WI0400176_Monitoring (Report)_20141014

Semi Annual Water Quality Monitoring Report
Prepared for
Surly County Closed C&D and Closed MSWLF, Mt. Airy
Submitted: October 1, 2014
P.D. Box 97
Garner, NC 27529
License No. C-0281
Mt. Airy, North Carolina
May 2014 RECEIVEDIDENR1DWR
OCT 14 2014
Water Quality Regional
Operations Sedon
UIC Permit Nurgber:WI0400176
SWS Facility Permit Number: 86-02
MESCO Project Number: G14432.0
Municipal p &N Engineering
_'
Mnmcipai Engmeenng Sen ices Company, VA
Garner and Boone, North Carolma

SECTION
Introductio:
Background --.Page I
Sampling Procedure _ _ �mm�mm�mmT Page 2
Field Parameter Data Paize 2
Laboratory Results _ _..m.�_ mm_ mm _ .Page 2
Groundwater Samples_ _ _ _ _ Page 3
Groundwater Characterization _ Page 3
Findings.__m.._...__._.___.___ Page 3
Closing_.. Page 4
FIGURES
Topographic Map with Site Location___ Figure 1
Potentiometric Map of Uppermost Aquifer wl VOCs Detected Above 2L Standards�Figure 2
Total Cumulative VOC Concentrations Pre/Post Injection Comparison. Figure 3
Bromide Tracer Concentrations Time Series Graph and Table Figure 4
Ir►:3IRS`
Sampling and Analysis 5ummary__.._._.__..._.._.._._. ........___
Table 1
Detections that Attain or are Above SWSL or 2L Standard
Table 2
Field Parameter Data Summary
Table 3
Hydrologic Properties at Monitoring Wells
Table 4
MNA Parameter Data Summary
__..Table 5
K-l",0r
Laboratory Analysis Report and Chains of Custody_________^_ _. _ _„m m ,Appendix A

License No C-CrZel
CtVILISANITARYIENVIRONMENTAI ENGINEERS SOLID WASTE MANAGEMENT
Municipal En �neerin
Services Cvrt�pany, P.Q.
SITE PLANNINGISUBDTV1SIONS :Sue
SURFACE IITILMY ENGINEERING (SUE)
October 1, 2014
Mr. Thomas Siusser, P.G.
Aquifer Protection Section -Underground Injection Control Program
Division of Water Quality
North Carolina Department of Environment and Natural Resources
1636 Mail Service Center
Raleigh, NC 27699-1636
Re: Semi Annual Water Qualitl, Monitoring Report
Surry County Closed C&D and Closed MSWLF, Mt. Airy
237 Landfill Road
Mount Airy, NC 27030
SWS Permit No. 86-02
UIC Permit No. W I0400176
MESCO Project No. G14032.0
Event Date(s) May 27-29, 2014
Dear Mr. Slusser:
Introduction
Municipal Engineering Services Company, PA (MESCO), on behalf of Surry County, appreciates the opportunity to
present this brief Semi -Annual ff'aler Quality Report that details a water quality monitoring event performed at the
Surry County Closed C&D and Closed Unlined Municipal Solid Waste Landfill (MSWLF) Facility (Permit # 86-02)
an May 27-29, 2014. The Injection Well Permit Application and Well Permit No. WI0400176 (4/15/13) requires
that Surry County provide this report to the Underground Injection Control (UIC) program on a semi-annual basis.
Laboratory analytical results indicate volatile organic compounds (VOCs) attributed to landfill activities continue to
persist in levels above 2L Standards at seven wells that monitor the uppermost aquifer downgradient of five
injection points. However, total VOC concentrations have decreased at all locations compared to their respective
baseline averages established during the five events prior to the first injection event performed in November 2011.
Background
The Surry County closed C&D and MSWLF, permit #86-02, is located at 237 Landfill Road in Mt. Airy North
Carolina. The site location topographic map is depicted in the attached Figure I_ Prior to becoming a C&D landfill
the subject area operated as a MSW unlined sanitary landfill that stopped receiving waste prior to January 1, 1999.
The MSWLF was closed with a low permeability cohesive soil cap per the Transition Plan. The top portion of the
southern unit served as an exclusive C&D landfill until prior to June 1, 2008 at which time it was properly closed
with another cohesive soil cap in accordance with the Closure Plan.
Per the SWS approved Corrective Action Plan enhanced bioremediation via substrate and tracer injection was
irrigated in the Southern and Northern AOCs in accordance with requirements outlined in the Injection Well Permit
Application and Well Permit No. WI0400176 (516/11) with the goal to reduce low level aliphatic and aromatic
chlorinated hydrocarbons in groundwater to below 2L Standards.
On November 2-3, 2011 an EOS-water emulsion with sodium bromide tracer was injected into three wells ( NV-2,
IW-3 and IW-5). Injection was attempted into IW-1 during this same event but due to the tightness of the formation
an insignificant amount (< 3 gallons of slurry) entered the uppermost aquifer_ For all intents and purposes IW-1
injection did not occur nor ever will be able to in the future. Monitoring of wells downgradient of this location will
continue to be monitored semi-annually as required by the NC Solid Waste Section (SWS). Any observed changes
in geochemistry downgradient of IWA is not attributed to the unsuccessful injection event. Details of the premier
injection event are provided in the Injection Event Record dated November 4, 2010.
PO Box 97. Garner. North Carolina 275`3 i919) 772-5393 PO Box 349 Boone. NC 23607 =8? 262-17S7

On October 24-25. 2012 similar substrates were injected into monitoring wells MW-411W-4 and MW-8I1W-6 in
fulfillment of Phase 2 of Corrective Action. Details of the second injection events is provided in the Injection Event
Record submitted January 10, 2013.
The LTIC injection Well Permit was renewed on April 15, 2013 which reduced monitoring frequency from
quarterly to semi-annually and the prescribed constituents listed in the approved application was also reduced
and vague.
Water quality at this facility has been monitored at ]east semi-annually since 1989 with historical data available
since 1994. This is the seventh post -injection water quality monitoring event with previous events performed on
February 9, 2012, May 30, 2012. August 20, 2012, October 23, 2012, May 29. 2013, October 29,2014. Previous
event reports have already been submitted to the UIC and SWS.
This report contains sampling procedures, field and laboratory results, groundwater characterization, and findings.
A potentiorretric map of the uppermost aquifer, time -series graphs of select constituents, a table of detections
compared to Standards, field data results table, groundwater flow directions/rates table and laboratory analytical
data results are also enclosed.
Sampling Procedure
MESCO personnel performed this sampling event targeting the parameters outlined in the JVarer Quality Sampling
and Analysis Plan (SAP) (DIN:18936) dated April 30, 2013 and approved by the SWS (DIN: 19938) on May 10,
2013. Monitored locations were consistent with the renewed Well Permit (4/15113).
Groundwater samples were collected and analyzed from fourteen wells which includes MWvR, MW-7, MW-9,
MW-12S, MW-13, MW-14, MW-16, MW-17, MW-18, MW-19, MW-20, MW-22, MW-23 and upgradient
background well MW-1. Additionally, water within all six injection wells were measured and visually evaluated in
an effort to determine the amount of residual organic substrate remaining in the wells which may help evaluate the
viability of these wells to be used for future water quality analysis. Monitoring locations are depicted on Figure 2.
Sampling was performed per the protocols outlined in the SWS approved Groundwater and Surface Water Sampling
and Analysis Plan which was submitted with the Corrective Action Plan (CAP) revision 2 dated December 10, 2010.
The depth to water in each well was electronically gaged prior to purging to quantify the static water level elevation.
Low -flow pumping methodology or bailing was utilized to adequately purge the wells a minimum of three well
volumes or until dry. During purging the stabilized field parameters were recorded. The samples were then placed
into laboratory -prepared, pre -preserved containers via a new disposable polyethylene bailer. Samples were kept on
ice, and transported within hold -times to a NC -certified laboratory under proper chain of custody (C-O-C) protocols.
Field Parameter Data
Field parameters recorded included depth to water, pH, specific conductance, temperature, dissolved oxygen (DO),
oxidation reduction potential (ORP), total dissolved solids (TDS) and turbidity. A summary of the field parameter
data since injection is presented in 'Table 3.
Laboratory Results
Pace Analytical Laboratories (PACE) of Huntersville and Asheville, NC performed the majority of the laboratory
analysis. Groundwater samples were analyzed for all the parameters requested by the SWS which includes
constituents listed in Appendix 1 of 40 CFR 259 plus select monitored natural attenuation parameters (MNA) at
select locations. Environmental Conservation Laboratories (ENCO) of Cary, NC analyzed select samples for the
bromide tracer. A sampling and analysis table summarizing the locations, target parameters and laboratory methods
is presented as Table 1. Water samples were reported at the laboratory specific Method Detection Limits (NOL),
which are quantifiable at or below the current Solid Waste Section Limits (SWSL). Laboratory results and C-O-Cs
are presented in Appendix A.

Groundwater Samples
The wells with Appendix I VOCs detected in concentrations in exceedance of their respective 2L Standard during
this event include MW-9 (I.4-dichlorobenzene, benzene, vinyl chloride), MW-13 (1.2-DCA). MW-14 (PCE), MW-
15 (PCE. TCE, 1.2-DCA. 1,1-DCA, benzene, vinyl chloride), MW-16 (I,4-dichlorobenzene, 1,2-DCP, 1,2-DCA,
benzene, vinyl chloride), MW-21 (1,2-DCA, i,l-DCA) and MW-22 (1,2-DCA). Although not regulatory applicable
the only constituents detected above the EPA established maximum contaminant levels (MCLs) or primary
"Drinking Water Standards" were vinyl chloride (NM-9, MW-16) and 1,1-dichloroethene (MW-15). Table 2
summarizes constituents detected in groundwater samples in concentrations above the current SWSL or North
Carolina Groundwater Standards (2L). MNA data presented in Table 5 continues to indicate that favorable
geochemical conditions exist for continued natural attenuation.
A site map depicting the concentrations and estimated horizontal extent of VOCs that exceeded the 2L Standard
during this event is presented on Figure 2.
Groundwater Characterization
A potentiometric map of the uppermost aquifer created from static groundwater elevations recorded during the May
2014 event is included as Figure 2. Groundwater flow rates and directions were calculated via modified Darcy's
equation and are included in Table 4. Groundwater flows in the unconfined and upper bedrock water -bearing zones
in a general southwesterly direction away from the waste limits. Calculated groundwater velocities were variable
but consistent compared to historical observations.
Findings
The laboratory results indicate that dissolved phase VOCs consisting primarily of chlorinated hydrocarbons continue
to be detected in groundwater samples collected from seven wells. All VOCs detected in concentrations above the
2L Standard during this event remain within their own respective historically identified range. Total cumulative
VOC concentrations were lower during this event compared to their own respective five event averages established
prior to injection in all locations as shown on Figure 3.
Evaluation of the injection wells (iW-1, lW-2. [W-3, iW-4, IW-5 and IW-6) continues to indicate that a considerable
amount of residual organic substrate remain in each of these wells rendering them unsuitable for representative
water quality analysis. The viscosity of the water in the injection wells precludes sample collection as either a
bailer would not descend or the check valve failed.
In an attempt to track migration of injectants bromide was targeted at MW-3R, MW-13, MW-14. MW-15. MW-16, .
MW-21 and background well MW-1. MW-16, located 86 feet downgradient of 1W-3, is the only location
exhibiting, tracer levels which may potentially indicate injectant communication. Based on the average linear
velocity rates of 1W-3 and MW-16 reported since injection the injectant was expected to reach MW-16 in May 2012.
Bromide concentrations exhibited a consistent increasing trend in MW-16 the first year following injection then has
decreased the last year (Figure 4). Calculations performed following injection indicates that reported levels of
bromide injected was insufficient to provide clear evidence of migration within the uppermost aquifer.

Closing
Water quality monitoring is planned to continue with the next event scheduled for October 2014. No further
injections are planned at this time but if they do Permit conditions will be met including giving the UIC advance
notice prior to installation or injection of any addition a] weII(s).
If you have any questions or comments regarding this report, please contact us at [phone] or by email at
infoli] rni mesco.com.
Sincerely,
MUNICIPAL ENGINEERING SERVICES CO., P.A.
LQ';
Jonathan Pfohl
Environmental Specialist
Enclosures
cc: Mr. Dennis Bledsoe
Surry County
Ms. Jaclynne Drummond (Electronic Copy Only y
5WS-Compliance Branch
Ms. Shuying Wang (Electronic Copy Only)
UIC

Figures

Topographic Map with Site Location
Surry County Closed Unlincd C&D and Closed Unlined MSWLF, Mt. Airy
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.- Sal. a •'!�` h.l ,.. ( . r, _ t M . 'l~�[
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-51
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237 Landfill Road ROAD CLASSIFICATION
Mount Airy, NC 28621 Primary highway, improved
road, Hare or
hard surface.. mproved surface
Lat:36-26-30A65 Secondary highway,
Lang•-80-34-15314 hard surface --. — Unimproved road .---___--
Northing:983356.18 Interstate Route 0 U. S. Route (DState Route
Easting:1537885.48
Closed Lnlincd C&U Landfill
Closed Unlined Sanitary Landfill
1 0 1 MILE
FIGURE 1

237 LANDFILL ROAD ""'"-"
—+ o
-- - o
NOW OR FORMERLY
OWNED BY
JOHNN Y COX
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IW-4
M.32
983A,
NOW OR FORMERLY OWNED B Y
I SHA WNA SUMMERS
EXISTING TOPOGRAPHIC CONTOURS
EXISITING ROADS
ESTIMATFD WASTE LIMITS UNLINED MSW do/OR C&D
LINER LIMITS OF SUBITLE D LINED MSWLF (MONITORED SEPERA TEL Y)
EXTENT OF COHESIVE CLAY CLOSURE UPON CLOSED MSW AND C&O
PROPERTY LINE EXTRAPOLATED FROM SURVEY AND GIS
- COMPLIANCE BOUNDARY (250' FROM EOW or 50' FROM PROPERTY LINE)
EXTENT OF VOC(s) DETECTED ABOVE SWSL & 2L STANDARD BEYOND COMPLIANCE BOUNDA
--•1090— ECIUIPOTENTIAL UPPERMOST GROUNDWATER CONTOURS
STREAM/CREEK/RIVER
WATER SUPPLY WELL (FACILITY CONSIDERS IT NON -POTABLE)
SW 1 44 SURFACE WATER MONITORING PUNT
NW-10 MONITORING WELL
NW2 IN ECBON WELL (NOT SAMPLED DURING THIS EVENT)
9760 GROUNDWATER POTENTIOMETRIC ELEVATION (AMSL)
•NOTE:ELEVATION NOT USED FOR CONTOURS
® SEDIMENT BASIN
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FIGURE 2
Sim.
CLOSED C&D LANDFILL and
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CLOSED MSWLF FACILITY
Municipal
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Figure 3
Total Cumulative VOC Concentrations PrelPost Injection Comparison
October 22, 2009 - May 28, 2014
.fw„waNwwfM, v m �,teW •=rwwnw sae [�c.�.n.er�.a •. /4 r+ frrf�
uvfw1W.U��� 1 M� �rao�C.�M. voC i.neMYMrf w IVf - fivff I
O:
LU
U :
UUJ
dwfnowv Ywf p w•� Itew Cw�w YOGG��wa�m•f •• Mx n 1�1�
me1w�no�nr v w f iTa� L1w.wen we una.ww-, ...w n fwn, i
r
Average of
first Five
Corrective
Oct May Oct May Oct Action May Statistical Trend'
2009 2010 2010 2011 2011 Events 2014 Difference Difference Between Oct
Well ID (uglL) (uglL) (ugll-) (uglL) (uglL) (uglL) (uglL) (uglL) (°Io) 2009-May 2014
INJECTION WELL (IW-1) UNSUCCESSFUL INJECTION SO DOWNGRADIENT WELLS NOT SHOWN
INJECTION WELL (IW-2) MONITORED DOWNGRADIENT BY MW-12S, MW-13 & MW-18
MW-12S 0.00 0.00 0-00 0-00 5-40 1.08 0.00 -1.08 -100 No Trend
MW-13 61.00 50.60 74.20 87.30 72.50 69.12 20.50 -48.62 -70 Downward
MW-18 0.00 0.00 0.00 0-00 0-00 0-00 0.00 0.00 0 No Trend
INJECTION WELL (IW-3) MONITORED DOWNGRADIENT BY MW-3R & MW-16
MW-3R
0.00
0.00
0.00
0.00
0.00
0-00
0.00
0.00
0
No Trend
MW-16
137-90
113-60
135.70
121.20
116.30
124.94
81.50
-43.44
-35
Downward
INJECTION WELL
(IW-4}
MONITORED DOWNGRADIENT BY MW-14, MW-21 & MW-23
MW-14
15.20
15.60
15.60
8.20
17.00
14.32
0.00
-14.32
-1�00
No Trend
MW-21
52.10
50.70
51.38
39A0
32 41
45.14
27.90
-17.24
-313
Downward
MW-23
4.30
0-00
0-00
0.00
0.00
0.86
0-00
-0.86
-100
No Trend
INJECTION
WELL
(IW-5] MONITORE❑
DOWNGRADIENT BY MW-15 & MW-19
MW-15
96.13
63.89
55.00
7&10
64.06
71-44
58.99
-12.45
-17
No Trend
-
MW-19
0-00
0-00
0.00
0.00
0.00
0-00
0.00
0-00
0
No Trend
INJECTION WELL (1W-6) NOT SHOWN AS NO WELLS DOWNGRADIENT WITHIN ZONE OF INFLUENCE
= Statistical Trend analysis via Sen's Slope Estimator at a 95% confidence level
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1

Figure 4
Bromide Tracer Concentrations Time Series Graph and Table
February 9, 2012 — May 28. 2014
Bromide Tracer Levels in MW-16
Located 87 feet ❑owngradient of IW-3 which was Injected on November 2, 2011
0.3000
0.2500
0.2000 -
1
0.1500
0.1000
0.0500
0.0000
141
Date
♦ MW-16
Date MW-16
219/2012
0.0380 0)
5/30/2012
0.13000)
8/20/2012
0,26000)
10/23/2012
0.2800 0)
5/30/2013
0.14000)
1 W31l2013
0,11000)
5/28/2014
0.2200 U)
0) = The reported value is between the laboratory method detection limit (MDL] and the laboratory method reporting limit (MRL),
= May 25. 2012 Calculated date injectant expected to reach MW-16 using average flow rates of IW-3 and MW-16 (155 tVyr) since injection occurred.
Surry County Closed C&❑ and Closed MSWLF. Mt. Airy Page 1 of 1

Tables

ry
FL
x
00
N_
0
0
3
c
3
A
C7
{7
th
po
W
N
h
rR)
i
N
Q
Co
-+
w
V
-►
M
-►
Lh
-+
�
i
w
-+
N
en
f�
V
L�
.'b
i
m
m
m
m
m
m
Reason Not Sampled
x
xxxxxxxxxxxxxxx
x
1
x
x
LabEPA8260B
VOCs
Total Metals
b
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
Lab EPA 6000/7000
—
x
Lab EPA 82608
1,3-Dichlorobenzene
x
x
x
Lab EPA 6000/7000
Total Metals (App II)
y
x
Lab 7470
Mercury, total
x
x
x
x
X
x
x
Lab EPA 9014
Total Cyanide
x
x
x
x
x
x
Lab SM18 4500-S D
Sulfide
x
x
x
x
x
x
EPA 310.2
Alkalinity
x
x
x
aL
rc
x
Lab RSK 175
Methane, Dissolved
x
x
x
x
x
x
EPA 300.0
Sulfate
x
x
x
x
x
x
Lab SM18 4500-S D
Sulfide
x
K
x
x
x
x
EPA 300.0
Chloride
a
n
x
x
x
x
x
x
SM 5310E
TOC
x
x
x
x
x
x
SM 52200
COD
x
x
x
x
x
x
Lab EPA 6010
Iron, total
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
field Meter
Dissolved Oxygen (DO)
k
x
x
x
x
x
x
x
x
x
x
x
x
x
I
x
x
Field Meter
Oxidation Reduction Potential (ORP)
?I
Lo
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
Field Meter
Temperature
-v
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
Field Meter
Conductivity
su
R
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
Field Meter
otal Dissolved Solids JDS)
W
x
x
x
x
x
x
x
x
x
x
x
x
k
x
x
Ix
IlField Meter
pH
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
Field Meter or Visual
Turbidity
x
x
x
x
x
x
x
f EPA 300.0
Bromide
w

Table 2
Detections in Water Samples above SWSL or 2L Standards
May 27-29, 2014
ample
parameter Name,
Sam
Result
Unit
MDL2
SWSL 3
2L,
MCL i
2L
Exceedance
ID
Amount
MVI1-7
1,4-Dichlorobenzene
5/28114
2.7
uglL
0.33
1
6
75
MW-7
Antimony, total
5/28/14
9.8
uglL
5
6
NE
8A
MW-7
Chlorobenzene
5128114
5.7
uglL
0.23
3
50
100
MW-7
Cobalt, total
5/28114
77.3
uglL
5
10
NE
7.3
MW-9
1,4-Dichlorobenzene
5128114
6.6
uglL
0.33
1
6
75
0.6
MW-9
Benzene
$128114
3.3
uglL
0.25
1
1
5
2.3
MW-9
cis-1,2-Dichioroethene
5128114
5.7
uglL
0.19
5
70
70
MW-9
Cobalt, total
5128/14
140
uglL
5
10
NE
70
MW-9
Vinyl chloride
5/28114
10.8
uglL
0.62
1
0.03
5
10-77
MW-13
1,2-Dichloroethane
5128114
0.47 j
uglL
0.12
1
0.4
5
0.07
MW-13
cis-1,2-❑ichloroethene
5128114
19.3
uglL
0.19
5
70
70
MW-13
Trichloroethene
5128114
1.2
uglL
0.47
1
3
5
MW-14
Tetrachioroethene
5128/14
0.891
ug1L
0.46
1
0.7
5
0.19
MW-15
1,1-Dichloroethane
5128114
14.2
ug1L
0.32
5
6
7
8.2
MW-15
1,2-Dichloroethane
5128/14
0.58 j
uglL
0.12
1
0.4
5
0.18
MW-15
1,4-Dichlorobenzene
5/28/14
3.6
uglL
0.33
1
6
75
MW-15
Benzene
5128114
2.3
uglL
0.26
1
1
5
1.3
MW-15
cis-1,2-❑ichloraethene
5128/14
35.2
uglL
0.19
5
70
70
MW-15
Tetrachloroethene
5128M4
0.74 j
uglL
0-46
1
0.7
5
0.04
MW-15
Trichloroethene
5128114
3.6
uglL
0.47
1
3
5
0.6
MW-15
Vinyl chloride
5128114
1.9
ug1L
0.62
1
0.03
5
1.87
MW-16
1,2-Dichloroethane
5128114
2.4
uglL
0.12
1
0.4
5
2
MW-16
1,2-Dichloropropane
5128114
3.2
ug1L
0.27
1
0.6
5
2.6
MW-16
1,4-Dichlorobenzene
5128114
15
ug1L
0.33
1
6
75
9
MW-16
Antimony, total
5128/14
15.9
uglL
5
6
NE
14.5
MW-16
Barium, total
5128/14
117
uglL
5
100
2000
2000
MW-16
Benzene
6128114
1.8
uglL
0.25
1
1
5
0.8
MW-16
Chlorobenzene
5/28114
5.B
uglL
0.23
3
50
100
MW-16
cis-1.2-Dichloroethene
5/28/14
46.6
ug1L
0.19
5
70
70
MW-16
Cobalt, total
5/28114
325
ug1L
5
10
NE
255
MW-16
Thallium, total
5/28114
9.5
uglL
5A
5.5
2
9.22
MW-16
Vinyl chloride
6128114
6.7
uglL
0.62
1
0.03
5
6.67
MW-16
Zinc, total
5128/14
13.5
uglL
10
10
1000
5000
MW-17
Cobalt, total
5/28/14
44.3
uglL
5
10
NE
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 2

Sample Sample a s 2L
ID Parameter Name, Date Result Unit MDL SWSL 2L• MCL Exceedance
Amount
MW-19 Vanadium, total 5/27114 6.4 j ug/L 5 25 NE 2.9
MW-19 Zinc, total 5127114 10.1 ug/L 10 10 1000 5000
MW-20 Cobalt, total 5127/14 14.2 ug/L 5 10 NE
MW-21
1,1-Dichloroethane
6128/14
6.3
uglL
0.32
5
6
7 0.3
MW-21
1,2-Dichloroethane
5128114
0.42 j
uglL
0.12
1
0.4
5 0.02
MW-21
cis-1,2-Dichloroethene
5128/14
20.1
ug/L
0.19
5
70
70
MW-21
Trichloroethene
5128/14
1.5
ug1L
0.47
1
3
5
MW-22
1,2-Dichloroethane
5128/14
0.51 j
ug1L
0.12
1
0.4
5 0.11
MW-22
1,4-Dichlorobenxene
5128114
2A
ug/L
0.33
1
6
75
MW-22
Cobalt, total
5128/14
37.3
ug1L
5
10
NE
EB
Methylene Chloride
5129/14
1 j
ug/L
0.97
1
4.6
5
1 Table contains Appendix I constituents detected at or above SWSL. GWP, 2L, or 2B
2 MDL = Method detection Limit
3SWSL = Solid Waste Section Reporting Limit
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard
s MCL = Maximum Conlaminant Level ("prinking Water Standard') not applicable regulatory Standard but shown for comparison purposes
} =The reported value is between the laboratory method detection limit (MDI_) and the laboratory method reporting limit (MRL),
adjusted for actual sample preparation data and moisture content, where applicable
BOLD = Concentration > 2L, or 2B Standard
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 2 of 2

Table 3
Field Parameter Data Summary
May 27-28. 2014
Parameter
Units
Depth to
Water'
ft (bloc)
Water TOC
Elevation Elevation
ft (amsl) ft (amsl)
Temp.
C
ORP
mV
❑O
mg/L
pH
5U
Specific
Conductance
umhoslctn
T_DS
mg1L
Turgidity_
Visual or NTU
MW-1
24-80
1109.55
1134-35
14-8
201
2.3
6.03
300
140
16-2
IW-2
39.61
1029.25
1068,86
NR
NR
NR
NR
NR
NR
>1000
MW-3R
X95
986,55
1017.50
15.2
119
0.5
7.82
200
90
Clear
IW-3
4U7
979.80
1020.57
NR
NR
NR
NR
NR
NR
>1000
IW-4
33-94
992.32
1026-26
NR
NR
NR
NR
NR
NR
>1000
IW-5
39.94
1040,24
1080.18
NR
NR
NR
NR
NR
NR
>1000
MW-6
22.38
1045,29
1067,67
13-9
-23
1-1
6-35
500
240
Slight
MV11-7
1 1-81
1061.69
1073,50
14.6
201
2-6
5-43
330
160
18.1
IW-6
40,98
1047.47
1088-45
NR
NR
NR
NR
NR
NR
>1000
MW-9
32,99
1061.08
1094-07
15-9
30
0.1
6,27
480
240
13.1
MW-12S
13.38
1012.42
1025-80
14.0
60
3-3
7-26
410
200
Clear
MW-12D
0.00
1027.05
1027,05
14.1
-91
1.4
7-35
160
120
Clear
MIN-13
25.23
983,25
1008.48
14.6
206
2-3
5,30
250
120
Clear
MW-14
35.39
983.41
1018,80
14.3
21
2.2
5,26
100
50
20.1
MW-15
51.12
1024.84
1075-96
14.8
27
0.4
5,32
140
70
>1000
MW-16
25.69
973.85
999-54
16-0
82
0.6
5,74
520
250
Clear
MW-17
8.39
957.04
965.43
13.1
78
1-4
6,05
310
150
Clear
MW-18
9.17
973.83
933.00
13-0
191
6.3
5,81
30
10
Slight
MW-19
9.84
936-43
946.27
13-1
273
3-0
5,52
50
30
Slight
MW-20
19.41
1062,78
1082-19
13.4
201
1.2
5,38
80
40
Clear
MW-21
5.44
959-92
965.36
13.7
203
1.9
5.01
210
100
163
MW-22
5.22
94&18
95140
16.4
233
4.1
5,83
280
140
Clear
MW-23
7.39
947.92
955.31
K7
211
4.3
6.98
100
40
Clear
Minimum
0,00
936.43
946.27�
13.0
-91
0.1
5,01
30
10
13-10
Average
2121
1006.27
1029.48
14.4
124
2.2
6.04
247
122
Slight
Maximum
51.12
1109.55
1134.35
16.4
273
6-3
7,82
520
250
>1000
btoc = Below top of casing
amsl = Above mean sea level
na = Not available
NR = No reading attempted
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1

Table 4
Hydrologic Properties at Monitoring Well Locations
May 27-28, 2014
Groundwater
Average Groundwater
Hydraulic Effective Hydraulic Linear Groundwater Potentiometric
Conductivity Porosity Gradient Velocity Rate depth Elevation
Monitoring
o
t lo)
jfeeti"feetj
(feetlyear)
Flow
(feet bloc)
{feet amsl}
Screened Interval
Well
(cm/second)
Direction
Lithology _
MW-1
4.30E-05
15
0.083
25
S18W
24.80
1109.55
Clay
IW-2
4.30E-05
15
0.024
7
576E
39.61
1029,25
Clay
MW-7
8.10E-04
15
0.319
1.785
N84W
11.81
1061,69
PWRIFractured Rock
IW-6
4.40E-04
15
0.113
342
S14E
40.98
1047,47
PWRIFractured Rock
MW-9
1.90E-04
15
0.038
50
S53E
32.99
1061.08
Sandy Silt
MW-13
2.06E-04
23
0,063
59
S36E
25.23
983.25
Saprolite
MW-18
2.04E-03
15
0.117
na
S39E
9.17
973.83
Saprolite
MW-19
1.10E-03
3
0,093
3,519
S14W
9.84
936.43
PWR
MW-21
1.28E-03
3
0.033
1,453
S55E
5.44
959.92
Saprolite/PWR
MW-22
9.88E-04
15
0.120
821
S29W
5.22
948.18
Saprolite
MW 23
3.04E-04
15
0.154
324
S40E
7.39
947.92
Sandy Sift
_
Minimum
4.30E-05
3
0.024
7
-
5.22
936.43
-
Average
6.77E-04
14
0.105
838
-
19.32
1005.32
-
Maximum
2.04E-03
23
0.319
3,519
-
40.98
1109.55
-
MW-3R
2.40E-04
5
na
na
na
40.77
976.73
Fractured Rock
IW-3
2.40E-05
5
0.028
14
S40W
30.95
989.62
Fractured Rock
IW-4
1.10E-04
5
0205
466
S41E
33.94
992.32
Fractured Rock
IW-5
1.50E-05
5
0.161
50
S63W
39.94
1040.24
Fractured Rock
MW-0
1.90E-05
5
0.191
75
S80W
22.38
1045.29
Fractured Rock
MW-12S
na
3
0.104
na
SO4W
13.38
1012.42
Fractured Rock
MW-120
1.30E-06
5
na
na
na
0.0o
1027.05
Fractured Rock
MW-14
7.45E-03
3
0.305
78,438
S72E
35.39
983.41
Fractured Rock
MW-15
7.21E-05
3
0.190
473
S06W
51.12
1024.84
Fractured Rock
MW-16
2.82E-05
3
0.157
152
S40W
25.69
973.85
Fractured Rock
MW-17
2.94E-04
3
0.102
1,031
S64W
8.39
957.04
Rock
MW-20
1.92E-04
3
0.107
707
S03E
19.41
1062.78
Rock
Minimum 1.30E-06 3 0-028 14 - 0.00 957.04 -
Average 7.68E-04 4 0.155 371 - 26.78 1007.13 -
Maximum 7.45E-03 5 0.305 1.031 - 51.12 1062.78 -
NOTE' Values for hydraulic conductivity determined via slug test by GAL MESCD, or Joyce.
Hydrologic gradient from water levels recorded on May 27-28, 2014.
Wells screened entirely in rock were not utilized for Row directionslgradienls,
Screens that traverse both rock and regolith assumed Raw in regolith dominates.
Flow rate for MW-14 was considered an oullier. therefore not included in the average or maximum.
na = Not availablelapplicable
Average Linear Velocity (Q) is defined by modified Darcy's equation:
K A K= hydraulic conductivity
where Q = n - dl
' rne= effective porosity
dh= head difference
d7= horizontal distance
Surry County Closed C&❑ and Closed MSWLF, Mt. Airy Page 1 of 1

Table 5
MNA Parameter Data Summary
May 28, 2014
Parameters
VFA — Acetic Acid
Method MDL' Units
AM23G NS _ ug/L
MW-1
MW-7
MW-9
MW-14
MW-15
PAW-21
5128114
5128/14
5128114
5126/14
5/26/14
5128/14
NS
NS
NS
NS
NS
NS
VFA — Butyric Acid
JAM23G
NS
ug/L
NS
NS
NS
NS
NS
NS
VFA — Lactic Acid
23G
NS
ug/L
NS
NS
NS
NS
NS
NS
VFA — Propionic Acid
M23G
NS
ug/L
NS
J NS
NS
NS
NS
NS
VFA — Pyruvic Acid
AM23G
NS
ug/L
NS
NS
NS
NS
NS
NS
Hydrogen
AM20GAX
NS
nM
NS
NS
NS
NS
NS
NS
Methane
RSK175
400
ug/L
<400
93500
1530000 2'
1 1570
9570002'
<4QQ
iEthene
AM20GAX
N5
I ug/L
NS
NS
NS
NS
NS
NS
Ethane
AM20GAX
NS
ug/L
NS
NS
NS
NS
NS
NS
CO2-Dissolved
Field HACH Kit
NS
mg/L
NS
NS
NS
NS
NS
NS
kalinity
SM 2320B
1000
uWL
81500
79100
112000
32400
1 44000
34500
Sulfate
EPA 300.0
2000
ug/L
7940
6570
1 a2000
2210
<2000
<20D0
Sulfide
SM 4500-52❑
100
ugtL
e-100
<100
--100
<100
<100
<100
Chloride
SM 4500-C1-E
1000
_ug/L
3270
28800"
45100 5
2710
1890
27600
OC
SM 531QB
1000
ug/L
2960
13900
8070
5666
8670
10700
COD
SM 5220D
25000
ug/L
<25000
35000
33000
<25000
<25000
45000
BOD
SM5210B
NS
ug/L
NS
NS
NS
NS
NS
NS
Iran
EPA 6010
50
ug/L
167
<50
449M
245
2640
<50
Nitrate
EPA 353.2
<20
1 uglL
NS
NS
NS
NS
NS
NS
Temperature
IField Instrument
0
C
14.8
2.6
15.9
14.3
14.8
13.7
ORP
Field Instrument
-900
mV
201
201
30
21
27
203
DO
Field Instrument
0
mg1L
2,3
2.6
0.8
2.2
0.4
1.9
pH
Field Instrument
0
5U
6.03
5.43
6.27
5.26
5.32
5.01
Speeft Conductance
Field Instrument
0
us/cm
300
330
480
10Q
140
210
Turbidity
Field Instrument
0
NTU
16.2
18.1
13.1
20.1
>1000
163
Notes:
MDL' = Lab Method Detection Limit or lowest field measurement possible.
Constituents detected below quantifiable limits are shown as c MDL value.
3100 = CO2 Concentration exceeds maximum capability of method used.
' Indicates dilution factor used
NS = Not Sampled
Surry County Closed C&D and CLosed MSWLF, MS. Airy Page 1 of 1

Appendix A
Laboratory Analysis Reports
Chains of Custody

V.- AnMyftsl a.rvluf, W. P.-A"yW.II.I-
�•.�. r—..r...... ,11dr.x17.RW.eincu2 WO.�SW- Ipn
Nr.Roe NL 2m7mce4fyt1Ca1 �Ajf��
wpm ra
L MA 1675• vpp2
June 12, 2014
Mr Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
REProject: Surry Closed-Mi. Airy RLIICj
Pace Project No.: 92203121
Dear W. Pfohl:
Enclosed are the analytical results for sarnple(s) received by She laboratory between May 28, 2014
and May 29, 2014. The results relate only To the samples included In this report. Results reperted
herein conform to the met current TNI standards and the laboratory's Ouality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Analyses were performed at the Pace AnaIylical Services location Indicated on The sample analyle
page for analysis unless otherwise footnoled.
It you have any questions concerning this repbn, please feel free to contact me
Sincerely,
Kevin Godwin
[e-mail]
Protect Manager
Enrlo.lirn.
REPORT OF LABORATORY ANALYSIS
rM r.wn rw notN r.vlen.c.d uapt n Air
..neuR M weNn win.frN o1 P— AnN11c.1 S.— rrr,
Pao. I el 73
N*cl: Sorry C7oeed Mt. Nry (LII C)
P.- Prolecl No. 9n031,11
Ch.AoIN Comk&twn ID.
9600 Kn ey Ave. SA* ,W, Hmle 01@, NC 2We
Moral Crean. DftN ho YI W CerI161:aBon ►. 377%
01 th CM ob" Fle1d Servlce. Certleteeon •. 33a2
Nerth Caca.N vo lter ter cvtiA tin, 0 12
5-1h C.rdmo CeR14Nlon /. 99006001
AsheyllN Cerurkarl9n 16s
2225 RwM W e Cf . AM"U.. NC 26604
flend.rNE LAP Cemllcavw/ E07W!
41.veohu.etl. Cerutlufm i' M NUM
rroM ri avAns L7r.l4
lno VA W Ceraicabon ■ 37i 12
CERTIFICATIONS
Ehmd.1NELAP Certd—eon /: E6162T
1Len11rclty LIST Cnrllerallon A. !{
Weal V.gr+e Ccrbrr v n /: 357
Ylrglr.IoNELAP Cnrtlec.lWn!' e80221
Norm C.Rdn. W-t-1. Cartlec~ /' e0
S.urh C.mm. C.Adc.h_ /: M30M
We.1 VYoI " C.rgmr .11at e. 356
Vlrgkll. WLAP COMI.O.n /' 46022;
REPORT OF LABORATORY ANALYSIS
lrw npPr dr.t nor Y npnrkcd �dr• n All
w�MM M wnr►n cwwwriMPary Nrryusr R»rr�. inc
PK. 2 PI 73

P—AnNy.wI 64-ca..
ce"I,y �OK.r rM'. & + Iw
+cal
. ;....�.� ;NMN7` 1
P—A..1y.-IIimniu Im-
p,� f
wwK vm. suw1OC
a��l'V M11 Dial•
H-W-A. Nc 200'M
.....v.e.�.
f7c41973i0�
PrU*o
$wry C1o.ed-MI My (LAC)
Ppc4 PrPl.ci N9.
92207121
Lab N
5—wi. ID
22303121001
MW-126
92203101002
1A W 11
12207121003
MW-11
92207121004
MW21
9220312100E
MW-1
9220112100L
MW-7
92203121007
MW-11
2220312IDDS
MW41
022031210DO
MW-6
12203121010
MW-14
12293121011
MW-3R
92207721012
MW 15
92291121013
mw•17
922JJMW14
MW20
92203121016
Mw•11
92205121016
MW22
97203121017
AIW.19
SAMPLE SUMMARY
M.tru
Ow Co0.clad
Dal. R.calyad
mw
=711414:35
0512MI 17:00
yvAler
OW2711413:30
O6f261141740
Aw.r
0=71141510
ON2&1417:00
Aims
M71141"
OW2W1417;00
W1l.I
092&14 00 05
05e2sn415.20
yimrer
0512IV 14 12 00
05QW141520
Waln
OW80140945
05R90141520
%%Ier
WM1411.40
MOF141920
v"t.r
05r20J14 11 ]5
0512VIA W20
we1e,
OSJ-2&141015
05129M416,20
W.1.r
05r2W1406:40
05FS9114 IL20
W i r
054&1411:00
054MIA 15:20
W.I.
ON7&1415.10
Osl29/1415:20
v wtei
0YL7114 06:05
=oil-t 1510
Weln
0Y2&1409: 10
05,79t1415.70
M lar
05r2W414 35
MW14 1520
vw.r
054704 15:10
OW14 "=
REPORT OF LABORATORY ANALYSIS
r1....>an .nr ro1a. r.praducW..,r.yl ., nn.
•..aW .r .1r.1.n uwrwM cal Pas. A-,y," S.,—. iz
P.Oc ],,173
PI.)-1
P.ca ProJKS Nc.
Scary 0.d-M1. Airy (NCI
922p1121
SAMPLE ANALYTE COUNT
Andye..
Lab 10
swnp1. 10
M Wl d
A"y.I.
kapmWd
Labwamly
12201171061
MNF176
EPA901D
JMw
15
PASI.A
EPA 6260
MCK
51
PAS1.0
W293121002
MW76
EPA 6010
JMW
15
PASI-A
EPA 6250
MCK
51
PASI-C
92W3121001
MW79
EPA 6010
JMW
15
PASl-A
EPA=0
MCK
51
PASI-C
12203121004
MW23
EPA WI
JMW
15
PAS1-A
EPA 6260
MCK
71
PASI-C
92213121J106
AIWI
EPA 6010
JMW
16
PASI-A
EPAUN
NIJ1
51
PA&C
SM 2320H
Mow
1
PASI-A
SM 4500$2n
SAE
1
PASaA
EPA 1000
SAE
!
PA ,A
SM 450o-C4E
s"
1
PA& -A
9M 45MCN•E
JDA
1
PASJ A
SM 5220D
EWS
I
PASI-A
SL153toe
SAE
1
PAS -A
922W121006
MW7
EPA 6010
JMW
15
PASJ•A
EPA 6260
NV1
51
PAW
Ski 2320
MOW
1
PASI-A
sm 450011M
SAE
1
PASr-ll
EPA 3000
SAE
1
PASI•A
SM 4600CI-E
SMw
1
PA51 A
SM 4500-CN-E
JDA
1
PASI A
SM 57200
EWS
I
PASI-A
SM 5210B
SAE
I
PAST -A
12203121DO7
MIN-15
EPA6010
JMW
16
PASJ-A
EPA 9260
Nul
5l
PASFC
Sm 23204]
MDW
1
PAS1-A
SM 450D520
SAE
I
PAST -A
EPA MG (I
SAE
I
PASI-A
SM 4500-CI-E
SMW
1
PASI-A
SM 4500-CN-E
JDA
I
PAST -A
SM S2200
EWS
I
PAST -A
SM 531013
SAE
I
PAST -A
92207171009
MVW21
EPA 6010
JMW
1E
PASI-A
EPA 6260
NU1
51
PASJ-C
REPORT OF LABORATORY ANALYSIS
11..r.wn 1n.4 rota r+pna.rw...e.pn an
..nwl.r wr+Iwr w 1 eJ P.0 An irry So— u..
P.g. 4 01 73

p— Analytleal
aarvle.j. Inc
2ceiVk11
Poo An*~ soco n4. aK
la
Pa1111rLAlll �LQI•
....,..�,r<u....
We.. A- 5� i00
rl�n^rprl,. NC MM
i7GMIgT54A1
/rai•
) �
! •r••.++` nr.
9AXKn.A� 5W.IM
�IO{1975AWi
SAMPLE ANALYTE COUNT
SAMPLE ANALYTE COUNT
R^Jeci: Slurs Cloand MI A.ry µNIC.)
ProJesl Surly CIm mql MI A," {il1Gl
Pace RnJeel Na . 9220112T
Pete Plopd NP 92201121
Arlalylaa
APalylra
L&h 0 S—pi. W
1Mthnd
Aaalyll,
A.panad
Lah—iory
Lb IQ SAmPM 10
Meehcd
Anarysla Rap^rlyd Lahvmwry
SM 2120E
MOW
I
PASI•A
$M 4500-"-E
JCA I PAST A
SM 4500SZD
SAE
1
PASI.A
Y220312t017 mvP119
SM 45001CNJ E
JOA 1 PASI-A
E PA 30O0
SAE
1
PASI-A
SM 4500-0 E
S"
I
PASI-A
SM 4500-CN-E
JOA
1
PASI-A
SM 122003
EWS
1
PASI-A
SM 50106
SAE
I
PASI A
121011219 MW-a
FP mlo
JMW
16
PASI A
EPA5260
Nol
51
PASIO
SM21208
MOW
I
PASHA
5M 4500-$20
SAE
1
FASI•A
EPA 3000
SAE
I
PASHA
510 000-10I.E
SMW
I
PASI-A
SM 52200
EWS
I
PASI-A
SM 53108
SAE
I
PASI•A
101203121410 MW-14
EPA6010
JMW
16
PASHA
EPA 1410
MTS
1
PASI-A
EPAIZ60
NUN
51
PASI-C
SM 2320B
MOW
I
PASI-A
$M 4WO-52❑
SAE
I
PASI A
EPA 300.0
SAE
I
PASI•A
SM 4%0-c1-E
SMYV
I
PASI-A
SM 52200
EWS
I
PASI-A
$M 53108
SAE
N
PASI.A
92200121nfT MW 3R
EPA5010
JMW
15
PASI A
EPA 9200
NUI
51
PASI-C
12207121012 MW.17
EPA601❑
JMW
15
PRS1-A
EPA v"
NUI
51
PASHC
92203121011 Mw.17
EPA5010
JMW
15
PASI-A
EPAl260
NUN
51
PASI-C
9220312TO14 MW-20
EPA15010
JMW
15
PASI-A
EPA 0250
NUI
51
PASI-C
922011"0113 MWti
EPA6010
JMW
15
PASI-A
EPA6260
NUN
52
PASI•C
SM 4500-CN•E
JOA
1
PASI-A
122031210% MW 22
EPA6010
JMW
13
PASI-A
EPA 5200
NUI
51
PASI-C
REPORT OF LABORATORY ANALYSIS
REPORT OF LABORATORY ANALYSIS
Ti.. r.PM YrY reel ta. nl�pdrRrp ..t+M ^ 0.A.
T .sport vnr m1 [. npmdic.a ..c.q n nn
.ahoue v., ,Mwn anaeni N�'f[. H..g1va� S.n.x. wti
P.O. 5 of 73
«Ma e1, y.dyn [arr..r.l er P,p. ana4..-.r .sarrcwa ^.
P4pa 6 oT 73

�dCeAnalyfiml r
ANALYTICAL RESULTS
044. Aowvq Fl 6.nl..s, Ins
sass K-v A" 5LW I
170411754)092
prated Sorry C4a44Mt. ANY Wl
Pace Project No. 92203121
Sample- MW-12E
L.trlAlt 9220112]001
C&WL4.d 052704 $4:35 R.ae1Wd: 052S114 17'00 Mani.. AM1m1er
R.pod
P... M.wm
R-Wis Lkwil,
Linul
MOL
OF
W.pred Anulyred CAS No 0.01
40101CP ummltW47.r
Artalyllcal W.": EPA Hots Prepwa6nn
Method. EPA3010
Anomaly
NO a&
0.0
5.0
1
M211415:56 03l1W14 19.59 7440.16.0
A,-
NO uQ&
100
SO
7
OWW1415: S5 051701141950 7440-36.2
Sal-
22.4J UWL
100
5-0
1
05QW1415-,M D50M141969 7440-39-3
Oerylaynr
NO upt
10
1 0
1
067W1411 $5 OSW14 t9 50 744041-1
Cadrtwm
NO -a&
1.0
7-0
1
054911414:55 0513W741959 744043-9
Ch.uttw.m
NU ugA,
10.0
SA
1
062W14 15:65 OSr3W14 19'S9 744047-3
Couall
NO ug4
$0.0
5-0
1
0L2W 14 15'56 OS71W14 *-59 7440.4a-4
Capper
NO ug&
10.0
5.9
1
05r2911415;55 051W1419:59 7440.504
i..d
NO.9&
10.0
i,d
1
M9014 ISSS OWNY1410,50 7439-02.1
ma.1
NO u67L
50.0
5.0
1
0529714 1615 0573N 1419'59 7440.024
Selorw.m
NO ug&
10.0
10.0
1
W21rIA 1S.SS 115110r14 1919 774112d9.2
Sal-
NO uS1L
10.0
5.0
1
062W14 15;55 0513W14 19:59 7440,22-4
Trurlwm
NO WA
5.5
5.4
1
MV1415;SS 05r3W141931 744("B-0
V.n.dunt
NO ug1L
26-0
so
I
OSR9114 16:35 0 001I4 19;50 i4404t2-2
Zatc
NO uUIL
10.0
too
1
05r2W14165S OW3W1419:59 74411.66A
6210 MaV Low L.T.I L1ndf1M
Anetybc.l M.1hod: EPAS260
Acelwie
NO.0A
too
10a
7
052791423i2 V-04-1
ACIylnndNe
NO uOrt-
200
19
1
O512W7421:52 $07.13-1
8a 1-
NO u9iL
1 0
025
1
OWlhrl4 23:SR 71.43-2
&omeudo omanan.
NO uW.
10
0.17
1
OWW14 2152 74.47.5
Sraow.eduwwnear.ne
NO ud%L
1 0
0.10
1
052111114 23:52 75-27-4
6romulo-
NO vq,L
30
016
1
062W742152 7545.2
Ernrnamnmmn.
NO ug(L
too
0.29
1
OSRW1423'52 74-63.9
2 Bumnone (ME75)
NO ugli
T00
0.96
1
OWW14 23:S2 7691.3
Carbon d•wlAde
NO uVIL
700
1.2
1
OWArl4 23:52 76-0-0
Cara- te9ucM.I&
NO W&
1-0
0.25
1
05/2911423;52 56.23.5
CItlr.r0berl74rl4
NO uWL
3-0
023
1
OSrlW 147312 104.90-7
CpWraethene
NA rWL
100
054
1
05r2W1427:52 75-00-3
Cltlurolmm
NO UNA
50
0.14
1
(&M 147332 674W3
C11Wram lh"
NO uW1
10
0111
1
O5f791142152 74.07.3
12-Olhromn-3 cMor.Wgpmm
N13 uA
13.0
2-6
1
05r29014 23-52 05-724
OfbronlodlWfathAlta
NO u04
1.0
0.21
1
OUM1421;52 724-45.1
12- Olb.nwa9,lga(EOBI
NO uA
1.0
0.27
1
05QW$423:52 $06.04
Oblomarrlelh,im
NO-Q&
too
021
1
054tvidl 23152 74-20-3
124 1.1tim bbam-
NO uA
5.0
0.20
1
oS2W 14 23'S2 05-SO-1
1.4.OkhlaebanzMla
NO uOIL
1.0
0.33
1
OS2W14 23:52 105.46.7
9r-t,4471gJofp-?Out..
NO ug4-
too
1,0
1
052W1423;52 170.57-0
I.I-O mmo11h1rte
OA4J uWL
5.0
0.12
1
o52911423:52 76.34-3
72-0Irtlttmo.11un.
NO uge-
1.0
U-12
1
o52W1421.52 107-064
1,1.OICIII.foaORrM
NO u64
5.0
0.54
1
05029V14 2152 754"
jell-1,2LYd4d1p17f1er1a
0-61J "A
6.0
0.19
1
062WI423: 52 1S6-59-2
trina•12-0IGdorw6wfle
NO "A
5.0
0.49
1
ZISIM,423:52 159-60-5
12-0Mt ulumopruPr
NO u61L
7.0
021
1
03r11r142352 7"?-6
1 ,3-0khloropopana
NO u6)L
1.0
021
1
05RW142332 142,264
W-1,]-[>I:rJwoprr.p ene
NO VA
1.0
0.13
1
o5729r1423:62 10061-01-5
REPORT OF LABORATORY ANALYSIS
iN. r4pon N41 rot be ..prvducad...up n h41,
04te 06.12r10r4 (it 20 AAt vnetwl.t. rrwn eo...m d P.0 ArhW 6ervtcel ue
Ai u 1 nNyne.t 6.rvN..- Inc.
2eAmlytical' �° °„ . ".
I�w -C MID
e7s vp,:
ANALYTICAL RESULTS
Project. Sorry Cla.ed MI. Ally 1UIC)
P.cr project No.: 82203F21
5.mpl.: MM125 I -A IO- Ong 3121001 Cuaedad 05271141435 R.Ci-d 052W141700 MahhL Y&Im
R.pon
parameters Rew111 Lpx11 L1rnll MOL OF Prepared Analysed CAS No Dual
9260 M6V LoW Lard L.rtdflll
Anr lytral Misthod: EPA 12R
trsrm-I-3-4kMwopropene
NOu6R
t.0
0.26
1 05RW1423:52 10061-02-5
Emylben me
NO uryi
1.0
0.30
f o612171423:52 100,41-4
2-mu-M.
NO u9Ai
500
0.45
1 O572W7423:52 5P1-76-0
Iodomelhm.
NO uOR
10.0
0.32
7 OSr2W7423:52 14-A94
Melhyls m Cnlarde
NO ug&
1.0
0.07
7 05/29114 21.52 76.09-2
4-Mr1hryl-2-pentanun. 1 M19NI
NO u6AL
too
0.33
1 052W 1423,52 106-10-i
styrene
NO ul +t
7 0
0.26
t 05RW 14 21:52 100.42.1,
1. 1.
NO ug&
S0
9.31
1 O5RW1423:52 630-20-0
1.1.22.7eaachlnraallene
NO u6A
3,0
0.40
1 05f29114 21:52 79.14-5
7e.adlroreemene
NO -W,
1 0
0.46
1 05+mla 23.52 127.10.4
Tulurne
NO MWL
1 0
0.26
1 Osusly 14 23:52 101.66-1
1,1,1 Trkhtom th-
NO kPg&
1.0
0.46
1 OSr2071423:52 7f•5S6
i,1,2-Yrkhloroathanr
NO uVL
t,0
020
1 O52W1423:52 79-00-5
Tri.hi. elhene
NO uyi
1.41
0.47
1 O62W1423.02 7001-0
TrlenloreT.reromem4ne
MD uOL
Ca
0.20
1 06r2P'1423:52 IS49-4
12,3�rndimrupropens
NO uOR
1.0
041
1 DUM1423,52 98,181
Vmyl acet w
NO UIFL
50.0
0.35
1 OWW14 23;52 104-05-4
Wyl ihlW64e
NO u6rL
10
002
t 062W1423:52 75,01.4
xyfene (Total)
NO UP&
5 0
Ojos
1 ORM14 23:52 1330-20-7
Swzn6sfes
4-13-111 ombenz.n. 1S)
N W
7a130
1 OL2111423152 460-004
12.OkWoremmaf•.•64 (S)
09 'A
70 130
7 OSY1W14 23 52 1706s-07 a
TNu.ne-d6 M
97 k
70-130
t 05fM 4 23:52 2017.2"
REPORT OF LABORATORY ANALYSIS
T k...1oe aJW iwt be r.PoducM...ur.l n h
Pao. 1 .113 Dow 06112r1614 09' 0 AM w ttn. wdrt• wea.M.r parr pr`1ynxar 5.-., i.e
P.C. a ar 72

�' �aceAnalytica�
ANALYTICAL RESULTS
Pow An Pvmyl 6.n4m, Irre
atr,O Kin.r +w• Nv. I
rnv►nr4 YC 7907B
I7D4A'S-MQ2
PT*Et Scary C$ ..61M Wry WIC)
Pace Prol.d No 02203UI
aample: m wia
Lob 107 62203121002
Calmeled 05727114 13:10 Renewed Dw26114 17 Do M.411 Mi.,
R.p.d
Pardmelen
Reallle u.1m
LI[ofl
M13L
OF
p[ep. of An.2y.ad CAS No. 0"
a0101Cp Graunawal.r
mmm"l mpinad. EPA 0010 Pr.pela6m M.pwa. EPA 30$0
AnNmeny
NO
6.0
5.0
1
OS79114 ISM DWM1420.02 7440-3a-0
Areenlc
7&
NO cask
100
50
1
OSrt911415.55 0573W 14 20 02 7440-362
B-lum
11.7J'jWL
1D0
6.0
1
05.291141555 O513W1420:02 7440-3D3
e#"%m
NO ago
10
10
1
15MUt: 15:55 Da13W142002 744041-7
Cadmtu.
NO .Iga.
1.9
1.0
1
V42911SS:55 OS W142002 7440.43.9
Chlamlum
NO UA
10.0
5.0
1
05.29114 15 M 0510W 14 20-02 744047-3
Ceb.4
Nfl•.Ok
100
8,0
1
OSR9fl415:55 OM142002 7440484
Copper
NO .wt
10.0
5.0
1
Ov2WI4I5:56 06f30142O.02 7440-we
L..4
ND u04
10.0
8.D
1
o5r29f141S;55 D573W142o.02 7439-92-1
N[vkm
NO utkL
50.0
6,0
1
DS W14 f 555 05FM14 20 07 7440-02 0
G.P-4lm
NO ugeL
10.0
10.0
1
DWW44 0555 65AW14 20.02 7MAD-2
341m
ND ugiL
10.0
191
1
D50 14 15:55 DN3W 14 20 02 7440-224
TmAufn
NO ugk
6.5
5.4
1
05r2D IA t5 55 D5f30114 20'0Z 7440.ZE-0
v4Pe4wm
NO u0,1
25.0
5.0
1
0572vf416:55 05f3W 1420.12 7440-02-2
Z.
NO U01L
10.0
10.0
1
OS1291141555 05f3014211.p2 744o-"l
■260 M5V Law L...I L.ndflp
Analytical M.dnd EPA 9260
Acetone
NO uWL
100
10.0
1
O511W 1400.04 67-64.1
Acr✓anpnl.
ND 1r0IL
70O
1.0
1
DFW14 00-0a 107.13-1
Be.ur4ne
NO Uqm-
1.0
0.25
1
OM14 DODS 7143-2
BromocMorom.alene
NO ygiL
30
D17
1
051=1400.00 74.97.5
&mm�6d+lmmm�tPmr
MD ugii
t D
n to
1
D573W 14 DO ON 75.274
a.-Inml
ND UA
3.D
0.20
1
DSY3011400.08 75-25•2
Oromemer[-r
NO U0&
100
029
1
05f3W1400.08 74.63-D
2-&Aanonr tMEKI
NO UD4,
100
0.96
1
D5f2W 14 DO-01 7E 0_30
CArban d.ntade
NO U01L
100
1.2
1
OSM14 no O6 754"
Green Iekanhlarlde
NO U9&
1 0
0.21
1
05f30114 00 08 W23-8
Chlmnb.nren.
NO UWL
3.0
1123
1
D5f30114 00 OE ID6-a0-7
ChfomMh a
NO UWL
10.a
054
1
DY30014 DD.Ol 75-00-3
Chg7afvrm
NO 4WL
5.0
014
1
05tM14 DO OS 67.6&3
Chgrom.n.ne
NO uyt
10
0.11
1
05FM14 00.01 74 67.3
12-ObrOma3-cllhrogropene
NO
13.0
7.5
I
ONIV140D:Oa W$24
Owoe h4xommmo.
NO uyi
3.0
021
1
D613W 14 WON 124.0•1
1,7. OWrelvnes+.n. fE DB1
NO uA
1.0
0.27
1
05M 14 DO -Oa IM93-4
ORromem.lh.r a
NO ti01i
10 D
Oil
1
D513W 14 00.08 74.95.1
1yDachky.oenrer..
NO Ugh-
5.o
a 30
1
DU30014 DO DR 95-50 1
1,4-13khgrapenimm
NO Upe.
1.4
033
f
D513W14 MDR 1a"154
beae-l.4-DNadofo-2-buhne
NO uA
l0o
1.0
1
DUM 14 DD'.Pa 11037E
I,l•01ch1meetm-
NO udR
SD
032
1
0513W 1400.09 7534.1
12-Oldeoroalhane
NO UyL
1 0
(112
1
DUM14 DD.D6 1074)&2
1,1 OlvMp Md"..
NO uqA
50
09
1
DS W14 DOOR 75-36-4
aa-1-Z-Didlleroerhene
NO U01L
5 D
0 19
I
O517W14 OD 0a 1S6.59.2
keen-1,2-OrcraervMtmne
NO tipl
S.D
0.49
1
O%W14006a 156460-5
1,2-DIr.{aprppruprne
NO UWt
10
027
1
WW1400 as 70•E7-5
1,3.OfcMmryanp.ne
NO Ug1L
to
02a
1
0573Wt4 00.08 14248-9
dF1.3•DlENl Vrnprn.
NO 1rgfL
1 a
all
1
06f30114 00.0a 10D61-01-5
REPORT OF LABORATORY ANALYSIS
nN.r4pn4 N.e iw[ d .vaA.c4d..rc.pt n r.w.
DateOW 12401a 06 20 AM
,I ..�aCe.4nalytiCal
..rnr..am Doll
ANALYTICAL RESULTS
P.-RnYyaWl $-I"1, lnn
9e00 K-, A.. Sian 100
ra­M: 7611e
0041e75-MAR
Pmisvl SL" Cwlea-w- Fxy illlc
Pave Pmjm No- M03121
SYnpl.: MWIS
L.b 10! tnO3121002
C.--lod
05127f 141330
Renewed 0646+141700 M.eu 1h11Mr
R.porl
Pp6m0en
R..u11e U.,t'
Limn
MOL OF
Prep.red mwy.ed CAS Na. Oua1
ISM MStf Law L-I Umdf6l
Wulytrnl Method EPA 6260
Karla-l.3-plcF.mapopene
NO uOR
10
026 1
06170f1400.0E 10061-02-6
E"ibaw-
ND Up4
1.0
0.30 1
DL W14 DOOR T00414
Z-mdgwor[.
NO Ip7L
50 0
046 1
05PMI4 00Aa 521 7"
Iodom.dllane
ND uA
10 0
012 1
*$gWl4 00:06 74-0a-4
Malaylene ChiWide
ND Ug4
10
097 1
DY W74 ODOR 75-042
4 Me1hy1-2-p.aungne(Ml6lq
ND U04
100
033 i
D573W1400Olt 106-10-1
51yf
ND UW1.
10
0.26 1
05r3W 1400.06 10042.5
1, 1, 1, 2 T.4adq- O&M.-
NO ago
50
033 1
55130f140d.06 4i3a-206
1,1,;�-Yetr.dllmve6[ene
NO uWL
3-0
040 1
051NY1400:06 7604-5
r/6avflkyoolhene
ND Ug1L
1.0
046 1
OM1400:09 121-16y
Tok"s
NO nlL
'I.0
076 1
OVA $400:09 1DE a6-D
1.1,1-TrINlwvelYlane
NO U04
1.0
0 as 1
DPW 14 WON 21.58.E
1,1,I.Trkhloro.d.en.
ND u94
10
0 29 1
HMO 14 DD D6 79.00-5
Trlyllpraemene
NO L,gk
1-0
047 1
OS3014 OD 06 7D-01-5
Tnehlpala[orom.th.ne
NO uWt
1.0
020 I
OYSW 1400'Oil 75411-4
1 ,2,3•Trld.lpnpinprre
ND [rgt
No
0 41 1
D573011R 00:09 96-1"
Vrryl. 11fle
NO Ug7L
500
035 1
050W$a OD as t0a-D5-4
WW cNmide
NO uvL
1 ❑
0..62 1
OSfo0114 0005 75-01­f
AVI..(7ol.4
ND kkwL
5.0
Oea I
O E11400:0E 1].30-20-7
swropalee
4 908pwabennn. f51
Da ',+
70 13E
1
OM W 14 00.0E 460-00-4
12-Dnh1cm..tV ne-4(SI
1011E
70-130
1
D5f3W 14 Do 09 17010"7-0
TMla9.-d6(SS
97'G
10. 110
I
OW 14 DO D6 2037-26-5
REPORT OF LABORATORYANALYSIS
e W1 N" m1 h.­0 n Adi
Page D of 73 Oak 06112r2014 ON 20 AM .snr e...Mr --I or I- Ary ley S.-.. I -
Pau, 10 M 73

%�4r�alytiCa�.
1 ..raN+i4a Ny
ANALYTICAL RESULTS
rift"bly1ael IiMK", M4.
"m M-"mR Slab Igo
Nunm".k, NC 2607E
1104f671-9
Plwpw Slay Clca.d-Mt A0y IUIC1
Pees Pioled No 02203121
Samplr. MW-49
Lab ID: 9220312063
CoUcled: OW2711415.10
Rmvwod= OWIV1417:00 Mo&.Ywter
Repm
Puemelen
fireu64 tmnll
tkrA
MOL
OF
Prepared An*md CAS No Quo,
10101CP Olourld m,
Pnelyucd M.I d EPA6010 Prapanlbn M.M.A EPA3010
Arw,„ IV
NO vqk
6 0
50
1
0526114 M" 0513w14 20:14 7440-35-0
A,"e
NO ugeL
too
50
1
0VM1415:55 OU300142014 7440.30.2
aanum
MJJ ugL
1DO
50
1
D52W'146555 DN'1001420'14 1440-39-3
63ryfe+r,l
NO ug&
1 0
1 0
1
MW14 $5:55 OW30414 20:14 744Di1.7
CON-
NO uuk
1.0
1.0
1
0520r14 65:55 051 W14 20:14 7440-41-9
ttlrvmbnn
NO ugh-
10.0
5.0
1
052911a 15:55 0513Wr1120:14 7440-41.3
CDdell
NO ug11.
10.0
5.0
1
OWW14 15.55 06WIll 20:14 74404114
Copper
NO ug1L
100
5.0
1
W2911415'55 0513011420:14 7440-50-6
L044
NO u07L
10.0
6.0
1
OSr29l1415'5S OS73W1420'14 7439.92.1
Wkc
NO uA
50-0
5.0
1
05awt415'55 0513W1420:14 7440-02-0
541. Nrri
NO ULA
10.0
10.0
1
OS291i116:55 05130114 Xi 7782.40.2
Syu
NO vgA
100
5.0
1
0512AM415:55 0113N1420-14 7440.22-4
Th.lfum
ND u01i
6.5
5.4
I
OWW1415:55 0W3Dr1426.14 7440-26-0
Vanadam
4AJ uWL
26.0
SA
1
05 %f]415'111 OW3011420:14 7440-62-2
Ylnc
10A ug1L
10.0
10.0
1
O5awI416'.65 OWM1420'14 7440.6E-6
1290 M9V Low Lw.l LaodfNl
AnMyh.A M49md EPAf260
Acelwre
NO 0&
100
10.0
1
DW3004 W25 67.64.1
Ao I-trw
NO ug&
20D
1.0
1
O'WWIA 00:26 107-134
efnr.n.
NOugA-
It
0.25
1
D571W1400:25 71-41-2
&omouNwomemene
NO ug+L
3.0
0.11,
1
ow3w11 00:25 Mor's
grvmodwwvmad,4n.
NO vWL
1.0
0.1E
1
O5r3W140025 7541-4
Slum ttm
NO uWL
3.0
031
1
OW30114 W26 75-MZ
&arrwa.On4ne
NO uW+L
10.0
020
1
06f10111 0016 74.93-11
2-0utanme {MEIc1
NO ',A
100
0.1E
1
05130114 00:25 76-03-3
Carbon dlHAede
NO ug1L
1DD
12
1
MM140025 M.$"
Carom l e9eeldw.dv
NO ug+L
1.0
025
4
M01140025 56.21.E
Chivrobr,l
NO ugIL
10
013
1
051311f140025 1D6-90-7
C1116roelhail.
NO ug+L
100
0.54
1
OW31V140025 75-00-1
ChWrvlumi
NO ug1L
5.0
044
1
D513w14 D0-25 674E-3
(;hP r '?w1hw6
NO ug1L
1-0
0-11
1
O5134V 14 00-25 74-87-3
t2-0bomo-s-dgorvprvperre
NO uu+L
130
2-5
1
0613w140025 96.12.6
Owrvnr6vhbomelh.ne
NO uWL
10
0.21
1
OV30e,4 DO 26 Q444-1
1,2-4iurw1leam.ne MDII)
NO N&
1.4
027
1
OWV14 DD26 106.934
PlbyoR mef"
NO uWL
10.0
0.21
1
05W 1400'25 74-25.3
12-Ok1,lwub.him.
NO uW1
SO
0.30
1
0513W140026 95-50-1
6,4-Dkf"ubr144ne
NO ug4
1.0
0.33
1
0613W14 00:25 106.4E-7
1r4P+s-1 A-Dicl ao 2blAsm
NtD .0&
100
1.0
1
OLSW$A 00:26 110-57-6
1.1-OkNoteNhrla
2.341 uWL
50
0.32
1
057 W4 Do 25 75.34-3
12.O1chlruvethme
NO uA
14
D.12
1
WWI di 00 25 107.W2
1,1-0kNolorlten0
NO ug+L
60
6.5E
1
WM1400.25 75.36.4
eN•1,2-Olw d..i 001h.ne
3.1J u01L
6.0
Dig
1
0513W140025 1WW2
tra11a-1,2 Orchlwaen,ene
ND uDR
5.0
049
1
OS13011400:25 154140.5
12-Dkhiwvurupane
NO ug4-
1.0
027
1
0513W1400:26 WV-5
I A'Dlchlw.O .....
NO ugeL
1.0
0.2E
1
05131111400.25 142.26.1
d4.13-1>cJaoopq pens
NO u111
1.0
0.13
1
OW=140025 10061-01-5
REPORT OF LABORATORY
ANALYSIS
t,e.l.Pun
rua nala �leese.d.
nc.vrn
Nx.
13 a OM12R0t4 96 20 AM
.nf... fy .Ik*. cwrantpl
aevr Ay1,a g 9.rvu1. in< pigs 11 PI 75
I - 1eAnalytical�
r�. iWii
ANALYTICAL RESULTS
Pa.e av4ly9eel6mbb. NN.
HwnN.Rra.. NG 1do76
{Tu l6Tsg3R2
Prwj_n So ly C1ve.d-ML Airy (111C)
P. Pruied N. 17203121
Sample: MW13
Lab 10: 92203121093
Cafadnd462714
15o0
R.cai..d 057161141? 6D Mau. Y9e44r
Repaq
Pufm.lele
ft wu Leus
LImN
MOL
OF
W.pa.ed Anm"d CAS No. Cum
6260 M5V L- Lens Landoll
Anelym.1 Me6,ud EPA 4260
oana•1.3-pcNorapiuyrhr
NO ugeL
1.0
026
1
O&W1400:25 10061.02-15
Fawk0a.w.
NO ug1L
10
0.30
1
0573w14 00.25 100.41-4
2-M...nme
NO uglL
500
0.4E
1
051,7W14 OD25 501.764
14dome6.ane
NO 1,q&
10 D
0.12
1
0&1"14 00-26 744214
Melivimm CNwide
NO wq&
1 0
a 97
1
061/0/14 00:25 76U1.2
4-Me1Wy1-7"nt1pu.la(mim
NO Lygk
100
033
1
05JW14 00:25 103-10.1
5lyN1w
NO 4&
1.0
0.26
1
OS "14 00.26 100-423
11,1,2 Tairm-N-mean
NO ug1L
5.0
0.33
1
057r W110025 610-21L6
1,1,2, 2•7.1radNw-free"
NO u01L
30
0.40
1
0613W140025 711-34.5
T•C.d,lwoelfr N
NO aWL
1.0
046
1
05f101140026 $27.6f4
ToRrena
NO UWL
1.0
0.211
1
DNIV1400:25 fah-66-3
1.1,1-T-hi..erih.ne
NA uD&
1.0
0.4E
1
M011►Was 71.5645
1,1,2 TnWlor..mene
NO u0k
1.0
029
1
05f3w11 Do:25 711LOO.5
711cMl then.
NO ago
1.0
CA?
1
05f1W 14 OD.26 70. "
TIKMorv6uwvrne Nra,.
NO lgft
10
0120
t
06f3W 7460:25 7S49-4
1,2,]-TnWaupvpev�
NO ugii
1 0
041
1
D&WI40025 961E-4
WWI ac.tfla
NO uu&
500
0.35
1
05f3W1f 00:25 106-054
1Anyl chWrW.
NO ug4
10
(162
1
Ow"I4 OD 25 75-014
Xy1.n.(Totap
NO ugfL
5-0
00
1
0513W1400.25 1M.10.7
Su7top ffa
4 Brvmvluvrownem. (Sl
01 %
M130
1
061YD114 00:25 460-00-4
12 OwAmosihene a4 IS)
100 %
70-130
1
OST3wl40025 1706007.0
TOWme-d6151
96 %
70-130
1
II&MIa 0025 2037.2a5
REPORT OF LABORATORY ANALYSIS
ih. l.ppn .hey rvIH ny.wucW. errwp n NN,
Pale. 0671226f 4 06:20 All r,..w„t e,4 w.,r•• cvaru a Pra Airrybral s.rvp.. lac
PROP 12 el 73

/`J�//1■ P.-A-lyllwr 6wWa4a, Ins Pas. Anpylrear l.rvr»., rm
WWKK A. 5W10a
17M1678am , "l�t�`°�' ,rcd✓-y4[pa
ANALYTICAL RESULTS ANALYTICAL RESULTS
F4w"I. Sw y Clvaed-LII. JWy ILWQ
P.ej..1 Slrty 0osed-041"(W4
P. ptepd N0. 92203121
pace Prvpcf N.. 02203121
5-0.: MW-13
Lab 10: A=121004
cwkcfad05R704 76:00
R-Ned: OW2&f 417:OD M.ku' Werw
Snnplw MYY-11
Lab lO: 12202021M
CeWslaeOSR711410.00 RI1v.lY.d CUM041700 MI": Mkr
Rvpon
R.p.0
Peremele./
Result. Lkft
LI.n4
M OL
Or
Ptepued Analyzed CAS Nv Oval
p.r.melen
Re.l94 lkrlla
LlrrA
WDL
OF Pd. w.d
An*jod c" No. Otral
"101cP OroOndrval.r
M.Iyr"I MM79red' EPA6010 Pmpamllw
Me111od: EPA
301D
4260 MsV LvW Layal LWWRll
A WyneA Mkl.od' EPA 4200
Anb"v
NOLPA
6-0
5.0
1
OVMd /1515 0573011420:17 7440,36-0
fron.-rJ-Diclomovip4no
NOuOR
40
0.26
1
U51Wf/00:41 1OW1-02-6
A. g, -
NO uuk
100
5,0
1
nW90416;55 05*W1e 2017 IMI-34.2
Elhyl6errzene
NO u911-
TO
11.30
1
O6r3W1400:41 100414
8.rtum
31.6J uQ&
f00
6.0
1
OSr221441555 0513W1420:17' 7440.304
2•Heaanpne
NO u04
00.0
D49
1
ON3W1400!41 501.764
B4fyllum
NO uA
1.0
1 0
I
06+2* 41515 OWN1420:17 744041.7
lednrn.lh.n.
NO uuit
Iva
0.32
1
06r1W1441"1 74414
C.dPYum
NO NA-
1.0
IA
1
DSrm%4 IS,% OSwi420:17 744041-9
Mal.rlene Chiatele
NO Uyt
1.0
097
1
CAW 4 00,41 mo"
GN"kim
NO uQ&
Poo
50
1
ON29f4415:55 OSl70J1420.17 7440-47.3
(MIOKy
NO u04
100
0.31
1
esw 140R41 $W MI
Ceha11
NO u01L
t0.0
!.O
1
05r2 Wf415!55 0% W$A2O:17 7440.464
s4w"e
NO ug&
Ta
0.28
1
ONSW14 OD 41 1d742-5
Capper
NO uv&
19.0
5.0
I
0WIV14 15:55 OMMA 20:17 744040-6
1,1-1,;-T.vAwpoen.ne
NO uv4
5.0
0.33
1
0S W14 f A l 1530 204
L.M
NO uglL
10.0
50
1
O5rm$4 15:55 05, W14 20:17 7436-92 t
1,12,2-TelracNorvefi...
NO ugi.
3.v
0.40
1
0517W14 00:41 7934.5
N1Ael
ND WIL
50.0
5.0
1
oww`l415:55 05f3W1420.17 7440-02-0
Trb-hl...04ene
NO ugiL
I
0.46
1
O& W1400:41 127.14.4
s.rereum
NO Ug1L
100
t0.0
1
115rM1415'56 0513W1420:17 T70249-2
Toluene
NO 1JO&
1.0
026
1
OWM1400:41 I0 II"
9.Ne.
NO ug&
10.0
5.0
1
05r2W1415:55 05f3W1420:17 7440.224
1,1.1-Trmhmroed-.
ND ugR
1.0
046
1
O& WI400.41 71.55-E
T1r.Mum
Wugl-
5.6
5.4
1
WM1415:56 05r3W1420:$7 7440.284
1, 1 ZTnchlpmefi-
NO ugIL
4.0
0]11
1
064WIA 0041 70-00-5
vm"um
ND UA
250
SO
1
06RW1416:5% OWW1420:17 744002
TftcNw"1ran.
NO 1,gIL
1.0
047
1
osem400'Al 79-01a
2hc
No up4-
10.0
10,0
1
OWW415:05 O& W1420;17 744046-6
irlchlero4uvrvme+ha+n
NO u9t
TO
020
1
0Sf3W14 DO.41 75-694
1 3-inrliln upropane
NO uglL
t.0
0.41
1
05r3W 14 00 41 96.164
AMMSY Low Lay.l LandRll
Anetyllv.l Me6.od' EPA 6260
Vinyl... W.
NO ug+L
50.0
0.35
I
05f3W 1409.41 106-05-a
Avelene
NO r.A
100
10.0
1
OWMA 00:41 67-04-1
Yetyl chlmlde
NO uglL
1.0
0.62
I
05130i4 00:41 IS 0 1 -4
ActyloWlr/e
NI7 UpiL
200
19
1
ON3011400:44 107.1}1
X01ene 1Tv4e1)
NO u01L
5.0
066
1
05r1W1400'41 IM-20-7
Benzine
No Ug&
1.0
0 25
1
06 W14 00:4T 7143.2
Surr004MA
&omadJ.rumeln.n!
NO 4A
30
017
1
05W1a 00:4$ 1447-1
ALSv F4 obrmfnn. I$1
99
70-130
1
OSr30r140041 460-00-4
&omadirlrloromedrane
NO'KA
1.0
014
1
OW3011400:41 my-4
12-❑Ichloreclhene d4 451
101 5s
M130
1
031]W1400:41 170e0-07-0
O.vmvlotm
NO V9h
1.0
026
1
OWMI400:41 76.25-2
Toluene d8 (31
08 x
74130
I
DN3W$400:41 2D07-26-5
BtwomK4raM
NO L4A
$0.0
029
t
OS13W1400.41 74,43-9
2-&d.non. SM EK)
NO ug
100
0.96
1
OWMI400:41 76.90d
Carbon di-1W.
NO ug/l-
1"
12
1
OU30114 00:41 M15 a
carbon il6avNwida
NO U0R
1.0
0.25
1
06f3W 14 OOL41 56.23.5
Chletebenxene
NO ugk
3.0
013
1
051IW1400-41 104410-7
Chlaroelhene
No "A
T0A
054
1
05f3011400.41 75-00-3
Ch1w.mrm
NO nk
5.0
0.14
4
0513W1400:41 97414-3
ehPo.em I-
NO ug&
1.0
0.11
1
0513W 1400.41 7447-0
12 016rvino-3-d0wt p-poh4
NO Link
11.0
2.0
1
051301 4 O0-41 96.12-6
W."r &lprp lilts
NO 1191E
30
D21
t
0613W1400 Al 124-49-1
1-2-Dlb,om iti. (E DO}
NO UWL
1.0
D27
T
05r3W 14 W.At 1W934
Dlhrvmvmeer.ne
NO upk
160
D71
1
D5l3W 1400:Al 74-06-3
1,7 OWNuoh.n.ene
NO .4iL
5.0
0.30
1
06f3W 44 00-41 955%I
1,44)"Iwobancen4
NO ugil
1-0
0.11
1
OM&1400:41 1WW?
Iram•1.4-glpNorv-2-0uhrra
NO uqk
100
10
1
061]W 1411MA1 110.57.6
I,1-Dk4lwrveth/ne
1-1J ugfL
5.0
0.32
1
OUM140041 75.34.3
1,2•DjCJ"*"uh.
NO yglL
1.0
012
1
Dr M14 MA1 1074)6-2
1,1-Oiddgvelh.ne
NO Lnik
5,0
056
1
D& W44 MA1 761354
6a-1,2-01dun.velhena
1.OJ uglL
5.0
0.19
1
05r3W1400:41 1%59-2
vans-1.2 Drchleroow.
ND p9&
S.D
0.40
1
05100R400.41 16640-5
1,2-Wo A.W.p.ne
NO uWL
10
027
1
05AW$4 M a 1 7667.E
1.3 OlvNerr W plln.
NO ppli
1 D
025
1
OLW 14 DO. 41 142-29-9
ae-1,}p1d.Wrpprogene
NO uWL
1-0
0 13
1
D6f3W4 o0'41 10061-01.5
REPORT OF LABORATORY
ANALYSIS
REPORT OF LABORATORY
ANALYSIS
TN..a,polt
ah.t notti niaoe.rce k. a.dpt.
U.
Th. tape ants mr --p-kroad. no.Pr n NA -
Om Le 06117120t4 0 0 AM
..ewurrn. rmre
eana.r.ref
Pw Nrhvc.l 9- rK. P.p. 13 of 73
Dare D6r 12r201A o4'241 AM
..,Atl . wtdr. ryr..rl w
Fl- M.•rl.al S.- u.
Page }/ M 73

.aw Awyou1 ie lo., Na.
Kk y M - %� 100
acee50O A )yflcal' Hunhrw Ak. NC 26076
I704)vI5,QR2
ANALYTICAL RESULTS
p,gjet1 5wry Ck1a.0,Mi. Airy ILNCI
Paco PtuJactNo.: 92MI21
BrnpW ktw-1 Le00: 9220112100I Cu4ected. D512&140605 Recelred DSQ1041520 M.tr4 kidkr
li.ppn
pwwnete Rewlla L"M Lrmll MDL ❑F Prepped Andyeed CAS f+v O.W
IO14 ICP Otoundw4lee
Andyll1.1 M.Ihpd EPA 6010 O. eperelon Method: EPA 30 TO
A,*mony
NO WQA
60
5.0
1 06103114 I k 30 06104114 20:09 7440.16.0
Ar.arMc
ND upi
too
5.0
1 O"31T4723O 051WI42006 7440,3a-2
Ewbum
19,2J U0L
I DO
5.0
1 OW3114 1 a 30 COMMIT 20:05 7440-3*4
eeryaklm
NO uOi
1 0
1.0
1 6150031$a t2:30 060040420:05 7440-41-7
C44mum
ND uOfL
t 0
1 0
1 OW103114 72.30 06W11420:08 744043.9
Chromium
ND -OIL
100
5.0
1 06103/14 72:30 05104114 20.06 744047.3
C65.11
NO u0&
10.0
50
1 06/03114 $2-30 ORM114 20.06 74411J64
Coppw
NO Ir
10.0
5.0
1 06/63/14 12:30 MM4114 20:06 74,60.504
Ir,r1
167J u01L
Soo
50.0
1 OdM3114 MID 0610111620:06 7439-6D4
Le.M
ND up+L
100
5.0
1 MUM 12:30 0"411420.08 7419,92.1
Nlckd
NO uO&
50 0
5.0
1 Oe103114 12:10 06104114 20:00 744042.0
5alerlwm
NO ug&
100
10.0
1 OWOH14 12:30 06A7414 2 M. 7762-40-2
Sar.r
ND Uy1L
10.0
5.0
1 000311412,30 OW-0420.08 7440.224
I'twaum
ND uO+L
55
5.4
1 06r03114 1230 OS 4114 20 06 7440.264
V.n.4um
ND ugVL
770
5.0
1 06N111412'30 0610411420:98 7H042-2
211c
NO Hy+L
100
IO0
1 064W1412.30 Odnw 1420'Oa 7440.66f
6M MSV Low L.V.I Ler.dl dl
Anelyticel M.6wd EPA Woo
Acalone
ND uWL
100
10.0
1 0N31e 14 03 44 6744.1
Auylonlhll.
ND uA
200
1.9
1 OU31J$40244 107.13-1
S.r12en.
ND uWL
1.0
0 25
1 D613111A 03-44 714"
&wrnr.rhlnvme914ne
ND up4
3.0
0.17
1 05 IA4 03:44 74-117•6
Bi-kill.-.1h.ne
NO rrg'L
To
0.16
t ON31044 03A4 75,27i
sfom ,arm
NO uWL
3 0
02a
1 D5031114 03:44 75-25,2
6komomellane
ND ua&
100
029
1 MIJ1403-44 7444
2 euulnane jMEKI
ND uIlL
Too
0.26
1 061111T4 02:44 76-033
Cer5w1 dleulAde,
ND uAi
100
12
1 OU31114 03-44 71r 1"
C.rtron leu.mmwii
NO uOA
1 0
025
1 ON11114 0344 W23.5
Cnlol."u-e
NO uA
3 D
0.23
I 0yy111A 03'44 106.96.7
chic-6-
ND upk
10.0
0 $4
1 ON31114 03:44 75-00-3
Ch1a1u4Am
NO uyL
5.0
Ole
1 451111t403:44 6745.3
Chi-Ift.n.
ND uW1
1.0
0 11
1 OW31114 03:44 7447.3
T2•0IOromo-1-ddwoprpp.n.
NO wUL
110
2 5
1 MI 03.144 96.12.6
Gkrwrwehlvrvm.Ilane
ND uA
3 O
D.21
1 owl Ise 03:44 1244a-1
12di1eeornw4ulrr. {E DB)
ND uAi
1.0
0 27
1 ON31114 03:44 $06.934
Obr.name6lene
NDuOL
100
0.21
1 OW111403:44 7446-3
12 Dltl4rcotreneene
ND vok
5.0
0.30
I
1 05 IA41 03:44 WWI
I.4-DWN&den2err.
ND u91.
I D
013
5 051311440344 TOS464
karts-f,4-Oivhlore•2•Weane
MD "A
IOD
10
1 D$:S111403-44 110d7-5
l,t-pkNoroedune
NO uq&
5.0
0 32
1 Mine 03:44 7634.1
i,2-plpNnoellrene
ND uOA
10
012
1 0513111403:44 107-06-2
I,1•DkNoroelrb n.
ND4k
S0
0.56
1 ON311140344 75-35.4
de•1,2•DIcM61aaU1env
NO ujVL
50
014
1 OS13111403:44 156-504
trans-l2-pdMorvau+ene
NO up4
50
OAO
1 05A11140144 15630-S
1.2 Oki4olwopane
NO uWT-
1.0
127
1 OU3104 03.44 78.87.5
}.3•Dlchlwopropepe
NO kq L
1 D
01E
1 MI 03:44 142.26-6
REPORT OF LABORATORY ANALYSIS
rlr. r.1m1 rh.4
rbr a r.prnduc.d..rup
.i AJI
17ela: ON I W201a 06:4 AM
Mewl rw ..awn ca.k.,,r =r
Par.. •rrrru:a S.n1ak Iz Pape 15 Or 73
gg�7..pp ❑�1 7,,1,�,I P.- ArWydw a.raleea, yes
frYl. rlr /u� fCB�' aeon Nv nAra 9,e1a 1m
Hwrw.,r. 4C 0607I
ry(405-e010e
7
ANALYTICAL RESULTS
Ptolect 3urry CW..d MI Nry jUICJ
Per.. Proled N6.: 022D3121
!ample: MY2.1 LAk W: 92203121006 Colhaled: 05I26114 0IpS RN*Vad: 0640114 15:20 Mmro. Nlkler
f *MM
pmemefem RaauM LAlld LN1Il MDL SIF prepared AnOyyad CAB No- poet
1260 1015V Low Lw.l LmndliN
Melyppd kg6wd' EPA 6160
de 1,3-D1MWrpplopen.
WD u0k
1.0
INne T,3 Olctawoprowpe
ND u0A
10
EthAems"
AID uyll
10
2-Neewlvrle
ND u011
1100
lodumel -
ND IIA
10.0
NM61Wne Crawlde
ND LWL
1-0
44Ae01y12-penlN+one (MIM
NO up4
100
BgnI1.
NO 1qi
10
1,1.J.2-T.IradWw-61A"w
NO upL
50
1,1,2.2• T401dWW-Ih elm
NO uyL
3.4
74"d,1=61h-
NO rryL
1 0
Token.
NO uAi
1.0
1,1,1-'rIkcK wedr.n.
Alp MAL
1.0
1,
ND up4
1.0
Trk:hlwnedene
NO VD&
1.9
TrkhlwoA.rorome u+ene
NO upL
1.0
12,3-Tnddoroprop.-
Alp uW1
1.0
Vny1 acelak
NO not
60.0
VMO cNorld.
NO MAIL
1 5
X*ne (ToW)
NO U01L
5.0
9rwo0.t..
4-&omv4uorouNlr.ne{SI
$00 %
M130
I,i-D+cMorosrhan6 d4 (51
" %
70 130
Toluen.-d6 tS)
29 %
70-130
21208 Alk.lY111y
Angyrlpel Melnud: SM Moe
AlkakrMM. Tow a CAC01
411600 VAL
5000
4WO19206r we►%w
A,,41yMp.I Method: SM 4500-320
SWld4
ND u01L
1000
105A tC Anil- 21 am"
An.lyuml Mevlod: EPA M.0
Behar.
ISW "OIL
250000
4600 CIAO nd.
Ank,00-1 Yelhpd: 5M 4500-0E
Cr0wm6
3270 UWL
1000
450OCNE Cyanid., Total
An hlkel Meemd. SM 4500-CN-E
Cyarrde
ND u(PL
ilia
92200 COO
Anafyllcal Malhad: SM 52200
Chemical OryOan O. m.nd
ND u0L
25000
631011 TOC
Arrplylkel kilt1h0d: SM 5110E
Tow Ol64pk Carhnn 2960 U01L 1000
0.43
1 0031114113 44 WIM-01.5
026
1 05111114 D3 4.4 t0 "24$
0.30
1 63411114 D3-44 10D-414
0.46
1 051)1114 03 44 59 t-7"
032
1 OW 111403.4A 74-66-4
0.01,
1 ON31114 03.44 75-OF2
0.33
1 OW31114 03:44 109-10.1
0.26
1 05MI140144 OW-42.5
OW
1 OY3111403-44 630-2"
0.40
1 05131154 03:44 7e•344
OAS
1 ON31114 03:44 127.18.4
0.20
t OW3111403:44 1O6-66.3
0.46
t OY31114 03.44 71 55.5
0.29
5 OSr31114 0344 79 00 5
047
t 05/1111403'44 1e-01e
020
1 0561 MIT 03:44 15494
0-41
t ON31114 03:44 06-14-4
0.35
t 05/31/14 03:44 104-09.4
0.62
I 05p I fld 03544 7"1.4
0."
1 ON31IT40344 1330-2017
MUM 03:44 460.00-4
0541A4 01:44 1105407-0
061 IM WA 20314"
Iwo 1 060" 14 14 OD
190 1 0610 0 4 $IN7 VMW25-6
2000 1 D"W 14 07,53 ta606-74 6
low I ON1111416W 16667-004
so 1 O&WI4 11:11 57-12•S
25000 1 od1011413.40
low 1 Q5rW142023 7440.44.6
REPORT OF LABORATORY ANALYSIS
T1w 1.pM M14a nelb rrpreduntl..rc.pl h MI
DOW OW 124014 D6 20 AM wt w "wI~ -1.0 Pew AlWWl Lanark N1c
P". le of 71

p... ,{nMyrle.r ,Iervle... Ind
raeAnalytical' �°° . `.,
I llirni.re.+1.. Mc 76we
Oo4lessac97
ANALrnCAL RESULTS
m*0 Sorry Ckmd-M1 Airy (UPC)
P,P" RuPad No. 92201121
S-Pl.: TAW-7 Lae W: 12"3121009 C.Uicied 06r19114 12 DO Ruolyed. DWaOI A 13 20 Maki- V6a1er
Renarl
a ler. A..Wt. 1-mit4 Ll" MOIL OF Pr.Pn.d Analyl4d CAS No 011M
60101CP 6rurrrdw4l.r
AnalylUal Mod ivd. EPA W$1) Prepatalon
Mo"d. EPA 301a
AMI-y
9E ugfL
6.0
S.0
1 MIOW14 12:30 DOW14 20 11 7440-36.0
Ar411ree
NO up6-
10.0
5.0
1 06A301412:30 0pfpu 1420:s1 7440-34-2
Brhrm
71,"u6rt
100
6.0
1 D6r0]f1412.30 0610411420: 11 7440.30.3
04ry1Yum
ND uyi
$.a
1 D
1 0511311412:30 OSPOW14 20-11 7440{14
Cadlnmm
NO ugA
10
1.0
1 4mwiA 12:19 96MV14 20:11 14404"
ChramUm
NO vk.
Ice
5.9
1 3M-V 1412:10 06fD411420: It 144047.3
000.11
17-3 UWL
1o.0
S 0
1 D6&O1114 12 30 06f01114 20: 11 744"4
Copper
NO u6+L
100
fill
1 06r6311412'30 W0.4y1420111 1440•SO•a
non
NO UWL
NO
So
1 D61OSt1412-30 06001420�11 H39.6941
1,60
ND uyt
10.0
SA
1 00 YI412:10 OUQI420:11 1130-92.1
NIdN
NO npYi
50.0
So
1 06A73fs472: 30 0"411420.1, 7440-D2-0
Selenium
NO up4
100
100
1 MV141230 OBA4l1120. 11 77 2.49.2
Sorer
NO upd
'ID
5O
1 DW311412:30 06A411420.11 7A40.224
ThelAum
NO ,Q&
6.6
5.4
1 0NO3r14123D WOW. 2D:t1 744Q26-0
V.nadlum
NO ugpt
25.0
5.0
1 96 V14 12:30 OW4114 20:11 744062.2
21nc
No uDA
10.0
100
1 ON31141134 OW4114 20:11 7440 6"
6210 MEV Low Laua1 Landllll
Merylfrel Mevlod EPA 11260
Acelune
ND vp+L
100
10.1,
1 05131114 03:59 67-64-1
ptaylerandn
No uW1
200
I9
t 0513111403159 107-s3-I
Benlene
D-732 vyL
1.p
025
1 03 VIA 03:59 1143.2
9romod.lcromer-
ND uu&
1.0
Q 17
t pSr31r14 0 :50 74-97•fi
8mmaddearemelharle
NO uy+L
1.0
0 16
t 06r31114 03�59 76.274
gromvform
NO ugfL
30
0.26
1 05r]1114 03:50 75.25.2
Srehram.lhan.
N6 uv+L
46.0
on
0y!]111403:5: 74-03.9
2 at" rmem1
NO uy/l
100
096
, 0573111A 03:59 7y9}3
C.rhorl dauAlde
NO uQ&
100
12
1 05r31114 01:59 75-15-0
C.r6on Ietrachktlde
NO uJ&
1.0
0-26
1 OS l"A 03:59 W23.5
Chkfo6entehe
6,7 �rprL
4.0
023
1 ON3111403:50 1MW'?
ChinrO.lh-.
NO rr6n
too
0.54
1 MI?1403:59 75.00.3
C"Wokrm
NO u04
6-1)
0.,4
1 OU31 MA 03:5: 57-W3
4;hIID 0me61"
ND 1WA
1 A
11 11
1 OY3,114 03574.67.3
12-D1rom0-3-d1Mfoprop4rre
ND uylL
.025
1 0513111403:5R W12-6
d6rlHnedlxxwn.6.uu
NO uv✓L
1.0
021
1 OW3111403:59 124-46-I
,2 1-�r0-thane (EDB]
NO Irg?L
10
027
1 05n NH 0159 10691-4
D,Pbromome6r.ne
NO IN&
10-0
0.21
1 1"1I14 03:,9 114-9'r1
I2• ktik b..2ene
NO 1.0
5.0
0.30
1 OSr311s40359 95-5D-1
1,4•Dlci6o mImmar10
2-7 uvfL
1-0
0.33
1 0N31I1403:59 106d6-7
truly-1.4-Wivro-2-ham
NDuU&
100
,.0
1 95f3111403:59 „0-57-0
I,I D4i1101oa91ano
NO uvIL
5-0
0.32
1 OS13 Nt403-SS 75.34.3
12 Dkhlotaallm
NO uOIL
1-0
0.12
1 M1014 03-59 107.06-2
1,1-0fchloraelhene
NO uWA
5.0
056
1 05A,f1403-K 7$.35-4
da-12-Drr)iiprnc9,en4
D361 uVL.
50
0-19
1 05f311fi 03511 1M-59-2
l
1.2.OreNa 9de
ND
I 56.63frW5,
1,2-DlcMaoprop.rre
NO LIO&
10
0.21
1 05f31114 03.59 70.57-5
I,3-Dichlw M.P.de
ND ug1L.
La
0.10
1 Q6f3,114 D3;59 142-20.9
REPORT OF LABORATORYANALYSIS
rl.. noon r.r.wra
r.P.orrxd. e.up�
i.x
D.1n 06ei Wnt4 09 70 AM
Perr Ar +A i q....,er I•c Paye 17 0173
t' TQ 60p
Pxe AnNrlNN,lan4.... Ih.� �^,r1• .k�11W. cM 74
I.W M.�n.�. NC ]607a
fAu*76aO92
ANALYTICAL RESULTS
Prole[1 Su"CWeed-h41 AIry 1111Lj
P.C. No . 92203121
S+mpla: MW7 LAID: 9220312t00a Cac,"r1 OSR6f1412 o0 Aviceiyed. D5,2W$&l5.20 MaYvr VII6Nr
glPA
P.rnme - Rayu6. ki1a Lrrdl MDL OF P,.P.r.d Anetyr4d CAS No. OLWA
6240 06V Low L-I L..dflll
An4lyilcu Method: EPA 626U
m , 3•dchtore0rayena
NO uyL 1 D
013 1
ONSl 014 0159 10011I
f-II-11-016lore..Pene
NO .D& 4.0
0?0 I
Milt403:59 101101-024
Enylluou."
NO 4& 1 0
030 1
Owlt$4 113:S9 100.4t-4
2 Nexennne
NO uQ& 60 ❑
0.46 1
DIW31114 03 59 S91-I6-0
lod.-th ne
NA LPA 10 0
012 1
0503IR4 03:59 74.66-a
fAv,%vIdne Chlarfdn
NO uQ& I 0
0 97 1
05111/14 03:59 75-Q9-2
4-Mchr1-2-penlenone 4011Ki
NO uIVL too
0.33 1
OU31It4 Pal fill IQ&To-1
St►
NO udlL 1 D
0.26 1
OW61114 03:59 IQ0 42 6
s 1,1,2•Teo4rhemrpe.r4
NO UAL S0
0.03 I
05f311,401:50 630.20-0
1,1,2,2-Te04 chwoe It-
NO we& 30
040 I
pSf3111403:5: 79.34.5
ToWli ede0rehe
NO nk 10
046 I
031317t40]:51271-164
Tolwnr
ND I*& 1 0
026 I
06r3t114:3.59 106•Sbl
t•T(W9woalhana
NO LvIL 10
046 1
05f31M43.66 7135-0
s 1,2-►nt:nl0r0ertlane
NO IpA I
029 1
0O13115403:59 7040.5
TrrAl0ru.lh.na
ND uD& 10
O47 1
0513111401:59 79.01-0
TekhbroAuorometnene
NO AIL 1.0
020 1
a5r3111401:59P 73-09-4
t 2.]-Tnchllroptop4ne
NO ugIL 1.0
0.41 1
owl '1403:so 96-164
V1rry4 80e4014
ND uak 5041
0 35 I
431 W4 01.5R 106-054
Wyl 411"ki.
ND v9,L t 0
0.62 1
D5131754 03 59 1"14
X*m-ITO-11
NO uto, 50
O66 1
O6f3,11403 so 133D-207
Sta.r.p.f..
4.&mm�4uara0eniene 191
99 fit 70.130
1
05/11/14 03 59 490-00-4
1 2-mm. ceM4a..d4 [S]
06 95 70-110
1
OS03171403.59 1706007-0
Toluene d6(s1
too % 70.130
1
OSf3sf 1403.69 2037-266
232013 Alhmlkn ft
AnNylkal Melhad: SM 23209
Alka4nity-Tnlal e4 CaCO3
75100 uyrl 5000
low 1
08f03114 14 11
4500320344Wa W4114r
Mel)lKal M.d1ad: SM 4500-SW
Sulfide
ND ugA- ION
100 s
('"W1416.41 16496-256
3011C Arians 26 Day.
n,r.lyllrad MaFod. EPA =.0
5ttkto
6670J dy4 250000
71Mi0 1
0"3,1406.06 1490679-6
ANO Chlorld4
Maivilca1 Ma91od: SM 4500•CI-E
Chlarlde
26600'IDL 2000
2000 2
O61111141600 15061-006
AS OCHE Cyahldo. Total
AnWy9c41 Melhad• SM 4500-CN E
cy-W.
6-6,1 uWL to D
so ,
oemlfta it 12 SI 17 6
62ZOD COD
M mflmM Melhod SM 52200
C h,""P Or7p.n DiriTmd
3S000 up4. 25o00
25ooa 4
D67IWt411.40
6310B TOC
Analyl4val M.deOd: SM 55t06
TOM Org 11l Cp6on
1390 up'L 1000
4000 t
05MO14 Peale 144044-0 M1
REPORT OF LABORATORY A NA LYSIS
Th. r.Pnn r.w rw1 M nPrOdurwd..ox.Pl n NY.
Dose O6fIW0140620 AM
6 073

I-- Analyd"4 9.Mc.a, Inc P.m A.Mole.l Sh k4., WK.
ceAnap�.. e 9WO h4nr.1 Ar. L[M 100 aceAna! 910 %.eef Aw 6,1k �00
lytrcal Hr+rw. MG min / f ` ��� • Hono O. NE 21111176
•.I.ne[awn un fl[N16759o9Q � .w+.yarww«m
17d4jeylLDOa7
ANALYTICAL RESULTS
P,.J-k. Surry C4o.. d-Mt Airy IWCI
Pere Proj.a No.. 92203121
prol.cf. Supry Ckead MI. pyfy ful C:f
Pau PI .1-1
NO.. 9220121
ANALYTICAL RESULTS
$a"IPW Me+f 15
Lau 1p: 92213121807
Co11e Iod05,7JI04 01 AS
A',eeOlyed. D6129r1d 15720 µe6q: V*bF
S.Inpt.: µNf-16
Lab IG- 92203121007 Callecled: GWl Jkl14 0g:d5 lib"Wad: DWlteI A 15'?a Mavu: V V.14r
Report
Report
Pnem.tera
Ft ... te umt,
LJlret
MDL
DF
Pr.P&W Analysed CAS No Qum
Paramslera
R. WI. 1k113 Lp"I
MOL
Of Prepared
Analysed CAS No dwl
6010 ICP 0r dw.ter
AnaMlcrkl Method: EPA 601D l reparalim Method: EPA 3010
6260 MSV Lew Lwel Lmcll ill
An.h/pwl Method: EPA 5260
Arramonv
ND uufL
6.0
6.0
1
OWI1412'30 06041t420-15 7440.36-0
da•1-3 olcfaoropwp.ne
NO uyL 1.0
0-13
1
051 IRA 04:15 )ON 1-01-6
o1luow
No uDfL
10.0
5.0
1
OW311412.30 061D441420.15 7440.36.2
vana•1-S•olstdotopropa.a
No uO,i 7.0
0.20
1
05131f1404:1S 10051-02$
Bar-
37.SJ ugfL
1DID
5A
I
06MV1412:30 OSf0421420:15 7440-39-5
Elhvlkk-z ne
No u;)k 1.0
030
1
OWW404'15 100-41.4
Beryllium
ND ug7L
fA
1-0
f
D6M31141Z20 0&0411420-15 7Wp-k1.7
2-Ne>tenone
Alp uulL Soo
DAB
1
M111404.15 591.7"
C4dml.m
ND uyL
1-0
1.4
1
D6f W 472-70 OWOQ 420115 7440J3a
lodometh.ne
No vDR 1D0
632
1
0SId1114 W.1S 74-06i
Chminhum
ND uyL
100
5.0
1
O6fa3114 12'10 06'040 $4 20:I S 744047.3
Methylene Chlorrde
No uG& 1.0
DIP
1
ON31014 04 15 75-0¢2
Cc6e11
ND u0R
10,0
59
1
OW301412:30 06+W7142015 7440.414
4•M*Ihv6,2-penlenone JM1951
No oo'L 100
039
1
05Y31114 Dal 15 1D410.1
Copps
NP uDt
10.0
60
1
ONV3f1412:30 057041142035 7440-504
Styrene
NO ugl 10
090
t
051311140415 10042.5
Ira+
2640 uD4
300
SOA
1
O MYt412:]A 061W1142015 743"o-6
i,1,1 ,2-T4tracNor-wan.
NO ugA, 5.0
0.33
1
0613111404:15 WO-20-5
Lead
ND uyL
10.0
5.0
I
O MU14 12,30 0610404 20.15 7439.92.1
1.1,2,2• Tevachlw"Ih one
NO uwt 1.0
0.40
I
06/31114 041S 79-34•S
NIcMN
ND uDR
SO
5.0
1
D6lolt4 12'30 WWI W 16 7440-02-D
Telraadorumene
0-743 uDrL 1.0
DAB
1
05411/14 D4'IS 127.15-4
S.Ieruym
No NyL
10.0
10.0
1
1161D3A4 12:30 COMO420:15 77112.49-2
7okme
No uyL 1.0
025
1
Mum 04.15 106.M3
Solver
No ug&
10.0
5.0
1
061a711412:]O O81G71420:15 7440.22-4
1,1,1•T1kd.bforwena
NO uWI- to
0,46
1
11"10404:15 21-.55-6
Yhnw.m
ND aryl
5.5
S.d
1
08703714 12'30 06fo411420'15 7440.26-0
1,1-TrlGhluaew4,ne
ND uyL 1.0
029
1
05131/14 IN: Is 79-00-5
V.nadwum
NID uA
25.0
5.0
f
O"W1412-36 06,'Od11420-15 74a662-?
Tlldhlm-M.na
3A dyi 10
0.47
1
D513101404'15 79.01.E
2-
NO uyL
Id.o
foo
1
O6f03f141730 061W71420-15 7440-06-6
TrkMao6unrvmetfiene
No uOR 1.0
d20
1
O61311404:15 75-09;
12.3•Tdcnloropropene
NO rig,L 1.0
O.a1
1
051310404:1S W13-4
62" MSV Law L"0 LandvWl
AA.ly mP Method: EPA a260
WO bamme
No u0b 50.0
0.35
1
M104 04.16 108-064
Acetone
NO u%L
100
10.0
1
owl ft4 W:15 6744-1
VYy4 Ndcrwo
I'lluofL 1-D
0.62
1
061310404:15 75-01-4
kn Acryo.
No .+g,l
200
19
1
05131"4 04 15 107.13.1
7C Am (7ota0
NO ugfL 10
0.66
1
oSfS11f4 44.16 1330.20-7
8.�7.ne
2-3 uyL
$.0
0.25
1
95r31114 (M 5 1143-2
swrpite.
&on+vnhkrvmadnna
NO 4&
3.0
0.17
1
05111114 (14:16 7447.5
MBram ilLwohenzene (5J
100 % ?0.110
1
D531114 IN 15 4E04)0-4
Bromodlchlurumewane
NO 4g1L
1.0
0.10
1
051210404:15 75.27i
1]-plcMorvetMne-dl (5)
97 % 70.130
1
OSA 1114 WW15 1706007-0
Bionwkm
NO uk
3.0
026
1
M1114 04:15 15.25-2
T.Iuk- de f51
go % 70-130
1
OW3104 04:15 2037.20.5
&omvmeaene
NpeW1
1 0 D
029
1
OW3111404:15 74-63.9
2320itAMal lnity
Anety11ce1Mathed:SM73709
x-&rtanme(MEl(1
ND uyL
too
096
I
IIW3111404, 15 76-93-5
Carbon d-Irlde
ND uyL
100
1-7
1
OSf3Ill 404-15 76.1 S-0
a kalnny. Tolal a. Co CL73
44M uDL 5000
low
1
o"W14141.23
Carom tatractw1 ma
ND ugi-
1 0
CIS
1
OSf3$11404-15 5&23-5
1500320 SuMde Wader
AnalyDtel Mewod: 5M 45065,20
Chluowil.n.
2.2J uyL
] 0
023
1
D513 N74 o4:15 10690-7
Chlvmv an.
0.66J uyL
100
0.54
1
M11140415 75.00-3
Saone.
ND uwL 1DO0
foo
I
06=01416-47 1149626.6
Chlorebrm
No uoL
6.0
o.14
I
M1114 04-15 47363
Chfe Inawerw
No uux
I.D
0.11
1
OW31114 W:1S 74.87_3
6Op,01C Rnlena 26 Oay.
M41yIlcel Method: EPA SIXI.a
1 2 pi6rvmo-3-chlwo{xopanc
No ugA
130
?.S
1
M104 W 15 96-12.6
5ulfat.
ND uyL 250000
2000
I
ONOV14 20:33 $4601.79.6
p�Iorrwchaorr.mat,.na
ND uDA
10
021
1
OSAl114 W:15 1244d-1
12-0Ibtomee w.m. (E DBI
No uD4
1.0
1127
1
OU31114 04 IS 105-93.4
46Od cedoa de
Ana114kah 106twd. aM 4500•C1•E
puomometnane
NA aryl
I .0
D.21
1
oSAV1404:15 74-95-3
Cnlorld.
1660 uWL f000
t000
1
36W1 1416a1 16967-06.6
1,2�plmlaoben:ene
NO ugh
5.0
D.30
1
05*101104 $5 9530-1
1.4 Omwob-aim
3.1 uDL
1 0
0.33
1
05737/54 0a:$5 1064E-7
45W NE Cyanid.. Total
l�a
Anelyll PA-0-4 9µ 4`soO-C7J•E
faN16-1,4 L11ehwro-2 Iwlvne
No uA
too
1.4
1
0613111404:IS 110.57$
1,1 •picl+lwvalh.ne
14,2 uDL
5.9
0.32
1
OV31114 04:15 7S-34-3
Cy4oiIM
Np u9+L f9.0
7.0
f
OdfOW14 It:fi 67.12.5
12.Ou3dwu.d+ane
o.68,1 uyL
1.0
0.12
1
05131114 04:1S 107-05-2
62200 COD
Aneloicat Method. SM 62200
1,!-plchlarv.lhene
NO -wt
11.0
p36
1
OSf3111404;15 76.3E-4
do-1,2 Dlcidn.oethvne
36.2 uWL
5A
0.19
7
Wr13117d W:16 1BII
Chemcat pry pen Demand
NO 'A?5nO
25W0
1
OWW4 1140
tom-1,2-plcrdoio�w.nc
NO n9R
5.0
0.49
1
Wi131114 o4:15 156.60-5
Sit oa roc
A"Wal Mewod. SM 5]10H
12-Dkf wg-p-.
ND uyL
5A
G-27
1
0S731114 04:16 76-67-5
1,3-OkWunpupan.
ND uyL
1.0
02a
I
Mill 4 D41 5 142-Z6-9
T;W organic Cwp
070 uyL 5000
sow
5
a6MN14 f0:13 7440.64.0
REPORT OF LABORATORY
ANALYSIS
REPORT OF LABORATORY
ANALYSIS
Ire. r.pen.hn
not h. r.pm
.e. w-.14 n
nAl
The reel,n eon wow
npud.e.o. e.e.oa x."
Ume Dist 12n014 ae 2O AM
v 11 out"-ftr oo -t W
Pace Antlec.r sort
na. Irv. Page 19 of 73
0.1e: tl6112a0l4 DE:2o AM
. -t u,..v me. we..+ri or
Pep Ar Ir oel Svww. vr:
Page 20 a173

Paw Analyeul a.nlwl, In.
aceAnalytical' 9M Kw v Are Shar.10D
INnne-a.dA. NC 29079
iv`rYt'+- 1p1�6i5.�a617
ANALYTICAL RESULTS
Plole[I 3h4ry Gluedd•Mt. Ivry (0c)
Pace Piopct Nv. 932R3 t 21
6ampie: VVIAZI Lat1POi 9220a121000 Caapcled05YaI1114040 Reavlyed. 05QWIA1570 Mablz.%Wmt
Raporl
Paremele.a
Rdeut. Lftb.
Ll..al
MOL
Of
P.epred Anelyred CAS No. O4ai
1010 ICP Oreundraler
As0owsl Moftd EPA 6010 Pnepa1allm Mallwd: EPA 30tp
Anunwny
NO uWL
0-0
5.0
1
OMWIA 1216 OWW42018 7440-360
AmNe
NO "OIL
lot
5.0
1
0610Nt412:30 05MQI420.18 7A40.30.2
Barium
63-AJ u01L
lop
5,0
1
OSM 11412-30 OM041t420'111 7440.39-3
9eryeklm
NO ugA,
1.0
1.0
1
ON031}A 12:3a D610U1429:18 1440-41-7
C.dr m
NO w-
1.D
1.0
1
01 12.34 O&W 4 20 18 7440.414
GH-OMK.rh
NO uqA
Inc[
5.0
1
OMUTA 1?30 D6104y14 20 18 1440-47-1
Cobalt
6.13 ugll
10.0
50
1
0610LN 1230 0611141142018 7440-404
rwvAr
A10 uqk
100
6.0
1
GMU14 $2 U p6164114 20 I 7440-50 9
trod
No ug?L
300
50.0
T
OtAyU1412:30 OW0411420:1a 7439-896
Lead
NO uq&
10.0
5.0
1
D&03114 12:30 05/04114 20:11 7431-92.1
Mckel
NO ug1L
50,0
$A
i
06fON14 1216 0610A114 N 14 7440-02-0
S.P.nnrm
NO u04
100
Inc
I
0810N1412:30 p6+04y142011 TMA9.2
SAV.r
NO uW1
100
50
1
O6N31141i=30 MOM 142010 7444/474
TpA14um
NO uO&
5.5
54
1
O61DN14123D 06M0420:16 7440-250
V-111.m
NO ug&
T5.p
50
1
0540111412'30 081040420:It 7440-02.2
2ehe
NO uuA
111.0
Inc
1
O"U1A t230 OSM411420.16 7440-8114
02e0 MSV Law• Laval Landi l6
A.Wvllcel M.6md EPA Von
AcHim
NO up1
100
10.0
1
05/31,14 04:31 07-04.t
ApylprAte.
NO up4
200
1-0
t
051310A 04:31 107.13.1
Benxane
NO upk
1.0
0.25
1
ONWIA 04;31 71-43-2
Bromaddvinrn.lhanv
NO uWt
3.0
017
1
ON710A 04:31 74.97,5
BfDmodrCnlarameMne
NO Leis
1.0
*IN
1
05F31114 04;31 75-2746
Bromalo+m
N0 u01L
3.6
020
1
UN31114 0431 7512&2
Bram0mea1e.la
NO ug1L
$0.0
02S
1
053111404:31 7423.9
2-Bulanone (MEN)
NO uglL
100
0.00
1
OS13111A 04:31 70-93.3
Oorbod dleulede
NO u91L
100
12
1
0513111404:11 75. 50
Cwllah taOddAN Ida
NO u01L
1.0
0.25
1
0541111404'31 56&23.5
Chl�rOhdnx.h.
O.ON uy4
2.0
0.23
1
OWIMA 0411 10&90.7
CNvrvelh-
NO uyL
loci
p54
1
05r3111404. 31 75-00-3
C11kav1o.m
NO NyL
5.0
014
1
0573N1404:31 6740.3
Chlervmenane
NO ug1L
1.0
0.11
1
0513111404:31 7"14
12-61. emn-3 rldprvprnP.ne
NO up4
13.0
2.1
1
ON31114001 W12-8
Dr&an dkk"memlave
NO uda
3.0
021
1
M3111404:31 124.46.I
12-Dit-Whmm. rEO61
NO.9&
10
027
1
(Will 40431 106914
Oro.pmnme9.A.K
NO '.'it,
10.0
021
1
Mill 404:31 74-W.1
1 2 ph:nlmr.nanrenv
NO ug1L
5.0
0.30
1
Mill 31 96-W1
.A-0kg0-b.nrvp6
0.703 ugeL
IA
1"3
1
0N311140411 106.46.7
b ana 1.4 CNUlarn-2-bu■P.
NO ug1L
100
1-0
1
OSP817140131 110-57$
1.1 10.1,1-mane
9-3 NO1L
5.9
0.32
1
Mill 404:21 75.34-3
1.2 0-11A0roelhave
O A" Lat
1.0
0.12
1
01MIll604:31 1040-1
1.1 D.1-4 v th-
NO ug1L
5.0
a,"
1
05/51114 OA]1 75.36J
da 12 Dkhlorovlhwne
20.1 uyL
5.0
0.12
1
05r3111A 0631 166.51012
unn41.2 LNnlw.evNl.hH
NO uq+L
50
016
1
051311140431 16660-5
I T-O.cli4nlpropeue
NO uR&
10
027
1
09311140431 78.07.E
1 S nw-hlnrvprvpnne
NO iig1L
1-0
0.28
1
05all140411 142.26-9
REPORT OF LABORATORY ANALYSIS
rIw-.Wn MY.wlea..P. d..apF kA
Date 0611 N76 [A 06 20 AM a.n" a.a �n..e.0 ­1 of Pep. Arl.iyaul s..w.. I� P.04 21 0113
.-f cmm)ytIcal'
An.yKWu.m.
ANALYTICAL RESULTS
PtoKct. Sung Goes d4Al "JU1C1
Pea ptojed No. 92203M
Faw Ar 0,14-t e.rvk.f, ln..
P670 Miner Are &.1. rd0
1ar.r .. NG le)?b
i704N 54atia
6eopld: a I
La6lO: 9220312100 Cnldwd; MN1413-40
RdcNyad: 0512811415:20 Maab: 9M11er
Repon
ParamvI*m
R.gila Urun Lrm11
MOIL
OF
Prepared Molmol CAB Na. OW
8260 MSV Low Level Landfill
Malyecal Method EPA 8250
de-1,3 OIGAoroprop.na
NO up2 I 0
0 13
1
D631114 04.31 10061-01-5
bar141,3-OChlOF.prapI-
NO up1L 1.0
026
1
061311140*11 1OW142-6
EOglpPnrarm
No OPAL 1.0
030
I
0573111404:31 100-414
7 Naxanana
NO ugA 30A
0 A6
I
O6r M4 04.31 501-76-0
ladarh.elh r..
NO uyL 1DD
0.32
1
ON31714 war 74-66.4
M.8ry1.n. Chh-d.
NO upll 1.0
97
119,
1
DY31114 QUIT 7549-2
A-1Aet1y1-2-P-t0w.(MION
NO uyt 100
0.1
ON3111404;31 10&101
64y..ne
NO uQ& 1 0
Awe
1
iW311140411 100-0-11
1.1, 1.I-Tee.chkw"Ihane
NO ug4- 5.0
0.33
1
MVIA 0413t 030,20-6
1.1.2,2-Tat-hiw-8,ene
NO UOL 3.0
040
1
ON3111404;31 79,34.6
1ab4Khlwpee+enn
NO uyL 1.0
046
1
ON31 F1404:31 127. 1"
Toeleaa
NO uok 1.0
026
1
OWIM 04:31 106-60-3
1,1,1•T"iorv69um6
NO"A. 1.0
0.49
1
060*11404;31 11-5545
1,12 Tndhto u.8lane
NO uglL 1.0
on
1
0575111A 04 31 79a N5
TrIchimoeihehd
1-5 u&t 10
047
1
05r1111404-31 19-Oi-6
TrleYdoyveuviometl.4ue
NO uW& 1.0
0.20
1
M111404:31 75-694
1,2,3-TdchloaaP "-*
NO uA t-0
0.41
1
0513111A 04:31 W-t64
WOPw-ty
NO ugL 50.0
0.35
1
ON311A 04.31 106 D5-4
Vwyt 01.1ld4
NO u0M1 1 0
D 62
1
05r3N14 CA 31 75-01 4
Keene ITotal)
NO up4_ S.0
0 06
1
0931114 04.31 1330-20 7
Sul.vpafaa
4-Bramo luw oaenren a (5)
S6 % 70.130
1
0151114 04:01 400 W4
1.2-li:ehlvraedune44 IS)
07 % Mt30
4
WWI 17060-07-0
T.Iuane-d6(S)
Ito % 10-130
1
OU311140421 2037.265
23"ll Alkalinity
Analyllcal Method SM 23206
Ask mtr - Total as CeCO3
14me u01L 5000
low
1
0MV14 1444
460082D Su1Rd. V81er
AruM-1 Meshed SM 4500-S20
S.nFde
NO ug& 10130
100
I
00+0NIA 15%7 10406.254
300.0 PC Anlon. 28 Days
M4lytkal Memo! EPA 300 0
SLOW.
NO ug1L 250000
2000
1
06r05/14 20.47 WOO 79.8
ABDO Ch4orlde
Arullyllcal Method SM 4500 C1-E
CPklnd.
27e00 ugIL Ion
1606
I
(61111141802 180ai1606
4WC NE Cyanid., To1.1
Anwyvu1 Memvd SM 4500-CN E
Cyar.1de
NO ug1L 100
5.0
1
1161OW14 11 17 57-12-5
62290 COO
Melylical Method SM 52200
Chenxal Orlrgen Demand
NO upi 2$000
2ZOOD
1
ow Ip114 1.1-40
93108 TOC
Matyenl Memad SM 53109
Tntat Organic Carbon 10700 ugiL I00o 1000 1 06f06114 00.m 1440.44.0
Odte 0611=1406.204M
REPORT OF LABORATORY ANALYSIS
TMa upon n" nplb iwr-a d. Axo.p1 M e4I.
r.n�wr n.. hA, morn et P" A -yew 5- hnr
PAev II el 73

Pan Aanynnr arrvlp.l. Ina.
P... AnAybrar a.rvrral, N.e.
aceAnalytical`
1e5nrtu^.r •r. 5�w Imo
.
ceAna rcal'
Wy 1 w c.y Az a... IOU
r
. r 4. HC ?d0i8
yny Oil. NL Y4076
17G4Ie7'✓ppYt
��r�
rirll is iSJi�7
ANALYTICAL
RESULTS
ANALYTICAL RESULTS
Ptofrcl Swry clo.ed4 l AAoy ltll C)
pmJw Sorry Clarrd
MI. wry [O1C}
Paca Plq.cl NO. 92203121
Pa" Prujecf No.: 92201121
Sample: MMI
L.1,10: 122d3121001 CWI.M.d 05f1611411 35
R.-,-d: DWZW141520 M." 1rJalar
5-pp.: MW-1
Lab III! IPM212-1041 CakePodDN2&1411-31 Reueiwed 05QS0415.20 Maoix VWw
Report
Rapbn
P.nmerere
R-M. I)rub Llmt
WL OF
Pr.pared Anafyma CAS N. Ou41
P.Iam erer.
R..A. Wk L1mlt
MOL OF prepmld
A.WVA.d CAS N.. tlud
4010 MP Omnedwmw
Au.lylkal Medved- EPA. 6010 PrnprrApw
Merhpd: EPA
31310
8240 M5V 4aw L.r4I Lvtdf111
AnYyLc-* Malhvd: EPA 6260
Ahlmrony
NO uOIL
6.0
SR 1
0610311412"30 O&W 14 201.21 7440,35.0
da-7.1 DwNurawop.n.
NO u04. to
0.13 T
W31114 04:" 19061-01-5
Anew
NOuyh
100
5.0 1
05MU1412:30 06MW14MI 7440-38-2
imp- l,3-Dlddaroplopene
NOUA 10
026 1
057310404:46 IOMI-02-5
O. ium
51.2J u9tL
100
5.0 1
0MV1412:30 0WoW42021 7440.19.3
E6lyben2enr
NO upi- 1.0
0.30 7
M10404:46 100-41-4
d.rylhum
NO u0h
1 D
1 0 1
06103114 12-30 Q&O4114 20'21 744041.7
2-Hmmnone
ND u0A 10-0
0.46 1
054V$74 04:46 5rM 7"
CadmWm
NO uWL
1-0
1-0 1
ONW 1412:30 06fWl14 2021 7144" -9
I".M.tn4n.
NO Me& 100
0-32 1
Q5+3114 04'46 14-W4
Chla mm
ND uWt
10.0
5.0 1
961 MA 17:10 06*4014 2021 744047-1
Memylmr ChIm6.
NO u01L 1.0
0.07 1
OSf IM 04:46 75-09-2
Came
140 UA
40.0
5.0 1
06 N141r30 W044T420:21 7440.48.4
4.MoIhVI-2-pen1vnm. I MIOKI
ND UgA. 100
0.13 1
ow -I 404:46 10&10-1
Cupp.,
ND.@A-
10.0
SA I
OMVI412:30 0&D41420:21 7440-50-0
Styrene
ND u07L 10
023 1
OSy3I01404:46 100-42-S
Iron
4490o u0rt
me
50.0 1
0&03014 12:10 OW4A4 2021 7439•1110.6
1, 1,f,2•TrCefMvrvenerl.
NO uQ& 5.0
0.23 1
0501M 04:46 030-70-0
Lend
ND Ir9,L
10.0
5.0 1
0&OY1412:10 OWW1420:21 7439.92-I
1.1,2,2-TekadYorvenarla
NO u9n 1.0
0A0 1
(15ti 1114 04.46 19-34-5
NIdN
N0 ug&
50.0
6.0 1
GWW14 12'30 CWUI14 2021 7440.02-0
TaaachIw.wh.h.
NO uWL 1.0
0.46 1
0&31114 04:46 W-16.4
Selenium
ND uglL
10.0
T0.0 I
0510311 a 12:30 OW04114 202T 778249-2
TeWena
NO WA 1.0
0.26 1
OU31114 04:45 1*811-1
Sdrm
ND u9&
10.0
so 1
OSMY14 1230 06r0411471127 7440-224
7,1,1-Trk31lgdelhene
NO ugh 1.0
0.46 1
MUM 04:46 71.55.E
Thellaim
NO ug&
5.5
5A 1
061p3f14 12:30 0&W714 20:21 7440,2E-0
1.1,2-Trkhkma6lane
NO 4A 1.0
020 1
OU31014 (M 45 794D&5
V.neA
NO uyrL
25.0
5.0 1
NOW141200 0610i1142027 7440-U-2
Trlohfur o41f4nr
NO uA 1.0
0.41 1
0613lf7404:46 79-013
4-
NO ugh
10.0
$0.0 1
O&OW1412:30 0&0411420:21 7440-86.6
Trknla oAuorvm40Mne
NO uyL 7.0
020 1
OW31r740449 7M9-4
1 ,Z,YTrkhkfapropan.
NO up4 10
0-41 1
MIr1404.46 W16-4
82ZO M9V Low Leyel t-010
Allldyec.l AleHlad: EPA Me
vino 4"u"
NO LIek 50.0
0.35 1
DS03W4 04:46 108-054
Acelw+a
NO UWL
100
10.0 1
05r1V1404:46 6734-1
Vefylcma We
10A'-U& 1.0
092 1
DSr311T404:46 75-01-4
Ariykuuldle
NO uDt
20D
TS I
0513111404-40 107-13-1
Xykne IToI.p
NO L.pJA 6.0
0.6E 1
MIJ14044e
B-Z-
33 uWL
ill
025 1
0Y3u14 W:46 M-4a4
9w vaf"
promo nloromemane
NO vq&
3.0
0.17 1
05R7114 04:46 74.97.5
4-Hmnw lUorobenrene 1S)
99 96 70.130
1
MV14 W 46 460.00.4
Dromodchlernmam.ne
NO ugh
1.0
D.16 1
06131114 OCAS 75.27.4
1,2-DI hldo.than.-d4 [S)
99 % 70-130
1
O'Y31114 04:46 17050-07-0
OwrlwWrm
NO u0h
3.0
D26 I
M1014 04 46 75.25.2
T-Mena-da f5I
Id0 % i0.710
1
05031014 04 4e 2037-26.4
llidmunaP.rlr
NO q)L
10.0
029 1
OW31114 04.46 74.83-9
2320H AIkalknfiy
AneNUcel Me erod SM 23208
2 $Idanwre (MEK)
ND vWt
100
0.96 1
Will 14 04-144 7a-93-3
CUP- dl-led.
No ug)L
I"
1 S! 1
OW3104 04:46 15-16-0
Afk.hMly, T91.1 A. CeCO3
112000 -WL 5000
1000 1
CM3014 H 24
Carbon IeVeaY wdr
NO u9R
1.0
0.2E 1
M1114 04:46 56-23.5
460OS20 sulfld. NMlar
A%alytical Merced: SM 4500-920
CAWIob.n2en.
2-43 UWL
1.0
0.23 1
M H1404:46 106.90.7
Chmmem.ne
1-93 .DrL
10.0
D.54 1
0&SIMI G4;46 75.003
Sullde
NO 49A. 1000
700 1
M03014 M53 19496•Yxt
Chm,.brm
NO uDIL
5.0
0.14 1
MIMI 04:46 67-0 -3
CMMM.00..
NOuA
1-0
0.11 1
owi101404:48 7447-9
300.0 IC AM-. 26 O.y.
PnalyrkN M.mod: EPA 300.0
12 Dlbromn-3-duwupuRanr
ND uA
tie
7-5 1
om 1114 04,46 9e424
SWIOIC
NO uok 25DOOD
20M7 1
ONW1421:00 14a0a-79-41
Of roawehgrowfw.
NO ug+L
1.0
0.21 1
MSr3111404*5124.46.1
12-perwlf Ih- (EW
NO ugk
1.0
027 1
0934114 04:46 10671.4
AM C4,110fld4
M.IW4.l Meewd SM 4500-Cu E
011.wwewther..
ND uOrL
10.0
0-21 1
0513Ill 4 04:46 74-01r3
ChWr:de
451DO u01L WOO
5000 5
DW1111410.02 161MI-M b
1,2-0kl4umben7ene
2.1J MWL
5.0
030 1
05r3104 04:46 95.50.1
1,4-0l" .......
1A ug&
1 0
0.31 1
05,11111,04491 1G6-W7
62200 COO
An.lyl"P Metrlod. SM 52300
1w-1,i-DItl1i0rP 2-hwrnr
ND 4&
700
I.0 1
05137f140446 IIMM
CherNul Oxy9.n Denrarw
33M uglL 25000
25000 1
OGI0114 13'40
1,1-1)0*0.0-
2.7J uOfL
5.0
0.32 1
ON3111404:40 75-34-3
1,2-OkhloroelMrw
O23J ugfL
1.0
0.12 1
0"M40448 107-06-2.
A3108 TOC
MelyOcel M.IhQIJ SM 53108
I,$,DKharovI"r a
NO mot
5.0
0.5E I
093111404:4: 75,3"
da-1,2-01c1Jmoemene
67 u01i
SO
0.19 1
05Ri174 W:415a-59-2
iylal O104n1c C.ravn
1070 u97L I000
70e0 I
O6r0er1a 01:04 744pJa-0
trans-1,2 DUJ+ororlh.ne
NO uph
50
0.49 1
0&3V 14 W 46 15660-5
f,2-dc40rroprop.na
NO u91L
1-0
017 1
Mau 14 04:46 7aa7-6
1,3-Dkhlgvprup.n.
NO uVk
to
0-28 1
061311140440 142.2&9
REPORT OF LABORATORY ANALYSIS
REPORT OF LABORATORY ANALYSIS
Thlr rrprr}.hal not D• rrgatlu[etl..xuq n
Na.
TN. r.F I en4 not fw r"rodca0.
--pt. Tul
O.ra: 0&421ZG14 08 20 AM
naqul n�. ,e.� w ..�Ior Pw
Negnd s.�p.1. �. PAU. 21 e1 73
U.I.' 06012f1014 05 20 AM
..n" we -n rn .A
P.c. Arly.rr 5-n P-
P.O.24 w 73

/Wila'ce Aaa)ytiol'
p44MN1en
ANALYTICAL RESULTS
Pau ■.4lyeu111. -1 res.
9e00 Nbr A.a Se.Y 100
HP�Yr.y4. NC 2WT41
Protect 5,my CI9404 Mi. Nry fU9 Cj
Pace Rohl No.. 112703921
$ample: MW44
Lah10: 12293121010
Cdkcied. GW26014 10 It
Recewed051291141520 M.10F VAI.
Rap.l
Penlmelue
Reauea LWIS
um6
MOL
OF
plepued AnKlrad CAS No Oua1
Soto ICP 0ro4gdWe141
An4Mk.l Me6tad: EPA 801 P Pf404r*J0" Me*04: EPA
1010
Arwmeny
NO.1pt
9.0
SD
1
1161031141230 a"WI42024 744D,36.0
A141.1c
NO ups
100
5.0
1
DOMY1412.30 06OV142024 7440-35-2
Bpflum
22.4.1 uW
1P0
5.Q
1
OLION1412:30 0810111420:24 7440-36-3
11"Oum
NO ZI
1.0
ID
1
DWI, 1 r 230 06mu 4 2024 744041-7
Cadmwm
NO aryl
to
10
1
06103d141230 06AW142024 1440.43-9
Chm-wen
NO 4,WL
10.0
50
1
DGMU14 42 30 O61W714 2024 744047-3
Cahall
NO kwk
10.0
5.0
1
0"311412.30 06691420.24 7440a84
Copper
NO .WL
10.0
50
1
DGM00141230 O&OV1420.24 7440-50a
froth
24" uyL
no
500
1
WON 141230 0d1W11420.24 7439.09E
L46d
NO Oyl.
10.0
5.0
1
OWN14 12'30 0 MMM420:24 7479.92-I
Wkm
NO vp1L
SO
511
1
DGeOW141230 09MW14 W24 7440-020
SWrn
NO uy1L
100
Ia.0
1
DWY141230 060OVI42024 778249-2
SIN.
NO up1L
100
5.0
1
060oL141230 OW041142024 7440-224
ThnAlhrm
NO ug&
5.5
11.4
1
0m)M4 12 30 D&OR14 20.24 1440-7"
V.waum
NO aryl.
25.0
13.0
1
OMM41; 10 96/W114 20.24 7440-62.2
Zinc
NO Owl.
10.0
$00
1
MMIO14 IZ30 P61W11420.24 74AW4
7470 Mercury
A.Wyee.l Merced EPA 7470 Pr.pare9on
Method; EW17470
Mercury
O.NJ uyi
020
0.10
1
0610711412:45 QWV1410:41 7439-97E
8280 M9V Low Lerpl 1,01416I
Arr.tyueM Method: EPA MO
Acalane
NO uox
100
f00
I
M1114 D602 67E4-1
Amwr4hlk
NO aryl.
200
1.9
1
05f3111405132 107-13-1
Benrm+
NO og
10
025
1
Mill 40502 7143.2
BTom do-mednn.
NO uga
3.0
0.17
1
0031114 65:02 74-97 S
lkn"Ckh1or61M6Hnl
NO uq%1
$.o
0.18
1
65R1n405.42 75-274
Bromo/erm
NO u9L
34
Die
1
05131/14 P5-02 7$.252
Brom.-Ihne
NO uU&
100
029
1
05n11140542 74E3-9
2 Bulml a WExl
NO WA
100
0.96
1
05031114 05 02 78-93-3
Comwk w0de
NO uyL
100
1 2
1
QSq 1/140502 7Y15•Q
Cerbon 1.0mchlonde
Nil UA
1.0
073
1
OW1114 05-P2 66.23-$
Chlorolnnlene
NO kIPA
3.0
0.23
1
0503101405.02 IM90-7
V4-math-e
NO uyi
10-0
0.54
1
05131114 05.02 75-00.1
cNarelwrn
NO UA
5A
0.14
1
05CIf140502 67-56.1
Chlmomeenn4
No .0a
10
oil
1
DW31114 0542 74E7-3
+ 2.O4uama l d+10r6plop-me
NO uµt
110
2.5
1
05131/14 05.02 96-$2-1
uihrohwdllwamnlhene
NO U04
3.0
Oil
1
05 V140"2 12448-1
12. NX0a 4min4{EDB]
NO u01L
1.8
027
1
M111405:02 106.6314
alWomo nnlhltne
NO uq-L
I00
021
1
DN311140592 74-95-3
1 2-Orrhla.vt.erueae
NO 4g&
50
030
1
a5A1114 0502 0-50 1
1.4 Dwhl-b.n7en4
NO vyL
I A
0.33
1
05 iIN 0"2 109-46-7
Trmn 1A. OWrwru•24ru1ene
NO uOIL
100
1 0
1
0513101405M 110.57-6
1.1 •QiCidMaelhana
P•1J uyL
57
032
1
050115405.W 7"-3
12-04dYavelMPr
NO W&
1.0
0 12
1
0513111E 05.02 f07A6.2
1.1-O4rNw aelnene
NO upA
50
ON
1
ON31f 1405:02 7535.4
d1-1.2-01chlp.evlhene
4.6J uWL
5-D
0-10
1
06411140502 lwwz
P.- ft"V ar ep.rr..., 4 .
2l4rly[ical I IunI.mN. HC 7rA7e
...Jti1k4 o.e 1704pTs9097
ANALYTICAL RESULTS
Project' Sufry Ck1uaM1 A1ry (UIC)
P401 Project No : 02203121
amepM: mmm Lb 10: 52Z03121010 Coeeclea. awar 1410'15 Received IrW2901413.20 M4ea NWer
Repml
P.ameten Re"lla urvd LWM MOL OF prep.red An.Nr.d CAS Ne Oual
6260 MSV LOW L►W LandlHl AAmry4fcal Memad: VPA 5260
Iran, 1 2-EWt*ft,.e1h.-
ND K&
50
0.49 1
OY311140592 156-W5
12-OKIA. pwpe..e
NO bpJL
1 7
027 1
0Y31)140602 7d47-5
1-3-0mmotopropana
NO uyL
1.0
02a 1
US031114 05:02 147-25-9
c4s•},3-plrjYprvpropme
NO WA
I D
0.13 1
MV1405:02 IK614i1-5
Pmn,1.1,OIc1101apl*we
NOuyL
10
0a 1
MI01405:02 1006t42-S
Edly474"-
NO r.pR
1.0
0-30 1
OU310141 05:02 10041-4
2-+pr4non.
NO r.uh
50.0
0-45 1
0513104 06:02 511.794
leaemelh4ne
NO uW4
10.0
032 1
06731/14 05:07 74-69 4
Me""& CWWde
NO uplL
10
0.97 t
05731/14 05:02 75 32-2
4•M46g1-2sarlimmme (WOKI
NO 4,DL
10D
0 33 1
ON3104 05:02 1W10-1
$ryrcne
ND uQ&
1 D
025 1
MI 05:02 100-42-5
1,1,5,2-Tetrpchlpve0+.ne
NO uyL
50
0.33 1
0511104 05.0k 63020E
1,1,2, 2-iekadi0rvem.n4
NO 4,01E
30
0.40 1
0513111405:02 79.34.5
74hachloroeth-
0.11J uyi
1 0
0-46 1
05131/14 05:02 127 16-4
Tahlena
NO uu&
10
0.26 1
MI11405,02 106-M3
1,1,}•Tnehwraeln.ne
Na u0A�
1 D
0.4! I
95A1n4 6$:02 71-SSE
1,1,2-Tidrlmnelh-
Na up1L
1.D
029 I
05 iMe 06:02 79-00-6
Trkhlmrrlhne
0.77J aryl
1.9
0.47 I
MIJ1405:02 79-01-6
hkhlwall"1om41hene
NO 4,p0.
1.0
0.20 1
OU31 F1405'02 ?"PA
1�,3.71khloroproL•4ne
NO Us&
1.0
041 1
MI 05,02 95-T"
V-0 if W1.
NO uy+L
SO
0.35 1
05RS1r14 05V2 109-0 -4
Vinyl ".-de
ND uA
1 D
0.62 I
Mi P1405'02 75-01-4
7lylene (7m.4
NO .g&
5.0
0.66 1
=104 05 02 1 M-20.7
Surropala.
4-Bfa...e4nwawnrene{S)
90 %
7p-130
1
MI01405;02 46D.00.4
t2-OkWboelhenl-01(9)
97%
MV0
1
0513VI40502 1706007-0
Taluene•d1(S}
10o%
70130
1
MIF1405A2 2017,46E
21208 Alhalln4y
APahldcal Method. 9M 25200
AIWa kty, Te1N .. CeCO3
1240Q uyi
5000
1000 I
0303114 ISAI
4500320 Strlll M MW
AP4lyllcel Ma md. SM 4500-320
34,1Ad1
NO u94
1000
IN 1
DSWIA 1$:$3 1549626.E
Si00-6 1C Anions 16 O%y
Mayucol Me mod. EPA
300 d
Sulmte
2210J dWL
250NO
2000 1
0619511421AI 14808-79-8
4600 Chl-W.
MMytkei Method: SM 4500 G E
Chlv6d.
271E auk
t000
1000 I
06rIleld III (It r5887 00-6
12200 COO
AA.40" Method SM 5220D
Chrnaealpeypen Ormond
ND up6
2S900
2NM I
06f1011413.40
83100 T4C
Ahdyt"I M6mad: SM 531 us
Toler Olp.nlc Cuhen
SW uWL
1000
IND I
0610E+14 0:63 744044-0
REPORT OF LABORATORY ANALYSIS REPORT OF LABORATORY ANALYSIS
TM TIpW M.N theta npvdrnY..-pk k. It• TM r.W+ N4. wi M..�o d e.r:.r4 w hA
Oaie 06112RDT4 06 NAM e.1 W a."M cw..nv W P"Afyhery 641- u.e p" 25 .173 Dale' OVQF2014 06 NAM a ,"m.+•. . n1 P- A -I f.... S.- i.c
page mNn

aceAnalyticaf
er�.rrm,in
ANALYTICAL RESULTS
P r-4..In l6ervlo. h-Mc.
GfM xrrv..x A✓e 3.61w
+l�n4rw�r.. NC p507a
1/tMlaes-w 7
P-Jed. Su+iy C;6. d-MI Airy tuICJ
P.- Proycl No. 92203121
3.t1p1.: MNh3A
LablO: 92203121011
C49eme4. OW&IA 06:40
Re.elred: 06Q11/14 1520 Mmbrbf- VIAL4ar
Rawl
P..r tere
Resume urks
1.I0111
Mot
OF
Prepared M.Nrad CA$ NO- Gump
60101CP 0rpundwe[er
MNyticel Me" EPA 6010 Preperobnn
McMod. EPA
1010
,wrtlmwv
NO u9/L
60
s.0
1
OWN1412:39 O6a7411420:21 7444-36-0
WwnM
NP"g&
t09
3.0
1
0&G71141P:30 OWW42027 7444-38.2
9-um
6.14 uyL
100
5.0
1
06103114 12-30 OW04014 20.77 7440-36a
a.ry9xrm
NO uyi
1.a
1.0
1
W07114 12:30 06/04114 2027 7440.41.7
Cad-
NO uOL
1.0
1.0
1
OW304 f2:30 OW04114 20:27 7440-4"
Chlumarm
NO uq&
10.0
5.0
I
05MV1412:30 0504r1420:27 7440-47.3
C0nel1
NO u91t
f 0.0
5.0
1
OWN14 12:30 061UM 20127 744048-4
Copper
NO 41L
10.0
5,0
1
O&OW14 1230 OGMI14 2027 7440.50-5
Lead
NO uOrL
10.0
5.1
I
03r1412:0 0 3&0411421121 7439.91-4
Nwlcel
NO UO&
SO
5.0
1
06106N3r14 fI30 OW0471420:27 7440-024
Selenium
NO ugA
10-0
10.9
1
OM311412:30 6610u142027 7782-49.2
36.
NO u9IL
10.0
5.0
1
0&031141220 08r0411420:27 7410-224
Tllalhum
NO uj rl
5A
5A
f
00mv,41230 OBIW7142027 7440-26-0
Var,edum
NO ug&
25.0
5.0
1
OMM412:30 061W1142027 T440-62.2
2nc
NO uOA
10.0
10.0
1
0143114 12-30 06104014 a.-V 7440.08-6
6260 M 9V Low Level L.Wfl6
Mmpy0ce1 Me6rod EPA 6260
Aceiune
NO uyi
100
101,
1
031 M4 05-17 57-041
AcrylenllrYe
NO uq&
200
1.9
1
05A11105, t7 IOM3-1
genlene
NO U$7L
1.0
0.26
1
05 l3 ,:65:17 71-43-2
Sr0m0cNa0mamane
NO ugA-
3.0
0,17
1
06r31040617 74.27.5
6roit+odiddWnmed+ene
NO uyL
1.a
0.1E
1
M11140511 75-27.4
0&0hwimm
NO uO+L
3.0
026
1
050MA 05:17 m2S-2
&orrwmea+ane
NOu@A-
100
029
1
05131r1405:17 7469-6
2 &dat+me IMENI
NO uq+L
100
0.9E
I
05r31144 06:17 7b83-7
Carbon hmA de
NO ug&
100
12
1
06r3411406, 17 75.15-4
Carbon l.beddwld.
NO uqa.
10
025
I
M111405:17 W23-5
Cnlorobenrene
NO up'L
3.0
(123
1
06131114 us, 17 106-M7
Cnwroelhene
NO VL
10.0
064
1
4S13$1140517 75-00.1
Chwrowrm
NO a0't
5.0
0.14
1
Mn VI40S-17 6141&1
Ci+wrorn./lene
NO ugA-
1.0
0.11
7
0611111405'17 74-87.3
12•0wrom.3•pda W>sop.11e
NO uWL
13,0
24
1
05MI14 as 17 P6-12-5
C1d+renwallpremep+erle
NO pqL
3.0
0121
1
05M, 146E-17 124Jb1
t2-0Ibronwe6+ane (EO6)
NO uyi
1.0
427
t
03131rt405117 106.99d
Olblemom.6lanv
NO uyl
t0,0
0.21
t
0 li I405:17 74.95.3
1,2-0kM.rOGenxene
NO VGA.
5.0
0.40
1
95i1114 CA:I I V'SO-1
1,4-0kNOrol>,u+rarb
NO VA
to
0.33
1
OW1114O5:f7 1011-w?
trula-1,4-Olw.ro 2-bu1en.
NO ug1L
100
1.0
1
053104 0517 11047-6
1,1-Om;NW"::QH.
NO uok
5.0
0.'32
1
MI t1e 05.11 7F04-3
I,2-0lptwr0.n+an.
NO �g4,
1.0
6.12
1
aV31114 65:17 107-06-2
1.1-DwN rueuwne
NO UWL
5.0
116E
1
OSr31114 05:17 76-35-4
d.-1�.-0IWwoeuiene
NO uO,i
5.0
0.19
1
0517171405:17 ts6-ss•2
eram•lypWowemene
NO Z&
5.0
0.49
1
0513111406:17 156-00-5
1A-D1d1:c11opene
No uA
1.0
0.27
1
0513 t11405:17 76.67-5
1 ,3.OIcNIOr.propaPe
NO uqx
19
112E
I
OEr3511405.17 142-T6Y
aa•1,3.Olddureq.pe+te
NO us&
1.0
0-13
1
g5r1f11446117 10061-0I-5
Paw;nNyrin16.rv1w1 rn
[iL 141k?afy[fCal • 966E nets., Are Swr 'LID
NunYnr4e. NC 26010
170e 16Tga09y
ANALYTICAL RESULTS
Project Slrry cia" •7AL N.y (up
Pate PraJea N..: 92263121
Sample: M9WR Lab 10- OUO3IM11 Cakded: 0"Mt406:40 Rece4yedOWWI415:20 Warm: mmf
Reparf
pelamelale Ratim Will. L H MOL OF PrapM ea AnNyaed CAS No Al101
6260 MSY Low Level Landflll
AnaMIc.1 Medtod: EPA 62E0
lrana•1,1.OichlWOplvpene
NO uyl
1.0
0.20
1 M1114 M t7 10061-02-4
Ethylbenzem
NO ugk
1.0
030
1 05111,1,10511 100-41-4
2-Nerenon.
NO ug&
50.0
44d
1 0S61r1406" 591.7E-0
todomethene
NO wg&
10.0
0.32
1 ON31114 05:17 74-6"
M.atylene Ghwnde
NO uu&
1.0
091
1 05731114 06;17 75-09.2
4(M18x)
NO ug1L
100
0.33
1 0513M405A7 109-10.1
Btyrehe
NO ugk
1.0
0.26
1 OW3111405,17 100.42.E
1,1, 4,2-Tatr.gto. oelhane
NO uWL
5-0
0.33
1 OW3111405:17 IIV-20-0
1,1,2,2.7.uadaorue6i4ne
NO npA.
3.0
0.40
1 OSWI1405117 79.345
Tetradtwr0.1hene
NA uOR
1.0
0.4E
1 OW21114 "A? f27-16-4
Toluene
NO uu&
1.0
0.28
1 Mina 06:17 106.6E-3
1,1,1-Tndllw.e6lane
NO uO,L
1,0
0-48
1 0&3f1140517 7$-55-0
1,1,2-1"dA.ue6lern
NO uqd-
to
a_"1
OW3111405'11 7940.5
Triohloreeat.ne
NO uryL
}.0
0.47
1 OW31114 05:11 7""
Tll�hlrrell.erumautwte
No u&L
1.0
"a
I 0611l14 05.17 16644
1,2, 3-7nchlnepr.pan.
NO Q0
1.0
0.41
1 OW111405:17 96-16-4
V" a.etale
NO UP&
50.0
035
1 05131/14 05:17 106.05.4
V"chl.flde
NOu0R
i.0
062
1 OV1111405:17 7"IL4
1Lylelt. [Tot.]
NO u01L
SA
0.94
1 .3111405:17 1350.20.7
Sunoprea
4-&om01uu0beniena (S)
1 46
70.130
1 OW31111 05:17 460,110-4
1.2-0I.Mw"kh--d4 (S)
96 %
7(1 30
1 06751114 all 17 17050-01-0
T.lnene-dm (S)
99 %
M130
t 060104 05:17 7037.26-3
REPORT OF LABORATORY ANALYSIS REPORTOF LABGRATORY ANALYSIS
FN-Noah Nw not W repn a d. noel n .JI T7.. repon"�tb. repwa.c.d, a "iA n ul.
One: OW12r201406:0AM .t_t--. nx..,.ctmp a.wrarl3N-1. P29e270173 Dale:11 IV21)140620AM rseioJlmefM c.n.udofP-A-"e se- x+c Page 250173

Pacekalyhcal�
.w,w.K•x*
ANALYTICAL RESULTS
[[ A..Myll[M Aarrin[, Inc n[ nelxr r.in..t Ar. &^ 10.
.._ft NC 2eO7a
(70AH95 PM
Ptnpcl Scary Clvaed-An. Pry ryrCl
P.,. Prele[3 Nv- 92203121
$erryll.' MW13
Lab10: 92203121012
Cu9rrcled 05+2&t4
t, 00
R. Wtd: OWW14 15:20 Maxb YWfar
Rep9n
Paramexn
Rn.Wr. UMI,
LIa0
AIDL
OF
arepa,ed Anepnd CAS NO Orla1
6010 POP 0f dwxpt
Anafleled M.Mod EPA 60t0 PrepareAvn Method: EPA 3010
Mummy
NO u01L
60
50
1
WON1412:30 D&WT42031 ?"0-M-O
Arms
NO uy+L
10 0
5 a
1
06/03714 12-30 05104114 20 31 7440130.2
B.rk+m
66.7J uO1L
too
50
1
0643114 12 30 06+04114 20 31 7440-30.3
El.vm m
NO -at
10
10
1
O60OW1412:70 0010111A 20-31 7440-A1.7
Cmrhm+m
NO ,np&
1 0
1.0
1
DSMN1412 30 (9f04114 2031 7e4043-9
Chrenflum
ND uyL
10.0
50
1
06&VIA 1230 0600142031 7440-47 3
Ceb.h
TAJ rDrL
100
50
1
06M3114 12 30 0&WI420:31 7440a6J
Golyrr
NO I1y4
10.9
1.0
1
haeaV 14 12:10 O&V4114 20.31 7440-% 4
Lead
NO MAIL
10.0
5.8
1
06.'03114 12.30 0&W1420.31 7430.02.1
Nfckel
NO uo4
50.0
5.0
1
0"W14 12 30 061041142031 744042-0
S.f.wm
RD ug)l
IOU
$00
1
DMWI412'31) OSOU14 W 31 776749-2
51Ner,
NO +,giL
10.0
5.0
1
06431114 12.30 00,04114 20:31 7440-22-4
Thauk+m
NO u01L
5.5
5A
1
MU14 12-30 0604114 2011 7440.26A
Anedrlm
NO ug&
25.0
1.0
1
061O31I4 12:30 L61W11420)1 7440-V 2
2Mc
NO UWL
to.0
ID0
1
OW30141230 0N0411420. 31 744066-0
0300 41SV Law Loral Lardfid
AMNyt"l Me9,od. EPA $260
Acefane
NO flgii
Igo
10.0
1
05/31114 05.33 044-1
Acryldnilnl.
HD ug1L
200
1.9
1
05131r1405:13 107.13•t
0-1...
NO uO+L
1.0
0.26
1
0513t114 05:31 71.43.2
BfvmocM.Nvm.a,flne
NO uyi
3.0
oil
1
ow$11405:73 14.07-5
&.mapchivr nnlekfAnr
NO WW1
1.0
0.16
1
W31114as: 33 75-274
&vmOlvm,
ND rUgL
3.0
029
1
05f311140533 75•15-2
&vmemetlf.nn
NO yyL
19.0
020
1
MV 140573 74434
2.ovt n ,. 1MEK7
ND ng+L
500
0.96
1
mill 7&93-3
Cafbve deufld!
NO uLVL
100
12
1
M111405.33 75A1 -C
C+frhon Ierrachk1100
NO 10&
1.0
O25
1
OW3111405,31 5&23-5
Cnlorohunnn.
024J uyi
3.9
0.23
1
Mill 495:33 1W907
ChImeolhane
ND riyL
10.0
0.54
1
Od13111405:33 76-00-3
Chlelokrnn
NO vg+L
SO
014
1
051311140513 0760.3
C41O."mane
ND u04.
1.0
Oil
1
MU1405'33 74-47-3
1,2.01ilromv3•dlkKvpropene
NO vtPl
12.0
25
1
o513111405: 13 9&126
Dibrom chl-limeAlar,a
ND OyL
3.0
0.21
1
o5r311140613 12446t
121D&b ethane(EDRI
NO-G&
t.0
0.27
1
Mill 405:31 100-934
0161e1rw.WpN a
NO ,g&
10.0
0.21
1
OSr3111406:1) 7495-3
T3 prMvr,s..faene
ND uqk
5.0
030
1
0&3111K 0533 96.50L1
t,4-DkManI. ..e
9-51J ug1L
1.0
033
1
0517171405:33 I05.48.7
1ars-f,4-d,Nmn-2-0xN..
NO ugfL
too
1.0
1
Odl3111405'33 110-576
1.1 Okhlaonl,ene
441 ug1L
5.0
0.32
1
M111405.13 M34.3
12-D1,014mnelli.n.
CAI`J ugrL
1.0
0.12
1
05/311140 15 107.0&2
I,1-DtNW.v lh.na
ND W1L
5.0
OS9
1
0513T11405: 33 M35J
da-1,z-DklJvfneO,me
tA3ua
5.0
0.19
1
0513511405'33 IW0.2
Ita1n•I2-Dlefomv.rhen.
NO itrj&
5o
0.49
1
o513t1140531 15640-5
12-DthlPrgKnp.ne
ND ug7L
1.0
0.21
1
0513111405:33 7647.5
I,3-Dtf9d vmavann
ND uo1L
1.0
0.29
1
051311140511 142-26.9
cle• 1.3-Dwhkl eProp ene
NO mok
1.0
0.13
1
05MI11406:33 1ON 141.5
REPORT Of
LABORATORY
ANALYSIS
twe naeK na m5 a apleo.e.e. ..r:.rR�
eM
tMb: 00f Ino 14 0620 AM
-Halt the -ft.
cen...4 m PK. An.akoM seryA. im Po a 20 a173
aceRnaly#rcal'
ANALYMAL RESULTS
Pee. Anrlyvuf 4..11p.- Me.
ven)..r.r.r.. Sar *47
n.nrr.�ne. HC 71V76
17W16I5 g0'F
Prnleel Sung Cieeed•MI kry 1VCl
Pace Pfeled NO : OM3127
Sample: MW13
Lab10: 92203121012
C94ded CWW1411.00
Rewired. 05129114 f5.20 Mow V61er
Repmi
Paremeren
Rerun. OWN
u"A
AIDL
OF
Prepeed Anmlymd CAS No O,lal
1IM M 9V Law Level Landfill
mWicalmolhod EPAa260
hem 1.3 OlddmePrvpene
NO uglL
1.D
0.26
f
OS1N11405:33 10061.02-li
£lnylf.nean.
NO tmA
1 0
0.34
1
OW1114 05:13 10041-4
2.fte..nnne
ND W&
50.0
0.45
1
OW2111403:33 591.16.0
Inaomen.n.
NO u6R
10.D
9.32
1
0513144 n:33 74-N-4
mmt. n. Cmplde
Nil vyA
1 0
0 R7
1
mil 14 a 11 71 02.2
4-Afe6fN.2�engnr.,e(MfBK)
NO 4&
100
0.33
1
9512111405:33 1O&1&1
Syrone
NO LID&
1.0
0.26
1
0513115405:33 IM42-5
1, 1, 1.2-7ee.ditm eyn.
NO Ll,&
5.0
033
1
GY3111405:33 630-20-6
1, 1,2,2• Tex. efODwa6fane
NO ,giL
3.0
0-40
1
ON311140533 79-344
Tehed,loroerhene
NO rg1L
10
0.46
1
05/31114 0541 127-18-4
7ekrene
NO up1L
10
0.20
1
a513171a 05,31 105.00.3
0.1-Tetchl."Ihorc
NO ug&
1.0
946
1
05*111405:33 2165-6
1.1,RTHcAlaro4rt�ank
NO ,g&
1.0
029
1
051111f40533 70-011-3
Trkrilwee0lene
1.2 upfL
t 0
0.47
1
QWII14 05:33 7401-0
hicnwrOAuomnfe0l.n.
NO Pg1L
10
0.20
1
0$131154 05:33 n4W4
12.3•TNonlvr.pOpAne
NO u%'L_
10
0.41
1
*w3I71405:13 96-16-4
Veh4 ecelale
NO .y1L
50.0
0.35
1
OS VI4 05:11 10&054
Ylnyl cfio.kle
NO ug1L
10
002
1
OW2111405'33 76-01-4
X"k Ta1a9
NO 11111L
50
066
1
051311140511 f130-20-7
Sw.ropa u
4-&vmvluwv0enime 15}
100 %
70-130
1
Mill 4 05:33 460-00-4
1-2-DIcPwwwlhona d4 (Sd
90 %
10.130
1
MV14 ft 31 IVII0-07-0
ieluene.d6 M)
,00%.
70-m
1
061311IA 0533 2037.26.5
REPORT OF LABORATORY ANALYSIS
rr+. •.con r..r nalrr �.w.�.d...ape h kN.
O.fe DR IW2014 06:20 AM +Ire•�f .. rn ia.n rw..rK PI P.pr A.ri,roM 6e.rrd. fM1�
Pepe 10 of 73

PaceAnaoical�
..nrA..r.a.mr.
ANALYTICAL RESULTS
P.O. A.00"t Nnl41e, f.
9800 K. ' Aw 5 1LO
rlud.r.e... NC 2WIa
1041975-ems
Prgeol BNrry Clue a-MI-Alr9 MC}
Pow PI9Jn6A No.: 62203/21
umpl.: M171F17
L6093: 12203121013
C011aWM. 05f2001415: 10 fedMed. 05729f141520 Matra V*14r
Report
Perundwe
RVILM LkAN
Lrw
MOL
OF
Ph.pMed Melyr4d CAS No. Cluel
6410 ICP 0r sdwller
A* -"*I Mai nod: EFA 6010 Plepe aim Medved; EPA 3010
Mim00y
5.6J ugoL
$.0
! 0
1
OMNI4 12:30 06ROVI4 20'34 7440.3&0
n.ewc
NO ug4-
10.0
50
1
Oft-111412-30 OMM42034 7440-36.2
Bwrum
67.5J uovt
100
5.0
1
0MV14 12-30 0OF04114 20:34 7440.39.1
B.ryp.hn,
ND up,t
1.0
It
1
0MV1412:30 OGM41I420:34 7440i1.7
Ca&Nr
NO ugA-
1.0
1.0
l
0610311412: 30 Od041420:74 744043.0
Chromum
NO ugfL
10.0
6.0
1
06M31412.30 WOW 1420:34 744047.3
CcE.1l
44.3 ugrL
100
50
1
09103f1412:30 0611TV 14 20 34 7440464
cupper
NO uA
IOO
50
1
06103f1412: 30 06RW1420:34 74e0-M-0
L.ed
NO ulpL
50.0
50
1
06f0M412.30 ON0d1420-34 747MA92.1
Nickel
e.1J ulvL
50.0
5.0
1
O6f0311412:30 06NV142034 74404n-G
Sel.rYum
NO ogre
10.0
10.0
1
DMU1412.30 M041T420.34 770249.2
Serer
NO ugA
100
s.4
1
06f0311412'30 O&OV 1420'34 7440.22-4
TMIMrm
NO �wL
6.5
5.4
1
0610N5412:30 06*01420:34 7440-26-0
V.n.dlum
NO ugi
25.0
5.8
1
OMMA 1210 06NV14 20:34 7440-52-2
Inc
NO .%
100
100
1
06A]1141rM OGAMIA 20:34 74404M-0
9260 M5V t.w L-M LendI01
Arh.11tcal Meowd: EPA6266
Aulwr.
NO umL
100
10.0
1
M 10 4 MA9 e7.64.1
AoWie.uip
NO hrgA_
200
19
1
0sn 111406:40 107-13.1
6.nnne
NO ugA
1 ❑
0.25
1
0541114 O4:49 71434
Oronwdrwome he
NO h.g1L
110
O 11
l
05MI14 05;49 74-97-5
&orP.dc W.im,l h.ne
NO awi
1 A
013
$
OW1114 05:49 M274
llt.-Crm
NO ug4-
3.0
026
1
05IJ1f14 iM 49 75.25.2
&0nwm.li.•.
NO u0&
$00
020
1
0&3111405J6 74.81.9
Z sulerhorhe (MEK)
NO gp&
100
0."
1
M311114 05 A9 74,93-3
C.Ibun dlwllld.
N0 UA
100
12
1
05f31114 051.0 MIS-0
0.14.I11.e. thixrde
NO ugi
10
0.25
1
MaV 1405,49 50.23.5
ChWro6......
027J aWL
1.0
0.21
1
051311IA as 49 106.00.7
Chluhdemaw
NO u6A.
100
0.54
1
05 WO 05:46 75A0-3
Chlomk4
NO ug&
sA
0.14
1
0673104 05:49 674B•3
d,wra .n.rh.
NO uV&
f u
4.11
1
067J1114 05:A9 111873
12-Oelr0ma-3KhlnrcPprupe0.
NO ugli
13A
2,6
1
05MIM 05'40 96,12-A
Orh.im.dd._.uwn.
NO uom-
3.0
0.21
1
Osr3111405'49 124-4bS
1,2-pbromoeesAne IEpO}
H13 uy
"1
0.27
I
0.5111114 0549 106-91i
DIGOm.m.lhen.
NO uo&
100
021
I
06r3111{05:49 74-95-3
12-OlddOrob.nawle
NO up4
5.0
A 30
1
aswI14 05'49 05-50-1
1A-Ok}hkroL.nr.n.
9.44J LWL
1.0
033
1
O5r3111405'4: 106-464
Verh4 I.A 016"a 2Palen.
NO VWL
1001.0
1
OSf3111405:4110-57-4
1,1-pcnlorONh.rre
NO upM-
6.0
0.32
1
OV311140s:49 75-34-3
1]-OKh1ar0.lhr
NO u%&
1.0
0.12
1
061311140549 107.OB•2
1.1-OkNot alhen.
NO IgfL
5.0
0.55
1
M111405AO 75.35.4
de 1.2 Dlcldaraaolare
O.65J 00fL
50
019
I
05 VIA 05 A6 IM-W2
Dena-i.2-OldeOrueererhe
NO ug4
6.0
049
1
06031/14 MAN 1%A6-5
1,2-0[NorOqupene
NO tr01L
10
027
1
OS M405.40 1947.5
1,3.Ownlarepop.n.
NOW&
1.0
9.26
1
OW111405AS t42.264
dr 1.]-0IWweprppene
NO LN&
10
0.13
1
ON311}405A9 10001-of-5
REPORT OF LABORATORY
ANALYSIS
rr.. rapwl
ihY rpl D• npr.duwtl..rc.p n M
Oe1. O61I Z7014 06:20 AM
,ae.m .w ..Arncw.i.n1 er
P_ A dv_ li,i Yc Pop 31 or 73
�" PaceA 4lical
...yPrlr w.
ANALYTICAL RESULTS
Pau AnYytl[elMwleM. Ma.
4tl00 Kr Fa sur lop
M~W-0.. Nc 70075
11w1l7&Moil
Phele.I SNrry Cldeed-Ml Airy IVI C)
Paco F *d No . 02201121
9unpl.: MW-17
Lab 10: 1U031;1013
(;a",d 0`.r VIA
IS 10
Re Fvvd: 0529114 15;0 Man,. Nele+
R.p.d
Parameters
Reih/l6 Li015
Lim
MOL
OF
Pre0w4d A.Oyr.d CAS No 0'.1
6260 May Low L.r.l t..Hill
M.Nl.cel Me9hod; EPA BIN
uene•s,3.Ow+Auop niene
NO up4
1 0
026
1
0513u1405'49 10%14)2.6
efttd r.rla
NO up4
10
0.10
1
OS13T1140549 100.41-4
2+lerenene
NO uLA,
50.0
0.46
1
05/31/14 OY 46 591-76-6
ludaln.th.rhe
NO uSo,
10.0
0.32
1
0513111405-49 7440-4
Mvllw nd Gaa W.
NO.0&
1A
0.97
1
0513111406Y1 115,09.2
CMeiVl 2-per,renooe JMISKI
NO ug4
100
0.33
1
M11140546 106-10•t
FAY—
NO u6+t
10
0_26
1
OW31114 HAD 10042-5
1, 1,1,2•TiPlwliNKpa*4 ne
NO up+t
5.0
033
1
OS13MA 05AS M-204
1.1,2,2-Te b. hlorod then.
NO upeL
3.0
11.40
1
M10 1405:49 7604-5
T.i.cbw_(han.
NO ugfL
1.0
0,46
1
W3111405:40 127-16•A
Toluene
NO ugfL
10
0.26
1
0513111405.49 1011-66 5
1,1.1 •Trlcnlnr0e9.an.
NO LWL
1.0
0.46
1
067311140549 71.554
1,1,2 TrtchloroeNen.
N13 ugAl
1.0
0.20
1
06f31)$4 05'46 79-00-5
Trkrhrw..thene
NO LWL
1.0
0.47
1
OSCIO140549 79.016
}rhprbeeumm�l.dh.n.
NO L19¢
1.0
0.20
1
95r3+1140540 7"0-4
1-7.3 irNy.IrrOp upw.n
NO 4WI
1.0
0.0
1
MIJ1405:49 %•16J
V"."law
NO upfL
50.0
0.35
1
Ml 01405-49 106-05-4
Vhyl cWwide
NO kg&
10
152
1
OU311:405A9 75-01-4
xvl.n. {Tully
NO ug!L
5.0
1.69
1
OSf311405411 1330-20-7
5.lregeNl
4-91vmO1.ryuuwerrn. [Sj
100 %
70-130
1
OY31114M 49 460-D"
I,2.OIMbroedvna•d+IS}
91 %
7D•s30
1
05f3111i 05.49 17060-07-0
iewene-d6(5)
104x
70.130
1
O5,1 40549 2037-26-5
REPORT OF LABORATORY ANALYSIS
iwarpa.r NY no16. nprotluc.d .xe.p[ n M.
O.I. 0611212014 08 20 AM ..nau1 Ni n..rrn cmr.nl W Pa AAdV" se�.P.., W
Pegs 32 0t 73

Pea. ■e.lylleelSYWe.f, In..
acekaiytiml "°°"" ` 7 Me
HunYl..ief HC 75975
.ww rrc+M.ru.•
Ilwb7sse92
ANALYTICAL RESULTS
Po).ot: Suay 019eed-Ml Ary(VIC)
P.c. Proleci No. 92203/21
64mp16- h1W-M Clio 10: W43VIO14 C06eded: O517711406:05 Recefyed 0512WI4 IS'20 Mmirit, Mm,
Repnd
Peremeters
R.aUu4 U.1%
Um0
MDL
OF
Pr.per.d Matyxed CAS No D115t
60t01CP a dw"
Andlytral Nt400d EPA 6010 Prepef40pn
MIWdd. E.RL3010
Anew,-v
NO up4.
60
50
1
0610311412.30 tl6,rIM/1420.37 744*1384
ov.."t
NO Lm;&
I.DIt
50
1
0"31141Z30 WW11420'37 7440-16-2
Bernrcn
23.43-Wi,
100
50
1
OOM311412:30 061040420:17 7440-30.3
BerylYrm
ND ulik
1.0
10
1
0610Y1412:30 ON0411420:37 744041.7
GedrNu-
NO un&
10
f.0
1
06r0311412'30 MWI420'37 7440.439
Chlomlum
W u0A
IDA
50
1
06MV1412:30 o61W11420:37 7440.47.1
Cuhm
14-2 u9+L
10.0
50
1
0610Y1412:30 061o411420:37 744"64
Copper
7.63 "A
to op
50
1
o"31141Z 10 OtM O1420:3i 7440-61114
Lead
NDUPA
10.0
5-0
1
OnW,412:30 061040420:31 7439-92.1
N1gP
NO UA
50.0
S0
1
0610311412:39 0610411120:37 144002-0
Se1.FWM
NO UWL
1D,0
10.0
1
OSMU14 f2.A0 ONW11420.37 T76249.2
Surer
NO vgA.
too
50
1
0610311412:30 96104r142037 1440424
ThalLum
ND .4A
5.5
5A
t
0WOY14 12 $0 06104114 20:37 7440.26-0
Ven.uUm
NO UWL
25.0
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1
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A-
ND -ok
I D.0
100
1
OSM3114 12:30 0& W114 20:37 744066-0
AM M5V Lew t.rd L. ,IFHI
Wryyr-1 whod EQAlino
Acelane
ND aryl
to
100
1
0$03104063S 674M1
Acuylerwuda
NO owl
20
Is
t
05OV14 06:35 107.13-1
ek-y"e
NO 40 A.
1 0
025
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OW111t1 05:35 71-43-2
Drompchlorom th-
NO ugA
30
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t
M111406:35 74.97.5
tkomodrclrwrameOlane
ND uQ&
4.0
0.14
1
0573111406:35 15-274
6lcmelerm
NO ugk
1.0
0-26
1
OA73111406:35 75-26-2
flw-lhene
NO uyt
1 o 0
0.29
1
OW31114 06:35 74-63-9
2•aalenmv WSKy
ND UWL
100
9.96
1
0sm 10406:35 76-93-3
Cnhwr dl. Akde
NA u04
100
1.2
1
M1114 06:15 75.16A
C.ebun lom aphlrxllN
NO ug&
1.0
0.25
1
0513111406:35 S6-23-5
Chlomhenren.
NO uDL
SA
023
1
OU3111106:35 106.90.7
Chimsuhane
NO ug4_
fan
054
1
OCJ 0406:35 754103
chi-ro
ND UOL
5.D
0.14
1
M111405:35 6736.3
Ch m"th4ne
NO uyA
1.0
O.V
1
Owl 11400:35 74-07.3
I]-Daomrr3•drWrepop.ne
ND uyA
11.0
2.5
1
OW31Ill 06:36 *12.5
DrMemedlleremelhene
NO A
3.0
021
1
OW3111106,35 124-4 A.1
1,2-04. om0.1thme IEDBI
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10
027
1
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phromomelhene
NO Hyt
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1
OWW14 06:35 24 95 ]
1�-bkhloroheni.rre
Nb Wk
5.0
0.10
1
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1.4-dcHnoneer4n4
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0.13
1
OSf31Ito 00:35 106-46-7
hu 1.4 0104po-2-term.
40 upR
too
10
1
05131"a 06.35 ?10.576
11-0khlorM6rene
NO up11
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032
1
051111t406:35 75-114-5
1Z4IWA,tW0elhene
NO uyi
19
0.12
a
u&3111406'36 107-06-2
11 DKhrornethe„e
NO VA
50
0.56
M
0513111406.35 76-154
cis 1,7 Dkh19meme '
0.74J VgA
5.0
0 19
t
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1
06/31114 06:35 155.60-5
s3 Dkrtd rcvraperr.
NO uyl
1.0
027
1
OW IOil 00:35 76-07-6
1,3-pldilwonropene
NO uLA
1.0
0 26
1
OS131119 05'35 142.29.9
de-1.l-Fhnhlorrrlrcnoene
NO upii
1 0
a.11
1
05l7511405:35 10061-01.5
REPORT OF LABORATORY ANALYSIS
7r.f r.pw1 M.e eel pf nP^lductl..rgM n hFl
Dail! W1202014 0620 AM .r..n4 ew .mrYrc vrww.rcr.r Par:. A-'O ur 5. ". ire Page 33 of 13
PaccAnalVtical
ANALYTICAL RESULTS
Prhptt Sung Closed-MM-Airy lL[CI
Pece Relecl Me 92201121
he. MetylYN MNluf. Ine-
xmx.lwr lw. sw l00
.v.n.r:a. NC 2e075
f70f16754M
Semple: II100-20
Loh 10: 92203121014
Cotlect.d n527+14 06 05
R.cel-d 9517WI4 162 11 Mat- W.I.,
FIWO
ppemelere
Rmdta 010l
L-I
MOL
OF
Prepared AnWpW CAB N. QiW
6M M5V Lew L.r.l LeMIt11
Mely6ml Method. EPA MM
keno. 1,3-IXcnlwr v.pear
NO uQ&
r 0
0.26
1
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E9rylh4 -c
NO u00.
t 0
0.30
l
06r2H1406.35 100-41-4
2441mnme
NO ug4
50.0
D49
1
M11140935 11111-76-6
Worrie6llne
NO upR
100
032
1
0541101404-15, 74.4114
M.Wytee.[:hl-ch,
NO Ny.L
10
097
1
OW Wl605-3S M09-2
4-M69ry1-2-p.nt.non. (6OBK)
NO ug4
100
033
1
a"V14 o6-35 t0610.1
$7Frene
NO uyt
1 0
0.25
1
Ow 111406.15 10042-A
1,1,1,2-Tetrachlnoelhene
NO ul)k
$0
0,33
1
050"11400: 35 630-me
1,7.2.2-TetrechloroeFene
NO ugfL
30
0.40
T
06r3171401A:35 743A-6
Tetl.chl-1hene
NO ugA
10
0.46
1
o571r14 O6:M 127.18.4
Tm"e
NO neat
1.0
0.26
1
OS1311I4 05:35 10lF663
1,1,1-TdchlolveDr4rrc
ND ug-
10
0.411.
1
QU311140035 71-56-0
1,1,2-Tdehlf+rneer4ne
ND up11
1.0
❑29
1
65r111140535 7WW6
Tlkhlftoelh ne
ND uyR
1 0
0.47
1
06n$11406:35 79-05-6
Ttk l u9uero"Ilrehe
NO u¢4
1.0
0.20
1
owl IIA 06:3s 75-60-4
12,}Trfabrvprop.ne
NO ugA
1 0
0.41
1
05131 f1405-35 W154
YYlyfecetefe
NDvpL
$00
D.35
1
0501rid 00.35 105-054
mo eMvlde
ND u01l
10
062
1
OS T1140675 76-014
Xvime lTpleq
NO vA
$.0
0.66
1
Mill 06:15 1330.20.7
Surmp4fea
4 6remeluorepen7ene ($)
100 %
70,130
1
DWI 1]4 04:35 460-00.4
12 ➢kMoroclhene-04 (5)
99 %
70 130
1
05131114 06:36 17066-01-0
Tcluane-de 161
99 %
70-130
1
0573111.10615 2037.26-6
De10 ovi 220140920 AM
REPORT OF LABORATORY ANALYSIS
T*ef rbpeH N.1 �.1 ha ^rprod.eec..rap! n M.
wumn.a..r.r.. ev,..,r el rea ArriyYw s..r.y. �
Ply. 34 u1 71

v.r:, Ar.ryve.l a.nrnl,lrK-
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W�r�. NC 2W71
110410lb om
ANALYTICAL. RESULTS
13,00,4: artyvr.a F1W Awry L&Ci
P.O. 11(go t1A5.: 92=121
Samp16: MY11.14 Loh 10: 11=2114019 rvhw.d 04121W1A 09:10 Recelred 0QW1415'20 Ma.lr Wel.r
P.r.me1er0
Rmat.
R.pon
lkvw L mll
MDL
OF
N.p.r.d Analy2ad CAS N. Qum
50101CP oft add al.t
An@" al Ma6w4 EPA 6010 Prepm loon Meows- EPA 3010
AnOmmq
16A ug7L
60
50
1
OWWA C1.30 0"116 20:0 7440-36 0
Asarr.c
NO uyL
ID.0
5.0
1
06MIT4 f230 06*W4 Zlt:AO 7440-3a-2
6.rNm
117 uWL
100
5.0
1
OWYf4 1230 66164114 20:A9 7440.M-3
Bv^m
NO uA
1 0
1.0
I
O&031141230 O&W l421)49 744DAI-I
c.dmwm
NO uA
1 0
1 Q
1
06MY14 tZ:30 QWU0IA 20'40 7440-4"
CNuma.m
a,24 uol,
10.0
50
1
OGMIVIA 1230 0610411420411 744047.2
Cobell
326 up4
10.0
50
1
OMY141230 060M1420:49 7440.494
Copper
NO u9&
to 0
5.0
1
05103114 12:30 OWN114 20:49 7440.504
Lead
NO u97L
109
60
1
01MV$4 IZ:30 Q W40420:49 743992-1
Wkel
laAJ u01L
500
5.0
1
ONOY141230 061WI420:49 7►4042-0
6aleryun,
NO u01L
100
100
1
D64311412:30 06A4114=A9 77U-04
9W.r
NO ug+L
10.0
60
1
061OU1412:90 060411420.49 7440.224
ThW*..
9.0 vp'L
5.5
5 4
1
o6N3114 1230 OW411420,49 7440.26-0
V.nrdlum
NO ug&
25.0
6.0
1
06103114 12:30 06101+1420A9 7440.62.2
ikw
13.6 uyL
100
1D0
t
061OW141130 Oar6U142049 74404641
0260 M6V Law Lw 4 L.ndh6
AdWytk.l M66wd.
EPA 0250
Aulane
No uA
10a
Ica
I
OW3101400-04 67-04.1
A.rrmminn
NO upt
200
1.4
1
M1014 00 W $07.13.4
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IjUA
t.0
4.26
1
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8rou16ct1womrrh.n.
NO ug&
3.0
0.17
1
Oey3111A 04:04 74-07.5
&olnoraclAprpm.ltlnu
NO uqA
1.0
0.16
1
OSP31FIA D6AA 7&27-4
&amnlwm
NO u9Al
30
026
1
0573111406:04 7625,2
&o.."cm le
NO 494
10.0
029
1
06✓31lta W04 74-83-9
2 Elu1anm6 IM£KI
NO 11D&
100
0.96
1
=1114 06:04 76-93-3
C4rbpn dl-Md.
NO ug4
100
12
1
Q5131114 06:04 Ml l5,Q
C.rbp trltradvpnde
NO uWL
1-0
0-24
1
05r3111406:04 56.2}S
Chktobr l.n.
6a uWL
3.0
0-23
1
O&71114 o8:04 106-o0.7
Chmto.nxle
NO up At
10.0
0.64
1
ea131114 06:04 7&00-3
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50
014
1
0573$11406W 6746-3
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NO .4
1.0
0I1
1
0613111406-04 7447-3
1,2-Ddr 3-.h1 wprnp.n.
NO uWL
130
Z3
1
(1w Ill 406.04 11&124
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3.0
021
1
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1,2-0R+romuelh.ne IEVe)
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1.0
0.27
1
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Dbtarwrrwdlcnr
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1,2-Olehlw.b.neene
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5.0
024
1
o6R111400W 541.73-1
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4.0
0.33
1
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par,.• 1,a.DIdH+.ra•2-burrn►
NO up&
100
1.0
1
oWlA4 06.04 11047-6
1,1-01c1ew-kh. a
2.81 ugoL
5.0
032
1
0wIR4 D0 qD4 75.34.3
1.2-01d+ao6nw
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1.0
012
1
mio$4061" 107-D&2
1,t.plcMprpeK,viy
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0573111400=04 15-35-4
d.-1,2-Dwhi.rwlh.nr
44.6 uWL
50
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1
05A1114 09:04 156.56.2
lr t -1,2 ON1Awoe e-6
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50
049
1
0&311ta 061.04 156.SO.6
t,2-Olphtwnp..pene
3,2 ugot
1 0
D.27
1
0573104 06704 7"7.5
T.34)phkuvpmprna
NO uWL
1.0
026
1
0N31114 O6:04 142,26.0
REPORT OF LABORATORY ANALYSIS
Ttw mftW.r not anpWuW_
r ptn
Mi
D.k: O&, z2oi4 06 20 AM
µ/yaw -.. ranenl of P"
Ar. rpr l 5.r.. r Pao. 35 of
�1 PaceMalytical'
ANALYTICAL RESULTS
P. An.ly114r a.nl.ee, Mc.
66001SrYwr Ar6 5- f W
Nurir.tvN Nu 7m1a
InRse�s9Le:
Pro)ml. 8uny Cloaad-IM. Wry ILXq
Papa Preleu No. 92203121
Samplw MV#14
LaE10: 92203121015
Cnn.d.d OS'28114 HAD
Re-,-dOS1791141520 Mate VWI.r
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pdamelem
Rouft Lh-b
Lrvyl
MOL
OF
plomoo An*ftd CAS No OWN
4240 A16V Low L6r6T L6 WVA
An"l-I Menwd EPA 6260
d.-1,3-Dld woptopw r
NO uglL
1.0
0-13
1
D5731714 65:04 10041-01-$
1,a-1,3-DKhklapr.prn►
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10
0.26
1
MI) 11f400.04 to061-0:-0
Eny4cn46nr
ND utjl
1.0
0.30
1
057J111406:04 101i41-4
2-Her.narH
NO U9L
50.0
0.45
1
e5731114 06:04 5" 7"
ludp nathanr
NO uWL
$0 0
0.37
1
IW3VIA 06:04 74-911-4
md6lplan. CNwlda
NO upA
I D
D.97
1
DN31114 09:04 ?"12
4 MstW,2-P.n4lnonv (MI&tj
NO uyL
100
0.33
1
OSr3u14 06'04 109-10-1
8lyrenr
NO 40'L
1.0
0.26
1
M1114 00.04 100.42-5
1,1, 1, 2-T►tr .PAw 1h.n.
NO LMJ&
5.9
0.E3
1
05131)1406:04 030.20-4
1,1.2-2•TA96dAw-M.rm
NO uW1.
3.0
0.40
1
054110406:04 79.34-6
Teb. h1.-1h n
NO uUA
t,0
0.46
1
0513t114 06.04 127-16i
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NO 4WL
1.0
Ole
t
OS13T114 06:04 100.04.3
I,I,1-Trlyrwpetn.ne
NO vat
1.9
0-4a
t
051MI1405:94 11.55-5
t,l,x-T1rJ,rwuenane
NO.Q4
1.0
o.29
1
0Sr3 V I-t 06.04 2Y00-5
TIICM.re.n.n.
9AYJ uOA
1.0
047
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0N3Ill A 00:04 7"l-a
Tneauro6uWe m.ne
NO mgA,
1.0
020
1
057311140504 75-694
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1-0
0 41
1
051311I4 06.04 96 l"
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NO u94
S00
035
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05731r14 06:04 1D6 05-4
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4.7-A
10
0.62
1
ON3NIA 05:04 75-01-4
xyl.na(Tow
ND uA
60
0.66
1
0WIM406A4 1330.20-7
Swrvpala.
a -&Om L6 .hen2ene l67
too 51,
M130
T
06A Ill 406.04 460-00-4
1,2-DW Wm"Lhmn.-4 (S)
97 'A
74-130
1
0&311I4 05.04 17060-0710
Tokmw&Lde S8)
1001E
70-130
1
OU3111A 000A Z037-29-S
4SWCNE Cyanic, Tout
Anal hml Mm" SM AWO-CWE
cy.Ndr
HA VA
to-0
54
1
06109/14 1116 57.12.5
REPORT OF LABORATORY ANALYSIS
I" r.pm r.l nol anpreeu .0 Dt n.a,
O.R. O61, 2YA914 06:20AM _, e.-Nn ­1 pl P.pr Ar Jy�W 5.mn., 1-
P49e 14 or 70

p494 Anmg1k4 Ymk--. eli,
aceAoalyfical' �p1{om-6e c28"
1ye.rrerd4. r+e 25076
"�prs`••"" r1M167vmO
ANALYTICAL RESULTS
F4*41 91nry Cp.ed•#11. AIry 11ACi
Pen Rom No- 0=312,
ErryW: My1F22 Lab ID! OZN3121016 CWIecMd- OWV1414.35 Rewyod. 6WMI41520 Mabot Y61hr
Ft.p.d
P.nrueler. Reeu14 LkNt Urns WL OF Prepe.d Ar pWmd C" N. qu.1
6O 10 ICP 0roundwNn
A..lylrcel Melhod: EPA 5050 Pr"milm MMhed• EPA 3010
An9mmy
ND uo4
6.0
5.0
1
M3114 12 30 06104114 2943 7440-36-Q
A-ft.
ND ugl-
100
5.4
1
Q"RI41230 06MV 420:63 7440-35-2
swum,
662J ,ppL
100
5.6
1
061030141230 061041142053 7440.39-3
fl-vollm
NO upA
1.0
10
1
06*30141210 05104142013 744041-7
tedm:um
ND uo4.
10
1 O
1
QKWJA 12.30 Dmwt4 20:53 1440-4 4
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NO u04
IOQ
$.4
1
0614301412:34 ONW1420S) 74/047.3
Cuaall
0-1 uu4
106
50
1
0MV141230 OWW1142Q 53 7460-04
Cepper
ND �g11
100
5.0
1
OW"14 t210 0610411420:53 7440-W4
Lead
NO uoA
10.0
5.6
1
06A337F1 12:30 OEM?% 20.53 7439.82.1
141!..1
NO pL
$00
5.0
1
mu, 061040420:53 T440.(12-0
9eler4um
NO ugk
10.0
$00
1
06003+14 t230 PWO4014 20:53 779240 a
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NO ,rµ4
100
$.9
1
M3014 12:" 05104046 20:53 7440-724
Th.leum
NO ug.k
5.6
5.4
1
MM1014 t2:1O 06M4114 20:51 7440.26-0
Venrldlum
NO nA
M 11
5.0
1
00/03114 1230 06+04114 20:53 7440.62.2
Zlnc
NO upA
100
too
I
GOMM U00 OOMM 20'S3 7440-65-4
4260 A13V Low Lerel LmWllll
Ae.tyl6cel MAOrnd FPA 5260
Acelme
NO uyL
10o
10.0
1
OW3 N14 06:51 674 -1
Aaylumlrlk
ND U A
200
1 9
1
O'W51r1406:51 t07.13.1
Benzene
0.42.1 11QlL
1.0
0.25
1
0513111405:51 71 43.2
&eN,Oq+lmnm.ln.ne
NO Iqk
3.0
(117
1
(1"1 r140651 74-27-
grnmedlwvrumeNem,
NO oA
1 Q
4 111
1
0513111408.51 M274
Slnmolorm
NO IrgA
30
026
1
0513111405:5t 75-25-2
&nrrinmethene
NO ugrL
tQ.O
"o
I
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2-Sld..,one(MEIS)
NO upA
100
0-96
1
owl" 40615t 78.93.3
r:vbl 4kObd-
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100
f2
1
p57311140631 75-15-0
Serbon(ebadlre 'do
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T.0
025
1
OE731r14%.$1 W2,M
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0.671 gJL
34
023
1
05r31n406.51 1011,M7
cN.0e51ene
NO uoA
t0.0
0.54
f
45r31r1406:51 75-00.3
CMzlo-
NO "A
5.0
0.14
f
Q513111400: Sl 6710-3
CMorert IhT
NO "9&
1.0
0.10
1
Mill 405:51 7437-3
"h 1,2.O.-3-C1NeluWvp4r+4
NO up)L
13.0
2.3
1
05all 14 06,51 W124
Dtlxa chlnremebli-
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30
021
1
051311144631 12446.1
12-13k o.lh.ne (EDS)
NO uIpL
10
027
1
05/31/14 06 51 105-93.4
Dbmearoerhrx+e
ND rlQ&
100
0.21
1
OVIII14 05 S1 14-95-3
1.2-OkNoroeanxene
4.36J ugrt
50
1130
1
0513U 14 0E-51 95.50• I
1,4-Olcr,lmab.nsnns
2A vA
1.0
0.33
1
1110211141041 101411-7
k--1,4-0 iYmn-2Tlukne
ND �411L
100
1.0
1
0503",40631 I10-574
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1.4J OL
5.0
0.32
1
O5f31114 06:51 71.34-3
124NChlaroelhrl
0.611 uoA
10
0.12
1
05R1114 06:31 107-0&2
1.1-ENCI."oelhene
NO Wit
5-0
ON
1
OU31114 W 51 75.35.4
,115-01ch1daemene
3.21 YyL
5.0
016
1
ON3111400.51 IN-5942
Ier+e-12-PC4o•oe0lene
NO upA
50
049
1
o67J111406:31 ISS-60-5
1oro ,7-OkWpnp-
NO uglL
1.0
027
1
ON3115400:51 7847.5
1,3•DlcNmwopene
No 'lux
I.0
0-25
1
Owl 11406:51 14241-6
ch• 1,3•Dlcwwppl Ppene
NO OWL
1.4
0-13
1
OW73101406:61 f006141.6
REPORT OF LABORATORY ANALYSIS
Tlrr epos V.r. rur M npi.pt.e....pl
n W.
O.m.OW127201A95:26AfA
G.rvweln Pop 37of73
-�a�eAnalytrcal'
ANALYTICAL RESULTS
n.lyllerr r-. e.nrr.a yr . a.y.q ...:.r J,.. 9vr.+00
w.1....+, HE more
Ptol.d. t wty Closed -MI Airy Nlc1
Pace k*d No. 02703121
Semple; MYV-U
Lb tD! 63263121016
Colk.W1 0S7511414.35
Recessed OSRW141520 461tIe Vd11..
Report
Peremeten
R... IN L1.k
Lml
MOL
OF
Prepared An.ly2ed CAS Ok 41M
9260 MSV Low Level L4. WM
A..W-I IA.thorl EPA 11200
1.- l 3tWdtmprep4rw
NO ugk
1.4
026
1
OSf311t406.51 ION10I4
E6rylbnnxerr4
NO uWt
10
030
1
05#310140651 100,414
2 aleaenerrc
NO upL
50.0
0 48
I
OU31014 CA $1 "1.?"
406cme5lrne
NO ug&
100
032
t
4513111A 0611 74454
M4drylene CNdide
NO upL
10
497
I
OWIr1A 06.51 75-08.2
4-Melnyl-2 P4ntmndne(MION
NO VOA
100
0.33
1
ON311110551 106.10.1
Styr m.
ND uo4-
1➢
026
1
OSWA4 OS'SI 10042-5
1,1,1,2-ryh.o14dr0eryene
ND up1L
5.0
0]0
f
OSM10400:51 63420-8
1.1,2.2-Telmchler pe6rerle
ND uWL
31D
0.40
I
0513111405:51 79,14.6
7e6ed4aoe6+err
ND uo+L
10
046
I
05131114061f 127.18.4
Tc4tene
NO uyi
110
0.26
I
051)1I140:5f 108•e8-3
0,1•Tflfto oelhen.
NO uok
1.9
0.411
1
OW31 r1At 05.51 71-554
I,#.2•T11d+lnenetn4nn
ND uQIL
1.0
0.29
1
0W3111405,51 79-Do-6
Trmh4uroelh-
NO ug1-
1.0
047
1
Mi1140651 TO 014
Trk"uro6um0rrxmhne
ND .4A
to
020
1
Owl;,A 0611 7549.4
12,17d Q4unprop.n.
NO uQ&
1.0
0.41
1
mill 1.0621 M-16-4
VANyl ecet.le
NO VOA
50.0
0.35
1
0513NIA 06:51 108-05-4
Vinyl Chlerye
NO uoR
10
552
1
V,13 1114 W 61 75-Q14
X0-ITOM)
NO rp11
5.0
OAS
1
05f311140511 1330.207
Sumooaru
4 &9moWwebenrene (S)
K %
70.130
I
osmll4Q6:51 464.004
1.2-RMMornctl+.ne d4151
97 %
71L130
1
OS031 fl105 a 17060.07.0
Tvwene d5(6)
100 %
70.130
1
ON1111-109$1 7037-26-5
4 Hoc NE CyenWil, Tufal
Anlly1"i N1 erred. sm 4500 CN-E
C7.mde
ND ngk
10.0
50
1
OSM14 Wit 51.12.5
REPORT OF LABORATORY ANALYSIS
T1rr r.pprr Nel rot d •epnGicrd. e.Wq.+h/
O.le OW 17M $104 70 AM .alnwl xr w4Y•. cw,len el P.ee M.'rt++ 9eww.. Ir.r p.Oe 36 of 73

ZaAmlytical'
ANALYTICAL RESULTS
Aeu An.lyoeal L.rrlue, hre.
9euo per Aw sw f o0
IinYrwoA NC 2a01fl
170416T5llL62
Prekel Sarre Glneed-ML Airy ILXCI
Pate Project No.: 922MI21
Sample: MNF1F
Lab 10: 12201171017
Cokctad05♦2711415A0
Re—ved: 05*90141570 Mom VVmrf
Report
Puemelore
R4eWt4 Lrele
Lle.t MDL DF
Pf.Pered Analya.d eAs Na. Qual
4600C NE C YMI", Tofal
Analylk.l M.Ihod: SM 4500•CN•E
1;re-J4
ND met
10.0 5 ❑ 1
OWW14 10:46 57.12.5
aceMalytica!'
+ pse. me
I
QUALITY CONTROL DATA
Plolecl: Sutty Clo.ed-MI. Wry rylCy
P.ce Pfopcl No : 92203t21
OC Belch: MERP6669 A—". Nlctlwd EPA 7470
4C Belch Method: EPA 7470 Amato. Dc—p".: 1470 Mercury
A..odeled Lab Saffpla. P2203121010
METHDU BLANK: 1212169
AeeodfHed Lab SA(Mka: 02203121010
Puemeur UARA
Metoury u1YL
MmIrm, VV&%?
81en1; Rap dmv
Resull LII111 "Zed DYel6ere
ND 020 OM31141636
Pw. A.Ard .l 6. 1—, lee.
WOO K—my A.. Su 100
r1,erM.H1e, Nc 7WIrs
Im4w64m
LABDRAYpRV CDHTROL SAAIPI.E- 1212170
Splk4 LCS LC6 76 R.c
Pard"t.n Wf6e Cane. Raadl V. Rao UrrAe QuaMerr
Mercury -WL 2.5 2.7 100 60420
MATRIX SPIKE i MATRIX SPIKE OLIPUCATE. 12112171 1212M72
MS MSO
022W12f010 Sp194 S4wke MS MSD MS MSD %R.. Mer
Pu Lff LIN6L Result Cone. Cont. RMA1 Revell SL PAC %Rec 0WE RPO RPO Dual
M.tcury u9& 0145 2.6 2.5 2.7 2.0 101 too 75.125 0 25
REPORT OF LABORATORY ANALYSIS REPORT OF LABORATORY ANALYSIS
I. r.pan rO ncl lr raprudw —pl - W TIV r.pnd ahal net d Npmaueed. •rupl o"
Dele: 0El t 2r2014 oa 20 AM ,n.ww ew eneen ea.rnt er Pw. Ararrbul S.— Inc Pape 39 of 73 Dole: ON127014 0620 AM wit—M. wn u for P.0 Artrec.l Ser s ft P.1)r 40 0 71

0,
1/-�aceAnalytical�
...1+.y.w•ctN,
QUALITY CONTROL DATA
Prge" S." Cln.edJM Airy jtoc]
Pecs Pmled No 92203121
CC SekhMPRPI15057 A.eryel. M.M.4 EPILSp10
OC Sakh K." EPA30}6 APeyw 0--www 5010 METMC Oro.Womte.
Aea0da14d Leh SSmpAe. 92Z0112}501,l2207 i;fO02, 9220512100], p22011Z10W
METHOD BLANK. 1206932
M69I3: VAWP
Aweemod Leh Semplee
M03121001. 92203121002. 92203121003. S2203121M
B1enk
Rep.,Ar9
Premele.
Ur.6e
Rnum
Limp Andymad Ow9Mm
Arr l""
uWL
NO
40 05130114 19 41
A.—
LVL
ND
100 o5rSo7141@41
9wrkim
4p•L
NO
100 05*UTA 19.41
BMymm.
irplL
ND
1 ❑ 05OW14 111 41
Cedrnlum
LVL
NO
10 O&wl41P.41
Chm-iun,
cigrL
ND
100 ONWI1419:41
Cn6.R
.,WL
NO
10.0 OSIW1419:41
CPPpof
UWL
NO
10.0 CEW141941
Lend
uWL
NO
10.0 S5p37Nte 19:41
Nk:kl1
up•L
NO
500 05*1VI41P 41
Seler.4cm
.WL
NO
$0.0 051SN1419:41
So—
UWL
ND
10.0 OW301141%41
Th.6xrm
uyl
ND
5.5 0573on41041
vo-49rn
up'L
NO
25.0 05=1419.4;
Zinc
up•L
NO
}00 051301141941
•444 A"my11.M $MVINE, W.
9e051ro.r An SWL.190
n wm.. NC 2lMB
LABORATORY CONTROL SAMPLE'
PMemeter
129SO33
Ilr.6k
Space
Cone
LCS
R4a.Nt
LCS
%Rec
%Rec
Llmee Oupolma
Apflmo y
upL
500
492
P9
80.125
Menu
uyL
Mm
467
9S
60-120
Elr m
IryL
500
443
97
80.120
B-Vm m
"WL
No
451
90
59.129
C4dr m
UWL
500
465
93
BO.120
ChrolrrNm
uyL
NO
455
93
90-120
Cu5i16
UWL
Soo
450
9e
60-1Z0
Copps.
up1L
500
485
93
WA20
La4d
iiWL
Soo
475
95
90.129
N-W
WL
590
40
9y
90.120
Selma,,
LVL
mm
480
46
60-120
Sayer
nyl
250
234
91
SO.120
Th.A..m
upiL
500
456
92
6a-120
V. dam
bp'L
500
457
91
60.12Q
Zuic
uprL
500
457
91
6d 120
e..0 r.---V..~—. m...+..i W.a... M.—wn-gi..ur.j.. �..... ww4.r.....w.i
REPORT OF LABORATORY ANALYSIS
P....Wrl Mie. rotN r.P o .d...wer+. No
D.1e' 06r 12R014 05 70 AM a.& —I Ny wn6.ncwre✓r. of P_"_ A,r'We 8. . 4c
-PaceArkWiCZ
QUALITY CONTROL DATA
Pea 4nety9.ei l.ry9e.. M.O.
9800 Nneey A.e S.ft td9
*w..e.re.N. HL 28078
1YO/y175.MA?
Propcl:
Pape Prej d N.
Burry CM-1, ll. AFy 1111CI
92203}21
MATRIX SPIKE 6
MATRIX SPIKE DUPLICATE
1209034
1209935
MS
MSD
92203116001
Spike
8*0
MS
A13.D
MS
MSD
%Rei
Me.
PMemete. LN4M
R&Kil
Cent.
Cone
Rew.11
ReeWl
K Rec
%Rec
Urine
RP0
flPD Gum
Anemany
upil
NO
500
500
607
909
161
102
75125
0
25
Amwc
UA
NO
509
509
480
405
95
97
75125
1
25
Barium
UOIL
61,f
Soo
Soo
494
ml
9e
99
75.125
I
25
BeryMum
uA
ND
500
500
461
400
92
94
T5-125
2
25
C.dmhcm
.ipq
ND
500
SO9
477
484
95
95
75125
1
25
LxPPmium
upfL
ND
500
Soo
472
484
94
97
75-125
2
26
robes
ud4-
ND
600
500
Oat
490
se
98
71}126
2
25
r Mg.
uWL
ND
500
500
476
486
Y6
97
7S 425
1
26
Le.d
-@A
ND
598
SW
475
485
95
P7
75 }Z5
2
26
Nickel
upA
ND
500
500
467
475
93
P5
75-125
2
25
S.1"mam
upli
ND
500
mm
467
493
97
29
75-125
1
26
54ve.
up4
ND
250
250
238
241
95
96
75.125
1
26
Th.Ikum
ugk
NO
500
go
40
472
93
W
M125
2
25
Venedium
upiL
ND
599
SOo
4e7
476
9309
76-125
2
25
DI,c
vWt
NO
500
500
460
471
p2
P4
75-1Z5
Z
26
—a...e..re.M.e.9.......Mn. ♦wicaw4.r---.- e.a.ee..e......—wwm.r—r.... -w... ,4. er..—,
REPORT OF LABORATORY ANALYSIS
rn. r.rerr .n...yc b• r.p,xu..d. ..owc � r.n
P4ge ii .173 Dale WI N2014 DS 20 AM
Pepe 42 DL 73

Paml AAA"M #W*a4, law.
�# WOO I[Lruvp Wa 5.0 TOO
F.INPf1.4N. Nc 2M76
•wit-0amn 17011d"'ON2
QUALITY CONTROL DATA
ProJnp: Svry Cloa< "A. Aky ILNC1
Pace Proppl Th,; 922MI21
AC Boom MPRPl18107 mall Mom" EPA6010
OC a&%h m.dwd: EM3010 Am"m DowIpa n SDI MET NC O4wndwmlw
A~aocld[ad LdS Samples: 92201121005, 92203121006, 9220312t007, 922031210D6, 92203721009, 9220312S01D, 922D1121011,
92203121012,922011210 T], 92203121 D14,92201121015,9220312105E
METHOD9LANK: 12tx519
Makl.. omial
Aaaou4led LW SamPlva=
92203121005, 92203121006, 922O312SODT, 9220312100e, 92203125009, 92201121010, 92201121011,
92203T21612. 922011210T3,ffi2D7121014. 92203121015, 92203121018
BNM
Repw*Q
Par.maler
LkA.
11e.4
L" Ar. "d CNYMn
AnV--w
UA
NO
6.0 OW411419:26
A—Ne
ugrL
NO
10.0 OSM411410: 26
a--
uyL
PPD
100 06A411419:28
eovNl—
uyL
NO
1.0 0810411419:26
Cadmium
'Wl-
ND
1.D 0610411419:26
Ctvofrka.
US&
NO
T0.0 OWD4$1419.26
Co6.F
ugfL
ND
$0.0 OSMAA419:29
Copper
uyL
NO
10.0 0810411419: 28
Iron
uWL
ND
MO OSA4f4 IT28
LPad
u,WL
NO
f00 0804t1419-2L
f*K.1
4WL
ND
50.0 05A II4 1$ 28
5.1enlum
uyL
NO
10.0 06A4l1419.28
SFvef
UWL
NO
10.0 06mm 1419.28
Thalli.al
uWL
ND
5.5 DBr041I41924
VeneWum
uyL
NO
2S.0 081D40141%28
Zinc
uWL
NO
10.0 D6764114 W.78
LABORATORY CONTROL SAMPLE:
Pdr4ma9.r
1212520
Lku%
Spa
Cone,
LCS
R-Wl
LCS
%Rn
% Rea
Llmlq Olumu—
An9momy
ugfL
600
40
09
60-120
Ami9c
uWL
500
477
95
60.120
e.rwrn
1WL
SOD
SOR
100
a0-120
U-Vy m
uprL
500
470
96
50.120
Cadml.m
UWL
S00
460
96
60.120
CNorNum
QWL
500
466
97
50.120
Coha6
upR
500
495
ilia
50.120
Copper
uyL
5DO
494
ilia
80-120
14W1
UWL
5000
4706
94
80.120
Lead
-WL
500
497
99
64-120
Nlcke1
uWL
500
47d
96
60-120
Sale w-
uorL
Soo
495
99
90-120
99pe1
uWL
250
242
97
60.120
7h.Hmm
0gR
500
4"
94
win
V.nadlum
awl.
506
46O
96
90.120
Znc
ugrL
50D
47a
16
60.12D
FuWW w.a—on—pp—.----".,.-umu.-cd,r.....p[--r__— wa. W—d r rnp.[of n...uae
REPORT OF LABORATORY ANALYSIS
iryafPpvn aFN np14a f.p�.tl, aeryPyrn Na
Oct mwi 712014 Oe 20 AM rwwW wnwn eemanl of Paw N Npul S.N— I-
;aceRnalyircal�
QUALITY CONTROL DATA
PaN AF4ryaul4larvlPH. Me.
99d9 wrrr w. sWt. lov
nunb,mN. NC 7M1n
ITDuevs-0o97
Pto'cl:
Pace PNrjecl NO.:
Sorry 094e1-Ml Airy WIC
JZMJ21
k1ATR t% SPIKE i MATRIX SPWE DUPLICATE-
1212521
1212522
MS
MSD
92203332N1
Spoke
Splka
MS
M3O
MS
MSO
%Rec
MIX
Par4mo,w QlAA
Result
Code
cant
Rmh
Rew1t
%Fine
%Rec
Unto
RFD
RFD Dual
AnOmmy
upfl
ND
500
500
474
403
95
97
75A25
2
25
Araerk
'WL
NO
500
500
454
460
91
F
75-125
3
25
B4num
ugfL
22SJ
500
500
490
511
94
9d
75 ?5
4
25
Berylwm
uVL
NO
500
SDO
454
471
of
94
76.725
4
26
CadlnWm
uVL
NO
500
500
456
467
ill
of
75--125
2
25
Clvomlum
ugfL
ND
SOO
500
462
416
92
98
75-125
3
25
Cobol
4WL
ND
500
Soo
464
4e0
93
96
75.126
1
26
Copper
u0lL
ND
5D0
5w
475
460
95
96
75-125
1
25
Iron
-WL
17N
5000
50N
46M
ON
69
93
M125
4
25
Load
uWL
ND
600
SOB
46S
47a
93
9a
755-M
3
26
Nlckal
WWL
ND
SDO
5DO
453
467
91
93
75-125
3
25
SNanafal
uWL
NO
500
NO
457
4i9
93
Be
7&125
2
25
Slayer
4WL
NO
250
250
229
235
91
94
7 -125
1
25
Thallklm
u&'L
ND
SOD
SOO
446
452
69
92
75-125
3
25
Vanadium
WgL
NO
SW
500
457
472
91
94
TS-125
3
25
4Pc
WW%,
NO
500
500
457
467
91
63
75.127
2
25
F.a W[a w.wnud on N.. P.p. u.n nW Wnn. in,wua Ly l.. Nx[: etl�rn..c.y[ r,r4.n yrr�.0 ,,,.i W P�•a«W7 a o,..p,,,el in...�, i
REPORT OF LABORATORY ANALYSIS
iros-.md NN npt➢4 [Fpioquue. a.cPptn Fa.
P.g. 4 3 of 71 Dale 6$1 Q'2014 08 20 AMwe,w1]n. wn1Yn ean.anl e}P4u Analpl:N 5anf.eP. ln<
Pay. 44 al 0

�'�P CeAnalyt�cal�
QUALITY CONTROL DATA
PrvJnct. Sorry Clo.ed MI Airy fIJICl
Pace Fe"d No 9220312t
GC Bald. MBVr2m995 Mey414 Me6md EPA 9760
OC Setch Wh9 d. EPA a21I0 Mays W9crofto. 6240 MSV Low Lmrel LW40N
A4ewmied Lab Ge"a: 92M 121001. 92M 121002, 92m3121003, 9MO3121004
METNOOBLAW 1209031 M9►tm V*Wr
Aaeodeted Lab So""s. 9220312i011l, 9220Sf 21002, 9220.1521003, 9I203121004
Pmmmelkt Luft Ilewu L.rr.l Aneyzed
1,t.1,2-Tetred+hroea.ene
uyL
ND
5.0 0512W14 t573
1.1,1•Trknlorn~6
opt
ND
10 05Q91t/ 15:03
1.1.22-Tuumd*anr9.mr..
uyL
ND
30 057Z9t1i 15.03
1, 1 ]-Ted+in.vethan.
OWL
ND
111 0112971 A f 1
1.I-OI Qwvethrle
uyL
ND
SA 9f1 05r241S.0]
1,1-0Ivwwo-trene
uyL
NO
5-0 05MM i5.OS
1$,3-Tlkt4wppvp4r.e
owl
NO
1 0 052W14 1, 03
1,2-Dbfo m3-chlmprnpme
uyL
NO
13.0 05r2W1415:08
I,I.Ort..vmvalhane IEDBI
uyL
ND
10 0Sr2W}4 15:03
1,2-dc+lblohenr9ne
uyL
NO
0
SO nR" 15:03
I �•ONd4a velmm�.
uyL
1413
1 a O&?V%4 is 03
t,2,DkhIwaptvpene
OWL
NO
10 05r2Wt4 ts.03
1.3•pu9aropropXne
I,yL
NO
1.O m1w 115'93
1,4-00dilo tlbefii.h.
OWL
NO
10 OW21F. 15:03
$Aulr.vne IMFA)
uyL
ND
100 06r2W14 16:03
x+le.mnpne
vwL
No
50.0 OWW1415.03
4 Metl+Yl-2-pemenenv (4MSK)
uyL
No
100 OSr4W1A 15'03
Acelvne
uyL
ND
100 4512W1416.01
Au ..mil
uyL
No
m0 0512W1415103
Bentevr
uyL
NO
10 OY2W141sea
erameehlaramelnene
OWL
ND
3.O 0502104 16:63
B, medlcf.Iwamelh".
uyl-
ND
1.0 owlwlil 15,03
Smmohmn
uorL
NO
ap 052W141503
B.omvm o-
OWL
ND
$0.0 O wil:15:67
Croon d'e�tmde
OWL
ND
100 05RW14 15R3
ceft telrenW.14.
uyL
NO
1.0 01*111$4 16:01
ClAaobeniene
uyL
NO
3.0 05 ." 15.03
CMwnen.ens
uyL
NO
ttl.a 65rWI415:03
CNv.olum
OWL
ND
5.0 05;2Wt41501
ClNvramelhene
ugfL
NO
1.O 05aW141503
u47,2-Gddnrwlhene
uyL
ND
5.0 o512W1415:05
plehlvrryvvpene
OWL
NO
1.0 95:2WI415.03
L791tnimcHwor h. 4ne
uyL
NO
3.0 Mon. 13A3
mmmemelhene
uVL
NO
100 062W14150
EN1ylb4nane
OWL
NO
1.0 05, W1416:03
todame a.mne
uyL
NO
10.0 0W2W141503
NL49Mene CNodde
uyL
NO
$4 05RW1A 15:0
$arena
uyL
ND
1.0 0"wlI 15:03
Temad+lwoem-
uyL
NO
1.0 OV2W141103
Tak.ene
uyL
NO
1.0 0 wl:15:03
tran-1 2 O1f0woem.ene
l.dL
NO
5.0 O5RW115.03
OON" m
Pear vv-1 memae• Inv.
Sew im.c.r n.e 5uw lao
r4.4en.ie NG 711tlie
Ir9.1e;59097
a...'r.. er...".v ea e..py......e. ,.w. ir'a...ear.'.-.w.-..�"e....'..n...,..r.'....n.nr...,'.n r m..gm.'ov....Ur
0 ce"Iyticalo
. plmd Ne
QUALITY CONTROL DATA
Prehce Burry Claied-MI Airy IVIC7
I3 c Project Nv-. 92200171
METHOD BLANK $209031 M.O. Vwter
Aa4adafed l-0 B4aple4: 92203 t 21 p61- 92205121002. 92m3121 W p. 922p3f 21004
0tenk Repvrllnq
parmmeler Vn9e Rewlt LltnK Anmyxed Ouam5er9
1,::1.3-T}chlprvpl-n4
uyL
NO
10 051=4 in
[revs l,44>C19rev-z-bwlme
OWL
NO
I
%00 45491l45: 03
rtchwroe9ene
uyL
ND
9 062WIa1S.a3
inO11n.94uppn.ekyne
ayL
NO
1 0 06ri9114 15 W
w'y7 e-W.
OWL
ND
$0.0 05r291t4 55 03
vmyl chledde
uyL
NO
..0 06r2W1415,07
1[YIetP lTetell
OWL
NO
50 0y29i1415�3
12-DidN..r0elt..v.�14 [31
%
92
70-t30 95R9114 !i•03
4 BrerneXuvro6.naene {Sl
K
96
7tl13tl 05029114 1503
Tog. dIl
%
97
10-130 052WI41510
n.a. A.wY.iw. e.rrwn. lne.
aaw.�.t 4'r. aua 100
HC 2WFN
I I W I! t'r9w
LABORATORY CONTROL SAMPLE
Prameler
120902
u"k,
Spike
1-1 c.
LCS
R."N
LCS
%Rem
% Rec
Lmrm Oum4Mn
l,taa-r9uadlaoelnen9
PyL
s0
s9e
101
70•t30
I,f,l-Tdd�kreelnene
uyL
5o
4111
96
70•t70
1,1�,2-T4hacNnrvethe0e
uyL
50
613
190
70.130
1,1,2-irltMorvtihr.e
UWL
50
50.6
$01
70.130
1,1-OkM.roell.mne
OWL
50
470
94
70•}30
1.4-0ivhlnrvelhene
uyL
50
47 0
94
FO-172
1 ,2,1TtldevrnPrvn n"e
I.yL
50
0.1
96
70-130
12•001,,"- uhlenprupene
9A
50
4a.2
96
mllm
I.2-0rxnmoethene tE OBf
llyl
50
49-t
9m
10-M
rz4ldae cbt "en.
uyL
5O
So
1L10
70•a30
1,2-DitWwo.1hXna
uyL
60
48 6
91
70.170
1,2. 01cillow 9pene
uyL
so
49.5
99
FD m
1,3-RGrlolupm01ne
OWL
51)
4q 9
100
7Q-120
1,4.p'rehlervbenaene
uyL
5v
49-1
9a
70.150
2-1301mr.vne NMEKI
OWL
100
67.73
66
70.145
2L,ee8nms
uyL
109
97,
q7
70. 144
A-laHnyF2•pvminonc Immm)
uyL
iw
91.73
92
10.40
Acnvne
up�L
im
9403
04
50.fFa
Afxyla+mne
IIyL
25O
2SF
95
7p-i4]
84nlene
uyL
s0
54.1
106
76.130
BrvmvcMwvmeth iu+e
..WL
60
190
96
70-130
Brnmvdlcmwvmaminlm
uprL
SO
ANTE
97
70.130
&omplvrm
uyL
50
4912
%
20-1]n
Brwnomelnena
uyL
50
3;7
54
54-%30
Cerben d'uW Pd.
uyL
50
49.93
100
F0.131
Cerbvn remechlw.d.
OWL
50
46.0
92
FO.132
el.lwv6enrene
uyL
70
47.4
95
TO.130
CmmGrff r"
uprL
50
421
65
64-t 34
CA.luelvrm
uyL
50
As 7
91
10-130
Cmnr.......e
uyL
''0
343
59
64-1 ]0
n..., .�e..•wmY... rnu..,. ,,.............,r...,
REPORT OF LABORATORY ANALYSIS REPORT OF LABORATORY ANALYSIS
t.w r.Pwl Wo -1 ee nPan e....F. n er. rn'. remd ... - k,e repro -d. e.apt n ru.
Dale WIV?014 09.20 AM ..e...r 0- e . c e..ant 0 Pau A-toLq s.v'c.. in< Pep! 45 of T3 bale: 0&t N201A 053O AM arm+v'4 e+e w.Rl.n ear+wrtel Pea meyeeeV Senlvem m't per 46 of 73

..P'ace�anarytr'cal'
• ..r1�.maN urr
❑UALtTY CONTROL DATA
P-pgt: Surry Cupaad-1011. AWY AACI
Pete P'." No.: MOZ121
P.- anery11u1 a"-.. Inc
9mp uwT M. Sal. Iau
Muri.wre RC M74
0041a7S.a090
I PaceRrt Vicaf'
I e...pnntlef wa
Pryecl: 5w1v Clowdfill !Dry MCI
Pace PFojW N9.: 02203121
OUALITY CONTROL DATA
PaN An.lynul m.rvic.1, krc,
Ba_G x.,�.F M. Surt. IfJC•
•h.•4•w.. nC 7YJ'+C
• i[V leis pf l:
LABORATORY CONTROL SAMPLE:
f2MU
QC batch A15V127034
Analyam Mamo0: EPA8260
Splk.
LCg
Lc-5
% R.c
DC Belch M.111od. EPA 5280
Analim DelCi44m. 12L0 MSV Love Level LmdAl
Pralnel.f
Holt
Cale
Re kt
%R.0
Lmft 12uauam
A4ao-wr t- h 5alnpme 112203121 ON, 9220312$006. 9=1 121007,92201121001, 92201121009, 92203121010. 922011210 I i.
de-1,2-olddorP.aiary
IWL
SO
45 0
95
70-131
92203121p12, 9220312tp13, 92203121014, 92203121pt5
d.- 1.3-0ItlAaoprvpnw
uyL
50
51 2
102
701a0
OOwemOcmm Pmmalrw
uyL
50
47 a
96
70-IV
MFTHOD KAMP( t210761
Maebl' VAIN
06mm owthanm
uyL
5a
47t
94
70-111
Amo .lad Lab S. nVM.: 922031pt005, 9220]121006, 92203121007, 92203521gpa•92203121009, 92203521010. 922p3}2f011,
Elhybsnsena
uplL
50
41.1
06
92203121612, 91203121017, 92205321014. 92F01121016
k.
uyL
log
23.1
27
49-110 LO
49-110
am* Rap"
C
M. alylan. cldPnd.
M.khVl
uyL
Do
l0
4a.t
96
e1-t30
P-nmer
Lhmn Kamm I" Andynd OUAIFAM
Stlaanc
uyL
50
522
104
Milo
1, 1, 1.2• Tm0acWwoalhmn.
uyL
NO 6-0 0W311140123
Teawaeoro.Cwpe
a04.
50
49.7
97
M130
1-I-Fchloro lh-
901L
NO I MV1401:23
Tuluam
uyL
50
497
90
70-110
1,1',2•T.t"ChPa ehme
VL
NO 3.0 QW11140123
Pafw 1.2 INEtwoomme
uWL
50
47.4
95
70.130
1,I,Z-Tdcht.-1hene
uyL
NO 1.0 M11140123
aan. 1.3-OlddoroprogvrFe
uyL
50
49.0
98
70-112
I,4-Dw-0e0+in.
Igo
NO SO OW3101401:21
Un-},4-nchwo-2•nulene
LOL
50
40.01
93
70441
1,14)ktA. th...
11yL
N13 5.0 05e01M aI:"
fildlk- mgl4
uyL
50
52.2
104
70-130
1,2,3-TncFMaopeop.n.
uyL
NO 1 0 OY IM 0123
TrkhmroAlxmmelhene
uyL
50
40.2
a0
67-133
l,i•OMu.Mv 3- Chtvmp, opn, m
UWL
ND 11-0 0§1111140123
SNIy1 .c.Mre
uyL
100
100
100
W157
1 J-Oft- wthane 1E69}
u901-
NO 10 0S IM4 0123
V-A chlgnd.
uyL
m
64.9
110
99 r3o
12-0I0Wxn owr ne
110'L
NO 5.0 05i31114 00.21
xymne lTamrl
uyL
It
147
9a
70410
9ipl
NO S 0 05ri 1114 0123
12-Ddi.-Mmne d4M
%
91
70-130
S,2till6Norpprowne
UWL
NO }0 W5f31f140121
48ram.wua ohen4ena(S)
X
97
70-130
f,3-0IcNadlaruerw
UWL
ND 5.0 0501040143
Toluene da Tel
%
100
70-120
1,3-0l.h9wvpr0p1ne
UA
NO FA OU311140113
1 A-Olcmameruerw
UWL
NO 1.a 01T311S40S:13
2-Bularwn. lMEKI
OWL
NO 100 MN1401:21
2 lla44nvrw
uWL
NO 500 0573111401.23
4-Methyl-2-pemm Nle (MIBKj
uyL
NO 100 05731114 0t 23
Acemne
upfL
NO 100 Mill
AcryluJtrM.
UWL
NO 200 05131114 01.23
Beni.ne
uyL
No 10 OSQU14 0123
&omocrllPromamene
uyL
NO 30 0U311140$23
Womveltnlvramelh4n.
uyL
NO 1.0 OFW31l140123
Biomoform
uyL
NO 30 0N3}11401,23
Bunn-th.ne
UWL
No 10.0 05ea 111401:23
Carbon dwl Ad.
u0R
NO 100 05031014 01 23
cerd9n Tea.Mhtwgae
UWL
NO 1.0 051311140123
Chf.o n -
owt-
NO 3.0 0501114 0123
Chtw"Ih.ne
uyL
RD 10.0 OU31114 01:23
CNor0.rn1
uyL
NO 5.0 owa IA40121
CTcw-mane
uyL
NO 1.0 Mal n40122
clm• 1.1-0Ichkroethme
UWL
NO 5.0 05131114 Ot:23
tic- I, 3 DI.M.vpropen.
oyL
NO 10 05R1(140t23
Ddw. mdddrl1p10lhwe
UWL
No 1-0 0WI114 01:23
p4lPmomelnule
uyL
NO I0-0 0573111401:23
Elhylneneene
OWL
NO tp 0513111401]3
Igdvmelh.n.
uyL
No 100 OSd317140123
M.vgAM4 CNaHde
UWL
NO 10 057111140123
Styrnle
uyL
NO 1A 051311140123
Teear:hloroelhane
u0K
NO 1.0 MV140123
HwwiV w.wnw en ex..eae rr.ti v�.n.r
i.gn.lwM w -ww."
rwe.m ea..l
rrwe .n •en W..n1M pnmwaN Y aln •w.L el Nrr r...n.
pxan r...r�r en wr.+P wr x. n. unnr innase e1 ar viw• �mn mxgpl.le.em 11rneM e.1111 ierw,.a m m. rynl ul la.,ewm.
REPORT OF LABORATORY
ANALYSIS
REPORT OF LABORATORY ANALYSIS
Try.- Nue Mt rFPm .-PtM4r
Tin 1.Wn 4n.1 not o. raama.:wt.--Pt.m
D41. OW N7014 Oa 20 AM
..e,out n. rni�w� wn...g al v- A.&)v 54mne,
P.R. 47 vl 71
pale ow Iwul4 Re 20 AM
.1M ,ew-ft. 1-*d or P.-M F, a 9.rvc4. lnc
Page 48 al 73

�P ceMalyheai
,..�yn..fr,...
QUALITY CONTROL DATA
Pau Anmlyuaal eerwaae, Ina.
9en5=M. sir.I00
r A4d.i nxl.- nc 2emm
c row167seo92
Ploje 1. Surr7 C1o9ed-M1. Alry IUICI
Pace Pre1e.4 N. 97E03121
METNQO BLANK1210751
M.bu VIMer
Amemamled Leb Smm lem 92203121005. 12205121006- 12203121007. 22203121009.
R2203121 M. 67183121010, 92203$21011,
VU03171012,92703121013, 92203121(1$ 4, 92203121015
B1.nk
A*P.,h g
par"etm
U-14
Re.11e
Unvm AAmly2ed O1u1N6e a
Toluene
uyL
N❑
1.0 0613111401:23
trend 1-2. O.dmnxne61er.4
ZL
NI)
50 ON310140123
bmm-t.3-L�clunnnrvpene
uyL
ND
1.0 m "1401-23
b I'm lkl: w_w hum-
UWL
ND
100 05a"140123
T11thW.neFwe
.014
NO
10 6NS1114d1;23
Tr4CWWuU 4K0nKmlene
uyL
ND
10 OSf3111401-23
Mnyl ecm.
uyL
Nil
00/313111410114
WO cAlrmd.
UWL
NO
1 0 06Y31114 0173
]Lylene(TpIMj
uyL
NO
90 OSRII140143
1-2-0kibWoem,44[S)
%
97
70-130 Mill 4 0 123
4-&omo6lroreben2 (51
'A
99
MAX mlF14 W23
Toluene•d4(91
%
100
To. 130 05731114 01223
LABORATORY CONTROL SAMPLE'
1210762
sot.
LCS
LCS
%Ric
PWAFnMer
LJr16m
Con.
Revell
7Y Rim
Lkl9u Ch1&I"
1,f-1,2 Te4red,IbraeFmne
uok
SO
465
93
70,130
1,r,1-rr d 1a nemeneme
UWL
s0
47 2
W
M130
1, 12,2-Tebehlelh.rnr
uyL
'A40.1
06
70.130
1,1,2-7NelJeroetllene
uyL
50
465
96
76-130
1,1 Qk11brpatllene
uyL
$0
495
69
70-130
1,1-OLN1Nxaetllnne
ugll
50
503
101
70.132
12.34"cJmmwnpwn
uyL
50
S00
100
70-130
1,2-Dlbrnmo-3bhleroPropme
uyL
56
499
160
M.
1,2-DlMvmoeel4nn ISM,
uyL
SO
4e.1
96
70-134
1Z-Dwbl.,dhenxen.
uyL
S6
404
97
70-130
1,7•DFdrlaroe9lenm
uyL
50
471
94
MIN
1,2-OKldlvpprripene
uyL
50
47 3
95
70-IW
1,}L7MLuv6enxene
UWL5u
47.4
95
74130
1,3-pchlorepropene
UWL
5041
3
95
mien
1 ,4 O:tfiw obM "
UWL
50
46.9
94
M-130
2.6ulm "0 MElf)
UWL
100
"NJ
100
70445
2-mm.enme
uyL
100
99.5
90
70-144
4 9e00.2oenlmrrm* { ORK
uyL
Ion
$"
107
M140
A-Im.
UgrL
Ion
96.9J
97
50476
AcryIW WWL6
uWL
230
247
19
70.143
Bmn2ena
Ily1
SO
411.E
96
704n
Brvmad11al9melnple
vyL
50
4911
0e
70-130
&omvd tllorvmelhene
UgeL
SO
46.3
03
70•I10
Bromolvrm
OWL
50
45.6
07
70,130
&emaw6mne
uyL
SO
46.2
02
$44"
Carbon dWidd
110R
SG
46.0J
96
70.131
C4rbm, leeadllmrde
VPOL
50
52.4
105
70-137
AwMe Pr.erlwl ran IN..... x. n h vxl. ir.M.M Yr w. -WI.' M�eeN exwl.e.r. ae MYhw.M W14.rM..Md b eN rg14 W M 1..un
Pen A.WYN
m164rvMe., W.
/*;5?
`epo1° 4" S.'100
1% .rr. " ae mle
..i.pow mn.
11N11e7&4M
QUALITY CONTROL DATA
PFOX f SUITy Cr9ma"l."IINct
Pence Pm*d N9' 92201121
LABORATORY CONTROL SIMPLE' L2 OR
Splka
LCS
LCS
%Re.
Pmrmmeler
U."
Cane-
Rem1N
%R..
LMm! OuewIw%
G1fel0ber1e4rle
UWL
50
45.4
91
70-130
Chlnrae(hm.
uyL
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5! 7
103
64.134
0*.mh r
UoeL
SO
471
94
70.136
0119,~hane
uyL
50
47.7
95
64.19
den-1,7-Dirnlorpe914n4
1prL
50
47.4
95
70-131
m-1,3-p J1luapropene
uyL
Sa
472
94
ml. to
Db7amadJnpmeIDene
nyL
SO
40.9
9$
70-IV
Q6rn _Nhene
UWL
SO
46.2
96
70-131
Ell0b. rene
uyL
S0
4S.4
91
M-130
lod.m ,,.m
UWL
100
95.0
95
49-166
M11010 ne Chtonrl4
UWL
$e
50.4
l62
63.130
Styrene
VL
50
46.7
97
70-110
7.tr.chlnre.0leae
UWL
50
410.5
99
10.130
Tahlmne
UVL
50
476
96
Milo
tr.r1a-f 2.01ddaeeFene
uyL
m
46 3
97
70.130
nem-1,3-01chlmepmen
IPWI.
5e
47.5
95
76-13t
N=a-dehlme-2 bu[ene
uyl.
SO
496J
99
70-141
Trrdllareetllvne
uyL
5a
461)
96
TO-130
TROhlprvMgram611M1te
LWk.
50
SS.6
111
62.133
wro 0"Imle
uyL
I11CF
90 I
99
W157
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uyL
SO
604
121
69-130
Xylme POW)
uyL
ISO
139
93
70 130
1.2.O1cMmr9mFeRm-04SSj
%
97
7o-130
4'em"kWoberltene (S)
%
99
70-150
7e6Nne-d6 IS}
%
102
70-130
MATRIX SPNE 6 MATRIX SPIKE DUPLICATE. 1211548
1211547
MS
MSQ
92203116003
Some
Spite MS
MSD
MS MSO
%Rec
Mm%
Permmeler
Oft Remull
r_
Can. Reaull
Reeue
% Rep 7. Re9
Um"
RPD APO Onml
1.1-01.14 mu"ne
uyL NO
50
50 542
$05
In T21
70,1%
7 30
0en7.m
.yL 0.421
so
w 52.0
56.3
103 112
79,144
a 30
Cbm,obentene
IrpA 0.36J
50
so 49 b
51.7
96 103
70-146
7 30
iduene
11yL NO
SO
50 40-5
52.1
97 104
70.155
7 3O
Tnchl.loethwe
uyL NO
50
50 541
577
IDb 115
e11-151
7 30
1,2-0kD'9w tOu -d4 i51
%
99 100
70.130
440r 6umoben2enp(S)
'A
100 101
70-130
T0lumee•d6 [Sj
%
101 10
70.130
a..wi. er.. .nit n,ro n..-in..-, Yr .r..a r .w.....r.M.4 Y",IM. M F. ..MI
REPORT OF LABORATORY ANALYSIS REPORT OF LABORATORY ANALYSIS
Tlw repen YEN rmlTw njmAueM, e.dW n M. T.w ..port N.r m1 tr r.Preduc d ..o n W.
D4Ie' MQJ701a 0420 AM .n..o.n e» N.i..n -Mof eeo. A_1, i U. . 4e pm0e 49 m 13 O.le 061121 o14 04 20 AM .T "w ,tane.nl or ne.. ArW.eaal yarM,.1. in P.U. SO of 73

�aceArWytrcal
QUALITY CONTROL DATA
Pea Ammytle.r ■wren, Inv-
UW rants Ar. Sum ,DO
I�wmfeW.. HC 2ea7e
rRmjff1S9o9'7
pr*ci
SwN CW..d-M1. Nry {LIrC}
Perm Project W :
92203121
qC B.rch:
MSVf1703S Ano"m McMd- EPA dao
OC B.hh Me6+od:
EPA 3260 Am" Onelpllon: 6264 MSV Ln.r L".I L.4P
Aa4.detad Lab 9ampin 02203121016
LIETHOD BLANK. 121076a
Mmrc- YYaw
A4.v Ied Lob$ampl.e' 9220JT21016
al-k
R.poftg
Paeerrmlet
u1e.
Rom
UWL An*ztd OuKAm
12•Te"cI0 "Ihmne
uyL
NO
1.0 0513let40547
T,1,1-incMwo.e+ene
uyL
NO
p1:0i
S,1.2,2-T.trohmweh
y
1.003�1
),1,2-T11cMwo.th.n.
uyt
NO
IID 0931040107
1.1-0Ic1Yaa6ianv
uyL
NO
5.0 0513111401.07
1,1-QcMaadmne
uyL
NO
5.0 OS7351140107
I.Uv7rKA10rop, OP010
WWL
NO
1.0 05r31H4111:01
1.2-dmomo-3 hloroprupene
uyL
NO
I3.0 05,31,140107
1]-Ditic m"rm,a 1E091
IVL
NO
IA 05f31l140107
1%•Dlcnlorpeen2ene
uyL
ND
5.0 05"111401.07
1,2-01rMaw6lene
uyL
ND
1.0 OSMI114 01:57
1.2.DIr18o1 epray.n.
up1L
NO
1.0 06771l140197
r,l-pldnaopropu+e
14L
NO
!.0 8L3111401:07
1,4.OIclJotob. a.ne
uyL
NO
10 OS13104131:07
Z411id o imEn1
uyL
NO
100 "Will 114 u197
2-H.x.nme
,WL
NO
50.4 OS ,M40107
4a4Myl•2y.ntrlpn. (MISK)
uyL
NO
100 05171114 27
Auler,.
uyL
NO
100 0MV140107
Aaybr llrk
uyL
NO
2Q0 05f3Sl140,:01
Benzene
uyL
NO
1.0 mil1401:67
81pmcW-Oh.na
uyL
NO
3.0 85l51l1401-07
eromcadnwum.tl,rle
uyL
NO
1.0 OWSI11401-07
&w.wMrm
uyL
NO
3.0 05r31114 01 07
&umOmeNer+e
uyL
NO
10 ❑ 95r31114 01 07
C.lbon deal I da
uyL
NO
100 05Y311L401:07
C.,b- Ab.dnwlda
uyL
NO
T O ml014 01.07
Cre="2R.,e
4WL
NO
30 051311140107
CMwoeth.ne
uyL
NO
10-0 OSal"A 01:07
ChrwoNt--
ulr`L
NO
50 OS+ U 40107
Gleorwneln.ne
uyL
No
19 05131r140107
cm.t �.OIdllwoeNn+.
uyL
NO
50 m1114.1 A7
ue-t,30lmluop Ppenv
,19ft
ND
1.0 ON3111401'01
OlbroemWaanedl.n.
ugfL
NO
S.0 85l3111401.07
Obronwrne6i.r.e
ugrt
ND
100 0513t1140107
E1pT�b.r+rave
ug,'L
NO
1.0 05,5111401-01
lodom.thene
uyL
NO
10.0 o5R1154 01:07
u.d+yt D. C.rlde
u4+L
NO
10 0L3111A 01,87
Sryru+.
ZL
NO
1 0 06/31114 01.07
7eu epNwovOwne
uWL
NO
10 owl 0401.87
Ta ...
uyL
NO
10 u5131114 01 07
uentr•1,Z Old-lrwovinene
uyL
NO
50 05 IA401:07
.ewin w«eniw cn axe .eee v.nh rW. � a+W h1 M rylwn• etl.wb �r+ir��e.e YYr.u1 v✓4 Werenm. w.0 rym.r� u.�r
REPORT OF LABORATORY ANALYSIS
inn nppn N'1 notp i.poa...d,.acept n M.
pu06 Date. Ow52I a 20 AM 1xM=r,ramn con 0p-A pf1 S--.. Irc
- QaceMalytical
QUALITY CONTROL DATA
Foycl. $wry Clmu J-MI Apy 1VICt
Pap. Project No. 92203121
METHOD BLANK r210761
Aaapclaled Lab UnV4us! 92203I21016
Ps-M. une.
M.M. +7ile1er
6fenh Reponln9
Hewn L1me A-ty-d Quaaerm
tam•1,3-D1d0vopfapene
uyL
NO
ID OS139140107
trove-1,i0tctduo2-pumne
uyL
NO
100 06l31l1i 01:07
T1"ID,v61hn+.
uyL
ND
1.1 06rS17140147
7rkhmf.16W.dre6renv
uyL
NO
I.0 8377 M48147
VArg1 epaltle
uyL
NO
50.0 84131/14 01;07
MnV4 prllorlde
uyL
NO
}.0 W31114 01.87
"1"170"',
uVL
NO
S.0 05r3111401:07
1,2-OlcMwoeN.ne-MIS}
'A
96
70-130 OS731P110147
4BrompAlrw Wr.111ei+. (9y
Y:
99
74.130 05rS5H441:47
TuWen.-d6(5)
x
99
70-IN 05A111401-07
Pees A..tyd4.18erHMe, W-
88W K.4" M $a 100
r4.imnae, kC Z"
r701 US4 092
LABORATORY CONTROL SMIPL.E.
$210759
*AA
LCS
LDS
%R.c
Peramaler
LN11ta
C9nc-
RReuk
9L RRc
U"Im COWAN..
2•791raaWrpepn4
uyL
50
472
04
7o-130
1,1,1•TrK1110ro41n.ne
uyL
50
464
97
70 Zia
1,1,2,2-TaFaWaluer,.nv
uyL
60
46.2
92
70130
1,1,2-Trrpipror0,anr
u9'L
5D
461
98
70-130
1,1•Dklip041nene
uyL
0
404
92
i0-130
1,1-0Kluorwm.ne
uprL
U
526
105
7l}112
12,14nchtpfopopm"
uBL
SO
1,2-0iMpmp•]all.rowoprla
uyL
50
45.7
97
70-t30
1,2•Dlb,o .efi4n. (EDB)
uyL
so
47.6
95
10-130
I,2-DkN..ben:ene
OWL
50
40.
98
10-13Q
1,2-0tmlwo.n.ne
uyL
60
49.0
96
to IN
1,2-Cemkfoproyanc
uyL
50
47.0
96
70-130
1,3-Oiduera+propane
uyL
50
47.2
94
70130
1,4-Daohlorohenren.
VOL
90
471
95
70-13D
2Autr+one IlAE%}
uyL
100
43.ld
93
70-545
2•Hs.anma
uyL
100
Soo
90
70.144
4•M.Ihyt 2�enr.nme;IMeKI
uyL
100
06.SJ
91
70.140
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100
92151
93
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uyL
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Zia95
70.143
11-2env
uyL
50
50.0
100
70. 30
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10
49.5
0
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&olr.=Qtom.81.11.
uyL
50
47.2
94
78.130
9lumarorm
uyL
50
476
95
70•I30
&om.melh.ne
uyL
50
45.8
92
S4-130
Cert+on dlwHdv
uyL
50
49.6J
9N
70.131
Cot- tetr.dLo.Ide
uyL
50
54$
In
Z132
CMarob.nem+e
LVI
50
461
02
70.130
CNlef..rhul.
uyL
50
53 3
107
64-134
Crdoroknn
uyL
50
48.6
93
70-138
Chl.rom.therre
IpIL
50
49.3
99
64-130
Rni.m•�ee s+w pre•w m MrweYl-'-'.1 ti'Itn..•eM.e�c�rer..n.Yrnr..rlmlr•�-'-� m W ryre.l.0 nn.1
REPORT OF LABORATORY ANALYSIS
T1w rwoa .t W mwad.d, -p
P.D. 510172 0.1.: 08l t 210140839 AM n Tll.
p- A 1,l S.nra. Iw
Pape 52 61 73

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r... +rc 7ePla
•••+�•�•�•
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QUALITY
CONTROL DATA
pt*acs, Suny Clm6W. Airy JtAC]
P6 P"d MP- M03124
LABORATORY CONTROL SA13PLE- M10769
Spike
LCS
LCS
% Rec
Pu.m.ler
V-0.
CC-
ReNI
% Rec
Lu}4M Wwikm
d6.1,2-Dlchklmelhe
uyL
5a
46.2
90
70.131
do.T 2-0 Nwpprpp-
uyL
50
41-5
95
70-100
t36ra1neelmlorvmelhane
uyL
50
A59
97
70.f30
OkRamamohme
uA
50
47 0
96
70.131
E9rylb.m-
UyL
50
46.5
93
MI 311
ro6o-@1hmve
ugmL
100
92 1
92
49 /60
M.bhyl-Chlerlda
uplL
5o
50.3
101
63-00
Wont
uyL
Sa
U 0
96
mi 30
T.h4c A-.e.en.
UVL
5a
Soo
701
70.130
Teweee
umk
Na
4AA
97
mt3a
Pam-1,2 Grfil o.ihen4
uyL
sa
503
tot
7W130
akne.l,3.Ochiwoprtwe4.
idyl
Sit
448
93
70.132
irAn.-1,A-Did imo 2-butwi
uyL
50
45-W
92
70.141
Todowupth1 a
uyL
50
4117
99
710-131}
Tdmfmwrvwravmemkve
uyL
5a
591
m18
62-133
1pmyl a-elale
uyL
Ion
06.1
97
66-}57
vmyl chw wt
uyL
50
62.6
125
69-130
XW4ne ITel.q
vWL
I56
lot
94
70-138
1,2•pdud Peamene-d/ ISI
%
91
10-197J
4-Brit lhunrvb...... ISI
%
98
10-130
Te6mene-46181
%
100
70-00
MATR rX SPIKE A MATRIX SPIRE OUPLICATE- $211546
1211549
ME
MSO
92m'J121016
Wks,
Spike MS
MS0
M6 WISP
%R4e
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Paremeler
Llnm A."
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%Rae %Roe
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RPO RPO Ou6I
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uplL NO
50
Se 59-4
71.8
$19 143
7u-166
19 30 u
B.nr.ne
uyL 0.42J
50
50 54.7
a7.4
109 t34
70-14a
21 N
0hlorvhentene
uyL 0 97J
50
0 51.1
62.7
100 124
70.146
20 30
Tokwne
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so
50 50.8
82.4
102 $25
70.1"
20 30
T11d11a[nelhwe
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50
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59-1
V13 13a
69451
20 30
1,2-twAo1oemene-w 01
%
100 100
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%
100 100
70.1]0
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%
100 f00
70-130
acekaliical�
QUALITY CONTROL DATA
Prry.el Sl ,y Clp.ed-ool Airy (UICI
P ece Pm Pre•.[ NO 92203121
OC Owl, WET!]1334 AAe44lk M@ffmd: SAV 232as
GC Barr.h MWh.d SM 2320e AmNvis Sawrolm: 2320B Au.aledly
AN6[lar.d Lab 8.m w DM3121005. 9220 12 1006, 92203} 2} 007, SM03121ON, 92M121 On. 92203} 21018
METNODBLANK: 121x366 MAIN: Mkilff
Agpe}a[ed Lab 511 mp144. 9220312 f 005. 92I0S12 f 006. 9Q203121007, 9220312100A, 9Z10312 5009, 92203121Q16
Bonk Repw-g
Pv.mafer Unlit Re" LNn4 Anrtyced OU49Fem
Aa,eprAty. Tvmal n C.CW UyL NO We WOU14 11 38
O4N A,�41yae411Nry1q., meK.
0 r .A.. 9m 10n
m 4~wo .. He 7m7a
Ittl4pmom
LABORATO" CONTROL OAMPLE: 1212389
Spk4 LCA LCS 'A Rep
PeFAmerar Un9. Cone. Renar 7k Roe LIRW OuM"m
Alk.6nity, T.A r r C.CO3 uyL BOOM 47600 45 90-I19
MATRIX SPIKE A MATRIX SPIKE UUPLIWE: 1212170
$212371
MB
M90
W03313010 "
6plu
MS
MSO
MB MSO %Rw
My
Parommma Lkft RmmA[ Cone.
Cane.
R44u11
R"A
%Rae %Re. Urdw
RP0 RPO Qual
Alk.woN. T.Ac mC.CO3 uyL 163 50M
SON
$How
INow
70 70 75.125
0 TO MI
"10L
MATRIX SPIKE A MATRIX SPIKE OUPUCATE: 1212072
1212373
MS
MSO
92MI2100e Spike
Spa.
MS MSO
M6 MW % Rat
Mnk
Pm.mm" LIn11k Raeull Comes.
Com.
Re ull R4 KA
%Rau %Rec Llrr41.
Rn RPO Quel
A06Ymh, 7e1.1 n C-cos uyL 34500 5Am0
50800
4141W 80400
W f72 7S•}26
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REPORT OF LABORATORY ANALYSIS REPORT OF LABORATORY ANALYSIS
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-om
QUALITY CONTROL DATA
P,60.1. SWIV M."M1. Ary IUICI
P.e. P,gacl No.. 92203121
aC Bash: IIWIC11323
Alulyna MNMod SM AIIW_S2O
QC Satch MW d SM 450462D
Analysis Desa196m- 450OS20 J5Ldkw Weir
Assoclsled LaM Sa"it. 92itl31210p5, 9220p121006,
82203121607. 72201121606
METHOD BLANK. 12119" Matrlr: yAMF
A..opatad t.b sarnfdea. 92203125005, 9224312itl06. 92203121007, 9226312100e
Bonk Repertlnp
Par I. Lk19a Raaldl uFrd Analy7.d 01619erf
Sulfide uyL NO 1o0O CM30141147
LABORATORY CON TROL SAMPLE: 1211965
Splk6 LCS LCS % Roc
P""wer OnO Cane R" %Rec Lkwi. OuaAA."
soled. uWL 500 sm 102 90-110
MATRIX SPIKE 6 MATRIX SPIKE DUPLICATE: 121196a
M21111169
MS
MSD
92293023007 Spke
$peke
MS
MSO
MS
MBU
%Rac
Mar
Prams lay Urft RmK Cmc
CPnc.
R-WI
ResuO
% R.c
% R.c
LInwk
RPO RPO Oual
SW9de PWt ND SOa
500
3MJ
309J
62
62
75425
0 20 Ml
MATRIX SPKKE 6, MATRIX SPIKE OLJP"TE1212570
12125T1
MS
MSO
92203023002 Spike
SQlks
MS
MSO
MS
MSD
% R.0
Ma
mnt PM.elm Vnft RMLUN Cu
Cone.
Rawl
Raauk
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%Rac
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500
464,E
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97
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REPORT OF LABORATORY ANALYSIS
Ily rfpdiNH n.l G. up.ACW, uwpyn M.
D.I. D4j 12l_014 ❑II20 AM wf....l... ,w.fYn consent el Paw ArnfeaW B.nw.. kc Pep. 55 of T3
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QUALITY CONTROL_ DATA
Pf*v Burry Cloaad•Mf A1ry IUICI
Pace Projad No . WM1121
OC 88", %ETW324 Analysis MMotlod' SM 4500-S20
OC BalcM MelMod: BM 4500-M An"'% Desulplbll 4500$20 swfw. ShYle+
AssodNad Leo Samples' 42203121pO9, 92203121010
METHOD BLANK 12112" Mabll' Weyer
As 4tod Lab 80 h"9. 9220352M009, 922p3121010
fllsnM R.partny
P—itt., lines R.R41 Limp Ang"cl W.Men
501140 uWL NO 1000 OW3014 1553
P... An.lrec.l S.rv.c.., Inc.
9e0G ri,rv•71QID
Hun�,wJ.. NC ]mTe
I7W Ie'!S-0O97
LABORATORY CONTROL SAMPLE. 1211999
SPOM
Lcs
LCS
%R..
Paramalsr Unlls
Cane.
RdwK
%Rae
L4u14 046AAM
&lid& u%tL
No
512J
f02
90 110
MATRIX SPIKE 6 MATRIX SPIKE DUPLICATE' $212002
$212ma
MS
PAW
92203346000
"o
Spwo MS
MSD
MS MSO %Rec
Mu
Palamehf Uf1Ila RA W1
Cone.
Cnnc. RaeWI
Rood[
-A Roe %Rec Lnft
RPD RPD Ou.l
Sufte uwt NO
500
500 493J
493J
94 99 75.125
0 20
MATRIX SPIKE R MATRIX SPIKE DUPLICATE 1212461
1212462
MS
MSD
92203313W4 Sok►
SWko
Me
MSO
MS MSO %floe Mat
Peesmaler UNIa Resuk Cato.
Cola.
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%Rac -A Roe Unit Rio RPO Owl
SWAB. 1WlL AID S00
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165J
166J
TT TT 75-125 ❑ 29
n.. up.unwm•.. yay. r..,... ...... ._i WM...' 'ed_n....',_w r,.wary­ up•..nuuw-r'.1 er ­..w,
REPORT OF LABORATORY ANALYSIS
Tx. ,.port m.A . 1 W .ep. . _PI M ".
bete OW H2O14 Oo.20 AM .n..c..f 1. r.n.n oon.. 1 o1 Pea ,yWpy .,,..Ny.. Inc Pay. M n, 72

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..w-64—
QUALITY CONTROL DATA
P-j-t %mClow MP.Arf1WC1
P.c. Pro7-u Hu. UM121
OC Belch IMETA119162 A.na1ler Meihvd EPA 100 0
QC B.Ip, Mel.od. EPA 3o0 0 Allp"'s Dm'=w1I1'n 300 0 IC An—.
Asrnneled Leh Sample.: 92203121M 922011210111
METHOD BLANK 1210663 MADd. Water
Aasxialed Leo 5—plea 92203121OM_ 42201121 ON
Blank Flopmou
Parameter Unlla R—Al Lknil Aheryted 00al6ete
$Willa r.y9. NA 250000 DM31140132
A.- AnNyenr I.fr1e.., Inn.
96aa.rw✓:.i Ara S-.r 100
1n..rwaa NC 2141e
170e1eTSww
LASORATORYCONTROLSAMPLE. WOW
Spike LCS LCS %Rea
Parm"o. WAs Cane. Revell %Rec Umlle arallen
Willa UWL 20NO 191ow 95 90.110
MATRIX SPIKE a MATRIX SPIKE DUPLICATE 1210617 12106"
M.i` M$O
92203023012 Sp41u Spke MS MSD MS MSO %Rec Men
Parnmelel WIN ReaWl Cunt. Conc. Rewll Rewe %Rat %Rec U-44 RPD RPD Quel
Willa "A 15201) 20000 20000 99900J 239001 7y ee 90 110 6 20 Ma
MATRIX SPIKE 6 MATRIX SPIKE OUPL ICATE1210e69
12t0590
MS
MSO
IR2203263009 Spike
Spiky
MS
MSO
MS Mn %Rec Max
pw"Irw Unlit Rnru11 Conc.
Can'.
R.eWI
Result
%Rec %Rec UFrkk RPD RFD Owl
Sullale uWL 13.2 20000
20000
36200J
y7 600J
125 121 9Q-110 1 20 MI
MOL
...wit a•r,.�.., o.. ww.r w a. rn. i•w.n.a Pr n.-we. ae.o......Pe ........r.�.r. w�.rr �. Pr........ �. �� r��...� �....�.�
REPORT OF LABORATORY ANALYSIS
T6. r.W r .6 -16. rwmdund..ra.p1- PA.
D.I.' D61 t 7?OtA 0120 AM ..e.e.d Fa.•nrn eu. Mof Plc. An..rey 4.—' i- Gape 57 01 73
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QUALITY CONTROL DATA
prolee awry ClosedMt. Airy (I11C)
Pete Pfoled No 92203121
ae Balah. weTAr19211
Analyele Ms*rod. EPA 300 0
QC B.Ith U.lhod' EPA 300 0
Anakpin D-.pNw: 30C 0 IC A+.Iana
Aasoaeled Leh Sengln: 9220312f0pT, 92203f21006,
92205121009- 92203121010
METKOV13LIINK: 1214099 MWW' 9WIsr
Aaswilled Leh Samples 92M 12X007. 92203121 DOB. 9220121 ON. 92203121070
el-k Raper"
Prometal Unea ReeuN LIM" Armlyzed aw11Mm
WIMP* ugrL NO 250000 o6ms,1414:56
LABORATORY C ONTROL SAMPLE 12WW
SPlke LC8 LCS %Rec
Paremeter Unla Cone. Rmat %Rea LhINa 0"4114"
Willa vWL 20090 lom 66 go -Ito
MATRIX SPIKE A MATRIX SPIKE DUPLICATE: t214101
1214102
MS
MSD
9220377000t
Slake
Show
ms
M$D
M$
MSO
%Rae
Mao
Perameler UFAS Re"
Cann.
earn.
Revell
Reatal
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%Rec
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RPO RFD awl
white uyL 2030
20000
20M
215o000
2140000
Sn
649
9o-10
0 20 M6
mQfL
J
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MATRIX CPICE 6 MATRIX SPIKE DUPLICATE $214103
121410e
MS
MSO
922033e6005
Spike
Sprke
MS
MSD
MS
MsD
%Rae
Mu
Paramefar Ur.4a Re"
Conc.
Conc
Rmil
Revell
%Rea
%Ras
UM6
RFD RPD Ou61
Supale uWL 7 4
20000
20000
03001
26e00J
103
f03
90.110
0 20
rryYl
REPORT OF LABORATORY ANALY515
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QUALITY CONTROL DATA
Pm)%t: $ wry Oo.e6-MI. Any NICI
Phu PrvJed No.: 9=1$21
OC BticMI: 'AETN1926Q
Ants Mtftd. $M 4500-a E
w ftch M0,1116d. SM 4690•G•E
AnatyRs Dsw pwo 4500 Chloride
Asudalad Lab Samples: 92203121C06, 02203I21006.922031210W, 92203121p06- 92203121009
149F(HDO BLANK- 1219156
Meta.: PAler
Aslodaled Ub Sllmpke: 92203121005, 9220312190t1,
92293721 W. 92203121006, 92203121009
Monk Reputing
Patsmelal t7nes
Result LX1111 FmYy"d Oue96e1e
Chiorlde uWL
NO 1000 ON11141742
LABORATORY CONTROL SAMPLE 12191S9
SPMW LCS LCS %Rac
Parir 1111` tins
Cana Reedt %Roc Lllntra LLalAars
Cldonde uplL
2DIM moo 1D3 90-110
MATRIX SPICE L MATRIX SPIKE O11PuCATE. 12191dO 1211161
MS mw
92203236001
"a Spoke M$ MSD MS MSO
%Roc Mee
Perimeter thins Reswl
Cana Cam. Rest41 Revel %Rsc %Rec
U1da RPD RPD goal
Chl.nde uplL 2.2
20000 20000 MOO 20700 93 92
75, 125 0 20
MWL
MATRIX SPIILE 6 MATRIX SPIKE OUPUCATE $219162 1219161
MS MSD
922033[3012
Splks Spike MS MSD MS MSO
%Re. MA.
Prsmarel uncle RneAl
Cont. Cara. Rawh Rem %Re. %Rea
Iimla RPO RPD 0-1
CNortde uyL 30.7
20M 20000 46700 46990 50 5$
M125 0 20 Ml
mWL
feMM'neelnYrltlr/yewalMwYY leNsetlN al M VMu'eWwi. e...yH .errs w wevwlr WI N er.e..M.ew M ryie.rey n.Mr
REPORT OF LABORATORY ANALYSIS
INe spurt N.1 rwI I1 npedtced. eeupin kd
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QUALITY CONTROL DATA
PF.Wt S—V Cloud MI. Aky 1111C)
Paco Pra od No.. 92203121
Oc Balch: VYETA F19261 Anelyal. Melhod SM 4500•C1 E
OC Belch Meow, SM 45ONCI-E A.&Iyw. 0e6w4etwn 4500 CNN Ida
Aesodued Lob Samples: SMM21010
METHOD BLANK 1210164
Associated Lea $e u0va 92203121010
Plaaeloplr Will
Chladda uprL
Ms9Xk. VAIdo
S1enk Repo.lFig
Rosw Umk AnWmd Ousmbm
NO low 060,110416.03
LABORATORY CONTROL SAMPLE: t210165
Epala LCS LCS %Red
PrameEer Vn" Cun. R-11 % Roc Lk"I s QwIk m
CrAonde OWL 20M 20400 102 20-110
MATRIX SPIKE A MATRIX SPIKE DUPLICATE: 1219166
1210167
MS
M5o
52201121010 Spike
SOS
MS
MSO
MS
MSD
% Rat
Mae
Par —I., un" Reodl Co—
Cons
RmLdl
Resin
% R"
% Rec
L1r.Y1a
RPD RPD Oual
ChkRlde uUtL 2710 20000
20000
21900
21900
95
96
75125
0 20
MATRIX SPIKE d MATRIX SPIKE OUPUCATE 12101416
1219169
M$
Asp
M03307002 Sp"
Spike
MS
USO
MS
MSO
`d Rac
Mae
Promoter Ions Res41 Co..
Can.
Resell
R..A
%Rea
%Roc
Lwift
IWO RPO Otrr
CNalde upL 17.7 20000
20000
37600
37100
99
97
75-125
1 20
-90L
...rl. o,...n1wa. n�. ws..l. n n.un�tr liwluae er a»-u.�r.-.wumn er...l .,nx..n •k.•wu �.rt.. e....nwa a In. rwm wtl�mrt
REPORT OF LABORATORY ANALYSIS
Oeta 0611 V2014 06 20 AM never., aw ,n4n ca.rm ul o.e. M Fp— Se nr.. Ix Page 60 oI 71

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QUALITY CONTROL DATA
P-Ject: Sutry C1o..¢M1 Airy ICJICI
P.ce Prol/e1 W . 92203121
OC BAteh VWTA09243
A1,Mr/Ie 1,401"A SM 4500-CM-E
OC B.tch Meried. SM 45WCN-E
A-rew Dewk"w 450OCNE CYAOIde, Total
A..odMed Leo S.nple.: 9220312I017
METHOD SLAW. 1216447
M4eIM lkrler
Aeeudnad Lab 9Ampl/e 0ZnV2t017
131enk Ropnnn0
PM.mnte" IJnka
Rend" Lkwl AAa/yxad
GNrlhl.
Cyarude WL
NO 1010 06l09M4 M0:32
LABORATORY CONTROL SAMPLE- 0416408
Spike LGS LGS %Rec
Parameter Lkdla
Cone Re"i % Rec LN4A
Ous11m
Cyw6de IO'L
100 107 101 90.120
MATS IK SPICE a MATRIX SPIKE DUPLICATE 12l%4D9
121"To
MS MSD
92203a M001
$pike 50k. MS MSD MS
MSD %Rec Mar
Pwem.lat Vnfk Result
Gm"e. Gene. Revues V.Result Rec
% See Ltw" RPD RPD Ouel
Cywicm uVL HD
100 100 110 117 rod
110 75-125 1 20
MATRIX SPIKE 3 MATRIX SPIKE DUPLICATE 12M6411 12194t2
MS MSD
V2203 mit
$We Spike MS MSD MS
Msa %ROC Met
Prrlmelet L"m Reno
Cm"6 Cent. Re&A Re.# %Rec
%Rae Llnwa RPD RPD Ou.l
CY.Wd. u01L ND
100 1D0 111 109 111)
10a M125 1 20
REPORT OF LABORATORY ANALYSIS
1M...Y,en enM re"b reyreArced...eepf n M
Lime 0at1212014 01•20AM ..neN eie ria/n donee 0 p/K/ Ar.lyper s.nwae Nt P.qe 61 e1 73
PaceAmlytical'
ewwA.[eaW —
I--Ar"wyeeo ftr cakWe-
9rLO e.or A.w &M t(m)
H�nMnr/. t1C ieo7e
ITI+Hnrs.9AB7
QUALITY CONTROL DATA
Pro*CLSu Clo.ed-W Airy ("JICI
P.o. Rnlecl No. 92203121
OC B.Ich VIETA119244
Malyei. Method' SM 45DD-CN-E
OC B.H h MOD d SM 4600-CN-E
An.". D—pli— 4500CHE CVMWde, Tald
Auod9led Lab Sawoks 022M 121005. W203121W& 92201121001. io2203 121 00a. 92200121015, 92203M210101
METHODSLANK: U16413
McLrlx: 3WMar
Awood-.d L.6 SamPlas: 9220312 M 0as, 92203121006-
92205121007, 97205 L I I00e. 92203121015- 82203121616
01-A Repoliln9
P.r.m.l.r IJr"Pa
R.wll Oren Anelyled Oa.9fwta
CYwA1e upll
NO 100 06=114 10:59
LABORATORY CONTROL SAMPLE' 1216414
Bplke L1C6 Lca % Rao
Pl.amete" 11nd.
Cone Raw11 %Rec urrim 9uemom
Cyanide -WL
100 110 110 k0-120
MATRIX SPICE A MATRIX SPIKE EWPGCAiE: 12104T5 121641E
MS MSD
1220num
Spike Silks MS MW MS MW
%Rac MHO
Pw.meter WON RwRt
Ce c- Cork. Rend Re.u6 %Rec 'A Rea
Liman RPD RPLS QmP
cvmd. WL NO
100 Ion Im 172 106 66
75-124 21 20 RI
MATRIX SPICE • MATRX SPIKE DUPLICATE 12K6417 121641a
MS MSD
9220.7121007
Sprke so*. MS M30 MS MSD
%Rec Mee
Pwe ow 11rm Rmkr
C u+ Cale- Re.W ReaWl % Rec %Rea
um9a RPO RPD 1]4MI
cyaMde 11Sy1 NO
t00 too a96 N.3 ai 96
7s t25 1 20
e.e.ln P.wn4e w. en.nil r..r w.e..e nTMvwe-rnw•..w.lwew..e.rn.rrnnrP.ww. 1 ww nyw.rw. w.rr
REPORT OF LABORATORY ANALYSIS
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Dare 06r 1 I7014 08'20 AM .M F. -,W, 9pn./e".1 P— S.r.Io1.. Im a2 of 77

a�►M
QUALITY CONTROL DATA
Plofecl: Scary Cloaad•IM Wry (UPC)
Pace F tPco l No.. 922011111
0C Balch: kVETAM9,250 Anayw MMhad. SM 5220D
OC Balch Mdtlud SM 52M An*W Daapom. 5220o coo
Atadaeladidb SHtpMa. it2203121005, 9220312100E.92203121007, 4720312100A• 9220312$009, MO3121010
METHODBLANK- 121037 Mabq. 90aaal
Ano"Ild Lab Sample' 92203121 M. 92203121009, 92203 t21007, 92NII2100, $2203121009, 92201f21010
Sleek Repwunp
Par.Pwler Llny. Rend) Wil A—lyred i]uaYRen'
Cnamlc.I Ceygen Drmend 64L ND 25000 06/10,14 11:40
Pau Anatyee.V e.rvleaf, Ina.
steno rcnctq iw. sw too
nr}rPn•.. Nc MIS
X t0410I �
LABORATORY CONTROL SAMPLE: 121663a
SP9u LCS LCS %Rep
Yram.tw unam cane. Rutdl %Rac LI11ft i0mmki n
ch—dt -A Oregon Dam" ugA. 750M 745000 99 90.110
MATRIX SPIKE 5 MATRIX SPIKE DLIPLK:ATE 12IN32 1216640
MS MSD
waa4omoc2 splka epaa MS MSD MS MSD %Rm Max
Prame[at LNdla Ran& Cent. cam Reuel Rwt9 %Rac %Re Loft RIND RPD Dual
Ch.tt.c.l Dayllon Demmd up1 76.0 760000 7s0ma 9e1000 8430" Paz I D2 75-14 0 20
mWL
MATRIX SPIKE A MATRIX SPIKE DUPUWE, 121"41
1218W
ma
MSD
9220312100E Spike
Sputa
MS
Mso
MS MSO % Rec
Mu
p.r.m.ler Ul,^ Result Cone-
Con.
Rnu1l
Revel
% Rec %R.e L mft
RPO RPD goal
CheaMcttl ONV94o Dem.tta WA No 750000
150000
721$'m
?Hopp
97 97 75.125
0 20
awpy v..r+w mryr. Pei row" iwO ill. `en1..+.—Lou wrynrar%.r..AL
REPORT OF LABORATORY ANALYSIS
rr.a r.pon rv. ear a raeres<erd, elerpt b u.
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w.tyx.YX. tr.n
itf4 F'1 r'+'n11I:
❑UALITY CONTROL DATA
Prnpcl Stwcy Cld.edatlL Ave IUI CI
Paco PF*01 NO.. 92203t2l
QC Balch IAIETNIS200
Aneym Method SM 5314)6
OC Belch Meowd: SM 53108
A,,4yala Deomlpbwt 531ou TOC
Aeochled Lab Sampler 92201121005
METHOD BLANK- 1213002 M.btr VWW
Awopeled Lab Sample. 92201121005
lmmk Repotbny
Pa..maler U." Revel Letn AP.yted qua36ua
TgI.I organic Carbon PAIL NO $M 06415A,I 14:41
LABORATORY CONTROLSAMPLE- 1213MI3
$peke LCS LCS % Rec
Penmew Ulm" Cenc Reau11 % Rec UrIlb 0u 06r.
Tola1 Or6194c Carbon OWL 25OW 24800 99 90-110
MATRIX SPKE 9• MATRIX SPIKE DUPLICATE 1213004
1213005
1t8
MSD
972937011001 splka
SPN4
MS
MSD
MS M5D
%Rec Mar
Pwsmoul LIAM R.atdt Cent-
Cenc.
R-0
R-KA
%Rae %R.c
Llmlh RPD RPD Dual
Total Organk C.r upiL 2.0 2s000
2$000
2E700
24700
107 107
75125 0 20
trwL
MATRIX SPIKE R MATRIX SPIKE DUPLCATE 1213009
1213007
MS
MSD
92203tl5M12 Spike
Spike
MS
MSD
MS MSD %Rec Ma.
Par.meler U1,1110 Re"I Cores.
CerK
R4.01
ReW1
%Rec %Rac U-Is RPD RPD Dual
TuVI Crp.rae Cmbm WL 2.4 25000
25M
mo0
26900
97 97 75.125 0 20
MWL
....n P...r.f.e en w. Py..,. � r....in �.e+..a.s a.. •w+u• wr.n ..wat.w,.. «. rr Mrn-r.. w...nr. m.,,.�et.,l M.r..w
AEPORTOF LABORATORY ANALYSIS
ihw t.peM1+hn .roir i.�Pprc.q uc.IN n Me
Date G&I772014 OE 2n AI.1 rtTwMM.n4tan cenrwN al wea An•F7ec41 Seer». Inc P.qe 64 .173

Paw Anslyoul Mnlws, Me. Papa Analye[ar
f� /gyp �1 ,1, / / ow*"—Y A+. B�"'(A r�/� �1 �... /�r�1 Ge00 Kero.1 A+. Out. 100
l ac kidMica H—w-A.. MC 7A0}9 w i�iwlyfiYGi rwmrr.wrn. H: ]M]n
a.rpYW— IT041a7Ya j a ,osi 17611315 gun
QUALITY CONTROL DATA
Prp)ecl'
SWIV CWAadMI A" ILNCI
Pip Pfejap No:
52200121
Oc Balch
YJEFAd19212 Ana" Method: SM 53109
Oc Balch MaPod:
SM i31 OB Ann" Deacrolas- 5310E 70C
Asionli ed Lab Samples: 9220312I009, 92203121007.92203121 ON. SM03121 MD. 92MI21010
METROO BLA►K 1214105 Mahe YIYI.t
Aeaod.Ied Lab Su". 92203121 M.92203t 21007. 9¢207121908.112203121Will. 9220312 to t0
Bland Rspa g
PUNDEWyaaa Rsatal LarR Analy"A OwMala
Tests Organic Carbon 1V& NO 1000 O610A714 2052
LABORATORY CONTROL SAMPLE 1214109
SPke LCS LOS % Raw
pwarnalet Unea on- R.uAI %Ric
Lknas Owens"
Total Organic C.rhm uprL 25000 74w 90 90-119
AMATRIX'5PWE A MATRIX SPIKE DIIPLCATE121410? 1214105
MS MSD
92 M14DDI Spike Spke MS 1a90 MS h1w %Rec MAN
peramekr 11111ni Rasull Cone. Cone. Rudt Ra.Ai In Ras %Rec LIMMIfs RPQ RPO Gull
T0161010Amc Carbon uyl N0 25000 25000 24JIM 244" 99 99 15-125 0 20
MATRIX SPIKE 6 MATRIX SPIKE DUPLICATE 1214109 1214110
MS MS0
97203121006 Spike Spae MS MSO MS Ni % Ric Mo
lawarPelsr onn Revell Conn. Cot - Result Reallt %Rec %Rec LIMO RP0 FIFO Oual
Total Ot9anie Carbon uplL 13900 25000 MW 32100 32000 73 73 M125 0 20 All
e.....y .e•M•ime". eau.•n.w nib narn...x n. -Ihi.. mexen• rae.w«�.w..Y..xla un�lnpi....rawwrwm or n....w.
REPORT OF LABORATORY ANALYSIS
TN. —,en hM rwr W r.prtyKp... upt n ti
DNS.: OW$ 212DI A 0620 AM .t9H.4 ew widen t of Pons Nylyoal Same
Pape e5 el 73
QUALIFIERS
Prated Sorry Ckned MI Alry (UIC1
Pay Projed N. 92?0312t
DEFINITIONS
OF - DdUjO FaClQ1, dT.paled, lati*JlMs the feclm apoled to Ole ltpmted data 6U! to thanpit in aanYns pl epai Mlon. d iLrit- of
Ilia 6emde Ah'a 1, pr mm6t— onrllenl
NO - Ne1 Nutted at or ebm* edyetad npor0ng tmll
J - PAIITeled corm uolw a6eYe thlr e*S*d wMrA dalkalell tail and 001pw Ins anAlaled 4"wing artN.
MOL • MNtled Merced Oelecupn 4w1
PAL - Pace R.patN Lima
RL - Rspennp LYPN
S • Swropele
12-Dlphur,41hydra rile (1270 isled an alyle) dac nip ee to Aiobm one
�enalNt.nt YAM EPA gwdeh—. 1nl eundad dole A,. d np4yad and h... bean lm.d 1. cetddete %—V" snd RPD Values
LCS(D) - L.ba.uwy Conn nl Sample [Oupinalel
MSID) • Mild. Spike ID.iplicalel
DI1P - Semple Duppcele
RPI1 - RA4wW. Pal cenl Dllerenw
NC - eta C61elAeble.
SG - Sacs GM - Clean -Lip
U - Ind"les the cnmpinurd vrae analytall ra, Wit not 6@IW ad
N-141tr weiipherryla min. dacornposes end rennet be Nepal ated from Dlphsnylamins U.ing Mselpd 5270. Tha natal reporlvd for
daeh snehie Is a carnbined opntanlrsH-
Add pf"mmilmt may not ba opwopnet. Im 2•U0aas 9lyhklyl wart,. Sytena. Intl VAIII ciA ftla
Pace An,"cal Is TNI aeo►etad. O:oi MR Pace PM la Me a itnkt NM of acciadxad anarylea
TM - The NELAC IngrW..
LABORATORIES
PAST A Pace Analylleal Sef.tces Aih.Wlle
PAST-C Pace AnalAcM Sonorea ChaPuOs
ANA LYTE OUALI F PER B
(-0 Malyle recovery In pie laboramry rontm as mole ILCS} wa. outalda QC amta.
MI Matrb: Doke recewery axc aided OC Omits. Balch mccepiod bred on h b&n" conlrm temple (LCS) Tva o fty
A16 Mslrl. spike and M.trrx spke duple to r—iry r1o1 .rake nlad .1,14,st :mtraV units dnio 1n a. hVI. III&& n.
HI RPD VAA N was mrlslds oonlrol INNIS
REPORT OF LABORATORY ANALYSIS
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Dnla. WInoIA D6.20 AM .T".*".ft. WM14 Ft Pope AfttociilS.nnya Nr
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1.y�Y„.rA„
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/ .-}°�CEAlk71y#1�1�
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..�aa'ahba—
17dpiS0o97
1 'w'
wwl^'
ITp4pP}9{pp
QUALITY CONTROL DATA CROSS REFERENCE TABLE
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Prgect
Svry 09..d Ml.
Nry IuIc7
Project
SWry C7a9.d-MI.
Wry (IIICI
Paco Project No..
9220312,
Pan Ploj.cl Na.
92201121
Analylkal
Analyti.ai
LAh 10
Sampl. ID
01C Batch MNhad
QC BMFh Amlyfical Mw61cd Balch
Lao 10
aww. 10
OC Balch Madwd
OC EWch Analytical
Method Balch
12203121001
Mri-155
EPAl0I0
AIPRPM6067 EPA6010
IM14632
l2203121002
6AW.1e
EPA3010
MPRPIt6067 EPAW10
ICP114532
12201121006
MW-1
EPA NOO
V&7A?18162
22203121093
MW-19
EPA 3010
MPRPA11067 EPA 60 t0
1GP114532
12201121005
MW7
EPA WO.0
VKTNIOI62
12203121004
MW-23
EPA3010
MPRP716067 EPAR10
ICP114552
12703121007
MWAS
EPA3000
VIETN19111
2203131o0!
f2103,
MW-21
EPA NO
VVETIV19211
NM121005
MW.t
EPA3010
MPRPn$t07 EPA Mp 10
IC idda
1 21001
MW-1
EPA10C.0
WETN19211
f22o112100!
92203121007
Mri•7
MW-15
EPA3010
EPA7011
MPRP 6107 EPA 6010
MPRP116101 EPAf010
ICP11456a
109456f
12203121010
MW-14
EPA300.0
WEYN 19211
1120312100!
MW-21
FMP 1010
MPRP115107 EPA6010
ICP114rj6!
92261721005
MW-1
SM 4500 CIE
WErArIN 0
112031110"
Mri-)
EPA3010
E10
MRP111o7 0
PI4
ICP111BM
MM1121076
MW-7
SM 4500•CIE
VVETN19260
MW4
E3
PA00
MPRPI15PA 60
f
922W0o
MW-16
M23121010
54500-C-E
WEOV 9260f2203121011
MWAR
EPA501O
MPRP115107 EPAB010
ICP114588
9122232003121o06
MW11
SM 4WO C14E
WETA11026D
9220111257012
6tW-113
EPA 01G
MPRP11611o77 EPA9O116
1CP11466a
109
SM 4500.CI-E
VOET.Vtffi60
1]
A
PR71fEPA60
.2,032
20412
EPAWO
MPRP1PA80
ICP11451
2032105
MW-14
SM aC1£
VVENf26MW-Y
12.3171Oil
W-6
E5310
MPP1607 EPA 6010
P46
IAW-t7
$11460 CN-E
WETN19244
1202
2301f
MW-
EAU 0
MPRP11EPA 60O
CP9
:22a031211006
72 212 004
MW-
SM 00CN•E
WETOV 244
71l22207111P101
MW--14
EPAWO
MERPM69 EPA 7i7O
MERG6H9
92301127aeY
Mw.15
EM 4700-C$
A119244
9220112100e
M 45WCE
WETN19244
MMWW-1136
EPA6260
MSV26895
22072101
MMW-16t
W
M 4500-C%
WETN182442100331217001
1
EPA 826
MSV995
122031$016
M2
W1
SM 45WC
WETNI
EPA660
M9VI6951100
91203121004
MW23
EPA 680
9
12203127017
SA450C91201120
N
VVEfN198224443
92207}I10o6
rZI
EVA4260
K45W270034
1l222003312711006
MW-1
520
WE-TN19250
f91227111
EPA8260
VR34
2112006
MW
SM 5720D
VVEN1250MV-7
07
A
24
111011217
M
SA220
VVErk9o2Ri2o0
203,21
MW-21
a
EPA260
MSVr27034
0700
2
SM 52200
WETN1925Of2o
12006
EPA6280
421
122031210Do',
MW
1M
1NMW-1
12203121 O10
6
BVR7034
201
f22030t6
MW114
5MM 520
MTN19250
9220321oll
MW3R
EPA6260
MSVY27034
MW-
S53$08
VVETNI86
92203121012
MW43
EPA6O
MSM7034
6W-17
EPA 960
MSV7234
9fl922031211
MW"-1
SM SMIS
WETNI92122013,T1oT3
M0,20
EPA
MS72703
z 112100
ri 5
$M55O9
VETN1f212822203121014
9225
0712101
W1f
EPA 11260
MSV27034
1I
2DIN7VIEW
9212
22032009
MW-9
SM531088
WETN 19212
921031210%
MW22
EPA9260
MSV127035
9223121010
MW-14
SM 53106
WETN 10212
91207121006
MW-1
SM 21206
Y&7131334
922aN71OOl
MW11
SM 23205
VYETI37334
42293121007
MWf!
SM 2720B
V4*TR1334
1:2113121 06
MW,T1
SM MOB
V&7131334
1220312100!
PAWS
SM 2110E
WET131334
92203121010
v%W14
SM 23206
VYET131334
921031210P5
MV44
SM 4500-520
yWT431323
92203121006
M6W
SM 4500•S20
MT13f323
92203$21007
MW11
SM 41 0o-SZD
VhETf31321
...Dot
pl.1
SM 4500.320
yVET131323
92203t1100S
MW4
SM 4540-32D
VVEMIt 324
02203121010
MW-14
SM 45O0-S2p
VyER31324
REPORT OF LABORATORY
ANALYSIS
REPORT OF LABORATORY
ANALYSIS
i r.•.W1 h"net lr nPrvtlueW.
—M n W.
TA. r.borl nM net ba Mpmb. . kc.pl., W1
D.1. o6l12120$4 06 20 AM
M4. - . w...m.e o..w .r P.c. A-I,ucM 6«ra..- I,t
Rape 67,0171
Del. 06, 1272014 06 20 AM
r,_J 9r r c.n 10 a— An.119W s.arc
P.04 64 .173

L-e' nq
Issuing Adlhl
F-CHR-CS-003-mv,14
Client Name: m rryu rl�l"�
Go urler. ❑ Fed 5x ❑ UPSO USPC CBrsnl❑ Commerasl❑' Poo Olhar
Cualedy Seal on Coolerl0ox Prvaant: 0 yea �0r ne Seals intaet ❑ yea ❑ no
Packing Malarial: ❑ sub" Wrap'BubfAe Bays ❑ No"
/Q Dlhel
Thermom star Used: IR Dun T1102 �Tt40Y type of 1ce:. (1 Blue Hone on be, edhg PM - blgun
Corm' evi C r 61 f.O BlaldplCH Tissue Is Frexen: r.A Ne�
Corrected Cooler Temp.:
Tamp should be mba a feet-9 b8'C Comments:
Wu and InlNals ravn .ur �I Ing
cvnlsnp;_ Y
Cha7ftMCtral Present: .s 0X. C1WA
T.
Chain of Cuel Flied Oue t7NA
2.
Chain of Cue Rd ulshed: ON. 23"
3,
J..
SaMpIff Hama d &22IVFA on CDC: L7:ia .Clrq DWA
S"
Sa Anhred wWn Hold Tm+e: w Ob. ONA.
5.
Short Hold time Anal Ws 1472hr : Oym 136i� DNA
B.
Rush Turn Around Time Requested; Ova OWA
7.
Sulfrdw VoJu�na: .s OH. Ow.
6.
CNmcl Conlainem Used: y { ke ONUA
-Pace Containers Used: 7 Yn 45W OWA
9"
Coulainens Intact: Ev., ❑N. FJW6
0.
FAlerad volume received far (heaved Teets Brea CLa ruA
11"
Sample Labels match COG: Urn Om ❑ WA
•Includes dataillmeANARa1 els Matrix:
12.
AN opnlel'w needlnp pmeerv.N.n hsys been dmkad. qyN One C7raA
AA c leinere rwedinp pm3aNs7bn are Pound to be In V11- LPN. OnuA
WreMwc* wNh EPA wvnvnerdatkn.
.0a VOA, .rarosd, TOC" OW, W-URO?-aw) Yes CIHd
13
Sa checked for dechbdnaliow r]Y_ ONo Drfm
14,
Heads re M VOA Nate rN m : Ore. rxi t3Nat
15.
Trip Blank Pnesenl: RY.N Ow . N'
rrip Blank Cusfady Sag it Present 77r.. One 04
Pace Tpip, f3Eank Lot p CK drehos
6.
Client NvtHlcadmV Resolution: Floid Osla Repulred7 Y 1 N
Parson Contacted: Oatemfw
Conrmenlaf ReeWulion:
SCURF Review: - ow; I of • 922031`1
SRF RNNYIewrW{y1`1
Hold W MA", dmcmiamcy s,Mctlny NryTh cwdana aompssna r.�!.EM�.�1 1�i��!1 aamotes. a copy of 01Is fv.m w l he aaM to fho North Cuoana DeMIR 11 1
Csrtllkellpn ONdv S La vul of hold, Inoprrsd ofeBervNIPM. out of lamp. 02203121
ince red co.dslnerej
PN969 0 73
MINIMUM
I
a

Awyrnw
Id: Apnl 07 2014
1012
Client Name: 0Ivjcpji
Cou ner; {_] Fed Ex [] UPSO USPS[J CkrAo �-Cwvnetde0' Puce Mar
Cuetvdy Ssai on CookvrMw Present: F.]yes I d ne Snr/eie inlad: 0 yea ❑ no
Packing Motorl at: ❑ Subble V fOp dBubble Baps. ❑ Mww ❑ Olrier
Thermometer Used; OR Gun Ta 102 1 Type of Ice: I] Blue None SarrWea m fps, q prams nu pequn
Teo COrmtubn Factor T1102' n C.nrrer}Irn T11 Nn f`nn H"ti
El oip load Tissue Is Fromm Ya 1q
Cvrceoted Cooler Temp.: i.� �C 9
Twnp thaed be above ff&OZN p VC Cwaments:
pale end to non eAsm]Nrq
Chain of Cwo6 Presefil' Y - ❑rfe OKA
1,
Chain of Cue Filed OuL ON. OWA
2
Chain of Cim R : r. LINO LIreu
3,
SEIMPlef Name 3 s atwe on COC: 4y LINO OWA
{,
San as Arrived wMin Hold Tuna: ae LINO LIWA
5,
Short Hold Time Anal tls �72h LIrae 6 QNA
a,
Rush Tum Around Time Ra ttd: OYw IfHo OWA
7.
Sulfxtent volume- rJNo OWA
e-
Canact Cmiainers Used v Ow, UK*
-Pose Coniahera U eed r 04. ❑WA
0-
Co0alnefsInracl: tA. tl-- L3
10,
FlRarad volume recelved Ior Olaaohred leala OYr Ole dWA
11.r,
SjInVa Labels rnindl COC, Orr ;p ❑k.
Anclutlee ealeAlmdlf)rAna eke Malri..
_ 5 - I5
12.&- `7uri ry6f,L.
As. ooryO"WO w*dkN pme.rvednr Nw been Neaee.
rfa LIra OWA
As=ntakw Fwo*.g presefrafwn" iM.nd to be M •Jrr ulW QWA
w"Imonca voh EPA nconvrxndMkn W�
- Yak =ftrm TOC. OSO, tM•CnP [WeMr) Idr.. ON.
13.
Se as checked low d echlorinslion: rr ❑ ❑"
14.
HoWspoed In VOA Vlals Birvn OYa Ns. f3WA
15.
Trip Blank Preami. Dyes Qno
Trip Blank Cusiody Saab Pre cant t7rn QNa
Pace Tdp Blm* Lois IF purchased :
16.
C11anl NoU6catlonl Resoluilan: sherd pera Requlred7 r r N
Parson Conla•r:led: ❑eiaITlnw,
C*nunenly Resdubw
SCURF ReY!/W: J pep_ 7S r
SRF Review pate:
Hwe. VOwnarnr ihw a dlsuspancy allaclinq Rath Celbinl oontpllance
•"Wn. a copy of this ipinl will ba eanl to Ohs NOM Carnllna OVIINR
CHllficalion 0111M ( 16 &A of hold, Wicanecl pfaaarvatNe, out of ferry+,
Mcprrers Laruuners)
2 2e
7R
HarAwnle proJad number
(d no label available)
Pay. I } or ] 3

L•,
A
I
1ns6.
11
No
MESON
NEMESES
EMEMBEEMMEW
MINEMEMEMEMI
MAINMENNAMMMM
GE
MEMAMEMEMEEM
MEN
MIN
■
mill,
P.g. n nl 73
27COA4Xical-
June 10. 2014
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NG 27529
RE: Project- SURRY BLANKS
Pace Project No.: 92203466
Pfu Rn Yr5cR1 bm�uf. Inc
oeno..xa��.v sUr �m
run��wif. NC 350 i8
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on May 29, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current T N I standards and the laboratory's Quality Assurance Manual, where appticabla. unless
otherwise noted in the body of the reporl.
Analyses were performed at the Pare Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
S-Z-
Kevin Godwin
kevi n.godwi n®pacelabs.com
Project Manager
EnChM .
REPORT OF LABORATORY ANALYSIS
TM. npu NW-1 b. nPn.dL-*d.--P1nM
wMwl",m cw —t c'a—A .rA s..rc.f. Inc
P.p. I oA 74

�" �aceAr+a�ytrcal
P4vl4d: SURRY BLANKS
Pecs Prvlad No. 92203466
C11MI00e6 C441fIcMian IDS
9600 Knay A- St. 100. e-1mvne. NC 26076
Nari Cardna CrnFxlp vWler CerSFcauarl i. 37706
Hari Car W ne Ft.ld SeMcea Cor OAcao �
Hari CYoln. 6N..I.m1.r Cmoewhon i' 12
SaLdh CMWni CWdACarWn 6 99W6%1
AaAerRM II.ritlft n Me
2225 Rtwarald. fk.. AahM1a. UG 76604
FlorldMl4ELAP CwtHka6al a E6.7646
MaaaadwaMu C466aaon F M•N000A
o4 Mr Cru 0rin.4p 61FIler Cmrlluaon 0- 37712
CERTIFICATIONS
FlpndafNEL+PCmnAc&coni E67627
Karduay LIST CeNicaWn e. 64
wnl Lhpra. Cmsklmvn ■ 351
IArgnlaNELAP Cwtk,&L6 n is 440221
Norm Caroana YYaalal.alM Ce1oba0en 6. 40
Sawh Caro9na Cr4F6a6on i. M30001
YAaet %&OWN CMNFea6on is 356
Yhpn WYEL.AP C.Mlk-wn i- 4602.22
REPORT OF LABORATORY ANALYSIS
1 W. r.M4 ep.r rw1 Ae —I- n t6A
we.tir 0. �— ce...m.r P--A,.t„d 54— 1-
P.0 Anaryee.t S.rvin �- me
D"HinerAr. Sur..
rtir w-p HL 2m3?a
I7NO15 909I
�aceAn Pi0) e
SAMPLE SUMMARY
Protect. SURRY BLANKS
Pap PL.i.cl No.: 92203456
Lab m
Bap 1. In
blame
Ode Cullearad
Date Received
92203464001
ES
mter
05R9&141420
0519n415:20
922n3466002
FS
lPhler
05R9114 14.39
051201ta 1520
92203466003
T9
W.ler
05nlPIA nQ.00
051211" ls'20
REPORT OF LA BORATORY ANALYS IS
Tl r.mn .full �t W r.predu . —ptn W.
Pape 2 of 24 ..en lh. r,..n.r. ca+.e.+tW V.- On VwN S.mw. me
P.- AnAylkal 3-vicae, h-
ee00.er.r Av. sua 1m
H.�—ae !eC 2e016
f7WW57 glr(j
Peak 3 .124

1'acEMalyrrial
a..R�..ea.r.
SAMPLE ANALYTE COUNT
p1mIe9t SURRY BLANKS
Pace Prnpcl No.. 9M03466
Pan RnarTue.i MrWv., Inv
9lpp0- A.. Su IM
1AA».r.r4.. Nc 2m7o
004AT$110112
'-�aCeR�alyfrcal�
PrDlect BURRY SLAW$
Pace Propd No. 9220346E
ANALYTICAL RESULTS
Pep An.1y11e.r aaNln., pre.
WMK-.7 A- 6Vu Ion
rKwr..... NG 761t16
4704p7541Ap
AnMylea
sample: Ell
Loh 10: 1220MOOl Cwlecled W291i414:20
Received U52904 IS 20 Maim Water
Lab 40 9a+npte 10
Method
Analysis
R.P9Aa4
La6Dra"
Reporl
Pw..eler.
Re. 9m omm Llmlf
MOL OF
Prepared Anely"d CAS No Duel
12200414001 EB
EPA 6010
JAW
IS
PASI-A
EPA 7470
MTS
1
PA$4-A
10101CP Dfenn tlrrNar
Melyl Me"d. EPA W 0 Prepaelvn
Molhed EPA
3010
EPA 11260
GAW
51
PASI-C
Mummy
NO ugIL 6.0
5O 1
061031t412'30 06104M420-S6 7440.36.0
SM 4560 =
SAE
I
PASI-A
Alaergr.
Berlum
NO w1k IOU
NO ug& $00
5.0 1
60 1
OOM3114 17.'30 OIFp4114 20 56 1W 36-2
0010311412.30 06/001420:$4 7440.11"
SM 4NO-CN{
JOA
1
PAXJ-A
BeryllWm
NO ugIL 1.0
1 0 1
OWO3114 12 ]0 061040 4 20'56 7440�1-7
92200495D02 F0
EPA 8OID
JMW
16
PASI-A
C_ m' -
NO u91L 10
4.0 1
O8f03l141230 OW0411420:% 744043-9
EPA 7470
PAYS
1
PASI.A
Chpo .
NO 4& 10.0
5.0 1
OSIOV1412.30 08041IA 20:56 7440417-3
Lah.6
NO u01L 10.0
50 1
Ill..' 12.30 0BA14+142056 744048.4
1-'PA 6260
f3AW
51
PASI-C
Lepper
NO ug& 100
5.0 1
OWOV1412:30 0810411420.5E Y440-50-8
93200466000 TB
EPA 8260
GAVY
51
PA.41•C
Lead
NO u2k 10.0
30 1
O8+OV141236 ORL-Ow 1420:56 7439.97.1
NI[001
NO K& 50.0
50 1
0"31141250 O61OH1420:56 7440.02.0
SNerwlm
NO 401E 10 ❑
10.0 1
OSMU14 12.,30 0 "14 20-56 7782419-2
Silver
Np ugA IOU
5.0 I
OWU1412.30 06f0411420:66 7440424
Thalk..
NO u0A- 5.3
5.4 1
OMWI41230 0610411420:54 7440.28-0
TKr
NO KA 100
50 t
06MVIAI2.56 1181O41$420i6 7440.11-5
Wn.ppm
NO uWL 25D
5O 1
OMV141200 O&1W$4204% 7440.62-2
Zinc
NO ug& 100
19.0 1
06PoSr1412-39 olkWI420:56 74404"
7470 M.rcursr
Anlpyllgl Meek": EPA 7470 PrepMAOen MempdEPA
74 70
14ereury
NO u06 020
0.10 1
06l02r14III 45 0610L1411:OS 7439-9741
6260 h11V Low Loved Landfill
AnW6nt Me Mod EPA 9260
A"IP .
NO uWL 100
Ina I.
06101114 16: 14 87-"1
",Y I4nle
NO uyi 200
19 1
OE101114 ISAA 107-13.1
8-1-
NO uglL 1.0
0.25 1
0610104 16:14 71 43-2
Bronwchlc.omvlhn�.
NO UA 3.0
017 1
0610104 19.14 74.97.E
Bren.e eWyo-mellune
NO uUtL I 1
016 1
0MI04 16: 14 75274
Bromnlwm
NO UA 1.0
0.2E 1
"MIF14 W14 7S2rr2
8lemomefhme
No uA 10.0
0.24 1
"MR14 is 14 74�&9
2-But.nnne(MEN)
NO ugL N10
0.96 1
MOU1416:14 7E-P}3
Carbon dul4de
NO uA $00
12 1
0"1114 10:14 7515-0
Coro-tew--h nde
NO ug11 10
0-26 1
08r0113416.14 %21-5
ChlDrotmeer..
NO ua& 111
0.23 1
06@1114 10:14 1g8-wt
ChIm"thm
NO up& 10.0
0.54 1
OW114 I6:14 7S0"
ChImParm
NO ugA. 5.0
0.14 1
0"1114 16,14 074115-3
Chl.mmaNane
NO ug�4 1.0
0.11 1
0610111416:14 74471
12-0E1 was 3t19ern4ropane
NO-GIL 130
2-6 1
OMII14 IIS 14 W12-1
Dbr d4cremetheme
NO ug1L 30
021 1
OMIO1418'14 124.4E-1
12-01ka-L-um-IE1)81
NO ug1L 10
OI7 f
OII141814 14
;WV-46M
OlpFomo Ih*ns
NO LIQA. 10.0
Oif t
0""14111:14 r4-Ps3
1 � OkNern6enzane
NO u91 1.o
0.30 I
am 11:4 15:14 0550.1
1A-0ICMDFOh.ntenl
N0u91L 1.0
033 1
OM" 416.14 10E.415.7
bars-t,l.pivlrloro-7 hulena
NO ugIL f00
t.0 1
0610111416:14 11O-W4
Ij-OkJedoerhane
NO u9.t 5.0
0.32 1
1IW1"141::,4 15.34.3
1 ,24 kmwOefhAnv
NO uplL 10
012 1
06l01114 7E.14 107.0E-2
1,1-pkhlaroerhene
NO u91L i0
0-56 1
IIMI0141a 14 75.3"
*.12 OICT001a.in-
NO ugA, 50
011 1
0601114 13'14 1WN-2
REPORT OF LA130RATORY ANALYSIS
REPORT OF LABORATORY ANALYSIS
T1.. report rM m1 C. r.rMrarwU...- t* ru.
7Na..penr.t -1 r r.,Md-m. r.eaprn
".
M.ra14 e..i --m f P4q A-"c.+ 6.. mb. a.
Page 4 of 24
Data 06/10/7014 07 62 AM
rster.l eM m ean.FM a1 Pau AW,, r S.- W Pape 5 .124

P... AnWVy 1 4erv1c.a, Ire. P_ Anery4eer lervrpr, Ine.
/! .'f'a//L@I�R31J�ffCr7�� ��•r�• 3­0D CB tyffC�� W%-,A.. S. W Iw
rwnw..r.. Nc M75 n�.d.rr.a.. Nc 2607e
1 ...w+:.s.. L1nA>81sgm2 1 -+�•�• I70A1e+o-w6c
ANALYTICAL RESULTS
ANALYTICAL RESULTS
propel: SLORRY BLANKS
pfOjecl: SDRRY BLANKS
Pece F4opd NO. 92203466
Pep. p141,0M4.: 97203406
6anpie: E9
Lob IO: 4220344600I Coleded: 0W2W1414:20 Recalyed: OW2W 14 15 20 Maw. NYler
8rnpie: FS
Lab 10: 42"61"4002 CO4eea4d: OWNit414:10
Reealyad0629O14 M:20 WIN. VW1af
Reporl
RepDn
Pndewler.
R"um
Lkeb Urd
MDL
OF Pfepred
Mew" CAS NO. Qlel
pm.".04di
119e111e Lpds
UwA
MOL OF
ptooxed An41yte6 GAS Na. Quit
624E *3V Law Le t L4ndtM
Ms1 IcW Mehod' EPA. MO
Solo Icp Groan dwAl.f
AM*f 1cel Melhed: EPA 601 o Pldpelatlnn
McOmd: EPA3010
rrem-l-2-pweoraeriene
NO u0it-
5 0
0.40
1
D4101114 Is 14 la640 5
An4meny
IUD u94
60
5.0 1
OW3114 1230 O&W14 20.59 7440-36-0
1.2-plrJ4a opopene
NO ug4-
1.0
0.27
1
D&OWA to 14 74-67-5
A..nlc
NO ug1L
100
6.0 1
OM301412.30 060414 20.59 7440-36.2
1,3 Ox"WWOP6ee
NO ug&
1.0
0.2E
1
BMIO$4 11114 142.21-0
awwk
NO Lv&
lDO
50 l
06MV1412-20 06104n4 2O:5p 7440-3�3
01.-13-ggeorapnpese
NoV%-L
1.0
0.13
1
064111411:14 t0061-014
0er06um
NDL101L
10
S.0 1
06431141230 010"1420:50 744041.7
LLArd 1,3-EWAWuprpp."
ND u%&
1.0
0.24
1
0641114 11.14 10061-0 4
Cd.l[e
ND vQ&
1 ❑
to t
OLOOV1412:30 0N04114 20:50 7440-43-9
E1hy1ban wm
NO ugk
1.0
0.10
1
0641114 ?$.14 100.41.4
ChromlueL
ND uVL
1110
6A 1
0510111412:10 06N4f1420:59 7440-07-3
2-HeAAnone
ND ugti
60.0
0.46
1
05101114 16 14 561-76-E
Cebem
ND ug1L
10 ❑
50 1
0643114 12:30 0WMN 20:5 , 7440164
Iodamelhene
NO uglL
10.0
0.12
1
09A1114 16 14 74-aa-4
Copper
NO uglL
400
50 1
0643114 12 30 DsM411420:59 7440-a0-6
"oft"Gludrlde
IA VIOL
1.0
0.97
1
061010416:14 73-09-2
t-nd
NO uyL
10D
50 1
MI)IF141230 DS4 11420!0 743942-1
44LMtlry1-2yenlelwne JAM UK)
NO ug,L
100
0.13
1
O6d0111416;14 10&10.$
N AW
NO uglL
501p
5.0 1
OMW14 12:30 0610411420:59 7440-02-0
Sly—
NO LWA
10
0.215
1
MMI04 16:14 10042-5
SeleNuni
NO ugA
1(]*
10.0 1
06MV14 12.30 OW04M420M 776249.2
11.1,2 Te4.("W" i.ne
NO 4&
5.0
0.31
1
0"V14 1AA4 830.204
%N.,
NO uWL
1D D
5.0 1
OM3014 12:30 ANW1420. 11 7440-n4
11,2,2-Te4e41b1oa1rane
NO LI&
3.0
0.40
1
od41114 14;14 ?"-5
Thxlwm
ND L.0,
55
5.4 1
061031141230 Odtl471420:51P 7440-26-0
TnYeprlAMeeCLare
NO.0&
1.0
0.4E
1
0"In4111:14 127.1E-4
7p.
NO uWL
100
5.0 1
ow3n41.2 so 6616u1420:so 7446-315
TPlu.ne
NO ugk
1.0
025
1
01911141d14 10940.3
VAne11-m
ND -,,1
25 0
SA 1
O61OW 4 62:30 0=404 20-39 744042-2
1.1.1-Tddlbrom11e1u
NO vok
10
0.40
1
o"1114 Is 14 71.66.E
721rc
ND uOL
100
10.E T
OWW1412:30 Owl 1420-59 7440-06-6
1.1-2 TrlcAwruan.nn
ND ug&
10
029
1
0610MI418.14 794)0.5
Trkhlor-11111 a
NO ugA
1.0
047
1
0 *111416.14 19-01-0
7470 Marcuty
A-Plucel Mad,ud.
EPA 7470 Pr ep nr e0wr Method: EPA 74 TO
TI KnI«olMwrom.n4ne
NO ug1L
10
020
1
0d011141014 75-SM
Mercury
40 uA
020
0 10 1
OSX 114 $1145 0"W14 10:06 14WO-41
1,2,3-TLtd'daoprppmn
ND U94
1.0
0.41
1
QMII14 14-14 95,t0.4
Wyl Acetate
ND ugA
50.0
0-35
1
OMI114 10 14 IWD5-4
62iO M9V Low Lord L-dR11
Andylled Me41od.
EPA OM0
Vnyl dllerld.
ND uglL
1.0
0-62
1
06*111414'14 75-M-4
Acahe
NO uIIL
1W
100 1
OMU141120 074M-1
kyir (Tpial)
NO 'OIL
5-0
0.6E
1
0"1114 is 14 1330-20-7
A.V1l Llrile
NO VIA
200
1.0 t
D61DIr1A 16.30 10,143-1
SufraOama
Ben rem
ND ug1L
1.0
0.25 t
0041f14 1430 7143.2
4-&on�o4uorobAnrena IS)
too %
70-130
1
o"ll141E-14 450-00-4
Blomnchlwarne6Larle
ND VIOL
7.0
a 11
74. 1-5
t-2-pkNueedune d4 i91
102 %
70-110
1
OMI11414:14 1706"?,o
&emodwaroniee+ane
NO volL
1.0
0.1E 1
0610111418:30 M27-4
TPluene-de ISj
97 %
70-130
1
OMI114 14-14 2037 26-5
&pmnwrm
ND ulll
30
0.7E 1
❑W1014 I830 75-25,2
46MZD 8.01d. YW W
AndyV..I Method'
SM 450O-52D
B&pmemepAna
NO u04
1041
029 1
❑"m4 16:30 74-03-9
7-BuVA . )ME K)
HD QU&
100
0.96 1
06101114 16:30 74-03.3
S0ede
NO VIOL
IWO
log
1
061041 14 1325 $4496.25,4
Carbon deul4de
ND LO&
100
1.2 1
OMI014 19:30 75-1"
A 600C NE CVAnlde, Total
Aneryllcel Metllod SM45DD-CN-E
Carbon lev..W.Wr
NO n/OL
1.0
025 1
oft 01416:30 86 •i"
Cnla Obennne
NO u61L
1.A
021 1
oem1114 1em 1A6-9o-7
%+emne
NO L.giL
too
so
1
0e10W141t:3t VA2-5
Cheroethao.
NO W&
10.0
0.54 1
0C41041530 754103
Chlorolornl
NO Llyl
5.0
0.14 1
06/01014 16-30 5745-3
Chwomvlane
NO ug&
1.0
0.11 1
o"104 111:" 14-07.3
1.2-p6romo-3-daornpropene
NO LKA
13 0
2.5 1
o"W4 Is 30 96.12.E
130 rt chlarometn
NO 41L
1.0
071 1
06f01114 10:39 17441-1
12 4Dpremoe6Lene(EDBI
NO ugA
1.0
O.27 1
0641f1416:10 1D6-93-4
pWrmllwnethane
NO "A
100
0.21 1
06101114 16:30 74.95.3
1-2.OkNoroCancana
NO uok
5.0
0.10 1
0610014 16:30 95-50.1
1,440K"mebenzona
NO ug&
1.0
0.13 1
061011141E-30 106-44F7
hem-1,4 -0Ipuoro-2-hNene
NO "OL
l00
1.0 1
OMI114 19-30 00-57-6
11-DkA4ethane
NO uWL
5.0
0-32 1
o"V14 1630 75-34-3
1,2-D6chlor0a1nene
ND UA
t 0
012 t
CWII14 S6 30 107-WZ
1,1 Drcl,lnrnemer,.
NO VOL
6.0
a so t
0"IJI& la'30 7s-354
ae-1.z DinLlorOetlLerLe
NO ug&
5.0
0.19 1
QW?l14 to 10 150,5W2
REPORT OF LABORATORY
ANALYSIS
REPORT OF LABORATORY ANALYSIS
rlr. t.p In rota raPvarw..vwq h4.
TNr
r.pon ne1 not l» r.prpd". euo.ntn
u
DM. MI Ono 14 07 52 AM
-u14�e
wnn.n ­ or
9e w+.il4ceL S.r,r... �
FA9e 6 at 24
43t1e 061tnolA 07 52 AM
.. hour th. --, - ­ W P.ce
1 .4- Sdm . Lrc Pape 7 W 24

ceArlalytical r
Prgect: 541RRY 6LANK5
Pace Pride.... MD3466
SenlpW F6
fia. melon
S240 MSV Low Level LAhdf41
}rMe-1,2-D W Iloroeth-
1,2-OICMpvprvpArH
,,3-D:onlvrvpropene
ue-, ]-pkM.opropene
irerw 1-] O� W oropap.r.a
Eery6en
2-Hex•
IvdamMr..n
Movhylene U4-4a
4 Merm 2 Pe04n.Ie (MIRK)
Styrene
t ,1,2-7etro W d oeFane
1.12.2•T.tr.dad -1h eve
Tehachto ethane
Sopron
} ,1, l7rk41I.peQI4rH
S -1 ,2 Frkhl.aelherle
Trkhlw oe91en4
Tfkh10ra9airinlalllM.
13,�TrichlorodK9pana
Y►qt ecel.Ie
Vtrry1 diorlde
xvlm (T." )
srrr.vger.e
4 •Brnmoliwrbllenxene (S)
1 2�JkNor oelhehe-0{ 151
Tnhrene•ua )Sy
ANALYTICAL RESULTS
Loh ID: 11=301002
i.pllodedW29,14 14 30
Report
R..A uwk
UvA
Mm
OF
ArWylleel Malhod: EPA SIM
NO u134
5.0
0-49
+
NO up4
1 0
0.21
f
NO up4
10
a28
1
NO 144
1.0
0.11
1
NO u04
1 0
0.20
1
NO ug4
I 0
0.3c
1
ND ugh
500
Q 44
1
NO ug1L
Ion
0.32
,
NO ug.'L
10
0 97
f
ND ugA
100
0 33
1
NO rr1DR
1.0
0 26
1
NO up4
6p
033
,
NO uv&
3 D
O.A.
1
NO "A
1 0
046
1
NO rrp4
1.0
0.2E
i
ND I4
ryg4
1.0
04a
I
Nil u
1.0
0-29
I
NO uglL
1.0
O.A7
i
NO •rgrL
10
020
I
NO u0K
I D
041
1
NO udk
500
0.35
I
ND ua.1
1 D
662
1
NO Lgk
50
066
1
100 %
7413o
I
IQD %
70-130
1
97 %
70.130
1
Pee. AneIym., aemul. Irw.
9NQ krle.r IW. Sl.re 1�
IruaMr..e. NC led is
I7Q1 piPr9097
0 Sr2&141520 1A.tro MN.
Prepwocl Analyzed CAS NO. Cluel
0641114 f0:30 15640.5
MU14 16:30 18-07 5
116r01 r14 IS 30 142-Z"
06411f41e:w 10061-01 5
Mille 1630 low -02-6
MI1141630 16a-414
06A111116:30 59,•7"
06Nx1 r1416,3{I TA-06.4
oft 111416:30 75.09-2
0"IM 10:30 IW 10,1
06101114 16:30 100.42.E
06M1r1416.SD 63Q-266
6yG1r1416:30 7P34-5
Q"1714 fa:30 127.$114
OSMII14 fe:lo 10b66.3
0114111
4,630 71-653
067911t41S:30 79-00•S
GtIM 1A 1e:30 79-0i-6
061pN14 16.30 75.69 a
06AI1T4 fe:30 9&164
0610104 19 N I❑e-95-4
0619111
4 f6 a4 7,Q1-4
Q641114 $a 30 1330-20.7
m"I'$ 1a:30 10-00-4
0RN1114 fa 3D 1r06Q-07i5
Q6101114 1a 30 203r-765
REPORT OF LAB0RATORYANALYSIB
• �•, •.rort ,n.� rr.1 w ..neeu<.d ..c.y, n pll.
Dole: ml Wall 14 07.62 A11 wrern4 vre x.Iirn mnwu or Poor AnNr•cn s.n.rar. In< Page 6 0124
27cekulytica)'
ANALYTICAL RESULTS
P Qject. SURRY BLANKS
Pm" Proy.al No.: 9228315E
TB Le6ID: e2203466003 Coe
Rep.
p4+emaiere ReWN LMdta Litm
pied M3V Lew Lrvel L.ndlpl
AneMe 1 M.11"O EPA020
At.lene
NO *& 1
AayWnArlle
NO ug& 2
6• 74-
RD 1p4
O-Zd,Inr6m M6n.
NO ug1L
lk ckhlaro wh-
NO uyL
61omabrm
NO 14&
&Pmvmc Tene
NO ug7L U
6ulanwrefMel[)
ND Loot 1
CAncon dl wMda
NO u91L
Carton Ieha ♦eorl[I.
ND wg4
Chbrohenxene
HID ug4
ChIm.mana
ND up,l 11
Chloroknn
NO ugA, I
Chloromanene
NO 0g4
1,20hr9mo•3 thwe oop. ne
NO up4 t
Dlhrumochiervmelh.ne
HD va
420bromoalhene(E DO)
ND ug4
plgrarnom.mnne
NO ug4 11
i,2-0kNwohanx.ne
ND u04 I
1,4-Dld4wohen xene
ND ugll
Ye1N-1,4-Dl0kKro 2hul.ne
ND ug4 i
1, 1.Okhlavelhene
ND up4 !
1 �-Dk#,amdIJQne
NO W&
1,1-Dlddere 0-.
NO 444 ,
ele-1,2-plui4oroelhene
ND ug4
Srena•13-i7lcMaonMane
ND uo4 !
1,x-01(Allalvpnpene
NO ug4
1,3-OkNwww ne
NO Valk.
Ne.1,3blahlo.W.p.n.
NO uy4
Y.rI►,,3.dchloropropene
NO up4
EITg6.neena
NO ug4-
2-Heranclre
ND o114 5f
Ipdpmeel"
40 ug4 11
Mamylene CNarlde
HO UA
a.Aleylyl-2-penknple;08K)
ND u94 1
sty-
NO uA
. 2•Tatradlimmit1611e
ND ug4
1,1,2,2-Tetroo&-k-aaFAno
ND u94.
Tetrachh10e01ene
NO .WL I
Tnplene
ND ug4
1.1,1-T,khhxaeerene
ND wk
,.1.2-Trlchromi,M no
ND o9'L
Trkhlwoemene
ND ug& 1
TI KhMoauroomrlmane
RD up4 1
12,3 Tnchlwoleopone
NO PO4
Vw ec41ele
ND UWL RI
rclM' OY
MDL
PA- An41ylK.1 e4ryrg4, M.,
9np] rtu.yl AM. SrN rW
I hrw,.w.. Nt; Nara
11M)et5-iCA2
B114 w w 144cehyd OWSIT4 Is 20 Maknl. NMk1
OF
Prepared Anelrxed CAS Nn C] ml
.0 i
0610171416:4e 67-01.1
9 f
OW0411416:46 107.13.1
is r
0610 171a IS.46 T1�S-2
17 r
0&❑11141a:49 T4-97-6
la I
mm 1,14,e:40 751,
26 1
06M 11410:44 7&2S4
89 ,
06r017,41a:46 74d3-6
36 1
04V011f4 ,e:4a 7e-93-3
2 I
0"11f4 IS'e6 16.1 S•0
IS 1
Mt114 14.46 56-23•5
23 I
0a10 ir14 1 e:46 I D& W7
S4 1
OsMI11413.0 764)0.3
14 7
06,a111416A6 61�5
11 I
OfY011141646 7'44l•3
5 ,
16
OBr❑i114 46 W12-e
iT 1
061017141a'46 1244b1
i7 1
06/01114 1114E I M-13-4
d1 I
06101714 ,646 74-96-3
S0 1
❑6r0171a 16:46 M-y0-1
S3 1
0"1114 16:40 I OS-a6-7
.0 1
11"1114 164a I10-67.6
SI 1
'"N141e:A6 75.D43
12 1
D6101r111646 107-0&2
16 1
06N101416:45 7535.4
19 1
06N1114 16:46 156.6C2
10 1
o601114 is 16a404
17 1
Q6m111410.45 76-07-5
76 1
06701r14 16t46 142.284
13 1
D" 1"10051-01-S
m I
06761114116:4e 11061-02-6
10 1
Dy017141648
IB 1
OdV11111646 591163
$2 +
0"HM 11145 7a-0S•4
i7 ,
D610111416:46 7699-2
13 ,
06a1H1416!46 toe-f D.I
6S 1
06 ..4, 16441 1DD-42-5
13 1
Oe 4111416*6 M204
IC 1
Oe101114 WAS 70-34.5
16 1
Q6r0111418:46 127.16A
Nl +
0"111416:46 106-66-3
la 1
06A111► 1646 li-5&6
!9 1
ON010,4 IS'46 74-QO-5
I] 1
6yO V141e-46 Tp.p1-6
ru +
116101n4 u:4e 75-e9J
H r
06r01l4 14:46 96 16.4
is 1
06101114 190 10e-0s-4
REPORT OF LABORATORY A NALYSI S
*lr. r-W w0 rot <r I.P�. wr.0 M ee.
Dec.'M10r2014o7:$zAM a.w..e..w.- 10P4 Herne s«re.,.It
Ppe 9 or 24

f4 n. "Vvp l lwwwvs, Inc F4c. •> Vllwl 6NVIi4a, In.-
3C8Rfl3±j1hC81 I1W01w1 ■- Ss, 100 peal n. , A.r s•n. too
...�.a. I* 4. "C 26016 ace anatvt�cal _1� .. RC 2>r116
I>wr7evbm •_ A; r ItwwIc75M 4
V
ANALYTMAL RESULTS
P"Ct SORRY BLANKS
Paca Prapcc No.. limu66
6rndm: TB
Lab 10: II=366060
C46rct.d. OSr29f 14 00 00 ROalred OY29r44 I620 M6eef: ftW
Report
Priam left
R/aldll twe
Llmt
IAOL DF
Prep41.4 An*sad CAS No Oual
6260 M5V Low L... I L..Mll
AnaryOc.l MatlbdEPA6260
vww VOW me
NO uA
1.0
062 1
OMIJ14 16:46 75-01-4
Xyl.rl. f iutal}
ND ulrl
70
066 1
0"1114 la:" 1330-20-7
Swmgxf..
4 Brolne6l.oro6enzena(5)
Pp %
20 150
1
061011%4 46,46 460W064
1,2-0klrlwu.d..r.a-34(S}
t04 %
70.130
t
OWIA416-46 i706407-0
inbrer.e de lSt
97 %
70.100
1
0610104 11:46 20 7-25.5
OVA LITY CONTROL DATA
pf*d BURRY BUNKS
Pace ",ul No. 92200466
0C Smith MERP4alI /N.1yu/ Wood EPA 74%
OC B11c11 M661ed: EPA 7470 M4fyNr D46o"w 747a Mercury
Aa6nda[.d L{6 SIIIp141. 92200466001, 92200466002
METHOD BUNK 1212169 Mew: ftbw
A.soodaHd LaA S6mp166: 9Qi0Y166001- 92200466002
Btbnk R6pwmg
Parameter Un6r R.6WI Lw6 Ar"zod 0wMn6
Mwclry Lrp4 NO 020 0MV1416M
LABORATORY CONTROL SAMPLE! 1212170
80ke LCS LC8 % Ran
Pal.—w LIME Cerro. R..A %Kra Limo Q-911—
M"W" UWL 2.5 2.7 109 on-120
MATRIX SPIKE 6 MATRIX SPIKE OUPLICATE' 1212171 1212172
MS MSO
922001n(110 Bp►. Spwa MS M80 MS MOO %R6c Mrs
PNWWW UNl. 0. 01 Ca4K. Cato Roam Ra6uk -ARoe: %R6e Uwft RPD RPD 0.&1
mw-ry -yL 0t4J 25 2.6 2.7 2.8 101 100 75425 11 25
r.«w1. r....aw o. a.. a.n ..... x. M.1. xeM,rw ey x. -u.+r.-..wn...�.n, _ _...,. a.,��� .r• �. w..«.w m w r�er a... ».�.
REPORT OF LABORATORY ANALYSIS REPORT OF LABORATORY ANALYSIS
TN., vW N.1.1 b. r.pmdurad-..ypl n M1{I, iMrlapen NY nnlG M1pr.dicM. .supin hY.
Dais' 06110A014 07 62 AM .n. 11.-ft. maraM.I Aa.. "Iplic.i a.nc.. Mc Peg. 10.12{ D.I.: 06/102014 07.52 AM ......r .y .Man omrarrvl P4u Nwllcal 5..war K P.yr 11 cI 24

PaCekulytiral�
F4oleel: SURRY BLANKS
Peae Proleci NP . 02203460
oC Batch MpRP115101
oC Batch Memod: EPA3010
Aeevdeled G8 Samphs 9220346WO1, 92203466002
METHOO BLANC 1217519
AueodeNd LW SIMISS 97203466001, 822034660M
Pnem*ly
Uplle
R..hmorry
uyrL
A.eer4c
uplL
Bark.m
twL
B"yN.en
YyL
Ckdr*"
uyL
Ch-rNNm
uyL
C t.11
uyL
Copper
uyL
Lead
uyL
Nk kel
uyL
9ekNwm
v91L
SweI
vyL
ThPkklm
uyL
7-
uyL
VannNum
uyL
Zna
uyl
9apO Xlre.yAW huh ��
�]c.+e� �5n. ) /. /
YM.nYr..H.. NC 2a976
'' l7LL I'U i�1��L�f
11HIN7S➢OW
�.yr-asam.
QUALITY CONTROL DATA
OuALITY CONTROL DATA
pral4ct M RRY BLANKS
Pa" Pt*d No. 92203466
Anayels Melhad: EPA 5010
Ans"m Onaom 6010 MET NC 1711kmAwwlm
Meme:V",
841k RepwWo
Reeud LMNI AnYyeed Oval6ere
NO
6.0 060401419.28
NO
1a.0 06AMO1411178
NO
100 001M11419:28
NO
10 06mvi41926
No
10 oemw411028
NO
10 0 OM4114 1911
NO
10 0 06/04114 19R6
NO
100 081MI14 10:28
NO
10 0 06/04711 19.a
1,
S0 0 081041" 18.29
NO
100 06AMM4112a
NO
111N4 OS11a 1826 :
NO
55 OM41fa 18211
NO
100 OWNI1419:2k
NO
25.0 Qlm 419:24
NO
70.0 O&MQIa 19:28
IARORAT DRY CONTROL SAMPLE:
1212590
Spike
LCS
LCS
%Roc
Pkreme*r
t1P11e
Curer.
R"A
%Am
Um4 OWeaken
Ara.mvn7
uyL
Soo
497
99
60.120
Am.—
uBL
500
477
95
60-170
Ban um
ue:
uyL
NO
G2
500
1
60.120
y in.
vyL
S00
479
96
60.120
C.Ormum
uyL
Soo
410
➢6
M-120
Ch,."� mm
1.yL
500
e86
97
$0.120
Coh.e
uyL
70o
895
99
60.120
Coppal
uprL
SM
494
99
80.120
Leed
uyL
S00
497
➢9
60-129
mckM
up�L
500
47a
96
60-120
SelenlPm
uyL
S00
495
99
60.120
Sorel
uyL
250
242
97
80'120
%Alkuhr
uglL
Soo
469
94
M-120
Tn
uyL
500
496
9➢
W 120
V.—A.-
uyL
Soo
4"
46
60.120
21nt
uyL
Soo
478
98
80-120
.n•n..p. —..P"...r —.14hr.n.•1mo:.rr.wn..em.Mw..n rY.r.r i.xlh P-...Ye Y m. h01. m. .1.
REPORT OF LABORATORY ANALYSIS
TM. 1.PPn NM W1 M Mwoourn. N ftj w 6A.
DO. O IOM1407'52AM .l mmilt- ear-e.0 at Pace Arahtcok 6en+ran,+nr
P.b An1176eal SmtNl. 4a6.
4870161 m Ara am% 100
.anN.M. NC 789r6
!1W Ie7"m
MATRM SPIKE 8 MATRIX SPIKE OUPUCATE: 1212521
MS
92243337001 5pik.
Peremehrr UNte Reauh Cone
M$D
69W.
Comma
1212522
MS
RemAt
MSO
RnWI
MS
%Ree
MSD
%Rae
%Res
Um16r
MITI
RPO RPO 0"
AMLk ony
uyL
NO
50o
500
474
483
95
97
75-175
2
25 T
Ameme
uyL
NO
500
500
454
"a
91
94
76.125
3
25
Bw4um
"IL
22.5.1
500
$00
4➢0
511
so
96
75-125
a
25
perylkum
uyL
NO
500
Soo
454
4?1
91
94
75.125
4
25
C6dm9llm
uyL
NP
500
SOO
ass
467
➢1
91
75.121
2
2S
Chrclrwm
uyL
NO
SOO
500
462
470
92
05
75.125
3
2.5
CoBR
uyL
NO
S00
500
464
am
93
9671.
125
3
25
Cavan
uyL
NO
500
500
475
489
85
96
7rr176
1
26
L4ed
uyL
NO
500
No
465
47a
91
N
1&1128
3
a
Nlokel
uyL
NO
600
590
450
a67
81
90
76.25
3
25
Sv "—
uyL
NO
500
590
467
4711
83
96
75.12S
2
75
J34—
uyL
NO
259
250
229
235
01
94
75.125
3
25
Thallw.m
uyL
NO
506
500
449
459
60
92
75.125
3
25
Tm
uyL
NO
500
am
461
401
93
98
76.125
3
2S
W-dl11m
uyL
NO
500
540
45,
412
01
94
'75.125
3
2S
?l-
uyL
NO
500
500
457
467
91
93
M125
2
25
n..�r�. o,...,rnm 1N•.....• .� in. ��.. ��..w.�.d Ir u�r-u.n.' .,.�.,,,.....,. r,«..n...�n.n r..�. wnmN4.. w...iew of w....ri
REPORT OF LABORATORY ANALYSIS
Tnr-Port*el-I.. -o.od a ..r.pl n kL
Ape 12 of 24 Dala' 0501 U2014 01 5: AM w.T w. —am cr P— r 14cel 5.rnaa w
Pepe t 3 PI 24

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i
. aceAnalytical
wnMnN.. NC 2m7B
r ••• r.�
(7wlars9ae2
QUALITY CONTROL DATA
Protect. BURRY BLANKS
Pspm Prood No. 92203465
OC sm r. MSVr2704$
W,aoymle Memod EPA e260
OC Sm1[h MetllvdEPAe260
Malyus Deanlphwl. 8260 MSV Low 1eve11-011
A.mwa.wd Lm Senple. 022034116OU 1. 92203469002- 9220 UGEM3
METH013 BLANK: 1211356 Motu, NAW
Aseeaaled L.b Samples. 92x0t4o96pQ1, 9220346600i, 9j!203466003
Brmnk RepprMty
Pmrmmmler Uall. Ramue UIrA M!.lpc.d
1,+,1,x-Te7.pJorampr.ne
udL
NO
5.0 On$1141323
s,t.1•Trkhtwoothwe
uyL
ND
I.0 O6rQ1n41323
7,722•Taeaddornatllme
uyL
MD
1.0 001011141323
1,1,2-TadKrK.amm�m
01
ND
1.0 013r0 tha 1323
1,1-pddWftlh:M
NO
ow
5.0 0111413:23
1•i-DWwcalnne
uyL
%D
5.0 06411141123
1,2,3-Tdcwwapropmne
u9rL
ND
1.0 D W11141123
12.Oihrvmo-]-d,loroprop.h!
uptL
NO
13-0 06W10141323
12-011bttlmwerm (EDB)
uQR
ND
1-0 o6mtr141123
1,2�Ictearohenr.nv
uptL
ND
6.0 OW011141323
l,2-Dowwwtn.nm
uylL
NO
1.0 o"V14 Ia23
1.7-fllcNorvprvpanr
ugiL
ND
1.0 0Q1017fi 113]
13-Dldawoprvpene
uyL
ND
1.0 06A 111419T3
1 ,4•DICN Gben2ene
uyL
ND
1.0 o6A11141323
&ow 2-dn. IMPKI
-A
NO
100 06/01H413:23
244exan on.
PyL
ND
50-0 0601 h41123
4•M.lh2POnunme lMISK)
uyL
NO
100 06f010141323
Acelon.
uyL
NO
100 06ro1 h411-23
A�Ylonbxe
uyL
NO
20O 0641M41323
Dories.
U90L
No
10 O Mlri4 1123
Sromodrlorumath-.
uprL
ND
1.0 O&0111411'21
BromodcKbr.rn.inrl6
uyL
NO
1A 0=1141121
Bromvlorm
uyL
NQ
3.0 06N1M41323
Bromumr9,anv
UWL
ND
10.0 o6W irl413:23
Carbon "`LOSJe
uyL
N➢
100 06r01+14 11Z3
Carbon lmad.jvfjde
uyL
MD
1.0 OBm1r1413z
Chleroh. 11
uyL
NO
3.0 OV01141323
cm:0014
-WL
NO
100 O W111413.23
CNnrvl9rm
uyL
ND
SA 05A m41121
Chlvrvm.d,ene
uyL
NO
1.0 0B101r141323
d.-1,2.Oldrkraatuen.
uyL
NO
5.0 06W1r1413T3
pe-1.3DiMloroprvpene
uyL
ND
1.0 0&O1h41923
D6rvmochloromeNene
uyL
ND
3.0 OWII1413"23
DAromomelhene
uyL
NO
10-0 NMI1323
EmN4rnrene
uyL
No
" "0+nf 11"
udwnethmrra
uyL
ND
10-0 06W11141323
Me knrleiie CbmnJa
uyL
ND
1.0 MR11y14 1129
Styrare
uyL
NO
10 05W1441123
T.ueHuoroOthMe
uyL
ND
A 06101r14l3123
Tolu.ne
uyL
NO
1-0 DEVOUT 413:23
buns,.2•pp.lurveonone
uyL
No
5.0 0N011'141322
oustre
ay�4x pry.na0 tin Wr Iwo Pan M yW. Nsuiae ay nn-uiw.• cawnn aa..a,..,n•.n .tnnN. rwlla.rrMMw re an rpn, el in. rrrwr
I �aceAnalytrcal
I
QUALITY CONTROL DATA
ArOpcl' SLIRRY BLANKS
Pan Props+ No.: 22203466
METHOO BLAW 1211 MO M.m.
Asaadelad Leh Semplva: 92203466001, 92203466002, 92203466003
BWrk
Parameter Untie R..WI
VybW
R.pwler9
L11nl1 An*nd Olro m6w.
u7arrme-lolm5,ff--
uuyyi
NO
1.0 501h4 323
0n.-
OuaiccNhalmcwNaap-n2reo-pne n
yL
No
160 06,41123
Td,Nn
D
0 0=10141323
NO
1) 0W4123
111L
vr,o ecersle
uyL
NO
6r0
too 010417Y3
i4r14 chl.00.
uyL
NO
1.0 oeN1h41373
Ayoens (Total)
uyL
NO
5.0 06A 1r14 13:23
1 2-oochlpro.th.-CA ($)
%
070.130
06OU14 13:21
4-Bromvnuwobenren. (s)
%
101
7G 130 0610N14 1321
Telu.ne-d6(6)
%
96
70.130 09A11141323
P.- An.1rk[ml arrvlp., N[.
9epo Kxx.y A.v 9�C! iCa
rlanyrwN.. }IL' .lure
!]p4le]55�2
LABORATORY CONTROL SAMPLE:
Par.mater
111113"
t1n1h
Spoke
Carty.
LCS
RaelAt
LCS
% Ra[
% Roc
Loma OuaLAen
1,1,1,2-706.4iNr.elhmne
uyL
50
5B.3
110
70.110
1,1.1•TdHtlwoed,snv
uyL
50
53.5
107
7413Q
1,1,2.2-Teknphlometlwe
uyL
50
53.1
107
7b 130
1,12-TricjA r ath"
uyL
50
54.1
100
70-t10
1,14CNJWG Lone
uyL
5o
►94
99
m130
t,t•pcMwoe6yene
uyL
50
49.4
99
70-132
12,3-TrI[MIXopro94ne
ayL
50
53-2
ice
10-130
1,2.01brume•3•ckYubproprne
uyL
50
46A
97
10.130
12-0rbrvmeepune SEDBJ
uyL
50
54 6
109
74130
1,2d7Ichlwota nm
uyL
90
63.6
197
70.13n
12.OIcMwomOwmr
uyL
30
54.e
110
70439
1,2-DkLlvmogrnpmne
uyL
50
51.7
103
70.130
1.3•Didrlvropropma
uyL
50
SSA
106
7M1130
I,4-DICMlwobancOna
uyL
50
52.6
105
70.130
2•Butomae (MEN
uyL
100
99.31
69
701-145
2�iermonr
uWL
too
09.7
lad
70-144
4-Memyl•2penlanvne (MIBK)
uyL
T00
99.11
99
70.540
Acelone
uyL
100
95.51
96
30-115
"c ,ltllor
uyL
250
250
$00
70.143
Ben2vne
uyL
5o
55.1
110
70.130
&omuctilorvme9une
uyL
50
544
log
70.130
&omprlldtloiemrttll.rN
uyL
So
56.4
113
70-130
Bramalorm
uyL
5o
531
1p6
To- 130
&vmvmem...
uyL
50
54 2
106
S4-130
Carbon gmuMd6
OWL
50
$09J
102
76.131
Carbon lepachlwide
up4
50
56 9
114
10-132
Chlarobenrene
uyL
50
5! 4
T
70-I30
01 oelhane
uyL
SO
109
62
094-134
GN.tolarm
uyL
50
123
105
70-130
Chlarwne""
uyL
50
fa 5
97
64.130
R.Mhp-W- a6ro.m... In.ir.nih mar br a. -unni rmnnn ••[r.l tyre.m •a.n.,..... W.. WW 0. rlehl.1. mru
REPORT OF LABORATORY ANALYSIS REPORT OF LABORATORY ANALYSIS
rive P.""l N r.em . rmr.P!n k41. TFN,ipon shm9 nor e. NprWu d, aim pi N 6111,
061e' 06t102014 07:52 Ah1 y6mvur ohm •rrnrn-v r W Pau An.ly" So-.- be PaOr 14 or 24 Oate: DW IW054 07:52 AM MO -A 1%wrlMn rornem or Pm[o Ar*WW llo ykn, h,c Pope 1S et 24

l + ,
eawpw..lae..
P ISCI STARRY BLANKS
P.ce P j&d No- pM.3466
LPPORATORY CONTROL SAMPLE'
l21i350
Pw meter
1Jnft
o l,7.O1dlfpe.fheno
uyL
dFt ]-()drirlfopopMie
VL
DlhlPmed+bromed-.P.
up1L
DFr9mOmeDl.he
uyL
Efnvfhen7en.
UWL
IrNomelhMn
uyL
Mnlhylene Chloride
uyL
Styrene
--yL
Teb.mlrnnem--vc
rrryL
Toluene
-IyL
hen.-1,2 N.ht flh-
uWL
hmtw.l,3 cmnlwpL,l.-1-ef-.
,TOIL
WWAu 1.4-otdNvw-2-hul.m.
uyL
TflChI. th-e
uofL
TrlchlwoMmrcmeth.ne
uyL
Vinyl dlfunom
�orL
Xv*" loml)
4WL
1.2-Okhlw Pe6-.ne.14 I3)
x
1.&nrnnllUmaMnzsn. [Sy
%
Towne -de Is1
36
QUALITY CONTROL DATA
9111*4
Cora
50
50
50
S0
so
100
50
so
$o
S0
50
50
50
so
50
00
i0
Ij0
LOS
R.Wt
40.9
SS.6
51.3
51.4
S0.0
120
524
U.;7 94.
51.6
50.5
$5.4
56.7J
56.6
46.2
106
57.1
$ 62
LOS
%Re
100
t11
103
109
100
12D
105
l01,
109
103
101
H1
113
I}4
95
106
114
102
99
102
100
v e. Anelene.l Serv-p �. -n.. . •+rni Are -CP.
mmnbm . NC 21W7
1rM pY�90e[
%Rec
UWMk Oumbllm
70-131
76-116
10-130
70-1711
70-I30
49-Ia0
61130
10-130
10-130
70-130
10-130
70132
10-141
70.130
62.133
64s67
1 130
70-130
70 130
70-130
70 130
MATRIX SPIKE SAMPLE
$211566
9Z20341150T1
$pike
MS
MS
%Roc
P.I.In4t.r
L1e1LL
Re4U11
Cone.
R..uk
%Re
LIN" 01uea6en
1.1,;,2-TeOechlwxm.ne
uyL
ND
50
967
113
70.130M0
1,1, 1-T4chremem4n.
-
50
64 7
129
70.1"
1,1,2,2-TenehlwnelP
,WI.NO
uyL
NO
So
502
1111
70.136
1,1,2-111rl✓Pm 91-
UWL
NO
SD
61 2
1U
70.13a
1,1�Itlevrvell-ene
uyL
NO
5D
Sfl.7
H7
70-130
1,1OkM9rnen-ebe
uarL
NO
50
61.3
173
70-166
1.3,}Tr4 i+foroProp.rie
upfL
ND
$0
569
Ila
70-f30
1,2-OQw %3-040raWa
uyL
NO
50
49.1
99
70-I30
1,24)&rwrwe 6-4n a fE DOI
uyL
NO
50
599
120
70-130
1�-0Icleavhen:ene
uyL
NO
50
59.6
119
70.134
1,2101cldnr tWv
UWL
NO
50
640
126
70430
T,j-DicMwnPrnlr.ne
uyL
NO
50
S0.5
I19
70-130
1,3•dduw-•Pr or.lte
uyL
ND
So
57 a
116
70-530
%4 01e16e---Senm-
UWL
NO
50
59 5
110
70.530
2-Bllle-mne IMEKI
uyL
NO
I00
965J
99
70-130
2-Inermlw-.
qw.
NO
A00
110
110
70-130
4.Melhyl-Z�enlenwfc I M15K}
t19A
I40
Io0
IN
199
70-530
Ac.wne
uyL
NO
100
105
103
10-f 30
Avylenib.r
ZL
NO
2S0
264
114
1. J.
Benzene
-WL
NO
50
64.a
I30
70-146
A--, w.Nw.n , N. e... M ti.n twin l d WMmN WMemn..ne-W. .rl.mrw-Ir m..nW%M rWh of e.n
REPORT OF LABORATORY ANALYSIS
Tl.. Tepee -Tonle. nern-c.-l. anon w ew.
CmI. 060107201407:52 AM WW-A W rrnllM aan4e1 of P-A.WyepN Gw-.W
P40e 16 el 24
.' .PaceAna)Wicai
QUALITY CONTROL DATA
P.- Anoyl l 94nrl .. Ine-
"MKK yAw 5i m0
rW.M•.w.. NL iWM
17P41675sOP7
Maj.". StARRY BLANKS
Pecs Pol.d No. 92203466
MATRIX SPIKE SAMPLE-
12t1566
92203456011
spike
us
Lis
% R.c
Perem.in
float
Roth
c-
R-Al
%Rec
LIm4 quMFen
BrrXn9chlblvmeth4n►
UprL
ND
50
62A
12S
10.}30
B+9modid-krom.nt.ne
U01L
NO
50
044
129
70.130
Bromolvlm
Mat
NO
50
55.a
112
79-1,o
Bromvfnvlh.ne
uyL
NO
50
05
131
70.130 M0
Cerhbn Q1U11de
UWL
NO
50
60.51
T21
70-In
Cvbm letred+exrde
"U&
NA
50
006
134
70•t30 M0
Chlwo6e4ren.
UWL
NO
60
59.2
$16
70-146
CMw-item
OWL
NO
So
44 4
oilM130
Chlvrtlfvrm
uyL
ND
50
613
123
70-130
CNory th-
uyL
NO
50
MA
$10
700.136
v.-12.illchlwvemene
uprL
ND
is
507
119
70-13a
c1.-1-} Dlchlwvprvp.ne
UyL
N0
50
1119
124
70->30
DtibrumUcFeu eme".
uyL
NO
50
560
112
70. 130
D,tirv.mrn6lti
UA
NO
50
61.5
123
70130
Ethylhe"md
uyL
ND
50
57.0
114
70.130
1vdd111 h-.
UWL
NO
100
$49
149
70-430 MO
Melhyt4no CNInr1Ue
01.
NO
50
61.4
123
70-130
slpen.
uyL
NO
5a
01.3
Ii3
70-l30
Tenmem&oemen.
nyL
ND
%
63.6
127
70-130
Toluene
UWL
ND
S0
00.3
521
70.}65
troro• 1.2. Ofchloro m6� ere
uyL
NO
50
614
123
70.130
lrn o.1,3-Dfdda awapene
Up'L
ND
50
61.9
124
70-130
gene-1,4-Dehl0.4bnene
uyL
NO
50
61 NJ
f24
70.130
TAchlwoelhw*
uyL
ND
56
sa.5
133
69-151
T-jcfilervlfu.-th.ne
yL
NO
50
U.1
26
10.130
acetme
N100
U
21
0vnp
0
Wo chlonee
Uyl
ND
50
71 7
143
70.130 MO
1,2-Dichrweeth.-A4 I51
%
1on
TO 130
448ywm-Suvrn6er - ISI
%
102
To- I
Toluene•em IS}
%
Tag
70.130
SAA}PLE DUPLICATE' 1211567
9220MG410t2
Dip Mo.
Perem w
Un6a
Ra4Ull
Re1NR I" RFD Qgm"A"
1,7.1240 ,-dAm oflh mne
UWL
NO
NO
I,I,1-TAdevfo.5rene
OWL
ND
ND
I,1$.2•Tetww-velhmne
uyL
NO
NO
I,I.2-TrkN%r9.Ihwe
uyL
NO
ND
I,}•Dldflw&mhmhe
UyL
NO
N0
1,1.p1d11wv.lhene
uyL
NO
NO
1,2, 34"WofeproprrN
01.
NO
ND
12-0IWamv-3 d0weprvpene
up4
ND
No
I,2-0wtbmbam.n4(MM
uyL
NO
40
I, 2•DK31f9ro6enzene
uyL
NO
NO
2-0lchlornem.ne
%pL
NO
NO
b.w4 erwen.-4 f.-.- toy •1,1..1
REPORT OF LABORATORYANALYSIS
the r.ppil l .- m- p..eP d- a 0 a W
Dale 0611 Or2014 07 52 AM r ea-t the ..ftY pe -1 d P.o. Ae V" se. uU
P.U. - T tt 24

Pau Ar Vdhsal■srriniN WK-
Pau.nryy AJ aawfc I.C.
WWKr A- 0NNf0o
.,�. • _ tw
aceRnafyticaf
Hv w*ms NC 2907a
/ aceArralwical
Hh ww . Rc M70
.nr wn
I71Y1y17Si0G2
new;acnrG. wn
004016,RM
QUALITY CONTROL DATA
QUALITY CONTROL DATA
PWp&CL SURRY BLANKS
Pro2ecL SURRY BLANKS
Para Pr**d No.: 92203405
Pace Proppt Np: 92203469
SIMPLE DUPLICATE 1211507
tlC 9atch WETA1341
Analyela Melhpd SM 4$"-S2D
022034Sa012
Dup Mal
CC Bauh Mamod. SM 4500-52D
Arwlyaia Deaalpaen 4500S20 Sulhwe Wryer
PremeGr
Uhye
Ralull
Reeuy RPD RPD
4uaYAem
Araodwed Lab SanV": 0220346BaM1
I2-NchtwoWupane
u1yL
ND
NO
13-Dida.. ropene
uWL
HD
ND
METHOD BLANK: 1213017
Maui.: Maier
1,4 i.NdAwobanrelle
IWL
ND
ND
Aaancteled Lab rwnpins'. =0345e0o1
2-Bwanone 1MEKj
uVL
NO
ND
014ny Rep-"
2-Nexenone
ugrL
ND
ND
Prameler unds
RaeuO UnA AnNyad Ow1ANa
4•Mell'o. 2•Pehlenafa(MISK)
1p1L
NO
ND
Aoelune
�6VL
NO
NO
SWM1de uyL
ND 1000 oo"141325
Aujo-K 11e
uWL
NO
NO
El n ehe
UOIL
ND
NO
&unochlorvmelnane
ugtt
ND
No
LABORATORY CONTROL SAMPLE' 12130i5
BrPmodlr7ddameUlarw
u
ND
ND
Sp1Me LCS LCS %Rep
BfolnO[Nm
uyL
W
NU
NO
Par ameW unya
Conn ReeuK KRao LK1Nh Ouulen
Br —duly
ugJL
NO
NO
SW111e uyL
500 5151 103 90�I I
Cale—dNWlde
uyL
ND
NO
Gabon tetlachk ide
uWI-
NO
No
Clwwob-zwe
uyL
ND
NO
MAATRI% SPIKE 6 MATRIX SPIKE DUPLICATE 1213010
1213020
CW—thane
AWL
N9
NO
MS M30
Chk—form
ugR
ND
NO
92703021014
Spike Splye MS MSO MS MSD
%Rao Mu
Chlwro wtr ne
ug+L
NO
NO
Paralheler UNu ReaW1
Cent. Cane. Reau11 Reaull %Rao %Rao
UrNis RPO RPD Ouel
cw 11 Dicnlwmth ane
uWL
ND
NO
^
ae-1,3 DIdrinwpropene
u01L
ND
No
Sulfide uyL NO
Sao Sop 400J 4901 $00 ISO
7"25 0 20
DCfeetetnitavf+iOU+acre
ugl-
NO
ND
p6romomernane
uyL
NO
NO
EULyNmri erw
ugfL
ND
NO
I -Mom""
UWL
NO
NO
Medlylena ChlOnda
uyL
NO
ND
Siywhe
uyL
NO
NO
Tevapldp kh—
uWt-
NO
NO
Tw.ww
uWL
ND
ND
Baru-1,24I.Iduwaune
uyL
NO
ND
10era•1,3-0ldWw prop o*
uyL
NO
ND
+lens-1,4-DWwo-2kulene
uyL
NO
ND
inchlarpef+ena
u11+L
NO
ND
Tnr7yoroAyoromemene
uyL
NO
ND
VAwo omwt
uVL
NO
ND
Vogl snadde
PWL
NO
NO
%yMrw (Telel)
uyL
ND
ND
1-2•plchlp pePrenp•d1(S)
74
103
102
4-&omoauorohenxn+e [Sj
%
9S
100 t
rpwene-a8is}
Be
95 a
Fu.+ui•w.i.d �.. w. y.p.... a—I.yw M.... Wr .. �F.,..i. ­1. p....­ vne. --aav-7auv-oowiw---enx•-rwn.r.- ii. er...ix.. y —ow i..W.
REPORT OF LABORATORY ANALYSlS REPORT OF LABORATORY ANALYSIS
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ndly
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QUALITY CONTROL DATA
Propel: BURRY 91ANKS
Pen Propel No.. 92203466
OC amen. VIOETNIO24S
Anartde MNhod SM 45CFCN-E
QC Sabi, Metlwd SM 45WME
k.Nst, oe„alptlon: 4WWAE Cyenlda, Tow
Aawciated Ls6 Sample: 9220349®DO1
METF+OGBLANK: t2lWil Marto: YiIM
Associated LAb Somptae 922004114401
alu* FloWinq
PWAMOMF Lin" Rerull U-0 Anslyoetl ❑e4101en
Cy,"de u91L NO 10.9 9RM20141I:27
LABORATORY CONTROL SAMPLE 12TS479
perm—W Units
Cyorade UA
Spike LCS LCS % Roc
Cane. Rnult %Hte Lp+Nu OusNNet9
100 1134 103 e0.1i0
MATRIX $WE 13 h1ATRIR SPIRE DUPLICATE: 1216421
1216422
MS
MSD
92203J65006 Spltre
"a,
M6
NISD MIS MW %Roc Mal
Px *T*r [tall R44101 Cone.
Cane.
R NmAl
RmRM %Roc %Roc Unft RPO RPO Oual
cyrAdo uwL NO too
100
04-1
92.5 92 9d 75-125 2 20
MATRIX SPIKE A MAT RIII $PIKE DUPLICATE 1216421 1216424
MS MSD
92204279003 Spke Soat MS MSO MS MSO %Rae ,Aar
PrameM Llrela Read Cane. Cow. ft-mm Rearm! %list %Rae Urnik ROD RPD qu4i
CyWvclo USA NO *0 100 907 "Il o6 66 75.125 1 20
RyyW Area.xlM an +N, DODO Ora le aN rnw xrne.+.e oe ue umN ewwn Dreier wh..e.e Arrnu. inn rr pnr.nhy ro nrrrynr pl w..Fr•in
REPORT OF LABORATORY ANALYSIS
TNa rwO epee nerea n9redaee. a,dpin M.
DAIs: OWtpr2014 07.52 AM .meal Nirm rP eawnt et Pau AnnNeal an.c.a asc.
Pa pe 20 ut 24
a�eAnalytr�ale
! one
f
QUALIFIERS
Pan ArralyeaM ■srvreas, am.
Sew Kavr M+ ewe Im
r nW— e. NC. 2epr9
f n1416M.0m
N*cL SURRY BLANKS
Pea Fr*d No. 92203466
DEFINRION6
Df DAukon Fedot, rl rcpoded, IePreNMte IhR reC[p, tl'Vlled IQ In! rinrNl+rd date dun 10 U+�nge• M aaFFPIa Pr4parellM. Qylllpn O1
the sample 4llgpol, or mpeture centard
ND - Nel Deleeled al or abeye ad}nted repwtlnq LmA
J EaNmelad Cancentra[lon above lie adpnled mAX1od dafaclhn kmX and below me edlualetl repwlMq IX11X
MOL-A4J (s d M em ed Delecibw LOW.
PRL • Pecs RIPn hoi Llnsit
R L - Reporl,np LOM
S - Sumogefe
l,2.OlphenylnydraHne 141270 Noted Anotyle) dec poaea to A4obenjone.
Camlalent Mth EPA gtildellnea, unrourded data ere dapiayed and nave bemused Ie caiariata % rec y and APD vaiun
LC6A - Laboratory Control S.WP. IlDuon.alel
MSLD)- Mem, SplAe 1pupNcalel
DUP - Semple Dup9cAe
RFD • RetatNe Percerd DdiereRce
NC - Net Cerc+Ae6te
SG • Sfta Go, - Omar, urk
U • ln6Celas the wmpaund w % w4yaed Im, but r r dev nod
N-ralree0d"nyrarekre detvr cses and canr.ol be separated mom DX1Mrryternl.4 vNnp Memod A270 Tns fesWt roponml Iw
em;h mna4yle Is a curnbined eoncennallon
Acid pree Ohm may not be ApproprlAle for 2-CNW"thyMrg4 elneF, Wand. and Vinyl chlondo
Pau AnaWoll Is ill aecre0Hv l Contact Yaw Porw PM for the w, en! NMI of scoAd I60 irAm"
TNI The 14ELAC Inatllµle
LABORATORIES
PAS -A Pace AnAlyltal Servitor • A~Ile
PASI.0 Pace Analyllral Sm"Icel • Chadolle
A NALYTE DUAUFIERE
MO Malna spike t#I!O ry W&d )F ntalrrk spl ka dutAlc4te ICcwelY "I outfide layerNrery bM 0 Nnwtk.
REPORT OF LABORATORY ANALYSIS
TN4rape,* WY W� apOdd md.. Wnto.
Dete. DW 10t2014 07 52 AM Maws"w.mae eau Pr pee.A ,wa, fuwcr. iK
Pape 21 o124

aceAndlytica)'
QUALITY CONTROL DATA CRDSS REFERENCE TABLE
v.c. xnryu�n e.rw�.a, Ir.c.
9aou Kxy Rr. SrA f 00
wrw...9.. MC mole
(7o4j imv
Pi*cr
Pace Protep No..
BURRY BLANKS
e2n03466
Anetyllul
Lab i0
Sample 10
OC BetCh M.Ihod
OC fWch Analytical M.ewd
Balch
92243466001
ES
EPA 3010
1APRF116107 EPA 11010
92203466002
FB
EPA 3010
MPRP[10107 EPA 5010
2p714566
1CPr145ae
92203456001
ES
EPA 7470
AIERPOW9 EPA 7470
MERC16449
112203456002
Fe
EPA 7470
MERPIS6e9 EPA 7470
MERCM449
12203466001
EB
EPA 9260
kl5VR7015
92203446007
FB
EPA e26a
MSW2104e
92203468N3
TB
EPA 6260
MSW2700
92203405001
Ell
5m 4600-BID
YYEVr 1341
922o]4a600l
EB
SM 4500-C N-E
YVETAr19245
REPORT OF LABORATORY ANALYSIS
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P.p. 22 of 24
document Nema:
Document Revised. Apfll u 11u1 A
Skm to Condttlon U do Recel ! SCUR
Pago 1 or
DocuN1ant Number,
15sumy Authority
- F-CHR-CS-003-rw.14
Pace HunterBvlNa Quality Olfk6
Client Name:
Courtier: (-1 Fed Ex i1 UP50 USPU ciiom0 mmercm Pace Ott.r_
Custody Seal an CoolerlBox Pmeaant: C] vat �•lQ/Iw Sao A mtatr D yet
L ] no
Packing Material: 0 Bubble Wrap 46unble 9a9a 0 None [] Other
Thermomator Used: IR Run Ti102 1 40 Type of fce: IQ Blua None
'Pj'5r^pWe n Ma. xAang p, <­ hat 1xgu
Temn Cn6metlnn Erin, T11n2- Nn rnrr Linn T4'M4 • Nn r'nrmrlinn
Corrected Cooler Tom Lf 'C
Temp ahovio be aeaka 0waay to a-C
9iologiaal Thous Is Frozen: Yel
Ca mmenu:
oale.ne Inwjla oIp/non e.aminlnp
Clem of Custody Presenl:
v ON* 01rrA
1-
Chaln of cumody Filed Out
Y D1a [INA
2.
Chain of cuslody naun
OHO LIMA
3-
Sam er Home iL S19rmliAre on COC:
6y, nW Ulm
4.
Ss as Arrhred wnhln Hold Time:
Ye. ONe ❑WA
S.
Short "d Time Anal eIe 472hr ;
Oyu Grim
6.
Rush Tum Around Time uaatod;
Ciro Ha O-VA
7.
SuiOcienl VOnlnuS:
Yea Ota LIMA
8.
CdlraCI Cdntalners Used
-Pete C@ntatnan Qmd.
0% DwA
Z, OHo DrWk
9.
Cunudners Inled:
Yw Ono QHtk
to.
Fdlered voliane 1ecalved roc UVeeoived toste
cyn C1Nv 94
11,
Sample Label% match COC.
• Intkades daiefnmaADJAnaI a Momw
w OH9 OWA
12
At —4Akr v. -.4m9 f-w vown Im" Been dla Ya6
All cmot ,& fWHW q pro l.lyaoan are fouie to Aa in
oonOollmw rrhn m E PA oocc msto
VUk ioeram. Mc. 4ad, Wi01to
vp OHe OWA
;3r U.A
yl'aZ
yet ❑no
13.
Sompla dhecked for dechioni-wi ion:
Uv.. ON. .
14.
Hamsdapace In VOA Vtere l �6mm -
❑Y. Jhe DWA
15,
Trip Blank Pre6ent
Trip 014nk Cmloay Seals Present
Pace Trip Blank Loll 4 k Chao ed -
Ely- ON.
Ely- UK. I0
16-
Client NotllleetloN RaaolLacin: FWW oela Fiequneo7 Y I N
Person Conlacled• DimalTi ne:
Commenl9l Reaolullen'
SCURF Review: Wa; 5 lo
WO# : 92203466
SRF Review: � 1 Ogle: 7 Jr .e . r jk
Role: Wh.nwer aura J aMoWaMy Affeding Noah Caroni 6arrlpltan0e �I��� I„II]j + � I.I
9WP%&. a onpy of Ohio term wO ha owl In rh North Cardona WINK I, f
c"AN16"n efhw 11.a out al hour inmost( pr.e.nratlra, put 0f temp, 92203465
ncormd cardaura)
Pape 2] of Z4

4y CHAIN-0E-CUSTODY 1 Analytical Request Document
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