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HomeMy WebLinkAboutWI0400176_W/ CORRECTIVE ACTION UPDATE_20180314BEN 2 USE oN.Y- ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event #: NC DENR I I Environmental Monitoring Division of Waste Management - Solid Waste Reporting Form Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6). Instructions: Prepare one form for each individually monitored unit. Please type or print legibly. Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 28 surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing condition, etc.). Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i). Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646. Solid Waste Monitoring' Data Submittal Information' Name of entity submitting data (laboratory, consultant, facility owner): Municipal Engineering Services Co., PA Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: Jonathan Pfohl Phone: E-mail: jpfohl@mesco.com NC Landfill Rule: Actual sampling dates (e.g., Facility name: Facility Address: Facility Permit # (.0500 or, 1600) October 20-24, 2006) Surry County Closed C&D and 237 Landfill Road 86-02 .1600 December 13-14, 2017 Closed MSW Landfill -Mt. Airy Mt. Airy, NC 27030 Environmental Status: (Check all that apply) Initial/Background Monitoring ® Detection Monitoring ❑X Assessment Monitoring ® Corrective Action of data submitted: (Check all that apply) Groundwater monitoring data from monitoring wells Groundwater monitoring data from private water supply wells ❑X Leachate monitoring data ❑ Surface water monitoring data Methane gas monitoring data Corrective action data (specify) MNA parameters on 7 wells Other(specify) Notification attached? No. No groundwater or surface water standards were exceeded. X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. Certification To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Steven R. Gandy, Ph.D., P.E. Senior Project Manager (919) 772-5393 Facility Re resents a Name (Print) ? , ) Title Signature , Date P.O. BOX 97, Garner, NC 27529 Facility Representative Address C-0281 NC PE Firm License Number (if applicable effective May 1, 2009) Revised 6/2009 (Area Code) Telephone Number Affix NC Licensed/ Professional Geologist Seal %0 H I Cq 11 fJ*, ®F ESS,, � s C 3'020 ® (P dree®o��G, ��/NEED••' � ®®w Semi -Annual Water Quality Monitoring Report with Corrective Action Update Prepared for Surry County Closed C&D and Closed MSWLF, Mt. Airy Mt. Airy, North Carolina December 2017 Permit Number: 86-02 MESCO Project Number: G17024.0 Municipal Engineering Services f Compasry, PA. Garner; NC 1 Boone, NC P.O. Box 97 Municipal Engineering Services Company, P.A Gamer, NC 27529 Gamer and Boone, North Carolina License No. C-0281 TABLE OF CONTENTS SECTION Introduction ........................................ Background........................................... Sampling Procedures............ Field Parameter Data Laboratory Results .................... Quality Control Samples Groundwater Samples......... Surface Water Samples..... Corrective Action Undati 1 2 2 2 3 3 4 5 5 MNA Analysis (AOCs Northern, Southern and MW-11)...................................................................................................................................................................................Page 5 Enhanced Bioremediation via Substrate Injection (AOC Southern and Northern)....................................................................................................Page 5 MW-I I AOC Investigations................................................................................................................................................................................................................................................................................Page 6 Groundwaterand Surface Water Characterization..........................................................................................................................................................................................................Page 6 Findings..................................................................................................................................................................................................................................................................................................................................................Page 7 Closing....................................................................................................................................................................................................................................................................................................................................................Page 8 Topographic Map with Site Location................................................................. Single Event Potentiometric Map of Uppermost Aquifer FIGURES 1 2 Total Cumulative VOC Concentrations Pre/Post Injection Comparison........................................................................................................................._Figure 1 Total Cumulative VOC Concentrations Time Series Graphs/Table........................................................................................................................................_Figure 2 TABLES Groundwater Monitoring Well Construction Table....................................................................................................................................................................................................Table 1 FieldObservations of Monitoring Locations.........................................................................................................................................................................................................................Table 2 FieldParameter Data Summary ................................................................................................................................................................................................................................................................. Table 3 Samplingand Analysis Summary ............................................................................................................................................................................................................................................................Table 4 Groundwaterand QC Sample Detections..................................................................................................................................................................................................................................Table 5 SurfaceWater Sample Detections............................................................................................................................................................................................................................................................Table 6 MNAParameter Data Summary .................................................................................................................................................................................................................................................................Table 7 Hydrologic Properties at Monitoring Well Locations.............................................................................................................................................................................................Table 8 APPENDICIES Laboratory Analysis Report and Chains of Custody................................................................................................................................................................................_Appendix A FieldSampling Parameter Data Sheet(s).......................................................................................................................................................................................................................Appendix B Municipal Engineering Services Company, P.A. March 14, 2018 Ms. laclynne Drummond Solid Waste Section (SWS) 2090 US 70 Highway Swannanoa, NC 28778 Re: Semi -Annual Water Quality Monitoring Report with Corrective Action Update Surry County Closed C&D and Closed MSWLF, Mount Airy Permit No. 86-02 MESCO Project No. G 17025.0 Event Date(s): December 13-14, 2017 Dear Ms, Drummond: Introduction On behalf of Surry County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this Semi - Annual Water Quality Report with Corrective Action Update for the winter 2017 event performed at the Surry County closed construction and demolition (C&D) and closed municipal solid waste landfill (MSWLF)-Mount Airy. NCDENR Solid Waste Rules 15A NCAC 13B.1632 requires that Surry County provide this report to the NC Solid Waste Section (SWS) on a semi-annual basis. This report documents the quality of the ground and surface waters during this monitoring event performed on December 13-14, 2017. Laboratory analytical results indicate volatile organic compounds (VOCs) in concentrations in excess of SWSL and 2L Standards continue to persist in samples collected from five wells that monitor the uppermost aquifer. The surface water samples collected from the local discharge feature remain unimpacted. Corrective action to remediate VOCs in groundwater is ongoing within all three areas of concern (AOC) as defined in the Corrective Action Plan (CAP) and improvement has been observed with updated information presented herein. Background The Surry County closed C&❑ and MSWLF, permit 486-02, is located at 237 Landfill Road in Mt. Airy North Carolina. The site location topographic map is depicted in the attached Sheet 1. Prior to becoming a C&D landfill the site operated as a MSW unlined sanitary landfill that consisted of two units. The northern unit was closed prior to October 1991. The southern unit is comprised of two contiguous portions. The first part stopped receiving waste 68 5hipwash Drive + Garner, NC 27529 • ph: 919-772-5393 b fx: 919-772-1176 a www.mesco.com P.O. Box 349 + Boone, NC 28607 • ph: 828-262-1767 d fx: 828-265-2601 8 www.mesco.com prior to October 1991 and the second part stopped receiving waste prior to January 1, 1999. Both portions of the southern unit were properly closed with a low permeability cohesive cap per the Transition Plan. The top portion of the southern unit served as an exclusive C&D landfill until prior to June 1, 2008 at which time it was properly closed with another cohesive cap in accordance with the Closure Plan. For continuity, both the northern and the southern units are monitored and reported together. Water quality at this facility has been monitored at least semi-annually since 1989 with historical data available since 1994. This event was performed in accordance with the NC SWS rules/regulations as promulgated in 15A NCAC 13B and as a condition of the post -closure portion of the permit to operate and memorandums this report contains sampling procedures, field and laboratory results, groundwater and surface water characterization, and findings. This report also contains a table of detections compared to Standards, field data results table, groundwater flow directions/rates table, field observations of the monitoring network table, a potentiometric map of the uppermost aquifer, histograms of historical detections, statistical trend analysis, laboratory analytical reports with chains -of - custody (C-O-C) and quality assurance/quality control data. Sampling Procedures The water quality monitoring program, current as of this event date, includes sampling locations and parameters as outlined in the Water Quality Sampling and Analysis Plan (SAP) (DIN:18936) dated April 30, 2013 and approved by the SWS (DIN: 18938) on May 10, 2013. Monitoring locations are shown on the enclosed potentiometric map (Sheet 2). MESCO personnel collected water samples from 20 downgradient groundwater monitoring wells (MW- 3R, MW-4, MW-6 through MW-11, MW-125, MW-12D, MW-13 through MW-23), one background well (MW-1), four surface water locations (SW-1, SW-2, SW-3 and SW-4), and the water supply well (SCALEHOUSE) that serves the facility. Data from two surface water points (SWN-1 and SWN-2) designated in the SAP for the adjacent Subtitle D Lined MSWLF are presented because this local discharge feature is shared by both permits. Quality control measures implemented during this event included the quantification of potential artifact contaminants via equipment (EB) and field (FB) blanks. Samples were not analyzed from the six injection wells (IW-1), (IW-2/MW-2), (IW- 3/MW-3RS), (IW-4/MW-4), (IW-5/MW-5) and (IW-6/MW-8) since they are exempt due to the presence of injectant residue which would yield unrepresentative water quality results. A summary of the construction of the water monitoring wells is presented on Table 1. The function and integrity of all monitoring locations were visually evaluated as documented on Table 2. The depth to water in each well was electronically gaged prior to purging to quantify the static water level elevation. Low -flow pumping methodology or bailing was utilized to adequately purge the wells to a minimum of three times the volume of standing water in the well or until dry. Surface water samples were collected from Stoney Creek discharge feature at previously designated locations. During well purging and surface water sample collection the required field parameters were recorded. The samples were then placed into laboratory -prepared, pre -preserved containers via a new disposable polyethylene bailer. Samples were collected, kept on ice, and transported to a NC -certified laboratory under proper C-O-C protocols within the specified hold times for each analysis. Field Parameter Data Stabilized field parameters were recorded during purging which included depth to water, pH, dissolved oxygen (DO), temperature, oxidation reduction potential (ORP), specific conductance and turbidity. The field parameter data 2 indicates the monitored groundwater is slightly acidic, reducing conditions, with relatively low specific conductance which is generally consistent relative to each other and congruent with data historically reported. Field parameter data recorded at the surface water locations were neutral in regard to pH and low specific conductance which is consistent with uncontaminated water. A summary of the field parameter data is presented in Table 3 and the field sampling data sheet is enclosed in Appendix B. Laboratory Results Pace Analytical Laboratory (PACE) of Huntersville and Asheville, NC performed the laboratory analysis of groundwater and surface water samples for the total recoverable constituents listed in 40 CFR Appendix I. A sampling and analysis table summarizing the locations, constituents, and methods is presented on Table 4. Laboratory results and C-O-Cs are contained in Appendix A. Water samples were analyzed to the laboratory -established Method Detection Limits (MDL), which are at or below the current Solid Waste Section Limit (SWSL). Table 5 summarizes constituents detected in groundwater and QC samples that attain or were above the current SWSL, SWS adopted Groundwater Protection Standards (GWP), North Carolina Groundwater Standards (2L) or the Maximum Contaminant Level (MCL) commonly referenced as the Federal "Drinking Water Standard". Table 6 lists the constituents detected in surface water and QC samples compared to the SWSL, the North Carolina Surface Water Standards (2B) for a Class C water -body and the MCL. Quality Control Samples No constituents were detected in either of the quality control blanks (EB, FB). Groundwater Samples Five metals were detected above the NC 2L/GWP Standard in samples collected from 11 wells including the background well (MW-1) as summarized in the following table. Metals Detected Above 2L/GWP Standards in Groundwater Cd Cr Co Tl Va SWSL 1 10 10 5.5 25 2L/GWP STD. 2 10 1 0.28 0.3 MW-1 (BG Well) 3 11.1 0.15 j MW-6 76.7 0.59 j MW-7 51.9 MW-9 187 0.37 j AM-11 8.8 J MW-13 15.6 MW-16 491 0.5 j MW-17 73.7 AM-20 12.4 0.42 j MW-22 3.2 j MW-23 2.3 5.7 j Concentrations in ug/L j = "j-qualified" since below the SWSL thus value is considered an estimate 3 Eight VOCs were detected above the NC 2L Standard in samples collected from five wells as summarized in the following table. VOCs Detected Above 2L Standards in Groundwater 1,1-DCA 1,4-DCB Benzene 1,2-DCA 1,2-DCP PCE TCE VC SWSL 5 1 1 1 1 1 1 1 2L STD. 6 6 1 0.4 0.6 0.7 3 0.03 MW-9 1.9 17.1 MW-11 1.2 MW-14 0.88 j MW-15 9.9 3.1 1.9 MW-16 15.7 1.4 1.7 1.5 4.1 Concentrations in ug/L. j = 'j-qualified" since below the SWSL thus value is considered an estimate The majority of the monitoring locations that were found to contain VOCs included a mixture of dissolved phase aromatic hydrocarbons and chlorinated aliphatic hydrocarbons. The only constituent which originated from an anthropogenic source in levels above the EPA established maximum contaminant levels (MCLs) primary "Drinking Water Standards" was vinyl chloride in samples MW-9 and MW-16. A site map depicting the concentrations and estimated horizontal extent of VOCs that exceeded the 2L Standard during this event is presented on Sheet 2. The on -site water supply well (SCALEHOUSE) continues to lack detections in excecdance of current groundwater or drinking water Standards. Surface Water Samples Contaminants were not detected in any of the surface water samples above any established NC 213 Surface Water Standards. Corrective Action Update Groundwater remediation continues to be implemented per the approved Corrective Action Plan (CAP) at the three designated areas of concern (AOC) (Northern, Southern and MW-11). A Corrective Action Evaluation Report (CAER) (DIN: 19361) was submitted on May 1, 2013 which demonstrated that the plumes continue to decrease and was approved by the the SWS on July 24, 2013 (DIN:19366). A historical summary of corrective actions performed to date are briefly presented in the following sections. MNAAnalysis (AOCs Northern, Southern and MW-11) Semi-annual MNA monitoring of a subset of 12 wells for the full suite of SWS recommended parameters was initiated on May 18, 2010 and performed for four consecutive semi-annual events to establish a baseline. A revised SAP prescribing 7 wells with various targeted MNA constituents was approved by the SWS and initiated during an event performed in May 2013. MNA monitoring was performed during this event for the parameters and frequency as listed in the current SAP. MNA parameters quantified during this event included CO2, turbidity, DO and ORR MNA parameters are presented on Table 7. 4 Enhanced Bioremediation via Substrate Injection (AOC Southern and Northern) Per the SWS approved Corrective Action Plan enhanced bioremediation via substrate and tracer injection was initiated in the Southern and Northern AOCs in accordance with requirements outlined in the Injection Well Permit Application and Well Permit No. WI0400176 (5/6/11) in an effort to reduce low level aliphatic and aromatic chlorinated hydrocarbons in groundwater to below the 2L Standards. An edible oil substate (EOS)-water emulsion with sodium bromide tracer was injected into four wells (IW-1, IW-2, IW-3 and IW-5) on November 2-3, 2011. Similar substrates were injected into monitoring wells MW-4/IW-4 and MW-8/IW-6 on October 24-25, 2012. Details of the injection events are provided in the Injection Event Record dated November 4, 2011 and January 10, 2013. As directed in the UIC Injection Well Permit renewed on April 15, 2013 semi-annual post -injection water quality monitoring of wells located downgradient of viable injection points (MW-3R, MW-7, MW-9, MW-12S, MW-13, MW-14, MW-15, MW-16, MW-17, MW-18, MW-19, MW-20, MW-21, MW-22, MW-23) and upgradient background well MW-1 was also performed in conjunction with this semi-annual event. Total VOC concentrations reported during this event were lower at all locations when compared to the respective moving averages of the five events preceding injection in the selected wells downgradient of the injection points (Figure 1). Evaluation of injection wells (IW-1, IW-2, IW-3, IW-4, IW-5, IW-6) continues to indicate that a considerable amount of white highly turbid (>1,000 NTU) viscous residual organic substrate and its byproducts remain in each of these wells rendering them unsuitable for representative water quality analysis. The viscosity of the water in the injection wells during this May 2014 event precludes sample collection as either a bailer will not descend or the check valve fails. IW-1 was verified to not be a viable injection well as less than 3 gallons of substrate was able to be injected into the low permeable fractured bedrock and injectant levels have remained above static conditions for over a year. For all intents and purposes IW-1 injection did not occur nor will be possible in the future. MW-11 AOC Investigations The CAP designated MW-11 as an area of concern due to detections of VOCs detected in exceedance of 2L Standards. MW-11 is located within the compliance boundary near the northern property line which is hydraulically upgradient of the closed northern landfill. The northern landfill closed before October 1991 which was before adoption of NC Section .1600 rules that address assessment and corrective action. VOCs have historically been detected in excess of the 2L Standard at MW-11 which include a mixture of aromatics (fuel hydrocarbons) and chlorinated hydocarbons (solvents). Over the past 4 years (8 semi-annual events) the only constituent detected in excess of 2L Standard and SWSL was 1,2-dichloropropane. The CAP prescribed MNA and enhanced biodegredation to remediate MW-I I AOC. MNA has been performed continuously semiannually at MW-11 the past 6 years. Enhanced biodegredation has not been initiated at MW-II AOC since hydrogeologic conditions relative to the source and property boundaries preclude it as an effective technique. MW-11 is positioned hydraulically upgradient of the source and is within the review boundary. A well was attempted to be installed at the property line 110 feet north of MW-11 on January 26, 2015 to delineate the extent of contamination. The potentiometric head at B-11R was expected to be at 25 feet (1132 ft amsl) but the boring encountered very competent rock at 9 ft and remained dry to 55 ft. (1102 ft amsl) for over 48 hours so was abandoned. 5 Groundwater and Surface Water Characterization A potentiometric map constructed from water elevations taken from the uppermost aquifer which consists of both saprolite and the hydraulically connected upper portion of the fractured bedrock system is enclosed as Sheet 2. Groundwater flow directions and velocity rates were calculated through modified Darcy's equation as shown on Table 8. Consistent with previous events the groundwater apparently flows in a general southeasterly direction towards the tributaries of the Ararat River. The calculated average linear velocity of groundwater indicates an approximate average of 817 ft/yr in the wells screened in regolith and 323 ft/yr in the wells screened in the bedrock. The consistent disparity in flow rates between wells is indicative of heterogeneous geologic conditions and/or a product of the limitations of the linear velocity equation when applied to anisotropic conditions which are characteristic of the geology of the Piedmont. Streams located within the facility boundaries were observed to be of moderate volume and flow with low turbidity. Findings The inorganic detections are believed to be a product of erosion of natural deposits and not an anthropogenic source. An ASD which provides technical site specific facts and site specific analytical data including evaluations of interwell (background), intrawell (baseline), metals in leachate, dissolved compared to total metals and a discussion that substantiating evidence that the metals are not anthropogenic was not approved by the SWS. A revised time -line and workplan dated January 25, 2018 (DIN:28728) was approved by the on January 30, 2018 (DIN: 28729). Turbidity and metal analysis is planned to be performed from a set of approved upgradient backgound wells over the next 2 years with results submitted within routine semi-annual water quality monitoring reports. An ASD addendum for metals is planned to be submitted in early 2020. Turbidity of background sample MW-1 was ND (<0.5 NTU) which is below the SWS recommended 10 NTU, therefore this data may be used an a future ASD-Addendum to statistically derive site -specific Standards. The on -site supply well and the surface water points remain unimpacted as indicated by the lack of detections in excess of the applicable Standards. The on -site supply well is not considered potable thus bottled water is provided for consumption and "Non -Potable Water" warning signs were observed. One or more Appendix I VOC(s) continue to be detected in quantifiable levels above the 2L Standard in samples collected from the uppermost aquifer at five locations (MW-9, MW-11, MW-14, MW-15 and MW-16). All VOC concentrations remain within their own respective historically identified range. Qualitative evaluation of VOC concentrations indicate a decreasing trend over time and distance from the landfill. During this event total cumulative VOC concentrations at all locations decreased compared to their respective five event averages preceding corrective action. (Figure 2). Results of statistical temporal trend analysis, using Sen's Slope Estimator at a 95% confidence level, compared to when corrective action began 7 years ago indicate that none of the individual well's cumulative VOC concentrations have increased except for MW-9. The Southern AOC and cumulative site -wide VOC levels continue to exhibit a decreasing trend. The area of the uppermost aquifer beyond the compliance boundary containing quantifiable concentrations of VOCs in exceedance of the 2L Standard during this event is estimated at 0.0 acres in the Northern AOC, 0.0 acres in the MW-11 AOC and 5.5 acres in the Southern AOC for a total facility wide area of 5.5 acres (Sheet 2). This is an 6 estimated 3 1 % retraction of facility -wide plume area (from 8 acres to 5.5 acres) compared to when corrective action was initiated 7 years ago. Evaluation of the most current water quality data continues to support assertions drawn in previous reports. Corrective action will continue except enhanced biodegradation will not occur at AOC MW-11 as was planned. A few VOCs persist in the upper portion of the aquifer but concentrations are decreasing over time and distance away from the landfill. The local discharge features which are all located within the property boundaries remain unimpacted. Data continues to indicate that the plumes within each AOC have stabilized and/or decreasing and there is adequate evidence that groundwater is naturally attenuating. Closing Water quality monitoring and corrective action is planned to continue in May 2018. If you have any questions regarding this report, please contact us at (919) 772-5393 or by email at jpfohl(2mesco.com. Sincerely, 'AL ENGINEERING SERVICES CO., P.A. Specialist Enclosures cc: Mr. Dennis Bledsoe Surry County F' Steven R. Gandy, . D, P.E. Senior Project Manger 7 Sheets Topographic Map with Site Location Surry County Landfill, Mt. Airy fl 237 Landfill Road Mount Airy, NC 28621 Lat: 36-26-30.065 Long:-80-34-15.314 Northing:983356.18 Easting:1537885.48 0 Surry Co Property Line O Closed Unlined C&D Landfill O Closed Unlined Sanitary Landfill O Active Lined MSW Landfill SHEET 1 2,37 LANDFILL ROAD 0WNED BY JDNNN Y COX IW-6 1044.44 MW-9 [� Benzene.1.9u9ri MW-9 Vmyi Chloride- 17.1 ugll 1 060.1 1 MW-11 MW-11 1128,38 1,2.DCP-1.2-w SCALEHOUSE (FACILITY NON -POTABLE WATER SUPPLY WELL) `7�rJ 1 r,1,t � 1kS an ,��_� -- --- i ���*�� ♦�l-- -- i - � f t-ate -_ ,� I RECYCLE AREA ■ '........� . AID rlousE �� �` 1 , yl f� I ii ,l ACTIVE J ri r+ i LCID �. - '' + BEFORE i'.■. - � i! 1 r it i I D L.F GLp5E 9 1991 M5 OrTo�ER ■ ;- , II t 1 ■ M W-20 1062.18 ■ SW-2 ---- - : - 'y*4. 0 m m a av _ MW■7 1060.59 + +' r' Il +r l 10 t. +,+I+, �401 it DASW - 1 } 1 M1� MW-S 1044.85 All r 1 A 'IL; I'r1 1. .I'r IJ 1 I} 1 I 1 1 lie 11, ■ 1 1 1 . L I r i l l ll 1111 # 1 t l r ti l +r r r Irlr -■ 14 i 4 it I + 1 + . 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I'll I r! 1 I '1 ■ + + j I { 1 + I' .. � � � -� { I I { I + I r '•� - f CLOSED C&D OVER CLOSED MSW STOPPED RECEIVING C&D BEFORE JUNE 1, 20 liilr ' / •`; `` # l •� r+ + j f �� ;- JI r + 1 ti 1 I. STOPPED RECEIVING MSW BYJANUARY 1, 1999 ACTIVE GCCS 1 1 �. 1 ti ■ 1, + I I I ! ,`'- .r , r I l+ '�' +11 ti.�' `. ■'� 1 1 + II { 11+k �'y �._ �_.' I;1,1 + I+ 1 ,,. " Iil+r,rr.I1 �," ! _ 1 1+1r,+ 11i` {kti.�'- _Yrr, •�,-.�. ,l rr r+r 1tiL., �� ■ _ ^ 1 1 I + I t I 11{�ti. ` F Fr' - �1+I 11 ■ 11 1 f l r l l y a �,�_ If r # .. -�-+• r 'rf rfl, I-_ r-. r -_ fi 027.05* r.. -12 p IW-2 1�- BMW-125 r 'F 1028.93 1012.08 4 ----v� - - ■ 973.11 i -z --- �► r 81.213 - ` 9 IW-5 SW-1 -- + ;� ■'./� 1 IW-4 •' - 988.05 mm moo low -22 947-36 14 1 r 935.53 _ 1 yrJ ` .1�rrl' , *�ii ■ �.f f IS r�r~. - .-••! 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I1'`�I tll ' 1,,� F- I y 1 r MW-6R �,..�• mil'"' MW-8 GRAPHIC 45❑ 0 225 SCALE 450 ( IN' FEET ) O WN ED B Y SURR Y COUN TY 958.62 NOW OR FORMERLY OWNED BY SHA WNA SUMMERS MW-14 MW-14 PCE - 0.615 0) ugrl 976.70 MW-15 Mw-16 1022.45 TCE - 3.1 ugll 1.1-DIcHoroelhane - 9.90 u00 r Vinyl Chloride - 1.9 uo LEGEND r { - - - EXISTING TOPOGRAPHIC CONTOURS = _ = = = EXISI TING ROADS i ES TIMA TED WASTE LIMITS UNLINED MS W &IOR C&D --- . _ ----- LINER LIMITS OF SUBI TLE D LINED MSWLF (MONITORED SEPERA TEL Y) ma -EXTENT OF COHESIVE CLAY CL DSURE UPON CLOSED M S W AND C&D PROPERTY LINE EXTRAPOLATED FROM SURVEY AND GIS n■■■■■■ii■ COMPLIANCE BOUNDARY (250' FROM EOW/50' FROM PROPERTY LINE) -1090 - EOUIPO TEN TIAL UPPERMOST GROUNDWATER CONTOURS STREAM/CREEK/RIVER 00 WATER SUPPLY WELL (FACILITY CONSIDERS IT NON -POTABLE) SW-3 44 SURFACE WATER MONITORING POINT MW-10 MONI TORING WELL hilt-2 INJECTION WELL (NOT SAMPLED DURING THIS EVENT) SEDIMEN T BA SIN EXTENT OF VOC(s) DETECTED ABOVE SWSL & 2L STANDARD BEYOND COMPLIANCE BOUNDARY Groundwater Levels & VOCs Detected Above 2L Standards December 13. 2017 AREA OF CONCERN per CAP WELL ID TOP OF CASING ELEVATION DEPTH TO WATER WATER ELEVATION BENZENE 1,2-DCP POE TCE 1,2-DCA 1,1-DCA VCM 1,4-DCB AREA OF 2L EXCEEDANCES BEYOND COMPLIANCE BOUNDARY (FTAMSL) (FTBTOC) (FTAMSL) (UgIL) (UgIL) (Ug/L) (UgIL) (Ug1L) (Ug1L) (Ug/L) (UgIL) (ACRES) 15A NCAC 2L Groundwater Quality Standard 1 0.6 0.7 3 0.38 6 0.03 6 BACKGROUN MW-1 1134.35 25.53 1108.82 IW-2 1068.86 39.93 1028.93 Not Sampled Converted to Injection Well Nov_ 2011 MW-3R* 1017.50 42.41 975,09 IW-3 1020.57 33.61 986.96 Not Sampled Converted to Injection Well Nov. 2011 IW-4 1026.26 38.21 988,05 Not Sampled Converted to Injection Well Oct. 2012 IW-5 1080.18 na NR Not Sampled Converted to Injection We II Nov. 2011 MW-12S 1025.80 13.72 1012.08 MW-12D* 1027.05 0.00 1027.05 MW-13 1008.48 27.19 981.29 SOUTHERN MW-14 1018.80 42.10 976.70 0.880) 5.53 MW-15 1075.96 53.51 1022.45 3.10 9.90 MW-16 999.54 27.52 972.02 1.40 1,70 1.50 4.10 15.70 MW-17 965.43 8.31 957.12 MW-18 983.00 9.89 973.11 MW-19 946.27 9.74 936.53 MW-21 965.36 6.74 958,62 MW-22 953.40 6.62 946,78 MW-23 955.31 7.95 947,36 MW-6 1067.67 22.82 1044.85 NORTHERN MW-7 1073.50 12.91 1060.59 0 IW-6 1088.45 44.01 1044.44 Not Sampled Converted to Injection Well Oct. 2012 MW-9 1094.07 33.96 1060.11 1.90) 17.10 MW-20 1 1082.19 1 20.01 1 1062.18 MVW-11 MW-11 1 1151.80 1 23.42 1 1128.38 1.20 1 1,90 1 4 * = Groundwater elevation not used for contouring (j} = "j" Qualified concentration <SWSL considered an estimate SHEET 2 o z " m z ti NJ D a CID n N r V) DATE BY REV- DESCRIPTION W o QD PCTENTICMETRIC MAP (DEC 73, 207 7) o • A M W1 TH VCCs DETECTED ABOVE 2L S TDs. CLOSED C&D LANDFILL and CLOSED MSWLF FACILITY MT. AIRY, NORTH CAROLINA Municipal Services P.O. BOX 97 GARNER, N.C. 27529 (919) 772-5393 Engineering Company, P.A. P.O. BOX 349 BOONE, N.C. 28607 _ (828) 262-1767 LICENSE NUMBER: C-0281 Figures Figure 1 Total Cumulative VOC Concentrations Pre/Post Injection Comparison October 22, 2009 - December 13, 2017 OO'NNG IENT OF IW-i 4:0T.i CUV-u -a HOC CONCENiRATIOXB} mx selvesG Ph IND a-t CLI +d C H o M aw.n anr•+n •un•+m .ww,e WNING ENT OF NYC(WQ CNWUA YOC CONCENi MOXBJ LU LU • H 111 � _ Z • N • O 4 3.. vX.a anrs vow. i WNING ENT OFN 4 (WQ CNWUA Y CONCENi MOXBJ vX.a anrs vow. O GMIENTOFIWd jT!T CNWLAINE YOC CONCENiRATIOXB� Z - , O N CJ 1 \ •YW.1i WA'-H Average of first Five Corrective Oct May Oct May Oct Action Dec Statistical Trend* 2009 2010 2010 2011 2011 Events 2017 Difference Difference Between Oct Well ID (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (%) 2009-Dec 2017 INJECTION WELL (IW-1) UNSUCCESSFUL INJECTION SO DOWNGRADIENT WELLS NOT SHOWN INJECTION WELL (IW-2) MONITORED DOWNGRADIENT BY MW-12S, MW-13 & MW-18 MW-12S 0.00 0.00 0.00 0.00 5.40 1.08 0.00 -1.08 -100 "No Trend" MW-13 61.00 50.60 74.20 87.30 72.50 69.12 28.91 -40.21 -58 �Downward� MW-18 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 "No Trend" INJECTION WELL (IW-3) MONITORED DOWNGRADIENT BY MW-3R & MW-16 MW-3R 0.00 0.00 1 0.00 0.00 0.00 0.00 0.00 0.00 0 "No Trend" MW-16 1137.90 113.60 135.70 121.20 116.30 124.94 38.41 -86.53 -69 IDownwardl INJECTION WELL (IW-4) MONITORED DOWNGRADIENT BY MW-14, MW-21 & MW-23 MW-14 15.20 15.60 15.60 8.20 17.00 14.32 11.56 -2.76 -19 �Downward� MW-21 52.10 50.70 51.38 39.10 32.41 45.14 17.82 -27.32 -61 . Downward MW-23 4.30 0.00 0.00 0.00 0.00 0.86 0.77 -0.09 -10 "No Trend" INJECTION WELL (IW-5) MONITORED DOWNGRADIENT BY MW-15 & MW-19 MW-15 96.13 63.89 55.00 78.10 64.06 71.44 41.17 -30.27 -42 �Downward� MW-19 0.00 0.00 0.00 0.00 0.00 0.00 1.64 1.64 0 "No Trend" INJECTION WELL (IW-6) NOT SHOWN AS NO WELLS DOWNGRADIENT WITHIN ZONE OF INFLUENCE * = Statistical Trend analysis via Sen's Slope Estimator at a 95% confidence level Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Figure 2 Total Cumulative VOC Concentrations Time Series Graphs/Table October 22, 2009 - December 13, 2017 I Total Cumulative VOC. 8011TW" ROC (TOTAL CIAWLRiIW YOC WNCEMMATRMI5] MORTMERRAOC [fOTILLCOMIILf E VOC C. MCENTRAMD"j Tuw aerri tiaM rxo YwWrut¢ou ar lwrp` ca �YN•r6lIYln1 •NY•t2 JRV.1] •INY.tr N%N .NKr6 MW.r} •y,y.,0 w x m • AOC Well ID Oct 2009 May 2010 Oct 2010 May 2011 Oct 2011 Average of first Five Corrective Action Events Dec 2017 Difference Difference Statistical Trend (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) N Oct 2009 - Dec 2017 Background MW-1 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend IW-2 (MW-2) 105.25 207.00 207.93 159.90 79.10 151.84 79.10 NS NS NS No Trend IW-3 (MW-3RS) 202.90 127.50 127.50 144.00 127.60 145.90 127.60 NS NS NS No Trend MW-3R 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend IW-4 (MW-4) 27.00 24.20 24.20 27.60 23.50 25.30 18.10 NS NS NS No Trend IW-5 (MW-5) 35.00 46.50 46.50 47.40 34.80 42.04 34.80 NS NS NS No Trend MW-12S 0.06 0.00 0.00 0.00 5.40 1.08 0.00 -1.08 -100 No Trend MW-12D 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend MW-13 61.00 50.60 74.20 87.30 72.50 69.12 28.91 -40.21 -58 Downward Southern MW-14 15.20 15.60 15.60 8.20 17.00 14.32 11.56 -2.76 -19 Downward MW-15 96.13 55.00 55.00 78.10 64.06 69.66 41.17 -28.49 -41 Downward MW-16 137.90 113.60 135.70 121.20 116.30 124.94 38.40 -86.54 -69 Downward MW-17 20.34 8.40 8.85 0.00 5.77 8.67 8.48 -0.19 -2 No Trend MW-18 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend MW-19 0.00 0.00 0.00 0.00 0.00 0.00 1.64 1.64 100 No Trend MW-21 52.10 50.70 51.38 39.10 32.41 45.14 17.82 -27.32 -61 Downward MW-22 28.90 23.80 23.80 11.66 5.20 18.67 1.88 -16.79 -90 Downward MW-23 4.30 0.00 0.00 0.00 0.00 0.86 0.77 -0.09 -10 No Trend Combined Total 786.02 722.90 770.66 724.46 583.64 717.54 410.23 -307.31 -43 Downward MW-6 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend MW-7 7.40 9.40 11.20 9.70 8.80 9.30 3.98 -5.32 -57 Downward Northern IW-6 (MW-8) 22.00 23.90 16.00 12.30 12.60 17.36 12.60 NS NS NS No Trend MW-9 23.50 20.40 23.20 25.80 22.90 23.16 46.00 22.84 99 Upward MW-20 0.00 0.00 0.00 0.00 0.00 0.00 0.56 0.56 100 No Trend Combined Total 52.90 53.70 50.40 47.80 44.30 49.82 67.74 17.92 36 No Trend MW-11 MW-11 10.10 6.00 6.00 5.44 23.20 10.15 4.98 -5.17 -51 No Trend SITEWIDE Combined Total 849.02 782.60 827.06 777.70 651.14 777.50 482.95 -294.55 -38 Downward N5 = Not sampled this event so most recent concentration shown and used in calculations " = Statistical trend analysis via Sen's Slope Estimator at a 95% Confidence Level Surry County Closed C&D and Closed MSW LF, Mt. Airy Page 1 of 1 Table Table 1 Groundwater Monitoring Well Construction Table December 13, 2017 Monitoring Well Date Installed Well Diameter Total Well Depth Top of Screen Depth Screen Length Geology of Screened Interval Top of Casing Elevation Ground Elevation Groundwater Elevation Depth to Water Latitude Longitude (inches) (ft bgs) (ft bgs) (ft) (ft amsl) (ft amsl) (ft amsl) (ft btoc) MW-1 11/28/89 2 40 30 10 Clay 1134.35 1133.15 1108.82 25.53 36.439211 -80.568133 IW-2 (was MW-2) 11/28/89 2 70 60 10 Clay 1068.86 1068.36 1028.93 39.93 36.435833 -80.568894 MW-3R 9/27/94 2 101 86 15 Rock 1017.50 1015.00 975.09 42.41 36.434725 -80.571989 IW-3 (was MW-3RS) 5/17/01 2 52 37 15 Rock 1020.57 1018.24 986.96 33.61 36.434656 -80.571858 IW-4 (was MW-4) 8/30/94 2 55.4 40.4 15 Rock 1026.26 1025.06 988.05 38.21 36.434686 -80.569200 IW-5 (was MW-5) 8/27/94 2 63 48 15 Rock 1080.18 1077.78 <1039.50 >40.68 36.434614 -80.570436 MW-6 9/7/94 2 29.7 14.7 15 Rock 1067.67 1065.61 1044.85 22.82 36.437431 -80.571067 MW-7 8/23/94 2 23 8 15 Rock 1073.50 1071.50 1060.59 12.91 36.438439 -80.570722 IW-6 (was MW-8) 8/16/94 2 54 39 15 Rock 1088.45 1086.45 1044.44 44.01 36.439278 -80.570381 MW-9 8/22/94 2 43.8 28.8 15 Rock 1094.07 1092.07 1060.11 33.96 36.439289 -80.571508 MW-11 8/15/94 2 40 25 15 Rock 1151.80 1150.40 1128.38 23.42 36.441589 -80.569558 MW-12S 5/31/01 2 51 11 40 Rock 1025.80 1023.25 1012.08 13.72 36.435942 -80.567972 MW-12D 5/30/01 2 100 90 10 Rock 1027.05 1023.75 >1027.05 0.00 36.435964 -80.567994 MW-13 5/30/06 2 35.78 20.78 15 Saprolite 1008.48 1005.75 981.29 27.19 36.435036 -80.568183 MW-14 5/30/06 2 48.03 33.03 15 Rock 1018.80 1016.11 976.70 42.10 36.434267 -80.569239 MW-15 6/22/06 2 57 42 15 Rock 1075.96 1073.23 1022.45 53.51 36.433797 -80.570467 MW-16 6/21/06 2 36.3 21.3 15 Rock 999.54 996.67 972.02 27.52 36.434536 -80.572117 MW-17 6/1/07 2 15.32 5.32 10 Rock 965.43 962.26 957.12 8.31 36.433558 -80.572517 MW-18 6/1/07 2 18.15 8.15 10 Saprolite 983.00 980.00 973.11 9.89 36.435453 -80.567050 MW-19 6/1/07 2 17.1 7.1 10 PWR 946.27 942.97 936.53 9.74 36.432231 -80.570556 MW-20 6/1/07 2 25.64 10.64 15 Rock 1082.19 1079.12 1062.18 20.01 36.439025 -80.571650 MW-21 6/1/07 2 15.41 5.41 10 Saprolite/PWR 965.36 962.22 958.62 6.74 36.434214 -80.568717 MW-22 6/1/07 2 16.04 6.04 10 Saprolite 953.40 950.23 946.78 6.62 36.432928 -80.571678 MW-23 6/1/07 2 17.1 7.1 1 10 Sandy Silt 955.31 952.09 1 947.36 1 7.95 1 36.432828 -80.569156 NOTE: bgs = below ground surface amsl= above mean sea level btoc = below top of casing (PVC well casing) Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1 Table 2 Field Observations of Monitoring Locations December 13, 2017 Location Viable Lack of Any Monitoring Evidence of Location Tampering Locked on Arrival & Departure Hinge/Hasp Operational Tagged or Labeled Concrete Surface Pad Appears Effective Comments MW-1 Yes Yes Yes Yes Yes Yes PR IW-1 No Yes Yes Yes Yes Yes Fouled since injection 11/2/11. IW-2 (was MW-2) No Yes Yes Yes Yes Yes Fouled since injection 11/2/11. No pad visible MW-3R Yes Yes Yes Yes Yes Yes PR IW-3 (was MW-3RS) No Yes Yes Yes Yes Yes Fouled since injection 11/2/11. IW-4 (was MW-4) No Yes Yes Yes Yes Yes Fouled since injection 10/24/12. IW-5 (was MW-5) No Yes Yes Yes Yes Yes Fouled since injection 11/2/11. Bailer would not descend MW-6 Yes Yes Yes Yes Yes Yes PR, Red Purge water MW-7 Yes Yes Yes Yes Yes Yes PR IW-6 (was MW-8) No Yes Yes Yes Yes Yes Fouled since injection 10/24/12. PR MW-9 Yes Yes Yes Yes Yes Yes MW-11 Yes Yes Yes Yes Yes Yes PR MW-12S Yes Yes Yes Yes Yes Yes MW-12D Yes Yes Yes Yes Yes Yes Flowing artesian MW-13 Yes Yes Yes Yes Yes Yes MW-14 Yes Yes Yes Yes Yes Yes MW-15 Yes Yes Yes Yes Yes Yes MW-16 Yes Yes Yes Yes Yes Yes Red purge water MW-17 Yes Yes Yes Yes Yes Yes MW-18 Yes Yes Yes Yes Yes Yes MW-19 Yes Yes Yes Yes Yes Yes MW-20 Yes Yes Yes Yes Yes Yes MW-21 Yes Yes Yes Yes Yes Yes MW-22 Yes Yes Yes Yes Yes Yes MW-23 Yes Yes Yes Yes Yes Yes SW-1 Yes Moderate gage height & flow SW-2 Yes Moderate gage height & flow SW-3 Yes Moderate gage height & flow SW-4 Yes Moderate gage height & flow SWN-1 Yes Moderate gage height & flow SWN-2 Yes Moderate gage height & flow SCALEHOUSE I Yes I I I I I I Sample from spigot next to well which is typical Any unusual field conditions, observations, or events: Injection wells (IW-1, IW-2, IW-3, IW-4, IW-5 and IW-6) exempt from laboratory analysis as SWS approved on May 10, 2013 (DIN:18938) Stormwater control improvements performed since May 2012 event. Visual markers (10 ft PVC pipes) remain secured to each monitoring well case PR= Concrete well pad replaced by County in Fall 2017. Slurry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1 Table 3 Field Parameter Data Summary December 13, 2017 Parameter Depth to Water Water Elevation TOC Elevation Temp. ORP DO pH Specific Conductance TDS Turbidity Units ft (btoc) ft (amsl) ft (amsl) C mV mg/L SU umhos/cm mg/L Visual or NTU MW-1 25.53 1108.82 1134.35 15.9 213 2.6 6.3 319 NR 1.21 IW-2 39.93 1028.93 1068.86 NR NR NR NR NR NR >1000 MW-3R 42.41 975.09 1017.50 15.4 119.0 1.1 8.3 303 NR Clear IW-3 33.61 986.96 1020.57 NR NR NR NR NR NR >1000 IW-4 38.21 988.05 1026.26 NR NR NR NR NR NR >1000 IW-5 na na 1080.18 NR NR NR NR NR NR NR MW-6 22.82 1044.85 1067.67 14.9 -27 0.8 6.8 417 NR Slight MW-7 12.91 1060.59 1073.50 15.5 113 0.7 6.5 311 NR Clear IW-6 44.01 1044.44 1088.45 NR NR NR NR NR NR >1000 MW-9 33.96 1060.11 1094.07 15.3 -23 0.8 6.1 417 NR Clear MW-11 23.42 1128.38 1151.80 15.1 113 2.8 6.5 438 NR Clear MW-12S 13.72 1012.08 1025.80 15.0 -97 0.8 5.1 147 NR Clear MW-12D 0.00 1027.05 1027.05 14.7 133 2.9 5.9 199 NR Slight MW-13 27.19 981.29 1008.48 14.9 187 0.8 6.1 221 NR Slight MW-14 42.1 976.70 1018.80 14.1 113 2.2 5.3 119 NR Clear MW-15 53.51 1022.45 1075.96 15.2 19 0.8 5.9 167 NR Clear MW-16 27.52 972.02 999.54 14.7 133 0.5 6.1 433 NR Slight MW-17 8.31 957.12 965.43 15.0 138 0.6 5.7 207 NR Clear MW-18 9.89 973.11 983.00 15.3 201 4.1 6.5 193 NR Clear MW-19 9.74 936.53 946.27 14.9 203 4.2 5.8 38 NR Clear MW-20 20.01 1062.18 1082.19 15.5 113 1.6 6.2 71 NR Slight MW-21 6.74 958.62 965.36 14.9 221 3.7 5.9 197 NR Clear MW-22 6.62 946.78 953.40 15.1 281 3.1 6.4 191 NR Clear MW-23 7.95 947.36 955.31 15.2 291 3.1 6.4 117 NR Clear Scalehouse na na na 14.3 228 4.2 6.9 731 NR Clear Minimum 0.00 936.53 946.27 14.1 -97 0.5 5.1 38 NR Clear Average 23.92 1008.67 1034.58 15.0 134 2.1 6.2 262 NR Clear Maximum 53.51 1128.38 1151.80 15.9 291 4.2 8.3 731 NR >1000 SW-1 - - - 5.3 NR NR 6.8 191 NR Clear SW-2 - - - 5.2 NR NR 6.7 121 NR Clear SW-3 - - - 5.2 NR NR 6.7 133 NR Clear SW-4 - - - 5.1 NR NR 6.9 231 NR Clear SWN-1 - - - 4.7 NR NR 6.9 103 NR Clear SWN-2 - - - 4.9 NR NR 7.1 97 NR Clear Minimum - - - 5.3 NR NR 7.1 231 NR Clear Average - - - 5.1 NR NR 6.9 146 NR Clear Maximum - - - 5.3 NR NR 7.1 231 NR Clear btoc = Below top of casing amsl = Above mean sea level na = Not available NR = No reading attempted Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1 Table 4 Sampling and Analysis Summary December 13-14, 2017 App. I App. II Field Parameter Tracer a Of O m c p O ° c - _ a a o 0 U ^ Q X _ N N 5 CU N Q ¢ .O N 'O 0) � p � > N N w N U m U m yr E a 6 a E O H> H ur 0 O H U H a H 2 m o o o m CO 0 U) N N O 00 ¢ O < oo¢ 00 a N N N N N N O d EL � LL LU CO uJ m o CO o W m(Z m m a?m m m aD LL J (0 J J LL LL LL I LL LL LL LL W IW-1 Not sampled since injection wells are exempt MW-1 X X X I X X I X X X IW-2 Not sampled since injection wells are exempt MW-3R X X X I X X I X X X IW-3 Not sampled since injection wells are exempt IW-4 Not sampled since injection wells are exempt IW-5 Not sampled since injection wells are exempt MW-6 X X X X X X X X MW-7 X X X X X X X X IW-6 Not sampled since injection wells are exempt MW-9 X X X X X X X X MW-11 X X X X X X X X MW-12S X X X X X X X X MW-12D X X X X X X X X MW-13 X X X X X X X X MW-14 X X X X X X X X MW-15 X X X X X X X X MW-16 X X X X X X X X MW-17 X X X X X X X X MW-18 X X X X X X X X MW-19 X X X X X X X X MW-20 X X X X X X X X MW-21 X X X X X X X X MW-22 X X X X X X X X MW-23 X X X X X X X X Scalehouse X X X X X X X X SW-1 X X X X X X SW-2 X X X X X X SW-3 X X X X X X SW-4 X X X X X X SWN-1 X X X X X X SWN 2 X X X X X X EB X X FIB X rr App I & II Lists = From current 4U GFK Lbd Injection wells exempt from monitoring except for turbidity and WLR per SWS approved SAP [189361 Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1 Table 5 Groundwater and QC Sample Detections December 13-14, 2017 Parameter Name MDL SWSL 2UGWP MCL 1 MW-1I MW-3R MW-6 MW-7 MW-9 MW-11 MW-12D MW-12S MW-13 MW-14 MW-15 MW-i6 MW-17 MW-18 MW-19 MW-20 MW-21 MW-22 MW-23 SCALEHOUSE EB FB Std BG S S S S S S S S S S S S S S S S S S I SUDDIV Well OC OC Metals (ADDendix I Arsenic, total 5 10 10 10 - Barium, total 2.5 100 700 2000 127 6.9 J 113 64.3 J 45 J 33.7 J 4.5 J 21.5 J 82.5 J 22.5 J 40.4 J 146 85.6 J 11.4 J 60.5 J 26 J 54.4 J 45 J 76.6 J 12.4 J Beryllium, total 0.5 1 4 4 Cadmium, total 0.5 1 2 5 3(.) 0.56 J 0.66 J 1.4 0.78 J 0.7 J 1.6 0.69 J 2.3 (N) Chromium, total 2.5 10 10 100 4.2 J 8 J 7.6 J 3.8 J 3.4 J 5.7 J Cobalt, total 2.5 10 1 NE 11.1 (N) 76.7 (N) 51.9 (N) 187 (N) 8.8 J (N) 15.6 (N) 491 (N) 73.7 12.4 (N) 3.2 J (N) Copper, total 2.5 10 1000 1300 6.1 J 12 8.4 J 2.6 J 9.5 J 4.2 J 3.8 J 4.1 J Lead, total 2.5 10 15 15 4.7 J Nickel, total 2.5 50 100 NE 5.1 J 7 J 2.6 J 6.7 J 6 J 4.4 J 2.7 J 3.2 J 27.1 J 9.7 J 2.9 J 3.7 J Thallium, total 0.03 5.5 0.28 2 0.15 J 0.59 J (N) 0.21 J 0.37 J (N) 0.053 J 0.11 J 0.031 J 0.07 J 0.5 J (N) 0.098 J 0.051 J 0.42 J 0.033 J 0.16 J 0.058 J Vanadium, total 2.5 25 0.3 NE 5.7 J (N) -- Zinc, total 5 10 1000 NE 48.3 7.4J 7.7J 10.1 8J 7.5J 5J 5.4J 17.5 5.6J 5J 14.7 7.6J 13.6 VOCs A endix I 1,1-Dichloroethane 0.32 5 6 NE 1.8 J 0.37 J 3 J 4.2 J 9.9 (L) 1.2 J 0.4 J 0.65 J 2.8 J 0.42 J 0.36 J 1,2-Dichlorobenzene 0.3 5 20 NE 1.1 J 1.8 J 11 1,2-Dichloroethane 0.24 1 0.4 5 1.7 (L) 1,2-Dichloropropane 0.27 1 0.6 5 1.2 (L) 0.3 J 1.5 (L) 1,4-Dichlorobenzene 0.33 1 6 75 1.1 4.9 1.7 3 4.2 15.7 (L) 3.3 0.77 J Benzene 0.25 1 1 5 0.28 J 1.9 (L) 0.6 J 0.57 J 1.4 (L) 0.43 J Chlorobenzene 0.23 3 50 100 2.3 J 1.8 J 0.71 J 0.95 J 2.8 J 6.4 2.4 J cis-1,2-Dichloroethene 0.19 5 70 70 0.3 J 36.4 1.6 J 20.8 6.6 33.6 29 0.95 J 0.99 J 0.56 J 14.2 0.69 J 0.41 J 0.31 J Tetrachloroethene 5 884 Trichloroethene 0 1 37 0.86 J 00 3.1 (L) 0.82 J Vinyl chloride 10.621 1 1 0.03 1 2 1 1 1 1 1 17.1 (L) I I I I 1 1 1.9 (L) 1 4.1 (L) General Parameter ASD-Metals Su Turbidity0.5 NE NE NE 2.1 12.1 1.1 1.2 4.7 -port) 14.6 31.6 9.3 8.2 53.1 5.3 2 5.3 0.62J 5 Units uglL, Blank cells means Not Detected, -- means not tested Red Bold Above Established MCLr21-IGWP Sod. Yellow Highlighted Above Established Federal MCL Drinking Water Std. No regulatory compliance significance. MDL = Mathotl Detection Limit, SWSL = Solid Waste Section Limit, 2UGW P Stmalmd! = NC 2L and IMAC Standards adopted by SW S, MCL = Madmum Contaminant La, 1 for Drinking Water J='Jyudified". Conc ration detected between MDL and SWSL. Considered estimated value IN) Preliminary source is believed to be Naturzl originating from erasion of natural deposits. Source not anth q ganic. (L) preliminary source Is believed to be anthropogenlc With leachate a landfill gas as transport mechanism A definitive source of the detections was not determined as part of this report. BG = Background Well Sample, QC = Quality Control Sample, S = Se Inal Well Sample Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1 Table 6 Surface Water Sample Detections December 13, 2017 Parameter Name MDL SWSL i 2B Std MCL SW-1 D SW-2 D SW-3 D SW-4 D Metals (Appendix I Barium, total 2.5 100 200000 2000 13.6 J 8.7 J 15.6 J 14.8 J Cobalt, total 2.5 10 270 NE 8.9 J 3.2 J Zinc, total 5 10 50 NE 9.1 J 7 J VOCs (Appendix 1) cis-1,2-Dichloroethene 0.19 1 5 1 4900 70 0.84 J Units ug/L, Blank cells means Not Detected, -- means not tested Red Bold Above Established 2B Std. Regulatory compliance Standard Yellow Highlighted Above Established Federal MCL Drinking Water Std. No regulatory compliance significance. MDL = Method Detection Limit, SWSL = Solid Waste Section Limit, 2B Standard = NC 2B Surface Water Standards adopted by SWS, MCL = Maximum Contaminant Level for Drinking Water J = "J-qualified". Concentration detected between MDL and SWSL. Considered estimated value D= Downstream of monitored unit Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1 Table 7 MNA Parameter Data Summary December 13, 2017 Parameters Method MDL* Units MW-1 MW-7 MW-9 MW-11 MW-14 MW-15 MW-21 12/13/17 12/13/17 12/13/17 12/13/17 12/13/17 12/13/17 12/13/17 VFA - Acetic Acid AM23G NS ug/L NS NS NS NS NS NS NS VFA - Butyric Acid AM23G NS ug/L NS NS NS NS NS NS NS VFA - Lactic Acid AM23G NS ug/L NS NS NS NS NS NS NS VFA - Propionic Acid AM23G NS ug/L NS NS NS NS NS NS NS VFA - Pyruvic Acid AM23G NS ug/L NS NS NS NS NS NS NS Hydrogen AM20GAX NS nM NS NS NS NS NS NS NS Methane AM20GAX NS ug/L NS NS NS NS NS NS NS Ethene AM20GAX NS ug/L NS NS NS NS NS NS NS Ethane AM20GAX NS ug/L NS NS NS NS NS NS NS CO2-Dissolved Field HACH Kit 10 mg/L 20 >100 >100 >100 >100 >100 >100 Alkalinity SM 2320B 1000 ug/L NS NS NS NS NS NS NS Sulfate EPA 300.0 1000 ug/L NS NS NS NS NS NS NS Sulfide SM 4500-S21D 100 ug/L NS NS NS NS NS NS NS Chloride SM 4500-CI-E 500 ug/L NS NS NS NS NS NS NS TOC SM 5310B 500 ug/L NS NS NS NS NS NS NS COD SM 5220D 12500 ug/L NS NS NS NS NS NS NS BOD SM5210B NS ug/L NS NS NS NS NS NS NS Ferrous Iron EPA 6010 500 ug/L NS NS NS NS NS NS NS Nitrate EPA 353.2 NS ug/L NS NS NS NS NS NS NS Temperature Field Instrument 0 C 15.9 15.5 15.3 15.1 14.1 15.2 14.9 ORP Field Instrument -900 mV 213 193 -23 113 113 19 221 DO Field Instrument 0 mg/L 2.6 0.7 0.8 2.8 2.2 0.8 3.7 pH Field Instrument 0 SU 6.3 6.5 6.1 5.5 5.3 5.9 5.9 Specific Conductance Field Instrument 0 us/cm 319 311 417 438 119 167 197 Turbidity Visual 1 0.5 1 NTU 1 <0.5 1 1.1 1 1.2 1 4.7 9.3 8.2 <0.5 Notes: VFA = Volatile Fatty Acids MDL* = Lab Method Detection Limit or lowest field measurement possible. Constituents detected below quantifiable limits are shown as < MDL value. >100 = CO2 Concentration exceeds maximum capability of method used. NS = Not Sampled Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1 Table 8 Hydrogeolofic Properties at Monitoring Well Locations December 13, 2017 Well Hydraulic Conductivity Effective Porosity Hydraulic Gradient Groundwater Average Linear Velocity Rate Flow Direction Immum Distance From Upgradient EOW (ft) Ground Water Depth Groundwater Potentiometric Elevation Screened Interval Lithology (cm/second) (ft/day) (°/u) (feet/feet) (feet/year) (feet btoc) (feet amsl) MW-1 4.30E-05 0.12 15 0.049 15 S21W 0 25.53 1108.82 Clay IW-2 4.30E-05 0.12 15 0.031 9 S49E - 39.93 1028.93 Clay MW-7 8.10E-04 2.30 15 0.118 659 N70W 704 12.91 1060.59 PWR / Fractured Rock IW-6 4.40E-04 1.25 15 0.107 325 S50E - 44.01 1044.44 PWR/ Fractured Rock MW-9 1.90E-04 0.54 15 0.005 7 S53E 614 33.96 1060.11 Sandy Sift MW-13 2.06E-04 0.58 23 0.064 60 S30W 1850 27.19 981.29 Saprolite MW-18 2.04E-03 5.78 15 0.144 na S23E 0 9.89 973.11 Saprolite MW-19 1.10E-03 3.12 3 0.077 2,925 S13W 2663 9.74 936.53 PWR MW-21 1.28E-03 3.63 3 0.069 3,046 S67E 2041 6.74 958.62 Saprolite/PWR MW-22 9.88E-04 2.80 15 0.140 954 S29W 2506 6.62 946.78 Saprolite MW-23 3.04E-04 0.86 15 0.083 173 S29E 2610 7.95 947.36 Sandy Sift Minimum 4.30E-05 0.12 3 0.005 7 0 6.62 936.53 Average 6.77E-04 1.92 14 0.081 817 1443 20.41 1004.23 Maximum 2.04E-03 5.78 23 0.144 3,046 2663 44.01 1108.82 MW-3R 2.40E-04 0.68 5 na na na 1,994 42.41 975.09 Fractured Rock IW-3 2.40E-05 0.07 5 0.249 123 S38W - 33.61 986.96 Fractured Rock IW-4 1.10E-04 0.31 5 0.195 444 S46E 38.21 988.05 Fractured Rock IW-5 1.50E-05 0.04 5 - S60E - - - Fractured Rock MW-6 1.90E-05 0.05 5 0.211 83 S85W 963 22.82 1044.85 Fractured Rock MW-11 3.10E-04 0.88 5 0.089 572 S19W 0 23.42 1128.38 Fractured Rock MW-12S na na 3 0.083 na S08E 0 13.72 1012.08 Fractured Rock MW-12D 1.30E-06 0.00 5 na na na 0 0.00 1027.05 Fractured Rock MW-14 7.45E-03 21.12 3 0.132 33,916 S73E 2098 42.10 976.70 Fractured Rock MW-15 7.21E-05 0.20 3 0.107 265 S07E 53.51 1022.45 Fractured Rock MW-16 2.82E-05 0.08 3 0.028 27 S52W 2089 27.52 972.02 Fractured Rock MW-17 2.94E-04 0.83 3 0.064 649 S78W 2547 8.31 957.12 Rock MW-20 1.92E-04 0.54 3 0.064 425 S21E 1 692 1 20.01 1 1062.18 1 Rock Minimum 1.30E-06 0.00 -3F 0.028 27 0 1 0.00 1 957.12 Average 7.30E-04 2.07 4 0.122 323 1154 27.14 1012.74 Maximum 7.45E-03 1 21.12 1 5 0.249 649 2547 53.51 1128.38 NOTE: Values for hydraulic conductivity determined via slug test by GAI, MESCO, or Joyce. Hydrologic gradient from water levels recorded on December 13, 2017. Wells screened entirely in rock were not utilized for flow directions/gradients. Screens that traverse both rock and regolith assumed flow in regolith dominates. Hydraulic Conducitivity value and flow rate for MW-14 was considered an outlier; therefore not included in the average or maximum. na = Not available/applicable Average Linear Velocity (Q) is defined by modified Darcy's equation: K A K= hydraulic conductivity where Q ri dl ne= effective porosity e dh=head difference dl= horizontal distance Slurry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Appendix A Laboratory Analysis Reports Chains of Custody lacieAnalXical" www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 January 10, 2018 Mr. Jonathan Pfohl Municipal Engineering Services 68 Shipwash Dr. Garner, NC 27529 RE: Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory on December 14, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Trey Carter trey. carter@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 CERTIFICATIONS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Minnesota Certification IDs 1700 Elm Street SE, Suite 200, Minneapolis, MN 55414- Michigan Certification #: 9909 2485 Minnesota Certification #: 027-053-137 A2LA Certification #: 2926.01 Mississippi Certification #: MN00064 Alabama Certification #: 40770 Montana Certification #: CERT0092 Alaska Contaminated Sites Certification #: 17-009 Nebraska Certification #: NE-OS-18-06 Alaska DW Certification M MN00064 Nevada Certification #: MN00064 Arizona Certification #: AZ0014 New Hampshire Certification #: 2081 Arkansas Certification #: 88-0680 New Jersey Certification M MN002 California Certification #: 2929 New York Certification #: 11647 CNMI Saipan Certification #:MP0003 North Carolina DW Certification #: 27700 Colorado Certification #: MN00064 North Carolina WW Certification #: 530 Connecticut Certification #: PH-0256 North Dakota Certification M R-036 EPA Region 8+Wyoming DW Certification #: via MN 027- Ohio DW Certification #: 41244 053-137 Ohio VAP Certification #: CL101 Florida Certification #: E87605 Oklahoma Certification #: 9507 Georgia Certification #: 959 Oregon NwTPH Certification #: MN300001 Guam EPA Certification #: MN00064 N0 Oregon Secondary Certification #: MN200001 Hawaii Certification #: MN0 Pennsylvania Certification #: 68-00563 : Idaho Certification #: MN00064 Puerto Rico Certification #: MN00064 Illinois Certification 20000 00011C-MN South Carolina Certification #:74003001 M 1 Indiana Certification #: Tennessee Certification #: TN02818 Iowa Certification #: Texas Certification #: T104704192 Kansas Certification #: E-10167 Utah Certification #: MN00 Kentucky DW Certification M 90062 Virginia Certification #: 163 Kentucky WW Certification M 90062 C64 Washington Certificationn ##: : 486 Louisiana DEQ Certification #: 03086 West Virginia DW Certification #: 9952 C Louisiana DW Certification #: MN00064 West Virginia DEP Certification #: 382 Maine Certification #: MN00064 Wisconsin Certification #: 999407970 Maryland Certification M 322 Massachusetts Certification #: M-MN064 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification M E87648 South Carolina Certification M 99030001 Massachusetts Certification #: M-NC030 Virginia/VELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Lab ID Sample ID Matrix Date Collected Date Received 92367133001 MW-1 Water 12/13/1711:35 12/14/17 12:40 92367133003 MW-12S Water 12/13/17 09:25 12/14/17 12:40 92367133004 MW-13 Water 12/13/1714:00 12/14/17 12:40 92367133005 MW-14 Water 12/13/1715:07 12/14/17 12:40 92367133006 MW-15 Water 12/13/1711:20 12/14/17 12:40 92367133007 MW-16 Water 12/13/1714:10 12/14/17 12:40 92367133008 MW-17 Water 12/13/17 08:35 12/14/17 12:40 92367133009 MW-18 Water 12/13/17 09:00 12/14/17 12:40 92367133010 MW-19 Water 12/13/1710:53 12/14/17 12:40 92367133011 MW-20 Water 12/13/1716:30 12/14/17 12:40 92367133012 MW-21 Water 12/13/1715:27 12/14/17 12:40 92367133013 MW-22 Water 12/13/1711:10 12/14/17 12:40 92367133014 MW-23 Water 12/13/1711:22 12/14/17 12:40 92367133015 MW-3R Water 12/13/1714:17 12/14/17 12:40 92367133016 MW-7 Water 12/13/1713:30 12/14/17 12:40 92367133017 MW-9 Water 12/13/1716:30 12/14/17 12:40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: Surry Closed -Mt. Airy (UIC) 92367133 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92367133001 MW-1 EPA6010 DS, SH1 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C EPA 180.1 MDW 1 PASI-A 92367133003 MW-12S EPA6010 DS, SH1 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C EPA 180.1 MDW 1 PASI-A 92367133004 MW-13 EPA6010 DS, SH1 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C EPA 180.1 MDW 1 PASI-A 92367133005 MW-14 EPA6010 DS, SH1 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C EPA 180.1 MDW 1 PASI-A 92367133006 MW-15 EPA6010 DS, SH1 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C EPA 180.1 MDW 1 PASI-A 92367133007 MW-16 EPA 6010 DS 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C EPA 180.1 MDW 1 PASI-A 92367133008 MW-17 EPA6010 DS, SH1 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C EPA 180.1 MDW 1 PASI-A 92367133009 MW-18 EPA6010 DS, SH1 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C EPA 180.1 MDW 1 PASI-A 92367133010 MW-19 EPA6010 DS, SH1 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C EPA 180.1 MDW 1 PASI-A 92367133011 MW-20 EPA6010 DS, SH1 14 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Analytes Lab ID Sample ID Method Analysts Reported Laboratory EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C EPA 180.1 MDW 1 PASI-A 92367133012 MW-21 EPA6010 DS, SH1 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C EPA 180.1 MDW 1 PASI-A 92367133013 MW-22 EPA6010 DS, SH1 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C EPA 180.1 MDW 1 PASI-A 92367133014 MW-23 EPA6010 DS, SH1 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C EPA 180.1 MDW 1 PASI-A 92367133015 MW-3R EPA6010 DS, SH1 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C EPA 180.1 MDW 1 PASI-A 92367133016 MW-7 EPA6010 DS, SH1 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C EPA 180.1 MDW 1 PASI-A 92367133017 MW-9 EPA6010 DS, SH1 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C EPA 180.1 MDW 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MWA Lab ID: 92367133001 Collected: 12/13/17 11:35 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Vanadium Zinc 1400111 -1 �41 :4 9 [y :2 LTA 61 Thallium 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane Date: 01/10/2018 06:01 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 12/20/17 13:35 12/28/17 06:08 7440-36-0 ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 06:08 7440-38-2 127 ug/L 100 2.5 1 12/20/17 13:35 12/28/17 06:08 7440-39-3 ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 06:08 7440-41-7 3.0 ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 06:08 7440-43-9 4.2J ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:08 7440-47-3 11.1 ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:08 7440-48-4 6.1J ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:08 7440-50-8 ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:08 7439-92-1 5.1J ug/L 50.0 2.5 1 12/20/17 13:35 12/28/17 06:08 7440-02-0 ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 06:08 7782-49-2 ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:08 7440-22-4 ND ug/L 25.0 2.5 1 12/20/17 13:35 12/28/17 06:08 7440-62-2 48.3 ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 20:11 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3020 0.15 ug/L 0.10 0.028 1 01/08/18 15:17 01/09/18 09:00 7440-28-0 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 12/16/17 05:42 67-64-1 ND ug/L 200 1.9 1 12/16/17 05:42 107-13-1 ND ug/L 1.0 0.25 1 12/16/17 05:42 71-43-2 ND ug/L 3.0 0.17 1 12/16/17 05:42 74-97-5 ND ug/L 1.0 0.18 1 12/16/17 05:42 75-27-4 ND ug/L 3.0 0.26 1 12/16/17 05:42 75-25-2 ND ug/L 10.0 0.29 1 12/16/17 05:42 74-83-9 ND ug/L 100 0.96 1 12/16/17 05:42 78-93-3 ND ug/L 100 1.2 1 12/16/17 05:42 75-15-0 ND ug/L 1.0 0.25 1 12/16/17 05:42 56-23-5 ND ug/L 3.0 0.23 1 12/16/17 05:42 108-90-7 ND ug/L 10.0 0.54 1 12/16/17 05:42 75-00-3 ND ug/L 5.0 0.14 1 12/16/17 05:42 67-66-3 ND ug/L 1.0 0.11 1 12/16/17 05:42 74-87-3 ND ug/L 13.0 2.0 1 12/16/17 05:42 96-12-8 ND ug/L 3.0 0.21 1 12/16/17 05:42 124-48-1 ND ug/L 1.0 0.27 1 12/16/17 05:42 106-93-4 ND ug/L 10.0 0.21 1 12/16/17 05:42 74-95-3 ND ug/L 5.0 0.30 1 12/16/17 05:42 95-50-1 ND ug/L 1.0 0.33 1 12/16/17 05:42 106-46-7 ND ug/L 100 1.0 1 12/16/17 05:42 110-57-6 ND ug/L 5.0 0.32 1 12/16/17 05:42 75-34-3 ND ug/L 1.0 0.24 1 12/16/17 05:42 107-06-2 ND ug/L 5.0 0.56 1 12/16/17 05:42 75-35-4 ND ug/L 5.0 0.19 1 12/16/17 05:42 156-59-2 ND ug/L 5.0 0.49 1 12/16/17 05:42 156-60-5 ND ug/L 1.0 0.27 1 12/16/17 05:42 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MWA Lab ID: 92367133001 Collected: 12/13/17 11:35 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 180.1 Turbidity Turbidity Date: 01/10/2018 06:01 PM Analytical Method: EPA 8260 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 100 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 1.0 ND ug/L 5.0 93 % 70-130 94 % 70-130 110 % 70-130 Analytical Method: EPA 180.1 ND NTU 1.0 0.13 1 12/16/17 05:42 10061-01-5 0.26 1 12/16/17 05:42 10061-02-6 0.30 1 12/16/17 05:42 100-41-4 0.46 1 12/16/17 05:42 591-78-6 0.32 1 12/16/17 05:42 74-88-4 0.97 1 12/16/17 05:42 75-09-2 0.33 1 12/16/17 05:42 108-10-1 0.26 1 12/16/17 05:42 100-42-5 0.33 1 12/16/17 05:42 630-20-6 0.40 1 12/16/17 05:42 79-34-5 0.46 1 12/16/17 05:42 127-18-4 0.26 1 12/16/17 05:42 108-88-3 0.48 1 12/16/17 05:42 71-55-6 0.29 1 12/16/17 05:42 79-00-5 0.47 1 12/16/17 05:42 79-01-6 0.20 1 12/16/17 05:42 75-69-4 0.41 1 12/16/17 05:42 96-18-4 0.35 1 12/16/17 05:42 108-05-4 0.62 1 12/16/17 05:42 75-01-4 0.66 1 12/16/17 05:42 1330-20-7 1 12/16/17 05:42 460-00-4 1 12/16/17 05:42 17060-07-0 1 12/16/17 05:42 2037-26-5 0.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 12/15/17 01:39 Page 7 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-12S Lab ID: 92367133003 Collected: 12/13/17 09:25 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Vanadium Zinc 1400111 -1 �41 :4 9 [y :2 LTA 61 Thallium 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane Date: 01/10/2018 06:01 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 12/20/17 13:35 12/28/17 06:17 7440-36-0 ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 06:17 7440-38-2 21.5J ug/L 100 2.5 1 12/20/17 13:35 12/28/17 06:17 7440-39-3 ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 06:17 7440-41-7 ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 06:17 7440-43-9 ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:17 7440-47-3 ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:17 7440-48-4 2.6J ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:17 7440-50-8 ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:17 7439-92-1 4.4J ug/L 50.0 2.5 1 12/20/17 13:35 12/28/17 06:17 7440-02-0 ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 06:17 7782-49-2 ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:17 7440-22-4 ND ug/L 25.0 2.5 1 12/20/17 13:35 12/28/17 06:17 7440-62-2 ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 20:20 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3020 ND ug/L 0.10 0.028 1 01/08/18 15:17 01/09/18 08:41 7440-28-0 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 12/16/17 06:00 67-64-1 ND ug/L 200 1.9 1 12/16/17 06:00 107-13-1 ND ug/L 1.0 0.25 1 12/16/17 06:00 71-43-2 ND ug/L 3.0 0.17 1 12/16/17 06:00 74-97-5 ND ug/L 1.0 0.18 1 12/16/17 06:00 75-27-4 ND ug/L 3.0 0.26 1 12/16/17 06:00 75-25-2 ND ug/L 10.0 0.29 1 12/16/17 06:00 74-83-9 ND ug/L 100 0.96 1 12/16/17 06:00 78-93-3 ND ug/L 100 1.2 1 12/16/17 06:00 75-15-0 ND ug/L 1.0 0.25 1 12/16/17 06:00 56-23-5 ND ug/L 3.0 0.23 1 12/16/17 06:00 108-90-7 ND ug/L 10.0 0.54 1 12/16/17 06:00 75-00-3 ND ug/L 5.0 0.14 1 12/16/17 06:00 67-66-3 ND ug/L 1.0 0.11 1 12/16/17 06:00 74-87-3 ND ug/L 13.0 2.0 1 12/16/17 06:00 96-12-8 ND ug/L 3.0 0.21 1 12/16/17 06:00 124-48-1 ND ug/L 1.0 0.27 1 12/16/17 06:00 106-93-4 ND ug/L 10.0 0.21 1 12/16/17 06:00 74-95-3 ND ug/L 5.0 0.30 1 12/16/17 06:00 95-50-1 ND ug/L 1.0 0.33 1 12/16/17 06:00 106-46-7 ND ug/L 100 1.0 1 12/16/17 06:00 110-57-6 ND ug/L 5.0 0.32 1 12/16/17 06:00 75-34-3 ND ug/L 1.0 0.24 1 12/16/17 06:00 107-06-2 ND ug/L 5.0 0.56 1 12/16/17 06:00 75-35-4 ND ug/L 5.0 0.19 1 12/16/17 06:00 156-59-2 ND ug/L 5.0 0.49 1 12/16/17 06:00 156-60-5 ND ug/L 1.0 0.27 1 12/16/17 06:00 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-12S Lab ID: 92367133003 Collected: 12/13/17 09:25 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 180.1 Turbidity Turbidity Date: 01/10/2018 06:01 PM Analytical Method: EPA 8260 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 100 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 1.0 ND ug/L 5.0 95 % 70-130 93 % 70-130 104 % 70-130 Analytical Method: EPA 180.1 14.6 NTU 1.0 0.13 1 12/16/17 06:00 10061-01-5 0.26 1 12/16/17 06:00 10061-02-6 0.30 1 12/16/17 06:00 100-41-4 0.46 1 12/16/17 06:00 591-78-6 0.32 1 12/16/17 06:00 74-88-4 0.97 1 12/16/17 06:00 75-09-2 0.33 1 12/16/17 06:00 108-10-1 0.26 1 12/16/17 06:00 100-42-5 0.33 1 12/16/17 06:00 630-20-6 0.40 1 12/16/17 06:00 79-34-5 0.46 1 12/16/17 06:00 127-18-4 0.26 1 12/16/17 06:00 108-88-3 0.48 1 12/16/17 06:00 71-55-6 0.29 1 12/16/17 06:00 79-00-5 0.47 1 12/16/17 06:00 79-01-6 0.20 1 12/16/17 06:00 75-69-4 0.41 1 12/16/17 06:00 96-18-4 0.35 1 12/16/17 06:00 108-05-4 0.62 1 12/16/17 06:00 75-01-4 0.66 1 12/16/17 06:00 1330-20-7 1 12/16/17 06:00 460-00-4 1 12/16/17 06:00 17060-07-0 1 12/16/17 06:00 2037-26-5 0.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 12/15/17 01:39 Page 9 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-13 Lab ID: 92367133004 Collected: 12/13/17 14:00 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Antimony ND ug/L 6.0 3.9 1 12/20/17 13:35 12/28/17 06:20 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 06:20 7440-38-2 Barium 82.5J ug/L 100 2.5 1 12/20/17 13:35 12/28/17 06:20 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 06:20 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 06:20 7440-43-9 Chromium ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:20 7440-47-3 Cobalt 15.6 ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:20 7440-48-4 Copper ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:20 7440-50-8 Lead ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:20 7439-92-1 Nickel 2.7J ug/L 50.0 2.5 1 12/20/17 13:35 12/28/17 06:20 7440-02-0 Selenium ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 06:20 7782-49-2 Silver ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:20 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 12/20/17 13:35 12/28/17 06:20 7440-62-2 Zinc 5.OJ ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 20:23 7440-66-6 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020 Thallium 0.11 ug/L 0.10 0.028 1 01/08/18 15:17 01/09/18 08:43 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 12/16/17 06:17 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 12/16/17 06:17 107-13-1 Benzene ND ug/L 1.0 0.25 1 12/16/17 06:17 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 12/16/17 06:17 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 12/16/17 06:17 75-27-4 Bromoform ND ug/L 3.0 0.26 1 12/16/17 06:17 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 12/16/17 06:17 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 12/16/17 06:17 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 12/16/17 06:17 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 12/16/17 06:17 56-23-5 Chlorobenzene 0.95J ug/L 3.0 0.23 1 12/16/17 06:17 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 12/16/17 06:17 75-00-3 Chloroform ND ug/L 5.0 0.14 1 12/16/17 06:17 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 12/16/17 06:17 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 12/16/17 06:17 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 12/16/17 06:17 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 12/16/17 06:17 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 12/16/17 06:17 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 12/16/17 06:17 95-50-1 1,4-Dichlorobenzene 3.0 ug/L 1.0 0.33 1 12/16/17 06:17 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 12/16/17 06:17 110-57-6 1,1-Dichloroethane 3.OJ ug/L 5.0 0.32 1 12/16/17 06:17 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 12/16/17 06:17 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 12/16/17 06:17 75-35-4 cis-1,2-Dichloroethene 20.8 ug/L 5.0 0.19 1 12/16/17 06:17 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 12/16/17 06:17 156-60-5 1,2-Dichloropropane 0.30J ug/L 1.0 0.27 1 12/16/17 06:17 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-13 Lab ID: 92367133004 Collected: 12/13/17 14:00 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 180.1 Turbidity Turbidity Date: 01/10/2018 06:01 PM Analytical Method: EPA 8260 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 100 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 0.86J ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 1.0 ND ug/L 5.0 97 % 70-130 95 % 70-130 104 % 70-130 Analytical Method: EPA 180.1 31.6 NTU 1.0 0.13 0.26 0.30 0.46 0.32 0.97 0.33 0.26 0.33 0.40 0.46 0.26 0.48 0.29 0.47 0.20 0.41 0.35 0.62 0.66 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 12/16/17 06:17 10061-01-5 12/16/17 06:17 10061-02-6 12/16/17 06:17 100-41-4 12/16/17 06:17 591-78-6 12/16/17 06:17 74-88-4 12/16/17 06:17 75-09-2 12/16/17 06:17 108-10-1 12/16/17 06:17 100-42-5 12/16/17 06:17 630-20-6 12/16/17 06:17 79-34-5 12/16/17 06:17 127-18-4 12/16/17 06:17 108-88-3 12/16/17 06:17 71-55-6 12/16/17 06:17 79-00-5 12/16/17 06:17 79-01-6 12/16/17 06:17 75-69-4 12/16/17 06:17 96-18-4 12/16/17 06:17 108-05-4 12/16/17 06:17 75-01-4 12/16/17 06:17 1330-20-7 12/16/17 06:17 460-00-4 12/16/17 06:17 17060-07-0 12/16/17 06:17 2037-26-5 12/15/17 01:39 D6 Page 11 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-14 Lab ID: 92367133005 Collected: 12/13/17 15:07 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Antimony ND ug/L 6.0 3.9 1 12/20/17 13:35 12/28/17 06:23 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 06:23 7440-38-2 Barium 22.5J ug/L 100 2.5 1 12/20/17 13:35 12/28/17 06:23 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 06:23 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 06:23 7440-43-9 Chromium ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:23 7440-47-3 Cobalt ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:23 7440-48-4 Copper ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:23 7440-50-8 Lead ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:23 7439-92-1 Nickel ND ug/L 50.0 2.5 1 12/20/17 13:35 12/28/17 06:23 7440-02-0 Selenium ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 06:23 7782-49-2 Silver ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:23 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 12/20/17 13:35 12/28/17 06:23 7440-62-2 Zinc ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 20:26 7440-66-6 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020 Thallium 0.031J ug/L 0.10 0.028 1 01/08/18 15:17 01/09/18 08:46 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 12/16/17 06:35 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 12/16/17 06:35 107-13-1 Benzene ND ug/L 1.0 0.25 1 12/16/17 06:35 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 12/16/17 06:35 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 12/16/17 06:35 75-27-4 Bromoform ND ug/L 3.0 0.26 1 12/16/17 06:35 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 12/16/17 06:35 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 12/16/17 06:35 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 12/16/17 06:35 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 12/16/17 06:35 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 12/16/17 06:35 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 12/16/17 06:35 75-00-3 Chloroform ND ug/L 5.0 0.14 1 12/16/17 06:35 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 12/16/17 06:35 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 12/16/17 06:35 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 12/16/17 06:35 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 12/16/17 06:35 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 12/16/17 06:35 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 12/16/17 06:35 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 12/16/17 06:35 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 12/16/17 06:35 110-57-6 1,1-Dichloroethane 4.2J ug/L 5.0 0.32 1 12/16/17 06:35 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 12/16/17 06:35 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 12/16/17 06:35 75-35-4 cis-1,2-Dichloroethene 6.6 ug/L 5.0 0.19 1 12/16/17 06:35 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 12/16/17 06:35 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 12/16/17 06:35 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-14 Lab ID: 92367133005 Collected: 12/13/17 15:07 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 180.1 Turbidity Turbidity Date: 01/10/2018 06:01 PM Analytical Method: EPA 8260 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 100 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 3.0 0.881 ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 0.76J ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 1.0 ND ug/L 5.0 97 % 70-130 93 % 70-130 105 % 70-130 Analytical Method: EPA 180.1 9.3 NTU 1.0 0.13 1 12/16/17 06:35 10061-01-5 0.26 1 12/16/17 06:35 10061-02-6 0.30 1 12/16/17 06:35 100-41-4 0.46 1 12/16/17 06:35 591-78-6 0.32 1 12/16/17 06:35 74-88-4 0.97 1 12/16/17 06:35 75-09-2 0.33 1 12/16/17 06:35 108-10-1 0.26 1 12/16/17 06:35 100-42-5 0.33 1 12/16/17 06:35 630-20-6 0.40 1 12/16/17 06:35 79-34-5 0.46 1 12/16/17 06:35 127-18-4 0.26 1 12/16/17 06:35 108-88-3 0.48 1 12/16/17 06:35 71-55-6 0.29 1 12/16/17 06:35 79-00-5 0.47 1 12/16/17 06:35 79-01-6 0.20 1 12/16/17 06:35 75-69-4 0.41 1 12/16/17 06:35 96-18-4 0.35 1 12/16/17 06:35 108-05-4 0.62 1 12/16/17 06:35 75-01-4 0.66 1 12/16/17 06:35 1330-20-7 1 12/16/17 06:35 460-00-4 1 12/16/17 06:35 17060-07-0 1 12/16/17 06:35 2037-26-5 0.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 12/15/17 01:39 Page 13 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-15 Lab ID: 92367133006 Collected: 12/13/17 11:20 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Vanadium Zinc 1400111 -1 �41 :4 9 [y :2 LTA 61 Thallium 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane Date: 01/10/2018 06:01 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 12/20/17 13:35 12/28/17 06:27 7440-36-0 ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 06:27 7440-38-2 40.4J ug/L 100 2.5 1 12/20/17 13:35 12/28/17 06:27 7440-39-3 ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 06:27 7440-41-7 0.78J ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 06:27 7440-43-9 ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:27 7440-47-3 ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:27 7440-48-4 ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:27 7440-50-8 ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:27 7439-92-1 3.2J ug/L 50.0 2.5 1 12/20/17 13:35 12/28/17 06:27 7440-02-0 ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 06:27 7782-49-2 ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:27 7440-22-4 ND ug/L 25.0 2.5 1 12/20/17 13:35 12/28/17 06:27 7440-62-2 5.4J ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 20:30 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3020 0.070J ug/L 0.10 0.028 1 01/08/18 15:17 01/09/18 08:49 7440-28-0 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 12/16/17 06:53 67-64-1 ND ug/L 200 1.9 1 12/16/17 06:53 107-13-1 0.57J ug/L 1.0 0.25 1 12/16/17 06:53 71-43-2 ND ug/L 3.0 0.17 1 12/16/17 06:53 74-97-5 ND ug/L 1.0 0.18 1 12/16/17 06:53 75-27-4 ND ug/L 3.0 0.26 1 12/16/17 06:53 75-25-2 ND ug/L 10.0 0.29 1 12/16/17 06:53 74-83-9 ND ug/L 100 0.96 1 12/16/17 06:53 78-93-3 ND ug/L 100 1.2 1 12/16/17 06:53 75-15-0 ND ug/L 1.0 0.25 1 12/16/17 06:53 56-23-5 2.8J ug/L 3.0 0.23 1 12/16/17 06:53 108-90-7 ND ug/L 10.0 0.54 1 12/16/17 06:53 75-00-3 ND ug/L 5.0 0.14 1 12/16/17 06:53 67-66-3 ND ug/L 1.0 0.11 1 12/16/17 06:53 74-87-3 ND ug/L 13.0 2.0 1 12/16/17 06:53 96-12-8 ND ug/L 3.0 0.21 1 12/16/17 06:53 124-48-1 ND ug/L 1.0 0.27 1 12/16/17 06:53 106-93-4 ND ug/L 10.0 0.21 1 12/16/17 06:53 74-95-3 ND ug/L 5.0 0.30 1 12/16/17 06:53 95-50-1 4.2 ug/L 1.0 0.33 1 12/16/17 06:53 106-46-7 ND ug/L 100 1.0 1 12/16/17 06:53 110-57-6 9.9 ug/L 5.0 0.32 1 12/16/17 06:53 75-34-3 ND ug/L 1.0 0.24 1 12/16/17 06:53 107-06-2 ND ug/L 5.0 0.56 1 12/16/17 06:53 75-35-4 33.6 ug/L 5.0 0.19 1 12/16/17 06:53 156-59-2 ND ug/L 5.0 0.49 1 12/16/17 06:53 156-60-5 ND ug/L 1.0 0.27 1 12/16/17 06:53 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 14 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-15 Lab ID: 92367133006 Collected: 12/13/17 11:20 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 180.1 Turbidity Turbidity Date: 01/10/2018 06:01 PM Analytical Method: EPA 8260 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 100 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 3.1 ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 1.9 ug/L 1.0 ND ug/L 5.0 95 % 70-130 94 % 70-130 112 % 70-130 Analytical Method: EPA 180.1 8.2 NTU 1.0 0.13 1 12/16/17 06:53 10061-01-5 0.26 1 12/16/17 06:53 10061-02-6 0.30 1 12/16/17 06:53 100-41-4 0.46 1 12/16/17 06:53 591-78-6 0.32 1 12/16/17 06:53 74-88-4 0.97 1 12/16/17 06:53 75-09-2 0.33 1 12/16/17 06:53 108-10-1 0.26 1 12/16/17 06:53 100-42-5 0.33 1 12/16/17 06:53 630-20-6 0.40 1 12/16/17 06:53 79-34-5 0.46 1 12/16/17 06:53 127-18-4 0.26 1 12/16/17 06:53 108-88-3 0.48 1 12/16/17 06:53 71-55-6 0.29 1 12/16/17 06:53 79-00-5 0.47 1 12/16/17 06:53 79-01-6 0.20 1 12/16/17 06:53 75-69-4 0.41 1 12/16/17 06:53 96-18-4 0.35 1 12/16/17 06:53 108-05-4 0.62 1 12/16/17 06:53 75-01-4 0.66 1 12/16/17 06:53 1330-20-7 1 12/16/17 06:53 460-00-4 1 12/16/17 06:53 17060-07-0 1 12/16/17 06:53 2037-26-5 0.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 12/15/17 01:39 Page 15 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-16 Lab ID: 92367133007 Collected: 12/13/17 14:10 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Antimony ND ug/L 6.0 3.9 1 12/20/17 13:35 12/28/17 20:33 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 20:33 7440-38-2 Barium 146 ug/L 100 2.5 1 12/20/17 13:35 12/28/17 20:33 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 20:33 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 20:33 7440-43-9 Chromium 7.6J ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 20:33 7440-47-3 Cobalt 491 ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 20:33 7440-48-4 Copper 9.5J ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 20:33 7440-50-8 Lead 4.7J ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 20:33 7439-92-1 Nickel 27.1J ug/L 50.0 2.5 1 12/20/17 13:35 12/28/17 20:33 7440-02-0 Selenium ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 20:33 7782-49-2 Silver ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 20:33 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 12/20/17 13:35 12/28/17 20:33 7440-62-2 Zinc 17.5 ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 20:33 7440-66-6 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020 Thallium 0.50 ug/L 0.10 0.028 1 01/08/18 15:17 01/09/18 08:52 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 12/16/17 07:10 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 12/16/17 07:10 107-13-1 Benzene 1.4 ug/L 1.0 0.25 1 12/16/17 07:10 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 12/16/17 07:10 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 12/16/17 07:10 75-27-4 Bromoform ND ug/L 3.0 0.26 1 12/16/17 07:10 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 12/16/17 07:10 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 12/16/17 07:10 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 12/16/17 07:10 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 12/16/17 07:10 56-23-5 Chlorobenzene 6.4 ug/L 3.0 0.23 1 12/16/17 07:10 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 12/16/17 07:10 75-00-3 Chloroform ND ug/L 5.0 0.14 1 12/16/17 07:10 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 12/16/17 07:10 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 12/16/17 07:10 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 12/16/17 07:10 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 12/16/17 07:10 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 12/16/17 07:10 74-95-3 1,2-Dichlorobenzene 1.81 ug/L 5.0 0.30 1 12/16/17 07:10 95-50-1 1,4-Dichlorobenzene 15.7 ug/L 1.0 0.33 1 12/16/17 07:10 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 12/16/17 07:10 110-57-6 1,1-Dichloroethane 1.2J ug/L 5.0 0.32 1 12/16/17 07:10 75-34-3 1,2-Dichloroethane 1.7 ug/L 1.0 0.24 1 12/16/17 07:10 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 12/16/17 07:10 75-35-4 cis-1,2-Dichloroethene 29.0 ug/L 5.0 0.19 1 12/16/17 07:10 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 12/16/17 07:10 156-60-5 1,2-Dichloropropane 1.5 ug/L 1.0 0.27 1 12/16/17 07:10 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-16 Lab ID: 92367133007 Collected: 12/13/17 14:10 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 180.1 Turbidity Turbidity Date: 01/10/2018 06:01 PM Analytical Method: EPA 8260 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 100 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 4.1 ug/L 1.0 ND ug/L 5.0 96 % 70-130 94 % 70-130 105 % 70-130 Analytical Method: EPA 180.1 53.1 NTU 1.0 0.13 1 12/16/17 07:10 10061-01-5 0.26 1 12/16/17 07:10 10061-02-6 0.30 1 12/16/17 07:10 100-41-4 0.46 1 12/16/17 07:10 591-78-6 0.32 1 12/16/17 07:10 74-88-4 0.97 1 12/16/17 07:10 75-09-2 0.33 1 12/16/17 07:10 108-10-1 0.26 1 12/16/17 07:10 100-42-5 0.33 1 12/16/17 07:10 630-20-6 0.40 1 12/16/17 07:10 79-34-5 0.46 1 12/16/17 07:10 127-18-4 0.26 1 12/16/17 07:10 108-88-3 0.48 1 12/16/17 07:10 71-55-6 0.29 1 12/16/17 07:10 79-00-5 0.47 1 12/16/17 07:10 79-01-6 0.20 1 12/16/17 07:10 75-69-4 0.41 1 12/16/17 07:10 96-18-4 0.35 1 12/16/17 07:10 108-05-4 0.62 1 12/16/17 07:10 75-01-4 0.66 1 12/16/17 07:10 1330-20-7 1 12/16/17 07:10 460-00-4 1 12/16/17 07:10 17060-07-0 1 12/16/17 07:10 2037-26-5 0.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 12/14/17 23:10 Page 17 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-17 Lab ID: 92367133008 Collected: 12/13/17 08:35 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Antimony ND ug/L 6.0 3.9 1 12/20/17 13:35 12/28/17 06:39 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 06:39 7440-38-2 Barium 85.6J ug/L 100 2.5 1 12/20/17 13:35 12/28/17 06:39 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 06:39 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 06:39 7440-43-9 Chromium 3.8J ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:39 7440-47-3 Cobalt 73.7 ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:39 7440-48-4 Copper ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:39 7440-50-8 Lead ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:39 7439-92-1 Nickel 9.7J ug/L 50.0 2.5 1 12/20/17 13:35 12/28/17 06:39 7440-02-0 Selenium ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 06:39 7782-49-2 Silver ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:39 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 12/20/17 13:35 12/28/17 06:39 7440-62-2 Zinc 5.6J ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 20:36 7440-66-6 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020 Thallium 0.0981 ug/L 0.10 0.028 1 01/08/18 15:17 01/09/18 08:55 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 12/16/17 07:28 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 12/16/17 07:28 107-13-1 Benzene 0.43J ug/L 1.0 0.25 1 12/16/17 07:28 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 12/16/17 07:28 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 12/16/17 07:28 75-27-4 Bromoform ND ug/L 3.0 0.26 1 12/16/17 07:28 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 12/16/17 07:28 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 12/16/17 07:28 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 12/16/17 07:28 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 12/16/17 07:28 56-23-5 Chlorobenzene 2.4J ug/L 3.0 0.23 1 12/16/17 07:28 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 12/16/17 07:28 75-00-3 Chloroform ND ug/L 5.0 0.14 1 12/16/17 07:28 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 12/16/17 07:28 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 12/16/17 07:28 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 12/16/17 07:28 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 12/16/17 07:28 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 12/16/17 07:28 74-95-3 1,2-Dichlorobenzene 1.0J ug/L 5.0 0.30 1 12/16/17 07:28 95-50-1 1,4-Dichlorobenzene 3.3 ug/L 1.0 0.33 1 12/16/17 07:28 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 12/16/17 07:28 110-57-6 1,1-Dichloroethane 0.40J ug/L 5.0 0.32 1 12/16/17 07:28 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 12/16/17 07:28 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 12/16/17 07:28 75-35-4 cis-1,2-Dichloroethene 0.95J ug/L 5.0 0.19 1 12/16/17 07:28 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 12/16/17 07:28 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 12/16/17 07:28 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-17 Lab ID: 92367133008 Collected: 12/13/17 08:35 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 180.1 Turbidity Turbidity Date: 01/10/2018 06:01 PM Analytical Method: EPA 8260 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 100 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 1.0 ND ug/L 5.0 96 % 70-130 97 % 70-130 100 % 70-130 Analytical Method: EPA 180.1 5.3 NTU 1.0 0.13 1 12/16/17 07:28 10061-01-5 0.26 1 12/16/17 07:28 10061-02-6 0.30 1 12/16/17 07:28 100-41-4 0.46 1 12/16/17 07:28 591-78-6 0.32 1 12/16/17 07:28 74-88-4 0.97 1 12/16/17 07:28 75-09-2 0.33 1 12/16/17 07:28 108-10-1 0.26 1 12/16/17 07:28 100-42-5 0.33 1 12/16/17 07:28 630-20-6 0.40 1 12/16/17 07:28 79-34-5 0.46 1 12/16/17 07:28 127-18-4 0.26 1 12/16/17 07:28 108-88-3 0.48 1 12/16/17 07:28 71-55-6 0.29 1 12/16/17 07:28 79-00-5 0.47 1 12/16/17 07:28 79-01-6 0.20 1 12/16/17 07:28 75-69-4 0.41 1 12/16/17 07:28 96-18-4 0.35 1 12/16/17 07:28 108-05-4 0.62 1 12/16/17 07:28 75-01-4 0.66 1 12/16/17 07:28 1330-20-7 1 12/16/17 07:28 460-00-4 1 12/16/17 07:28 17060-07-0 1 12/16/17 07:28 2037-26-5 0.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 12/15/17 01:39 Page 19 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-18 Lab ID: 92367133009 Collected: 12/13/17 09:00 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Antimony ND ug/L 6.0 3.9 1 12/20/17 13:35 12/28/17 06:43 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 06:43 7440-38-2 Barium 11.4J ug/L 100 2.5 1 12/20/17 13:35 12/28/17 06:43 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 06:43 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 06:43 7440-43-9 Chromium ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:43 7440-47-3 Cobalt ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:43 7440-48-4 Copper ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:43 7440-50-8 Lead ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:43 7439-92-1 Nickel ND ug/L 50.0 2.5 1 12/20/17 13:35 12/28/17 06:43 7440-02-0 Selenium ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 06:43 7782-49-2 Silver ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:43 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 12/20/17 13:35 12/28/17 06:43 7440-62-2 Zinc ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 20:46 7440-66-6 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020 Thallium ND ug/L 0.10 0.028 1 01/08/18 15:17 01/09/18 08:58 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 12/16/17 07:46 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 12/16/17 07:46 107-13-1 Benzene ND ug/L 1.0 0.25 1 12/16/17 07:46 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 12/16/17 07:46 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 12/16/17 07:46 75-27-4 Bromoform ND ug/L 3.0 0.26 1 12/16/17 07:46 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 12/16/17 07:46 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 12/16/17 07:46 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 12/16/17 07:46 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 12/16/17 07:46 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 12/16/17 07:46 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 12/16/17 07:46 75-00-3 Chloroform ND ug/L 5.0 0.14 1 12/16/17 07:46 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 12/16/17 07:46 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 12/16/17 07:46 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 12/16/17 07:46 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 12/16/17 07:46 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 12/16/17 07:46 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 12/16/17 07:46 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 12/16/17 07:46 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 12/16/17 07:46 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 12/16/17 07:46 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 12/16/17 07:46 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 12/16/17 07:46 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 12/16/17 07:46 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 12/16/17 07:46 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 12/16/17 07:46 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-18 Lab ID: 92367133009 Collected: 12/13/17 09:00 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 180.1 Turbidity Turbidity Date: 01/10/2018 06:01 PM Analytical Method: EPA 8260 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 100 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 1.0 ND ug/L 5.0 93 % 70-130 97 % 70-130 100 % 70-130 Analytical Method: EPA 180.1 2.0 NTU 1.0 0.13 1 12/16/17 07:46 10061-01-5 0.26 1 12/16/17 07:46 10061-02-6 0.30 1 12/16/17 07:46 100-41-4 0.46 1 12/16/17 07:46 591-78-6 0.32 1 12/16/17 07:46 74-88-4 0.97 1 12/16/17 07:46 75-09-2 0.33 1 12/16/17 07:46 108-10-1 0.26 1 12/16/17 07:46 100-42-5 0.33 1 12/16/17 07:46 630-20-6 0.40 1 12/16/17 07:46 79-34-5 0.46 1 12/16/17 07:46 127-18-4 0.26 1 12/16/17 07:46 108-88-3 0.48 1 12/16/17 07:46 71-55-6 0.29 1 12/16/17 07:46 79-00-5 0.47 1 12/16/17 07:46 79-01-6 0.20 1 12/16/17 07:46 75-69-4 0.41 1 12/16/17 07:46 96-18-4 0.35 1 12/16/17 07:46 108-05-4 0.62 1 12/16/17 07:46 75-01-4 0.66 1 12/16/17 07:46 1330-20-7 1 12/16/17 07:46 460-00-4 1 12/16/17 07:46 17060-07-0 1 12/16/17 07:46 2037-26-5 0.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 12/15/17 01:39 Page 21 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-19 Lab ID: 92367133010 Collected: 12/13/17 10:53 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Antimony ND ug/L 6.0 3.9 1 12/20/17 13:35 12/28/17 06:46 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 06:46 7440-38-2 Barium 60.5J ug/L 100 2.5 1 12/20/17 13:35 12/28/17 06:46 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 06:46 7440-41-7 Cadmium 0.70J ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 06:46 7440-43-9 Chromium ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:46 7440-47-3 Cobalt ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:46 7440-48-4 Copper 4.2J ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:46 7440-50-8 Lead ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:46 7439-92-1 Nickel ND ug/L 50.0 2.5 1 12/20/17 13:35 12/28/17 06:46 7440-02-0 Selenium ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 06:46 7782-49-2 Silver ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:46 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 12/20/17 13:35 12/28/17 06:46 7440-62-2 Zinc 5.OJ ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 20:49 7440-66-6 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020 Thallium 0.0511 ug/L 0.10 0.028 1 01/08/18 15:17 01/09/18 09:14 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 12/16/17 08:03 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 12/16/17 08:03 107-13-1 Benzene ND ug/L 1.0 0.25 1 12/16/17 08:03 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 12/16/17 08:03 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 12/16/17 08:03 75-27-4 Bromoform ND ug/L 3.0 0.26 1 12/16/17 08:03 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 12/16/17 08:03 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 12/16/17 08:03 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 12/16/17 08:03 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 12/16/17 08:03 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 12/16/17 08:03 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 12/16/17 08:03 75-00-3 Chloroform ND ug/L 5.0 0.14 1 12/16/17 08:03 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 12/16/17 08:03 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 12/16/17 08:03 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 12/16/17 08:03 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 12/16/17 08:03 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 12/16/17 08:03 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 12/16/17 08:03 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 12/16/17 08:03 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 12/16/17 08:03 110-57-6 1,1-Dichloroethane 0.65J ug/L 5.0 0.32 1 12/16/17 08:03 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 12/16/17 08:03 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 12/16/17 08:03 75-35-4 cis-1,2-Dichloroethene 0.991 ug/L 5.0 0.19 1 12/16/17 08:03 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 12/16/17 08:03 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 12/16/17 08:03 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-19 Lab ID: 92367133010 Collected: 12/13/17 10:53 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 180.1 Turbidity Turbidity Date: 01/10/2018 06:01 PM Analytical Method: EPA 8260 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 100 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 1.0 ND ug/L 5.0 95 % 70-130 93 % 70-130 105 % 70-130 Analytical Method: EPA 180.1 5.3 NTU 1.0 0.13 1 12/16/17 08:03 10061-01-5 0.26 1 12/16/17 08:03 10061-02-6 0.30 1 12/16/17 08:03 100-41-4 0.46 1 12/16/17 08:03 591-78-6 0.32 1 12/16/17 08:03 74-88-4 0.97 1 12/16/17 08:03 75-09-2 0.33 1 12/16/17 08:03 108-10-1 0.26 1 12/16/17 08:03 100-42-5 0.33 1 12/16/17 08:03 630-20-6 0.40 1 12/16/17 08:03 79-34-5 0.46 1 12/16/17 08:03 127-18-4 0.26 1 12/16/17 08:03 108-88-3 0.48 1 12/16/17 08:03 71-55-6 0.29 1 12/16/17 08:03 79-00-5 0.47 1 12/16/17 08:03 79-01-6 0.20 1 12/16/17 08:03 75-69-4 0.41 1 12/16/17 08:03 96-18-4 0.35 1 12/16/17 08:03 108-05-4 0.62 1 12/16/17 08:03 75-01-4 0.66 1 12/16/17 08:03 1330-20-7 1 12/16/17 08:03 460-00-4 1 12/16/17 08:03 17060-07-0 1 12/16/17 08:03 2037-26-5 0.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 12/15/17 01:39 Page 23 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-20 Lab ID: 92367133011 Collected: 12/13/17 16:30 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Antimony ND ug/L 6.0 3.9 1 12/20/17 13:35 12/28/17 06:49 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 06:49 7440-38-2 Barium 26.OJ ug/L 100 2.5 1 12/20/17 13:35 12/28/17 06:49 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 06:49 7440-41-7 Cadmium 1.6 ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 06:49 7440-43-9 Chromium ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:49 7440-47-3 Cobalt 12.4 ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:49 7440-48-4 Copper 3.8J ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:49 7440-50-8 Lead ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:49 7439-92-1 Nickel ND ug/L 50.0 2.5 1 12/20/17 13:35 12/28/17 06:49 7440-02-0 Selenium ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 06:49 7782-49-2 Silver ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:49 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 12/20/17 13:35 12/28/17 06:49 7440-62-2 Zinc 14.7 ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 20:52 7440-66-6 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020 Thallium 0.42 ug/L 0.10 0.028 1 01/08/18 15:17 01/09/18 09:17 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 12/16/17 08:21 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 12/16/17 08:21 107-13-1 Benzene ND ug/L 1.0 0.25 1 12/16/17 08:21 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 12/16/17 08:21 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 12/16/17 08:21 75-27-4 Bromoform ND ug/L 3.0 0.26 1 12/16/17 08:21 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 12/16/17 08:21 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 12/16/17 08:21 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 12/16/17 08:21 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 12/16/17 08:21 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 12/16/17 08:21 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 12/16/17 08:21 75-00-3 Chloroform ND ug/L 5.0 0.14 1 12/16/17 08:21 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 12/16/17 08:21 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 12/16/17 08:21 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 12/16/17 08:21 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 12/16/17 08:21 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 12/16/17 08:21 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 12/16/17 08:21 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 12/16/17 08:21 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 12/16/17 08:21 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 12/16/17 08:21 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 12/16/17 08:21 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 12/16/17 08:21 75-35-4 cis-1,2-Dichloroethene 0.56J ug/L 5.0 0.19 1 12/16/17 08:21 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 12/16/17 08:21 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 12/16/17 08:21 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-20 Lab ID: 92367133011 Collected: 12/13/17 16:30 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 180.1 Turbidity Turbidity Date: 01/10/2018 06:01 PM Analytical Method: EPA 8260 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 100 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 1.0 ND ug/L 5.0 95 % 70-130 97 % 70-130 102 % 70-130 Analytical Method: EPA 180.1 ND NTU 1.0 0.13 1 12/16/17 08:21 10061-01-5 0.26 1 12/16/17 08:21 10061-02-6 0.30 1 12/16/17 08:21 100-41-4 0.46 1 12/16/17 08:21 591-78-6 0.32 1 12/16/17 08:21 74-88-4 0.97 1 12/16/17 08:21 75-09-2 0.33 1 12/16/17 08:21 108-10-1 0.26 1 12/16/17 08:21 100-42-5 0.33 1 12/16/17 08:21 630-20-6 0.40 1 12/16/17 08:21 79-34-5 0.46 1 12/16/17 08:21 127-18-4 0.26 1 12/16/17 08:21 108-88-3 0.48 1 12/16/17 08:21 71-55-6 0.29 1 12/16/17 08:21 79-00-5 0.47 1 12/16/17 08:21 79-01-6 0.20 1 12/16/17 08:21 75-69-4 0.41 1 12/16/17 08:21 96-18-4 0.35 1 12/16/17 08:21 108-05-4 0.62 1 12/16/17 08:21 75-01-4 0.66 1 12/16/17 08:21 1330-20-7 1 12/16/17 08:21 460-00-4 1 12/16/17 08:21 17060-07-0 1 12/16/17 08:21 2037-26-5 0.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 12/15/17 01:39 Page 25 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-21 Lab ID: 92367133012 Collected: 12/13/17 15:27 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Antimony ND ug/L 6.0 3.9 1 12/20/17 13:35 12/28/17 06:52 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 06:52 7440-38-2 Barium 54.4J ug/L 100 2.5 1 12/20/17 13:35 12/28/17 06:52 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 06:52 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 06:52 7440-43-9 Chromium ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:52 7440-47-3 Cobalt ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:52 7440-48-4 Copper ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:52 7440-50-8 Lead ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:52 7439-92-1 Nickel ND ug/L 50.0 2.5 1 12/20/17 13:35 12/28/17 06:52 7440-02-0 Selenium ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 06:52 7782-49-2 Silver ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:52 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 12/20/17 13:35 12/28/17 06:52 7440-62-2 Zinc ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 20:55 7440-66-6 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020 Thallium 0.033J ug/L 0.10 0.028 1 01/08/18 15:17 01/09/18 09:20 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 12/16/17 08:39 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 12/16/17 08:39 107-13-1 Benzene ND ug/L 1.0 0.25 1 12/16/17 08:39 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 12/16/17 08:39 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 12/16/17 08:39 75-27-4 Bromoform ND ug/L 3.0 0.26 1 12/16/17 08:39 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 12/16/17 08:39 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 12/16/17 08:39 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 12/16/17 08:39 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 12/16/17 08:39 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 12/16/17 08:39 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 12/16/17 08:39 75-00-3 Chloroform ND ug/L 5.0 0.14 1 12/16/17 08:39 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 12/16/17 08:39 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 12/16/17 08:39 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 12/16/17 08:39 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 12/16/17 08:39 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 12/16/17 08:39 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 12/16/17 08:39 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 12/16/17 08:39 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 12/16/17 08:39 110-57-6 1,1-Dichloroethane 2.8J ug/L 5.0 0.32 1 12/16/17 08:39 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 12/16/17 08:39 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 12/16/17 08:39 75-35-4 cis-1,2-Dichloroethene 14.2 ug/L 5.0 0.19 1 12/16/17 08:39 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 12/16/17 08:39 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 12/16/17 08:39 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-21 Lab ID: 92367133012 Collected: 12/13/17 15:27 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 180.1 Turbidity Turbidity Date: 01/10/2018 06:01 PM Analytical Method: EPA 8260 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 100 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 0.82J ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 1.0 ND ug/L 5.0 92 % 70-130 93 % 70-130 104 % 70-130 Analytical Method: EPA 180.1 ND NTU 1.0 0.13 1 12/16/17 08:39 10061-01-5 0.26 1 12/16/17 08:39 10061-02-6 0.30 1 12/16/17 08:39 100-41-4 0.46 1 12/16/17 08:39 591-78-6 0.32 1 12/16/17 08:39 74-88-4 0.97 1 12/16/17 08:39 75-09-2 0.33 1 12/16/17 08:39 108-10-1 0.26 1 12/16/17 08:39 100-42-5 0.33 1 12/16/17 08:39 630-20-6 0.40 1 12/16/17 08:39 79-34-5 0.46 1 12/16/17 08:39 127-18-4 0.26 1 12/16/17 08:39 108-88-3 0.48 1 12/16/17 08:39 71-55-6 0.29 1 12/16/17 08:39 79-00-5 0.47 1 12/16/17 08:39 79-01-6 0.20 1 12/16/17 08:39 75-69-4 0.41 1 12/16/17 08:39 96-18-4 0.35 1 12/16/17 08:39 108-05-4 0.62 1 12/16/17 08:39 75-01-4 0.66 1 12/16/17 08:39 1330-20-7 1 12/16/17 08:39 460-00-4 1 12/16/17 08:39 17060-07-0 1 12/16/17 08:39 2037-26-5 0.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 12/15/17 01:39 Page 27 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-22 Lab ID: 92367133013 Collected: 12/13/17 11:10 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Vanadium Zinc 1400111 -1 �41 :4 9 [y :2 LTA 61 Thallium 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane Date: 01/10/2018 06:01 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 12/20/17 13:35 12/28/17 06:55 7440-36-0 ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 06:55 7440-38-2 45.OJ ug/L 100 2.5 1 12/20/17 13:35 12/28/17 06:55 7440-39-3 ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 06:55 7440-41-7 0.69J ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 06:55 7440-43-9 ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:55 7440-47-3 3.2J ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:55 7440-48-4 ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:55 7440-50-8 ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:55 7439-92-1 2.9J ug/L 50.0 2.5 1 12/20/17 13:35 12/28/17 06:55 7440-02-0 ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 06:55 7782-49-2 ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:55 7440-22-4 ND ug/L 25.0 2.5 1 12/20/17 13:35 12/28/17 06:55 7440-62-2 ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 20:58 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3020 0.16 ug/L 0.10 0.028 1 01/08/18 15:17 01/09/18 09:23 7440-28-0 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 12/16/17 08:56 67-64-1 ND ug/L 200 1.9 1 12/16/17 08:56 107-13-1 ND ug/L 1.0 0.25 1 12/16/17 08:56 71-43-2 ND ug/L 3.0 0.17 1 12/16/17 08:56 74-97-5 ND ug/L 1.0 0.18 1 12/16/17 08:56 75-27-4 ND ug/L 3.0 0.26 1 12/16/17 08:56 75-25-2 ND ug/L 10.0 0.29 1 12/16/17 08:56 74-83-9 ND ug/L 100 0.96 1 12/16/17 08:56 78-93-3 ND ug/L 100 1.2 1 12/16/17 08:56 75-15-0 ND ug/L 1.0 0.25 1 12/16/17 08:56 56-23-5 ND ug/L 3.0 0.23 1 12/16/17 08:56 108-90-7 ND ug/L 10.0 0.54 1 12/16/17 08:56 75-00-3 ND ug/L 5.0 0.14 1 12/16/17 08:56 67-66-3 ND ug/L 1.0 0.11 1 12/16/17 08:56 74-87-3 ND ug/L 13.0 2.0 1 12/16/17 08:56 96-12-8 ND ug/L 3.0 0.21 1 12/16/17 08:56 124-48-1 ND ug/L 1.0 0.27 1 12/16/17 08:56 106-93-4 ND ug/L 10.0 0.21 1 12/16/17 08:56 74-95-3 ND ug/L 5.0 0.30 1 12/16/17 08:56 95-50-1 0.77J ug/L 1.0 0.33 1 12/16/17 08:56 106-46-7 ND ug/L 100 1.0 1 12/16/17 08:56 110-57-6 0.42J ug/L 5.0 0.32 1 12/16/17 08:56 75-34-3 ND ug/L 1.0 0.24 1 12/16/17 08:56 107-06-2 ND ug/L 5.0 0.56 1 12/16/17 08:56 75-35-4 0.69J ug/L 5.0 0.19 1 12/16/17 08:56 156-59-2 ND ug/L 5.0 0.49 1 12/16/17 08:56 156-60-5 ND ug/L 1.0 0.27 1 12/16/17 08:56 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 28 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-22 Lab ID: 92367133013 Collected: 12/13/17 11:10 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 180.1 Turbidity Turbidity Date: 01/10/2018 06:01 PM Analytical Method: EPA 8260 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 100 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 1.0 ND ug/L 5.0 91 % 70-130 98 % 70-130 100 % 70-130 Analytical Method: EPA 180.1 0.62J NTU 1.0 0.13 1 12/16/17 08:56 10061-01-5 0.26 1 12/16/17 08:56 10061-02-6 0.30 1 12/16/17 08:56 100-41-4 0.46 1 12/16/17 08:56 591-78-6 0.32 1 12/16/17 08:56 74-88-4 0.97 1 12/16/17 08:56 75-09-2 0.33 1 12/16/17 08:56 108-10-1 0.26 1 12/16/17 08:56 100-42-5 0.33 1 12/16/17 08:56 630-20-6 0.40 1 12/16/17 08:56 79-34-5 0.46 1 12/16/17 08:56 127-18-4 0.26 1 12/16/17 08:56 108-88-3 0.48 1 12/16/17 08:56 71-55-6 0.29 1 12/16/17 08:56 79-00-5 0.47 1 12/16/17 08:56 79-01-6 0.20 1 12/16/17 08:56 75-69-4 0.41 1 12/16/17 08:56 96-18-4 0.35 1 12/16/17 08:56 108-05-4 0.62 1 12/16/17 08:56 75-01-4 0.66 1 12/16/17 08:56 1330-20-7 1 12/16/17 08:56 460-00-4 1 12/16/17 08:56 17060-07-0 1 12/16/17 08:56 2037-26-5 0.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 12/15/17 01:39 Page 29 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-23 Lab ID: 92367133014 Collected: 12/13/17 11:22 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Vanadium Zinc 1400111 -1 �41 :4 9 [y :2 LTA 61 Thallium 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane Date: 01/10/2018 06:01 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 12/20/17 13:35 12/28/17 06:58 7440-36-0 ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 06:58 7440-38-2 76.6J ug/L 100 2.5 1 12/20/17 13:35 12/28/17 06:58 7440-39-3 ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 06:58 7440-41-7 2.3 ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 06:58 7440-43-9 3.4J ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:58 7440-47-3 ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:58 7440-48-4 ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:58 7440-50-8 ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:58 7439-92-1 ND ug/L 50.0 2.5 1 12/20/17 13:35 12/28/17 06:58 7440-02-0 ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 06:58 7782-49-2 ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 06:58 7440-22-4 5.7J ug/L 25.0 2.5 1 12/20/17 13:35 12/28/17 06:58 7440-62-2 7.6J ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 21:01 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3020 0.058J ug/L 0.10 0.028 1 01/08/18 15:17 01/09/18 09:26 7440-28-0 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 12/16/17 09:14 67-64-1 ND ug/L 200 1.9 1 12/16/17 09:14 107-13-1 ND ug/L 1.0 0.25 1 12/16/17 09:14 71-43-2 ND ug/L 3.0 0.17 1 12/16/17 09:14 74-97-5 ND ug/L 1.0 0.18 1 12/16/17 09:14 75-27-4 ND ug/L 3.0 0.26 1 12/16/17 09:14 75-25-2 ND ug/L 10.0 0.29 1 12/16/17 09:14 74-83-9 ND ug/L 100 0.96 1 12/16/17 09:14 78-93-3 ND ug/L 100 1.2 1 12/16/17 09:14 75-15-0 ND ug/L 1.0 0.25 1 12/16/17 09:14 56-23-5 ND ug/L 3.0 0.23 1 12/16/17 09:14 108-90-7 ND ug/L 10.0 0.54 1 12/16/17 09:14 75-00-3 ND ug/L 5.0 0.14 1 12/16/17 09:14 67-66-3 ND ug/L 1.0 0.11 1 12/16/17 09:14 74-87-3 ND ug/L 13.0 2.0 1 12/16/17 09:14 96-12-8 ND ug/L 3.0 0.21 1 12/16/17 09:14 124-48-1 ND ug/L 1.0 0.27 1 12/16/17 09:14 106-93-4 ND ug/L 10.0 0.21 1 12/16/17 09:14 74-95-3 ND ug/L 5.0 0.30 1 12/16/17 09:14 95-50-1 ND ug/L 1.0 0.33 1 12/16/17 09:14 106-46-7 ND ug/L 100 1.0 1 12/16/17 09:14 110-57-6 0.36J ug/L 5.0 0.32 1 12/16/17 09:14 75-34-3 ND ug/L 1.0 0.24 1 12/16/17 09:14 107-06-2 ND ug/L 5.0 0.56 1 12/16/17 09:14 75-35-4 0.41J ug/L 5.0 0.19 1 12/16/17 09:14 156-59-2 ND ug/L 5.0 0.49 1 12/16/17 09:14 156-60-5 ND ug/L 1.0 0.27 1 12/16/17 09:14 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 30 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-23 Lab ID: 92367133014 Collected: 12/13/17 11:22 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 180.1 Turbidity Turbidity Date: 01/10/2018 06:01 PM Analytical Method: EPA 8260 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 100 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 1.0 ND ug/L 5.0 94 % 70-130 94 % 70-130 111 % 70-130 Analytical Method: EPA 180.1 5.0 NTU 1.0 0.13 1 12/16/17 09:14 10061-01-5 0.26 1 12/16/17 09:14 10061-02-6 0.30 1 12/16/17 09:14 100-41-4 0.46 1 12/16/17 09:14 591-78-6 0.32 1 12/16/17 09:14 74-88-4 0.97 1 12/16/17 09:14 75-09-2 0.33 1 12/16/17 09:14 108-10-1 0.26 1 12/16/17 09:14 100-42-5 0.33 1 12/16/17 09:14 630-20-6 0.40 1 12/16/17 09:14 79-34-5 0.46 1 12/16/17 09:14 127-18-4 0.26 1 12/16/17 09:14 108-88-3 0.48 1 12/16/17 09:14 71-55-6 0.29 1 12/16/17 09:14 79-00-5 0.47 1 12/16/17 09:14 79-01-6 0.20 1 12/16/17 09:14 75-69-4 0.41 1 12/16/17 09:14 96-18-4 0.35 1 12/16/17 09:14 108-05-4 0.62 1 12/16/17 09:14 75-01-4 0.66 1 12/16/17 09:14 1330-20-7 1 12/16/17 09:14 460-00-4 1 12/16/17 09:14 17060-07-0 1 12/16/17 09:14 2037-26-5 0.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 12/15/17 01:39 Page 31 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-3R Lab ID: 92367133015 Collected: 12/13/17 14:17 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Antimony ND ug/L 6.0 3.9 1 12/20/17 13:35 12/28/17 07:01 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 07:01 7440-38-2 Barium 6.9J ug/L 100 2.5 1 12/20/17 13:35 12/28/17 07:01 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 07:01 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 07:01 7440-43-9 Chromium ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 07:01 7440-47-3 Cobalt ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 07:01 7440-48-4 Copper ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 07:01 7440-50-8 Lead ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 07:01 7439-92-1 Nickel ND ug/L 50.0 2.5 1 12/20/17 13:35 12/28/17 07:01 7440-02-0 Selenium ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 07:01 7782-49-2 Silver ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 07:01 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 12/20/17 13:35 12/28/17 07:01 7440-62-2 Zinc ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 21:04 7440-66-6 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020 Thallium ND ug/L 0.10 0.028 1 01/08/18 15:17 01/09/18 09:28 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 12/16/17 09:32 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 12/16/17 09:32 107-13-1 Benzene ND ug/L 1.0 0.25 1 12/16/17 09:32 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 12/16/17 09:32 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 12/16/17 09:32 75-27-4 Bromoform ND ug/L 3.0 0.26 1 12/16/17 09:32 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 12/16/17 09:32 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 12/16/17 09:32 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 12/16/17 09:32 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 12/16/17 09:32 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 12/16/17 09:32 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 12/16/17 09:32 75-00-3 Chloroform ND ug/L 5.0 0.14 1 12/16/17 09:32 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 12/16/17 09:32 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 12/16/17 09:32 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 12/16/17 09:32 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 12/16/17 09:32 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 12/16/17 09:32 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 12/16/17 09:32 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 12/16/17 09:32 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 12/16/17 09:32 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 12/16/17 09:32 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 12/16/17 09:32 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 12/16/17 09:32 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 12/16/17 09:32 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 12/16/17 09:32 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 12/16/17 09:32 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-3R Lab ID: 92367133015 Collected: 12/13/17 14:17 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 180.1 Turbidity Turbidity Date: 01/10/2018 06:01 PM Analytical Method: EPA 8260 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 100 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 1.0 ND ug/L 5.0 95 % 70-130 96 % 70-130 104 % 70-130 Analytical Method: EPA 180.1 2.1 NTU 1.0 0.13 1 12/16/17 09:32 10061-01-5 0.26 1 12/16/17 09:32 10061-02-6 0.30 1 12/16/17 09:32 100-41-4 0.46 1 12/16/17 09:32 591-78-6 0.32 1 12/16/17 09:32 74-88-4 0.97 1 12/16/17 09:32 75-09-2 0.33 1 12/16/17 09:32 108-10-1 0.26 1 12/16/17 09:32 100-42-5 0.33 1 12/16/17 09:32 630-20-6 0.40 1 12/16/17 09:32 79-34-5 0.46 1 12/16/17 09:32 127-18-4 0.26 1 12/16/17 09:32 108-88-3 0.48 1 12/16/17 09:32 71-55-6 0.29 1 12/16/17 09:32 79-00-5 0.47 1 12/16/17 09:32 79-01-6 0.20 1 12/16/17 09:32 75-69-4 0.41 1 12/16/17 09:32 96-18-4 0.35 1 12/16/17 09:32 108-05-4 0.62 1 12/16/17 09:32 75-01-4 0.66 1 12/16/17 09:32 1330-20-7 1 12/16/17 09:32 460-00-4 1 12/16/17 09:32 17060-07-0 1 12/16/17 09:32 2037-26-5 0.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 12/14/17 23:10 Page 33 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-7 Lab ID: 92367133016 Collected: 12/13/17 13:30 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Antimony ND ug/L 6.0 3.9 1 12/20/17 13:35 12/28/17 07:05 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 07:05 7440-38-2 Barium 64.3J ug/L 100 2.5 1 12/20/17 13:35 12/28/17 07:05 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 07:05 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 07:05 7440-43-9 Chromium ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 07:05 7440-47-3 Cobalt 51.9 ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 07:05 7440-48-4 Copper ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 07:05 7440-50-8 Lead ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 07:05 7439-92-1 Nickel 2.6J ug/L 50.0 2.5 1 12/20/17 13:35 12/28/17 07:05 7440-02-0 Selenium ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 07:05 7782-49-2 Silver ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 07:05 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 12/20/17 13:35 12/28/17 07:05 7440-62-2 Zinc 7.7J ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 21:08 7440-66-6 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020 Thallium 0.21 ug/L 0.10 0.028 1 01/08/18 15:17 01/09/18 09:31 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 12/16/17 09:49 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 12/16/17 09:49 107-13-1 Benzene 0.28J ug/L 1.0 0.25 1 12/16/17 09:49 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 12/16/17 09:49 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 12/16/17 09:49 75-27-4 Bromoform ND ug/L 3.0 0.26 1 12/16/17 09:49 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 12/16/17 09:49 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 12/16/17 09:49 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 12/16/17 09:49 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 12/16/17 09:49 56-23-5 Chlorobenzene 2.3J ug/L 3.0 0.23 1 12/16/17 09:49 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 12/16/17 09:49 75-00-3 Chloroform ND ug/L 5.0 0.14 1 12/16/17 09:49 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 12/16/17 09:49 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 12/16/17 09:49 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 12/16/17 09:49 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 12/16/17 09:49 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 12/16/17 09:49 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 12/16/17 09:49 95-50-1 1,4-Dichlorobenzene 1.1 ug/L 1.0 0.33 1 12/16/17 09:49 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 12/16/17 09:49 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 12/16/17 09:49 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 12/16/17 09:49 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 12/16/17 09:49 75-35-4 cis-1,2-Dichloroethene 0.30J ug/L 5.0 0.19 1 12/16/17 09:49 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 12/16/17 09:49 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 12/16/17 09:49 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-7 Lab ID: 92367133016 Collected: 12/13/17 13:30 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 180.1 Turbidity Turbidity Date: 01/10/2018 06:01 PM Analytical Method: EPA 8260 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 100 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 1.0 ND ug/L 5.0 96 % 70-130 93 % 70-130 102 % 70-130 Analytical Method: EPA 180.1 1.1 NTU 1.0 0.13 1 12/16/17 09:49 10061-01-5 0.26 1 12/16/17 09:49 10061-02-6 0.30 1 12/16/17 09:49 100-41-4 0.46 1 12/16/17 09:49 591-78-6 0.32 1 12/16/17 09:49 74-88-4 0.97 1 12/16/17 09:49 75-09-2 0.33 1 12/16/17 09:49 108-10-1 0.26 1 12/16/17 09:49 100-42-5 0.33 1 12/16/17 09:49 630-20-6 0.40 1 12/16/17 09:49 79-34-5 0.46 1 12/16/17 09:49 127-18-4 0.26 1 12/16/17 09:49 108-88-3 0.48 1 12/16/17 09:49 71-55-6 0.29 1 12/16/17 09:49 79-00-5 0.47 1 12/16/17 09:49 79-01-6 0.20 1 12/16/17 09:49 75-69-4 0.41 1 12/16/17 09:49 96-18-4 0.35 1 12/16/17 09:49 108-05-4 0.62 1 12/16/17 09:49 75-01-4 0.66 1 12/16/17 09:49 1330-20-7 1 12/16/17 09:49 460-00-4 1 12/16/17 09:49 17060-07-0 1 12/16/17 09:49 2037-26-5 0.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 12/14/17 23:10 Page 35 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-9 Lab ID: 92367133017 Collected: 12/13/17 16:30 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Antimony ND ug/L 6.0 3.9 1 12/20/17 13:35 12/28/17 07:14 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 07:14 7440-38-2 Barium 45.OJ ug/L 100 2.5 1 12/20/17 13:35 12/28/17 07:14 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 07:14 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 12/20/17 13:35 12/28/17 07:14 7440-43-9 Chromium ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 07:14 7440-47-3 Cobalt 187 ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 07:14 7440-48-4 Copper ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 07:14 7440-50-8 Lead ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 07:14 7439-92-1 Nickel 6.7J ug/L 50.0 2.5 1 12/20/17 13:35 12/28/17 07:14 7440-02-0 Selenium ND ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 07:14 7782-49-2 Silver ND ug/L 10.0 2.5 1 12/20/17 13:35 12/28/17 07:14 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 12/20/17 13:35 12/28/17 07:14 7440-62-2 Zinc 10.1 ug/L 10.0 5.0 1 12/20/17 13:35 12/28/17 21:11 7440-66-6 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020 Thallium 0.37 ug/L 0.10 0.028 1 01/08/18 15:17 01/09/18 09:34 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 12/16/17 10:07 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 12/16/17 10:07 107-13-1 Benzene 1.9 ug/L 1.0 0.25 1 12/16/17 10:07 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 12/16/17 10:07 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 12/16/17 10:07 75-27-4 Bromoform ND ug/L 3.0 0.26 1 12/16/17 10:07 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 12/16/17 10:07 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 12/16/17 10:07 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 12/16/17 10:07 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 12/16/17 10:07 56-23-5 Chlorobenzene 1.81 ug/L 3.0 0.23 1 12/16/17 10:07 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 12/16/17 10:07 75-00-3 Chloroform ND ug/L 5.0 0.14 1 12/16/17 10:07 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 12/16/17 10:07 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 12/16/17 10:07 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 12/16/17 10:07 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 12/16/17 10:07 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 12/16/17 10:07 74-95-3 1,2-Dichlorobenzene 1.1J ug/L 5.0 0.30 1 12/16/17 10:07 95-50-1 1,4-Dichlorobenzene 4.9 ug/L 1.0 0.33 1 12/16/17 10:07 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 12/16/17 10:07 110-57-6 1,1-Dichloroethane 1.8J ug/L 5.0 0.32 1 12/16/17 10:07 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 12/16/17 10:07 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 12/16/17 10:07 75-35-4 cis-1,2-Dichloroethene 36.4 ug/L 5.0 0.19 1 12/16/17 10:07 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 12/16/17 10:07 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 12/16/17 10:07 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Sample: MW-9 Lab ID: 92367133017 Collected: 12/13/17 16:30 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 180.1 Turbidity Turbidity Date: 01/10/2018 06:01 PM Analytical Method: EPA 8260 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 100 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 17.1 ug/L 1.0 ND ug/L 5.0 91 % 70-130 94 % 70-130 110 % 70-130 Analytical Method: EPA 180.1 1.2 NTU 1.0 0.13 0.26 0.30 0.46 0.32 0.97 0.33 0.26 0.33 0.40 0.46 0.26 0.48 0.29 0.47 0.20 0.41 0.35 0.62 0.66 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 12/16/17 10:07 10061-01-5 12/16/17 10:07 10061-02-6 12/16/17 10:07 100-41-4 12/16/17 10:07 591-78-6 12/16/17 10:07 74-88-4 12/16/17 10:07 75-09-2 12/16/17 10:07 108-10-1 12/16/17 10:07 100-42-5 12/16/17 10:07 630-20-6 12/16/17 10:07 79-34-5 12/16/17 10:07 127-18-4 12/16/17 10:07 108-88-3 12/16/17 10:07 71-55-6 12/16/17 10:07 79-00-5 12/16/17 10:07 79-01-6 12/16/17 10:07 75-69-4 12/16/17 10:07 96-18-4 12/16/17 10:07 108-05-4 12/16/17 10:07 75-01-4 12/16/17 10:07 1330-20-7 12/16/17 10:07 460-00-4 12/16/17 10:07 17060-07-0 12/16/17 10:07 2037-26-5 12/14/17 23:10 D6 Page 37 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 QC Batch: 391734 Analysis Method: EPA 6010 QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92367133001, 92367133003, 92367133004, 92367133005, 92367133006, 92367133007, 92367133008, 92367133009,92367133010,92367133011,92367133012,92367133013,92367133014,92367133015, 92367133016,92367133017 METHOD BLANK: 2173201 Matrix: Water Associated Lab Samples: 92367133001, 92367133003, 92367133004, 92367133005, 92367133006, 92367133007, 92367133008, 92367133009,92367133010,92367133011,92367133012,92367133013,92367133014,92367133015, 92367133016,92367133017 Parameter Units Blank Result Reporting Limit MDL Antimony ug/L ND 5.0 3.9 Arsenic ug/L ND 10.0 5.0 Barium ug/L ND 5.0 2.5 Beryllium ug/L ND 1.0 0.50 Cadmium ug/L ND 1.0 0.50 Chromium ug/L ND 5.0 2.5 Cobalt ug/L ND 5.0 2.5 Copper ug/L ND 5.0 2.5 Lead ug/L ND 5.0 2.5 Nickel ug/L ND 5.0 2.5 Selenium ug/L ND 10.0 5.0 Silver ug/L ND 5.0 2.5 Vanadium ug/L ND 5.0 2.5 Zinc ug/L ND 10.0 5.0 Analyzed Qualifiers 12/28/17 06:01 12/28/17 06:01 12/28/17 06:01 12/28/17 06:01 12/28/17 06:01 12/28/17 06:01 12/28/17 06:01 12/28/17 06:01 12/28/17 06:01 12/28/17 06:01 12/28/17 06:01 12/28/17 06:01 12/28/17 06:01 12/28/17 19:58 LABORATORY CONTROL SAMPLE: Parameter 2173202 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 500 454 91 80-120 Arsenic ug/L 500 439 88 80-120 Barium ug/L 500 470 94 80-120 Beryllium ug/L 500 467 93 80-120 Cadmium ug/L 500 454 91 80-120 Chromium ug/L 500 470 94 80-120 Cobalt ug/L 500 453 91 80-120 Copper ug/L 500 472 94 80-120 Lead ug/L 500 445 89 80-120 Nickel ug/L 500 456 91 80-120 Selenium ug/L 500 437 87 80-120 Silver ug/L 250 231 92 80-120 Vanadium ug/L 500 466 93 80-120 Zinc ug/L 500 448 90 80-120 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: Surry Closed -Mt. Airy 92367133 (UIC) MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2173203 2173204 MS MSD 92367133001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 511 506 102 101 75-125 1 20 Arsenic ug/L ND 500 500 488 482 98 96 75-125 1 20 Barium ug/L 127 500 500 648 637 104 102 75-125 2 20 Beryllium ug/L ND 500 500 492 489 98 98 75-125 1 20 Cadmium ug/L 3.0 500 500 480 478 95 95 75-125 1 20 Chromium ug/L 4.2J 500 500 491 482 97 96 75-125 2 20 Cobalt ug/L 11.1 500 500 500 495 98 97 75-125 1 20 Copper ug/L 6.1J 500 500 521 517 103 102 75-125 1 20 Lead ug/L ND 500 500 485 480 97 96 75-125 1 20 Nickel ug/L 5.1J 500 500 488 482 97 95 75-125 1 20 Selenium ug/L ND 500 500 444 440 89 88 75-125 1 20 Silver ug/L ND 250 250 249 248 99 99 75-125 0 20 Vanadium ug/L ND 500 500 501 494 100 99 75-125 1 20 Zinc ug/L 48.3 500 500 514 504 93 91 75-125 2 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 QC Batch: 517022 Analysis Method: EPA 6020B QC Batch Method: EPA 3020 Analysis Description: 6020E Water UPD5 Associated Lab Samples: 92367133001, 92367133003, 92367133004, 92367133005, 92367133006, 92367133007, 92367133008, 92367133009,92367133010,92367133011,92367133012,92367133013,92367133014,92367133015, 92367133016,92367133017 METHOD BLANK: 2809368 Matrix: Water Associated Lab Samples: 92367133001, 92367133003, 92367133004, 92367133005, 92367133006, 92367133007, 92367133008, 92367133009,92367133010,92367133011,92367133012,92367133013,92367133014,92367133015, 92367133016,92367133017 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Thallium ug/L ND 0.10 0.028 01/09/18 08:10 LABORATORY CONTROL SAMPLE: 2809369 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Thallium ug/L 100 109 109 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2809370 2809371 MS MSD 92367133001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Thallium ug/L 0.15 100 100 107 104 107 104 75-125 3 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 40 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 QC Batch: 391129 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92367133001, 92367133003, 92367133004, 92367133005, 92367133006, 92367133007, 92367133008, 92367133009,92367133010,92367133011,92367133012,92367133013,92367133014,92367133015, 92367133016 METHOD BLANK: 2170174 Matrix: Water Associated Lab Samples: 92367133001, 92367133003, 92367133004, 92367133005, 92367133006, 92367133007, 92367133008, 92367133009,92367133010,92367133011,92367133012,92367133013,92367133014,92367133015, 92367133016 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 5.0 0.33 12/16/17 03:39 1,1,1-Trichloroethane ug/L ND 1.0 0.48 12/16/17 03:39 1,1,2,2-Tetrachloroethane ug/L ND 3.0 0.40 12/16/17 03:39 1,1,2-Trichloroethane ug/L ND 1.0 0.29 12/16/17 03:39 1,1-Dichloroethane ug/L ND 5.0 0.32 12/16/17 03:39 1,1-Dichloroethene ug/L ND 5.0 0.56 12/16/17 03:39 1,2,3-Trichloropropane ug/L ND 1.0 0.41 12/16/17 03:39 1,2-Dibromo-3-chloropropane ug/L ND 13.0 2.0 12/16/17 03:39 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 12/16/17 03:39 1,2-Dichlorobenzene ug/L ND 5.0 0.30 12/16/17 03:39 1,2-Dichloroethane ug/L ND 1.0 0.24 12/16/17 03:39 1,2-Dichloropropane ug/L ND 1.0 0.27 12/16/17 03:39 1,4-Dichlorobenzene ug/L ND 1.0 0.33 12/16/17 03:39 2-Butanone (MEK) ug/L ND 100 0.96 12/16/17 03:39 2-Hexanone ug/L ND 50.0 0.46 12/16/17 03:39 4-Methyl-2-pentanone (MIBK) ug/L ND 100 0.33 12/16/17 03:39 Acetone ug/L ND 100 10.0 12/16/17 03:39 Acrylonitrile ug/L ND 200 1.9 12/16/17 03:39 Benzene ug/L ND 1.0 0.25 12/16/17 03:39 Bromochloromethane ug/L ND 3.0 0.17 12/16/17 03:39 Bromodichloromethane ug/L ND 1.0 0.18 12/16/17 03:39 Bromoform ug/L ND 3.0 0.26 12/16/17 03:39 Bromomethane ug/L ND 10.0 0.29 12/16/17 03:39 Carbon disulfide ug/L ND 100 1.2 12/16/17 03:39 Carbon tetrachloride ug/L ND 1.0 0.25 12/16/17 03:39 Chlorobenzene ug/L ND 3.0 0.23 12/16/17 03:39 Chloroethane ug/L ND 10.0 0.54 12/16/17 03:39 Chloroform ug/L 0.14J 5.0 0.14 12/16/17 03:39 Chloromethane ug/L ND 1.0 0.11 12/16/17 03:39 cis-1,2-Dichloroethene ug/L ND 5.0 0.19 12/16/17 03:39 cis-1,3-Dichloropropene ug/L ND 1.0 0.13 12/16/17 03:39 Dibromochloromethane ug/L ND 3.0 0.21 12/16/17 03:39 Dibromomethane ug/L ND 10.0 0.21 12/16/17 03:39 Ethylbenzene ug/L ND 1.0 0.30 12/16/17 03:39 lodomethane ug/L ND 10.0 0.32 12/16/17 03:39 Methylene Chloride ug/L ND 1.0 0.97 12/16/17 03:39 Styrene ug/L ND 1.0 0.26 12/16/17 03:39 Tetrachloroethene ug/L ND 1.0 0.46 12/16/17 03:39 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 METHOD BLANK: 2170174 Matrix: Water Associated Lab Samples: 92367133001, 92367133003, 92367133004, 92367133005, 92367133006, 92367133007, 92367133008, 92367133009,92367133010,92367133011,92367133012,92367133013,92367133014,92367133015, 92367133016 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Toluene ug/L ND 1.0 0.26 12/16/17 03:39 trans-1,2-Dichloroethene ug/L ND 5.0 0.49 12/16/17 03:39 trans- 1,3-Dichloropropene ug/L ND 1.0 0.26 12/16/17 03:39 trans-1,4-Dichloro-2-butene ug/L ND 100 1.0 12/16/17 03:39 Trichloroethene ug/L ND 1.0 0.47 12/16/17 03:39 Trichlorofluoromethane ug/L ND 1.0 0.20 12/16/17 03:39 Vinyl acetate ug/L ND 50.0 0.35 12/16/17 03:39 Vinyl chloride ug/L ND 1.0 0.62 12/16/17 03:39 Xylene (Total) ug/L ND 5.0 0.66 12/16/17 03:39 1,2-Dichloroethane-d4 (S) % 97 70-130 12/16/17 03:39 4-Bromofluorobenzene (S) % 95 70-130 12/16/17 03:39 Toluene-d8 (S) % 103 70-130 12/16/17 03:39 LABORATORY CONTROL SAMPLE: Parameter 2170175 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 49.9 100 80-125 1,1,1-Trichloroethane ug/L 50 47.9 96 71-129 1,1,2,2-Tetrachloroethane ug/L 50 48.1 96 79-124 1,1,2-Trichloroethane ug/L 50 57.1 114 85-125 1,1-Dichloroethane ug/L 50 49.3 99 73-126 1,1-Dichloroethene ug/L 50 47.8 96 66-135 1,2,3-Trichloropropane ug/L 50 50.1 100 75-130 1,2-Dibromo-3-chloropropane ug/L 50 48.5 97 71-133 1,2-Dibromoethane (EDB) ug/L 50 49.2 98 83-124 1,2-Dichlorobenzene ug/L 50 50.2 100 80-133 1,2-Dichloroethane ug/L 50 48.0 96 67-128 1,2-Dichloropropane ug/L 50 51.2 102 75-132 1,4-Dichlorobenzene ug/L 50 48.9 98 78-130 2-Butanone (MEK) ug/L 100 102 102 61-144 2-Hexanone ug/L 100 113 113 68-143 4-Methyl-2-pentanone (MIBK) ug/L 100 117 117 72-135 Acetone ug/L 100 105 105 48-146 Acrylonitrile ug/L 250 261 105 40-160 Benzene ug/L 50 48.9 98 80-125 Bromochloromethane ug/L 50 49.4 99 71-125 Bromodichloromethane ug/L 50 49.1 98 78-124 Bromoform ug/L 50 48.0 96 71-128 Bromomethane ug/L 50 50.8 102 40-160 Carbon disulfide ug/L 50 47.3J 95 50-160 Carbon tetrachloride ug/L 50 48.5 97 69-131 Chlorobenzene ug/L 50 48.6 97 81-122 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 LABORATORY CONTROL SAMPLE: Parameter 2170175 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Chloroethane ug/L 50 58.3 117 39-148 Chloroform ug/L 50 45.7 91 73-127 Chloromethane ug/L 50 47.1 94 44-146 cis-1,2-Dichloroethene ug/L 50 51.2 102 74-124 cis-1,3-Dichloropropene ug/L 50 56.1 112 72-132 Dibromochloromethane ug/L 50 48.9 98 78-125 Dibromomethane ug/L 50 51.3 103 82-120 Ethylbenzene ug/L 50 50.7 101 79-121 lodomethane ug/L 100 104 104 39-154 Methylene Chloride ug/L 50 51.9 104 64-133 Styrene ug/L 50 50.6 101 84-126 Tetrachloroethene ug/L 50 46.6 93 78-122 Toluene ug/L 50 53.5 107 80-121 trans-1,2-Dichloroethene ug/L 50 49.1 98 71-127 trans- 1,3-Dichloropropene ug/L 50 58.2 116 69-141 trans-1,4-Dichloro-2-butene ug/L 50 59.9J 120 40-160 Trichloroethene ug/L 50 48.1 96 78-122 Trichlorofluoromethane ug/L 50 45.3 91 53-137 Vinyl acetate ug/L 100 113 113 40-160 Vinyl chloride ug/L 50 51.7 103 58-137 Xylene (Total) ug/L 150 155 103 81-126 1,2-Dichloroethane-d4 (S) % 91 70-130 4-Bromofluorobenzene (S) % 101 70-130 Toluene-d8 (S) % 111 70-130 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2172259 MS 92367098006 Spike Parameter Units Result Conc. MSD Spike Conc. 2172260 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits Max RPD RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 22.4 21.8 112 109 70-130 3 30 1,1,1-Trichloroethane ug/L ND 20 20 23.4 23.0 117 115 70-130 2 30 1,1,2,2-Tetrachloroethane ug/L ND 20 20 20.8 19.9 104 99 70-130 4 30 1,1,2-Trichloroethane ug/L ND 20 20 22.1 21.4 110 107 70-130 3 30 1,1-Dichloroethane ug/L ND 20 20 21.6 21.5 108 107 70-130 1 30 1,1-Dichloroethene ug/L ND 20 20 23.6 23.5 118 117 70-166 0 30 1,2,3-Trichloropropane ug/L ND 20 20 21.8 19.8 109 99 70-130 9 30 1,2-Dibromo-3- ug/L ND 20 20 23.4 21.9 117 109 70-130 7 30 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 20 20 22.5 21.4 112 107 70-130 5 30 1,2-Dichlorobenzene ug/L ND 20 20 22.5 21.6 113 108 70-130 4 30 1,2-Dichloroethane ug/L ND 20 20 20.0 19.7 100 99 70-130 1 30 1,2-Dichloropropane ug/L ND 20 20 22.2 21.1 111 106 70-130 5 30 1,4-Dichlorobenzene ug/L ND 20 20 22.8 21.4 114 107 70-130 6 30 2-Butanone (MEK) ug/L ND 40 40 45.5J 41.5J 114 104 70-130 9 30 2-Hexanone ug/L ND 40 40 47.2J 43.6J 118 109 70-130 8 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2172259 2172260 MS MSD 92367098006 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 4-Methyl-2-pentanone ug/L ND 40 40 44.1J 42.OJ 110 105 70-130 5 30 (MIBK) Acetone ug/L ND 40 40 46.7J 41.8J 117 105 70-130 11 30 Acrylonitrile ug/L ND 100 100 107J 99.91 107 100 70-130 7 30 Benzene ug/L ND 20 20 22.3 21.3 112 107 70-148 5 30 Bromochloromethane ug/L ND 20 20 22.0 20.8 110 104 70-130 5 30 Bromodichloromethane ug/L ND 20 20 22.1 21.1 110 105 70-130 5 30 Bromoform ug/L ND 20 20 21.6 20.6 108 103 70-130 5 30 Bromomethane ug/L ND 20 20 19.2 19.9 96 100 70-130 4 30 Carbon disulfide ug/L ND 20 20 22.7J 21.8J 113 109 70-130 4 30 Carbon tetrachloride ug/L ND 20 20 24.4 23.9 122 119 70-130 2 30 Chlorobenzene ug/L ND 20 20 22.7 21.7 113 109 70-146 4 30 Chloroethane ug/L ND 20 20 25.7 24.3 129 122 70-130 6 30 Chloroform ug/L ND 20 20 21.3 21.3 107 106 70-130 0 30 Chloromethane ug/L ND 20 20 23.0 22.5 115 113 70-130 2 30 cis-1,2-Dichloroethene ug/L ND 20 20 21.9 21.8 109 109 70-130 0 30 cis-1,3-Dichloropropene ug/L ND 20 20 22.3 21.0 111 105 70-130 6 30 Dibromochloromethane ug/L ND 20 20 23.4 22.3 117 111 70-130 5 30 Dibromomethane ug/L ND 20 20 21.8 21.0 109 105 70-130 3 30 Ethylbenzene ug/L ND 20 20 23.6 22.7 118 113 70-130 4 30 Iodomethane ug/L ND 40 40 36.6 34.0 92 85 70-130 7 30 Methylene Chloride ug/L ND 20 20 18.2 17.7 91 88 70-130 3 30 Styrene ug/L ND 20 20 22.1 21.9 111 110 70-130 1 30 Tetrachloroethene ug/L ND 20 20 23.9 23.4 119 117 70-130 2 30 Toluene ug/L ND 20 20 22.7 21.9 114 109 70-155 4 30 trans-1,2-Dichloroethene ug/L ND 20 20 22.2 22.0 111 110 70-130 1 30 trans-1,3-Dichloropropene ug/L ND 20 20 21.5 21.3 107 106 70-130 1 30 trans-1,4-Dichloro-2-butene ug/L ND 20 20 24.9J 21.2J 124 106 70-130 16 30 Trichloroethene ug/L ND 20 20 23.3 22.2 116 111 69-151 5 30 Trichlorofluoromethane ug/L ND 20 20 24.1 23.7 120 118 70-130 2 30 Vinyl acetate ug/L ND 40 40 37.7J 35.3J 94 88 70-130 7 30 Vinyl chloride ug/L ND 20 20 26.2 26.2 131 131 70-130 0 30 M1 1,2-Dichloroethane-d4 (S) % 97 96 70-130 4-Bromofluorobenzene (S) % 98 97 70-130 Toluene-d8 (S) % 100 99 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 QC Batch: 391131 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92367133017 METHOD BLANK: 2170179 Associated Lab Samples: 92367133017 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 0.33 12/16/17 03:56 1,1,1-Trichloroethane ug/L ND 1.0 0.48 12/16/17 03:56 1,1,2,2-Tetrachloroethane ug/L ND 3.0 0.40 12/16/17 03:56 1,1,2-Trichloroethane ug/L ND 1.0 0.29 12/16/17 03:56 1,1-Dichloroethane ug/L ND 5.0 0.32 12/16/17 03:56 1,1-Dichloroethene ug/L ND 5.0 0.56 12/16/17 03:56 1,2,3-Trichloropropane ug/L ND 1.0 0.41 12/16/17 03:56 1,2-Dibromo-3-chloropropane ug/L ND 13.0 2.0 12/16/17 03:56 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 12/16/17 03:56 1,2-Dichlorobenzene ug/L ND 5.0 0.30 12/16/17 03:56 1,2-Dichloroethane ug/L ND 1.0 0.24 12/16/17 03:56 1,2-Dichloropropane ug/L ND 1.0 0.27 12/16/17 03:56 1,4-Dichlorobenzene ug/L ND 1.0 0.33 12/16/17 03:56 2-Butanone (MEK) ug/L ND 100 0.96 12/16/17 03:56 2-Hexanone ug/L ND 50.0 0.46 12/16/17 03:56 4-Methyl-2-pentanone (MIBK) ug/L ND 100 0.33 12/16/17 03:56 Acetone ug/L ND 100 10.0 12/16/17 03:56 Acrylonitrile ug/L ND 200 1.9 12/16/17 03:56 Benzene ug/L ND 1.0 0.25 12/16/17 03:56 Bromochloromethane ug/L ND 3.0 0.17 12/16/17 03:56 Bromodichloromethane ug/L ND 1.0 0.18 12/16/17 03:56 Bromoform ug/L ND 3.0 0.26 12/16/17 03:56 Bromomethane ug/L ND 10.0 0.29 12/16/17 03:56 Carbon disulfide ug/L ND 100 1.2 12/16/17 03:56 Carbon tetrachloride ug/L ND 1.0 0.25 12/16/17 03:56 Chlorobenzene ug/L ND 3.0 0.23 12/16/17 03:56 Chloroethane ug/L ND 10.0 0.54 12/16/17 03:56 Chloroform ug/L 0.14J 5.0 0.14 12/16/17 03:56 Chloromethane ug/L ND 1.0 0.11 12/16/17 03:56 cis-1,2-Dichloroethene ug/L ND 5.0 0.19 12/16/17 03:56 cis-1,3-Dichloropropene ug/L ND 1.0 0.13 12/16/17 03:56 Dibromochloromethane ug/L ND 3.0 0.21 12/16/17 03:56 Dibromomethane ug/L ND 10.0 0.21 12/16/17 03:56 Ethylbenzene ug/L ND 1.0 0.30 12/16/17 03:56 lodomethane ug/L ND 10.0 0.32 12/16/17 03:56 Methylene Chloride ug/L ND 1.0 0.97 12/16/17 03:56 Styrene ug/L ND 1.0 0.26 12/16/17 03:56 Tetrachloroethene ug/L ND 1.0 0.46 12/16/17 03:56 Toluene ug/L ND 1.0 0.26 12/16/17 03:56 trans-1,2-Dichloroethene ug/L ND 5.0 0.49 12/16/17 03:56 trans- 1,3-Dichloropropene ug/L ND 1.0 0.26 12/16/17 03:56 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 METHOD BLANK: 2170179 Matrix: Water Associated Lab Samples: 92367133017 Blank Reporting Parameter Units Result Limit MDL Analyzed trans-1,4-Dichloro-2-butene ug/L ND 100 1.0 12/16/17 03:56 Trichloroethene ug/L ND 1.0 0.47 12/16/17 03:56 Trichlorofluoromethane ug/L ND 1.0 0.20 12/16/17 03:56 Vinyl acetate ug/L ND 50.0 0.35 12/16/17 03:56 Vinyl chloride ug/L ND 1.0 0.62 12/16/17 03:56 Xylene (Total) ug/L ND 5.0 0.66 12/16/17 03:56 1,2-Dichloroethane-d4 (S) % 93 70-130 12/16/17 03:56 4-Bromofluorobenzene (S) % 96 70-130 12/16/17 03:56 Toluene-d8 (S) % 111 70-130 12/16/17 03:56 LABORATORY CONTROL SAMPLE: Parameter 2170180 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 50.2 100 80-125 1,1,1-Trichloroethane ug/L 50 47.6 95 71-129 1,1,2,2-Tetrachloroethane ug/L 50 48.3 97 79-124 1,1,2-Trichloroethane ug/L 50 52.5 105 85-125 1,1-Dichloroethane ug/L 50 45.6 91 73-126 1,1-Dichloroethene ug/L 50 47.0 94 66-135 1,2,3-Trichloropropane ug/L 50 50.6 101 75-130 1,2-Dibromo-3-chloropropane ug/L 50 50.3 101 71-133 1,2-Dibromoethane (EDB) ug/L 50 50.4 101 83-124 1,2-Dichlorobenzene ug/L 50 52.2 104 80-133 1,2-Dichloroethane ug/L 50 51.3 103 67-128 1,2-Dichloropropane ug/L 50 52.0 104 75-132 1,4-Dichlorobenzene ug/L 50 50.3 101 78-130 2-Butanone (MEK) ug/L 100 103 103 61-144 2-Hexanone ug/L 100 112 112 68-143 4-Methyl-2-pentanone (MIBK) ug/L 100 105 105 72-135 Acetone ug/L 100 98.6J 99 48-146 Acrylonitrile ug/L 250 234 94 40-160 Benzene ug/L 50 50.1 100 80-125 Bromochloromethane ug/L 50 48.5 97 71-125 Bromodichloromethane ug/L 50 51.0 102 78-124 Bromoform ug/L 50 49.0 98 71-128 Bromomethane ug/L 50 49.6 99 40-160 Carbon disulfide ug/L 50 45.1J 90 50-160 Carbon tetrachloride ug/L 50 48.2 96 69-131 Chlorobenzene ug/L 50 49.8 100 81-122 Chloroethane ug/L 50 55.0 110 39-148 Chloroform ug/L 50 45.7 91 73-127 Chloromethane ug/L 50 46.8 94 44-146 cis-1,2-Dichloroethene ug/L 50 48.2 96 74-124 cis-1,3-Dichloropropene ug/L 50 57.0 114 72-132 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 LABORATORY CONTROL SAMPLE: 2170180 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Dibromochloromethane ug/L 50 49.8 100 78-125 Dibromomethane ug/L 50 52.4 105 82-120 Ethylbenzene ug/L 50 49.9 100 79-121 lodomethane ug/L 100 98.1 98 39-154 Methylene Chloride ug/L 50 47.8 96 64-133 Styrene ug/L 50 50.5 101 84-126 Tetrachloroethene ug/L 50 48.3 97 78-122 Toluene ug/L 50 51.1 102 80-121 trans-1,2-Dichloroethene ug/L 50 46.0 92 71-127 trans- 1,3-Dichloropropene ug/L 50 52.7 105 69-141 trans-1,4-Dichloro-2-butene ug/L 50 58.7J 117 40-160 Trichloroethene ug/L 50 48.9 98 78-122 Trichlorofluoromethane ug/L 50 45.6 91 53-137 Vinyl acetate ug/L 100 99.5 100 40-160 Vinyl chloride ug/L 50 51.7 103 58-137 Xylene (Total) ug/L 150 154 103 81-126 1,2-Dichloroethane-d4 (S) % 96 70-130 4-Bromofluorobenzene (S) % 97 70-130 Toluene-d8 (S) % 105 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2172253 2172254 MS MSD 92367135005 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 21.8 21.0 109 105 70-130 4 30 1,1,1-Trichloroethane ug/L ND 20 20 23.1 22.8 116 114 70-130 1 30 1,1,2,2-Tetrachloroethane ug/L ND 20 20 20.4 19.9 102 100 70-130 2 30 1,1,2-Trichloroethane ug/L ND 20 20 21.1 21.0 105 105 70-130 0 30 1,1-Dichloroethane ug/L 2.5J 20 20 24.5 23.9 110 107 70-130 3 30 1,1-Dichloroethene ug/L ND 20 20 23.6 23.4 118 117 70-166 1 30 1,2,3-Trichloropropane ug/L ND 20 20 21.0 20.1 105 100 70-130 5 30 1,2-Dibromo-3- ug/L ND 20 20 22.0 20.5 110 103 70-130 7 30 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 20 20 21.8 21.1 109 105 70-130 3 30 1,2-Dichlorobenzene ug/L ND 20 20 22.0 21.6 110 108 70-130 2 30 1,2-Dichloroethane ug/L ND 20 20 20.2 19.8 101 99 70-130 2 30 1,2-Dichloropropane ug/L ND 20 20 21.3 20.7 106 104 70-130 3 30 1,4-Dichlorobenzene ug/L ND 20 20 21.8 21.3 109 106 70-130 3 30 2-Butanone (MEK) ug/L ND 40 40 44AJ 42.2J 111 106 70-130 5 30 2-Hexanone ug/L ND 40 40 44.8J 42.9J 112 107 70-130 4 30 4-Methyl-2-pentanone ug/L ND 40 40 42.6J 40.8J 107 102 70-130 4 30 (MIBK) Acetone ug/L ND 40 40 46AJ 44AJ 116 111 70-130 4 30 Acrylonitrile ug/L ND 100 100 105J 1001 105 100 70-130 5 30 Benzene ug/L ND 20 20 21.5 21.4 107 107 70-148 0 30 Bromochloromethane ug/L ND 20 20 21.6 20.9 108 104 70-130 3 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2172253 2172254 MS MSD 92367135005 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Bromodichloromethane ug/L ND 20 20 21.0 21.3 105 106 70-130 1 30 Bromoform ug/L ND 20 20 20.8 19.6 104 98 70-130 6 30 Bromomethane ug/L ND 20 20 20.2 20.6 101 103 70-130 2 30 Carbon disulfide ug/L ND 20 20 22.3J 22.OJ 111 110 70-130 1 30 Carbon tetrachloride ug/L ND 20 20 23.5 23.8 118 119 70-130 1 30 Chlorobenzene ug/L ND 20 20 21.5 21.6 107 108 70-146 0 30 Chloroethane ug/L ND 20 20 26.9 26.2 134 131 70-130 3 30 M1 Chloroform ug/L ND 20 20 21.5 21.0 107 105 70-130 2 30 Chloromethane ug/L ND 20 20 23.1 19.3 115 96 70-130 18 30 cis-1,2-Dichloroethene ug/L ND 20 20 22.7 21.8 113 108 70-130 4 30 cis-1,3-Dichloropropene ug/L ND 20 20 20.7 20.9 103 105 70-130 1 30 Dibromochloromethane ug/L ND 20 20 21.8 21.2 109 106 70-130 3 30 Dibromomethane ug/L ND 20 20 21.2 20.8 106 104 70-130 2 30 Ethylbenzene ug/L ND 20 20 22.6 22.3 113 112 70-130 1 30 Iodomethane ug/L ND 40 40 35.9 39.1 90 98 70-130 8 30 Methylene Chloride ug/L ND 20 20 19.2 18.9 96 94 70-130 2 30 Styrene ug/L ND 20 20 21.5 21.2 108 106 70-130 1 30 Tetrachloroethene ug/L ND 20 20 22.8 22.4 114 112 70-130 1 30 Toluene ug/L ND 20 20 22.0 21.8 110 109 70-155 1 30 trans-1,2-Dichloroethene ug/L ND 20 20 22.2 22.2 111 111 70-130 0 30 trans-1,3-Dichloropropene ug/L ND 20 20 21.1 21.0 106 105 70-130 1 30 trans-1,4-Dichloro-2-butene ug/L ND 20 20 21AJ 21.OJ 105 105 70-130 0 30 Trichloroethene ug/L ND 20 20 21.9 22.2 109 111 69-151 1 30 Trichlorofluoromethane ug/L ND 20 20 24.3 24.0 121 120 70-130 1 30 Vinyl acetate ug/L ND 40 40 36.7J 35.OJ 92 88 70-130 5 30 Vinyl chloride ug/L ND 20 20 25.2 25.1 126 125 70-130 1 30 1,2-Dichloroethane-d4 (S) % 101 98 70-130 4-Bromofluorobenzene (S) % 97 98 70-130 Toluene-d8 (S) % 99 99 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 QC Batch: 391009 Analysis Method: EPA 180.1 QC Batch Method: EPA 180.1 Analysis Description: 180.1 Turbidity Associated Lab Samples: 92367133007, 92367133015, 92367133016, 92367133017 METHOD BLANK: 2169592 Matrix: Water Associated Lab Samples: 92367133007, 92367133015, 92367133016, 92367133017 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Turbidity NTU ND 1.0 0.50 12/14/17 23:10 LABORATORY CONTROL SAMPLE: 2169593 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Turbidity NTU 10 10.0 100 90-110 SAMPLE DUPLICATE: 2169594 92367133002 Dup Max Parameter Units Result Result RPD RPD Qualifiers Turbidity NTU 7.5 D6 SAMPLE DUPLICATE: 2169595 92367133017 Dup Max Parameter Units Result Result RPD RPD Qualifiers Turbidity NTU 1.2 1.1 14 10 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 49 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 QC Batch: 391010 Analysis Method: EPA 180.1 QC Batch Method: EPA 180.1 Analysis Description: 180.1 Turbidity Associated Lab Samples: 92367133001, 92367133003, 92367133004, 92367133005, 92367133006, 92367133008, 92367133009, 92367133010,92367133011,92367133012,92367133013,92367133014 METHOD BLANK: 2169596 Matrix: Water Associated Lab Samples: 92367133001, 92367133003, 92367133004, 92367133005, 92367133006, 92367133008, 92367133009, 92367133010,92367133011,92367133012,92367133013,92367133014 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Turbidity NTU ND 1.0 0.50 12/15/17 01:39 LABORATORY CONTROL SAMPLE: 2169597 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Turbidity NTU 10 10.1 101 90-110 SAMPLE DUPLICATE: 2169598 92367133005 Dup Max Parameter Units Result Result RPD RPD Qualifiers Turbidity NTU 9.3 9.7 4 10 SAMPLE DUPLICATE: 2169599 92367133004 Dup Max Parameter Units Result Result RPD RPD Qualifiers Turbidity NTU 31.6 36.1 13 10 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 50 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte PASI-M Pace Analytical Services - Minneapolis ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 51 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92367133001 MW-1 EPA 3010A 391734 EPA 6010 391907 92367133003 MW-12S EPA 3010A 391734 EPA 6010 391907 92367133004 MW-13 EPA 3010A 391734 EPA 6010 391907 92367133005 MW-14 EPA 3010A 391734 EPA 6010 391907 92367133006 MW-15 EPA 3010A 391734 EPA 6010 391907 92367133007 MW-16 EPA 3010A 391734 EPA 6010 391907 92367133008 MW-17 EPA 3010A 391734 EPA 6010 391907 92367133009 MW-18 EPA 3010A 391734 EPA 6010 391907 92367133010 MW-19 EPA 3010A 391734 EPA 6010 391907 92367133011 MW-20 EPA 3010A 391734 EPA 6010 391907 92367133012 MW-21 EPA 3010A 391734 EPA 6010 391907 92367133013 MW-22 EPA 3010A 391734 EPA 6010 391907 92367133014 MW-23 EPA 3010A 391734 EPA 6010 391907 92367133015 MW-3R EPA 3010A 391734 EPA 6010 391907 92367133016 MW-7 EPA 3010A 391734 EPA 6010 391907 92367133017 MW-9 EPA 3010A 391734 EPA 6010 391907 92367133001 MW-1 EPA 3020 517022 EPA 6020B 517185 92367133003 MW-12S EPA 3020 517022 EPA 6020B 517185 92367133004 MW-13 EPA 3020 517022 EPA 6020B 517185 92367133005 MW-14 EPA 3020 517022 EPA 6020B 517185 92367133006 MW-15 EPA 3020 517022 EPA 6020B 517185 92367133007 MW-16 EPA 3020 517022 EPA 6020B 517185 92367133008 MW-17 EPA 3020 517022 EPA 6020B 517185 92367133009 MW-18 EPA 3020 517022 EPA 6020B 517185 92367133010 MW-19 EPA 3020 517022 EPA 6020B 517185 92367133011 MW-20 EPA 3020 517022 EPA 6020B 517185 92367133012 MW-21 EPA 3020 517022 EPA 6020B 517185 92367133013 MW-22 EPA 3020 517022 EPA 6020B 517185 92367133014 MW-23 EPA 3020 517022 EPA 6020B 517185 92367133015 MW-3R EPA 3020 517022 EPA 6020B 517185 92367133016 MW-7 EPA 3020 517022 EPA 6020B 517185 92367133017 MW-9 EPA 3020 517022 EPA 6020B 517185 92367133001 MW-1 EPA 8260 391129 92367133003 MW-12S EPA 8260 391129 92367133004 MW-13 EPA 8260 391129 92367133005 MW-14 EPA 8260 391129 92367133006 MW-15 EPA 8260 391129 92367133007 MW-16 EPA 8260 391129 92367133008 MW-17 EPA 8260 391129 92367133009 MW-18 EPA 8260 391129 92367133010 MW-19 EPA 8260 391129 92367133011 MW-20 EPA 8260 391129 92367133012 MW-21 EPA 8260 391129 92367133013 MW-22 EPA 8260 391129 92367133014 MW-23 EPA 8260 391129 92367133015 MW-3R EPA 8260 391129 92367133016 MW-7 EPA 8260 391129 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /10/2018 06:01 PM without the written consent of Pace Analytical Services, LLC. Page 52 of 58 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Surry Closed -Mt. Airy (UIC) Pace Project No.: 92367133 Lab ID Sample ID QC Batch Method QC Batch 92367133017 MW-9 EPA 8260 391131 92367133001 MW-1 EPA 180.1 391010 92367133003 MW-12S EPA 180.1 391010 92367133004 MW-13 EPA 180.1 391010 92367133005 MW-14 EPA 180.1 391010 92367133006 MW-15 EPA 180.1 391010 92367133007 MW-16 EPA 180.1 391009 92367133008 MW-17 EPA 180.1 391010 92367133009 MW-18 EPA 180.1 391010 92367133010 MW-19 EPA 180.1 391010 92367133011 MW-20 EPA 180.1 391010 92367133012 MW-21 EPA 180.1 391010 92367133013 MW-22 EPA 180.1 391010 92367133014 MW-23 EPA 180.1 391010 92367133015 MW-3R EPA 180.1 391009 92367133016 MW-7 EPA 180.1 391009 92367133017 MW-9 EPA 180.1 391009 Date: 01/10/2018 06:01 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Method Analytical Batch Page 53 of 58 Document Name: Document Revised: August 4, 2017 27cmnapical` Sample Condition Upon Receipt(SCURj Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.04 Pace Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersvills�) Rale€gh❑ Mechanicsville❑ • Client Name: WOE : 92367133 Courier: ❑ Commercial Custody seal Present? !T� [:]Fed Ex UPS Project UPS []ClientII III !I II II I IIII III ace ❑Other: 92367133 ❑Yes Seals Intact? ❑Yes 11Pb Packing Material: ❑Bubble Wrap , (Bubble Bags [-]None ❑ Othe Thermometer: �t ❑Blue �iR un lD: Type of Ice: Corr ectlon�3etar: Cooler Temp Corrected (•C): 4 V USDA Regulated Soil 6)/A, water sample] Did samples priginate in a quarantine Zone withfn the United States: CA, NY, or SC (check mapsl? I—IYps N1 Date/Initials Person Examinl LC.-Al Mn r Blalo Ical ssue Frozen? ❑Yes ❑N/A ❑None Temp should be above freezing to VC ❑samples out of temp criteria. samples on ice, coaling process has begun Did samples originate from a foreign source Ontergrionaily, in6udine Hawaii and Puerto Ricoi? IFlYes a Comments/Discrepanry: Chain of Custody Present? es ❑No ❑N/A 1. Samples Arrived within Hold Time? �es Elmo ❑N/A 2. Short Hold Time Analysis (472 hr.)> 6y1s AIV ❑N/A 3. Rush Turn Around Time Requested? yes VD. ❑N/A 4. Sufficient Volume? (� AS ❑No ❑N/A S. Correct Containers Used? -Pace Containers Used? s [:]No [:]NO❑N/A ❑N/A 6. nu c1c lc � a 0q 1 J 1 `� `` (( Containers Intact? es ❑No ❑N/A 7. Dissolved analysis: Samples Field Filtered? ❑Yes ❑No A 8. Sample Labels Match COC? -Includes Date/Time/ID/Analysis Matrix: ❑Yes - ,jSN ❑NIA 9. 1 1 Neadspace in VOA Vials (n5.6mmj? ❑Yes ❑No /A 10. C pp ` �il 4 i Trip Blank Present? Trip Blank Custody Seals Present? Elves ❑Yes N ❑No ❑NIA rOA 11. -'i gtn�-� CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Sample Discrepancy: Lot In of split containers Date/Time: Field Data Required? UYes LjNo Project Manager SCURF Review: Date! Project Manager SRF Review: (C Date: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers) Page 54 of 58 v CD (D Ur Cn 0 00 R O 1 m 0 Z, m 2 n Y c 3 'r. 2 �a a v m C Ln rq `* 3 m � a r O a m C �n 1 A a � to 3 rD d CL 4 to C � � rL d O 7 N 3 O a n v i4 m n � m c ro w a Item! !F 'Q w a1 * R 2� z Z7 7 f zz�2� z z _ BP4U-125 mL Plastic Unpreserved (N/A) (Cl-) fD S n BP3U-2SO mL Plastic Unpreserved (N/A) D 3 CL w S BP2U-SOO mL Plastic Unpreserved (N/A) =w Q- O. 3 BP1U-1 liter Plastic Unpreserved {N/A) Cr -0 S S 0 4i f0 BP4S-125 mL Plastic H2504 (pH < 2} (Cl •* p � � 7/717'RPM-250 mL plastic HNO3 (pH < 2) n Cr n X +i+ n .* m BP4Z-12S mL Plastic ZN Acetate & NaOH (>9) 7 V -a m 2 BP4C-125 mL Plastic NaOH (ph > 12) (CI-) ro ro 3 1 CL WGFiI-Wide- moot hed Glass jar Unpreserved O� p I AG11.1-1 liter Amber Unpreserved {N/A} (CI-) CM M CL R O n _S AGZH-1liter Amber HCf{pH<2) 4A O AG3U-250 mL Amber Unpreserved (N/A) (CI-} K AG15-1 liter Amber H2504 (pH < 2) O AG35-250 mL Amber H2504 (pH < 2) AG3A(OG3A)-250 ml.Amber NH4CI (N/A)(CI-) y'l UG9H-40 mL VOA HCI (N/A) �M F � V69T-40 ml. VOA Na2S203 (N/A) Q N n VG9U-40 mL VOA Unp {N/A} UG9P-40 mL VOA 1-43PO4 IN/A) 3 VOAK (6 vials per kit)-5035 kit (N/A) Z 1 � V/GK (3 vials per kit)-VPH/Gas kit (N/A) n ItV SP5T-125 ml Sterife Plastic (N/A— lab) 1 N SP2T-250 mL Sterile Pla5tiC [N/A — lab) 3 n Its la rEzzz 4 zzz BP3A-250 mL Plastic (NH2)2504 (9.3-9.7) W e+• CLbltainer ro N VSGU-20 mi Scintillation vials (N/A) IJ N G N (>D v As Cb A to 3 m 0 n :3 D O Q p n � c rn 3 w 3 v m 0 2r w W n C 0 0 n C K rD r. -a' t] 73 m < c an vo v a > m m � N G Coo o¢ n N C m ' a CD V LU CD (D U1 0) O 00 3 m O ro m �o c `m x v ro. � �n CL o C m rr m 3 'm M m � rt d r a 1q m -w O m � a � ro c 3 +R m 1O Q. 4 A u y w Ca � m -p o' M A 3 a a�n a v A 4 a m a_ A Item# * 'a M z z z z z BP4U-125 mL Plastic Unpreserved (N/A) (Cl-) C 0 f C 8P3U-250 mL Plastic Unpreserved (N/A) '= d ? O w BP2U-SOD mL Plastic Unpreserved (N/A) Fm C o G .., 3 a BPiU-7 liter Plastic Unpreserved (N/A) Cr -C 7- O X trod 3 �. BP45-125 mL Plastic H2504 (pH <2) (Cl-) 0 BP3N-2S0 mL plastic HNO3 (pH < 2] O Cr a O u+ n X •► ro r, BP42.125 mL Plastic 2N Acetate & NaOH (>9) zzzzzzzzz BP4C-125 mPlastic NaOH (pH > 12] [CI-] Cr n w Cr a CD ro CL WGFU-Wide-mouthed Glass jar Unpreserved AG2U-1liter Amber Unpreserved (N/A) (CI-) Cr ro Q- w, n „0 AGZH-1 liter Amber HCl (pH < 2) N O 7 AG 3U-250 mL Am ber Unpreserved (N/A) (Cl-] ,w.r AGIS- 1 liter AmberH2504 (pH < 2) C AG35-250 mL Amber H2SO4 (pH < 2) zzzzzzzzzz AG3A1DG3A]-250 ml-Amber NH4Cl (N/A](CI-] DG9H-40 mL VOA HCl (N/A) V 0 VG9T-40 mL VOA Na2S203 {N/A] fD n V459U-40 mL VOA Unp (N/A) DG9P-40 mL VOA H3PO4 (N/A] r 3 VOAK (6 vials per kit)-5035 kit (N/A) Z ; WGK 13 vials per kit]-VPH/Gas kit (N/A) ro SP5T-}25mLSterile Plastic (N/A -lab) iIz N SPZT-250 mL Sterile Plastic (N/A - lab) 3 ■ CP r BP3A-250 mL Plastic (NH2)2504 (9.3-9.7) � a Cubitainer r+ f ■vim VSGU-20 mL SCintiilatian vials (N/A) N V� GN t0 v 00 LO ' .PaeeAnalytira7 Section A Section B Required Client Information: Required Project Information: Company. Municipal Engineering Services Report To: Jonathan Pfohl Address 6B Shipwash Dr. Copy To: Garner, NC 27529 EmaiC jpfohl@mesco.com mesco.com Purchase Order #: Phone: (919)772-5393 Fax Project Name, Surry Closed -Mt. Airy[ Requested Due Date: Project 9: MATRIX CODE CDtL Dnnkmg WTI. DW o V W�te, Wash Wnlm WT WW Q Produd P a SAMPLE ID S o.uSoud od Su ❑L _ START One Character per box. ww wa (A-Z, -9 ! -I Other aT O Sample Ids must be unique Tos.ue 75 x TIATIT111 L ¢ s W ~ 2 w 1 MW-1 WT 3 MW-125 W7 4 MW-13 WT 5 MW-14 WT 6 MW-15 WT 7 MW-16 WT Z WT WT tIAW- V11T N!T Ap61TIONAL COMMENTS R NQUISHEDBYIAFFILEA U CHAIN I Analytical Request Document TION o -OF -CUSTODY The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. LO Iv Section C M d L Invoice Information: Page : Of Attention: Company Name: Address: Regulatory Agency Pace Quote: UIC) Pace Project Manager: trey. carter pacelabs.Com, State! Location Face Profile #: 2103-3 NC Requested Anal sls Filtered Y!N dECTFD z O Preservatives 6 H U � o d END F w F a x a w N o , — t c N z U m m m r a v [7 `a m fL.-3L' 7.. DATE TIME z z � O z a p X f `—I& 1 1 7 x I X X di 1 x x 7c x x X UCYv -}u x x X x x �^ x x X X X GX X C, ar v x x x DATE} TIME ACCEPTED BY I AFFILIATION RATE TIME SAMPLE CONDITIONS r 1Z' C1 -5 N IPLER NAME AND SIGNATURE PRINT Name of SAMPLER: SIGNATURE of SAMPLE U � C � N m DATE Signed: � � 1.1. � f � °' r i } cn c } ;0-9 CHAIN -OF -CUSTODY 1 Analytical Request Document FaceAwlyficaf The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Required Client Information: Required Project Information: Invoice Information: Page : Of 2 Company: Municipal Engineering Services Report To. Jonathan Pfohl Atlenlion: Address: 68 Shipwash Dr. Copy To: Company Name: Garner, NC 27529 Address: Regulatory Agency Email: jpfohl mescD.Com Purchase Order4: Pace Quote. Phone: (919)772-5393 Fax Project Name: Surry Closed -Mt. Airy (UIC) Pace Project Manager: trey rarter pacelabs.com, State I Location Requested Due Date: Protect #: Pace Profile 2103-3 NC Re nested Anal sis Filtared 4YINI z ,xaTRa coos o COLLECTED Z Preservatives } o orfnkmgwat�, ow Water WT s U O Waste Water WJJ b � � O z SAMPLE 1D o 7 m m 0l5o1'a OL - START END c One Character per box. wip. wP (A-Z, 0-9 ! , -} Olhc, CT 00 >w h Z Sample Ids must be unique T a, Ts tv n - v a K d O N `mG Q ¢ 4 —711 ~ DATE TIME DATE TIME # _ _ = z z 0 Z Z 13 MW-22 wT ;7.13 Il .1 t X X X 14 MW-23 w-r 1 X X X 15 MW-3R WT �`' 7` X X X Jj C 16 MW-7 VYr �L� X X X o 17 MW-9 WT 18 19 20 21 22 23 24 ADDITIONAL COMMENTS RELINQUISHED BY I AMUATION DATE TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS SAMPLER NAME AND SIGNATURE _ PRINT Name of SAMPLER: 11 VL o_ 2 m Z o z Z SIGNATURE of SAMPLER: DATE Signed: `i'a l 1 j !w M1 00 LO 0 eo a� d lacieAnalXical" www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 January 30, 2018 Mr. Jonathan Pfohl Municipal Engineering Services 68 Shipwash Dr. Garner, NC 27529 RE: Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92367075 Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory on December 14, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. This report was revised on January 30, 2018 to apply custom reporting limit to thalium by 6020 on Pace samples 001-004. If you have any questions concerning this report, please feel free to contact me. Sincerely, - �� Trey Carter trey. carter@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 29 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 CERTIFICATIONS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92367075 Minnesota Certification IDs 1700 Elm Street SE, Suite 200, Minneapolis, MN 55414- Michigan Certification #: 9909 2485 Minnesota Certification #: 027-053-137 A21-A Certification #: 2926.01 Mississippi Certification #: MN00064 Alabama Certification #: 40770 Montana Certification #: CERT0092 Alaska Contaminated Sites Certification #: 17-009 Nebraska Certification #: NE-OS-18-06 Alaska DW Certification M MN00064 Nevada Certification #: MN00064 Arizona Certification #: AZ0014 New Hampshire Certification #: 2081 Arkansas Certification #: 88-0680 New Jersey Certification M MN002 California Certification #: 2929 New York Certification #: 11647 CNMI Saipan Certification #:MP0003 North Carolina DW Certification #: 27700 Colorado Certification #: MN00064 North Carolina WW Certification #: 530 Connecticut Certification #: PH-0256 North Dakota Certification M R-036 EPA Region 8+Wyoming DW Certification #: via MN 027- Ohio DW Certification #: 41244 053-137 Ohio VAP Certification #: CL101 Florida Certification #: E87605 Oklahoma Certification #: 9507 Georgia Certification #: 959 Oregon NwTPH Certification #: MN300001 Guam EPA Certification #: MN00064 N0 Oregon Secondary Certification #: MN200001 Hawaii Certification #: MN0 Pennsylvania Certification #: 68-00563 : Idaho Certification #: MN00064 Puerto Rico Certification #: MN00064 Illinois Certification 20000 00011C-MN South Carolina Certification #:74003001 M 1 Indiana Certification #: Tennessee Certification #: TN02818 Iowa Certification #: Texas Certification #: T104704192 Kansas Certification #: E-10167 Utah Certification #: MN00 Kentucky DW Certification M 90062 Virginia Certification #: 163 Kentucky WW Certification M 90062 C64 Washington Certificationn ##: : 486 Louisiana DEQ Certification #: 03086 West Virginia DW Certification #: 9952 C Louisiana DW Certification #: MN00064 West Virginia DEP Certification #: 382 Maine Certification #: MN00064 Wisconsin Certification #: 999407970 Maryland Certification M 322 Massachusetts Certification #: M-MN064 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification M E87648 South Carolina Certification M 99030001 Massachusetts Certification #: M-NC030 Virginia/VELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 29 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92367075 Lab ID Sample ID Matrix Date Collected Date Received 92367075001 MW-11 Water 12/13/1715:19 12/14/1712:40 92367075002 MW-6 Water 12/13/1713:35 12/14/1712:40 92367075003 SCALEHOUSE Water 12/13/1715:25 12/14/1712:40 92367075011 MW-12D Water 12/13/17 09:20 12/14/17 17:15 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 29 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: SURRY CLOSED -MT. AIRY (AM) 92367075 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92367075001 MW-11 EPA6010 SH1 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C EPA 180.1 MDW 1 PASI-A 92367075002 MW-6 EPA6010 SH1 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C EPA 180.1 MDW 1 PASI-A 92367075003 SCALEHOUSE EPA6010 SH1 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C EPA 180.1 MDW 1 PASI-A 92367075011 MW-12D EPA 6010 SER 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 29 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92367075 Sample: MW-11 Lab ID: 92367075001 Collected: 12/13/17 15:19 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Vanadium Zinc 1400111 -1 �41 :4 9 [y :2 LTA 61 Thallium 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane Date: 01/30/2018 11:53 AM Analytical Method: EPA 6010 Preparation Method: EPA 301 OA ND ug/L 6.0 3.9 1 12/19/17 09:00 12/20/17 18:49 7440-36-0 ND ug/L 10.0 5.0 1 12/19/17 09:00 12/20/17 18:49 7440-38-2 33.7J ug/L 100 2.5 1 12/19/17 09:00 12/20/17 18:49 7440-39-3 ND ug/L 1.0 0.50 1 12/19/17 09:00 12/20/17 18:49 7440-41-7 0.66J ug/L 1.0 0.50 1 12/19/17 09:00 12/20/17 18:49 7440-43-9 8.01 ug/L 10.0 2.5 1 12/19/17 09:00 12/20/17 18:49 7440-47-3 8.81 ug/L 10.0 2.5 1 12/19/17 09:00 12/22/17 12:48 7440-48-4 ND ug/L 10.0 2.5 1 12/19/17 09:00 12/20/17 18:49 7440-50-8 ND ug/L 10.0 2.5 1 12/19/17 09:00 12/20/17 18:49 7439-92-1 6.OJ ug/L 50.0 2.5 1 12/19/17 09:00 12/20/17 18:49 7440-02-0 ND ug/L 10.0 5.0 1 12/19/17 09:00 12/20/17 18:49 7782-49-2 ND ug/L 10.0 2.5 1 12/19/17 09:00 12/20/17 18:49 7440-22-4 ND ug/L 25.0 2.5 1 12/19/17 09:00 12/20/17 18:49 7440-62-2 8.01 ug/L 10.0 5.0 1 12/19/17 09:00 12/20/17 18:49 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3020 0.053J ug/L 5.5 0.028 1 01/08/18 11:42 01/08/18 23:31 7440-28-0 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 12/15/17 23:14 67-64-1 ND ug/L 200 1.9 1 12/15/17 23:14 107-13-1 0.60J ug/L 1.0 0.25 1 12/15/17 23:14 71-43-2 ND ug/L 3.0 0.17 1 12/15/17 23:14 74-97-5 ND ug/L 1.0 0.18 1 12/15/17 23:14 75-27-4 ND ug/L 3.0 0.26 1 12/15/17 23:14 75-25-2 ND ug/L 10.0 0.29 1 12/15/17 23:14 74-83-9 ND ug/L 100 0.96 1 12/15/17 23:14 78-93-3 ND ug/L 100 1.2 1 12/15/17 23:14 75-15-0 ND ug/L 1.0 0.25 1 12/15/17 23:14 56-23-5 0.71J ug/L 3.0 0.23 1 12/15/17 23:14 108-90-7 ND ug/L 10.0 0.54 1 12/15/17 23:14 75-00-3 ND ug/L 5.0 0.14 1 12/15/17 23:14 67-66-3 ND ug/L 1.0 0.11 1 12/15/17 23:14 74-87-3 ND ug/L 13.0 2.0 1 12/15/17 23:14 96-12-8 ND ug/L 3.0 0.21 1 12/15/17 23:14 124-48-1 ND ug/L 1.0 0.27 1 12/15/17 23:14 106-93-4 ND ug/L 10.0 0.21 1 12/15/17 23:14 74-95-3 ND ug/L 5.0 0.30 1 12/15/17 23:14 95-50-1 1.7 ug/L 1.0 0.33 1 12/15/17 23:14 106-46-7 ND ug/L 100 1.0 1 12/15/17 23:14 110-57-6 0.37J ug/L 5.0 0.32 1 12/15/17 23:14 75-34-3 ND ug/L 1.0 0.24 1 12/15/17 23:14 107-06-2 ND ug/L 5.0 0.56 1 12/15/17 23:14 75-35-4 1.6J ug/L 5.0 0.19 1 12/15/17 23:14 156-59-2 ND ug/L 5.0 0.49 1 12/15/17 23:14 156-60-5 1.2 ug/L 1.0 0.27 1 12/15/17 23:14 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 29 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92367075 Sample: MW-11 Lab ID: 92367075001 Collected: 12/13/17 15:19 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 180.1 Turbidity Turbidity Date: 01/30/2018 11:53 AM Analytical Method: EPA 8260 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 100 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 1.0 ND ug/L 5.0 99 % 70-130 99 % 70-130 101 % 70-130 Analytical Method: EPA 180.1 4.7 NTU 1.0 0.13 1 12/15/17 23:14 10061-01-5 0.26 1 12/15/17 23:14 10061-02-6 0.30 1 12/15/17 23:14 100-41-4 0.46 1 12/15/17 23:14 591-78-6 0.32 1 12/15/17 23:14 74-88-4 0.97 1 12/15/17 23:14 75-09-2 0.33 1 12/15/17 23:14 108-10-1 0.26 1 12/15/17 23:14 100-42-5 0.33 1 12/15/17 23:14 630-20-6 0.40 1 12/15/17 23:14 79-34-5 0.46 1 12/15/17 23:14 127-18-4 0.26 1 12/15/17 23:14 108-88-3 0.48 1 12/15/17 23:14 71-55-6 0.29 1 12/15/17 23:14 79-00-5 0.47 1 12/15/17 23:14 79-01-6 0.20 1 12/15/17 23:14 75-69-4 0.41 1 12/15/17 23:14 96-18-4 0.35 1 12/15/17 23:14 108-05-4 0.62 1 12/15/17 23:14 75-01-4 0.66 1 12/15/17 23:14 1330-20-7 1 12/15/17 23:14 460-00-4 1 12/15/17 23:14 17060-07-0 1 12/15/17 23:14 2037-26-5 0.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 12/15/17 01:39 Page 6 of 29 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92367075 Sample: MW-6 Lab ID: 92367075002 Collected: 12/13/17 13:35 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Vanadium Zinc 1400111 -1 �41 :4 9 [y :2 LTA 61 Thallium 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane Date: 01/30/2018 11:53 AM Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 12/19/17 09:00 12/20/17 18:53 7440-36-0 ND ug/L 10.0 5.0 1 12/19/17 09:00 12/20/17 18:53 7440-38-2 113 ug/L 100 2.5 1 12/19/17 09:00 12/20/17 18:53 7440-39-3 ND ug/L 1.0 0.50 1 12/19/17 09:00 12/20/17 18:53 7440-41-7 0.56J ug/L 1.0 0.50 1 12/19/17 09:00 12/20/17 18:53 7440-43-9 ND ug/L 10.0 2.5 1 12/19/17 09:00 12/20/17 18:53 7440-47-3 76.7 ug/L 10.0 2.5 1 12/19/17 09:00 12/22/17 12:58 7440-48-4 12.0 ug/L 10.0 2.5 1 12/19/17 09:00 12/20/17 18:53 7440-50-8 ND ug/L 10.0 2.5 1 12/19/17 09:00 12/20/17 18:53 7439-92-1 7.OJ ug/L 50.0 2.5 1 12/19/17 09:00 12/20/17 18:53 7440-02-0 ND ug/L 10.0 5.0 1 12/19/17 09:00 12/20/17 18:53 7782-49-2 ND ug/L 10.0 2.5 1 12/19/17 09:00 12/20/17 18:53 7440-22-4 ND ug/L 25.0 2.5 1 12/19/17 09:00 12/20/17 18:53 7440-62-2 7.4J ug/L 10.0 5.0 1 12/19/17 09:00 12/20/17 18:53 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3020 0.591 ug/L 5.5 0.028 1 01/08/18 11:42 01/08/18 23:34 7440-28-0 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 12/15/17 23:31 67-64-1 ND ug/L 200 1.9 1 12/15/17 23:31 107-13-1 ND ug/L 1.0 0.25 1 12/15/17 23:31 71-43-2 ND ug/L 3.0 0.17 1 12/15/17 23:31 74-97-5 ND ug/L 1.0 0.18 1 12/15/17 23:31 75-27-4 ND ug/L 3.0 0.26 1 12/15/17 23:31 75-25-2 ND ug/L 10.0 0.29 1 12/15/17 23:31 74-83-9 ND ug/L 100 0.96 1 12/15/17 23:31 78-93-3 ND ug/L 100 1.2 1 12/15/17 23:31 75-15-0 ND ug/L 1.0 0.25 1 12/15/17 23:31 56-23-5 ND ug/L 3.0 0.23 1 12/15/17 23:31 108-90-7 ND ug/L 10.0 0.54 1 12/15/17 23:31 75-00-3 ND ug/L 5.0 0.14 1 12/15/17 23:31 67-66-3 ND ug/L 1.0 0.11 1 12/15/17 23:31 74-87-3 ND ug/L 13.0 2.0 1 12/15/17 23:31 96-12-8 ND ug/L 3.0 0.21 1 12/15/17 23:31 124-48-1 ND ug/L 1.0 0.27 1 12/15/17 23:31 106-93-4 ND ug/L 10.0 0.21 1 12/15/17 23:31 74-95-3 ND ug/L 5.0 0.30 1 12/15/17 23:31 95-50-1 ND ug/L 1.0 0.33 1 12/15/17 23:31 106-46-7 ND ug/L 100 1.0 1 12/15/17 23:31 110-57-6 ND ug/L 5.0 0.32 1 12/15/17 23:31 75-34-3 ND ug/L 1.0 0.24 1 12/15/17 23:31 107-06-2 ND ug/L 5.0 0.56 1 12/15/17 23:31 75-35-4 ND ug/L 5.0 0.19 1 12/15/17 23:31 156-59-2 ND ug/L 5.0 0.49 1 12/15/17 23:31 156-60-5 ND ug/L 1.0 0.27 1 12/15/17 23:31 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 29 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92367075 Sample: MW-6 Lab ID: 92367075002 Collected: 12/13/17 13:35 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 180.1 Turbidity Turbidity Date: 01/30/2018 11:53 AM Analytical Method: EPA 8260 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 100 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 1.0 ND ug/L 5.0 98 % 70-130 103 % 70-130 101 % 70-130 Analytical Method: EPA 180.1 12.1 NTU 1.0 0.13 1 12/15/17 23:31 10061-01-5 0.26 1 12/15/17 23:31 10061-02-6 0.30 1 12/15/17 23:31 100-41-4 0.46 1 12/15/17 23:31 591-78-6 0.32 1 12/15/17 23:31 74-88-4 0.97 1 12/15/17 23:31 75-09-2 0.33 1 12/15/17 23:31 108-10-1 0.26 1 12/15/17 23:31 100-42-5 0.33 1 12/15/17 23:31 630-20-6 0.40 1 12/15/17 23:31 79-34-5 0.46 1 12/15/17 23:31 127-18-4 0.26 1 12/15/17 23:31 108-88-3 0.48 1 12/15/17 23:31 71-55-6 0.29 1 12/15/17 23:31 79-00-5 0.47 1 12/15/17 23:31 79-01-6 0.20 1 12/15/17 23:31 75-69-4 0.41 1 12/15/17 23:31 96-18-4 0.35 1 12/15/17 23:31 108-05-4 0.62 1 12/15/17 23:31 75-01-4 0.66 1 12/15/17 23:31 1330-20-7 1 12/15/17 23:31 460-00-4 1 12/15/17 23:31 17060-07-0 1 12/15/17 23:31 2037-26-5 0.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 12/14/17 23:10 Page 8 of 29 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92367075 Sample: SCALEHOUSE Lab ID: 92367075003 Collected: 12/13/17 15:25 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Vanadium Zinc 1400111 -1 �41 :4 9 [y :2 LTA 61 Thallium 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane Date: 01/30/2018 11:53 AM Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 12/19/17 09:00 12/20/17 18:57 7440-36-0 ND ug/L 10.0 5.0 1 12/19/17 09:00 12/20/17 18:57 7440-38-2 12.4J ug/L 100 2.5 1 12/19/17 09:00 12/20/17 18:57 7440-39-3 ND ug/L 1.0 0.50 1 12/19/17 09:00 12/20/17 18:57 7440-41-7 ND ug/L 1.0 0.50 1 12/19/17 09:00 12/20/17 18:57 7440-43-9 5.7J ug/L 10.0 2.5 1 12/19/17 09:00 12/20/17 18:57 7440-47-3 ND ug/L 10.0 2.5 1 12/19/17 09:00 12/22/17 13:01 7440-48-4 4.1J ug/L 10.0 2.5 1 12/19/17 09:00 12/20/17 18:57 7440-50-8 ND ug/L 10.0 2.5 1 12/19/17 09:00 12/20/17 18:57 7439-92-1 3.7J ug/L 50.0 2.5 1 12/19/17 09:00 12/20/17 18:57 7440-02-0 ND ug/L 10.0 5.0 1 12/19/17 09:00 12/20/17 18:57 7782-49-2 ND ug/L 10.0 2.5 1 12/19/17 09:00 12/20/17 18:57 7440-22-4 ND ug/L 25.0 2.5 1 12/19/17 09:00 12/20/17 18:57 7440-62-2 13.6 ug/L 10.0 5.0 1 12/19/17 09:00 12/20/17 18:57 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3020 ND ug/L 5.5 0.028 1 01/08/18 11:42 01/08/18 23:37 7440-28-0 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 12/15/17 23:49 67-64-1 ND ug/L 200 1.9 1 12/15/17 23:49 107-13-1 ND ug/L 1.0 0.25 1 12/15/17 23:49 71-43-2 ND ug/L 3.0 0.17 1 12/15/17 23:49 74-97-5 ND ug/L 1.0 0.18 1 12/15/17 23:49 75-27-4 ND ug/L 3.0 0.26 1 12/15/17 23:49 75-25-2 ND ug/L 10.0 0.29 1 12/15/17 23:49 74-83-9 ND ug/L 100 0.96 1 12/15/17 23:49 78-93-3 ND ug/L 100 1.2 1 12/15/17 23:49 75-15-0 ND ug/L 1.0 0.25 1 12/15/17 23:49 56-23-5 ND ug/L 3.0 0.23 1 12/15/17 23:49 108-90-7 ND ug/L 10.0 0.54 1 12/15/17 23:49 75-00-3 ND ug/L 5.0 0.14 1 12/15/17 23:49 67-66-3 ND ug/L 1.0 0.11 1 12/15/17 23:49 74-87-3 ND ug/L 13.0 2.0 1 12/15/17 23:49 96-12-8 ND ug/L 3.0 0.21 1 12/15/17 23:49 124-48-1 ND ug/L 1.0 0.27 1 12/15/17 23:49 106-93-4 ND ug/L 10.0 0.21 1 12/15/17 23:49 74-95-3 ND ug/L 5.0 0.30 1 12/15/17 23:49 95-50-1 ND ug/L 1.0 0.33 1 12/15/17 23:49 106-46-7 ND ug/L 100 1.0 1 12/15/17 23:49 110-57-6 ND ug/L 5.0 0.32 1 12/15/17 23:49 75-34-3 ND ug/L 1.0 0.24 1 12/15/17 23:49 107-06-2 ND ug/L 5.0 0.56 1 12/15/17 23:49 75-35-4 0.31J ug/L 5.0 0.19 1 12/15/17 23:49 156-59-2 ND ug/L 5.0 0.49 1 12/15/17 23:49 156-60-5 ND ug/L 1.0 0.27 1 12/15/17 23:49 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 9 of 29 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92367075 Sample: SCALEHOUSE Lab ID: 92367075003 Collected: 12/13/17 15:25 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 180.1 Turbidity Turbidity Date: 01/30/2018 11:53 AM Analytical Method: EPA 8260 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 100 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 50.0 ND ug/L 1.0 ND ug/L 5.0 97 % 70-130 99 % 70-130 100 % 70-130 Analytical Method: EPA 180.1 ND NTU 1.0 0.13 1 12/15/17 23:49 10061-01-5 0.26 1 12/15/17 23:49 10061-02-6 0.30 1 12/15/17 23:49 100-41-4 0.46 1 12/15/17 23:49 591-78-6 0.32 1 12/15/17 23:49 74-88-4 0.97 1 12/15/17 23:49 75-09-2 0.33 1 12/15/17 23:49 108-10-1 0.26 1 12/15/17 23:49 100-42-5 0.33 1 12/15/17 23:49 630-20-6 0.40 1 12/15/17 23:49 79-34-5 0.46 1 12/15/17 23:49 127-18-4 0.26 1 12/15/17 23:49 108-88-3 0.48 1 12/15/17 23:49 71-55-6 0.29 1 12/15/17 23:49 79-00-5 0.47 1 12/15/17 23:49 79-01-6 0.20 1 12/15/17 23:49 75-69-4 0.41 1 12/15/17 23:49 96-18-4 0.35 1 12/15/17 23:49 108-05-4 0.62 1 12/15/17 23:49 75-01-4 0.66 1 12/15/17 23:49 1330-20-7 1 12/15/17 23:49 460-00-4 1 12/15/17 23:49 17060-07-0 1 12/15/17 23:49 2037-26-5 0.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 12/15/17 01:39 Page 10 of 29 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92367075 Sample: MW-12D Lab ID: 92367075011 Collected: 12/13/17 09:20 Received: 12/14/17 17:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Antimony ND ug/L 6.0 3.9 1 01/02/18 11:30 01/02/18 22:44 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:44 7440-38-2 Barium 4.5J ug/L 100 2.5 1 01/02/18 11:30 01/02/18 22:44 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 01/02/18 11:30 01/02/18 22:44 7440-41-7 Cadmium 1.4 ug/L 1.0 0.50 1 01/02/18 11:30 01/02/18 22:44 7440-43-9 Chromium ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:44 7440-47-3 Cobalt ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:44 7440-48-4 Copper 8.4J ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:44 7440-50-8 Lead ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:44 7439-92-1 Nickel ND ug/L 50.0 2.5 1 01/02/18 11:30 01/02/18 22:44 7440-02-0 Selenium ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:44 7782-49-2 Silver ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:44 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 01/02/18 11:30 01/02/18 22:44 7440-62-2 Zinc 7.5J ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:44 7440-66-6 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020 Thallium ND ug/L 5.5 0.028 1 01/08/18 12:39 01/09/18 00:03 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 12/16/17 00:07 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 12/16/17 00:07 107-13-1 Benzene ND ug/L 1.0 0.25 1 12/16/17 00:07 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 12/16/17 00:07 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 12/16/17 00:07 75-27-4 Bromoform ND ug/L 3.0 0.26 1 12/16/17 00:07 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 12/16/17 00:07 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 12/16/17 00:07 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 12/16/17 00:07 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 12/16/17 00:07 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 12/16/17 00:07 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 12/16/17 00:07 75-00-3 Chloroform ND ug/L 5.0 0.14 1 12/16/17 00:07 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 12/16/17 00:07 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 12/16/17 00:07 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 12/16/17 00:07 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 12/16/17 00:07 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 12/16/17 00:07 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 12/16/17 00:07 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 12/16/17 00:07 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 12/16/17 00:07 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 12/16/17 00:07 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 12/16/17 00:07 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 12/16/17 00:07 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 12/16/17 00:07 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 12/16/17 00:07 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 12/16/17 00:07 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /30/2018 11:53 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 29 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92367075 Sample: MW-12D Lab ID: 92367075011 Collected: 12/13/17 09:20 Received: 12/14/17 17:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 12/16/17 00:07 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 12/16/17 00:07 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 12/16/17 00:07 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 12/16/17 00:07 591-78-6 lodomethane ND ug/L 10.0 0.32 1 12/16/17 00:07 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 12/16/17 00:07 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 12/16/17 00:07 108-10-1 Styrene ND ug/L 1.0 0.26 1 12/16/17 00:07 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 12/16/17 00:07 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 12/16/17 00:07 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 12/16/17 00:07 127-18-4 Toluene ND ug/L 1.0 0.26 1 12/16/17 00:07 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 12/16/17 00:07 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 12/16/17 00:07 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 12/16/17 00:07 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 12/16/17 00:07 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 12/16/17 00:07 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 12/16/17 00:07 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 12/16/17 00:07 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 12/16/17 00:07 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 12/16/17 00:07 460-00-4 1,2-Dichloroethane-d4 (S) 98 % 70-130 1 12/16/17 00:07 17060-07-0 Toluene-d8 (S) 105 % 70-130 1 12/16/17 00:07 2037-26-5 Date: 01/30/2018 11:53 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 12 of 29 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92367075 QC Batch: 391501 Analysis Method: EPA 6010 QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92367075001, 92367075002, 92367075003 METHOD BLANK: 2171978 Matrix: Associated Lab Samples: 92367075001, 92367075002, 92367075003 Blank Parameter Units Result Water Reporting Limit Antimony ug/L ND 5.0 Arsenic ug/L ND 10.0 Barium ug/L ND 5.0 Beryllium ug/L ND 1.0 Cadmium ug/L ND 1.0 Chromium ug/L ND 5.0 Cobalt ug/L ND 5.0 Copper ug/L ND 5.0 Lead ug/L ND 5.0 Nickel ug/L ND 5.0 Selenium ug/L ND 10.0 Silver ug/L ND 5.0 Vanadium ug/L ND 5.0 Zinc ug/L ND 10.0 MDL Analyzed 3.9 12/20/17 17:15 5.0 12/20/17 17:15 2.5 12/20/17 17:15 0.50 12/20/17 17:15 0.50 12/20/17 17:15 2.5 12/20/17 17:15 2.5 12/22/17 12:42 2.5 12/20/17 17:15 2.5 12/20/17 17:15 2.5 12/20/17 17:15 5.0 12/20/17 17:15 2.5 12/20/17 17:15 2.5 12/20/17 17:15 5.0 12/20/17 17:15 LABORATORY CONTROL SAMPLE: Parameter 2171979 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 500 486 97 80-120 Arsenic ug/L 500 472 94 80-120 Barium ug/L 500 500 100 80-120 Beryllium ug/L 500 514 103 80-120 Cadmium ug/L 500 477 95 80-120 Chromium ug/L 500 496 99 80-120 Cobalt ug/L 500 481 96 80-120 Copper ug/L 500 494 99 80-120 Lead ug/L 500 466 93 80-120 Nickel ug/L 500 473 95 80-120 Selenium ug/L 500 461 92 80-120 Silver ug/L 250 242 97 80-120 Vanadium ug/L 500 496 99 80-120 Zinc ug/L 500 470 94 80-120 Qualifiers Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2171980 2171981 MS MSD 92366996031 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 498 502 100 100 75-125 1 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /30/2018 11:53 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 29 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: SURRY CLOSED -MT. 92367075 AIRY (AM) MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2171980 2171981 MS MSD 92366996031 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Arsenic ug/L ND 500 500 484 495 97 99 75-125 2 20 Barium ug/L 74.2 500 500 571 580 99 101 75-125 2 20 Beryllium ug/L ND 500 500 506 514 101 103 75-125 2 20 Cadmium ug/L ND 500 500 495 501 99 100 75-125 1 20 Chromium ug/L 2.8J 500 500 500 510 99 101 75-125 2 20 Cobalt ug/L 500 500 492 499 98 99 75-125 1 20 Copper ug/L ND 500 500 497 505 99 101 75-125 2 20 Lead ug/L ND 500 500 477 483 95 97 75-125 1 20 Nickel ug/L 3.7J 500 500 486 493 96 98 75-125 1 20 Selenium ug/L ND 500 500 486 496 97 99 75-125 2 20 Silver ug/L ND 250 250 246 250 98 100 75-125 2 20 Vanadium ug/L ND 500 500 498 506 100 101 75-125 2 20 Zinc ug/L ND 500 500 500 509 99 101 75-125 2 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /30/2018 11:53 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 29 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92367075 QC Batch: 391698 Analysis Method: EPA 6010 QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92367075011 METHOD BLANK: 2173086 Associated Lab Samples: 92367075011 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Antimony ug/L ND 5.0 3.9 01/02/18 22:00 Arsenic ug/L ND 10.0 5.0 01/02/18 22:00 Barium ug/L ND 5.0 2.5 01/02/18 22:00 Beryllium ug/L ND 1.0 0.50 01/02/18 22:00 Cadmium ug/L ND 1.0 0.50 01/02/18 22:00 Chromium ug/L ND 5.0 2.5 01/02/18 22:00 Cobalt ug/L ND 5.0 2.5 01/02/18 22:00 Copper ug/L ND 5.0 2.5 01/02/18 22:00 Lead ug/L ND 5.0 2.5 01/02/18 22:00 Nickel ug/L ND 5.0 2.5 01/02/18 22:00 Selenium ug/L ND 10.0 5.0 01/02/18 22:00 Silver ug/L ND 5.0 2.5 01/02/18 22:00 Vanadium ug/L ND 5.0 2.5 01/02/18 22:00 Zinc ug/L ND 10.0 5.0 01/02/18 22:00 LABORATORY CONTROL SAMPLE: Parameter 2173087 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 500 491 98 80-120 Arsenic ug/L 500 471 94 80-120 Barium ug/L 500 489 98 80-120 Beryllium ug/L 500 498 100 80-120 Cadmium ug/L 500 479 96 80-120 Chromium ug/L 500 481 96 80-120 Cobalt ug/L 500 479 96 80-120 Copper ug/L 500 502 100 80-120 Lead ug/L 500 471 94 80-120 Nickel ug/L 500 476 95 80-120 Selenium ug/L 500 476 95 80-120 Silver ug/L 250 242 97 80-120 Vanadium ug/L 500 484 97 80-120 Zinc ug/L 500 467 93 80-120 Qualifiers Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2173088 2173089 MS MSD 92366776001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 505 504 101 101 75-125 0 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /30/2018 11:53 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 29 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: SURRY CLOSED -MT. 92367075 AIRY (AM) MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2173088 2173089 MS MSD 92366776001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Arsenic ug/L ND 500 500 487 484 97 97 75-125 1 20 Barium ug/L 13.6J 500 500 510 509 99 99 75-125 0 20 Beryllium ug/L ND 500 500 505 503 101 101 75-125 0 20 Cadmium ug/L ND 500 500 498 496 100 99 75-125 0 20 Chromium ug/L ND 500 500 500 492 100 98 75-125 2 20 Cobalt ug/L ND 500 500 494 491 99 98 75-125 1 20 Copper ug/L ND 500 500 507 506 101 101 75-125 0 20 Lead ug/L ND 500 500 488 484 98 97 75-125 1 20 Nickel ug/L ND 500 500 492 488 98 98 75-125 1 20 Selenium ug/L ND 500 500 505 502 101 100 75-125 1 20 Silver ug/L ND 250 250 252 251 101 100 75-125 0 20 Vanadium ug/L ND 500 500 503 498 101 100 75-125 1 20 Zinc ug/L ND 500 500 496 491 99 98 75-125 1 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /30/2018 11:53 AM without the written consent of Pace Analytical Services, LLC. Page 16 of 29 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92367075 QC Batch: 517019 Analysis Method: EPA 6020B QC Batch Method: EPA 3020 Analysis Description: 6020E Water UPD5 Associated Lab Samples: 92367075001, 92367075002, 92367075003 METHOD BLANK: 2809356 Matrix: Water Associated Lab Samples: 92367075001, 92367075002, 92367075003 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Thallium ug/L ND 5.5 0.028 01/08/18 22:14 LABORATORY CONTROL SAMPLE: 2809357 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Thallium ug/L 100 105 105 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2809358 2809359 MS MSD 92366378001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Thallium ug/L ND 100 100 103 106 103 106 75-125 2 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /30/2018 11:53 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 29 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92367075 QC Batch: 517021 Analysis Method: EPA 6020B QC Batch Method: EPA 3020 Analysis Description: 6020E Water UPD5 Associated Lab Samples: 92367075011 METHOD BLANK: 2809364 Matrix: Water Associated Lab Samples: 92367075011 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Thallium ug/L ND 5.5 0.028 01/08/18 23:46 LABORATORY CONTROL SAMPLE: 2809365 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Thallium ug/L 100 108 108 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2809366 2809367 MS MSD 92367075011 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Thallium ug/L ND 100 100 106 107 106 107 75-125 1 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /30/2018 11:53 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 29 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92367075 QC Batch: 391124 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92367075001, 92367075002, 92367075003, 92367075011 METHOD BLANK: 2170158 Matrix: Water Associated Lab Samples: 92367075001, 92367075002, 92367075003, 92367075011 Blank Reporting Parameter Units Result Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 0.33 12/15/17 15:35 1,1,1-Trichloroethane ug/L ND 1.0 0.48 12/15/17 15:35 1,1,2,2-Tetrachloroethane ug/L ND 3.0 0.40 12/15/17 15:35 1,1,2-Trichloroethane ug/L ND 1.0 0.29 12/15/17 15:35 1,1-Dichloroethane ug/L ND 5.0 0.32 12/15/17 15:35 1,1-Dichloroethene ug/L ND 5.0 0.56 12/15/17 15:35 1,2,3-Trichloropropane ug/L ND 1.0 0.41 12/15/17 15:35 1,2-Dibromo-3-chloropropane ug/L ND 13.0 2.0 12/15/17 15:35 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 12/15/17 15:35 1,2-Dichlorobenzene ug/L ND 5.0 0.30 12/15/17 15:35 1,2-Dichloroethane ug/L ND 1.0 0.24 12/15/17 15:35 1,2-Dichloropropane ug/L ND 1.0 0.27 12/15/17 15:35 1,4-Dichlorobenzene ug/L ND 1.0 0.33 12/15/17 15:35 2-Butanone (MEK) ug/L ND 100 0.96 12/15/17 15:35 2-Hexanone ug/L ND 50.0 0.46 12/15/17 15:35 4-Methyl-2-pentanone (MIBK) ug/L ND 100 0.33 12/15/17 15:35 Acetone ug/L ND 100 10.0 12/15/17 15:35 Acrylonitrile ug/L ND 200 1.9 12/15/17 15:35 Benzene ug/L ND 1.0 0.25 12/15/17 15:35 Bromochloromethane ug/L ND 3.0 0.17 12/15/17 15:35 Bromodichloromethane ug/L ND 1.0 0.18 12/15/17 15:35 Bromoform ug/L ND 3.0 0.26 12/15/17 15:35 Bromomethane ug/L ND 10.0 0.29 12/15/17 15:35 Carbon disulfide ug/L ND 100 1.2 12/15/17 15:35 Carbon tetrachloride ug/L ND 1.0 0.25 12/15/17 15:35 Chlorobenzene ug/L ND 3.0 0.23 12/15/17 15:35 Chloroethane ug/L ND 10.0 0.54 12/15/17 15:35 Chloroform ug/L 0.16J 5.0 0.14 12/15/17 15:35 Chloromethane ug/L ND 1.0 0.11 12/15/17 15:35 cis-1,2-Dichloroethene ug/L ND 5.0 0.19 12/15/17 15:35 cis-1,3-Dichloropropene ug/L ND 1.0 0.13 12/15/17 15:35 Dibromochloromethane ug/L ND 3.0 0.21 12/15/17 15:35 Dibromomethane ug/L ND 10.0 0.21 12/15/17 15:35 Ethylbenzene ug/L ND 1.0 0.30 12/15/17 15:35 lodomethane ug/L ND 10.0 0.32 12/15/17 15:35 Methylene Chloride ug/L ND 1.0 0.97 12/15/17 15:35 Styrene ug/L ND 1.0 0.26 12/15/17 15:35 Tetrachloroethene ug/L ND 1.0 0.46 12/15/17 15:35 Toluene ug/L ND 1.0 0.26 12/15/17 15:35 trans-1,2-Dichloroethene ug/L ND 5.0 0.49 12/15/17 15:35 trans- 1,3-Dichloropropene ug/L ND 1.0 0.26 12/15/17 15:35 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /30/2018 11:53 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 29 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92367075 METHOD BLANK: 2170158 Matrix: Water Associated Lab Samples: 92367075001, 92367075002, 92367075003, 92367075011 Blank Reporting Parameter Units Result Limit MDL Analyzed trans-1,4-Dichloro-2-butene ug/L ND 100 1.0 12/15/17 15:35 Trichloroethene ug/L ND 1.0 0.47 12/15/17 15:35 Trichlorofluoromethane ug/L ND 1.0 0.20 12/15/17 15:35 Vinyl acetate ug/L ND 50.0 0.35 12/15/17 15:35 Vinyl chloride ug/L ND 1.0 0.62 12/15/17 15:35 Xylene (Total) ug/L ND 5.0 0.66 12/15/17 15:35 1,2-Dichloroethane-d4 (S) % 93 70-130 12/15/17 15:35 4-Bromofluorobenzene (S) % 98 70-130 12/15/17 15:35 Toluene-d8 (S) % 101 70-130 12/15/17 15:35 LABORATORY CONTROL SAMPLE: Parameter 2170159 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 48.3 97 80-125 1,1,1-Trichloroethane ug/L 50 39.1 78 71-129 1,1,2,2-Tetrachloroethane ug/L 50 46.5 93 79-124 1,1,2-Trichloroethane ug/L 50 46.0 92 85-125 1,1-Dichloroethane ug/L 50 46.3 93 73-126 1,1-Dichloroethene ug/L 50 40.1 80 66-135 1,2,3-Trichloropropane ug/L 50 42.1 84 75-130 1,2-Dibromo-3-chloropropane ug/L 50 47.2 94 71-133 1,2-Dibromoethane (EDB) ug/L 50 45.5 91 83-124 1,2-Dichlorobenzene ug/L 50 46.3 93 80-133 1,2-Dichloroethane ug/L 50 44.1 88 67-128 1,2-Dichloropropane ug/L 50 46.7 93 75-132 1,4-Dichlorobenzene ug/L 50 47.4 95 78-130 2-Butanone (MEK) ug/L 100 78.1J 78 61-144 2-Hexanone ug/L 100 90.4 90 68-143 4-Methyl-2-pentanone (MIBK) ug/L 100 81.6J 82 72-135 Acetone ug/L 100 88.2J 88 48-146 Acrylonitrile ug/L 250 240 96 40-160 Benzene ug/L 50 48.2 96 80-125 Bromochloromethane ug/L 50 43.6 87 71-125 Bromodichloromethane ug/L 50 45.8 92 78-124 Bromoform ug/L 50 53.0 106 71-128 Bromomethane ug/L 50 44.4 89 40-160 Carbon disulfide ug/L 50 45AJ 91 50-160 Carbon tetrachloride ug/L 50 43.8 88 69-131 Chlorobenzene ug/L 50 46.5 93 81-122 Chloroethane ug/L 50 46.1 92 39-148 Chloroform ug/L 50 36.4 73 73-127 Chloromethane ug/L 50 40.4 81 44-146 cis-1,2-Dichloroethene ug/L 50 37.5 75 74-124 cis-1,3-Dichloropropene ug/L 50 51.8 104 72-132 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /30/2018 11:53 AM without the written consent of Pace Analytical Services, LLC. Page 20 of 29 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92367075 LABORATORY CONTROL SAMPLE: 2170159 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Dibromochloromethane ug/L 50 46.1 92 78-125 Dibromomethane ug/L 50 51.4 103 82-120 Ethylbenzene ug/L 50 45.8 92 79-121 lodomethane ug/L 100 110 110 39-154 Methylene Chloride ug/L 50 46.3 93 64-133 Styrene ug/L 50 49.0 98 84-126 Tetrachloroethene ug/L 50 49.4 99 78-122 Toluene ug/L 50 45.4 91 80-121 trans-1,2-Dichloroethene ug/L 50 42.0 84 71-127 trans- 1,3-Dichloropropene ug/L 50 45.5 91 69-141 trans-1,4-Dichloro-2-butene ug/L 50 65AJ 131 40-160 Trichloroethene ug/L 50 47.7 95 78-122 Trichlorofluoromethane ug/L 50 41.7 83 53-137 Vinyl acetate ug/L 100 85.6 86 40-160 Vinyl chloride ug/L 50 46.9 94 58-137 Xylene (Total) ug/L 150 140 93 81-126 1,2-Dichloroethane-d4 (S) % 83 70-130 4-Bromofluorobenzene (S) % 101 70-130 Toluene-d8 (S) % 103 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2170160 2170161 MS MSD 92366996023 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 18.6 21.3 93 106 70-130 13 30 1,1,1-Trichloroethane ug/L ND 20 20 19.6 22.9 98 114 70-130 15 30 1,1,2,2-Tetrachloroethane ug/L ND 20 20 17.2 19.7 86 98 70-130 13 30 1,1,2-Trichloroethane ug/L ND 20 20 19.8 22.7 99 113 70-130 13 30 1,1-Dichloroethane ug/L 1.4 20 20 18.8 21.5 87 101 70-130 13 30 1,1-Dichloroethene ug/L ND 20 20 18.2 20.9 91 105 70-166 14 30 1,2,3-Trichloropropane ug/L ND 20 20 17.3 20.2 87 101 70-130 15 30 1,2-Dibromo-3- ug/L ND 20 20 15.5 20.1 77 101 70-130 26 30 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 20 20 17.9 21.0 89 105 70-130 16 30 1,2-Dichlorobenzene ug/L ND 20 20 18.2 21.8 90 109 70-130 18 30 1,2-Dichloroethane ug/L ND 20 20 18.6 21.3 93 106 70-130 13 30 1,2-Dichloropropane ug/L ND 20 20 19.6 22.4 98 112 70-130 14 30 1,4-Dichlorobenzene ug/L ND 20 20 18.1 20.2 90 101 70-130 11 30 2-Butanone (MEK) ug/L ND 40 40 37.7J 45AJ 94 114 70-130 18 30 2-Hexanone ug/L ND 40 40 40.1J 45AJ 100 114 70-130 13 30 4-Methyl-2-pentanone ug/L ND 40 40 38.8J 44.6J 97 111 70-130 14 30 (MIBK) Acetone ug/L ND 40 40 35.OJ 41.3J 88 103 70-130 16 30 Acrylonitrile ug/L ND 100 100 81.5J 96.1J 81 96 70-130 16 30 Benzene ug/L ND 20 20 18.9 23.0 94 115 70-148 20 30 Bromochloromethane ug/L ND 20 20 18.9 21.8 95 109 70-130 14 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /30/2018 11:53 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 29 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92367075 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2170160 2170161 MS MSD 92366996023 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Bromodichloromethane ug/L ND 20 20 18.9 21.1 94 106 70-130 11 30 Bromoform ug/L ND 20 20 15.8 19.2 79 96 70-130 20 30 Bromomethane ug/L ND 20 20 17.9 20.4 89 102 70-130 13 30 Carbon disulfide ug/L ND 20 20 18.2J 20.2J 91 101 70-130 10 30 Carbon tetrachloride ug/L ND 20 20 19.6 24.5 98 123 70-130 22 30 Chlorobenzene ug/L ND 20 20 18.7 21.4 94 107 70-146 13 30 Chloroethane ug/L ND 20 20 21.2 23.9 106 119 70-130 12 30 Chloroform ug/L ND 20 20 18.4 20.9 92 105 70-130 13 30 Chloromethane ug/L ND 20 20 18.6 20.8 93 104 70-130 11 30 cis-1,2-Dichloroethene ug/L 0.55J 20 20 20.4 22.8 99 111 70-130 11 30 cis-1,3-Dichloropropene ug/L ND 20 20 20.3 22.8 101 114 70-130 12 30 Dibromochloromethane ug/L ND 20 20 17.4 20.6 87 103 70-130 17 30 Dibromomethane ug/L ND 20 20 18.1 21.7 91 108 70-130 18 30 Ethylbenzene ug/L ND 20 20 19.4 21.7 97 108 70-130 11 30 lodomethane ug/L ND 40 40 36.0 40.2 90 101 70-130 11 30 Methylene Chloride ug/L ND 20 20 15.1 18.9 76 95 70-130 22 30 Styrene ug/L ND 20 20 18.1 20.8 91 104 70-130 14 30 Tetrachloroethene ug/L 1.3 20 20 20.3 22.4 95 106 70-130 10 30 Toluene ug/L ND 20 20 19.5 22.4 98 112 70-155 14 30 trans-1,2-Dichloroethene ug/L ND 20 20 17.9 20.3 89 101 70-130 13 30 trans-1,3-Dichloropropene ug/L ND 20 20 19.5 22.3 98 112 70-130 14 30 trans-1,4-Dichloro-2-butene ug/L ND 20 20 18.6J 21.1J 93 105 70-130 12 30 Trichloroethene ug/L ND 20 20 19.1 22.1 94 109 69-151 15 30 Trichlorofluoromethane ug/L ND 20 20 18.3 20.7 91 104 70-130 13 30 Vinyl acetate ug/L ND 40 40 29.6J 33.2J 74 83 70-130 11 30 Vinyl chloride ug/L ND 20 20 20.4 23.2 102 116 70-130 13 30 1,2-Dichloroethane-d4 (S) % 94 93 70-130 4-Bromofluorobenzene (S) % 99 97 70-130 Toluene-d8 (S) % 104 104 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /30/2018 11:53 AM without the written consent of Pace Analytical Services, LLC. Page 22 of 29 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92367075 QC Batch: 391009 Analysis Method: EPA 180.1 QC Batch Method: EPA 180.1 Analysis Description: 180.1 Turbidity Associated Lab Samples: 92367075002 METHOD BLANK: 2169592 Matrix: Water Associated Lab Samples: 92367075002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Turbidity NTU ND 1.0 0.50 12/14/17 23:10 LABORATORY CONTROL SAMPLE: 2169593 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Turbidity NTU 10 10.0 100 90-110 SAMPLE DUPLICATE: 2169594 92367133002 Dup Max Parameter Units Result Result RPD RPD Qualifiers Turbidity NTU 7.5 D6 SAMPLE DUPLICATE: 2169595 92367133017 Dup Max Parameter Units Result Result RPD RPD Qualifiers Turbidity NTU 1.2 1.1 14 10 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /30/2018 11:53 AM without the written consent of Pace Analytical Services, LLC. Page 23 of 29 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92367075 QC Batch: 391010 Analysis Method: EPA 180.1 QC Batch Method: EPA 180.1 Analysis Description: 180.1 Turbidity Associated Lab Samples: 92367075001, 92367075003 METHOD BLANK: 2169596 Matrix: Water Associated Lab Samples: 92367075001, 92367075003 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Turbidity NTU ND 1.0 0.50 12/15/17 01:39 LABORATORY CONTROL SAMPLE: 2169597 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Turbidity NTU 10 10.1 101 90-110 SAMPLE DUPLICATE: 2169598 92367133005 Dup Max Parameter Units Result Result RPD RPD Qualifiers Turbidity NTU 9.3 9.7 4 10 SAMPLE DUPLICATE: 2169599 92367133004 Dup Max Parameter Units Result Result RPD RPD Qualifiers Turbidity NTU 31.6 36.1 13 10 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /30/2018 11:53 AM without the written consent of Pace Analytical Services, LLC. Page 24 of 29 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: SURRY CLOSED -MT. AIRY (AM) Pace Project No.: 92367075 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte PASI-M Pace Analytical Services - Minneapolis WORKORDER QUALIFIERS WO: 92367075 [1] Report revised on 1.30.18 to correct reporting limits for 6020 analytes. ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /30/2018 11:53 AM without the written consent of Pace Analytical Services, LLC. Page 25 of 29 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: SURRY CLOSED -MT. AIRY (AM) 92367075 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92367075001 MW-11 EPA 3010A 391501 EPA 6010 391629 92367075002 MW-6 EPA 3010A 391501 EPA 6010 391629 92367075003 SCALEHOUSE EPA 3010A 391501 EPA6010 391629 92367075011 MW-12D EPA 3010A 391698 EPA 6010 391786 92367075001 MW-11 EPA 3020 517019 EPA 6020B 517158 92367075002 MW-6 EPA 3020 517019 EPA 6020B 517158 92367075003 SCALEHOUSE EPA 3020 517019 EPA 6020B 517158 92367075011 MW-12D EPA 3020 517021 EPA 6020B 517159 92367075001 MW-11 EPA 8260 391124 92367075002 MW-6 EPA 8260 391124 92367075003 SCALEHOUSE EPA 8260 391124 92367075011 MW-12D EPA 8260 391124 92367075001 MW-11 EPA 180.1 391010 92367075002 MW-6 EPA 180.1 391009 92367075003 SCALEHOUSE EPA 180.1 391010 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /30/2018 11:53 AM without the written consent of Pace Analytical Services, LLC. Page 26 of 29 Document Name: Document Revised. August 4, 2017 Sample Condition Upon Receipt(SCUR) Page 1 of 2 _� aceAnapical Document No.: Issuing Authority: F-CAR-CS-033-Rev.04 Pace Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersvill Raleigh❑ Mechanicsville❑ Sample Condition Client Na Wv# : 92367075 Upon ReceiptProject #: l [Hurter: 1111111 Jill J11J1 ❑Fed Ex ❑UPS 'CUSPS ❑Client 111111 ❑ Commercial ace ❑other. ` 92367015 Custody Seal Present? [—]YesL [�I�b Seals Intact? ❑Yes o I f 1 `" 1 Date/InitlaEs Person Examining t = `''1 J Packing Material: ❑Bubble Wrap ubble Bags [—]None ❑ other Blologlc ljssue Frozen? Thermomet r ', ❑Yes i4o ❑N/A ,� � � �XVet ❑Blue ❑None 7- "R", un 1D: T f Ice: rx� Correction Factor: Cooler Temp Corrected (°C): J - V Temp should be above freezing to VC [)Samples out of temp criteria. Samples on ice, cooling process has begun USDA Regulated Soil 4)/A, water sampiel Did samples n fia a in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source V ter �ionally, ❑Yes including Hawaii and Puerto Ricoj7 [:]Ye s N Comments/Discrepancy: Chain of Custody Present? Y s ❑No ❑N/A 1, Samples Arrived within Hold Time? QJfVJs ❑No N/A 2. Short Hold Time Analysis (c72 hr.)? Dyes o ❑N/A 3. Rush Turn Around Time Requested? ❑Yes o ❑NIA 4. Sufficient Volume? s ❑No ❑N/A 5. Correct Containers Used? 'Q�s ❑No ❑N/A 6. -Pace Containers Used? es ❑No ❑N/A Containers Intact? ❑No ❑N/A 7, Dissolved analysis: Samples Field Filtered? ❑Yes 0 No Sample labels Match CDC? Dyes (S)o N/A rl -Includes Date/Time/ID/Analysis Matrix: Headspace in VOA Vials (>5-6mm)? Dyes ❑No I &A 10 Trip Blank Present? [—]yes ❑N/A 11. Trip Blank Custody Seals Present? ❑yes ❑No N CLIENT NOT IFICATION/RESOLUTION Field Data Required? ❑Yes ❑No Person Contacted: Date/Time: Comments/Sample Discrepancy: Lot ID of split containers: Project Manager SCURF Review: �L Date: Project Manager SRF Review: �� Date: Iz i f 7 Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out Df temp, incorrect containers) Page 27 of 29 Document Name: Document Revised: August 4, 2017 Sample Condition Upon Receipt{SCUR) Page 2 of 2 Document No.: Issuing Authority: 'ace Analytical F-CAR-CS-033-Rev.04 Pace Quality dffice *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. "Bottom half of box is to list number of bottles Project It WO# : 92367075 PM: RWC Due Date: 12/29/17 CLIENT: 92-Municipal a E u Z M 4 > u E 7 a M. M Z v 2 n j u E w 7 m a m 2 `a u E o 7 N a m Z m v n u M 4 - 7 .•+ a m v N x O N v a E N H v a m ry v m z a J E Z nv a m ^ O z m w v ry — a E N a c. w v -- N r+ T O z a J E n a a M Z C _ N M :7 E m q 3 u a Z m v c n E ¢ a - ''+ l7 a¢¢ N T a u x p E a - L7 u Z 'Q Z v a E a .� E Ln m L7 ry v v 4 ry x a E ¢ v - ,1 l7 a N V x a 0 N 2 a E a < E N mm l7 a u ¢ Z _ U r C1 L E ¢ E o ^ N M Lf l7 a 4 z = ¢ o > E C) CM l7 a>> ¢ m z ¢ p > E p m l7 ¢ — ? ? 4 D > E 4 m l7 z O T d o > E a l7 a> Q Z v; y A V O ¢ Z ° Q m = A !0 ¢ « h N a v n A I a v J E n a u< m ml a = " A E N m r1 m C a 3 U> a ? y _ E l7 L Z ca 1 2 3 4 n 5 6 7 S 4 10 11 12 pH Adjustment Log for Preserved Samples Sample la Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot d Page 28 of 29 M N ZZalj4imf Section A Required Client Information: Company: Municipal Engin Address es SHpwash Dr Garner. NC 27529 Email jpfohl@mesco.Com Phone (9t9}772-5393 Reouested Due Date Fax SAMPLE ID One Character per box. (A-Z. 0-9 1, -) Sample Ids must be unique W D.1 F 1 MVII-11 2 MW-12D 3 Mw-& 4 Scalehouse 5 6 8 Section B Required Project Information: Report To: Jonathan Pfohl Copy To ,Purchase Order #: Prejecl Name, Burry Closer Proiect #: CHAIN -OF -CUSTODY 1 Analytical Request Document o The Chain -of -Custody is a LEGAL DOCLJMENT- All relevant fields must be completed accurately. rn N Iv Section C M Invoice Information: Page 1 Of 1 1L Attention: Company Name: AddressReaulatary A enc Pace Quote. AM) Pace Project Manager. trey ,carfer pacelabs.com, State 1 Location Pace Profile W 2103-3 NC MATRCODE � COLLECTED z o Preservative5I% Z } a punkin Wales pW q U Water WT U Wa.te WotG, WW Prod-1 P _ 4 [7 W O O O to m s0'`vsoim t� START END oL w N V wiP,, wR z m p m Ail AR Q Othn OT % w F` Z 0 O d ? T`: Y d Q V< DATE TIME ATE TIME Q __ _ s 0 z z H w113 "I x x x wT wT x x x WT x x x VV7 ADDITtONALCOMMENTS RELINQUISHED BY I AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION DATE TIME I ci L L SAMPLE CONDITIONS SAMPLER NAME AND SIGNATURE o U PRINT Name of SAMPLER: a; a SIGNATURE of SAMPLER: 1 „ DATE Signed: ;} I , 7'I t w y w y Al m 5-1V) lacieAnalXical" www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 January 09, 2018 Mr. Jonathan Pfohl Municipal Engineering Services 68 Shipwash Dr. Garner, NC 27529 RE: Project: Surry MSWLF SWs Pace Project No.: 92366776 Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory on December 13, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Trey Carter trey. carter@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 36 lacmnalytical' www.pacelabs.corn Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Surry MSWLF SWs Pace Project No.: 92366776 Minnesota Certification IDs 1700 Elm Street SE, Suite 200, Minneapolis, MN 55414- 2485 A21-A Certification #: 2926.01 Alabama Certification #: 40770 Alaska Contaminated Sites Certification #: 17-009 Alaska DW Certification #: MN00064 Arizona Certification #: AZ0014 Arkansas Certification #: 88-0680 California Certification #: 2929 CNMI Saipan Certification #:MP0003 Colorado Certification #: MN00064 Connecticut Certification #: PH-0256 EPA Region 8+Wyoming DW Certification #: via MN 027- 053-137 Florida Certification #: E87605 Georgia Certification #: 959 Guam EPA Certification #: MN00064 Hawaii Certification #: MN00064 Idaho Certification #: MN00064 Illinois Certification #: 200011 Indiana Certification #: C-MN-01 Iowa Certification #: 368 Kansas Certification #: E-10167 Kentucky DW Certification #: 90062 Kentucky WW Certification #: 90062 Louisiana DEQ Certification #: 03086 Louisiana DW Certification #: MN00064 Maine Certification #: MN00064 Maryland Certification #: 322 Massachusetts Certification #: M-MN064 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Michigan Certification #: 9909 Minnesota Certification #: 027-053-137 Mississippi Certification #: MN00064 Montana Certification #: CERT0092 Nebraska Certification #: NE-OS-18-06 Nevada Certification #: MN00064 New Hampshire Certification #: 2081 New Jersey Certification #: MN002 New York Certification #: 11647 North Carolina DW Certification #: 27700 North Carolina WW Certification #: 530 North Dakota Certification #: R-036 Ohio DW Certification #: 41244 Ohio VAP Certification #: CL101 Oklahoma Certification #: 9507 Oregon NwTPH Certification #: MN300001 Oregon Secondary Certification #: MN200001 Pennsylvania Certification #: 68-00563 Puerto Rico Certification #: MN00064 South Carolina Certification #:74003001 Tennessee Certification #: TN02818 Texas Certification #: T104704192 Utah Certification #: MN00064 Virginia Certification #: 460163 Washington Certification #: C486 West Virginia DW Certification #: 9952 C West Virginia DEP Certification #: 382 Wisconsin Certification #: 999407970 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: Surry MSWLF SWs Pace Project No.: 92366776 Lab ID Sample ID Matrix Date Collected Date Received 92366776001 SW-1 Water 12/12/17 17:02 12/13/17 09:00 92366776002 SW-2 Water 12/12/17 17:00 12/13/17 09:00 92366776003 SW-3 Water 12/12/17 14:00 12/13/17 09:00 92366776004 SW-4 Water 12/12/17 14:05 12/13/17 09:00 92366776005 SW -A Water 12/12/17 16:10 12/13/17 09:00 92366776006 SW-13 Water 12/12/17 16:20 12/13/17 09:00 92366776007 SWN-1 Water 12/12/17 16:00 12/13/17 09:00 92366776008 SWN-2 Water 12/12/17 15:55 12/13/17 09:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: Surry MSWLF SWs 92366776 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92366776001 SW-1 EPA 6010 SER 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C 92366776002 SW-2 EPA 6010 SER 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C 92366776003 SW-3 EPA 6010 SER 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C 92366776004 SW-4 EPA 6010 SER 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C 92366776005 SW -A EPA 6010 SER 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C 92366776006 SW-B EPA 6010 SER 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C 92366776007 SWN-1 EPA 6010 SER 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C 92366776008 SWN-2 EPA 6010 SER 14 PASI-A EPA 6020E TT3 1 PASI-M EPA 8260 CAH 50 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry MSWLF SWs Pace Project No.: 92366776 Sample: SW-1 Lab ID: 92366776001 Collected: 12/12/17 17:02 Received: 12/13/17 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Vanadium Zinc 1400111 -1 �41 :4 9 [y :2 LTA 61 Thallium 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane Date: 01 /09/2018 11:46 AM Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 01/02/18 11:30 01/02/18 22:06 7440-36-0 ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:06 7440-38-2 13.6J ug/L 100 2.5 1 01/02/18 11:30 01/02/18 22:06 7440-39-3 ND ug/L 1.0 0.50 1 01/02/18 11:30 01/02/18 22:06 7440-41-7 ND ug/L 1.0 0.50 1 01/02/18 11:30 01/02/18 22:06 7440-43-9 ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:06 7440-47-3 ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:06 7440-48-4 ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:06 7440-50-8 ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:06 7439-92-1 ND ug/L 50.0 2.5 1 01/02/18 11:30 01/02/18 22:06 7440-02-0 ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:06 7782-49-2 ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:06 7440-22-4 ND ug/L 25.0 2.5 1 01/02/18 11:30 01/02/18 22:06 7440-62-2 ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:06 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3020 ND ug/L 0.10 0.028 1 01/08/18 08:43 01/08/18 12:13 7440-28-0 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 12/15/17 03:47 67-64-1 ND ug/L 200 1.9 1 12/15/17 03:47 107-13-1 ND ug/L 1.0 0.25 1 12/15/17 03:47 71-43-2 ND ug/L 3.0 0.17 1 12/15/17 03:47 74-97-5 ND ug/L 1.0 0.18 1 12/15/17 03:47 75-27-4 ND ug/L 3.0 0.26 1 12/15/17 03:47 75-25-2 ND ug/L 10.0 0.29 1 12/15/17 03:47 74-83-9 ND ug/L 100 0.96 1 12/15/17 03:47 78-93-3 ND ug/L 100 1.2 1 12/15/17 03:47 75-15-0 ND ug/L 1.0 0.25 1 12/15/17 03:47 56-23-5 ND ug/L 3.0 0.23 1 12/15/17 03:47 108-90-7 ND ug/L 10.0 0.54 1 12/15/17 03:47 75-00-3 ND ug/L 5.0 0.14 1 12/15/17 03:47 67-66-3 ND ug/L 1.0 0.11 1 12/15/17 03:47 74-87-3 ND ug/L 13.0 2.0 1 12/15/17 03:47 96-12-8 ND ug/L 3.0 0.21 1 12/15/17 03:47 124-48-1 ND ug/L 1.0 0.27 1 12/15/17 03:47 106-93-4 ND ug/L 10.0 0.21 1 12/15/17 03:47 74-95-3 ND ug/L 5.0 0.30 1 12/15/17 03:47 95-50-1 ND ug/L 1.0 0.33 1 12/15/17 03:47 106-46-7 ND ug/L 100 1.0 1 12/15/17 03:47 110-57-6 ND ug/L 5.0 0.32 1 12/15/17 03:47 75-34-3 ND ug/L 1.0 0.24 1 12/15/17 03:47 107-06-2 ND ug/L 5.0 0.56 1 12/15/17 03:47 75-35-4 ND ug/L 5.0 0.19 1 12/15/17 03:47 156-59-2 ND ug/L 5.0 0.49 1 12/15/17 03:47 156-60-5 ND ug/L 1.0 0.27 1 12/15/17 03:47 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry MSWLF SWs Pace Project No.: 92366776 Sample: SW-1 Lab ID: 92366776001 Collected: 12/12/17 17:02 Received: 12/13/17 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 12/15/17 03:47 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 12/15/17 03:47 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 12/15/17 03:47 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 12/15/17 03:47 591-78-6 lodomethane ND ug/L 10.0 0.32 1 12/15/17 03:47 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 12/15/17 03:47 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 12/15/17 03:47 108-10-1 Styrene ND ug/L 1.0 0.26 1 12/15/17 03:47 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 12/15/17 03:47 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 12/15/17 03:47 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 12/15/17 03:47 127-18-4 Toluene ND ug/L 1.0 0.26 1 12/15/17 03:47 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 12/15/17 03:47 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 12/15/17 03:47 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 12/15/17 03:47 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 12/15/17 03:47 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 12/15/17 03:47 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 12/15/17 03:47 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 12/15/17 03:47 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 12/15/17 03:47 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 12/15/17 03:47 460-00-4 1,2-Dichloroethane-d4 (S) 100 % 70-130 1 12/15/17 03:47 17060-07-0 Toluene-d8 (S) 104 % 70-130 1 12/15/17 03:47 2037-26-5 Date: 01 /09/2018 11:46 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry MSWLF SWs Pace Project No.: 92366776 Sample: SW-2 Lab ID: 92366776002 Collected: 12/12/17 17:00 Received: 12/13/17 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Vanadium Zinc 1400111 -1 �41 :4 9 [y :2 LTA 61 Thallium 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane Date: 01 /09/2018 11:46 AM Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 01/02/18 11:30 01/02/18 22:16 7440-36-0 ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:16 7440-38-2 8.7J ug/L 100 2.5 1 01/02/18 11:30 01/02/18 22:16 7440-39-3 ND ug/L 1.0 0.50 1 01/02/18 11:30 01/02/18 22:16 7440-41-7 ND ug/L 1.0 0.50 1 01/02/18 11:30 01/02/18 22:16 7440-43-9 ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:16 7440-47-3 8.91 ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:16 7440-48-4 ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:16 7440-50-8 ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:16 7439-92-1 ND ug/L 50.0 2.5 1 01/02/18 11:30 01/02/18 22:16 7440-02-0 ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:16 7782-49-2 ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:16 7440-22-4 ND ug/L 25.0 2.5 1 01/02/18 11:30 01/02/18 22:16 7440-62-2 ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:16 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3020 ND ug/L 0.10 0.028 1 01/08/18 08:43 01/08/18 12:32 7440-28-0 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 12/15/17 04:05 67-64-1 ND ug/L 200 1.9 1 12/15/17 04:05 107-13-1 ND ug/L 1.0 0.25 1 12/15/17 04:05 71-43-2 ND ug/L 3.0 0.17 1 12/15/17 04:05 74-97-5 ND ug/L 1.0 0.18 1 12/15/17 04:05 75-27-4 ND ug/L 3.0 0.26 1 12/15/17 04:05 75-25-2 ND ug/L 10.0 0.29 1 12/15/17 04:05 74-83-9 ND ug/L 100 0.96 1 12/15/17 04:05 78-93-3 ND ug/L 100 1.2 1 12/15/17 04:05 75-15-0 ND ug/L 1.0 0.25 1 12/15/17 04:05 56-23-5 ND ug/L 3.0 0.23 1 12/15/17 04:05 108-90-7 ND ug/L 10.0 0.54 1 12/15/17 04:05 75-00-3 ND ug/L 5.0 0.14 1 12/15/17 04:05 67-66-3 ND ug/L 1.0 0.11 1 12/15/17 04:05 74-87-3 ND ug/L 13.0 2.0 1 12/15/17 04:05 96-12-8 ND ug/L 3.0 0.21 1 12/15/17 04:05 124-48-1 ND ug/L 1.0 0.27 1 12/15/17 04:05 106-93-4 ND ug/L 10.0 0.21 1 12/15/17 04:05 74-95-3 ND ug/L 5.0 0.30 1 12/15/17 04:05 95-50-1 ND ug/L 1.0 0.33 1 12/15/17 04:05 106-46-7 ND ug/L 100 1.0 1 12/15/17 04:05 110-57-6 ND ug/L 5.0 0.32 1 12/15/17 04:05 75-34-3 ND ug/L 1.0 0.24 1 12/15/17 04:05 107-06-2 ND ug/L 5.0 0.56 1 12/15/17 04:05 75-35-4 0.84J ug/L 5.0 0.19 1 12/15/17 04:05 156-59-2 ND ug/L 5.0 0.49 1 12/15/17 04:05 156-60-5 ND ug/L 1.0 0.27 1 12/15/17 04:05 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry MSWLF SWs Pace Project No.: 92366776 Sample: SW-2 Lab ID: 92366776002 Collected: 12/12/17 17:00 Received: 12/13/17 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 12/15/17 04:05 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 12/15/17 04:05 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 12/15/17 04:05 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 12/15/17 04:05 591-78-6 lodomethane ND ug/L 10.0 0.32 1 12/15/17 04:05 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 12/15/17 04:05 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 12/15/17 04:05 108-10-1 Styrene ND ug/L 1.0 0.26 1 12/15/17 04:05 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 12/15/17 04:05 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 12/15/17 04:05 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 12/15/17 04:05 127-18-4 Toluene ND ug/L 1.0 0.26 1 12/15/17 04:05 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 12/15/17 04:05 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 12/15/17 04:05 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 12/15/17 04:05 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 12/15/17 04:05 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 12/15/17 04:05 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 12/15/17 04:05 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 12/15/17 04:05 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 12/15/17 04:05 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 12/15/17 04:05 460-00-4 1,2-Dichloroethane-d4 (S) 99 % 70-130 1 12/15/17 04:05 17060-07-0 Toluene-d8 (S) 105 % 70-130 1 12/15/17 04:05 2037-26-5 Date: 01 /09/2018 11:46 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry MSWLF SWs Pace Project No.: 92366776 Sample: SW-3 Lab ID: 92366776003 Collected: 12/12/17 14:00 Received: 12/13/17 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Vanadium Zinc 1400111 -1 �41 :4 9 [y :2 LTA 61 Thallium 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane Date: 01 /09/2018 11:46 AM Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 01/02/18 11:30 01/02/18 22:25 7440-36-0 ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:25 7440-38-2 15.6J ug/L 100 2.5 1 01/02/18 11:30 01/02/18 22:25 7440-39-3 ND ug/L 1.0 0.50 1 01/02/18 11:30 01/02/18 22:25 7440-41-7 ND ug/L 1.0 0.50 1 01/02/18 11:30 01/02/18 22:25 7440-43-9 ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:25 7440-47-3 3.2J ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:25 7440-48-4 ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:25 7440-50-8 ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:25 7439-92-1 ND ug/L 50.0 2.5 1 01/02/18 11:30 01/02/18 22:25 7440-02-0 ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:25 7782-49-2 ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:25 7440-22-4 ND ug/L 25.0 2.5 1 01/02/18 11:30 01/02/18 22:25 7440-62-2 ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:25 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3020 ND ug/L 0.10 0.028 1 01/08/18 08:43 01/08/18 12:16 7440-28-0 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 12/15/17 04:23 67-64-1 ND ug/L 200 1.9 1 12/15/17 04:23 107-13-1 ND ug/L 1.0 0.25 1 12/15/17 04:23 71-43-2 ND ug/L 3.0 0.17 1 12/15/17 04:23 74-97-5 ND ug/L 1.0 0.18 1 12/15/17 04:23 75-27-4 ND ug/L 3.0 0.26 1 12/15/17 04:23 75-25-2 ND ug/L 10.0 0.29 1 12/15/17 04:23 74-83-9 ND ug/L 100 0.96 1 12/15/17 04:23 78-93-3 ND ug/L 100 1.2 1 12/15/17 04:23 75-15-0 ND ug/L 1.0 0.25 1 12/15/17 04:23 56-23-5 ND ug/L 3.0 0.23 1 12/15/17 04:23 108-90-7 ND ug/L 10.0 0.54 1 12/15/17 04:23 75-00-3 ND ug/L 5.0 0.14 1 12/15/17 04:23 67-66-3 ND ug/L 1.0 0.11 1 12/15/17 04:23 74-87-3 ND ug/L 13.0 2.0 1 12/15/17 04:23 96-12-8 ND ug/L 3.0 0.21 1 12/15/17 04:23 124-48-1 ND ug/L 1.0 0.27 1 12/15/17 04:23 106-93-4 ND ug/L 10.0 0.21 1 12/15/17 04:23 74-95-3 ND ug/L 5.0 0.30 1 12/15/17 04:23 95-50-1 ND ug/L 1.0 0.33 1 12/15/17 04:23 106-46-7 ND ug/L 100 1.0 1 12/15/17 04:23 110-57-6 ND ug/L 5.0 0.32 1 12/15/17 04:23 75-34-3 ND ug/L 1.0 0.24 1 12/15/17 04:23 107-06-2 ND ug/L 5.0 0.56 1 12/15/17 04:23 75-35-4 ND ug/L 5.0 0.19 1 12/15/17 04:23 156-59-2 ND ug/L 5.0 0.49 1 12/15/17 04:23 156-60-5 ND ug/L 1.0 0.27 1 12/15/17 04:23 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 9 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry MSWLF SWs Pace Project No.: 92366776 Sample: SW-3 Lab ID: 92366776003 Collected: 12/12/17 14:00 Received: 12/13/17 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 12/15/17 04:23 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 12/15/17 04:23 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 12/15/17 04:23 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 12/15/17 04:23 591-78-6 lodomethane ND ug/L 10.0 0.32 1 12/15/17 04:23 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 12/15/17 04:23 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 12/15/17 04:23 108-10-1 Styrene ND ug/L 1.0 0.26 1 12/15/17 04:23 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 12/15/17 04:23 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 12/15/17 04:23 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 12/15/17 04:23 127-18-4 Toluene ND ug/L 1.0 0.26 1 12/15/17 04:23 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 12/15/17 04:23 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 12/15/17 04:23 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 12/15/17 04:23 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 12/15/17 04:23 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 12/15/17 04:23 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 12/15/17 04:23 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 12/15/17 04:23 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 12/15/17 04:23 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 12/15/17 04:23 460-00-4 1,2-Dichloroethane-d4 (S) 99 % 70-130 1 12/15/17 04:23 17060-07-0 Toluene-d8 (S) 102 % 70-130 1 12/15/17 04:23 2037-26-5 Date: 01 /09/2018 11:46 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry MSWLF SWs Pace Project No.: 92366776 Sample: SW-4 Lab ID: 92366776004 Collected: 12/12/17 14:05 Received: 12/13/17 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Antimony ND ug/L 6.0 3.9 1 01/02/18 11:30 01/02/18 22:28 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:28 7440-38-2 Barium 14.8J ug/L 100 2.5 1 01/02/18 11:30 01/02/18 22:28 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 01/02/18 11:30 01/02/18 22:28 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 01/02/18 11:30 01/02/18 22:28 7440-43-9 Chromium ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:28 7440-47-3 Cobalt ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:28 7440-48-4 Copper ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:28 7440-50-8 Lead ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:28 7439-92-1 Nickel ND ug/L 50.0 2.5 1 01/02/18 11:30 01/02/18 22:28 7440-02-0 Selenium ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:28 7782-49-2 Silver ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:28 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 01/02/18 11:30 01/02/18 22:28 7440-62-2 Zinc ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:28 7440-66-6 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020 Thallium ND ug/L 0.10 0.028 1 01/08/18 08:43 01/08/18 12:18 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 12/15/17 04:40 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 12/15/17 04:40 107-13-1 Benzene ND ug/L 1.0 0.25 1 12/15/17 04:40 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 12/15/17 04:40 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 12/15/17 04:40 75-27-4 Bromoform ND ug/L 3.0 0.26 1 12/15/17 04:40 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 12/15/17 04:40 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 12/15/17 04:40 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 12/15/17 04:40 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 12/15/17 04:40 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 12/15/17 04:40 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 12/15/17 04:40 75-00-3 Chloroform ND ug/L 5.0 0.14 1 12/15/17 04:40 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 12/15/17 04:40 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 12/15/17 04:40 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 12/15/17 04:40 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 12/15/17 04:40 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 12/15/17 04:40 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 12/15/17 04:40 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 12/15/17 04:40 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 12/15/17 04:40 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 12/15/17 04:40 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 12/15/17 04:40 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 12/15/17 04:40 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 12/15/17 04:40 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 12/15/17 04:40 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 12/15/17 04:40 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry MSWLF SWs Pace Project No.: 92366776 Sample: SW-4 Lab ID: 92366776004 Collected: 12/12/17 14:05 Received: 12/13/17 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 12/15/17 04:40 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 12/15/17 04:40 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 12/15/17 04:40 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 12/15/17 04:40 591-78-6 lodomethane ND ug/L 10.0 0.32 1 12/15/17 04:40 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 12/15/17 04:40 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 12/15/17 04:40 108-10-1 Styrene ND ug/L 1.0 0.26 1 12/15/17 04:40 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 12/15/17 04:40 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 12/15/17 04:40 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 12/15/17 04:40 127-18-4 Toluene ND ug/L 1.0 0.26 1 12/15/17 04:40 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 12/15/17 04:40 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 12/15/17 04:40 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 12/15/17 04:40 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 12/15/17 04:40 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 12/15/17 04:40 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 12/15/17 04:40 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 12/15/17 04:40 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 12/15/17 04:40 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 12/15/17 04:40 460-00-4 1,2-Dichloroethane-d4 (S) 99 % 70-130 1 12/15/17 04:40 17060-07-0 Toluene-d8 (S) 106 % 70-130 1 12/15/17 04:40 2037-26-5 Date: 01 /09/2018 11:46 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 12 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry MSWLF SWs Pace Project No.: 92366776 Sample: SW -A Lab ID: 92366776005 Collected: 12/12/17 16:10 Received: 12/13/17 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 301 OA Antimony ND ug/L 6.0 3.9 1 01/02/18 11:30 01/02/18 22:31 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:31 7440-38-2 Barium 13.OJ ug/L 100 2.5 1 01/02/18 11:30 01/02/18 22:31 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 01/02/18 11:30 01/02/18 22:31 7440-41-7 Cadmium 0.84J ug/L 1.0 0.50 1 01/02/18 11:30 01/02/18 22:31 7440-43-9 Chromium ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:31 7440-47-3 Cobalt ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:31 7440-48-4 Copper ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:31 7440-50-8 Lead ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:31 7439-92-1 Nickel ND ug/L 50.0 2.5 1 01/02/18 11:30 01/02/18 22:31 7440-02-0 Selenium ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:31 7782-49-2 Silver ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:31 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 01/02/18 11:30 01/02/18 22:31 7440-62-2 Zinc ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:31 7440-66-6 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020 Thallium ND ug/L 0.10 0.028 1 01/08/18 08:43 01/08/18 12:21 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 12/15/17 04:58 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 12/15/17 04:58 107-13-1 Benzene ND ug/L 1.0 0.25 1 12/15/17 04:58 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 12/15/17 04:58 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 12/15/17 04:58 75-27-4 Bromoform ND ug/L 3.0 0.26 1 12/15/17 04:58 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 12/15/17 04:58 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 12/15/17 04:58 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 12/15/17 04:58 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 12/15/17 04:58 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 12/15/17 04:58 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 12/15/17 04:58 75-00-3 Chloroform ND ug/L 5.0 0.14 1 12/15/17 04:58 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 12/15/17 04:58 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 12/15/17 04:58 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 12/15/17 04:58 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 12/15/17 04:58 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 12/15/17 04:58 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 12/15/17 04:58 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 12/15/17 04:58 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 12/15/17 04:58 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 12/15/17 04:58 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 12/15/17 04:58 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 12/15/17 04:58 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 12/15/17 04:58 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 12/15/17 04:58 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 12/15/17 04:58 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry MSWLF SWs Pace Project No.: 92366776 Sample: SW -A Lab ID: 92366776005 Collected: 12/12/17 16:10 Received: 12/13/17 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 12/15/17 04:58 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 12/15/17 04:58 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 12/15/17 04:58 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 12/15/17 04:58 591-78-6 lodomethane ND ug/L 10.0 0.32 1 12/15/17 04:58 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 12/15/17 04:58 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 12/15/17 04:58 108-10-1 Styrene ND ug/L 1.0 0.26 1 12/15/17 04:58 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 12/15/17 04:58 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 12/15/17 04:58 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 12/15/17 04:58 127-18-4 Toluene ND ug/L 1.0 0.26 1 12/15/17 04:58 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 12/15/17 04:58 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 12/15/17 04:58 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 12/15/17 04:58 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 12/15/17 04:58 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 12/15/17 04:58 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 12/15/17 04:58 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 12/15/17 04:58 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 12/15/17 04:58 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 93 % 70-130 1 12/15/17 04:58 460-00-4 1,2-Dichloroethane-d4 (S) 86 % 70-130 1 12/15/17 04:58 17060-07-0 Toluene-d8 (S) 101 % 70-130 1 12/15/17 04:58 2037-26-5 Date: 01 /09/2018 11:46 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 14 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry MSWLF SWs Pace Project No.: 92366776 Sample: SW-B Lab ID: 92366776006 Collected: 12/12/17 16:20 Received: 12/13/17 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Antimony ND ug/L 6.0 3.9 1 01/02/18 11:30 01/02/18 22:35 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:35 7440-38-2 Barium 12.8J ug/L 100 2.5 1 01/02/18 11:30 01/02/18 22:35 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 01/02/18 11:30 01/02/18 22:35 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 01/02/18 11:30 01/02/18 22:35 7440-43-9 Chromium ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:35 7440-47-3 Cobalt ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:35 7440-48-4 Copper ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:35 7440-50-8 Lead ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:35 7439-92-1 Nickel ND ug/L 50.0 2.5 1 01/02/18 11:30 01/02/18 22:35 7440-02-0 Selenium ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:35 7782-49-2 Silver ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:35 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 01/02/18 11:30 01/02/18 22:35 7440-62-2 Zinc ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:35 7440-66-6 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020 Thallium ND ug/L 0.10 0.028 1 01/08/18 08:43 01/08/18 12:24 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 12/15/17 05:16 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 12/15/17 05:16 107-13-1 Benzene ND ug/L 1.0 0.25 1 12/15/17 05:16 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 12/15/17 05:16 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 12/15/17 05:16 75-27-4 Bromoform ND ug/L 3.0 0.26 1 12/15/17 05:16 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 12/15/17 05:16 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 12/15/17 05:16 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 12/15/17 05:16 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 12/15/17 05:16 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 12/15/17 05:16 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 12/15/17 05:16 75-00-3 Chloroform ND ug/L 5.0 0.14 1 12/15/17 05:16 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 12/15/17 05:16 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 12/15/17 05:16 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 12/15/17 05:16 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 12/15/17 05:16 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 12/15/17 05:16 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 12/15/17 05:16 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 12/15/17 05:16 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 12/15/17 05:16 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 12/15/17 05:16 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 12/15/17 05:16 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 12/15/17 05:16 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 12/15/17 05:16 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 12/15/17 05:16 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 12/15/17 05:16 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry MSWLF SWs Pace Project No.: 92366776 Sample: SW-B Lab ID: 92366776006 Collected: 12/12/17 16:20 Received: 12/13/17 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 12/15/17 05:16 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 12/15/17 05:16 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 12/15/17 05:16 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 12/15/17 05:16 591-78-6 lodomethane ND ug/L 10.0 0.32 1 12/15/17 05:16 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 12/15/17 05:16 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 12/15/17 05:16 108-10-1 Styrene ND ug/L 1.0 0.26 1 12/15/17 05:16 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 12/15/17 05:16 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 12/15/17 05:16 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 12/15/17 05:16 127-18-4 Toluene ND ug/L 1.0 0.26 1 12/15/17 05:16 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 12/15/17 05:16 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 12/15/17 05:16 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 12/15/17 05:16 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 12/15/17 05:16 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 12/15/17 05:16 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 12/15/17 05:16 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 12/15/17 05:16 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 12/15/17 05:16 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 91 % 70-130 1 12/15/17 05:16 460-00-4 1,2-Dichloroethane-d4 (S) 97 % 70-130 1 12/15/17 05:16 17060-07-0 Toluene-d8 (S) 97 % 70-130 1 12/15/17 05:16 2037-26-5 Date: 01 /09/2018 11:46 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 16 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry MSWLF SWs Pace Project No.: 92366776 Sample: SWN-1 Lab ID: 92366776007 Collected: 12/12/17 16:00 Received: 12/13/17 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Antimony ND ug/L 6.0 3.9 1 01/02/18 11:30 01/02/18 22:38 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:38 7440-38-2 Barium 12.6J ug/L 100 2.5 1 01/02/18 11:30 01/02/18 22:38 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 01/02/18 11:30 01/02/18 22:38 7440-41-7 Cadmium ND ug/L 1.0 0.50 1 01/02/18 11:30 01/02/18 22:38 7440-43-9 Chromium ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:38 7440-47-3 Cobalt ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:38 7440-48-4 Copper ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:38 7440-50-8 Lead ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:38 7439-92-1 Nickel ND ug/L 50.0 2.5 1 01/02/18 11:30 01/02/18 22:38 7440-02-0 Selenium ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:38 7782-49-2 Silver ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:38 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 01/02/18 11:30 01/02/18 22:38 7440-62-2 Zinc ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:38 7440-66-6 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020 Thallium ND ug/L 0.10 0.028 1 01/08/18 08:43 01/08/18 12:27 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 12/15/17 05:33 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 12/15/17 05:33 107-13-1 Benzene ND ug/L 1.0 0.25 1 12/15/17 05:33 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 12/15/17 05:33 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 12/15/17 05:33 75-27-4 Bromoform ND ug/L 3.0 0.26 1 12/15/17 05:33 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 12/15/17 05:33 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 12/15/17 05:33 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 12/15/17 05:33 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 12/15/17 05:33 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 12/15/17 05:33 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 12/15/17 05:33 75-00-3 Chloroform ND ug/L 5.0 0.14 1 12/15/17 05:33 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 12/15/17 05:33 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 12/15/17 05:33 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 12/15/17 05:33 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 12/15/17 05:33 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 12/15/17 05:33 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 12/15/17 05:33 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 12/15/17 05:33 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 12/15/17 05:33 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 12/15/17 05:33 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 12/15/17 05:33 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 12/15/17 05:33 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 12/15/17 05:33 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 12/15/17 05:33 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 12/15/17 05:33 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry MSWLF SWs Pace Project No.: 92366776 Sample: SWN-1 Lab ID: 92366776007 Collected: 12/12/17 16:00 Received: 12/13/17 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 12/15/17 05:33 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 12/15/17 05:33 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 12/15/17 05:33 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 12/15/17 05:33 591-78-6 lodomethane ND ug/L 10.0 0.32 1 12/15/17 05:33 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 12/15/17 05:33 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 12/15/17 05:33 108-10-1 Styrene ND ug/L 1.0 0.26 1 12/15/17 05:33 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 12/15/17 05:33 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 12/15/17 05:33 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 12/15/17 05:33 127-18-4 Toluene ND ug/L 1.0 0.26 1 12/15/17 05:33 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 12/15/17 05:33 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 12/15/17 05:33 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 12/15/17 05:33 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 12/15/17 05:33 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 12/15/17 05:33 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 12/15/17 05:33 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 12/15/17 05:33 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 12/15/17 05:33 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 95 % 70-130 1 12/15/17 05:33 460-00-4 1,2-Dichloroethane-d4 (S) 102 % 70-130 1 12/15/17 05:33 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 12/15/17 05:33 2037-26-5 Date: 01 /09/2018 11:46 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 18 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry MSWLF SWs Pace Project No.: 92366776 Sample: SWN-2 Lab ID: 92366776008 Collected: 12/12/17 15:55 Received: 12/13/17 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 301 OA Antimony ND ug/L 6.0 3.9 1 01/02/18 11:30 01/02/18 22:41 7440-36-0 Arsenic ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:41 7440-38-2 Barium 13.OJ ug/L 100 2.5 1 01/02/18 11:30 01/02/18 22:41 7440-39-3 Beryllium ND ug/L 1.0 0.50 1 01/02/18 11:30 01/02/18 22:41 7440-41-7 Cadmium 1.2 ug/L 1.0 0.50 1 01/02/18 11:30 01/02/18 22:41 7440-43-9 Chromium ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:41 7440-47-3 Cobalt ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:41 7440-48-4 Copper ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:41 7440-50-8 Lead ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:41 7439-92-1 Nickel ND ug/L 50.0 2.5 1 01/02/18 11:30 01/02/18 22:41 7440-02-0 Selenium ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:41 7782-49-2 Silver ND ug/L 10.0 2.5 1 01/02/18 11:30 01/02/18 22:41 7440-22-4 Vanadium ND ug/L 25.0 2.5 1 01/02/18 11:30 01/02/18 22:41 7440-62-2 Zinc ND ug/L 10.0 5.0 1 01/02/18 11:30 01/02/18 22:41 7440-66-6 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020 Thallium ND ug/L 0.10 0.028 1 01/08/18 08:43 01/08/18 12:30 7440-28-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 12/15/17 05:51 67-64-1 Acrylonitrile ND ug/L 200 1.9 1 12/15/17 05:51 107-13-1 Benzene ND ug/L 1.0 0.25 1 12/15/17 05:51 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 12/15/17 05:51 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 12/15/17 05:51 75-27-4 Bromoform ND ug/L 3.0 0.26 1 12/15/17 05:51 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 12/15/17 05:51 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 12/15/17 05:51 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 12/15/17 05:51 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 12/15/17 05:51 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 12/15/17 05:51 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 12/15/17 05:51 75-00-3 Chloroform ND ug/L 5.0 0.14 1 12/15/17 05:51 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 12/15/17 05:51 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 12/15/17 05:51 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 12/15/17 05:51 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 12/15/17 05:51 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 12/15/17 05:51 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 12/15/17 05:51 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 12/15/17 05:51 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 12/15/17 05:51 110-57-6 1,1-Dichloroethane ND ug/L 5.0 0.32 1 12/15/17 05:51 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 12/15/17 05:51 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 12/15/17 05:51 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 12/15/17 05:51 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 12/15/17 05:51 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 12/15/17 05:51 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry MSWLF SWs Pace Project No.: 92366776 Sample: SWN-2 Lab ID: 92366776008 Collected: 12/12/17 15:55 Received: 12/13/17 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 12/15/17 05:51 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 12/15/17 05:51 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 12/15/17 05:51 100-41-4 2-Hexanone ND ug/L 50.0 0.46 1 12/15/17 05:51 591-78-6 lodomethane ND ug/L 10.0 0.32 1 12/15/17 05:51 74-88-4 Methylene Chloride ND ug/L 1.0 0.97 1 12/15/17 05:51 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 12/15/17 05:51 108-10-1 Styrene ND ug/L 1.0 0.26 1 12/15/17 05:51 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 12/15/17 05:51 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 12/15/17 05:51 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 12/15/17 05:51 127-18-4 Toluene ND ug/L 1.0 0.26 1 12/15/17 05:51 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 12/15/17 05:51 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 12/15/17 05:51 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 12/15/17 05:51 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 12/15/17 05:51 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 12/15/17 05:51 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 12/15/17 05:51 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 12/15/17 05:51 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 12/15/17 05:51 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 87 % 70-130 1 12/15/17 05:51 460-00-4 1,2-Dichloroethane-d4 (S) 89 % 70-130 1 12/15/17 05:51 17060-07-0 Toluene-d8 (S) 114 % 70-130 1 12/15/17 05:51 2037-26-5 Date: 01 /09/2018 11:46 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 20 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry MSWLF SWs Pace Project No.: 92366776 QC Batch: 391698 Analysis Method: EPA 6010 QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92366776001, 92366776002, 92366776003, 92366776004, 92366776005, 92366776006, 92366776007, 92366776008 METHOD BLANK: 2173086 Matrix: Water Associated Lab Samples: 92366776001, 92366776002, 92366776003, 92366776004, 92366776005, 92366776006, 92366776007, 92366776008 Parameter Units Antimony ug/L Arsenic ug/L Barium ug/L Beryllium ug/L Cadmium ug/L Chromium ug/L Cobalt ug/L Copper ug/L Lead ug/L Nickel ug/L Selenium ug/L Silver ug/L Vanadium ug/L Zinc ug/L Blank Result Reporting Limit MDL Analyzed Qualifiers ND 5.0 3.9 01 /02/18 22:00 ND 10.0 5.0 01 /02/18 22:00 ND 5.0 2.5 01 /02/18 22:00 ND 1.0 0.50 01 /02/18 22:00 ND 1.0 0.50 01 /02/18 22:00 ND 5.0 2.5 01 /02/18 22:00 ND 5.0 2.5 01 /02/18 22:00 ND 5.0 2.5 01 /02/18 22:00 ND 5.0 2.5 01 /02/18 22:00 ND 5.0 2.5 01 /02/18 22:00 ND 10.0 5.0 01 /02/18 22:00 ND 5.0 2.5 01 /02/18 22:00 ND 5.0 2.5 01 /02/18 22:00 ND 10.0 5.0 01 /02/18 22:00 LABORATORY CONTROL SAMPLE: Parameter 2173087 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 500 491 98 80-120 Arsenic ug/L 500 471 94 80-120 Barium ug/L 500 489 98 80-120 Beryllium ug/L 500 498 100 80-120 Cadmium ug/L 500 479 96 80-120 Chromium ug/L 500 481 96 80-120 Cobalt ug/L 500 479 96 80-120 Copper ug/L 500 502 100 80-120 Lead ug/L 500 471 94 80-120 Nickel ug/L 500 476 95 80-120 Selenium ug/L 500 476 95 80-120 Silver ug/L 250 242 97 80-120 Vanadium ug/L 500 484 97 80-120 Zinc ug/L 500 467 93 80-120 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry MSWLF SWs Pace Project No.: 92366776 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2173088 2173089 MS MSD 92366776001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 505 504 101 101 75-125 0 20 Arsenic ug/L ND 500 500 487 484 97 97 75-125 1 20 Barium ug/L 13.6J 500 500 510 509 99 99 75-125 0 20 Beryllium ug/L ND 500 500 505 503 101 101 75-125 0 20 Cadmium ug/L ND 500 500 498 496 100 99 75-125 0 20 Chromium ug/L ND 500 500 500 492 100 98 75-125 2 20 Cobalt ug/L ND 500 500 494 491 99 98 75-125 1 20 Copper ug/L ND 500 500 507 506 101 101 75-125 0 20 Lead ug/L ND 500 500 488 484 98 97 75-125 1 20 Nickel ug/L ND 500 500 492 488 98 98 75-125 1 20 Selenium ug/L ND 500 500 505 502 101 100 75-125 1 20 Silver ug/L ND 250 250 252 251 101 100 75-125 0 20 Vanadium ug/L ND 500 500 503 498 101 100 75-125 1 20 Zinc ug/L ND 500 500 496 491 99 98 75-125 1 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 22 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry MSWLF SWs Pace Project No.: 92366776 QC Batch: 516784 Analysis Method: EPA 6020B QC Batch Method: EPA 3020 Analysis Description: 6020E Water UPD5 Associated Lab Samples: 92366776001, 92366776002, 92366776003, 92366776004, 92366776005, 92366776006, 92366776007, 92366776008 METHOD BLANK: 2808129 Matrix: Water Associated Lab Samples: 92366776001, 92366776002, 92366776003, 92366776004, 92366776005, 92366776006, 92366776007, 92366776008 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Thallium ug/L ND 0.10 0.028 01/08/1811:42 LABORATORY CONTROL SAMPLE: 2808130 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Thallium ug/L 100 102 102 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2808131 2808132 MS MSD 92366776002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Thallium ug/L ND 100 100 107 102 107 102 75-125 5 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 23 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry MSWLF SWs Pace Project No.: 92366776 QC Batch: 390968 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92366776001, 92366776002, 92366776003, 92366776004, 92366776005, 92366776006, 92366776007, 92366776008 METHOD BLANK: 2169247 Matrix: Water Associated Lab Samples: 92366776001, 92366776002, 92366776003, 92366776004, 92366776005, 92366776006, 92366776007, 92366776008 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 5.0 0.33 12/15/17 03:12 1,1,1-Trichloroethane ug/L ND 1.0 0.48 12/15/17 03:12 1,1,2,2-Tetrachloroethane ug/L ND 3.0 0.40 12/15/17 03:12 1,1,2-Trichloroethane ug/L ND 1.0 0.29 12/15/17 03:12 1,1-Dichloroethane ug/L ND 5.0 0.32 12/15/17 03:12 1,1-Dichloroethene ug/L ND 5.0 0.56 12/15/17 03:12 1,2,3-Trichloropropane ug/L ND 1.0 0.41 12/15/17 03:12 1,2-Dibromo-3-chloropropane ug/L ND 13.0 2.0 12/15/17 03:12 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 12/15/17 03:12 1,2-Dichlorobenzene ug/L ND 5.0 0.30 12/15/17 03:12 1,2-Dichloroethane ug/L ND 1.0 0.24 12/15/17 03:12 1,2-Dichloropropane ug/L ND 1.0 0.27 12/15/17 03:12 1,4-Dichlorobenzene ug/L ND 1.0 0.33 12/15/17 03:12 2-Butanone (MEK) ug/L ND 100 0.96 12/15/17 03:12 2-Hexanone ug/L ND 50.0 0.46 12/15/17 03:12 4-Methyl-2-pentanone (MIBK) ug/L ND 100 0.33 12/15/17 03:12 Acetone ug/L ND 100 10.0 12/15/17 03:12 Acrylonitrile ug/L ND 200 1.9 12/15/17 03:12 Benzene ug/L ND 1.0 0.25 12/15/17 03:12 Bromochloromethane ug/L ND 3.0 0.17 12/15/17 03:12 Bromodichloromethane ug/L ND 1.0 0.18 12/15/17 03:12 Bromoform ug/L ND 3.0 0.26 12/15/17 03:12 Bromomethane ug/L ND 10.0 0.29 12/15/17 03:12 Carbon disulfide ug/L ND 100 1.2 12/15/17 03:12 Carbon tetrachloride ug/L ND 1.0 0.25 12/15/17 03:12 Chlorobenzene ug/L ND 3.0 0.23 12/15/17 03:12 Chloroethane ug/L ND 10.0 0.54 12/15/17 03:12 Chloroform ug/L ND 5.0 0.14 12/15/17 03:12 Chloromethane ug/L ND 1.0 0.11 12/15/17 03:12 cis-1,2-Dichloroethene ug/L ND 5.0 0.19 12/15/17 03:12 cis-1,3-Dichloropropene ug/L ND 1.0 0.13 12/15/17 03:12 Dibromochloromethane ug/L ND 3.0 0.21 12/15/17 03:12 Dibromomethane ug/L ND 10.0 0.21 12/15/17 03:12 Ethylbenzene ug/L ND 1.0 0.30 12/15/17 03:12 lodomethane ug/L ND 10.0 0.32 12/15/17 03:12 Methylene Chloride ug/L ND 1.0 0.97 12/15/17 03:12 Styrene ug/L ND 1.0 0.26 12/15/17 03:12 Tetrachloroethene ug/L ND 1.0 0.46 12/15/17 03:12 Toluene ug/L ND 1.0 0.26 12/15/17 03:12 trans-1,2-Dichloroethene ug/L ND 5.0 0.49 12/15/17 03:12 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 24 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry MSWLF SWs Pace Project No.: 92366776 METHOD BLANK: 2169247 Matrix: Water Associated Lab Samples: 92366776001, 92366776002, 92366776003, 92366776004, 92366776005, 92366776006, 92366776007, 92366776008 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers trans- 1,3-Dichloropropene ug/L ND 1.0 0.26 12/15/17 03:12 trans-1,4-Dichloro-2-butene ug/L ND 100 1.0 12/15/17 03:12 Trichloroethene ug/L ND 1.0 0.47 12/15/17 03:12 Trichlorofluoromethane ug/L ND 1.0 0.20 12/15/17 03:12 Vinyl acetate ug/L ND 50.0 0.35 12/15/17 03:12 Vinyl chloride ug/L ND 1.0 0.62 12/15/17 03:12 Xylene (Total) ug/L ND 5.0 0.66 12/15/17 03:12 1,2-Dichloroethane-d4 (S) % 100 70-130 12/15/17 03:12 4-Bromofluorobenzene (S) % 98 70-130 12/15/17 03:12 Toluene-d8 (S) % 105 70-130 12/15/17 03:12 LABORATORY CONTROL SAMPLE: Parameter 2169248 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 47.6 95 80-125 1,1,1-Trichloroethane ug/L 50 47.9 96 71-129 1,1,2,2-Tetrachloroethane ug/L 50 46.8 94 79-124 1,1,2-Trichloroethane ug/L 50 52.7 105 85-125 1,1-Dichloroethane ug/L 50 47.8 96 73-126 1,1-Dichloroethene ug/L 50 47.4 95 66-135 1,2,3-Trichloropropane ug/L 50 50.3 101 75-130 1,2-Dibromo-3-chloropropane ug/L 50 48.6 97 71-133 1,2-Dibromoethane (EDB) ug/L 50 48.6 97 83-124 1,2-Dichlorobenzene ug/L 50 48.2 96 80-133 1,2-Dichloroethane ug/L 50 50.2 100 67-128 1,2-Dichloropropane ug/L 50 50.4 101 75-132 1,4-Dichlorobenzene ug/L 50 47.0 94 78-130 2-Butanone (MEK) ug/L 100 109 109 61-144 2-Hexanone ug/L 100 114 114 68-143 4-Methyl-2-pentanone (MIBK) ug/L 100 109 109 72-135 Acetone ug/L 100 106 106 48-146 Acrylonitrile ug/L 250 252 101 40-160 Benzene ug/L 50 47.8 96 80-125 Bromochloromethane ug/L 50 49.2 98 71-125 Bromodichloromethane ug/L 50 49.0 98 78-124 Bromoform ug/L 50 47.4 95 71-128 Bromomethane ug/L 50 36.0 72 40-160 Carbon disulfide ug/L 50 44.5J 89 50-160 Carbon tetrachloride ug/L 50 48.5 97 69-131 Chlorobenzene ug/L 50 48.0 96 81-122 Chloroethane ug/L 50 52.4 105 39-148 Chloroform ug/L 50 46.4 93 73-127 Chloromethane ug/L 50 44.2 88 44-146 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 25 of 36 Pace Analytical Services, LLC aceAnalXical� 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Surry MSWLF SWs Pace Project No.: 92366776 LABORATORY CONTROL SAMPLE: Parameter 2169248 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers cis-1,2-Dichloroethene ug/L 50 49.5 99 74-124 cis-1,3-Dichloropropene ug/L 50 53.7 107 72-132 Dibromochloromethane ug/L 50 47.5 95 78-125 Dibromomethane ug/L 50 47.4 95 82-120 Ethylbenzene ug/L 50 48.9 98 79-121 lodomethane ug/L 100 83.6 84 39-154 Methylene Chloride ug/L 50 51.0 102 64-133 Styrene ug/L 50 48.6 97 84-126 Tetrachloroethene ug/L 50 46.0 92 78-122 Toluene ug/L 50 49.6 99 80-121 trans-1,2-Dichloroethene ug/L 50 47.7 95 71-127 trans- 1,3-Dichloropropene ug/L 50 53.3 107 69-141 trans-1,4-Dichloro-2-butene ug/L 50 61.1J 122 40-160 Trichloroethene ug/L 50 46.7 93 78-122 Trichlorofluoromethane ug/L 50 42.8 86 53-137 Vinyl acetate ug/L 100 107 107 40-160 Vinyl chloride ug/L 50 48.7 97 58-137 Xylene (Total) ug/L 150 148 99 81-126 1,2-Dichloroethane-d4 (S) % 98 70-130 4-Bromofluorobenzene (S) % 97 70-130 Toluene-d8 (S) % 106 70-130 MATRIX SPIKE SAMPLE: Parameter 2169888 Units 92366776001 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 21.4 107 70-130 1,1,1-Trichloroethane ug/L ND 20 20.8 104 70-130 1,1,2,2-Tetrachloroethane ug/L ND 20 17.9 89 70-130 1,1,2-Trichloroethane ug/L ND 20 21.9 109 70-130 1,1-Dichloroethane ug/L ND 20 20.2 101 70-130 1,1-Dichloroethene ug/L ND 20 16.2 81 70-166 1,2,3-Trichloropropane ug/L ND 20 18.2 91 70-130 1,2-Dibromo-3-chloropropane ug/L ND 20 19.8 99 70-130 1,2-Dibromoethane (EDB) ug/L ND 20 22.0 110 70-130 1,2-Dichlorobenzene ug/L ND 20 21.1 106 70-130 1,2-Dichloroethane ug/L ND 20 19.8 99 70-130 1,2-Dichloropropane ug/L ND 20 19.5 97 70-130 1,4-Dichlorobenzene ug/L ND 20 20.6 103 70-130 2-Butanone (MEK) ug/L ND 40 41.1J 103 70-130 2-Hexanone ug/L ND 40 39AJ 98 70-130 4-Methyl-2-pentanone (MIBK) ug/L ND 40 38.3J 96 70-130 Acetone ug/L ND 40 34.8J 87 70-130 Acrylonitrile ug/L ND 100 93.5J 94 70-130 Benzene ug/L ND 20 22.4 112 70-148 Bromochloromethane ug/L ND 20 19.7 98 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 26 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry MSWLF SWs Pace Project No.: 92366776 MATRIX SPIKE SAMPLE: Parameter 2169888 Units 92366776001 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers Bromodichloromethane ug/L ND 20 19.1 96 70-130 Bromoform ug/L ND 20 21.3 106 70-130 Bromomethane ug/L ND 20 20.2 101 70-130 Carbon disulfide ug/L ND 20 17.2J 86 70-130 Carbon tetrachloride ug/L ND 20 21.4 107 70-130 Chlorobenzene ug/L ND 20 21.3 106 70-146 Chloroethane ug/L ND 20 22.1 111 70-130 Chloroform ug/L ND 20 18.0 90 70-130 Chloromethane ug/L ND 20 17.8 89 70-130 cis-1,2-Dichloroethene ug/L ND 20 19.3 96 70-130 cis-1,3-Dichloropropene ug/L ND 20 25.0 125 70-130 Dibromochloromethane ug/L ND 20 21.8 109 70-130 Dibromomethane ug/L ND 20 21.5 108 70-130 Ethylbenzene ug/L ND 20 20.9 105 70-130 lodomethane ug/L ND 40 43.1 108 70-130 Methylene Chloride ug/L ND 20 14.8 74 70-130 Styrene ug/L ND 20 20.7 103 70-130 Tetrachloroethene ug/L ND 20 23.8 119 70-130 Toluene ug/L ND 20 23.1 116 70-155 trans-1,2-Dichloroethene ug/L ND 20 20.5 103 70-130 trans- 1,3-Dichloropropene ug/L ND 20 21.3 106 70-130 trans-1,4-Dichloro-2-butene ug/L ND 20 19.5J 97 70-130 Trichloroethene ug/L ND 20 22.1 111 69-151 Trichlorofluoromethane ug/L ND 20 19.3 96 70-130 Vinyl acetate ug/L ND 40 40.3J 101 70-130 Vinyl chloride ug/L ND 20 21.0 105 70-130 1,2-Dichloroethane-d4 (S) % 92 70-130 4-Bromofluorobenzene (S) % 92 70-130 Toluene-d8(S) % 110 70-130 SAMPLE DUPLICATE: 2169889 Parameter Units 92366776002 Result Dup Result RPD Max RPD Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND ND 30 1,1,1-Trichloroethane ug/L ND ND 30 1,1,2,2-Tetrachloroethane ug/L ND ND 30 1,1,2-Trichloroethane ug/L ND ND 30 1,1-Dichloroethane ug/L ND ND 30 1,1-Dichloroethene ug/L ND ND 30 1,2,3-Trichloropropane ug/L ND ND 30 1,2-Dibromo-3-chloropropane ug/L ND ND 30 1,2-Dibromoethane (EDB) ug/L ND ND 30 1,2-Dichlorobenzene ug/L ND ND 30 1,2-Dichloroethane ug/L ND ND 30 1,2-Dichloropropene ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 27 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry MSWLF SWs Pace Project No.: 92366776 SAMPLE DUPLICATE: 2169889 Parameter Units 92366776002 Result Dup Result 1,4-Dichlorobenzene ug/L ND ND 2-Butanone (MEK) ug/L ND ND 2-Hexanone ug/L ND ND 4-Methyl-2-pentanone (MIBK) ug/L ND ND Acetone ug/L ND ND Acrylonitrile ug/L ND ND Benzene ug/L ND ND Bromochloromethane ug/L ND ND Bromodichloromethane ug/L ND ND Bromoform ug/L ND ND Bromomethane ug/L ND ND Carbon disulfide ug/L ND ND Carbon tetrachloride ug/L ND ND Chlorobenzene ug/L ND ND Chloroethane ug/L ND ND Chloroform ug/L ND ND Chloromethane ug/L ND ND cis-1,2-Dichloroethene ug/L 0.84J 0.72J cis-1,3-Dichloropropene ug/L ND ND Dibromochloromethane ug/L ND ND Dibromomethane ug/L ND ND Ethylbenzene ug/L ND ND lodomethane ug/L ND ND Methylene Chloride ug/L ND ND Styrene ug/L ND ND Tetrachloroethene ug/L ND ND Toluene ug/L ND ND trans-1,2-Dichloroethene ug/L ND ND trans- 1,3-Dichloropropene ug/L ND ND trans-1,4-Dichloro-2-butene ug/L ND ND Trichloroethene ug/L ND ND Trichlorofluoromethane ug/L ND ND Vinyl acetate ug/L ND ND Vinyl chloride ug/L ND ND Xylene (Total) ug/L ND ND 1,2-Dichloroethane-d4 (S) % 99 82 4-Bromofluorobenzene (S) % 96 93 Toluene-d8(S) % 105 101 Max RPD RPD Qualifiers 19 3 4 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 28 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: Surry MSWLF SWs Pace Project No.: 92366776 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte PASI-M Pace Analytical Services - Minneapolis REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 29 of 36 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Surry MSWLF SWs Pace Project No.: 92366776 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92366776001 SW-1 EPA 3010A 391698 EPA 6010 391786 92366776002 SW-2 EPA 3010A 391698 EPA 6010 391786 92366776003 SW-3 EPA 3010A 391698 EPA 6010 391786 92366776004 SW-4 EPA 3010A 391698 EPA 6010 391786 92366776005 SW -A EPA 3010A 391698 EPA 6010 391786 92366776006 SW-B EPA 3010A 391698 EPA 6010 391786 92366776007 SWN-1 EPA 3010A 391698 EPA 6010 391786 92366776008 SWN-2 EPA 3010A 391698 EPA 6010 391786 92366776001 SW-1 EPA 3020 516784 EPA 6020B 517092 92366776002 SW-2 EPA 3020 516784 EPA 6020B 517092 92366776003 SW-3 EPA 3020 516784 EPA 6020B 517092 92366776004 SW-4 EPA 3020 516784 EPA 6020B 517092 92366776005 SW -A EPA 3020 516784 EPA 6020B 517092 92366776006 SW-B EPA 3020 516784 EPA 6020B 517092 92366776007 SWN-1 EPA 3020 516784 EPA 6020B 517092 92366776008 SWN-2 EPA 3020 516784 EPA 6020B 517092 92366776001 SW-1 EPA 8260 390968 92366776002 SW-2 EPA 8260 390968 92366776003 SW-3 EPA 8260 390968 92366776004 SW-4 EPA 8260 390968 92366776005 SW -A EPA 8260 390968 92366776006 SW-B EPA 8260 390968 92366776007 SWN-1 EPA 8260 390968 92366776008 SWN-2 EPA 8260 390968 Date: 01 /09/2018 11:46 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 30 of 36 Document Name: Document Revised: August 4, 2017 53ce Sample Condition Upon Receipt(SCUR) Page 1 of 2 No.: Issuing Authority: AnapicalDocument f-CAR-[S 033 Rev.04 Pace Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑ Raleigh[] Mechanicsville[] Sample Condition Client: Name: / W V # : 92366776 Upon Project H: I C j+ Cour[:]Fedier: Fed Ex ❑UPup S ❑V5P5 ❑Client ❑ Commercial ❑Pace ❑Other: 92366776 Custody Seal Present? ❑Yes No Seals Intact? es ❑No v ❑❑Y Date/Initials Person Examining Contents: Packing Material: []Bubble Wrap ubble Bags [:]None❑ Other Biological Tissue Frozen? _, Thermometer: —7 t Gvet [IIR Gun ID� : L � Type Ice: � ❑Blue [-]None ❑Yes []No ❑N/A f of Correction Factor: Cooler Temp Corrected (°C): I I I Temp should he above freezing to VC ❑samples out of temp criteria. Samples on ice, cooNng process has begun USDA Regulated Soil (© N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC {check mapsi? r1YPs 17-IN'. Did samples originate from a foreign source (internationally, includine Hawaii and Puerto Ricol? FlYes FNo Comments/Discrepancy: Chain of Custody Present? Yes []No ❑N/A I. Samples Arrived within Hold Time? oyes ❑No ❑N/A 2. Short Hold Time Analysis (<72 hr.)? ❑Yes J:Jfq_o /, ❑N/A 3. Rush Turn Around Time Requested? ❑Yes Z36o ❑N/A 4. Sufficient Volume? ❑V9r.. ❑No ❑N/A 5. Correct Containers Used? -Pace Containers Used? ©Vs —' 21is []No ❑N/A . ❑No ❑N/A 6. Containers Intact? (3res [:)No —QN/A 7. Dissolved analysis: Samples Field Filtered? ❑Yes -[]No ❑N/A 8. Sample Labels Match COC? -Includes Date/Time/ID/Analysis Matrix: 13es []NO ❑N/A 9. Headspace in VOA Vials (.,5-6mm)? ❑Yes DNZ! ❑NIA 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes ❑Yes 0go- ❑N/A ❑No ❑N)A' 11. CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Sample Discrepancy: Lot ID of split containers: Date/Time: Field Data Required? ❑Yes ❑No Project Manager SCURF Review: Date: i2�ls-I Project Manager SRF Review: �C Date: Z jS f Nate: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect cantalners) Page 31 of 36 3 m v 0 v A c .mi 0 m •� ro. i a rL o m C N A A 3 v`, o r O m G� Cn 1 N a M rD fD r0 m a � fl. c m N y o tp D 0 C m o G a � C a A N ,n 0 a N �... o m w ai L. a W N Item7t f1b C zzzzzzzzzzzv BP4U-125 mL Plastic Unpreserved IN/A) (Cl-) rn A n BP3U-2S0 mL Plastic Unpreserved (N/A) o g fl- 3 3 O d i BPZU-500 mL Plastic Unpreserved IN/A) o m C- e 3 a 6P1U-1 liter Plastic Unpreserved (NIA) 8- 'a 2:0 x = BP45-125 mL Plastic H2504 (pH < 2) (Cl-) '" O .. m p Cr — n X to n — BP3N-250 mL plastic HNO3 (pH c 2) rn BP4Z-125 mL Plastic ZN Acetate & NaOH {>9) :3 'R -0 r m z BP4C-125 mL Plastic NaOH IpH > 12) (Cl-), Cr ro fD WGFU-wide-mouthed Glass jar Unpreserved 1 O� O ' AG1U-1 liter Amber Unpreserved (N/A) (Cl-) 00 CL OXV _�„ n► � O � � 1 � AG1H-1 liter Amber HC! (pH c 2) N o 7 0i n AGM -250 mL Amber Unpreserved (N/A) (CI-) AG1S-1 liter Amber H2SO4 (pH < 2) AG3S-250 mL Amber H2504 (pH c 21 AG3A(dG3A)-250MLAmber NH4ClIN/A)(CI-) I �/ N l� j 1 .•,� �j :,� J oG98-40 ML VOA HCI (N/A) V Q VG9T-4p mL VOA Na2S203 {N/A) n es V1591.1-40 mL VOA Unp (N/A) DG9P-40 mL VOA H3PO4 IN/A) r I m. VOAK 16 vials per kit)-5035 kit (N/A) z M V/GK (3vials per kit)-VPH/Gas kit IN/A) . . ra N (D L Sterile Plastic {N/A —lab) l SPST-175 m3 \L m ! C B V SP2T-250 mL Sterile Plastic (N/A — lab) / e A C r+ In BP3A-250 mL Plastic {NH2)2504 (9.3-9.7) m r~ _ \I Cubitainer V J VSGU-20 mL Scintillation vials (N/A) N GN N 00 h+ aceanalyircar CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section S Section C Required Client Information: Required Project Information: Invoice Information: Page: 1 Of 1 Company. Municipal Engineering Services Report To: Jonathan Pfohl Attention Address68 Shipwash Dr. Copy To Company Name: Garner. NC 27529 Address: Re ulato A enc Email jpfohl mesco,cum Purchase Order #: Pace Quote. Phone: f919y772-5393 Fax Project Name: Surry MSWLF SWs Pace Project Manager: lrey.carter pacelabs,ram, State I Location Requested Due Date, Project #: Pace Profile #, 21 D3-3 NC Requested Analysis Filtered YIN MATRIX cone _ — r O COLLECTED $ Preservatives Z Dr,0,n9water ow wrww wT V 3 ~ 0 w-rr:w.kr ww Product P SAMPLE ID S—So„a si a m a Y w N p O O Z 0,1 OL c' START END r n f m m e One Character per box. wm� wp a w rn u {A-Z, 6-9 f, •1 A-, AR o w a m w _ Sample Ids must be unique � oue Ts x J Lu w 4 a q (}u �� a Q U Q m C O _ m Z 2 i rn `m = Q d _ N DATE TIME TIME u = :2 O Z Z 1 SW-1 WT ``DATE f yllr� X X L 2 SW-2 vVT rf x x L 3 SW-3 WT TcGI X X C- 3 4 wiCII a x x $ SW -A WT -fv � \ X X V�a 6 sw-D WT `i : aL 3 x x 7 SWN-1 WT X X � $ SWN-2 WT �5.� L 7— x X 9 S1 WT X X 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY/l AFFILWTION TIME ACCEPTED BY r AFFILIATION DATE TIMEr SAMPLE CONDITIONS 1,ti tv �] n1 i 1 [ f;1 pDATE �. I j'i 'i 7}j 7 z SAMPLER NAME AND SIGNATURE c� PRINT Name of SAMPLER: CL w m Z , `m o ? 2 m ? SIGNATURE of SAMPLER: I DATE Signed: + � m Y'c } Document Name: Document Revised: August 4, 2017 .11 c?CBf�flcilCdr< Sample Condition Upon ReceiptjSCUR) Page 1 of 2 Document No,: Issuing Authority: F-CAR-CS-033-Rev.04 pace Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑j+' RaleRaleigh[](�M`echaanicsville❑ ConditionSample Client Name: W0 ' 92366 fec16 Upon-Receiptc Project #: i ct n I ��� II IIII II II I II II Courier: ❑Fed Ex ❑UPS CUSPS ❑Client ❑ Commercial ❑nce ❑Other: 92366776 Custody Seal Present? [-]Yes E)No Seals Intact? ❑Yes ❑No i,� Z-j3�1� -� Date/Initials Person Examining Contents: Packing Material: [-]Bubble Wrap ��ubble Bags [-]None ❑ other Blologlcal Tissue Frozen? Thermometer. 7 �i ❑Goer ❑ IR Gun ID: �� 1 AI 1 Type Ice: []Yes �]No ❑N/A ©0lue ❑None of / Correction Factor: Cooler Temp Corrected (•C): t t ` I Temp should be above freezing to 6•C ❑5arnples out of temp criteria. Samples on ice, cooling process has begun USDA Regulated Soil ( aN/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or 5C (check maps)? Did samples originate from a foreign source (internationally, 71v— f_N , inrludinc Hawaii and Puerto Rimi7 FlYes MNo Comments/Discrepancy: Chain of Custody Present? ❑Ya []NO N/A 1. Samples Arrived within Hold Time? Yes ❑No ❑N/A 2. Short Hold Time Analysis (02 hr,l? ❑Yes -ONo ,-❑N/A 3. Rush Turn Around Time Requested? ❑Yes .0f�fo N/A 4. Sufficient volume? QVes .- ❑No ❑N/A S. Correct Containers Used? -Pace Containers Used? ©�f/es�, Ayes [:]NO❑N/A []No ❑N/A b. Containers Intact? j3Yes [:]No __DN/A 7. Dissolved analysis: Samples Field Filtered? ❑Yes- -❑No ❑N/A 8. Sample Labels Match COO -Includes Date/Time/ID/Analysis Matrix: .0 es []No []N/A 9. Headspace in VOA Vials (>5.fimm)? ❑Yes ON6-" ❑N/A 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes ❑Yes 1316- ❑N/A [-]NO L_J+rlA 11. CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Sample Discrepancy: Lot ID of split containers: Date/Time: Field Data Required? LIYes CJNo Project Manager SCURF Review: r (C Date: Project Manager SRF Review: —rC Date: 7 rS I Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DMNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers) Page 34 of 36 Document Name: Document Revised: August 4, 2017 �,OceAnaVica!" Sample Condition Upon Receipt(SCUfi) Page 2 of 2 Document No.: Issuing Authority: F-CAR•CS-033-Rev.04 Pace Quality Office *Check mark top half of box if pH and/or dechlorination Project 4 WO# : 92366776 Is verified and within the acceptance range for PM: RWC Due Date: 12/28/17 preservation samples. •LIE'NT: 92-Municipal "Bottom half of box is to list number of bottles n 0 N U 4 = Z N z .n N Q a v w d Z 6 N v v o7J c 2 v w cr a v m m _ 0 s Q m Q 2 vi y 5 a a a a a a a E E E E E a ry > O O a a n ^ a N E E E E E E E w v E v E M E E E E O E E E E " r M N CDO O vi r N r+ G N N N N N yv 7 H .K Ln ry — Ln ry [7 a ❑ q p q O q ❑ Y M ry ✓i C 0 a ,y ry z a 0. 2 a Vm a Nm Vm waear W N l7 mE 0 Na W ma 0 Ma U m W m m a Na G Llnm 7 z t7 >N\ m7 mA m7 m a a o > > > 1 \N z \\Ni, 3 5 5 1 7 c� \N 7 1 S 1 9 10 11 12 N\N pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot a Page 35 of 36 ' -�ceAral�rrcar CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Required Client Informalion: Required Project Information: Invoice Information: Page: 1 Of 1 Company Municipal Engineering Services Report To, ,Sonalhan Piohl Attention: Address: 68 Shipwash Dr, Copy To: Company Name: Gamer, NO 27529 Address: Regulatory Agency Email jptohl mescD corn Purchase Order #: Pace Quote: Phone: (919)772-5393 Irax Project Name: Surry MSWLF SWs Pace Project Manager tray.carter pacelahs,com, State Location Requested Due Data: Project #: Pace Profile #. 21 D3-3 NC Requested Analysis Filtered !N _ a y M TRiX CODE — COLLECTED z Preservatives } !d + Drmk.ng Ww. Dw W.M., WT U P r o W-1. Wm�� ww Product P o y ¢ w J SAMPLE ID S.11r—lid Sr E' START END o w d m ° m oa nL One Character pefr box. w�P� WP w a Z to U 19 o {A-2, U^91 -! OtW OTT } w N ] V Sample Ids must be unique T.—. Ts K JT""T"" — ? w K'V 1, a ° o d c Q ry o z o m N m L m = Q ¢ cc Q L) m ;+ 7 7 7" N DATE TIME w '* = z x z z O z z C. �� V ii 1 SW-1 WT `14,a X X r„ ti U 2 SW-2 WTf�C X X 3 SW-3 WT X X 4 �3 saa�- Uu - I V T Z: C; X X r C.0 5 1 SW -A WT -it' > h X X C.?' 6 SW-e WT `� �( s l a x 7 SWN-1 WT L� ,L"` X X 8 SWN-2 WT :�5� L r X X v L� 9 s WT X x 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BYrAFFiL1AT1ON DATE TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS �' �titi�.� �.� f �5(I. Ia.lta.i{� S ,3 t��.L--/ ;, �� •� �,:� ,,�, -�,�� / 7 SAMPLER NAME AND SIGNATURE c 0 v m PRINT Name of SAMPLER: u z °' o z E R 2 SIGNATURE of SAMPLER: DATE Signed: v lacieAnalXical" www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 January 02, 2018 Mr. Jonathan Pfohl Municipal Engineering Services 68 Shipwash Dr. Garner, NC 27529 RE: Project: Surry Pace Project No.: 92367144 Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory on December 14, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Trey Carter trey. carter@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 12 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Surry Pace Project No.: 92367144 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 12 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: Surry Pace Project No.: 92367144 Lab ID Sample ID Matrix Date Collected Date Received 92367144001 92367144002 OW4-11S OW4-12 Water Water 12/13/1717:15 12/13/1717:30 12/14/1712:40 12/14/1712:40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 12 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: Surry 92367144 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92367144001 OW4-11S EPA 180.1 MDW 1 PASI-A 92367144002 OW4-12 EPA 180.1 MDW 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 12 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Pace Project No.: 92367144 Sample: OW4-11S Lab ID: 92367144001 Collected: 12/13/17 17:15 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 180.1 Turbidity Analytical Method: EPA 180.1 Turbidity 3.2 NTU 1.0 0.50 1 12/15/17 01:39 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /02/2018 09:30 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 12 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Pace Project No.: 92367144 Sample: OW4-12 Lab ID: 92367144002 Collected: 12/13/17 17:30 Received: 12/14/17 12:40 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 180.1 Turbidity Analytical Method: EPA 180.1 Turbidity 1.3 NTU 1.0 0.50 1 12/15/17 01:39 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /02/2018 09:30 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 12 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Pace Project No.: 92367144 QC Batch: 391010 Analysis Method: EPA 180.1 QC Batch Method: EPA 180.1 Analysis Description: 180.1 Turbidity Associated Lab Samples: 92367144001, 92367144002 METHOD BLANK: 2169596 Matrix: Water Associated Lab Samples: 92367144001, 92367144002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Turbidity NTU ND 1.0 0.50 12/15/17 01:39 LABORATORY CONTROL SAMPLE: 2169597 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Turbidity NTU 10 10.1 101 90-110 SAMPLE DUPLICATE: 2169598 92367133005 Dup Max Parameter Units Result Result RPD RPD Qualifiers Turbidity NTU 9.3 9.7 4 10 SAMPLE DUPLICATE: 2169599 92367133004 Dup Max Parameter Units Result Result RPD RPD Qualifiers Turbidity NTU 31.6 36.1 13 10 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /02/2018 09:30 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 12 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: Surry Pace Project No.: 92367144 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /02/2018 09:30 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 12 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Surry Pace Project No.: 92367144 Lab ID Sample ID QC Batch Method QC Batch 92367144001 OW4-11S EPA 180.1 391010 92367144002 OW4-12 EPA 180.1 391010 Date: 01/02/2018 09:30 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Method Analytical Batch Page 9 of 12 USDA Regulated 5o N/A, water sample]) Did sample o4i inate i�a quarantine zone within the United States: CA, NY, or SC (check maps)? I—'I�__ It3:._ Document Name: Document Revised: August 4, 2017 Sample Condition Upon Recelpt(SCUR) Page 1 of 2 c7CEAfTr3jlCclj Document No.: Issuing Authority: F-CAR-CS-033•Rev.04 Pace Quality Office Laboratory receiving samples: Asheville ❑ Etfen❑ Greenwood ❑ Huntersvillt% Raleigh[] Mechanicsville❑ Sample Condition Client Name:uponReceipt WO# : 92367144 c Project q: jj Courier: Fed Ex ❑LIPS 111 L❑IUSPS ❑ Commercial ❑Client `''��""Ce ❑Other: 92367144 Custody Seat Present? ❑Yes 1--biNo Seals Intact? ❑Yes 11-fiN0 Date/Initials Person Examining s: 1 ` Packing Material; ❑Bubble Wrap []Bubble Bags of Ice: one ❑ Other Blologl Tissue Frozen? Thermometer: ❑Yeso ❑N/A t' R Gun tD: �et []Blue ❑None pe Correction actor: Cooler Temp Corrected VC); Temp should be above freezing to VC ❑Samples out of temp criteria. Samples on ice, cooling process has begun DA samples originate from a foreign source (internationally, including Hawaii and Puerto Rico)? [-]Yes Comments/Disereo a n rv- Chain of Custody Present? es []NO ❑N/A 1. Samples Arrived within Hold lime? Y s ❑No ❑N/A 2 �$�hort Hold Time Analysis (c72 hr.)? Y s ❑N/A 3. Turn Around Time Requested? []yes ❑N/A 4 Sufficient Volume? es ❑No ❑N/A 5. Correct Containers Used? -Pace Containers es ONO ❑N/A 6, N� I Used? Cyr s ONO ❑ N/A Uti Containers Intact? es EINa ❑N/A 7, l7issolved analysis: Samples Field Filtered? Elyes ❑No /A S. Sample Labels Match COC? ❑Yes Po ❑N/A g. -Includes Date/Time/ID/Analysis Matrix: Headspace in VOA Vials i>5.6mm)? El Yes ❑Na /A 10. Trip Blank Present? ❑Ves ❑N/A 11. Trip Blank Custody Seals Present? ❑Yes [:]No N/A [LIENTNpTIFICA710N/RESOLUTION Field Data Required? [--]Yes ONO Person Contacted: Comments/Sample Discrepancy: Lot ID of split containers: Date/Time: Project Manager SCURF Review: rL Date: �Z Project Manager 5RF Review: [C Date: 17 6� 17 Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form wilt be sent to the North Carolina DEHNR Certification office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers) Page 10 of 12 N CO (D 9 m 3 v 0 m w K ro T C 0 m �a Q 0 w n a A ro m f- rr a r o a � 0 m � CL M N 4C 3 to m 0 C. C- H ty m ro CL as 4 M A 3 c m y Q A � n m c d a a CO v Cn w - N F+ Item# z z z Zz z i f` . BP4U-125 mL Plastic Unpreserved (N/A) (Cl-) f BP3U-250 mi Plastic Unpreserved (N/A) BP2U-5OO mL Plastic Unpreserved (N/A) SPIU-1 liter Plastic Unpreserved (N/A) BP4S-125 mL Plastic H2SO4 (pH < 2) (Cl-) BP3N-250 mL plastic HNO3 (pH < 2) 8P4Z-125 mL Plastic ZN Acetate & NaOH (>9) 8P4C-125 mL Plastic NaOH (pH > 12) ICI-) WGFU-Wide-mouthed Glass jar Unpreserved AG1U-1 liter Amber Unpreserved (N/A) (Cl-) AGIH-1 liter Amber HCI (pH < 2) AG3U-250 mL Amber Unpreserved (N/A) (Cl-) AGIS- 1 liter AmberH25O4 IPH < 2) AG3S-250 m1 Amber H2SO4 (pH < 2) AG3A(OG3A)-250 mLAmber NH4CI (N/A) (Cl-) �. ❑G9H-00 ML VOA HCI (N/A) VG9T-40 mL VOA Na2S203 (NIA) VG91.1-40 mL VOA Unp (N/A) OG9P-40 mL VOA H3PO4 (N/A) VOAK (b vials per kit)-5035 kit (N/A) V/GK (3 vials per kit)-VPH/Gas kit (N/A) SPST-325 mL Sterile Plastic (N/A — labI SPZT-250 mL Sterile Plastic (N/A — lab) BP3A-250 mL Plastic INH2)2504 (9.3-9.7) CUbitalner VSGU-20 mL Scintillation vials (N/A) GN L 03 m C S .O�* C < =! 7c °: CL 3 C d N 7 7 ,Z- N CL r! O m o N X (A 7 y� S O a- � O X 7 im 3 is al rn 7 CL m 0 3 O Cr C. m M p n 7 m O 7 3 is f t'9 U C ro O lu r ro N L� r+ J 0 m io r' 0 A 4 Q O 0 n � c C) C m C)3 (� C � W 3 � 7U Z � 6f m ro In n .. A t0- 1AI2114ica! Section A Required Client Information: Company. Municipal Engineering Services Address, 304 E Main Street Elkin, NC 28621 Email, Phone IFax Requested Due Date ik to F- SAMPLE ID One Character per box. JA-2, 0-9 1. -) Sample Ids must be unique 4 MW-14 6 M1N_a a 7 Mw-1 8 10 ]12 Section B Required Project Information: Report To: Pfohl, Jonathan Copy To - Purchase Order #: Project Name: Surry Project #: N CHAIN -OF -CUSTODY / Analytical Request Document N The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. a) Section C Invoice Information: Page: 1 Of 1 Allention: Comnanv Name. le t: a Yi z rnaraix CODE ° COLLECTEC z Preservatives } D, k..9 Welnl OW V O Wote1 WT Walla W31 C+ WW Q lull Potlud p � J Sodlsorid Oil OIL � START END q Wipe WIP Air AR Omer OT o U F $ < a M N }s m T-sue Ts TDATETIME 00 Q N DATE TIME S z== z z 2 O �� WT �i i s �; f i x x k x x x x VVT x x V%T wT x t- ADDITIONAL. COMMENTS RELINQUISHED BY !AFFILIATION DATE TIME - 1�4) a. 1 F ACCEPTED BYl AFFILIATION State 1 Lc NC DATE TIME SAMPLE CONDITIONS l y�L, �• G PLER NAME AND SIGNATURE PRINT Name of SAMPLER- 0 t f 'i• SIGNATURE of SAMPLER: DATE Signed: j z "—' o z_ E u z iTl�;i17 au} 'NL) Inc} lacieAnalXical" www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 January 09, 2018 Mr. Jonathan Pfohl Municipal Engineering Services 68 Shipwash Dr. Garner, NC 27529 RE: Project: SURRY BLANKS Pace Project No.: 92367285 Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory on December 15, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Trey Carter trey. carter@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 CERTIFICATIONS Project: SURRY BLANKS Pace Project No.: 92367285 Minnesota Certification IDs 1700 Elm Street SE, Suite 200, Minneapolis, MN 55414- Michigan Certification #: 9909 2485 Minnesota Certification #: 027-053-137 A21-A Certification #: 2926.01 Mississippi Certification #: MN00064 Alabama Certification #: 40770 Montana Certification #: CERT0092 Alaska Contaminated Sites Certification #: 17-009 Nebraska Certification #: NE-OS-18-06 Alaska DW Certification M MN00064 Nevada Certification #: MN00064 Arizona Certification #: AZ0014 New Hampshire Certification #: 2081 Arkansas Certification #: 88-0680 New Jersey Certification M MN002 California Certification #: 2929 New York Certification #: 11647 CNMI Saipan Certification #:MP0003 North Carolina DW Certification #: 27700 Colorado Certification #: MN00064 North Carolina WW Certification #: 530 Connecticut Certification #: PH-0256 North Dakota Certification M R-036 EPA Region 8+Wyoming DW Certification #: via MN 027- Ohio DW Certification #: 41244 053-137 Ohio VAP Certification #: CL101 Florida Certification #: E87605 Oklahoma Certification #: 9507 Georgia Certification #: 959 Oregon NwTPH Certification #: MN300001 Guam EPA Certification #: MN00064 N0 Oregon Secondary Certification #: MN200001 Hawaii Certification #: MN0 Pennsylvania Certification #: 68-00563 : Idaho Certification #: MN00064 Puerto Rico Certification #: MN00064 Illinois Certification 20000 00011C-MN South Carolina Certification #:74003001 M 1 Indiana Certification #: Tennessee Certification #: TN02818 Iowa Certification #: Texas Certification #: T104704192 Kansas Certification #: E-10167 Utah Certification #: MN00 Kentucky DW Certification M 90062 Virginia Certification #: 163 Kentucky WW Certification M 90062 C64 Washington Certificationn ##: : 486 Louisiana DEQ Certification #: 03086 West Virginia DW Certification #: 9952 C Louisiana DW Certification #: MN00064 West Virginia DEP Certification #: 382 Maine Certification #: MN00064 Wisconsin Certification #: 999407970 Maryland Certification M 322 Massachusetts Certification #: M-MN064 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification M E87648 South Carolina Certification M 99030001 Massachusetts Certification #: M-NC030 Virginia/VELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: SURRY BLANKS Pace Project No.: 92367285 Lab ID Sample ID Matrix Date Collected Date Received 92367285001 92367285002 EB FB Water Water 12/14/1716:00 12/14/1716:05 12/15/1714:25 12/15/1714:25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: SURRY BLANKS 92367285 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92367285001 EB EPA6010 DS, SH1 15 PASI-A EPA 6020E TT3 1 PASI-M EPA 7470 SER 1 PASI-A EPA 8260 GAW 67 PASI-C 92367285002 FB EPA 8260 GAW 67 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY BLANKS Pace Project No.: 92367285 Sample: EB Lab ID: 92367285001 Collected: 12/14/17 16:00 Received: 12/15/17 14:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Tin Vanadium Zinc 6020B MET ICPMS Thallium 7470 Mercury Mercury 8260 MSV Low Level Landfill Acetone Acetonitrile Acrolein Acrylonitrile Allyl chloride Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane Chloroprene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene Date: 01/09/2018 05:59 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010A ND ug/L 6.0 3.9 1 12/20/17 05:50 12/27/17 23:06 7440-36-0 ND ug/L 10.0 5.0 1 12/20/17 05:50 12/27/17 23:06 7440-38-2 ND ug/L 100 2.5 1 12/20/17 05:50 12/27/17 23:06 7440-39-3 ND ug/L 1.0 0.50 1 12/20/17 05:50 12/27/17 23:06 7440-41-7 ND ug/L 1.0 0.50 1 12/20/17 05:50 12/27/17 23:06 7440-43-9 ND ug/L 10.0 2.5 1 12/20/17 05:50 12/27/17 23:06 7440-47-3 ND ug/L 10.0 2.5 1 12/20/17 05:50 12/27/17 23:06 7440-48-4 ND ug/L 10.0 2.5 1 12/20/17 05:50 12/27/17 23:06 7440-50-8 ND ug/L 10.0 2.5 1 12/20/17 05:50 12/27/17 23:06 7439-92-1 ND ug/L 50.0 2.5 1 12/20/17 05:50 12/27/17 23:06 7440-02-0 ND ug/L 10.0 5.0 1 12/20/17 05:50 12/28/17 22:36 7782-49-2 ND ug/L 10.0 2.5 1 12/20/17 05:50 12/27/17 23:06 7440-22-4 ND ug/L 100 2.5 1 12/20/17 05:50 12/27/17 23:06 7440-31-5 ND ug/L 25.0 2.5 1 12/20/17 05:50 12/27/17 23:06 7440-62-2 ND ug/L 10.0 5.0 1 12/20/17 05:50 12/27/17 23:06 7440-66-6 Analytical Method: EPA 6020E Preparation Method: EPA 3020 ND ug/L 0.10 0.028 1 01/08/18 09:09 01/08/18 15:09 7440-28-0 Analytical Method: EPA 7470 Preparation Method: EPA 7470 ND ug/L 0.20 0.10 1 12/26/17 16:20 12/27/17 04:31 7439-97-6 Analytical Method: EPA 8260 ND ug/L 100 10.0 1 12/20/17 03:27 67-64-1 ND ug/L 55.0 2.2 1 12/20/17 03:27 75-05-8 ND ug/L 53.0 1.6 1 12/20/17 03:27 107-02-8 ND ug/L 200 1.9 1 12/20/17 03:27 107-13-1 ND ug/L 10.0 1.5 1 12/20/17 03:27 107-05-1 ND ug/L 1.0 0.25 1 12/20/17 03:27 71-43-2 ND ug/L 3.0 0.17 1 12/20/17 03:27 74-97-5 ND ug/L 1.0 0.18 1 12/20/17 03:27 75-27-4 ND ug/L 3.0 0.26 1 12/20/17 03:27 75-25-2 ND ug/L 10.0 0.29 1 12/20/17 03:27 74-83-9 ND ug/L 100 0.96 1 12/20/17 03:27 78-93-3 ND ug/L 100 1.2 1 12/20/17 03:27 75-15-0 ND ug/L 1.0 0.25 1 12/20/17 03:27 56-23-5 ND ug/L 3.0 0.23 1 12/20/17 03:27 108-90-7 ND ug/L 10.0 0.54 1 12/20/17 03:27 75-00-3 ND ug/L 5.0 0.14 1 12/20/17 03:27 67-66-3 ND ug/L 1.0 0.11 1 12/20/17 03:27 74-87-3 ND ug/L 20.0 0.27 1 12/20/17 03:27 126-99-8 ND ug/L 13.0 2.0 1 12/20/17 03:27 96-12-8 ND ug/L 3.0 0.21 1 12/20/17 03:27 124-48-1 ND ug/L 1.0 0.27 1 12/20/17 03:27 106-93-4 ND ug/L 10.0 0.21 1 12/20/17 03:27 74-95-3 ND ug/L 5.0 0.30 1 12/20/17 03:27 95-50-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY BLANKS Pace Project No.: 92367285 Sample: EB Lab ID: 92367285001 Collected: 12/14/17 16:00 Received: 12/15/17 14:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 1,3-Dichlorobenzene ND ug/L 5.0 0.24 1 12/20/17 03:27 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 12/20/17 03:27 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 12/20/17 03:27 110-57-6 Dichlorodifluoromethane ND ug/L 5.0 0.21 1 12/20/17 03:27 75-71-8 1,1-Dichloroethane ND ug/L 5.0 0.32 1 12/20/17 03:27 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 12/20/17 03:27 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 12/20/17 03:27 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 12/20/17 03:27 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 12/20/17 03:27 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 12/20/17 03:27 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 12/20/17 03:27 142-28-9 2,2-Dichloropropane ND ug/L 15.0 0.13 1 12/20/17 03:27 594-20-7 1,1-Dichloropropene ND ug/L 5.0 0.49 1 12/20/17 03:27 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 12/20/17 03:27 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 12/20/17 03:27 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 12/20/17 03:27 100-41-4 Ethyl methacrylate ND ug/L 10.0 0.20 1 12/20/17 03:27 97-63-2 Hexachloro-1,3-butadiene ND ug/L 10.0 0.71 1 12/20/17 03:27 87-68-3 2-Hexanone ND ug/L 50.0 0.46 1 12/20/17 03:27 591-78-6 lodomethane ND ug/L 10.0 0.32 1 12/20/17 03:27 74-88-4 Isobutanol ND ug/L 100 35.0 1 12/20/17 03:27 78-83-1 Methacrylonitrile ND ug/L 100 0.93 1 12/20/17 03:27 126-98-7 Methylene Chloride ND ug/L 1.0 0.97 1 12/20/17 03:27 75-09-2 Methyl methacrylate ND ug/L 30.0 2.0 1 12/20/17 03:27 80-62-6 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 12/20/17 03:27 108-10-1 Naphthalene ND ug/L 10.0 0.24 1 12/20/17 03:27 91-20-3 Propionitrile ND ug/L 150 3.6 1 12/20/17 03:27 107-12-0 Styrene ND ug/L 1.0 0.26 1 12/20/17 03:27 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 12/20/17 03:27 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 12/20/17 03:27 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 12/20/17 03:27 127-18-4 Toluene ND ug/L 1.0 0.26 1 12/20/17 03:27 108-88-3 1,2,4-Trichlorobenzene ND ug/L 10.0 0.35 1 12/20/17 03:27 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 12/20/17 03:27 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 12/20/17 03:27 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 12/20/17 03:27 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 12/20/17 03:27 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 12/20/17 03:27 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 12/20/17 03:27 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 12/20/17 03:27 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 12/20/17 03:27 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 12/20/17 03:27 460-00-4 1,2-Dichloroethane-d4 (S) 95 % 70-130 1 12/20/17 03:27 17060-07-0 Toluene-d8 (S) 127 % 70-130 1 12/20/17 03:27 2037-26-5 Date: 01/09/2018 05:59 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY BLANKS Pace Project No.: 92367285 Sample: FB Lab ID: 92367285002 Collected: 12/14/17 16:05 Received: 12/15/17 14:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Acetone ND ug/L 100 10.0 1 12/20/17 03:44 67-64-1 Acetonitrile ND ug/L 55.0 2.2 1 12/20/17 03:44 75-05-8 Acrolein ND ug/L 53.0 1.6 1 12/20/17 03:44 107-02-8 Acrylonitrile ND ug/L 200 1.9 1 12/20/17 03:44 107-13-1 Allyl chloride ND ug/L 10.0 1.5 1 12/20/17 03:44 107-05-1 Benzene ND ug/L 1.0 0.25 1 12/20/17 03:44 71-43-2 Bromochloromethane ND ug/L 3.0 0.17 1 12/20/17 03:44 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 12/20/17 03:44 75-27-4 Bromoform ND ug/L 3.0 0.26 1 12/20/17 03:44 75-25-2 Bromomethane ND ug/L 10.0 0.29 1 12/20/17 03:44 74-83-9 2-Butanone (MEK) ND ug/L 100 0.96 1 12/20/17 03:44 78-93-3 Carbon disulfide ND ug/L 100 1.2 1 12/20/17 03:44 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 12/20/17 03:44 56-23-5 Chlorobenzene ND ug/L 3.0 0.23 1 12/20/17 03:44 108-90-7 Chloroethane ND ug/L 10.0 0.54 1 12/20/17 03:44 75-00-3 Chloroform ND ug/L 5.0 0.14 1 12/20/17 03:44 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 12/20/17 03:44 74-87-3 Chloroprene ND ug/L 20.0 0.27 1 12/20/17 03:44 126-99-8 1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.0 1 12/20/17 03:44 96-12-8 Dibromochloromethane ND ug/L 3.0 0.21 1 12/20/17 03:44 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 12/20/17 03:44 106-93-4 Dibromomethane ND ug/L 10.0 0.21 1 12/20/17 03:44 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 12/20/17 03:44 95-50-1 1,3-Dichlorobenzene ND ug/L 5.0 0.24 1 12/20/17 03:44 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 12/20/17 03:44 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 12/20/17 03:44 110-57-6 Dichlorodifluoromethane ND ug/L 5.0 0.21 1 12/20/17 03:44 75-71-8 1,1-Dichloroethane ND ug/L 5.0 0.32 1 12/20/17 03:44 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.24 1 12/20/17 03:44 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.56 1 12/20/17 03:44 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 0.19 1 12/20/17 03:44 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 0.49 1 12/20/17 03:44 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 12/20/17 03:44 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 12/20/17 03:44 142-28-9 2,2-Dichloropropane ND ug/L 15.0 0.13 1 12/20/17 03:44 594-20-7 1,1-Dichloropropene ND ug/L 5.0 0.49 1 12/20/17 03:44 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 12/20/17 03:44 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 12/20/17 03:44 10061-02-6 Ethylbenzene ND ug/L 1.0 0.30 1 12/20/17 03:44 100-41-4 Ethyl methacrylate ND ug/L 10.0 0.20 1 12/20/17 03:44 97-63-2 Hexachloro-1,3-butadiene ND ug/L 10.0 0.71 1 12/20/17 03:44 87-68-3 2-Hexanone ND ug/L 50.0 0.46 1 12/20/17 03:44 591-78-6 lodomethane ND ug/L 10.0 0.32 1 12/20/17 03:44 74-88-4 Isobutanol ND ug/L 100 35.0 1 12/20/17 03:44 78-83-1 Methacrylonitrile ND ug/L 100 0.93 1 12/20/17 03:44 126-98-7 Methylene Chloride ND ug/L 1.0 0.97 1 12/20/17 03:44 75-09-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SURRY BLANKS Pace Project No.: 92367285 Sample: FB Lab ID: 92367285002 Collected: 12/14/17 16:05 Received: 12/15/17 14:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260 Methyl methacrylate ND ug/L 30.0 2.0 1 12/20/17 03:44 80-62-6 4-Methyl-2-pentanone (MIBK) ND ug/L 100 0.33 1 12/20/17 03:44 108-10-1 Naphthalene ND ug/L 10.0 0.24 1 12/20/17 03:44 91-20-3 Propionitrile ND ug/L 150 3.6 1 12/20/17 03:44 107-12-0 Styrene ND ug/L 1.0 0.26 1 12/20/17 03:44 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.33 1 12/20/17 03:44 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 3.0 0.40 1 12/20/17 03:44 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 12/20/17 03:44 127-18-4 Toluene ND ug/L 1.0 0.26 1 12/20/17 03:44 108-88-3 1,2,4-Trichlorobenzene ND ug/L 10.0 0.35 1 12/20/17 03:44 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 12/20/17 03:44 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 12/20/17 03:44 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 12/20/17 03:44 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 12/20/17 03:44 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 12/20/17 03:44 96-18-4 Vinyl acetate ND ug/L 50.0 0.35 1 12/20/17 03:44 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 12/20/17 03:44 75-01-4 Xylene (Total) ND ug/L 5.0 0.66 1 12/20/17 03:44 1330-20-7 Surrogates 4-Bromofluorobenzene (S) 92 % 70-130 1 12/20/17 03:44 460-00-4 1,2-Dichloroethane-d4 (S) 94 % 70-130 1 12/20/17 03:44 17060-07-0 Toluene-d8 (S) 108 % 70-130 1 12/20/17 03:44 2037-26-5 Date: 01/09/2018 05:59 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BLANKS Pace Project No.: 92367285 QC Batch: 391836 Analysis Method: EPA 7470 QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury Associated Lab Samples: 92367285001 METHOD BLANK: 2173800 Matrix: Water Associated Lab Samples: 92367285001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Mercury ug/L ND 0.20 0.10 12/27/17 04:27 LABORATORY CONTROL SAMPLE: 2173801 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.7 106 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2173802 2173803 MS MSD 92367285001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Mercury ug/L ND 2.5 2.5 2.5 2.8 100 110 75-125 10 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BLANKS Pace Project No.: 92367285 QC Batch: 391699 Analysis Method: EPA 6010 QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92367285001 METHOD BLANK: 2173090 Associated Lab Samples: 92367285001 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Qualifiers Antimony ug/L ND 5.0 3.9 12/27/17 21:44 Arsenic ug/L ND 10.0 5.0 12/27/17 21:44 Barium ug/L ND 5.0 2.5 12/27/17 21:44 Beryllium ug/L ND 1.0 0.50 12/27/17 21:44 Cadmium ug/L ND 1.0 0.50 12/27/17 21:44 Chromium ug/L ND 5.0 2.5 12/27/17 21:44 Cobalt ug/L ND 5.0 2.5 12/27/17 21:44 Copper ug/L ND 5.0 2.5 12/27/17 21:44 Lead ug/L ND 5.0 2.5 12/27/17 21:44 Nickel ug/L ND 5.0 2.5 12/27/17 21:44 Selenium ug/L ND 10.0 5.0 12/28/17 21:14 Silver ug/L ND 5.0 2.5 12/27/17 21:44 Tin ug/L ND 5.0 2.5 12/27/17 21:44 Vanadium ug/L ND 5.0 2.5 12/27/17 21:44 Zinc ug/L ND 10.0 5.0 12/28/17 21:14 LABORATORY CONTROL SAMPLE: 2173091 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Antimony ug/L 500 485 97 80-120 Arsenic ug/L 500 468 94 80-120 Barium ug/L 500 481 96 80-120 Beryllium ug/L 500 494 99 80-120 Cadmium ug/L 500 444 89 80-120 Chromium ug/L 500 458 92 80-120 Cobalt ug/L 500 472 94 80-120 Copper ug/L 500 513 103 80-120 Lead ug/L 500 463 93 80-120 Nickel ug/L 500 458 92 80-120 Selenium ug/L 500 410 82 80-120 Silver ug/L 250 240 96 80-120 Tin ug/L 500 476 95 80-120 Vanadium ug/L 500 487 97 80-120 Zinc ug/L 500 441 88 80-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: SURRY BLANKS 92367285 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2173092 2173093 MS MSD 92366848001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 512 524 102 105 75-125 2 20 Arsenic ug/L ND 500 500 498 508 100 102 75-125 2 20 Barium ug/L 28AJ 500 500 526 536 100 102 75-125 2 20 Beryllium ug/L ND 500 500 514 528 103 106 75-125 3 20 Cadmium ug/L 1.2 500 500 472 481 94 96 75-125 2 20 Chromium ug/L ND 500 500 478 490 96 98 75-125 2 20 Cobalt ug/L ND 500 500 489 498 98 100 75-125 2 20 Copper ug/L ND 500 500 527 539 105 107 75-125 2 20 Lead ug/L ND 500 500 480 490 96 98 75-125 2 20 Nickel ug/L ND 500 500 479 488 96 97 75-125 2 20 Selenium ug/L ND 500 500 441 455 88 91 75-125 3 20 Silver ug/L ND 250 250 254 260 101 104 75-125 2 20 Tin ug/L ND 500 500 501 511 100 102 75-125 2 20 Vanadium ug/L ND 500 500 508 521 101 104 75-125 3 20 Zinc ug/L ND 500 500 469 478 93 95 75-125 2 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BLANKS Pace Project No.: 92367285 QC Batch: 517023 Analysis Method: EPA 6020B QC Batch Method: EPA 3020 Analysis Description: 6020E Water UPD5 Associated Lab Samples: 92367285001 METHOD BLANK: 2809372 Matrix: Water Associated Lab Samples: 92367285001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Thallium ug/L ND 0.10 0.028 01/08/1814:52 LABORATORY CONTROL SAMPLE: 2809373 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Thallium ug/L 100 104 104 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2809374 2809375 MS MSD 92367285001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Thallium ug/L ND 100 100 100 94.3 100 94 75-125 6 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BLANKS Pace Project No.: 92367285 QC Batch: 391641 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92367285001, 92367285002 METHOD BLANK: 2172868 Associated Lab Samples: 92367285001, 92367285002 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 0.33 12/19/17 17:51 1,1,1-Trichloroethane ug/L ND 1.0 0.48 12/19/17 17:51 1,1,2,2-Tetrachloroethane ug/L ND 3.0 0.40 12/19/17 17:51 1,1,2-Trichloroethane ug/L ND 1.0 0.29 12/19/17 17:51 1,1-Dichloroethane ug/L ND 5.0 0.32 12/19/17 17:51 1,1-Dichloroethene ug/L ND 5.0 0.56 12/19/17 17:51 1,1-Dichloropropene ug/L ND 5.0 0.49 12/19/17 17:51 1,2,3-Trichloropropane ug/L ND 1.0 0.41 12/19/17 17:51 1,2,4-Trichlorobenzene ug/L ND 10.0 0.35 12/19/17 17:51 1,2-Dibromo-3-chloropropane ug/L ND 13.0 2.0 12/19/17 17:51 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 12/19/17 17:51 1,2-Dichlorobenzene ug/L ND 5.0 0.30 12/19/17 17:51 1,2-Dichloroethane ug/L ND 1.0 0.24 12/19/17 17:51 1,2-Dichloropropane ug/L ND 1.0 0.27 12/19/17 17:51 1,3-Dichlorobenzene ug/L ND 5.0 0.24 12/19/17 17:51 1,3-Dichloropropane ug/L ND 1.0 0.28 12/19/17 17:51 1,4-Dichlorobenzene ug/L ND 1.0 0.33 12/19/17 17:51 2,2-Dichloropropane ug/L ND 15.0 0.13 12/19/17 17:51 2-Butanone (MEK) ug/L ND 100 0.96 12/19/17 17:51 2-Hexanone ug/L ND 50.0 0.46 12/19/17 17:51 4-Methyl-2-pentanone (MIBK) ug/L ND 100 0.33 12/19/17 17:51 Acetone ug/L ND 100 10.0 12/19/17 17:51 Acetonitrile ug/L ND 55.0 2.2 12/19/17 17:51 Acrolein ug/L ND 53.0 1.6 12/19/17 17:51 Acrylonitrile ug/L ND 200 1.9 12/19/17 17:51 Allyl chloride ug/L ND 10.0 1.5 12/19/17 17:51 Benzene ug/L ND 1.0 0.25 12/19/17 17:51 Bromochloromethane ug/L ND 3.0 0.17 12/19/17 17:51 Bromodichloromethane ug/L ND 1.0 0.18 12/19/17 17:51 Bromoform ug/L ND 3.0 0.26 12/19/17 17:51 Bromomethane ug/L ND 10.0 0.29 12/19/17 17:51 Carbon disulfide ug/L ND 100 1.2 12/19/17 17:51 Carbon tetrachloride ug/L ND 1.0 0.25 12/19/17 17:51 Chlorobenzene ug/L ND 3.0 0.23 12/19/17 17:51 Chloroethane ug/L ND 10.0 0.54 12/19/17 17:51 Chloroform ug/L ND 5.0 0.14 12/19/17 17:51 Chloromethane ug/L ND 1.0 0.11 12/19/17 17:51 Chloroprene ug/L ND 20.0 0.27 12/19/17 17:51 cis-1,2-Dichloroethene ug/L ND 5.0 0.19 12/19/17 17:51 cis-1,3-Dichloropropene ug/L ND 1.0 0.13 12/19/17 17:51 Dibromochloromethane ug/L ND 3.0 0.21 12/19/17 17:51 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BLANKS Pace Project No.: 92367285 METHOD BLANK: 2172868 Associated Lab Samples: 92367285001, 92367285002 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Dibromomethane ug/L ND 10.0 0.21 12/19/17 17:51 Dichlorodifluoromethane ug/L ND 5.0 0.21 12/19/17 17:51 Ethyl methacrylate ug/L ND 10.0 0.20 12/19/17 17:51 Ethylbenzene ug/L ND 1.0 0.30 12/19/17 17:51 Hexachloro-1,3-butadiene ug/L ND 10.0 0.71 12/19/17 17:51 lodomethane ug/L ND 10.0 0.32 12/19/17 17:51 Isobutanol ug/L ND 100 35.0 12/19/17 17:51 Methacrylonitrile ug/L ND 100 0.93 12/19/17 17:51 Methyl methacrylate ug/L ND 30.0 2.0 12/19/17 17:51 Methylene Chloride ug/L ND 1.0 0.97 12/19/17 17:51 Naphthalene ug/L ND 10.0 0.24 12/19/17 17:51 Propionitrile ug/L ND 150 3.6 12/19/17 17:51 Styrene ug/L ND 1.0 0.26 12/19/17 17:51 Tetrachloroethene ug/L ND 1.0 0.46 12/19/17 17:51 Toluene ug/L ND 1.0 0.26 12/19/17 17:51 trans-1,2-Dichloroethene ug/L ND 5.0 0.49 12/19/17 17:51 trans- 1,3-Dichloropropene ug/L ND 1.0 0.26 12/19/17 17:51 trans-1,4-Dichloro-2-butene ug/L ND 100 1.0 12/19/17 17:51 Trichloroethene ug/L ND 1.0 0.47 12/19/17 17:51 Trichlorofluoromethane ug/L 0.20J 1.0 0.20 12/19/17 17:51 Vinyl acetate ug/L ND 50.0 0.35 12/19/17 17:51 Vinyl chloride ug/L ND 1.0 0.62 12/19/17 17:51 Xylene (Total) ug/L ND 5.0 0.66 12/19/17 17:51 1,2-Dichloroethane-d4 (S) % 91 70-130 12/19/17 17:51 4-Bromofluorobenzene (S) % 105 70-130 12/19/17 17:51 Toluene-d8 (S) % 105 70-130 12/19/17 17:51 LABORATORY CONTROL SAMPLE: Parameter 2172869 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 49.2 98 80-125 1,1,1-Trichloroethane ug/L 50 47.0 94 71-129 1,1,2,2-Tetrachloroethane ug/L 50 47.0 94 79-124 1,1,2-Trichloroethane ug/L 50 50.3 101 85-125 1,1-Dichloroethane ug/L 50 44.3 89 73-126 1,1-Dichloroethene ug/L 50 52.5 105 66-135 1,1-Dichloropropene ug/L 50 47.3 95 74-135 1,2,3-Trichloropropane ug/L 50 47.2 94 75-130 1,2,4-Trichlorobenzene ug/L 50 50.8 102 75-134 1,2-Dibromo-3-chloropropane ug/L 50 48.9 98 71-133 1,2-Dibromoethane (EDB) ug/L 50 52.8 106 83-124 1,2-Dichlorobenzene ug/L 50 46.1 92 80-133 1,2-Dichloroethane ug/L 50 45.4 91 67-128 1,2-Dichloropropane ug/L 50 47.3 95 75-132 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BLANKS Pace Project No.: 92367285 LABORATORY CONTROL SAMPLE: Parameter 2172869 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,3-Dichlorobenzene ug/L 50 47.9 96 77-130 1,3-Dichloropropane ug/L 50 51.8 104 76-131 1,4-Dichlorobenzene ug/L 50 49.8 100 78-130 2,2-Dichloropropane ug/L 50 45.9 92 40-160 2-Butanone (MEK) ug/L 100 98.9J 99 61-144 2-Hexanone ug/L 100 92.3 92 68-143 4-Methyl-2-pentanone (MIBK) ug/L 100 86.8J 87 72-135 Acetone ug/L 100 85.1J 85 48-146 Acetonitrile ug/L 500 433 87 62-150 Acrolein ug/L 250 282 113 24-160 Acrylonitrile ug/L 250 220 88 40-160 Allyl chloride ug/L 50 44.9 90 66-137 Benzene ug/L 50 45.6 91 80-125 Bromochloromethane ug/L 50 46.7 93 71-125 Bromodichloromethane ug/L 50 46.3 93 78-124 Bromoform ug/L 50 49.1 98 71-128 Bromomethane ug/L 50 41.9 84 40-160 Carbon disulfide ug/L 50 51.9J 104 50-160 Carbon tetrachloride ug/L 50 46.3 93 69-131 Chlorobenzene ug/L 50 45.8 92 81-122 Chloroethane ug/L 50 46.6 93 39-148 Chloroform ug/L 50 43.9 88 73-127 Chloromethane ug/L 50 41.5 83 44-146 Chloroprene ug/L 50 45.9 92 75-145 cis-1,2-Dichloroethene ug/L 50 46.2 92 74-124 cis-1,3-Dichloropropene ug/L 50 50.8 102 72-132 Dibromochloromethane ug/L 50 49.8 100 78-125 Dibromomethane ug/L 50 44.9 90 82-120 Dichlorodifluoromethane ug/L 50 42.3 85 34-157 Ethyl methacrylate ug/L 50 44.6 89 82-121 Ethylbenzene ug/L 50 45.3 91 79-121 Hexachloro-1,3-butadiene ug/L 50 47.9 96 72-131 lodomethane ug/L 100 98.1 98 39-154 Isobutanol ug/L 1000 1040 104 34-160 Methacrylonitrile ug/L 500 482 96 74-134 Methyl methacrylate ug/L 50 44.8 90 84-124 Methylene Chloride ug/L 50 45.8 92 64-133 Naphthalene ug/L 50 50.6 101 73-133 Propionitrile ug/L 500 462 92 73-140 Styrene ug/L 50 46.5 93 84-126 Tetrachloroethene ug/L 50 49.0 98 78-122 Toluene ug/L 50 45.0 90 80-121 trans-1,2-Dichloroethene ug/L 50 43.1 86 71-127 trans- 1,3-Dichloropropene ug/L 50 49.1 98 69-141 trans-1,4-Dichloro-2-butene ug/L 50 49.3J 99 40-160 Trichloroethene ug/L 50 48.2 96 78-122 Trichlorofluoromethane ug/L 50 45.0 90 53-137 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BLANKS Pace Project No.: 92367285 LABORATORY CONTROL SAMPLE: 2172869 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Vinyl acetate ug/L 100 92.3 92 40-160 Vinyl chloride ug/L 50 46.2 92 58-137 Xylene (Total) ug/L 150 143 96 81-126 1,2-Dichloroethane-d4 (S) % 98 70-130 4-Bromofluorobenzene (S) % 97 70-130 Toluene-d8 (S) % 96 70-130 MATRIX SPIKE SAMPLE: 2172883 92367284009 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 19.3 97 70-130 1,1,1-Trichloroethane ug/L ND 20 20.8 104 70-130 1,1,2,2-Tetrachloroethane ug/L ND 20 19.2 96 70-130 1,1,2-Trichloroethane ug/L ND 20 26.2 131 70-130 M1 1,1-Dichloroethane ug/L ND 20 20.1 100 70-130 1,1-Dichloroethene ug/L ND 20 25.3 126 70-166 1,1-Dichloropropene ug/L ND 20 19.1 96 70-130 1,2,3-Trichloropropane ug/L ND 20 19.4 97 70-130 1,2,4-Trichlorobenzene ug/L ND 20 21.3 107 70-130 1,2-Dibromo-3-chloropropane ug/L ND 20 18.5 93 70-130 1,2-Dibromoethane (EDB) ug/L ND 20 21.3 107 70-130 1,2-Dichlorobenzene ug/L ND 20 20.6 103 70-130 1,2-Dichloroethane ug/L ND 20 19.2 96 70-130 1,2-Dichloropropane ug/L ND 20 20.3 102 70-130 1,3-Dichlorobenzene ug/L ND 20 21.2 106 70-130 1,3-Dichloropropane ug/L ND 20 22.2 111 70-130 1,4-Dichlorobenzene ug/L ND 20 21.0 105 70-130 2,2-Dichloropropane ug/L ND 20 20.7 104 70-130 2-Butanone (MEK) ug/L ND 40 37.9J 95 70-130 2-Hexanone ug/L ND 40 37.8J 94 70-130 4-Methyl-2-pentanone (MIBK) ug/L ND 40 45.5J 114 70-130 Acetone ug/L ND 40 37.1J 93 70-130 Acetonitrile ug/L ND 200 179 90 70-130 Acrolein ug/L ND 100 102 102 70-130 Acrylonitrile ug/L ND 100 91AJ 91 70-130 Allyl chloride ug/L ND 20 18.6 93 70-130 Benzene ug/L ND 20 20.2 101 70-148 Bromochloromethane ug/L ND 20 20.1 101 70-130 Bromodichloromethane ug/L ND 20 19.9 100 70-130 Bromoform ug/L ND 20 18.1 90 70-130 Bromomethane ug/L ND 20 14.9 75 70-130 Carbon disulfide ug/L ND 20 24AJ 122 70-130 Carbon tetrachloride ug/L ND 20 21.2 106 70-130 Chlorobenzene ug/L ND 20 21.0 105 70-146 Chloroethane ug/L ND 20 26.1 131 70-130 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SURRY BLANKS Pace Project No.: 92367285 MATRIX SPIKE SAMPLE: Parameter 2172883 Units 92367284009 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers Chloroform ug/L ND 20 18.9 95 70-130 Chloromethane ug/L ND 20 14.9 75 70-130 Chloroprene ug/L ND 20 21.4 107 70-130 cis-1,2-Dichloroethene ug/L ND 20 20.7 104 70-130 cis-1,3-Dichloropropene ug/L ND 20 20.9 105 70-130 Dibromochloromethane ug/L ND 20 19.2 96 70-130 Dibromomethane ug/L ND 20 19.8 99 70-130 Dichlorodifluoromethane ug/L ND 20 19.8 99 70-130 Ethyl methacrylate ug/L ND 20 20.2 101 70-130 Ethylbenzene ug/L ND 20 21.2 106 70-130 Hexachloro-1,3-butadiene ug/L ND 20 19.6 98 70-130 lodomethane ug/L ND 40 32.7 82 70-130 Isobutanol ug/L ND 400 289 72 70-130 Methacrylonitrile ug/L ND 200 192 96 70-130 Methyl methacrylate ug/L ND 20 18.9J 94 70-130 Methylene Chloride ug/L ND 20 19.4 97 70-130 Naphthalene ug/L ND 20 21.6 108 70-130 Propionitrile ug/L ND 200 187 93 70-130 Styrene ug/L ND 20 20.8 104 70-130 Tetrachloroethene ug/L ND 20 20.9 104 70-130 Toluene ug/L ND 20 19.8 99 70-155 trans-1,2-Dichloroethene ug/L ND 20 20.5 103 70-130 trans- 1,3-Dichloropropene ug/L ND 20 25.2 126 70-130 trans-1,4-Dichloro-2-butene ug/L ND 20 15.9J 80 70-130 Trichloroethene ug/L ND 20 20.9 104 69-151 Trichlorofluoromethane ug/L ND 20 23.0 115 70-130 Vinyl acetate ug/L ND 40 36.1J 90 70-130 Vinyl chloride ug/L ND 20 20.5 102 70-130 1,2-Dichloroethane-d4 (S) % 99 70-130 4-Bromofluorobenzene (S) % 101 70-130 Toluene-d8 (S) % 96 70-130 SAMPLE DUPLICATE: 2172882 92367284008 Dup Max Parameter Units Result Result RPD RPD Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND ND 30 1,1,1-Trichloroethane ug/L ND ND 30 1,1,2,2-Tetrachloroethane ug/L ND ND 30 1,1,2-Trichloroethane ug/L ND ND 30 1,1-Dichloroethane ug/L ND ND 30 1,1-Dichloroethene ug/L ND ND 30 1,1-Dichloropropene ug/L ND ND 30 1,2,3-Trichloropropane ug/L ND ND 30 1,2,4-Trichlorobenzene ug/L ND ND 30 1,2-Dibromo-3-chloropropane ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 24 Pace Analytical Services, LLC aceAnalXical� 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: SURRY BLANKS Pace Project No.: 92367285 SAMPLE DUPLICATE: 2172882 Parameter Units 92367284008 Result Dup Result RPD Max RPD Qualifiers 1,2-Dibromoethane (EDB) ug/L ND ND 30 1,2-Dichlorobenzene ug/L ND ND 30 1,2-Dichloroethane ug/L ND ND 30 1,2-Dichloropropane ug/L ND ND 30 1,3-Dichlorobenzene ug/L ND ND 30 1,3-Dichloropropane ug/L ND ND 30 1,4-Dichlorobenzene ug/L ND ND 30 2,2-Dichloropropane ug/L ND ND 30 2-Butanone (MEK) ug/L ND ND 30 2-Hexanone ug/L ND ND 30 4-Methyl-2-pentanone (MIBK) ug/L ND ND 30 Acetone ug/L ND ND 30 Acetonitrile ug/L ND ND 30 Acrolein ug/L ND ND 30 Acrylonitrile ug/L ND ND 30 Allyl chloride ug/L ND ND 30 Benzene ug/L ND ND 30 Bromochloromethane ug/L ND ND 30 Bromodichloromethane ug/L ND ND 30 Bromoform ug/L ND ND 30 Bromomethane ug/L ND ND 30 Carbon disulfide ug/L ND ND 30 Carbon tetrachloride ug/L ND ND 30 Chlorobenzene ug/L ND ND 30 Chloroethane ug/L ND ND 30 Chloroform ug/L ND ND 30 Chloromethane ug/L ND ND 30 Chloroprene ug/L ND ND 30 cis-1,2-Dichloroethene ug/L ND ND 30 cis-1,3-Dichloropropene ug/L ND ND 30 Dibromochloromethane ug/L ND ND 30 Dibromomethane ug/L ND ND 30 Dichlorodifluoromethane ug/L ND ND 30 Ethyl methacrylate ug/L ND ND 30 Ethylbenzene ug/L ND ND 30 Hexachloro-1,3-butadiene ug/L ND ND 30 lodomethane ug/L ND ND 30 Isobutanol ug/L ND ND 30 Methacrylonitrile ug/L ND ND 30 Methyl methacrylate ug/L ND ND 30 Methylene Chloride ug/L ND ND 30 Naphthalene ug/L ND ND 30 Propionitrile ug/L ND ND 30 Styrene ug/L ND ND 30 Tetrachloroethene ug/L ND ND 30 Toluene ug/L ND ND 30 trans-1,2-Dichloroethene ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SURRY BLANKS Pace Project No.: 92367285 SAMPLE DUPLICATE: 2172882 Parameter trans- 1,3-Dichloropropene trans-1,4-Dichloro-2-butene Trichloroethene Trichlorofluoromethane Vinyl acetate Vinyl chloride Xylene (Total) 1,2-Dichloroethane-d4 (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) QUALITY CONTROL DATA Units 92367284008 Result Dup Result ug/L ND ND ug/L ND ND ug/L ND ND ug/L ND 0.20J ug/L ND ND ug/L ND ND ug/L ND ND 93 94 % 95 97 126 110 IVV 1 2 13 Max RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: SURRY BLANKS Pace Project No.: 92367285 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte PASI-M Pace Analytical Services - Minneapolis ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /09/2018 05:59 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: SURRY BLANKS Pace Project No.: 92367285 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92367285001 EB EPA 3010A 391699 EPA 6010 391785 92367285001 EB EPA 3020 517023 EPA 6020B 517131 92367285001 EB EPA 7470 391836 EPA 7470 391889 92367285001 EB EPA 8260 391641 92367285002 FB EPA 8260 391641 Date: 01/09/2018 05:59 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 21 of 24 Document Name: Document Revised: August 4, 2017 Sample Condition Upon Receipt(SOUR) Page 1 of 2 Document NO.: Issuing Authority: r c?CE/�Rc�><ICdj F-CAR-CS-033-Rev.04 Pace Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Client Name: Courier:Fed ❑ P " Commercial ce Custody Seal Present? ❑Yes Huntersville.L�----I Raleigh❑ Mechanicsville❑ WO:92367285 Project I#: ]Client/ 92367285 �1 0 II —y Date/Initlals Person Examining Contents: 2+ t5' (/ Packing Material: ❑Bubble Wrap �bble Bags ❑None ❑ Other Biological Tissue Frozen? / Thermometer; ❑Yes ❑No ,❑#{� R 6un 1D:�OolerTernp et ❑Blue ❑NoneT pe of Ice:Correction Factor; Corrected (°C): J�j — 2 , C' — Temp should be above freezing to 6"C ❑5amples out of temp criteria. Samples on ice, cooling process has begun USDA Regulated Soi) N/A, water sample) Did samples on ' In a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (i ❑Yes No including Hawaii and Puerto Rico)? ❑Yes No Comments/Discreoancv: Chain of Custody Present? Samples Arrived within Hold Time? Short Hold Time Analysis (02 hr.)? Rush Turn Around Time Requested? Sufficient Volume? Correct Containers Used? -Pace Containers Used? Containers Intact? Dissolved analysis: Samples Field Filtered? Sample Labels Match CDC? -Includes Date/Time/ID/Analys Headspace in VOA Vials (>5-6mm' Trip Blank Present? Trip Blank Custody Seals Present? CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Sample Discrepancy: Lot ID of split containers: s Matrix: Seals Intact? ❑Yes No QY9' [IN. ❑N/A F-1*rs' I71No nNJA ❑Yes ❑N/A L,.JYes ❑N/A ❑Yes QV-0 []N/A 1. 2. 3. 4. S. 6, Date/Time: 6'U v— Field Data Required? ❑Yes [—]No Project Manager SCURF Review: --C-c Date: _ (Z/I `(/(7 Project Manager SRF Review: —cc Date: 12 ) I �f y Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e - Out of hold, incorrect preservative, out of temp, incorrect containers) Page 22 of 24 3 a m 0 a m m i C O 7 A T. X n Q. C v m vt m .-r � 3 r+ d r o O w Oa C 1 m a � � LON 3 t0 a � Ln M w c P � 7 N a 3 n 3 a ci a v 10 m a m a M 0 x zzzzzzzzz zz BP4U-125 mL Plastic Unpreserved (N/A) (CI-) n OP3U-250 mL Plastic Unpreserved (N/A) o 01 '"! CL 0 3• w SP2U-SOO mL Plastic Unpreserved(N/A) „ t L CU 3. a 9P1U-1 liter Plastic Unpreserved {N/A) Cr v "• S iv q x 0 --h H BP45-125 mL Plastic H2504 (pH <2) (CI-) T • F 0 BP3N-25D mL plastic HNO3 (pH < 2) 0 Cr n O x OP42-125 mL Plastic 2N Acetate & NaOH 1>9) ,;, r, C HP4C-125 mL Plastic NaOH (pH > 12) (Cl-)CL 3 [� WGPU-Wide-mouthed Glass jar Unpreserved 1 O� q 1 AG1U-1 liter Amber Unpreserved (NIA) (Cl.) Cr a w y, r0 S Z,XZ77zzzzz AG1H-1 liter Amber HCI (pH < 21 � 4A O :3. AG3U-250 mL Amber Unpreserved (N/A) (Cl-) ,O1r O AG15-1. liter Amber H2504 (pH < 2) AG35-150 ml Amber H2504 (pH < 2) AG3A(DG3A)-25D MLAmber NH4Cl (N/A)(CI-) D69H-00 mL VOA HC1 IN/A) O VG9T-40 mL VOA Na2S203 (NIA) n VG9L1-10 mL VOA Unp (N/A) r DG9P-40 mL VOA H3PO4 (N/A) r 3 M •• m O VOAK (5 vials per kit)•5035 kit (N/A1 V/GK (3 vials per kit)-VPH/Gas kit (N/A) • • SPST-125 mL Sterile Plastic (N/A —lab) SPZT-250 mL Sterile Plastic IN/A — lab) C M• d O N W �-• t 13 0 d BP3A-250 ml. Plastic (NH2)2504 (9.3-9.7) a A l0 Cuhitainer O VSGU-20 mL Scin[iiiation vials [N/A) ` ] O N GN �I.d Go A A ceAna!}dical Section A Required Client Information: Company Municipal Eng, Address P.O. Box 97 Garner, NC 27529 Email To: ipfohl a'7mesco Phoney 919-772-5393 Requesled Due DalerTAT: 10 CHAIN -OF -CUSTODY / Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. IL Section B Section C Required Project Information: Invoice Information: Page : 1 Of I Services Report To: Jonathan Pfohl Allenlion. Municipal Engineering Services Copy To� Company Name: Address. 1'� Regulatory Agency Purchase Order No. (�; h i Pace Quote Reference: Clienl Project SD'. s) Pace Project Manager. Trey Carter State 1 Location :fault) container Order Number: Pace ProNe #: 21 D3-3 North Carolina COLLECTED Preservatives I! NJ N MATRIX CODE a U-k..gwaa.r Dw — o 0 W.1e, wT SAMPLE ID was,ewwl. ww O Z s p,od„d P START END One Character per Lox. S.WS6,d St0. CL tA-Z, 0-9 1, -) wi a wp Ja w Sample Ids must be unique AnP AR r a F r olh., OT T-- TS o O a Q. w m to N 5 up�DATE r Z Z nr ]Yr TIME DATE TIME h � 2_ If � inrr r_ .Si6s L'•a� '? - � 10 11 12 ADDITIONAL COMMENTS BY I AFFILIATION DATE I TIME 112 ACCEPTED BYr tI91W5 DATE I TIME I SAMPLE CONDITIONS SAMPLER NAME AND SIGNATURE v l m PRINT Name of SAMPLER: � � ? JOnatFfein,Pfohl SIGNATURE of SAMPLER: DATE Signed: i � l 1, { w n", m tr p °o m = 1 'j f i— D' !� U U VJ } Appendix B Field Sampling Parameter Data Sheet(s) Muniapal L/ IJLI I� i'-oP�ar, 'uS Project: Surry Co Closed C&D and Closed MSWLF-Mt. Airy Samplers: J. Pfohl Page_1_of 1 Sampling Parameters Water Quality Parameters (Stabilized) Monitoring Point Sample Date 'tz Sample Time Depth to Water (BTOP) Static Lab Parameters to be analyzed for Volume Purged (Gal) Sample Type Goes Dry During Purge Total Depth Measured as expected Total Depth Expected CO2 (mg") DO (mg/L) ORP pH Temp. © Specific Cond. (us/cm TDS (mg/L) :.5 Z 3 ~ CH4 Gas Vapors MW-1 I.� 0', UIC, �i �p� 40 -`'I T 3 IW-2''f, WLR & T - - - 68.08 - - - - - - - MW-3R 1 ,' ;+ 1-11C Pit, L oP 100 IW-3 0 WLR & T - - - 52 IW-4„a, WLR&T - - - 57 - - - - - - - IW-5 WLR & T - - - tea 64 MW-6 z ... AM x 31 - Cad �a is �11 MW-7 ?�°; UIC . 25 - IR IW-6 t` WLR & T - - - 56 - - - - - - - >I;dC-0 MW-9 mo UIC 1" I,I 46 -�, i MW-11 ',. i AM " tv.l 40 - t'Z ! i 4y A l MW-12D `11 E6+, _ AM 127 1hF 100 - J'7 �P+ g,` 0 Ga 1m MW-12S ', UIC { i4 51 -,1 I'f MW-13 .k UIC 35.78 MW-14 °, L) l UIC I + , 48.03 ri MW-15 ,tt 5 3'i UIC ; 56.98 a 1° t. ` v 7- MW-16 UIC 36.28 MW-17 UIC Df 15.32 - ; , i sfi <' C. MW-18 UIC r• 18.15i�'u MW-19 ; UIC a'+ 17.1 MW-20 UIC 25.64,. MW-21 UIC i �£ 15.41 MW-22 , _. UIC 16.04 - 3, i [fit MW-23 UIC a,,y 17.1 _ �, I 17 - SCALEHOURtip I AM � - `� 222 - t, JJ D=JtaIf11e55 Jleel Diller, a D=Ulbpo5dUle Diller, r=Low lluw rump, ru=rulyeu Uly VT=Very Turbid, MT=Moderately Turbid, ST=Slightly Turbid, C=Clear NR=No Reading Attempted, NS=No Sample Obtained (> 114 4 4