville LA 985516 Back -Up ORC Scott Austin City of Statesville LA 991939 Additional Back -Up ORCs (if applicable) If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application program, provide the candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training school and certification test: 4. Complete the following tables regarding management of the residuals land application program: a. Plant Available Nitroffen Summary: Determine the maximum plant available nitrogen (PAN) generated by all residuals source -generating facilities as currently certified and proposed for certification with this application and list the results in the following table: Maximum amount of residuals to be certified: 4th Creek @ 1,056 dry tons per year. PAN Pounds of PAN per Dry Ton (Weighted Average) Pounds of PAN per Year Surface Incorporation or Injection Surface Incorporation or Injection First -Year 27.24 mg/kg 26,5051bs Five -Year Maximum Adjusted 136.19 mg/kg 132,5231bs b. Land Application Site Use Summary: Summarize information regarding the land application sites as currently certified and proposed for certification with this application: Category Use Acres Comments Crops Forest or Plantation Row Crops Hay 14.1 Fescue Hay Pasture Total: Methods Surface Incorporation or Injection Total: FORM: RLAP 06-16 Page 2 of 5 c. Residuals Land Application Summary: Determine the minimum acreage required to land apply the residuals as currentl certified and proposed for certification assuming the scenarios listed in the following table: Assumed Application Rate (lbs PAN/ac-yr) Acres Required Using First -Year PAN Concentrations Acres Required Using Five -Year Maximum Adjusted PAN Concentrations Surface Incorporation or Injection Surface Incorporation or Injection 50 530 2,650 100 265 1,325.25 150 177 884 200 133 663 6. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application of the proposed residuals due to the violation of North Carolina Administrative Code (e.g. not enough storage, not enough land, vector reduction practices not in place, etc.): 7. Specify type of residuals program (See Instruction F): X❑ Non -dedicated❑ Dedicated If Dedicated, specify the following (check all that apply): ❑ Residuals program contains any land application site(s) that receives residuals at rates or frequencies greater than agronomic rates, explain; ❑ Residuals program contains any land application site(s) that is used primarily for residuals disposal, and agricultural crop production is of secondary importance, explain; ❑ Residuals program contains any land application site(s) that receives residuals through fixed irrigation facilities or irrigation facilities fed through a fixed supply system, explain; IV. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source Complete and submit the following Residuals Source Certification and all associated documentation. Residuals Source Certification V. LAND APPLICATION SITE INFORMATION: (Required for all new, renewed, or modified land application site) Complete and submit the following Land Applications Site Certification and all associated documentation. Land Application Siite Certification. doc FORM: RLAP 06-16 Page 3 of 5 rote: Item VI. Applicable to Dedicated Program with fixed irrigation system only. . DESIGN INFORMATION FOR FIXED IRRIGATION SYSTEM 1. The irrigation system is: ❑ Spray ❑ Drip 2. Disposal system is: ❑ existing ❑ proposed. 3. Minimum depth to mean seasonal high water table (SHWT) within irrigation sites(s) per Soil Scientist's Evaluation: ' feet below ground surface. Rules 15A NCAC 02T .0505(p) requires at least one -foot vertical separation between SHWT and ground surface. 4. Are there any artificial drainage or water movement structures within 200 feet of any irrigation area? El Yes or ❑ No If Yes, please explain if the soil scientist report addresses artificial structures and please indicate if structures are to be maintained or modified: 5. Loading rates recommended by the Soil Scientist Evaluation: Soil Series Fields within Soil Area Recommended Loading Rate (in/hr) Recommended Loading Rate (in/yr) 6. Design loading rates are equal or less than the loading rates recommended by Soil Scientist? ❑ Yes or ❑ No If No, explain why i3A NtA(1 On is not met: ; 7. Non -dedicated System Design (fill in the appropriate information for either a spray or drip irrigation system): Field / Zone Design Area (ft2) Number of Nozzles Maximum Application Rate (gallons/hr) Design Annual Loading Rate (gallons/yr) Total Spray Irrigation Design Element Plan Sheet Number Specification Page Number Wetted diameter of nozzles ft Wetted area of nozzles ft2 LL Nozzle capacity ? gpm Nozzle manufacturer / model / Elevation of highest nozzle ft FORM: RLAP 06-16 Page 4 of 5 Applicant's Certification (signing authority must be in compliance with 15A NCAC 02T .0106): The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105. Yes El No, Explain; SitvA U1zfe'(us Auc-,. veczrer (Signature Authority's Name — PLEASE PRINT) (Title) attest that this application for 3 (Facility Name) has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources may not -conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed and that if all required supporting information and attachments are not included, this application package will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes §143-215.6A and §143-215.6B, any person who knowingly makes any false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to exceed $10,000 as well as civil penalties up to $25,000 per violation. Signature: Date: 0(f FORM: RLAP 06-16 Page 5 of 5 Division of Water Resources Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 11-15): ❑ Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ❑ For new or renewed permits, submit a separate certification for each source facility. ❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. ❑ Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source -Generating Facility Information: ❑ For each source facility, attach the following: ❑ Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Mop ailidOtiPP fOf i §tll ❑ Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. ❑ Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. ❑ Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: ❑ For each source facility, attach the following: ❑ Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. ❑ Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1 RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: Andy Smith Status Code Facility Permit Holder Facility Name County Permit Number Maximum Dry Tons Per Year Current b Proposed R City of Statesville 3rd Creek WWTP Iredell NC0020591 975 N/A a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted) b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility). SUMMARY FOR FORM: RSC 06-16 Page 1 litWR <„------ - ,, ,___-----,--- D" ivision of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: 3th Creek WWTP 2. Facility permit holder is: ❑ Federal, Ol State, E Local Government, or 0; Private. Facility permit issued by: ® Div. of Water Resources, 0 Div. of Environmental Health, or 0 Other (explain:1). 3. Facility contact person and title: Andy Smith, Assistant Director Complete mailing address: PO Box 1111 City: Statesville State: NC Zip: 28687-1111 Telephone number: (704) 878-3438 E-mail address: asmith@statesvillenc.net 4. Facility physical address: 444 Third Creek Road City: Statesville State: NC Zip: 2867711 Coordinates: Latitude: 35° 75' N" Longitude: 80° 84' W" Datum: 1 Level of accuracy: , a- __ _ a Method of measurement: GPS 5. Purpose of the facility: treatment of municipal wastewater, 0 treatment of 100% domestic wastewater, 0 treatment of potable water, 0 treatment of 100% industrial wastewater, El treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: 60 % industrial and 40 % domestic) 0 other (explain: 1). 6. Does the facility have an approved pretreatment program: ►! Yes 0; No FORM: RSC 06-16 7. Facility permitted/design flow: 6.0 MGD and facility average daily flow: 0.9 MGD 8. Average amount of residuals being generated at this facility 500 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: Two 2 meter belt presses Type and volume of residuals storage (i.e., outside of residuals treatment units): 3 million gallon aerobic digester 11. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 40 CFR Part 503 or 0' 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: Biological 0 Non -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 06-16 Page 1 of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: Q yes El no. If yes, list the nnmber(s): �T1 b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: 0yes El no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Prism and Date of analysis: 8/22/17 Passed corrosivity test: i yes Li no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: E yes 0 no. Flashpoint: i I °F (> 140°F) Passed reactivity test: w yes Lino. HCN: I mg/kg (<250) & H2S: ; mg/kg (<500) TCLP Parameter Limit (mg/l) Result (mg/l) TCLP Parameter Limit (mg/I) Result (mg/l) Arsenic 5.0 <0.050 Hexachlorobenzene 0.13 <0.050 Barium 100.0 <5.0 Hexachloro-1,3-Butadiene 0.5 <0.050 Benzene 0.5 <0.025 Hexachloroethane 3.0 <0.050 Cadmium 1.0 <0.025 Lead 5.0 <0.050 Carbon Tetrachloride 0.5 <0.025 Lindane 0.4 Chlordane 0.03 <0.0025 Mercury 0.2 <0.010 Chlorobenzene 100.0 <5.0 Methoxychlor 10.0 <0.00050 Chloroform 6.0 <0.30 Methyl Ethyl Ketone 200.0 <10 Chromium 5.0 <0.25 Nitrobenzene 2.0 <0.050 m-Cresol 200.0 Pentachlorophenol 100.0 <0.25 o-Cresol 200.0 I Pyridine 5.0 <0.25 p-Cresol 200.0 Selenium 1.0 <0.10 Cresol 200.0 Silver 5.0 <0.25 2,4-D 10.0 Tetrachloroethylene 0.7 <0.035 1,4-Dichlorobenzene 7.5 <0.38 Toxaphene , 0.5 <0.025 1,2-Dichloroethane 0.5 <0.025 Trichloroethylene 0.5 <0.025 1,1-Dichloroethylene 0.7 <000083 2,4,5-Trichlorophenol 400.0 <0.25 2,4-Dinitrotoluene 0.13 <0.050 2,4,6-Trichlorophenol 2.0 <0.10 Endrin 0.02 <0.00050 2,4,5-TP (Silvex) 1.0 Heptachlor and its Hydroxide 0.008 <0.00050 Vinyl Chloride 0.2 <0.20 FORM: RSC 06-16 Page 2 of 5 pir Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Waypoint and Date of analysis: 1/13/17 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 3.34 Cadmium 85 39 13.2 Copper 4,300 1,500 327 Lead 840 300 84.6 Mercury 57 17 <0.400 Molybdenum 75 n/a 19.4 Nickel 420 420 53.3 ' Selenium 100 100 6.87 Zinc 7,500 2,800 1,020 b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: i and Date of analysis: Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) Q >0but<25 30 200 210 OI > 25 but < 50 34 220 240 > 50 but < 75 39 260 270 > 75 but < 100 46 300 320 Q > 100 but < 125 53 360 390 > 125 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5 Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 13.96 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Waypoint and Date of analysis: 1/13/17 Parameter Result (mg/kg) Aluminum 14,400 Ammonia -Nitrogen 2,650 Calcium 14,300 Magnesium 3,280 Nitrate -Nitrite Nitrogen 159 pH (Standard Unit) 6.61 Phosphorus 16,300 Potassium 3,490 Sodium 1,310 Total Kj eldahl Nitrogen 43,100 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): _} [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This rate is a (check one): 0default value, or Q actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: , .._. e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (1st) Year PAN (mg/kg) Five -Year Maximum Adjusted PAN • (mg/kg) Surface 27.24 Injection/Incorporation 136.19 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: FORM: RSC 06-16 Page 4 of 5 ra. thogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: For Distribution/Land Application of Class A or Equivalent: ❑; A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or ❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): ❑,, Altemative 1 [15A NCAC 02T.1106(b)(3)(A)] - Time/Temperature Compliance. ❑! Altemative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment. ❑; Alternative 3 [15A NCAC 02T.1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 4 [15A NCAC 02T.1106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. El Alternative 5 [15A NCAC 02T.1106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑{ composting, ❑; heat drying, ❑ heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Land Application of Class B: ❑' Alternative 1 [15A NCAC 02T.1106(c)(1)] - Fecal Coliform Density Demonstration. Alternative 2 [15A NCAC 02T.1106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: ►1 aerobic digestion, El air drying, ❑ anaerobic digestion, ❑I composting, or ❑', lime stabilization. c. For Surface Disposal: ❑'; Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. • Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. El Exempt - If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 1 8. Vector Attraction Reduction (VAR): Per 1 $A NhA 09T:1 107, specify how residuals will meet the VAR requirements: Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). El Alternative 2 [15A NCAC 02T.1107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). Er Alternative 3 [15A NCAC 02T.1107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). Z Altemative 4 [15A NCAC 02T.1107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). • Alternative 5 [15A NCAC 02T.1107(a)(5)] - 14-Day Aerobic Processes. ❑; Alternative 6 [15A NCAC 02T.1107(a)(6)] - Alkaline Stabilization. ❑; Alternative 7 [15A NCAC 02T.1107(a)(7)] - Drying of Stabilized Residuals. El Alternative 8 [15A NCAC 02T.1107(a)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [15A NCAC 02T.1107(a)(9)] - Injection. ❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation. • Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.1107(b)(2)]. El Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 WR 'vision of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources LAND APPLICATION SITE CERTIFICATION INSTRUCTIONS FOR FORM: LASC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This certification provides detailed information of receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 06-16 or FORM: SDR 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Land Application Site Certification (FORM: LASC 06-16): ❑ Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. For new or renewed permits, submit the requested information for all land application sites. ❑ For modified permits, submit the requested information for only those sites that are new, transferred or affected by the proposed modification. B. Land Application Site Information: R The status of the land application site with respect to this residuals land application program must be provided in table I. The status categories and their corresponding codes are as follows: + New (N) + Renewed (R) ♦ Modified (M) 0 Transferred (T) ♦ Deleted (D) ❑ Attach the following in accordance with each status code: Required Item Status Code N R T M County Board Notification. doc tiff ✓ '/ '/ * Land Owner Agreement (If applicable) ✓ ✓ ✓ ✓ Setback Waiver Agreement An updated for Residuals vicinity/setback map in accordance with the "Map Guidance ✓ ✓ ✓ Land Application Permits" A soils and Evaluation Policy" agronomic evaluation in accordance with the "Soil Scientist ✓ INSTRUCTIONS FOR FORM: LASC 06-16 Page 1 of 3 An updated accounting of the land application site's cumulative pollutant loading rates (CPLRs) ✓ V Required Item Status Code N R T M For previously permitted sites without a soil series name indicated in the Attachment B, submit County Soil Survey Map (or equivalent) clearly indicate the location of the land application site and in accordance with the soil map requirements in the "Soil Scientist Evaluation Policy" ✓ ✓ V Acknowledgement of field transfer from Land Owner (Fields may not be permitted to multiple Permittees over the same time period) * This item may be required for land application site with a status code "M", please contact the Division if you need assistant in determining attachment requirements. ® Crop Type should include the most likely crop types for the life of the permit (five years). ® Predominant Soils Series Name must be either the name of the soil indicated in Attachment `B" of the existing permit, or name of the soil series as provided by the licensed soil scientist. ® Predominant Soil Mapping Unit or Representative Slope: Either the Soil Mapping Unit or the representative slope of each site must be provided. The predominant soil -mapping unit must be consistent with the predominant soil series name. Please note that the soil mapping units are variable between Counties, so care should be taken in properly identifying the correct mapping unit. If a representative slope is provided, it must be determined accordingly: ❑ For sites previously permitted for use, but do not have an established soil mapping unit (the mapping unit provides information on both the soil series name and the slope of the soil), the Applicant may determine the representative slope by using the average slope provided in the County Soil Survey (or equivalent). A soil type with a slope range of 4 - 8% would have a representative slope of 6%. ❑ New Sites to be permitted must have slopes determined as part of the soils report prepared by a licensed soil scientist. Acceptable methods for determining location coordinates (i.e., latitude and longitude) and their corresponding codes are as follows: • Address Matching (ADD) • Digital or Raw Photo Extraction (EXT) • Aerial Photography with Ground Control (AER) • Geodetic Quality GPS Survey (GEO) • Cadastral Survey (SUR) • LORAN-C Navigation Device (LOR) • Conversion from Coordinate Plane (CP) • Navigation Quality GPS-(GPS) • Conversion from Township -Section -Range (TSR) • Remote Sensing (RS) • Conversion from Universal Trans Mere (UTM) • Zip Code Centroid (ZIP) • Map Interpretation by Digital or Manual Extraction (MAP) C. Waterbody and Classifications Information: (new sites only) ❑ Use an 8.5 by 11-inch copy of the portion of a 7.5-minute USGS Topographic Map to identify the location where the residuals program activities are planned to occur as well as the closest downslope surface waters as clearly as possible. Each map portion must be labeled with the map name and number, the identified location, and be of clear and reproducible quality. ❑ Surface water body classifications information may be found at: p;//deb, o, an/aboutidivi.8 I tt,/water_ ro mime sflal ann ingLeJ as sfte ationl•siandardsLeinaifieations ❑ Any questions concerning the waterbody and its classification, please contact the Division's regional offices. ❑ A list of the Division's regional offices, their county coverage, and their contact infoiuiation may be downloaded at: http://deq,nc,gov/contact/re gional-offices ❑ General Instructions: There are 17 river basins in North Carolina. Each basin has associated waterbodies with assigned subbasins, location descriptions, stream index numbers and established classifications. 1. Identify the project area on a 7.5 minute USGS topographical map (an 8.5 x 11-inch sheet showing the project area should be submitted with the permit application regardless of whether a Stream classification was completed). 2. Determine the names of all the closest down slope surface waters from the project site. For unnamed tributaries, see Table 1: Unnamed Tributaries Entering Other States or for Specific Basin Areas. Label any unnamed tributaries as "UT to stream name" as the waterbody name. 3. Open the link http://deq.nc.gov/about/divisions/water-resources/planning/classification-standards/classifications. ❑ Stream Classification Process: One of the options below may be used depending on the known initial project information. ❑ KNOWN BASIN WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Select proper basin from the List all Waterbodies in Basin sorted report. Sort hydrologically as this will provide the proper location descriptions if multiple runs. INSTRUCTIONS FOR FORM: LASC 06-16 Page 2 of 3 2. Locate the name of the identified waterbody (from General Directions) on the list. 3. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 4. Record all Basins, Stream Index Numbers and Classifications applicable to the project. ❑ KNOWN COUNTY WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Select the proper county from the List all Waterbodies in county, hydrologically report. 2. Locate the name of the identified waterbody (from General Directions) on the list. 3. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 4. Record all Basins, Stream Index Numbers and Classifications applicable to the project. ❑ UNKNOWN BASIN WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Use the Clickable basin map to hydrologically sorted list report. 2. Click on the approximate project location to bring up the hydrologically sorted list. 3. Locate the name of the identified waterbody (from General Directions) on the list. 4. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 5. Record all Basins, Stream Index Numbers and Classifications applicable to the project. ❑ Notes on index number and unnamed streams: Unnamed Streams 15A NCAC 02B .0301(i). ❑ Any stream which is not named in the schedule of stream classifications carries the same classification as that assigned to the stream segment to which it is tributary (at the point of entry) except: (A) unnamed streams specifically described in the schedule of classifications; (B) unnamed freshwaters tributary to tidal saltwaters will be classified "C"; or (C) after November 1, 1986, any newly created areas of tidal saltwater which are connected to Class SA waters by approved dredging projects will be classified "SC" unless case -by -case reclassification proceedings are conducted. ❑ The following river basins have different policies for unnamed streams entering other states or for specific areas of the basin: Unnamed Tributaries Entering Other States or for Specific Basin Areas Hiwassee River Basin Streams entering Georgia or Tennessee shall be classified "C Tr." Little Tennesse River Basin And Savannah River Drainage Area Streams entering Georgia or Tennessee shall be classified "C Tr." Such streams in the Savannah River drainage area entering South Carolina shall be classified "B Tr." French Broad River Basin Streams entering Tennessee will be classified "B." Watauga River Basin Streams entering the State of Tennessee are classified "C." Broad River Basin Streams entering South Carolina are classified "C." New River Basin Streams entering the State of Tennessee are classified "C." Catawba River Basin Streams entering South Carolina are classified "C." Yadkin -Pee Dee River Basin Streams entering Virginia are classified "C," and such streams entering South Carolina are classified "C." Lumber River Basin Streams entering South Carolina are classified "C Sw." Roanoke River Basin Streams entering ,Virginia are classified "C." Except that all backwaters of John H. Kerr Reservoir and the North Carolina portion of streams tributary thereto not otherwise named or described shall carry the classification "B," and all backwaters of Lake Gaston and the North Carolina portion of streams tributary thereto not otherwise named or described shall carry the classification "C and B." Chowan River Basin Streams entering Virginia are classified "C." Tar -Pamlico River Basin All drainage canals not noted in the schedule are classified "C Sw." except the main drainage canals to Pamlico Sound and its bays which shall be classified "SC." Pasquotank River Basin All drainage canals not noted in the schedule are classified "C." INSTRUCTIONS FOR FORM: LASC 06-16 Page 3 of 3 LAND APPLICATION SITE CERTIFICATION Applicant's name: City of Statesville Land application sites currently certified: 29.4 net acres and Total to be certified: 29.4 net acres. I. LAND APPLICATION SITE INFORMATION (See Instruction 13): Status Code" Site/Field ID Landowner(s) Lessee(s) or•Operator(s) Net Acres County Crop(s) Predominant Soil Series Nameb Mapping Unit or Rep. Slope` R 02 City of Statesville 3rd Creek WWTP 14.10 Iredell Fescue Hay Cecil CeB2 2-6% N - —, N 1 N- - -- - -- _ — _, N -- i 1 N } t N r i N ______ , — :_�— _ t ... __-1 i d Status Code for land application sites are: + N (New) ♦ R (Renewed) + M (Modified) + T (Transferred) e D (Deleted) b Soil Series Name (i.e. Appling, Cecil, etc.) 'Mapping Unit must be consistent with those used in the County Soil Survey (i.e. for a 2-8% slope Cecil in Anson County the mapping unit is CeB2) II. WATERBODY AND CLASSIFICATIONS INFORMATION (See Instruction C): Site/Field ID Latitude Longitude Location Datum Location Method Code Location Accuracy Waterbody Subbasin and Stream Index No. Current and Proposed p Class 02 35° 44' 24" 80° 50' 24" NAD 83 ADD Nearest Second 03-07-06/03040102 C C ° II° ' " NAD 83 ADD Nearest Second 1 8 0 " ° ' ' '" NAD 83 ADD Nearest Second , 1 0 ' '' i- If ° ' " NAD 83 ADD Nearest Second ° ; _ . __II ° •„ NAD 83 ADD Nearest Second 1 j ! ,. NAD 83 ADD Nearest Second ; _. — ° '`° r� , _ ° - ` � NAD 83 ADD Nearest Second [ -- -I _ ° , —. �° `" _:° NAD 83 ADD Nearest Second _ _I Note: Please keep the site information (I.) and waterbody information (II.) of the same field on the same page. FORM: LASC 06-16 ISM LABORATORIES, INC. City of Statesville, NC Andy Smith P.O. Box 1111 Statesville, NC 28687 IFull -Service Analytical & Environmental Solutions NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Project: Sludge (Hazardous Testing) Project No.: 3rd Creek Sludge Lab Submittal Date: 08/22/2017 Prism Work Order: 7080391 Case Narrative 09/11/2017 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Narrative Notes: Reactivity analysis was subcontracted to GCAL. TCLP Herbicide analysis was subcontracted to AES. Laboratory reports are attached. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Robbi A. Jones Reviewed By Robbi A. Jones President/Project Manager President/Project Manager Data Qualifiers Key Reference: CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken. D RPD value outside of the control limits. ICV ICV result is above the control limits. Analyte not detected in the sample. No further action taken. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 24 R aI M Full -Service Analytical & I Environmental Solutions LSBORATORIE$ ING ent Sample ID Third Creek Sludge Sample Receipt Summary 09/11/2017 Prism Work Order: 7080391 Lab Sample ID Matrix Date Sampled Date Received 7080391-01 Solid 08/22/17 08/22/17 Samples were received in good condition at 3.9 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 I Page 2 of 24 I Full -Service Analytical & Environmental Solutions 77LABORATORIES ING ity of Statesville, NC Attn: Andy Smith P.O. Box 1111 Statesville, NC 28687 Project: Sludge (Hazardous Testing) Project No.: 3rd Creek Sludge Sample Matrix: Solid Laboratory Report 09/11/2017 Client Sample ID: Third Creek Sludge Prism Sample ID: 7080391-01 Prism Work Order: 7080391 Time Collected: 08/22/17 11:55 Time Submitted: 08/22/17 15:30 Parameter Result Units Report Limit MDL Dilution Method Analysis Analyst Factor Date/Time Batch ID General Chemistry Parameters % Solids Corrosivity-pH Ignitability TCLP Extraction by EPA 1311 23.2 4.8 Pass % by 0.100 Weight' pH Units mm/sec 0.10 0.100 1 *SM2540 G 8/31/17 16:00 JLB P710012 1 *9045D 8/24/17 10:47 BMS P7H0445 1 *1030 8/24/17 9:00 BMS P7H0440 TCLP Extraction TCLP Extraction TCLP Metals Complete Complete N/A N/A 1 *1311 8/26/17 10:05 JAB P7H0487 1 *1311 ZHE 9/6/17 12:34 KDM P710063 Mercury Arsenic Barium Cadmium Chromium Lead Selenium Silver BRL BRL BRL BRL BRL BR L BRL BRL TCLP Organochlorine Pesticides by GC/ECD mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0.010 0.050 5.0 0.025 0.25 0.050 0.10 0.25 0.000030 1 0.012 1 0.0065 1 0.00065 1 0.0038 1 0.0080 1 0.022 1 0.00050 1 *7470A *6010D *6010D *6010D *6010D *6010D *6010D *6010D 9/1/17 12:38 JAB 8/28/17 15:44 JAB 8/28/17 15:44 JAB 8/28/17 15:44 JAB 8/28/17 15:44 JAB 8/28/17 15:44 JAB 8/28/17 15:44 JAB 8/28/17 15:44 JAB P7H0572 P7H0505 P7H0505 P7H0505 P7H0505 P7H0505 P7H0505 P7H0505 Chlordane Dieldrin Endrin gamma-BHC Heptachlor Heptachlor Epoxide Methoxychlor Toxaphene BRL BRL BRL BRL BRL BRL BRL BRLCCV mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L 0.0025 0.00050 0.00050 0.00050 0.00050 0.00050 0.00050 0.025 0.00047 1 0.000070 1 0.000075 1 0.000065 1 0.000085 1 0.000065 1 0.00020 1 0.00037 1 *8081B *8081B *8081B *8081B *8081B *8081B *8081 B *8081B 8/28/17 17:35 JMC 8/28/17 17:35 JMC 8/28/17 17:35 JMC 8/28/17 17:35 JMC 8/28/17 17:35 JMC 8/28/17 17:35 JMC 8/28/17 17:35 JMC 8/28/17 17:35 JMC P7H0495 P7H0495 P7H0495 P7H0495 P7H0495 P7H0495 P7H0495 P7H0495 Surrogate Recovery Control Limits Decachlorobiphenyl Tetrachloro-m-xylene TCLP Semivolatile Organic Compounds by GC/MS 83 % 81 % 13-186 40-134 2,4,5-Trichlorophenol 2,4,6-Trichlo roph enol 2,4-Dinitrotoluene 2-Methylphenol 3/4-Methylphenol Hexachlorobenzene Hexachlorobutadiene Hexachloroethane Nitrobenzene Pentachlorophenol BRL BRL BRL BRL BRL BRL BRL BRLICv BRL BRL mg/L 0.25 0.0016 1 *8270D 8/29/17 18:54 JMV P7H0520 mg/L 0.10 0.0018 1 *8270D 8/29/17 18:54 JMV P7H0520 mg/L 0.050 0.0014 1 *8270D 8/29/17 18:54 JMV P7H0520 mg/L 0.050 0.0018 1 *8270D 8/29/17 18:54 JMV P7H0520 mg/L 0.050 0.0015 1 *8270D 8/29/17 18:54 JMV P7H0520 mg/L 0.050 0.0013 1 *8270D 8/29/17 18:54 JMV P7H0520 mg/L 0.050 0.0021 1 *8270D 8/29/17 18:54 JMV P7H0520 mg/L 0.050 0.0017 1 *8270D 8/29/17 18:54 JMV P7H0520 mg/L 0.050 0.0026 1 *8270D 8/29/17 18:54 JMV P7H0520 mg/L 0.25 0.0012 1 *8270D 8/29/17 18:54 JMV P7H0520 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 24 IS LABORATORIES, INM 0. y of Statesville, NC ttn: Andy Smith P.O. Box 1111 Statesville, NC 28687 Parameter Full -Service Analytical & Environmental Solutions Result Project: Sludge (Hazardous Testing) Project No.: 3rd Creek Sludge Sample Matrix: Solid Units Report MDL Limit Laboratory Report 09/11/2017 Client Sample ID: Third Creek Sludge Prism Sample ID: 7080391-01 Prism Work Order: 7080391 Time Collected: 08/22/17 11:55 Time Submitted: 08/22/17 15:30 Dilution Method Analysis Analyst Factor Date/Time Batch ID Pyridine BRLICV mg/L 0.25 0.0010 1 *8270D 8/29/17 18:54 JMV P7H0520 Surrogate Recovery Control Limits 2,4,6-Tri bromophenol 2-Fluorobiphenyl 2-Fluorophenol Nitrobenzene-d5 Phenol-d5 Terphenyl-d14 TCLP Volatile Organic Compounds by GC/MS 71 % 71 % 49 % 60 % 32 % 83 % 43-140 44-119 19-119 44-120 11-52 50-134 1,1-Dichloroethylene 1,2-Dichloroethane 1,4-Dichlorobenzene Benzene Carbon Tetrachloride Chlorobenzene Chloroform Methyl Ethyl Ketone (2-Butanone) Tetrachloroethylene Trichloroethylene Vinyl chloride BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL mg/L 0.035 0.00083 1 *8260B 9/6/17 14:28 KDM P710064 mg/L 0.025 0.00066 1 *8260B 9/6/17 14:28 KDM P710064 mg/L 0.38 0.00050 1 *8260B 9/6/17 14:28 KDM P710064 mg/L 0.025 0.00048 1 *8260B 9/6/17 14:28 KDM P710064 mg/L 0.025 0.0011 1 *8260B 9/6/17 14:28 KDM P710064 mg/L 5.0 0.00062 1 *82603 9/6/17 14:28 KDM P710064 mg/L 0.30 0.00076 1 *82608 9/6/17 14:28 KDM P710064 mg/L 10 0.0024 1 *8260B 9/6/17 14:28 KDM P710064 mg/L 0.035 0.00098 1 *8260B 9/6/17 14:28 KDM P710064 mg/L 0.025 0.00078 1 *8260B 9/6/17 14:28 KDM P710064 mg/L 0.020 0.00097 1 *8260B 9/6/17 14:28 KDM P710064 Surrogate Recovery Control Limits 4-Bromofluorobenzene Dibromofluoromethane Toluene-d8 103 % 102 % 99 % 80-124 75-129 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 24 Sample Extraction Data Method: Solids, Dry Weight Number Batch Initial Final Date/Time 80391-01 P710012 30 g 30 g 08/31/17 16:00 Prep Method: 1311 Lab Number Batch Initial Final Date/Time 7080391-01 7080391-01 Prep Method: 3010A Lab Number P710063 P7H0487 Batch 12.5 g 100 g 250 mL 2000 mL 09/05/17 15:33 08/25/17 15:30 Initial Final Date/Time 7080391-01 Prep Method: 7470A Lab Number P7H0505 10 mL 50 mL 08/28/17 10:25 Batch Initial Final Date/Time 7080391-01 Prep Method: 3510C GC Lab Number P7H0572 20 mL 30 mL 09/01/17 7:25 Batch Initial Final Date/Time 7080391-01 Prep Method: 3510C MS Lab Number P7H0495 200 mL 10 mL 08/28/17 9:49 Batch Initial Final Date/Time 7080391-01 Prep Method: 5030B Lab Number P7H0520 200 mL 1 mL 08/29/17 9:41 Batch Initial Final Date/Time 7080391-01 P710064 1 mL 10 mL 09/06/17 9:52 Subcontracted Analyses The following analyses were subcontracted to Analytical Environmental Services , Inc. Lab Number Analysis 7080391-01 Herbicides TCLP (Sub) The following analyses were subcontracted to Gulf Coast Analytical Labs, Inc. Lab Number Analysis 7080391-01 Reactivity, Cyanide (Sub) 7080391-01 Reactivity, Sulfide (Sub) This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 24 II NN 07 CUSTODY' RECORD R It }) LAaOnA'I"OnIEs. INC. 49 Spr'nghrook Road • Phone 794152e- 364 Client Company Name: C u �, Report To/Contact Name: A Full -Service Analytical & Environmental Solutions Charlotte, NC 25217 Fax: 7t)k/525.4499 svra ' g e rr :Drc. Reporting Address: 6'Jwipi_ i5Jai) Q° , -i r PAGE DC (MIPSTE 0 70 EMS!U! D3C PROPER MUMS: Project Name: Short Hold Analysis: (Ves) (No) UST Project: (Ves) (NO) `:Please ATTACH any project specific reporting (QC LEVEL i Dl Oil DV) provisions and/or QC Requirements invoice To: Address: S.emples IN'FAC'i won arrial?: Received ON`WET ICE?<• `. PROPER'PRESERVATIVES iiidicted? Receivers WITHIN:HcLD1NG TIMES? CUST(1D'YSEAI S NTACT? VOLATILESIIec,;d W/OU:C.I tDSPAC? • PROPER CONTAINERS used? Lq- F _ TEMP: Therm {C!i_:� � "'. -Obsei:ved: ' y °C i. Carl :E_ °C YES. intone: o e- Y •- O a u v rg) Irax YcY2sy (Nol: et3'r-o'V " 00)30 TO BE POLLED ON BY CLIENT/SAMPLING PERSONNELEmail Certification: IELAC Do® FL MC Purchase Order No./Billing Reference Address: Requested Due Date O 1 Day O 2 Days O 3 Days ® 4 Days O 5 Days Type: PDFr_Excel Other "Wonting Days" ® 6-9 Days Be SC ®�GiEG� N/A EDD O Standard 10 days ®pue Appoovedust Site Location Herne: Samples received after 14:00 will be processed next business day. Water Chlorinated: YES NO Sample Iced Upon Collection: YES NO_ Side Location Physical Address: Turnaround time is based on business days, excluding weekends and holidays. (SEE REVERSE FOR TERMS Si CONDITIONS REGARDING SERVICES RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) CLIENT DESCRIPTION DATE COLLECTED TIME COLLECTED MATRIX (SOIL, SAMPLE CONTAINER PRESERVA- TIVES TIVES ANALYST :REQUESTED //// / REMARKS // PRISM LAB ID MO. *TYPE VPE SEE BELOW NO. SIZE MVLDTARY HOURS WATER OR SLUDGE) 7g9a0J Caccif g fici 55 to " aI10a ( p" 11 a qi TC1�P lk."r SQQ qI' v t1 RE -4Fes`it0'(f0 r/r1LJ 0 4 ?L_Si l �I((� 4All1' :. _ I ...1, ti Vol v red 3 pc d ;9 Hr, ICE P ll RL; FOCI e f 'J Sampler's Signature y �.�°r�;�i� ! + 'f Sampled By Name)19 &] �r� t '.'� B © Y fig !T3rviy4R[ip,}1�L} r1O!Fu Ts l Cs'ri (Print q9' u9,%� A c�b Affiliation Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized. r( _ -.�wFp {. t!r!�,4i] A Resin fished By: (Signa { e) Vic' ti // Reei e B SI n7<ue� t 9 1 rf ,�"✓ Dal :-- ' - •. Military/Hours /Hours ry '') Additional Comments sitO A!rlVe Time: Re1J s .tshed By: (Signature) "'-_ R'.,ce1,ed By: (Signature) '�' Date S!te e nrtU e Time: �1 P gp! We Bi y: (Sig `a ure) Received F`'� Prism,-y]boratories lay ��c / Date f=!old :Tech l-oc, � ii ?i i (� ��N: 0 f'1, i',� 'C') - V " I -2 @ 530 -:Mifeade: v od of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CU.��rr"rODY SEALS FOR TRA ilSPORTATION TO THE LABORATORY. COC Group No. CO 0) SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNYIL RECEIVED AT THE LABORATORY. G d Ex ❑UPS ❑ Hand -delivered C�ism Field Service ❑ Other - 7 oto r `I o )ES: LIST: -- CRjj6�UNDWATER: (DRINKING WATER: SOLID WAS T P: RCRA: CERCLA LAl�°[r�i OLL OTl D�CLv: r't - lv C®SC ©NC ©SC 0IC ®SC 1 NC ®SC INC ®SC ElNC0SC C11NC 0SC ®NC ®SC ONC ®SC . R� ` `° I°` ® O O o ® 0 0 ® _INTAENER Oi=lsrw+if•_,`-i- TYPE CODES: A = Amber C = Clear G= Glass P = Plastic: TL = Teflon -Lined Can VIA = Vntatile Clrnanina Anakrcts 17arr I -foam Snaral :-" AccESS A NA LYTICA INC. MALY MAL REPORT CLIENT Prism Laboratories PO Box 240543 Charlotte, NC 28224 ATTENTION Robbi Jones PR...MOT D 7080391 LABORATORY REPORT NUMBER 217082416 DATE 08/29/2017 Primary Data Review By Secondary Data Review By f" " i ./ ..---,--L----/--ti:i — 4 Authorized Signature PLEASE NOTE: Ashley B. Amick Project Manager, Access Analytical, Inc. aamick@accessanalyticalinc.com - Unless othenrrise noted, all analysis on this report per at Gulf Coast Analytical Labs (GCAL), 7979 Innovation Park Dr., Baton Rouge, LA 70320. - GCAL is SCDHEC certified laboratory # 73006, 11lCDEHR certified lab # 618, GA certified lab # LA-01955, NELAP certified laboratory 01955 - Local support services for this project are provided by Access Analytical, Inc.. Access Analytical is a representative of GCAL serving clients in the SC/NC/GA areas. All questions regarding this report should be directed to your local Access Analytical representative at 803.781.4243 or toll free at 888.315.4243. Lab Report#: 217082416 Poe 1 of 11 I Page 7 of 24 AttAt.S71e:A. t'-o.31.")Recr-tiR17.5, LLC NELAP CERTIFICATE NUMBER: 01955 DOD ELAP CERTIFICATE NUMBER: L14243 NALYT1CAL RESULTS• PERFORMED BY GCAL, LLC 7979 Innovation Park Dr. Baton Rouge, LA 70820 Report Date 08/29/2017 GCAL Report 217082416 iI Project 7080391 Deliver To Robbi-Jones Prism Laboratories PO Box 240543 Charlotte, NC 28224 800-529-6364 Additional Recipients NONE PJLA Test trig DtiD ELAP Lab Reportg: 217082416 13(-ir, 9 nf I I I Page 8 of 24 9 t iILAL L CJFATORI,,S. LLC Report#: 217082416 Project ID: 7080391 Report Date: 08/29/2017 Laboratory Endorsement Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized agencies. The samples and their corresponding extracts wit be maintained for a period of 30 days unless otherwise arranged. Following this retention period the samples will be disposed in accordance with GCAL's Standard Operating Procedures. Common Abbreviations that may be Utilized in this Report ND Indicates the result was Not Detected at the specified reporting limit NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030 DO Indicates the result was Diluted Out illrl Indicates the result was subject to Matrix Interference TN T C Indicates the result was Too Numerous To Count SUBC Indicates the analysis was Sub -Contracted FLD Indicates the analysis was performed in the Field DL Detection Limit DL Diluted analysis — when appended to Client Sample ID LOD Limit of Detection LOQ Limit of Quantitation RE Re -analysis CF HPLC or GC Confirmation 00:01 Reported as a time equivalent to 12:00 AM Reporting Flags that may be Utilized in this Report J or I Indicates the result is between the MDL and LOQ J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria U Indicates the compound was analyzed for but not detected B or V Indicates the analyte was detected in the associated Method Blank Q Indicates a non -compliant QC Result (See Q Flag Application Report) Indicates a non -compliant or not applicable QC recovery or RPD — see narrative E The result is estimated because it exceeded the instrument calibration range E Metals - % diference for the serial dilution is > 10% P RPD between primary and confirmation result is greater than 40 Sample receipt at GCAL is documented through the attached chain of custody. In accordance with NELAC, this report shall be reproduced only in full and with the written permission of GCAL. The results contained within this report relate only to the samples reported. The documented results are presented within this report. This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited. I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee, as verified by the following signature. Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if applicable. i ( { t ` /////ire , Authorized Signature GCAL Report 217082416 Lab Report#: 217082416 Ponca of 11 I Page 9 of 24 r.: G 1 LVTICAL I&OoR:TO PIES, ILC Report#: 217082416 Project ID: 7080391 Report Date: 08/29/2017 Certifications Certification Certification Number DOD ELAP L14-243 Alabama 01955 Arkansas 12-060-0 Colorado 01955 Delaware 01955 Florida E87854 Georgia 01955 Hawaii 01955 Idaho 01955 Illinois 200048 Indiana 01955 Kansas E-10354 Kentucky 95 Louisiana 01955 Maryland 01955 Massachusetts 01955 Michigan 01955 Mississippi 01955 Missouri 01955 Montana N/A Nebraska 01955 New Mexico 01955 North Carolina 618 North Dakota R-195 Oklahoma 9403 South Carolina 73006001 South Dakota 01955 Tennessee 01955 Texas T104704178 Vermont 01955 Virginia 460215 USDA Soil Permit P330-10-00117 Lab Reportt: 217082416 Porno ^_ of 11 I Page 10 of 24 eO AfQRI_S. LLC Reperi#: 217082416 Project ID: 7080391 Case Narralve Client: Access Analytical Report: 217082416 Report Date: 08/29/2017 Gulf Coast Analytical Laboratories received and analyzed the sample(s) listed on the Report Sample Summary page of this report. Receipt of the sample(s) is documented by the attached chain of custody. This applies only to the sample(s) listed in this report. No sample integrity or quality control exceptions were identified unless noted below. o anon ales were found for the Analyzed sample(s). Lab Report#: 217082416 Pan. F of 11 Page 11 of 24 ANALVTICAL L•1130!“101:111S. LLG GCAL ID Client ID 21708241601 Third Creek Sludge Report#: 217082416 Project ID: 7080391 Sampe Summary Ililatrin Collect Date/Time Solid 08/22/2017 11:55 Report Date: 08/29/2017 Receive Date/Time 08/24/2017 11:20 Lab Report#: 217082416 PR,-ir 6 nf 11 Page 12 of 24 I 01. ANALY iltAL 1 ARONATO RISS. I.LC Report#: 217082416 Project ID: 7080391 Report Date: 08/29/2017 Summary of Compounds Detected No analytes were detected for analyses performed by GCAL. Lab Report#: 217082416 Panp 7 nf 11 I Page 13 of 24 LVTILAL LSB•-i:I STokc_5 LLC Report#: 217082416- Project ID: 7080391 Report Date: 08/29/2017 Sample Results Third Creek Sludge Collect Date 08/22/2017 11:55 Receive Date 08/24/2017 11:20 GCAL ID 21708241601 Matrix Solid EPA 9012B Prep Date 08/24/2017 12:00 Prep Batch 616831 Prep Method EPA 7.3.3.2 Dilution Analysis Date 1 08/25/2017 15:46 By Analytical Batch DMT 616946 CAS;r' 57-12-5R EPA 9034 Parameter Reactivity. Cyanide Result DL 250U 250 LOQ 250 Units mg/kg Prep Date 08/24/2017 12:00 Prep Batch 616832 Prep Method EPA 7.3.4.2 Dilution Analysis Date 1 08/25/2017 14:00 By Analytical Batch MOS 616937 CAS# 18496-25-8R Parameter Reactivity Sulfide Result 250U DL 250 LOQ 250 Units mg/kg Lab Report#: 217082416 Pane R of 11 I Page 14 of 24 . I ALVTICSL 1.I!°F41°^nlc.5. LtC Report#: 217082416 Project ID: 7080391 Report Date: 08/29/2017 General Chemistry QC Summary Analytical Batch Client ID 616937 GCAL ID Prep Batch Sample Type 616832 Prep Date Prep Method Analysis Date EPA 7.3.4.2 Matrix MB616832 1714951 MB 08/24/2017 10:00 08/25/2017 14:00 Solid LCS616832 1714952 LCS 08/24/2017 10:00 08/25/2017 14:00 Solid EPA 9034 Units Result I mg/kg DL Spike Added Result %R Control Limits%R Reactivity Sulfide 118496-25-8R 250U 250 1000 1074 107 47 - 135 Analytical Batch Client ID 616937 GCALID Prep Batch Sample Type 616832 Prep Date Prep Method Analysis Date EPA 7.3.4.2 Matrix ATF 17-003; ATF Leaded .. 21708222001 SAMPLE 08/24/2017 10:00 08/25/2017 14:00 Solid 1714285DUP 1714953 DUP 08/24/2017 10:00 08/25/2017 14:00 Solid EPA 9034 Units Result I mg/kg DL Result RPD RPD Limit Reactivity Sulfide 118496-25-8R 0 250 0 0 25 Analytical Batch Client ID 616946 GOAL ID Prep Batch Sample Type 616831 Prep Date Prep Method Analysis Date EPA 7.3.3.2 Matrix MB616831 1714948 MB 08/24/2017 10:00 08/25/2017 15:11 Solid LCS616831 1714949 LCS 08/24/2017 10:00 08/25/2017 17:36 Solid EPA 9012B Units Result I mg/kg DL Spike Added Result %R Control Limits%R Reactivity Cyanide I 57-12-5R 250U 250 250 3.2 1 1 - 25 Analytical Batch Client ID 616946 GCALID Prep Batch Sample Type 616831 Prep Date Prep Method Analysis Date EPA 7.3.3.2 Matrix ATF 17-003; ATF Leaded .. 21708222001 SAMPLE 08/24/2017 10:00 08/25/2017 15:16 Solid 1714285DUP 1714950 DUP 08/24/2017 10:00 08/25/2017 15:18 Solid EPA 9012B Units Result mg/kg DL Result RPD RPD Limit Reactivity Cyanide I 57-12-5R 0.0 250 0.0 0 20 Lab Report#: 217082416 IPana p of 11 Page 15 of 24 Ciis t uD 565 Access Analytical tr . ;. �• i - 1. ' ,-t l SDG ` l a I Fun -Service Analytical a l -IC pjii Environmental Solutions SUBCONTRACT ORDER Prism Laboratories, Inc. 7080391 1 /Uc5Z'16 C AE :Iy (1 `� Certification: LAC_ NC SC IA NIA USACE_ Other ____ SENDING LABORATORV: _ RECEIVING LABORATORY: Prism Lab P. O. Box Charlotte; Phone: 800-529-6364 Fax: 704-'i75-0409 Project Manager; ,raforias, Inc. F40543 rc 23224-0543 Robbi A. Jones Gulf Coast Ana .1ylical Labs, Inc. 10781 Coursey Blvd Baton Rouge, LA 70316 Phone :(225) 769-4900 Fax: (225) 767-57 i 7 Analysis Due Expires Laboratory ID Comments Sample HDi 7030391-0H. Solid S::mpled:C31Z2/I7 it:5� . �.. . c{ i )' Reactivity, Reactivity, 'onlahters S Su1fidc (Sub) Cyanide (Sub) y.+plied: 08/29/17 11:55 09/05/17 11:55 Li, 5-C 3 - CM } ev 524 Gar 0 , 1 Y 0 -_ �. � _ ) o -,1J-1-i. l L 3-a3-i7 case B5 .� Date Received By t f Date Released B • Date Retj\ (1133x, ;a i ,; Date Release B ✓ Date Received By Date Dale ecerved by Faze l of 1 Page 16 of 24 bZ Jo Li, abed SAMPLE RECEIVING CHECKLIST 1 1 III LL 2 1 7° 8 2 4 1 6 SAMPLE DF UVERY GROUP 217032416 CHECKLIST YES NO Client PP`Vi AEC 4565 -Access Analytical Transport Method I LupC Samples received with proper thermal preservation? err' Radioactivity is <1600 cpm? If no, record cpm value in notes section. Pi . Profile Number 80251 Received By Savage, Tiffany R COC relinquished and complete (including samplelDs, collect times, and sampler)? U _.-. .. ------- ..... —._... _. _... - __..._...... . All containers received in good condition and within hold time? All sample labels and containers received match the chain of custody? Mil[ _.___ _...._ . Preservative added to any containers? [ ae If received, was headspace for VOC water containers < 6mm? v [ Samples collected in containers provided by GOAL? Line ltem(s) 4 - Solid Receive Date(s) 08/24/17 COOLERS D9SCRIEPANCIES LAB PR IESERVATIONS Airbill Thermometer ID C-29 Temp °C None l .bne 7700 9612 2948 4.5 NOTES Revision 1.6 Page 1of1 Lab Report t: 217082416 Page 11 of 11 • XESS A N A :NC - ANALYTICAL REPORT CLIENT Prism Laboratories PO Box 240543 Charlotte NC 282240543 ATTENTION Robbi A. Jones PROJECT ID 7080391 LABORATORY REPORT `UMBER 1708N87 DATE September 08, 2017 Primary Data Review By Chris Pafford Project Manager, AES PLEASE NOTE: Secondary Data Review By Ashley Amick Project Manager, Access Analytical aamick@axs-inc.com Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc), 3080 Presidential Drive, Atlanta, GA 30340. AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582, NE LAP certified laboratory # E87582 ALMA-LAP,LLC Laboratory ID:100671 for Industrial Hygiene samples (Organics, Metals, PCM Asbestos, Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal) Direct Examination. Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243 E=: Page Page 18 of 24 Full -Service Analytical & Environmental Solutions 6S air 03iffi i 0t` Si SUBCONTRACT ORDER Prism Laboratories, Inc. 7080391 Orl Certification: DIBLACUSACB NC t7 SC_ Other N/A SENDING LABORATORY: Prism Laboratories, Inc. P.O. Box 240543 Charlotte, NC 28224-0543 Phone: 8 00-529-63 64 Fax: 704-525-0409 Project Manager: RobbiA. Jones Analysis Due Expires Sample ID: 7080391-01 Said Sampled:08./22/1711:55 Herbicides TCLP (Sub) Containers Supplied: 08/29/17 11:55 RECEIVING LABORATORY: Analytical Enviromnental Services, Inc. 3080 Presidential Parkway Atlanta, GA 30340 Phone :(770) 457-8177 Fax: NA Releed By rfeCA C� Released By c may-/7 Date Date Released By Date Released By Date Date Advs. g(a4n- i ES Date Page Page 19 of 24 Full -Service Analytical Environmental Solutions IABORA1 RIEa ING SENDING LABORATORY: Prism Laboratories, Inc. P. 0. Box 240543 Charlotte, NC 28224-0543 Phone: 800-529-6364 Fax: 704-525-0409 Project Manager: RobbiA. Jones Analysis Due Sample ID:7080391-01 Solid Herbicides TCLP (Sub) Containers Supplred- ilD S'd{{ o k6s Dtl rg)Z .11:- .5. M - SUBCON d RACT ORDER Prism Laboratories, Inc. 708 392 Expires SamplFd:08/22/17 I1:55 08/29/17 11:55 Certification_ I1BLAC USACE NC '-f SC Other N/A RECEIVING LABORATORY: Analytical Environmental Services, Inc. 3080 Presidential Parkway Atlanta, GA 30340 Phone :(770) 457-8177 Fax: NA Laboratory ID Comments Rele ' ' By / Date Released By Date Released By Date Released By Dare Received B}l PLA Received B 7 6 (JI /I I A,fi `l'S/ 1 (1 fc0 l r Date gMg- /cop Received 111W Received By Date Date Date Page I of I Page Page 20 of 24 Analytical Environmentai Services, Inc Date: 8-Sep-17 Client: Prism Laboratories Project: 7080391 Lab ID: 1708N87 Case Narrative Sample Receiving Nonconformance: Insufficient sample was received 08-24-17 for TCLP SW1311/8151A. Additional sample was received 08-31-17(0/10.30. Page Page 21 of 24 Analytical Environmental Services, }Inc Date: 8-Sep-17 Client: Lab Order Project Name: Lab ID: Prism Laboratories 1708N87 7080391 1708N87-001A Client Sample ID: Tag Number: Collection Date: Matrix: Third Creek Sludge 7080391-01 8/22/2017 11:55:00 AM Solid Analyses Result Qual MDL Reporting Limit Units BatchED DF Date Analyzed Analyst HERBICIDES, TCLP SW131I/8151A 2,4,5-TP (Silvex) 2,4-D Surr: DCAA BRL BRL 79 0.030 0.051 0 0.20 0.20 50.1-132 (SW3SIOC) tng/1. 247636 tng/L 247636 %REC 247636 09/07/2017 13:54 09/07/2017 13:54 09/07/2017 13:54 EI EI EI Qualifiers: Value exceeds maximum contaminant level BRL Not Detected at MDL H Holding times for preparation or analysis exceeded N A.ialyte not NELAC certified B Analyte detected in the associated method blank E Estimated value above gtantitation range S Spike Recovery outside limits due to matrix > Greater than Result value J Estimated value detected below Reporting Limit < Less than Result value Page I Page 22 of 24 -frZ to EZ e6ed AES ANALYTICAL it,i n.VatzoNMENTAL SEIWICES,1NC. 1. Client Name: Access Aft afivUcii,, fnc. SAMPLE/COOLER RECEIPT CHECKLIST 2. Carrier: FedEx°❑ UPS ❑ USPS❑ Client ❑ Courier❑ Othei 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. Yes No N/A AES Work Order Number: 1703ICI87 Shipping container/cooler received in good condition? (o () damaged • leaking • other. Custody seals present on shipping container? (' i6' Custody seals intact on shipping container? T) o Temperature blanks present? 0 (Y' 0 Cooler temperature(s) within limits of 0-6°C? [See item 13 and 14 for temperature recordings.] �o 0 ' -' ") / -' Cooling Initiated for recently collected samples / ice present • Chain of Custody (COC) present? io Chain of Custody signed, dated, and timed when relinquished and received? fO V�y� Sampler name and/or signature on COC? o I \.J� / Were all samples received within holding time? is.,,) ) TAT marked on the COC? () o �(;`. If no TAT indicated, proceeded with standard TAT per Terms & Conditions. El 13. Cooler 1 Temperature 1.3 14. Cooler 5 Temperature 15. Comments: 16. 17. 18. 19. 20. 21. 22, 23. 24. 25. 26. °C Cooler 2 Temperature °C Cooler 6 Temperature °C Cooler 3 Temperature °C Cooler 7 Temperature °C Cooler 4 Temperature °C Cooler 8 Temperature oc oC Yes No N/A I certify that I have completed sections 1-15 (dated initials). TD 8/24/17 Were sample containers intact upon receipt? 1. 0(' . Custody seals present on sample containers? l)° Custody seals intact on sample containers? (-'. 0 ;o - Do sample container labels match the COC? 00 incomplete info • illegibleNI no label • other • Are analyses.requested indicated on the COC? () Were all of the samples listed on the COC received? (o. 0 0 samples received but not listed on COC • samples listed on COC not received ■ Was the sample collection date/time noted? 'o Did we receive sufficient sample volume for indicated analyses? io. � Were samples received in appropriate containers? (o ( 0 Were VOA samples received without headspace (< 1/4" bubble)? 0. Were trip blanks submitted? ` J o. listed on COC il not listed on COC • 27, Comments: 28. 29. 30. This section only applies to samples where pH can be checked at Sample Receipt. Yes No N/A Details I certifythat I have completed sections 16-27 (dated initials). MJ 8/24/17 Have containers needing chemical preservation been checked? '' I 0 Containers meet preservation guidelines? I Was pH adjusted at Sample Receipt? I 0 0-1 e--- Note: Certain analyses require chemical preservation but must be checked in the laboratory and not upon Sample Receipt such as Coliforms, VOCs and OII & GreasefrPH. I certify that I have completed sections 28-30 (dated initials). Checklist 6.9.17 Rev 2 MJ 8/24/17 Page 6 of 7 reaa 173 Jo 17z abed Analytical Environmental Services, Inc Client: Project Name: Worlcortler: Prism Laboratories 7080391 1708N87 Date: 8-Sep-17 ANALYTICAL QC SUMMARY REPORT atchID: 247636 Sample ID: MB-247636 Client ID: SampleType: MBLK Analyte TestCode: HERBICIDES, TCLP SW1311/8151A Units: mg/L BatchID: 247636 Prep Date: 09/05/2017 Run No: 351385 Analysis Date: 09/06/2017 Seq No: 7728375 Result RPT Limit SPK value SPK Ref Val %REC Low Limit high Limit RPD Ref Val %RPD RPD Limit Qual 2,4,5-TP (Silvex) 2,4-D Surr: DCAA BRL BRL 0.3448 0.20 0.20 0 0.5000 69.0 50.1 132 Sample ID: LCS-247636 Client ID: SampleType: LCS Analyte TestCode: HERBICIDES, TCLP SW1311/8151A Units: nig/L BatcllID: 247636 Prep Date: 09/05/2017 Run No: 351385 Analysis Date: 09/06/2017 Seq No: 7728376 Result RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit Qual 2,4,5-TP (Silvex) 2,4-D Surr: DCAA 0.2936 0.2616 0.3058 0.20 0.20 0 0.5000 0.5000 0,5000 58.7 52.3 61.2 50.7 50.1 50.1 117 119 132 Sample ID: 1708S44-001BMS Client ID: SampleType: MS Analyte TestCode: HERBICIDES, TCLP SW1311/8151A Units: ing/L BatchlD: 247636 Prep Date: 09/05/2017 Run No: 351385 Analysis Date: 09/06/2017 Seq No: 7728379 Result RPT Limit SPIC value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit Qual 2,4,5-TP (Silvex) 2,4-D Surr: DCAA 0.03509 0.2194 0.3162 0.20 0.20 0 0.5000 0.5000 0.5000 7.02 43.9 63.2 46.3 43.3 50.1 126 132 132 JS Qualifiers: > Greater than Result value BRL Below reporting limit J Estimated value detected below Reporting Limit Rpt Lim Reporting Limit < Less than Result value E Estimated (value above quantization range) N Analyte not NELAC certified S Spike Recovery outside limits due to matrix B Analyte detected in the associated method blank H Holding times for preparation or analysis exceeded R RPD outside limits due to matrix Page 7of7 ,111111. Legend Date: May 10, 2018 Dwg: 2018SWR003 INFLUENT FINE - SCREENS 48- AEROBIC DIGESTER #1 0 0 0 BELT FILTER PRESS FEED PUMP STATION HAUL - SCREENINGS INFLUENT PUMP STATION 24- a n _ FLOW METER GRIT VAULT CHAMBER SPUTTER BOX V HAUL_ GRIT 9S BELT FILTER I` PRESSES HAUL SLUDGE CAKE TO 4TH CREEK WWTP McGill ASSOCIATES ENGINEERING•PLANNING•PINANCE I2858STAF8F,LWHNW IIIIXWLY,NC28601 88R21)UbiV4 FIRMIIOPL®IC915, AEROBIC DIGESTER #2 (0 0 0 0 0 0 TO PLANT SANITARY SEWER SYSTEM 24' ANOXIC BASINS BIGI ANAERO BASINS OXIDATION DITCHES O 38 WAS UNE %"7"//7,3" AS UNE FLOW METER VAULT WAS VALVE & METER RAS/WAS PUMP STATION .0 FUTURE POTENTIAL PROCESSES I I r - i i. I- i I H - I I i Ir J SPUTTER BOX CLARIFIERS SPUTTER ae' BOX x- CHLORINE CONTACT 1 r- I I FUTURE I I --1 POTENTIAL f --1 PROCESS I L J NON -POTABLE WATER POST AERATION FLOW METER FIGURE - PROCESS FLOW DIAGRAM THIRD CREEK WASTEWATER TREATMENT PLANT EXPANSION CITY OF STATESVILLE IREDELL COUNTY, NORTH CAROLINA SPILL f! ESPONSE PLAN PROJECT: City of Statesville Land Application Permit W00014543 IN THE UNLIKELY EVENT OF A SPILL, THE FOLLOWING ACTIONS SHALL BE TAKEN IMMEDIATELY: 1. MANAGEMENT OF SPILL CLEAN-UP ACTIVITIES: The Fourth Creek WWTP Supervisor shall take immediate charge and initiate clean-up activities. The City of Statesville labor and equipment is to be: utilized. In the event additional labor and.equipment is required, assistance may be requested from the NC Department of Transportation and other private contractors as necessary. 2. HALT THE SOURCE OF THE SPILL: Such as a ruptured container or damaged transport unit. 3. 'CONTAIN THE SPILL: Form a barrier. Sufficient quantities of straw shall be used for such purposes. Earthen barriers may be constructed to augment the straw bale containment area of the spill. The Operations Manager or the person in charge on the spill site will advise the clean-up personnel where to get the straw, lime, and other items necessary to complete the clean-up operation, i:e., local farmers, farm supply centers, nurseries, etc. 4. CLEAN-UP: Employ front-end loaders, vacuum equipment, sludge application vehicles, and/or local septic tank service to remove as much of the spilled material as possible. Straw and/or sand should be scattered in the spill area to soak up the remaining material. The straw- and sand -soaked material will be collected and removed to a disposal area approved by representatives of the state regulatory agency. 5. FINAL CLEAN-UP: Employ rotary brush sweeper if needed, and apply lime to the spill area upon the approval of the clean-up efforts by the state regulatory representative. If the event occurs on private property, the clean-up will be completed to the satisfaction of the property owner and state regulatory representatives. The ultimate goal will be to restore the spill area to its original condition if possible. 6. NOTIFICATION: As soon as possible after the spill occurs, the City of Statesville Operations staff will notify the Fourth Creek WWTP Supervisor, and they will then be responsible for notifying other key City of Statesville personnel. 7.. REPORTING: The City of Statesville personnel will notify the Mooresville Regional office (704) 235-2198 as soon as possible, but not more than 24 hours after, or on the next working day following the occurrence. The Fourth Creek WWTP Supervisor shall provide a written report within 48 hours of the spill to the Technical Services Director. The report shall list all relative information and actions taken. The City of Statesville personnel will file a written report to the Mooresville Regional cake of the NCDENR within 5 days of the occurrence. For after-hours reporting the Division's emergency number shall°be=called to report all incidences (800-662-7956 or 800-858-0368 or 919-733-3300) • 11Pa.ge 5/2/2018 OPERATIONS AND MAINTENANCE PLAN The City of Statesville Land Application Permit WQ0014543 Inspection Plan Inspections for the Land Application site will be conducted on an as needed basis. The inspection frequency is based on the time frame that it is going to take to complete the project and the amount of dry tons to be processed from this facility. The inspections will consist of inspecting the Bio-Solids loading area. These inspections will consist of: 1. Verifying that all of the equipment is working properly. 2. Verify that all containment walls and curbing are working properly. 3. Insure that all manned equipment has a copy of the spill control plan, the permit, and the operations and maintenance plan. 4. Verifying that the, correct number samples of the Class B product have been taken and that it meets the criteria for the . Land Application Permit. 5. The records will be kept in the project files in the respective office for the project. 6. The Permittee or Inspector shall report by telephone to the Mooresville Regional Office at 704-235-2198 as soon as possible but no later than 24 hours after or the next working day following the occurrence or the first knowledge of the occurrence of the following. • Any occurrence with the distribution program resulting in the land application of significant amounts of material that is abnormal in quantity or characteristics. • Any time that self -monitoring indicates that the facility has gone out of compliance with the permit. • Any process failure that: results in the system not adequately treating the residuals. • Any spill or discharge from a vehicle or piping system during residuals transportation. • •Any release that requires immediate reporting outside of normal business hours shall be called in to DENR at 1800- 662-7956, 1-800-858-0368, or 1-919-733-3300. These numbers are to be called in the event of a release to surface waters, imminent failure of a storage system when the event occurs outside of normal business hours. • Within 5 days of the first notice of on occurrence a written response in the form of a letter shall be sent to DENR outlining the actions taken or purposed actions taken to ensure that the problem does not recur. Persons responsible for inspections on this project are as follows: Andy Smith, 4th Creek. WWTP ORC or his designee Andy Smith is the designated WWTP ORC for this project and his designees are the backup ORC's for this project. 21Pa.ge 5/2/2018 OPERATIONS AND MAINTENANCE PLAN The City of Statesville Land Application Permit WQ0014543 Sampling Plan Sampling for this project consists of sampling the residuals during the time that land application is occurring. This will result in one round of sampling to occurbefore land application commences in order to insure that the residuals are suitable for land application. Based on the dry tonnage of this plant this will be six samples for all parameters per year. The residuals shall be sampled annually for the following: (Regulatory level in milligrams per liter in parentheses.) Arsenic (5.0) 1, 4-Dichlorobenzene (7.5) Nitrobenzene (2.0) Barium (100.0) 1, 2-Dichloroethane (0.5) Pentachlorophenol (100.0) Benzene: (0.5) Cadmium (1.0) Carbon tetrachloride (0.5).Chlordane (0.03) Chlorobenzene (100.0) Chloroform (6.0) Chromium (5.0) M-Cresol (200.0) o- Cresol (200.0) p- Cresol (200.0) Cresol (200.0) 2,4-D (10.0) 1, 1-Diichloroethylene (0.7) 2, 4-Dinitrotoluene (0.13) Endrin (0.02) Hexachlorobenzene (0.13 Heptachlor (and its hydroxide) (0.008) Hexachloro-1,3-butadiene (0.5) Hexachlorethane (3.0) Lead (5.0) Lindane (0.4) Mercury (0.2) Methoxychlor (10.0) Methyl ethyl ketone (200.0) Pyridine (5.0).. Selenium (1.0) Silver (5.0) Tetrachloroethylene (0.7) Toxaphene (0.5) Trichloroethylene (0.5) 2,4,5-Trichlorophenol (400.0) 2,4,6-Trichlorophenol (2.0) 2,4,5 TP ( Silvex) (1.0) Vinyl Chloride (0.2) The residuals will also be sampled based on the chart below for the following constituents Dry Tons Generated (short tons per year) Monitoring Frequency (Established in 40 CFR 503 and 15A NCAC 02T.1111) <319 1 time per year =>319-<1,650 1 per Quarter (4 times per year) =>1,650-<16,500 1 every 60 days (6 times per year) =>16,500 1 every month (12 times per year) Aluminum Ammonia -Nitrogen Arsenic Cadmium Calcium Copper Lead Sodium Adsorption Ratio (SAR) Magnesium Mercury Molybdenum Nickel Nitrate -Nitrite Nitrogen Phosphorous Potassium pH Plant Available Nitrogen (calculation) Selenium Sodium % Total Solids Total kjeldahl Nitrogen Zinc In order to meet pathogen and vector requirements the material will go through an aerobically digested treatment process. The residuals will meet pathogen and vector requirements through pH, time and temperature requirements. The samples will be pulled from the storage pads that are currently holding the Sta-Lime product. The samples that will be pulled are a TCLP and nutrient and metals sample to prove that the material is suitable for distribution. The nutrient and metal and TCLP sample will be collected randomly and consist of individual samples mixed together in order to get the composite sample for these parameters. This material is very consistent based on the fact that these residuals are thoroughly digested and mixed before processing and should not experience any seasonal fluctuations in the residuals. The following people are responsible for sampling: Andy Smith, Plant Manager or his designee. 31Page 5/2/2018 OPERATIONS AND MAINTENANCE PLAN The City of Statesville Land Application Permit WQ0014543 Operational Functions The operation function of this project is going to involve loading dewatered belt press sludge. The dewatered belt press sludge will be loaded into the trucks that are suitable to transport and spread this product without spillage or leakage. during transport. The dewatered belt press sludge will be spread at agronomic rates that are determined by the soil samples from the fields that the City of Statesville staff has collected. SAFETY MEASURES The City of Statesville believes in operating in a safety conscious manner and is has all employees participate in monthly safety courses that are designed to help its employees recognize safety issues and take steps to prevent accidents from occurring. In addition all City of Statesville, Water Resources employees have the authority to stop operations if they think any aspect of the operation is going to cause environmental or personal harm. Maintenance Schedule The City of Statesville will follow the maintenance schedule as recommended by the processing equipment manufacturer. 5/2/2018