HomeMy WebLinkAboutWI0400091_Monitoring (Report)_20090420KL EINFEL DER
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o°� Quarterly HiSQC Monitoring Report
Gilbarco
7304 West Friendly Avenue
Greensboro, North Carolina
Kleinfelder Project No. 97746
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April 17, 2009
Mr. Qu Qi
Aquifer Protection Section — UIC Staff
DENR — Division of Water Quality
1636 Mail Service Center
Raleigh, North Carolina 27699-1636
Reference: Quarterly HiSQC Monitoring Report
Gilbarco
7300 West Friendly Avenue
Greensboro, North Carolina
Kleinfelder Project No. 97746
Dear Mr. Qi:
Kleinfelder is pleased to provide our quarterly monitoring report for the Underground
Injection Control {UIC} Permit for treatment of groundwater with the HiSOC system at
the referenced site. This report summarizes our field activities, observations, and
includes the analytical results of the groundwater samples. Should you have any
questions or require additional information, please d❑ not hesitate to contact Chris Hay
at your convenience.
Very truly yours,
Christopher W. ay, E.I.
Environmental Group Manager
Gail G. Licayan, P.E.
Project Professional
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313 Gallimore Dairy Road, Greensboro, NC 27409 p 1336.668.0093 f 1 336.668.3868
GILBARCO
Greensboro, North Carolina
Groundwater Incident Nos. 12960 And 15123
SITE INFORMATION
Address:
Contact:
Telephone:
Latitude and Longitude
Risk Classification:
Lana Use Category -
LAND OWNERSHIP
Name:
Address:
Telephone:
Attention:
RELEASE INFORMATION
April 17, 2009
7300 West Friendly Avenue
Greensboro, North Carolina
Ms. Beth Money
336.547.5130
36.0901 °N, 79.9282 °W
Low
Commercial
Gilbarcv
7300 West Friendly Avenue
Greensboro, North Carolina 27420
336.547.5130
Ms. Beth Money
Cause of Release: Release from a 1,000-gallon diesel UST and four
550-gallon gasoline USTs was discovered in
November and December 1994. The quantity
released is unknown.
ENVIRONMENTAL CONSULTANT
Name: Kleinfelder
Address: Post Office Box 18846
Greensboro, North Carolina 27419-8846
Telephone: 336.668.0093
Attention: Mr. Christopher W. Hay
Seal and Si]6►fiertifying Professional Engineer
�' 'E Si ���f����
I, Gail cite-Q , a s ivnai Engineer for Kleinfelder do certify that the information
contained ir)i%m*Drt�' c&rect and accurate to the best of my knowledge.
Gail G ..p?�'r 7��1
Registered ioplira Engineer No. 031532
977461 GS009R022 Page l RELOVED DENR i DWO April 17, 2009
Copyright 2009 Kleinfelder AQIIIFFP PRnTFrTIN4 qR-TION
APR 2 0 ?i11r'9
TABLE OF CONTENTS
1.0 INTRODUCTION................................................................................. ....... ...........1
2.0 GROUNDWATER MONITORING ACTIVITIES ............... ...................... I ..... ........ I ... 11
3.0 GROUNDWATER ANALYTICAL RESULTS............................................................2
4.0 HiSOC INSTALLATION AND MONITORING...........................................................3
5.0 CONCLUSIONS AND RECOMMENDATIONS.........................................................5
TABLES
1 Groundwater Elevation Data
2 Aquifer Characteristics Field Analysis Summary
3 Summary of Groundwater Sample Results
4 Historical Summary of Groundwater Sample Results
5 Estimated Dissolved Hydrogen Concentrations at Injection Wells
6 Estimated Hydrogen Consumption
FIGURES
1 Site Location Map
2 Site Plan
3 Groundwater Potentiometric Surface Map
4 Total VOCs Concentrations
5 Total Chlorinated Hydrocarbons
APPENDICES
A Laboratory Reports and Chain -of -Custody Documents
B Total VOC Graphs
977461 GS009R022 Page ii April 17, 2009
Copyright 2009 Kieinfelder
1.0 INTRODUCTION
The subject site is located at 7300 West Friendly Avenue in Greensboro, Guilford
County; North Carolina (Figure 1). There are currently two open groundwater incidents
(Incident Nos. 12960 and 15123). The incidents have a commingled plume and are
being treated with the same corrective action plan. A pump and treat system is
operating at the site. The system consists of four recovery wells, an oil -water
separator, and an air stripping system.
In January 2008, Kleinfelder submitted a CAP Addendum recommending the use of
HiSOC and iSOC technology to degrade the chlorinated and petroleum hydrocarbons in
groundwater at the site. This technology will work in concert with the existing
groundwater recovery system and supplement the ability of the system to contain the
contaminant plume within the property limits and reduce contaminant levels. The
KSOC system was installed in June of 2008 and began operating on June 13, 2008.
The baseline sampling event was conducted on June 5, 2008. The purpose of this
report is to summarize the quarterly monitoring of the HiSOC system performed on
March 5 and 27, 2009.
2.0 GROUNDWATER MONITORING ACTIVITIES
Static water levels were measured in the existing monitoring wells on -site on March 5,
2009. Groundwater samples were collected from ten of the monitoring wells (MW-7,
MW-11. MW-13, MW-13D, MW-14, MW-23D, MW-24, MW-25, MW-42. and MW-45)
and analyzed for VOCs by EPA Methods 601 and 602, isopropyl ether, methyl tert-butyl
ether, ethylene dibromide, and xylenes. In response to a letter from NCDENR
requesting that MW-14D and MW-43D be included in future monitoring events,
groundwater samples were collected from these wells on March 27, 2009. Field
parameters including oxidation-reduction potential (ORP), pH, conductivity, dissolved
oxygen, and temperature of representative groundwater samples were also recorded
from each monitoring well sampled. Groundwater elevations in the existing monitoring
wells were used to determine the groundwater flow direction, average hydraulic
gradient, and plume orientation. Table 1 provides a summary of monitoring well
construction details and the groundwater elevations measured on March 5, 2009. The
97746 1 GS009R022 Page 1 April 17, 2009
Copyright 2009 Kleinfelder
monitoring well locations are shown on Figure 2. The static water levels measured on
March 5, 2009 between monitoring wells MW-32 and MW-45 indicate a horizontal
groundwater flow gradient of 0.04 feet per foot to the northwest. A groundwater flow
map of the shallow aquifer based on the March 5, 2009 groundwater elevations are
shown on Figure 3. Free product was not observed in any of the monitoring wells
during the sampling event.
Based on data provided in the October 1995 Corrective Action Plan, the surficial aquifer
has an average hydraulic conductivity of 0.09 feet per day. The average groundwater
velocity is estimated to be 0.01 feet per day (4 feet per year), based on the average
groundwater gradient from the March 5, 2009. water level measurements and an
estimated effective porosity of thirty percent.
Groundwater samples were collected from monitoring wells MW-7, MW-11, MW-13,
MW-13D, MW-14, MW-14D, MW-23D, MW-24, MW-25, MW-42, MW-43D, and MW-45
using disposable polyethylene bailers. The wells were purged of three well volumes of
water or until they were bailed dry. Groundwater purged from the monitoring wells was
disposed of in the on -site groundwater recovery system. Groundwater samples were
collected and placed in laboratory prepared containers. The samples were maintained
on ice until delivered to Pace Analytical Laboratories in Huntersville, North Carolina.
3.0 GROUNDWATER ANALYTICAL RESULTS
The groundwater field analysis generally indicates that the subsurface environment is
within acceptable limits for biodegradation to occur. The field measurements recorded
on March 5 and 27, 2009 are summarized in Table 2, which includes the preferred
conditions for natural biodegradation of chlorinated compounds within the groundwater
plume. Conductivity is recorded for quality control and sampling consistency.
Volatile organic compounds were detected at levels above the respective North
Carolina groundwater quality standards established in 15 NCAC, Subchapter 2L (2L
Standards) in each of the twelve monitoring wells sampled. The analytical results are
summarized in Table 3 and a historical summary of groundwater sampling results is
presented in Table 4. Chain -of -custody documents were maintained throughout the
97746 J GS009R022 Page 2 April 17, 2009
Copyright 2009 Kleinfeider
collection and transportation process and are included in Appendix A with the laboratory
reports.
Historical total volatile organic compound concentrations for each monitoring well
sampled are shown in individual graphs included in Appendix B. The individual graphs
of the total VCC concentration for each monitoring well indicate MW-7, MW-11, MW-
13D, MW-14, MW-14D, MW-24, MW-42, and MW-43❑ generally have trends of
decreasing contaminant levels. The graph of contaminant concentrations in MW-45
indicates the total VOCs level remains fairly consistent. Monitoring wells MW-13 and
MW-23D graphs show a recent increase; however, they have tetrachloroethene
concentrations below the laboratory detection limits. The increase in contaminant
levels in these weals is caused by increases in cis- 1,2-dichloroethene and vinyl chloride
which are degradation components of tetrachloroethene. The trend of rising
contaminant concentrations are of concern in monitoring well MW-25. Total VOCs
concentrations detected during the March 2009 sampling event are shown on Figure 4.
The current hydrogen injection phase of the corrective action plan targets the reduction
of chlorinated hydrocarbon contaminant levels in the groundwater. The oxygen
injection phase will target the reduction of petroleum hydrocarbons. The volatile
organic compounds targeted during the hydrogen and oxygen injection phases of the
corrective action plan are separated in Table 4 by a double line. Total chlorinated
hydrocarbons concentrations detected during the March 2009 sampling event are
shown on Figure 5. Historical chlorinated hydrocarbon contaminant levels generally
follow the decreasing trend of total VOCs in MW-7, MW-11, MW-13D, MW-14, MW-
14D, MW-24, MW-42, and MW-43D; consistent levels in MW-13, MW-23D, MW-45;
and the rising trend in MW-25.
4.0 HiSGC INSTALLATION AND MONITORING
Kleinfelder applied for a permit from the Underground Injection Control (UIC) Program
for the installation of a hydrogen and oxygen delivery system for remediation of
contaminants in groundwater at the site. A permit dated March 20, 2008 was issued for
the site (Injection Well Permit W10400091). The permit is effective through April 30,
2010.
97746 I GS009R022 Page 3 April 17, 2009
Copyright 2009 Kleinfelder
Installation of the injection equipment was initiated on April 9 through April 11, 2008.
The existing protective casings were removed from monitoring wells MW-7, MW-10,
MW-23D, MW-29, and MW-34. Ten -inch diameter PVC casings were installed to a
depth of five feet below ground surface adjacent to the monitoring well locations to hold
the hydrogen cylinders. Six to ten inches of gravel was placed in the bottom of each
casing. Excavations were completed for installation of twenty four -inch square, steel
well vaults and the vaults were set in concrete flush with the ground surface. Protective
vaults were also installed adjacent to the existing above grade protective covers for
monitoring wells MW-14D. MW-15, MW-16, MW-24, and MW-43D. The 15-inch by 24-
inch PVC protective vaults were installed over the cylinder casings. Vents were
installed in the protective vaults to allow hydrogen to be released in the case of a leak
from the delivery system.
The HiSOC equipment from InVentures was installed at the site in ten existing
monitoring wells (MW-7, MW-10, MW-14D, MW-15. MW-16, MW-23D, MW-24, MW-
29, MW-34, and MW-431D) on June 13, 2008. Within each injection well is a HiSOC
unit and filter. Hydrogen is supplied from a compressed gas cylinder with a regulator
and gauge connected to the HiSOC unit by Parflex tubing and a support cable. Four -
foot grounding rods were installed and connected to the regulator assembly of the gas
cylinders. The HISOC installation locations are shown on the figures in orange.
In anaerobic bioremediation applications. the HiSOC supersaturates the treatment well
with dissolved hydrogen, typically at a concentration of 1 to 4 parts per million (ppm)
depending on the immersion depth of the HiSOC unit in groundwater. The dissolved
hydrogen concentration achieved in the injection well depends on the height of the
water column in the well. Each atmosphere of pressure allows for a maximum of
approximately 1.6 ppm of dissolved hydrogen. Table 5 estimates the dissolved
hydrogen concentrations in each of the injection wells. These concentrations are
estimated based on the approximate pressure at the installation depth of the HiSOC
based on the depth of the water column in the injection wells. The calculation is made
with the assumption that 1.6 ppm of hydrogen is dissolved in the groundwater per
atmosphere of pressure.
Hydrogen
is infused from
the HiSOC into the treatment
well at a typical rate of 28
standard
cubic centimeters
per minute or approximately
1.4 cubic feet per day. The
hydrogen
consumption in
each of the injection wells
is tracked to estimate the
97746 1 GS009R022 Page 4 April 17. 2009
copyright 2009 Kleinfelder
remaining service life of the hydrogen cylinders. Table 6 shows the recorded hydrogen
cylinder pressures and estimates a date for each injection well that the cylinder should
be replaced. It is anticipated that the hydrogen cylinders will be replaced prior to the
next quarterly monitoring event scheduled for June 2009,
The HiSOC produces a convection current in the well with a designed release bubble
from the top of the HiSCC to distribute dissolved hydrogen rich water throughout the
screened interval. A curtain of hydrogen rich water disperses around the well into the
adjacent groundwater forming a treatment zone allowing enhanced bioremediation to
degrade the target contaminants.
41IMI61DON RDS]Z&V_'L'18JM:me]&IAI =1K'IITAd[a]iI'll
The groundwater potentiometric map indicates that the groundwater flow direction at
the site is from the southeast to the northwest under a gradient of 0.04 feet per foot as
measured between MW-32 and MW-45. Groundwater aquifer characteristics
monitored during the sampling event indicate suitable conditions for biodegradation of
chlorinated hydrocarbons exist at the site. Both the total chlorinated hydrocarbons and
petroleum hydrocarbons contaminant levels in monitoring wells MW-7, MW-11, MW-
13D, MW-14, MW-24, and MW-42 have decreased when compared to the groundwater
contamination levels during the baseline sampling event in June 2008. Monitoring wells
MW-14❑ and MW-43❑ were not sampled during the June baseline sampling event;
however, contaminant levels in both wells have decreased since their most recent
sampling in 2006. Groundwater contaminant levels in monitoring wells MW-13,
MW-23D and MW-45 remained consistent with the baseline levels and monitoring well
MW-25 showed an increase. Monitoring well MW-13 and MW-23D have
tetrachloroethene concentrations below the laboratory detection limits. The increase in
contaminant levels in these wells is caused by increases in cis-1,2-dichloroethene and
vinyl chloride which are degradation components of tetrachloroethene. Monitoring well
MW-25 also shows an increase in these degradation components; however, there is an
increase in tetrachloroethene as well. A comparison of total chlorinated hydrocarbons
in the ten monitoring wells sampled since the baseline sampling event in June 2008
indicate a reduction by 33 percent.
977461 GS009R022 Page 5 April 17, 2009
Copyright 2009 Kleinfelder
Corrective action monitoring will be conducted on a quarterly schedule and the next
event should be scheduled for June 2009. During the next sampling event, we
recommend the following wells are sampled: MW-7, MW-13, MW-13D, MW-14,
MW-14D, MW-16, MW-23D, MW-24, MW-25, MW-42, MW-43D, and MW-45. We also
recommend moving the HiSQC unit from monitoring well MW-10 to MW-25. Monthly
system checks should also be conducted during the next quarter to monitor the rate of
hydrogen consumption of the HiSOC delivery system.
Copies of this report have been mailed to the Guilford County Department of
Environmental Health in Greensboro, North Carolina and the SIC Program in Raleigh,
North Carolina.
977461 GS009R022 Page 6 April 17, 2009
Copyright 2009 Kleinfelder
TABLE 1: GROUNDWATER ELEVATION DATA
Well ID
Total Depth
{feet TOC)
TOC Elevation
(feet}
Date Water
Level
Measured
Static Water
Level
feet TOC
Groundwater
Elevation
feet
MVV-7
29.9
861.19
03/05/09
5.82
855.37
MVV-10
336
857.68
03/05/09
7.1E
850.52
MW-11
25.1
859.26
03/05/09
12.80
846.46
MW-12
16.8
851.50
03/05/09
4.17
847.33
MW-12D
27.0
851.06
03/05/09
5.85
845.21
MW-13
24.2
861.29
03/05/09
14.10
847.19
MW-13D
39.4
860.40
03/05/09
12.93
847.47
MVV-14
24.8
859.32
03/05/09
17.65
841.67
MW-14❑
41.0
859.26
03105M9
18.80
840.46
MW-15
25.2
857.71
03/05/09
12.08
845.63
MW-16
35.2
863.60
03/05/09
27.95
835.65
MW-23D
57.1
860.90
03/05/09
15.26
845.64
MW-24
58.8
858.81
03/05/09
20.40
838.41
MW-25
168.9
86147
03/05/09
22.83
838.64
MW-27
44.0
862.74
03/05/09
13.13
849.61
MVV-28
23.8
861.54
03/05/09
8.04
853.50
MW-29
18.8
861.13
03/05/09
4.28
856.85
MW-30
73.4
862.28
03/05/09
12.83
849.45
MW-31
19.0
861.73
03/05/09
10.74
850.99
MW-32
19.6
861.76
03105/09
9.27
852A9
MW-33
21.0
861.77
03/05/09
14.83
846.94
MW-34
21.0
860.45
03/05/09
well flooded
---
MW-40
29.7
860.62
03/05/09
9.53
851.09
MW-41
20.3
860.52
03/05/09
6.90
853.62
MW-42
35.0
865.32
03/05/09
29.37
835.95
MW-43D
53.0
865.47
03/05/09
29.62
835.85
M W -44
28.5
NM
---
---
--
MVV-45
36.2
86179
03/05/09
27.29
834.50
Notes:
feet TOC = feet below top of well casing
NM = Not measured
97746 1 GS009RO22
Copyrighl 2009 Kleinfelder Page 1 of 1 April 17. 2009
TABLE 2: AQUIFER CHARACTERISTICS FIELD ANALYSIS SUMMARY
Monitoring Well
Sample
Date
Temperature
[ °C j
pH
Conductivity
(m5lcm)
DissolvedRedox
Oxygen
m �L
(mV)
Preferred
Conditions
200C
S<pH<9
--
<0.5 mg1L
<50 mV
MW-7
03/05/09
17.78
7.72
0.234
0.70
-134.7
MW-11
03/05/09
18.07
6.40
0.323
0.85
131.7
MW-13
03/05/09
19.94
6.31
0.396
1.92
427.7
MW-130
03/05/09
18.32
6.41
0.412
0.93
98.3
MW-14
03/05/09
16.35
6.61
0.166
5.37
115.3
MW-14D
03/27/09
16.21
6.52
0.283
1.18
68.7
MW-23D
03/05/09
17.36
7.51
0.705
0.52
-117.7
MW-24
03/05/09
15.79
6.96
0.557
0.29
-61.7
MW-25
03/05/09
15.94
8.22
0.254
0.19
-122.0
MW-42
03/05/09
15.00
7.30
1.415
5.27
292.1
MW-43❑
03/27/09
14.83
6.81
0.393
1.71
-38.0
MW-45
03/05/09
14.37
7.41
0.457
1.03
-26.5
Notes:
Redox = oxidation-reduction potential
°C = degrees Celsius
m51cm = millisiemens per centimeter
mg/L = milligrams per liter, analogous to parts per million
mV = millivolts
Conductivity is measured for consistency in groundwater sample collection.
97746 1 GS009R022
Copyright 2009 Kleinfelder Page 1 of 1 April 17, 2009
TABLE 3: SUMMARY OF GROUNDWATER SAMPLE RESULTS
Parameter
NCGS 2L
Standard
Analytic I Results
Sample ID
MVV-7
MW-11
MW-13
MW-13D MVV-14
MW-140
MVV-23D
MVV-24
MW-25
I MW-42
I MW-43❑ j MW-45
Collection Date
03/05/09
03/05/09
1 03/05/09
03/05/09 03/05/09
03/27/09
03/05/09
03/05/09
03/05109
1 03/05/09
t 03/27/09 1 03/05/09
Volatile Organic Com ounds by EPA Method 6011602 IL
Tetrachloroethene
0.7
BDL
1.3
BDL
BDL
32
10.6
BDL
1,250
24.9
2J
BDL
1.3
Trichloroethene
2.8
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
8.3
BDL
BDL
BDL
cis-1,2-Dichloroethene
70
935
1.5
119
14.6
BDL
1.0
173
466
51
BDL
BDL
8DL
1,1-Dichloroethene
7
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
1.1
BDL
9.3
BDL
Vinyl Chloride
0.015
BDL
BDL
BDL
3.4
BDL
BDL
19.4
BDL
BDL
BDL
BDL
BDL
1,1-Dichloroethane
70
BDL
BDL
BDL
8DL
BDL
BDL
1.1
BDL
BDL
BDL
1.6
BDL
1.1,1•Trichloroethane
200
BDL
BDL
t BDL
j BDL
I BDL I
BDL
I BDL
I BDL
I BDL
I BDL
1 1.2
1 BDL
Total Chlorinated Hydrocarbons
935
3
119
18
32
12
194
1,716
85
3
12
1
Benzene
1
BDL
BDL
BDL
BDL
BDL
BDL
1.7
117
BDL
BDL
9.0
BDL
Eth (benzene
550
749
BDL
SQL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
7.5
BDL
Total X lenes
530
723
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
MTBE
200
BDL
BDL
3.1
13.4
BDL
BDL
194
BDL
4.8
BDL
3.6
BDL
Diisopropyl ether
70
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
Naphthalene
21
384
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
4.4
BDL
Total Petroleum Hydrocarbons
1,856
0
3
13
0
0
196
117
5
0
25
0
Total VOCs
2,791
3
122
31
32
12
389
1.833
90
3
37
1
Notes:
NCGS 2L Standard = North Carolina Groundwater Standard
BDL = Below Detection Limits
pg1L = Micrograms per liter, analogous to parts per billion
BOLD = Concentration exceeds the NCGS 2L Standard
MTSE = Methyl-tert-butyl ether
97746 1 G5009RO22
Copyright 2009 Kleinfelder Page 1 of 1 April 17, 2009
TABLE 4: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS
Sample 10
Chlorinated H dracarbone
Total
Chlorinated
Hydrocarbons
Petroleum H drocarborm Total
Benzene Toluene Ethylbenzene Totalxylenes MTBE DiLsopropylelher Naphthalene Petroleum
Hydrocarbons
1 1.000 550 530 2D0 70 21
TotalVOCs
Collection Date
Tesrachlprnetnene
TrtChioroelhene
c45
o et
Dlrhirohane
1,1-Drchloroelhena Vinyl Chloride
11-oichlorowhane
1,2-Dichloroethane
Irans•1,2-
❑Ichtoroathane
111-Trnchloroethan
NCGS 2L Std
0.7
2 8
70
7 0 015
TO
0 38
100
200
MW-7
09/27/90
790
190
SOL
BDL
BDL
BDL
BDL
BOL
59
1.039
6SO
5,309
1,600
5,700
BDL
BDL
BDL
13150
14.189
01/14192
BDL
360
BDL
BDL
BDL
BDL
BDL
BDL
BDL
360
480
3,900
2,100
7,11D0
BDL
BDL
BDL
13 5B0
13.940
0311IM
BDL
SOL
BDL
354
BOL
BDL
BDL
BDL
239
592
468
8,920
2,200
8,99D
BDL
SOL
BDL
20.578
21.170
05,r25199
8DL
BDL
SOL
723
BDL
BDL
BDL
BDL
347
1.070
253
2,280
2,290
10,80D
BDL
BDL
BDL
15.623
16.693
04122/03
BDL
BDL
BDL
BDL
BDL
8DL
BDL
BDL
Be
Be
BDL
220
2,400
5,700
BDL
60
BDL
8.380
8468
06/30104
BDL
BDL
2,300
BDL
BDL
BDL
BDL
BDL
BOL
2.300
BDL
110
1,800
3,800
BDL
8DL
620
6.230
B.530
OWM05
BDL
BDL
2,1D0
BDL
BDL
SOL
BDL
BDL
SOL
2.1DO
BDL
BDL
1,600
3,020
BOL
BDL
520
5.140
7.240
OBI25106
BDL
BDL
2,000
14
BDL
BOL
BDL
1 5
14
2030.
1.7
23
370
380
11
3 3
82
B71
2 901
1211410G
3,6
4
2,100
570
BDL
15
BDL
51
13
2711
4.1
39
5,300
1,660
80L
BDL
440
3.443
6.154
06/05108
BDL
BDL
1,750
BDL
SOL
BDL
SOL
BDL
BDL
1.750
SOL
SUL
1,040
1,280
BDL
BDL
401
2.721
4.471
09/04/06
SUL
BDL
1,190
BDL
BDL
SUL
BDL
BDL
BDL
1190
8pL
BDL
788
873
BDL
SUL
301
1.962
3.152
01/05109
BDL
SOL
7"
BDL
BDL
BDL
BDL
BDL
BDL
798
BDL
BDL
643
598
BDL
BDL
3"
1.549
2.347
03J05109
BDL
BOL
935
BDL
BDL
BDL
BDL
SDL
BDL
935
BDL
BDL
748
723I
BDL
BDL
384
1.B56
Z791
MW-8{ehandonedl
0W27190 BOL SDL
BDL
BDL
BDL
BDL
BDL
BDL BDL
0
BDL
BDL
BDL
1
BDL
BDL
BDL
1
1
01114192 SUL SDL
BDL
BDL
BDL
BDL
BDL
SOL BDL
0
BDL
SOL
_ SUL
BDL
BDL
BDL
BDL
0
0
05/15/92 BDL SUL
BDL
BDL
BDL
BDL
SOL
BDL BDL
0
SOL
BDL
BpL
SUL
SOL
BDL
BDL
0
0
MW-9(abandoned)
OW27M
10
2 SOL
BDL SOL
BDL
SOL BOL
BDL
12
2
SOL
SDL
SOL
BOL
SOL
BDL
2
14
01/14192
SOL
SOL SOL
BDL BOL
BOL
BOL BDL
SOL
0
SOL
SOL
BDL
BOL
I SOL
SOL
BDL
D
0
051T5192
SDL
BDL BDL
BDL SOL
BDL
BOL BDL
BDL
0
BDL
BDL
BDL
SOL
SOL
SOL
BDL
0
0
MW-10
09/27/90
76
140
SOL
SOL
SOL
BDL
SOL
BDL
140
356
2,900
66
801
670
SOL
BDL
SOL
3.635
3.992
01/14/92
SOL
78
SOL
120
SOL
BDL
SOL
BDL
SOL
198
2,900
BDL
SOL
120
SOL
BDL
BDL
3.020
3.215
03111/98
SOL
BDL
BDL
13,9
BDL
BDL
BDL
SOL
BDL
14
234
BDL
BDL
BDL
SOL
BDL
BDL
234
248
0512M9
SOL
SUL
BDL
SOL
SOL
SOL
BOL
BDL
SOL
0
36
BOL
BDL
SOL
SDL
BDL
SOL
36
36
10110102
6.9
23
SDL
44
BOL
SOL
BOL
BOL
73
20
220
85
15
71
2,200
16
BDL
2.532
2.551
04/22103
3.2
1 3
BOL
BDL
BUL
BDL
SOL
BAL
2 6
7
47
BDL
SOL
SOL
1,100
2 9
SOL
1.150
1.157
Dfil''J0104
BDL
BDL
8 T
BDL
BDL
BDL
8DL
BDL
BDL
8
22
BOL
2 B
5.8
770
2 8
BDL
803
812
06/24 5
BDL
BDL
BDL
BOL
SOL
BDL
8DL
BDL
BDL
0
43
BDt
BDL
BOL
690
BDL
BDL
723
723
08/24106
BDL
BDL
3
SOL
SOL
BDL
BDL
BDL
SOL
3
8.1
SOL
BDL
BDL
360
4 3
BDL
372
375
MW-11
06/30/04
Z.1
3
1 4
SOL
SOL
BDL
BDL
SUL
SOL
7
SOL
BDL
BDL
BDL
41
SOL
BOL
4
11
08/15/05
S
3.4
97
BDL
BDL
BOL
BOL
8131.
SOL
18
SOL
BDL
BDL
BDL
22
SOL
8DL
2
21
08P24106
4.9
25
52
SOL
BDL
BDL
SOL
SOL
BDL
13
SOL
BDL
81)L
BDL
44
SOL
SOL
4
17
MOWS
6,9
15
50
BOL
BDL
BDL
BDL
BOL
BDL
13
SOL
BDL
SOL
BDL
BDL
SOL
BDL
0
13
09104108
BDL
BDL
BDL
SOL
BDL
8DL
BDL
SOL
SOL
0
BOL
BDL
SOL
SOL
BDL
SOL
BDL
0
0
01105109
2.7
1 6
2 5
BDL
BDL
BDL
SDL
BOL
BOL
7
BDL
81)L
BDL
BDL
1 1
BDL
SOL
1
8
03105M
1.3
BOL
15
SOL
BDL
BDL
SOL
SOL
BOL
3
SUL
SOL
SOL
SOL
SOL
BDL
BpL
0
3
MW-12
D9127190
BDL
BDL
BDL
SOL
BDL
BDL
SOL
BDL
BDL
0
SOL
BDL
8DL
BDL
BDL
BDL
BDL
0
a
01/14/92
BDL
SOL
8DL
SOL
BDL
BDL
BDL
BOL
BDL
0
SOL
BDL
BDL
BOL
BDL
BDL
BDL
0
0
03111/98
BDL
SOL
BDL
SOL
SOL
BDL
BDL
BDL
SOL
0
SUL
BDL
BDL
SOL
SOL
SOL
SOL
0
0
05/26/99
SOL
BDL
BDL
BOL
SOL
SUL
BDL
SUL
SOL
0
BDL
SOL
BDL
13DL
BDL
BDL
SOL
0
0
06W04
BDL
SOL
SOL
BDL
SOL
SUL
BDL
SUL
BDL
0
BDL
BDL
BOL
SOL
BDL
SOL
SOL
0
0
08/15/05
SOL
BOL
SOL
BDL
BDL
BDL
BDL
BDL
BDL
0
BDL
BDL
SOL
SOL
90L
SOL
SOL
0
0
08/24/06
BDL
BDL
SOL
SOL
BDL
SOL
BDL
SOL
BDL
0
BDL
BDL
BDL
BOL
SOL
SOL
BDL
0
0
MW-12D
09/27/90
SOL
BDL
SOL
SOL
BDL
8DL
BDL
SOL
SOL
0
BDL
BDL
SOL
BDL
SOL
BDL
SOL
0
0
01/14192
BDL
SOL
SOL
BDL
BDL
SOL
BDL
SOL
BDL
0
SOL
SOL
SDL
SOL
SOL
BDL
BDL
0
0
03/11198
BDL
BOL
BDL
BDL
BDL
BDL
SOL
BDL
BDL
0
SDL
BDL
BOL
BDL
SOL
BDL
SOL
0
0
05128/99
SUL
BOL
SOL
BDL
SOL
SOL
SOL
SOL
BDL
0
SOL
BDL
BDL
SOL
SOL
8DL
BOL
0
0
OW30/04
BDL
SOL
SOL
SOL
SUL
BDL
SOL
SOL
SOL
0
SOL
SOL
BDL
SOL
BDL
BDL
BDL
0
0
08/15/05
SOL
8DL
BDL
SOL
SOL
BDL
SOL
BDL
SOL
0
BDL
BDL
BDL
BDL
SDL
BDL
SOL
0
0
D8I24M6
BOL
BDL
BOIL
9DL
SOL
BDL
SOL
BDL
BDL
0
BDL
SDL
BDL
SOL
SOL
BDL
BDL
0
0
Notes:
All units measured in ygfL
BDL - Below Detection Llmils
NCGS 2L Sid - North Carolina Groundwater Standard
BOLO - Concenlralion exceeds the 2L Groundwater quality Standard
MTSE - Methyl *W butyl ether
97746 1 GS0O9R022
Copyright 2009 Klemtelder Page 1 of 4 April 17, 2009
TABLE 4: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS
Sample ID
Chlorinated H drocarbons
Total
Chlorinated
Hydrocarbons
Petroleum Hydrocarbons
Total
Petroleum
Hydrocarbons
Total VOcs
Collection Dare
os-1.2
Tetrachlaroethene Trichldroetnene c
D,Crtloroelhene
7 T-pichloromhene Vinyl Chlonde
1 1-Dichloroethane
1.2-Dirhmreelhane
0ans-1 2
Dichioroelhane
1.1.1-Tnchicroe!
Benzene
Toluene
Elhylhenzene
Total %ylenes
MTBE
Onsopropyl ether
Naphthalene
NCGS2LSid
07 2.8 79
7 0015
70
0.38
100
200
1
1,000
550
530
200
J 70
21
MW-13
09/26/90
2
BDL
SOL
SOL
SOL
SOL
SOL
BDL
SOL
2 SOL.
BDL
SOL
SOL
BDL
SOL
BDL
0
2
01114/92
130
36
SOL
SOL.
SOL
SOL
SOL
BpL
BDL
166 BDL
BDL
SOL
SOL
BOL
SOL
SOL
0
166
05115192
130
20
SOL
SOL
SOL
SOL
SOL
SOL
SOL
15O SOL
SOL
SOL
BDL
BDL
SOL
SOL
0
ISO
0311IM
2.5
41
BDL
BOL
BDL
SOL
SOL
SOL
BDL
7 SOL
SOL
SOL
SOL
BOL
BDL
SOL
a
7
05126I99
41
1s
BpL
SOL
BDL
BDL
BDL
SOL
SOL
19 BpL
SOL
SOL
SOL
BDL
BDL
SOL
0
19
06/30104
BDL
6.5
140
SOL
BDL
BDL
BDL
SOL
SOL
147 BDL
BDL
8DL
SOL
13
BDL
SOL
13
160
09/15/05
SOL
SOL
110
BDL
SOL
BDL
SOL
SOL
SOL
110 SDL
8DL
SOL
SOL
BDL
BDL
SOL
O 1
110
08+24l06
BDL
2.9
110
SOL
SOL
SOL
BDL
1 t
SOL
114 SOL
SDL
SOL
SOL
5.4
SOL
SOL
5
119
❑610510e
SOL
BDL
94.7
SOL
SOL
SOL
BDL
SOL
SOL
95 SA
SDL
BDL
SOL
BDL
SOL
BDL
6
101
09104me
BDL
SDL
679
BDL
SOL
SOL
SDL
SDL
SOL
68 BDL
8DL
SOL
SOL
BDL
SOL
SOL
0
Be
01105109
SOL
SOL
667
SOL
SOL
BDL
SOL
SOL
BOL
69 3.2
SDL
BDL
SOL
52
SOL
SOL
8
77
03105109
BDL
SOL
11S
BDL
SOL
8DL
SOL
SOL
SOL
119 BDL
BDL
BDL
BDL
3.1
SOL
BOL
3
122
MW-13D
06130104
SOL
SOL
t8
BDL
1.5
BDL
SOL
BDL
SOL
20
IA
SOL
BDL
BDL
26
11
SOL
28
48
08115105
SOL
SOL
37
BDL
1.4
SOL
SOL
BDL
SOL
38
SOL
8DL
BDL
BDL
20
1.3
SOL
21
60
OW41DS
BDL
SOL
30
SOL
1.3
SOL
SOL
BDL
SOL
31
SOL
BDL
Dot
SOL
19
BDL
SOL
19
50
0610510E
SOL
SOL
216
SOL
3.2
SOL
SOL
SOL
SOL
25
SOL
SOL
30
36
12.5
17
SOL
21
46
09104M
BDL
SOL
152
BDL
3A
BDL
BDL
SOL
BOL
18
SOL
BDL
SOL
SOL
176
BDL
SOL
18
36
OV05109
SOL
SOL
174
SOL
4.2
SOL
SOL
SOL
BOL
22
SOL
SOL
SOL
SOL
16.3
1 1
BDL
17
39
03105/09
BDL
BDL
146
BDL
34
SOL
BDL
SOL
SOL
18
SOL
BDL
BDL
SOL
134
BDL
BDL
13
31
MW-14
09/26/90
1,300
8DL
BDL
9DL
SDL
SOL
BDL
SDL
BDL
1.300
SOL
SOL
SOL
BDL
BDL
SOL
SOL
0
01114/92
1,400
8DL
SOL
BDL
BDL
SOL
180
SOL
100
1.680
SOL
60
SOL
100
ROL
SOL
SOL
160
840
03/11/98
en
SOL
SOL
BDL
SOL
BpL
BDL
Dot
BOL
80
SOL
SOL
BDL
SOL
BDL
SOL
BDL
0
0
0512SMS
67
SOL
SOL
SOL
SOL
SOL
aDL
SOL
SOL
67
SOL
SOL
SOL
SOL
BDL
SOL
SOL
0
j30'
7
D4122103
110
BDL
SOL
BDL
SOL
SOL
SOL
SOL
SDL
110
1.1
1.7
SOL
19
BDL
SOL
SOL
5
15
06MX4
80
SOL
6OL
BDL
SOL
BDL
BDL
SOL
SOL
80
SOL
SOL
SDL
SOL
BOL
BDL
BDL
0
0
08/16/05
58
SOL
8DL
BDL
SOL
BOL
SOL
SOL
8DL
58
SOL
BOL
SOL
SOL
BDL
BDL
BOL
0
e
08/24106
46
SOL
SOL
BDL
BDL
BDL
SOL
SOL
SOL
46
BDL
BDL
BDL
SOL
DDL
BDL
BDL
06
06/,05108
54.0
SOL
SOL
SOL
BDL
BDL
BDL
BDL
BDL
54
SOL
SOL
BOL
BOL
BDL
SOL
BDL
❑
54
09/04100
50.0
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
50
SOL
BDL
SOL
SOL
BOL
SOL
8DL
0
50
❑,05+❑9
293
SOL
BDL
SOL
SOL
8Dl
SOL
SOL
SOL
30
BDL
SOL
SOL
SOL
SOL
SOL
SOL
0
30
03105109
32
SOL
BOL
SOL
BDL
BOL
BpL
SOL
BDL
32
BOL
BDL
BDL
SDL
SOL
BDL
BDL
0
32
MW-14D
09127M
110
3
BDL
sa
BDL
5
SOL
BOL
20
196
46
1
BDL
5
BDL
SOL
SOL
51
247
01114/92
200
SOL
SOL
BDL
BDL
BpL
SOL
SOL
SOL
200
65
3
SOL
SOL
BDL
SOL
aDL
68
268
05/15/92
55
SOL
SOL
2.1
8DL
SOL
SOL
BDL
SOL
58
4,7
SOL
SOL
BDL
BDL
BOL
ODL
5
63
09109/92
210
BDL
SOL
23
SOL
SM
SOL
BDL
13
246
220
SOL
SOL
SOL
BDL
SOL
BDL
220
466
03111/98
3S,4
BDL
BDL
10.6
SOL
SOL
SOL
BDL
BDL
46
SA
SOL
BDL
BDL
BDL
SOL
8DL
6
52
05/25/99
201
BDL
SDL
25
BDL
SOL
BDL
SOL
BOL
226
67
SOL
BDL
BDL
BDL
SOL
SOL
67
293
1011=2 1
79
28
BOL
4
SOL
4.2
BDL
BDL
SOL
90
6.3
BDL
SOL
BDL
11
29
SOL
48
138
04122J03
40
SOL
BDL
12
SOL
SOL
SOL
SOL
SOL
41
SOL
SOL
SOL
BDL
SOL
15
SOL
2
43
06/30104
29
SOL
30
35
SOL
2.2
SOL
SOL
SOL
35
BpL
SOL
SOL
BDL
33
8DL
BDL
3
38
❑81161D5
55
} 8
15
3.3
BDL
BDL
SOL
BOL
SOL
75
5.4
SOL
SOL
SOL
3.2
7 3
DDL
16
91
OB114106
47
2
17
14
BOL
HDL
SOL
Dot
BDL
67
1.3
SOL
SOL
BOL
2.4
64
SDL
10
78
03/27109
10.0
SOL
10
SOL
BDL
SOL
SOL
BpL
BpL
12
8DL
SOL
BDL
BDL
80L
SOL
BDL
❑
12
MW-i 5
0927190
SOL
SOL
SOL
SOL
BDL
BDL
SOL
SOL
BDL
0
BDL
SOL
BDL
BDL
SOL
SOL
SOL
0
0
01/14/92
SOL
SOL
SOL
SDL
BDL
BDL
SDL
SOL
8DL
0
SOL
SOL
SOL
BDL
BDL
SOL
SOL
0
0
03111198
BDL
SOL
SOL
BDL
BDL
8DL
SOL
SOL
BDL
0
SOL
BDL
BDL
BOL
BOL
SOL
BDL
0
0
05125199
4.9
3
SOL
BDL
BDL
SOL
SOL
SOL
SOL
8
BOL
BDL
BDL
BOL
6DL
SOL
SDL
0
B
10110/02
13
7A
SOL
BDL
BDL
14
SOL
SOL
8DL
22
SOL
BDL
BDL
SOL
29
SOL
BDL
29
51
04/22/03
11
5
BDL
SDL
SOL
14
SOL
BDL
8DL
17
SOL
8DL
SOL
SOL
17
SOL
8DL
17
34
06/30/04
7.5
3.9
a8
SOL
SOL
SOL
SOL
BDL
8DL
97
SOL
SRL
BDL
SOL
18
SOL
BDL
18
OW16105
5.8
2 3
47
SDL
BDL
BOL
BDL
8DL
BDL
56
BDL
BpL
BDL
8OL
15
BDL
SDL
15
08/24/06
5.5
5
48
BDL
BDL
B17L
BDL
BDL
BDL
59
BOL
BOL
BDL
8DL
8
BDL
BDL
6
67
Notes:
All units measured in N91
BDL - Below Detection Lim its
NCGS 2L Std - North Carolina Groundwater Standard
SOLD - Concen0ation exceeds the 2L Groundwater Quality Standard
MTBE • Methyl -left butyl ether
97746 1 GS009R022
Copyright 2009 Kleinfelder Page 2 of 4 April 17, 2009
TABLE 4: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS
Sample 10
Chlornated H drocarbons
Total
Chlorinated
Hydrocarbons
Petroleum Hydrocarbons
Total
Petroleum
Hydrocarbons
Total VOCs
Collection Dale
Telradlloroethene Tnchlordelhana
Cis 1'2
Dichloraaihene
i 1-Dichlor9athene
Vinyl Chloride f,1-Dlchloraelhane
1,2-Dahlomethane Irans 1'2
Dichloroethane
7,1 1-Tnchlcroethan
8enxene
Toluene
Elhylbenzene
Total Xylenes
MTSE
❑lisopropyl ether
Naphthalene
NCGS 2L Std
0.7 28
70
7
0 015 70
0 3B 100
200
i
1 am
550
530
200
70
21
MW-16
Os126190
ROL
SOL
BDL
ROL
SOL
SDL
BDL
BDL
BDL
0
SDL
SDL
SOL
SOL
SDL
SDL
BDL
0
0
01/14/92
ROL
BDL
BDL
ROL
SDL
ROL
SOL
ROL
ROL
0
ROL
BDL
BOL
SOL
SOL
ROL
BDL
0
0
0317115E
1.9
SOL
SOL
SOL
SOL
ROL
BDL
SOL
SOL
2
ROL
HDL
ROL
SOL
SDL
SDL
ROL
0
2
DW2199
2.4
BDL
SOL
BDL
SOL
SOL
SDL
ROL
SOL
2
SOL
BDL
BDL
BDL
SOL
BDL
SOL
0
2
10/10102
22
3.a
ROL
18
SOL
SOL
SOL
SOL
SOL
28
SOL
BDL
ROL
ROL
SOL
BDL
SDL
0
28
04/22/03
46
6.6
BDL
3.6
ROL
ROL
SOL
ROL
ROL
58
BDL
BRL
SOL
SOL
dDL
SDL
BOL
0
58
1761301D4
31
7A
24
2 7
BDL
t
BDL
SOL
SOL
66
BDL
SOL
SOL
SOL
SDL
SOL
BDL
0
66
061151D5
30
4.4
ROL
18
BDL
SDL
8DL
BDL
SDL
36
SDL
RQL
8DL
8DL
BRL
17
BOL
77
53
06125/06
36
7,4
31
2.9
BDL
ROL
SOL
BDL
ROL
77
SRL
SOL
BDL
SDL
SDL
BDL
SOl-
0
77
MW-17(aoandoned 01143105)
09126/90
1
BDL
SOL
SOL
SDL
BDL
SOL
ROL
SOL
1
SOL
BDL
SOL
SOL
SOL
ROL
RDL
0
1
01/14/92
SOL
3
ROL
BDl
ROL
SOL
BDL
ROL
BDL
3
8QL
BDL
SOL
BOL
BDL
SDL
SOL
0
3
03/11/90
SDL
SOL
BDL
ROL
BDL
ROL
BDL
ROL
ROL
0
SOL
BDL
BRL
SQL
6DL
BDL
BDL
D
D
05102199
ROL
ROL
SOL
SOL
SOL
ROL
BDL
ROL
BDL
0
BDL
9DL
130L
SQL
ROL
SOL
BDL
D
0
0613004
Sal-
SDL
BDL
BDL
BDL
BDL
ROL
SOL
0
SDL
8DL
SOL
8DL
17
SOL
BDL
17
17
-RDL
MW-23D
09/27/90
ROL
2
BDL
ROL
BDL
5
5
BDL
SDL
12
1
SOL
SDL
SOL
ROL
8DL
SOL
1
13
01114W
SDL
BDL
BDL
BDL
BDL
8DL
ROL
BDL
BDL
D
ROL
BDL
SOL
ROL
SQL
RDL
BDL
0
0
05115192
BDL
22
ROL
SOL
ROL
5.3
ROL
BDL
BDL
8
46
8DL
SOL
ROL
SOL
SOL
ROL
45
53
09M9192
1.8
6.3
SOL
54
BDL
65
2
BDL
BDL
22
6.3
RDL
ROL
BDL
ROL
RDL
SOL
6
28
0311119E
2.5
25
SOL
1 4
ROL
2.9
BDL
BDL
4
13
T1
37
SOL
SDL
ROL
SDL
SOL
11
24
175J26199
ROL
4.1
SOL
24
ROL
5 7
2.6
BDL
SOL
15
3,1
SOL
SOL
SDL
ROL
BDL
SOL
3
1B
06/30/04
ROL
ROL
200
SOL
ROL
SDL
BDL
SOL
BDL
2DO
SOL
ROL
BDL
BDL
500
12
SOL
512
712
08115ro5
ROL
ROL
280
BDL
SDL
SOL
SOL
BDL
SOL
280
BDL
SDL
SOL
BDL
310
SOL
BDL
310
590
DW4106
SOL
f 1
340
SOL
1.9
SOL
SDL
BDL
SOL
343
1.8
9OL
BDL
BDL
310
9.1
ROL
321
664
OM908
SDL
BDL
166
SOL
BDL
ROL
aDL
SOL
SOL
166
SOL
SOL
20.2
236
208
8DL
ROL
252
418
09/04108
SOL
BDL
5.3
ROL
ROL
ROL
SOL
SOL
SDL
5
BDL
SOL
SOL
BDL
19.3
SDL
8DL
19
25
Ut1O"
SOL
ROL
15.3
SOL
BDL
ROL
SOL
BDL
ROL
15
SDL
SOL
ROL
SOL
376
8DL
BDL
315
53
03/05109
SOL
BDL
173
BDL
19.4
11
SOL
BDL
ROL
194
1J
SOL
ROL
BDL
794
SDL
SOL
196
389
MW-24
09127/90
630
28
SDL
60
BDL
ROL
SOL
SOL
BDL
718
1,500
80
BDL
80
SDL
SDL
SOL
1.660
2 378
01114/92
3,11100
110
BDL
200
ROL
ROL
56
SOL
80
4.246
1,800
260
ROL
340
BOL
130L
BDL
2.400
6646
05115/92
1,400
25
SDL
49
8DL
ROL
ROL
ROL
SOL
1.4W
1,800
150
ROL
801-
BDL
SOL
BDL
1.980
3.410
09/09192
2,700
ROL
SOL
SOL
SOL
SOL
ROL
SOL
100
2.800
2,500
150
ROL
15D
BDL
SOL
BDL
2800
SAW
03/11196
1,230
ROL
SOL
SOL
ROL
ROL
SOL
SOL
ROL
1.230
1,920
8DL
SOL
SOL
ROL
SOL
RDL
1.920
3.150
05125199
637
ROL
SDL
BDL
SDL
BDL
ROL
ROL
BDL
637
1,610
SOL
ROL
SOL
SOL
SOL
BDL
1.510
2.147
1oil W02
2,000
66
BDL
31
SOL
11
2.9
SOL
4.9
2.117
1,700
16
14
27
180
530
BDL
2.454
4.572
04122103
640
24
SOL
17
SOL
64
8DL
ROL
7 8
689
No
64
ROL
63
81
18O
SOL
774
1.463
0613"
870
SOL
370
SOL
ROL
ROL
ROL
SOL
SOL
1.240
280
ROL
ROL
SOL
74
200
SOL
$54
1794
D8116ro5
1,300
62
570
ROL
ROL
SDL
ROL
BDL
SOL
1.932
420
ROL
BDL
SOL
69
170
SOL
059
2,591
OEr24106
2,200
94
770
15
SOL
64
1.2
1 2
6.5
3.083
660
4.8
ROL
104
78
t60
5.6
919
4 002
06105/08
1,840
ROL
545
SOL
ROL
SOL
BDL
BDL
SOL
2.385
210
ROL
ROL
ROL
551
140
SOL
405
2,790
09/04/08
1,430
51.7
349
BDL
ROL
SOL
ROL
SOL
ROL
1.831
253
ROL
BDL
BOL
BDL
603
RDL
313
2.144
01105109
1,610
78.4
517
SOL
SOL
SOL
BDL
SOL
SOL
2.205
28O
ROL
BDL
ROL
70.9
716
SOL
467
2,672
03/65/09
1,260
SDL
466
ROL
BDL
ROL
SOL
SOL
SOL
1.716
117
SDL
BDL
SOL
ROL
SOL
SQL
117
1.633
MW-25
03111/98
8,9
3,5
BDL
ROL
ROL
ROL
SOL
SOL
ROL
12
8DL
ROL
SDL
ROL
SOL
SOL
RDL
0
12
0s26199
10
3.8
SDL
ROL
RDL
ROL
SDL
SDL
ROL
14
ROL
BDL
RDL
SOL
BDL
SOL
BDL
0
14
06/30104
6.1
3.5
99
ROL
BDL
ROL
SOL
BDL
ROL
22
ROL
SOL
BDL
ROL
SOL
4.4
8DL
4
26
08116/05
17
3.9
31
ROL
ROL
ROL
ROL
BDL
SDL
52
HDL
BDL
SOL
ROL
36
SOL
BDL
4
56
013l25106
20
4.9
51
SOL
BDL
ROL
8DL
SOL
BDL
76
8DL
SOL
SOL
SDL
1 a
4.3
SOL
6
82
06105M
11.7
3,2
23.5
SOL
SOL
ROL
SOL
SOL
BDL
38
SOL
ROL
1.3
SOL
22
4.2
SOL
a
46
M04M
18.7
5.2
332
SRL
SOL
ROL
SDL
SOL
ROL
57
SOL
ROL
BOL
SOL
3
48
BDL
8
65
D1ros109
22 9
6.5
46.6
1 1
BDL
1 1
ROL
BOL
BDL
78
BDL
RDL
ROL
ROL
4 8
6.2
BRL
11
89
03rO5ro9
249
6.3
51
11
BDL
RQL
SDL
BDL
BDL
85
BDL
8GL
ROL
ROL
4.8
6OL
BDL
5
90
MW-26 {abandoned 01103106)
27121104
SOL
SOL
ROL
SOL
SDL
SOL
ROL
SOL
SOL
0
SOL
SOL
SOL
BDL
RDL
SOL
ROL
0
0
0&15105
SOL
BDL
8DL
SDL
SOL
SOL
SOL
ROL
ROL
0
SOL
SOL
81)1-
SOL
RDL
ROL
SOL
0
0
MW-27
10110102
SOL
SOL
SOL
BDL ROL
SOL
ROL
ROL
SDL
0
2,3 2
47
78
2.3
SOL
ROL
72
72
071011D4
SOL
ROL
BOL
BDL BDL
SOL
BDL
RDL
SOl-
0
5,4 2 7
34
7 9
11
8OL
77
TB
7a
08/16105
RDL
SAL
RDL
BDL BDL
BDL
ROL
BDL
SOL
0
12 4.1
18D
34
3.5
Bill
30
264
264
11101105
SOL
SOL
6DL
SOL BDL
SOL
ROL
ROL
BDL
0
6,2 2 4
38
3 1
BDL
80L
16
fib
66
Notes:
All units measured in NgIL
BDL - Below Detection Limits
NCGS 2L Std. - North Carolina Groundwater Standard
BOLD - Concentration exceeds the 2L Groundwater 0uably Standard
MTBE - Malhyl-lerl butyl ether
97746 1 GS009R022
Copyright 2DD9!Slain}elder Page 3 of 4 April 17, 2009
TABLE 4-, HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS
Sample ID
Chlorinated arbO H drocns
Tonal
Chlorinated
Hydrocarbons
Petroleum Hydrocarbons
Total
Petrotsum
Hydrocarbons
Total VOCs
Dale
Teiractrloroelherte
Trichloroerhene
CM-1 1,1-Drchlaroethene
Dichlaroet hene
Vinyl Chloride
1 1-Drchloraethane
1.2-DIdllnroatkiane
trans-1.2•
Drchl oetnane
1 1 1-Trichlwoelhan
Benzene
Toluene
E0lylbenxane
Total Xylenes
MTBE Dnsopropyl ether
Naphthalene
NCGSron
CGS 2L Std
0.7
2.8
70 7
0015
70
038
t00
200
1
],000
55Q
530
200 70
2t
MM1.28
10110/02
SOL
SOL
SOL
SOL
SOL
BDL
BDL
BDL
BDL
0 11
10
1 22
1 45
225
BDL
23
BRL
82
62
07101/04
BDL
SOL
SOL
SOL
BOL
SOL
BDL
BDL
BDL
0
95
51
1,50D
1,066
BDL
BDL
480
3.191
3.191
08/15/05
RL
BDL[
BOL
SDL
BDL
DL
O
0
210
8
,
750
4.078
4.078
DL
8DL
BD
L
SOL
SOL
DL
85
SOL
Q
170
6
200
BDL
BL
8005/2
4.726
4 725
12/14106
BDL
BDL
BDL
SOL
SOL
SOL
BDL
BOL
BOL
0
400
BOL
1 2,500
530
SOL
BDL
940
4.070
4.070
MVV-29
0710110-0
23
SOL 250
BDL
8DL
SOL
SOL
BDL
SOL
303
BDL
SOL
21
BDL
BDL
BDL
SOL
21
324
08/15/05
39
4,2 29
BOL
BDL
SOL
SOL
BDL
BDL
72
BDL
BOL
SOL
BDL
BDL
BDL
BOL
0 11
72
08125M6
5
22 38
BDL
BDL
SOL
BDL
BDL
BDL
45
BDL
I SOL
I BDL
I SOL
BDL
BDL
I SOL 11
0
H 45
MW-30
07/01104
SOL
SOL
BDL
BDL
BDL
BOL BDL
BDL
BDL
0
BDL
BDL
SOL
BDL
2,200
SOL
SOL
2.200
2,200
0&16105
SOL
SOL
200
43
77
BDL BDL
BDL
BOL
320
74
BDL
56
BDL
510
SOL
BDL
642
962
08/25/06
BDL
SOL
23
1 25
16
BDL SOL
BDL
SOL
42
23
SOL
26
2
1,500
13
BDL
1541
1,5B2
MW-31
10110102
BDL
SOL
SOL
SOL
SOL
SOL
SOL
8DL
BDL
❑
BOL
320
2,600
7,900
SOL
BDL
SOL
10.820
10,820
04122103
BDL
SOL
BDL
SOL
SOL
SOL
SOL
SOL
BDL
0
BDL
310
1,800
4,600
SQL
SOL
SOL
6 710
6.710
07/01104
BDL
BDL
53
SOL
SOL
SOL
BDL
SOL
SOL
53
18
64
590
1,360
SOL
BRL
400
2452
2.505
W15105
BDL
SOL
46
SOL
BDL
SOL
BDL
BDL
SOL
48
SOL
67
1,100
1,490
BDL
SOL
750
3407
3,455
11101/06
BDL
BDL
SOL
SOL
SOL
SOL
BDL
BDL
9DL
0
SOL
BDL
1,700
390
BRL
SOL
720
2.510
2.810
MW-32
07101104
SOL
BDL
SOL
BDL
BDL
SOL
BOL
BOL
BDL
❑
BDL
BOL
BDL
SOL
290
SOL
ROL
29D
290
08115M5
BOL
BDL
BDL
SOL
SOL
SOL
SOL
BDL
BDL
❑
BDL
BOL
SOL
SOL
180
SOL
BDL
180
180
00/25/06
BDL
6OL
BDL
SDL
BDL
BDL
SOL
SOL
SOL
0
1,400
280
190
900
16,000
32
180
17.662
17662
11101/06
SDL
BDL
SOL
BDL
BDL
BOL
ROL
SOL
SOL
0
1,400
320
340
9DD
20,000
SOL
SOL
22.950
229W
121141❑6
BDL
SOL
BDL
SOL
BDL
SOL
BDL
SOL
SOL
0
1,50D
3.700
1,700
8,000
16,000
SDL
1,100
32.000
32OW
VW-23
10/10/02
SOL
BDL I BDL
I SOL I 9DL
T SOL
I BDL I SOL
BOt
0
8DL
BDL
BDL
8p4
8QL
BOL
BDL
0
0
06/30/04
BDL
BDL 7.6
SDL 8DL
BDL
BDL SOL
BDL
2
BDL
BDL
BDL
8DL
BDL
SOL
SOL
0
2
08115/05
SOL
SOL 5.6
BDL 8DL
SOL
SOLSOL
SOL
6
BDL
BDL
BDL
SOL
SOL
81311.
BDL
0
6
08/25106
SOL
BDL 5.7
SOL BDL
SOL
SOL SDL
SOL
6
BOL
BDL
BDL
I 9DL
I SOL
I SOL
I BDL 110
6
MW-34
D4122103
BDL
100
BDL
15
BDL
72
BDL
SOL
SOL
122
BDL
SOL
BDL
SOL
BDL
SOL SOL
0
122
07/01104130
63
6.3
BDL7.4
SDL
BDLL
207
5
BDL
9
37
SOL
BDL
BDL
BDL
BDL
BDL
127
BDL
[—BDL
L
D08/16
BDL
BD
BDL BDL
0
127
06/25106
8DL
59
24
4.8
SOL
23
SOL
SDL
BDL
90
SOL
SOL
8DL
SOL
BDL BOL
0
90
MW-40
11/01106 BDL BDL BDL BDL BDL BDL BOL SOL SOL 0 250 230 280 552 ROL BDL 134 11 1.442 1.442
MLV-01
04f22103 SAL
SOL
BDL BDL
SOL
SOL
SOL
BDL
BDL
0
7,200
1 5,600
1 2,400
1 t0,8D0
SOL
SOL
SOL
27,000
27,000
07/08/44 SOL
SOL
SOL SOL
SOL
SOL
SOL
ROL
BDL
0
7,DDD
6,600
2,600
1.3,309
1 SOL
520
770
30.790
30.790
08116/05 BDL
SOL
SOL BDL
SOL
SOL
SOL
SOL
BDL
0
5,400
4,900
2,500
9,700
SOL
230
780
23.510
23,510
08124M BDL
SOL
BOL SOL
SOL
SOL
BDL
SOL
SOL
0
3,100
3,000
1,000
2,900
ROL
64
16
10.022
10.022
MW-42
01/10/06
36.0
BDL
7 5
61
BOL
16
BDL
BDL
BDL
51
BDL
SOL
BDL
8DL
SQL
SOL
32
3
54
08125106
27A
BDL
47
35
SOL
15
BDL
ROL
BDL
37
SOL
BDL
SOL
8DL
BDL
SOL
SOL
0
37
061051Q8
6.3
BDL
BDL
SOL
SOL
BOL
SOL
BDL
SOL
5
SOL
SOL
SOL
BDL
BDL
SOL
BDL
0
5
091D4108
5,7
SOL
SOL
BDL
SOL
SOL
BDL
BDL
BDL
6
SOL
SOL
BDL
BDL
SOL
BOL
BDL
0
6
011051D9
5.3
BDL
SOL
SOL
SOL
SOL
SOL
BDL
SOL
5
SOL
SOL
BDL
SOL
SOL
SOL
BDL
0
5
03IM09
2.7
SOL
SOL
BDL
SOL
SOL
BDL
BDL
SOL
3
SOL
SOL
SOL
SOL
BDL
SOL
SOL
0
3
N1W-43❑
01/10106 1
390
12.0 110
42.0
SOL
6.8
SOL
BDL
BDL
561
4A
BDL
SOL
SOL
36.0
6B.0
SOL
109
670
03/27109
SOL
SOL SOL
9.3
SOL
SOL
1.6
BDL 1
12 JL
12
H 9.0
1 SOL
1 75
1 SDL
1 36
SOL
1 4.4
H25
37
MW-44
04/11/07 ROL 21 BDL SOL SOL SOL BDL BDL BOL 2 SOL SOL SOL BDL SOL BDL SOL 0 2
MW-46
09113/07
BDL
BDL
BDL
SOL
SOL
BOL
BDL
SOL
BDL
0
BDL
BDL
SOL
BDL
SOL
SOL
BDL
0
0
06105108
1,2
SOL
SOL
BDL
SOL
SOL
SOL
SOL
SOL
1
BDL
SOL
ROL
BDL
SOL
SOL
SOL
0
1
W05108
1.2
BDL
BDL
SOL
ROL
BDL
SOL
SOL
SOL
1
601-
BDL
BDL
SOL
SOL
BDL
SOL
0
1
091041o'
BDL
BDL
BDL
BDL
BDL
BDL
SOL
BOL
SOL
0
SOL
BDL
SOL
SOL
SOL
SOL
RUL
0
0
01,05*9
1,4
12
BDL
BOL
BDL
BDL
SOL
SOL
BOL
3
SOL
SOL
BOL
SOL
SOL
SOL
BDL
❑
3
03/05/09
1.3
SOL
BDL
BOL
BDL
BDL
SOL
BDL
SOL
1
SOL
SOL
SOL
BOL
SOL
BOL
BDL
0
1
Notaa:
All unis measured to NgIL
SOL - Below Detection Limns
NCGS 2L Sid - North Carolina Groundwater Standard
BOLO - Concentration axooeds the 2L Groundwater Quality Standard
MTBE - Methyl-1eS butyl ether
97746 [ GS009RO22
Copyright 2009 Klarntelder Page 4 of 4 April 17, 2009
TABLE 5: ESTIMATED DISSOLVED HYDROGEN CONCENTRATIONS AT INJECTION WELLS
Well ID
Total Depth
(feet TOC)
TOC Elevation
(feet)
Bottom
Elevation (feet)
Date Water
Level Checked
Static Water
Level
(feet TOC)
Groundwater
Elevation (feet)
Depth of Water
(feet)
Estimated
Dissolved
Hydrogen
Concentration
(ppm)
MW-7
29.9
861.19
831.29
03/05/09
5.82
855.37
24.08
2.7
MW-10
33.6
860.36
826.76
03/05/09
7.16
853.20
26.44
2.8
MW-14❑
41.0
859.26
818.26
03/05/09
18.80
840.46
22.20
2.6
MW-15
25.2
857.71
832.51
03/05/09
12.08
845.63
13.12
2.2
MW-16
35.2
863.60
828.40
03/05/09
27.95
835.65
7.25
1.9
MW-23D
571
860.90
803.80
03/05/09
15.26
845.64
41.84
3.6
MW-24
58.8
858.81
800.01
03/05/09
20.40
838.41
38.40
3.4
MW-29
18.8
861.13
842.33
03/05/09
4.28
856.85
14.52
2.3
MW-34
21.0
860.45
839.45
03/05/09
well flooded
---
---
---
MW-43D
53.0
865.47
812.47
03/05/09
29.62
835.85
23.38
2.7
Notes:
feet TOC = feet below top of well casing
ppm = parts per million
Hydrogen concentrations are estimated based on a saturated hydrogen content of 1.6 ppm per atmosphere.
97746 1 GS009R022
Copyright 2009 Kleinfelder Page 1 of 1 April 17, 2009
TABLE 6: ESTIMATED HYDROGEN CONSUMPTION
Date Water
Original
Cylinder
Estimated Volume
Estimated Date
Date Hydrogen
Level and
Days Elapsed
Average Hydrogen
Injection
Cylinder
Pressure on
of Hydrogen
Cylinder Must be
Cylinder
Cylinder
Since Cylinder
Use per Day
Well ID
Pressure
3127109
Remaining (cubic
Changed Based on
Installed
Pressure
Installation
(psi/day)
�pstf
(psi)
feet]
Pressure
Recorded
MW-7
03/27/09
2,000
03/27/09
2,000
191
0
27.3
06/04/09
MW-10
02/11/09
1,500
03/27/09
900
115
44
13.6
05/24/09
MW-14❑
03/27/09
1.700
03/27/09
1,700
191
0
19.1
06/18/09
MW-15
01/30/09
1.900
03/27/09
1,300
131
56
10.7
07/17/09
MW-16
03/27/09
1.900
03/27/09
1,900
191
0
15.0
07/25/09
MW-23D
03/27/09
1.900
03/27/09
1.900
191
0
36.8
05/14/09
MW-24
03/27/09
2,000
03/27/09
2.000
191
0
17.1
07/16/09
MW-29
01 /30/09
1.900
03/27/09
1.000
101
56
16.1
05/22/09
MW-34
03/27/09
2.000
03/27/09
2,000
191
0
22.1
06/20/09
MW-43D
02/11/09
1.900
03/27/09
1.000
101
44
20.5
05/10/09
Notes:
psi = pounds per square inch
All hydrogen cylinders must be replaced prior to the cylinder pressure tailing below 50 psi.
97746 1 GS009RO22
Copyright 2009 Kleinfelder Page 1 of 1 April 17, 2009
FIGURES
a
.�7i wl V
�+II T P • i
dsh' ip.Ch :
A.
sss aae
qw goo
• • � -- — I' �Gas'Eline�• 4 r '� V II ■
`.. �.
Ga8ornes � ..
aso
,'� � _ • � sa Ch J
MIA
f , `*� •if_.
• liSJ y'� !
4 -� ■ + 5
FIGURE 1
SITE LOCATION MAP
KL EINFEL DER GFdena
730Q West Friendly Avenue
Bright People. Right Solutions. Greensboro, North Carolina
APPRCVEDBY
313 GALLIMORE DAIRY ROAD DATE 4-14-2009 SCALE. 1" = 2.000
GREENSBORO, NORTH CAR OLINA
PHONE: 336.668.0093 SOURCE VSGS 7.5 TOPOGRAPHIC MAP.
GUILFORD QUADRANGLE C44, PROJECT NO: 97746
M W-45
4
r MW-42
MW-12D
MW-12
MW-14 SUf3
MW-25 TATIQ
R _ ATER
TANK
4�MW-41 N 1 MW-130
MW-40 ❑ MW-ii MW-13 LL
RVV-3
RW-2
AV
a�
MW-28
RW-4 MW-32
MW-31
L
W-33
MW-2 MW-30
M W-44
EXISTING
PARKING
EXISTING
PARKING
EXISTING
BUILDING
LEGEND
INJECTION WELL LOCATION
MW-94 MONITORING WELL LOCATION � FIGURE 2
SITE PLAN
❑ RW-3 RECOVERY WELL LOCATION
� rL EINFEL E►4 Friendly
7300 West Friendly Avenue
Bright People. Right Solutions. Greensboro, North Carolina
APPROVED BY
313 GALLIMORE DAIRY ROAD WE 4-54-2009 SCALE I" = IN'
GREENSOOR0. NORTH CAROLINA
PHONE. 336 668.0093
DRAWN 8Y CWk PROJECT NO 97746
835
4MW-45
834.50
835
840
rv, �ti
836.65
v, �ti• :: ;
835.86
845
MW-42 :.� V..Vv
Mw-1xD
835.95 838.41 845.63
845.21
MW-12
MW44
MW-25 >�
847.33
840
84167
838.64
sue
TATIO
840
- ATER
8
T
MW-41
Mrir +u 1
Mw-13D
853.62 Q
853.20
847.47
845
MIN-40
W-3
MW-11
MW-13
851.09 W-2 MVv � ❑
855.37
4
846.45 f
847.19
85or")
845
845.64
MW-34 1,61
MW 2-
7
856.88 mr MW-28
853.50
RW-4
850
MW-32
845
852,49
MW-31—/ 850
Mw-33*
846.94
850.99
M W -30
855
855
849.45
MW-27
_
849,61
r
lit W -44
EXISTING
PARKING
LEGEND
EXISTING
i
INJECTION WELL LOCATION AND
EXISTING
PARKING
855.37
GROUNDWATER ELEVATION
BUILDING
MW-14
MONITORING WELL LOCATION AND
841.67
GROUNDWATER ELEVATION
❑ RW-7
RECOVERY WELL LOCATION
842_,,,
GROUNDWATER CONTOUR LINE
NOTES -
GROUNDWATER ELEVATIONS WERE RECORDED MARCH 5, 2009
MONITORING WELLS MW-13D, MW-23D. AND MW-25 ARE SCREENED
BELOW THE WATER TABLE AND WERE NOT USED TO GENERATE
THE GROUNDWATER CONTOURS.
EXISTING
PARKING
LEGEND
i MW-7 INJECTION WELL LOCATION
MW-14
MONITORING WELL LOCATION WITH
30
TOTAL VOCs CONCENTRATION (ug/L)
❑ RW-3
RECOVERY WELL LOCATION
1.000_^
TOTAL VOCs ISOCONCENTRATION LINE
NOTE
SAMPLES COLLECTED ON MARCH 5 AND 27. 2009
A
MW-42
3
37
M W-12
MW-12D
M W-1 'ti
32 MW-25
90 TATI
1 ATER
TANK
BUL
MW-41 F i
12 U7 1 MW-13D 1
10,000 RW-3 � 31 MW-13
122
M W-i 1 � MW-40 3A,
R W-2 2,791
1,00 369
100
OL
MW-31 -MW^28 I
EXISTING
BUILDING
MW-30 MW-44
EXISTING
PARKING
EXISTING
PARKING
1 8DL
ti
12 M 3 -42
1 . Q00 M W-12D
Af
r,t :
MW-1 1.71fi4 Mw-12
32 MW-25 sus
BS ATE❑
.12 ATE
TANK mFl BDL
' MW-13d
MW-41 AIF 19
,&RW-3 mw-13
MW�O
MW-T 1 119
DL 3
RW-2 935
} 194
MW-34 r.
M W-28
RW-4
M W-31
-33
W-32 MW
Mw-2 �►
LEGEND
'S MW-7 INJECTION WELL LOCATION
MW-14 MONITORING WELL LOCATION WITH
30 TOTAL CHLORINATED HYDROCARBONS CONCENTRATION (ug/L)
❑ RW-3 RECOVERY WELL LOCATION
r, r, TOTAL CHLORINATED HYDROCARBONS ISOCONCENTRATION LINE
NOTE:
SAMPLES COLLECTED ON MARCH 5 AND 27, 2009
EXISTING
BUILDING
MW-30
M W-44
EXISTING
PARKING
x Pace Analytical Services, Inc. Pace Analytical Services, Inc.
zfflaeeAnalytical 2225 Riverside Or 9800 KinCey Ave. Suite 100
www.pace;abs.com Asheville, NC 28804 Huntersville, NC 28078
(828)254.7178
March 20, 2009
Ms. Gail Licayan
Trigon/Kleinfelder, Inc.
313 Gallimore Dairy Rd
Greensboro, NC 27409
RE: Project: Gilbarcc 042-08-018
Pace Project No. 9239387
Dear Ms. Licayan:
Enclosed are the analytical results for sample(s) received by the laboratory on March 06, 2009. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable. unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie McKee
bonnie. m ckee@paceia bs. corn
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent or Pace Analytical services, irnc..
(704)875-9092
Page 1 of 18
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
- la eAnal �[ral 2225 Riverside [)r 9600 KinceyAve. Suite 100
www-pacelabs.com Asheville, NC 28804 Huntersvifle, NC 28078
(828)254-7176 (704)875-9092
Projecl: Gilbarco 042-08-018
Pace Project No.: 9239387
Charlotte Certification IDS
West Virginia Certification #: 357
Virginia Certfication #: 00213
Tennessee Certification #: 04010
South Carolina prinking Water Cart. #: 990060003
South Carolina Certification #- 99DO60001
Pennsylvania Certification #: 68-00784
Connecticut Certification # PH-0104
Asheville Certification IDs
West Virginia Certification #: 356
Virginia Certification #: 00072
Connecticut Certification #: PH-0106
Florida/NELAP Certification #: E87548
Tennessee Certification #: 2980
South Carolina Certification #: 99030001
South Carolina Bioassay Certification #: 99030002
Eden Certification IDS
North Carolina Wastewater Certification #- 633
Virginia Drinking Water Certification #- 00424
CERTIFICATIONS
North Carolina Field Services Certification # 5342
North Carolina Drinking Water Certification #: 37706
New Jersey Certification #- NC012
Louisiana/LEtAP Certification #: 04034
Kentucky UST Certification #. 84
Florida/NELAP Certification # E87627
North Carolina Wastewater Certification # 12
Pennsylvania Certification #: 68-03578
North Carolina Wastewater Certification # 40
North Carolina Drinking Water Certification #: 37712
North Carolina Bioassay Certification #: 9
New Jersey Certification # NCO11
Massachusetts Certification # M-NC030
LouisianalLELAP Certification #: 03096
North Carolina Drinking Water Certification #: 37738
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
without the written consent of PaCe Analytical Services, Inc.
ir
Page 2 of 18
q.
aceAnalytrcal
wrrw.pacelabs.c=
Pace Analytical Services, Inc.
2225 Riverside ❑r
Asheville, INC 28804
t828y254-7176
Pace Analytical Services, Inc.
9800 Kmcey Ave. Suite 100
Huntersvifle, NC 28078
(704)875.9092
Project: Gilbarco 042-08-018
Pace Project Na 9239387
SAMPLE SUMMARY
Lab ID
Sample ID
Matrix
date Collected
Date Received
9239387001
MW-7
Water
03105r0915-10
03105/0915.00
9239387002
MW-11
Water
03/05/09 09:43
03/06/09 15.00
9239387003
MW-13
Water
03/05/09 09:45
03/06/09 15:00
9239387004
MW-13D
Water
03/05/09 09:08
03/06/09 15:00
9239387005
MW-14
Water
0310510914-50
03106/0915-00
9239387006
MW-23D
Water
03/05/09 09:32
03/06/09 15:00
9239387007
MW-24
Water
03/05/09 15:03
03/06/09 15
00
9239387008
MW-25
Water
03/05/09 14:46
03/06/09 15
00
9239387009
MW-42
Water
03/0510911:04
03/0610915:00
9239387010
MW-45
Water
03105/0911:11
03/0610915.00
REPORT OF LABORATORY ANALYSJS
This report shall not be reproduced, except in full.
without the written consent of�Pace
,Analytical Services. inc
Page 3 of 18
e. Pace Analytical Services, Inc. Pace Analytical Services, Inc,
aeeAnalytieal 2225 Riverside dr. 9800 Kincey Ave. Suite 100
wwwpacePabs.mm Asheville, NC 28804 Huntersville, NC 2HO75
(828)254-7176 (704)875-9092
SAMPLE ANALYTE COUNT
Project: Gilbarco 042-08-018
Pace Project No.. 9239387
Analytes
Lab ID
Sample I❑
Method
Analysts
Reported
9239387001
MW-7
EPA 6 01160 2
DHW
40
9239387002
MW-11
EPA 6011602
DHW
40
9239387003
MW-13
EPA 601 /602
DHW
40
9239387004
MW13D
EPA 6011602
DHW
40
9239387005
MW-14
EPA601/602
DHW
40
9239387006
MW-23D
EPA601/602
❑HW
40
9239387007
MW-24
EPA601/602
DHW
40
9239387008
MW-25
EPA601/602
DHW
40
9239387009
MW-42
EPA 6011602
DHW
40
9239387010
MW-45
EPA 6011602
DHW
40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
Page 4 of 18
www.pacela6tmm
Project: Gllbarco 042-08-018
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 29804
(828)254-7176
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersviile, NC 28078
(704)875-9092
Pace Protect No.: 9239387
Sample: MW-7 Lab ID:/3239387001 Collected: 03/05/09 15:10 Received: 03/06/09 15:00 Matrix. Water
Report
Parameters Results Units Limit MDL ❑F Prepared Analyzed CAS No. Dual
6011602 Volatiles Analytical Method: EPA 601/602
Benzene
NO ug/L
50.0
50.0
50
03/19/09 11:42
71-43-2
Bromodichloromethene
ND ug/L
50.0
50.0
50
03119/09 11:41
75-27-4
Bromoform
ND ug/L
50.0
50.0
50
03119/0911,41
75-25-2
Bromomethane
NO ug/L
50.0
50.0
50
03/19/09 11 Al
74-83-9
Carbon tetrachloride
NO ug/L
50.0
50.0
50
03/19/09 11:41
56-23-5
Chlorobenzene
NO ug/L
50,0
50.0
50
0311 9/09 11:41
108-90-7
Chloroethane
NO uglL
50.0
50.0
50
03/19/09 11:41
75-00-3
Chloroform
NO ug1L
50.0
50.0
50
03/19/09 11:41
67-66-3
Chloromethane
NO ug/L
100
100
50
03/19/09 11:41
74-87-3
Dibromochlaromethane
ND ug/L
50.0
50.0
50
0311910911,41
124-48-1
1,2-Dibromoethane (EDB)
ND ug1L
50.0
50.0
50
03/19/09 11 Al
106-93-4
1,2-Dichlorobenzene
NO ug/L
50.0
50.0
50
03/19/09 11:41
95-50-1
1,3-Dichlorobenzene
NO ug/L
50.0
50.0
50
03119/0911.41
541-73-1
1.4-Dichlorobenzene
NO ug/L
50.0
50.0
50
03/19/09 11 Al
106-46-7
❑ichlorodifluoromethane
NO ug/L
50.0
50.0
50
03/19/09 11:41
75-71-8
1,1-Dichloroethane
NO ug/L
50-0
50A
50
03/19/09 111-41
75-34-3
1,2-Dichlorcethane
NO ug/L
50.0
50.0
50
03/19/09 11:41
107-06-2
1,1-Dichloroethene
NO ug/L
50.0
50.0
50
03/1910911:41
75-35-4
cis- 1,2-DthIoroethene
935 ug/L
50.0
50.0
50
03/19/09 1141
156-59-2
trans-1,2-Dichloroethene
ND ug/L
50.0
50.0
50
0311910911-41
156-60-5
1,2-Dichloropropane
N❑ uglL
50.0
50.0
50
0311910911:41
78-87-5
cis- 1,3-DichIoropropene
ND uglL
50.0
50.0
50
0311910911Al
10061-01-5
trans-1,3-Dichtoropropene
NO ug/L
50.0
50.0
50
03/79/0911,41
10061-02-6
Diisopropyl ether
NO ug/L
50.D
50.0
50
03119/0911,42
108-20-3
Ethylbenzene
749 ug/L
50.0
50.0
50
03/19/09 11:42
100-41-4
Methylene Chloride
NO ug/L
100
100
50
03/19/09 11:41
75-09-2
Methyl-tert-butyl ether
NO ug/L
50.0
50.0
50
03/19/09 11:42
1634-04-4
Naphthalene
384 ug/L
100
100
50
03119109 11:42
91-20-3
1.1.2,2-Tetrachloroethane
N❑ uglL
50.0
%0
50
03/19/09 11:41
79-34-5
Tetrachloroethene
NO uglL
50.0
50.0
50
03/19/09 11:41
127-18-4
Toluene
NO ug/L
50.0
50.0
50
03119/09 11:42
108-88-3
1,1,1-Trichloroethane
ND ug/L
50.0
50.0
50
0311910911:41
71-55-6
1,1,2-Trichloroethane
NO ug/L
50.0
50.0
5D
03/19/09 11:41
79-00-5
Trichloroethene
NO ug/L
50.0
50.1)
50
0311910911:41
79-01-6
Tdchlo►ofluaromethane
NO ug/L
50.0
50.0
50
03/19/09 11:41
75-69-4
Vinyl chloride
ND ug/L
50.0
50.0
50
03/19/09 11:41
75-01-4
Xylene (Total)
723 ugIL
100
100
50
03/19/09 11 A2
f 330-20-7
m&p-Xylene
723 ug/L
100
100
50
03/19/09 11:42
1330-20-7
o-Xyiene
NO ug/L
50.0
50.0
50
03/19/09 11:42
95-47-6
1-Chioro-3-fluorobenzene (S)
125 %
65-137
50
03/19/09 11:41
625-98-9
Date: 03/20/2009 04:43 PM REPORT OF LABORATORY ANALYSIS Page 5 of 18
This report shall not be reproduced, except in Tull,
without the written consent of Pace Analytical Services, Inc..
s Pace Analytical Services, Inc. Pace Analytical Services, Inc.
lace Analytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
wwwpaa43b,s.wm Asheville. NC 28804 Huntersville, NC 28078
(828)254-7176 (704)875-9092
ANALYTICAL RESULTS
Project: Gil barco 042-0M18
Pace Project No,: 9239387
Sample: MW 11 Lab Id: 9239387002 Collected: 03105/09 09:43 Received: 03/06/09 15:00 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
6011602 Volatiles Analytical Method: EPA 6011602
Benzene
ND uglL
1.D
1.0
1
03/19/09 13:05
71-43-2
Bromodichloromethane
ND uglL
1.0
1.0
1
03/19/09 13:04
75-27.4
Bromoform
NO uglL
1.0
1 A
1
03/19/09 13:04
75-25-2
Bromomethane
NO uglL
1.0
1.0
1
03/19/09 13:04
74-83-9
Carbon tetrachloride
NO ug1L
1.0
1 A
1
03/19/09 13:04
56-23-5
Chlorobenzene
NO uglL
1.0
1.0
1
03119/0913:04
108-90-7
Chloroethane
NO ug1L
1.0
1.0
1
03/19/0913:04
75-00-3
Chloroform
NO uglL
1.0
1.0
1
03/1910913:D4
67.-66-3
Chloromethane
ND uglL
2.0
2.0
1
D311910913:04
74-87-3
Dibromochloromethane
NO uglL
1.0
1.0
1
03/19/09 13:04
124-48.1
1,2-Dibromoethane (EDB)
NO uglL
1.0
1.0
1
03/19/09 13:04
106-93-4
1,2-Dichlorobenzene
NO uglL
1.0
1.0
1
03/1910913:04
95-50-1
1,3-Dichlorobenzene
NO uglL
1.0
1.0
1
03119/0913:04
541-73-1
1 A-Dichlorobenzene
NO ug1L
1.0
1 A
1
03119/09 13:04
1 D646-7
❑ichlorodifiuoromethane
NO uglL
1.0
1.0
1
03119/0913:04
75-71-8
1,1-Dichloroethane
NO uglL
1.0
1.0
1
03/1910913:04
75-34-3
1,2-Dichloroethane
NO uglL
1.0
1.0
1
03/1910913:04
107.06-2
1,1-Dichloroethene
NO uglL
1.0
1.0
1
03119/0913:D4
75-35-4
cis-1,2-Dichloroethene
1.5 uglL
1.0
1.0
1
03/1910913-D4
156-59-2
trans-f ,2-Dichloroethene
NO ug/L
1 A
1-0
1
03/19/09 13:04
156-60-5
1,2-Dichloropropane
NO uglL
1.0
1.0
1
03/19/09 13:04
78-87-5
cis- 1,3-Dichloropropene
ND uglL
1.0
1.0
1
03/1910913:04
10061-01-5
trans-1,3-Dichloropropene
NO uglL
1.0
1.0
1
03/1910913:04
10061-02-6
Diisopropyl ether
NO uglL
1.0
1.0
1
03/19/09 13:05
1 o8-20-3
Ethyibenzene
NO uglL
1.D
1.0
1
03119/0913:05
1OD-41-4
Methylene Chloride
ND uglL
2.0
2.0
1
03/19/09 13:04
75-09-2
Methyl-tert-butyl ether
NO uglL
1.0
1.0
1
03/19109 13:05
1634-04-4
Naphthalene
ND uglL
2.0
2.0
1
03/1910913:05
91-20-3
1,1,2,2-Tetrachloroethane
ND uglL
1.0
1.0
1
0311910913:D4
79-34-5
Tetrachloroethene
1.3 uglL
1.0
1.0
1
03/19/09 13:04
127-18-4
Toluene
NO uglL
1.0
1.0
1
03/19/09 13:05
108-88-3
1,1,1-Trichloroethane
NO uglL
1.0
1.0
1
03/1910913:04
71-55-6
1.1,2-Trichloroethane
ND uglL
1.0
1.0
1
0311910913:04
79-00-5
Trichloroethene
NO ug1L
1.0
1.D
1
03/1910913:04
79-01-6
Trichlorofluoromethane
ND uglL
1.0
1.0
1
03/19/09 13:04
75-69-4
Vinyl chloride
NO ug1L
1.0
1.0
1
03/19/09 13:04
75-01-4
Xylene (Total)
NO uglL
2.0
2.0
1
03/19/09 13:05
1330-20-7
m&p-Xylene
NO uglL
2.0
2.0
1
03/19/09 13:05
1330-20-7
o-Xylene
NO uglL
1.0
1.0
1
03/19/09 13:05
95-47-6
1 -C h lo ro- 3-ftu o ro benze n e (S)
126 %
65-137
1
03/19/09 13:04
625-98-9
Date. 03/20/2009 04:43 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent
of Pace AnalyhcaI Services, Inc..
Page 6 of 18
N Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalytical 2225 Riverside Dr. H00 Kincey Ave. Suite 100
w wparwaosclom Asheville, NC 28804 Huntersviile. NC 28078
(828)254-7176 (704)875-9082
ANALYTICAL RESULTS
Project Gilbarco 042-08-018
Pace Project No.: 9239387
Sample: NW-13 Lab ID: 9239387003 Collected: 03/05/09 09745 Received: 03/06/09 15:00 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
601/602 Volatiles Analytical Method: EPA 6011602
Benzene
ND ug)L
2.5
2.5
2.5
03/19109 14:27
7143-2
Bromodichloromethane
ND uglL
2.5
2.5
2.5
03/19/09 14:26
75-27-4
Bromoform
NO uglL
2.5
2.5
2.5
0311910914:26
75-25-2
Bromornethane
ND uglL
2.5
2.5
2.5
D311910914:26
74-83-9
Carbon tetrachloride
NO uglL
2.5
2.5
2.5
03/19/09 14:26
56-23-5
Chlorobenzene
ND uglL
2.5
2.5
2.5
03/19/09 14:26
108-90-7
Chloroethane
N❑ uglL
2.5
2.5
2.5
03/1910914:26
75-00-3
Chloroform
NO ug1L
2.5
2.5
2.5
03/19/09 14:26
67-66-3
Chloramethane
NO uglL
5.0
5.0
2.5
03/19/09 14:26
74-87-3
❑ibromochloromethane
NO uglL
2.5
2.5
2.5
03/19/09 14:26
124-48-1
1,2-Dibromoethane (EDB)
NO uglL
2.5
2.5
2.5
03/19/09 14:26
106-93-4
1,2-Dichlorobenzene
NO uglL
2.5
2.5
2.5
03/19/09 1416
95-50-1
1,3-Dichlorobenzene
ND uglL
2.5
2.5
2.5
03/1910914:26
541-73-1
1,4-Dichlorobenzene
ND uglL
2.5
2.5
2.5
03/19/09 14:26
106-46-7
Dichlorod i8uoromethane
NO uglL
2.5
2.5
2.5
03/1910914:26
75-71-8
1,1-Dichloroethane
NO uglL
2.5
2.5
2.5
03/19/09 14:26
75-34-3
1,2-❑ichloraethane
NO uglL
2.5
2.5
2.5
0311910914:26
107-06-2
1,1-Dichloroethene
ND uglL
2.5
2.5
2.5
03/19/09 14:26
75-35.4
cis-1,2-Dichloroethene
119 uglL
2.5
2.5
2.5
03/19/09 14:26
156-59-2
trans-1,2-Dichloroethene
ND uglL
2.5
2.5
2.5
0311910914:26
156-60-5
1,2-Dichloropropane
ND uglL
2.5
2.5
2.5
03119/09 14:26
78-87-5
cis- 1,3-DichIoreprope ne
ND ug1L
2.5
2.5
2.5
03/19/09 14:26
10061-01-5
trans-1,3-❑ichloropropene
ND uglL
2.5
2.5
2.5
03/19/09 14.26
10061-02-6
Diisopropyl ether
ND uglL
2.5
2.5
2.5
03/19/09 14:27
108-20-3
Ethylbenzene
NO uglL
2.5
2.5
2.5
03/1910914:27
100-41-4
Methylene Chloride
NO ug1L
5.0
5.0
2.5
03/19/09 14.26
75-D9.2
Methyl-tert-butyl ether
3.1 uglL
2.5
2.5
2.5
03/19/09 14:27
1634-04-4
Naphthalene
ND uglL
5.0
5.0
2.5
0311910914:27
91-2D-3
1.1,2,2-Tetrachloroethane
ND uglL
2.5
2.5
2.5
03/1910914,26
79-34-5
Tetrachloroethene
ND uglL
2.5
2.5
2.5
031191D914.26
127-18.4
Toluene
NO uglL
2.5
2.5
2.5
03/19/09 14:27
108-88-3
1,1,1-Tdchloroethane
NO uglL
2.5
2.5
2.5
0311910914:26
71-55-6
1,1,2-Trichloroethane
NO uglL
2.5
2.5
25
03/19/09 14:26
79-00-5
Tdchloroethene
ND uglL
2.5
2.5
2.5
03/19/09 14:26
79.01-6
Trichlorofluoromethane
NO ug1L
2.5
2.5
2.5
03/19/09 1426
75-69-4
Vinyl chloride
NO uglL
2.5
2.5
2.5
03119J09 14,26
75-01-4
Xylene (Total)
NO uglL
5.0
5.0
2.5
03/19/09 14,27
133D-20-7
m&p-Xylene
NO ug&
5.0
5.0
2.5
03/19/0914-27
1330-20-7
o-Xylene
NO uglL
2.5
2.5
2.5
03/19/0914:27
95-47-6
1-Chloro-3-fluorobenzene (S)
105 %
65-137
2.5
03/19/09 14:26
625-98-9
Date: 03/20/2009 04:43 PM REPORT OF LABORATORY ANALYSIS Page 7 of 18
This report shall not be reproduced. except in full,
without the written con sent
of�Pare
..Ana lytical Services, Inc.
J�4
m Pace Analytical Services, Inc, Pace Analytical Services, Inc.
aceAnalXical 2225 Riverside Dr. 980o KinceyAve. Suite 1 oo
WWWpavelabxmm Asheville, NC 28B04 Huntersvi4e, NC 2807E
(828)254-7178 (704)875.9092
ANALYTICAL RESULTS
Project: Gilbarco 042-08-018
Pace Project No.: 9239387
Sample- MW-130 Lab ID: 9239387004 Collected; 03/05/09 09:08 Received- 03/06/09 15:00 Matrix: Water
Report
Parameters Results Units Limit MDL ❑F Prepared Anatyzed CAS No. Qual
601/602 Volatiles
Benzene
Bromodich loromethane
Bromofomn
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
D i bromo ch lorometh a n e
12-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Di ch I orod ifl uo romettl a ne
1,1-Dichloroethane
1,2-Dichloroethane
1, 1 -Di ch lo roethene
cis- 1,2-Dichloroethene
trans-1,2-Dichloroethene
1, 2-Dichloropropane
cis-1,3-Dichloropropene
trans-1 ,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
1,1,22-Tetrachloroethane
Tetra ch lo roethene
Toluene
1,1,1-Trichloroethane
1,1,2-Thchloroethane
Trichloroethene
Trich to roftuo ro meth an e
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
1-Chloro-3-fluorobenzene (S)
Date: 03/20/2009 04:43 PM
Analytical Met had: EPA 6 01160 2
ND ug/L
1.0
1.0
1
03/19/09 15:09
71-43-2
ND ug/L
1.0
1.0
1
03/19/09 15:08
75-274
ND ug/L
1.0
1.0
1
03/1910915:08
75-25-2
NO ug/L
1.0
1,0
1
03119M915:08
74-83-9
NO ug/L
1.D
1.0
1
03/1910915:08
56-23-5
NO uglL
1.0
1.0
1
03/19M 15:08
108-90-7
ND uglL
1.0
1.0
1
03119/0915:08
75-00-3
NO ug/L
1.0
1.0
1
0311910915:08
67-68-3
NO ug/L
2.0
2.0
1
03/19/09 15:08
74-87-3
NO ug/L
1.0
1.0
1
03/19/09 15:08
124-48-1
NO ug/L
1.0
1.0
1
0311910915:08
106-93-4
NO ug1L
1.D
1.0
1
D3/19/0915:08
95-50-1
NO uglL
1.0
1.0
1
03/19/09 15:08
541-73-1
N❑ uglL
1.0
1.0
1
03/19/09 15:o8
106-46-7
NO ug/L
1.0
1.0
1
0311910915:08
75-71-8
NO ug/L
1.0
1-0
1
03119/0915:08
75-34-3
NO ug/L
1.0
1.0
1
03/19/09 15:08
107-06-2
NO ug/L
1.0
1.0
1
03/1910915-08
75-35-4
14.6 ug/L
1.0
1.0
1
031191D9 15:08
156-59-2
N❑ ug/L
1.0
1.0
1
03/19/09 15:08
156-60-5
NO ug/L
1.0
1.0
1
03/19/09 15:08
78-87-5
NO ug/L
1.0
1.0
1
03/19/09 15:08
10061-01-5
NO ug/L
1-0
1.0
1
03119/0915:08
10061-02-6
NO ug/L
1.0
1 A
1
03119/09 15:09
108-20-3
ND uglL
1.0
1.0
1
03/19/09 15:09
100-41-4
N❑ ug/L
2.0
2.0
1
03/19/09 15:08
75-09-2
13.4 ug/L
1.0
1.0
1
03/19/09 15:09
1634-04-4
NO ug/L
2.0
2.0
1
03/19109 15:09
91-20-3
NO ug/L
1.0
1.0
1
03/19/09 15:08
79-34-5
NO ug/L
1.0
1.D
1
03/1910915:08
127-18-4
NO ug/L
1.0
1.0
1
03/1910915:09
108-88-3
ND ug/L
1.0
1.0
1
03/19/09 15:08
71-55-6
NO ug/L
1.0
1-0
1
03/19/09 15:08
79-00-5
NO ug/L
1.D
1.0
1
03/19/09 15:08
79-01-6
NO ug/L
1.0
1.0
1
03/19/09 15:08
75-69-4
3.4 ug/L
1.0
1.0
1
03/19/09 15:08
75-01-4
NO ug/L
2.0
2,0
1
03/19/0915:09
1330-20-7
ND ug/L
2.0
2.0
1
03)19109 15:09
1330-20-7
NO uglL
1.0
1.0
1
03119/09 15:09
95-47-6
127 %
65-137
1
03119/09 15:08
625-98-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page 8 of 18
; laceAnaiXkal
www.pacelabsrorn
Project: Gilbarco 042-08-018
Pace Analytical Services. Inc.
2225 Riverside Dr
Asheville, NC 2 88 04
(828)254.7176
ANALYTICAL RESULTS
Pace Analytical Services, Inc,
98DO Kincey Ave. Suite 100
Huntersville, NC 28078
(704)675-9092
Pace Project No.: 9239387
Sample: MW-14 Lab ID: 9239387005 Collected: 03/05/09 14:50 Received: 031D6109 15.00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No Qual
6011602 Volatiles Analytical Method: EPA 6011602
Benzene
ND ug/L
1.0
1.0
1
03/19/09 15.50
71-43-2
Bromodichloromethane
ND ug/L
1.0
1.0
1
03/19/09 15.50
75-27-4
Bromoform
ND uglL
1.0
1.0
1
03/1910915:50
75-25-2
Bromomethane
ND ug1L
1 0
1.0
1
03/19/09 15:50
74-83-9
Carbon tetrachloride
ND uglL
1.0
1.0
1
03/19/09 15:50
56-23-5
Chlorobenzene
ND ug/L
1.0
1.0
1
03/19/09 15:50
108.90-7
Chloroethane
ND uglL
1.0
1.0
1
03/19/09 15:50
75-00-3
Chloroform
N❑ ug1L
1.0
1.0
1
03/19/09 15:50
67-66-3
Chloromethane
ND uglL
2.0
2.0
1
03/19/09 15:50
74-87-3
Dibromochloromethane
ND uglL
1.0
1.0
1
03/19/09 15:50
124-48.1
1,2-Dibromoethane (EDB)
ND uglL
1.0
1.0
1
03/19/09 15:50
106-93-4
1,2-Dichtorobenzene
ND ugIL
1 0
1.0
1
03/19109 15750
95-50-1
1,3-Dichlofobenzene
ND ug/L
1.0
1.0
1
03/1910915:50
541-73-1
1,4-DichIOrobenzene
ND ug/L
1.0
1.D
1
03/19/0915:50
106.46-7
D i ch to rod M u o ro metha ne
ND uglL
1.0
1.0
1
0311910915:50
75-71-8
1,1-Dichloroethane
ND ug1L
11,01
1.0
1
03/19/09 15:50
75-34-3
1,2-Dichloroethane
ND uglL
1.0
1.0
1
03/19/0915,50
107-05-2
1.1-Dichloroethene
ND uglL
1.0
1.0
1
03/19/09 15:50
75-35-4
cis-1,2-Dichloroethene
ND ug1L
1.0
1.0
1
03119/09 15:50
156-59-2
trans-1.2-Dichloroethene
ND ug1L
1.0
1.0
1
03/19/09 15:50
156-60-5
1,2-Dichloropropane
ND ug1L
1.0
1.0
1
03119/09 15:50
78-87-5
cis-1.3-DichIoropropene
ND ug/L
1.0
1.0
1
03/19/09 15:50
10061-01-5
trans 1 3-❑ichloropropene
ND ug/L
1.0
1.0
1
03/19/09 15:50
10061-02-6
Diisopropyl ether
ND ug1L
1.0
1.D
1
03/19/09 15:50
108-20-3
Ethylbenzene
ND uglL
1.0
1.0
1
03/19/09 15:50
100-41-4
Methylene Chloride
ND uglL
2.0
2.0
1
03/19/09 15:50
75-09-2
Methyl-tert-butyl ether
ND uglL
1.0
1.0
1
03/19/09 15:50
1634-044
Naphthalene
ND ug/L
2.0
2.0
1
03/19/09 15:50
91-20-3
1,1,2,2-Tetrachforoethane
ND ug1L
1.0
1.0
1
03/19/09 15:50
79-34-5
Tetrachloroethene
32.0 ug1L
1.0
1.0
1
D311910915:50
127-18-4
Toluene
ND ug/L
1.0
1.0
1
03119M915:50
108-88-3
1. 1, 1 -Trich lo roet h a ne
ND uglL
1.0
1.0
1
03/19/09 15 50
71-55-6
1,1,2-Trichioroethane
ND uglL
1.0
1.0
1
D311910915,50
79-00-5
Tfichloroethene
ND uglL
1.0
1.0
1
0311910915:50
79-01-6
Trichlorofluoromethane
ND uglL
1.0
1.0
1
031t9109 15:50
75-69-4
Vinyl chloride
ND uglL
1.0
1.0
1
03/19/09 15,50
75-01-4
Xylene (Total)
ND ug/L
2 0
2.0
1
03/19/09 15:50
1330-20-7
m&p-Xyiene
ND ug1L
2.0
2.0
1
03/19/09 15:50
1330-2D-7
o-Xylene
ND uglL
1.0
1.0
1
03/19/0915:50
95-47-6
1-Chlore-3-ffuorobenzene (S)
142 %
65-137
1
03/19/09 15:50
625-98-9 50
Date: 03/20/2009 04:43 PM REPORT OF LABORATORY ANALYSIS Page 9 of 18
This report shall not be reproduced, except in full,
without the written consent of Pare Analytical Services, Inc..
A Pace Analytical Services, Inc. Pace Analytical Services, Inc.
ceAnalj&cal 2225 Riverside dr. 9800 IGncey Ave. Suite 100
wn,N,paoeWs Gam Asheville, NC 28804 Huntersville, NC 28078
(829)254-7176
(704)875-9092
ANALYTICAL RESULTS
Project: Gilbarco 042-08-018
Pace Project No.: 9239387
Sample: MW-23D Lab ID: 9239387006 Collected: 03/05/09 09:32 Received: 03/06/09 15:00 Matrix: Water
Report
Parameters
Results Units
Limit
MDL
❑F
Prepared Analyzed
CAS No.
601/602 Voiatiles
Analytical Method: EPA 6011602
Benzene
1.7 uglL
1.0
1.0
1
03/19/09 16:31
71-43.2
Bromodichioromethane
NO uglL
1.0
1.0
1
03/19/09 16:31
75-27-4
Bromoform
ND uglL
1.0
1.0
1
03/19/09 16:31
75-25-2
Bromomethane
NO ug1L
1.0
1.0
1
03/1910916:31
74-83-9
Carbon tetrachloride
NO ug1L
1.0
1.0
1
03119/09 16:31
56-23-5
Chlorobenzene
NO uglL
1.0
1.0
1
0311910916:31
108-90-7
Chloroethane
NO uglL
1.0
1.0
1
0311 GIM9 16:31
75-00-3
Chloroform
ND uglL
1.0
1.0
1
03/19/09 16:31
67-66-3
Chloromethane
NO uglL
2.0
2.0
1
03/19/09 16,31
74-87-3
Dibromochloromethane
NO ug1L
1.0
1.0
1
03/19109 16:31
124-48-1
1,2-Dibromoethane (EDB)
NO uglL
1.0
1.0
1
03/19/09 16:31
106-934
1,2-Dichlorobenzene
ND uglL
1.0
1.0
1
03/19/09 16:31
95-50-1
1,3-Dichlorobenzene
NO uglL
1.0
1 A
1
03/19/09 16:31
541-73-1
1,4-Dichlorobenzene
ND uglL
1.0
1.0
1
03/19/09 16:31
106-46-7
DichiorodMuoromethane
ND uglL
1.0
1.0
1
03/19/09 16:31
75-71-8
1,1-Dichloroethane
1.1 uglL
1.0
1.0
1
03119/0916:31
75-34-3
1,2-Dichloroethane
ND uglL
1.0
1.0
1
03/19/09 16:31
107-06-2
1,1-Dichloroethene
NO uglL
1.0
1.0
1
0311910916:31
75-35-4
cis- 1.2-Dichloroethene
173 ug1L
1.0
1.0
1
03/19/09 16:31
156-59-2
trans-1,2-Dichloroethene
ND ug1L
1.0
1.0
1
03/19/09 16:31
156-60-5
1,2-Dichloropropane
NO ug1L
1.0
1.0
1
03/19/09 16,31
78-87-5
cis-1,3-Dichloropropene
N❑ ug1L
1.0
1.0
1
03/19/09 16:31
10061-01-5
trans-1,3-Dichloropropene
ND uglL
1.0
1.0
1
03/19/09 16,31
10061-02-6
Diisopropyt ether
NO uglL
1.0
1.0
1
03/19109 16:31
108-20-3
Ethylbenzene
ND uglL
1.0
1.0
1
03/19/09 16:31
100-41-4
Methylene Chloride
NO uglL
2.0
2.0
1
03/19/09 16:31
75-09-2
Methyl-tert-butyl ether
194 uglL
1 A
1.0
1
03/19/09 16:31
1634-04-4
Naphthalene
NO uglL
2,0
2.0
1
03119/0916:31
91-20-3
1,1.2,2-Tetrachtoroethane
ND uglL
1.0
1.0
1
03/19/09 16:31
79-34-5
Tetrachloroethene
NO uglL
1.0
1.0
1
03/19/09 16:31
127-18-4
Toluene
ND ug1L
1.0
1.0
1
0311910916:31
108-88-3
1,1,1-Trichloroethane
ND uglL
1.0
1.0
1
03/1910916:31
71-55-6
1,1,2-Trichloroethane
ND ug1L
1.0
1.13
1
03/1910916.31
79-00-5
Trichloroethene
ND uglL
1.0
1.D
1
03/1910916:31
79-01-6
Trichloroiluoromethane
NO uglL
1.0
1.0
1
0311910916.31
75-69-4
Vinyl chloride
19.4 ug1L
1.0
1.0
1
03/19/09 16:31
75-01-4
Xylene (Total)
N❑ uglL
2.0
2.0
1
03/19/09 16:31
1330-20-7
m&p-Xylene
NO uglL
2.0
2.0
1
03/19109 16:31
1330-20-7
o-Xylene
NO ug1L
1.0
1.0
1
03/19/09 16.31
95-47-6
1-ChIoro-3-fluorobe nzene (S)
115 °%
65-137
1
03/19/09 16:31
625-98-9
E
Qual
Date: 03/20/2009 04 43 PM REPORT OF LABORATORY ANALYSIS Page 10 of 18
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
c Pace Analytical Services, Inc. Pace Analytical Services, Inc.
IaXAnalytical 2225 Riverside Dr. 9800 ttincey Ave. Suite too
www Qacpiaas mm Asheville, NC 28804 Huntersville, NG 28078
(828)254-7178 (704)875-9092
ANALYTICAL RESULTS
Project: Gilbarco 042-08.018
Pace Project No.: 9239387
Sample: MW-24 Lab ID: 92393870D7 Collected: 03/05/09 15:03 Received: 03/06/09 15:00 Matrix: Water
Report
Parameters Resu{ts Units Limit MDL DF Prepared Analyzed CAS No. Llual
6011602 Volatiles
Benzene
Br omod ich l orometh ane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chioroethane
Chloroform
Chloromethane
D ib romoch iorometh a n e
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
D ich lorod if f u o rom eth a n e
1,1-Dichloroethane
1,2-Dichloroethene
1, 1 -Dichloroethene
cis-1,2-Dichloroethene
trans-1, 2-0ichloroethene
1.2-Dichloropropane
cis-1,3-D ich I o rop ro pen e
trans-1 ,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Tdchloroethane
1,1,2-Trichloroethane
Trich loroethene
Trich io rofl u o ro metha n e
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
1 -C h I oro-3 A u o robenze n e (S)
Date: 03/20/2009 04:43 PM
Analytical Method: EPA 6011602
117 uglL
50,0
50.0
50
03/191091712
71-43-2
NO uglL
50.0
50.0
50
03/19/09 17:12
75-27-4
NO uglL
50.0
50.0
50
03/19/09 17:12
75-25-2
NO uglL
50.0
50.0
50
03/19/09 17:12
74-83-9
NO uglL
50.0
50.0
50
03/19/09 17:12
56-23-5
ND uglL
50.0
50.0
50
03/19/091T12
108-90-7
ND ug1L
50.0
50.0
50
031191D9 17:12
75-00-3
NO uglL
50.0
50.0
50
03/19/09 17:12
67-66-3
NO ug1L
100
100
50
03/19/09 17,12
74-87-3
ND uglL
50,0
50.0
50
03/19/09 17:12
124-48-1
ND uglL
50.0
50.0
50
03/19/09 17:12
106-93-4
NO uglL
5D.0
50.D
50
03/19/09 17.12
95-50-1
NO uglL
50.4
50.0
50
03/19/0917 12
541-73-1
ND uglL
50.0
50-0
50
03/19/09 17:12
106-46-7
NO uglL
50.0
50.0
50
03/19/09 17712
75-71-8
NO uglL
%0
50.0
50
03/19/091712
75-34-3
NO uglL
50.0
50.0
50
03/19/091712
107-06-2
NO uglL
50.0
50.0
50
03/19/09 1712
75-35-4
466 uglL
50.0
50.0
50
03/19/09 1712
156-59-2
ND uglL
50.0
50-0
50
03/19/09 1712
156-60-5
ND uglL
%0
50-0
50
03/19/09 17.12
78-87-5
NO uglL
50A
50.0
50
0311910917:12
10051-01-5
NO uglL
50.0
50.0
50
03/1910917:12
10061-02-6
NO uglL
50.0
50.0
50
03/19/09 1712
108-20-3
NO uglL
50.0
50.0
50
03/19/09 17:12
100-41-4
ND ug1L
100
100
50
03/19/09 17:12
75-09-2
NO uglL
50.D
50.0
50
03/19/0917:12
1634-04-4
ND uglL
100
100
50
03/1910917:12
91-20-3
ND uglL
500
50.0
50
03/19/09 17:12
79-34-5
1250 uglL
50.0
50-0
50
03/19/09 17:12
127-18-4
ND ug1L
50.0
50.0
50
03/19/09 17:12
108-88-3
ND uglL
50.0
5D.0
50
D311910917:12
71-55-6
ND uglL
50.0
50.0
50
03/19/09 17:12
79-00-5
NO uglL
50.0
50,D
50
03/1910917:12
79-01-6
NO uglL
50.0
50.0
50
0311910917A2
75.69-4
NO uglL
50.0
50.0
5o
03/191091T12
75-01-4
NO uglL
100
100
50
03/19/09 17:12
1330-20-7
NO uglL
100
100
50
03/19/09 17:12
1330-20-7
ND ug/L
50.0
50.0
50
03/19/09 1712
95-47-6
140 %
65-137
50
03/19/09 17:12
625-98-9 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent
ry ' of Pace Analytical Seices, Inc..
11E&C.
Page 11 of 18
e
'CeAnalyfical
www.paoelahs.mm
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 26804
(828)254-7176
Pace Analytical Services, Inc.
9800 Klncey Ave. Suite 100
Huntersville, NC 28078
(704)875.9092
Project. Gilbarco 042-08-018
Pace Project No. 9239387
ANALYTICAL RESULTS
Sample: MW-25
Parameters
Lab ID: 9239387008
Results Units
Collected:
Report
Limit
03105/09 14A6
MDL OF
Received: 03/06/09 15:00 Matrix: Water
Prepared Analyzed CAS No. Quaff
6011602 Volatiles
Analytical Method: EPA 601/602
Benzene
NO uglL
1,0
1.0
1
03/19/09 17:54
71-43-2
Bromodichloromethane
ND uglL
1.0
1.0
1
03/19/09 17:54
75-27-4
Bromoform
ND uglL
1.0
1.0
1
03/19/09 17:54
75-25-2
Bromomethane
ND ug1L
1.0
1.0
1
03/19/09 17:54
74-83-9
Carbon tetrachloride
ND uglL
1.0
1.0
1
03/19/09 17:54
56-23-5
Chlorobenzene
NO uglL
1.0
1.0
1
03/19/0917754
108-90-7
Chloroethane
NO ug1L
1.0
1.0
1
03/19/09 17.54
75-00-3
Chloroform
NO uglL
1.0
1.0
1
03119/0917:54
67-66-3
Chloromethane
NO uglL
2.0
2.0
1
03/19/0917:54
74-87-3
Dibromochloromethane
ND uglL
1.0
1.0
1
03/19/09 17:54
124-48-1
1,2-Dibromoethane (ED8)
NO uglL
1.0
1.0
1
03/19/09 17:54
106-93-4
1,2-Dichlorobenzene
NO uglL
1.0
1.0
1
03/19109 17:54
95-50-1
1,3-DicNorobenzene
ND ug1L
1.0
1.0
1
03/19109 17:54
541-73-1
1,4-Dichlorohenzene
ND ug1L
1.0
1.0
1
03/19/09 17:54
106-46-7
❑ichlorodifluoromethane
NO uglL
1.0
1.0
1
D3119109 17:54
75-71-8
1,1-Dichloroethane
ND uglL
1.0
1.0
1
D311910917.54
75-34-3
1,2-Dichloroethane
NO uglL
1.0
1.0
1
0311910917:54
107-06-2
1.1-Di chloroethane
1.1 uglL
1.0
1.0
1
03/19/0917.54
75-35-4
cis- 1,2-Dichloroethene
51.0 uglL
1.0
1.0
1
03/19/09 17:54
156-59-2
trans-1,2-Dichloroethane
ND uglL
1.0
1.0
1
03/19/09 17:54
156-60-5
1,2-Dichloropropane
NO uglL
1.0
1.0
1
03/19/09 1 T54
78-87-5
cis-1,3-Dichloropropene
NO uglL
1.0
1.0
1
03/19/09 17:54
10061-01-5
trans-1,3-Dichlorop rope ne
ND ug1L
1.0
1.0
1
0311910917:54
10061-02-6
Diisopropyl ether
NO uglL
1.0
1.0
1
03/19/09 17:54
108-20-3
Ethylbenzene
NO uglL
1.0
1.0
1
03/19109 17:54
100-41-4
Methylene Chloride
NO uglL
2.0
2.D
1
03/19/09 17:54
75-09-2
Methyl -tent -butyl ether
4.8 uglL
1.0
1.0
1
03/19/09 17:54
1634-04-4
Naphthalene
NO uglL
2,0
2.0
1
03/19/0917:54
91-20-3
1,1,2,2-Tetrachloroethane
N❑ uglL
1.0
1.0
1
03/19/09 17:54
79-34-5
Tetrachloroethene
24.9 uglL
1.0
1.0
1
03/19109 17:54
127-18-4
Toluene
NO ug1L
1.0
1.0
1
03/19109 17:54
108-88-3
1,1,1-Trichloroethane
ND uglL
1.0
1-0
1
03/19/09 17:54
71-55-6
1.12-Trich0oroethane
NO uglL
1.0
1.0
1
031191D91T54
79-00-5
Trichloroethene
8.3 uglL
1.0
1.0
1
03/19/09 17:54
79-01-6
Thchlarol9uoromethane
ND ug1L
1.0
1.0
1
03/19/09 17:54
75-69-4
Vinyl chloride
NO uglL
1.0
1.0
1
03/19/09 17:54
75-01-4
Xylene (Total)
ND ug1L
2.0
2.0
1
03/19/09 17:54
1330-20-7
m&p-Xylene
NO uglL
2.0
2.0
1
03/19/09 17:54
1330.20.7
o-Xylene
NO uglL
1-0
1.0
1
03/19/09 17:54
95-47-6
1 -C h loro-3 -flu o ro benzen e (5)
131 %
65-137
1
03/19/09 17:54
625-98-9
Date: 03/20/2009 04:43 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in to.
witheut the written consent of Pace Analytical Services, Inc..
Page 12 of 18
n Pace Analytical Services, Inc. Pace Analytical Services, Inc.
_ laceAnalyfical 2225 Riverside Dr 9800 Kincey Ave. Suile 100
wrrw,parslabs.rom Asheville, NC 28804 Huntersville. NC 28078
(828)254.7176 (704)875-9092
ANALYTICAL RESULTS
Project: Gilbarco 042-08.018
Pace Project No.' 9239387
Sample: MNW-42 Lab ID: 9239387009 Collected: 03/05/09 11:04 Received: 03/06/09 15:00 Matrix: Water
Report
Parameters Results Units Limit MDL DP Prepared Analyzed CAS No. Qual
6011602 Volatiles
Benzene
B ro mad ich I o ro metha ne
Bromoform
Bromomethane
Carbon tetrachloride
Chiorobenzene
Chloroethane
Chloroform
Chloromethane
D ib ro m och to rometha n e
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
D ich to rod ifl uo rometh a n e
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis- 1,3-❑ichtoroprope ne
trans- l,3-Dich ioropropen e
Diisopropyl ether
Ethylbenzene
Methylene Chloride
MethyMert-butyl ether
Naphthalene
1.1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichtoroethane
1,1.2-Thchtoroethane
Trichloroethene
Trich to rofl u o rometh ane
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
1-Chioro-3-fluorobenzene (S)
Date: 03/20/2009 04A3 PM
Analytical Method: EPA 601 /602
NO uglL
1.0
1.0
1
03/19/09 18:36
71-43-2
NO uglL
1.0
1.0
1
03/19/09 18:35
75-27-4
NO uglL
1.0
1.0
1
03/19/09 18,35
75-25-2
NO uglL
1.0
1.0
1
03/19/09 18:35
74-83-9
NO uglL
1.0
1.0
1
03/19/09 18'35
56-23-5
NO uglL
1.0
1.0
1
03119/0918:35
108-90-7
NO uglL
1.0
1.0
1
03/1910918:35
75-00-3
NO uglL
1 0
1,0
1
031191091835
67-66-3
ND ug1L
2.0
2.0
1
03/19/09 18:35
74-87-3
NO uglL
1.0
1 A
1
03/19/09 18:35
124-48-1
NO uglL
1.0
1.0
1
03/19/09 18735
106-93-4
NO uglL
1.0
1.0
1
03/19/09 19:35
95-5D-1
NO uglL
1.0
1.0
1
03/19/0918,35
541-73-1
NO uglL
1-0
1.0
1
03/1910918,35
1D6-46-7
NO uglL
1.0
1.0
1
03119/0918:35
75-71-8
ND ug1L
1.0
1.0
1
03/19/09 18:35
75-34-3
ND uglL
1.0
1.0
1
03/19/09 18:35
107-06-2
NO uglL
1.0
1.0
1
03/19/09 18!35
75-35-4
NO uglL
1.0
1.0
1
03/19/09 18:35
156-59-2
ND uglL
1.0
1,0
1
03/19/09 18:35
156-60-5
NO uglL
1.0
1.0
1
03/19/09 18:35
78-87-5
NO uglL
1,0
1.0
1
0311910918:35
10061-01-5
NO uglL
1.0
1.0
1
03/19/09 18'35
10061-02-6
NO uglL
1,0
1.0
1
03119/0918:36
108-20-3
NO uglL
1.0
1.0
1
03119/0918:36
100-41-4
NO uglL
2.0
2.0
1
03/19/09 18:35
75-09-2
ND uglL
1.0
1.0
1
03/19/09 1836
1634-04-4
NO uglL
2.0
2A
1
03/19/09 18:36
91-20-3
ND ug1L
1.0
1.0
1
03/19M918:35
79-34-5
2.7 uglL
1.0
1.0
1
03119/0918:35
127-18-4
NO uglL
1.0
1.0
1
03/1910918:36
108-88-3
ND uglL
1A
1,0
1
03/19/09 18:35
71-55-6
NO uglL
1.0
1.0
1
03/19/09 18:35
79-00-5
NO uglL
1.0
1.0
1
03119/0918:35
79-01-6
NO uglL
1.0
1.0
1
03119/09 18:35
75-69-4
NO uglL
1.0
1,0
1
0311910918,35
75-01-4
NO uglL
2.0
2.0
1
03/19/09 18:36
1330-20-7
NO uglL
2.0
2.0
1
03/19/09 18:36
1330-20-7
NO ug1L
1.0
1.0
1
03/19/09 18:36
95-47-6
127 %
65-137
1
03119/09 18:35
625-98-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, Inc..
Page 13 of 18
laceAnalyfical
Pace Analytical Services. Inc. Pace Analytical Services, Inc.
2225 Riverside Dr. 9800 Kincey Ave. Suite 100
swwpa+�efahscorn Asheville, NC 28804 Huntersville, NC 28078
(828)254-7178 t704j875-9092
ANALYTICAL RESULTS
Project. Gilbarco 042-08-018
Pace Project No.: 9239387
Sample: MW 45 Lab ID: 9239387010 Collected: 03/05/09 11:11 Received 03/06/09 15:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6011602 Volatiies Analytical Method: EPA6011602
Benzene
NO uglL
1.0
1.0
1
03119/09 19: 17
71-43-2
Bromodichloromethane
NO uglL
1.0
1.0
1
03/19/09 19:17
75-27-4
Bromoform
NO uglL
1.0
1 0
1
03/19/09 19:17
75.25-2
Bromomethane
NO ug1L
1.0
1.0
1
03/19/09 19:17
74-83-9
Carbon tetrachloride
NO ug/L
1-0
1.0
1
03/19/09 19 17
56-23-5
Chlorobenzene
NO ug1L
1.0
1.0
1
03/19109 19,17
108-90-7
Chioroethane
NO ug/L
1.D
1.0
1
03/19/09 19:17
75-00-3
Chloroform
ND ug/L
1.0
1.0
1
03/19/09 19:17
67-66-3
Chloromethane
NO ugIL
2.0
2.0
1
03/19/0919:17
74-87-3
Dibromochlor0methane
NO uglL
1.0
1.0
1
03119/0919:17
124-48-1
1,2-Dibromoethane (EDB)
NO ug1L
1.0
1 A
1
03/19/09 19:17
106-93-4
1,2-Dichlorobenzene
NO uglL
1.0
1.0
1
03/19/09 1 9: 17
95-50-1
1,3-Dichiorobenzene
NO ugIL
1.0
1.0
1
03/19/09 19,17
541-73-1
1,4-Dichlorobenzene
NO ug/L
1.0
1.0
1
0311910919:17
106-46-7
Dichiorodi luoromethane
ND ug/L
1.0
1.0
1
OW19109 19:17
75-71-8
1,1-Dichloroethane
NO ugIL
1.0
1.0
1
03/19/09 19:17
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1.0
1
03/19/09 19.17
107-06.2
1,1-Dichloroethane
ND uglL
1.0
1.0
1
03/19/09 19:17
75-35-4
cis-1,2-Dichloroethene
NO ugIL
1.0
1.a
1
03/19/0919717
156-59-2
trans-1,2-Dichloroethene
ND ug1L
1.0
1.0
1
03/1910919:17
156-60-5
1,2-Dichloropropane
N❑ uglL
1.0
1.0
1
03119/0919:17
78-87-5
cis-1,3-Dichioropropene
ND ug11
1.0
1.0
1
03/19109 19:17
10061-01-5
trans-1,3-Dichtoropropene
ND uglL
1.0
1.0
1
03119/0919:17
10061-02-6
Diisopropyl ether
NO ug/L
1 A
1.0
1
03/19/09 19:17
108-20-3
Ethylbenzene
NO ug/L
1.0
1.0
1
03/19109 19:17
100-41-4
Methylene Chloride
ND ug/L
2.0
2.0
1
03/19/09 19:17
75-09-2
MethyMert-butyl ether
NO ug/L
1.0
1.0
1
03/19109 19,17
1634-D4-4
Naphthalene
NO ugIL
2.0
2.0
1
0311910919:17
91-20-3
1,1,2,2-Tetrachloroethane
N❑ uglL
1,0
1,0
1
031191091917
79-34-5
Tetfachloroethene
1.3 uglL
1.0
1.0
1
03/19/09 19.17
127-18-4
Toluene
ND uglL
1.0
1.0
1
03/19/09 19:17
108-88-3
1,1,1-Trichloroethane
NO ugIL
1.0
1.0
1
03/1910919:17
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
10
1
03119/0919:17
79-00-5
Trichloroethane
NO uglL
1.0
1,0
1
03/19/091917
79-01-6
ThchloTofluoromethane
NO ug/L
1.0
1.0
1
03119/0919:17
75-69-4
1Cnyi chloride
NO ug/L
1.0
1.0
1
D3119109 19,17
75-01-4
Xylene (Total)
NO ugIL
2.0
2.0
1
03/19109 19:17
1330-20-7
m&p-Xylene
NO uglL
2.0
2.0
1
03/19109 1917
1330-20-7
a-Xylene
NO uglL
1.0
1.0
1
03/19/09 19,17
95-47-6
1-Chloro-3-fluorobenzene (5)
119 %
65-137
1
03/19/09 19:17
625-98-9
Date: 03/20/2009 04:43 PM
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced, except in full.
without the written consent of Pace
.A�nalyticaI Services, Inc..
s
Page 14 of 18
acePace Analytical Services, Inc. Pace Analytical services, Inc.
Analytrcal' 2225 Riverside Dr 9800 KinceyAve. Suite 100
wrvw.pareWs.cum Asheville, NC 28804 Huntersviile, NC 28078
028)254.7178 (704)875.9092
QUALITY CONTROL DATA
Project. Giibarco 042-08-018
Pace Project No 9239387
QC Batch: GCV12999 Analysis Method: EPA 601 /602
QC Batch Method. EPA 60 V602 Analysis Description: 6011602 GCV Water
Associated Lab Samples. 9239387001, 9239387002, 9239387003. 9239387004, 9239387005. 9239387006, 9239387007, 9239387008.
9239387009.9239387010
METHOD BLANK. 251095 Matrix: Water
Associated Lab Samples. 9239387001, 9239387002. 9239387003, 9239387004, 9239387005. 9239387006, 9239387007. 9239387008,
9239387009.9239387010
Parameter
Units
Blank
Result
Reporting
Limit
Analyzed Qualifiers
1,1,1-Trichloroethane
uglL
NO
1.0
03119/0911.00
1112,2-Tetrachioroethane
ug/L
NO
1.0
0311910911:00
1,12-Trichloroethane
ug/L
NO
1.0
03/19109 11 :00
1.1-Dichloroethane
ug/L
ND
1.0
03/19109 11 :00
1,1-Dichloroethene
uglL
NO
1.0
03/19/09 11 00
12-❑ibromoethane (EDB)
ug/L
NO
1.0
03/19/09 11:00
12-Dichlorobenzene
ug/L
NO
1.0
03/1910911:00
1,2-Dichloroethane
ug/L
NO
1.0
03119/09 11 :00
1,2-Dichloropropane
ug/L
ND
1.0
0311910911:00
1,3-Dichlorobenzene
ug/L
ND
1.0
03119/091100
1.4-Dichlorobenzene
ug/L
NO
1.0
03119/09 11 :00
Benzene
ug/L
NO
1.0
03119/0911:00
Bromodichloromethane
ug/L
ND
1.0
0311910911:00
Bromoform
ug/L
ND
1.0
0311910911:00
Bromomethane
ug/L
ND
1.0
03/1910911:00
Carbon tetrachloride
ug1L
NO
1.0
03/19/09 11,00
Chlorobenzene
uglL
NO
1.0
03/1910911:00
Chioroethane
ug/L
NO
1.0
03/19109 11 :00
Chloroform
ug/L
NO
1.0
03/19/091100
Chloromethane
ug/L
NO
2.0
0311910911,00
cis-1.2-Dichloroethene
ug/L
NO
1.0
03119/0911:00
cis-1.3-Dichloropropene
ug/L
NO
1.0
03119/0911:00
Dibromochloromethane
ug/L
NO
1.0
0311910911:00
❑ichlorodifluoromethane
ug/L
N❑
10
03/19/0911:00
Diisopropyl ether
ug/L
ND
1.0
03/19/09 11:00
Ethylbenzene
uglL
ND
1.0
03119/0911100
m&p-Xylene
ug/L
ND
2.0
03119/0911,00
Methyl-tert-butyl ether
ug/L
NO
1.0
03/19/09 WOO
Methylene Chloride
ug/L
ND
2.0
03/19/09 11:00
Naphthalene
ug/L
ND
2.0
03119/0911:00
o-Xylene
ugJL
ND
10
03/1910911.00
Tetrachloroethene
ug/L
ND
1.0
0311910911:00
Toluene
ug/L
ND
1.0
03/19/0911:00
trans- 1,2-Dichloroethene
ug/L
ND
1.0
03/1910911:00
trans- 1,3-Dichloropropene
ug1L
ND
1.0
0311910911:00
Trichlorciethene
ug/L
NO
1.0
03/19109 11 : 00
Trichlorofluoromethane
ug/L
NO
1.0
03/1910911:00
Vinyl chloride
ug/L
NO
1.0
03/19/09 11.00
Xylene (Total)
ug/L
NO
2.0
03119109 11:00
1-Chloro-3-fluorobenzene (S)
%
121
65-137
03/19/09 11 00
Date : 0312012OD9 04A3 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
without the written consent of Pac/e+Analybral Services, Inc .
Page 15 of 18
e Pace Analytical Services, Inc.
acmwlytical 2225 Riverside Qr.
xavn:pacels6s. caul
Asheville, NC 28004
(828)254-7178
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Wuntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Gilbarco 042-08-018
Pace Project No.: 9239387
LABORATORY CONTROL SAMPLE.
251096
Spike
LC5
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
1,1.1-Trichloroethane
uglL
20
22.9
115
41-138
1,1,2,2-TetrachIoroethane
uglL
20
20.9
104
8-184
1,1,2-T6chloroethane
uglL
20
21.7
109
39-136
1, 1 -Dichloroethane
uglL
20
20.7
103
47-132
1,1-Dichloroethene
uglL
20
23.0
115
28-167
1,2-Dibromoethane (EDB)
uglL
20
23.1
116
50-150
1,2-Dichlorobenzene
uglL
20
20.7
104
1-208
1,2-Dichloroethane
uglL
20
21.6
108
51-147
1,2-Dichloropropane
uglL
20
19.6
98
44-156
1,3-Dichlorobenzene
uglL
20
20.3
101
7-187
1,4-Dichlorobenzene
uglL
20
21.5
107
42-143
Benzene
uglL
20
20.8
104
39-150
Bromodichloromethane
uglL
20
20A
102
42-172
Bromoform
uglL
20
21.8
1 D9
13-159
Bromomethane
uglL
20
26.2
131
1-144
Carbon tetrachloride
uglL
20
24.1
120
43-143
Chlorobenzene
ug/L
20
21.5
107
38-150
Chloroethane
uglL
20
22.1
111
46-137
Chloroform
uglL
20
22.2
111
49-133
Chloromethane
uglL
20
30.9
155
1-193
cis-1,2-Dichioroethene
uglL
20
21X
105
38-155
cis, 1,3-Dichloropropene
uglL
20
21A
107
22-178
Dibromochloromethane
uglL
20
21.5
108
24-191
Dichloroddluoromethane
uglL
20
21.5
108
48-157
Diisoprapyl ether
uglL
20
20.2
101
89-108
Ethylbenzene
ug1L
20
21.1
105
32-160
m8p-Xylene
uglL
40
42.8
107
82-115
Methyl-tert-butyl ether
uglL
20
20.0
100
88-110
Methylene Chlonde
uglL
20
18.9
94
25-162
Naphthalene
uglL
20
19.6
98
50-150
o-Xylene
uglL
20
21.8
109
91-110
Tetrachloroethene
uglL
20
21.7
108
26-162
Toluene
uglL
20
21,2
106
46-148
trans-1,2-Dichloroethene
ug1L
20
22.5
112
38-155
trans-1,3-Dichloropropene
uglL
20
19.4
97
22-178
Trichloroethene
uglL
20
21.7
108
35-146
Trichlorofluoromethane
uglL
20
23.2
116
21-156
Vinyl chloride
uglL
20
24.8
124
28-163
Xylene (Total)
uglL
60
64.6
108
50-150
1-Chloro-3-fluorobenzene (S)
%
117
65-137
Qualifies
SAMPLE DUPLICATE: 251097
9239387001 Dup Max
Parameter Units Result Result RPD RPD
1,1.1-Trichloroethane uglL NO NO 30
1,1,22-Tetrach1oroethane uglL ND ND 30
1,1,2-Trichloroethane uglL ND NO 30
Date: 03/20/2009 04:43 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
Page 16 of 18
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
I)FaceAnalj4ical 2225 Riverside Dr 9800 KmceyAve Suite 100
www.Pare7aas.curr Asheville. INC 28804 Huntersvilie, NC 28078
(828)254-7176 (704)875.9092
DUALITY CONTROL DATA
Project Gilbarco 042-08-018
Pace Project No.. 923,3387
SAMPLE DUPLICATE: 251097
Parameter
Units
9239387001
Resutt
❑up
Result
1, 1 -Dichloroethane
ug/L
NO
R NO
1,1-Dichloroethene
ug/L
NO
NO
1,2-Dibromoethane (EDB)
uglL
NO
NO
1,2-Dichlorobenzene
ug/L
ND
NO
1,2-Dichlaroethane
ug/L
ND
NO
1,2-Dichloropropene
ug/L
NO
NO
1.3-Dichlorobenzene
ug/L
NO
N❑
1,4-Dichlorobenzene
uglL
NO
ND
Benzene
ug/L
NO
NO
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
N❑
ND
Bromomethane
ug/L
N❑
NO
Carbon tetrachloride
ug/L
ND
NO
Chlorobenzene
ug/L
N❑
ND
Chloroethane
ug/L
ND
NO
Chloroform
uglL
ND
N❑
Chloromethane
ug/L
NO
NO
cis-1,2-Dlchloroetnene
ug/L
935
852
cis- 1.3-Dichloropropene
ug/L
NO
NO
❑ibromochloromethane
ug/L
Na
NO
Dichlorodrttuoromethane
ug/L
ND
NO
Diisopropyl ether
ug/L
ND
NO
Ethylbenzene
ug1L
749
752
m&p-Xylene
ug/L
723
729
Methyl-tert-butyl ether
ug/L
NO
ND
Methylene Chloride
ug/L
ND
NO
Naphthalene
ugfL
384
376
o-Xylene
ug/L
NO
ND
Tetrachloroethene
ug/L
NO
NO
Toluene
ug/L
ND
ND
trans-1,2-Dichlorcethene
uglL
NO
ND
trans-1,3-Dichloropropene
ug/L
NO
ND
Trichioroethene
ug/L
NO
ND
TriChlorofiuoramethane
uglL
NO
ND
Vinyl chloride
ug/L
ND
NO
Xylene (Total)
ug/L
723
729
1-Chloro-3-fluorobenzene (S)
%
125
116
Date. 03/20/2009 04 43 PM
Max
RPD RPD
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pack -Analytical Services, inc.
• i.i la
9
4
8
2
8
8
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Qualifiers
Page 17 of 18
ace Anal rcal r
www.panWabs.com
Pac*Ana" cal Services, tnc.
2225 Riverside Dr.
Asheville. NC 28804
(828)254-7176
Pace Analytical Services, Inc.
9800KinceyAve. Suile loo
Huntersville, NC 28078
(704)875-9092
QUALIFIERS
Project: Gilbarco 042-08-018
Pace Project No.: 9239387
t17*1f211[193ni
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1.2-0iphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
❑UP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical Is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
LJ - Indicates the compound was analyzed for, but not detected.
ANALYTE QUALIFIERS
E Analyte concentration exceeded the calibration range. The reported result is estimated.
So Surrogate recovery outside laboratory control limits.
Date- 03/20/2009 04A3 PM REPORT OF LABORATORY ANALYSIS Page 18 of 18
This report shall not be reproduced. except in rule,
w4thout the written consent of Pace Analytical Services, Inc .
dceMa�yt+ca�
Section A
Required Client infortnafion:
Section 9
Required Project Information;
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section C
Invoice Information'
Pa e : 1 Of +
Company Trl onlKleinfelder, Inc.
Report To. Gail Lica an
Alters ion Gail Lica an
Address 313 Gallimore Dairy Rd
Copy To:
Company Name Tri onlKleinfelder, Inc -
Greensboro, NC 27409
Address 313 Gal}imore Dairy Rd, Greensboro, N
Email To glicayanQkleinfelder.corn
Purchase Order No
Pace Quote Reference
Phone 336 668-0093 Irax
Ctienl Project ID GILBARCO 042-08-018
Pace Pra}ect Manager McKee, Bonnie
Requested Due Date(TAT 10 Da Default
Container Order Number 8484
Pace Profile N
North Carolina
ru.leix CODE
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❑
U
COLLECTED
Preservatives
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SIGNATURE of SAMPLER: �/]®.�y
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DATE Signed: /�
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Pace Analytical Services. Inc. Pace Analytical Services, Inc.
aeeftlytical 2225 Riverside DF 9800 KinceyAve Suite 100
www.pare4b5.f0m Asheville. NC 28804 Hunlersviile NC 28078
l828)254.7176
April 08. 2009
Ms. Gail Licayan
Trigon/Kleinfelder, Inc.
313 Gallimore Dairy Rd
Greensboro. NC 27409
RE: Project: GILBARCD 97746
Pace Project No.: 9240955
Dear Ms. Licayan:
Enclosed are the analytical results for sample(s) received by the laboratory on March 27, 2009. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report. please feel free to contact me.
Sincerely,
Bonnie McKee
bonnie-mckee@pacelabs.com
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSES
This report shall not be reproduced, except in lull,
without the written ccnseyntt of Pace
Aria lyllcaI Services, Inc.
(704)875.9092
page t of 9
m Pace Analytical Services, Inc. Pace Analytical Services, Inc.
laceAnalytical 2225 Riverside ❑r 9800 KinceyAve. Suite loo
AvwpaceraGsr-'Gm Asheville, NG 28804 Huntersville, NC 28078
(828)254.7178 (704)875.9092
CERTIFICATIONS
Project: GILBARCO 97746
Pace Project No.: 9240955
Charlotte Certification IDs
West Virginia Certification #: 357
North Carolina Field Serwces Certification #: 5342
Virginia Certification #: 00213
North Carolina Drinking Water Certification # 37706
Tennessee Certification #: 04010
Mew Jersey Certification #: NC012
South Carolina Drinking Water Cert. #: 990060003
Louisiana/LELAP Certification #- 04034
South Carolina Certification #: 990060001
Kentucky LIST Certification #: 84
Pennsylvania Certification #: 88-00784
Florida)NELAP Certification # E87627
Connecticut Certification #: PH-0104
North Carolina Wastewater Certification #: 12
Asheville Certification lDs
West Virginia Certification * 356
Pennsylvania Certification #: 68-D3578
Virginia Certification #: 00072
North Carolina Wastewater Certification #: 40
Connecticut Certification #: PH-0106
North Carolina Drinking Water Certification #: 37712
FloddalNELAP Certification #: E87648
North Carolina Bioassay Certification #: 9
Tennessee Certification #: 298D
New Jersey Certification #: NCO11
South Carolina Certification #. 99030001
Massachusetts Certification #: M-NC030
South Carolina Bioassay Certification #: 99030002
Louisiana/LELAP Certification #: 03095
Eden Certification IDs
North Carolina Wastewater Certification * 633 North Carolina prinking Water Certification #: 37738
Virginia Drinking Water Certification #: 00424
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
Page 2 of 9
�aceAnal ical
www.pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville INC 28804
t828j254.7176
SAMPLE SUMMARY
Project
GILBARCO 97746
Pace Project No.
9240955
Lab ID
Sample ID Matrix
9240955001
MW-14❑ Water
9240955002
MW-43❑ Water
Hate Collected
Date Received
03/27/09 09:09
03/27/09 14A0
03/2710910:07
03127/0914.40
REPORT OF LABORATORY ANALYSIS
This report shall riot be reproduced, except in full,
without the written consent of Pacee►Ana lytical Services, Inc.
Pace Analytical Services, Inc.
9800 Kinney Ave. Suite 100
Huntersville, NC 28078
(704)875-9D92
Page 3 of 9
Pace Analytical Services, Inc. Pace Analytical ServIcea, Inc.
aceAnalylical ' 2225 RNerside Dr. 9800 IOncey Ave. Suite 100
WWWwParelabsxonl Asheville, NC 28804 Huntersville. NC 28078
(828)254-7176 (704)875-9092
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
GILBARCO 97746
9240955
Analytes
Lab ID
Sample I❑
Method Analysts Reported
9240955001
MW-14D
EPA601/602 ❑H11V 40
9240955002
MW-431)
EPA6011602 ❑HW 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduoed, except in full.
without the written consent
of Pac�e+A:nalytical Services. Inc..
Page 4 of 9
e Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aeeA,aalXica1 2225 Riverside Dr. 9800 KinceyAve. Suite top
www4pa,BJabs corn Asheville. NC 28804 Huntersville, NC 28078
(82B)2547175 (704)a75-9092
ANALYTICAL RESULTS
Project: GILBARCO 97746
Pace Project No.: 9240955
Sample: MW-14D Lab ID: 9240955001 Collected: 03/27/09 09:09 Received: 03/27/09 14:40 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Clual
6011602 Volatiles Analytical Method: EPA 6011602
Benzene
ND uglL
1.0
1.0
1
04/03/09 01:17
7143-2
Bromadichloromethane
ND uglL
1.0
1.0
1
04/03/09 01:17
75-274
Bromoform
N❑ uglL
1.1)
1.0
1
04/03/09 01:17
75-25-2
Bromomethane
ND uglL
1,0
1 A
1
04/03109 0 1; 17
74-83-9
Carbon tetrachloride
ND uglL
1.a
1.0
1
04/03/09 01:17
56-23-5
Chlorobenzene
ND uglL
1.0
1.0
1
04/03/09 01:17
108-90-7
Chloroethane
ND uglL
10
1.0
1
D4103109 01:17
75-00-3
Chloroform
ND ug1L
1.0
1.0
1
04/03/09 01:17
67-66-3
Chloromethane
N❑ uglL
2.0
2.0
1
04/03/09 01;17
74-87-3
Dihromochloromethane
ND uglL
1.0
1.0
1
04/03/09 01.17
124-48-1
1,2-Dibromoethane (EDB)
ND ug1L
1.0
1.0
1
04/03/09 01:17
106-93-4
1,2-Dichlorobenzene
ND ug1L
1.D
1.D
1
04/03/09 01 17
95-50-1
1.3-Dichlorobenzene
N❑ ugJL
1.0
1.0
1
04103/090117
541-73-1
1.4-Dichlorobenzene
ND uglL
1.0
1.a
1
04/03/09 01:17
10646--7
Dichlorodifluoromethane
ND uglL
1.0
1.a
1
04/03/09 01:17
75-71-8
1,1-Dichloroethene
ND uglL
1.0
1.0
1
04/03/09 01,17
75-34-3
1.2-Dichioroethane
ND uglL
1.0
1.0
1
04/03/09 01:17
107-06.2
1,1-Dichloroethene
ND uglL
1.0
1.0
1
04103/0901:17
75-35-4
cis- 1,2-Dichloroe the ne
1.0 uglL
1.0
1.0
1
04/03/09 01:17
156-59-2
trans-1,2-Dichloroethene
ND uglL
1.0
1.0
1
04/03/09 01:17
156-60-5
1,2-Dichlaropropane
ND uglL
1.0
1.0
1
04/03/09 01:17
78-87-5
cis-1,3-Dichloropropene
ND uglL
1.0
1.0
1
04/03/09 0117
10061-01-5
trans- 1,3-Dichloropropene
N❑ uglL
1.0
1.0
1
04103/09 01 ; 17
10061-02-6
Diisopropyl ether
ND uglL
1.0
1.0
1
04/03/09 01:17
108-20-3
Ethylbenzene
ND ugJL
1.a
1.0
1
04/03/09 01:17
100-41-4
Methylene Chloride
ND ugJL
2,0
2.0
1
04/03/09 01:17
75-09-2
Methyl-tert-butyl ether
ND uglL
1.0
1.0
1
04/03/09 01:17
1634-04-4
Naphthalene
ND uglL
2.0
2.0
1
04/03/09 01:17
91-20-3
1.1.2.2-Tetrachloroethane
ND uglL
1.0
1.0
1
D4103109 01.17
79-34-5
Tetrachloroethene
10.6 uglL
1.0
1.0
1
W03/09 01:17
127-18-4
Toluene
ND uglL
1.D
1.0
1
D4103109 01:17
108-88-3
1,1,1-Trichloroethane
N❑ ugJL
1.0
1.0
1
04103/0901;17
71-55-6
1,1,2-Trichtoroethane
ND uglL
1.0
1.0
1
W0310901,17
79-00-5
Trichloroethene
ND uglL
1.0
1.0
1
04/03/09 01.17
79-01-6
Trichlorofluoromethane
ND ugJL
1.0
1.4
1
04/03/09 01 ' 17
75-69-4
Vinyl chloride
ND uglL
1.0
1.0
1
04/03/09 0117
75-01-4
Xylene (Total)
ND ugJL
2.a
2.0
1
04/03/09 01:17
1330-20-7
m&p-Xylene
ND uglL
2.0
2.0
1
04/03109 01:17
1330-20-7
o-Xylene
N❑ ugJL
1.0
1.0
1
04/03/09 01:17
95-47-6
1-Chlaro-3-fluarobenzene (S)
124 %
65-137
1
04/03/09 01:17
625-98-9
Date: D410812009 04 15 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, 1nc..
Page 5 of 9
IMAnalytical"
www.pacewaccvn
Pace Analytical Services, Ine.
2225 Riverside Or
Asheville, NC 28804
(82B)254-7176
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28076
(704)875.9092
Project GILBARCQ 97746
ANALYTICAL RESULTS
Pace Project No.: 9240955
Sample: MW43D Lab ID: 9240965002 Collected: 03/27/09 10:07 Received: 03/27/09 14.40 Matrix: Water
Report
Parameters
Results Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
6011602 Volatiles
Analytical Method- EPA 601/602
Benzene
9.0 uglL
1.D
1.0
1
04/04/09 05:02
71-43-2
Bromodichloromethane
ND uglL
1.0
1.0
1
04/04/09 05:02
75-27-4
Bromoform
ND uglL
1.0
1.0
1
D4104109 05:02
75-25-2
Bromomethane
N❑ uglL
1.0
1.0
1
04/04/09 05:02
74-83-9
Carbon tetrachloride
ND uglL
1.0
1.0
1
04/04/09 05:02
56-23-5
Chlorobenzene
ND uglL
1.0
1 A
1
04/04/09 05:02
108-90-7
Chioroethane
ND uglL
1.0
10
1
D4104109 05:02
75-00-3
Chloroform
ND uglL
1.0
1.0
1
04/04/09 05:02
67-66-3
Chloromethane
N❑ uglL
2.0
2.0
1
04104/09 05:02
74-87-3
Dibromochloromethane
ND uglL
1.0
1.0
1
04/04/09 05:02
124-48-1
1,2-Dibramoethane (EDB)
ND ug1L
1.0
1.0
1
04/04/09 05702
106-93-4
1.2-Dichlorobenzene
ND ug1L
1.0
1.0
1
04/04/09 05.02
95-50-1
1,3-Dichlorobenzene
ND ug1L
1.0
1.0
1
04/04/09 05:02
541-73-1
1,4-Dichlorobenzene
ND uglL
1.0
1.0
1
04/04/09 05:02
106-46-7
Dichlorodifluoromethane
ND uglL
1.0
1.0
1
04/04/09 05:02
75-71-8
1,1-Dichloroethane
1.6 uglL
1.0
1.0
1
04/04/0905:02
75-34-3
1,2-Dichloroethane
N❑ uglL
1.0
1.0
1
04/04/09 05:02
107-06-2
1,1-Dichloroethene
9.3 uglL
1.0
1.0
1
04/04/09 05702
75-35-4
cis-1,2-Dichloroethene
ND uglL
1.0
1.0
1
04/04/09 05:02
156-59-2
trans-1,2-Dichloroethene
ND uglL
1.0
1.0
1
041D4109 05:02
156-60-5
1,2-Dichloropropane
ND uglL
1.0
1.D
1
04/04/09 05 02
78-87-5
cis-1,3-Dichloropropene
ND ug1L
1.0
1.0
1
04/04/0905:02
1D061-01-5
tra ns- 1 .3-D ich to ro prope n e
IN ug1L
1.0
1.0
1
041D4109 05,02
10061-02-6
Diisopropyl ether
ND ugIL
1.0
1,0
1
04/04/09 05:02
108-20-3
Ethylbenzene
7.5 ug/L
1.0
1.0
1
04/04109 05702
100-41-4
Methylene Chloride
ND uglL
2.0
2.0
1
04/04/09 05:02
75-09-2
Methyl-tert-butyl ether
3.6 uglL
1.0
1.0
1
04/04/09 05:02
1634-04-4
Naphthalene
4.4 ug1L
2.0
2.0
1
04/04/09 05:02
91-20-3
1,1,2,2-Tetrachtoroethane
ND uglL
1.0
1.0
1
D4104109 05A2
79-34-5
Tetrachloroethene
ND uglL
1.0
1.0
1
041041D9 D5:02
127-18-4
Toluene
ND uglL
1.0
1.0
1
04104/09 05:02
108-88-3
1, 1, 1 -Trich loroeth a n e
1.2 uglL
1.0
1.0
1
04/04/09 05:02
71-55-6
1,1,2-T6chloroethane
ND ug1L
1.0
1.0
1
04104/09 05:02
79-00-5
Trichloroethene
ND ug/L
1,0
1.0
1
0410410905:02
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1.0
1
04/04/09 05,02
75-69-4
Vinyl chfohde
ND uglL
1.0
1.0
1
04/04/09 05A2
75-01-4
Xylene (Total)
ND ug1L
2.0
2.0
1
04/04/09 05:02
1330-20-7
m&p-Xylene
ND uglL
2.0
2,0
1
04/04/09 05:02
1330-20-7
o-Xylene
ND uglL
1.0
1.0
1
04/04/09 05:02
95-47-6
1-Chloro-3-fluofobenzene (S)
105 %
65-137
1
04/04/09 05:02
625-98-9
Date? 04108/2009 04:15 PM REPORT OF LABORATORY ANALYSIS Page 6 of 9
This report shall not be reproduced. except in full,
without the written consent of Pace Analytical Services, Inc..
laceAnal rca�
www.parefabs.wm
Project: GILBARCO 97746
Pace Project No : 9240955
Pace Analytical Services, Inc.
2225 Riverside Or
Asheville, INC 28804
(628)254-7176
QUALITY CONTROL DATA
QC Batch- GCV13043 Analysis Method EPA 601/602
QC Batch Method EPA 601 /602 Analysis Description. 6011602 GCV Water
Associated Lab Samples, 9240955001. 9240955002
METHOD BLANK- 268263
Matrix
Water
Associated Lab Samples:
9240955001. 9240955002
Blank
Reporting
Parameter
Units
Result
Limit
Anatyzed
1,1,1-Trichloroethane
uglL
ND
1.0
04/02/09 18.21
1,1.2.2-Tetrachloroethane
ug1L
ND
1.0
04/02/0918.21
1,1.2-Trichloroethane
uglL
ND
1.0
0410210918:21
1,1-Dichloroethane
uglL
ND
1.0
04/0210918:21
1,1-Dichioroethene
uglL
ND
1.0
04/0210918-21
1,2-Dibromoethane (EDS)
ug/L
N❑
1.0
04/02/09 18:21
1,2-Dichlorobenzene
uglL
ND
1.0
041021091821
1,2-Dichlorcethane
ug1L
ND
1.0
04102M918:21
1,2-Dichloropropane
uglL
ND
1.0
04102/0918:21
1,3-Dichlorobenzene
uglL
ND
1.0
04/02/09 18:21
1,4-Dichlorobenzene
uglL
ND
1.0
04/02/091811
Benzene
ug/L
ND
1.0
0410210918721
Bromodichloromethane
uglL
ND
1.0
04/0210918:21
Bromoform
uglL
ND
10
04/0210918:21
Bromomethane
ug1L
NO
1.0
0410210910:21
Carbon tetrachloride
uglL
ND
1.0
04/02/09 18:21
Chlorobenzene
uglL
ND
1.0
04/02/09 18 21
Chloroethane
ug/L
ND
1.0
0410210918.21
Chloroform
uglL
ND
1.0
04/02/09 18 21
Chloromethane
ug1L
ND
2.0
04102/0918:21
cis-1,2-1Dichloroethene
uglL
ND
1.0
04102/0918:21
cis- 1,3-Dichloropropene
uglL
ND
1.0
04/0210918:21
Dibromochloromethane
uglL
ND
1.0
04/0210918:21
Dichlcrodifiuoromethane
ug/L
N❑
1.0
04102/091821
Diisopropyl ether
uglL
ND
1.0
04/02/09 18 21
Ethylbenzene
ug/L
ND
1.0
04/02/09 18:21
m&p-Xylene
uglL
ND
2.0
04102M9 18:21
Methyl-tert-butyl ether
uglL
N❑
1.0
04/02/09 18:21
Methylene Chloride
uglL
ND
2.0
04/02/09 18:21
Naphthalene
uglL
N❑
2.0
04/02/09 18:21
o-Xylene
uglL
ND
1.0
04/02/0918:21
Tetrachloroethene
uglL
ND
1.0
0410210918:21
Toluene
uglL
N❑
1.0
04/0210918:21
trans-1.2-Dichloroethene
ug/L
ND
1.0
04/02/09 18 21
trans- 1,3-Dichloropropene
uglL
N❑
1.0
04/0210918,21
Trichloroethene
uglL
ND
1.0
04/0210918:21
Trichlorofluoromethane
uglL
N❑
1.0
04/02/09 18 21
Vinyl chloride
uglL
ND
1.0
04/02/09 18:21
Xylene (Total)
uglL
N❑
2.0
04/02/09 18 21
1-Chloro-3-fluorobenzene (S)
°I
109
65-137
04/02/09 18.21
Date: 04/08/2009 04:15 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Qualifiers
Pace Analytical Services, Inc.
9800 Kinrey Ave Suite 100
Huntersville, NC 28078
(704)875-9092
Page 7 of 9
e
pace Analytical Services, Inc.
lj/ iml
2225 Riverside Dr.
wawpaceiabscom
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(828)254-7176
QUALITY CONTROL DATA
Project: GILBARCO 97746
Pace Project No.. 9240955
LABORATORY CONTROL SAMPLE
Parameter
258264
Units
Spike
Conc.
LCS
Result
LCS
°% Rec
°% Rec
Limits
1,1,1-Trichloroethane
uglL
20
19.8
99
41-138
1,1,22-Tetrachloroethane
ugfL
20
20.2
101
8-184
1,1,2-Trichloroethane
ug/L
20
21.6
108
39-136
1,1-Dichloroethane
ugIL
20
20.0
100
47-132
1,1-Dichloroethene
uglL
20
20.3
101
28-167
1,2-Dibromoethane (EDB)
uglL
20
21.8
109
50-150
1,2-Dichlorobenzene
uglL
20
19.3
96
1-208
1,2-Dichloroethane
uglL
20
21.3
107
51-147
1,2-Dichloropropane
uglL
20
19.6
98
44-156
1,3-Dichlorobenzene
ug/L
20
22.0
110
7-187
i ,4-Dichlorobenzene
ugfL
20
17.5
88
42-143
Benzene
ug1L
20
19.9
100
39-150
Bromodichloromethane
ug/L
20
21.2
106
42-172
Bromoform
uglL
20
21.2
106
13-159
Bromamethane
uglL
20
18.3
91
1-144
Carbon tetrachloride
uglL
20
20.8
1 D4
43-143
Chlorobenzene
ug/L
20
19.4
97
38-150
Chloroethane
uglL
20
19.5
97
46-137
Chloroform
uglL
20
20.6
103
49-133
Chloromethane
uglL
20
18.3
91
1-193
cis- 1,2•Dichtoroethene
uglL
20
19.7
98
38-155
cis-1,3-Dichloropropene
ugfL
20
21.8
109
22-178
Dibromachloromethane
uglL
20
21.1
106
24-191
Dichlerodifluofomethane
uglt-
20
13.2
66
48-157
Diisopropyl ether
uglL
20
18.3
91
89-108
Ethyibenzene
uglL
20
21.1
105
32-160
m&p-Xylene
uglL
40
43.3
108
82-115
Methyl-tert-butyl ether
uglL
20
18.2
91
88-110
Methylene Chloride
uglL
20
19.4
97
25-162
Naphthalene
ug/L
20
17.9
90
50-150
o-Xylene
ug/L
20
21.3
106
91-110
Tetrachloroethene
uglL
20
19.7
98
26-162
Toluene
uglL
20
20.4
102
46-148
trans-1,2-❑ichioroethene
uglL
20
21.0
105
38-155
trans-1,3-Dichloropropene
uglL
20
20.5
103
22.178
Trichloroethene
ug/L
20
21.2
106
35-146
Trichlorofluoremethane
ug/L
20
20.5
103
21-156
Vinyl chloride
ug/L
20
18.7
93
28-163
Xylene (Total)
uglL
60
64.6
108
50-150
1 -C h I oro-3-fluo ra be nze n e (S)
%
119
65-137
Date: 04/08/2009 04:15 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent � of Pace Analytical Services, Inc..
leg
PacaAnalyticaI Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)875-9092
Qualifiers
Page 8of9
Pace Analytical Services, Inc. Pace Analytical Services. Inc.
/aceAna,(Xieal • 2225 Riverside Dr 9900 Kincey Ave. Suite 100
www,paWab&COm Asheville. NC 28804 Huntefsville, NC 28078
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QUALIFIERS
Project: GILSARCO 97746
Pace Project No : 9240955
DEFINITIONS
DF - Dilution Factor, if reported. represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit
S - Surrogate
1.2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines. unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NEtAP accredited. Contact your Pace PM for the current list of accredited analytes.
U - Indicates the compound was analyzed for, but not detected.
Date 04M812009 04:15 PM REPORT OF LABORATORY ANALYSIS Page 9 of 9
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Lk I. . .
PaceAnalltical
J`
iuww naru[ahc rnm
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOGLIMENT. All relevant fields must be completed accurately.
Section A Section B Section
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SAMPLER NAME AND SIGNATURE
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ORIGINAL
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SIGNATURE of SAMPLER: 1&') �. �xe„r_ - z +an Ina
TOTAL VOLATILE ORGANIC COMPOUNDS
VERSUS TIME IN MW-T
25,000
Q 15,000
0
n
m
v
0
in
7-
ca
i�: 10,000
5,000
11 4-- -- i - f - -T i i r -- • 7 . T I 'T - r
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o 0 l s e t o r � °� s s 6 o
Date
25
20
i 10
5
m
TOTAL VOLATILE ORGANIC COMPOUNDS
VERSUS TIME IN MW-11
;al VOCs
.
L/o�0 ���0 �01) �ol�� �0�o
S 6' 0
Date
180
160
140
120
W,
3
N
80
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ME
40
20
TOTAL VOLATILE ORGANIC COMPOUNDS
VERSUS TIME IN MW-13
.31
- Y
10 �d �a �d �� �� �a � �� Ll to ��, 14 L1 ��, tl 1, L1 10 �� ll
79 �s 79 79 'a �9 �9 ')� ri0 7b �0 �0 �0 h r!0 h0 �i0 '�o '�0 'J �
o i ? 0 s b' J o j ? �u S b' .9 O
Date
ZE
0
n 40
m
m
0
30
r
20
90
0
TOTAL VOLATILE ORGANIC COMPOUNDS
VERSUS TIME IN MW-13❑
°s
o6'
1--Total VOCs
Date
✓a1) ,
0
am
1,800
1,600
1,400
0 1,000
EA
.11
400
0
TOTAL VOLATILE ORGANIC COMPOUNDS
VERSUS TIME IN MW-14
190 r 2 s '96' � 0 O 7 2 o 07 s 0 l> & .9 0
Date
TOTAL VOLATILE ORGANIC COMPOUNDS
VERSUS TIME IN MW-14D
Axis]
450
350
0 300
n
m
¢1. 250
0
200
150
100
kill
Total VOCs
0 i I
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V.
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Q
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s
n
Date
m
700
n 500
7-
t
r
300
200
100
TOTAL VOLATILE ORGANIC COMPOUNDS
VERSUS TIME IN MW-23D
9 rls 7s9 '7� ,79 't9 �9 /!.� 7' rla 'ia 'lp �0 �o �a rl, /ia /ia rid /
19
Date
7,000
i iTi
5,000
n
n 4,000
m
w
u 3,000
r
1,000
TOTAL VOLATILE ORGANIC COMPOUNDS
VERSUS TIME IN MW-24
9 �9 'o '9 A 'o 1 '9 'o 'o 'o 'o 'o 70 go
0 7 ? 0 Q s 0 � � - � � s s 9 0
Date
TOTAL VOLATILE ORGANIC COMPOUNDS
VERSUS TIME IN MW-25
w
m
m
70
40
30
20
10
0 I --- -- - - - - - - 1 1 --I I l
vo �a Vol),
'0 70 ?o 'o �, go o 'o �� �W,
9 a 0 � s 6 j s 9 0
Date
Al
40
w
n
m
30
r
Wi
10
TOTAL VOLATILE ORGANIC COMPOUNDS
VERSUS TIME IN MW-42
Date
800
700
600
500
0
3
n
m
3
rr
°* 400
a
N
fa
Q
300
200
100
0
TOTAL VOLATILE ORGANIC COMPOUNDS
VERSUS TIME IN MW-43D
Date
--$-- Total VOCs
3
2
0
n
co
m
a'
TOTAL VOLATILE ORGANIC COMPOUNDS
VERSUS TIME IN MW-45
o6, oy
Date
0